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Sample records for mas technique monitoramento

  1. Two-Stage MAS Technique for Analysis of DRA Elements and Arrays on Finite Ground Planes

    DEFF Research Database (Denmark)

    Larsen, Niels Vesterdal; Breinbjerg, Olav

    2007-01-01

    A two-stage Method of Auxiliary Sources (MAS) technique is proposed for analysis of dielectric resonator antenna (DRA) elements and arrays on finite ground planes (FGPs). The problem is solved by first analysing the DRA on an infinite ground plane (IGP) and then using this solution to model the FGP...

  2. SISTEMA DE MONITORAMENTO AUTOMATIZADO

    Directory of Open Access Journals (Sweden)

    Raiane viana Souza

    2016-11-01

    Full Text Available Atualmente existe uma grande necessidade de ter sistemas que auxiliem no monitoramento de ambientes, por exemplo: uma residência; permitindo assim que o usuário possa controlar e ter acesso a tudo que acontece quando o mesmo estiver ausente. Este projeto propõe realizar o desenvolvimento de um sistema de monitoramento automatizado, cujo objetivo é identificar a presença de pessoas e capturar temperaturas de um ambiente. O sistema é composto por um microcontrolador Arduíno, no qual estará acoplado: uma Webcam, sensores de presença e temperatura e um módulo wifi, que possibilitará o envio dos dados capturados ao servidor web. No protótipo desenvolvido foram implantados todos os recursos definidos com base nos requisitos do usuário, dentre os quais podem-se destacar: permitir detectar a presença de pessoas em ambiente, capturar imagens, capturar temperatura em um intervalo de tempo específico e enviar todos os dados para o servidor; permitir que o usuário visualize as informações capturadas através de um site; gerar relatórios e gráficos com as informações capturadas e permitir que o usuário exporte as informações em formato de arquivo.

  3. 1H MAS NMR (magic-angle spinning nuclear magnetic resonance) techniques for the quantitative determination of hydrogen types in solid catalysts and supports.

    Science.gov (United States)

    Kennedy, Gordon J; Afeworki, Mobae; Calabro, David C; Chase, Clarence E; Smiley, Randolph J

    2004-06-01

    Distinct hydrogen species are present in important inorganic solids such as zeolites, silicoaluminophosphates (SAPOs), mesoporous materials, amorphous silicas, and aluminas. These H species include hydrogens associated with acidic sites such as Al(OH)Si, non-framework aluminum sites, silanols, and surface functionalities. Direct and quantitative methodology to identify, measure, and monitor these hydrogen species are key to monitoring catalyst activity, optimizing synthesis conditions, tracking post-synthesis structural modifications, and in the preparation of novel catalytic materials. Many workers have developed several techniques to address these issues, including 1H MAS NMR (magic-angle spinning nuclear magnetic resonance). 1H MAS NMR offers many potential advantages over other techniques, but care is needed in recognizing experimental limitations and developing sample handling and NMR methodology to obtain quantitatively reliable data. A simplified approach is described that permits vacuum dehydration of multiple samples simultaneously and directly in the MAS rotor without the need for epoxy, flame sealing, or extensive glovebox use. We have found that careful optimization of important NMR conditions, such as magnetic field homogeneity and magic angle setting are necessary to acquire quantitative, high-resolution spectra that accurately measure the concentrations of the different hydrogen species present. Details of this 1H MAS NMR methodology with representative applications to zeolites, SAPOs, M41S, and silicas as a function of synthesis conditions and post-synthesis treatments (i.e., steaming, thermal dehydroxylation, and functionalization) are presented.

  4. Les schémas de sélection ovins laitiers en France : utilisation et importance des techniques modernes de reproduction

    OpenAIRE

    Astruc, J.M.; Lagriffoul, G.; Belloc, J.P.; Briois, M.; Cachenaut, J.B.; Horent, M.H.; Teinturier, M.H.

    1995-01-01

    La mise en oeuvre de programmes de sélection laitière, à l’échelle de toute une population ovine, suppose de développer un travail de sélection entre éleveurs, fondé sur l’organisation et la valorisation de liens génétiques entre troupeaux, essentiellement grâce à l’utilisation de l’IA. La situation en France est à cet égard révélatrice des différents niveaux d’organisation des schémas de sélection.

  5. CACTI: MONITORAMENTO PREDITIVO DE ATIVOS DE REDE

    Directory of Open Access Journals (Sweden)

    Gian Sávio Morais

    2016-11-01

    Full Text Available Este trabalho trata da adoção da ferramenta de monitoramento de ativos de rede Cacti na rede de computadores de uma empresa localizada em Santa Rita do Sapucaí – MG, onde foram detectados problemas de interrupção em serviços classificados como críticos para o contínuo andamento das demais atividades da empresa. O objetivo da ferramenta é monitorar preditivamente esses dispositivos em missão crítica a fim de reduzir as possíveis falhas que possam vir a ocorrer, facilitando a detecção de mal funcionamento e viabilizando ações preventivas e corretivas. O Cacti coleta, armazena e apresenta informações sobre o funcionamento dos dispositivos através de gráficos, se comunicando com os ativos na rede através do protocolo SNMP. Com essa solução, é possível modificar a ferramenta de modo a se adequar ao cenário à ser implantado, permitindo melhores resultados. O foco dos resultados é reduzir consideravelmente as ações corretivas e manter maior disponibilidade nos serviços críticos da empresa.

  6. E/Z MAS demonstration

    International Nuclear Information System (INIS)

    Boor, M.G.; Hurford, J.M.; Landry, R.P.; Martinez, B.J.; Solem, A.M.; Whiteson, R.; Zardecki, A.

    1998-01-01

    Los Alamos National Laboratory has developed E/Z MAS, a new generation nuclear material accountability application based on the latest technology and designed for facilities required to track nuclear materials with a simple-to-use interface. E/Z MAS is based on years of experience spent developing nuclear material accounting systems. E/Z MAS uses a modern relational database with a web server and enables users on a classified local area network to interact with the database with web browsers. The E/Z MAS Demonstration poster session demonstrates the E/Z MAS functions required by an operational nuclear facility to track material as it enters and leaves a facility and to account for the material as it moves through a process. The generation of internal facility reports and external reports for the Russian Federal system will be demonstrated. Bar-code readers will be used to demonstrate the ability of EZ MAS to automate certain functions, such as physical inventories at facilities

  7. Monitoramento auditivo na ototoxidade Auditory monitoring in ototoxicity

    Directory of Open Access Journals (Sweden)

    Lilian Cassia Bornia Jacob

    2006-12-01

    Full Text Available Algumas drogas, denominadas ototóxicas, têm a capacidade de lesar os sistemas auditivo e vestibular. O avanço tecnológico tem disponibilizado inúmeros recursos para realizar o monitoramento da audição, porém, apesar da disponibilização de protocolos de avaliação internacionais, existem controvérsias quanto à escolha do procedimento de maior sensibilidade e especificidade para este fim. OBJETIVO: Analisar os procedimentos audiológicos utilizados no monitoramento auditivo dos indivíduos expostos à medicação ototóxica. METODOLOGIA: Realizou-se busca eletrônica nas bases de dados MEDLINE e LILACS, a partir da combinação entre os descritores que caracterizaram as temáticas monitoramento auditivo, ototoxicidade e câncer. A literatura apontou dois principais procedimentos efetivos no monitoramento: a audiometria de altas freqüências e as emissões otoacústicas. Ambos permitem que a alteração no sistema auditivo seja identificada antes que haja um comprometimento dos limiares tonais na faixa de freqüências convencional, e conseqüentemente na habilidade de compreensão da fala. CONCLUSÃO: O protocolo de monitoramento auditivo foi sugerido considerando a capacidade do paciente em responder aos testes comportamentais e a etapa do monitoramento (primeira avaliação ou subseqüentes. No caso de portadores de câncer, o monitoramento auditivo deve ser disponibilizado no local de tratamento do indivíduo.Some pharmaceutical products are capable of damaging the human auditory system. Technological progress has provided numerous resources to monitor hearing but there still is some controversy regarding the selection of the most sensitive and specific tests. OBJECTIVE: to analyze audiological procedures used in the auditory monitoring of individuals exposed to ototoxic medication. METHODS: we searched the MEDLINE and LILACS literature databases, using terms pertinent to audiological monitoring, ototoxicity and cancer. The

  8. Quartz Crystal Temperature Sensor for MAS NMR

    Science.gov (United States)

    Simon, Gerald

    1997-10-01

    Quartz crystal temperature sensors (QCTS) were tested for the first time as wireless thermometers in NMR MAS rotors utilizing the NMR RF technique itself for exiting and receiving electro-mechanical quartz resonances. This new tool in MAS NMR has a high sensitivity, linearity, and precision. When compared to the frequently used calibration of the variable temperature in the NMR system by a solid state NMR chemical shift thermometer (CST), such as lead nitrate, QCTS shows a number of advantages. It is an inert thermometer in close contact with solid samples operating parallel to the NMR experiment. QCTS can be manufactured for any frequency to be near a NMR frequency of interest (typically 1 to 2 MHz below or above). Due to the strong response of the crystal, signal detection is possible without changing the tuning of the MAS probe. The NMR signal is not influenced due to the relative sharp crystal resonance, restricted excitation by finite pulses, high probeQvalues, and commonly used audio filters. The quadratic dependence of the temperature increase on spinning speed is the same for the QCTS and for the CST lead nitrate and is discussed in terms of frictional heat in accordance with the literature about lead nitrate and with the results of a simple rotor speed jump experiment with differently radial located lead nitrate in the rotor.

  9. Monitoramento e incentivos em redes de franquias brasileiras

    OpenAIRE

    Bianca Maria da Silva

    2015-01-01

    Redes de franquia constituem um tipo de arranjo híbrido de governança onde, normalmente, lojas próprias e franqueadas operam sob uma mesma marca e formato de negócios. Considerando que taxas de franquia (fixas e variáveis) estão entres as principais fontes de receita do franqueador senão a principal, este trabalho tem por objetivo identificar evidências quanto a fixação destas taxas por redes de franquia. A variação de tais taxas é comparada à capacidade de monitoramento das redes, consideran...

  10. High Tech M&As

    DEFF Research Database (Denmark)

    Toppenberg, Gustav

    2013-01-01

    Technology driven industries have seen fast moving technology changes, higher complexity and reduced product life cycles. These emerging trends present challenges for companies in industries where technology is at the forefront. The extant research deals with ‘low-tech’ industries and majority...... of findings are not applicable to the high-tech industry; in fact this industry has many additional challenges. In this study, we aim to explore the process of M&A in the high-tech industry by drawing on extant literature and empirical field work. The paper outlines a research project in progress which...... intends to provide theoretical, empirical and practical contributions in answering the research question: what role does Operations and IT play in creating value in high-tech M&As? The research adds a needed perspective on M&A literature by unveiling unique challenges and opportunities faced by the M...

  11. Invasive Hemodynamic Monitoring in Small Animals/ Monitoramento Hemodinâmico Invasivo em Pequenos Animais

    Directory of Open Access Journals (Sweden)

    Paulo Sérgio Patto dos Santos

    2002-05-01

    Full Text Available The aim of this paper was to revise the several homodynamic variables that can be monitored by invasive techniques, direct or indirectly, such as arterial pressure, central venous pressure, cardiac output, systemic vascular resistance, among others. Such techniques offer more accuracy and reliability, and also allow a continuous monitoring, being of great importance and utility in the treatment of the critically ill patient. As they are invasive techniques, they aren’t free of risks and the professional must decide for their utilization analysing the advantages and disadvantages.Com este artigo objetivou-se revisar os diversos parâmetros hemodinâmicos que podem ser monitorados de maneira invasiva, direta ou indiretamente, como a pressão arterial, pressão venosa central, débito cardíaco, resistência vascular periférica, entre outros. Tais técnicas oferecem uma maior confiabilidade e precisão, além de permitirem um monitoramento contínuo, sendo de grande importância e utilidade no tratamento de pacientes em estado crítico. Por serem técnicas invasivas, não são isentas de risco, cabendo ao profissional, face as vantagens e desvantagens inerentes a cada uma, bem como ao estado clínico do paciente, optar ou não pela sua utilização.

  12. Fluid flow dynamics in MAS systems

    Science.gov (United States)

    Wilhelm, Dirk; Purea, Armin; Engelke, Frank

    2015-08-01

    The turbine system and the radial bearing of a high performance magic angle spinning (MAS) probe with 1.3 mm-rotor diameter has been analyzed for spinning rates up to 67 kHz. We focused mainly on the fluid flow properties of the MAS system. Therefore, computational fluid dynamics (CFD) simulations and fluid measurements of the turbine and the radial bearings have been performed. CFD simulation and measurement results of the 1.3 mm-MAS rotor system show relatively low efficiency (about 25%) compared to standard turbo machines outside the realm of MAS. However, in particular, MAS turbines are mainly optimized for speed and stability instead of efficiency. We have compared MAS systems for rotor diameter of 1.3-7 mm converted to dimensionless values with classical turbomachinery systems showing that the operation parameters (rotor diameter, inlet mass flow, spinning rate) are in the favorable range. This dimensionless analysis also supports radial turbines for low speed MAS probes and diagonal turbines for high speed MAS probes. Consequently, a change from Pelton type MAS turbines to diagonal turbines might be worth considering for high speed applications. CFD simulations of the radial bearings have been compared with basic theoretical values proposing considerably smaller frictional loss values. The discrepancies might be due to the simple linear flow profile employed for the theoretical model. Frictional losses generated inside the radial bearings result in undesired heat-up of the rotor. The rotor surface temperature distribution computed by CFD simulations show a large temperature gradient over the rotor.

  13. Hierarchical MAS based control strategy for microgrid

    Energy Technology Data Exchange (ETDEWEB)

    Xiao, Z.; Li, T.; Huang, M.; Shi, J.; Yang, J.; Yu, J. [School of Information Science and Engineering, Yunnan University, Kunming 650091 (China); Xiao, Z. [School of Electrical and Electronic Engineering, Nanyang Technological University, Western Catchment Area, 639798 (Singapore); Wu, W. [Communication Branch of Yunnan Power Grid Corporation, Kunming, Yunnan 650217 (China)

    2010-09-15

    Microgrids have become a hot topic driven by the dual pressures of environmental protection concerns and the energy crisis. In this paper, a challenge for the distributed control of a modern electric grid incorporating clusters of residential microgrids is elaborated and a hierarchical multi-agent system (MAS) is proposed as a solution. The issues of how to realize the hierarchical MAS and how to improve coordination and control strategies are discussed. Based on MATLAB and ZEUS platforms, bilateral switching between grid-connected mode and island mode is performed under control of the proposed MAS to enhance and support its effectiveness. (authors)

  14. MAS NMR of HIV-1 protein assemblies

    Science.gov (United States)

    Suiter, Christopher L.; Quinn, Caitlin M.; Lu, Manman; Hou, Guangjin; Zhang, Huilan; Polenova, Tatyana

    2015-04-01

    The negative global impact of the AIDS pandemic is well known. In this perspective article, the utility of magic angle spinning (MAS) NMR spectroscopy to answer pressing questions related to the structure and dynamics of HIV-1 protein assemblies is examined. In recent years, MAS NMR has undergone major technological developments enabling studies of large viral assemblies. We discuss some of these evolving methods and technologies and provide a perspective on the current state of MAS NMR as applied to the investigations into structure and dynamics of HIV-1 assemblies of CA capsid protein and of Gag maturation intermediates.

  15. PROPAGANDA POLITIK PARTAI GERINDRA DALAM GAME MAS GARUDA PADA PEMILU 2014 (Analisis Deskriptif Game Online Mas Garuda

    Directory of Open Access Journals (Sweden)

    Angga Satrya Putra

    2016-03-01

    Full Text Available The purpose of this study was to determine how the meaning of the look and content of the online game “Garuda Mas”. This game contains aspects of politically charged designations so that it can become a propaganda technique. The subject of this study is the game “Garuda Mas” which has been input on social media Facebook.Methods of data collection using documentary and literature. Data analysis using descriptive techniques. Data validity checking techniques using triangulation source.The results showed that the game “MAS GARUDA” can form the perspective of the players against Mas Garuda as a superhero figure hopes the Indonesian people who are able to overcome all the problems that exist in Indonesia. This game is a form of creative campaigns using propaganda techniques inserted in the game that has the power to change the mindset of every player. Change of mindset occurs because the player did not have an opportunity to think critically on aspects marking contained in the game. By indirectly the players will feel the emotional of this game and assume characterizations “Garuda Mas” in this game is a truth that can be believed.Keywords: Descriptive, Online Games, Mas Garuda, Partai Gerindra

  16. UAV Robust Strategy Control Based on MAS

    Directory of Open Access Journals (Sweden)

    Jian Han

    2014-01-01

    Full Text Available A novel multiagent system (MAS has been proposed to integrate individual UAV (unmanned aerial vehicle to form a UAV team which can accomplish complex missions with better efficiency and effect. The MAS based UAV team control is more able to conquer dynamic situations and enhance the performance of any single UAV. In this paper, the MAS proposed and established combines the reacting and thinking abilities to be an initiative and autonomous hybrid system which can solve missions involving coordinated flight and cooperative operation. The MAS uses BDI model to support its logical perception and to classify the different missions; then the missions will be allocated by utilizing auction mechanism after analyzing dynamic parameters. Prim potential algorithm, particle swarm algorithm, and reallocation mechanism are proposed to realize the rational decomposing and optimal allocation in order to reach the maximum profit. After simulation, the MAS has been proved to be able to promote the success ratio and raise the robustness, while realizing feasibility of coordinated flight and optimality of cooperative mission.

  17. Perspective of MAS in Power System via a Fuzzy Framework

    Directory of Open Access Journals (Sweden)

    S. Razini

    2017-03-01

    Full Text Available Multi agent systems (MAS are popularly used in practice, however; a few studies have looked at MAS capabilities from the power engineering perspective. This paper presents the results of an investigation concerning the compatibility of MAS capabilities in different power engineering categories. Five MAS capabilities and seven power system categories are established. A framework for applying MAS in power engineering is developed. A fuzzy inference system is adopted to evaluate the paper proposed framework. Two approaches, namely simulation and real, are considered for different power categories. The paper shows that MAS capabilities are generally compatible with both approaches, although compatibility of MAS with real approach is more significant. The paper concludes that in the near future MAS is anticipated to be a key important tool in the development of intelligent systems and smart grids in power system. This paper contributes to thinking on perspective of MAS in power System.

  18. Monitoramento geodésico tridimensional em ensaios estruturais de madeira

    Directory of Open Access Journals (Sweden)

    Camila Zonta

    Full Text Available Uma parceria entre o Laboratório de Instrumentação Geodésica e o Laboratório de Tecnologia da Madeira, ambos da Universidade Federal do Paraná, possibilitou o desenvolvimento deste projeto. Optou-se em inserir métodos geodésicos, aplicáveis ao monitoramento de estruturas, em ensaios estruturais de madeira. Realizaram-se ensaios de flexão estática em painéis compensados de madeira, com uso de uma Máquina Universal de Ensaios, aplicando-se juntamente o monitoramento de deslocamentos de pontos de interesse através do método de irradiação tridimensional. Ao final do ensaio estrutural foram analisadas e comparadas as flechas de deslocamento (deformação na componente vertical dos corpos de prova obtidas pela máquina de ensaios e pelo monitoramento geodésico. Como também, observou-se o comportamento tridimensional dos corpos de prova no decorrer dos ensaios. Desta forma, testando técnicas e método geodésico como uma nova proposta de verificação de deslocamentos em ensaios estruturais de madeira. Estatisticamente comprovou-se que os valores dos deslocamentos centrais dos painéis - flechas máximas - obtidos pelo monitoramento geodésico foram iguais aos resultados da máquina universal de ensaios. Confirmando assim, que o método proposto e as técnicas geodésicas testadas, podem também, ser aplicadas em laboratório em ensaios estruturais de madeira.

  19. Sistema de monitoramento remoto online de sinais cardíacos via rede GPRS

    OpenAIRE

    Vargas, Ricardo Emanuel Vaz

    2008-01-01

    Doenças cardiovasculares são consideradas atualmente a principal causa de morte e de lesões físicas limitantes e definitivas, que ocorrem em muitas das vezes em idade precoce. O exame de ECG é considerado, pelos especialistas, o padrão ouro para diagnóstico desse tipo de doença. Isso porque tal exame é barato, não-invasivo e fundamental para diagnóstico de diversas arritmias cardíacas. Portanto, o monitoramento de ECG pode significar a diferença entre o falecimento e a vida de muitos pa...

  20. Subsídios para o monitoramento de formigas cortadeiras em plantios florestais no Planalto Catarinense

    OpenAIRE

    Hoffer, Hadson

    2015-01-01

    O objetivo deste trabalho foi fornecer subsídios para o monitoramento de formigas cortadeiras em plantios florestais no Planalto Catarinense, conhecendo as espécies de formigas cortadeiras da região, sua associação com o tipo de solo e a distribuição espaço-temporal dos danos causados em Pinus taeda. Para isso foram percorridos plantios florestais em sete municípios do Planalto Catarinense na busca por ninhos de formigas cortadeiras. As coletas ocorreram em cinco diferentes tipos de solo com ...

  1. {sup 1}H HR-MAS NMR and S180 cells: metabolite assignment and evaluation of pulse sequence

    Energy Technology Data Exchange (ETDEWEB)

    Oliveira, Aline L. de; Martinelli, Bruno César B.; Lião, Luciano M. [Universidade Federal de Goiás (UFG), Goiânia, GO (Brazil). Instituto de Química. Lab. de RMN; Pereira, Flávia C.; Silveira-Lacerda, Elisangela P. [Universidade Federal de Goiás (UFG), Goiânia, GO (Brazil). Instituto de Ciências Biológicas. Laboratório Genética Molecular e Citogenética; Alcantara, Glaucia B., E-mail: glaucia.alcantara@ufms.br [Universidade Federal de Mato Grosso do Sul (UFMS), Campo Grande, MS (Brazil). Inst. de Química

    2014-07-01

    High resolution magic angle spinning {sup 1}H nuclear magnetic resonance spectroscopy (HR-MAS NMR) is a useful technique for evaluation of intact cells and tissues. However, optimal NMR parameters are crucial in obtaining reliable results. To identify the key steps for the optimization of HR-MAS NMR parameters, we assessed different pulse sequences and NMR parameters using sarcoma 180 (S180) cells. A complete assignment of the metabolites of S180 is given to assist future studies. (author)

  2. 1H HR-MAS NMR and S180 cells: metabolite assignment and evaluation of pulse sequence

    International Nuclear Information System (INIS)

    Oliveira, Aline L. de; Martinelli, Bruno César B.; Lião, Luciano M.; Pereira, Flávia C.; Silveira-Lacerda, Elisangela P.; Alcantara, Glaucia B.

    2014-01-01

    High resolution magic angle spinning 1 H nuclear magnetic resonance spectroscopy (HR-MAS NMR) is a useful technique for evaluation of intact cells and tissues. However, optimal NMR parameters are crucial in obtaining reliable results. To identify the key steps for the optimization of HR-MAS NMR parameters, we assessed different pulse sequences and NMR parameters using sarcoma 180 (S180) cells. A complete assignment of the metabolites of S180 is given to assist future studies. (author)

  3. O uso de medidas intelectuais na análise do monitoramento metacognitivo de crianças

    Directory of Open Access Journals (Sweden)

    Marília Zampieri

    Full Text Available O monitoramento metacognitivo é uma das habilidades compreendidas pela metacognição. É avaliado utilizando-se instrumentos de autorrelato ou pela formulação de julgamentos. O objetivo do presente estudo foi investigar o monitoramento metacognitivo de crianças durante a realização de três subtestes de uma bateria de inteligência, cujo referencial é o Modelo Cattell-Horn-Carroll. Os participantes responderam aos subtestes e foram solicitados a emitir estimativas sobre seu desempenho. Os resultados indicaram que a amostra já apresentava habilidades de monitoramento cognitivo e algumas medidas de monitoramento mostraram-se significativamente melhores para o subteste Desempenho em Matemática. Os dados são relevantes para confirmar, na população nacional, as informações da literatura internacional, e também para discutir a importância do incentivo e estímulo ao treinamento das habilidades metacognitivas.

  4. DAMPAK KEBIJAKAN PEMERINTAH TERHADAP KOMODITAS PISANG MAS KIRANA

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    Ariq Dewi Maharani

    2016-10-01

    Full Text Available ABSTRAKPenelitian ini bertujuan untuk menganalisis aspek profitabilitas pisang mas Kirana di Kabupaten Lumajang, dan menganalisis dampak kebijakan pemerintah terhadap pisang mas Kirana di Kabupaten Lumajang. Penentuan lokasi dilakukan secara sengaja (purposive method di Kabupaten Lumajang. Data yang digunakan meliputi data primer dan data sekunder. Analisa data menggunakan Policy Analysis Matrix (PAM untuk menganalisis aspek profitabilitas dan dampak kebijakan pemerintah terhadap pisang mas Kirana. Hasil penelitian menunjukkan bahwa Komoditas pisang mas Kirana menguntungkan secara finansial dan ekonomi yang ditunjukkan dengan keuntungan privat (PP Rp 10.444.911,8 per hektar dan keuntungan sosial (SP sebesar Rp 23.108.983,7 per hektar. Keuntungan privat pisang mas Kirana lebih kecil daripada keuntungan sosialnya (PPmas Kirana, terdapat dampak kebijakan subsidi terhadap harga-harga input pada usahatani pisang mas Kirana; masih belum ada lembaga yang dapat memberikan pelayanan yang kompetitif serta informasi yang lengkap dan rendahnya harga beli pisang mas Kirana di dalam negeri. ABSTRACTThe purpose of this research for: to analyse the aspect of profitability Kirana Mas banana and to analyse impact of government policy on Kirana Mas banana in Lumajang District. Determination of location was done intentionally or purposive method in Lumajang regency. The data that was used covering primary data and secondary data. Data analysis used Policy Analysis Matrix (PAM for knowing of profitability aspect and impact of government policy on Kirana Mas banana. The results showed that Commodity of Kirana Mas banana has financially and economically beneficial, shown by private profit (PP Rp 10,444,911.8 per hectare and social benefits (SP Rp 23,108,983.7 per hectare. Private profits of “Kirana mas” banana are smaller than social benefit (PP

  5. CAMEX-4 ER-2 MODIS AIRBORNE SIMULATOR (MAS) V1

    Data.gov (United States)

    National Aeronautics and Space Administration — The MODIS Airborne Simulator (MAS) is an airborne scanning spectrometer that acquires high spatial resolution imagery of cloud and surface features from its vantage...

  6. Chemical profile of beans cultivars (Phaseolus vulgaris) by 1H NMR - high resolution magic angle spinning (HR-MAS);Perfil quimico de cultivares de feijao (Phaseolus vulgaris) pela tecnica de high resolution magic angle spinning (HR-MAS)

    Energy Technology Data Exchange (ETDEWEB)

    Liao, Luciano Morais; Choze, Rafael; Cavalcante, Pedro Paulo Araujo; Santos, Suzana da Costa; Ferri, Pedro Henrique, E-mail: luciano@quimica.ufg.b [Universidade Federal de Goias (UFG), Goiania, GO (Brazil). Inst. de Quimica; Ferreira, Antonio Gilberto [Universidade Federal de Sao Carlos (UFScar), SP (Brazil). Dept. de Quimica

    2010-07-01

    The application of one-dimensional proton high-resolution magic angle spinning ({sup 1}H HR-MAS) NMR combined with a typical advantages of solid and liquid-state NMR techniques was used as input variables for the multivariate statistical analysis. In this paper, different cultivars of beans (Phaseolus vulgaris) developed and in development by EMBRAPA - Arroz e Feijao were analyzed by {sup 1}H HR-MAS, which have been demonstrated to be a valuable tool in its differentiation according chemical composition and avoid the manipulation of the samples as used in other techniques. (author)

  7. Sistema embarcado para monitoramento sem fio de sinais em soldagem a arco elétrico com abordagem tecnológica Embedded system for wireless signal monitoring during arc welding with technological approach

    Directory of Open Access Journals (Sweden)

    Marcus Vinícius Ribeiro Machado

    2012-06-01

    Full Text Available Industrialmente, o processo de soldagem a arco é o mais importante na produção e reparo de equipamentos, e sendo um processo especial de fabricação, que não pode ser completamente inspecionado contra imperfeições somente após sua finalização, o monitoramento da produção se faz necessário. Este monitoramento é tecnologicamente requerido pelas normas ISO 3834:2005 e ISO 17662:2005, que dizem que o fabricante deve adotar medidas para garantir a qualidade necessária, além de especificarem os dados que devem ser monitorados e a correta calibração dos sistemas e equipamentos de medida. Este, portanto, pode ser usado para garantir documentação do processo e tomadas de ações corretivas. Existem sistemas que realizam o monitoramento satisfatoriamente, mas o uso de comunicação por cabos e/ou com computador dedicado dificultam suas aplicações industriais. Então, um sistema embarcado, independente, que monitore diferentes sinais do processo de soldagem e que se comunique de forma robusta e flexível a diferentes equipamentos é fundamental para a indústria. Este sistema deve ser de utilização simplificada e apresentar o estado da arte em tecnologia de comunicação. Devido a essa necessidade, foi então projetado e construído um sistema para monitoramento sem fio de sinais em soldagem a arco elétrico, denominado de MoSo Wi-Fi. Três canais de aquisição estão disponíveis (tensão, corrente e velocidade de alimentação de arame, sendo validados pela instrumentação de soldagens TIG CA e MIG/MAG (curto-circuito, goticular e pulsado, demonstrando grande aplicabilidade e robustez a um baixo custo de hardware.Industrially, arc welding process is the most important in equipment production and repair, and being a special manufacturing process, which cannot be completely inspected for flaws only after its completion, production monitoring is necessary. This monitoring is technologically required by ISO 3834:2005 and ISO 17662

  8. Monitoramento de informação em mídias sociais: o e-Monitor Dengue

    Directory of Open Access Journals (Sweden)

    Michele Nacif Antunes

    Full Text Available Este artigo apresenta os resultados preliminares da pesquisa "Monitoramento de informação sobre doenças negligenciadas: o e-Monitor Dengue". O e-Monitor Dengue é um sistema de monitoramento de informação na Internet feito por meio de um mecanismo robô, software ou agente inteligente que vasculha os sites sobre dengue disponíveis na Internet. Resultados de pesquisas anteriores indicaram novas perspectivas para o monitoramento, principalmente, por meio das mídias sociais. Dentre as mídias sociais, considera-se que o Twitter pode desempenhar um papel na gestão da informação ao permitir identificar usuários que podem atuar como filtro de informação, sendo possível acessar diretamente a informação mais relevante para uma determinada área de interesse. Assim, a partir do monitoramento do Twitter, a primeira pergunta a ser respondida no âmbito da pesquisa em andamento foi "Quem fala sobre dengue?". Inicialmente, foi possível identificar a relação dos atores/perfis localizados na cidade do Rio de Janeiro e Niterói com maior ocorrência do termo "dengue" em suas mensagens. Os perfis foram cadastrados no sistema de monitoramento e são monitorados constantemente. Outra pergunta a ser respondida foi "Quando se fala de dengue?". Observa-se que o número de twetts acompanha o crescimento do número de casos de dengue. São indícios de que há uma relação entre os rumores sobre dengue e o aumento de número de casos notificados. Evidencia-se, desta forma, que realizar o monitoramento nas mídias sociais durante o período de epidemia e fazer sua relação com a situação epidemiológica da dengue pode ser uma estratégia importante para as autoridades em vigilância epidemiológica.

  9. Increased vascular sympathetic modulation in mice with Mas receptor deficiency

    Science.gov (United States)

    Rabello Casali, Karina; Ravizzoni Dartora, Daniela; Moura, Marina; Bertagnolli, Mariane; Bader, Michael; Haibara, Andrea; Alenina, Natalia; Irigoyen, Maria Claudia; Santos, Robson A

    2016-01-01

    Introduction: The angiotensin-converting enzyme 2 (ACE2)/angiotensin (Ang)-(1–7)/Mas axis could modulate the heart rate (HR) and blood pressure variabilities (BPV) which are important predictors of cardiovascular risk and provide information about the autonomic modulation of the cardiovascular system. Therefore we investigated the effect of Mas deficiency on autonomic modulation in wild type and Mas-knockout (KO) mice. Methods: Blood pressure was recorded at high sample rate (4000 Hz). Stationary sequences of 200–250 beats were randomly chosen. Frequency domain analysis of HR and BPV was performed with an autoregressive algorithm on the pulse interval sequences and on respective systolic sequences. Results: The KO group presented an increase of systolic arterial pressure (SAP; 127.26±11.20 vs 135.07±6.98 mmHg), BPV (3.54±1.54 vs 5.87±2.12 mmHg2), and low-frequency component of systolic BPV (0.12±0.11 vs 0.47±0.34 mmHg2). Conclusions: The deletion of Mas receptor is associated with an increase of SAP and with an increased BPV, indicating alterations in autonomic control. Increase of sympathetic vascular modulation in absence of Mas evidences the important role of Ang-(1–7)/Mas on cardiovascular regulation. Moreover, the absence of significant changes in HR and HRV can indicate an adaptation of autonomic cardiac balance. Our results suggest that the Ang-(1–7)/Mas axis seems more important in autonomic modulation of arterial pressure than HR. PMID:27080540

  10. Big Data e mídias sociais: monitoramento das redes como ferramenta de gestão

    Directory of Open Access Journals (Sweden)

    Gisiela Hasse Klein

    Full Text Available Resumo A pesquisa avalia se o monitoramento de mídias sociais pode ser uma ferramenta de previsão de padrões epidemiológicos. Para tanto, foram monitoradas as mídias sociais Facebook, Twitter, Instagram, Flickr, Youtube e blogs no Estado de Santa Catarina entre 24 de janeiro de 2016 e 27 de fevereiro de 2016. Os rumores sobre dengue, chikungunya, zika, Aedes aegypti e microcefalia foram relacionados ao número de casos suspeitos, confirmados ou descartados pela Vigilância Epidemiológica de Santa Catarina no mesmo período. Os resultados obtidos mostram que há forte correlação entre as variáveis e que o monitoramento pode ser usado como um modelo preditivo por profissionais da saúde e gestores públicos.

  11. HR-MAS NMR allied to chemometric on Hancornia speciosa varieties differentiation

    Energy Technology Data Exchange (ETDEWEB)

    Flores, Igor S. [Instituto Federal de Goiás (IFG), Luziânia, GO (Brazil); Silva, Andressa K.; Chaves, Lazaro J.; Collevatti, Rosane G.; Lião, Luciano M., E-mail: lucianoliao@ufg.br [Universidade Federal de Goiás (UFG), Goiânia, GO (Brazil); Furquim, Leonnardo C. [Faculdade Objetivo, GO (Brazil); Castro, Carlos F.S. [Instituto Federal de Educação, Ciência e Tecnologia Goiano (IFGoiano), GO (Brazil)

    2018-05-01

    This work describes the potential of chemometric analyses applied to {sup 1}H high-resolution magic angle spinning nuclear magnetic resonance ({sup 1}H HR-MAS NMR) data for the chemotaxonomic investigation of Hancornia speciosa (Apocynaceae) varieties. This plant, popularly known as mangaba, has a complex morphological differentiation and thus chemical analyses can be used for their taxonomic classification. In comparison to traditional techniques, {sup 1}H HR-MAS NMR allied with chemometrics provided a simple and low cost method for chemotaxonomy. Leaves of four varieties of H. speciosa from a common garden experiment was studied and demonstrated that H. speciosa var. speciosa differs from others due to its specific metabolic profile, and var. pubescens was discriminated based on its high phenolic compound content. The distinction between the latter variety and gardineri is important once it allows for the selection of samples with greater commercial value, once they produce the largest and heaviest fruits. (author)

  12. O MONITORAMENTO DE NOTÍCIAS COMO FERRAMENTA PARA A INTELIGÊNCIA COMPETITIVATHE CLIPPING AS TOLL FOR COMPETITIVE INTELLIGENCE

    Directory of Open Access Journals (Sweden)

    Ariane Barbosa Lemos

    2011-07-01

    Full Text Available O artigo apresenta um diagnóstico do serviço de monitoramento de notícias (clipping. No estudo, foram investigados os processos de elaboração desse serviço por uma empresa especializada e sua utilização por parte de organizações dos setores de educação executiva, jurídico e entretenimento. Conclui que tanto a empresa clipadora quanto seus clientes consideram o clipping útil para o processo decisório e o serviço é visto de forma complementar a ação geral de inteligência competitiva das organizações. Palavras-chave inteligência competitiva, monitoramento ambiental, fontes de informação e monitoramento de notícias. Abstract The paper presents a diagnostic study about a clipping service. This study focused the development of the service provided by a specialized firm and its use by organizations operating in the executive education, legal and entertainment areas. It concludes that both the company and your customers consider clipping useful for decision making and the clipping is seen as complementary to general action of competitive intelligence organizations. Keywords competitive intelligence, environmental scanning, information source and clipping.

  13. MONITORAMENTO DE PLATAFORMAS DE POÇOS DE PETRÓLEO ATRAVÉS DE DISPOSITIVOS MÓVEIS

    Directory of Open Access Journals (Sweden)

    Clayton Maciel Costa

    2012-06-01

    Full Text Available A expansão da Web, o advento das novas tecnologias de informação e comunicação e a massificação dos dispositivos móveis tornaram possíveis novas possibilidades de gerenciamento, interações e compartilhamento de informações. Na área petrolífera, sistemas de monitoramento utilizando dispositivos móveis vêm sendo utilizados para otimização de processos, monitoramento de dados, geração de relatórios, geração de alertas e identificação de falhas em tempo-real nas plataformas petrolíferas. Contudo, ainda são poucos os sistemas que identificam problemas em tempo-real, já que a maioria não emprega técnicas de sistemas de tempo-real. Este artigo propõe o sistema SiMoS, um sistema de tempo-real para o monitoramento remoto de plataformas de poços de petróleo através de dispositivos móveis.

  14. MAS: Malware Analysis System Based on Hardware-Assisted Virtualization Technology

    Science.gov (United States)

    Kim, Taehyoung; Kim, Inhyuk; Min, Changwoo; Eom, Young Ik

    There are many analysis techniques in order to analyze malicious codes. However, recently malicious codes often evade detection using stealthy obfuscation techniques, and attack computing systems. We propose an enhanced dynamic binary instrumentation using hardware-assisted virtualization technology. As a machine-level analyzer, our system can be isolated from almost the whole threats of malware, and provides single step analysis environment. Proposed system also supports rapid system call analysis environment. We implement our malware analysis system (referred as MAS) on the KVM hypervisor with Intel VT-x virtualization support. Our experiments with benchmarks show that the proposed system provides efficient analysis environment with low overhead.

  15. KINERJA USAHA TANAMAN HIAS POTONG PT PESONA DAUN MAS ASRI

    Directory of Open Access Journals (Sweden)

    Muhamad Arief Bangun Sanjaya

    2017-01-01

    Full Text Available Pesona Daun Mas Asri is a company in cut flowers  and leaves cultivation. The  achievement is shown by the performance of the company. The overall company’s performance contributes in developing the company’s vision. Balanced score card is a management tool used to observe and maintain the stability between financial indicators (financial perspective and non financial indicators (customer, business internal process, growth and learning.  The objective of the journal is to plan the performance of the company using balanced scorecard approach, analyze and calculate the vision, mission and strategy implemented by Pesona Daun Mas in it business activity..  The result for every strategic target shows that the performance of Pesona Daun Mas is excellent with the achieved score of 78,04%.  However the target for the selling growth level and marketing activities are classified as average which means that it still needs to be developed.   Keywords:  balanced scorecard, performance evaluation, KPI performance index, ornamental plants cutAbstrakPesona Daun Mas Asri merupakan perusahaan yang bergerak dalam bidang budi daya bunga potong dan daun potong. Pencapaian dalam menjalankan sebuah perusahaan dapat dilihat dari kinerja perusahaan tersebut.Kinerja perusahaan Pesona Daun Mas Asri secara keseluruhan dapat berkontribusi untuk mengembangkan perusahaan dalam mencapai visi. Balanced scorecard adalah salah satu alat manajemen yang dapat melihat dan menjaga keseimbangan antara indikator keuangan (perspektif keuangan dan indikator non-keuangan (pelanggan, proses bisnisinternal, pertumbuhan dan pembelajaran. Tujuan dari jurnal ini adalah untuk merancang pengukuran kinerja perusahaan dengan pendekatan Balanced scorecard. Penelitian ini juga bertujuan menganalisis dan mengukur pelaksanaan visi, misi dan strategi yang dijalankan oleh Pesona Daun Mas Asri dalam kegiatan bisnisnya. Selain itu, memberikan saran dan rekomendasi, serta merumuskan implikasi

  16. 31P Solid-state MAS NMR spectra

    International Nuclear Information System (INIS)

    Grobet, P.J.; Geerts, H.; Martens, J.A.; Jacobs, P.A.

    1989-01-01

    The structures of the silicoaluminiophosphates MCM-1 and MCM9 were characterized by 27 Al and 31 P MAS NMR. The structural identity of MCM-1 and its silicon-free homologue AlPO 4 -H 3 is demonstrated. The presence of a structural mixture in MCM-9 is confirmed. 31 P MAS NMR spectra of MCM-9 could be interpreted as a superposition of spectra of VPI-5, AlPO 4 -H 3 and SAPO-11 phases. (author). 12 refs.; 3 figs.; 1 tab

  17. MAS2-8 radar and digital control unit

    Science.gov (United States)

    Oberg, J. M.; Ulaby, F. T.

    1974-01-01

    The design of the MAS 2-8 (2 to 8 GHz microwave-active spectrometer), a ground-based sensor system, is presented. A major modification in 1974 to the MAS 2-8, that of a control subsystem to automate the data-taking operation, is the prime focus. The digital control unit automatically changes all system parameters except FM rate and records the return signal on paper tape. The overall system operation and a detailed discussion of the design and operation of the digital control unit are presented.

  18. The evolution of the MasAgro hubs

    NARCIS (Netherlands)

    Camacho-Villa, Tania Carolina; Almekinders, Conny; Hellin, Jon; Martinez-Cruz, Tania Eulalia; Rendon-Medel, Roberto; Guevara-Hernández, Francisco; Beuchelt, Tina D.; Govaerts, Bram

    2016-01-01

    Purpose: Little is known about effective ways to operationalize agricultural innovation processes. We use the MasAgro program in Mexico (which aims to increase maize and wheat productivity, profitability and sustainability), and the experiences of middle level ‘hub managers’, to understand how

  19. Angiotensin type 2 receptor (AT2R) and receptor Mas

    DEFF Research Database (Denmark)

    Villela, Daniel; Leonhardt, Julia; Patel, Neal

    2015-01-01

    The angiotensin type 2 receptor (AT2R) and the receptor Mas are components of the protective arms of the renin-angiotensin system (RAS), i.e. they both mediate tissue protective and regenerative actions. The spectrum of actions of these two receptors and their signalling mechanisms display striki...

  20. Gamma-radiation induced cross-links in ethylene-propylene rubber studied by CP-MAS NMR

    International Nuclear Information System (INIS)

    Sohma, J.; Shiotani, M.; Murakami, S.

    1983-01-01

    A new technique of 13 C-NMR, the CP-MAS method, was applied to study a chemistry of cross-links induced by #betta#-irradiation of ethylene-propylene rubber. The chemical species of cross-linking points were specified with their relative concentrations by the analysis of the CP-MAS spectra obtained before and after the irradiation. It was found that the short branches were also formed by the irradiation. A comparison was made between the cross-links detected by the CP-MAS method and those obtained by the Charlesby-Pinner analysis of the gelation caused by the #betta#-irradiation. The conventional 13 C-NMR of the cross-linked and swollen EPR provided us an information on the sol parts of the sample but little information on the cross-links in the gel parts. (author)

  1. Deuterium and lithium-6 MAS NMR studies of manganese oxide electrode materials

    Science.gov (United States)

    Paik, Younkee

    Electrolytic manganese dioxide (EMD) is used world wide as the cathode materials in both lithium and alkaline primary (non-rechargeable) batteries. We have developed deuterium and lithium MAS NMR techniques to study EMD and related manganese oxides and hydroxides, where diffraction techniques are of limited value due to a highly defective nature of the structures. Deuterons in EMD, manganite, groutite, and deuterium-intercalated pyrolusite and ramsdellite were detected by NMR, for the first time, and their locations and motions in the structures were analyzed by applying variable temperature NMR techniques. Discharge mechanisms of EMD in alkaline (aqueous) electrolytes were studied, in conjunction with step potential electrochemical spectroscopic (SPECS) method, and five distinctive discharge processes were proposed. EMD is usually heat-treated at about 300--400°C to remove water to be used in lithium batteries. Details of the effects of heat-treatment, such as structural and compositional changes as a function of heat-treatment temperature, were studied by a combination of MAS NMR, XRD, and thermogravimetric analysis. Lithium local environments in heat-treated EMD (HEMD) that were discharged in lithium cells, were described in terms of related environments found in model compounds pyrolusite and ramsdellite where specific Li + sites were detected by MAS NMR and the hyperfine shift scale method of Grey et al. Acid-leaching of Li2MnO3 represents an approach for synthesizing new or modified manganese oxide electrode materials for lithium rechargeable batteries. Progressive removal of lithium from specific crystallographic sites, followed by a gradual change of the crystal structure, was monitored by a combination of NMR and XRD techniques.

  2. ERP sistēmas ieviešana

    OpenAIRE

    Proskurins, Aleksandrs

    2008-01-01

    Šajā darbā tika apskatīta informācijas sistēmu klasifikācija, uzņēmuma resursu plānošanas sistēmas (ERP) definīcija un tās vieta IS klasifikācijā. Tika apskatīti ERP sistēmu ieviešanas teorētiskie aspekti, izstrādes un pielāgošanas specifika, kā arī tika izanalizēti vairāki ERP sistēmas ieviešanas projekti Latvijas uzņēmumos.

  3. Localização de áreas de monitoramento telemétrico em ambientes aquáticos da Amazônia Location of telemetric monitoring sites in Amazon floodplain lakes

    Directory of Open Access Journals (Sweden)

    Ivan Bergier Tavares de Lima

    2006-01-01

    Full Text Available O presente trabalho demonstra a aplicabilidade de imagens de sensoriamento remoto e de métodos de processamento de imagens digitais para definição de locais adequados à instalação de sistemas telemétricos de monitoramento de variáveis ambientais em sistemas aquáticos, localizados em regiões de difícil acesso. A técnica consiste essencialmente da aplicação de operações Booleanas entre mapas da pluma do Rio Amazonas e de zonas inundadas do Lago de Curuai em diferentes etapas do ciclo hidrológico. A localização exata para o sistema de monitoramento telemétrico será vital para o desenvolvimento de modelos de troca de gases traço entre a planície de inundação Amazônica e a atmosfera.The present work illustrates the application of remote sensing and image processing methods to define appropriate sites for installing buoy moored telemetric systems at the surface of Amazon floodplain lakes for long-term limnologic-micrometeorologic monitoring. The technique consists essentially of Boolean operations over Amazon plume maps and historic inundation of the Curuai Lake at distinct stages of the hydrologic cycle. The precise location for the long-term monitoring is vital to the development of models concerning air-water trace gas exchange in the Amazon floodplains.

  4. Monitoramento do ciclo estral de cutias (Dasyprocta leporina Lichtenstein, 1823 através de citologia esfoliativa vaginal e ultrassonografia

    Directory of Open Access Journals (Sweden)

    Lívia B. Campos

    2015-02-01

    Full Text Available O objetivo deste estudo foi monitorar o ciclo estral em cutias (Dasyprocta leporina criadas em cativeiro no semiárido brasileiro. Durante 70 dias, cinco cutias foram diariamente submetidas a citologia esfoliativa vaginal, e o monitoramento ultrassonográfico ovariano foi realizado a cada três dias. Um total de 8 ciclos estrais foi completamente monitorado, com duração de 28,2±0,7 dias, variando de 24 a 31 dias. Pela citologia esfoliativa vaginal, houve uma predominância de células superficiais nas fases de proestro e estro (P0,05. Os folículos foram identificados durante as fases estrogênicas (proestro e estro, com diâmetro médio de 1±0,5mm. Em apenas 12,5% das fases luteais, corpos lúteos medindo 1,4±0,9mm foram identificados. Conclui-se que a associação da citologia vaginal e da ultrassonografia ovariana constitui uma alternativa viável para o monitoramento de ciclos estrais e identificação das fases estrogênicas em cutias da espécie Dasyprocta leporina

  5. Measuring proton shift tensors with ultrafast MAS NMR.

    Science.gov (United States)

    Miah, Habeeba K; Bennett, David A; Iuga, Dinu; Titman, Jeremy J

    2013-10-01

    A new proton anisotropic-isotropic shift correlation experiment is described which operates with ultrafast MAS, resulting in good resolution of isotropic proton shifts in the detection dimension. The new experiment makes use of a recoupling sequence designed using symmetry principles which reintroduces the proton chemical shift anisotropy in the indirect dimension. The experiment has been used to measure the proton shift tensor parameters for the OH hydrogen-bonded protons in tyrosine·HCl and citric acid at Larmor frequencies of up to 850 MHz. Copyright © 2013 Elsevier Inc. All rights reserved.

  6. A General Protocol for Temperature Calibration of MAS NMR Probes at Arbitrary Spinning Speeds

    Science.gov (United States)

    Guan, Xudong; Stark, Ruth E.

    2010-01-01

    A protocol using 207Pb NMR of solid lead nitrate was developed to determine the temperature of magic-angle spinning (MAS) NMR probes over a range of nominal set temperatures and spinning speeds. Using BioMAS and fastMAS probes with typical sample spinning rates of 8 and 35 kHz, respectively, empirical equations were devised to predict the respective sample temperatures. These procedures provide a straightforward recipe for temperature calibration of any MAS probe. PMID:21036557

  7. Monitoramento e Controle de Projetos de Desenvolvimento de Software com o Scrum: Avaliação da Produção Científica

    Directory of Open Access Journals (Sweden)

    Alexandre Guido Vallerão

    2013-12-01

    Full Text Available O objetivo principal deste estudo é a realização de bibliometria da produção científica dos últimos cinco anos sobre processos de monitoramento e controle de projetos de desenvolvimento de software gerenciados com o método Scrum, envolvendo as principais bases de publicações de periódicos, teses e dissertações. Para isso, foram definidos como eixos temáticos os métodos ágeis, o método Scrum, software e monitoramento e controle de projetos. Foram pesquisadas bases de publicações nos portais Capes e Web of Knowledge, sendo a relevância dos artigos encontrados determinada pelo h-index. Com base no conjunto de publicações localizadas, foram determinadas suas principais abordagens sobre aqueles processos de monitoramento e controle. Os resultados da pesquisa indicam uma pequena produção científica destinada ao monitoramento e controle de projetos de desenvolvimento de software com uso de métodos ágeis, revelando em número ainda menor aqueles com o uso do método Scrum, o que sugere oportunidades de pesquisa e consequente incremento da produção científica relacionada a esse tema contemporâneo às organizações.DOI:10.5585/gep.v4i2.154

  8. What drives cross-border M&As in commercial banking?

    NARCIS (Netherlands)

    Galamhussen, Mohamed; Hennart, Jean-Francois; Pinheiro, Carlos Manuel

    2016-01-01

    Using a gravity model, we analyze the determinants of the probability that commercial banks in 89 acquiring countries and 118 target countries will undertake M&As over a 30-year period (1981–2010) and of the value of these M&As. We find that the value of cross-border M&As increases with the size of

  9. Radiofrequency fields in MAS solid state NMR probes

    Science.gov (United States)

    Tošner, Zdeněk; Purea, Armin; Struppe, Jochem O.; Wegner, Sebastian; Engelke, Frank; Glaser, Steffen J.; Reif, Bernd

    2017-11-01

    We present a detailed analysis of the radiofrequency (RF) field over full volume of a rotor that is generated in a solenoid coil. On top of the usually considered static distribution of amplitudes along the coil axis we describe dynamic radial RF inhomogeneities induced by sample rotation. During magic angle spinning (MAS), the mechanical rotation of the sample about the magic angle, a spin packet travels through areas of different RF fields and experiences periodical modulations of both the RF amplitude and the phase. These modulations become particularly severe at the end regions of the coil where the relative RF amplitude varies up to ±25% and the RF phase changes within ±30°. Using extensive numerical simulations we demonstrate effects of RF inhomogeneity on pulse calibration and for the ramped CP experiment performed at a wide range of MAS rates. In addition, we review various methods to map RF fields using a B0 gradient along the sample (rotor axis) for imaging purposes. Under such a gradient, a nutation experiment provides directly the RF amplitude distribution, a cross polarization experiment images the correlation of the RF fields on the two channels according to the Hartmann-Hahn matching condition, while a spin-lock experiment allows to calibrate the RF amplitude employing the rotary resonance recoupling condition. Knowledge of the RF field distribution in a coil provides key to understand its effects on performance of a pulse sequence at the spectrometer and enables to set robustness requirements in the experimental design.

  10. Influence of using high kV and low m As techniques in the dose of patients submitted to X ray thorax examinations; Influencia do uso de tecnicas de alto kV e baixo mAs na dose em pacientes submetidos a exames de raios X de torax

    Energy Technology Data Exchange (ETDEWEB)

    Oliveira, Paulo Marcio Campos de, E-mail: pmco@cdtn.b [Universidade Federal de Minas Gerais (UFMG), Belo Horizonte, MG (Brazil). Dept. de Engenharia Nuclear. Programa de Pos-Graduacao em Ciencias e Tecnicas Nucleares; Squair, Peterson Lima; Lacerda, Marco Aurelio de Sousa; Silva, Teogenes Augusto da, E-mail: pls@cdtn.b, E-mail: masl@cdtn.b, E-mail: silvata@cdtn.b [Centro de Desenvolvimento da Tecnologia Nuclear (CDTN/CNEN-MG), Belo Horizonte, MG (Brazil)

    2011-07-01

    Dosimetric studies of patients subject to radiodiagnostic have got a special attention in Brazil although they are not required by the Brazilian legislation. However, in several Brazilian clinics there have been observed the use of techniques with lower peak voltage and higher electric charges values in spite the European Commission recommends the high voltages with low electric charge values in order to reduce the patient dose. This work compares three methodologies for evaluating the organ absorbed doses in patients undergoing chest x-rays at two techniques (80 k Vp and 10 m As; 120 k Vp and 2 m As): the PCXMC and CALDose{sub X} Monte Carlo based software and experimental measurements with T L dosimeters in a anthropomorphic phantom. The experimental measurements showed the technique with high voltage was dose reduced by approximately 60% in the entrance skin in relation to low voltage technique and the software showed similar dose reduction, shows the importance of adopting techniques which have high voltage values and low electrical charges, unlike usually found on chest x-rays in some hospitals and clinics in Brazil. (author)

  11. Genotyping by sequencing (GBS, an ultimate marker-assisted selection (MAS tool to accelerate plant breeding

    Directory of Open Access Journals (Sweden)

    Jiangfeng eHe

    2014-09-01

    Full Text Available Marker-assisted selection (MAS refers to the use of molecular markers to assist phenotypic selections in crop improvement. Several types of molecular markers, such as single nucleotide polymorphism (SNP, have been identified and effectively used in plant breeding. The application of next-generation sequencing (NGS technologies has led to remarkable advances in whole genome sequencing, which provides ultra-throughput sequences to revolutionize plant genotyping and breeding. To further broaden NGS usages to large crop genomes such as maize and wheat, genotyping by sequencing (GBS has been developed and applied in sequencing multiplexed samples that combine molecular marker discovery and genotyping. GBS is a novel application of NGS protocols for discovering and genotyping SNPs in crop genomes and populations. The GBS approach includes the digestion of genomic DNA with restriction enzymes followed by the ligation of barcode adapter, PCR amplification and sequencing of the amplified DNA pool on a single lane of flow cells. Bioinformatic pipelines are needed to analyze and interpret GBS datasets. As an ultimate MAS tool and a cost-effective technique, GBS has been successfully used in implementing genome-wide association study (GWAS, genomic diversity study, genetic linkage analysis, molecular marker discovery and genomic selection (GS under a large scale of plant breeding programs.

  12. Monitoring nitrogen nutrition in cotton Monitoramento da nutrição nitrogenada do algodoeiro

    Directory of Open Access Journals (Sweden)

    Ciro Antonio Rosolem

    2010-10-01

    Full Text Available Both N excess and deficiency may affect cotton yield and quality. It would therefore be useful to base the N management fertilization on the monitoring of the nutritional status. This study investigated the correlations among the following determination methods of the N nutritional status of cotton (Gossypium hirsutum L., var. Latifolia: chlorophyll readings (SPAD-502®, Minolta, specific-ion nitrate meter (Nitrate Meter C-141, Horiba-Cardy®, and laboratory analysis (conventional foliar diagnosis. Samples were taken weekly from two weeks before flowering to the fifth week after the first flower. The experiment was conducted on the Fazenda Santa Tereza, Itapeva, State of São Paulo, Brazil. The crop was fertilized with 40 kg ha-1 N at planting and 0, 30, 60, 90, and 120 kg ha-1 of side-dressed N. The range of leaf N contents reported as adequate for samples taken 80-90 days after plant emergence (traditional foliar diagnosis may be used as reference from the beginning of flowering when the plant is not stressed. Specific-ion nitrate meter readings can be used as a nutritional indicator of cotton nutrition from one week after pinhead until the third week of flowering. In this case, plants are well-nourished when readings exceed 8,000 mg L-1 NO3-. The chlorophyll meter can also be used to estimate the nutritional status of cotton from the third week of flowering. In this case the readings should be above 48 in well-nourished plants.Tanto o excesso como a deficiência de N podem levar a decréscimos na produção e qualidade do algodão. Assim, o monitoramento do estado nutricional da planta pode ajudar no manejo da adubação nitrogenada. Um experimento foi realizado para estudar as correlações entre métodos de determinação do estado nutricional do algodoeiro (Gossypium hirsutum L., var. Latifolia. Os métodos usados foram um medidor de clorofila (SPAD-502®, Minolta, um medidor específico de ions para nitrato (Nitrate Meter C-141, Horiba

  13. Controle estatístico de processo aplicado ao monitoramento de envase da tintura de iodo

    Directory of Open Access Journals (Sweden)

    Paulo Alexandre Nunes Neto

    2010-06-01

    Full Text Available A aplicação do controle estatístico para monitorar o desempenho da etapa de envase de formas farmacêuticas líquidas consiste em obter informações e estabelecer estratégias para a validação do processo, assim como possibilitar o gerenciamento deste a partir da percepção do comportamento das variáveis críticas do produto durante a produção. Esta etapa do processo possui como variável crítica o volume de envase. Variações neste parâmetro fora dos limites de qualidade pré-estabelecidos pela legislação refletem ineficiências durante o processo podendo ocasionar a reprovação do produto. Para demonstrar de forma objetiva o grau de segurança requerida para este tipo de processo foram utilizadas ferramentas do controle estatístico de processo (CEP para estudar e validar o desempenho da etapa de envase da tintura de iodo fabricada pela indústria farmacêutica Lapon Química e Natural Ltda. (Limoeiro - PE, Brasil, bem como verificar a estabilidade estatística e capacidade do processo. As atividades de melhoria, através da identificação e eliminação das causas especiais de variação do processo, permitiram a redução de sua variabilidade, assegurando uma melhoria contínua da qualidade nos resultados da produção. Palavras-chave: Controle estatístico de processo. Monitoramento de envase. Validação de processo. Tintura de iodo. ABSTRACT Statistical process control applied to used in monitoring the iodine tincture fill phase Statistical control is used to monitor the performance of the fill phase in the manufacture of liquid pharmaceutical forms, to obtain information and establish criteria for process validation, as well as to enable control of the process, by observing the behavior of the critical variables during production. The critical variable at this stage of the process is the filling volume. Variations in this parameter outside the established legal quality limits reflect inefficiency in the process that may

  14. Monitoramento da cadeia do frio: novas tecnologias e recentes avanços

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    Wigberto Antonio Spagnol

    2017-11-01

    Full Text Available Resumo A economia, atualmente, é impulsionada pela alta competitividade, exigindo que os setores de produção e logística sejam ágeis, flexíveis e com capacidade de ação para a solução de dificuldades. A logística é de extrema importância para as operações das cadeias de alimentos perecíveis, como carnes, peixes, lácteos, frutas e produtos hortícolas, assim como para determinados produtos da indústria farmacêutica, como vacinas, biomedicamentos e hemoderivados, que necessitam do uso da cadeia do frio devido à sua perecibilidade. A temperatura é o fator mais importante para a conservação da qualidade e manutenção da vida útil destes produtos, sendo a refrigeração um dos métodos mais amplamente utilizados para retardar o desenvolvimento de vários fatores que conduzem à sua deterioração. Dentre os desafios para a melhoria de incertezas da cadeia do frio, há a mitigação de riscos de ruptura da mesma. Sabe-se que há variações inevitáveis das condições de conservação dos produtos durante as etapas da cadeia de frio, as quais causam alteração da vida útil de alimentos perecíveis. Seja no transporte ou nas câmaras frias de armazenagem, há flutuação de temperatura em torno da condição ideal, sendo que ainda hoje, na maioria dos sistemas, o monitoramento da temperatura é realizado por pouquíssimos sensores. Embora poucas tecnologias de monitoração de temperatura sejam utilizadas para inibir os riscos de perda de qualidade e obter a segurança alimentar, estas são utilizadas de forma independente, nos diferentes elos da cadeia logística do frio. Esses desafios têm impulsionado esforços de grupos de pesquisas de países desenvolvidos para o aperfeiçoamento de aplicações de rede de sensores sem fio (RSSF e de identificação por radiofrequência (RFID, com base em dispositivos sensores. Este trabalho aborda aspectos importantes da aplicação destas novas tecnologias, que são capazes de

  15. The MAS Six Years in Power in Bolivia

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    Ton Salman

    2012-04-01

    Full Text Available Review Essay of:– The Rise of Evo Morales and the MAS, by Sven Harten. London/New York: Zed Books, 2011.– Evo Morales and the Movimiento al Socialismo in Bolivia; The First Term in Context, edited by Adrian J. Pearce. London, Institute for the Study of the Americas, 2011.– El estado de derecho como tiranía, by Luis Tapia. La Paz: CIDES/UMSA, 2011.– From Rebellion to Reform in Bolivia: Class Struggle, Indigenous Liberation and the Politics of Evo Morales, by Jeffery R. Webber. Chicago: Haymarket Books, 2011.– La democracia desde los márgenes: Transformaciones en el campo político boliviano, by María Teresa Zegada, with Claudia Arce, Gabriela Canedo and Alber Quispe. La Paz: Muela del Diablo Editores/CLACSO, 2011.

  16. TOKSISITAS LETAL MOLUSKISIDA NIKLOSAMIDA PADA BENIH IKAN MAS (Cyprinus carpio

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    Yosmaniar Yosmaniar

    2009-04-01

    Full Text Available Penggunaan moluskisida untuk menanggulangi hama dalam budidaya tanaman padi yang semakin meningkat berpotensi mencemari lingkungan perairan, karena mengandung residu dari bahan aktifnya. Moluskisida niklosamida (C13H8Cl2N2O4 merupakan bahan aktif pestisida yang digunakan untuk memberantas hama keong mas atau siput murbei (Pomacea sp. di sawah. Dengan demikian, bahan tersebut memiliki potensi untuk mencemari lahan tempat usaha budidaya ikan. Penelitian ini bertujuan untuk mengetahui potensi toksisitas akut niklosamida terhadap benih ikan mas (Cyprinus carpio yang ditunjukkan oleh nilai Median Lethal Concentration (LC50 24, 48, dan 96 jam. Penelitian dilakukan di Instalasi Riset Lingkungan Perikanan Budidaya dan Toksikologi, Cibalagung-Bogor. Menggunakan ikan mas dengan bobot individu 2,47 ± 0,13 g. Moluskisida yang digunakan mengandung bahan aktif niklosamida 250g/L. Wadah pengujian berupa 21 unit akuarium kaca berukuran 40 cm x 20 cm x 20 cm yang dilengkapi aerasi serta saluran pemasukan dan pengeluaran. Jumlah ikan uji setiap wadah 10 ekor dengan peubah yang diukur adalah mortalitas ikan. Selama penelitian ikan tidak diberi makan. Tahapan penelitian terdiri atas penentuan nilai ambang atas-bawah, nilai lethal time dan LC50 -24, 48, 72, dan 96 jam. Data diolah dengan analisis probit program LC50. Hasil penelitian menunjukkan bahwa nilai LC50-24, 48, 72, dan 96 jam terhadap benih ikan mas adalah 0,8012 (0,7140—0,8990; 0,5999 (0,5356—0,6719; 0,4511 (0,4067—0,5004; dan 0,3849 mg/L (0,3684—0,4061. Hal ini menunjukkan niklosamida termasuk pestisida yang memiliki toksisitas sangat tinggi (golongan A. The use of molluscicide in aquatic as well as in terresterial agro ecosystem without properly controlled may produce detrimental effects on freshwater fisheries. Molluscicide utilization for golden apple snail (Pomacea sp. control in rice field has increased. The ingredient potencially has a possibility to pollute aquaculture water. The

  17. Food Waste Composting Study from Makanan Ringan Mas

    Science.gov (United States)

    Kadir, A. A.; Ismail, S. N. M.; Jamaludin, S. N.

    2016-07-01

    The poor management of municipal solid waste in Malaysia has worsened over the years especially on food waste. Food waste represents almost 60% of the total municipal solid waste disposed in the landfill. Composting is one of low cost alternative method to dispose the food waste. This study is conducted to compost the food waste generation in Makanan Ringan Mas, which is a medium scale industry in Parit Kuari Darat due to the lack knowledge and exposure of food waste recycling practice. The aim of this study is to identify the physical and chemical parameters of composting food waste from Makanan Ringan Mas. The physical parameters were tested for temperature and pH value and the chemical parameter are Nitrogen, Phosphorus and Potassium. In this study, backyard composting was conducted with 6 reactors. Tapioca peel was used as fermentation liquid and soil and coconut grated were used as the fermentation bed. Backyard composting was conducted with six reactors. The overall results from the study showed that the temperature of the reactors were within the range which are from 30° to 50°C. The result of this study revealed that all the reactors which contain processed food waste tend to produce pH value within the range of 5 to 6 which can be categorized as slightly acidic. Meanwhile, the reactors which contained raw food waste tend to produce pH value within the range of 7 to 8 which can be categorized as neutral. The highest NPK obtained is from Reactor B that process only raw food waste. The average value of Nitrogen is 48540 mg/L, Phosphorus is 410 mg/L and Potassium is 1550 mg/L. From the comparison with common chemical fertilizer, it shows that NPK value from the composting are much lower than NPK of the common chemical fertilizer. However, comparison with NPK of organic fertilizer shown only slightly difference value in NPK.

  18. Avaliação do sistema de monitoramento computadorizado de digestão in vitro: 1. Testes preliminares

    OpenAIRE

    Campos Fábio Prudêncio de; Lanna Dante Pazzanese Duarte; Bose Máx Lázaro Vieira; Boin Celso

    2000-01-01

    O objetivo deste trabalho foi testar o sistema de monitoramento computadorizado da produção de gás in vitro. Essa técnica facilita estudos da degradação das frações solúveis e insolúveis das forragens, quantificadas pela produção de gás (CO2 e CH4) oriunda do metabolismo microbiano e medida por sensor de pressão. Diversas quantidades de amostras (50 a 110 mg de feno de alfafa) e outros alimentos foram testadas. Também, a influência da quantidade de líquido ruminal (2,0 ou 3,0 mL), com ou sem ...

  19. Monitoramento geodésico tridimensional aplicado em ensaios estruturais de painéis compensados de madeira

    OpenAIRE

    Zonta, Camila

    2013-01-01

    Resumo: Uma parceria entre o Laboratório de Instrumentação Geodésica e o Laboratório de Tecnologia da Madeira, ambos da Universidade Federal do Paraná, possibilitou o desenvolvimento deste projeto. A junção das áreas, Levantamento Geodésico e Tecnologia da Madeira, mostra-se um conjunto inovador na avaliação de ensaios estruturais e monitoramento de estruturas de madeira. Desta forma, realizaram-se neste trabalho ensaios de flexão estática em painéis compensados de madeira com uso de uma Máqu...

  20. Monitoramento do percevejo marrom Euschistus heros (Hemiptera: Pentatomidae por feromônio sexual em lavoura de soja

    Directory of Open Access Journals (Sweden)

    Valvenarg Pereira da Silva

    2014-11-01

    Full Text Available O objetivo deste trabalho foi avaliar a eficiência das formulações septo de borracha e lure do feromônio sexual do percevejo marrom Euschistus heros e compará-la ao método do pano de batida, para o monitoramento dessa praga em lavoura de soja. Os tratamentos foram: feromônio em septo de borracha, feromônio em lure e amostragem com pano de batida. As amostragens foram realizadas semanalmente durante a fase reprodutiva da soja (dez semanas. Para estimar a densidade populacional de percevejos e compará-la à captura nas armadilhas de feromônio, foram efetuados quatro panos de batida por semana em todas as parcelas; além disso, foi determinado o número de percevejos capturados nas armadilhas por semana. Os danos provocados pelos percevejos nas sementes foram analisados pelo teste de tetrazólio. As formulações do feromônio foram eficientes na captura de E. heros, e a formulação em lure capturou mais percevejos. O controle precoce da população, indicado pelo nível de controle nas armadilhas com feromônio, resultou em sementes com maior qualidade do que as provenientes das parcelas monitoradas pelo pano de batida. Assim, as armadilhas com feromônio são mais eficientes que o pano de batida para o monitoramento das populações de percevejos durante a fase crítica do ataque deste inseto nas lavouras de soja.

  1. Qualidade do leite: utopia sem um programa sério de monitoramento da ocorrência de mastite bovina

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    Helio Langoni

    2013-05-01

    Full Text Available As mastites continuam sendo um dos principais problemas a onerar a pecuária leiteira, além dos aspectos de saúde pública, considerando-se a veiculação de patógenos causadores de doença em humanos. Sua múltipla etiologia, com o envolvimento de inúmeros patógenos, requer um programa de controle rigoroso para o seu monitoramento e controle de qualidade do leite, pautado em ações diagnósticas e de vigilância epidemiológica com relação a parâmetros que indiretamente associam-se à ocorrência de mastites nos rebanhos, como California Mastitis Test (CMT e Contagem de Células Somáticas (CCS/mL de leite, de amostras de leite individuais composta de cada vaca, bem como do tanque de expansão, o que permite ainda o monitoramento da Contagem Bacteriana Total (CBT, que tende a se relacionar com a ocorrência de mastites, principalmente subclínicas. Destacam-se ainda aspectos de exame microbiológico do leite e da importância da ordenha como ponto crucial nas mastites, enfatizando aspectos relevantes do processo de ordenha com fatores de risco para a ocorrência das mastites. Baseando-se nestes aspectos, apresenta-se esta revisão, acreditando-se na possibilidade de obtenção de produtos lácteos de melhor qualidade, com o comprometimento de todos os envolvidos na cadeia produtiva do leite, conscientes de que a qualidade do leite depende de todos, valendo-se também os consumidores, que são os elementos finais da cadeia produtiva do leite.

  2. Antioxidant capacity of cornelian cherry (Cornus mas L.) - comparison between permanganate reducing antioxidant capacity and other antioxidant methods.

    Science.gov (United States)

    Popović, Boris M; Stajner, Dubravka; Slavko, Kevrešan; Sandra, Bijelić

    2012-09-15

    Ethanol extracts (80% in water) of 10 cornelian cherry (Cornus mas L.) genotypes were studied for antioxidant properties, using methods including DPPH(), ()NO, O(2)(-) and ()OH antiradical powers, FRAP, total phenolic and anthocyanin content (TPC and ACC) and also one relatively new, permanganate method (permanganate reducing antioxidant capacity-PRAC). Lipid peroxidation (LP) was also determined as an indicator of oxidative stress. The data from different procedures were compared and analysed by multivariate techniques (correlation matrix calculation and principal component analysis (PCA)). Significant positive correlations were obtained between TPC, ACC and DPPH(), ()NO, O(2)(-), and ()OH antiradical powers, and also between PRAC and TPC, ACC and FRAP. PCA found two major clusters of cornelian cherry, based on antiradical power, FRAP and PRAC and also on chemical composition. Chemometric evaluation showed close interdependence between PRAC method and FRAP and ACC. There was a huge variation between C. mas genotypes in terms of antioxidant activity. Copyright © 2012 Elsevier Ltd. All rights reserved.

  3. Angiotensin-(1-7)/Mas axis integrity is required for the expression of object recognition memory.

    Science.gov (United States)

    Lazaroni, Thiago L N; Raslan, Ana Cláudia S; Fontes, Walkiria R P; de Oliveira, Marilene L; Bader, Michael; Alenina, Natalia; Moraes, Márcio F D; Dos Santos, Robson A; Pereira, Grace S

    2012-01-01

    It has been shown that the brain has its own intrinsic renin-angiotensin system (RAS) and angiotensin-(1-7) (Ang-(1-7)) is particularly interesting, because it appears to counterbalance most of the Ang II effects. Ang-(1-7) exerts its biological function through activation of the G-protein-coupled receptor Mas. Interestingly, hippocampus is one of the regions with higher expression of Mas. However, the role of Ang-(1-7)/Mas axis in hippocampus-dependent memories is still poorly understood. Here we demonstrated that Mas ablation, as well as the blockade of Mas in the CA1-hippocampus, impaired object recognition memory (ORM). We also demonstrated that the blockade of Ang II receptors AT1, but not AT2, recovers ORM impairment of Mas-deficient mice. Considering that high concentrations of Ang-(1-7) may activate AT1 receptors, nonspecifically, we evaluate the levels of Ang-(1-7) and its main precursors Ang I and Ang II in the hippocampus of Mas-deficient mice. The Ang I and Ang II levels are unaltered in the whole hipocampus of MasKo. However, Ang-(1-7) concentration is increased in the whole hippocampus of MasKo mice, as well as in the CA1 area. Taken together, our findings suggest that the functionality of the Ang-(1-7)/Mas axis is essential for normal ORM processing. Copyright © 2011 Elsevier Inc. All rights reserved.

  4. Monitoramento por radiotelemetria da área de uso de onça parda reintroduzida no entorno do Parque Estadual da Serra do Brigadeiro - MG, Brasil Radiotelemetry monitoring of the home range of cougar reintroduced at the surroundings of the State Park of Serra do Brigadeiro - MG, Brazil

    Directory of Open Access Journals (Sweden)

    João Bosco Gonçalves de Barros

    2011-07-01

    Full Text Available Um exemplar macho, subadulto de onça parda reintroduzido foi monitorado por técnica de radiotelemetria. O monitoramento foi de 110 dias, realizado de forma aleatória, com intervalos descontínuos. Os dados do acompanhamento sugerem que a área utilizada por este espécime seja de, aproximadamente, 26km². Esta configura o menor índice já descrito para a espécie, porém, deve-se ressaltar a importância deste monitoramento básico, visto a incipiência do comportamento de um felino de grande porte reintroduzido em habitat natural após período em cativeiro.One subadult male specimen of a reintroduced mountain lion was monitored using the radio telemetry technique. The monitoring lasted 110 days, being randomly distributed. Data of the monitoring through radiotelemetry suggested that the home range of this specimen was of approximately 26km². This sets as the smallest home range described for this species. However, the importance of this basic monitoring should be emphasized, since information of the behavior of a large feline reintroduced in its natural habitat after a period in captivity is incipient.

  5. Evidence for Heterodimerization and Functional Interaction of the Angiotensin Type 2 Receptor and the Receptor MAS.

    Science.gov (United States)

    Leonhardt, Julia; Villela, Daniel C; Teichmann, Anke; Münter, Lisa-Marie; Mayer, Magnus C; Mardahl, Maibritt; Kirsch, Sebastian; Namsolleck, Pawel; Lucht, Kristin; Benz, Verena; Alenina, Natalia; Daniell, Nicholas; Horiuchi, Masatsugu; Iwai, Masaru; Multhaup, Gerhard; Schülein, Ralf; Bader, Michael; Santos, Robson A; Unger, Thomas; Steckelings, Ulrike Muscha

    2017-06-01

    The angiotensin type 2 receptor (AT2R) and the receptor MAS are receptors of the protective arm of the renin-angiotensin system. They mediate strikingly similar actions. Moreover, in various studies, AT2R antagonists blocked the effects of MAS agonists and vice versa. Such cross-inhibition may indicate heterodimerization of these receptors. Therefore, this study investigated the molecular and functional interplay between MAS and the AT2R. Molecular interactions were assessed by fluorescence resonance energy transfer and by cross correlation spectroscopy in human embryonic kidney-293 cells transfected with vectors encoding fluorophore-tagged MAS or AT2R. Functional interaction of AT2R and MAS was studied in astrocytes with CX3C chemokine receptor-1 messenger RNA expression as readout. Coexpression of fluorophore-tagged AT2R and MAS resulted in a fluorescence resonance energy transfer efficiency of 10.8 ± 0.8%, indicating that AT2R and MAS are capable to form heterodimers. Heterodimerization was verified by competition experiments using untagged AT2R and MAS. Specificity of dimerization of AT2R and MAS was supported by lack of dimerization with the transient receptor potential cation channel, subfamily C-member 6. Dimerization of the AT2R was abolished when it was mutated at cysteine residue 35. AT2R and MAS stimulation with the respective agonists, Compound 21 or angiotensin-(1-7), significantly induced CX3C chemokine receptor-1 messenger RNA expression. Effects of each agonist were blocked by an AT2R antagonist (PD123319) and also by a MAS antagonist (A-779). Knockout of a single of these receptors made astrocytes unresponsive for both agonists. Our results suggest that MAS and the AT2R form heterodimers and that-at least in astrocytes-both receptors functionally depend on each other. © 2017 American Heart Association, Inc.

  6. Distributed Cooperation Solution Method of Complex System Based on MAS

    Science.gov (United States)

    Weijin, Jiang; Yuhui, Xu

    To adapt the model in reconfiguring fault diagnosing to dynamic environment and the needs of solving the tasks of complex system fully, the paper introduced multi-Agent and related technology to the complicated fault diagnosis, an integrated intelligent control system is studied in this paper. Based on the thought of the structure of diagnostic decision and hierarchy in modeling, based on multi-layer decomposition strategy of diagnosis task, a multi-agent synchronous diagnosis federation integrated different knowledge expression modes and inference mechanisms are presented, the functions of management agent, diagnosis agent and decision agent are analyzed, the organization and evolution of agents in the system are proposed, and the corresponding conflict resolution algorithm in given, Layered structure of abstract agent with public attributes is build. System architecture is realized based on MAS distributed layered blackboard. The real world application shows that the proposed control structure successfully solves the fault diagnose problem of the complex plant, and the special advantage in the distributed domain.

  7. Multi-Robot Remote Interaction with FS-MAS

    Directory of Open Access Journals (Sweden)

    Yunliang Jiang

    2013-02-01

    Full Text Available The need to reduce bandwidth, improve productivity, autonomy and the scalability in multi-robot teleoperation has been recognized for a long time. In this article we propose a novel finite state machine mobile agent based on the network interaction service model, namely FS-MAS. This model consists of three finite state machines, namely the Finite State Mobile Agent (FS-Agent, which is the basic service module. The Service Content Finite State Machine (Content-FS, using the XML language to define workflow, to describe service content and service computation process. The Mobile Agent computation model Finite State Machine (MACM-FS, used to describe the service implementation. Finally, we apply this service model to the multi-robot system, the initial realization completing complex tasks in the form of multi-robot scheduling. This demonstrates that the robot has greatly improved intelligence, and provides a wide solution space for critical issues such as task division, rational and efficient use of resource and multi-robot collaboration.

  8. PEMANFAATAN TANAMAN ATRAKTAN MENGENDALIKAN HAMA KEONG MAS PADI

    Directory of Open Access Journals (Sweden)

    Ameilia Zuliyanti Siregar

    2018-01-01

    In Indonesia, many plantation as use as beneficial plants. This study aims to obtain an effective formula that can be used as a biopesticide to control snail pests during the vegetative phase from May to July 2017 using random non-factorial methods at two rice planting locations in the Village Lae parira, Dairi, North Sumatra. Design with 6 treatments and 3 replicates (ie control, neem leaves (Azadirachta indica, tobacco leaf (Nicotiana tabacum, sweet potato leaf (Manihot glaziovii, noni fruit, Morinda citrifolia, and betel nut (Areca catechu and papaya (Carica papaya as an eco-friendly herbaceous and biopesticide. Based on the study recorded in sampling for 7 days with 6 treatments had significant effect on the percentage affected by the clump of rice attacked and the percentage of death. Pearson correlation value recorded percentage of death and percentage of impacted  showed a very significant relationship. Neem is the best biopesticide in controlling mollusicides, followed by betel nuts, tobacco, poisonous yams and noni. Death of 100% snail mas will prevent damage to the clump of rice plants Dairi, North Sumatra. All biopesticide treatments were tested to control snail pests in rice plants that will increase agicultural productivity in maintaining food security in Dairi, North Sumatra.

  9. HR-MAS NMR for rapid identification of illicit substances in tablets and Blotter papers seized by Police Department

    Energy Technology Data Exchange (ETDEWEB)

    Souza, Luciano F.; Vieira, Tarcísio S.; Lião, Luciano M., E-mail: lucianoliao@ufg.br [Universidade Federal de Goiás (UFG), Goiânia, GO (Brazil). Instituto de Química; Alcantara, Glaucia B. [Universidade Federal de Mato Grosso do Sul (UFMS), Campo Grande, MS (Brazil). Instituto de Química

    2016-07-01

    Illicit substances found in blotter papers and tablets seized by police are traditionally identified and characterized from extracts of these materials. However, the procedures involved in extraction stages can result in artifacts and even contamination of the samples to be analyzed. On the other hand, high-resolution magic angle spinning nuclear magnetic resonance (HR-MAS NMR) is a technique that requires no pretreatment steps, enabling direct analysis of the material, including the analysis of new illegal synthetic psychoactive substances. This study presents and discusses applications of the HR-MAS NMR in the analysis of tablets and blotter papers seized. Additional analysis in solution of the extracts of these materials was performed to compare the obtained spectral resolution signals. The results demonstrated that the HR-MAS NMR allowed the rapid identification of 3,4-methylenedioxy-N-methylcathinone (methylone), 4-methylmethcathinone (mephedrone), 2,5-dimethoxy-4-bromoamphetamine (DOB) and 2-(4-bromo-2,5-dimethoxyphenyl)-N-[(2- methoxyphenyl)methyl]ethanamine (25B-NBOMe) in samples of tablets and blotter papers seized in Goiás State, Brazil. (author)

  10. HR-MAS NMR for rapid identification of illicit substances in tablets and Blotter papers seized by Police Department

    International Nuclear Information System (INIS)

    Souza, Luciano F.; Vieira, Tarcísio S.; Lião, Luciano M.; Alcantara, Glaucia B.

    2016-01-01

    Illicit substances found in blotter papers and tablets seized by police are traditionally identified and characterized from extracts of these materials. However, the procedures involved in extraction stages can result in artifacts and even contamination of the samples to be analyzed. On the other hand, high-resolution magic angle spinning nuclear magnetic resonance (HR-MAS NMR) is a technique that requires no pretreatment steps, enabling direct analysis of the material, including the analysis of new illegal synthetic psychoactive substances. This study presents and discusses applications of the HR-MAS NMR in the analysis of tablets and blotter papers seized. Additional analysis in solution of the extracts of these materials was performed to compare the obtained spectral resolution signals. The results demonstrated that the HR-MAS NMR allowed the rapid identification of 3,4-methylenedioxy-N-methylcathinone (methylone), 4-methylmethcathinone (mephedrone), 2,5-dimethoxy-4-bromoamphetamine (DOB) and 2-(4-bromo-2,5-dimethoxyphenyl)-N-[(2- methoxyphenyl)methyl]ethanamine (25B-NBOMe) in samples of tablets and blotter papers seized in Goiás State, Brazil. (author)

  11. Método para monitoramento de ninfas de cigarras e controle com inseticidas em reflorestamentos com paricá Method for monitoring nymphs of cicadas and control with insecticides in reforestations with paricá

    Directory of Open Access Journals (Sweden)

    Alexandre Mehl Lunz

    2010-07-01

    Full Text Available O objetivo deste trabalho foi estabelecer um método para o monitoramento da população de cigarras (Quesada gigas e para a avaliação da eficácia de doses de thiamethoxam, carbofuran e imidaclopride no controle de ninfas, em reflorestamento com paricá (Schizolobium parahyba var. amazonicum. Foram utilizadas as seguintes dosagens de inseticidas: 2,0, 4,0 e 6,0 kg ha-1 do produto comercial Actara (250 WG, para o princípio ativo thiamethoxan; 7,15, 14,30, 21,45 L ha-1 de Furadan (350 FS, para o carbofuran; e 4,5, 9,0, 13,5 L ha-1 de Provado (200 SC, para o imidaclopride. As três dosagens de cada produto foram aplicadas em área total. Foram realizadas três avaliações quinzenais, posteriores à aplicação, em que foram contabilizados os números de buracos e de ninfas vivas, por meio da abertura, com implemento tratorizado, de trincheiras com 7 m de comprimento, 0,8 m de largura e 0,07 m de profundidade. Todos os princípios ativos testados foram eficientes na redução da população de ninfas de Q. gigas, mas não houve efeito significativo das doses avaliadas. Os princípios ativos carbofuran e thiamethoxan são os mais promissores, com controle de 75-80% da infestação de ninfas. A abertura de trincheiras com o implemento tratorizado é eficaz no monitoramento da população de ninfas de Q. gigas, em reflorestamentos com paricá.The objective of this work was to establish a method for cicad (Quesada gigas population monitoring and for the evaluation of the effectiveness of thiamethoxam, carbofuran and imidacloprid doses on the control of cicad nymphs, in reforestation with paricá (Schizolobium parahyba var. amazonicum. The following insecticide doses were used: 2.0, 4.0, and 6.0 kg ha-1 of Actara (250 WG commercial product, for thiamethoxam active principle; 7.15, 14.30, and 21.45 L ha-1 of Furadan (350 FS, for carbofuran; 4.0, 9.0, and 13.5 L ha-1 of Provado (200 SC, for imidacloprid. The three doses of each product were applied in

  12. Local environments and lithium adsorption on the iron oxyhydroxides lepidocrocite (gamma-FeOOH) and goethite (alpha-FeOOH): A 2H-2 and 7Li solid-state MAS NMR study

    DEFF Research Database (Denmark)

    Nielsen, Ulla Gro; Grey, Clare P.; Paik, Jonkim

    2008-01-01

    2H and 7LiMAS NMR spectroscopy techniques were applied to study the local surface and bulk environments of iron oxyhydroxide lepiclocrocite (gamma-FeOOH). 2H variable-temperature (VT) MAS NMR experiments were performed, showing the presence of short-range, strong antiferromagnetic correlations......, even at temperatures above the Neel temperature, TN, 77 K. The formation of a Li+ inner-sphere complex on the surface of lepiclocrocite was confirmed by the observation of a signal with a large 7Li hyperfine shift in the 7Li  MAS NMR spectrum. The effect of pH and relative humidity (RH...

  13. Monitoramento de fatores de risco para doenças crônicas por entrevistas telefônicas

    Directory of Open Access Journals (Sweden)

    Monteiro Carlos Augusto

    2005-01-01

    Full Text Available OBJETIVO: Descrever métodos e resultados iniciais de sistema de monitoramento de fatores de risco para doenças crônicas não transmissíveis por meio de entrevistas telefônicas. MÉTODOS: Estudou-se amostra probabilística (n=2.122 da população adulta do Município de São Paulo residente em domicílios conectados à rede de telefonia fixa, com amostragem realizada em duas etapas: sorteio de linhas telefônicas e sorteio do morador do domicílio a ser entrevistado. Foi aplicado questionário para investigar características demográficas e socioeconômicas, padrão de alimentação e de atividade física, consumo de cigarros e de bebidas alcoólicas, peso e altura recordados e auto-referência a diagnóstico médico de hipertensão arterial e diabetes, entre outros quesitos. Foram calculadas estimativas sobre a prevalência de fatores de risco selecionados para doenças crônicas não transmissíveis para a população adulta com telefone e para a população adulta total do município. Neste último caso, população total, foram aplicados à amostra fatores de ponderação que levaram em conta diferenças demográficas e socioeconômicas entre a população com telefone e a população total do município. RESULTADOS: Foram observadas diferenças substanciais entre os sexos quanto à freqüência da maioria dos fatores de risco estudados, sendo significativamente mais freqüentes em homens o consumo insuficiente de frutas e hortaliças, o consumo excessivo de bebidas alcoólicas e o excesso de peso; e nas mulheres foram mais freqüentes o sedentarismo e a hipertensão. Possibilidades adicionais de estratificação da prevalência de fatores de risco permitidas pelo sistema de monitoramento foram ilustradas a partir de exemplos abrangendo faixa etária, nível de escolaridade e área de residência na cidade dos entrevistados. CONCLUSÕES: O desempenho do sistema de monitoramento, avaliado a partir da representatividade e confiabilidade

  14. MONITORAMENTO DAS ÁGUAS DO RIO MOSSORÓ/RN, NO PERÍODO DE ABRIL/2005 A JULHO/2006

    Directory of Open Access Journals (Sweden)

    Valdiery Silva de Araújo

    2007-12-01

    Full Text Available O trabalho tem por objetivo realizar uma comparação da qualidade físico-química e microbiológica entre três pontos de monitoramento do Rio Mossoró: Barragem do Genésio (utmx-681464; utmy-9422890, Barragem Central (utmx-683867; utmy-9425546 e Barragem Passagem de Pedra (utmx-690119; utmy-9429968 no município Mossoró/RN. Os pontos encontram-se sob diferentes influências antrópicas e foram monitorados no período de abril/2005 a julho/2006, sendo analisadas as seguintes variáveis: coliformes totais, coliformes termotolerantes, oxigênio dissolvido (OD, demanda química de oxigênio (DQO, nitrato, zinco, cobre, chumbo, cromo, mercúrio, cádmio, pH, temperatura, cor e turbidez. Além dessas análises, ainda houve outras variáveis como nitrogênio total, sólidos totais, fósforo total, demanda bioquímica de oxigênio (DBO que somadas as citadas serviram de base de cálculo para o Índice de Qualidade de Águas – IQA da primeira coleta de 2007 (10 de jan.. Embora à sazonalidade climática altere as concentrações dos contaminantes por intermédio da variação do volume do rio, a Barragem do Genésio, situada a montante da cidade, apresenta-se como o ponto de menor concentração das variáveis analisadas. A Barragem Central, localizada no centro da cidade, responde pelas maiores concentrações analisadas durante o período, resultado do lançamento de esgotos domésticos e industriais sem o devido tratamento. Outra característica observada nesse ponto é a proliferação anormal de macrófitas e algas, indicando o processo da eutrofização. Em termos de Índice de Qualidade das Águas, conclui-se que há diminuição da qualidade no sentido montante-jusante, embora o IQA da Barragem Central e Passagem de Pedra sejam semelhantes. PALAVRAS-CHAVE: Rio Mossoró. Monitoramento. Índice de Qualidade das Águas. Eutrofização. Autodepuração.

  15. E/Z MAS: An easy-to-use computerized materials control and accountability system

    International Nuclear Information System (INIS)

    Anderson, L.K.; Boor, M.G.; Hurford, J.M.; Landry, R.P.; Martinez, B.J.; Solem, A.M.; Whiteson, R.; Zardecki, A.

    1998-01-01

    Nuclear facilities that handle and process nuclear materials are required to track their nuclear holdings and to keep adequate records that manage and control the inventory of those holdings. The complexity of a system that does this job is directly proportional to the complexity of the facility's operations. This paper describes an approach to computerized materials protection, control, and accountability (MPC and A) that was introduced by Los Alamos National Laboratory (LANL) in the fall of 1997. This new system, E/Z MAS, is the latest addition to the LANL suite of computerized MPC and A tools, which also includes the CoreMAS system. E/Z MAS was initially designed to address the needs of those facilities that have small to modest MPC and A needs but has been expanded to provide full functionality for any facility. The system name, E/Z MAS, reflects the system's easy-to-use characteristics, which include ease of installation and ease of software maintenance. Both CoreMAS and E/Z MAS have been provided to facilities in the Former Soviet Union to assist them in implementing a computerized MPC and A system that meets their needs. In this paper the authors will address the functionality of CoreMAS and E/Z MAS, and an argument in favor of intranet-based material control and accountability will be advanced

  16. Evidence for Heterodimerization and Functional Interaction of the Angiotensin Type 2 Receptor and the Receptor MAS

    DEFF Research Database (Denmark)

    Leonhardt, Julia; Villela, Daniel C.; Teichmann, Anke

    2017-01-01

    The angiotensin type 2 receptor (AT2R) and the receptor MAS are receptors of the protective arm of the renin-angiotensin system. They mediate strikingly similar actions. Moreover, in various studies, AT2R antagonists blocked the effects of MAS agonists and vice versa. Such cross-inhibition may in...

  17. Angiotensin-(1-7)/Mas axis modulates fear memory and extinction in mice.

    Science.gov (United States)

    Lazaroni, Thiago Luiz do Nascimento; Bastos, Cristiane Perácio; Moraes, Márcio Flávio Dutra; Santos, Robson Souza; Pereira, Grace Schenatto

    2016-01-01

    Inappropriate defense-alerting reaction to fear is a common feature of neuropsychiatric diseases. Therefore, impairments in brain circuits, as well as in molecular pathways underlying the neurovegetative adjustments to fear may play an essential role on developing neuropsychiatric disorders. Here we tested the hypothesis that interfering with angiotensin-(1-7) [Ang-(1-7)]/Mas receptor axis homeostasis, which appears to be essential to arterial pressure control, would affect fear memory and extinction. Mas knockout (MasKO) mice, in FVB/N background, showed normal cued fear memory and extinction, but increased freezing in response to context. Next, as FVB/N has poor performance in contextual fear memory, we tested MasKO in mixed 129xC57BL/6 background. MasKO mice behaved similarly to wild-type (WT), but memory extinction was slower in contextual fear conditioning to a weak protocol (1CS/US). In addition, delayed extinction in MasKO mice was even more pronounced after a stronger protocol (3CS/US). We showed previously that Angiotensin II receptor AT1 antagonist, losantan, rescued object recognition memory deficit in MasKO mice. Here, losartan was also effective. Memory extinction was accelerated in MasKO mice after treatment with losartan. In conclusion, we showed for the first time that Ang-(1-7)/Mas axis may modulate fear memory extinction. Furthermore, we suggest MasKO mice as an animal model to study post-traumatic stress disorder (PTSD). Copyright © 2015 Elsevier Inc. All rights reserved.

  18. Avaliação do sistema de monitoramento computadorizado de digestão in vitro: 1. Testes preliminares

    Directory of Open Access Journals (Sweden)

    Campos Fábio Prudêncio de

    2000-01-01

    Full Text Available O objetivo deste trabalho foi testar o sistema de monitoramento computadorizado da produção de gás in vitro. Essa técnica facilita estudos da degradação das frações solúveis e insolúveis das forragens, quantificadas pela produção de gás (CO2 e CH4 oriunda do metabolismo microbiano e medida por sensor de pressão. Diversas quantidades de amostras (50 a 110 mg de feno de alfafa e outros alimentos foram testadas. Também, a influência da quantidade de líquido ruminal (2,0 ou 3,0 mL, com ou sem barras magnéticas agitadoras nos frascos incubatórios, na digestibilidade de 100 mg de feno de alfafa, foi estudada. A quantidade de 100 mg de amostra, 2,0 mL de líquido ruminal e sem barra magnética agitadora, proporcionou os menores coeficientes de variação na produção de gás. Em conclusão, 2,0 mL de líquido ruminal, sem barra e com 100 mg de amostra, apresentaram maior precisão na curva de digestão.

  19. Monitoramento de interações farmacocinéticas entre plantas medicinais e fitoterápicos e os medicamentos convencionais pelo sistema de farmacovigilância brasileiro

    Directory of Open Access Journals (Sweden)

    André Luís Dias Araujo MAZZARI

    2014-12-01

    Full Text Available O consumo de plantas medicinais e fitoterápicos está cada vez mais em expansão pelo mundo. Contudo, os fitoterápicos, como qualquer xenobiótico, podem causar alterações farmacocinéticas no organismo, ocasionando distúrbios nos metabolismos de fase 1 e fase 2, devido à inibição ou indução de enzimas metabólicas. Em caso de coadministração de plantas medicinais e/ou fitoterápicos com medicamentos convencionais, poderá haver interações que comprometem a eficácia do último, ocasionando uma falha terapêutica. Como ensaios pré-clínicos farmacocinéticos não são uma exigência regulatória para que um medicamento fitoterápico seja registrado, os casos de interações com fármacos convencionais (Herb-Drug Interactions - HDI acabam sendo revelados somente na fase de pós- -comercialização, ou seja, pelos sistemas de farmacovigilância. Inúmeros países já reportaram casos de HDI através de seus respectivos centros de farmacovigilância à Organização Mundial de Saúde (OMS, mas até o momento, o Brasil não reportou nenhum oficialmente. Além disso, durante os primeiros 10 anos de monitoramento, nenhum caso de HDI envolvendo plantas medicinais brasileiras foi apresentado. Sabe-se que aproximadamente 90% da população brasileira fazem uso de plantas medicinais e fitoterápicos, e que casos de HDI podem estar acontecendo sem serem percebidos e/ou notificados. Para que este cenário mude, é necessário que se adote medidas que visem ao estímulo do profissional de saúde à comunicação de suspeita de HDI para o centro de farmacovigilância, bem como a educação continuada destes profissionais, com a inclusão de especialistas em medicina tradicional no sistema de saúde, além de campanhas de prevenção à automedicação de plantas medicinais e fitoterápicos pela população, que atualmente não é praticado no Brasil.

  20. Residue specific hydration of primary cell wall potato pectin identified by solid-state 13C single-pulse MAS and CP/MAS NMR spectroscopy

    DEFF Research Database (Denmark)

    Larsen, Flemming Hofmann; Chrestensen, Inge Byg; Damager, Iben

    2011-01-01

    Hydration of rhamnogalacturonan-I (RG-I) derived from potato cell wall was analyzed by 13C single-pulse (SP) magic-angle-spinning (MAS) and 13C cross-polarization (CP) MAS nuclear magnetic resonance (NMR) and supported by 2H SP/MAS NMR experiments. The study shows that the arabinan side chains...... hydrate more readily than the galactan side chains and suggests that the overall hydration properties can be controlled by modifying the ratio of these side chains. Enzymatic modification of native (NA) RG-I provided samples with reduced content of arabinan (sample DA), galactan (sample DG), or both side...... chains (sample DB). Results of these samples suggested that hydration properties were determined by the length and character of the side chains. NA and DA exhibited similar hydration characteristics, whereas DG and DB were difficult to hydrate because of the less hydrophilic properties of the rhamnose...

  1. Hydronephrosis alters cardiac ACE2 and Mas receptor expression in mice.

    Science.gov (United States)

    Zhang, Yanling; Ma, Lulu; Wu, Junyan; Chen, Tingting

    2015-06-01

    Hydronephrosis is characterized by substantial loss of tubules and affects renin secretion in the kidney. However, whether alterations of angiotensin-converting enzyme (ACE), ACE2 and Mas receptor in the heart are observed in hydronephrosis is unknown. Thus, we assessed these components in hydronephrotic mice treated with AT1 receptor blockade and ACE inhibitor. Hydronephrosis was induced by left ureteral ligation in Balb/C mice except sham-operated animals. The levels of cardiac ACE, ACE2 and Mas receptor were measured after treatment of losartan or enalapril. Hydronephrosis led to an increase of ACE level and a decrease of ACE2 and Mas receptor in the heart. Losartan decreased cardiac ACE level, but ACE2 and Mas receptor levels significantly increased in hydronephrotic mice (p Hydronephrosis increased cardiac ACE and suppressed ACE2 and Mas receptor levels. AT1 blockade caused sustained activation of cardiac ACE2 and Mas receptor, but ACE inhibitor had the limitation of such activation of Mas receptor in hydronephrotic animals. © The Author(s) 2015.

  2. PENGEMBANGAN EKOWISATA BERBASIS KERAKYATAN DI BANJAR NYUH KUNING, DESA MAS, UBUD

    Directory of Open Access Journals (Sweden)

    AGUNG SRI SULISTYAWATI

    2015-06-01

    Full Text Available The objective of this study is (1 to identify the potential of Banjar Nyuh Kuning Mas Village, Ubud has to offer as means of attraction in ecotourism which may be accomplished by identifying physical and non physical potential. (2 to develope a community based strategy in ecotourism. The sampling technique used is purposive sampling and accidental sampling. Data collection is accomplished through observatioan, questionaire, focus group discussion and documentation. Data analysis is by qualitative descriptive and SWOT. The result of this study is that Banjar Nyuh Kuning has the potential to be developed as an ecotourism on the basis of physical and non physical grounds. The perception of the community and tourists are in agreement to the developement of ecotourism activity which incorporate local community, nature oriented activity and has the potential to increase their income, thus resulting in a destination for leisure and recreation. There are a few results of alternative strategies such as; development strategies of ecotourism products, development strategies of human resources, development strategies of management and strategies in upgrading security. To make Banjar Nyuh Kuning as an attraction for ecotourism activity which is based on nature then the strategy for development has to be efficient and limited. Further study has to be taken for the marketing aspect and managing ecotourism object to further the developent in a comprehensive manner.

  3. Molybdenum modified phosphate glasses studied by 31P MAS NMR and Raman spectroscopy.

    Science.gov (United States)

    Szumera, Magdalena

    2015-02-25

    Glasses have been synthesized in the system P2O5-SiO2-K2O-MgO-CaO modified by addition of MoO3. Glasses were prepared by conventional fusion method from 40 g batches. The influence of Mo-cations on the analysed glass structure was investigated by means of Raman and (31)P MAS-NMR techniques. It has been found that molybdate units can form Mo[MoO4/MoO6]-O-P and/or Mo[MoO4/MoO6]-O-Si bonds with non-bridging oxygens atoms of Q2 methaphosphate units, resulting in the transformation of chain methaphosphate structure into pyrophosphate and finally into orthophosphate structure. It has been also found that increasing amount of MoO3 in the structure of investigated glasses causes their gradual depolymerization and molybdenum ions in the analysed glass matrix act as modifying cations. Copyright © 2014 Elsevier B.V. All rights reserved.

  4. Renewable energy sources monitoring systems; Sistema de monitoramento de fontes de energias renovaveis

    Energy Technology Data Exchange (ETDEWEB)

    Souza, Teofilo Miguel de; Canto, Mario Afonso Ribeiro do [Universidade Estadual Paulista (UNESP), Guaratingueta, SP (Brazil). Centro de Energias Renovaveis], e-mail: teofilo@feg.unesp.br

    2004-07-01

    The development of techniques and products for use of sources of energy renewed it depends on economic and technical parameters that result of revenue analyses and acting for its improvement. With the objective of to provide and to facilitate the access the information on the future acting of products and techniques of generation of energy of alternative sources and you renewed of energy, it was developed a collection project and storage of data of reduced cost and of facilitated visualization. The system developed in platform of software LabView controls a system of acquisition of data through interface RS-232 and it stores the data in files Excel or Files text, depending on the application type. The system of acquisition of data consists of a circuit of conditioning of analogic signs for digital signs, a control circuit and a circuit of communication type interface serial asynchronous RS-232. (author)

  5. Variação local na composição da comunidade de aves no Parque Estadual Carlos Botelho, São Miguel Arcanjo – SP e proposta para o monitoramento do impacto do ecoturismo. Local variation in bird communities composition at Carlos Botelho State Park, São Miguel Arcanjo – SP, Southeastern Brazil and proposals for monitoring the impact of ecotourism.

    Directory of Open Access Journals (Sweden)

    Bruna Gonçalves da SILVA

    2010-12-01

    Full Text Available Como todas as atividades humanas, o ecoturismo apresenta o potencial de impactar negativamente o meio ambiente, necessitando ser monitorado e manejado. As aves podem ser incluídas em protocolos de monitoramento desse impacto, porém devem ser considerados outros fatores que influenciam a composição das comunidades de aves antes de se propor tais protocolos. Dentre estes se destaca a influência da heterogeneidade estrutural da vegetação sobre a distribuição e a abundância das aves. Os objetivos deste trabalho foram: verificar como esse fator atua localmente numa área de Mata Atlântica sob uso público e propor um protocolo de monitoramento de impacto dessa atividade que utilize as aves como indicadores. A avifauna foi amostrada ao longo de duas trilhas, uma na qual o turismo é monitorado e outra sob o sistema autoguiado. A heterogeneidade estrutural ao longo dessas trilhas foi avaliada, e as duas comunidades de aves comparadas em relação à riqueza, composição de espécies, abundância relativa, diversidade e estrutura trófica. Foram utilizados os métodos de pontos de escuta e o de pontos quadrantes. As trilhas diferiram significativamente na maioria dos parâmetros de estrutura da vegetação analisados e na composição de espécies de aves, mas não nos demais parâmetros considerados para a avifauna. Dezessete espécies apresentaram abundância relativa significativamente diferente entre as áreas e, destas, seis relacionadas a parâmetros estruturais da vegetação. Propõe-se a avaliação do impacto do uso público sobre a avifauna em cada uma das trilhas através do monitoramento da abundância relativa das espécies considerando possíveis alterações estruturais na vegetação local e o monitoramento de 15 espécies de fácil detecção e que não diferiram significativamente em abundância relativa entre as trilhas.Like all human activities, ecotourism has the potential to negatively impact the environment and need

  6. Smoke, Clouds and Radiation Brazil NASA ER-2 Moderate Resolution Imaging Spectrometer (MODIS) Airborne Simulator (MAS) Data

    Data.gov (United States)

    National Aeronautics and Space Administration — SCARB_ER2_MAS data are Smoke, Clouds and Radiation Brazil (SCARB) NASA ER2 Moderate Resolution Imaging Spectrometer (MODIS) Airborne Simulator (MAS)...

  7. Indicadores da Qualidade do Substrato para Monitoramento de Áreas de Mineração Revegetadas

    Directory of Open Access Journals (Sweden)

    Raquel Olimpia Peláez Ocampo Almeida

    Full Text Available Um procedimento para monitoramento e obtenção de indicadores para avaliação da recuperação ambiental de áreas mineradas foi desenvolvido e testado. Quatro bacias de disposição de rejeitos de mineração de areia industrial revegetadas em épocas distintas constituíram uma cronossequência de 14 anos que possibilitou a observação das mudanças das características físicas e químicas do substrato e o estabelecimento de relações com parâmetros de crescimento da vegetação. Uma análise de covariâncias multivariada entre os indicadores identificou a densidade de solo, teores de matéria orgânica e fósforo e pH como os mais apropriados para avaliar a qualidade do substrato e para atuarem como indicadores de resultados de ações de recuperação das bacias estudadas. Esse procedimento mostrou-se um instrumento de fácil aplicação para o acompanhamento da evolução da recuperação ambiental e para a obtenção de parâmetros quantitativos que facilitem a avaliação dos resultados das ações de recuperação.

  8. Prospecção e monitoramento informacional no processo de inteligência competitiva Information scanning and information mining in the process of competitive intelligence

    Directory of Open Access Journals (Sweden)

    Marta Lígia Pomim Valentim

    2004-01-01

    Full Text Available A prospecção e o monitoramento informacional são atividades base para a inteligência competitiva, entendida como um processo dinâmico, composto pela gestão da informação e pela gestão do conhecimento. O processo de inteligência competitiva (I. C. nas organizações ocorre a partir de diferentes atividades informacionais, dentre elas estão as ligadas a prospecção e ao monitoramento. O papel destas atividades é essencial, pois alimentam todo o processo com dados, informação e conhecimento, constroem diversas estruturas formais e informais de informação dentro da organização, além do que, as atividades de prospecção e monitoramento geram serviços e produtos informacionais sistematizados, com alto valor agregado.The information scanning and information mining are activities base for the competitive intelligence, understood as a dynamic process, composed by the information management and knowledge management. The process of competitive intelligence (I. C. in the organizations it happens starting from different informational activities, they are the tied up ones information scanning and information mining. The function of these activities is essential, because they feed the whole process with data, information and knowledge, they build several formal structures and you inform inside of information of the organization, in addition, the information scanning and information mining activities generate information services and products systematized, with high value aggregate.

  9. MONITORAMENTO DA QUALIDADE DA ÁGUA DO RIO CAVEIRAS NO PLANALTO SERRANO DE SANTA CATARINA COM SUPORTE DE TECNOLOGIAS DE GEOMÁTICA

    Directory of Open Access Journals (Sweden)

    Sílvio Luís Luís Rafaeli Neto

    2013-04-01

    Full Text Available O monitoramento da qualidade da água em bacias hidrográficas possui forte componente espacial, uma vez que os locais de monitoramento distribuem-se no espaço geográfico. Em se tratando de bacias, em que o talvegue principal se estende por dezenas de quilômetros, há que se utilizar tecnologias de suporte ao planejamento dos locais de amostragem, definição de rotas de acesso e estudo do uso e da ocupação do solo como forma de subsidiar o processo de análise dos resultados. O rio Caveiras está situado na região serrana de Santa Catarina com uma bacia hidrográfica com cerca de 2400 km2. A jusante do seu terço superior, destaca-se a captação de água para o abastecimento da cidade de Lages, seguida de uma Pequena Central Hidrelétrica (PCH com cerca de 2 MW de potência instalada. Em breve, serão construídas mais três PCHs a jusante da existente, formandouma sequência de quatro ambientes lênticos. Este trabalho tem por objetivo apresentar um estudo de caso de aplicação de tecnologias de Geomática no monitoramento da qualidade da água do rio Caveiras antes da construção das PCHs, como subsídio à avaliação dos impactos ambientais destes empreendimentos.

  10. Desenvolvimento da compreensão leitora através do monitoramento da leitura Improving reading comprehension by developing monitoring strategies

    Directory of Open Access Journals (Sweden)

    Carmen Lucia Göbel Coelho

    2010-01-01

    Full Text Available Este estudo teve como objetivo examinar o progresso da compreensão leitora através do desenvolvimento da habilidade de monitoramento a partir do emprego do paradigma de detecção de erros. Adolescentes distribuídos nos grupos experimental e controle realizaram as tarefas de monitoramento e leitura (teste de Cloze como pré-teste e pós-teste, tendo sido controladas: habilidade verbal, atenção e memória de trabalho. Os grupos não diferiram em suas habilidades lingüístico-cognitivas, nem em seu desempenho nas tarefas do pré-teste. Após a intervenção, o grupo experimental foi significativamente melhor do que o grupo controle nas tarefas de leitura e de monitoramento. Tais evidências sugerem que o progresso no desenvolvimento da compreensão de texto está relacionado à eficiência com que os adolescentes monitoram sua leitura.The present study examines whether the development of monitoring strategies improves textual comprehension skills using an error detection methodology for checking it. Adolescents distributed into experimental and control groups were presented to the monitoring and cloze tasks of pre- and post-tests where tasks like verbal ability, attention and working memory were controlled. The experimental and control groups did not differ in their linguistic-cognitive abilities or in their performance in the pre-test tasks. However, the performance of the experimental group was significantly better than the control group in the reading and monitoring tasks carried out after the intervention. The evidences found in this study suggest that text comprehension can be improved by the efficiency adolescents monitor their reading process.

  11. Multinuclear MAS NMR studies on coked zeolites H-ZSM-5

    International Nuclear Information System (INIS)

    Ernst, H.; Freude, D.; Hunger, M.; Pfeifer, H.

    1991-01-01

    During the cracking process carbonaceous materials are deposited on the outer or inner surface of the catalyst. These deposits are in many cases the main cause of catalyst deactivation. Magic angle spinning (MAS) NMR investigations and catalytic n-hexane cracking were carried out on H-ZSM-5 zeolites after a mild hydrothermal de-alumination. By 13 C CP MAS NMR it could be shown that the enhanced catalytic activity does not enhance the coke formation and that the chemical nature of these deposits is essentially aromatic. From 1 H MAS NMR studies performed on shallow-bed activated sealed samples and 27 Al and 29 Si MAS NMR on rehydrated samples it follows that for high coke concentrations the catalyst deactivation is caused mainly by blocking of Broensted acid sites. (author). 27 refs.; 3 figs.; 2 tabs

  12. 48 CFR 538.270 - Evaluation of multiple award schedule (MAS) offers.

    Science.gov (United States)

    2010-10-01

    ... SERVICES ADMINISTRATION SPECIAL CATEGORIES OF CONTRACTING FEDERAL SUPPLY SCHEDULE CONTRACTING Establishing and Administering Federal Supply Schedules 538.270 Evaluation of multiple award schedule (MAS) offers... determining the Government's price negotiation objectives, consider the following factors: (1) Aggregate...

  13. FAUNA DE FORMIGAS COMO FERRAMENTA PARA MONITORAMENTO DE ÁREA DE MINERAÇÃO REABILITADA NA ILHA DA MADEIRA, ITAGUAÍ, RJ

    OpenAIRE

    Pereira, Marcos Paulo dos Santos; Queiroz, Jarbas Marçal; Valcarcel, Ricardo; Mayhé-Nunes, Antônio José

    2007-01-01

    RESUMO A riqueza e diversidade de espécies de formigas podem ser maiores em ambientes de complexidade mais elevada devido a uma maior disponibilidade de nichos presentes. Em razão da conexão entre os organismos e as características dos habitats, as formigas têm sido utilizadas como ferramentas no monitoramento ambiental de áreas perturbadas. Neste estudo, foi investigada a estrutura da comunidade de formigas em parcelas utilizadas para reabilitação de uma área de mineração na Ilha da Madeira,...

  14. Desenvolvimento de uma rede de sensores sem fio aplicada no monitoramento da variabilidade térmica em casas de vegetação

    OpenAIRE

    Barbosa, Rogério Zanarde [UNESP

    2015-01-01

    Este é um trabalho de tecnologia computacional aplicada na área agrícola, cujo objetivo principal do trabalho é desenvolver uma rede de sensores sem fio, que envolve aspectos de software e hardware, para o monitoramento térmico no interior de uma casa de vegetação. Além da rede propriamente dita, o trabalho também inclui a sua aplicação no levantamento quantitativo da variabilidade térmica na casa de vegetação o que pode ser aplicado em diversas atividades agrícolas a serem desenvolvidas no i...

  15. Monitoramento eletrônico de presos no RS: uma leitura bakhtiniana do discurso do gênero reportagem na esfera jornalística

    OpenAIRE

    Rosa, Renata Faria Amaro da Silva da

    2015-01-01

    Este trabalho propõe uma análise de construção dos sentidos do discurso em reportagens sobre o monitoramento eletrônico de presos no Rio Grande do Sul (RS), a partir da análise de discursos impressos no Jornal Zero Hora (ZH) entre os meses de janeiro e maio do ano de 2013, na perspectiva da Teoria da Enunciação de Bakhtin e seu Círculo. A pesquisa, fundamentada na teoria dialógica bakhtiniana, de forma mais específica, busca identificar vozes discursivas que compõem o discurso, reconhecer ele...

  16. MAS Integration and Controllership Effectiveness: Evidence of a Preparer-User Perception Gap

    OpenAIRE

    Weißenberger, Barbara E.; Angelkort, Hendrik; Holthoff, Gero

    2012-01-01

    Recent evidence suggests that managers establish a positive link between management accounting system (MAS) integration and controllership effectiveness, which is fully mediated by the perceived consistency of financial language. Our paper extends this research by analyzing whether controllers have similar perceptions on MAS design. Testing a series of multi-group structural equation models, we find evidence for a preparer-user perception gap with respect to the mediating impact of a consiste...

  17. MONITORAMENTO DE AVICULTURA A PARTIR DE TÉCNICAS DE VISÃO COMPUTACIONAL

    Directory of Open Access Journals (Sweden)

    Alyne Yumi Kodama Saltoratto

    2013-12-01

    Full Text Available To get a poultry farming with good incomes, it is necessary to constant monitoring by the producer, where the issues related to animal welfare should be seen as an economic benefit and not a requirement. With the great advances in computing and with current capacity of image processing, it is possible based on frames from videos, to extract sufficient data to provide monitoring of chicken (chicks. Therefore, this work presents a tool for monitoring of aviculture from frame images from videos. In the proposed methodology of this research, techniques were applied to reduce the brightness (intensity of the image as well as mathematical morphology and flooding algorithm as some of the procedures applied to images. Monitoring data of chicken, generated by analysis of the images, proved satisfactory in determining the frequency to stay in certain locations of the creation places.

  18. 1H HR-MAS NMR Spectroscopy and the Metabolite Determination of Typical Foods in Mediterranean Diet

    Directory of Open Access Journals (Sweden)

    Carmelo Corsaro

    2015-01-01

    Full Text Available NMR spectroscopy has become an experimental technique widely used in food science. The experimental procedures that allow precise and quantitative analysis on different foods are relatively simple. For a better sensitivity and resolution, NMR spectroscopy is usually applied to liquid sample by means of extraction procedures that can be addressed to the observation of particular compounds. For the study of semisolid systems such as intact tissues, High-Resolution Magic Angle Spinning (HR-MAS has received great attention within the biomedical area and beyond. Metabolic profiling and metabolism changes can be investigated both in animal organs and in foods. In this work we present a proton HR-MAS NMR study on the typical vegetable foods of Mediterranean diet such as the Protected Geographical Indication (PGI cherry tomato of Pachino, the PGI Interdonato lemon of Messina, several Protected Designation of Origin (PDO extra virgin olive oils from Sicily, and the Traditional Italian Food Product (PAT red garlic of Nubia. We were able to identify and quantify the main metabolites within the studied systems that can be used for their characterization and authentication.

  19. Genotyping-by-sequencing (GBS), an ultimate marker-assisted selection (MAS) tool to accelerate plant breeding.

    Science.gov (United States)

    He, Jiangfeng; Zhao, Xiaoqing; Laroche, André; Lu, Zhen-Xiang; Liu, HongKui; Li, Ziqin

    2014-01-01

    Marker-assisted selection (MAS) refers to the use of molecular markers to assist phenotypic selections in crop improvement. Several types of molecular markers, such as single nucleotide polymorphism (SNP), have been identified and effectively used in plant breeding. The application of next-generation sequencing (NGS) technologies has led to remarkable advances in whole genome sequencing, which provides ultra-throughput sequences to revolutionize plant genotyping and breeding. To further broaden NGS usages to large crop genomes such as maize and wheat, genotyping-by-sequencing (GBS) has been developed and applied in sequencing multiplexed samples that combine molecular marker discovery and genotyping. GBS is a novel application of NGS protocols for discovering and genotyping SNPs in crop genomes and populations. The GBS approach includes the digestion of genomic DNA with restriction enzymes followed by the ligation of barcode adapter, PCR amplification and sequencing of the amplified DNA pool on a single lane of flow cells. Bioinformatic pipelines are needed to analyze and interpret GBS datasets. As an ultimate MAS tool and a cost-effective technique, GBS has been successfully used in implementing genome-wide association study (GWAS), genomic diversity study, genetic linkage analysis, molecular marker discovery and genomic selection under a large scale of plant breeding programs.

  20. Emprego de estações totais robotizadas na automação, controle e aquisição de dados, voltado ao monitoramento de barragens

    Directory of Open Access Journals (Sweden)

    Marco Aurélio Debus Nadal

    2017-02-01

    Full Text Available Atualmente com a evolução do instrumental utilizado em levantamentos geodésicos, especialmente no que diz respeito a robotização de estações totais, é possível a utilização destes em monitoramento geodésico contínuo, principalmente em estruturas de grande porte. No presente trabalho foi abordada a maneira de se estabelecer comunicação e controle destes instrumentos de medição através do desenvolvimento de programas que permitiram o envio e o recebimento de dados, em uma comunicação entre a estação total robotizada e o computador. Foram testadas as interfaces de comunicação que o instrumento utilizado neste trabalho, dentre elas: conexão via cabo serial, Bluetooth®, e link de rádio. Também foi estudado o protocolo de comunicação específico para este instrumento, disponibilizado pelo fabricante. O objetivo foi o desenvolvimento de um programa de computador que permitisse o controle de uma estação total robotizada Leica TCRA1205, voltado a aplicações de monitoramento geodésico.

  1. A inovação tecnológica como ferramenta para monitoramento da saúde dos trabalhadores de enfermagem

    Directory of Open Access Journals (Sweden)

    Patrícia Campos Pavan Baptista

    2011-12-01

    Full Text Available O objetivo do estudo é descrever o processo de construção do software Sistema de Monitoramento da Saúde dos Trabalhadores de Enfermagem, uma inovação tecnológica desenvolvida para captar os agravos à saúde dos trabalhadores de enfermagem e os determinantes potenciais de desgaste e/ou fortalecimento, monitorando a saúde por meio de indicadores. O desenvolvimento do software englobou as fases de definição do objetivo, escolha do referencial teórico, estruturação do conteúdo e desenvolvimento da arquitetura do sistema. Considera-se importante a socialização deste processo aos pequisadores, gerentes e trabalhadores interessados na temática, uma vez que o monitoramento da situação de saúde dos trabalhadores de enfermagem é uma ação indispensável para o planejamento de estratégias que possam minimizar a ocorrência dos acidentes e das doenças ocupacionais, promovendo melhoria das condições de trabalho e qualidade de vida.

  2. MONITORAMENTO DOS PARÂMETROS FÍSICO-QUÍMICOS NA COMPOSTAGEM DE RESÍDUOS AGROINDUSTRIAIS

    Directory of Open Access Journals (Sweden)

    Talita Dantas Pedrosa

    2013-11-01

    Full Text Available Os processos de compostagem têm se estabelecido como formas eficientes de minimizar a problemática ambiental e de reduzir o volume de resíduos sólidos orgânicos descartados. Esse trabalho tem como objetivos monitorar o processo de compostagem de resíduos agroindustriais e avaliar a qualidade do composto final com base na Portaria N° 01/83 do Ministério da Agricultura, Pecuária e Abastecimento. Para  isso foram montadas  pilhas  de resíduos agroindustriais em solo exposto com monitoramento dos parâmetros: temperatura, pH, sólidos voláteis, umidade e relação C/N. Ao final da compostagem  foi avaliado a qualidade do composto produzido, o qual  alcançou parcialmente os requisitos mínimos exigidos pela legislação brasileira, mostrando-se eficiente para o tratamento de resíduos agroindustriais.Palavra-chave: resíduos orgânicos, matéria orgânica, meio ambiente.MONITORING OF PHYSICAL AND CHEMICAL PARAMETERS IN AGROINDUSTRIAL WASTE COMPOSTING ABSTRACTThe composting processes have been established as an effective way to minimize the environmental problems and reduce the volume of organic solid waste disposed. This study aimed to monitor the composting process of agroindustrial wastes and evaluate the final product quality. For this were assembled stacks of agroindustrial residues in exposed soil to monitoring the parameters as: temperature, pH, volatile solids, moisture and C/N ratio. At the end of composting was rated the quality of the produced compost  and its partially achieved the minimum required by Brazilian law, being effective for the treatment of industrial residues.Keywords: organic waste, organic matter, environmental. DOI: http://dx.doi.org/10.14583/2318-7670.v01n01a08

  3. Neuroprotective Mechanisms of the ACE2-Angiotensin-(1-7)-Mas Axis in Stroke

    DEFF Research Database (Denmark)

    Bennion, Douglas M; Haltigan, Emily; Regenhardt, Robert W

    2015-01-01

    The discovery of beneficial neuroprotective effects of the angiotensin converting enzyme 2-angiotensin-(1-7)-Mas axis [ACE2-Ang-(1-7)-Mas] in ischemic and hemorrhagic stroke has spurred interest in a more complete characterization of its mechanisms of action. Here, we summarize findings that desc......The discovery of beneficial neuroprotective effects of the angiotensin converting enzyme 2-angiotensin-(1-7)-Mas axis [ACE2-Ang-(1-7)-Mas] in ischemic and hemorrhagic stroke has spurred interest in a more complete characterization of its mechanisms of action. Here, we summarize findings...... that describe the protective role of the ACE2-Ang-(1-7)-Mas axis in stroke, along with a focused discussion on the potential mechanisms of neuroprotective effects of Ang-(1-7) in stroke. The latter incorporates evidence describing the actions of Ang-(1-7) to counter the deleterious effects of angiotensin II...... complete understanding of the mechanisms of action of Ang-(1-7) to elicit neuroprotection will serve as an essential step toward research into potential targeted therapeutics in the clinical setting....

  4. A software framework for analysing solid-state MAS NMR data

    International Nuclear Information System (INIS)

    Stevens, Tim J.; Fogh, Rasmus H.; Boucher, Wayne; Higman, Victoria A.; Eisenmenger, Frank; Bardiaux, Benjamin; Rossum, Barth-Jan van; Oschkinat, Hartmut; Laue, Ernest D.

    2011-01-01

    Solid-state magic-angle-spinning (MAS) NMR of proteins has undergone many rapid methodological developments in recent years, enabling detailed studies of protein structure, function and dynamics. Software development, however, has not kept pace with these advances and data analysis is mostly performed using tools developed for solution NMR which do not directly address solid-state specific issues. Here we present additions to the CcpNmr Analysis software package which enable easier identification of spinning side bands, straightforward analysis of double quantum spectra, automatic consideration of non-uniform labelling schemes, as well as extension of other existing features to the needs of solid-state MAS data. To underpin this, we have updated and extended the CCPN data model and experiment descriptions to include transfer types and nomenclature appropriate for solid-state NMR experiments, as well as a set of experiment prototypes covering the experiments commonly employed by solid-sate MAS protein NMR spectroscopists. This work not only improves solid-state MAS NMR data analysis but provides a platform for anyone who uses the CCPN data model for programming, data transfer, or data archival involving solid-state MAS NMR data.

  5. Escala de atitudes frente ao dinheiro (MAS: Teste de modelos e poder preditivo

    Directory of Open Access Journals (Sweden)

    Carlos Eduardo Pimentel

    2012-01-01

    Full Text Available The social importance attached to money and its role as an important motivator of behavior justifies the study of its psychosocial aspects. But there is a lack of studies concerning attitudinal or psychological aspects of money in Brazil. In order to encourage research in this context, the validity of the Money Attitudes Scale (MAS was tested using confirmatory factor approaches. Results supported a brief 16-items version of the scale and replicated the factor analytic pattern with satisfactory internal consistency for the factors of power, retention, distrust, and anxiety. Age differences were observed regarding money attitudes of power, and the predictive role of the MAS to account for consumer behavior was also confirmed. This version of the MAS shows evidences of factorial validity and reliability, justifying its use in future research.

  6. Development of a generic, computerized nuclear material accountability system: NucMAS

    International Nuclear Information System (INIS)

    Cornell, M.D.; O'Leary, J.M.

    1987-01-01

    The application NucMAS provides basic computerized accountability functions for the Savannah River Plant (SRP) Separations Department Material Balance Areas (MBA's). These functions include data entry, data management, calculations, and report generation. NucMAS can be used both for routine reporting to the SRP central Material Control and Accounting (MC and A) system and for rapid ad hoc queries in emergency situations. The system is designed to work with any process handling one or more of the 17 accountable nuclear materials specified by the Department of Energy (DOE). It relies on user-supplied configuration data to drive data prompts, report headings, data validations, and calculations

  7. Microbiological monitoring of clean rooms in development of vaccines Monitoramento microbiológico de áreas classificadas em desenvolvimento de vacinas

    Directory of Open Access Journals (Sweden)

    Carla Lílian de Agostini Utescher

    2007-12-01

    Full Text Available The aim of the present work was to evaluate an environmental monitoring program for clean rooms, or classified environments, involved in the filling and quality control of biological products produced by Butantan Institute, São Paulo, Brazil. This monitoring established the quantification, characterization and seasonality of the microorganisms in air and operators and, moreover, determined the alert and action limits. The total detectable microbial number showed some contrasts in installed air purification systems and in the operational impact on adopted procedures. The typical microbial population consisted of Staphylococcus sp, Micrococcus sp, Bacillus sp and Penicillium sp. The highest microorganism concentration occurred during summer and springtime. The established internal alert and action limits supported the operational procedures. Therefore, the environmental monitoring program is recommended for other laboratories involved in the production of vaccines, hyperimmune sera and biopharmaceuticals.O presente trabalho teve por objetivo avaliar um programa de monitoramento microbiológico ambiental para áreas limpas, ou ambientes classificados, envolvidas na produção, envasamento e controle dos imunobiológicos produzidos pelo Instituto Butantan. Este monitoramento permitiu a quantificação, a caracterização e a sazonalidade da população microbiana presente no ar e nos operadores, e a determinação dos limites de alerta e ação. O número total de bactérias detectáveis revelou diferenças nos sistemas de purificação de ar instalados e o impacto operacional ocasionado pelos procedimentos realizados. A população microbiana característica foi composta por bactérias dos gêneros Staphylococcus sp, Micrococcus sp, Bacillus sp e por fungos filamentosos do gênero Penicillium sp. A maior concentração de microrganismos ocorreu nos períodos de verão e primavera. Os limites internos de alerta e ação estabelecidos asseguram os

  8. Monitoramento e prevenção do supertreinamento em atletas Monitorización y prevención del superentrenamiento en atletas Monitoring and prevention of overtraining in athletes

    Directory of Open Access Journals (Sweden)

    Rodrigo Nascimento Alves

    2006-10-01

    Full Text Available O supertreinamento é caracterizado pelo desequilíbrio entre estresse e recuperação. Além disso, os fatores de estresse podem ser encontrados não apenas em situações do treinamento e da competição, mas também naquelas relacionadas a extratreinamento e extracompetição. Por sua vez, os atletas, na tentativa de alcançar altos níveis de desempenho com o treinamento, podem tornar-se excessivamente treinados, exibindo sinais e sintomas do supertreinamento. Esses sintomas podem manifestar-se por queda no desempenho, fadiga crônica, infecções respiratórias e alterações do humor. Embora não exista indicação de que o supertreinamento cause danos irreversíveis ao atleta, o risco de lesão, doenças ou retirada prematura do esporte é aumentado, diminuindo sobremaneira as expectativas e a qualidade de vida dos atletas no esporte. Baseado nesses acometimentos, pretendeu-se estudar parâmetros e instrumentos, através de uma revisão bibliográfica, com possibilidade de monitoramento e prevenção nos âmbitos fisiológico e psicológico. Conclui-se que, para o monitoramento, a melhor estratégia é associar parâmetros psicológicos com avaliações fisiológicas. É preconizada a implantação de programa sistematizado de prevenção aos efeitos nocivos no desempenho, na saúde e, conseqüentemente, no bem-estar do atleta.El exceso de entrenamiento o superentrenamiento está caracterizado por el desequilibrio entre estrés y recuperación. Además de esto, los factores de estrés pueden ser encontrados no apenas en situaciones de entrenamiento y de competición, sino también en aquellas relacionadas al extra entrenamiento y extra competición. A su vez, los atletas, en la tentativa de alcanzar altos niveles de desempeño con el entrenamiento, pueden acabar en excesos, exhibiendo señales y síntomas de superentrenamiento. Estos síntomas pueden manifestarse mediante la disminución del desempeño, fatiga crónica, infecciones

  9. MONITORAMENTO ELETRÔNICO DAS RESPOSTAS COMPORTAMENTAIS DE VACAS EM LACTAÇÃO ALOJADAS EM FREESTALL CLIMATIZADO

    Directory of Open Access Journals (Sweden)

    Soraia V. Matarazzo

    2007-11-01

    Full Text Available O trabalho teve como objetivo empregar o monitoramento eletrônico para avaliar as respostas comportamentais de vacas em lactação alojadas em freestall climatizado. Quatro vídeo-câmeras foram instaladas em cada tratamento, nos locais estratégicos do freestall, de modo a capturar, em tempo real o deslocamento dos animais. O experimento teve duração de 28 dias consecutivos do mês de novembro de 2003, no qual as imagens foram gravadas durante sete dias, no intervalo das 9 às 17 horas. Foram utilizadas 15 vacas em lactação, multíparas, com produção média de 20 kg de leite dia-1. Os tratamentos adotados foram: ausência de ventilação (V0, ventilação (V e ventilação + nebulização (VN posicionados na área de descanso dos animais. Os dados referentes à temperatura do bulbo seco (TBS e umidade relativa do ar (UR foram mensurados a cada 15 minutos ao longo das 24 horas no interior da instalação e no ambiente externo. A UR mostrou-se mais elevada nos tratamentos V0 (61,8% e VN (61,8% quando comparada ao tratamento V(60,3%. O THI mostrou-se mais elevado em V (75,0, quando comparado ao tratamento V0 (74,5 e VN (74,3. Os animais submetidos ao tratamento V (108,3 min passaram mais tempo na área de alimentação quando comparados com V0 (60,7 min e VN (72,5 min. Os animais do tratamento V (19,3 min permaneceram um período maior na área do bebedouro em relação a V0 (8,3 min e VN (12,7 min que não diferiram entre si. Foram observadas diferenças na preferência pelo lado da instalação. A área de descanso apresentava camas adjacentes à área de alimentação e adjacentes ao bebedouro. As vacas dos tratamentos V0 (189,0 min e V (167,3 min permaneceram maior tempo nas camas adjacentes à área de alimentação. Por outro lado, as vacas do tratamento VN (164,0 min passaram mais tempo nas camas adjacentes a área do bebedouro em relação aos animais do tratamento V (26,7 min. Foi constatado maior tempo em pé no

  10. Who bears the burden of international taxation? Evidence from cross-border M&As

    NARCIS (Netherlands)

    Huizinga, H.P.; Voget, J.; Wagner, W.B.

    2012-01-01

    Cross-border M&As can trigger additional taxation of the target's income in the form of non-resident dividend withholding taxes and acquirer-country corporate income taxation. This paper finds that this additional international taxation is fully capitalized into lower takeover premiums. In contrast,

  11. Acceptance Test Report for the Modular Automation System (MAS) Manufactured by Honeywell Inc

    International Nuclear Information System (INIS)

    ANDERSON, D.L.

    2000-01-01

    This document details the performance of the acceptance test of the Honeywell MAS Control System for equipment to be installed in gloveboxes HA-20MB and HA-211 at a later date. Equipment that was anticipated included 6 stabilization furnaces, only three and their associated equipment were installed

  12. SecMAS: Security Enhanced Monitoring and Analysis Systems for Wireless Sensor Networks

    Directory of Open Access Journals (Sweden)

    Ding Chao

    2016-01-01

    Full Text Available The monitoring, control, and security guarantee for the communication in the wireless sensor networks (WSNs are currently treated as three independent issues and addressed separately through specialized tools. However, most cases of WSNs applications requires the network administrator change the network configuration in a very short time to response to the change of observed phenomenon with security guarantee. To meet this requirement, we propose a security enhanced monitoring and control platform named SecMAS for WSNs, which provides the real-time visualization about network states and online reconfiguration of the network properties and behaviours in a resource-efficient way. Besides, basic cryptographic primitives and part of the anomaly detection functionalities are implemented in SecMAS to enabling the secure communication in WSNs. Furthermore, we conduct experiments to evaluate the performance of SecMAS in terms of the latency, throughput, communication overhead, and the security capacity. The experimental results demonstrate that the SecMAS system achieves stable, efficient and secure data collection with lightweight quick-response network control.

  13. Improved background suppression in 1H MAS NMR using composite pulses

    Science.gov (United States)

    Odedra, Smita; Wimperis, Stephen

    2012-08-01

    A well known feature of 1H MAS NMR spectroscopy, particularly of solids where the concentration of 1H nuclei is low, is the presence in the spectrum of a significant broad "background" signal arising from 1H nuclei that are outside the MAS rotor and radiofrequency coil, probably located on the surfaces of the static components of the probehead. A popular method of suppressing this unwanted signal is the "depth pulse" method, consisting of a 90° pulse followed by one or two 180° pulses that are phase cycled according to the "Exorcycle" scheme, which removes signal associated with imperfect 180° pulses. Consequently, only spins in the centre of the radiofrequency coil contribute to the 1H MAS spectrum, while those experiencing a low B1 field outside the coil are suppressed. Although very effective at removing background signal from the spectrum, one drawback with this approach is that significant loss of the desired signal from the sample also occurs. Here we investigate the 1H background suppression problem and, in particular, the use of novel antisymmetric passband composite pulses to replace the simple pulses in a depth pulse experiment. We show that it is possible to improve the intensity of the 1H signals of interest while still maintaining effective background suppression. We expect that these results will be relevant to 1H MAS NMR studies of, for example, nominally perdeuterated biological samples or nominally anhydrous inorganic materials.

  14. Improved background suppression in ¹H MAS NMR using composite pulses.

    Science.gov (United States)

    Odedra, Smita; Wimperis, Stephen

    2012-08-01

    A well known feature of ¹H MAS NMR spectroscopy, particularly of solids where the concentration of ¹H nuclei is low, is the presence in the spectrum of a significant broad "background" signal arising from ¹H nuclei that are outside the MAS rotor and radiofrequency coil, probably located on the surfaces of the static components of the probehead. A popular method of suppressing this unwanted signal is the "depth pulse" method, consisting of a 90° pulse followed by one or two 180° pulses that are phase cycled according to the "Exorcycle" scheme, which removes signal associated with imperfect 180° pulses. Consequently, only spins in the centre of the radiofrequency coil contribute to the ¹H MAS spectrum, while those experiencing a low B₁ field outside the coil are suppressed. Although very effective at removing background signal from the spectrum, one drawback with this approach is that significant loss of the desired signal from the sample also occurs. Here we investigate the ¹H background suppression problem and, in particular, the use of novel antisymmetric passband composite pulses to replace the simple pulses in a depth pulse experiment. We show that it is possible to improve the intensity of the ¹H signals of interest while still maintaining effective background suppression. We expect that these results will be relevant to ¹H MAS NMR studies of, for example, nominally perdeuterated biological samples or nominally anhydrous inorganic materials. Copyright © 2012 Elsevier Inc. All rights reserved.

  15. Characterization and significance of ACE2 and Mas receptor in human colon adenocarcinoma.

    Science.gov (United States)

    Bernardi, Stella; Zennaro, Cristina; Palmisano, Silvia; Velkoska, Elena; Sabato, Nicoletta; Toffoli, Barbara; Giacomel, Greta; Buri, Luigi; Zanconati, Fabrizio; Bellini, Giuseppe; Burrell, Louise M; De Manzini, Nicolò; Fabris, Bruno

    2012-03-01

    A new arm of the renin-angiotensin system (RAS) has been recently characterized; this includes angiotensin converting enzyme (ACE)2 and angiotensin (Ang)1-7, a heptapeptide acting through the Mas receptor (MasR). Recent studies show that Ang1-7 has an antiproliferative action on lung adenocarcinoma cells. The aim of this study was to characterize RAS expression in human colon adenocarcinoma and to investigate whether Ang1-7 exerts an antiproliferative effect on human colon adenocarcinoma cells. Gene, protein expression and enzymatic activity of the main components of the RAS were determined on non-neoplastic colon mucosa as well as on the tumor mass and the mucosa taken 5 cm distant from it, both collected from patients with colon adenocarcinoma. Two different human colon cancer cell lines were treated with AngII and Ang1-7. The novel finding of this study was that MasR was significantly upregulated in colon adenocarcinoma compared with non-neoplastic colon mucosa, which showed little or no expression of it. ACE gene expression and enzymatic activity were also increased in the tumors. However, AngII and Ang1-7 did not have any pro-/antiproliferative effects in the cell lines studied. The data suggest that upregulation of the MasR could be used as a diagnostic marker of colon adenocarcinoma.

  16. 77 FR 43084 - Multiple Award Schedule (MAS) Program Continuous Open Season-Operational Change

    Science.gov (United States)

    2012-07-23

    ... (GSA), Federal Acquisition Service (FAS) intends to institute a Demand Based Model (DBM) designed to... will restore and maintain the MAS program's value to Federal agencies as a streamlined acquisition... adding innovative solutions, improving pricing and simplifying the buying experience. DATES: This change...

  17. 29Si MAS NMR for the zeolite Y - gallium oxide system

    International Nuclear Information System (INIS)

    Sulikowski, B.; Derewinski, M.; Olejniczak, Z.; Segnowski, S.

    1994-01-01

    Wide-pore zeolites modified by gallium oxide has been prepared for catalytic use. Its physico-chemical and catalytic properties have been studied. The structure changes of the catalyst have been investigated by means of MAS NMR spectroscopy. Spectra of 29 Si has been described and discussed

  18. An Analysis of the Rise and Fall of the AA-MAS Policy

    Science.gov (United States)

    Lazarus, Sheryl S.; Thurlow, Martha L.; Ysseldyke, James E.; Edwards, Lynn M.

    2015-01-01

    In 2005, to address concerns about students who might fall in the "gap" between the regular assessment and the alternate assessment based on alternate achievement standards (AA-AAS), the U.S. Department of Education announced that states could develop alternate assessments based on modified achievement standards (AA-MAS). This article…

  19. Considerations for Consortia as States Transition Away from AA-MAS. NCEO Brief. Number 7

    Science.gov (United States)

    National Center on Educational Outcomes, 2014

    2014-01-01

    States with an alternate assessment based on modified achievement standards (AA-MAS) that received a flexibility waiver from some of the requirements of No Child Left Behind are required to phase out their use of this assessment. And, on August 23, 2013, the U.S. Department of Education published a proposed rollback of regulation that allowed the…

  20. Successfully Transitioning from the AA-MAS to the General Assessment. NCEO Policy Directions. Number 22

    Science.gov (United States)

    Lazarus, Sheryl; Thurlow, Martha; Christensen, Laurene; Shyyan, Vitaliy

    2014-01-01

    Federal policy initiatives such as the flexibility waivers for accountability are requiring that states transition away from the use of an alternate assessment based on modified achievement standards (AA-MAS). It is expected that those students who had participated in that assessment will instead participate in the state's general assessment (or a…

  1. Marker-assisted-selection (MAS): A fast track to increase genetic ...

    African Journals Online (AJOL)

    Mapping and tagging of agriculturally important genes have been greatly facilitated by an array of molecular markers in crop plants. Marker-assisted selection (MAS) is gaining considerable importance as it would improve the efficiency of plant breeding through precise transfer of genomic regions of interest (foreground ...

  2. HUBUNGAN ANTARA PERTUMBUHAN DENGAN KEBERADAAN GEN TAHAN PENYAKIT MAJOR HISTOCOMPATIBILITY COMPLEX (MHC PADA IKAN MAS (Cyprinus carpio

    Directory of Open Access Journals (Sweden)

    Erma Primanita Hayuningtyas

    2016-04-01

    Full Text Available Wabah penyakit koi herpes virus (KHV di Indonesia yang terjadi sejak tahun 2002 merupakan salah satu faktor yang memicu kemerosotan produksi ikan mas budidaya. Pembentukan strain unggul ikan mas tahan KHV dapat menjadi solusi bagi permasalahan tersebut. Pemilihan genotip ikan mas tahan KHV dengan marka molekuler gen major histocompatibility complex class II (MHC-II, khususnya pada alel Cyca DAB 1*05 akan membantu dalam kegiatan seleksi. Penelitian ini bertujuan untuk mengetahui keberadaan gen MHC-II pada populasi dasar G0 ikan mas strain Rajadanu dan hubungannya dengan pertumbuhan (bobot. Metode deteksi keberadaan gen MHC-II pada dua kelompok ikan dengan ukuran berbeda dilakukan dengan teknik PCR. Hubungan antara pertumbuhan ikan mas dengan persentase kemunculan gen MHC-II dianalisis dengan menggunakan program SPSS (Statistical Package for the Social Sciences, sehingga diperoleh korelasi di antara keduanya. Hasil penelitian menunjukkan bahwa hubungan antara pertumbuhan dengan persentase keberadaan gen MHC-II berkorelasi negatif dengan nilai R = -0,742. Hal ini mengindikasikan bahwa semakin cepat pertumbuhan populasi ikan mas maka semakin sedikit persentase individu yang mempunyai gen MHC-II pada setiap populasi ikan mas. Sehingga populasi ikan mas yang pertumbuhannya lambat memiliki tingkat persentase positif MHC-II lebih tinggi (85,71%-100% dibandingkan populasi ikan mas yang pertumbuhannya cepat (42,86%-85,71%.

  3. 1H and 23Na MAS NMR spectroscopy of cationic species in CO2 selective alkaline earth metal porous silicoaluminophosphates prepared via liquid and solid state ion exchange

    International Nuclear Information System (INIS)

    Arévalo-Hidalgo, Ana G.; Dugar, Sneha; Fu, Riqiang; Hernández-Maldonado, Arturo J.

    2012-01-01

    The location of extraframework cations in Sr 2+ and Ba 2+ ion-exchanged SAPO-34 was estimated by means of 1 H and 23 Na MAS NMR spectroscopy and spectral deconvolution. Incorporation of the alkaline earth metal cations onto the SAPO framework was achieved via liquid state ion exchange, coupled partial detemplation/solid-state ion exchange, and combination of both techniques. MAS NMR revealed that the level of ion exchange was limited by the presence of protons and sodium cations near hexagonal prisms (site SI), which are relatively difficult to exchange with the alkaline earth metal due to steric and charge repulsion criteria. In addition, the presence of ammonium cations in the supercages facilitated the exchange of otherwise tenacious hydrogen as corroborated by unit cell compositional data as well as enhanced CO 2 adsorption at low partial pressures. The extraframework ammonium species were produced from partial detemplation of the structure-directing agent employed for the SAPO-34 synthesis, tetraethylammonium. - Graphical abstract: MAS NMR was used to elucidate the position the cationic species in alkaline earth metal exchanged silicoaluminophosphates. These species played a significant role during the ion exchange process and, therefore, the materials ultimate CO 2 adsorption performance. Highlights: ► Location of extraframework Sr 2+ or Ba 2+ cations was estimated by means of 1 H and 23 Na MAS NMR. ► Level of Sr 2+ or Ba 2+ ion exchange was limited by the presence of protons and sodium cations. ► Presence of ammonium cations in the supercages facilitated the exchange. ► Sr 2+ and Ba 2+ ion exchanged SAPOs are outstanding CO 2 adsorbents.

  4. PENGARUH IKLAN DAN ATRIBUT PRODUK TERHADAP KEPUTUSAN PEMBELIAN SMARTPHONE SAMSUNG SERI GALAXY (SURVEI PADA PELANGGAN ITC ROXY MAS

    Directory of Open Access Journals (Sweden)

    Basrah Saidani

    2013-04-01

    Full Text Available Generally, the purpose of this research are: 1 to get more knowledge about Advertising, product attributes and the decision to purchase smartphone Samsung Galaxy series,. 2 to get more knowledge about the influence of Advertising to purchasing decisions smartphone Samsung Galaxy series, 3 to get more knowledge about the influence of product attributes to purchasing decisions smartphone Samsung Galaxy series, 4 to get more knowledge about influence of Advertising and product attributes simultaneously the decision to purchase smartphone Samsung Galaxy series. The observation unit in this research is 100 respondents visitors ITC Roxy Mas – Jakarta to purchase smartphone Samsung Galaxy series. Technique of determining the sample using a convenience sampling technique. Data collection techniques using the questionnaire Liker scale from 1 to 5. Descriptive analysis results showed: 1 the Advertising from Samsung Galaxy series is good enough as a whole but still lacking in message Acceptance and message retention. 2 Attribute a good product overall dimesi dominated by product futures, 3 the decision to purchase is dominated by post-purchase where consumers get satisfaction after buying the Samsung Galaxy series. Hypothesis testing results showed: 1 Advertising have a significant effect on purchasing decisions, 2 product attributes have a significant effect on purchasing decisions, 3 Advertising and product attributes a significant effect on purchasing decisions.

  5. Participation and Performance Reporting for the Alternate Assessment Based on Modified Achievement Standards (AA-MAS). Technical Report 58

    Science.gov (United States)

    Albus, Deb; Thurlow, Martha L.; Lazarus, Sheryl S.

    2011-01-01

    This report examines publicly reported participation and performance data for the alternate assessment based on modified achievement standards (AA-MAS). The authors' analysis of these data included all states publicly reporting AA-MAS data, regardless of whether they had received approval to use the results for Title I accountability calculations.…

  6. Angiotensin II Type 2 Receptor and Receptor Mas Are Colocalized and Functionally Interdependent in Obese Zucker Rat Kidney

    DEFF Research Database (Denmark)

    Patel, Sanket N; Ali, Quaisar; Samuel, Preethi

    2017-01-01

    The actions of angiotensin II type 2 receptor (AT2R) and the receptor Mas (MasR) are complex but show similar pronatriuretic function; particularly, AT2R expression and natriuretic function are enhanced in obese/diabetic rat kidney. In light of some reports suggesting a potential positive...... interaction between these receptors, we tested hypothesis that renal AT2R and MasR physically interact and are interdependent to stimulate cell signaling and promote natriuresis in obese rats. We found that infusion of AT2R agonist C21 in obese Zucker rats (OZR) increased urine flow and urinary Na excretion...... coimmunoprecipitated with MasR in cortical homogenate of OZR. Immunoblotting of cortical homogenate cross-linked with zero-length oxidative (sulfhydryl groups) cross-linker cupric-phenanthroline revealed a shift of AT2R and MasR bands upward with overlapping migration for their complexes which were sensitive...

  7. Monitoramento da adesão ao tratamento com lítio Monitoring the compliance to lithium treatment

    Directory of Open Access Journals (Sweden)

    Adriane Ribeiro Rosa

    2006-01-01

    Full Text Available CONTEXTO: O lítio é utilizado como medicamento de escolha para o tratamento dos transtornos de humor bipolar. Mostra-se eficaz em reduzir as crises maníacas e depressivas do transtorno do humor bipolar, além de exercer efeito anti-suicida. No entanto, a efetividade do lítio é comprometida pela baixa adesão ao tratamento, por sua vez influenciada por características dos pacientes e pelas características farmacológicas do lítio, que dificultam seu uso. OBJETIVO: Revisar alguns aspectos farmacológicos clínicos do lítio e sua importância para a monitorização terapêutica do lítio, por meio de dosagens e de escalas de auto-relato em português para avaliar a falta de adesão ao lítio. MÉTODO: Foi realizada revisão da literatura básica e clínica sobre lítio disponível em artigos científicos em língua inglesa e portuguesa acessados pelo PUBMED e SCIELO, usando as palavras "lítio", "monitoramento", "cooperação" OU "adesão". RESULTADOS: O lítio é um fármaco de muito baixo índice terapêutico e farmacocinética muito individual, fato que justifica a necessidade de monitorização terapêutica intensiva, por meio de determinação da concentração sérica e hemática. As taxas de adesão ao lítio em pacientes brasileiros que freqüentam os ambulatórios específicos para transtornos bipolares estão entre 60 e 85%, sendo mais elevadas que a de pacientes tratados sem acompanhamento psicoeducativo (adesão em torno de 46%. Os pacientes não aderentes apresentavam um menor nível de conhecimento sobre o lítio e sobre a doença, e mais atitudes negativas dos pacientes ao uso de medicamentos, além de receio dos efeitos adversos. CONCLUSÃO: A monitorização laboratorial e por escalas auxilia na adesão ao tratamento, por auxiliar na individualização terapêutica e ajuste de doses de lítio, além de detectar as interações medicamentosas e as atitudes dos pacientes em relação a sua doença e tratamentos

  8. MAS-based Distributed Coordinated Control and Optimization in Microgrid and Microgrid Clusters: A Comprehensive Overview

    DEFF Research Database (Denmark)

    Han, Yang; Zhang, Ke; Hong, Li

    2018-01-01

    The increasing integration of the distributed renewable energy sources highlights the requirement to design various control strategies for microgrids (MGs) and microgrid clusters (MGCs). The multi-agent system (MAS)-based distributed coordinated control strategies shows the benefits to balance...... the power and energy, stabilize voltage and frequency, achieve economic and coordinated operation among the MGs and MGCs. However, the complex and diverse combinations of distributed generations in multi-agent system increase the complexity of system control and operation. In order to design the optimized...... configuration and control strategy using MAS, the topology models and mathematic models such as the graph topology model, non-cooperative game model, the genetic algorithm and particle swarm optimization algorithm are summarized. The merits and drawbacks of these control methods are compared. Moreover, since...

  9. Le Kāmasūtra et la « pulsion shastrique » en Inde

    OpenAIRE

    Naudou, Elizabeth

    2013-01-01

    Le mot « shastrique » fait référence au traité (śāstra) d’où sont issus les Kāmasūtra, (plus généralement appelé le Kāmasūtra), « aphorismes sur l’amour » : le Kāmaśāstra, « traité sur l’amour ». Qui dit śāstra, dit, en Inde, exposé religieux ou scientifique, d’où l’expression « pulsion shastrique » que l’on pourrait rendre par « pulsion encyclopédique énumérative et classificatoire ». Le but de cet exposé est de replacer le texte dans cette structure mentale typiquement indienne, qui reflète...

  10. El Proyecto Sismico "LARSE" - Trabajando Hacia un Futuro con Mas Seguridad para Los Angeles

    Science.gov (United States)

    Henyey, Thomas L.; Fuis, Gary S.; Benthien, Mark L.; Burdette, Thomas R.; Christofferson, Shari A.; Clayton, Robert W.; Criley, Edward E.; Davis, Paul M.; Hendley, James W.; Kohler, Monica D.; Lutter, William J.; McRaney, John K.; Murphy, Janice M.; Okaya, David A.; Ryberg, Trond; Simila, Gerald W.; Stauffer, Peter H.

    1999-01-01

    La region de Los Angeles contiene una red de fallas activas, incluyendo muchas fallas por empuje que son profundas y no rompen la superficie de la tierra. Estas fallas ocultas incluyen la falla anteriormente desconocida que fue responsable por la devastacion que ocurrio durante el terremoto de Northridge en enero de 1994, el terremoto mas costoso en la historia de los Estados Unidos. El Experimento Sismico en la Region de Los Angeles (Los Angeles Region Seismic Experiment, LARSE), esta localizando los peligros ocultos de los terremotos debajo de la region de Los Angeles para mejorar la construccion de las estructuras que pueden apoyar terremotos que son inevitables en el futuro, y que ayudaran a los cientificos determinar donde occurira el sacudimento mas fuerte y poderoso.

  11. Mas Gusó: a Roman military Settlement in the suburbium of Emporiae

    Directory of Open Access Journals (Sweden)

    Josep Casas Genover

    2016-11-01

    Full Text Available Although the site of Mas Gusó (province of Girona has been interpreted as a Roman uilla, this is actually a public building. Its existence have to be contextualized within the frame of the structures established by the Roman authority for territorial control closely linked to the creation of a new road network and a tax collection system. We also analyse its survival until the 3rd century AD, which are closely related to the nearby city of Emporiae.

  12. Effectiveness of FitoMas-E in the cultivation of chickpea under two soil moisture levels

    Directory of Open Access Journals (Sweden)

    Yanitza Meriño Hernández

    2018-01-01

    Full Text Available To evaluate the effect of FitoMas-E on the performance of the chickpea, in conditions of drought stress, was the objective of this investigation. An experiment was conducted in the Intensive Garden "Río de Guisa" in the municipality of Guisa during the period from November to February 2014. Four treatments were applied, distributed in a randomized block design with three repetitions, on a "Pardo mullido grisaceo" soil, comparing the application of FitoMas-E under two soil moisture regimes, with and without water stress. The yield of grain and its components were evaluated at the time of harvest maturity, to analyze the responses of these variables to the treatments applied. An analysis of variance was performed using the statistical package STASTISTICA version 8.0 for Windows and the means of the treatments were compared using the Tukey Multiple Range test. The variables that showed a greater response to the treatments imposed were the number of legumes per plant, number of seeds per plant, the mass of 100 seeds and the yield of grain, which ranged between 0.9 and 0.93 t ha-1 for the treatments 2 and 4 respectively. The results obtained in this research showed that the chickpea crop achieved the best productive indicators when the plants were under water stress conditions and received the application of FitoMas-E.

  13. Stanowisko badawcze do oceny efektów utwardzania mas ze szkłem wodnym

    Directory of Open Access Journals (Sweden)

    M. Stachowicz

    2012-12-01

    Full Text Available W pracy przedstawiono wyniki badań nad możliwością zastosowania nowego stanowiska badawczego do oceny, na podstawie końcowejzawartości wody, finalnego efektu utwardzania wybranymi metodami mas ze szkłem wodnym. Badania wykonano na innowacyjnym,mobilnym stanowisku mikrofalowej linii szczelinowej wykorzystującej zjawisko występowania fali stojącej w falowodzie. Badaniompoddano pięć mas sporządzonych z dostępnymi w handlu gatunkami szkła wodnego, które utwardzano trzema, wybranymi metodami:mikrofalową, klasyczną oraz w procesie CO2. Wykazano, na przykładzie mas ze szkłem wodnym, że prezentowane, mobilne stanowiskopomiarowe może, na podstawie określenia końcowej zawartości wody, służyć z powodzeniem do oceny ostatecznego efektu utwardzaniamas formierskich i rdzeniowych.

  14. Indicadores propostos pela UNGASS e o monitoramento da epidemia de Aids no Brasil Proposed UNGASS indicators and the monitoring of the AIDS epidemic in Brazil

    Directory of Open Access Journals (Sweden)

    Aristides Barbosa Junior

    2006-04-01

    Full Text Available O objetivo do estudo foi analisar o processo de monitoramento de indicadores centrais propostos pela UNGASS, em nível nacional, vis-à-vis aos indicadores do Programa Nacional de DST e Aids. Foram avaliados os dois conjuntos de indicadores propostos, respectivamente, em 2002 e 2005, para o monitoramento de progresso da Declaração de Compromisso da UNGASS. Foram analisadas a disponibilidade de informações e as limitações para o cálculo dos indicadores propostos no Brasil, incluindo discussão sobre a adequação dos indicadores propostos para o monitoramento da epidemia brasileira. Dos 13 indicadores quantitativos inicialmente propostos pela UNGASS, cinco não estão incluídos no sistema de monitoramento do Programa Pacional. Um deles não foi incluído por ser um indicador qualitativo. Dois dos indicadores foram considerados de pouca utilidade e dois não foram contemplados pela falta de dados disponíveis para o seu cálculo. Como o Brasil é caracterizado por ter uma epidemia concentrada, no segundo conjunto de indicadores propostos pela UNGASS, prioriza-se o acompanhamento da epidemia entre as populações sob maior risco. Destacou-se que o Programa Nacional centra seus esforços no desenvolvimento, adaptação e transferência de metodologias de amostragem em populações de difícil acesso. Tais ações são voltadas para a estimação do tamanho dos grupos vulneráveis, bem como para obter mais informações sobre seu comportamento, atitudes e práticas. Concluiu-se que, pela possibilidade de comparações internacionais dos avanços conseguidos, a proposição de indicadores supranacionais estimula os países a discutir e viabilizar sua construção. De maneira complementar, os sistemas nacionais de monitoramento devem ser focados na melhoria do programa, cobrindo áreas que permitam avaliar as ações de controle e intervenções específicas.The objective of this study was to analyze, on the national level, the process of

  15. Impacto do monitoramento telefônico de gestantes na prevalência da prematuridade e análise dos fatores de risco associados em Piracicaba, São Paulo, Brasil

    Directory of Open Access Journals (Sweden)

    Rogerio Antonio Tuon

    2016-01-01

    Full Text Available Resumo: Objetivou-se verificar o impacto do monitoramento telefônico na prevalência da prematuridade e identificar os fatores de risco associados ao parto prematuro através de estudo transversal, de universo de gestantes monitoradas nos anos de 2010, 2011 e 2012 (n = 2.739. Utilizou-se estimação de modelos de regressão logística múltipla hierarquizada, considerando permanência no modelo p ≤ 0,05. A prevalência de prematuridade foi de 8,34% nas gestantes monitoradas e de 10,18% nas não monitoradas (p = 0,0058, sendo inversamente proporcional ao número de monitoramentos (p < 0,0001. As variáveis associadas foram: idade materna menor que 19 anos, antecedentes de dois ou mais filhos mortos, gestação múltipla, diabetes e hipertensão arterial, menor número de monitoramentos telefônicos, atividades laborais em pé e/ou carga de peso, fumo, número de consultas pré-natal, sem ultrassonografia, diabetes gestacional, gravidez múltipla e anomalia fetal. Com custos baixos, a estratégia demonstrou ser efetiva na redução da ocorrência do parto prematuro.

  16. Monitoramento contínuo do potencial redox e de variáveis complementares em ambiente hipersazonal no Pantanal Norte

    Directory of Open Access Journals (Sweden)

    Indira Ashant Martins Messias

    2013-06-01

    Full Text Available A análise conjunta do potencial redox com outras variáveis pode ser útil para o entendimento da dinâmica dos solos hidromórficos, ao longo de todo o ciclo hidrológico a que o Pantanal está submetido. Neste trabalho, foram estudados o potencial redox e algumas variáveis do solo (CO2, O2, temperatura, umidade e potencial matricial pelo monitoramento contínuo e ininterrupto. Para isso, foram realizadas determinações nas profundidades de 10 e 30 cm num Planossolo Háplico alítico gleissólico, na fitofisionomia Cerrado sensu stricto. O trabalho foi realizado de fevereiro de 2010 a julho de 2011 na RPPN (Reserva Particular do Patrimônio Natural/Sistema Nacional de Unidades de Conservação - SNUC, Estância Ecológica SESC (Serviço Social do Comércio Pantanal, município de Barão de Melgaço, nordeste do Pantanal de Mato Grosso. Os valores do potencial redox variaram de 636 mV (enchente a -341 mV (cheia, caracterizando ambiente anaeróbico na estação da cheia e ambiente oxidado nas demais estações do ciclo hidrológico, o que indica que o potencial redox é ferramenta versátil para compreender as reações de oxirredução nos solos hidromórficos do Pantanal mato-grossense, pois os valores diminuíram quando o teor de umidade era elevado. Além disto, o estudo evidenciou também que o monitoramento contínuo de variáveis complementares pode ser importante por permitir análise mais aprofundada das condições de hipersazonalidade, em que esses solos estão submetidos. Neste contexto, o potencial matricial e a umidade foram as variáveis de maior importância para explicar a variação do conjunto de dados obtidos ao longo do ciclo hidrológico, o que indica que esses parâmetros físicos são determinantes nos processos biológicos desse solo tropical com hipersazonalidade hídrica.

  17. Solução do Solo e Análise de Componentes Principais para Monitoramento da Aplicação de Lodo de Esgoto

    Directory of Open Access Journals (Sweden)

    Aline Renée Coscione

    2014-10-01

    Full Text Available O uso agrícola do lodo é uma alternativa viável para a reciclagem de nutrientes, embora haja certa preocupação com o aumento de espécies químicas solúveis originadas da mineralização da fração orgânica. Assim, para conhecer a disponibilidade de nutrientes e o risco de contaminação do solo e da água, o estudo da solução do solo é uma ferramenta valiosa. Nesses estudos, o número de variáveis utilizadas ultrapassa facilmente uma dezena, e ferramentas de análise exploratória, como a análise de componentes principais (ACP, revelam a existência ou não de amostras anômalas, de relações entre as variáveis medidas e sua contribuição relativa e de relações ou agrupamentos entre amostras. O objetivo deste trabalho foi identificar variáveis relacionadas com a solução do solo e alteradas, em razão do uso do lodo de esgoto e da adubação mineral, de forma a complementar os procedimentos para monitoramento/avaliação de áreas que recebem esse tipo de resíduo. A composição da solução do solo de uma área que recebeu lodo de esgoto por sete anos consecutivos foi estudada dos 22 aos 46 meses após a sua última aplicação. Com a solução do solo foi possível, por meio da ACP, distinguir as áreas em função da adubação aplicada. Após quatro anos da interrupção das aplicações sucessivas de lodo de esgoto, não verificou-se concentração apreciável de metais na solução do solo, embora ainda seja possível identificar traços da mineralização do resíduo. As variáveis pH, Mn2+, COD, SO4(2-, NO3- e NH4+ na solução do solo podem ser utilizadas no monitoramento de áreas tratadas com lodo de esgoto.

  18. In situ high temperature MAS NMR study of the mechanisms of catalysis. Ethane aromatization on Zn-modified zeolite BEA.

    Science.gov (United States)

    Arzumanov, Sergei S; Gabrienko, Anton A; Freude, Dieter; Stepanov, Alexander G

    2009-04-01

    Ethane conversion into aromatic hydrocarbons over Zn-modified zeolite BEA has been analyzed by high-temperature MAS NMR spectroscopy. Information about intermediates (Zn-ethyl species) and reaction products (mainly toluene and methane), which were formed under the conditions of a batch reactor, was obtained by (13)C MAS NMR. Kinetics of the reaction, which was monitored by (1)H MAS NMR in situ at the temperature of 573K, provided information about the reaction mechanism. Simulation of the experimental kinetics within the frames of the possible kinetic schemes of the reaction demonstrates that a large amount of methane evolved under ethane aromatization arises from the stage of direct ethane hydrogenolysis.

  19. Suture-free technique for canine ureteral resection-anastomosis using a microvascular anastomotic system: a cadaveric study.

    Science.gov (United States)

    Wavreille, Vincent; Adin, Christopher A; Arango, Johnattan; Ham, Kathleen L; Byron, Julie K; McLoughlin, Mary A

    2015-01-01

    To describe a suture-free technique for canine ureteral resection-anastomosis using a microvascular anastomotic system (MAS) and to compare surgical time and burst pressure of hand-sewn (HS) ureteral end-to-end anastomosis with the MAS technique. Experimental ex vivo study. Canine cadavers (n = 8). For each cadaver, 1 ureter was randomly assigned to undergo HS anastomosis and the contralateral ureter had MAS anastomosis. The first 3 cadavers (6 ureters) were used to refine the MAS technique. In the other 5 dogs, surgical time and ureteral burst pressure were compared between groups (n = 5 ureters/group). Preliminary procedures showed that selective impaling of the mucosa and submucosa (without muscularis and adventitia) is necessary to allow complete mechanical interlock of the anastomotic rings for the MAS technique. Median anastomotic time was significantly shorter for MAS (7.6 min) than HS (16.6 min; p = .029) and burst pressure higher for MAS (393 cm H2 O) than HS (180 cm H2 O; p = .012). This study demonstrated the feasibility of a suture-free technique of canine ureteral resection-anastomosis using a commercially available MAS. The MAS anastomosis was faster and had higher burst strength compared with the HS anastomosis. © Copyright 2014 by The American College of Veterinary Surgeons.

  20. Monitoramento de indicadores geoquímicos e avaliação de biodegradação em área contaminada com óleo diesel Monitoring of geochemical indicators and biodegradation evaluation at a site contaminated with diesel oil

    Directory of Open Access Journals (Sweden)

    Adriano Pinto Mariano

    2007-09-01

    Full Text Available A biorremediação natural da água subterrânea contaminada com óleo diesel em um posto de combustíveis foi avaliada mediante o monitoramento de indicadores geoquímicos e ensaios laboratoriais de biodegradação. Durante um período de dois anos foram realizadas quatro coletas de água subterrânea para a avaliação de diversos parâmetros físico-químicos e a concentração de hidrocarbonetos. As análises microbiológicas consistiram na contagem de bactérias heterotróficas totais, na verificação da presença de bactérias hidrocarbonoclásticas e no teste de biodegradabilidade utilizando o indicador redox DCPIP. Foi possível identificar fatores que corroboram o emprego da técnica de biorremediação natural para o tratamento da água subterrânea, contudo, a presença de hidrocarbonetos retidos no solo representa uma fonte contínua de contaminação, por isso se faz necessário o monitoramento a longo prazo.The natural bioremediation of the groundwater contaminated with diesel oil at a petrol station was evaluated by monitoring geochemical indicators and biodegradation tests in laboratory. During two years the groundwater was collected four times. Different physic-chemical parameters and the concentration of hydrocarbons were evaluated. Microbiological analyses consisted of total heterotrophic bacteria counting, verification of the presence of hydrocarbonoclastic bacteria and the biodegradability test using the redox indicator DCPIP. It was possible to identify factors that confirm the use of the natural bioremediation technique as a treatment to the groundwater, however, hydrocarbons retained in the soil represent a continuous source of contamination, and for this reason, a long term monitoring is necessary.

  1. Variable temperature 127I MAS NMR of β-AgI

    International Nuclear Information System (INIS)

    Wagner, G.W.

    1991-01-01

    Variable temperature 127 I MAS NMR of β-AgI powder, measured from 123 to 413 K is sensitive to Ag + diffusion through the iodine lattice. In low temperature spectra, the iodine ions appear to be in nearly static environments in agreement with the low temperature crystal structure. However, at higher temperatures, substantial broadening of the central transition linewidth is consistent with the presence of two types of Ag + diffusion with activation energies of 0.17 and 0.0080 eV. (author). 15 refs.; 5 figs.; 1 tab

  2. Fauna de formigas como ferramenta para monitoramento de área de mineração reabilitada na Ilha da Madeira, Itaguaí, RJ.

    Directory of Open Access Journals (Sweden)

    Marcos Paulo dos Santos Pereira

    2010-08-01

    Full Text Available A riqueza e diversidade de espécies de formigas podem ser maiores em ambientes de complexidade mais elevada devido a uma maior disponibilidade de nichos presentes. Em razão da conexão entre os organismos e as características dos habitats, as formigas têm sido utilizadas como ferramentas no monitoramento ambiental de áreas perturbadas. Neste estudo, foi investigada a estrutura da comunidade de formigas em parcelas utilizadas para reabilitação de uma área de mineração na Ilha da Madeira, Itaguaí, RJ. Encontrou-se uma fauna diferenciada de formigas e maior riqueza de espécies em parcelas nas quais foi utilizado um maior número de espécies arbóreas nativas do que em parcelas com poucas espécies arbóreas ou sem nenhuma intervenção conservacionista.

  3. MONITORAMENTO DE SEDIMENTOS E REJEITOS DA USINA DE FERRO CARAJÁS ATRAVÉS DO SISTEMA DE GEOBARRAGEM (ESTUDO DE CASO

    Directory of Open Access Journals (Sweden)

    José Carlos Oliveira

    2007-12-01

    Full Text Available Com o objetivo de dar suporte atividades diárias de controle e para auxiliar a tomada de decisões na operação das barragens das minas de ferro da CVRD, Carajás-PA, foi desenvolvido, em parceria com a empresa Geoexplore Consultoria e Serviços, um sistema de Gestão de Barragens baseado em geotecnologias. O GeoBarragem foi concebido para atuar na coleta de dados de campo, no armazenamento dos dados relacionados à gestão das barragens, na análise e integração espacial e na simulação do preenchimento das barragens. É composto por um coletor de dados através de Handheld, um Sistema Gerenciador de Banco de Dados, um software para integração e análise espacial de dados e um simulador de preenchimento de barragens. Palavras chave: Monitoramento; Sedimentos e rejeitos; Geobarragem Minas de Ferro de Carajás.

  4. Monitoramento do desenvolvimento de macrófitas aquáticas em laboratório por meio de imagens digitais

    Directory of Open Access Journals (Sweden)

    Felipe Aparecido Gabriel de Miranda

    2014-06-01

    Full Text Available Este trabalho teve como objetivo avaliar a precisão e a acurácia do processamento de imagens digitais terrestres e o desenvolvimento da macrófita aquática Lemna sp. Cerca de 1.281 plantas de lemna foram dispostas em três delimitadores, no interior de um tanque de piscicultura, e tiveram seu desenvolvimento monitorado durante quinze dias consecutivos, por meio de fotografias capturadas com uma câmera  fotográfica digital Samsung, sensor  1/2,3”, CCD com 12,3 mega-pixels. As fotografias foram processadas no programa computacional SPRING 5.1.6, sendo utilizado como classificador digital o algoritmo de maxiverossimilhança. A avaliação da precisão foi realizada pela comparação das áreas mapeadas e a acurácia por meio da exatidão do reconhecimento dos pixels classificados. Os resultados revelam o potencial da técnica no monitoramento diário da macrófita, bem como de sua distribuição espacial desta. Acrescenta-se que o método, além de ser de fácil realização, não provoca distúrbios nas plantas.

  5. MODIS Airborne Simulator (MAS) Measurements Taken Onboard the NASAER-2 During the TOGA COARE Intensive Observing Period

    Data.gov (United States)

    National Aeronautics and Space Administration — The TOGA COARE Data Information System has responsibility for distributing information about TOGA COAREdatasets and access paths.The MAS data are available upon...

  6. Exposure (mAs) optimisation of a multi-detector CT protocol for hepatic lesion detection: are thinner slices better?

    International Nuclear Information System (INIS)

    Dobeli, Karen L.; Lewis, Sarah J.; Meikle, Steven R.; Brennan, Patrick C.; Thiele, David L.

    2014-01-01

    The purpose of this work was to determine the exposure-optimised slice thickness for hepatic lesion detection with CT. A phantom containing spheres (diameter 9.5, 4.8 and 2.4mm) with CT density 10 HU below the background (50 HU) was scanned at 125, 100, 75 and 50 mAs. Data were reconstructed at 5-, 3- and 1-mm slice thicknesses. Noise, contrast-to-noise ratio (CNR), area under the curve (AUC) as calculated using receiver operating characteristic analysis and sensitivity representing lesion detection were calculated and compared. Compared with the 125 mAs/5mm slice thickness setting, significant reductions in AUC were found for 75 mAs (P<0.01) and 50 mAs (P<0.05) at 1- and 3-mm thicknesses, respectively; sensitivity for the 9.5-mm sphere was significantly reduced for 75 (P<0.05) and 50 mAs (P<0.01) at 1-mm thickness; sensitivity for the 4.8-mm sphere was significantly lower for 100, 75 and 50 mAs at all three slice thicknesses (P<0.05). The 2.4-mm sphere was rarely detected. At each slice thickness, noise at 100, 75 and 50 mAs exposures was approximately 10, 30 and 50% higher, respectively, than that at 125 mAs exposure. CNRs decreased in an irregular manner with reductions in exposure and slice thickness. This study demonstrated no advantage to using slices below 5mm thickness, and consequently thinner slices are not necessarily better.

  7. El medievalismo fértil de Paloma Díaz-Mas

    Directory of Open Access Journals (Sweden)

    Rafael M. Mérida Jiménez

    2001-01-01

    Full Text Available The author of this article is concerned with trying to understand why Paloma Díaz-Mas, the writer of such an excellent novel as La tierra fértil (1999, has not received much critical attention. He underlines three main reasons. First, she does not live in Madrid or Barcelona and so she is far away from the main centres of cultural power. Second, she teaches Spanish literature in the Basque Country, a political and linguistic community which significantly differs from that of many other writers. Third, she writes historical novels, which does not appear to be very fashionable in Spain these days. Moreover, Díaz-Mas is a woman writer who does not make use of the most commonly available feminine patterns, and she does not seem to offer a model easy to include in a given feminist methodology either. However, Mérida-Jiménez argues that Paloma provides an intelligent deconstruction of “male authority” through subtle rhetorical means, as well as a representation of the weakness of his “domination” in very innovative ways, such as those derived from the dialectics between history and fiction, centrality and marginality, heterosexuality and homosexuality, individual and society, dream and reason or tradition and modernity.

  8. Active and passive fire protection system in academic building KH. Mas Mansur, Islamic University of Indonesia

    Directory of Open Access Journals (Sweden)

    Suryoputro M. Ragil

    2018-01-01

    Full Text Available According to the theory of fire triangle, the existence of combustible materials, heat, and oxygen can cause fire disaster. KH. Mas Mansur building, Islamic University of Indonesia has a fire protection, but rarely to be checked regularly and the number of equipment is less standard as well as the lack of an evacuation route map to facilitate the evacuation process. Inside the building also does not provide safety signs such as the evacuation directions, exit, and warning in case of fire. Therefore, researchers analysed the infrastructure of prevention and control in the building KH. Mas Mansur. Researchers used the method of observation, interviews, and checklist to know the condition directly, and compare with the standard regulations. Results concordance rate of existing infrastructure is 67% fire extinguisher, hydrant box 56%, 71% alarms, sprinkler 0%, 40% detectors, emergency doors 71%, 50% emergency stairs, assembly point 0% and directions 0%. The current results were below the standard of at least 80%. As for recommendations, researchers create a new evacuation map then put the existing infrastructure according to standard regulations, and it had consulted with the specialist of Occupational Safety and Health in the field of fire.

  9. MODELAGEM DE UM SISTEMA MULTIAGENTE DE APOIO À PBL UTILIZANDO A METODOLOGIA MAS-COMMONKADS+

    Directory of Open Access Journals (Sweden)

    Laysa Mabel de Oliveira Fontes

    2014-10-01

    Full Text Available A aprendizagem baseada em problema (Problem-Based Learning - PBL é um método no qual os estudantes aprendem através da resolução de um problema que, em geral, não possui uma solução trivial e uma única solução correta. A PBL destaca o trabalho em equipe como um dos principais requisitos para o sucesso do processo de aprendizagem, ou seja, a colaboração é essencial. No entanto, a implantação de um método de ensino com base na PBL não é uma tarefa trivial. Em Ambientes Virtuais de Aprendizagem (AVAs, a complexidade de implantação deste método é ainda maior, pois o facilitador nem sempre pode detectar possíveis problemas na colaboração, nem possui todas as informações necessárias para aplicar as técnicas de aprendizagem deste método. Desta forma, este artigo apresenta o processo de modelagem de um Sistema Multiagente (SMA de apoio à PBL. O SMA proposto foi modelado utilizando a metodologia MAS-CommonKADS+, que consiste em uma extensão da metodologia MAS-CommonKADS.

  10. ANALISIS PERHITUNGAN DAN PELAPORAN PAJAK PERTAMBAHAN NILAI PADA PT FAJAR MAS KARYATAMA

    Directory of Open Access Journals (Sweden)

    MARINDO PUTRA

    2017-05-01

    Full Text Available Value Added Tax (VAT is Tax that imposed on any apreciation in value of the goods or services in its circulation from producers to consumers. Through the calculation dan reporting is good, then the company may be said it has complied with the applicable rules in order to enhance the national development budget of the Government. PT Fajar Mas Karyatama as a company engaged intrade of goods subject to VAT, as in general make a purchase with Input Tax which may be credited. The purpose of this study to know whether the application of VAT and VAT underpayment or overpayment in accordance with law of VAT No. 42 of 2009. This study used a comparative method. The company will account for and report the delivery of Added Value Tax in the Notice Period of Added Value Tax (VAT Period SPT. VAT calculations made by company are the basis for the report required to implement Tax Laws for the companies. Conclusion is that application of VAT in the calculating and reporting of PT Fajar Mas Karyatama was almost accordance with the VAT Act applied and through the application of VAT, namely the purchase and sale of Taxable Goods so that the sum of the difference by the number of Input Tax or Output Tax generate VAT Less/More Pay at the end each mont, it is accordance with the Law of VAT No. 42 of 2009.

  11. Quality of Milk Pasteurized Produced By UD. Gading Mas During Storage in Refrigerator

    Directory of Open Access Journals (Sweden)

    Manik Eirry Sawitri

    2012-02-01

    Full Text Available The aim of this research was to study pasteurized milk quality produced by UD. Gading Mas on pH, Acidity, alcohol test and TPC during 5 days storage in refrigerator. On first day showed that  weight mass 1,06 (w/w; fat content 2,00 (g/100g,  protein content 3,02  (g/100g, Zn 1,67 ppm, Cu<0,005 ppm, Pb 0,02 ppm,  As  0,0120 ppm, Hg< 0,0002 ppm, Sn 1,60 ppm dan Cd < 0,001 ppm and organoleptic test included color, flavor and taste were normal. Pasteurized milk characteristic during 5 days refrigeration for pH were 6,57;6,58;6,73;6,60 and 6,50 respectively. Acidity were 1,147 %, 0,145 %, 0,145%, 0,157 %, 0,156 % and 0,175  % respectively. TPC were 6,16 x 101, 1,2. 104; 3,15.104, 0,42.106 and 3,5.108 respectively. It concluded that pasteurized milk produced by UD Gading Mas fulfilled SNI quality standard based on weight mass, pH, acidity, fat, protein, heavy metal content, organoleptic test and TPC.   Keywords: pasteurized milk, quality, refrigerator

  12. Elektroniskās naudas sistēmas WebMoney

    OpenAIRE

    Zablocka, Jelena

    2011-01-01

    Šī darba mērķis ir pamatojoties uz speciālo literatūru un pieejamu statistisko informāciju izskatīt jautājumu par elektroniskās naudas būtību, raksturot un parādīt tās veidus, analizēt un izskatīt elektroniskās naudas izmantošanas problēmas, izpētīt un norādīt tās izmantošanas perspektīvas, novērtēt tās uzskaites un kontroles operāciju problēmas, kas ir sastopamas, izmantojot elektronisko naudu praksē. Darbs sastāv no 5 nodaļām. Pirmajā nodaļā aplūkoti elektroniskās naudas jēdziens un ...

  13. Increasing brain angiotensin converting enzyme 2 activity decreases anxiety-like behavior in male mice by activating central Mas receptors.

    Science.gov (United States)

    Wang, Lei; de Kloet, Annette D; Pati, Dipanwita; Hiller, Helmut; Smith, Justin A; Pioquinto, David J; Ludin, Jacob A; Oh, S Paul; Katovich, Michael J; Frazier, Charles J; Raizada, Mohan K; Krause, Eric G

    2016-06-01

    Over-activation of the brain renin-angiotensin system (RAS) has been implicated in the etiology of anxiety disorders. Angiotensin converting enzyme 2 (ACE2) inhibits RAS activity by converting angiotensin-II, the effector peptide of RAS, to angiotensin-(1-7), which activates the Mas receptor (MasR). Whether increasing brain ACE2 activity reduces anxiety by stimulating central MasR is unknown. To test the hypothesis that increasing brain ACE2 activity reduces anxiety-like behavior via central MasR stimulation, we generated male mice overexpressing ACE2 (ACE2 KI mice) and wild type littermate controls (WT). ACE2 KI mice explored the open arms of the elevated plus maze (EPM) significantly more than WT, suggesting increasing ACE2 activity is anxiolytic. Central delivery of diminazene aceturate, an ACE2 activator, to C57BL/6 mice also reduced anxiety-like behavior in the EPM, but centrally administering ACE2 KI mice A-779, a MasR antagonist, abolished their anxiolytic phenotype, suggesting that ACE2 reduces anxiety-like behavior by activating central MasR. To identify the brain circuits mediating these effects, we measured Fos, a marker of neuronal activation, subsequent to EPM exposure and found that ACE2 KI mice had decreased Fos in the bed nucleus of stria terminalis but had increased Fos in the basolateral amygdala (BLA). Within the BLA, we determined that ∼62% of GABAergic neurons contained MasR mRNA and expression of MasR mRNA was upregulated by ACE2 overexpression, suggesting that ACE2 may influence GABA neurotransmission within the BLA via MasR activation. Indeed, ACE2 overexpression was associated with increased frequency of spontaneous inhibitory postsynaptic currents (indicative of presynaptic release of GABA) onto BLA pyramidal neurons and central infusion of A-779 eliminated this effect. Collectively, these results suggest that ACE2 may reduce anxiety-like behavior by activating central MasR that facilitate GABA release onto pyramidal neurons within the

  14. The Structure of the Fantômas Novel Series by Pierre Souvestre and Marcel Allain and the Problem of Seriality in Popular Literature

    Directory of Open Access Journals (Sweden)

    Kirill A. Chekalov

    2017-12-01

    Full Text Available The essay examines the structure of a 32-volume series of Fantômas novels created by Pierre Souvestre and Marcel Allain; it traces the origins and development of the serial genre and generic novelties related to seriality. The latter include a relative autonomy of each story in each volume and interconnection of the volumes via the figure of the criminal “slipping away” from the hands of justice. The study compares poetological techniques of the fabula development and points out specific features of the Belle époque reality as represented through the introduction of recognizable “cultural signs,” varia- tions of everyday incidents, and newspaper chronicle of criminal events. It also analyzes the image of Fantômas and other recurrent characters of the series (such as Juve, Fan- dor, Hélène, Lady Maud Beltham, etc. The authors examine para-literary features that can be traced in many other different forms such as TV series and graphic novels. They include (1 mythologization of the main character as embodiment of Evil, or a “criminal genius”; (2 confusion of the real and the fictional, verisimilar and extraordinary, horri- ble and comic based on the variations of literary and journalistic clichés; (3 repetition of plot patterns, (4 attempts to guess and to meet reader’s expectations.

  15. Research on the theory and methodology of integrating GIS and MAS and its application in simulating of pedestrians flows in a crowd's activity centre of Shanghai metropolitan

    Science.gov (United States)

    Liu, Miaolong; Chen, Peng

    2006-10-01

    Based on the development trend of research on urban morphology and its evolution from macro scale to micro scale, a new tight-coupling integrating method of GIS and MAS has been discussed briefly in this paper. After analyzing the characteristics and mechanism of pedestrian's flows in a crowds' activity center in a metropolitan, a prototype and mathematical expression of pedestrian's flows simulation have been put forward in the paper. A few key expressions and techniques for treating the specific behaviors of pedestrians flows, especially how the individuals of the flows make a decision to follow a original designed direction, how to make a decision whether stop or change his movement and select a new direction when the individuals meet a obstacle have been explored and discussed in detail. Using some tools provided by general GIS systems (such as ArcGIS 9) and a few specific programming languages, a new software system integrating GIS and MAS applicable for simulating pedestrians flows in a crowd activity centre has been developed successfully. Under the environment supported by the software system, as an applicable case, a dynamic evolution process of the pedestrian's flows (dispersed process for the spectators) in a crowds' activity center - The Shanghai Stadium has been simulated successfully. The successful simulating of a case of emergence when one or more exits emerge accidents will be very useful for managing and treating crowds' safety in a lot of assembling centers. At the end of the paper, some new research problems have been pointed out for the future.

  16. Determination of structural topology of a membrane protein in lipid bilayers using polarization optimized experiments (POE) for static and MAS solid state NMR spectroscopy

    Energy Technology Data Exchange (ETDEWEB)

    Mote, Kaustubh R. [University of Minnesota, Department of Chemistry (United States); Gopinath, T. [University of Minnesota, Department of Biochemistry, Molecular Biology and Biophysics (United States); Veglia, Gianluigi, E-mail: vegli001@umn.edu [University of Minnesota, Department of Chemistry (United States)

    2013-10-15

    The low sensitivity inherent to both the static and magic angle spinning techniques of solid-state NMR (ssNMR) spectroscopy has thus far limited the routine application of multidimensional experiments to determine the structure of membrane proteins in lipid bilayers. Here, we demonstrate the advantage of using a recently developed class of experiments, polarization optimized experiments, for both static and MAS spectroscopy to achieve higher sensitivity and substantial time-savings for 2D and 3D experiments. We used sarcolipin, a single pass membrane protein, reconstituted in oriented bicelles (for oriented ssNMR) and multilamellar vesicles (for MAS ssNMR) as a benchmark. The restraints derived by these experiments are then combined into a hybrid energy function to allow simultaneous determination of structure and topology. The resulting structural ensemble converged to a helical conformation with a backbone RMSD {approx}0.44 A, a tilt angle of 24 Degree-Sign {+-} 1 Degree-Sign , and an azimuthal angle of 55 Degree-Sign {+-} 6 Degree-Sign . This work represents a crucial first step toward obtaining high-resolution structures of large membrane proteins using combined multidimensional oriented solid-state NMR and magic angle spinning solid-state NMR.

  17. New marine commons along the Chilean coast – the management areas (MAs of Peñuelas and Chigualoco

    Directory of Open Access Journals (Sweden)

    Gloria L. Gallardo Fernández

    2011-09-01

    Full Text Available To halt degradation of benthic resources in Chile, management areas (MAs were set up under the Territorial Use Rights in Fisheries (TURFs framework in the late 1990s. Integrated into the global market, MAs have since expanded along the Chilean coast, involving thousands of small-scale artisanal fishers. This paper analyses how economic criteria relates to social and ecological performance of Chilean MAs, by applying TURFs, commons and co-management theory to two cases: MAs Peñuelas and Chigualoco. To collect and analyse data Participatory Rural Appraisal tools, interviews and official statistics and reports were used. Our results show that MAs’ economic benefits are connected to fluctuations on the global market. Adapting to changing world market prices then becomes paramount. TURFs’ main goal is ecological conservation, but achieving this seems to depend on meeting fishers’ livelihoods; failure to do so likely results in failure to meet conservation objectives. A serious weakness of the Chilean TURFs system is that it does not pay enough attention to fishers’ livelihoods or to the global market context. Furthermore, there is a strong relationship between good economic benefits and social sustainability. But irrespective of economic performance, fisher organizations have been empowered and gained increased resource control with the TURFs system. At policy level, a differentiated and more flexible system could be more suitable for existing heterogeneous MAs and their particular economic, social and ecological challenges. For improved economic sustainability and resource conservation, a system with multiple-species managing MAs could be promoted as well. Finally, to enhance theory of commons, co-management and TURFs, we argue for greater acknowledgement of TURFs’ social benefits in addition to economic assessments. More attention should also be paid to global market conditions of which MAs are dependent and in which they are embedded

  18. Lipid bilayer-bound conformation of an integral membrane beta barrel protein by multidimensional MAS NMR

    International Nuclear Information System (INIS)

    Eddy, Matthew T.; Su, Yongchao; Silvers, Robert; Andreas, Loren; Clark, Lindsay; Wagner, Gerhard; Pintacuda, Guido; Emsley, Lyndon; Griffin, Robert G.

    2015-01-01

    The human voltage dependent anion channel 1 (VDAC) is a 32 kDa β-barrel integral membrane protein that controls the transport of ions across the outer mitochondrial membrane. Despite the determination of VDAC solution and diffraction structures, a structural basis for the mechanism of its function is not yet fully understood. Biophysical studies suggest VDAC requires a lipid bilayer to achieve full function, motivating the need for atomic resolution structural information of VDAC in a membrane environment. Here we report an essential step toward that goal: extensive assignments of backbone and side chain resonances for VDAC in DMPC lipid bilayers via magic angle spinning nuclear magnetic resonance (MAS NMR). VDAC reconstituted into DMPC lipid bilayers spontaneously forms two-dimensional lipid crystals, showing remarkable spectral resolution (0.5–0.3 ppm for 13 C line widths and <0.5 ppm 15 N line widths at 750 MHz). In addition to the benefits of working in a lipid bilayer, several distinct advantages are observed with the lipid crystalline preparation. First, the strong signals and sharp line widths facilitated extensive NMR resonance assignments for an integral membrane β-barrel protein in lipid bilayers by MAS NMR. Second, a large number of residues in loop regions were readily observed and assigned, which can be challenging in detergent-solubilized membrane proteins where loop regions are often not detected due to line broadening from conformational exchange. Third, complete backbone and side chain chemical shift assignments could be obtained for the first 25 residues, which comprise the functionally important N-terminus. The reported assignments allow us to compare predicted torsion angles for VDAC prepared in DMPC 2D lipid crystals, DMPC liposomes, and LDAO-solubilized samples to address the possible effects of the membrane mimetic environment on the conformation of the protein. Concluding, we discuss the strengths and weaknesses of the reported

  19. Monitoramento do desenvolvimento infantil realizado no Brasil La monitoración del desarrollo infantil realizada en Brasil Monitoring of child development held in Brazil

    Directory of Open Access Journals (Sweden)

    Silvio Cesar Zeppone

    2012-12-01

    Full Text Available OBJETIVO: Revisar a literatura científica para verificar como a vigilância do desenvolvimento infantil vem sendo realizada no Brasil. FONTES DE DADOS: Pesquisa em bases de dados (PubMed, Medline, SciELO e Banco de Teses da Coordenação de Aperfeiçoamento de Pessoal de Nível Superior sobre estudos das práticas médicas em relação à vigilância e ao monitoramento do desenvolvimento infantil no Brasil, de 2000 a 2011. Os termos usados para pesquisa foram: vigilância de desenvolvimento infantil, intervenção precoce, triagem de desenvolvimento e testes de triagem de desenvolvimento. Foram encontrados dez textos referentes ao tema em estudo. Artigos originais, de revisão e teses foram revisados, bem como as listas de referências das publicações sobre o assunto. SÍNTESE DOS DADOS: Os estudos sobre a prática do monitoramento do desenvolvimento infantil no Brasil apontam uma importante falha, desde a formação do médico pediatra até a prática clínica, em relação a este tema. CONCLUSÕES: Há necessidade urgente, principalmente frente a uma população emergente de prematuros, que os pediatras façam uma reciclagem do conhecimento sobre o desenvolvimento infantil.OBJETIVO: Revisar la literatura científica para verificar cómo la vigilancia del desarrollo infantil viene siendo realizada en Brasil. FUENTES DE DATOS: Investigación en las bases de datos (Pubmed, Medline, SciELO y Base de Tesis CAPES sobre estudios de las prácticas médicas respecto a la vigilancia y monitoración del desarrollo infantil en Brasil de 2000 a 2011. Los términos usados para la investigación fueron: vigilancia de desarrollo infantil, intervención temprana, screening de desarrollo y pruebas de screening de desarrollo. Se encontraron 10 textos relativos al tema en estudio. Artículos originales, de revisión y tesis fueron revisados, así como las listas de referencias de las publicaciones sobre el tema. SÍNTESIS DE LOS DATOS: Los estudios sobre la pr

  20. Análise de prontuários de pacientes oncológicos quanto ao monitoramento auditivo Analyzing medical records of oncologic patients for audiological monitoring

    Directory of Open Access Journals (Sweden)

    Juliana Cunha da Costa

    2009-06-01

    Full Text Available OBJETIVO: realizar uma análise retrospectiva dos prontuários de pacientes oncológicos quanto ao monitoramento auditivo. MÉTODOS: foram utilizados os prontuários dos pacientes em atendimento durante os meses de setembro a novembro de 2006. A amostra constituiu-se de 25 prontuários de indivíduos com idade compreendida entre um e 53 anos. Foram analisados os dados quanto aos seguintes aspectos: idade, sexo, classificação do câncer, tempo de apresentação da doença, medicamentos utilizados, tempo de tratamento quimioterápico, doenças associadas, realização de avaliação otorrinolaringológica e audiológica. RESULTADOS: verificou-se a falta de acompanhamento audiológico e otorrinolaringológico. A Vincristina foi o medicamento ototóxico mais utilizado. O tipo de câncer de maior ocorrência no setor foi a Leucemia Linfocítica aguda. O tempo que os indivíduos apresentavam o câncer foi de aproximadamente 16 meses e o tempo de tratamento quimioterápico desses pacientes foi em torno de 11 meses. Observou-se, também, a presença de doenças associadas ao câncer nos indivíduos pesquisados. CONCLUSÃO: constatou-se a necessidade de se instalar programas de monitoramento auditivo nos setores que realizam quimioterapia em pacientes oncológicos, uma vez que este tratamento utiliza medicamentos ototóxicos em diversas patologias.PURPOSE: to accomplish a retrospective analysis for medical records of oncologic patient for audiological monitoring. METHODS: the patients' medical records in attendance were used from September to November, 2006. The sample constituted of 25 medical records of individuals with ages between 1 and 53-year old. The data were analyzed as for the following aspects: age, sex, cancer classification, time having the disease, used drugs, time of chemotherapy treatment, associated diseases, accomplishment of otorhinolaryngologic and audiologic evaluation. RESULTS: we verified the lack of audiologic and

  1. Low dose multi-detector CT of the chest (iLEAD Study): Visual ranking of different simulated mAs levels

    International Nuclear Information System (INIS)

    Ley-Zaporozhan, Julia; Ley, Sebastian; Krummenauer, Frank; Ohno, Yoshiharu; Hatabu, Hiroto; Kauczor, Hans-Ulrich

    2010-01-01

    Purpose: Detailed evaluation of the lung parenchyma might be impaired by use of low dose CT as image noise increases and subsequently image quality decreases. The aim of our study was to determine the accuracy of visual perception of differences in image quality and noise at low dose chest CT. Materials and methods: Forty-four patients suffering from emphysema underwent CT (Aquilion-16, 120 kV, 150 mAs, 1 mm-collimation). Original raw data were used for simulation of 10 different mAs settings from 10 mAs to 100 mAs in 10 mAs increments. Three representative hard copy images (carina, 4 cm above, 5 cm below) were printed for evaluation of lung parenchyma (high-resolution kernel, lung window) and mediastinum (soft-kernel, soft tissue window). Ranking of expected low mAs level was performed for lung and soft tissue separately based on visual perception by three-blinded chest radiologist independently. Results were compared to the real simulated mAs. Results: The accuracy for correct ranking of the original 150 mAs scan was 89% for lung and 86% for soft tissue while it was 99% for the simulated 10 mAs for both windows. In comparison to the lowest mAs a significant error increase was found for the lung at 60-100 mAs (with error increase of 30-47%) for reader-I; 60-100 mAs for (33-64%) for reader-II and 70-100 mAs (38-57%) for reader-III. For the soft tissue: 60-150 mAs (with error increase of 28-63%) for reader-I; 50-100 mAs (35-56%) for reader-II and 50-90 mAs (35-40%) for reader-III. Conclusion: Simulated dose levels below 60 mAs (=42 mAs eff ) were clearly differentiated from higher dose levels by all readers. Therefore, imaging doses could be lowered down to 60 mAs without a diagnostically relevant increase in noise impairing image quality.

  2. Premises and Limitations in Defining and Measuring Synergy from M&As

    Directory of Open Access Journals (Sweden)

    Aevoae George Marian

    2017-01-01

    Full Text Available Mergers and acquisitions are performed worldwide mainly because of synergy. Although many invoke the term synergy as the key motivation of why they engage in M&As, research has led us to understand that it is not very clear in terms of what it actually is. In the scientific literature, synergy is mostly defined as being “2+2=5”. Thus, we first thought that it can only be a positive effect. But, latter on, we found out that synergy is not only positive, it can be negative as well, known as negative synergy or dyssynergy. The purpose of this paper is to shed some light on what is synergy, how can we quantify and classify it and why acquiring firms tend to pay more for the target firm. We believe that there is a link between the amount of premium paid for a target firm and the expectations for synergy.

  3. 1H CSA parameters by ultrafast MAS NMR: Measurement and applications to structure refinement.

    Science.gov (United States)

    Miah, Habeeba K; Cresswell, Rosalie; Iuga, Dinu; Titman, Jeremy J

    2017-10-01

    A 1 H anisotropic-isotropic chemical shift correlation experiment which employs symmetry-based recoupling sequences to reintroduce the chemical shift anisotropy in ν 1 and ultrafast MAS to resolve 1 H sites in ν 2 is described. This experiment is used to measure 1 H shift parameters for L-ascorbic acid, a compound with a relatively complex hydrogen-bonding network in the solid. The 1 H CSAs of hydrogen-bonded sites with resolved isotropic shifts can be extracted directly from the recoupled lineshapes. In combination with DFT calculations, hydrogen positions in crystal structures obtained from X-ray and neutron diffraction are refined by comparison with simulations of the full two-dimensional NMR spectrum. The improved resolution afforded by the second dimension allows even unresolved hydrogen-bonded sites 1 H to be assigned and their shift parameters to be obtained. Copyright © 2017 Elsevier Inc. All rights reserved.

  4. Adding real data to detect emotions by means of smart resource artifacts in MAS

    Directory of Open Access Journals (Sweden)

    Jaime RINCÓN

    2016-12-01

    Full Text Available This article proposes an application of a social emotional model, which allows to extract, analyse, represent and manage the social emotion of a group of entities. Specifically, the application is based on how music can influence in a positive or negative way over emotional states. The proposed approach employs the JaCalIVE framework, which facilitates the development of this kind of environments. A physical device called smart resource offers to agents processed sensor data as a service. So that, agents obtain real data from a smart resource. MAS uses the smart resource as an artifact by means of a specific communications protocol. The framework includes a design method and a physical simulator. In this way, the social emotional model allows the creation of simulations over JaCalIVE, in which the emotional states are used in the decision-making of the agents.

  5. Assessing Heterogeneity of Osteolytic Lesions in Multiple Myeloma by 1H HR-MAS NMR Metabolomics

    Directory of Open Access Journals (Sweden)

    Laurette Tavel

    2016-10-01

    Full Text Available Multiple myeloma (MM is a malignancy of plasma cells characterized by multifocal osteolytic bone lesions. Macroscopic and genetic heterogeneity has been documented within MM lesions. Understanding the bases of such heterogeneity may unveil relevant features of MM pathobiology. To this aim, we deployed unbiased 1H high-resolution magic-angle spinning (HR-MAS nuclear magnetic resonance (NMR metabolomics to analyze multiple biopsy specimens of osteolytic lesions from one case of pathological fracture caused by MM. Multivariate analyses on normalized metabolite peak integrals allowed clusterization of samples in accordance with a posteriori histological findings. We investigated the relationship between morphological and NMR features by merging morphological data and metabolite profiling into a single correlation matrix. Data-merging addressed tissue heterogeneity, and greatly facilitated the mapping of lesions and nearby healthy tissues. Our proof-of-principle study reveals integrated metabolomics and histomorphology as a promising approach for the targeted study of osteolytic lesions.

  6. Marrero Regalado y Aguiar: El arte masónico oficial de la Postguerra en Canarias

    Directory of Open Access Journals (Sweden)

    David Martín López

    2008-12-01

    Full Text Available La masonería, como institución filantrópica y bien asentada durante la II República en España, fue totalmente rechazada por Franco desde su Alzamiento de 1936. Sin embargo, la protección oficial de la masonería en Canarias hizo que artistas masones como José Aguiar o como el arquitecto Marrero Regalado pudieran materializar su estética en numerosos proyectos para un nuevo Estado, en el que la concepción masónica del Ser Humano aparece como lenguaje encubierto y subversivo.

  7. Altimetria GNSS de precisão aplicada ao monitoramento da dinâmica sedimentar costeira de curta duração em escala regional

    Directory of Open Access Journals (Sweden)

    Marcelo Soares Teles Santos

    Full Text Available Este trabalho apresenta metodologia utilizada na altimetria GNSS de precisão aplicada em estudos costeiros de praias arenosas localizadas no Litoral Setentrional do Rio Grande do Norte, baseada em cálculo, modelagem e remoção da Componente Sistemática (CS do modelo geoidal. Os métodos foram aplicados e avaliados utilizando o modelo geoidal MAPGEO. O cálculo da CS foi realizado em Referências de Nível (RNs localizadas na área de estudo pela subtração entre as alturas geoidais gravimétricas, obtidas pelo modelo geoidal, e as geométricas, obtidas pelo posicionamento GNSS em RNs. Após modelagem e remoção da CS, por um modelo superfície polinomial quadrático, a CS calculada, com média de -0,498 m, Desvio Padrão (DP de 0,110 m e Erro Quadrático Médio (EQM de 0,509 m, passou a ter média nula, DP de 0,065 m e EQM de 0,062 m. Avaliações realizadas a partir de pontos de controle externos ao modelo mostraram que a metodologia forneceu acurácia decimétrica à altimetria GNSS, adequada ao monitoramento da elevada dinâmica sedimentar em ambientes costeiros, fato comprovado no estudo de caso apresentado.

  8. Controle de obras por RFID: sistema de monitoramento e controle para equipamentos de segurança no canteiro de obras

    Directory of Open Access Journals (Sweden)

    Victor Hugo Mazon de Oliveira

    Full Text Available Resumo É relevante o papel da Tecnologia da Informação e Comunicação (TIC aplicada à cadeia produtiva da construção, em particular na gestão de equipamentos de segurança, cujas práticas convencionais de controle têm mostrado eficiência limitada. Sendo assim, este trabalho apresenta o estudo do desenvolvimento de um sistema de monitoramento e controle remoto de equipamentos de segurança utilizando a tecnologia Radio Frequency Identification (RFID administrado pelo software, também desenvolvido nesta pesquisa, intitulado Controle de Obras por RFID. A rotina de ensaios combinou testes de laboratório para hospedagem e validação do sistema e experimentos em um canteiro de obras para a verificação do sistema em um ambiente real de construção. O modelo mostrou-se eficiente na identificação e localização dos equipamentos por meio da indicação de sua posição em imagens em planta. O modelo forneceu também relatórios gráficos e textuais que exibem as características de cada equipamento e apresentam os seguintes dados: nome, obra, local, marca, material, estado de conservação, previsão de revisão e responsável. A introdução da TIC no desenvolvimento de ferramentas, como o sistema proposto por este estudo, contribui para o avanço da gestão de equipamentos de segurança no canteiro de obras, podendo ser extrapolado para a gestão de outros componentes.

  9. PROGRAMA CIENTÍFICO PARA O MONITORAMENTO EM TEMPO REAL OU PÓS-PROCESSADO DAS IRREGULARIDADES IONOSFÉRICAS E CINTILAÇÃO DOS SINAIS GNSS

    Directory of Open Access Journals (Sweden)

    Vinícius Amadeu Stuani Pereira

    Full Text Available O Brasil é um dos países que mais sofrem os efeitos provocados pela ionosfera, principalmente os oriundos da Anomalia de Ionização Equatorial, irregularidades ionosféricas e cintilação dos sinais GNSS (Global Navigation Satellite System. Várias estratégias podem ser utilizadas para minimizar os efeitos, tais como: modelos ionosféricos, arquivos IONEX ou a combinação linear ion-free. Em se tratando do monitoramento da ionosfera a situação é diferente. A quantidade de instrumentos dedicados ao estudo da camada ionosférica é reduzida no âmbito brasileiro. Neste contexto foi desenvolvido o programa científico denominado Ion_Index, com objetivo de estimar indicadores dos níveis de irregularidades da ionosfera e de cintilação dos sinais GNSS em tempo real ou pós-processado, utilizando a infraestrutura já existente de dados GNSS de redes ativas públicas, como a RBMC, a GNSS-SP e a CALIBRA, transformando assim estações GNSS em estações monitoras da camada ionosférica. Dessa forma é proporcionado um aumento na resolução espacial das informações sobre o comportamento da ionosfera na região brasileira, permitindo um melhor entendimento e contribuindo para o desenvolvimento ou aprimoramento de modelos de mitigação. Experimentos utilizando dados de ionossondas digitais e de receptores PolaRxS-PRO da Septentrio (fontes externas comprovam a eficiência do programa

  10. Painel de Monitoramento Municipal: bases para a construção de um instrumento de gestão dos serviços de saúde

    Directory of Open Access Journals (Sweden)

    Sylvia Christina de Andrade Grimm

    Full Text Available Resumo OBJETIVO: descrever e analisar criticamente os caminhos percorridos e o referencial técnico utilizado na construção do Painel de Monitoramento da Secretaria Municipal da Saúde de São Paulo (SMS/SP, destacar suas potencialidades e limites para a tomada de decisão. MÉTODOS: pesquisa qualitativa, baseada na análise de documentos da gestão e entrevistas semiestruturadas com atores-chave; foi realizada uma análise temática do material, para compreensão das escolhas técnicas e caminhos percorridos na construção do Painel. RESULTADOS: o Painel disponibiliza relatórios numéricos e gráficos utilizando quatro modelos de análise estatística, de maneira a facilitar o acesso às informações pelos usuários de distintas instâncias da gestão e agilizar a análise de dados. CONCLUSÃO: o Painel de Monitoramento da SMS/SP propicia alternativas de análise para os distintos níveis de gestão, potencializando decisões descentralizadas; constitui uma estratégia ágil e adequada ao monitoramento, além da possibilidade de sua utilização em diferentes contextos de gestão e extensão territorial.

  11. Detecção de emissão espontânea de luz em ensaios de colimetria aplicados ao monitoramento de efluentes sanitários Spontaneous light emission in coliforms test applied to wastewater monitoring

    Directory of Open Access Journals (Sweden)

    Samuel Ricardo dos Santos

    2011-03-01

    Full Text Available No presente trabalho avaliou-se o potencial do emprego da técnica biofotônica ao monitoramento da qualidade microbiológica de efluentes sanitários, por meio da detecção de emissão ultrafraca de luz em testes envolvendo bactéria do grupo coliforme. Foram acompanhados os padrões de emissão de luz em câmara escura com o uso de efluente doméstico, antes e após tratamento, incubados em meio nutritivo à base de lactose e lauril triptose. O controle foi efetuado com o uso de cepa de Escherichia coli (ATCC 25.922, tendo seu crescimento sido monitorado por emissão de luz em câmara escura com fotomultiplicador acoplado. Os dados demonstraram que o monitoramento microbiológico pode ser efetuado por meio técnica biofotônica, podendo ser aplicado, com respostas rápidas, ao monitoramento microbiológico de efluentes, por meio de testes envolvendo coliformes.The spontaneous light emission of living systems emerge as a promising methodology that applied to microbiological in monitoring water can lead to short-term analysis. The present study evaluated the potential of biophoton measurements applied to wastewater monitoring by using ultraweak light emission in coliform tests. The procedure is based on photon-counting measurements inside a dark-chamber, of wastewater samples, before and after treatment, inoculated in nutrient presence/absence medium (lactose and lauryl triptose broth. Strain of Escherichia coli (ATCC 25,922 was used in control tests by monitoring the light emission inside a dark-chamber with an acoplade photomultiplier. The data showed that microbiological monitoring can be done by photon-counting in real-time applied to microbiological wastewater monitoring using coliform test.

  12. Badania jakości regeneratu ze zużytych mas ze spoiwem organicznym

    Directory of Open Access Journals (Sweden)

    R. Dańko

    2012-12-01

    Full Text Available W publikacji przedstawiono uzupełniające metody badań oraz aparaturę do oceny jakości regeneratu i tych właściwości masformierskich ze spoiwami utwardzanymi chemicznie, przygotowywanych z regeneratem, które są istotne dla kompleksowej oceny procesurecyklingu osnowy. Nowoczesne systemy oceny mas formierskich wymagają bardziej wnikliwego podejścia do czynników decydującychzarówno o ich przydatności technologicznej jak również o wpływie na otaczające środowisko naturalne. W tym kontekście pełna ocenajakości zregenerowanej osnowy wykracza poza zwyczajowo stosowane metody instrumentalne i wymaga ich uzupełnienia o bardziejzaawansowane aparaturowo metody badawcze. Pozwala to szerzej spojrzeć na ocenę zregenerowanej osnowy, zarówno w aspekcie jejużycia do sporządzania mas formierskich, jako substytutu świeżego piasku, ale także pod kątem ochrony środowiska. Do takichnowoczesnych metod można zaliczyć między innymi analizę ziarnową regeneratu za pomocą dyfrakcji laserowej, a także ocenęgazotwórczości masy formierskiej oraz identyfikację rodzaju emitowanych gazów i zawartości w nich gazów z grupy BTEX, które sąszczególnie niebezpieczne z punktu widzenia BHP.

  13. Role of Mas receptor in renal blood flow response to angiotensin-(1-7) in ovariectomized estradiol treated rats.

    Science.gov (United States)

    Saberi, Shadan; Dehghani, Aghdas; Nematbakhsh, Mehdi

    2016-01-01

    The angiotensin 1-7 (Ang 1-7), is abundantly produced in kidneys and antagonizes the function of angiotensin II through Mas receptor (MasR) or other unknown mechanisms. In the current study, the role of MasR and steroid hormone estrogen on renal blood flow response to Ang 1-7 administration was investigated in ovariectomized (OV) female rats. OV female Wistar-rats received estradiol (500 μg/kg/week) or vehicle for two weeks. In the day of the experiment, the animals were anesthetized, cannulated, and the responses including mean arterial pressure, renal blood flow (RBF), and renal vascular resistance at the constant level of renal perfusion pressure to graded infusion of Ang 1-7 at 0, 100 and 300 ng/kg/min were determined in OV and OV estradiol-treated (OVE) rats, treated with vehicle or MasR antagonist; A779. RBF response to Ang 1-7 infusion increased dose-dependently in vehicle (Pdose <0.001) and A779-treated (Pdose <0.01) animals. However, when MasR was blocked, the RBF response to Ang 1-7 significantly increased in OV animals compared with OVE rats (P<0.05). When estradiol was limited by ovariectomy, A779 increased RBF response to Ang 1-7 administration, while this response was attenuated in OVE animals.

  14. Modified Ashworth Scale (MAS) Model based on Clinical Data Measurement towards Quantitative Evaluation of Upper Limb Spasticity

    Science.gov (United States)

    Puzi, A. Ahmad; Sidek, S. N.; Mat Rosly, H.; Daud, N.; Yusof, H. Md

    2017-11-01

    Spasticity is common symptom presented amongst people with sensorimotor disabilities. Imbalanced signals from the central nervous systems (CNS) which are composed of the brain and spinal cord to the muscles ultimately leading to the injury and death of motor neurons. In clinical practice, the therapist assesses muscle spasticity using a standard assessment tool like Modified Ashworth Scale (MAS), Modified Tardiue Scale (MTS) or Fugl-Meyer Assessment (FMA). This is done subjectively based on the experience and perception of the therapist subjected to the patient fatigue level and body posture. However, the inconsistency in the assessment is prevalent and could affect the efficacy of the rehabilitation process. Thus, the aim of this paper is to describe the methodology of data collection and the quantitative model of MAS developed to satisfy its description. Two subjects with MAS of 2 and 3 spasticity levels were involved in the clinical data measurement. Their level of spasticity was verified by expert therapist using current practice. Data collection was established using mechanical system equipped with data acquisition system and LABVIEW software. The procedure engaged repeated series of flexion of the affected arm that was moved against the platform using a lever mechanism and performed by the therapist. The data was then analyzed to investigate the characteristics of spasticity signal in correspondence to the MAS description. Experimental results revealed that the methodology used to quantify spasticity satisfied the MAS tool requirement according to the description. Therefore, the result is crucial and useful towards the development of formal spasticity quantification model.

  15. X-ray fluorescent analysis on Indo-Pacific glass beads from Sungai Mas archaeological sites, Kedah, Malaysia

    International Nuclear Information System (INIS)

    Zuliskandar Ramli; Nik Hassan Shuhaimi; Nik Abdul Rahman; Abdul Latif Samian

    2011-01-01

    Sungai Mas was an ancient port-kingdom located on West Coast of Peninsula Malaysia in a district of Kota Kuala Muda, Kedah, Malaysia. The port-kingdom evolved as an entrepot since fifth century AD and continuously visited by international trader from India, China, Middle East and Europe until eighteenth century AD. Sungai Mas was also one of the Indo-Pacific beads making centers in Southeast Asia since sixth to thirteenth century AD and also produced pottery and brick. X-ray fluorescent analysis (XRF) on Sungai Mas Indo-Pacific beads is carried out to determine whether the glass beads originated from Arikamedu, India or locally made by community in Sungai Mas. Totally, twenty-two samples of beads and beads materials assayed by XRF were chosen. Contents of nine major elements and nine trace elements, which might be present of flux, stabilizer, colorants or opacifier were examined. The elements Si, Na, K, Ca, Fe, Al, Ti, Mn, Mg, Cu, Pb, Zr, Sr, Ba, La, U, Ni and Cr were detectable in all samples. The concentration of elements found are discussed in terms of flux, silica or lead base glass, color and/or opacity of the glass beads and glass samples. The result showed that Sungai Mas produced their own Indo-Pacific beads from sixth to thirteenth century AD. (author)

  16. The demands and benefits of ergonomics in Sri Lankan apparel industry: A case study at MAS holdings.

    Science.gov (United States)

    Abeysekera, John; Illankoon, Prasanna

    2016-10-17

    Apparel exports bring in sizeable foreign income to Sri Lanka. To protect and promote this industry is a paramount need. This can be carried out by applying Human Factors/Ergonomics (HFE) which has proved to control negative effects at work places. This paper reports a case study which describes the demands and benefits of HFE in MAS Holdings which owns a large share of the apparel industry in Sri Lanka. The study consisted of walk through observation survey, a questionnaire survey and ergonomic work place analysis followed by a training programme to selected employees in three companies. Positive responses to questionnaires revealed good ergonomic practices in the work places surveyed. Ergonomically unfit chairs and potential hazards e.g. exposure to noise and hot environment were detected. It is seen that MAS have introduced strategies originated by Toyota Production System viz. 5S, Kaizen, six sigma etc., which are in fact ergonomic methods. A progressive project MAS boast of viz. 'MAS Operating System' (MOS) empowers training and development to employees. MAS Holdings has adequately realized the benefits of applying HFE as evident by the number of awards received. Relevant companies were advised to take appropriate corrective measures to control the potential hazards.

  17. Uma nova abordagem para a implementação de um sistema multiagente para a configuração e o monitoramento da produção de pequenas séries

    OpenAIRE

    Roloff, Mário Lucio

    2014-01-01

    Tese (doutorado) - Universidade Federal de Santa Catarina, Centro Tecnológico, Programa de Pós-Graduação em Engenharia de Automação e Sistemas, Florianópolis, 2014 A Produção de Pequenas Séries (PPS) é um tipo de manufatura caracterizado pela alta diversidade de produtos a serem produzidos associada a tamanhos de lotes reduzidos - possivelmente unitários. Neste sistema de produção as tecnologias empregadas para configuração e monitoramento do processo devem priorizar a produção sem defeito...

  18. Comparison of radiographic technique by computer simulation

    International Nuclear Information System (INIS)

    Brochi, M.A.C.; Ghilardi Neto, T.

    1989-01-01

    A computational algorithm to compare radiographic techniques (KVp, mAs and filters) is developed based in the fixation of parameters that defines the images, such as optical density and constrast. Before the experience, the results were used in a radiography of thorax. (author) [pt

  19. The effect of FF-MAS on porcine cumulus-oocyte complex maturation, fertilization and pronucleus formation in vitro

    DEFF Research Database (Denmark)

    Færge, Inger; Strejcek, Frantisek; Laurincik, Jozef

    2006-01-01

    mechanically using a fine glass pipette under constant pH and in vitro fertilized with fresh semen (5 x 105 spermatozoa/ml). The presumptive zygotes were evaluated 18 h after fertilization. The addition of pFF increased the monospermic as well as the polyspermic penetration of oocytes. In the absence of p......FF, the addition of FF-MAS decreased the polyspermic penetration rate, wehreas FF-MAS in combination with pFF decreased monospermic and increased polyspermic penetration. The degeneration rate of ova decreased in the presence of FF-MAS irrespective of the presence or absence of pFF. In the absence of pFF, FF...

  20. 1H line width dependence on MAS speed in solid state NMR - Comparison of experiment and simulation

    Science.gov (United States)

    Sternberg, Ulrich; Witter, Raiker; Kuprov, Ilya; Lamley, Jonathan M.; Oss, Andres; Lewandowski, Józef R.; Samoson, Ago

    2018-06-01

    Recent developments in magic angle spinning (MAS) technology permit spinning frequencies of ≥100 kHz. We examine the effect of such fast MAS rates upon nuclear magnetic resonance proton line widths in the multi-spin system of β-Asp-Ala crystal. We perform powder pattern simulations employing Fokker-Plank approach with periodic boundary conditions and 1H-chemical shift tensors calculated using the bond polarization theory. The theoretical predictions mirror well the experimental results. Both approaches demonstrate that homogeneous broadening has a linear-quadratic dependency on the inverse of the MAS spinning frequency and that, at the faster end of the spinning frequencies, the residual spectral line broadening becomes dominated by chemical shift distributions and susceptibility effects even for crystalline systems.

  1. Relation Between Acid and Catalytic Properties of Chlorinated Gamma-Alumina. a 31p Mas Nmr and Ftir Investigation

    Directory of Open Access Journals (Sweden)

    Guillaume D.

    1999-07-01

    Full Text Available In this paper, we have studied the effect of chlorine on the surface properties of gamma-alumina, especially on their acid properties. The use of FTIR spectroscopy and 31P MAS NMR of adsorbed trimethylphosphine allows to propose a chlorination mechanism. To correlate the surface properties of these chlorinated gamma-alumina with their catalytic properties, we have used a model reaction, the cracking of n-heptane under reforming conditions. The analysis of the correlation between acid properties determined by 31P MAS NMR and the catalytic results (in terms of activities and selectivities allows to identify which sites are involved in the cracking reaction.

  2. Decision-making support system based on MAS for emergency response to nuclear accidents of marine pressurized-water reactor

    International Nuclear Information System (INIS)

    Chen Dengke; Zhang Dafa; Jiang Wei; Chen Yonghong

    2007-01-01

    Emergency decision-making to Marine Pressurized-Water Reactor (MPWR) was severely restricted by the complex environment. To enhance the emergency decision-making ability of MPWR, reducing the effect of emergencies, an emergency Decision-making Support System (DSS) which based on Multi-agent System (MAS) was presented. In the system, the HLA/RTI was used as the support environment, and the structure and the Control Agent (SCA), Analyse Agent (AA), Countermeasure Agent (CA), Evaluation Agent (EVA) and Environment Agent (ENA) were designed. The MAS were with the characteristics of autonomy, reactivity and initiative, which were fully used in the system to make effective decision for emergencies. (authors)

  3. Autolīzinga kompānijas AS "mogo" reklāmas kampaņu izstrāde, izmantojot Facebook reklāmas rīkus

    OpenAIRE

    Ābeltiņš, Elvis

    2017-01-01

    Diplomdarba tēma ir “Autolīzinga kompānijas AS “mogo” reklāmas kampaņu izstrāde, izmantojot Facebook reklāmas rīkus”. Vadošais sociālais tīkls Facebook nodrošina plašas reklāmas izvietošanas iespējas un tā auditorijas apjoms ir sasniedzis tradicionālajiem medijiem līdzvērtīgu izmēru. Darba analītiskajā daļā tiek kategorizētas digitālā mārketinga metodes, kā arī apkopota sociālo tīklu lietotāju statistika Latvijā un pasaulē. Projekta daļā autors salīdzina un analizē Facebook reklāmas izvietoša...

  4. Histopathologic alterations observed in fish gills as a tool in environmental monitoring Alterações histopatológicas observadas nas brânquias de peixes como instrumento no monitoramento ambiental

    Directory of Open Access Journals (Sweden)

    F. Flores-Lopes

    2011-02-01

    Full Text Available The gills of fish have a great external contact surface and are particularly sensitive to chemical and physical changes in the aquatic environment. The aim of this study was to examine the histopathologic alterations in the gills of Astyanax fasciatus and Cyanocharax alburnus and to determine if there is a correlation between the severity of the alterations and environmental degradation and if this biological system can be used as a tool for evaluating water quality in monitoring programmes. The gills of 107 specimens of Astyanax fasciatus and 116 of Cyanocharax alburnus were collected seasonally and processed using routine histologic techniques for fixing and embedding in paraffin and staining of sections with haematoxylin and eosin. The main alterations observed in both species were alteration of the structure of the epithelium, vacuolisation, hyperplasia of the epithelium of the primary lamella, epithelial lifting, and alteration of the structure and occurrence of aneurysms in the secondary lamella. The locations Gasometer and F. do Celupa were the ones that showed the highest frequencies of moderate and severe alterations as the highest "histopathologic alterations index" means. The most severe alterations were found to be related to the most impacted environment, indicating the presence of stressors in the water.As brânquias de peixes apresentam uma grande superfície de contato com o meio externo e são particularmente sensíveis às mudanças químicas e físicas do ambiente aquático. Este trabalho descreve as alterações histopatológicas observadas nas brânquias das espécies Astyanax fasciatus e Cyanocharax alburnus, testando-se a presença de correlação entre o grau de severidade das alterações e degradação ambiental. Pode ser utilizada na avaliação da qualidade da água em programas de monitoramento. Brânquias de 107 exemplares de Astyanax fasciatus e 116 de Cyanocharax alburnus, coletados sazonalmente, foram preparadas

  5. Proton chemical shift tensors determined by 3D ultrafast MAS double-quantum NMR spectroscopy

    International Nuclear Information System (INIS)

    Zhang, Rongchun; Mroue, Kamal H.; Ramamoorthy, Ayyalusamy

    2015-01-01

    Proton NMR spectroscopy in the solid state has recently attracted much attention owing to the significant enhancement in spectral resolution afforded by the remarkable advances in ultrafast magic angle spinning (MAS) capabilities. In particular, proton chemical shift anisotropy (CSA) has become an important tool for obtaining specific insights into inter/intra-molecular hydrogen bonding. However, even at the highest currently feasible spinning frequencies (110–120 kHz), 1 H MAS NMR spectra of rigid solids still suffer from poor resolution and severe peak overlap caused by the strong 1 H– 1 H homonuclear dipolar couplings and narrow 1 H chemical shift (CS) ranges, which render it difficult to determine the CSA of specific proton sites in the standard CSA/single-quantum (SQ) chemical shift correlation experiment. Herein, we propose a three-dimensional (3D) 1 H double-quantum (DQ) chemical shift/CSA/SQ chemical shift correlation experiment to extract the CS tensors of proton sites whose signals are not well resolved along the single-quantum chemical shift dimension. As extracted from the 3D spectrum, the F1/F3 (DQ/SQ) projection provides valuable information about 1 H– 1 H proximities, which might also reveal the hydrogen-bonding connectivities. In addition, the F2/F3 (CSA/SQ) correlation spectrum, which is similar to the regular 2D CSA/SQ correlation experiment, yields chemical shift anisotropic line shapes at different isotropic chemical shifts. More importantly, since the F2/F1 (CSA/DQ) spectrum correlates the CSA with the DQ signal induced by two neighboring proton sites, the CSA spectrum sliced at a specific DQ chemical shift position contains the CSA information of two neighboring spins indicated by the DQ chemical shift. If these two spins have different CS tensors, both tensors can be extracted by numerical fitting. We believe that this robust and elegant single-channel proton-based 3D experiment provides useful atomistic-level structural and dynamical

  6. Monitoramento de umidade do solo em videira utilizando tensiômetria | Soil moisture monitoring using vine tensiometry

    Directory of Open Access Journals (Sweden)

    Jucicléia Soares da Silva

    2016-04-01

    Knowledge of the factors related to the development of the vine is very important because it has implications for the production. Thus, the aim of this study was to determine the moisture, using the monitoring technique tensiometry fingerstick. The experiment was conducted in the agricultural area of the Federal Institute of Education, Science and Technology Pernambucano Hinterland on the campus located in Petrolina Rural Zone - PE and a privately owned table grape. They were carried out in the areas of collecting undisturbed soil samples to obtain the retention curve of water through the soil. Three batteries tensiometers were installed at depths of 0-0.3 and 0.3-0.6 m in the IF field and 0-0, 2, 0.2-0.4 and 0.4-0.6 m the privately owned area for table grapes and three batteries in the depth of 0-0.3 and 0.3-0.6 m in the IF area for wine grape. It was concluded that the moisture in the upper layers in the table grape and wine IF always stood above the field capacity, indicating problems of surface leaching. The moisture in the lower layers in the table grape on private property stood close and slightly above the field capacity, indicating deep leaching problems.

  7. Aplicação de índices das condições de vegetação no monitoramento em tempo quase real da seca em Moçambique usando NOAA_AVHRR- NDVI

    Directory of Open Access Journals (Sweden)

    Paulo Alberto Covele

    2011-12-01

    Full Text Available Este artigo tem por objetivo aplicar diferentes índices das condições de vegetação e avaliar suas diferenças e aptidão no monitoramento da distribuição espacial e temporal da seca em Moçambique com base em imagens NDVI da NOAA- AVHRR. Para tanto, avalia as differenças de aptidão dos índices das condições de vegetação especialmente o Índice das Condições de Vegetação (Vegetation Condition Index- VCI, Índice Padronizado de Vegetação (Standardized Vegetation Index- SVI e o Indicador de Productividade da Vegetação (Vegetation Productivity Indicator- VPI no monitoramento da seca em Moçambique. Estes índices são derivados a partir de imagens da Diferença Normalizada do Índice da Vegetação (Normalized Difference Vegetation Index- NDVI de 1981 a 2005, produzidas a partir dos canais 1 e 2 do sensor Advanced Very Higher Resolution Radiometer (AVHRR a bordo dos satélites da National Oceanic and Atmospheric Administration (NOAA.

  8. Monitoramento da qualidade físico-química da água do estuário do Rio Paraíba – Cabedelo, PB

    Directory of Open Access Journals (Sweden)

    Liz Jully Hiluey Correia

    2015-12-01

    Full Text Available Este trabalho teve como objetivo realizar o monitoramento da qualidade da água do estuário do Rio Paraíba, a fim de subsidiar ações de proteção e/ou recuperação do ambiente aquático, além de sinalizar o potencial risco de contaminação dos mariscos. O estudo foi desenvolvido em área de extração de mariscos, localizada no Rio Paraíba, em Cabedelo-PB. As amostras foram coletadas em triplicata, em seis pontos, entre os meses de maio e agosto de 2014. Os parâmetros (temperatura, turbidez, pH, condutividade elétrica, oxigênio dissolvido (OD, amônia, nitrito e fosfato foram avaliados seguindo a metodologia do APHA (1998. Os resultados ratificam a existência de atividades causadoras da elevada concentração do teor de amônia e do baixo nível de OD no ambiente aquático. A dinâmica da maré e as condições físicas do ambiente aceleraram a reação de nitrificação. As concentrações de fosfato e nitrito estiveram dentro do limite máximo estabelecido na resolução n° 357/05 do CONAMA. Tendo em vista a potencialização dos riscos de contaminação dos mariscos devido à poluição hídrica, faz-se necessária uma intervenção dos órgãos fiscalizadores quanto ao lançamento direto de resíduos sólidos e líquidos no estuário, de forma a garantir a integridade do ambiente aquático e a saúde dos consumidores.

  9. Algoritmo para monitoramento da incidência da malária na Amazônia brasileira, 2003 a 2010

    Directory of Open Access Journals (Sweden)

    Rui Moreira Braz

    2014-03-01

    Full Text Available OBJETIVO: Avaliar um algoritmo para detecção da variação da incidência da malária nos municípios da Amazônia brasileira. MÉTODOS: Avaliou-se um sistema de monitoramento automatizado, baseado em um algoritmo desenvolvido anteriormente pelos autores. O algoritmo utiliza o diagrama de controle por quartis para classificação dos municípios em quatro grupos, conforme a variação da incidência da malária: grupo 1 (redução da incidência-aqueles com incidência abaixo dos valores esperados; grupo 2 (incidência esperada-aqueles com incidência dentro dos valores esperados; grupo 3 (epidemia-aqueles com incidência acima dos valores esperados; grupo 4 (caso esporádico-aqueles com apenas um caso durante o ano. O período de análise foi de 2003 a 2010. Foram estudados todos os municípios existentes nos nove estados que compõem a Amazônia brasileira (805 municípios em 2003 e 807 a partir de 2004. RESULTADOS: Com base nessa metodologia, os municípios da região foram assim classificados: grupo 1, 152 municípios (18,8% da região em 2003 e 109 (13,5% em 2010; grupo 2, 206 (25,6% em 2003 e 331 (41,0% em 2010; grupo 3, 391 (48,6% em 2003 e 308 (38,2% em 2010; e grupo 4, 56 (7,0% em 2003 e 59 (7,3% em 2010. CONCLUSÕES: O algoritmo possibilitou verificar que, na Amazônia brasileira, o número de municípios com epidemias de malária em 2010 diminuiu em relação a 2003, enquanto o número de municípios com incidência esperada aumentou. No mesmo período, houve pouca variação no número de municípios com redução da incidência e daqueles com casos esporádicos.

  10. Monitoramento não invasivo baseado na biorreatância revela instabilidade hemodinâmica significativa durante cesárea eletiva sob raquianestesia

    Directory of Open Access Journals (Sweden)

    Anne Doherty

    2011-06-01

    Full Text Available JUSTIFICATIVA E OBJETIVOS: O monitoramento da pressão arterial oferece uma compreensão limitada das consequências hemodinâmicas da raquianestesia para cesariana. O objetivo deste estudo foi avaliar, com o auxílio do monitor de débito cardíaco não invasivo baseado na biorreatância, as alterações hemodinâmicas durante cesariana eletiva sob raquianestesia, na qual doses intermitentes de fenilefrina foram utilizados para prevenir e tratar a hipotensão. MÉTODOS: Este estudo observacional foi realizado após aprovação da comissão de ética na pesquisa e assinatura do consentimento informado. Pacientes saudáveis marcadas para cesariana eletiva sob raquianestesia foram avaliadas. Doses intermitentes de fenilefrina foram administrados para manter a pressão arterial sistólica nos níveis basais e as pacientes foram avaliadas com o monitor de débito cardíaco não invasivo baseado na biorreatância. Os dados hemodinâmicos foram colhidos continuamente no momento basal e durante os períodos pós-raquianestesia e pós-nascimento do feto. Os dados foram analisados usando ANOVA para modelos mistos e um p < 0,05 foi considerado significativo. RESULTADOS: A pressão arterial sistólica foi mantida entre 79,2% ± 14,2 e 105,9% ± 10,0 dos valores basais durante o período pós-raquianestesia e 78,4% ± 11,13 e 100,9% ± 10,7 dos valores basais no período pós-nascimento do feto (média ± DP. Flutuações significativas foram observadas na pressão arterial sistólica, frequência cardíaca e débito cardíaco no período pós-nascimento. CONCLUSÕES: Um novo monitor não invasivo, baseado na biorreatância, revelou flutuações hemodinâmicas significativas durante a cesariana sob raquianestesia, a despeito das tentativas de manter a pressão arterial nos níveis basais com doses intermitentes de fenilefrina.

  11. Can Memory Assessment Services (MAS) in England be categorized? A national survey.

    Science.gov (United States)

    Chrysanthaki, T; Fernandes, B; Smith, S; Black, N

    2017-12-01

    The effectiveness and efficiency of memory assessment services (MASs) is unknown. Our aim was to determine if a typology can be constructed, based on shared structural and process characteristics, as a basis for a non-randomized evaluation of their effectiveness and cost-effectiveness. Survey of random sample of 73 MASs in 2015; comparison of characteristics and investigation of inter-correlation. It was not possible to group characteristics to form the basis of a typology of MASs. However, there was considerable variation in staff numbers (20-fold), new patients per whole-time equivalent (WTE) staff (20-fold), skill mix and the nurse:doctor ratio (1-10). The operational performance also varied: first appointments (50-120 minutes); time for first follow-up (2-12 weeks); frequency of follow-up in first year (1-5). These differences were not associated with the number of new patients per WTE staff or the accreditation status of the MAS. Post diagnosis, all MASs provided pharmacological treatment but the availability of non-pharmacological support varied, with half providing none or only one intervention while others providing four or more. In the absence of any clear typology, evaluation of MASs will need to focus on the impact of individual structural and process characteristics on outcomes. © The Author 2017. Published by Oxford University Press on behalf of Faculty of Public Health. All rights reserved. For permissions, please e-mail: journals.permissions@oup.com

  12. MAS Based Distributed Automatic Generation Control for Cyber-Physical Microgrid System

    Institute of Scientific and Technical Information of China (English)

    Zhongwen Li; Chuanzhi Zang; Peng Zeng; Haibin Yu; Hepeng Li

    2016-01-01

    The microgrid is a typical cyber-physical microgrid system(CPMS). The physical unconventional distributed generators(DGs) are intermittent and inverter-interfaced which makes them very different to control. The cyber components,such as the embedded computer and communication network,are equipped with DGs, to process and transmit the necessary information for the controllers. In order to ensure system-wide observability, controllability and stabilization for the microgrid,the cyber and physical component need to be integrated. For the physical component of CPMS, the droop-control method is popular as it can be applied in both modes of operation to improve the grid transient performance. Traditional droop control methods have the drawback of the inherent trade-off between power sharing and voltage and frequency regulation. In this paper, the global information(such as the average voltage and the output active power of the microgrid and so on) are acquired distributedly based on multi-agent system(MAS). Based on the global information from cyber components of CPMS, automatic generation control(AGC) and automatic voltage control(AVC)are proposed to deal with the drawback of traditional droop control. Simulation studies in PSCAD demonstrate the effectiveness of the proposed control methods.

  13. MAS Based Distributed Automatic Generation Control for Cyber-Physical Microgrid System

    Institute of Scientific and Technical Information of China (English)

    Zhongwen Li; Chuanzhi Zang; Peng Zeng; Haibin Yu; Hepeng Li

    2016-01-01

    The microgrid is a typical cyber-physical micro grid system (CPMS).The physical unconventional distributed generators (DGs) are intermittent and inverter-interfaced which makes them very different to control.The cyber components,such as the embedded computer and communication network,are equipped with DGs,to process and transmit the necessary information for the controllers.In order to ensure system-wide observability,controllability and stabilization for the microgrid,the cyber and physical component need to be integrated.For the physical component of CPMS,the droop-control method is popular as it can be applied in both modes of operation to improve the grid transient performance.Traditional droop control methods have the drawback of the inherent trade-off between power sharing and voltage and frequency regulation.In this paper,the global information (such as the average voltage and the output active power of the microgrid and so on) are acquired distributedly based on multi-agent system (MAS).Based on the global information from cyber components of CPMS,automatic generation control (AGC) and automatic voltage control (AVC) are proposed to deal with the drawback of traditional droop control.Simulation studies in PSCAD demonstrate the effectiveness of the proposed control methods.

  14. Healthcare benefits linked with Below Poverty Line registration in India: Observations from Maharashtra Anaemia Study (MAS).

    Science.gov (United States)

    Ahankari, Anand; Fogarty, Andrew; Tata, Laila; Myles, Puja

    2017-01-01

    A 2015 Lancet paper by Patel et al. on healthcare access in India comprehensively discussed national health programmes where some benefits are linked with the country's Below Poverty Line (BPL) registration scheme. BPL registration aims to support poor families by providing free/subsidised healthcare. Technical issues in obtaining BPL registration by poor families have been previously reported in the Indian literature; however there are no data on family assets of BPL registrants. Here, we provide evidence of family-level assets among BPL registration holders (and non-BPL households) using original research data from the Maharashtra Anaemia Study (MAS). Social and health data from 287 pregnant women and 891 adolescent girls (representing 1178 family households) across 34 villages in Maharashtra state, India, were analysed. Several assets were shown to be similarly distributed between BPL and non-BPL households; a large proportion of families who would probably be eligible were not registered, whereas BPL-registered families often had significant assets that should not make them eligible. This is likely to be the first published evidence where asset distribution such as agricultural land, housing structures and livestock are compared between BPL and non-BPL households in a rural population. These findings may help planning BPL administration to allocate health benefits equitably, which is an integral part of national health programmes.

  15. Quality Analysis of Ceramic Tent Product With Six Sigma Method in PT. Mas Keramik KIA

    Science.gov (United States)

    Suryadi, A.; Ardiansyah P., F.; Ngatilah, Y.

    2018-01-01

    PT. KIA Keramik Mas is a company engaged in manufacturing, which produces ceramic tiles, one of the problems faced by this company is the number of defects found, in the July - December 2015 amounted to 6,259,945 units producing tiles and discovered defects by 960 683 units with an object research is ceramic tile products, among some of the defects found several characteristics of defects that occur include rugged body, coincide, grainy, scratched, and colors distorted. The purpose of this study was to determine the quality of the product and propose improvements that reduce the number of such defects, using quality control methods that Six Sigma. Six Sigma is used to generate a defect that does not exceed 3.4 DPMO (defects per million opportunities) or zero defect which is an approach to calculate the number of defects per million possibilities. Average quality ceramic tile products during the month of July - December 2015 was on a sigma of 3.37 with DPMO of 30 586, which means that one million opportunities that exist there will be 30 586 (3,05%) the possibility that the process of making the ceramic tile defect or defects occur, so to get to the required target of Six Sigma improvement.

  16. Nutritional value of Rosa spp. l. and Cornus mas l. fruits, as affected by storage conditions

    Directory of Open Access Journals (Sweden)

    Craita-Maria Rosu

    2011-12-01

    Full Text Available A comparison between two storage methods (freezing and drying of fruits, in terms of ascorbic acid, carotenes, total sugar and protein content in Rosa spp. L. species and Cornus mas L. was performed. In the dried rose hips, the major losses were registered at the level of ascorbic acid content (32.04–50.25 %, followed by carotenes (30.85–52.08 %, total sugar (21.57–34.6 % and protein content (21.33–46.89 %. The freezing method resulted in a better preservation of ascorbic acid (only 19.80–29.21 % decrease and total sugar content (3.41–12.94 % increase. In the preserved cornelian cherry fruits, no statistically significant differences were registered between fruits categories, except carotene content, which was dramatically decreased in dried fruits (88.23 %. For cornelian cherry fruits, both storage methods induced a decrease of ascorbic acid and protein contents (57.60 and 46.32 % and an increase of total sugar level (37.60 %.

  17. Tendencias clave para el tercer gobierno del MAS, Bolivia 2015-2019

    Directory of Open Access Journals (Sweden)

    Xavier Albó

    2016-03-01

    Esta presentación tiene como trasfondo el Plan Nacional de Desarrollo y pretende resaltar algunos de los logros del presidente Evo Morales y los desafíos que enfrenta en su tercer gobierno (2015-2019. Comienza revisando información demográfica básica, según el Censo de 2012, para luego centrarse en la economía: los hidrocarburos, la minería, la producción agropecuaria y la ecología. El boom de la quinua, la expansión de la frontera agrícola y la suspensión de la construcción de una carretera que atraviese el TIPNIS son algunos de los temas que se discuten. Internacionalmente, hay motivos de optimismo con relación a la demanda marítima de Bolivia, mientras que, a nivel nacional, el MAS aseguró una victoria parlamentaria en el año 2014. Las reformas menos exitosas son las del órgano judicial. La presentación termina revisando los movimientos sociales que permitieron la formación la de Asamblea Constituyente y el asunto de la autonomía municipal, departamental e indígena.

  18. Characterization of coal structure by CP/MAS carbon-13 NMR spectrometry

    International Nuclear Information System (INIS)

    Yoshida, T.; Maekawa, Y.

    1987-01-01

    Cross-polarization (CP)/magic angle spinning (MAS) carbon-13 nuclear magnetic resonance (n.m.r.) spectrometry has been applied to the analysis of the whole structures of different ranks of coal. Three basic structural parameters, namely carbon aromaticity fa, new carbon aromaticity fa', and atomic H/C ratio for the hypothetical unsubstituted aromatic nuclei Haru/Car, were derived from the combined data of ultimate analysis, the distributions of carbon and oxygen functional groups obtained from the spectrum and the distribution of four types of methylene carbon groups in coal. Both fa and fa' values generally increased with coal rank and ranged from 0.51 to 0.71 and from 0.62 to 0.76, respectively. Haru/Car value tended to decrease with coal rank although the value was greatly affected by the types of hydroaromatic methylene carbons to aromatic rings. The values indicated that lower-rank coals consisted mainly of 1-3 aromatic rings, and higher-rank coals, 3-5 aromatic rings. 24 refs.; 5 figs.; 4 tabs

  19. The Neuroprotective Effect of Cornus mas on Brain Tissue of Wistar Rats

    Directory of Open Access Journals (Sweden)

    Renata Francik

    2014-01-01

    Full Text Available Cornelian cherry (Cornus mas is a valuable source of phenolic antioxidants. Flavonoid derivatives as nonenzymatic antioxidants are important in the pathophysiology of many diseases including neurological disorders (e.g., Alzheimer’s disease or heart disease. In this study, we examined the effect of an addition of freeze-dried fruit of cornelian cherry on three types of diets: control diet, fructose diet, and diet enriched in fats (high-fat diet. This effect was studied by determining the following antioxidant parameters in both brain tissue and plasma in rats: catalase, ferric reducing ability of plasma, paraoxonase, protein carbonyl groups, and free thiol groups. Results indicate that both fructose diet and high-fat diet affect the antioxidant capacity of the organism. Furthermore, an addition of cornelian cherry resulted in increased activity of catalase in brain tissue, while in plasma it caused the opposite effect. In turn, with regard to paraoxonase activity in both brain tissue and plasma, it had a stimulating effect. Adding cornelian cherry to the tested diets increased the activity of PON in both tested tissues. Moreover, protective effect of fruits of this plant was observed in the process of oxidation of proteins by decreasing levels of protein carbonyl groups and thiol groups in brain tissue as well as in plasma.

  20. CINEMA E LITERATURA: mediações em “Bonitinha, mas ordinária”

    Directory of Open Access Journals (Sweden)

    Elen Duarte MIRANDA e SILVA

    2011-01-01

    Full Text Available A partir de um intenso movimento de metamorfoses técnicas e narrativas, o cinema passou de seu estado inicial de mero copiador da realidade à categoria de arte e vem estabelecendo uma forte e íntima relação de diálogo com a literatura. É a partir dessa relação que o destaque dessa pesquisa consiste em uma análise sobre a literatura dramatúrgica de Nelson Rodrigues e sua respectiva adaptação pelo cinema de Braz Chediak, com ênfase no trabalho em parceria entre escritor e cineasta:Bonitinha, mas ordinária: até que ponto o filme se subordina ao texto? Há inventividade na inscrição cinematográfica de Braz? Qual o teor criativo da narrativa do cineasta? Em que instância o filme foi produzido? Qual a tendência estética adotada pelo diretor? Essas questões são desvendadas através da colaboração teórica de Roland Barthes, Ismail Xavier, Sábato Malgadi e Robert Stam, bem como alguns outros estudiosos que pensam cinema e literatura e entram em cena para adensarem a análise feita sobre o objeto colocado em foco.

  1. Characterization of cornelian cherry (Cornus mas L. genotypes - genetic resources for food production in Czech Republic

    Directory of Open Access Journals (Sweden)

    Sochor Jiri

    2014-01-01

    Full Text Available The aim of the study was to determine and compare both technological properties and polyphenol content in fruits of eight cornellian cherry (Cornus mas L. cultivars from Czech Republic. The fruits of cultivar ´Vydubeckij´ had the highest dry matter (17.4% and soluble solid (15.8% content among searched cultivars. The highest crude protein and phosphorus values were determined in the fruits of the ´Titus´ cultivar as 10.9 g of crude protein and 435 mg of phosphorus for per kg fresh weight (FW base. The ´Elegantnyj´ and ´Vydubeckij´ cultivars are found to be more suitable for canning industry. The fruits of the ´Vydubeckij´ cultivar contained 10.8 g of pectin and 22.4 g of citric acid per kg fresh weight base, and could be important for technological use because of their excellent gelling ability. ´Devin´,´Vydubeckij´ and ´Titus´ cultivars had the most valuable source of chlorogenic acid (135.6, 110.9 and 115.1 mg per 100 g FW, respectively and quercetin (24.9, 25.2 and 24.2 mg per 100 g FW, respectively. This work should contribute to the popularization of this fruit specie as a valuable source of technological parameters for human nutrition and the canning industry.

  2. Conformational analysis of capsaicin using 13C, 15N MAS NMR, GIAO DFT and GA calculations

    Science.gov (United States)

    Siudem, Paweł; Paradowska, Katarzyna; Bukowicki, Jarosław

    2017-10-01

    Capsaicin produced by plants from genus Capsicum exerts multiple pharmacological effects and has found applications in food and pharmaceutical industry. The alkaloid was studied by a combined approach: solid-state NMR, GA conformational search and GIAO DFT methods. The 13C CPMAS NMR spectra were recorded using variable contact time and dipolar dephasing experiments. The results of cross-polarization (CP) kinetics, such as TCP values and long T1ρH (100-200 ms), indicated that the capsaicin molecule is fairly mobile, especially at the end of the aliphatic chain. The15N MAS NMR spectrum showed one narrow signal at -255 ppm. Genetic algorithm (GA) search with multi modal optimization was used to find low-energy conformations of capsaicin. Theoretical GIAO DFT calculations were performed using different basis sets to characterize five selected conformations. 13C CPMAS NMR was used as a validation method and the experimental chemical shifts were compared with those calculated for selected stable conformers. Conformational analysis suggests that the side chain can be bent or extended. A comparison of the experimental and the calculated chemical shifts indicates that solid capsaicin does not have the same structure as those established by PWXRD.

  3. KERAGAAN PERTUMBUHAN BENIH IKAN MAS (Cyprinus carpio STRAIN MAJALAYA, LOKAL BOGOR DAN RAJADANU DI KOLAM CIJERUK, BOGOR-JAWA BARAT

    Directory of Open Access Journals (Sweden)

    Otong Zenal Arifin

    2016-11-01

    Full Text Available Penelitian ini bertujuan untuk mendapatkan strain ikan mas yang memiliki keragaan pertumbuhan yang baik sebagai spesies kandidat untuk program seleksi. Tiga strain ikan mas (majalaya, lokal Bogor, dan rajadanu dipelihara dalam jaring yang diletakkan di kolam Instalasi Penelitian Cijeruk, Bogor selama 6 minggu. Hasil penelitian menunjukkan bahwa tidak ada perbedaan nyata untuk parameter pertambahan bobot dan sintasan dari 3 strain ikan mas yang diuji, sedangkan untuk pertambahan panjang individual (mm per bulan ada perbedaan yang sangat nyata (P<0,05. Strain ikan mas rajadanu memiliki pertambahan panjang terbaik (16,0 ± 1,41 dan berbeda dengan majalaya (10,3 ± 4,50 serta lokal (10,8 ± 2,06. Objective of this study is to produce good performance of common carp by comparing three promising strains majalaya, local, and rajadanu. The study was carry out using floating net cages placed in earthen pond at The Cijeruk Germ Plasm Research Station. During the study, growth and survival rate were observed were observed for six weeks. The results indicated there was no significant difference for growth of weight and survival rate. However, growth of standard length was significantly different (P<0.05. Rajadanu made the best growth of standard length (16.0 ± 1.41 and was different from majalaya (10.3 ± 4.50 and local strain (10.8 ± 2.06.

  4. Exploring high-resolution magic angle spinning (HR-MAS) NMR spectroscopy for metabonomic analysis of apples.

    Science.gov (United States)

    Vermathen, Martina; Marzorati, Mattia; Vermathen, Peter

    2012-01-01

    Classical liquid-state high-resolution (HR) NMR spectroscopy has proved a powerful tool in the metabonomic analysis of liquid food samples like fruit juices. In this paper the application of (1)H high-resolution magic angle spinning (HR-MAS) NMR spectroscopy to apple tissue is presented probing its potential for metabonomic studies. The (1)H HR-MAS NMR spectra are discussed in terms of the chemical composition of apple tissue and compared to liquid-state NMR spectra of apple juice. Differences indicate that specific metabolic changes are induced by juice preparation. The feasibility of HR-MAS NMR-based multivariate analysis is demonstrated by a study distinguishing three different apple cultivars by principal component analysis (PCA). Preliminary results are shown from subsequent studies comparing three different cultivation methods by means of PCA and partial least squares discriminant analysis (PLS-DA) of the HR-MAS NMR data. The compounds responsible for discriminating organically grown apples are discussed. Finally, an outlook of our ongoing work is given including a longitudinal study on apples.

  5. A preliminary study of the relation between adsorption and CP-MAS-NMR characteristics of fused silica model substrates

    NARCIS (Netherlands)

    Scholten, A.B.; Janssen, J.G.M.; Haan, de J.W.; Cramers, C.A.M.G.; Sandra, P.J.F.; Devos, G.; Sandra, P.

    1993-01-01

    The fumed silica model substrate Aerosil was trimethylsilylated to different extents and studied by the combination of IGC and 29Si CP-MAS-NMR. Dihydroxydisiloxane groups were shown to be chemically more reactive than monohydroxytrisiloxane groups. Chromatographic experiments showed that these

  6. Study on MAs transmutation of accelerator-driven system sodium-cooled fast reactor loaded with metallic fuel

    International Nuclear Information System (INIS)

    Han Song; Yang Yongwei

    2007-01-01

    Through the analysis of the effect of heavy metal actinides on the effective multiplication constant (k eff ) of the core in accelerator-driven system (ADS) sodium-cooled fast reactor loaded with metallic fuel, we gave the method for determining fuel components. the characteristics of minor actinides (MAs) transmutation was analyzed in detail. 3D burn-up code COUPLE, which couples MCNP4c3 and ORIGEN2, was applied to the neutron simulation and burn up calculation. The results of optimized scheme shows that adjusting the proportion of 239 Pu and maintaining the value during the burn-up cycle is an efficient method of designing k eff and keeping stable during the burn-up cycle. Spallation neutrons lead to the neutron spectrum harder at inner core than that at outer core. It is in favor of improving MA's fission cross sections and the capture-to-fission ratio. The total MAs transmutation support ratio 8.3 achieves excellent transmutation effect. For higher flux at inner core leads to obvious differences on transmutation efficiency,only disposing MAs at inner core is in favor of decreasing the loading mass and improving MAs transmutation effect. (authors)

  7. States' Participation Guidelines for Alternate Assessments Based on Modified Academic Achievement Standards (AA-MAS) in 2008. Synthesis Report 71

    Science.gov (United States)

    Lazarus, Sheryl S.; Rogers, Christopher; Cormier, Damien; Thurlow, Martha L.

    2008-01-01

    Federal regulations (U.S. Department of Education, 2007a) provide states with the flexibility to offer an alternate assessment based on modified academic achievement standards (AA-MAS). This assessment option is for a small group of students with disabilities who can make significant progress, but may not reach grade-level achievement within the…

  8. Improved quantification of alite and belite in anhydrous Portland cements by 29Si MAS NMR: Effects of paramagnetic ions

    DEFF Research Database (Denmark)

    Poulsen, Søren Lundsted; Kocaba, Vanessa; Le Saoût, Gwenn

    2009-01-01

    The applicability, reliability, and repeatability of 29Si MAS NMR for determination of the quantities of alite (Ca3SiO5) and belite (Ca2SiO4) in anhydrous Portland cement was investigated in detail for 11 commercial Portland cements and the results compared with phase quantifications based...

  9. EVALUASI DAYA TAHAN IKAN MAS HASIL SELEKSI BERDASARKAN MARKA MOLEKULER MHC-II TERHADAP INFEKSI KOI HERPES VIRUS

    Directory of Open Access Journals (Sweden)

    Erma Primanita Hayuningtyas

    2015-03-01

    mengevaluasi daya tahan benih ikan mas F-1 terseleksi terhadap infeksi KHV melalui uji tantang. Sebagai pembanding, digunakan ikan mas populasi benih F-1 non-seleksi dan populasi benih ikan mas dari unit pembenihan rakyat (UPR. Ikan uji berupa benih ikan mas Rajadanu berumur dua bulan dengan bobot ratarata 5,5±0,5 g. Jumlah benih pada masing-masing wadah perlakuan sebanyak 30 ekor dengan tiga kali pengulangan. Wadah pengujian berupa akuarium berukuran 40 cm x 60 cm x 40 cm dengan kepadatan 1 ekor/L. Parameter yang diamati adalah sintasan, deteksi KHV, analisis ekspresi gen MHC-II, dan gambaran darah ikan. Hasil penelitian menunjukkan bahwa populasi benih F-1 terseleksi memiliki daya tahan lebih baik dengan sintasan 93,33% dibandingkan populasi benih F-1 non-seleksi sebesar 85,55% dan populasi benih dari UPR sebesar 81,11%. Daya tahan yang tinggi pada populasi benih F-1 terseleksi didukung oleh hasil deteksi KHV yang negatif dan ersentase jumlah limfosit yang lebih tinggi sebesar 91,67%; serta rendahnya persentase monosit dan heterofil, selain itu, tidak adanya eosinofil dan basofil. Ekspresi gen MHC-II terdeteksi pada berbagai organ, ekspresi tertinggi ditemukan pada organ limpa.

  10. Angiotensin-converting enzyme 2, Angiotensin-(1-7) and Mas: new players of the Renin Angiotensin System

    DEFF Research Database (Denmark)

    Santos, Robson AS; Ferreira, Anderson J; Verano-Braga, Thiago

    2013-01-01

    /proliferative arm of the RAS consisting of ACE, Ang II and AT1 receptor. In this brief review, we will discuss recent findings related to the biological role of the ACE2/Ang-(1-7)/Mas arm in the cardiovascular and renal systems, as well as in metabolism. In addition, we will highlight the potential interactions...

  11. New perspectives of 19F MAS NMR in the characterization of amorphous forms of atorvastatin in dosage formulations

    Czech Academy of Sciences Publication Activity Database

    Brus, Jiří; Urbanová, Martina; Šeděnková, Ivana; Brusová, H.

    2011-01-01

    Roč. 409, 1/2 (2011), s. 62-74 ISSN 0378-5173 R&D Projects: GA MŠk 2B08021 Institutional research plan: CEZ:AV0Z40500505 Keywords : 19F MAS NMR * factor analysis * polymorphism Subject RIV: CB - Analytical Chemistry, Separation Impact factor: 3.350, year: 2011

  12. {sup 1}H and {sup 23}Na MAS NMR spectroscopy of cationic species in CO{sub 2} selective alkaline earth metal porous silicoaluminophosphates prepared via liquid and solid state ion exchange

    Energy Technology Data Exchange (ETDEWEB)

    Arevalo-Hidalgo, Ana G. [Department of Chemical Engineering, University of Puerto Rico-Mayagueez Campus, Mayagueez, PR 00681-9000 (Puerto Rico); Dugar, Sneha; Fu, Riqiang [National High Magnetic Field Laboratory, Florida State University, Tallahassee, FL 32310 (United States); Hernandez-Maldonado, Arturo J., E-mail: arturoj.hernandez@upr.edu [Department of Chemical Engineering, University of Puerto Rico-Mayagueez Campus, Mayagueez, PR 00681-9000 (Puerto Rico)

    2012-07-15

    The location of extraframework cations in Sr{sup 2+} and Ba{sup 2+} ion-exchanged SAPO-34 was estimated by means of {sup 1}H and {sup 23}Na MAS NMR spectroscopy and spectral deconvolution. Incorporation of the alkaline earth metal cations onto the SAPO framework was achieved via liquid state ion exchange, coupled partial detemplation/solid-state ion exchange, and combination of both techniques. MAS NMR revealed that the level of ion exchange was limited by the presence of protons and sodium cations near hexagonal prisms (site SI), which are relatively difficult to exchange with the alkaline earth metal due to steric and charge repulsion criteria. In addition, the presence of ammonium cations in the supercages facilitated the exchange of otherwise tenacious hydrogen as corroborated by unit cell compositional data as well as enhanced CO{sub 2} adsorption at low partial pressures. The extraframework ammonium species were produced from partial detemplation of the structure-directing agent employed for the SAPO-34 synthesis, tetraethylammonium. - Graphical abstract: MAS NMR was used to elucidate the position the cationic species in alkaline earth metal exchanged silicoaluminophosphates. These species played a significant role during the ion exchange process and, therefore, the materials ultimate CO{sub 2} adsorption performance. Highlights: Black-Right-Pointing-Pointer Location of extraframework Sr{sup 2+} or Ba{sup 2+} cations was estimated by means of {sup 1}H and {sup 23}Na MAS NMR. Black-Right-Pointing-Pointer Level of Sr{sup 2+} or Ba{sup 2+} ion exchange was limited by the presence of protons and sodium cations. Black-Right-Pointing-Pointer Presence of ammonium cations in the supercages facilitated the exchange. Black-Right-Pointing-Pointer Sr{sup 2+} and Ba{sup 2+} ion exchanged SAPOs are outstanding CO{sub 2} adsorbents.

  13. KANDUNGAN KIMIA SERAT KENAF DARI KOMPOS KULIT UDANG DENGAN PESTISIDA ALAMI KEONG MAS

    Directory of Open Access Journals (Sweden)

    Rusmini Rusmini

    2017-10-01

    Full Text Available Kenaf cultivation generally uses chemical fertilizers and pesticides to increase production despite the adverse effects of those chemicals toward environmental ecosystem. Meanwhile, there are a lot of unutilized wastes produced from agriculture and fishery. Kenaf is an environmentally friendly producer of natural fibers and can produce diversified products, such as paper, wallcover, car interior, geotextile, soil safer, fiber drain, particle board, and plastic reinforcement as well as biofuel industry raw materials. The research aims to produce chemistry fiber kenaf best with the provision of organic fertilizer shrimp compost and natural pesticide snail mas. The study used a Randomized Block Design with two factors with the first factor compost of shrimp (k consisting of 3 levels and the second factor was vegetable pesticide consisting of three levels (p. In each of these studies repeated as many as 2 replications so that there are 18 overall treatment. The observed variables of chemical fiber content include holocellulose, cellulose and lignin. Data obtained, analyzed using analysis of variance  and continued with the smallest real difference test at 5% test level. The results showed that there was holocellulose content in the best kenaf fiber in the treatment of p2 k2 that was equal to 80,28005, for the best cellulose content was p0ko taht was equal to 40,5695 %while for lignin was not continued further test because it showed no real difference. Penanaman  tanaman  kenaf  umumnya menggunakan pupuk kimia untuk meningkatkan produksi, padahal pupuk kimia berbahaya bagi ekosistem lingkungan, sementara banyak sekali limbah pertanian dan perikanan yang tidak termanfaatkan bahkan  menjadi sampah.   Kenaf merupakan tanaman penghasil serat alam yang ramah lingkungan dan bisa menghasilkan berbagai produk diversifikasi, seperti : kertas, pelapis dinding, interior mobil, geotekstil, soil safer, fiber drain, particle board, dan reinforcement plastik

  14. Experimental investigation of drying characteristics of cornelian cherry fruits ( Cornus mas L.)

    Science.gov (United States)

    Ozgen, Filiz

    2015-03-01

    Major target of present paper is to investigate the drying kinetics of cornelian cherry fruits ( Cornus mas L.) in a convective dryer, by varying the temperature and the velocity of drying air. Freshly harvested fruits are dried at drying air temperature of 35, 45 and 55 °C. The considered drying air velocities are V air = 1 and 1.5 m/s for each temperature. The required drying time is determined by taking into consideration the moisture ratio measurements. When the moisture ratio reaches up to 10 % at the selected drying air temperature, then the time is determined ( t = 40-67 h). The moisture ratio, fruit temperature and energy requirement are presented as the functions of drying time. The lowest drying time (40 h) is obtained when the air temperature is 55 °C and air velocity is 1.5 m/s. The highest drying time (67 h) is found under the conditions of 35 °C temperature and 1 m/s velocity. Both the drying air temperature and the air velocity significantly affect the required energy for drying system. The minimum amount of required energy is found as 51.12 kWh, at 55 °C and 1 m/s, whilst the maximum energy requirement is 106.7 kWh, at 35 °C and 1.5 m/s. It is also found that, air temperature significantly influences the total drying time. Moreover, the energy consumption is decreasing with increasing air temperature. The effects of three parameters (air temperature, air velocity and drying time) on drying characteristics have also been analysed by means of analysis of variance method to show the effecting levels. The experimental results have a good agreement with the predicted ones.

  15. A rheological model for glassforming silicate melts in the systems CAS, MAS, MCAS

    International Nuclear Information System (INIS)

    Giordano, Daniele; Russell, J K

    2007-01-01

    Viscosity is the single most important property governing the efficacy, rates, and nature of melt transport. Viscosity is intimately related to the structure and thermodynamics properties of the melts and is a reflection of the mechanisms of single atoms slipping over potential energy barriers. The ability to predict melt viscosity accurately is, therefore, of critical importance for gaining new insights into the structure of silicate melts. Simple composition melts, having a reduced number of components, offer an advantage for understanding the relationships between the chemical composition, structural organization and the rheological properties of a melt. Here we have compiled a large database of ∼970 experimental measurements of melt viscosity for the simple chemical systems MAS, CAS and MCAS. These data are used to create a single chemical model for predicting the non-Arrhenian viscosity as a function of temperature (T) and composition (X) across the entire MCAS system. The T-dependence of viscosity is accounted for by the three parameters in each of the model functions: (i) Vogel-Fulcher-Tamman (VFT); (ii) Adam-Gibbs (AG); and (iii) Avramov (AV). The literature shows that, in these systems, viscosity converges to a common value of the pre-exponential factors (A) that can be assumed to be independent of composition. The other two adjustable parameters in each equation are expanded to capture the effects of composition. The resulting models are continuous across T-X space. The values and implications of the optimal parameters returned for each model are compared and discussed. A similar approach is likely to be applicable to a variety of non-silicate multicomponent glassforming systems

  16. Reducing radiation dose in liver enhanced CT scan by setting mAs according to plain scan noise

    International Nuclear Information System (INIS)

    Yang Shangwen; He Jian; Yang Xianfeng; Zhou Kefeng; Xin Xiaoyan; Hu Anning; Zhu Bin

    2013-01-01

    Objective: To investigate the feasibility of setting mAs in liver enhanced CT scan according to plain scan noise with fixed mA CT scanner, in order to reduce the radiation dose. Methods: One hundred continuous patients underwent liver enhanced CT scan (group A) prospectively. Two hundred and fifty mAs was used in plain and enhanced CT scans. Noises of plain and venous phase CT images were measured, and the image quality was evaluated. The equation between mAs of enhanced scan and noise of plain scan image was derived. Another 100 continuous patients underwent liver enhanced CT scan (group B). Enhanced scan mAs was calculated from noise on plain scan by using the equation above. Noises on venous phase images were measured and the image quality was measured. Based on body mass index (BMI), patients in groups A and B were divided into three subgroups respectively: BMI < 18.5 kg/m 2 , 18.5 kg/m 2 ≤ BMI < 25.0 kg/m 2 and BMI ≥ 25.0 kg/m 2 . Image quality score was compared with nonparametric rank sum test, CT dose index (CTDI) and effective dose (ED) were measured and compared between each subgroup with 2 independent samples t or t' test. Results: The equation between enhanced scan mAs (mAsX) and plain scan noise (SDp) was as follows: mAsX = mAs1 × [(0.989 × SDp + 1.06) /SDx] 2 , mAs1 = 250 mAs, SDx = 13. In patients with BMI < 18.5 kg/m 2 , ED of group A [(6.86 ± 0.38) mSv, n = 12] was significantly higher than group B [(2.66 ± 0.46) mSv, n = 10)] (t = 18.52, P < 0.01). In patients with 18.5 kg/m 2 ≤ BMI < 25.0 kg/m 2 , ED of group A [(7.08 ± 0.91) mSv, n = 66] was significantly higher than group B [(4.50 ± 1.41) mSv, n = 73] (t' = 10.57, P < 0.01). In patients with BMI ≥ 25.0 kg/m 2 , there was no significant difference between EDs of group A (7.54 ± 0.62 mSv, n = 22) and group B [(8.19 ± 3.16) mSv, n = 17] (t' = 0.89, P = 0.39). Image quality of 5 patients in group A and none in group B did not meet the diagnostic requirement

  17. Avaliação da contaminação no entorno de um aterro de resíduos sólidos urbanos com base em resultados de poços de monitoramento

    Directory of Open Access Journals (Sweden)

    Giulliana Mondelli

    2016-03-01

    Full Text Available RESUMO Este artigo apresenta o monitoramento ambiental das águas subterrâneas do entorno do aterro de resíduos sólidos urbanos (RSU de Bauru, São Paulo, Brasil. Paralelamente às diversas pesquisas realizadas na área durante o período de janeiro de 2003 a abril de 2008, foram construídos 14 poços de monitoramento em diferentes fases da investigação geoambiental, seguindo as normas vigentes na época e as necessidades observadas durante a interpretação dos resultados desta investigação, para confirmação da contaminação da área. As amostras foram coletadas com bailer , após o período de chuvas e de estiagem de cada ano. São apresentados os resultados obtidos ao longo do tempo para os seguintes parâmetros: nível d'água, pH, condutividade elétrica (CE, Ca2+, Cl, Fe total, DQO, NH4 +, Zn2+, Na+, K+, além da relação demanda biológica de oxigênio/demanda química de oxigênio (DBO/DQO. Os resultados do longo período de monitoramento permitiram a análise de cada parâmetro em função do que ocorria superficialmente ao aterro, assim como com características naturais do aquífero. Conclui-se que a pluma de contaminação varia conforme o ponto de disposição e as características dos resíduos depositados, cuja recuperação e atenuação deverão ocorrer com o encerramento das atividades do aterro.

  18. Experimental article – Reducing effective dose to a paediatric phantom by using different combinations of kVp, mAs and additional filtration whilst maintaining image quality

    NARCIS (Netherlands)

    Huizinga, Elsbeth; Schaake, Wouter; Visser, Ruurd; Bloomfield, Charlotte; Boavida, Filipa; Chabloz, Diane; Crausaz, Emilie; Hustveit, Hanne; Knight, Heidi; Pereira, Anna; Harsaker, Vanja

    2015-01-01

    Purpose: To determine whether using different combinations of kVp and mAs with additional filtration can reduce the effective dose to a paediatric phantom whilst maintaining diagnostic image quality. Methods: 27 images of a paediatric AP pelvis phantom were acquired with different kVp, mAs and

  19. Experimental article – Reducing effective dose to a paediatric phantom by using different combinations of kVp, mAs and additional filtration whilst maintaining image quality

    NARCIS (Netherlands)

    Elsbeth Huizinga; Ana Pereira; Wouter Schaake; Charlotte Bloomfield; Heidi Knight; Emilie Crausaz; Hanne Hustveit; Ruurd Visser; Vanja Harsaker; Diane Chabloz; Filipa Boavida

    2015-01-01

    Purpose: To determine whether using different combinations of kVp and mAs with additional filtration can reduce the effective dose to a paediatric phantom whilst maintaining diagnostic image quality. Methods: 27 images of a paediatric AP pelvis phantom were acquired with different kVp, mAs

  20. Who Are the Students Who May Qualify for an Alternate Assessment Based on Modified Academic Achievement Standards (AA-MAS)?: Focus Group Results. Synthesis Report 79

    Science.gov (United States)

    Berndt, Sandra; Ebben, Barbara; Kubinski, Eva; Sim, Grant; Liu, Kristin; Lazarus, Sheryl; Thurlow, Martha; Christian, Elizabeth

    2011-01-01

    Beginning in 2007, federal regulations to two major education laws gave state departments of education the option to develop an alternate assessment based on modified achievement standards (AA-MAS) for some students with disabilities. The regulations stated that the AA-MAS was intended for students who were being instructed in the grade-level…

  1. MUNICIPAL ENVIRONMENTAL MANAGEMENT: A PROPOSAL OF INSTRUMENTS FOR DIAGNOSIS OF PUBLIC ENVIRONMENTAL POLICIES IN THE METROPOLITAN AREA OF SALVADOR (MAS

    Directory of Open Access Journals (Sweden)

    Tânia Cristina Azevedo

    2016-04-01

    Full Text Available The aim in this paper is to propose a model for mapping strategies of municipal environmental management for local environmental public policies. To do so, the study adopted a theoretical approach. More specifically, there is discussion on the concepts of public policies and the scenario of the Brazilian municipal environmental management, a brief history of the aspects that involve current national environmental policies. Methodologically, a bibliographical study was carried out through a literature review, which enabled the proposal of instruments for mapping actions and strategies of environmental management in the municipalities of the Metropolitan Area of Salvador (MAS. This theoretical study resulted in the creation of a model form that will be used by empirical researches for mapping the environmental public policies in the MAS City Halls.

  2. Characterizing crystal disorder of trospium chloride: a comprehensive,(13) C CP/MAS NMR, DSC, FTIR, and XRPD study.

    Science.gov (United States)

    Urbanova, Martina; Sturcova, Adriana; Brus, Jiri; Benes, Hynek; Skorepova, Eliska; Kratochvil, Bohumil; Cejka, Jan; Sedenkova, Ivana; Kobera, Libor; Policianova, Olivia; Sturc, Antonin

    2013-04-01

    Analysis of C cross-polarization magic angle spinning (CP/MAS) nuclear magnetic resonance (NMR), differential scanning calorimetry (DSC), Fourier transform infrared (FTIR), and X-ray powder diffraction data of trospium chloride (TCl) products crystallized from different mixtures of water-ethanol [φ(EtOH) = 0.5-1.0] at various temperatures (0°C, 20°C) and initial concentrations (saturated solution, 30%-50% excess of solvent) revealed extensive structural variability of TCl. Although (13) C CP/MAS NMR spectra indicated broad variety of structural phases arising from molecular disorder, temperature-modulated DSC identified presence of two distinct components in the products. FTIR spectra revealed alterations in the hydrogen bonding network (ionic hydrogen bond formation), whereas the X-ray diffraction reflected unchanged unit cell parameters. These results were explained by a two-component character of TCl products in which a dominant polymorphic form is accompanied by partly separated nanocrystalline domains of a secondary phase that does not provide clear Bragg reflections. These phases slightly differ in the degree of molecular disorder, in the quality of crystal lattice and hydrogen bonding network. It is also demonstrated that, for the quality control of such complex products, (13) C CP/MAS NMR spectroscopy combined with factor analysis (FA) can satisfactorily be used for categorizing the individual samples: FA of (13) C CP/MAS NMR spectra found clear relationships between the extent of molecular disorder and crystallization conditions. © 2013 Wiley Periodicals, Inc. and the American Pharmacists Association J Pharm Sci 102:1235-1248, 2013. Copyright © 2013 Wiley Periodicals, Inc.

  3. Analisis Laporan Keuangan Untuk Menilai Kinerja Keuangan PT. Sinar Mas Agro Resources and Technology. Tbk periode 2009, 2010 dan 2011

    OpenAIRE

    Monica, Marnala Stevi

    2015-01-01

    This study aims to look at how the development of the financial performance. Sinar Mas Agro Resources and Technology. Tbk for 3 years ie 2009, 2010 and 2011. In assessing the financial performance of the financial statements required to be analyzed. Financial statement analysis can be done using financial ratio analysis. Financial ratios are used in assessing the financial performance of this is the Current Ratio, Quick Ratio, Debt to Equity Ratio (DER), Debt to Asset Ratio (DAR), Total Asset...

  4. Genotyping-by-sequencing (GBS), an ultimate marker-assisted selection (MAS) tool to accelerate plant breeding

    OpenAIRE

    He, Jiangfeng; Zhao, Xiaoqing; Laroche, André; Lu, Zhen-Xiang; Liu, HongKui; Li, Ziqin

    2014-01-01

    Marker-assisted selection (MAS) refers to the use of molecular markers to assist phenotypic selections in crop improvement. Several types of molecular markers, such as single nucleotide polymorphism (SNP), have been identified and effectively used in plant breeding. The application of next-generation sequencing (NGS) technologies has led to remarkable advances in whole genome sequencing, which provides ultra-throughput sequences to revolutionize plant genotyping and breeding. To further broad...

  5. Characterization of solid polymer dispersions of active pharmaceutical ingredients by 19F MAS NMR and factor analysis

    Czech Academy of Sciences Publication Activity Database

    Urbanová, Martina; Brus, Jiří; Šeděnková, Ivana; Policianová, Olivia; Kobera, Libor

    2013-01-01

    Roč. 100, 1 January (2013), s. 59-66 ISSN 1386-1425 R&D Projects: GA ČR GPP106/11/P426; GA MŠk 2B08021 Institutional research plan: CEZ:AV0Z40500505 Institutional support: RVO:61389013 Keywords : solid-state NMR * factor analysis * 19F MAS NMR Subject RIV: FR - Pharmacology ; Medidal Chemistry Impact factor: 2.129, year: 2013

  6. 1 H MAS NMR study of structure of hybrid siloxane-based networks and the interaction with quartz filler

    Czech Academy of Sciences Publication Activity Database

    Brus, Jiří; Škrdlantová, M.

    2001-01-01

    Roč. 281, 1-3 (2001), s. 61-71 ISSN 0022-3093 R&D Projects: GA ČR GA203/98/P290; GA AV ČR KSK2050602 Institutional research plan: CEZ:AV0Z4050913 Keywords : hybrid siloxane networks * 1 H MAS NMR spectroscopy * hydrogen bonds Subject RIV: CD - Macromolecular Chemistry Impact factor: 1.363, year: 2001

  7. Role of Mas receptor in renal blood flow response to angiotensin (1-7) in male and female rats.

    Science.gov (United States)

    Nematbakhsh, Mehdi; Safari, Tahereh

    2014-01-01

    Epidemiologic and clinical studies have shown that progression of renal disease in male is faster than that in female. However, the exact mechanisms are not well recognized. Angiotensin (1-7) (Ang 1-7) receptor, called "Mas", is an element in the depressor arm of renin angiotensin system (RAS), and its expression is enhanced in females. We test the hypothesis that Mas receptor (MasR) blockade (A779) attenuates renal blood flow (RBF) in response to infusion of graded doses of Ang 1-7 in female rats. Male and female Wistar rats were anesthetized and catheterized. Then, the mean arterial pressure (MAP), RBF, and controlled renal perfusion pressure (RPP) responses to infusion of graded doses of Ang 1-7 (100-1000 ng/kg/min i.v.) with and without A779 were measured in the animals. Basal MAP, RPP, RBF, and renal vascular resistance (RVR) were not significantly different between the two groups. After Ang 1-7 administration, RPP was controlled at a constant level. However, RBF increased in a dose-related manner in response to Ang 1-7 infusion in both male and female rats (Pdoserenal diseases.

  8. Stilistiskie izteiksmes līdzekļi Coca-Cola reklāmas plakātos

    OpenAIRE

    Gudre, Anete

    2017-01-01

    Šajā darbā tika pētīti mākslinieciskie un fonētiskie stila izteiksmes līdzekļi un to lietojums Coca-Cola reklāmas plakātos. Kā arī tika analizēti Coca-Cola reklāmas plakātu vizuālie elementi. Tēma tika izvēlēta, lai redzētu atšķirību starp mākslinieciskās izteiksmes līdzekļiem un, lai redzētu, cik bieži tie tiek izmantoti izvēlētajos reklāmas plakātos. Darbā tika aplūkoti vispopulārākie mākslinieciskās izteiksmes līdzekļi – metafora, epitets, personifikācija un hiperbola. Multimediju analīze ...

  9. Quality of Kelantan drinking water and knowledge, attitude and practice among the population of Pasir Mas, Malaysia.

    Science.gov (United States)

    Ab Razak, N H; Praveena, S M; Aris, A Z; Hashim, Z

    2016-02-01

    Information about the quality of drinking water, together with analysis of knowledge, attitude and practice (KAP) analysis and health risk assessment (HRA) remain limited. The aims of this study were: (1) to ascertain the level of KAP regarding heavy metal contamination of drinking water in Pasir Mas; (2) to determine the concentration of heavy metals (Al, Cr, Cu, Fe, Ni, Pb, Zn and Cd) in drinking water in Pasir Mas; and (3) to estimate the health risks (non-carcinogenic and carcinogenic) caused by heavy metal exposure through drinking water using hazard quotient and lifetime cancer risk. Information on KAP was collected using a standardized questionnaire. Heavy metal analysis of drinking water samples was performed using graphite furnace atomic absorption spectrophotometry. The population of Pasir Mas has good knowledge (80%), a less positive attitude (93%) and good practice (81%) towards heavy metal contamination of drinking water. The concentrations of heavy metals analysed in this study were found to be below the permissible limits for drinking water set by the Malaysian Ministry of Health and the World Health Organization. The HRA showed no potential non-carcinogenic and carcinogenic risks from the intake of heavy metal through drinking water. By investigating the quality of drinking water, KAP and HRA, the results of this study will provide authorities with the knowledge and resources to improve the management of drinking water quality in the future. Copyright © 2015 The Royal Society for Public Health. Published by Elsevier Ltd. All rights reserved.

  10. A new aluminium-hydrate species in hydrated Portland cements characterized by 27Al and 29Si MAS NMR spectroscopy

    International Nuclear Information System (INIS)

    Andersen, Morten Daugaard; Jakobsen, Hans J.; Skibsted, Jorgen

    2006-01-01

    Recent 27 Al MAS NMR studies of hydrated Portland cements and calcium-silicate-hydrate (C-S-H) phases have shown a resonance from Al in octahedral coordination, which cannot be assigned to the well-known aluminate species in hydrated Portland cements. This resonance, which exhibits the isotropic chemical shift δ iso = 5.0 ppm and the quadrupole product parameter P Q = 1.2 MHz, has been characterized in detail by 27 Al MAS and 27 Al{ 1 H} CP/MAS NMR for different hydrated white Portland cements and C-S-H phases. These experiments demonstrate that the resonance originates from an amorphous or disordered aluminate hydrate which contains Al(OH) 6 3- or O x Al(OH) 6-x (3+x)- units. The formation of the new aluminate hydrate is related to the formation of C-S-H at ambient temperatures, however, it decomposes by thermal treatment at temperatures of 70-90 o C. From the experiments in this work it is proposed that the new aluminate hydrate is either an amorphous/disordered aluminate hydroxide or a calcium aluminate hydrate, produced as a separate phase or as a nanostructured surface precipitate on the C-S-H phase. Finally, the possibilities of Al 3+ for Ca 2+ substitution in the principal layers and interlayers of the C-S-H structure are discussed

  11. Avaliação do sistema de monitoramento computadorizado de digestão in vitro: 1. Testes preliminares Evaluation of a computerized monitoring on in vitro digestion system: 1. Preliminary tests

    OpenAIRE

    Fábio Prudêncio de Campos; Dante Pazzanese Duarte Lanna; Máx Lázaro Vieira Bose; Celso Boin

    2000-01-01

    O objetivo deste trabalho foi testar o sistema de monitoramento computadorizado da produção de gás in vitro. Essa técnica facilita estudos da degradação das frações solúveis e insolúveis das forragens, quantificadas pela produção de gás (CO2 e CH4) oriunda do metabolismo microbiano e medida por sensor de pressão. Diversas quantidades de amostras (50 a 110 mg de feno de alfafa) e outros alimentos foram testadas. Também, a influência da quantidade de líquido ruminal (2,0 ou 3,0 mL), com ou sem ...

  12. Nova abordagem metodológica para locação, modelagem 3D e monitoramento de barragens subterrâneas no semiárido brasileiro

    OpenAIRE

    Lima, Alexandre de Oliveira

    2013-01-01

    Apesar do número significativo de barragens construídas nos últimos anos no Brasil e mesmo em outros países, são poucos os estudos técnicos que dão suporte a este crescimento. Com o objetivo de propor uma nova abordagem metodológica para o processo de locação e monitoramento de barragens subterrâneas, em condições de clima semiárido, foram realizados estudos em duas sub-bacias hidrográficas (do rio das Cobras e Pau Lavrado) ambas situadas no semiárido do Estado do Rio Grande. Nesta nova abord...

  13. TILLANDSIA USNEOIDES (L.) COMO FERRAMENTA DE MONITORAMENTO DE POLUIÇÃO ATMOSFÉRICO PARA METAIS-TRAÇO NOS MUNICÍPIOS DE CAMPINAS E PAULÍNIA, ESTADO DE SÃO PAULO, SP, BRASIL

    OpenAIRE

    Ferreira, Guilherme Gonçalves

    2014-01-01

    http://dx.doi.org/10.5902/2236117011293O monitoramento da atmosfera na região de Campinas e Paulínia com a introdução em campo da bromélia Tillandsia usneoides (L.) abrangeu sete áreas de acordo com a identificação de possíveis fontes e distâncias envolvidas durante cinco períodos entre Abril (2009) a Março (2010). Os objetivos foram conhecer as variações espaciais e sazonais das concentrações de metais-traço em T. usneoides a partir de análises por ICP-MS e a relação com os dados climáticos ...

  14. Monitoramento físico-químico de um biorreator com resíduos sólidos urbanos em escala piloto na cidade de Campina Grande (PB)

    OpenAIRE

    Ribeiro, Libânia da Silva; Silva, Alessandra dos Santos; Alves, Flaviano de Souza; Melo, Márcio Camargo de; Paiva, William de; Monteiro, Veruschka Escarião Dessoles

    2016-01-01

    RESUMO O monitoramento dos parâmetros físico-químicos em resíduos sólidos urbanos (RSU) é de grande importância, por descrever as condições nas quais os fenômenos de degradação se processam. O pH, assim como a demanda biológica de oxigênio (DBO) e a demanda química de oxigênio (DQO), permite acompanhar o processo de decomposição dos RSU em aterros sanitários, indicando a evolução da degradação microbiológica da matéria orgânica e a evolução global do processo de estabilização da massa de resí...

  15. PARÂMETROS REPRODUTIVOS DE MATRIZES SUÍNAS INSEMINADAS COM SÊMEN DILUÍDO EM ÁGUA DE COCO APÓS MONITORAMENTO ULTRA-SONOGRÁFICO TRANSCUTÂNEO

    Directory of Open Access Journals (Sweden)

    Pierre Castro Soares

    2006-10-01

    Full Text Available Com o objetivo de avaliar o efeito de diluidores de sêmen (MERK III, BTS e água de coco acrescida de citrato de sódio a 5% sobre parâmetros reprodutivos de matrizes suínas, utilizou-se sêmen diluído nas concentrações de 4x109 e 8x109 espermatozóides/100ml na inseminação artificial de 173 fêmeas púberes e 184 adultas, com prévio monitoramento ultra-sonográfico do estro e ovulação. O diagnóstico de gestação também foi realizado por ultra-sonografia transcutânea. Os dados revelaram altas percentagens (89,5% a 95,6% de prenhes das matrizes suínas púberes e adultas, sem variação significativa entre os tipos de diluidores utilizados. Sugere-se, portanto, que a água de coco in natura pode ser utilizada na diluição de sêmen suíno, significando uma alternativa de baixo custo, e que monitoramento ultra-sonográfico transcutâneo constitui um método auxiliar no diagnóstico de estro, ovulação e prenhez. PALAVRAS-CHAVE: Suíno, sêmen, água de coco, MERK III, BTS, ultra-sonografia.

  16. Avaliação de atrativos alimentares utilizados no monitoramento de mosca-das-frutas em pessegueiro na lapa- PR Food attractants used in the monitoring of fruit flies in peach trees in lapa, Paraná (PR, Brazil

    Directory of Open Access Journals (Sweden)

    Lino Bittencourt Monteiro

    2007-04-01

    Full Text Available As moscas-das-frutas do gênero Anastrepha são uma praga-chave na cultura do pessegueiro no Paraná. Atrativos alimentares foram testados para determinar a sua eficiência no monitoramento de moscas-das-frutas capturadas em frascos caça-moscas McPhail. O experimento foi conduzido por três anos, sendo que, em 2002, foram testados como atrativo o suco de uva da marca Maguari®, o hidrolisado enzimático de proteína da marca BioAnastrepha® e o vinagre da marca Chemin Agrin®. Nos dois anos seguintes, o vinagre foi substituído pelo composto protéico hidrolisável da marca Torula®. As substâncias atrativas à base de proteína foram as mais eficientes na captura de Anastrepha spp., e as capturas ocorreram antecipadas em relação ao suco de uva. De acordo com os resultados, recomendam-se atrativos à base de proteína para monitoramento de Anastrepha spp em pessegueiro, na Lapa.Fruit flies of Anastrepha genus are a key pest in peach trees in Paraná. Food attractants were tested to determine their efficiency in monitoring fruit flies captured in McPhail fly traps. The experiment was conducted over a period of three years. In 2002 the following attractors were tested: Maguari® brand grape juice, BioAnastrepha® brand hydrolyzed enzymatic protein and Chemin Agrin® vinegar. Over the next two years, the vinegar was replaced by Torula® hydrolyzed protein compound. Protein-based attractants were the most efficient in trapping Anastrepha spp. and captured flies earlier comparing to grape juice. According to the results, the use of protein-based attractants for monitoring Anastrepha spp in the Lapa peach trees was recommended.

  17. Role of RENAL nephrometry scoring system in planning surgical intervention in patients with localized renal mas

    OpenAIRE

    Mohamed Samir Shaaban; Tamer Mohammed Abou Youssif; Ahmed Mostafa; Hossam Eldin Hegazy; Mohammed Adel Atta

    2015-01-01

    Purpose: The study was designed to validate the value of preoperative planning using RENAL nephrometry scoring system in patients having organ confined renal tumors and undergoing surgical intervention and to assess its correlation with the surgical technique. Patient and methods: Forty patients with organ-confined renal masses underwent RENAL nephrometry scoring which was correlated with the surgical technique either radical or nephron-sparing surgery. Result: RENAL nephrometry scoring...

  18. KEBIJAKAN INVESTASI ASING BIDANG PERTAMBANGAN DI KABUPATEN POHUWATO PROVINSI GORONTALO KEBIJAKAN INVESTASI ASING BIDANG PERTAMBANGAN DI KABUPATEN POHUWATO PROVINSI GORONTALO KEBIJAKAN INVESTASI ASING BIDANG PERTAMBANGAN DI KABUPATEN POHUWATO PROVINSI GORONTALO KASUS PT. PANI DHARMA MAS KASUS PT. PANI DHARMA MAS KASUS PT. PANI DHARMA MAS

    OpenAIRE

    PUYO, AJENG MAWADDAH PUYO AJENG MAWADDAH PUYO AJENG MAWADDAH

    2016-01-01

    2016 AJENG MAWADDAH PUYO, E 131 12 003, "Kebijakan Investasi Asing Dalam Bidang Pertambangan di Kabupaten Pohuwato Provinsi Gorontalo Kasus PT. Pani Dharma MAS", dibawah bimbingan Dr. H. Adi Suryadi B., MA selaku pembimbing I dan Pusparida Syahdan. S.sos., MSI, Departemen Ilmu Hubungan internasional, Fakultas Ilmu Sosial dan Ilmu Politik, Universitas Hasanuddin. Penelitian ini bertujuan untuk mengetahui peran stakeholders dalam perumusan kebijakan investasi asing da...

  19. ACE-2/Ang1-7/Mas cascade mediates ACE inhibitor, captopril, protective effects in estrogen-deficient osteoporotic rats.

    Science.gov (United States)

    Abuohashish, Hatem M; Ahmed, Mohammed M; Sabry, Dina; Khattab, Mahmoud M; Al-Rejaie, Salim S

    2017-08-01

    The local role of the renin angiotensin system (RAS) was documented recently beside its conventional systemic functions. Studies showed that the effector angiotensin II (AngII) alters bone health, while inhibition of the angiotensin converting enzyme (ACE-1) preserved these effects. The newly identified Ang1-7 exerts numerous beneficial effects opposing the AngII. Thus, the current study examines the role of Ang1-7 in mediating the osteo-preservative effects of ACEI (captopril) through the G-protein coupled Mas receptor using an ovariectomized (OVX) rat model of osteoporosis. 8 weeks after the surgical procedures, captopril was administered orally (40mgkg -1 d -1 ), while the specific Mas receptor blocker (A-779) was delivered at infusion rate of 400ngkg -1 min -1 for 6 weeks. Bone metabolic markers were measured in serum and urine. Minerals concentrations were quantified in serum, urine and femoral bones by inductive coupled plasma mass spectroscopy (ICP-MS). Trabecular and cortical morphometry was analyzed in the right distal femurs using micro-CT. Finally, the expressions of RAS peptides, enzymes and receptors along with the receptor activator of NF-κB ligand (RANKL) and osteoprotegerin (OPG) were determined femurs heads. OVX animals markedly showed altered bone metabolism and mineralization along with disturbed bone micro-structure. Captopril significantly restored the metabolic bone bio-markers and corrected Ca 2+ and P values in urine and bones of estrogen deficient rats. Moreover, the trabecular and cortical morphometric features were repaired by captopril in OVX groups. Captopril also improved the expressions of ACE-2, Ang1-7, Mas and OPG, while abolished OVX-induced up-regulation of ACE-1, AngII, Ang type 1 receptor (AT1R) and RANKL. Inhibition of Ang1-7 cascade by A-779 significantly eradicated captopril protective effects on bone metabolism, mineralization and micro-structure. A-779 also restored OVX effects on RANKL expression and ACE-1/AngII/AT1R

  20. Mas-allatotropin in the developing antennal lobe of the sphinx moth Manduca sexta: distribution, time course, developmental regulation, and colocalization with other neuropeptides.

    Science.gov (United States)

    Utz, Sandra; Huetteroth, Wolf; Vömel, Matthias; Schachtner, Joachim

    2008-01-01

    The paired antennal lobes (ALs) of the sphinx moth Manduca sexta serve as a well-established model for studying development of the primary integration centers for odor information in the brain. To further reveal the role of neuropeptides during AL development, we have analyzed cellular distribution, developmental time course, and regulation of the neuropeptide M. sexta allatotropin (Mas-AT). On the basis of morphology and appearance during AL formation, seven major types of Mas-AT-immunoreactive (ir) cells could be distinguished. Mas-AT-ir cells are identified as local, projection, and centrifugal neurons, which are either persisting larval or newly added adult-specific neurons. Complementary immunostaining with antisera against two other neuropeptide families (A-type allatostatins, RFamides) revealed colocalization within three of the Mas-AT-ir cell types. On the basis of this neurochemistry, the most prominent type of Mas-AT-ir neurons, the local AT neurons (LATn), could be divided in three subpopulations. The appearance of the Mas-AT-ir cell types occurring during metamorphosis parallels the rising titer of the developmental hormone 20-hydroxyecdysone (20E). Artificially shifting the 20E titer to an earlier developmental time point resulted in the precocious occurrence of Mas-AT immunostaining. This result supports the hypothesis that the pupal rise of 20E is causative for Mas-AT expression during AL development. Comparing localization and developmental time course of Mas-AT and other neuropeptides with the time course of AL formation suggests various functions for these neuropeptides during development, including an involvement in the formation of the olfactory glomeruli.

  1. Genomic tools and and prospects for new breeding techniques in flower bulb crops

    Science.gov (United States)

    For many of the new breeding techniques, sequence information is of the utmost importance. In addition to current breeding techniques, such as marker-assisted selection (MAS) and genetic modification (GM), new breeding techniques such as zinc finger nucleases, oligonucleotide-mediated mutagenesis, R...

  2. NOMEX - a universal diagnostic dosemeter, mA.s, and kV meter for acceotance test measurements and quality assurance

    International Nuclear Information System (INIS)

    Hein, G.; Pychlau, P.; Schuele, E.

    1992-01-01

    A universal diagnostic dosemeter is introduced which was designed for acceptance test measurements and quality assurance. It can also be used for periodic constancy checks. To facilitate the comprehensive tests, the NOMEX can measure all important quantities, such as dose and dose rate, mean peak voltage, exposure time, mA.s product, dose per mA.s, dose per pulse, attenuation factor, relative standard deviation and length dose product in CT. All these quantities, except the mA.s product, are measured non-invasively. The instrument's concept, its applications and technical data are described. (author)

  3. Monitoring the viability of citrus rootstocks seeds stored under refrigeration Monitoramento da viabilidade de sementes porta-enxertos de citros armazenados em câmara fria

    Directory of Open Access Journals (Sweden)

    Sérgio Alves de Carvalho

    2013-03-01

    .O.D. germination chamber, the latter being the faster and more suitable method.A muda cítrica é resultado do processo de enxertia, sendo os porta-enxertos geralmente propagados por meio de sementes. O objetivo desta pesquisa foi caracterizar, em duas condições ambientais, a viabilidade e a expressão da poliembrionia de sementes de porta-enxertos de citros armazenadas durante diferentes períodos sob refrigeração. As variedades porta-enxertos avaliadas foram: limão-Cravo (Citrus limonia Osb. cv. Limeira, Trifoliata (Poncirus trifoliata Raf cv. Limeira, Citrumelo (P. trifoliata x C. paradisi Macf. cv. Swingle, tangerina Sunki (C. sunki Hort. ex Tanaka e limão Volkameriano (C. volkameriana Ten. & Pasq. cv. Catania 2. O delineamento experimental foi o de blocos casualisados, em esquema fatorial 11 x 5 x 2, em 4 repetições, avaliando-se, do tempo zero ao décimo mês de armazenamento, as cinco variedades e os dois ambientes: câmara de germinação e crescimento tipo B.O.D. ("Biological Oxigen Demand" - a 25º C e casa de vegetação (22 °C to 36 °C. Cada parcela foi composta por 24 sementes, utilizando-se de placas de Petri com papel-filtro na câmara B.O.D e bandejas com substrato na casa de vegetação. Avaliou-se mensalmente a taxa de germinação e expressão da poliembrionia. Concluiu-se que as sementes do Trifoliata e do citrumelo Swingle podem ser armazenadas em câmara fria por até sete meses, e as de limão Volkameriano, de limão Cravo e de tangerina Sunki, por até dez meses. Independentemente da variedade porta-enxerto, a taxa de expressão da poliembrionia foi ligeiramente superior em casa de vegetação, mantendo-se estável nos dois ambientes até o sétimo mês, a partir do qual diminuiu bruscamente. As sementes de Citrumelo expressaram a maior taxa de poliembrionia (18,8%, seguida das dos limões Cravo e Volkameriano (valor médio 13,7%, tangerina Sunki (9,4% e Trifiloata (3,2%. Apesar de algumas diferenças entre variedades, o monitoramento da

  4. Remote Sensing of Radiative and Microphysical Properties of Clouds During TC (sup 4): Results from MAS, MASTER, MODIS, and MISR

    Science.gov (United States)

    King, Michael D.; Platnick, Steven; Wind, Galina; Arnold, G. Thomas; Dominguez, Roseanne T.

    2010-01-01

    The Moderate Resolution Imaging Spectroradiometer (MODIS) Airborne Simulator (MAS) and MODIS/Advanced Spaceborne Thermal Emission and Reflection Radiometer (ASTER) Airborne Simulator (MASTER) were used to obtain measurements of the bidirectional reflectance and brightness temperature of clouds at 50 discrete wavelengths between 0.47 and 14.2 microns (12.9 microns for MASTER). These observations were obtained from the NASA ER-2 aircraft as part of the Tropical Composition, Cloud and Climate Coupling (TC4) experiment conducted over Central America and surrounding Pacific and Atlantic Oceans between 17 July and 8 August 2007. Multispectral images in eleven distinct bands were used to derive a confidence in clear sky (or alternatively the probability Of cloud) over land and ocean ecosystems. Based on the results of individual tests run as part of the cloud mask, an algorithm was developed to estimate the phase of the clouds (liquid water, ice, or undetermined phase). The cloud optical thickness and effective radius were derived for both liquid water and ice clouds that were detected during each flight, using a nearly identical algorithm to that implemented operationally to process MODIS Cloud data from the Aqua and Terra satellites (Collection 5). This analysis shows that the cloud mask developed for operational use on MODIS, and tested using MAS and MASTER data in TC(sup 4), is quite capable of distinguishing both liquid water and ice clouds during daytime conditions over both land and ocean. The cloud optical thickness and effective radius retrievals use five distinct bands of the MAS (or MASTER), and these results were compared with nearly simultaneous retrievals of marine liquid water clouds from MODIS on the Terra spacecraft. Finally, this MODIS-based algorithm was adapted to Multiangle Imaging SpectroRadiometer (MISR) data to infer the cloud optical thickness Of liquid water clouds from MISR. Results of this analysis are compared and contrasted.

  5. Sistema de visão por infravermelho próximo para monitoramento de processos de soldagem a arco Near-infrared vision system for arc-welding monitoring

    Directory of Open Access Journals (Sweden)

    Carolina Pimenta Mota

    2013-03-01

    Full Text Available A visão, o sentido predileto do ser humano, e sua grande capacidade de captar, processar e interpretar grandes quantidades de dados de natureza visual tem sido, ao longo dos anos, um grande estímulo para o desenvolvimento de técnicas e de dispositivos tecnológicos que a reproduzam num sistema computacional. Nos processos de soldagem, a visão pode fornecer dados na inspeção e qualidade da junta soldada, no monitoramento de parâmetros, na correção de trajetórias até, por fim, no estudo dos fenômenos envolvidos no processo. Porém, a radiação luminosa emitida pelo arco representa uma barreira para tais estudos baseados na visualização do processo. Uma das formas utilizadas atualmente para se obter a visualização do processo, sem a interferência do arco, consiste em iluminar o processo com o infravermelho próximo e utilizar filtros de interferência (passa-faixa, em torno deste mesmo comprimento de onda, durante a aquisição das imagens. Uma solução para a iluminação infravermelha, de aplicação crescente, envolve o uso de diodos laser de alta potência, com baixo custo e menor complexidade de instalação do que os lasers convencionais. Desta forma, a proposta deste trabalho foi a criação de um sistema de visão dos processos de soldagem a arco, de baixo custo e alta flexibilidade, indo desde a caracterização dos espectros de emissão luminosa do arco, passando pela criação de uma topologia de acionamento para o diodo de alta potência no infravermelho próximo, respeitando suas limitações de uso e maximizando a potência luminosa emitida, criação dos circuitos de controle, escolha dos equipamentos e componentes ópticos e, por fim, projeto e aplicação de um protótipo em processos de soldagem. As limitações do sistema de visão, como um todo, foram encontradas através de sua aplicação com soldagem TIG e MIG/MAG. Nestes ensaios, embora não tenha sido capaz de sobrepor a luz do arco, o sistema

  6. 27Al Magic Angle Spinning–Nuclear Magnetic Resonance (MAS-NMR) Analyses Applied to Historical Mortars

    Czech Academy of Sciences Publication Activity Database

    Hanzlíček, Tomáš; Perná, Ivana; Brus, Jiří

    2013-01-01

    Roč. 7, č. 2 (2013), s. 153-164 ISSN 1558-3058 R&D Projects: GA AV ČR IAA300460702 Institutional research plan: CEZ:AV0Z30460519; CEZ:AV0Z40500505 Keywords : mortars * magic angle spinning –nuclear magnetic resonance (MAS-NMR) in solid state * alumina-silicates Subject RIV: DM - Solid Waste and Recycling Impact factor: 0.714, year: 2013 http://www.tandfonline.com/doi/abs/10.1080/15583058.2011.624253

  7. Pharmacological significance of the interplay between angiotensin receptors: MAS receptors as putative final mediators of the effects elicited by angiotensin AT1 receptors antagonists.

    Science.gov (United States)

    Pernomian, Larissa; Pernomian, Laena; Gomes, Mayara S; da Silva, Carlos H T P

    2015-12-15

    The interplay between angiotensin AT1 receptors and MAS receptors relies on several inward regulatory mechanisms from renin-angiotensin system (RAS) including the functional crosstalk between angiotensin II and angiotensin-(1-7), the competitive AT1 antagonism exhibited by angiotensin-(1-7), the antagonist feature assigned to AT1/MAS heterodimerization on AT1 signaling and the AT1-mediated downregulation of angiotensin-converting enzyme 2 (ACE2). Recently, such interplay has acquired an important significance to RAS Pharmacology since a few studies have supporting strong evidences that MAS receptors mediate the effects elicited by AT1 antagonists. The present Perspective provides an overview of the regulatory mechanisms involving AT1 and MAS receptors, their significance to RAS Pharmacology and the future directions on the interplay between angiotensin receptors. Copyright © 2015 Elsevier B.V. All rights reserved.

  8. Intelligent business processes composition based on mas, semantic and cloud integration (IPCASCI)

    OpenAIRE

    García Coria, José Alberto

    2014-01-01

    [EN]Component reuse is one of the techniques that most clearly contributes to the evolution of the software industry by providing efficient mechanisms to create quality software. Reuse increases both software reliability, due to the fact that it uses previously tested software components, and development productivity, and leads to a clear reduction in cost. Web services have become are an standard for application development on cloud computing environments and are essential ...

  9. Microscopic structural analysis of fractured silk fibers from Bombyx mori and Samia cynthia ricini using 13C CP/MAS NMR with a 1 mm microcoil MAS NMR probehead

    KAUST Repository

    Yamauchi, Kazuo

    2010-07-01

    Conformational changes have been studied in silk fibers from the domestic silkworm Bombyx mori and a wild silkworm Samia cynthia ricini as a result of fractured by stretching. About 300 samples consisting of only the fractured regions of [1-13C]Ala or [1-13C]Gly labeled silk fibers were collected and observed by 13C CP/MAS NMR spectra. The total amount of these fractured fibers is only about 1 mg and therefore we used a home-built 1 mm microcoil MAS NMR probehead. A very small increase in the fraction of random coil was noted for the alanine regions of both silk fibroins and for the glycine region of B. mori silk fibroin. However, there is no difference in the spectra before and after fractured for the glycine region of S. c. ricini silk fibroin. Thus, the influence of fracture occurs exclusively at the Ala region for S. c. ricini. The relationship between sequence, fracture and structure is discussed. © 2010 Elsevier Inc. All rights reserved.

  10. Determination of the structural changes by Raman and {sup 13}C CP/MAS NMR spectroscopy on native corn starch with plasticizers

    Energy Technology Data Exchange (ETDEWEB)

    Cozar, O. [Academy of Romanian Scientists, Splaiul Independentei 54, 050094, Bucharest, Romania and National Institute of Research-Development for Machines and Installations Designed to Agriculture and Food Industry - INMA Bucureşti - Cluj-Napoca Branch (Romania); Filip, C.; Tripon, C. [National Institute for Research and Development of Isotopic and Molecular Technologies, 65-103 Donath, 400293 Cluj-Napoca (Romania); Cioica, N.; Coţa, C.; Nagy, E. M. [National Institute of Research-Development for Machines and Installations Designed to Agriculture and Food Industry - INMA Bucureşti - Cluj-Napoca Branch, RO-400458 Cluj-Napoca (Romania)

    2013-11-13

    The plasticizing - antiplasticizing effect of water and glycerol contents on native corn starch samples is investigated by FT-Raman and {sup 13}C CP/MAS NMR spectroscopy. The presence of both amorphous and crystalline structural phases was evidenced in pure native corn starch and also in the samples containing plasticizers. Among the crystalline starch structures, the A- and V- types were suggested by CP/MAS NMR spectra.

  11. Effects of Cornus mas L. and Morus rubra L. extracts on penicillin-induced epileptiform activity: an electrophysiological and biochemical study.

    Science.gov (United States)

    Tubaş, Filiz; Per, Sedat; Taşdemir, Abdulkadir; Bayram, Ayşe Kaçar; Yıldırım, Mehmet; Uzun, Aydın; Saraymen, Recep; Gümüş, Hakan; Elmalı, Ferhan; Per, Hüseyin

    2017-01-01

    Traditionally, Morus rubra L. (Moraceae) (red mulberry) and Cornus mas L. (Cornacea) (cornelian cherry) fruits are eaten fresh and are also used in marmalades, juices, jam, natural dyes in Turkey and are believed to have beneficial effects in case of multiple health issues such as antipyretic, diarrhea and intestinal parasites. However, the effects of M. rubra and C. mas on epilepsy has not been known. This study evaluates the effects of M. rubra and C. mas extracts on penicillin-induced epileptiform activity. Sixty Wistar rats randomly divided into ten groups (n=6): control, sham, penicillin, penicillin+M. rubra extract (2.5, 5, 10, 20 mg/kg) and penicillin+C. mas extract (2.5, 5, 10 mg/kg). Epileptiform activity was induced by using penicillin (500 IU, i.c.) and electrocorticogram records (150 min) were obtained. Also, biochemical analysis in blood samples were evaluated. According to the electrocorticogram analysis, the effective dose was detected as 10 mg/kg for both C. mas and M. rubra. This dose decreased the spike frequencies of convulsions while amplitude wasn't changed by both substances. In erythrocyte studies, there were significant differences regarding nitric oxide in the control, sham and penicillin groups. There were significant differences regarding malondialdehyde in all groups. In the plasma, there were significant differences among groups regarding xanthine oxidase in the penicillin‑C. mas and penicillin‑M. rubra groups. There were differences regarding malondialdehyde in the penicillin-C. mas and M. rubra-C. mas groups. Both extracts reduced the frequency of epileptiform activity. After administration of the extracts malondialdehyde levels decreased also in both erythrocytes and plasma.

  12. Classification of astrocyto-mas and meningiomas using statistical discriminant analysis on MRI data

    International Nuclear Information System (INIS)

    Siromoney, Anna; Prasad, G.N.S.; Raghuram, Lakshminarayan; Korah, Ipeson; Siromoney, Arul; Chandrasekaran, R.

    2001-01-01

    The objective of this study was to investigate the usefulness of Multivariate Discriminant Analysis for classifying two groups of primary brain tumours, astrocytomas and meningiomas, from Magnetic Resonance Images. Discriminant analysis is a multivariate technique concerned with separating distinct sets of objects and with allocating new objects to previously defined groups. Allocation or classification rules are usually developed from learning examples in a supervised learning environment. Data from signal intensity measurements in the multiple scan performed on each patient in routine clinical scanning was analysed using Fisher's Classification, which is one method of discriminant analysis

  13. Medical Imaging Teacher: A program to simulate X-ray images of the body by considering kVp, mAs and FFD values

    Directory of Open Access Journals (Sweden)

    Umit Kara

    2017-06-01

    Full Text Available Introduction: Teaching styles and methods have been constantly changing in the recent years. In the 1980s and 90s, the world was introduced to various developed devices, such as smart boards and early generation smart phones that had an immediate innovative effect on education. These advancements has resulted in a considerable improvement in the current educational techniques. The innovations in medical techniques and their quality is of paramount importance. The aim of this study was to provide an innovative and useful software on radiological applications and contribute to the related literature. Materials and Methods: The Medical Imaging Teacher (MIT program was created and the prototype application was implemented on the Android platform for free use. The programing and testing of the usability of the application were performed by the users of the Google Play Store. Results: In this program, we have developed new software to simulate the X-ray images of the body by considering the peak kilovoltage (kVp, milliamperage per second (mAs, and film focus distance (FFD values. The application has been downloaded more than 1,000 times without paid advertising. We enrolled 131 participants, who made comments and gave 4.8 points on average. Conclusion: It can be concluded that with innovative digital programs, such as the MIT, the medical machine-based learning and medical applications have risen to new levels. The software on medical testing and examination is gaining increasing popularity among the health-related applications for smart phones.

  14. Brain angiotensin-(1-7)/Mas axis: A new target to reduce the cardiovascular risk to emotional stress.

    Science.gov (United States)

    Fontes, Marco Antônio Peliky; Martins Lima, Augusto; Santos, Robson Augusto Souza dos

    2016-04-01

    Emotional stress is now considered a risk factor for several diseases including cardiac arrhythmias and hypertension. It is well known that the activation of neuroendocrine and autonomic mechanisms features the response to emotional stress. However, its link to cardiovascular diseases and the regulatory mechanisms involved remain to be further comprehended. The renin-angiotensin system (RAS) plays an important role in homeostasis on all body systems. Specifically in the brain, the RAS regulates a number of physiological aspects. Recent data indicate that the activation of angiotensin-converting enzyme/angiotensin II/AT1 receptor axis facilitates the emotional stress responses. On the other hand, growing evidence indicates that its counterregulatory axis, the angiotensin-converting enzyme 2 (ACE2)/(Ang)iotensin-(1-7)/Mas axis, reduces anxiety and attenuates the physiological responses to emotional stress. The present review focuses on angiotensin-(1-7)/Mas axis as a promising target to attenuate the physiological response to emotional stress reducing the risk of cardiovascular diseases. Copyright © 2015 Elsevier Ltd. All rights reserved.

  15. Productivity differences and food security: a metafrontier analysis of rain-fed maize farmers in MasAgro in Mexico

    Directory of Open Access Journals (Sweden)

    M. Laura Donnet

    2017-04-01

    Full Text Available Rain-fed maize production in Mexico includes approximately 6 million hectares which variation in productivity represents huge challenges to meeting the sustainable intensification goals of the Sustainable Modernization of Traditional Agriculture (MasAgro program. We use the information available from farmers participating in this program to investigate the differences in productivity and the effects of the promoted practices and technologies in seven defined rain-fed maize regions. We do this by applying metafrontier analysis to measure the technical efficiency and the technology gap. The results show a range of technical efficiency from 70 to 100%, which indicates the gains that can be achieved through improved management of the current inputs and practices of farmers in the program, and a range of the environment–technology gap between 32 and 82%, which indicates the limitations of the production environment which would require innovations in technologies and policies particularly adapted for the dry, the tropical and the more traditional regions. Furthermore, the results show that the use of hybrid seed and selling into maize markets have the largest impact in increasing maize yields in all regions. The difference between the MasAgro farmers and the average farmers in each region suggest that scaling the project will contribute to increasing maize production and Mexico’s food self-sufficiency.

  16. Minho Affective Sentences (MAS): Probing the roles of sex, mood, and empathy in affective ratings of verbal stimuli.

    Science.gov (United States)

    Pinheiro, Ana P; Dias, Marcelo; Pedrosa, João; Soares, Ana P

    2017-04-01

    During social communication, words and sentences play a critical role in the expression of emotional meaning. The Minho Affective Sentences (MAS) were developed to respond to the lack of a standardized sentence battery with normative affective ratings: 192 neutral, positive, and negative declarative sentences were strictly controlled for psycholinguistic variables such as numbers of words and letters and per-million word frequency. The sentences were designed to represent examples of each of the five basic emotions (anger, sadness, disgust, fear, and happiness) and of neutral situations. These sentences were presented to 536 participants who rated the stimuli using both dimensional and categorical measures of emotions. Sex differences were also explored. Additionally, we probed how personality, empathy, and mood from a subset of 40 participants modulated the affective ratings. Our results confirmed that the MAS affective norms are valid measures to guide the selection of stimuli for experimental studies of emotion. The combination of dimensional and categorical ratings provided a more fine-grained characterization of the affective properties of the sentences. Moreover, the affective ratings of positive and negative sentences were not only modulated by participants' sex, but also by individual differences in empathy and mood state. Together, our results indicate that, in their quest to reveal the neurofunctional underpinnings of verbal emotional processing, researchers should consider not only the role of sex, but also of interindividual differences in empathy and mood states, in responses to the emotional meaning of sentences.

  17. Surface Characterization of Some Novel Bonded Phase Packing Materials for HPLC Columns Using MAS-NMR Spectroscopy

    Directory of Open Access Journals (Sweden)

    Jude Abia

    2015-03-01

    Full Text Available Information on the surface properties of three novel chemically bonded phase packing materials for High performance liquid chromatography (HPLC were obtained using spectra obtained by solid state cross-polarization (CP magic-angle spinning (MAS nuclear magnetic resonance (NMR spectroscopic experiments for the 29Si, and 13C nuclei. These packing materials were: Cogent bidentate C18 bonded to type-C silica, hybrid packing materials XTerra MS C18, and XBridge Prep. C18. The spectra obtained using cross-polarization magic angle spinning (CP-MAS on the Cogent bidentate C18 bonded to type-C silica show the surface to be densely populated with hydride groups (Si-H, with a relative surface coverage exceeding 80%. The hybrid packing materials XTerra and XBridge gave spectra that reveal the silicon atoms to be bonded to organic moieties embedded in the molecular structure of these materials with over 90% of the alkyl silicon atoms found within the completely condensed silicon environments. The hydrolytic stability of these materials were investigated in acidic aqueous solutions at pHs of 7.0 and 3.0, and it was found that while the samples of XTerra and XBridge were not affected by hydrolysis at this pH range, the sample of Cogent lost a significant proportion of its Si-H groups after five days of treatment in acidic aqueous solution.

  18. Klientu attiecību pārvaldības sistēmas izveide autoservisam

    OpenAIRE

    Jaunzems, Ģirts

    2012-01-01

    Diplomdarba tēma ir Klientu attiecību pārvaldības sistēmas izveide autoservisam. Tā mērķis ir izstrādāt un ieviest pielāgotu klientu attiecību pārvaldības sistēmu nelielam autoservisam, tādējādi atvieglojot klientu un viņu darbības vēstures uzskaiti. Lai sasniegtu diplomdarba mērķi, darba autors izpētīja teorētiskos informācijas avotus, salīdzināja divas klientu pārvaldības sistēmas, kā arī izstrādāja sistēmu konkrētam uzņēmumam, veicot arī tās izmaksu analīzi. Diplomdarbā ir secināts, ...

  19. Perilaku Alturisme Karyawan (Studi Kasus pada Mandor Perkebunan Sawit Perseroan Terbatas (PT.Tribuana Mas Kabupaten Tapin

    Directory of Open Access Journals (Sweden)

    Asty Wulandari

    2017-11-01

    Full Text Available One of the tasks of developing into adulthood is to work to meet the needs of his life. Technological advances, materialism, hedonism and the demands of the post-industrial society's needs make some people work brutally for what they want to be fulfilled. Even people are apathetic to the surrounding environment. Nevertheless, there are still a handful of employees who care about their environmental conditions by behaving altruism as happened in PT.Tribuana Mas (TBM. The purpose of this study is to describe employee altruism behavior and explore the factors that encourage employees to behave altruism. The results of the research on 3 employees of PT.Tribuana Mas plantation, Afdeling Juliet conducted qualitatively (nonparticipant observation and in-depth interview, altruism behavioral components are mostly the same, that is behaving helpfully, considering the rights and welfare of others, sharing and honesty. While the different components are seen from the behavior of donating & generosity and Cooperation. Components of altruism behavior reflected on the employees are also in accordance with the teachings of Islam, the namely charity with the foundation of god (ikhlas and there are still nuanced humanity. It is influenced by various factors, both situational (external and within (internal

  20. Mas d’Is (Penàguila, Alicante: farms and Early Neolithic causewayed camps in the Serpis valley

    Directory of Open Access Journals (Sweden)

    Bernabeu Auban, Joan

    2003-12-01

    Full Text Available In this paper, results from recent archaeological field work carried out in the Neolithic village of Mas d’Is (Penàguila, Alicante are presented. We focus on an important set of domestic and monumental architectural structures. Integration of data from the site in a regional context allows us to rethink the social relations of the first farmers in the area. At the same time, radiocarbon data from our excavations show a finer chronology of the neolithization in Western Mediterranean, and what is more important to approach its historical process.

    En este trabajo presentamos los resultados de los recientes trabajos llevados a cabo en la aldea neolítica de Mas d’Is (Penàguila, Alicante, centrándonos en las estructuras documentadas. La integración de los datos obtenidos en un contexto regional nos permiten plantear algunas reflexiones sobre la Arqueología social de los primeros agricultores, al tiempo que las dataciones radiocarbónicas permiten ir ajustando la cronología de la neolitización del Mediterráneo Occidental, así como el desarrollo de dicho proceso histórico.

  1. PERANAN GAYA KEPEMIMPINAN YANG EFEKTIF DALAM UPAYA MENINGKATKAN SEMANGAT DAN KEGAIRAHAN KERJA KARYAWAN DI TOSERBA SINAR MAS SIDOARJO

    Directory of Open Access Journals (Sweden)

    Eddy Madiono Sutanto

    2000-01-01

    Full Text Available Leadership represents something that should be possessed by each leader of an organization. The effectiveness of a leader is determined by his ability to influence and direct the members of the organization. In order test the style of leadership which is effective at Toserba Sinar Mas in Sidoarjo, this research seeks to determine the relationship of leadership style with enthusiasm and excitement for work. In this study, it is found that the most effective leadership style is leadership which is adapted to the situation of the people being led. There is an indication that enthusiasm and excitement (measured by the level of absenteeism and worker turnover for work may decline as a result of unfavorable leadership. Abstract in Bahasa Indonesia : Kepemimpinan merupakan suatu hal yang seharusnya dimiliki oleh setiap pemimpin organisasi. Efektivitas seorang pemimpin ditentukan oleh kepiawaiannya mempengaruhi dan mengarahkan para anggotanya. Di dalam rangka untuk menguji gaya kepemimpinan yang efektif di Toserba Sinar Mas, Sidoarjo, maka penelitian ini dilakukan untuk membuktikan hubungan antara gaya kepemimpinan dengan semangat dan kegairahan kerja. Di dalam penelitian ini diungkapkan bahwa gaya kepemimpinan yang efektif adalah kepemimpinan yang disesuaikan dengan situasi dan kondisi dari orang-orang yang dipimpin. Indikasi turunnya semangat dan kegairahan kerja ditunjukkan dengan tingginya tingkat absensi dan perpindahan karyawan. Hal itu timbul sebagai akibat dari kepemimpinan yang tidak disenangi. Kata kunci: gaya kepemimpinan, semangat kerja, kegairahan kerja, tingkat absensi, tingkat perpindahan

  2. Des schémas équivalents pour les circuits couplés multi-enroulements

    Science.gov (United States)

    Keradec, J. P.; Cogitore, B.; Laveuve, E.; Bensoam, M.

    1994-04-01

    The aim of this paper is to represent the electrical behaviour of any number of magnetically coupled windings with couplers and inductors. Two methods, mathematicaly justified, are proposed. The second one introduces only positive inductances. As an exemple, it is applied to the representation of a three column three phase transformer. The obtained circuits supply the requisite guide to design more complete circuits which allow the high frequency behaviour of wound components to be taken into account, especialy in electronics simulation softwares. Le but de cet article est de traduire le comportement électrique d'un nombre quelconque d'enroulements magnétiquement couplés, par des coupleurs et des inductances. Deux méthodes, établies mathématiquement, sont proposées. La seconde n'introduit que des inductances positives. A titre d'exemple, elle est appliquée à la représentation d'un transformateur triphasé à trois colonnes. Les schémas obtenus fournissent l'indispensable ossature de schémas plus complets, aptes à représenter le comportement haute fréquence des composants bobinés, notamment dans un logiciel de simulation électronique.

  3. Monitoramento físico-químico de um biorreator com resíduos sólidos urbanos em escala piloto na cidade de Campina Grande (PB

    Directory of Open Access Journals (Sweden)

    Libânia da Silva Ribeiro

    2016-03-01

    Full Text Available RESUMO O monitoramento dos parâmetros físico-químicos em resíduos sólidos urbanos (RSU é de grande importância, por descrever as condições nas quais os fenômenos de degradação se processam. O pH, assim como a demanda biológica de oxigênio (DBO e a demanda química de oxigênio (DQO, permite acompanhar o processo de decomposição dos RSU em aterros sanitários, indicando a evolução da degradação microbiológica da matéria orgânica e a evolução global do processo de estabilização da massa de resíduos. Este trabalho teve como objetivo avaliar, por meio dos parâmetros físico-químicos, a decomposição dos RSU depositados em um biorreator na cidade de Campina Grande (PB. Este estudo contou com a construção de um biorreator que simula um aterro sanitário em escala real. Os resultados inicialmente mostraram que os resíduos apresentaram altas concentrações de DQO e DBO e baixos valores de pH. Ao longo do monitoramento houve crescimento do pH e redução nas concentrações de DQO e DBO. Pode-se concluir que a biodegradação dos resíduos se desenvolveu de maneira eficaz, de acordo com o tempo de degradação para o período monitorado, e que a matéria orgânica encontra-se em estágio avançado de decomposição.

  4. Monitoramento da salinidade de águas subterrâneas em várzea cultivada com cana-de-açúcar fertirrigada com vinhaça

    Directory of Open Access Journals (Sweden)

    Wellington P. da Silva

    2014-04-01

    Full Text Available Propôs-se, neste trabalho, avaliar o risco potencial da vinhaça em proporcionar a salinidade e sodicidade das águas subterrâneas em área de várzea cultivada com cana-de-açúcar. O experimento foi conduzido em uma Usina da Mata Sul de Pernambuco durante o período de dezembro de 2010 a setembro de 2011. O dispositivo experimental adotado foi composto de uma malha georreferenciada de 81 poços de monitoramento distribuídos ao longo de uma área de 7,5 ha constituindo três subáreas com 2,5 ha, todas cultivadas com cana-de-açúcar. Na área foram aplicadas doses equivalentes a 50, 60 e 65 m³ ha-1 de vinhaça de mosto de melaço. Para a avaliação da qualidade da água subterrânea foram realizadas seis amostragens e analisados os parâmetros CE, pH, Na+, Ca2+, Mg2+ e RAS. A aplicação de doses de vinhaça até 65 m³ ha-1, em áreas de várzea, para os parâmetros analisados, não proporcionou riscos de salinização das águas subterrâneas nem, tampouco, a CE e a RAS para a salinidade e sodicidade no período avaliado. O monitoramento dos parâmetros químicos do lençol freático mostrou, ao longo do tempo, redução de suas concentrações em função da precipitação pluviométrica ocorrida no período estudado.

  5. Incorporation of phosphorus guest ions in the calcium silicate phases of Portland cement from 31P MAS NMR spectroscopy.

    Science.gov (United States)

    Poulsen, Søren L; Jakobsen, Hans J; Skibsted, Jørgen

    2010-06-21

    Portland cements may contain small quantities of phosphorus (typically below 0.5 wt % P(2)O(5)), originating from either the raw materials or alternative sources of fuel used to heat the cement kilns. This work reports the first (31)P MAS NMR study of anhydrous and hydrated Portland cements that focuses on the phase and site preferences of the (PO(4))(3-) guest ions in the main clinker phases and hydration products. The observed (31)P chemical shifts (10 to -2 ppm), the (31)P chemical shift anisotropy, and the resemblance of the lineshapes in the (31)P and (29)Si MAS NMR spectra strongly suggest that (PO(4))(3-) units are incorporated in the calcium silicate phases, alite (Ca(3)SiO(5)) and belite (Ca(2)SiO(4)), by substitution for (SiO(4))(4-) tetrahedra. This assignment is further supported by a determination of the spin-lattice relaxation times for (31)P in alite and belite, which exhibit the same ratio as observed for the corresponding (29)Si relaxation times. From simulations of the intensities, observed in inversion-recovery spectra for a white Portland cement, it is deduced that 1.3% and 2.1% of the Si sites in alite and belite, respectively, are replaced by phosphorus. Charge balance may potentially be achieved to some extent by a coupled substitution mechanism where Ca(2+) is replaced by Fe(3+) ions, which may account for the interaction of the (31)P spins with paramagnetic Fe(3+) ions as observed for the ordinary Portland cements. A minor fraction of phosphorus may also be present in the separate phase Ca(3)(PO(4))(2), as indicated by the observation of a narrow resonance at delta((31)P) = 3.0 ppm for two of the studied cements. (31)P{(1)H} CP/MAS NMR spectra following the hydration of a white Portland cement show that the resonances from the hydrous phosphate species fall in the same spectral range as observed for (PO(4))(3-) incorporated in alite. This similarity and the absence of a large (31)P chemical shift ansitropy indicate that the hydrous (PO(4

  6. Determination of structure of oriented samples using two-dimensional solid state NMR techniques

    International Nuclear Information System (INIS)

    Jin Hong; Harbison, G.S.

    1990-01-01

    One dimensional and two-dimensional MAS techniques can give detailed information about the structure and dynamics of oriented systems. We describe the application of such techniques to the liquid-crystalline polymer poly(p-phenyleneterphtalimide) (PPTA), and thence deduce the solid-state structure of the material. (author). 9 refs.; 6 figs

  7. Residual dipolar couplings in sup 3 sup 1 P MAS spectra of PPh sub 3 substituted cobalt complexes

    CERN Document Server

    Szalontai, G

    2002-01-01

    Residual dipolar couplings between sup 3 sup 1 P- sup 5 sup 9 Co spin pairs were studied in sup 3 sup 1 P MAS spectra of mono- and dinuclear cobalt-triphenylphosphine complexes. These spectra can provide important information such as the scalar coupling between the dipolar phosphorus and the quadrupolar cobalt nuclei normally not available from solution phase studies. In case of complementary (NQR or x-ray) data even the relative orientation of the interacting shielding, dipolar, scalar couplings, and electric field gradient tensors or internuclear distances can be determined. Examples are shown both for well resolved and practically unresolved cases, factors which possibly control the spectral resolution are discussed in detail. (author)

  8. Spin-echo based diagonal peak suppression in solid-state MAS NMR homonuclear chemical shift correlation spectra

    Science.gov (United States)

    Wang, Kaiyu; Zhang, Zhiyong; Ding, Xiaoyan; Tian, Fang; Huang, Yuqing; Chen, Zhong; Fu, Riqiang

    2018-02-01

    The feasibility of using the spin-echo based diagonal peak suppression method in solid-state MAS NMR homonuclear chemical shift correlation experiments is demonstrated. A complete phase cycling is designed in such a way that in the indirect dimension only the spin diffused signals are evolved, while all signals not involved in polarization transfer are refocused for cancellation. A data processing procedure is further introduced to reconstruct this acquired spectrum into a conventional two-dimensional homonuclear chemical shift correlation spectrum. A uniformly 13C, 15N labeled Fmoc-valine sample and the transmembrane domain of a human protein, LR11 (sorLA), in native Escherichia coli membranes have been used to illustrate the capability of the proposed method in comparison with standard 13C-13C chemical shift correlation experiments.

  9. Hydration properties and phosphorous speciation in native, gelatinized and enzymatically modified potato starch analyzed by solid-state MAS NMR

    DEFF Research Database (Denmark)

    Larsen, Flemming H.; Kasprzak, Miroslaw Marek; Lærke, Helle Nygaard

    2013-01-01

    Hydration of granular, gelatinized and molecularly modified states of potato starch in terms of molecular mobility were analyzed by 13C and 31P solid-state MAS NMR. Gelatinization (GEL) tremendously reduced the immobile fraction compared to native (NA) starch granules. This effect was enhanced...... by enzyme-assisted catalytic branching with branching enzyme (BE) or combined BE and β-amylase (BB) catalyzed exo-hydrolysis. Carbons of the glycosidic α-1,6 linkages required high hydration rates before adopting uniform chemical shifts indicating solid-state disorder and poor water accessibility...... regions was only observed in NA starch. Moreover phosphorous was observed in a minor pH-insensitive form and as major phosphate in hydrated GEL and BE starches....

  10. Studies using 27Al MAS NMR of AFm and AFt phases and the formation of Friedel's salt

    International Nuclear Information System (INIS)

    Jones, M.R.; Macphee, D.E.; Chudek, J.A.; Hunter, G.; Lannegrand, R.; Talero, R.; Scrimgeour, S.N.

    2003-01-01

    This paper describes the application of the magic angle spinning (MAS) NMR spectroscopy to study the chemical environment of 27 Al-bearing phases in Portland cement-based concrete. A specific methodology is described that allows reliable spectra to be determined for combinations of different types of cements and fillers (in this case, Portland cement, fly ash, slag, silica fume, metakaolin and limestone filler). As well as the study of 'molecular structure' of cement matrix, the paper reviews the mechanism of Friedel's salt formation in cement systems. Mechanisms based on ion exchange of chloride for hydroxide in hydroxy-AF m and on chloride absorption on formation are discussed. Finally, the nature of the chloride/hydrate binding phenomena are described to provide a reasonable robust and fundamental picture of the role different cements can play in the provision of overall concrete durability to chloride ingress from a chemical perspective

  11. Morphological and Biochemical Characteristics of Fruits of Different Cornelian Cherry (Cornus mas L. Genotypes from Spontaneous Flora

    Directory of Open Access Journals (Sweden)

    Felicia-Constantina CORNESCU

    2017-12-01

    Full Text Available The current study was carried out on six local cornelian cherry (Cornus mas L. genotypes, grown in Turceni town (Gorj county and Baita village (Hunedoara county, in Romania. Several morphological and biochemical characteristics of cultivars were determined. Fruit weight and fruit flesh ratio of the analyzed genotypes ranged from 1.33 to 2.31 g and 61.53 to 78.58% respectively. Soluble solid contents were determined, the lowest noted as 10% and the highest as 25.5%. Results have shown that there was a high diversity in cornelian cherry populations within different ecological areas. Differences were exhibited in terms of fruit size and biochemical characteristics. The results of the study are useful for attempting to select superior genotypes of cornelian cherry for culture.

  12. 27Al MAS NMR spectroscopic identification of reaction intermediates in the carbothermal reduction and nitridation of alumina

    International Nuclear Information System (INIS)

    Jung, Woo-Sik; Chae, Seen-Ae

    2010-01-01

    The reaction intermediates in the carbothermal reduction and nitridation (CRN) reaction of γ-Al 2 O 3 were identified by 27 Al magic-angle spinning (MAS) nuclear magnetic resonance (NMR) spectroscopy. This identification ruled out the possibility of a reaction mechanism involving the gaseous reaction intermediates. In the CRN reaction of γ-Al 2 O 3 , AlO 4 units were converted to AlN stepwise via AlN x O 4-x (x = 1, 2, 3) intermediates, while AlO 6 units were more slowly converted to AlN than AlO 4 units and the NMR peaks of partially nitridated AlO 6 units were not detected. The NMR peak intensities of partially nitridated AlO 4 units became weaker with increasing reaction temperature.

  13. Antenatal betamethasone attenuates the angiotensin-(1-7)-Mas receptor-nitric oxide axis in isolated proximal tubule cells.

    Science.gov (United States)

    Su, Yixin; Bi, Jianli; Pulgar, Victor M; Chappell, Mark C; Rose, James C

    2017-06-01

    We previously reported a sex-specific effect of antenatal treatment with betamethasone (Beta) on sodium (Na + ) excretion in adult sheep whereby treated males but not females had an attenuated natriuretic response to angiotensin-(1-7) [Ang-(1-7)]. The present study determined the Na + uptake and nitric oxide (NO) response to low-dose Ang-(1-7) (1 pM) in renal proximal tubule cells (RPTC) from adult male and female sheep antenatally exposed to Beta or vehicle. Data were expressed as percentage of basal uptake or area under the curve for Na + or percentage of control for NO. Male Beta RPTC exhibited greater Na + uptake than male vehicle cells (433 ± 28 vs. 330 ± 26%; P 0.05). Ang-(1-7) significantly inhibited Na + uptake in RPTC from vehicle male (214 ± 11%) and from both vehicle (190 ± 14%) and Beta (209 ± 11%) females but failed to attenuate Na + uptake in Beta male cells. Beta exposure also abolished stimulation of NO by Ang-(1-7) in male but not female RPTC. Both the Na + and NO responses to Ang-(1-7) were blocked by Mas receptor antagonist d-Ala 7 -Ang-(1-7). We conclude that the tubular Ang-(1-7)-Mas-NO pathway is attenuated in males and not females by antenatal Beta exposure. Moreover, since primary cultures of RPTC retain both the sex and Beta-induced phenotype of the adult kidney in vivo they appear to be an appropriate cell model to examine the effects of fetal programming on Na + handling by the renal tubules. Copyright © 2017 the American Physiological Society.

  14. Fetal betamethasone exposure attenuates angiotensin-(1-7)-Mas receptor expression in the dorsal medulla of adult sheep.

    Science.gov (United States)

    Marshall, Allyson C; Shaltout, Hossam A; Nautiyal, Manisha; Rose, James C; Chappell, Mark C; Diz, Debra I

    2013-06-01

    Glucocorticoids including betamethasone (BM) are routinely administered to women entering into early preterm labor to facilitate fetal lung development and decrease infant mortality; however, fetal steroid exposure may lead to deleterious long term consequences. In a sheep model of fetal programming, BM-exposed (BMX) offspring exhibit elevated mean arterial pressure (MAP) and decreased baroreflex sensitivity (BRS) for control of heart rate by 0.5-years of age associated with changes in the circulating and renal renin-angiotensin systems (RAS). In the brain solitary tract nucleus, angiotensin (Ang) II actions through the AT1 receptor oppose the beneficial actions of Ang-(1-7) at the Mas receptor for BRS regulation. Therefore, we examined Ang peptides, angiotensinogen (Aogen), and receptor expression in this brain region of exposed and control offspring of 0.5- and 1.8-years of age. Mas protein expression was significantly lower (>40%) in the dorsal medulla of BMX animals at both ages; however, AT1 receptor expression was not changed. BMX offspring exhibited a higher ratio of Ang II to Ang-(1-7) (2.30±0.36 versus 0.99±0.28; p<0.01) and Ang II to Ang I at 0.5-years. Although total Aogen was unchanged, Ang I-intact Aogen was lower in 0.5-year BMX animals (0.78±0.06 vs. 1.94±0.41; p<0.05) suggesting a greater degree of enzymatic processing of the precursor protein in exposed animals. We conclude that in utero BM exposure promotes an imbalance in the central RAS pathways of Ang II and Ang-(1-7) that may contribute to the elevated MAP and lower BRS in this model. Copyright © 2013 Elsevier Inc. All rights reserved.

  15. Avaliação executiva de indicadores no governo do estado de Minas Gerais: análise da implementação de uma ferramenta de monitoramento e avaliação

    Directory of Open Access Journals (Sweden)

    Éber Gonçalves

    2011-12-01

    Full Text Available A Avaliação Executiva de Indicadores (AEI é uma tecnologia criada pelo governo de Minas Gerais, por intermédio do Programa Estado para Resultados, para ser empregada na avaliação sistemática da qualidade dos indicadores monitorados no âmbito da gestão estratégica do estado de Minas Gerais. O instrumento consiste em 34 perguntas, reunidas em quatro eixos temáticos: produção dos dados, produção do indicador, conceito e metodologia, e uso e comunicação. Os quesitos avaliados estão associados aos atributos desejáveis aos indicadores, como clareza, relevância, adequação, tempestividade e especificidade. A metodologia desenvolvida foi aplicada na avaliação da carteira de indicadores de 2009, composta por 104 indicadores. A avaliação resultou na identificação das características positivas e das lacunas do processo de produção de cada indicador, referenciando o trabalho de consolidação da carteira de indicadores na gestão para resultados. A AEI agrega valor à atividade de monitoramento, incentivando o desenvolvimento de medidas adequadas dos resultados das políticas públicas e contribuindo para o fortalecimento do modelo de contratação de resultado na gestão mineira.

  16. Monitoramento das águas subterrâneas e lixiviado do local de disposição dos resíduos sólidos urbanos do município de Passo Fundo

    Directory of Open Access Journals (Sweden)

    Márcia Helena Beck

    2009-12-01

    Full Text Available O objetivo desta pesquisa foi o monitoramento das águas subterrâneas e do lixiviado, do local de disposição de resíduos sólidos urbanos do município de Passo Fundo, uma parceria entre universidade e instituição pública, no intuito de investigar possíveis danos ao meio ambiente. Para isto foram executadas analises físico-químicas durante o período de junho de 2004 a janeiro de 2005 no local de disposição destes resíduos. Os resultados demonstraram que os valores encontrados nas águas subterrâneas, de cloreto, sódio, zinco, cobre, nitrito e dureza obedeceram aos padrões de potabilidade. Porém, a qualidade destas águas está comprometida, devido aos valores de condutividade elétrica, DBO e DQO. Pode-se concluir deste estudo que as águas subterrâneas estão contaminadas com o lixiviado produzido pelos resíduos sólidos, provenientes da deposição dos resíduos sólidos urbanos, produzidos pela cidade de Passo Fundo.

  17. Valsartan attenuates intimal hyperplasia in balloon-injured rat aortic arteries through modulating the angiotensin-converting enzyme 2-angiotensin-(1-7)-Mas receptor axis.

    Science.gov (United States)

    Li, Yonghong; Cai, Shanglang; Wang, Qixin; Zhou, Jingwei; Hou, Bo; Yu, Haichu; Ge, Zhiming; Guan, Renyan; Liu, Xu

    2016-05-15

    The role of the Mas receptor in the activity of valsartan against intimal hyperplasia is unclear. Herein, we investigated the role of the angiotensin-converting enzyme 2 (ACE2)-angiotensin-(1-7)-Mas receptor axis on the activity of valsartan against intimal hyperplasiain balloon-injured rat aortic arteries. Wistar rats were randomized equally into the sham control group, injured group, and injured plus valsartan (20 mg/kg/d)-treated group. Valsartan significantly attenuated the vascular smooth muscle cell proliferation and intimal and medial thickening on days 14 and 28 after injury. The angiotensin-(1-7) levels as well as ACE2 and Mas receptor mRNA/protein expression were significantly decreased in the injured rats, compared to the uninjured rats; meanwhile, the angiotensin II level as well as the ACE and AT1 receptor mRNA/protein expression were increased (all P valsartan significantly increased the angiotensin-(1-7) levels as well as ACE2 and Mas receptor mRNA/protein expression but decreased the angiotensin II level, ACE and AT1 receptor mRNA/protein expression, as well as the p-ERK protein expression, compared to the injured group (all P valsartan attenuates neointimal hyperplasiain balloon-injured rat aortic arteries through activation of the ACE2-angiotensin-(1-7)-Mas axis as well as inhibition of the ACE-angiotensin II-AT1 and p-ERK pathways. Copyright © 2016 Elsevier Inc. All rights reserved.

  18. Reorientation of the Methyl Group in MAs(III) is the Rate-Limiting Step in the ArsM As(III) S-Adenosylmethionine Methyltransferase Reaction.

    Science.gov (United States)

    Packianathan, Charles; Li, Jiaojiao; Kandavelu, Palani; Sankaran, Banumathi; Rosen, Barry P

    2018-03-01

    The most common biotransformation of trivalent inorganic arsenic (As(III)) is methylation to mono-, di-, and trimethylated species. Methylation is catalyzed by As(III) S -adenosylmethionine (SAM) methyltransferase (termed ArsM in microbes and AS3MT in animals). Methylarsenite (MAs(III)) is both the product of the first methylation step and the substrate of the second methylation step. When the rate of the overall methylation reaction was determined with As(III) as the substrate, the first methylation step was rapid, whereas the second methylation step was slow. In contrast, when MAs(III) was used as the substrate, the rate of methylation was as fast as the first methylation step when As(III) was used as the substrate. These results indicate that there is a slow conformational change between the first and second methylation steps. The structure of CmArsM from the thermophilic alga Cyanidioschyzon merolae sp. 5508 was determined with bound MAs(III) at 2.27 Å resolution. The methyl group is facing the solvent, as would be expected when MAs(III) is bound as the substrate rather than facing the SAM-binding site, as would be expected for MAs(III) as a product. We propose that the rate-limiting step in arsenic methylation is slow reorientation of the methyl group from the SAM-binding site to the solvent, which is linked to the conformation of the side chain of a conserved residue Tyr70.

  19. Lielveikalu RIMI reklāmas kampaņas ─ auditorijas uzmanības piesaistes analīze

    OpenAIRE

    Fjodorova, Margarita

    2008-01-01

    Mana darba tēma ir „Lielveikalu „RIMI” reklāmas kampaņas – auditorijas uzmanības piesaistes analīze.” Es apskatu 2003. – 2008.gada „RIMI” video reklāmas, lai pierādītu sava darba hipotēzi, ka „RIMI” lielveikalu video reklāmās laika posmā no 2003. līdz 2008. gadam nav bijis vienotu auditorijas uzmanības piesaistes elementu, bet tie tika ieturēti tikai kādas konkrētas reklāmas kampaņas robežās kā galvenie auditorijas uzmanības piesaistes elementi. Sava darba teorētiskajā daļā es pieturēšos pie ...

  20. CONCEPTUALIZACIÓN Y ANÁLISIS DE UN SISTEMA MULTI-AGENTE PEDAGÓGICO UTILIZANDO LA METODOLOGÍA MAS-COMMONKADS

    Directory of Open Access Journals (Sweden)

    JOVANI ALBERTO JIMÉNEZ BUILES

    2009-01-01

    Full Text Available En este artículo se presentan la conceptualización y el análisis de un sistema multi-agente (MAS pedagógico utilizando la metodología MAS-CommonKADS; la cual es una de las más reconocidaspara el modelado de MAS. El propósito de la fase de conceptualización es comprender el problema, identificar los actores activos y pasivo, además de elaborar los requisitos que permitan formular unos objetivos para generar la solución. En la fase de análisis se definen los modelos de agente, tareas, coordinación, comunicación, organizacióny experiencia (conocimientos. Ambas fases fueron validadas mediante la construcción del ambiente multi agente pedagógico ALLEGRO.

  1. Experimental techniques; Techniques experimentales

    Energy Technology Data Exchange (ETDEWEB)

    Roussel-Chomaz, P. [GANIL CNRS/IN2P3, CEA/DSM, 14 - Caen (France)

    2007-07-01

    This lecture presents the experimental techniques, developed in the last 10 or 15 years, in order to perform a new class of experiments with exotic nuclei, where the reactions induced by these nuclei allow to get information on their structure. A brief review of the secondary beams production methods will be given, with some examples of facilities in operation or under project. The important developments performed recently on cryogenic targets will be presented. The different detection systems will be reviewed, both the beam detectors before the targets, and the many kind of detectors necessary to detect all outgoing particles after the reaction: magnetic spectrometer for the heavy fragment, detection systems for the target recoil nucleus, {gamma} detectors. Finally, several typical examples of experiments will be detailed, in order to illustrate the use of each detector either alone, or in coincidence with others. (author)

  2. Angiotensin (1-7) ameliorates the structural and biochemical alterations of ovariectomy-induced osteoporosis in rats via activation of ACE-2/Mas receptor axis.

    Science.gov (United States)

    Abuohashish, Hatem M; Ahmed, Mohammed M; Sabry, Dina; Khattab, Mahmoud M; Al-Rejaie, Salim S

    2017-05-23

    The local and systemic renin angiotensin system (RAS) influences the skeletal system micro-structure and metabolism. Studies suggested angiotensin 1-7 (Ang(1-7)) as the beneficial RAS molecule via Mas receptor activation. This study examines the function of Ang(1-7) in bone micro-architecture and metabolism in an ovariectomized (OVX) rodent model of osteoporosis. OVX rats showed structural and bone metabolic degeneration in parallel with suppressed expressions of the angiotensin converting enzyme-2 (ACE-2)/Ang(1-7)/Mas components. The infusion of Ang(1-7) markedly alleviated the altered bone metabolism and significantly enhanced both trabecular (metaphyseal) and cortical (metaphyseal-diaphyseal) morphometry. Urinary and bones minerals were also improved in OVX rats by Ang(1-7). The infusion of the heptapeptide enhanced ACE-2/Mas receptor expressions, while down-regulated AngII, ACE, and AngII type-1 receptor (AT1R) in OVX animals. Moreover, Ang(1-7) markedly improved osteoprotegerin (OPG) and lowered receptor activator NF-κB ligand (RANKL) expressions. The defensive properties of Ang(1-7) on bone metabolism, structure and minerals were considerably eradicated after blockage of Mas receptor with A-779. Ang(1-7)-induced up-regulated ACE-2/Ang(1-7)/Mas cascade and OPG expressions were abolished and the expressions of ACE/AngII/AT1R and RANKL were provoked by A-779. These findings shows for the first time the novel valuable therapeutic role of Ang(1-7) on bone health and metabolism through the ACE-2/Mas cascade.

  3. Radiation doses during chest examinations using dose modulation techniques in multislice CT scanner

    OpenAIRE

    Livingstone Roshan; Pradip Joe; Dinakran Paul; Srikanth B

    2010-01-01

    Objective: To evaluate the radiation dose and image quality using a manual protocol and dose modulation techniques in a 6-slice CT scanner. Materials and Methods: Two hundred and twenty-one patients who underwent contrast-enhanced CT of the chest were included in the study. For the manual protocol settings, constant tube potential (kV) and tube current-time product (mAs) of 140 kV and 120 mAs, respectively, were used. The angular and z-axis dose modulation techniques utilized a constant tu...

  4. Electromagnetic Scattering Analysis of Coated Conductors With Edges Using the Method of Auxiliary Sources (MAS) in Conjunction With the Standard Impedance Boundary Condition (SIBC)

    DEFF Research Database (Denmark)

    Anastassiu, H.T.; D.I.Kaklamani, H.T.; Economou, D.P.

    2002-01-01

    A novel combination of the method of auxiliary sources (MAS) and the standard impedance boundary condition (SIBC) is employed in the analysis of transverse magnetic (TM) plane wave scattering from infinite, coated, perfectly conducting cylinders with square cross sections. The scatterer is initia......A novel combination of the method of auxiliary sources (MAS) and the standard impedance boundary condition (SIBC) is employed in the analysis of transverse magnetic (TM) plane wave scattering from infinite, coated, perfectly conducting cylinders with square cross sections. The scatterer...

  5. Efektifitas Nannochloropsis sp. terhadap sistem imun non-spesifik ikan mas Cyprinus carpio yang diinfeksi Virus Herpes

    Directory of Open Access Journals (Sweden)

    Arafik Lamadi

    2017-11-01

    Full Text Available The aim of this research was to determine the effect of Nannochlorpsisis sp. against the common carp (Cyprinus carpio leukocyte profile, infected with Koi Hepesvirus (KHV. The  descriptive observational method wa used in this study. This research was conducted for 4 weeks, using common carp length 12±0,3 cm as many as 7 fish. The tested experiment was P1: without infested by Nannochlorpsisis sp. and KH; P2: Infested by  Nannochlorpsisis sp. and without KHV infected; P3: Infected by Nannochloropsis sp. and KHV; P4;  Not infected by Nannochlorpsisis sp. and  infected by KHV. Evey tratment in three replications. The results showed that the highest total leukocyte was obtained in P3 (37.600 cells/ml, followed by  P4 (29.650 cells / ml, P2 (28,500 cells / ml and P1 (21,150 cells / ml. Leukocyte differentiation test on P1 (neutrophil 6.2%, lymphocyte 68.0%, monocyte 17.0%, P2 (neutrophil 6.6%, lymphocyte 72.3%, monocyte 18.3%, P3 (neutrophil 7.9%, lymphocyte 66.1%, monocytes 24.3%, P4 (neutrophils 11.2%, lymphocytes 57.6%, monocytes 37.6%. The higher survivla rate was recorded in P2 (100%. It is concluded that  Nannochloropsis sp. can enhance the common carp immune sytem. Penelitian ini bertujuan untuk mengetahui pengaruh pemberian Nannochlorpsis sp. terhadap profil leukosit ikan mas (Cyprinus carpio yang terinfeksi Koi Herves Virus (KHV. Penelitian ini menggunakan metode deskriptif observasional dengan membandingkan hasil pada perlakuan 1 P1: (tanpa pemberian Nannochlorpsis sp. dan tidak diinfeksi KHV, 2 P2 (diberikan Nannochlorpsis sp dan tanpa diinfeksi KHV, 3 P3 (diberikan Nannochlorpsisis sp dan diinfeksi KHV, 4 P4 (tanpa pemberian Nannochlorpsis sp. dan diinfeksi KHV, masing-masing perlakukan 3 kali ulangan. Penelitian ini dilakukan selama 4 minggu dengan menggunakan Ikan mas berukuran 12±0,3  cm sebanyak 120 ekor. Hasil perhitungan total leukosit tertinggi diperoleh pada P3 (37.600 sel/ml, selanjutnya berturut-turut  P4 (29.650  sel

  6. PAPARAN SENG DI PERAIRAN KALIGARANG TERHADAP EKSPRESI Zn-THIONEIN DAN KONSENTRASI SENG PADA HATI IKAN MAS

    Directory of Open Access Journals (Sweden)

    NK Dewi

    2013-07-01

    Full Text Available Penelitian bertujuan mengetahui paparan seng (Zn di perairan Kaligarang terhadap ekspresi Zn-thionein dan konsentrasi seng pada hati ikan mas (Cyprinus carpio L. Sebanyak 200 ekor ikan dibagi menjadi dua kelompok, masing-masing kelompok 100 ekor. Kelompok kontrol dipelihara di kolam ikan di Balai Benih Ikan Kabupaten Semarang, sedangkan kelompok perlakuan dipelihara pada karamba jaring apung di bagian hilir sungai Kaligarang. Setiap minggu sampel ikan diambil masing-masing lima ekor dari kedua kelompok secara acak untuk diambil organ hatinya dan dianalisis konsentrasi seng dan Zn-thionein. Ikan pada kedua kelompok dipelihara hingga Zn-thionein muncul pada hati ikan. Metallothionein diisolasi dari hati ikan dan dianalisis menggunakan metode High-Performance Liquid Chromatography, dengan larutan standar seng. Setiap satu minggu sekali, konsentrasi seng terlarut pada sampel air dari kedua kelompok diukur dengan metode Atomic Absorption Spectroscopy hingga Zn-thionein muncul. Hasil penelitian menunjukkan bahwa konsentrasi seng yang terlarut dalam air sungai Kaligarang adalah 0,078 mg/l, lebih tinggi dari nilai baku mutu air kelas I (0,05 mg/l. Rata-rata konsentrasi seng yang terabsorbi oleh hati ikan mas pada minggu ke-6 adalah 0,025868 mg/l, lebih rendah dari batas maksimum cemaran seng (100 mg/kg. Rata-rata konsentrasi seng pada hati ikan sebesar 0,025868 µg/g dapat menginduksi munculnya Zn-thionein pada hati ikan mas yang hidup di perairan Kaligarang pada minggu ke-6 perlakuan. The research aims to find concentration of dissolved zinc in the water of Kaligarang River and absorbed zinc concentration inside the liver of carp, also to analyze zinc exposure in Kaligarang River toward Zn-thionein induction inside the liver of carp. The concentration of dissolved zinc was measured using Atomic Absorption Spectroscopy method until Zn-thionein emerges. Metallothionein was isolated from the liver of carp and analyzed using High-Performance Liquid

  7. Tagging of blast resistance gene(s) to DNA markers and marker-assisted selection (MAS) in rice improvement

    International Nuclear Information System (INIS)

    Zhuang, J.Y.; Lu, J.; Qian, H.R.; Lin, H.X.; Zheng, K.L.

    1998-01-01

    This paper reports progress made on the tagging of blast resistance gene(s) to DNA markers and on the initiation of marker-assisted selection (MAS) for blast resistance in rice improvement. A pair of near isogenic lines, K8OR and K79S, were developed using a Chinese landrace Hong-jiao-zhan as the resistance donor. Ten putatively positive markers were identified by screening 177 mapped DNA markers. Using the F 2 population of 143 plants and the derived F 3 lines, three Restriction Fragment Length Polymorphism (RFLP) markers (RG81, RG869 and RZ397) on chromosome 12 of rice were identified to be closely linked to the blast resistance gene Pi-12(t). The genetic distance between Pi-12(t) and the closest marker RG869 was 5.1 cM. By employing the bulk segregant analysis (BSA) procedure, six of 199 arbitrary primers were found to produce positive Randomly Amplified Polymorphic DNA (RAPD) bands. Tight linkage between Pi-12(t) and three RAPD bands, each from a different primer, was confirmed after amplification of DNA of all F 2 individuals. Two fragments were cloned and sequenced, and two sequence characterised amplified re-ion (SCAR) markers were established. In two other F 3 populations, Xian-feng I/Tetep and Xian-feng, 1/Hong-jiao-zhan, the blast resistance was found to be controlled by interactions of two or more genes. One resistance gene was located in the vicinity of RG81 in both populations. Work to identify other gene(s) is currently under way. Marker assisted selection for blast resistance was initiated. Crosses were made between elite varieties and blast resistance donors to develop populations for DNA marker-assisted selection of blast resistance. In addition, 48 varieties widely used in current rice breeding programs were provided by rice breeders. DNA marker-based polymorphism among, these varieties and resistance donors were analysed to produce a database for future MAS program. (author)

  8. Uso do levantamento aéreo expedito convencional e digital para o monitoramento da cobertura florestal no Paraná: estado da arte e potencialidades Conventional aerial sketchmapping and digital aerial sketchmapping development for forest monitoring in Paraná: state of art and potentialities

    Directory of Open Access Journals (Sweden)

    Fernando Luís Dlugosz

    2010-12-01

    Full Text Available

    O artigo apresenta uma abordagem sobre a técnica de Levantamento Aéreo Expedito no que diz respeito às suas características, aplicações e potencialidades para as condições brasileiras, principalmente no monitoramento das mudanças na cobertura florestal no Estado do Paraná. O método consiste na observação e anotação de feições ou fenômenos a partir de  sobrevoos na área de interesse, voando a baixas altitudes ao longo de uma rota pré-determinada. Também são apresentadas as vantagens da introdução da sistematização digital, que definiu a nova  denominação para a técnica como Levantamento Aéreo Expedito Digital. Neste caso, as anotações são realizadas digitalmente sobre tela sensível ao toque, de um computador portátil e não sobre mapa em papel, como na técnica convencional. O desenvolvimento de metodologias que demonstrem eficiência técnica e viabilidade econômica tem recebido maior ênfase em pesquisa, em função da necessidade da obtenção de informações confiáveis para subsidiar a tomada de decisões, em nível governamental, para um adequado processo de fiscalização e/ou de planejamento de uma determinada região. Considerando a dinâmica de uso da terra e a necessidade de se monitorar a cobertura vegetal,  pode-se afirmar que o Levantamento Aéreo Expedito apresenta elevado potencial de aplicação às condições brasileiras e ainda ótima relação custo-benefício.

    doi: 10.4336/2010.pfb.30.63.245

    This paper presents an approach to the technique of aerial sketchmapping in respect to its characteristics, applications and potential for use in Brazil, mainly to monitor changes in forest cover in Paraná state. The method consists of observation and annotation of features or phenomena from overflights in the area of interest flying at low altitudes along a predetermined route. It also presents the advantages obtained with the introduction of digital aerial sketchmapping, which

  9. Ceļu satiksmes drošības direkcijas (CSDD) sociālo reklāmas kampaņu klipu semiotiskā analīze (2003. - 2013.)

    OpenAIRE

    Lapinska, Ginta

    2014-01-01

    Bakalaura darba tēma ir „Ceļu satiksmes drošības direkcijas (CSDD) sociālo reklāmas kampaņu klipu semiotiskā analīze (2003. - 2013.)”. CSDD reklāmas gadu gaitā ir pārliecinājušas reklāmas industriju un auditoriju, tāpēc būtiski ir noskaidrot, kādi ir izmantotie semiotiskie elementi un kā to izmantojums gadu gaitā ir mainījies. Darba mērķis ir izpētīt vienojošos semiotiskos elementus CSDD reklāmas kampaņu klipos no 2003.-2013. gadam. Teorētiskajā daļā aplūkotas tēmas: reklāmas, kampaņas ...

  10. Cooperating systems: Layered MAS

    Science.gov (United States)

    Rochowiak, Daniel

    1990-01-01

    Distributed intelligent systems can be distinguished by the models that they use. The model developed focuses on layered multiagent system conceived of as a bureaucracy in which a distributed data base serves as a central means of communication. The various generic bureaus of such a system is described and a basic vocabulary for such systems is presented. In presenting the bureaus and vocabularies, special attention is given to the sorts of reasonings that are appropriate. A bureaucratic model has a hierarchy of master system and work group that organizes E agents and B agents. The master system provides the administrative services and support facilities for the work groups.

  11. Editorial. Un paso mas

    Directory of Open Access Journals (Sweden)

    Jaime Fandiño Franky

    2014-04-01

    Full Text Available La Fundación Premio Nacional de Epilepsia Margaret Merz de Fandiño, en sus tres convocatorias, ha motivado a los grupos empeñados en el estudio del sistema nervioso para pensar en profundizar en los misterios de la ciencia.

  12. El universo mas pequeno

    CERN Multimedia

    Rivera, Alicia

    2007-01-01

    The future of the exploration of the microcosmos will be in a ring formed by more than 8'000 magnets. With the new great particle acceleator LHC, nearly finished in Geneva, scientists will see how the universe was created just after the Big Bang. (3 pages with photos)

  13. Monitoramento de indicadores de saúde em Instituições de Longa Permanência para Idosos | Monitoring of health indicators in Long Permanence Institutions for the Elderly

    Directory of Open Access Journals (Sweden)

    Karla Cristina Marques Afonso Ferreira

    2016-08-01

    Full Text Available O presente estudo avaliará como as Instituições de Longa Permanência para Idosos (ILPI do município de Natal estão se comportando frente à avaliação e monitoramento de indicadores. Trata-se de um estudo descritivo e longitudinal realizado junto à Vigilância Sanitária (VISA e as ILPI no município de Natal. O estudo utilizou os relatórios enviados pelas instituições à VISA no período de 2013 a 2014. A população desse estudo foi as 16 ILPI cadastradas no município de Natal, RN. O período de coleta dos dados se deu nos meses de junho a agosto de 2015. Quanto aos indicadores, observou-se que as ILPI apresentaram, em 2013 e 2014, respectivamente, uma elevada taxa de mortalidade (3,9%; 11%, altas taxas de incidências de diarreia (5,8%; 24,5%, desidratação (3,9%; 23,6%, úlcera de decúbito (2,6%; 21,6% e desnutrição (11%; 27,3% sobre o total de idosos institucionalizados. Em se tratando de quedas com lesão, poucas instituições notificaram a ocorrência desse evento, o que inviabiliza o monitoramento de um dos agravos de maior prevalência no meio institucional. Todos esses esforços poderão contribuir com ações que favoreçam a melhoria da atenção e assistência aos idosos institucionalizados, na perspectiva de que possam ser realizadas atividades conjuntas de promoção da saúde e prevenção de agravos à saúde. ================================================= This study aimed to present health indicators that identify problems related to elders who reside in Long Permanence Institutions for the Elderly (Brazilian acronym ILPI. It consists of a descriptive and longitudinal study conducted in collaboration with the Sanitary Surveillance (Brazilian acronym VISA and the ILPI of Natal city. The study included reports sent by the institutions to the Sanitary Surveillance between 2013 and 2014. The population in the study was composed by 16 ILPI registered by VISA. Data were collected between June and August 2015. As

  14. Monitoramento in situ e em tempo real de variáveis morfológicas do poli(cloreto de vinila usando espectroscopia NIR Monitoring in situ and in real time the morphological variables of pvc using NIR spectroscopy

    Directory of Open Access Journals (Sweden)

    João M. de Faria Jr.

    2009-06-01

    Full Text Available Este trabalho ilustra o uso de espectroscopia do infravermelho próximo (NIRS para fins de monitoramento da polimerização em suspensão de cloreto de vinila em tempo real. Resultados inéditos mostraram que é possível acompanhar a evolução de importantes propriedades morfológicas de resinas de PVC [poli(cloreto de vinila], como por exemplo, BD (densidade aparente, CPA (absorção de plastificante a frio, DTP (distribuição de tamanho de partículas e Dp (diâmetro de partícula. Mostrou-se também, pela primeira vez, que é possível analisar quantitativamente, com o auxílio da sonda NIRS in situ, a estrutura morfológica da partícula de PVC. Com a possibilidade de predizer a evolução dinâmica dos parâmetros morfológicos em tempo real, mostrou-se que é possível injetar dispersantes e variar a velocidade de agitação durante a reação para fins de controle das variáveis BD, CPA e DTP do PVC, até que o ponto de identificação da partícula seja atingido. Por meio do monitoramento e da estratégia de controle proposta, é possível antecipar fugas de temperatura no reator, aumentar a segurança do processo, diminuir o tempo de desenvolvimento de resinas com características morfológicas diferenciadas, evitando perdas de margem oriundas da venda de produtos fora de especificação, e otimizar os recursos para o desenvolvimento de novos produtos.This work illustrates the use of near infrared spectroscopy (NIRS for monitoring of the suspension polymerization of vinyl chloride in real time. Obtained results showed that it is possible to track in situ and in real time important morphological properties of PVC resins, such as BD (bulk density, CPA (cold plasticizer absorption, PSD (particle size distribution and Dp (average particle diameter. It was also shown for the first time that it is possible to analyze quantitatively, with the help of in situ NIRS probe, the morphological structure of the PVC particles. As a consequence, it

  15. Therapeutic drug monitoring of tacrolimus in pancreas transplantation at São Lucas Hospital Monitoramento terapêutico de tacrolimus em transplante de pâncreas no Hospital São Lucas

    Directory of Open Access Journals (Sweden)

    Luciana Mello de Oliveira

    2007-10-01

    Full Text Available Tacrolimus (FK 506, a potent immunosuppressive drug used in prevention and treatment of rejection of transplanted organs, exhibits efficacy related to its blood levels and has a narrow therapeutic index. These factors require frequent monitoring of patients blood levels, in attempt to adjust the dose to reach the best drug concentration with minimum side effects. In this historic study, the authors evaluated tacrolimus blood profile in patients submitted to pancreas transplantation between June 2002 and March 2004. The results show that blood levels were, mostly, within subtherapeutic (39.1% and toxic (43.4% ranges. Considering post-transplantation period, subtherapeutic levels were more frequent until three months after the graft receiving (51.1% and between three and six months (41.9%, whereas toxic levels were more common six months after the transplantation (63%. Patients who received pancreas/kidney transplantation showed a tendency to present toxic levels. The same did not happen with the patients who received isolated pancreas and pancreas after kidney; these patients presented subtherapeutic blood levels in all post-transplantation periods. The results found in this study reassure the importance of therapeutic monitoring to achieve the adequate blood levels of tacrolimus following pancreas transplantation.O tacrolimus (FK506, um potente imunossupressor utilizado na profilaxia e no tratamento de rejeições pós-transplante, exibe eficácia relacionada com sua concentração sangüínea e possui estreita janela terapêutica. Esses fatores requerem o freqüente monitoramento dos níveis sangüíneos em pacientes que fazem uso do fármaco, tendo como objetivo o ajuste de dose para uma concentração terapêutica ótima com efeitos colaterais mínimos. Este estudo retrospectivo foi realizado através do acesso à base de dados do Laboratório de Patologia Clínica do Hospital São Lucas, da Pontifícia Universidade Católica do Rio Grande do

  16. TPR system: a powerful technique to monitor carbon nanotube formation during chemical vapour deposition; Sistema RTP: uma tecnica poderosa para o monitoramento da formacao de nanotubos de carbono durante o processo por deposicao de vapor quimico

    Energy Technology Data Exchange (ETDEWEB)

    Tristao, Juliana Cristina; Moura, Flavia Cristina Camilo; Lago, Rochel Montero, E-mail: rochel@ufmg.b [Universidade Federal de Minas Gerais (DQ/UFMG), Belo Horizonte, MG (Brazil). Dept. de Quimica; Sapag, Karim [Universidade Nacional de San Luis (Argentina). Lab. de Ciencias de Superficies y Medios Porosos

    2010-07-01

    In this work, a TPR (Temperature Programmed Reduction) system is used as a powerful tool to monitor carbon nanotubes production during CVD (Chemical Vapour Deposition), The experiments were carried out using catalyst precursors based on Fe-Mo supported on Al{sub 2}O{sub 3} and methane as carbon source. As methane reacts on the Fe metal surface, carbon is deposited and H2 is produced. TPR is very sensitive to the presence of H2 and affords information on the temperature where catalyst is active to form different forms of carbon, the reaction kinetics, the catalyst deactivation and carbon yields. (author)

  17. Structural investigations of borosilicate glasses containing MoO{sub 3} by MAS NMR and Raman spectroscopies

    Energy Technology Data Exchange (ETDEWEB)

    Caurant, D., E-mail: daniel-caurant@enscp.f [Laboratoire de Chimie de la Matiere Condensee de Paris, UMR-CNRS 7574, Ecole Nationale Superieure de Chimie de Paris (ENSCP, ParisTech), 11 rue Pierre et Marie Curie, 75231 Paris (France); Majerus, O.; Fadel, E.; Quintas, A. [Laboratoire de Chimie de la Matiere Condensee de Paris, UMR-CNRS 7574, Ecole Nationale Superieure de Chimie de Paris (ENSCP, ParisTech), 11 rue Pierre et Marie Curie, 75231 Paris (France); Gervais, C. [Laboratoire de Chimie de la Matiere Condensee de Paris, UMR-CNRS 7574, Universite Pierre et Marie Curie, 75252 Paris (France); Charpentier, T. [CEA, IRAMIS, Service Interdisciplinaire sur les Systemes Moleculaires et Materiaux, CEA Saclay, 91191 Gif-sur-Yvette (France); Neuville, D. [Physique des Mineraux et des Magmas, UMR-CNRS 7047, Institut de Physique du Globe, place Jussieu, 75252 Paris (France)

    2010-01-01

    High molybdenum concentration in glass compositions may lead to alkali and alkaline-earth molybdates crystallization during melt cooling that must be controlled particularly during the preparation of highly radioactive nuclear glassy waste forms. To understand the effect of molybdenum addition on the structure of a simplified nuclear glass and to know how composition changes can affect molybdates crystallization tendency, the structure of two glass series belonging to the SiO{sub 2}-B{sub 2}O{sub 3}-Na{sub 2}O-CaO-MoO{sub 3} system was studied by {sup 29}Si, {sup 11}B, {sup 23}Na MAS NMR and Raman spectroscopies by increasing MoO{sub 3} or B{sub 2}O{sub 3} concentrations. Increasing MoO{sub 3} amount induced an increase of the silicate network reticulation but no significant effect was observed on the proportion of BO{sub 4}{sup -} units and on the distribution of Na{sup +} cations in glass structure. By increasing B{sub 2}O{sub 3} concentration, a strong evolution of the distribution of Na{sup +} cations was observed that could explain the evolution of the nature of molybdate crystals (CaMoO{sub 4} or Na{sub 2}MoO{sub 4}) formed during melt cooling.

  18. Um ano de muitas preocupações, mas também de esperanças

    Directory of Open Access Journals (Sweden)

    Gabriela Litre

    2015-12-01

    Full Text Available O ano de 2015 foi farto em notícias ruins, mas se encerra com perspectivas boas. As más notícias confirmam que o mundo parece estar de cabeça para baixo, ao menos em matéria ambiental e de segurança internacional. Pioraram as condições climáticas globais; fanáticos religiosos lançaram ataques terroristas de grandes proporções, como os do dia 13 de novembro em Paris, além da surpreendente constituição de uma base territorial onde reina o terror, no Oriente Médio; uma persistente situação da pobreza extrema e de fome em grande escala em alguns países contrasta com a prosperidade em algumas nações; desastres ambientais e instabilidades políticas regionais e nacionais acontecem em cada continente. No Brasil, o rompimento de uma represa de lama e resíduos tóxicos de uma mineradora, em Mariana, Minas Gerais, provocou o que possivelmente seja a pior catástrofe ambiental já registrada no País.

  19. Preču uzskaites sistēmas izstrāde Django ietvarā

    OpenAIRE

    Kokorevičs, Miķelis

    2014-01-01

    Django ietvars ir moderns un pilnvērtīgs tīmekļa ietvars, kas ir veidots Python programmēšanas valodā. Šajā darbā, tiek pētīta Django ietvara funkcionalitāte un piemērotība individuālu preču uzskaites sistēmu izstrādē. Galvenie darba uzdevumi ir izpētīt Django ietvara iespējas un apkopot preču uzskaites sistēmas izstrādei nozīmīgākās priekšrocības. Šī darba rezultātā, tika aprakstīta Django ietvara funkcionalitāte, iespējas un uzbūve. Tika veikts salīdzinājums starp populārākajiem Pyth...

  20. Climate change adaptation in Tanjung Mas – Semarang: a comparison between male- and female-headed households

    Science.gov (United States)

    Handayani, W.; Ananda, M. R.; Esariti, L.; Anggraeni, M.

    2018-03-01

    Mainly due to its complexity, the effort to mainstream gender in addressing climate change issues has been far from the satisfying result. However, there is an urgent call to accommodate gender lens issues and to become more gender sensitive in an attempt to have an effective intervention in responding climate change impact. To enrich the reports on gender and climate change adaptation in city-based case, this paper aims to elaborate climate change adaptation in Tanjung Mas – Semarang city focusing on the gender perspective analysis in male- and female-headed households. The quantitative descriptive method is applied to carry out the analyses, including adaptive strategy and gender role analyses. The research result indicates there are not any significant differences in the climate change adaptation strategies applied in male- and female-headed households. This shows that women in the female-headed households, with their double burden, performed well in managing their roles. Therefore, in particular perspective, it may not be relevant to state that woman and female-headed households are likely to be more vulnerable compared with their counterparts.

  1. Written Exercises: Ancestral Magic and Emergent Intellectuals in Mia Couto, Lhoussain Azergui and Dorota Masłowska

    Directory of Open Access Journals (Sweden)

    Ewa Łukaszyk

    2016-12-01

    Full Text Available Written Exercises: Ancestral Magic and Emergent Intellectuals in Mia Couto, Lhoussain Azergui and Dorota Masłowska The article consists in a comparative reading of three novels: Um rio chamado tempo by Mia Couto, Le pain des corbeaux by Lhoussain Azergui and Paw królowej by Dorota Masłowska. In spite of the difference of the historical circumstances of Mozambique, Morocco and Poland, these three books meet at an intersecting point: the emergence of an intelligentsia that uses literacy and writing as an instrument to deconstruct the post-colonial concept of nation and to operate a trans-colonial renegotiation of identity. By the notion of trans-colonial, I understand the opposition against new kinds of symbolic violence that emerged after the end of the colonial period; here this new form of oppression is related to the concept of national unity – an artificial construct that leaves no place for a dualism or pluralism of cultural reality (two shores of the Zambezi river, Arab and Berber dualism in Morocco, “small homelands” in Poland. The young heroes of the novels grasp the pen in order to break through the falseness or the taboos created by the fathers, establishing, at the same time, the relation of solidarity with the world of the grandfathers. The act of writing becomes an actualization of the ancestral universe of magic. The settlement of accounts with the parental generation concerns the vision of nation built upon the resistance against the colonizer (it also refers to the Polish cultural formation, based on the tradition of uprisings and resistance against the Russians.   Ćwiczenia pisemne: magia przodków i nowi intelektualiści w powieściach Mii Couto, Lhoussaina Azerguiego i Doroty Masłowskiej Na podstawie powieści Um rio chamado tempo, uma casa chamada terra Mii Couto (2002, Le pain des corbeaux Lhoussaina Azerguiego (2012 oraz Paw królowej Doroty Masłowskiej (2005 dokonano analizy zjawiska wyłonienia się nowej

  2. Structure of Selected Derivates of p-Hydroxy Cynamonic Acid According to 13C CP MAS NMR and DFT Calculation

    International Nuclear Information System (INIS)

    Pisklak, D.M.; Wawer, I.; Tkaczyk, M.

    2005-01-01

    Derivatives of p-hydroxy cynamonic acid are widely occurring in fruits, vegetables, tea and coffee. They exhibit strong antioxidant activity due to the presence of phenolic group. Epidemiological, biological and biochemical data support health beneficial role of this group of compounds and anticarcinogenic, antimutagenic and antiinflamatory effects have been reported. The most common caffeic acid contributes significantly to the total polyphenol intake and has been suggested to play a role in the apparent association between the regular consumption of polyphenol-rich food and beverages, and the prevetion of inflammatory and proliferative diseases. 13 C MAS NMR spectra were recorded on a BRUKER DSX 400 spectrometer at 400,13. Powder samples were spun in a 4 mm rotor at 10 kHz ( 13 C). Signals were assigned:- By comparison with solution spectra; - Using dipolar dephasing and variable contact time experiments; - Confirmed by DFT calculations of shielding constants. The differences in chemical shifts between solution and solid state spectra are due to the formation of intramolecular and intermolecular hydrogen bonds, including C-OH...OC within cyclic dimers. (author)

  3. Quality of spelt pasta enriched with eggs and identification of eggs using 13C MAS NMR spectroscopy

    Directory of Open Access Journals (Sweden)

    Filipović Jelena S.

    2015-01-01

    Full Text Available This paper deals with the characteristics of spelt pasta enriched with eggs. Eggs were added to spelt farina in the quantity of 0, 124 or 248 g/kg (equivalent to 0, 3 or 6 eggs, respectively. Post-hoc Tukey’s HSD test at 95% confidence limit showed significant differences between various samples. Relatively low coefficients of variation have been obtained for each applied assay (1.25-12.42%, which confirmed the high accuracy measurements and statistically significant results. Standard score analysis is applied for accessing the contribution of eggs content to spelt pasta quality. Maximum scores regarding quality (0.89 and chemical characteristics (0.70, have been obtained for 6 eggs spelt pasta formulation. It is also shown that the presence of eggs in pasta can be clearly confirmed by 13C MAS NMR spectroscopy. Simultaneous increase in area of peak positioned at 29.5 and 176 ppm is directly associated with the increase in the content of added eggs in the corresponding samples. Pertinent data point at positive contribution of eggs to the spelt pasta and also that NMR spectrum can be used in the egg quantity control. [Projekat Ministarstva nauke Republike Srbije, br. TRI 46005 i br. TR 31029

  4. Protective effects of vitamin E and Cornus mas fruit extract on methotrexate-induced cytotoxicity in sperms of adult mice

    Directory of Open Access Journals (Sweden)

    Leila Zarei

    2014-03-01

    Full Text Available This study was aimed to assess the protective effects of Cornus mas fruit extract (CMFE and vitamin E (Vit E on sperm quality parameters in the methotrexate (MTX-treated mice. Forty-eight young adult male mice (8-12 weeks were randomly divided into six groups including control and test groups. The control group received normal saline orally , and the test groups were treated MTX (20 mg kg-1, ip, once weekly, MTX + CMFE (250 mg kg-1, MTX + CMFE (500 mg kg-1, MTX + CMFE (1000 mg kg-1, and MTX + Vit E (100 IU kg-1, po for 35 consecutive days. On day 35, after euthanasia the epididymal sperms were isolated. Then the total mean sperm count, sperm viability and motility were determined. The total antioxidant capacity (TAOC of all experimental groups were also evaluated. The MTX-treated animals showed a significant changes in all parameters of sperm quality assessment compared to the control group. Both Vit E and CMFE were able to protect from MTX-induced effects on sperm maturity and DNA damage. Co-administration of MTX and CMFE and/or Vit E resulted in protection from MTX-reduced TAOC. In conclusion, these data suggested that MTX administration could adversely affect the sperm quality. Moreover, the protective effect of Vit E and CMFE on MTX-induced sperm toxicity was also documented.

  5. Lightweight hydrogen-storage material Mg0.65Sc0.35D2 studied with 2H and 2H–{45Sc} MAS NMR exchange spectroscopy

    NARCIS (Netherlands)

    Srinivasan, S.; Magusin, P.C.M.M.

    2011-01-01

    Using double-quantum 2H MAS NMR with 45Sc recoupling and Bloch–Siegert compensated 2H–{45Sc} TRAPDOR we have identified the overlapping NMR signals of deuterium with and without scandium neighbors in Mg0.65Sc0.35D2, a candidate lightweight material for hydrogen storage. At room temperature we also

  6. Protein resonance assignment at MAS frequencies approaching 100 kHz: a quantitative comparison of J-coupling and dipolar-coupling-based transfer methods

    Energy Technology Data Exchange (ETDEWEB)

    Penzel, Susanne; Smith, Albert A.; Agarwal, Vipin; Hunkeler, Andreas [ETH Zürich, Physical Chemistry (Switzerland); Org, Mai-Liis; Samoson, Ago, E-mail: ago.samoson@ttu.ee [Tallinn University of Technology, NMR Instituut, Tartu Teadus, Tehnomeedikum (Estonia); Böckmann, Anja, E-mail: a.bockmann@ibcp.fr [UMR 5086 CNRS/Université de Lyon 1, Institut de Biologie et Chimie des Protéines (France); Ernst, Matthias, E-mail: maer@ethz.ch; Meier, Beat H., E-mail: beme@ethz.ch [ETH Zürich, Physical Chemistry (Switzerland)

    2015-10-15

    We discuss the optimum experimental conditions to obtain assignment spectra for solid proteins at magic-angle spinning (MAS) frequencies around 100 kHz. We present a systematic examination of the MAS dependence of the amide proton T{sub 2}′ times and a site-specific comparison of T{sub 2}′ at 93 kHz versus 60 kHz MAS frequency. A quantitative analysis of transfer efficiencies of building blocks, as they are used for typical 3D experiments, was performed. To do this, we compared dipolar-coupling and J-coupling based transfer steps. The building blocks were then combined into 3D experiments for sequential resonance assignment, where we evaluated signal-to-noise ratio and information content of the different 3D spectra in order to identify the best assignment strategy. Based on this comparison, six experiments were selected to optimally assign the model protein ubiquitin, solely using spectra acquired at 93 kHz MAS. Within 3 days of instrument time, the required spectra were recorded from which the backbone resonances have been assigned to over 96 %.

  7. Personālā datora sistēmas bloka vides snieguma novērtējums un ekodizaina analīze

    OpenAIRE

    Šteina, Māra

    2009-01-01

    Maģistra darba „Personālā datora sistēmas bloka vides snieguma novērtējums un ekodizaina analīze” pamatā ir biroja datora sistēmas bloka ietekmes uz vidi novērtējums visā tā dzīves cikla laikā, izvērtējot arī lietotāju un iesaistīto pušu nozīmi. Darbs sastāv no divām daļām – teorētiskās un praktiskās. Pirmā daļa ir teorētiskajā daļa, kurā autore apskatīja pieejamos literatūras avotus un citu autoru darbus, izvērtējot tēmas aktualitāti, galvenās problēmas un to risinājumus. Otrā daļa ...

  8. KrasMAS: Implementation of a nuclear material computerized accounting system at the Mining and Chemical Combine through the Russian/US cooperative MPC and A program

    International Nuclear Information System (INIS)

    Dorofeev, K.V.; Zhidkov, V.V.; Martinez, B.J.; Perry, R.T.; Scott, S.C.

    1998-01-01

    The Russian/US Mining and Chemical Combine (Gorno-Kimichesky Kombinat, GKhK, also referred to as Krasnoyarsk-26) Material Protection, Control and Accounting (MPC and A) project was initiated in June 1996. A critical component of the ongoing cooperative MPC and A enhancements at the GKhK is the implementation of a computerized nuclear material control and accountability (MC and A) system. This system must meet the MC and A requirements of the GKhK by integrating the information generated by numerous existing and new MC and A components in place at the GKhK (e.g., scales, bar-code equipment, NDA measurement systems). During the first phase of this effort, the GKhK adapted CoreMAS (developed at Los Alamos National Laboratory) for use in the PuO 2 storage facility. This included formulation of Web-based user interfaces for plant personnel, Russification of the existing user interface, and at the functional level, modification of the CoreMAS stored procedures. The modified system is referred to as KrasMAS and builds upon completed work on CoreMAS. Ongoing efforts include adding GKhK specific report forms and expanding the functionality of the system for implementation at the radiochemical processing and reactor plants of the GKhK. Collaborations with other Russian facilities for appropriate parts of these efforts will be pursued

  9. A MAS NMR and DRIFT study of the Ga species in Ga/H-ZSM5 catalysts and their effect on propane ammoxidation

    NARCIS (Netherlands)

    Pal, P.; Quartararo, J.; Hamid, abd S.B.; Derouane, E.G.; Védrine, J.C.; Magusin, P.C.M.M.; Anderson, B.G.

    2005-01-01

    71Ga, 27Al and 29Si MAS-NMR and DRIFT spectroscopies were used to characterize the state of gallium in Ga/H-ZSM5 catalysts tested for their ability to catalyse the ammoxidation of propane. Ga-species were observed in two different possible environments: octahedrally-coordinated gallium in small

  10. Characteristics and Sampling Efficiencies of Two Impactor Bioaerosol Samplers: MAS-100(Registered) (Microbial Air Monitoring System) and Single-Stage Andersen Viable Microbial Samplers

    National Research Council Canada - National Science Library

    Hottell, K

    2004-01-01

    .... A petri dish with agar is used as the impaction surface for these samplers. The MAS-l00 is a single-stage impactor that aspirates air through a 400-hole perforated entry plate onto an agar plate at an airflow rate of 100 L/min...

  11. Hydration kinetics for the alite, belite, and calcium aluminate phase in Portland cements from 27Al and 29Si MAS NMR spectroscopy

    DEFF Research Database (Denmark)

    Skibsted, Jørgen; Jensen, Ole Mejlhede; Jakobsen, Hans Jørgen

    1997-01-01

    29Si magic-angle spinning (MAS) NMR spectroscopy is shown to be a valuable tool for obtaining the quantities of alite and belite in hydrated Portland cements. The hydration (1-180 days) of a white Portland cement with 10 wt.% silica fume added is investigated and the degrees of hydration for alite...

  12. Banku reklāmas stratēģiju un valsts ekonomiskā stāvokļa mijiedarbība

    OpenAIRE

    Vernere, Elīna

    2009-01-01

    Darba tēma ir banku reklāmas stratēģiju un valsts ekonomiskā stāvokļa mijiedarbība. Galvenais pētījuma mērķis bija izprast, kā pašreizējā valsts ekonomiskā situācija izmainījusi sabiedrības vajadzības, pieprasījumu pēc banku pakalpojumiem un līdz ar to arī banku komunikāciju ar saviem klientiem ar vides reklāmas ziņojumu palīdzību. Galvenais pētījuma uzsvars tika likts uz reklāmas ziņojumu emocionālajiem un racionālajiem aspektiem. Papildus veiktajam pētījumam tika apskatīta arī reklāmas teor...

  13. Extratores de cápsulas porosas para o monitoramento da condutividade elétrica e do teor de potássio na solução de um solo

    Directory of Open Access Journals (Sweden)

    Silva Ênio Farias de França e

    2000-01-01

    Full Text Available Este trabalho teve como objetivo avaliar a utilização de extratores de cápsulas porosas no monitoramento da condutividade elétrica e da concentração de potássio na solução do solo, em uma área cultivada com tomates e fertirrigada com três níveis de potássio e frequências de aplicação de um e três dias. Os valores de condutividade elétrica e concentração de potássio encontrados na solução do solo foram corrigidos para a umidade da pasta saturada, em função das diferentes umidades do solo no momento da extração. Os valores de condutividade elétrica obtidos com os extratores de cápsulas porosas e corrigidos para a umidade da pasta subestimaram os medidos no extrato da pasta saturada em torno de 16%. Para as concentrações de potássio, a mesma tendência foi observada, sendo a magnitude cerca de 10%. Os coeficientes de determinação (R² foram superiores a 0,7 para as duas variáveis analisadas. A condutividade elétrica e a concentração de potássio podem ser avaliadas utilizando-se extratores de solução, com precisão razoável.

  14. Mapeamento das preferências de atores estratégicos sobre os critérios de priorização para o monitoramento do horizonte tecnológico em saúde

    Directory of Open Access Journals (Sweden)

    Aline do Nascimento

    Full Text Available Resumo: Entre as etapas básicas de um sistema de monitoramento do horizonte de tecnologias emergentes, estão a filtragem e a priorização dessas tecnologias. Este trabalho tem por objetivo mapear as preferências dos atores estratégicos do Sistema Único de Saúde (SUS quanto aos critérios de filtragem e priorização. Foram selecionados dois critérios de filtragem (horizonte de tempo e inovação e oito critérios de priorização (relevância: epidemiológica, nas políticas de saúde e na prática clínica; impacto: orçamentário no SUS, no custo para o serviço em saúde e na mortalidade; segurança, e aspectos legais, éticos e sociais. A análise de correspondência múltipla foi aplicada para mapear as preferências dos atores nos grupos e entre grupos. Dois grupos foram mais homogêneos entre si e determinantes para a seleção dos critérios de priorização. A influência da formação profissional foi maior que a institucional. A metodologia permitiu a seleção de critérios de forma transparente e a análise das preferências individuais dos participantes.

  15. The cave paintings of the Covatina del Tossalet del Mas de la Rambla», Vilafranca, Castellón | Las pinturas rupestres de la "Covatina del Tossalet del Mas de la Rambla", Villafranca, Castellón | Las pinturas rupestres de la "Covatina del Tossalet del Mas de la Rambla", Villafranca, Castellón

    Directory of Open Access Journals (Sweden)

    Norberto Mesado Olivier

    1989-12-01

    Full Text Available Vilafranca, en el linde N del País, conserva en «La Covatina del Tossalet del Mas de la Rambla», un grupo de unas 24 figuras pertenecientes al tradicionalmennte denominado «Arte Levantino», y que recientemente hemos convenido en llamar «Arte Rupestre del Neolítico Inciso». Destaca por novedosa la caza de una gran ave rapaz (posiblemente un córvido, herida por un proyectil procedente de una honda, arma que lleva un bello cazador en «vuelo», el cual viste sofisticadamente. Otro grupo de figuras humanas singulares aparecen capturando víboras, práctica que llegó tanto en Vilafranca como en el vecino pueblo de Castellfort, a los inicios del siglo XX. Tan singular depredación habrá de relacionarse con la extracción del mortífero veneno de la «vípera Latasti». Su empleo tanto pudo servir para empozoñar las puntas de las saetas de los cazadores prehistóricos de este importantísimo foco del Maestrazgo, o como «fármacos» al estilo de la «Triaca Magna». | Vilafranca, dans la limite Nord du Pays, a dans «La Covatina del Tossalet del Mas de la Rambla», un groupe d'unes 24 figures appartenant au traditionnelment dénomme «Arte Levantino» et que récemment on a accordé dénomé «Art Rupestre du Néolithique Haché». Détache, par nouvelle, la chasse d'un gran oiseau de proie (possiblement un Corvidé, bléssé par un projectile originaire d'une fronde d'un chasseur, lequel est habillé sophistiquément. Un autre groupe de figures humaines se trouve chassant des vipéres, usage qui est arrivé á Vilafranca jusqu'au XXéme siécle. Cette singuliére chasse doit étre lié a l'extraction du poison meutrier de la «Vipera Latasti». Sa finalité aurait bien pu étre empoisonner les pointes dis fleches utilisées par les chasseurs préhistoriques de cette tres importante aire du «Maestrazgo»; ou bien comme «medicament» du méme type que la »Triarca Magna».

  16. Pre- And Post-Enron Learnings On Learning In M&A Environments - A Qualitative Study In Preparation Of A Dissertation On The Influence Of Management Andragogy On Executives Ability To Successfully Manage M&As

    OpenAIRE

    Jacqueline Fendt

    2011-01-01

    In a global economy characterized by convergence and consolidation, by shareholder pressure, by the war for talent, for knowledge and for customer bondage, Merger and Acquisition transactions (M&As) are seen as a fast, efficient and spectacular way to innovate. M&As are therefore a frequently used strategic tool for corporate development. However, as of now, more than 75% of all M&As fail to meet objectives and 50% even destroy shareholder value. M&As often fail due to poor leadership. Th...

  17. Fluxos informacionais para o monitoramento da implementação da Convenção 182 da Organização Internacional do Trabalho sobre as Piores Formas do Trabalho Infantil: análise comparada dos contextos brasileiro e canadense

    OpenAIRE

    Pedro Alves Barbosa Neto

    2013-01-01

    Este trabalho investiga os fluxos informacionais desenvolvidos no âmbito do monitoramento da implementação da Convenção 182, Sobre as Piores Formas do Trabalho Infantil, da Organização Internacional do Trabalho (OIT), comparando os contextos brasileiro e canadense. A Convenção tem como objetivo principal a erradicação do trabalho infantil manifestado em suas piores formas das práticas cotidianas vigentes e as qualifica em um grupo de quatro categorias principais, quais sejam: a) trabalho forç...

  18. Role of Mas Receptor Antagonist A799 in Renal Blood Flow Response to Ang 1-7 after Bradykinin Administration in Ovariectomized Estradiol-Treated Rats

    Directory of Open Access Journals (Sweden)

    Aghdas Dehghani

    2015-01-01

    Full Text Available Background. The accompanied role of Mas receptor (MasR, bradykinin (BK, and female sex hormone on renal blood flow (RBF response to angiotensin 1-7 is not well defined. We investigated the role of MasR antagonist (A779 and BK on RBF response to Ang 1-7 infusion in ovariectomized estradiol-treated rats. Methods. Ovariectomized Wistar rats received estradiol (OVE or vehicle (OV for two weeks. Catheterized animals were subjected to BK and A799 infusion and mean arterial pressure (MAP, RBF, and renal vascular resistance (RVR responses to Ang 1-7 (0, 100, and 300 ng kg−1 min−1 were determined. Results. Percentage change of RBF (%RBF in response to Ang1-7 infusion increased in a dose-dependent manner. In the presence of BK, when MasR was not blocked, %RBF response to Ang 1-7 in OVE group was greater than OV group significantly (P<0.05. Infusion of 300 ng kg−1 min−1 Ang 1-7 increased RBF by 6.9±1.9% in OVE group versus 0.9±1.8% in OV group. However when MasR was blocked, %RBF response to Ang 1-7 in OV group was greater than OVE group insignificantly. Conclusion. Coadministration of BK and A779 compared to BK alone increased RBF response to Ang 1-7 in vehicle treated rats. Such observation was not seen in estradiol treated rats.

  19. A Bio-Economic Case Study of Canadian Honey Bee (Hymenoptera: Apidae) Colonies: Marker-Assisted Selection (MAS) in Queen Breeding Affects Beekeeper Profits

    Science.gov (United States)

    Baylis, Kathy; Hoover, Shelley E.; Currie, Rob W.; Melathopoulos, Andony P.; Pernal, Stephen F.; Foster, Leonard J.; Guarna, M. Marta

    2017-01-01

    Abstract Over the past decade in North America and Europe, winter losses of honey bee (Hymenoptera: Apidae) colonies have increased dramatically. Scientific consensus attributes these losses to multifactorial causes including altered parasite and pathogen profiles, lack of proper nutrition due to agricultural monocultures, exposure to pesticides, management, and weather. One method to reduce colony loss and increase productivity is through selective breeding of queens to produce disease-, pathogen-, and mite-resistant stock. Historically, the only method for identifying desirable traits in honey bees to improve breeding was through observation of bee behavior. A team of Canadian scientists have recently identified markers in bee antennae that correspond to behavioral traits in bees and can be tested for in a laboratory. These scientists have demonstrated that this marker-assisted selection (MAS) can be used to produce hygienic, pathogen-resistant honey bee colonies. Based on this research, we present a beekeeping case study where a beekeeper’s profit function is used to evaluate the economic impact of adopting colonies selected for hygienic behavior using MAS into an apiary. Our results show a net profit gain from an MAS colony of between 2% and 5% when Varroa mites are effectively treated. In the case of ineffective treatment, MAS generates a net profit benefit of between 9% and 96% depending on the Varroa load. When a Varroa mite population has developed some treatment resistance, we show that MAS colonies generate a net profit gain of between 8% and 112% depending on the Varroa load and degree of treatment resistance. PMID:28334400

  20. A Bio-Economic Case Study of Canadian Honey Bee (Hymenoptera: Apidae) Colonies: Marker-Assisted Selection (MAS) in Queen Breeding Affects Beekeeper Profits.

    Science.gov (United States)

    Bixby, Miriam; Baylis, Kathy; Hoover, Shelley E; Currie, Rob W; Melathopoulos, Andony P; Pernal, Stephen F; Foster, Leonard J; Guarna, M Marta

    2017-06-01

    Over the past decade in North America and Europe, winter losses of honey bee (Hymenoptera: Apidae) colonies have increased dramatically. Scientific consensus attributes these losses to multifactorial causes including altered parasite and pathogen profiles, lack of proper nutrition due to agricultural monocultures, exposure to pesticides, management, and weather. One method to reduce colony loss and increase productivity is through selective breeding of queens to produce disease-, pathogen-, and mite-resistant stock. Historically, the only method for identifying desirable traits in honey bees to improve breeding was through observation of bee behavior. A team of Canadian scientists have recently identified markers in bee antennae that correspond to behavioral traits in bees and can be tested for in a laboratory. These scientists have demonstrated that this marker-assisted selection (MAS) can be used to produce hygienic, pathogen-resistant honey bee colonies. Based on this research, we present a beekeeping case study where a beekeeper's profit function is used to evaluate the economic impact of adopting colonies selected for hygienic behavior using MAS into an apiary. Our results show a net profit gain from an MAS colony of between 2% and 5% when Varroa mites are effectively treated. In the case of ineffective treatment, MAS generates a net profit benefit of between 9% and 96% depending on the Varroa load. When a Varroa mite population has developed some treatment resistance, we show that MAS colonies generate a net profit gain of between 8% and 112% depending on the Varroa load and degree of treatment resistance. © The Authors 2017. Published by Oxford University Press on behalf of Entomological Society of America.

  1. The ACE-2/Ang1-7/Mas cascade enhances bone structure and metabolism following angiotensin-II type 1 receptor blockade.

    Science.gov (United States)

    Abuohashish, Hatem M; Ahmed, Mohammed M; Sabry, Dina; Khattab, Mahmoud M; Al-Rejaie, Salim S

    2017-07-15

    The renin angiotensin system (RAS) regulates numerous systemic functions and is expressed locally in skeletal tissues. Angiotensin1-7 (Ang1-7) is a beneficial member of the RAS, and the therapeutic effects of a large number of angiotensin receptors blockers (ARBs) are mediated by an Ang1-7-dependent cascade. This study examines whether the reported osteo-preservative effects of losartan are mediated through the angiotensin converting enzyme2 (ACE-2)/Ang1-7/Mas pathway in ovariectomized (OVX) rats. Sham and OVX animals received losartan (10mg/kg/d p.o.) for 6 weeks. A specific Mas receptor blocker (A-779) was delivered via mini-osmotic pumps during the losartan treatment period. Serum and urine bone metabolism biomarker levels were measured. Bone trabecular and cortical morphometry were quantified in distal femurs, whereas mineral contents were estimated in ashed bones, serum and urine. Finally, the expression of RAS components, the receptor activator of NF-κB ligand (RANKL) and osteoprotegerin (OPG) was determined. Losartan significantly improved the elevated bone metabolism marker levels and altered trabecular and cortical structures in OVX animals, and restored normal urinary and skeletal mineral levels. Mas receptor inhibition significantly abolished all osteo-protective effects of losartan and enhanced the deleterious effects of OVX. Losartan enhanced OVX-induced up-regulation of ACE-1, AngII, angiotensin type 1 (AT 1 ) receptor and RANKL expression, and increased ACE-2, Ang1-7, Mas and OPG expression in OVX animals. However, A-779 significantly eradicated the effects of losartan on RAS components and RANKL/OPG expression. Thus, Ang1-7 are involved in the osteo-preservative effects of losartan via Mas receptor, which may add therapeutic value to this well-known antihypertensive agent. Copyright © 2017 Elsevier B.V. All rights reserved.

  2. Kayseri İlinin Gastronomi Turizmine Yönelik Bir SWOT Analizi Çalışması

    Directory of Open Access Journals (Sweden)

    Doç. Dr. Taşkın DENİZ

    2017-09-01

    Full Text Available Kayseri ili tarihi, kültürel ve doğal güzellikleri ile yüksek bir turizm potansiyeline sahiptir. Binlerce yıllık geçmişe sahip bir yerleşim merkezi olan Kayseri, farklı özelliklere sahip çok sayıda kültüre ev sahipliği yapması sebebi ile adeta bir kültür beşiği durumundadır. Söz konusu kültürel zenginliğin yansıması Kayseri mutfağında ve geleneksel lezzetlerinde de kendisini göstermektedir. Bu araştırmada literatür araştırması kapsamında Kayseri ilinin SWOT analizi ve Kayseri mutfağının gastronomi ürünleri açısından bir değerlendirilmesi yapılmış, Kayseri ilin gastronomi turizmi potansiyeli hakkında görüşler ortaya konmuştur. Elde edilen sonuçlara göre, Kayserinin rakipleri arasında rekabet avantajı kazanmak, marka haline gelmek ve yerel ekonomiye katkıda bulunmak için gastronomi turizminden elde ettiği payı arttırması gerektiği tespit edilmiştir.

  3. Distributed decision-making in electric power system transmission maintenance scheduling using multi-agent systems (MAS)

    Science.gov (United States)

    Zhang, Zhong

    In this work, motivated by the need to coordinate transmission maintenance scheduling among a multiplicity of self-interested entities in restructured power industry, a distributed decision support framework based on multiagent negotiation systems (MANS) is developed. An innovative risk-based transmission maintenance optimization procedure is introduced. Several models for linking condition monitoring information to the equipment's instantaneous failure probability are presented, which enable quantitative evaluation of the effectiveness of maintenance activities in terms of system cumulative risk reduction. Methodologies of statistical processing, equipment deterioration evaluation and time-dependent failure probability calculation are also described. A novel framework capable of facilitating distributed decision-making through multiagent negotiation is developed. A multiagent negotiation model is developed and illustrated that accounts for uncertainty and enables social rationality. Some issues of multiagent negotiation convergence and scalability are discussed. The relationships between agent-based negotiation and auction systems are also identified. A four-step MAS design methodology for constructing multiagent systems for power system applications is presented. A generic multiagent negotiation system, capable of inter-agent communication and distributed decision support through inter-agent negotiations, is implemented. A multiagent system framework for facilitating the automated integration of condition monitoring information and maintenance scheduling for power transformers is developed. Simulations of multiagent negotiation-based maintenance scheduling among several independent utilities are provided. It is shown to be a viable alternative solution paradigm to the traditional centralized optimization approach in today's deregulated environment. This multiagent system framework not only facilitates the decision-making among competing power system entities, but

  4. PENGENDALIAN RISIKO KESEHATAN KARENA PAJANAN MERKURI PADA KEGIATAN TAMBANG EMAS TRADISIONAL DI KABUPATEN GUNUNG MAS, KALIMANTAN TENGAH

    Directory of Open Access Journals (Sweden)

    Inswiasri Inswiasri

    2012-11-01

    Full Text Available Increasing informal gold mining activities can cause environmental pollution and affected the public health. So that, the study was needed in order to assess health risk of population working in or living near informal gold mining and processing in Gunung Mas District, Central Kalimantan. Subjects in cross sectional study were 112 informal miners and 112 living near informal gold mining and processing. We measured content of mercury in ambient, water and fish; and interviewed the subjects. Subjects completed the questionnaire. Estimation of health risk assessment and system dynamics analysis to handle the health risk were conducted too. Detection of mercury using Atomic Absorption Spectrophotometer (AAS and cold vapour method was conducted at Ecology Health Research Center Laboratory. The result showed that; the mean concentration of airborne mercury was 0.072 + 0,0198 mg/m3 in mining area and 0.0369 +0,0092 mg/m3 in out side of mining area respectively. The highest mean level of mercury in fish 0.3167 ppm from market in Kurun District. Intake of inhalation mercury 0.02285 mg/kg, day for miners and 0.01406 mg/kg, day for non-miner living near the informal mining and processing. Mean of RQ inhalation 76.160 for miners and 46.876 for non-miners living near the informal mining and processing. RQ inhalation tend to increase time to time. The miners have to handle mercury emission using retort. Keywords: Risk assessment, informal gold miner, air pollution, mercury

  5. Acceleration of natural-abundance solid-state MAS NMR measurements on bone by paramagnetic relaxation from gadolinium-DTPA

    Science.gov (United States)

    Mroue, Kamal H.; Zhang, Rongchun; Zhu, Peizhi; McNerny, Erin; Kohn, David H.; Morris, Michael D.; Ramamoorthy, Ayyalusamy

    2014-07-01

    Reducing the data collection time without affecting the signal intensity and spectral resolution is one of the major challenges for the widespread application of multidimensional nuclear magnetic resonance (NMR) spectroscopy, especially in experiments conducted on complex heterogeneous biological systems such as bone. In most of these experiments, the NMR data collection time is ultimately governed by the proton spin-lattice relaxation times (T1). For over two decades, gadolinium(III)-DTPA (Gd-DTPA, DTPA = Diethylene triamine pentaacetic acid) has been one of the most widely used contrast-enhancement agents in magnetic resonance imaging (MRI). In this study, we demonstrate that Gd-DTPA can also be effectively used to enhance the longitudinal relaxation rates of protons in solid-state NMR experiments conducted on bone without significant line-broadening and chemical-shift-perturbation side effects. Using bovine cortical bone samples incubated in different concentrations of Gd-DTPA complex, the 1H T1 values were calculated from data collected by 1H spin-inversion recovery method detected in natural-abundance 13C cross-polarization magic angle spinning (CPMAS) NMR experiments. Our results reveal that the 1H T1 values can be successfully reduced by a factor of 3.5 using as low as 10 mM Gd-DTPA without reducing the spectral resolution and thus enabling faster data acquisition of the 13C CPMAS spectra. These results obtained from 13C-detected CPMAS experiments were further confirmed using 1H-detected ultrafast MAS experiments on Gd-DTPA doped bone samples. This approach considerably improves the signal-to-noise ratio per unit time of NMR experiments applied to bone samples by reducing the experimental time required to acquire the same number of scans.

  6. Validation of a low dose simulation technique for computed tomography images.

    Directory of Open Access Journals (Sweden)

    Daniela Muenzel

    Full Text Available PURPOSE: Evaluation of a new software tool for generation of simulated low-dose computed tomography (CT images from an original higher dose scan. MATERIALS AND METHODS: Original CT scan data (100 mAs, 80 mAs, 60 mAs, 40 mAs, 20 mAs, 10 mAs; 100 kV of a swine were acquired (approved by the regional governmental commission for animal protection. Simulations of CT acquisition with a lower dose (simulated 10-80 mAs were calculated using a low-dose simulation algorithm. The simulations were compared to the originals of the same dose level with regard to density values and image noise. Four radiologists assessed the realistic visual appearance of the simulated images. RESULTS: Image characteristics of simulated low dose scans were similar to the originals. Mean overall discrepancy of image noise and CT values was -1.2% (range -9% to 3.2% and -0.2% (range -8.2% to 3.2%, respectively, p>0.05. Confidence intervals of discrepancies ranged between 0.9-10.2 HU (noise and 1.9-13.4 HU (CT values, without significant differences (p>0.05. Subjective observer evaluation of image appearance showed no visually detectable difference. CONCLUSION: Simulated low dose images showed excellent agreement with the originals concerning image noise, CT density values, and subjective assessment of the visual appearance of the simulated images. An authentic low-dose simulation opens up opportunity with regard to staff education, protocol optimization and introduction of new techniques.

  7. Dismantling techniques

    International Nuclear Information System (INIS)

    Wiese, E.

    1998-01-01

    Most of the dismantling techniques used in a Decontamination and Dismantlement (D and D) project are taken from conventional demolition practices. Some modifications to the techniques are made to limit exposure to the workers or to lessen the spread of contamination to the work area. When working on a D and D project, it is best to keep the dismantling techniques and tools as simple as possible. The workers will be more efficient and safer using techniques that are familiar to them. Prior experience with the technique or use of mock-ups is the best way to keep workers safe and to keep the project on schedule

  8. Dismantling techniques

    Energy Technology Data Exchange (ETDEWEB)

    Wiese, E.

    1998-03-13

    Most of the dismantling techniques used in a Decontamination and Dismantlement (D and D) project are taken from conventional demolition practices. Some modifications to the techniques are made to limit exposure to the workers or to lessen the spread of contamination to the work area. When working on a D and D project, it is best to keep the dismantling techniques and tools as simple as possible. The workers will be more efficient and safer using techniques that are familiar to them. Prior experience with the technique or use of mock-ups is the best way to keep workers safe and to keep the project on schedule.

  9. Utilização da TDR para monitoramento da solução de nitrato de potássio em Latossolo Vermelho-Amarelo Use of tdr for monitoring the potassium nitrate solution in dystrophic Red-Yellow Latossol

    Directory of Open Access Journals (Sweden)

    Leonardo do N. Lopes

    2010-10-01

    Full Text Available O conhecimento da distribuição e armazenamento da solução no solo é de grande importância para a agricultura, pois a interação entre os nutrientes e a água é um dos fatores que influenciam diretamente no rendimento das culturas. Das várias técnicas utilizadas para o monitoramento da solução no solo, a reflectometria no domínio do tempo (TDR vem sendo bastante difundida entre os pesquisadores por apresentar inúmeras vantagens, dentre as quais a mensuração em tempo real e a possibilidade de leituras automatizadas. O principal objetivo desta pesquisa foi avaliar a distribuição da solução de KNO3 no perfil de um Latossolo Vermelho-Amarelo. Sondas de Reflectometria no Domínio do Tempo (TDR foram utilizadas para monitorar a distribuição de solução no solo aplicada por gotejadores de fluxo constante nas vazões de 2; 4 e 8 L h-1. Considerando-se os resultados de diferentes perfis, observou-se maior armazenamento da solução próxima ao gotejador, diminuindo progressivamente para frente de molhamento. Pouco mais da metade da solução aplicada (65% foi armazenada na primeira camada (0-0,10 m para todos os ensaios, e 22% foi armazenada na próxima camada (0,10-0,20 m. Comparando-se diferentes taxas de aplicação, observou-se maior armazenamento de água para o gotejador de 4 L h-1, com 60; 72 e 63% de solução de KNO3 aplicada acumulada na primeira camada (0-0,10 m para gotejadores de 2; 4 e 8 L h-1, respectivamente. Os resultados sugerem que, com base no volume e frequência utilizada neste experimento, seria vantajoso aplicar pequenas quantidades de água em intervalos mais frequentes para reduzir perdas por percolação.Knowledge of water distribution in soil is of great importance to agriculture, since water is one of the factors that most influence the yield of crops. There are many techniques used for monitoring of soil water content, the Time Domain Reflectometry (TDR has been widespread among researchers to present

  10. Os biocombustíveis no Brasil: panorama atual, emissões gasosas e os métodos analíticos de monitoramento da qualidade do ar referente a gases de natureza orgânica / Biofuels in Brazil: the current scene, gaseous emissions and analytical methods on air quality monitoring concerned to organic gases

    Directory of Open Access Journals (Sweden)

    Waldir Nagel Schirmer

    2012-04-01

    Full Text Available ResumoA diminuição das reservas de petróleo, aliada às oscilações de seu preço e à pressão pela preservação do meio ambiente, evidenciam a necessidade de se diversificar a matriz energética mundial, por meio do uso de combustíveis renováveis. Grande parte da literatura referente a esse tema reporta, de fato, a redução significativa da grande maioria dos principais poluentes atmosféricos regulamentados. O presente trabalho aborda uma revisão do panorama dos biocombustíveis no Brasil (com ênfase no biodiesel, de modo sucinto, enfatizando os ganhos ambientais ao se substituir a matriz energética atual (predominantemente de origem fóssil, por combustíveis renováveis de origem vegetal. Traz ainda as principais técnicas de monitoramento no que se refere à amostragem e análise de gases orgânicos (especialmente compostos orgânicos voláteis, uma vez que compostos dessa natureza figuram entre os maiores poluentes do ar. Semelhantemente ao que se observa em âmbito internacional, a expectativa é de que, também no Brasil, ocorra um aumento no controle de fontes de poluentes dessa natureza, como a adoção de padrões de emissão mais rígidos (específicos para fontes de diferentes naturezas e a inclusão de um programa de medida e controle/abatimento desses poluentes.AbstractThe decrease of petroleum reserves, coupled with its price fluctuations and pressure for the preservation of the environment, highlight the need to diversify the global energy matrix, by means of the use of renewable fuels. The literature on this subject reports a significant reduction of the vast majority of major air pollutants regulated. This paper is a review of the scene of biofuels in Brazil (focusing on biodiesel, with emphasis in the environmental benefits by replacing the current energy matrix (mainly fossil fuels by renewable sources with vegetable origin. It also brings the main techniques for monitoring in relation to sampling and analysis of

  11. Un lote de armamento ibérico procedente de la necrópolis del Mas de Barberán (Nogueruelas, Teruel

    Directory of Open Access Journals (Sweden)

    Izquierdo Peraile, Isabel

    1999-12-01

    Full Text Available In this paper we publish an Ibenan set of weapons -swords, lances and dagger essentially-, coming from the cemetery of the settlement so-called Mas de Barberán (Nogueruelas, Teruel. An anthropomorphic stele with an inscription recently studied is associated to the same site. This stele represents an armed with disk-cuirass masculine personage.

    En este trabajo presentamos un lote inédito de armamento ibérico espadas, lanzas y puñal esencialmente procedente de la necrópolis correspondiente al poblado del Mas de Barberán (Nogueruelas, Teruel. Al mismo yacimiento se asocia la estela antropomorfa con inscripción que representa un personaje masculino armado con disco-coraza, recientemente estudiada.

  12. “Estado Nación laico y secularización masónica en México”

    Directory of Open Access Journals (Sweden)

    Carlos Francisco Martínez Moreno

    2011-01-01

    Full Text Available Este artículo busca mostrar cómo y porqué los masones practicantes del Rito Nacional Mexicano en el siglo XIX secularizaron su tradición para responder a sus compromisos sociales, patrióticos, liberales y democráticos. Además, muestra cómo ellos sustituyeron La Biblia por la Constitución Política de los Estados Unidos Mexicanos en sus juramentos masónicos, en un contexto social en el que jurarla se consideraba un anatema por el Papa Pío IX y el clero católico, y en un contexto masónico adverso en el que sustituir el Libro de la Ley y participar en la política como masones era contravenir la tradición especulativa londinense.

  13. Avaliação da comunidade de macroinvertebrados aquáticos como ferramenta para o monitoramento de um reservatório na bacia do rio Pitangui, Paraná, Brasil

    Directory of Open Access Journals (Sweden)

    Ivana F Barbola

    2011-06-01

    Full Text Available Os macroinvertebrados bentônicos e nectônicos representam elementos importantes na estrutura e funcionamento dos ecossistemas aquáticos e sua distribuição é influenciada pela natureza química do substrato, composição da vegetação e profundidade da lâmina d'água. O conhecimento desta fauna contribui para a avaliação da qualidade da água e a elaboração de ações visando à conservação da biodiversidade. No presente estudo foram avaliadas diferentes medidas bióticas da comunidade de invertebrados da represa de Alagados, importante manancial da cidade de Ponta Grossa, no Paraná. Em cinco diferentes pontos de amostragem, foram coletados 18.473 exemplares de macroinvertebrados aquáticos ou semi-aquáticos, pertencentes a 46 táxons dos filos Annelida (Hirudinea e Oligochaeta, Mollusca (Gastropoda, Platyhelminthes (Turbellaria, Nematoda e Arthropoda (Arachnida, Crustacea e Insecta. Esta comunidade foi constituída predominantemente por organismos predadores (45,7% dos táxons amostrados, seguidos de coletores e/ou filtradores (23,9%; raspadores (15,2%, fragmentadores (13% e detritívoros (2,2%. De modo geral, os índices de diversidade (H' e equitabilidade (J foram significativamente baixos para os cinco locais investigados, com H' variando de 0,3301 a 1,0396. Quanto à tolerância dos organismos à poluição orgânica, alguns táxons mais sensíveis foram muito raros (Plecoptera ou em baixa frequência (Trichoptera e Ephemeroptera. Entre os grupos mais resistentes a ambientes poluídos estão os Chironomidae e os Hirudinea, ambos bastante comuns nas amostras de Alagados. Este estudo reforça a importância da análise de bioindicadores na avaliação da qualidade de água para consumo humano e também para a conservação de ecossistemas, considerando que um programa de monitoramento ambiental deve integrar medidas físicas, químicas e biológicas.

  14. The angiotensin-(1-7/Mas axis counteracts angiotensin II-dependent and –independent pro-inflammatory signaling in human vascular smooth muscle cells

    Directory of Open Access Journals (Sweden)

    Laura A Villalobos

    2016-12-01

    Full Text Available Background and aims: Targeting inflammation is nowadays considered as a challenging pharmacological strategy to prevent or delay the development of vascular diseases. Angiotensin-(1-7 is a member of the renin-angiotensin system (RAS that binds Mas receptors and has gained growing attention in the last years as a regulator of vascular homeostasis. Here, we explored the capacity of Ang-(1-7 to counteract human aortic smooth muscle cell (HASMC inflammation triggered by RAS-dependent and –independent stimuli, such as Ang II or interleukin (IL-1.Methods and Results: In cultured HASMC, the expression of iNOS and the release of nitric oxide were stimulated by both Ang II and IL-1, as determined by Western blot and indirect immunofluorescence or the Griess method, respectively. iNOS induction was inhibited by Ang-(1-7 in a concentration-dependent manner. This effect was equally blocked by two different Mas receptor antagonists, A779 and D-Pro7-Ang-(1-7, suggesting the participation of a unique Mas receptor subtype. Using pharmacological inhibitors, the induction of iNOS was proven to rely on the consecutive upstream activation of NADPH oxidase and NF-B. Indeed, Ang-(1-7 markedly inhibited the activation of the NADPH oxidase and subsequently of NF-B, as determined by lucigenin-derived chemiluminiscence and electromobility shift assay, respectively.Conclusion: Ang-(1-7 can act as a counter-regulator of the inflammation of vascular smooth muscle cells triggered by Ang II, but also by other stimuli beyond the RAS. Activating or mimicking the Ang-(1-7/Mas axis may represent a pharmacological opportunity to attenuate the pro-inflammatory environment that promotes and sustains the development of vascular diseases.

  15. Optimal degree of protonation for {sup 1}H detection of aliphatic sites in randomly deuterated proteins as a function of the MAS frequency

    Energy Technology Data Exchange (ETDEWEB)

    Asami, Sam [Helmholtz-Zentrum Muenchen (HMGU), Deutsches Forschungszentrum fuer Gesundheit und Umwelt (HMGU) (Germany); Szekely, Kathrin; Schanda, Paul; Meier, Beat H. [Eidgenoessische Technische Hochschule Zuerich (ETH Zuerich) (Switzerland); Reif, Bernd, E-mail: reif@tum.de [Helmholtz-Zentrum Muenchen (HMGU), Deutsches Forschungszentrum fuer Gesundheit und Umwelt (HMGU) (Germany)

    2012-10-15

    The {sup 1}H dipolar network, which is the major obstacle for applying proton detection in the solid-state, can be reduced by deuteration, employing the RAP (Reduced Adjoining Protonation) labeling scheme, which yields random protonation at non-exchangeable sites. We present here a systematic study on the optimal degree of random sidechain protonation in RAP samples as a function of the MAS (magic angle spinning) frequency. In particular, we compare {sup 1}H sensitivity and linewidth of a microcrystalline protein, the SH3 domain of chicken {alpha}-spectrin, for samples, prepared with 5-25 % H{sub 2}O in the E. coli growth medium, in the MAS frequency range of 20-60 kHz. At an external field of 19.96 T (850 MHz), we find that using a proton concentration between 15 and 25 % in the M9 medium yields the best compromise in terms of sensitivity and resolution, with an achievable average {sup 1}H linewidth on the order of 40-50 Hz. Comparing sensitivities at a MAS frequency of 60 versus 20 kHz, a gain in sensitivity by a factor of 4-4.5 is observed in INEPT-based {sup 1}H detected 1D {sup 1}H,{sup 13}C correlation experiments. In total, we find that spectra recorded with a 1.3 mm rotor at 60 kHz have almost the same sensitivity as spectra recorded with a fully packed 3.2 mm rotor at 20 kHz, even though {approx}20 Multiplication-Sign less material is employed. The improved sensitivity is attributed to {sup 1}H line narrowing due to fast MAS and to the increased efficiency of the 1.3 mm coil.

  16. Translation Techniques

    OpenAIRE

    Marcia Pinheiro

    2015-01-01

    In this paper, we discuss three translation techniques: literal, cultural, and artistic. Literal translation is a well-known technique, which means that it is quite easy to find sources on the topic. Cultural and artistic translation may be new terms. Whilst cultural translation focuses on matching contexts, artistic translation focuses on matching reactions. Because literal translation matches only words, it is not hard to find situations in which we should not use this technique.  Because a...

  17. Anomalous H/D isotope effect on 35Cl NQR frequencies and H/D isotope effect on 1H MAS NMR spectra in pyrrolidinium p-chlorobenzoate

    International Nuclear Information System (INIS)

    Nakano, Ryo; Honda, Hisashi; Nakata, Eiichi; Takamizawa, Satoshi; Noro, Sumiko; Kimura, Taiki; Kyo, Shin-shin; Ishimaru, Shin'ichi; Miyake, Ryosuke

    2010-01-01

    An anomalous isotope effect was observed in the 35 Cl NQR frequency of pyrrolidinium p-chlorobenzoate (C 4 H 8 NH 2 + ·ClC 6 H 4 COO - ) by deuterium substitution of hydrogen atoms which form two kinds of N-H...O type hydrogen bonds. Large negative frequency shifts of the 35 Cl resonance lines, reaching 309 kHz at 77 K and 267 kHz at 293 K, were obtained upon deuteration, although the Cl atom in the molecule formed no hydrogen bonds in the crystal. 1 H MAS NMR lines showed significant changes by the deuterium substitution, while in contrast, small shifts of 13 C CP/MAS NMR signals were obtained. Our measurements of 1 H NMR spin-lattice relaxation times (T 1 ) suggested that the H/D isotope shifts detected from the 35 Cl NQR frequencies and 1 H NMR spectra are due to structural changes rather than molecular dynamics. Single-crystal X-ray diffraction measurements showed two remarkable H/D isotope differences in the molecular arrangements, (1) the N-H length along the crystallographic a axis became 1 pm shorter, and (2) the dihedral angle between benzene and the pyrrolidine ring changed by 1.1(2)deg upon deuteration. Using density functional theory estimations, the anomalous 35 Cl NQR frequency shifts and 1 H MAS NMR line-shape changes could be explained by the dihedral angle change rather than the N-H length difference. (author)

  18. Feminism and Postmodernism in Paloma Díaz-Mas's "The World According to Valdés" and "In Search of a Portrait"

    Directory of Open Access Journals (Sweden)

    Fuencisla Zomeño

    2002-06-01

    Full Text Available This paper analyzes the influence of postmodernism in Paloma Díaz-Mas's feminist approach through two short stories, "The World According to Valdés," and "In Search of a Portrait." The political situation after Franco's death embraced democracy which allowed writers to pay more attention to intellectual concerns. Women writers steered the radical positions of the 1970s toward a more philosophical and intellectual analysis of reality and artistic expression during the eighties. In these two short stories, Díaz-Mas addresses women's issues by questioning the scope of modernist and humanist views. She criticizes the modernist concept of unity (text/identity pointing out the discrimination that this unity creates in art, through the distinction between high art/mass culture; and in the individual, through the distinction between feminine/masculine and high/low. Even though Díaz-Mas's main characters in the two stories are women, she does not solely focus on defending them, but she contrasts present and past to parody the causes which produce discrimination in the social and artistic processes.

  19. UJI APLIKASI VAKSIN HYDROVAC UNTUK PENCEGAHAN PENYAKIT MERAH PADA IKAN MAS (Cyprinus carpio DAN GURAME (Osphronemus gouramy DI BALAI BENIH IKAN PANDAK KABUPATEN BANYUMAS

    Directory of Open Access Journals (Sweden)

    Indrawati Indrawati

    2009-06-01

    Full Text Available Uji aplikasi vaksin ini bertujuan untuk mengetahui pengaruh pemberian vaksin hydrovac terhadap perkembangan kesehatan ikan mas dan gurami, serta mendapatkan informasi tentang cara pengendalian, melalui tindakan pencegahan ikan air tawar yang terserang wabah penyakit Aeromonas hydrophila. Sebanyak 39 ekor ikan mas (Cyprinus carpio dengan bobot rata-rata 1 kg dan panjang rata-rata 30 cm dan108 ekor ikan gurami (Osphronemus gouramy L. dengan bobot rata-rata 250 g dan panjang rata-rata 10 cm yang berasal dari Balai Benih Ikan (BBI Pandak Kabupaten Banyumas, digunakan sebagai ikan uji. Vaksin yang digunakan adalah “vaksin hydrovac” yang diproduksi oleh Laboratorium Patologi Ikan. Balai Riset Perikanan Budidaya Air Tawar, Bogor. Vaksin diaplikasikan dengan cara dicampur pelet dengan dosis 2--3 mL per kilogram bobot badan ikan yang diberikan selama 5--7 hari berturut-turut dan setelah satu bulan kemudian dilakukan vaksinasi ulangan (booster terhadap ikan yang telah divaksin dengan cara yang sama. Hasil uji menunjukkan bahwa ikan baik ikan mas maupun gurame yang divaksin menunjukkan angka sintasan yang cukup tinggi apabila dibandingkan dengan ikan yang tidak divaksin. Mortalitas ikan uji yang tidak divaksin terjadi mulai minggu ke-5 dan ke-6.

  20. Comparison of adaptive statistical iterative and filtered back projection reconstruction techniques in brain CT

    International Nuclear Information System (INIS)

    Ren, Qingguo; Dewan, Sheilesh Kumar; Li, Ming; Li, Jianying; Mao, Dingbiao; Wang, Zhenglei; Hua, Yanqing

    2012-01-01

    Purpose: To compare image quality and visualization of normal structures and lesions in brain computed tomography (CT) with adaptive statistical iterative reconstruction (ASIR) and filtered back projection (FBP) reconstruction techniques in different X-ray tube current–time products. Materials and methods: In this IRB-approved prospective study, forty patients (nineteen men, twenty-one women; mean age 69.5 ± 11.2 years) received brain scan at different tube current–time products (300 and 200 mAs) in 64-section multi-detector CT (GE, Discovery CT750 HD). Images were reconstructed with FBP and four levels of ASIR-FBP blending. Two radiologists (please note that our hospital is renowned for its geriatric medicine department, and these two radiologists are more experienced in chronic cerebral vascular disease than in neoplastic disease, so this research did not contain cerebral tumors but as a discussion) assessed all the reconstructed images for visibility of normal structures, lesion conspicuity, image contrast and diagnostic confidence in a blinded and randomized manner. Volume CT dose index (CTDI vol ) and dose-length product (DLP) were recorded. All the data were analyzed by using SPSS 13.0 statistical analysis software. Results: There was no statistically significant difference between the image qualities at 200 mAs with 50% ASIR blending technique and 300 mAs with FBP technique (p > .05). While between the image qualities at 200 mAs with FBP and 300 mAs with FBP technique a statistically significant difference (p < .05) was found. Conclusion: ASIR provided same image quality and diagnostic ability in brain imaging with greater than 30% dose reduction compared with FBP reconstruction technique

  1. Comparison of adaptive statistical iterative and filtered back projection reconstruction techniques in brain CT

    Energy Technology Data Exchange (ETDEWEB)

    Ren, Qingguo, E-mail: renqg83@163.com [Department of Radiology, Hua Dong Hospital of Fudan University, Shanghai 200040 (China); Dewan, Sheilesh Kumar, E-mail: sheilesh_d1@hotmail.com [Department of Geriatrics, Hua Dong Hospital of Fudan University, Shanghai 200040 (China); Li, Ming, E-mail: minli77@163.com [Department of Radiology, Hua Dong Hospital of Fudan University, Shanghai 200040 (China); Li, Jianying, E-mail: Jianying.Li@med.ge.com [CT Imaging Research Center, GE Healthcare China, Beijing (China); Mao, Dingbiao, E-mail: maodingbiao74@163.com [Department of Radiology, Hua Dong Hospital of Fudan University, Shanghai 200040 (China); Wang, Zhenglei, E-mail: Williswang_doc@yahoo.com.cn [Department of Radiology, Shanghai Electricity Hospital, Shanghai 200050 (China); Hua, Yanqing, E-mail: cjr.huayanqing@vip.163.com [Department of Radiology, Hua Dong Hospital of Fudan University, Shanghai 200040 (China)

    2012-10-15

    Purpose: To compare image quality and visualization of normal structures and lesions in brain computed tomography (CT) with adaptive statistical iterative reconstruction (ASIR) and filtered back projection (FBP) reconstruction techniques in different X-ray tube current–time products. Materials and methods: In this IRB-approved prospective study, forty patients (nineteen men, twenty-one women; mean age 69.5 ± 11.2 years) received brain scan at different tube current–time products (300 and 200 mAs) in 64-section multi-detector CT (GE, Discovery CT750 HD). Images were reconstructed with FBP and four levels of ASIR-FBP blending. Two radiologists (please note that our hospital is renowned for its geriatric medicine department, and these two radiologists are more experienced in chronic cerebral vascular disease than in neoplastic disease, so this research did not contain cerebral tumors but as a discussion) assessed all the reconstructed images for visibility of normal structures, lesion conspicuity, image contrast and diagnostic confidence in a blinded and randomized manner. Volume CT dose index (CTDI{sub vol}) and dose-length product (DLP) were recorded. All the data were analyzed by using SPSS 13.0 statistical analysis software. Results: There was no statistically significant difference between the image qualities at 200 mAs with 50% ASIR blending technique and 300 mAs with FBP technique (p > .05). While between the image qualities at 200 mAs with FBP and 300 mAs with FBP technique a statistically significant difference (p < .05) was found. Conclusion: ASIR provided same image quality and diagnostic ability in brain imaging with greater than 30% dose reduction compared with FBP reconstruction technique.

  2. Detecção e monitoramento da resistência do tripes Frankliniella occidentalis ao inseticida espinosade Detection and monitoring of resistance to the insecticide spinosad in the thrips Frankliniella occidentalis

    Directory of Open Access Journals (Sweden)

    Débora Soller Rais

    2013-01-01

    Full Text Available O tripes Frankliniella occidentalis (Pergande (Thysanoptera: Thripidae é uma das pragas mais importantes em cultivos protegidos, principalmente de plantas ornamentais e hortícolas. Entre os problemas enfrentados pelos agricultores estão a dificuldade de seu controle com o uso de inseticidas devido à sua preferência pelas partes internas das flores e a evolução de resistência aos agroquímicos. O objetivo da pesquisa foi caracterizar a resistência de F. occidentalis a espinosade e avaliar a frequência de insetos resistentes ao inseticida, em áreas comerciais de crisântemo de diversos municípios do Estado de São Paulo. Seleções para resistência a espinosade foram realizadas em laboratório, utilizando-se uma população de F. occidentalis, coletada em 2007 de um cultivo comercial de crisântemo em Campinas (SP. No decorrer de sete seleções para resistência, a CL50 de espinosade passou de 8,41 mg i.a. L-1 para 1111 mg i.a. L-1. Comparando-se a linhagem resistente (R (selecionada e a suscetível (S, a razão de resistência (CL50 R/CL50 S atingiu valores de ≈280 vezes. Estabeleceu-se uma concentração discriminatória de 98 mg i.a. L-1 para o monitoramento da resistência de F. occidentalis a espinosade. O monitoramento foi realizado coletando-se 19 populações do tripes em áreas comerciais de crisântemo no Estado de São Paulo. Os bioensaios foram realizados com ninfas de segundo ínstar de F. occidentalis, colocadas em arenas de folha de feijão. As aplicações de espinosade, na sua concentração discriminatória, foram realizadas sobre as ninfas em torre de Potter. Os resultados indicaram alta variabilidade entre as populações com relação à suscetibilidade a espinosade. Foram observadas populações com até 40,7% de insetos resistentes. Este é o primeiro relato de resistência de F. occidentalis a espinosade no Brasil.The thrips Frankliniella occidentalis (Pergande (Thysanoptera: Thripidae is one of the major

  3. Detecção e monitoramento da resistência do tripes Frankliniella occidentalis ao inseticida espinosade Detection and monitoring of resistance to the insecticide spinosad in the thrips Frankliniella occidentalis

    Directory of Open Access Journals (Sweden)

    Débora Soller Rais

    2013-03-01

    Full Text Available O tripes Frankliniella occidentalis (Pergande (Thysanoptera: Thripidae é uma das pragas mais importantes em cultivos protegidos, principalmente de plantas ornamentais e hortícolas. Entre os problemas enfrentados pelos agricultores estão a dificuldade de seu controle com o uso de inseticidas devido à sua preferência pelas partes internas das flores e a evolução de resistência aos agroquímicos. O objetivo da pesquisa foi caracterizar a resistência de F. occidentalis a espinosade e avaliar a frequência de insetos resistentes ao inseticida, em áreas comerciais de crisântemo de diversos municípios do Estado de São Paulo. Seleções para resistência a espinosade foram realizadas em laboratório, utilizando-se uma população de F. occidentalis, coletada em 2007 de um cultivo comercial de crisântemo em Campinas (SP. No decorrer de sete seleções para resistência, a CL50 de espinosade passou de 8,41 mg i.a. L-1 para 1111 mg i.a. L-1. Comparando-se a linhagem resistente (R (selecionada e a suscetível (S, a razão de resistência (CL50 R/CL50 S atingiu valores de ≈280 vezes. Estabeleceu-se uma concentração discriminatória de 98 mg i.a. L-1 para o monitoramento da resistência de F. occidentalis a espinosade. O monitoramento foi realizado coletando-se 19 populações do tripes em áreas comerciais de crisântemo no Estado de São Paulo. Os bioensaios foram realizados com ninfas de segundo ínstar de F. occidentalis, colocadas em arenas de folha de feijão. As aplicações de espinosade, na sua concentração discriminatória, foram realizadas sobre as ninfas em torre de Potter. Os resultados indicaram alta variabilidade entre as populações com relação à suscetibilidade a espinosade. Foram observadas populações com até 40,7% de insetos resistentes. Este é o primeiro relato de resistência de F. occidentalis a espinosade no Brasil.The thrips Frankliniella occidentalis (Pergande (Thysanoptera: Thripidae is one of the major

  4. Diagnostic techniques

    International Nuclear Information System (INIS)

    Berquist, T.H.; Bender, C.E.; James, E.M.; Brown, M.L.; McLeod, R.A.; Broderick, D.F.; Welch, T.J.

    1989-01-01

    Proper application of imaging procedures is essential to obtain needed information for diagnosis and therapy planning in patients with suspected foot and/or ankle pathology. This paper provides basic background data for the numerous imaging techniques

  5. MONITORAMENTO DA MICROBIOTA DE IOGURTES COMERCIAIS

    Directory of Open Access Journals (Sweden)

    Simone de Souza Fernandes

    2011-10-01

    Full Text Available Iogurte é um leite fermentado resultante de interação microbiana mutualista entre as bactérias Streptococcus thermophilus e Lactobacillus delbrueckii subsp. bulgaricus. Para que a qualidade do iogurte seja garantida, o número de estreptococos deve ser igual ao de lactobacilos, portanto uma proporção de 1:1. Durante o armazenamento dos iogurtes expostos para venda podem ocorrer pós-acidificação e modificação nesta proporção. Os objetivos desta pesquisa foram avaliar iogurtes de quatro diferentes fabricantes denominados A, B, C e D quanto ao numero e equilíbrio entre cocos e bacilos durante o armazenamento, e sua relação com acidez e pH. Para tanto, foram avaliados iogurtes com até 20 dias de fabricação (faixa A e mais de 20 dias (faixa B. Foi verificado um desequilíbrio no número de lactobacilos que foi inferior ao de estreptococos e, considerado inadequado, em duas das quatro marcas comerciais. Nos iogurtes da marca A houve redução significativa no número de lactobacilos da faixa A para faixa B levando a um aumento na proporção de cocos relativa ao de bacilos. Não foi observada diferença significativa de acidez e pH relacionados ao tempo de vida de prateleira nas quatro marcas de iogurte. A acidez dos iogurtes do fabricante D mostrou-se significativamente mais elevada (P<0,05 que a dos demais, embora não tenha resultado em maior redução de pH. Todas as amostras analisadas atenderam a legislação vigente no que se refere ao mínimo exigido de bactérias láticas totais.

  6. MONITORAMENTO PARA PREVER EPIDEMIAS UTILIZANDO REDES SOCIAIS

    Directory of Open Access Journals (Sweden)

    Bruno Neves Santos

    2014-06-01

    Full Text Available Actually social networks have been attracting millions of users, because they are favorable environments for studying many computing themes (distributed systems, traffic patterns over the internet, data mining, multimedia systems, among others, directed to different areas (epidemiology, politics, sports, marketing. The concept created over the social networks became a key theme for researches related to processing and organization of huge amount of data. On this context, this research proposes an application that is able to collect data shared over the social network named Twitter, process this data and generate information in order to obtain results that permit identify probable concentrations of a certain disease on a determined place and period, assisting the epidemiology.

  7. Decomposition techniques

    Science.gov (United States)

    Chao, T.T.; Sanzolone, R.F.

    1992-01-01

    Sample decomposition is a fundamental and integral step in the procedure of geochemical analysis. It is often the limiting factor to sample throughput, especially with the recent application of the fast and modern multi-element measurement instrumentation. The complexity of geological materials makes it necessary to choose the sample decomposition technique that is compatible with the specific objective of the analysis. When selecting a decomposition technique, consideration should be given to the chemical and mineralogical characteristics of the sample, elements to be determined, precision and accuracy requirements, sample throughput, technical capability of personnel, and time constraints. This paper addresses these concerns and discusses the attributes and limitations of many techniques of sample decomposition along with examples of their application to geochemical analysis. The chemical properties of reagents as to their function as decomposition agents are also reviewed. The section on acid dissolution techniques addresses the various inorganic acids that are used individually or in combination in both open and closed systems. Fluxes used in sample fusion are discussed. The promising microwave-oven technology and the emerging field of automation are also examined. A section on applications highlights the use of decomposition techniques for the determination of Au, platinum group elements (PGEs), Hg, U, hydride-forming elements, rare earth elements (REEs), and multi-elements in geological materials. Partial dissolution techniques used for geochemical exploration which have been treated in detail elsewhere are not discussed here; nor are fire-assaying for noble metals and decomposition techniques for X-ray fluorescence or nuclear methods be discussed. ?? 1992.

  8. Combined use of EPR and 23Na MAS NMR spectroscopy for assessing the properties of the mixed cobalt-nickel-manganese layers of P3-NayCo1-2xNixMnxO2.

    Science.gov (United States)

    Kalapsazova, M; Ivanova, S; Kukeva, R; Simova, S; Wegner, S; Zhecheva, E; Stoyanova, R

    2017-10-11

    Knowledge on the formation of mixed transition metal layers on lithium and sodium transition metal oxides, Li/Na(Co,Ni,Mn,)O 2 , determines the ability to control their electrochemical properties as electrode materials in alkaline ion batteries. Taking this into account, herein we combine the EPR and 23 Na MAS NMR spectroscopic techniques to gain insights into the structural peculiarities of the mixed cobalt-nickel-manganese layers of Na y Co 1-2x Ni x Mn x O 2 with a three-layer stacking (P3-type) structure. Two types of compositions are examined where diamagnetic Co 3+ and paramagnetic Ni 3+ and Mn 4+ are stabilized: Na 2/3 Co 1/3 Ni 1/3 Mn 1/3 O 2 and Na 1/2 Ni 1/2 Mn 1/2 O 2 . EPR spectroscopy operating in the X- and Q-band region is applied with an aim to improve the spectra resolution and, on the other hand, to provide straightforward information on the coordination of the transition metal ions inside the layers. The analysis of EPR spectra is based on the reference for the Mn 4+ and Ni 2+ ions occurring simultaneously in oxides with two layer stacking, P2-Na 2/3 Ni 1/3 Mn 2/3 O 2 . Complementary to EPR, 23 Na MAS NMR spectroscopy at high spinning rates is undertaken to assess the local structure of the Na nucleus in the layered P3-Na y Co 1-2x Ni x Mn x O 2 oxides. All results are discussed taking into account the EPR and NMR data for the well-known lithium analogues O3-LiCo 1/3 Ni 1/3 Mn 1/3 O 2 and O3-LiNi 1/2 Mn 1/2 O 2 . Finally, the structure peculiarities of the transition metal layers extracted from the EPR and NMR methods are demonstrated by electrochemical intercalation of Li + ions into P3-Na y Co 1-2x Ni x Mn x O 2 .

  9. Evidence for radiation induced crosslinking in polytetrafluoroethylene by means of high-resolution solid-state 19F high-speed MAS NMR

    International Nuclear Information System (INIS)

    Katoh, Etsuko; Sugisawa, Hisashi; Oshima, Akihiro; Tabata, Yoneho; Seguchi, Tadao; Yamazaki, Toshimasa

    1999-01-01

    Radiation effects on molecular structure of polytetrafluoroethylene (PTFE) were studied by high-resolution solid-state 19 F high speed magic angle spinning (HS MAS) NMR spectroscopy. Samples used for the NMR studies were prepared by electron beam irradiation of PTFE with a wide range of irradiation doses from 0.5-10 MGy in the molten state at 340 deg. C under oxygen-free atmosphere. While the non-irradiated PTFE displayed only an intense peak of the internal CF 2 , several new signals corresponding to CF 3 , CF 2 and CF groups were observed for the PTFE which was high temperature irradiated at 340 deg. C in oxygen-free atmosphere (hti-PTFE). Intensities of these new signals increased with an increase of irradiation dose. The present solid-state 19 F HS MAS NMR studies provide not only the first experimental evidence regarding the existence of crosslinking structure in hti-PTFE, directly detected as the CF signal, but also the crosslinking density which can be estimated from a proportion of the CF versus total fluorine signal intensities. The higher the irradiation dose, the higher the crosslinking density; hti-PTFE with 10 MGy contains one crosslinking site per approximately 24 CF 2 groups, while the hti-PTFE with 5 MGy contains one crosslinking site per approximately 36 CF 2 groups. Further, G value of crosslinking (G(x)) was estimated from the signal intensities of 19 F HS MAS NMR spectra. The highest G(x)-value, 1.85, was observed for the 2MGy hti-PTFE sample, suggesting that crosslinking of PTFE is formed most efficaciously with 2 MGy irradiation in the molten state at 340 deg. C under oxygen-free atmosphere

  10. High field 27Al MAS NMR and TPD studies of active sites in ethanol dehydration using thermally treated transitional aluminas as catalysts

    Energy Technology Data Exchange (ETDEWEB)

    Hu, Jian Zhi; Xu, Suochang; Kwak, Ja Hun; Hu, Mary Y.; Wan, Chuan; Zhao, Zhenchao; Szanyi, Janos; Bao, Xinhe; Han, Xiuwen; Wang, Yong; Peden, Charles H. F.

    2016-04-01

    Gamma-, sigma- and theta-Al2O3 are well known metastable “transitional” alumina structural polymorphs. Upon heating, Al2O3 transitions to the so-called and Al2O3 polymorphs and finally forms the thermally stable Al2O3. The poorly developed crystallinity and co-existence of the , , and Al2O3 prior to forming all Al2O3, making it difficult to characterize the structures as well as to quantify the various phases of the transition alumina. As a result, there are significant controversies in the literatures. In this work, a detailed NMR analysis was carried out at high magnetic field on three special aluminum oxide samples where the, , , Al2O3 phases are made dominant, respectively, by controlling the synthesis conditions. The goal is to simplify, including making unambiguous, spectral assignments in 27Al MAS NMR spectra of transition alumina that have not yet been commonly agreed previously. Specifically, quantitative 1D 27Al MAS NMR was used to quantify the ratios of the different alumina structural units, 2D MQMAS 27Al MAS was used for obtaining the highest spectral resolution to guide the analysis of the 1D spectrum, and a saturation pulse sequence was integrated into the 1D NMR to select the amorphous structures, including obtain spectra where the penta-coordinate sites are observed with enhanced relative intensity. Collectively, this study uniquely assigns Al-peaks (both octahedral and tetrahedral) to the Al2O3 and the Al2O3 phases and offers a new way of understanding, including quantifying, the different structural units and sites in transition alumina samples.

  11. Rice herbicide monitoring in two Brazilian rivers during the rice growing season Monitoramento de herbicidas em dois rios brasileiros durante o período de cultivo do arroz

    Directory of Open Access Journals (Sweden)

    Enio Marchesan

    2007-01-01

    Full Text Available Irrigated rice production can involve environmental contamination with pesticides due to the proximity of the fields to rivers and to management problems. During three years (2000 to 2003 the rice herbicides clomazone, propanil and quinclorac were quantified in water during the rice growing season, in the Vacacaí and Vacacaí-Mirim Rivers, located in Rio Grande do Sul (RS State, Brazil. Water samples were taken at several locations in each river, selected by their importance in terms of rice drainage area. The samples were analyzed by HPLC-UV. At least one herbicide was detected in 41% of the samples from the Vacacaí River and 33% from the Vacacaí-Mirim River. The most frequent herbicide in both rivers and in each year was clomazone. The amount of herbicides in the river water was dependent on the rainfall regime. River water contamination by rice herbicides is probably caused by the rice water management used in the fields. The maintenance of flooded areas makes herbicides prone to contaminate the environment. To reduce the environmental contamination risk it is necessary to adopt measures to avoid overflow of flooded rice fields, keeping paddy water in the field for time enough to reduce the herbicide concentration before its release and enhancing the quality of the levees to reduce the probability of paddy rice overflow.No cultivo de arroz irrigado a possibilidade de contaminação dos mananciais hídricos é ampliada pelas características peculiares das áreas e do sistema de produção. Um estudo de monitoramento foi conduzido durante três anos (2000 a 2003, nos rios Vacacaí e Vacacaí-Mirim, localizados no Estado do Rio Grande do Sul, Brasil, buscando quantificar os herbicidas clomazone, propanil e quinclorac durante o período de cultivo do arroz. As amostras de água foram coletadas em vários locais em cada rio. Os locais de coleta foram selecionados pela importância em termos da captação da água de drenagem. As amostras foram

  12. Digital monitoring of mycelium growth kinetics and vigor of shiitake (Lentinula edodes (Berk. Pegler on agar medium Monitoramento digital do crescimento e vigor do shiitake (Lentinula edodes (Berk. Pegler em meio de cultura

    Directory of Open Access Journals (Sweden)

    Renato Mamede de Castro Montini

    2006-03-01

    .0, desenvolvido pela University of Texas Health Science Center, San Antonio, Texas. O modelo estatístico que melhor explicou a cinética de crescimento miceliano em área (mm², das linhagens de cogumelos L. edodes, tem como componente determinístico a exponencial de uma função Gompertz. O vigor, avaliado através da cor do micélio (em escala de tons do cinza, revelou um comportamento similar entre as linhagens, com valor máximo entre o 4º e 5º dia e, em seguida apresentou declínio. Em meios de cultura mais enriquecidos, a velocidade de crescimento das linhagens de L. edodes foi menor e o vigor maior. O monitoramento digital permite uma avaliação objetiva do crescimento e vigor do L. edodes in vitro.

  13. Monitoramento da autenticidade de amostras de bebidas alcoólicas enviadas ao Instituto Adolfo Lutz em São Paulo Evaluation of authenticity of alcoholic beverage samples examined by the Instituto Adolfo Lutz (São Paulo, Brazil

    Directory of Open Access Journals (Sweden)

    Leticia Araujo Farah NAGATO

    2001-01-01

    Full Text Available Este trabalho teve como objetivo verificar a autenticidade de bebidas alcoólicas (whisky, vodka, conhaque de gengibre, etc. enviadas para análise ao Instituto Adolfo Lutz no período de 1993 a agosto de 1999. Devido à presença no mercado nacional de bebidas alcoólicas clandestinas, principalmente aquelas com alto valor agregado, foi realizado o monitoramento através da análise de composição química destas bebidas. Normalmente estes produtos são elaborados com álcool, água, aroma e corante caramelo e que por falta de controle dessas matérias-primas, podem oferecer risco potencial à saúde humana pela presença de metanol. A técnica empregada na análise dos componentes secundários e metanol das amostras foi realizada através da cromatografia em fase gasosa com detector de ionização de chama. Observou-se que em 608 amostras de bebidas alcoólicas analisadas, 391 eram falsificadas e dentre estas 2 apresentaram teores de metanol acima do limite tolerado (200mg/100mL de álcool anidro pela legislação em vigor. Os resultados obtidos sugerem uma grande persistência em se produzir bebidas alcoólicas falsificadas. Desta forma, é muito importante estar sempre monitorando estes produtos e identificando os diferentes tipos de falsificações existentes no país.This work aimed at verifying the authenticity of alcoholic beverages (whisky, vodka, ginger spirit, etc. sent for analysis by the Instituto Adolfo Lutz, São Paulo from 1993 to August 1999. The chemical composition of these drinks was studied because of the presence of illicit alcoholic beverages on the national market, especially those with a high commercial value. These products are usually elaborated with alcohol, water, flavor and caramel coloring. Since there is no control over these raw materials, these drinks could offer a potential risk to human health because of the presence of methanol. The method employed in the analysis of congeners and methanol in alcoholic

  14. Observation of immobile regions in natural rubber at ambient temperature by solid-state C-13 CP/MAS NMR spectroscopy

    DEFF Research Database (Denmark)

    Larsen, F.H.; Rasmussen, T.; Pedersen, Walther Batsberg

    1999-01-01

    Employing C-13 CP/MAS NMR spectroscopy, the existence of immobile regions in natural rubber (cis-1,4-polyisoprene) corresponding to a few percent of the monomer units has been detected at ambient temperature. For synthetic rubbers no immobile regions have been detected at all. Applying different...... physical and chemical treatments to natural rubber it is shown that mastication, gamma-irradiation, and increasing the temperature, slightly above the ambient, reduce the amount of immobile regions. (C) 1999 Elsevier Science Ltd. All rights reserved....

  15. Investigating sorption on iron-oxyhydroxide soil minerals by solid-state NMR spectroscopy: a 6Li MAS NMR study of adsorption and absorption on goethite

    DEFF Research Database (Denmark)

    Nielsen, Ulla Gro; Paik, Younkee; Julmis, Keinia

    2005-01-01

    High-resolution 2H MAS NMR spectra can be obtained for nanocrystalline particles of goethite (alpha-FeOOH, particle size approximately 4-10 nm) at room temperature, facilitating NMR studies of sorption under environmentally relevant conditions. Li sorption was investigated as a function of pH, th...... on the goethite surface. Even larger Li hyperfine shifts (289 ppm) were observed for Li+-exchanged goethite, which contains lithium ions in the tunnels of the goethite structure, confirming the Li assignment of the 145 ppm Li resonance to the surface sites. Udgivelsesdato: 2005-Oct-6...

  16. Entrenamiento y fisiología del ejercicio en la pubertad : Análisis de las creencias actuales mas frecuentes

    OpenAIRE

    Mirco, Gustavo Ariel

    2013-01-01

    El presente trabajo forma parte de la especialización en fisiología del ejercicio de la Universidad Nacional de La Plata, Argentina. En este estudio se pudo comprobar la existencia de diversas creencias en cuanto a las prácticas de entrenamientos físico-deportivos en edades puberales. En primer lugar se seleccionaron algunas de las creencias consideradas mas relevantes en cuanto al impacto que pudieran ocasionar en los jóvenes practicantes. Posteriormente se confecciono un instrumento de reco...

  17. Uso del FitoMas-E® como atenuante del estrés salino (NaCl durante la emergencia y crecimiento inicial de Ocimum basilicum L.

    Directory of Open Access Journals (Sweden)

    D. Batista-Sánchez

    2015-01-01

    Full Text Available El uso de bioestimulantes vegetales estimula la emergencia y el crecimiento vegetal debido a que están compuestos por sustancias naturales como carbohidratos, péptidos de bajo peso molecular y aminoácidos, activadores de las funciones fisiológicas de las plantas, por lo que su aplicación permite un mejor aprovechamiento de los nutrientes y representa una opción para enfrentar problemas de estrés abiótico por salinidad. El objetivo de este estudio fue determinar el efecto del bioestimulante FitoMas-E® derivado de la caña de azúcar como atenuante de la salinidad en la emergencia y el crecimiento de plántulas de variedades de albahaca (Ocimum basilicum L. con respuesta diferencial al estrés por salinidad. Tres variedades de albahaca: Napoletano, Emily y Nufar se sometieron a cuatro concentraciones de NaCl (0, 50, 100 y 150 mM y cuatro dosis de FitoMas-E® (0, 0.5, 1.0 y 1.5 mL L-1 en un diseño completamente al azar con arreglo factorial con cuatro repeticiones. El trabajo se desarrolló en una estructura de malla sombra y las variables que se midieron fueron: porcentaje y tasa de emergencia, longitud de radícula, altura de la plántula, biomasa fresca y seca de radícula y de parte aérea. Los resultados evidenciaron que en condiciones de estrés salino (NaCl de moderado a severo, las variables disminuyeron significativamente. Largo de raíz, altura de planta y biomasa seca de raíz en 150 mM de NaCl fueron las más afectadas. Se observó que cuando se aplicó FitoMas-E® las plantas incrementaron significativamente sus valores en las variables, largo de raíz 32% y altura de planta 41%, lo que revela el efecto estimulante del FitoMas-E®, siendo 0.5 mL L-1 la dosis estimulante para la variedad Napoletano y 1.0 mL L-1 para la variedad Emily, aún y cuando se encontraban en condiciones de estrés salino hasta 100 mM de NaCl. Para la concentración de 150 mM se evidenció una afectación extrema para las variedades Emily y Nufar.

  18. Monitoramento em Promoção de Saúde: uma experiência de capacitação de adultos em um Estado do Nordeste brasileiro Monitoring in Health Promotion: an experience in the training of adults in a Brazilian northeastern state

    Directory of Open Access Journals (Sweden)

    Elizabeth Moreira dos Santos

    2012-12-01

    Full Text Available Este artigo tem como objetivo descrever e refletir, sistematicamente, sobre a experiência de implantação de processos de monitoramento do Programa Ação Saúde (PAS como uma experiência de tradução, contextualizada na interface entre a atenção básica do Sistema Único de Saúde (SUS e comunidades com características urbano-rurais. O PAS constituiu-se como uma proposta pedagógica baseada em competências e utilizou a metodologia da problematização. Os processos do PAS são tomados sob a ótica das operações de tradução, tais como: problematização, mobilização, enredamento e alinhamento. O monitoramento desses processos coloca em destaque os dilemas da mensuração, acompanhamento e reflexão compartilhada de seus efeitos tangíveis e intangíveis. A implementação do sistema de monitoramento intermediada por uma instituição pública acadêmica buscou contribuir para modelos de parcerias público-privadas em políticas de desenvolvimento social. Dentre as conexões promissoras estabelecidas no PAS, foi enfatizada a identificação da agenda pública no setor saúde como rota a ser fortalecida e potencializada, bem como ações de advocacy em torno da escolha de temáticas e prioridades locais. Concluiu-se que a configuração da rede de promoção de saúde foi influenciada por contextos geopolíticos diferenciados dos municípios, em especial para a sustentabilidade e implementação dos projetos locais e o estímulo a uma cultura local em Monitoramento e Avaliação - M&A.This article aims to systematically describe and reflect on the experience of implementing monitoring processes of the Programa Ação Saúde (PAS, or Health Action Programme, as an experience of translation, contextualized in the interface between primary care from the Sistema Único de Saúde (SUS, or Unified Health System, and communities with urban-rural characteristics. The PAS has established itself as a pedagogic proposition based on skills and

  19. Análise de Distorções na Soldagem de Juntas em “X” e “V” em Modelos Reduzidos em Escala de Anéis Segmentados Utilizando o Monitoramento Contínuo com Sensores a Laser

    Directory of Open Access Journals (Sweden)

    Jonathas Henrique Pereira

    2016-03-01

    Full Text Available Resumo Distorções em componentes soldados são alterações permanente de forma e dimensões resultantes das deformações plásticas que ocorrem devido as tensões térmicas desenvolvidas durante o processo de soldagem. Em função dos elevados custos para corrigir essas distorções de soldagem, existe grande interesse das indústrias em prever, monitorar e controlar estas distorções. Este trabalho compara as distorções ocorridas durante a soldagem de modelos de anel segmentado em escala reduzida com dois tipos de juntas (“X” e “V” utilizando a metodologia de monitoramento contínuo da evolução das distorções de soldagem com sensores a laser. Para o monitoramento contínuo são utilizados sensores a laser que são apoiados sobre a peça e os feixes foram projetados em um anteparo translúcido colocado em frente ao mesmo. Com a progressão da distorção durante a soldagem os feixes luminosos se movimentam pelo anteparo proporcionalmente a deformações ocorridas na peça. Os deslocamentos dos pontos luminosos refletidos no anteparo são filmados pelo lado oposto do anteparo. A discretização da filmagem permite analisar as deformações ao longo do processo soldagem e determinar a evolução das distorções em função do tempo. Foi confirmado que as soldagens realizadas em juntas em “X” apresentam menores valores de distorções que as juntas em “V”. Os resultados demostram que para os corpos de prova utilizados neste experimento pelo menos 60% da distorção ocorreu após a extinção do arco. Pelos testes experimentais foi possível afirmar que a técnica de monitoramento com sensores a laser é viável para utilizar na indústria e laboratórios de soldagem, porém faz-se necessário otimizar o processamento dos dados obtidos pela filmagem, permitindo um monitoramento instantâneo. A informação sobre a evolução das distorções durante a soldagem será útil para definir e monitorar de forma mais eficiente o

  20. Pengaruh Harga, Kualitas Produk, Dan Citra Merek Terhadap Keputusan Pembelian Kecap Manis Merek Bango (Studi Kasus Pada Ibu Rumah Tangga Di Komplek Villa Mutiara Johor Ii Dan Taman Johor Mas)

    OpenAIRE

    Nurlisa

    2013-01-01

    This research aims to determine the effects of pricing, product quality and brand image have a significant and positive impact on purchasing decision Bango soy sauce brands on housewife in Komplek Villa Mutiara Johor II and Taman Johor Mas. The population in this research was all the housewife in the Komplek Villa Mutiara Johor II and Taman Johor Mas. Data analyzing method is by using descriptive analyzing method and multiple linear regression. Kind of this research is causal comparative. Thi...

  1. Neutron techniques

    International Nuclear Information System (INIS)

    Charlton, J.S.

    1986-01-01

    The way in which neutrons interact with matter such as slowing-down, diffusion, neutron absorption and moderation are described. The use of neutron techniques in industry, in moisture gages, level and interface measurements, the detection of blockages, boron analysis in ore feedstock and industrial radiography are discussed. (author)

  2. AVALIAÇÃO DE MÉTODOS DE REDUÇÃO DE SONDAGENS BATIMÉTRICAS AO NÍVEL D'ÁGUA INSTANTÂNEO PARA MONITORAMENTO DE ASSOREAMENTO: ESTUDO DE CASO DO RESERVATÓRIO DA USINA HIDRELÉTRICA MAUÁ

    Directory of Open Access Journals (Sweden)

    Wesley Andersen Mezine

    Full Text Available O setor elétrico brasileiro está estruturado para garantir o fornecimento de energia elétrica à toda a nação, sendo que a geração é feita em sua maioria através de usinas hidrelétricas, onde o reservatório desempenha peça fundamental no processo de geração. O assoreamento de reservatórios pode impactar diretamente na operação e manutenção de usinas hidrelétricas, reduzindo a sua capacidade de armazenamento e vida útil. O monitoramento e a avaliação do volume assoreado do reservatório é uma importante ferramenta para o acompanhamento do processo de assoreamento e para fornecer as informações necessárias para embasar a tomada de decisões de forma a evitar a interrupção no processo de geração de energia, bem como danos ambientais. Neste trabalho foram testados três formas diferentes de realizar a redução do nível d'água instantâneo em levantamentos realizados com um ecobatímetro voltadas para o monitoramento de reservatórios: observações com RTK móvel, medições feitas na margem do reservatório com o RTK estático e leituras da régua linimétrica. Através dos cálculos das incertezas verticais totais e teste estatístico das duas médias constatou-se que as duas últimas técnicas apresentaram resultados equivalentes e sua aplicação é viável na área de estudo

  3. Reply to Mas et al.: Comment on Gebhardt et al. MAD-MEX: Automatic Wall-to-Wall Land Cover Monitoring for the Mexican REDD-MRV Program Using All Landsat Data. Remote Sens. 2014, 6, 3923–3943

    Directory of Open Access Journals (Sweden)

    Michael Schmidt

    2016-06-01

    Full Text Available Mas, J.F. et al. have submitted a paper [1] for publication, which aims to respond to a paper published by Gebhardt et al. [2]. Mas, J.F. et al. had received a consultancy in 2013 to assess the quality of the early prototype products partly described in Gebhardt et al. in 2014. This consultancy, although a formal non-disclosure agreement had not been demanded, was awarded under the mutual understanding that the data handed over to Mas et al. constitute the early development phase of the program. Therefore, Mas et al. had been asked to give an assessment on the quality of the prototypes to obtain a proof of concept for the proposed workflow of MAD-Mex. It was clear that this assessment would suffer from limited availability of high quality training and validation data available in 2013. Mas et al. finally did not execute the consultancy due to the limited vector processing capacities in their lab. In October 2014, we sent the latest products, version 4.2 of the MAD-Mex products, including the more than 200,000 validation points gathered from independent expert interpreters of all Mexican ecosystems. Mas et al. did not respond to this transfer or to our request to collaborate in the quality control and assessment of MAD-Mex.

  4. Os desastres podem até cair dos céus... Mas a culpa não é de Deus

    Directory of Open Access Journals (Sweden)

    Josué Petrônio Quirino de Oliveira

    2014-12-01

    Full Text Available O propósito desta pesquisa é apresentar uma reflexão sobre o descaso em que a politica de enfrentamento aos desastres naturais vem sendo abordada no Brasil nos últimos 100 anos.  Com uma população cada vez mais urbana as cidades passam a ser o centro não só do poder econômico e político, mas também dos mais diversos eventos decorrentes das mudanças climáticas. Uma série de problemas agrava essa urbanização vulnerável e desencadeiam uma crise socioambiental determinada por fatores sociais, políticos, econômicos, tecnológicos, culturais e ecológicos que, de forma integrada, provocam consequências devastadoras. Inundações, deslizamentos, ciclones, incêndios florestais, enxurradas, estiagens, enchentes, secas e terremotos provocam impactos inesperados e pressionam ainda mais este quadro urbano complexo a uma dinâmica preocupante. O desastre não são as principais ameaças, mas a incapacidade de planejamento e enfrentamento na gestão dos desastres demostraram o descaso com a questão foi tratado no país ao longo de décadas.

  5. Reklāmas ietekme uz patērētāju izvēles veikšanā

    OpenAIRE

    Asejevs, Aleksandrs

    2012-01-01

    Bakalaura darba tēma izvēlēta „Reklāmas ietekme uz patērētāju izvēles veikšanā”. Pastiprinoties konkurencei valstu iekšzemes tirgū, uzņēmumi savas preces un pakalpojumus virza globālajā tirgū. Starptautiskajā mārketingā reklāma tiek izmantota kā viens no mārketinga komunikācijas līdzekļiem, ar kura palīdzību uzņēmumi patērētajiem virzītu savas preces un pakalpojumus. Darba mērķis: balstoties uz veiktās aptaujas rezultātiem, izstrādāt priekšlikumus reklāmas pilnveidošanai Latvijā. Lai...

  6. Obtaining aluminas from the thermal decomposition of their different precursors: An {sup 27}Al MAS NMR and X-ray powder diffraction studies

    Energy Technology Data Exchange (ETDEWEB)

    Chagas, L.H.; De Carvalho, G.S.G. [Universidade Federal de Juiz de Fora, Departamento de Química, Grupo de Físico-Química de Sólidos e Interfaces, 36036-330 Juiz de Fora, MG (Brazil); San Gil, R.A.S. [Universidade Federal do Rio de Janeiro, Instituto de Química, 21949-900 Rio de Janeiro, RJ (Brazil); Chiaro, S.S.X. [PETROBRAS-CENPES, 21941-915 Rio de Janeiro, RJ (Brazil); Leitão, A.A. [Universidade Federal de Juiz de Fora, Departamento de Química, Grupo de Físico-Química de Sólidos e Interfaces, 36036-330 Juiz de Fora, MG (Brazil); Diniz, R., E-mail: renata.diniz@ufjf.edu.br [Universidade Federal de Juiz de Fora, Departamento de Química, Grupo de Físico-Química de Sólidos e Interfaces, 36036-330 Juiz de Fora, MG (Brazil)

    2014-01-01

    Graphical abstract: - Highlights: • We synthesized three precursors of alumina from different methods. • The calcination of the precursors generated several alumina polymorphs. • XRD and NMR were used for structural investigation of the polymorphs. • The synthesis route determines the structural and textural properties of the solids. - Abstract: A commercial sample of Boehmite was used as precursor of alumina polymorphs. For comparison, three other precursors were synthesized from different methods. Particularly, the use of excess of urea promoted a very crystalline form of basic aluminum carbonate. The characteristics of the four precursors were investigated by thermal, vibrational and X-ray powder diffraction (XRD) analysis. Additionally, the nuclear magnetic resonance, with magic angle spinning ({sup 27}Al MAS NMR), was used to verify the coordination of aluminum cations. Each precursor was calcined at various temperatures generating alumina polymorphs, which were structurally analyzed by XRD and {sup 27}Al MAS NMR. Due to interest in catalysis supports, special attention was given to the γ-Al{sub 2}O{sub 3} phase, which in addition to structural investigation was subjected to textural analysis. The results showed that, from different synthesis procedures and common route of calcination, one can obtain materials with the same composition but with different structural and textural properties, which in turn can significantly influence the performance of a supported catalyst.

  7. High field 27Al MAS NMR and TPD studies of active sites in ethanol dehydration using thermally treated transitional aluminas as catalysts

    Energy Technology Data Exchange (ETDEWEB)

    Hu, Jian Zhi; Xu, Suochang; Kwak, Ja Hun; Hu, Mary Y.; Wan, Chuan; Zhao, Zhenchao; Szanyi, Janos; Bao, Xinhe; Han, Xiuwen; Wang, Yong; Peden, Charles H. F.

    2016-04-01

    High field quantitative 27Al MAS NMR and temperature programmed desorption (TPD) of ethanol are used to study the surface and phase transformation of gamma-Al2O3 during calcination in the temperature range of 500 to 1300 degrees C. Following ethanol adsorption, ethylene is generated during TPD with a desorption temperature > 200 degrees C. With increasing calcination temperature prior to TPD, the amount of ethylene produced decreases monotonically. Significantly, 27Al MAS NMR reveals that the amount of penta-coordinate Al3+ ions (Lewis acid sites) also decreases with increasing calcination temperature. In fact, a strong correlation between the amount of penta-coordinate Al3+ ions and the amount of strongly adsorbed ethanol molecules (i.e., the ones that convert to ethylene during TPD) is obtained. This result indicates that the penta-coordinate aluminum sites are the catalytic active sites on alumina surfaces during ethanol dehydration reaction across the entire course of gamma- to alpha-Al2O3 phase transformations.

  8. Lima masónica: las logias simbólicas y su progreso en el medio urbano a fines del siglo XIX

    Directory of Open Access Journals (Sweden)

    Chocano, Magdalena

    2010-08-01

    Full Text Available This article deals with the organization of the Grand Lodge of Peru, founded in 1882. Using Masonic publications and sources, it aims to establish the dynamics of its local lodges and to assess the character of Masonic activity in Peru at the end of the 19th century. Finally, it examines the political positioning of the Masonic leadership and its performance in the national political scene where it challenged Catholic exclusivity.

    Este artículo presenta un análisis de la organización de la Gran Logia del Perú, fundada en 1882. A partir de las fuentes masónicas, se busca establecer la dinámica de cada logia y el carácter del accionar masónico. Finalmente, se examinan las actitudes políticas que fomentaron sus dirigentes y su actuación en la escena nacional donde desafiaron al exclusivismo católico.

  9. Interneta vietne "YouTube" kā reklāmas un infoizklaides kanāls 2008. gada pirmajā ceturksnī

    OpenAIRE

    Reinberga, Ieva

    2008-01-01

    Bakalaura darba mērķis ir izpētīt, kādus komunikācijas uzdevumus veikusi interneta vietne www.YouTube.com – reklāmas, izklaides, informācijas vai citus - laika periodā no 2008. gada 1. janvāra līdz 2008. gada 31. martam, konstatējot vietnes saturā reklāmai, izklaidei un informācijai raksturīgās iezīmes. Pētījums tiek balstīts uz reklāmas, infoklaides, interneta tehnoloģiju, spēles teorijas, populārās kultūras teorijām, kā arī, atsaucoties uz līdzšinējām analīzēm par vietnes YouTube vēstur...

  10. "Okarte" reklāmas kampaņas "Onedēļa" komunikācija internetā 2013. gadā

    OpenAIRE

    Volonts, Kaspars

    2013-01-01

    Bakalaura darba tēma ir “"Okarte" reklāmas kampaņa "Onedēļa" komunikācija internetā 2013. gadā”. Tēma par zīmola komunikāciju interneta vidē ir aktuāla, jo interneta lietotāju skaits Latvijā aug katru gadu. Latvijā strādājošiem zīmoliem arvien biežāk jāsaskarās ar savu mērķauditoriju, izmantojot internetu. Bakalaura darba pētījuma mērķis ir izpētīt kā “Latvijas Mobilā Telefona” priekšapmaksas kartes “Okarte” zīmols komunicē savu tēlu un reklāmas kampaņu interneta vidē 2013.gadā. Ša...

  11. "KinLeaves" reklāmas aktivitātes sociālajā tīklā “Facebook” 2016. gadā

    OpenAIRE

    Mandrika, Dana

    2017-01-01

    Bakalaura darba mērķis ir izpētīt, kādas reklāmas aktivitātes uzņēmums ir veicis un noskaidrot, vai sociālajā tīklā “Facebook” ar reklāmas aktivitātēm ir iespējams sasniegt mērķauditoriju. Darbs sastāv no trīs daļām – teorētiskās, metodoloģiskās un empīriskās. Teorētisko daļu veido nodaļas par reklāmu, sociālo tīklu vietnēm, sociālo tīklu „Facebook” un reklāmu sociālo tīklu vietnēs. Metodoloģiskajā daļā apskatītas pētījumā izmantotās metodes - kontentanalīze, intervija, anketēšana. Empīrisk...

  12. Personāla atlases un apmācības sistēmas pilnveidošana uzņēmumā "X"

    OpenAIRE

    Strode, Gunta

    2012-01-01

    Bakalaura darbā „Personāla atlases un apmācības sistēmas pilnveidošana uzņēmumā „X” ” tiek izskatīti un analizēti jautājumi par personāla atlases un apmācības procesu. Darbs sastāv no trim daļām. Pirmajā daļā tiek raksturoti personāla atlases mērķi un atlases organizēšanas kārtība. Otrajā daļā tiek raksturota personāla apmācības nozīme un organizēšanas nosacījumi. Trešajā daļā tiek pētīta personāla atlases un apmācības sistēmas pilnveidošana uzņēmumā „X”. Pamatojoties uz veiktajiem ...

  13. 1H-detected MAS solid-state NMR experiments enable the simultaneous mapping of rigid and dynamic domains of membrane proteins

    Science.gov (United States)

    Gopinath, T.; Nelson, Sarah E. D.; Veglia, Gianluigi

    2017-12-01

    Magic angle spinning (MAS) solid-state NMR (ssNMR) spectroscopy is emerging as a unique method for the atomic resolution structure determination of native membrane proteins in lipid bilayers. Although 13C-detected ssNMR experiments continue to play a major role, recent technological developments have made it possible to carry out 1H-detected experiments, boosting both sensitivity and resolution. Here, we describe a new set of 1H-detected hybrid pulse sequences that combine through-bond and through-space correlation elements into single experiments, enabling the simultaneous detection of rigid and dynamic domains of membrane proteins. As proof-of-principle, we applied these new pulse sequences to the membrane protein phospholamban (PLN) reconstituted in lipid bilayers under moderate MAS conditions. The cross-polarization (CP) based elements enabled the detection of the relatively immobile residues of PLN in the transmembrane domain using through-space correlations; whereas the most dynamic region, which is in equilibrium between folded and unfolded states, was mapped by through-bond INEPT-based elements. These new 1H-detected experiments will enable one to detect not only the most populated (ground) states of biomacromolecules, but also sparsely populated high-energy (excited) states for a complete characterization of protein free energy landscapes.

  14. Um ambiente multiagent system (MAS distribuído aplicado à gestão integrada da operação portuária

    Directory of Open Access Journals (Sweden)

    Rodrigo de Alvarenga Rosa

    2016-09-01

    Full Text Available Tendo em vista o aumento do transporte marítimo no mundo e a consequente demanda por operações nos portos, os operadores buscam formas de minimizar o tempo de permanência dos navios no porto. Para atracar um navio, os portos necessitam ter disponíveis diversos recursos. Assim, planejar a designação de recursos eficientemente para não atrasar a atracação dos navios é vital para os portos. Esta designação é dinâmica, pois atrasos e antecipações na chegada dos navios ocorrem por diversos fatores demandando assim que ela seja atualizada constantemente. Este artigo propõe um Multiagent System (MAS para resolução da designação de recursos de forma distribuída e em tempo real, visando reduzir o tempo de espera para atracação dos navios. Testes foram realizados em 27 cenários e os resultados mostraram que o MAS resolveu instâncias de teste de grande porte e nos cenários mais próximos do real, ele resolveu em um tempo pequeno e com soluções estáveis.

  15. Clinical value of CARE dose 4D technique in decreasing CT scanning dose of adult chest

    International Nuclear Information System (INIS)

    Wu Aiqin; Zheng Wenlong; Xu Chongyong; Fang Bidong; Ge Wen

    2011-01-01

    Objective: To investigate the value of CARE Dose 4D technique in decreasing radiation dose and improving image quality of multi-slice spiral CT in adult chest scanning. Methods: 100 patients of chest CT scanning were equally divided into study group and control group randomly. CARE Dose 4D Technique was used in study group. Effective mAs value, volume CT dose index (CTDI vol ) and dose length product (DLP) were displayed automatically in machine while chest scanning; those values and actual mAs value of every image were recorded respectively. The image quality at apex of lung, lower edge of aorta arch, middle area of left atrium and base of lung on every image of 400 images was judged and classified as three level (excellent, good, poor) by two deputy chief physicians with double blind method, the image noise at corresponding parts was measured. Results: While setting 80 mAs for quality reference mAs, the effective mAs value in study group most decreased 44 mAs than control group with an average decrease of 9.60 (12.0%), CTDI vol with 4.75 mGy with an average decrease of 0.95 mCy (11.0%), DLP 99.50% in study group, with 98.0% in control group. But it was higher at apex of lung and base of lung, lower at middle area of left atrium, and similar at lower edge of aorta arch in study group than contrast group. The image noise were lower at apex of lung and base of lung in study group than control group (t =6.299 and 2.332, all P<0.05), higher at middle area of left atrium in study group than control group (t=3.078, P<0.05) and similar at lower edge of aorta arch in study group than control group (t=1.191, P>0.05). Conclusions: CARE Dose 4D technique provides a function regulated mAs real-time on line, it not only raises utilization rate of radiation and decreases radiation dose, but also promises and increases image quality in chest CT scanning, and has some clinical significance. (authors)

  16. 13C and 15N CP/MAS, 1H-15N SCT CP/MAS and FTIR spectroscopy as tools for qualitative detection of the presence of zwitterionic and non-ionic forms of ansa-macrolide 3-formylrifamycin SV and its derivatives in solid state.

    Science.gov (United States)

    Przybylski, Piotr; Pyta, Krystian; Klich, Katarzyna; Schilf, Wojciech; Kamieński, Bohdan

    2014-01-01

    (13)C, (15)N CP/MAS, including (1)H-(13)C and (1)H-(15)N short contact time CP/MAS experiments, and FTIR methods were applied for detailed structural characterization of ansa-macrolides as 3-formylrifamycin SV (1) and its derivatives (2-6) in crystal and in powder forms. Although HPLC chromatograms for 2/CH3 OH and 2/CH3 CCl3 were the same for rifampicin crystals dissolved in respective solvents, the UV-vis data recorded for them were different in 300-375 nm region. Detailed solid state (13)C and (15)N CP/MAS NMR and FTIR studies revealed that rifampicin (2), in contrast to 3-formylrifamycin SV (1) and its amino derivatives (3-6), can occur in pure non-ionic or zwitterionic forms in crystal and in pure these forms or a mixture of them in a powder. Multinuclear CP/MAS and FTIR studies demonstrated also that 3-6 derivatives were present exclusively in pure zwitterionic forms, both in powder and in crystal. On the basis of the solid state NMR and FTIR studies, two conformers of 3-formylrifamycin SV were detected in powder form due to the different orientations of carbonyl group of amide moiety. The PM6 molecular modeling at the semi-empirical level of theory, allowed visualization the most energetically favorable non-ionic and zwitterionic forms of 1-6 antibiotics, strongly stabilized via intramolecular H-bonds. FTIR studies indicated that the originally adopted forms of these type antibiotics in crystal or in powder are stable in standard laboratory conditions in time. The results presented point to the fact that because of a possible presence of two forms of rifampicin (compound 2), quantification of the content of this antibiotic in relevant pharmaceuticals needs caution. Copyright © 2013 John Wiley & Sons, Ltd.

  17. Astrophysical techniques

    CERN Document Server

    Kitchin, CR

    2013-01-01

    DetectorsOptical DetectionRadio and Microwave DetectionX-Ray and Gamma-Ray DetectionCosmic Ray DetectorsNeutrino DetectorsGravitational Radiation Dark Matter and Dark Energy Detection ImagingThe Inverse ProblemPhotographyElectronic ImagingScanningInterferometrySpeckle InterferometryOccultationsRadarElectronic ImagesPhotometryPhotometryPhotometersSpectroscopySpectroscopy SpectroscopesOther TechniquesAstrometryPolarimetrySolar StudiesMagnetometryComputers and The Internet.

  18. Presentation Technique

    International Nuclear Information System (INIS)

    Froejmark, M.

    1992-10-01

    The report presents a wide, easily understandable description of presentation technique and man-machine communication. General fundamentals for the man-machine interface are illustrated, and the factors that affect the interface are described. A model is presented for describing the operators work situation, based on three different levels in the operators behaviour. The operator reacts routinely in the face of simple, known problems, and reacts in accordance with predetermined plans in the face of more complex, recognizable problems. Deep fundamental knowledge is necessary for truly complex questions. Today's technical status and future development have been studied. In the future, the operator interface will be based on standard software. Functions such as zooming, integration of video pictures, and sound reproduction will become common. Video walls may be expected to come into use in situations in which several persons simultaneously need access to the same information. A summary of the fundamental rules for the design of good picture ergonomics and design requirements for control rooms are included in the report. In conclusion, the report describes a presentation technique within the Distribution Automation and Demand Side Management area and analyses the know-how requirements within Vattenfall. If different systems are integrated, such as geographical information systems and operation monitoring systems, strict demands are made on the expertise of the users for achieving a user-friendly technique which is matched to the needs of the human being. (3 figs.)

  19. Astrophysical techniques

    Energy Technology Data Exchange (ETDEWEB)

    Kitchin, C R

    1984-01-01

    The subject is covered in chapters, entitled: detectors (optical and infrared detection; radio and microwave detection; X-ray and gamma-ray detection; cosmic ray detectors; neutrino detectors; gravitational radiation); imaging (photography; electronic imaging; scanning; interferometry; speckle interferometry; occultations; radar); photometry and photometers; spectroscopy and spectroscopes; other techniques (astrometry; polarimetry; solar studies; magnetometry). Appendices: magnitudes and spectral types of bright stars; north polar sequence; standard stars for the UBV photometric system; standard stars for the UVBY photometric system; standard stars for MK spectral types; standard stars for polarimetry; Julian date; catalogues; answers to the exercises.

  20. Llizarov technique

    International Nuclear Information System (INIS)

    Shankman, S.; Rosenberg, Z.S.; Frankel, V.; Golyakhovsky, V.

    1990-01-01

    This paper illustrates the radiographic manifestations of the Ilizarov distraction technique for the correction of short and deformed limbs. The radiographs of 130 patients who underwent Ilizarov distraction at 160 sites since December 1986 were reviewed retrospectively. Reasons for correction included fracture nonunion and malunion idiopathic leg length discrepancy, achondroplasia, and neurofibromatosis with tibial pseudarthrosis. Ninety patients were adults, and 40 were children. In order to assess cortical bone development during the fixation phase, CT of the regenerate bone was performed in 17 patients. Conventional tomograms were obtained in 20 patients for the evaluation of delayed or hypoplastic union at the distraction site

  1. Experimental Techniques

    International Nuclear Information System (INIS)

    Fournier, D.; Serin, L.

    1995-01-01

    Experimental techniques to be used in the new generation of high energy physics are presented. The emphasis is put on the new ATLAS and CMS detectors for the CERN LHC. For the most important elements of these detectors, a description of the underlying physics processes is given, sometimes with reference to comparable detectors used in the past. Some comparative global performances of the two detectors are also given, with reference to benchmark physics processes (detection of the Higgs boson in various mass regions, etc). (author)

  2. Individualization of radiographic techniques in computerized radiology; Individualizacao das tecnicas radiograficas em radiologia computadorizada

    Energy Technology Data Exchange (ETDEWEB)

    Abrantes, M.E.S.; Oliveira, A.H. de, E-mail: marcosabrantes2003@yahoo.com.br [Universidade Federal de Minas Gerais (DEN/UFMG), Belo Horizonte, MG (Brazil). Departamento de Engenharia Nuclear; Feliz, W.F.; Stoppa, L.G.; Paiva, O.A. [Universidade Federal de Minas Gerais (UFADTI/UFMG), Belo Horizonte, MG (Brazil). Hospital das Clinicas. Unidade Funcional Apoio Diagnostico e Terapeutica por Imagem; Oliveira, G.A.P. [Universidade Federal de Minas Gerais (DEN/UFMG), Belo Horizonte, MG (Brazil). Departamento de Anatomia e Imagem

    2015-07-01

    This work aims to produce information for image quality implementation in a radiology sector based on previous assessments of the images by questionnaires, acceptance and quality, as step of recognition of the parameters used in radiographic techniques. After this research data raised were divided into male group, female, PA and PF thickness, body mass index, type of biotypes, anthropomorphic parameters, body evaluation associated with the constant tension and additional filtration. The results show the predominance of the 35 and 40 constant with additional filtering from 0.5 to 1.5 mmAl, voltage for male gender (PA PF) 86-92 kV and 96-112 kV voltage for female gender of 85-98 kV and 96-112 kV, respectively. The load applied to the tube for males (PA and PF) is between 5-10 and 5-16 mA.s mA.s and for females (PA and PF) is between 6.3 to 8 mA.s and 9-14 mA.s.

  3. Study of an optimization protocol for radiographic techniques in computerized radiology

    International Nuclear Information System (INIS)

    Abrantes, Marcos Eugenio Silva

    2015-01-01

    This work is designed to produce information for the improvement of image quality to deployment in a radiology department based on previous reviews of the images by questionnaires of acceptance and quality e recognition of the parameters used in chest radiographic techniques. The data collected were divided by male, female, PA and LAT thickness, body mass index, biotypes, anthropomorphic parameters and body evaluation associated with constant voltage and the additional filtration. The results show the predominance of 35 and 40 constants with additional filtration from 0.5 to 1.5 mmAl, voltage in male: (PA and LAT) 86-92 kV and 96-112 kV, female: 85-98 kV and 96-112 kV. The charge applied to the tube for males: (PA and LAT) 5-10 mA.s and 5-16 mA.s, female: (PA and LAT) 6.3-8 mA.s and 9-14 mA.s. Absorbed doses for males: (PA and PF) 0.04-0.17 mGy and 0.03-0.19 mGy and from female (PA and PF) from 0.03-0.22 mGy and 0, 04-0.17 mGy. This procedure can be used in radiology department to implement and acceptance in the quality of images. (author)

  4. GEOGRAFIA DA DENGUE: UMA ANÁLISE DAS POLÍTICAS DE CONTROLE E MONITORAMENTO DO AEDES AEGYPTI EM MANAUS/ Geography of Dengue: an analysis of the control and monitoring policies of Aedes aegypti in Manaus

    Directory of Open Access Journals (Sweden)

    Renato Ferreira de Souza

    2018-04-01

    Full Text Available Manaus apresentou uma expansão urbana impulsionada pelo advento da Zona Franca, resultando numa insuficiente infraestrutura urbana para atender o aumento populacional, atraído pelo crescimento industrial e comercial da capital amazonense, a partir da década de 1970. Dessa forma, ampliaram-se os problemas de saneamento básico, comprometendo a qualidade de vida de sua população. O controle do dengue torna-se um grande desafio, não só para os geógrafos, mas também para as políticas de controle de endemias. As zonas norte e leste de Manaus caracterizam-se por bairros mais pobres, onde degradação ambiental e desigualdades sociais ameaçam o acesso a um ambiente saudável. Infelizmente muitas pessoas não têm o cuidado de manter o ambiente limpo e livre de proliferação de mosquitos, principalmente o do vetor da dengue. Nesse sentido, é importante desenvolver um trabalho de sensibilização junto às escolas, pois as crianças e adolescentes são base para serem multiplicadores de divulgação dos cuidados necessários contra a dengue.

  5. Solid state NMR of proteins at high MAS frequencies: symmetry-based mixing and simultaneous acquisition of chemical shift correlation spectra

    International Nuclear Information System (INIS)

    Bellstedt, Peter; Herbst, Christian; Häfner, Sabine; Leppert, Jörg; Görlach, Matthias; Ramachandran, Ramadurai

    2012-01-01

    We have carried out chemical shift correlation experiments with symmetry-based mixing sequences at high MAS frequencies and examined different strategies to simultaneously acquire 3D correlation spectra that are commonly required in the structural studies of proteins. The potential of numerically optimised symmetry-based mixing sequences and the simultaneous recording of chemical shift correlation spectra such as: 3D NCAC and 3D NHH with dual receivers, 3D NC′C and 3D C′NCA with sequential 13 C acquisitions, 3D NHH and 3D NC′H with sequential 1 H acquisitions and 3D CANH and 3D C’NH with broadband 13 C– 15 N mixing are demonstrated using microcrystalline samples of the β1 immunoglobulin binding domain of protein G (GB1) and the chicken α-spectrin SH3 domain.

  6. Deafness memories in Antonio Lobo Antunes’ chronicles “O surdo” (1998 and “Não foi com certeza assim mas faz de conta” (2002

    Directory of Open Access Journals (Sweden)

    Alessandra Gomes Silva

    2017-06-01

    Full Text Available This work intends to analyze some images and meanings attributed to deafness in two chronicles of Portuguese writer António Lobo Antunes: “Não foi com certeza assim mas faz de conta” (2002 and “O surdo” (1998. We are also interested in the type of creation of these texts, drawing a parallel with the kind of reflection developed in some writings of Walter Benjamin, basically in “One-way street” and “Berlin childhood”. In both authors, the fictional production is linked to the issue of memory, taking as its starting point the contact with a seemingly simple everyday object. Finally, we emphasize the discussion of the normalization of bodies, based on the issue of not hearing and how it is socially perceived.---DOI: http://dx.doi.org/10.22409/abriluff.2017n18a369

  7. Design of high-power, broadband 180o pulses and mixing sequences for fast MAS solid state chemical shift correlation NMR spectroscopy

    International Nuclear Information System (INIS)

    Herbst, Christian; Herbst, Jirada; Kirschstein, Anika; Leppert, Joerg; Ohlenschlaeger, Oliver; Goerlach, Matthias; Ramachandran, Ramadurai

    2009-01-01

    An approach for the design of high-power, broadband 180 o pulses and mixing sequences for generating dipolar and scalar coupling mediated 13 C- 13 C chemical shift correlation spectra of isotopically labelled biological systems at fast magic-angle spinning frequencies without 1 H decoupling during mixing is presented. Considering RF field strengths in the range of 100-120 kHz, as typically available in MAS probes employed at high spinning speeds, and limited B 1 field inhomogeneities, the Fourier coefficients defining the phase modulation profile of the RF pulses were optimised numerically to obtain broadband inversion and refocussing pulses and mixing sequences. Experimental measurements were carried out to assess the performance characteristics of the mixing sequences reported here

  8. El sueño de Venecia o el guiño de los clásicos en la narrativa de Paloma Díaz-Mas

    Directory of Open Access Journals (Sweden)

    Neus Samblancat

    2010-06-01

    Full Text Available Su artículo propone que la concepción de la obra de Paloma Díaz-Mas, El sueño de Venecia, como palimpsesto literario nos conduce a un análisis intertextual donde cada capítulo de la novela nos remite a un género y a unas voces de época. Los clásicos, como el resto de la producción narrativa de la autora, guiñan el ojo a lo largo de una obra que plantea una reflexión sobre la fragilidad de la razón y de la humana Memoria a la hora de conocer la Historia y de explicar una historia.

  9. Siber Kimliklerin Kişiliğe Yansıması: Proteus Etki (Tanımı, Nedenleri Ve Önlenmesi)

    OpenAIRE

    TANHAN, Fuat; ALAV, Özlem

    2015-01-01

    Hayatın vazgeçilmez bir parçası haline gelmiş olan teknoloji ve internet bireyi ve toplumu farklı yönlerden etkisi altına alabilmektedir. Teknoloji ve internet sanal çevre diye bilinen yeni bir sosyal dünyanın oluşmasına neden olmuştur. Sanal dünya, sınırları neredeyse çizilemeyen bir çevre sunmakta ve bu çevre içinde bulunan bireyleri, kurumları etkilemekte ve dönüştürmektedir.  Söz konusu etki, kimi yönlerden olumlu, kimi yönlerden ise olumsuzlaşmaktadır. Sanal dünyadaki ilişkiler, kimlikle...

  10. "La escuadra, el compás y la lira. Poemas publicados en la prensa masónica puertorriqueña, 1883-1887"

    Directory of Open Access Journals (Sweden)

    Miguel A. Pereira Rivera

    2013-01-01

    Full Text Available El autor analizó los poemas publicados en varios periódicos masónicos puertorriqueños publicados durante losaños 1883-1887, para evaluar como éstos pudieron promover una “lectura dominante” de los principiosasociados a la modernidad en el Puerto Rico del Siglo XIX. Se presenta información sobre los periódicos,incluyendo su historial y datos biográficos de sus editores.Para este esfuerzo investigativo se utilizaron, ademásde los periódicos de la época citada, fuentes documentales primarias de laGran Logia Soberana de Libres yAceptados Masones de Puerto Rico.

  11. Entrevista a un masón. Perspectiva antropológica de una realidad ignorada (José J. L. Gómez

    Directory of Open Access Journals (Sweden)

    Carlos Peláez Paz

    2007-05-01

    Full Text Available El texto nos acerca a una realidad declarada ignorada, que suscita la fantasía y la especulación morbosa de lo desconocido, de aquello que situamos entre la leyenda, lo esotérico y la realidad. Aleccionados en el prejuicio contra la masonería, hemos crecido en los temores, malentendidos, estereotipos e incluso una cierta estigmatización de masones y logias, presentes en el recorrido de nuestra historia, teñida por las luchas políticas y fratricidas de las diversas Españas y el, recordado en el libro, “contubernio judeo masónico”.

  12. Solid state NMR of proteins at high MAS frequencies: symmetry-based mixing and simultaneous acquisition of chemical shift correlation spectra

    Energy Technology Data Exchange (ETDEWEB)

    Bellstedt, Peter [Fritz Lipmann Institute, Biomolecular NMR spectroscopy, Leibniz Institute for Age Research (Germany); Herbst, Christian [Ubon Ratchathani University, Department of Physics, Faculty of Science (Thailand); Haefner, Sabine; Leppert, Joerg; Goerlach, Matthias; Ramachandran, Ramadurai, E-mail: raman@fli-leibniz.de [Fritz Lipmann Institute, Biomolecular NMR spectroscopy, Leibniz Institute for Age Research (Germany)

    2012-12-15

    We have carried out chemical shift correlation experiments with symmetry-based mixing sequences at high MAS frequencies and examined different strategies to simultaneously acquire 3D correlation spectra that are commonly required in the structural studies of proteins. The potential of numerically optimised symmetry-based mixing sequences and the simultaneous recording of chemical shift correlation spectra such as: 3D NCAC and 3D NHH with dual receivers, 3D NC Prime C and 3D C Prime NCA with sequential {sup 13}C acquisitions, 3D NHH and 3D NC Prime H with sequential {sup 1}H acquisitions and 3D CANH and 3D C'NH with broadband {sup 13}C-{sup 15}N mixing are demonstrated using microcrystalline samples of the {beta}1 immunoglobulin binding domain of protein G (GB1) and the chicken {alpha}-spectrin SH3 domain.

  13. 13C CP MAS NMR and GIAO-CHF/DFT calculations of flavonoids: Morin, kaempferol, tricin, genistein, formononetin and 3,7-dihydroxyflavone

    Science.gov (United States)

    Zielińska, Agnieszka; Paradowska, Katarzyna; Jakowski, Jacek; Wawer, Iwona

    2008-02-01

    13C CP MAS NMR spectra of the flavonoids: morin, kaempferol, 3,7-dihydroxyflavone, tricin and isoflavones: genistein and formononetin were recorded to characterize solid-state conformations. Intramolecular hydrogen bonds forming five-, six- and seven-membered rings are present in the two morin molecules in the crystals - their 13C resonances have been assigned with the aid of the calculated shielding constants. Linear relationships between the calculated shielding constants σDFT (ppm) and chemical shifts ( δCPMAS, ppm) were obtained for all studied compounds. Higher correlation coefficients suggest that the conformation with "clockwise" orientation of both OH groups is more probable in the solid 3,7-dihydroxyflavone, whereas in the solid formononetin the OH and OCH 3 substituents are directed "anticlockwise". The barrier to the rotation of phenyl ring B decreases in the order: morin (2'-OH, 3-OH) > kaempferol (3-OH) > tricin.

  14. Pour le plaisir de la chose : analyse de contenu des conceptions et des usages du Kâmasûtra dans l'Occident contemporain

    OpenAIRE

    Robidas, Josiane

    2010-01-01

    Ce mémoire a pour but de retracer comment le Kāmasūtra, traité classique hindou sur l'art de vivre et d'aimer, est présenté et véhiculé dans l'Occident depuis sa première traduction, tant pour son interprétation, sa diffusion et sa réception que pour ce qu'il permet comme regards sur les représentations des sexualités occidentales. L'analyse de contenu a été faite à partir d'un corpus très hétérogène, contenant à la fois des traductions, des ouvrages scientifiques (qui permettent notamment la...

  15. Fate of [15N]glycine in peat as determined by 13C and 15N CP-MAS NMR spectroscopy

    International Nuclear Information System (INIS)

    Benzing-Purdie, L.M.; Cheshire, M.V.; Williams, B.L.; Sparling, G.P.; Ratcliffe, C.I.; Ripmeester, J.A.

    1986-01-01

    Peat samples, nonsterile, sterilized by γ irradiation or autoclaving, were incubated with [ 15 N]glycine for a period of 6 months. The 13 C NMR data showed the established trend of increased humification with decreasing particle size and that autoclaving had significantly disturbed the humification-particle size distribution. The 15 N CP-MAS NMR spectra showed the presence of [ 15 N]glycine in all fractions after incubation. 15 NH 4 + , a result of either biological or chemical deamination, was one of the main products in the nonsterile peat series. The 15 N spectra also showed resonances corresponding to amine, secondary amide, and pyrrole-type nitrogen and the presence of glycine derivatives and melanoidins. The results presented give the first spectroscopic evidence of the possible involvement of the Maillard reaction in the humification process

  16. Industrial technique

    International Nuclear Information System (INIS)

    Robertson, D.H.

    1975-01-01

    Techniques for selectively extracting and storing only krypton and xenon in the waste gases that are released from a pressurized water nuclear power reactor are described. The illustrative fluorocarbon absorption system has three separation stages: an initial gas-fluorocarbon absorber, a flash chamber and fractionator for segregating all of the absorbed gases from the loaded absorber stage fluorocarbon (save for the krypton and xenon), and a stripper that receives the partially loaded fluorocarbon liquid directly from the fractionator in order to separate only the krypton and xenon. A molecular sieve filter dries the input process gas, a cartridge type solvent filter is used to remove radiation degradation products from the loaded liquid that flows from the absorber, a cold trap gas drier is provided to remove residual solvent vapor from the separated krypton and xenon, and radiation detectors automatically activate valves to establish safe conditions in the event of an accident or plant failure. (U.S.)

  17. Experimental techniques

    International Nuclear Information System (INIS)

    Roussel-Chomaz, P.

    2007-01-01

    This lecture presents the experimental techniques, developed in the last 10 or 15 years, in order to perform a new class of experiments with exotic nuclei, where the reactions induced by these nuclei allow to get information on their structure. A brief review of the secondary beams production methods will be given, with some examples of facilities in operation or under project. The important developments performed recently on cryogenic targets will be presented. The different detection systems will be reviewed, both the beam detectors before the targets, and the many kind of detectors necessary to detect all outgoing particles after the reaction: magnetic spectrometer for the heavy fragment, detection systems for the target recoil nucleus, γ detectors. Finally, several typical examples of experiments will be detailed, in order to illustrate the use of each detector either alone, or in coincidence with others. (author)

  18. Combinatorial techniques

    CERN Document Server

    Sane, Sharad S

    2013-01-01

    This is a basic text on combinatorics that deals with all the three aspects of the discipline: tricks, techniques and theory, and attempts to blend them. The book has several distinctive features. Probability and random variables with their interconnections to permutations are discussed. The theme of parity has been specially included and it covers applications ranging from solving the Nim game to the quadratic reciprocity law. Chapters related to geometry include triangulations and Sperner's theorem, classification of regular polytopes, tilings and an introduction to the Eulcidean Ramsey theory. Material on group actions covers Sylow theory, automorphism groups and a classification of finite subgroups of orthogonal groups. All chapters have a large number of exercises with varying degrees of difficulty, ranging from material suitable for Mathematical Olympiads to research.

  19. Bridging the Gap between ABM and MAS: A Disaster-Rescue Simulation Using Jason and NetLogo

    Directory of Open Access Journals (Sweden)

    Wulfrano Arturo Luna-Ramirez

    2018-04-01

    Full Text Available An agent is an autonomous computer system situated in an environment to fulfill a design objective. Multi-Agent Systems aim to solve problems in a flexible and robust way by assembling sets of agents interacting in cooperative or competitive ways for the sake of possibly common objectives. Multi-Agent Systems have been applied to several domains ranging from many industrial sectors, e-commerce, health and even entertainment. Agent-Based Modeling, a sort of Multi-Agent Systems, is a technique used to study complex systems in a wide range of domains. A natural or social system can be represented, modeled and explained through a simulation based on agents and interactions. Such a simulation can comprise a variety of agent architectures like reactive and cognitive agents. Despite cognitive agents being highly relevant to simulate social systems due their capability of modelling aspects of human behaviour ranging from individuals to crowds, they still have not been applied extensively. A challenging and socially relevant domain are the Disaster-Rescue simulations that can benefit from using cognitive agents to develop a realistic simulation. In this paper, a Multi-Agent System applied to the Disaster-Rescue domain involving cognitive agents based on the Belief–Desire–Intention architecture is presented. The system aims to bridge the gap in combining Agent-Based Modelling and Multi-Agent Systems approaches by integrating two major platforms in the field of Agent-Based Modeling and Belief-Desire Intention multi-agent systems, namely, NetLogo and Jason.

  20. Identifikasi Waste pada Produksi Kayu Lapis dengan Pendekatan Lean Manufacturing untuk Meningkatkan Kualitas Proses Produksi (Studi Kasus : PT Sumber Mas Indah Plywood

    Directory of Open Access Journals (Sweden)

    Miftahus Shomad

    2017-03-01

    Full Text Available This research aimed at identifying the wastes of plywood production in PT Sumber MasIndah Plywood. Results were then utilized to determine methods in reducing wastes. Theidentification of waste was carried out using lean manufacturing approach. The data werecollected from manufacturer records, study to determine processing time, as well as interviewand quisioners which were distributed to workers in each department. Big picture mapping andvalue stream mapping tools (VALSAT were then utilized to process the data. Results ofanalyses using big picture mapping showed that total production lead time was 438,8 minutes,with 235,97 minutes of them were value added activities; and 27 days of total information leadtime. Workshop waste analyses resulted in the highest waste generated during plywoodproduction process. Those were 133 waiting time (delay, 113 defect and 78 excessivetransportation. Further analyses using VALSAT showed three methods to identify the data inmore detail, namely process activity mapping (PAM, supply chain response matrix (SCRMand quality filter mapping (QFM. Results from PAM method revealed 125 activities duringproduction, consist 62 value added activities, 33 necessary but non value added activities and 30non value added activities. While results from SCRM showed the average 22,63 days of totalorder fulfillment process comprised of 4,13 days of total physical stock and 18,5 days of totallead time. QFM result showed ratio of scrap defect reject 0,4% and ratio of scrap defect UTY3,46%. In general waste in plywood production at PT Sumber Mas Indah Plywood wasgenerated from worker, material, machinery, methods and environment. One of the ways toimprove it is by applying pull system (Kanban

  1. Mas-related G protein coupled receptor-X2: A potential new target for modulating mast cell-mediated allergic and inflammatory diseases.

    Science.gov (United States)

    Ali, Hydar

    2016-12-01

    Mast cells (MCs) are tissue resident immune cells that are best known for their roles in allergic and inflammatory diseases. In addition to the high affinity IgE receptor (FcεRI), MCs express numerous G protein coupled receptors (GPCRs), which are the most common targets of drug therapy. Neurokinin 1 receptor (NK-1R) is expressed on MCs and contributes to IgE and non-IgE-mediated responses in mice. Although NK-1R antagonists are highly effective in modulating experimental allergic and inflammatory responses in mice they lack efficacy in humans. This article reviews recent findings that demonstrate that while neuropeptides (NPs) activate murine MCs via NK-1R and Mas related G protein coupled receptor B2 (MrgprB2), they activate human MCs via Mas-related G protein coupled receptor X2 (MRGPRX2). Interestingly, conventional NK-1R antagonists have off-target activity against mouse MrgprB2 but not human MRGPRX2. These findings suggest that the failure to translate studies with NK-1R antagonists from in vivo mouse studies to the clinic likely reflects their lack of effect on human MRGPRX2. A unique feature of MRGPRX2 that distinguishes it from other GPCRs is that it is activated by a diverse group of ligands that include; neuropeptides, cysteine proteases, antimicrobial peptides and cationic proteins released from activated eosinophils. Thus, the development of small molecule MRGPRX2-specific antagonists or neutralizing antibodies may provide new targets for the treatment of MC-mediated allergic and inflammatory diseases.

  2. Transitions in Al Coordination during Gibbsite Crystallization Using High-Field 27 Al and 23 Na MAS NMR Spectroscopy

    Energy Technology Data Exchange (ETDEWEB)

    Hu, Jian Zhi [Pacific Northwest National Laboratory, Richland, Washington 99354, United States; Zhang, Xin [Pacific Northwest National Laboratory, Richland, Washington 99354, United States; Jaegers, Nicholas R. [Pacific Northwest National Laboratory, Richland, Washington 99354, United States; Washington State University, Pullman, Washington 99164, United States; Wan, Chuan [Pacific Northwest National Laboratory, Richland, Washington 99354, United States; Graham, Trent R. [Pacific Northwest National Laboratory, Richland, Washington 99354, United States; Washington State University, Pullman, Washington 99164, United States; Hu, Mary [Pacific Northwest National Laboratory, Richland, Washington 99354, United States; Pearce, Carolyn I. [Pacific Northwest National Laboratory, Richland, Washington 99354, United States; Felmy, Andrew R. [Pacific Northwest National Laboratory, Richland, Washington 99354, United States; Washington State University, Pullman, Washington 99164, United States; Clark, Sue B. [Pacific Northwest National Laboratory, Richland, Washington 99354, United States; Washington State University, Pullman, Washington 99164, United States; Rosso, Kevin M. [Pacific Northwest National Laboratory, Richland, Washington 99354, United States

    2017-11-30

    Mechanisms of nucleation and growth of Al hydroxides such as gibbsite from aqueous solution, particularly in highly alkaline conditions, remain poorly understood. In this work, quantitative 27Al and 22Na MAS NMR experiments were conducted on solid samples extracted from the crystallization of gibbsite from an amorphous aluminum hydroxide gel precursor. The use of high magnetic field and fast sample spinning allowed transitional tetrahedral (AlT) and pentahedral (AlP) aluminum species to be observed along with the octahedral aluminum (AlO) that dominates the gibbsite product. Low-coordinated Al species could be detected at concentrations as low as 0.1% of the total Al sites. It is established that (a) AlT and AlP coexist on the surface of growing gibbsites even with a combined percentage over the total Al sites of less than 1%; (b) Different synthesis methods generate gibbsite with varying amounts of low-coordinated Al; (c) the amorphous gel precursor contains a significant amount of low-coordinated Al sites with AO: AlP: AlT ratios of approximately 4:2:1; (d) upon hydration, the external, low-coordinated Al sites become six-fold coordinated by interacting with the oxygen in H2O and the 27Al MAS NMR peak position shifts to that for the AlO sites; (e) gibbsite with increased long range order is synthesized over longer times by gradually incorporating residual AlP and AlT sites into octahedrally-coordinated AlO sites; (f) trace Na is predominantly a surface species on gibbsite particles. These findings provide a basis for understanding the gibbsite crystallization mechanism, along with a general means of characterizing gibbsite surface properties that are of equal importance for understanding related processes such as dissolution behavior.

  3. High, but not low, exercise volume shifts the balance of renin-angiotensin system toward ACE2/Mas receptor axis in skeletal muscle in obese rats.

    Science.gov (United States)

    Frantz, Eliete Dalla Corte; Giori, Isabele Gomes; Machado, Marcus Vinícius; Magliano, D'Angelo Carlo; Freitas, Fernanda Marques; Andrade, Mariana Sodré Boêta; Vieira, Aline Bomfim; Nóbrega, Antonio Claudio Lucas; Tibiriçá, Eduardo

    2017-10-01

    Metabolic syndrome is a cluster of metabolic risk factors that is linked to central obesity, elevated blood pressure, insulin resistance (IR), and dyslipidemia, where the renin-angiotensin system (RAS) may provide a link among them. This study aimed to evaluate volume exercise effects comparing low vs. high volume of chronic aerobic exercise on RAS axes in skeletal muscle in a diet-induced obesity (DIO) rat model. For this, male Wistar-Kyoto rats were fed a standard chow (SC) diet or a high-fat (HF) diet for 32 wk. Animals receiving the HF diet were randomly divided into low exercise volume (LEV, 150 min/wk) and high exercise volume (HEV, 300 min/wk) at the 20th week. After 12 wk of aerobic treadmill training, the body mass and composition, blood pressure, glucose and lipid metabolism, RAS axes, insulin signaling, and inflammatory pathway were performed. HEV slowed the body mass gain, reduced intra-abdominal fat pad and leptin levels, improved total and peripheral body composition and inflammatory cytokine, reduced angiotensin II type 1 receptor expression, and increased Mas receptor protein expression compared with the HF animals. Sedentary groups (SC and HF) presented lower time to exhaustion and maximal velocity compared with the LEV and HEV groups. Both exercise training groups showed reduced resting systolic blood pressure and heart rate, improved glucose tolerance, IR, insulin signaling, and lipid profile. We conclude that the HEV, but not LEV, shifted the balance of RAS toward the ACE2/Mas receptor axis in skeletal muscle, presenting protective effects against the DIO model. Copyright © 2017 the American Physiological Society.

  4. CP/MAS 13C NMR characterization of the isomeric states and intermolecular packing in tris(8-hydroxyquinoline) aluminum(III) (Alq3).

    Science.gov (United States)

    Kaji, Hironori; Kusaka, Yasunari; Onoyama, Goro; Horii, Fumitaka

    2006-04-05

    The isomeric states and intermolecular packing of tris(8-hydroxyquinoline) aluminum(III) (Alq(3)) in the alpha-, gamma-, and delta-crystalline forms and in the amorphous state, which are important for understanding the light-emitting and electron-transport properties, have been analyzed by CP/MAS (13)C NMR. This simple NMR experiment shows that the isomeric state of alpha- and amorphous Alq(3) is meridional, whereas that of gamma- and delta-Alq(3) is facial. In the amorphous Alq(3), the inclusion of facial isomers has been under debate. Our experiments show that meridional isomers are dominant in the amorphous Alq(3), although the existence of facial isomers cannot be completely denied. The local structure of amorphous Alq(3) is similar to that of alpha-Alq(3) and is significantly different from those of gamma- and delta-Alq(3). Among these Alq(3) samples, the effect of intermolecular interaction is not found only for gamma-Alq(3). This finding can explain the good solvent solubility of gamma-Alq(3), compared with the other crystalline forms. It is also shown that the structures are locally disordered not only for amorphous Alq(3) but also for alpha-Alq(3), although clear X-ray diffraction peaks are observed for alpha-Alq(3). In contrast, the local structures of gamma- and delta-Alq(3) are well defined. A clear relation is found between the spectral patterns of CP/MAS (13)C NMR and the fluorescence wavelengths; the samples, which consist of facial isomers, show blue-shifted fluorescence compared with those of meridionals.

  5. Solid state CP/MAS 13C n.m.r. analysis of particle size and density fractions of soil incubated with uniformly labelled 13C-glucose

    International Nuclear Information System (INIS)

    Baldock, J.A.; Oades, J.M.

    1990-01-01

    A soil incubated for 34 days in the absence (control) and presence (treated) of uniformly labelled 13 C-glucose was dispersed using an ultrasonic probe and fractionated by sedimentation in water and a polytungstate solution of density 2.0 Mg m -3 . Solid state CP/MAS 13 C n.m.r. (cross polarization/magic angle spinning 13 C nuclear magnetic resonance) spectroscopy was used to characterize the chemical structure of the native soil organic carbon and the residual substrate carbon in the fractions of the control and treated soils. To obtain quantitative results it was essential to determine the spin lattice relaxation time in a rotating frame of the individual carbon types in the spectra as the relaxation behaviour of the native organic material in the clay fraction was different from that of the residual substrate carbon. The residual substrate carbon was found to accumulate in predominantly alkyl and O-alkyl structures in both fractions. However, significant amounts of acetal and carboxyl carbon were also observed in the clay fraction. Little if any aromatic or phenolic carbon was synthesized by the soil microorganisms utilizing substrate carbon. Dipolar dephasing CP/MAS 13 C n.m.r. experiments were also performed and allowed the proportion of each type of carbon which was protonated and nonprotonated to be estimated. Essentially all of the O-alkyl and acetal carbon, 25-40% of the aromatic carbon and 66-80% of the alkyl carbon was protonated in the fractions isolated from the treated soil. 24 refs., 4 figs., 2 tabs

  6. Computerized tomography in the Community of Madrid. Techniques used in the studies

    International Nuclear Information System (INIS)

    Ruiz Sanz, S.; Calzado, S.; Rodriguez, R.; Melchor, M.

    1994-01-01

    The main object of the present work was the knowledge of technique and geometrical factors most frequently used to perform computed tomography (CT) examinations in health centres of the Community of Madrid. A sample of actual examinations to patient in several CT rooms was taken. In this way up to about 1500 individual values of technique factors data (kVp, mAs, slice thickness, couch increment and number of slices) were recorded. Mean values and ranges of such parameters are given for each examination type. Mean values for each scanner are analysed and the average mAs are compared to those recommended by the manufacturer for two types of examination (head and abdomen). The number of ''series of slices'' used to perform the examination was also analysed. (Author) 4 refs

  7. Veikala „Dīvāni un Dīvāni” reklāmas analīze un pilnveidošanas iespējas.

    OpenAIRE

    Alsiņa, Madara

    2013-01-01

    Bakalaura darba tēma „Veikala „Dīvāni un Dīvāni” reklāmas analīze un pilnveidošanas iespējas”. Bakalaura darba mērķis ir, pamatojoties uz teorijā gūtajām atziņām par reklāmu, izanalizēt veikala „Dīvāni un Dīvāni” reklāmas pasākumus, to stiprās un vājās puses, novērtēt reklāmas komunikatīvo efektivitāti, kā arī izstrādāt priekšlikumus veikala „Dīvāni un Dīvāni” reklāmas pilnveidošanai. Pirmajā darba daļā tiek apskatīti reklāmas kā mārketinga komunikāciju elementa teorētiskie aspekti – ...

  8. Industrial technique

    International Nuclear Information System (INIS)

    Jabsen, F.S.

    1975-01-01

    An illustrative embodiment of the invention discloses a technique for disassembling a nuclear reactor fuel element without destroying the individual fuel pins and other structural components from which the element is assembled. A traveling bridge and trolley that span a water-filled spent fuel storage pool support a strongback. The strongback is under water and provides a working surface on which the spent fuel element is placed for inspection and for the manipulation that is associated with disassembly and assembly. To remove, in a non-destructive manner, the grids that hold the fuel pins in the proper relative positions within the element, bars are inserted through apertures in the grids with the aid of special tools. These bars are rotated to flex the adjacent grid walls and, in this way relax the physical engagement between protruding portions of the grid walls and the associated fuel pins. With the grid structure so flexed to relax the physical grip on the individual fuel pins, these pins can be withdrawn for inspection or replacement as necessary without imposing a need to destroy fuel element components. (U.S.)

  9. Avaliação do desempenho de sistemas alagados construídos de escoamento horizontal subsuperficial tratando efluente de reator UASB, com base em quatro anos de monitoramento

    Directory of Open Access Journals (Sweden)

    Jocilene Ferreira Costa

    Full Text Available RESUMO Um sistema composto por um reator anaeróbio tipo upflow anaerobic sludge blanket (UASB, seguido de um sistema de alagados construídos (SAC de escoamento horizontal subsuperficial compreendendo duas unidades em paralelo (50 habitantes cada, foi avaliado para o tratamento de águas residuárias geradas na cidade de Belo Horizonte, Minas Gerais, Brasil. Uma unidade foi plantada com Typha latifolia e a outra não foi vegetada. Amostras semanais do efluente do reator UASB e do efluente das unidades do SAC foram avaliadas por um período de quatro anos de operação do sistema. Nas taxas de aplicação praticadas (média de 0,11 m3.m-2.d-1, o efluente final apresentou excelente qualidade em termos de matéria orgânica e sólidos suspensos, mas baixa capacidade de remoção de nitrogênio. Os valores médios de concentração no efluente das unidades plantadas e não plantadas foram, respectivamente, demanda bioquímica de oxigênio: 25 e 23 mg.L-1; demanda química de oxigênio: 50 e 55 mg.L-1; sólidos suspensos totais: 10 e 8 mg.L-1; nitrogênio Kjeldahl total: 30 e 31 mg.L-1; e nitrogênio amoniacal: 27 e 28 mg.L-1. Não se observou diferença significativa entre as concentrações efluentes das unidades plantada e não plantada para a maioria dos constituintes investigados.

  10. Authenticity study of Phyllanthus species by NMR and FT-IR techniques coupled with chemometric methods

    International Nuclear Information System (INIS)

    Santos, Maiara S.; Pereira-Filho, Edenir R.; Ferreira, Antonio G.; Boffo, Elisangela F.; Figueira, Glyn M.

    2012-01-01

    The importance of medicinal plants and their use in industrial applications is increasing worldwide, especially in Brazil. Phyllanthus species, popularly known as 'quebra-pedras' in Brazil, are used in folk medicine for treating urinary infections and renal calculus. This paper reports an authenticity study, based on herbal drugs from Phyllanthus species, involving commercial and authentic samples using spectroscopic techniques: FT-IR, 1 H HR-MAS NMR and 1 H NMR in solution, combined with chemometric analysis. The spectroscopic techniques evaluated, coupled with chemometric methods, have great potential in the investigation of complex matrices. Furthermore, several metabolites were identified by the NMR techniques. (author)

  11. Authenticity study of Phyllanthus species by NMR and FT-IR Techniques coupled with chemometric methods

    Directory of Open Access Journals (Sweden)

    Maiara S. Santos

    2012-01-01

    Full Text Available The importance of medicinal plants and their use in industrial applications is increasing worldwide, especially in Brazil. Phyllanthus species, popularly known as "quebra-pedras" in Brazil, are used in folk medicine for treating urinary infections and renal calculus. This paper reports an authenticity study, based on herbal drugs from Phyllanthus species, involving commercial and authentic samples using spectroscopic techniques: FT-IR, ¹H HR-MAS NMR and ¹H NMR in solution, combined with chemometric analysis. The spectroscopic techniques evaluated, coupled with chemometric methods, have great potential in the investigation of complex matrices. Furthermore, several metabolites were identified by the NMR techniques.

  12. Authenticity study of Phyllanthus species by NMR and FT-IR techniques coupled with chemometric methods

    Energy Technology Data Exchange (ETDEWEB)

    Santos, Maiara S.; Pereira-Filho, Edenir R.; Ferreira, Antonio G. [Universidade Federal de Sao Carlos (UFSCAR), SP (Brazil). Dept. de Quimica; Boffo, Elisangela F. [Universidade Federal da Bahia (UFBA), Salvador, BA (Brazil). Inst. de Quimica; Figueira, Glyn M., E-mail: maiarassantos@yahoo.com.br [Universidade Estadual de Campinas (UNICAMP), Campinas, SP (Brazil). Centro Pluridisciplinar de Pesquisas Quimicas, Biologicas e Agricolas

    2012-07-01

    The importance of medicinal plants and their use in industrial applications is increasing worldwide, especially in Brazil. Phyllanthus species, popularly known as 'quebra-pedras' in Brazil, are used in folk medicine for treating urinary infections and renal calculus. This paper reports an authenticity study, based on herbal drugs from Phyllanthus species, involving commercial and authentic samples using spectroscopic techniques: FT-IR, {sup 1}H HR-MAS NMR and {sup 1}H NMR in solution, combined with chemometric analysis. The spectroscopic techniques evaluated, coupled with chemometric methods, have great potential in the investigation of complex matrices. Furthermore, several metabolites were identified by the NMR techniques. (author)

  13. Authenticity study of Phyllanthus species by NMR and FT-IR techniques coupled with chemometric methods

    Energy Technology Data Exchange (ETDEWEB)

    Santos, Maiara S.; Pereira-Filho, Edenir R.; Ferreira, Antonio G. [Universidade Federal de Sao Carlos (UFSCAR), SP (Brazil). Dept. de Quimica; Boffo, Elisangela F. [Universidade Federal da Bahia (UFBA), Salvador, BA (Brazil). Inst. de Quimica; Figueira, Glyn M., E-mail: maiarassantos@yahoo.com.br [Universidade Estadual de Campinas (UNICAMP), Campinas, SP (Brazil). Centro Pluridisciplinar de Pesquisas Quimicas, Biologicas e Agricolas

    2012-07-01

    The importance of medicinal plants and their use in industrial applications is increasing worldwide, especially in Brazil. Phyllanthus species, popularly known as 'quebra-pedras' in Brazil, are used in folk medicine for treating urinary infections and renal calculus. This paper reports an authenticity study, based on herbal drugs from Phyllanthus species, involving commercial and authentic samples using spectroscopic techniques: FT-IR, {sup 1}H HR-MAS NMR and {sup 1}H NMR in solution, combined with chemometric analysis. The spectroscopic techniques evaluated, coupled with chemometric methods, have great potential in the investigation of complex matrices. Furthermore, several metabolites were identified by the NMR techniques. (author)

  14. Techniques de combustion Combustin Techniques

    Directory of Open Access Journals (Sweden)

    Perthuis E.

    2006-11-01

    Full Text Available L'efficacité d'un processus de chauffage par flamme est étroitement liée à la maîtrise des techniques de combustion. Le brûleur, organe essentiel de l'équipement de chauffe, doit d'une part assurer une combustion complète pour utiliser au mieux l'énergie potentielle du combustible et, d'autre part, provoquer dans le foyer les conditions aérodynamiques les plus propices oux transferts de chaleur. En s'appuyant sur les études expérimentales effectuées à la Fondation de Recherches Internationales sur les Flammes (FRIF, au Groupe d'Étude des Flammes de Gaz Naturel (GEFGN et à l'Institut Français du Pétrole (IFP et sur des réalisations industrielles, on présente les propriétés essentielles des flammes de diffusion aux combustibles liquides et gazeux obtenues avec ou sans mise en rotation des fluides, et leurs répercussions sur les transferts thermiques. La recherche des températures de combustion élevées conduit à envisager la marche à excès d'air réduit, le réchauffage de l'air ou son enrichissement à l'oxygène. Par quelques exemples, on évoque l'influence de ces paramètres d'exploitation sur l'économie possible en combustible. The efficiency of a flame heating process is closely linked ta the mastery of, combustion techniques. The burner, an essential element in any heating equipment, must provide complete combustion sa as to make optimum use of the potential energy in the fuel while, at the same time, creating the most suitable conditions for heat transfers in the combustion chamber. On the basis of experimental research performed by FRIF, GEFGN and IFP and of industrial achievements, this article describesthe essential properties of diffusion flames fed by liquid and gaseous fuels and produced with or without fluid swirling, and the effects of such flames on heat transfers. The search for high combustion temperatures means that consideration must be given to operating with reduced excess air, heating the air or

  15. Metallic nature of Sn{sub 1-} {sub x} Sb {sub x} O{sub 2{+-}} {sub {delta}} (x=0.0, 0.10 and 0.20) mixed oxides: Probed by {sup 119}Sn MAS NMR

    Energy Technology Data Exchange (ETDEWEB)

    Jayakumar, O.D. [Chemistry Division, Bhabha Atomic Research Centre, Trombay, Mumbai 400085 (India)]. E-mail: ddjaya@apsara.barc.ernet.in; Sudarsan, V. [Chemistry Division, Bhabha Atomic Research Centre, Trombay, Mumbai 400085 (India); Kulshreshtha, S.K. [Chemistry Division, Bhabha Atomic Research Centre, Trombay, Mumbai 400085 (India)

    2007-04-15

    Antimony doped SnO{sub 2} samples were prepared by co-precipitation method and characterized by X-ray diffraction (XRD), {sup 119}Sn magic angle spinning nuclear magnetic resonance (MAS NMR) and variable temperature electrical conductivity measurements. Based on {sup 119}Sn MAS NMR measurements on these samples, it was established that only above 400 deg. C, the structural units of antimony and tin interacts, resulting in the metallic nature. Metallic behavior of the high-temperature heated samples was further confirmed by the variable temperature electrical conductivity measurements.

  16. De masonería, control y otras lealtades fraternales: el rescate de Porfirio Díaz por un hermano masón

    Directory of Open Access Journals (Sweden)

    Guillermo de los Reyes Heredia

    2015-01-01

    Full Text Available En este artículo se explora el papel que jugó Porfirio Díaz dentro de la masonería y su relación con dichainstitución. Se analiza una de las historias que comprueban que Díaz logró ciertos beneficios gracias a suafiliación masónica desde antes que fuera presidente de México. Esta historia narra la manera en que Díazlogró entrar de contrabando a México con la ayuda de un hermano masón en 1876, después de su breve exilioen Nuevo Orleans a bordo del buque de vapor, “City of Havana”. En un principio se pensaba que ésta erasimplemente una leyenda más del folklore que envuelve a la masonería. Sin embargo, dos testimonios, ambosde masones que iban en el mismo barco ratifican la historia que incluso el mismo historiador de la masoneríanorteamericana, William Deslow, catalogaba como un incidente, “no verificado.”Asimismo, se describe cómo Díaz promovió la unificación de las logias del rito escocés en unainstitución que se llamó La Gran Dieta Simbólica. La razón principal por la cual Díaz promovió talunificación, como se afirma en este artículo, fue para llevar a cabo su plan de pacificación nacional. Díazsabía que tenía que obtener el control de la masonería para evitar que ésta le causara problemas para lograr elorden y progreso que caracterizó a su gobierno. Por tal motivo, el dictador siempre vigiló que ni la masonería,ni cualquier otra institución que hubiera podido tener cierta influencia en la sociedad estuvieran fuera de sucontrol.

  17. Mas Roig Mini-Grid

    DEFF Research Database (Denmark)

    Salas, Pep; Guerrero, Josep M.

    2014-01-01

    This paper presents a microgrid project, named Basic Distributed Nodes (NoBaDis), deployed in a stand-alone farm in Girona, Spain. NoBaDis is based on intensive use of information to maximize the penetration of renewable energy through two main strategies: anticipation and opportunity. The loads...... are classified in four different types according to priority and are controlled by intelligent sockets interconnected in a mesh network. Each socket measures the main electric parameters, communicates to the local computer bidirectionality by using ZigBee communications, and is able to switch on/off the loads....... The power system is composed by low-density energy sources (renewable) and high-density cogeneration engine. These elements can be interconnected in two different configurations to test different scenarios. After 5 years of operation, the results has shown the importance of real-time management system...

  18. Healthcare benefits linked with Below Poverty Line registration in India: Observations from Maharashtra Anaemia Study (MAS [version 1; referees: 2 approved

    Directory of Open Access Journals (Sweden)

    Anand Ahankari

    2017-01-01

    Full Text Available A 2015 Lancet paper by Patel et al. on healthcare access in India comprehensively discussed national health programmes where some benefits are linked with the country’s Below Poverty Line (BPL registration scheme. BPL registration aims to support poor families by providing free/subsidised healthcare. Technical issues in obtaining BPL registration by poor families have been previously reported in the Indian literature; however there are no data on family assets of BPL registrants. Here, we provide evidence of family-level assets among BPL registration holders (and non-BPL households using original research data from the Maharashtra Anaemia Study (MAS.   Social and health data from 287 pregnant women and 891 adolescent girls (representing 1178 family households across 34 villages in Maharashtra state, India, were analysed. Several assets were shown to be similarly distributed between BPL and non-BPL households; a large proportion of families who would probably be eligible were not registered, whereas BPL-registered families often had significant assets that should not make them eligible. This is likely to be the first published evidence where asset distribution such as agricultural land, housing structures and livestock are compared between BPL and non-BPL households in a rural population. These findings may help planning BPL administration to allocate health benefits equitably, which is an integral part of national health programmes.

  19. Loģistikas pārvaldības sistēmas izstrāde, izmantojot Spring un Hibernate ietvarus

    OpenAIRE

    Ziļickis, Intars

    2009-01-01

    Kvalifikācijas darbā “Loģistikas pārvaldības sistēmas izstrāde, izmantojot Spring un Hibernate ietvarus” ir aprakstīta pogrammatūras izstrāde. Ir iekļauti programmatūras prasību un projektējumu aprakstoši dokumenti, dati par izstrādē izmantotajiem rīkiem un tehnoloģijām, kā arī aprakstīta programmatūras kvalitātes nodrošināšana, testēšana un darbietilpības aprēķins. Loģistikas pārvaldības sistēma ir paredzēta kompānijām, kas nodarbojas ar loģistikas pārvedumu izpildi, vieglākai pārve...

  20. Žurnāla SHAPE pārpozicionēšanas stratēģijas problēmas un risinājumi.

    OpenAIRE

    Nikodemusa, Zane

    2013-01-01

    Maģistra darba tēma ir „Žurnāla SHAPE pārpozicionēšanas stratēģijas problēmas un risinājumi”. Maģistra darba mērķis ir izpētīt žurnāla SHAPE pārpozicionēšanas stratēģiju, tās ieguvumus un zaudējumus no uzņēmuma skatu punkta, kā arī ietekmējošos faktorus un risinājumus turpmākai tirgus pozīcijas stiprināšanai. Darba gaitā autore izmanto dažādas informācijas apkopošanas un analīzes metodes. Teorētiskās daļas veidošanai darba autore izmantoja literatūras referatīvās analīzes metodi. Informāci...

  1. Numerical design of RNnν symmetry-based RF pulse schemes for recoupling and decoupling of nuclear spin interactions at high MAS frequencies

    International Nuclear Information System (INIS)

    Herbst, Christian; Herbst, Jirada; Leppert, Joerg; Ohlenschlaeger, Oliver; Goerlach, Matthias; Ramachandran, Ramadurai

    2009-01-01

    An approach for the efficient implementation of RN n ν symmetry-based pulse schemes that are often employed for recoupling and decoupling of nuclear spin interactions in biological solid state NMR investigations is demonstrated at high magic-angle spinning frequencies. RF pulse sequences belonging to the RN n ν symmetry involve the repeated application of the pulse sandwich {R φ R -φ }, corresponding to a propagator U RF = exp(-i4φI z ), where φ = πν/N and R is typically a pulse that rotates the nuclear spins through 180 o about the x-axis. In this study, broadband, phase-modulated 180 o pulses of constant amplitude were employed as the initial 'R' element and the phase-modulation profile of this 'R' element was numerically optimised for generating RN n ν symmetry-based pulse schemes with satisfactory magnetisation transfer characteristics. At representative MAS frequencies, RF pulse sequences were implemented for achieving 13 C- 13 C double-quantum dipolar recoupling and through bond scalar coupling mediated chemical shift correlation and evaluated via numerical simulations and experimental measurements. The results from these investigations are presented here

  2. Recoupling and decoupling of nuclear spin interactions at high MAS frequencies: numerical design of CNnν symmetry-based RF pulse schemes

    International Nuclear Information System (INIS)

    Herbst, Christian; Herbst, Jirada; Kirschstein, Anika; Leppert, Joerg; Ohlenschlaeger, Oliver; Goerlach, Matthias; Ramachandran, Ramadurai

    2009-01-01

    The CN n ν class of RF pulse schemes, commonly employed for recoupling and decoupling of nuclear spin interactions in magic angle spinning solid state NMR studies of biological systems, involves the application of a basic 'C' element corresponding to an RF cycle with unity propagator. In this study, the design of CN n ν symmetry-based RF pulse sequences for achieving 13 C- 13 C double-quantum dipolar recoupling and through bond scalar coupling mediated 13 C- 13 C chemical shift correlation has been examined at high MAS frequencies employing broadband, constant-amplitude, phase-modulated basic 'C' elements. The basic elements were implemented as a sandwich of a small number of short pulses of equal duration with each pulse characterised by an RF phase value. The phase-modulation profile of the 'C' element was optimised numerically so as to generate efficient RF pulse sequences. The performances of the sequences were evaluated via numerical simulations and experimental measurements and are presented here

  3. Effects of solvent concentration and composition on protein dynamics: 13C MAS NMR studies of elastin in glycerol-water mixtures.

    Science.gov (United States)

    Demuth, Dominik; Haase, Nils; Malzacher, Daniel; Vogel, Michael

    2015-08-01

    We use (13)C CP MAS NMR to investigate the dependence of elastin dynamics on the concentration and composition of the solvent at various temperatures. For elastin in pure glycerol, line-shape analysis shows that larger-scale fluctuations of the protein backbone require a minimum glycerol concentration of ~0.6 g/g at ambient temperature, while smaller-scale fluctuations are activated at lower solvation levels of ~0.2 g/g. Immersing elastin in various glycerol-water mixtures, we observe at room temperature that the protein mobility is higher for lower glycerol fractions in the solvent and, thus, lower solvent viscosity. When decreasing the temperature, the elastin spectra approach the line shape for the rigid protein at 245 K for all studied samples, indicating that the protein ceases to be mobile on the experimental time scale of ~10(-5) s. Our findings yield evidence for a strong coupling between elastin fluctuations and solvent dynamics and, hence, such interaction is not restricted to the case of protein-water mixtures. Spectral resolution of different carbon species reveals that the protein-solvent couplings can, however, be different for side chain and backbone units. We discuss these results against the background of the slaving model for protein dynamics. Copyright © 2015 Elsevier B.V. All rights reserved.

  4. Activation of mas-related G-protein-coupled receptors by the house dust mite cysteine protease Der p1 provides a new mechanism linking allergy and inflammation.

    Science.gov (United States)

    Reddy, Vemuri B; Lerner, Ethan A

    2017-10-20

    Cysteine and serine proteases function via protease-activated and mas-related G-protein-coupled receptors (Mrgprs) to contribute to allergy and inflammation. Der p1 is a cysteine protease and major allergen from the house dust mite and is associated with allergic rhinitis and allergic asthma. Der p1 activates protease-activated receptor 2 and induces the release of the pro-inflammatory cytokine IL-6 from cells. However, the possibility that Der p1 acts on Mrgprs has not been considered. We report here that ratiometric calcium imaging reveals that Der p1 activates the human receptor MRGPRX1 and the mouse homolog MrgprC11, implicated previously in itch. Der p1 cleavage of N-terminal receptor peptides followed by site-directed mutagenesis of the cleavage sites links receptor activation to specific amino acid residues. Der p1 also induced the release of IL-6 from heterologous cells expressing MRGPRX1. In summary, activation of Mrgprs by the allergen Der p1 may contribute to inflammation. © 2017 by The American Society for Biochemistry and Molecular Biology, Inc.

  5. Glycerin-Induced Conformational Changes in Bombyx mori Silk Fibroin Film Monitored by (13)C CP/MAS NMR and ¹H DQMAS NMR.

    Science.gov (United States)

    Asakura, Tetsuo; Endo, Masanori; Hirayama, Misaki; Arai, Hiroki; Aoki, Akihiro; Tasei, Yugo

    2016-09-09

    In order to improve the stiff and brittle characteristics of pure Bombyx mori (B. mori) silk fibroin (SF) film in the dry state, glycerin (Glyc) has been used as a plasticizer. However, there have been very limited studies on the structural characterization of the Glyc-blended SF film. In this study, (13)C Cross Polarization/Magic Angle Spinning nuclear magnetic resonance (CP/MAS NMR) was used to monitor the conformational changes in the films by changing the Glyc concentration. The presence of only 5 wt % Glyc in the film induced a significant conformational change in SF where Silk I* (repeated type II β-turn and no α-helix) newly appeared. Upon further increase in Glyc concentration, the percentage of Silk I* increased linearly up to 9 wt % Glyc and then tended to be almost constant (30%). This value (30%) was the same as the fraction of Ala residue within the Silk I* form out of all Ala residues of SF present in B. mori mature silkworm. The ¹H DQMAS NMR spectra of Glyc-blended SF films confirmed the appearance of Silk I* in the Glyc-blended SF film. A structural model of Glyc-SF complex including the Silk I* form was proposed with the guidance of the Molecular Dynamics (MD) simulation using ¹H-¹H distance constraints obtained from the ¹H Double-Quantum Magic Angle Spinning (DQMAS) NMR spectra.

  6. 1904-1905 Rus-Japon Savaşı’nın Japon Manga kitaplarına yansıması

    OpenAIRE

    DAVARCI, Yasemin

    2015-01-01

          Bu çalışmada, 1904-1905 Rus-Japon Savaşının, Japon manga kitaplarına yansıması ele alınmıştır. Japonya’nın Rusya gibi büyük bir gücü yenerek dünya sahnesinde önemli güçler arasına girmesinde dönüm noktalarından biri olan bu savaşın, Japon toplumuna mangalar aracılığı ile nasıl yansıtıldığı incelenmiştir. Japon manga sanatçılarının Rus-Japon Savaşına bakış açılarının da görülebileceği bu çalışmada; İngilizce, Japonca ve Türkçe akademik kitap v...

  7. A MAS NMR and DRIFT study of the Ga species in Ga/H-ZSM5 catalysts and their effect on propane ammoxidation

    Energy Technology Data Exchange (ETDEWEB)

    Pal, P. [Indian Inst. of Petroleum, Dehradun (India). Catalysis Division; Quartararo, J. [Liverpool Univ., Liverpool (United Kingdom). Leverhulme Centre for Innovative Catalysis, Dept. of Chemistry; Abd Hamid, S.B. [Malaya Univ., Postgraduate School, Bangunan (Malaysia); Derouane, E.G. [Algarve Univ., Faro (Portugal). Faculdade de Ciencias e Tecnologia; Vedrine, J.C. [Laboratoire de Physico-Chimie des Surface, Paris (France). Faculdade de Ciencias e Tecnologia; Magusin, P.C.M.M.; Anderson, B.G. [Eindhoven Univ. of Technology, Eindhoven (Netherlands). Schuit Institute of Catalysis

    2005-07-01

    This paper presents the results of a study that sought information about the nature and environment of the gallium (Ga) species in Ga/H-ZSM5 zeolites following H{sub 2}-O{sub 2} redox treatments applied during their activation by use of magic-angle spinning (MAS) {sup 71}Ga, {sup 27}Al, and {sup 29}Si NMR spectroscopy (Ga coordination) complemented by diffuse reflectance FT IR (DRIFT) spectroscopy (Bronsted acidity). This information was then correlated with their catalytic behavior for the ammoxidation of propane. Ga species were observed in several environments: octahedrally coordinated gallium in small Ga{sub 2}O{sub 3} particles at the external surface of the zeolite crystals; octahedrally coordinated gallium in GaO(OH) or related species; and tetrahedrally coordinated gallium in cationic-exchange positions inside the zeolite. Redox (H{sub 2}-O{sub 2}) cycles promote the migration of gallium from the GaO(OH) or Ga{sub 2}O{sub 3} species at the external surface of the zeolite crystals to cationic-exchange sites within the zeolite channels. It was concluded that the redox treatment had a beneficial effect on its catalytic performance for the ammoxidation of propane, which occurs via a bifunctional mechanism. The main product was acetonitrile at high gallium and aluminium contents. It was suggested that higher yields in acrylonitrile could be obtained through Ga-modified zeolites with a higher gallium and lower aluminium content. 22 refs., 1 tab., 6 figs.

  8. Kukuļņemšanas un kukuļdošanas kvalifikācijas problēmas

    OpenAIRE

    Brauere, Jolanta

    2010-01-01

    Bakalaura darba nosaukums ir „Kukuļņemšanas un kukuļdošanas kvalifikācijas problēmas”. Darba mērķis ir izpētīt normatīvos aktus, speciālo juridisko literatūru un judikatūru, nolūkā konstatēt problēmas kukuļņemšanas un kukuļdošanas kvalifikācijā. Lai sasniegtu šo mērķi, darbā tika aplūkota kukuļņemšanas un kukuļdošanas vēsturiskā attīstība, tādējādi sniedzot nelielu ieskatu par kukuļņemšanas un kukuļdošanas juridiskā pamata vēsturiskās attīstības posmiem no 19.gadsimta līdz mūsdienām. Darb...

  9. Mācību video materiālu izstrāde tēmas „Elektrība” apguvei vidusskolas fizikā

    OpenAIRE

    Kravis, Kārlis

    2013-01-01

    Diplomdarbā „Mācību video materiālu izstrāde tēmas „Elektrība” apguvei vidusskolas fizikā” ir izveidoti, aprobēti un ekspertu izvērtēti 15 mācību video. Tēma „Elektrība”, it īpaši elektrostatikas jautājumi, ir abstrakti skolēna izpratnei, jo fizikālie procesi notiek mikropasaules līmenī. Līdz ar sabiedrības pieprasījumu par mācību materiālu digitalizāciju un esošo materiālu piedāvājumu ir aktualizējies jautājums, kā kvalitatīvus digitālos materiālus izmantot mācību procesā skolēnu zināšanu un...

  10. Interneta sociālie tīkli draugiem.lv, mammam/tetiem.lv un twitter.com kā reklāmas nesēji Latvijā (2009.gads)

    OpenAIRE

    Vismane, Inese

    2010-01-01

    Maģistra darba tēma ir „Interneta sociālie tīkli draugiem.lv, mammam/tetiem.lv un twitter.com kā reklāmas nesēji Latvijā (2009.gads)”. Darba mērķis ir izpētīt Latvijas interneta sociālo tīklu vidi kā potenciāli augošu un reklāmai piemērotu, kā arī izpētīt pamanāmākos reklāmas gadījumus šajos portālos. Teorijas daļā tiek apskatīta Web 2.0 ēra, interneta reklāmas un sociālo mediju mārketinga īpatnības, sociālo tīklu fenomens un teorijas, Latvijas reklāmas tirgus un auditorija, kā arī sociāl...

  11. "McDonald's" reklāmas analīze Latvijā un Maltā - starpkultūru atšķirīgā uztvere

    OpenAIRE

    Barkēviča, Santa

    2016-01-01

    Darbā ““McDonald's” reklāmas analīze Latvijā un Maltā – starpkultūru atšķirīgā uztvere” galvenais problēmjautājums, kas jānoskaidro, vai starptautisks uzņēmums var izmantot viena stila reklāmas kampaņu divās dažādās valstīs – Latvijā un Maltā. Galvenais darba mērķis ir noskaidrot, vai starptautisks uzņēmums var veidot vienu reklāmas kampaņu shēmu, un to izmantot dažādās valstīs, kur atrodas tā franšīzes vai filiāles, un kā starpkultūru atšķirība ietekmē reklāmas uztveri. Veicot aptaujas, inte...

  12. Electronic mail monitoring in the work environment: the conflict between the employer’s directive power and his/her employee’s privacy right Monitoramento do correio eletrônico em ambiente de trabalho: o conflito entre o poder diretivo do empregador e o direito à intimidade de seu preposto

    Directory of Open Access Journals (Sweden)

    Wesley Tomaszewski

    2007-11-01

    Full Text Available The purpose of this article is to deal with the monitoring practiced by entrepreneurs as to the use of information technologies by their representatives in the work environment, which was enabled by the technological revolution originated in the globalization process. The theme in study also includes the confrontation of constitutionally assured rights in the employer/employee relationship and the position adopted by the courts concerning this problem. O presente artigo tem por escopo discutir o monitoramento praticado por empresários no tocante à utilização das tecnologias da informação por seus prepostos, no ambiente de trabalho, possibilitado pela revolução tecnológica oriunda do processo de globalização. O tema em estudo abrange ainda o confronto de direitos constitucionalmente assegurados na relação entre o empregado e o empregador e o posicionamento adotado pelos tribunais diante da problemática suscitada.

  13. Un análisis institucional de la implicación del proceso de cambio de los SCG en la evolución de la eficiencia de las PYME An institutional analysis of the implication of the MAS change process for the evolution of SMSC efficiency

    Directory of Open Access Journals (Sweden)

    Carlos Eduardo Facin Lavarda

    2009-04-01

    Full Text Available El objetivo general de este trabajo es conocer la relación existente entre el proceso de cambio de un Sistema de Contabilidad de Gestión (SCG en las pequeñas y medianas empresas (PYME y el éxito que genera dicho cambio. El éxito del cambio del SCG se va a medir a través de dos indicadores. El primer indicador, el éxito interno, medirá la distancia que existe entre las expectativas (qué se esperaba de las nuevas técnicas de gestión implantadas y las realidades (qué son. El segundo indicador, el éxito externo, medirá la variación en el nivel de eficiencia relativa de la empresa dentro de su sector. La hipótesis básica de este estudio, plantea que el proceso de cambio puede explicar el nivel de éxito (interno-externo alcanzado en el cambio de un SCG. Para captar y analizar los datos, utilizaremos dos técnicas: el Análisis Envolvente de Datos (DEA y el método del Estudio de Caso (EDC. Los resultados de la investigación permitieron conocer los que factores influyeron, y por tanto explican el éxito de un cambio en los SCG de una PYME del sector de la madera y mueble de la Comunidad Valenciana, España, entre ellos: los conocimientos y habilidades de los agentes implicados en el cambio, la influencia de los expertos externos, la profesionalización de la gestión, los recursos informáticos, la formación interna en SCG, la confianza entre los agentes y la implicación de las personas. Además, hemos observado que los cambios producidos a lo largo de los años analizados influyeron positivamente en el nivel de eficiencia de la organización.This study's general objective is to get to know the relation between the change process of a Management Accounting System (MASO in small and medium-sized companies (SMSC and the success of this change. The success of the MAS change is measured by two indicators. The first, internal success, measures the distance between the expectations (what was expected about the new management techniques

  14. SU-G-IeP3-14: Updating Tools for Radiographic Technique Charts

    Energy Technology Data Exchange (ETDEWEB)

    Walz-Flannigan, A; Lucas, J; Buchanan, K; Schueler, B [Mayo Clinic, Rochester, MN (United States)

    2016-06-15

    Purpose: Manual technique selection in radiography is needed for imaging situations where there is difficulty in proper positioning for AEC, prosthesis, for non-bucky imaging, or for guiding image repeats. Basic information about how to provide consistent image signal and contrast for various kV and tissue thickness is needed to create manual technique charts, and relevant for physicists involved in technique chart optimization. Guidance on technique combinations and rules-of-thumb to provide consistent image signal still in use today are based on measurements with optical density of screen-film combinations and older generation x-ray systems. Tools such as a kV-scale chart can be useful to know how to modify mAs when kV is changed in order to maintain consistent image receptor signal level. We evaluate these tools for modern equipment for use in optimizing proper size scaled techniques. Methods: We used a water phantom to measure calibrated signal change for CR and DR (with grid) for various beam energies. Tube current values were calculated that would yield a consistent image signal response. Data was fit to provide sufficient granularity of detail to compose technique-scale chart. Tissue thickness approximated equivalence to 80% of water depth. Results: We created updated technique-scale charts, providing mAs and kV combinations to achieve consistent signal for CR and DR for various tissue equivalent thicknesses. We show how this information can be used to create properly scaled size-based manual technique charts. Conclusion: Relative scaling of mAs and kV for constant signal (i.e. the shape of the curve) appears substantially similar between film-screen and CR/DR. This supports the notion that image receptor related differences are minor factors for relative (not absolute) changes in mAs with varying kV. However, as demonstrated creation of these difficult to find detailed technique-scales are useful tools for manual chart optimization.

  15. Monitoramento da presença de Mycoplasma hyopneumoniae em granjas de suínos durante a implementação de programas de erradicação Monitoring the presence of Mycoplasma hyopneumoniae in swine farms during the implementation of eradication programs

    Directory of Open Access Journals (Sweden)

    Pablo Jesús Tamiozzo

    2011-04-01

    Full Text Available O objetivo deste estudo foi monitorar a presença de M. hyopneumoniae em granjas suínas durante a implementação de programas de erradicação utilizando diferentes técnicas de diagnóstico focalizando no PCR. Trabalhou-se com uma empresa que possuía três granjas, uma parto-terminação (390 matrizes, uma múltiplo-sítio (4100 matrizes e uma nova granja que povoava suas novas instalações. Nas duas primeiras, foi desenvolvido um programa de despovoamento parcial para erradicar a pneumonia enzoótica suína, a última foi povoada pelos suínos dos anteriores após a erradicação. Nos três rebanhos, os suínos foram monitorados por: sorologia (ELISA, PCR, lesões pulmonares macro e microscópicas e a presença de tosse não produtiva. A ausência de tosse, a baixa porcentagem de suínos soropositivos na fase de terminação e a baixa proporção de lesões pulmonares no abate sugerem que a pneumonia enzoótica suína foi erradicada, mas não o agente causativo -M. hyopneumoniae- cujo DNA foi detectado pela PCR, mostrando diferentes comportamentos de acordo com o rebanho.The aim of this study was to monitor the presence of M. hyopneumoniae in pig farms during the implementation of eradication programs using different diagnostic techniques focusing on PCR. They worked with a company owner of three farms, a farrow-to-finish (390 sows, a multiple-site (4100 sows and a new one that was populated its new facility. In the first two were developed a partial depopulation program to eradicate swine enzootic pneumonia, the latter one was populated with pigs after the previous eradication. In the three farms, the pigs were monitored by: serology (ELISA, PCR, macroscopic and microscopic lung lesions and the presence of non-productive cough. The absence of cough, low percentage of seropositive pigs in the finishing stage and the low proportion of lung lesions at slaughter suggest that swine enzootic pneumonia was eradicated, but not the causative agent

  16. The generalized multipole technique for light scattering recent developments

    CERN Document Server

    Eremin, Yuri

    2018-01-01

    This book presents the Generalized Multipole Technique as a fast and powerful theoretical and computation tool to simulate light scattering by nonspherical particles. It also demonstrates the considerable potential of the method. In recent years, the concept has been applied in new fields, such as simulation of electron energy loss spectroscopy and has been used to extend other methods, like the null-field method, making it more widely applicable. The authors discuss particular implementations of the GMT methods, such as the Discrete Sources Method (DSM), Multiple Multipole Program (MMP), the Method of Auxiliary Sources (MAS), the Filamentary Current Method (FCM), the Method of Fictitious Sources (MFS) and the Null-Field Method with Discrete Sources (NFM-DS). The Generalized Multipole Technique is a surface-based method to find the solution of a boundary-value problem for a given differential equation by expanding the fields in terms of fundamental or other singular solutions of this equation. The amplitudes ...

  17. Restaging of patients with lymphoma. Comparison of low dose CT (20 mAs) with contrast enhanced diagnostic CT in combined [18F]-FDG PET/CT

    International Nuclear Information System (INIS)

    Fougere, C. la; Pfluger, T.; Schneider, V.; Hacker, M.; Broeckel, N.; Bartenstein, P.; Tiling, R.; Morhard, D.; Hundt, W.; Becker, C.

    2008-01-01

    Aim: assessment of the clinical benefit of i.v. contrast enhanced diagnostic CT (CE-CT) compared to low dose CT with 20 mAs (LD-CT) without contrast medium in combined [ 18 F]-FDG PET/CT examinations in restaging of patients with lymphoma. Patients, methods: 45 patients with non-Hodgkin lymphoma (n = 35) and Hodgkin's disease (n = 10) were included into this study. PET, LD-CT and CE-CT were analyzed separately as well as side-by-side. Lymphoma involvement was evaluated separately for seven regions. Indeterminate diagnoses were accepted whenever there was a discrepancy between PET and CT findings. Results for combined reading were calculated by rating indeterminate diagnoses according the suggestions of either CT or PET. Each patient had a clinical follow-up evaluation for > 6 months. Results: region-based evaluation suggested a sensitivity/specificity of 66/93% for LD-CT, 87%/91% for CE-CT, 95%/96% for PET, 94%/99% for PET/LD-CT and 96%/99% for PET/CE-CT. The data for PET/CT were obtained by rating indeterminate results according to the suggestions of PET, which turned out to be superior to CT. Lymphoma staging was changed in two patients using PET/CE-CT as compared to PET/LD-CT. Conclusion: overall, there was no significant difference between PET/LD-CT and PET/CE-CT. However, PET/CE-CT yielded a more precise lesion delineation than PET/LD-CT. This was due to the improved image quality of CE-CT and might lead to a more accurate investigation of lymphoma. (orig.)

  18. Emerging Roles for MAS-Related G Protein-Coupled Receptor-X2 in Host Defense Peptide, Opioid, and Neuropeptide-Mediated Inflammatory Reactions.

    Science.gov (United States)

    Ali, Hydar

    2017-01-01

    Mast cells (MCs) are tissue-resident immune cells that contribute to host defense but are best known for their roles in allergic and inflammatory diseases. In humans, MCs are divided into two subtypes based on the protease content of their secretory granules. Thus, human lung MCs contain only tryptase and are known as MC T , whereas skin MCs contain both tryptase and chymase and are known as MC TC . Patients with severe asthma display elevated MCs in the lung, which undergo phenotypic change from MC T to MC TC . Although the human genome contains four Mas related G protein coupled receptor X (MRGPRX) genes, an important feature of MC TC is that they selectively express MRGPRX2. It is activated by antimicrobial host defense peptides such as human β-defensins and the cathelicidin LL-37 and likely contributes to host defense. MRGPRX2 is also a receptor for the neuropeptide substance P, major basic protein, eosinophil peroxidase, opioids, and many FDA-approved cationic drugs. Increased expression of MRGPRX2 or enhanced downstream signaling likely contributes to chronic inflammatory diseases such as rosacea, atopic dermatitis, chronic urticaria, and severe asthma. In this chapter, I will discuss the expression profile and function of MRGPRX1-4 and review the emerging roles of MRGPRX2 on host defense, chronic inflammatory diseases, and drug-induced pseudoallergic reactions. I will also examine the novel aspects of MRGPRX2 signaling in MCs as it related to degranulation and review the mechanisms of its regulation. © 2017 Elsevier Inc. All rights reserved.

  19. Differential Regulation of Mas-Related G Protein-Coupled Receptor X2-Mediated Mast Cell Degranulation by Antimicrobial Host Defense Peptides and Porphyromonas gingivalis Lipopolysaccharide.

    Science.gov (United States)

    Gupta, Kshitij; Idahosa, Chizobam; Roy, Saptarshi; Lee, Donguk; Subramanian, Hariharan; Dhingra, Anuradha; Boesze-Battaglia, Kathleen; Korostoff, Jonathan; Ali, Hydar

    2017-10-01

    Porphyromonas gingivalis is a keystone pathogen that contributes to periodontal pathogenesis by disrupting host-microbe homeostasis and promoting dysbiosis. The virulence of P. gingivalis likely reflects an alteration in the lipid A composition of its lipopolysaccharide (LPS) from the penta-acylated ( Pg LPS 1690 ) to the tetra-acylated ( Pg LPS 1435/1449 ) form. Mast cells play an important role in periodontitis, but the mechanisms of their activation and regulation remain unknown. The expression of epithelium- and neutrophil-derived host defense peptides (HDPs) (LL-37 and human β-defensin-3), which activate mast cells via Mas-related G protein-coupled receptor X2 (MRGPRX2), is increased in periodontitis. We found that MRGPRX2-expressing mast cells are present in normal gingiva and that their numbers are elevated in patients with chronic periodontitis. Furthermore, HDPs stimulated degranulation in a human mast cell line (LAD2) and in RBL-2H3 cells stably expressing MRGPRX2 (RBL-MRGPRX2). Pg LPS 1690 caused substantial inhibition of HDP-induced mast cell degranulation, but Pg LPS 1435/1449 had no effect. A fluorescently labeled HDP (FAM-LL-37) bound to RBL-MRGPRX2 cells, and Pg LPS 1690 inhibited this binding, but Pg LPS 1435/1449 had no effect. These findings suggest that low-level inflammation induced by HDP/MRGPRX2-mediated mast cell degranulation contributes to gingival homeostasis but that sustained inflammation due to elevated levels of both HDPs and MRGPRX2-expressing mast cells promotes periodontal disease. Furthermore, differential regulation of HDP-induced mast cell degranulation by Pg LPS 1690 and Pg LPS 1435/1449 may contribute to the modulation of disease progression. Copyright © 2017 American Society for Microbiology.

  20. Effect of Mas-related gene (Mrg) receptors on hyperalgesia in rats with CFA-induced inflammation via direct and indirect mechanisms.

    Science.gov (United States)

    Jiang, Jianping; Wang, Dongmei; Zhou, Xiaolong; Huo, Yuping; Chen, Tingjun; Hu, Fenjuan; Quirion, Rémi; Hong, Yanguo

    2013-11-01

    Mas oncogene-related gene (Mrg) receptors are exclusively distributed in small-sized neurons in trigeminal and dorsal root ganglia (DRG). We investigated the effects of MrgC receptor activation on inflammatory hyperalgesia and its mechanisms. A selective MrgC receptor agonist, bovine adrenal medulla peptide 8-22 (BAM8-22) or melanocyte-stimulating hormone (MSH) or the μ-opioid receptor (MOR) antagonist CTAP was administered intrathecally (i.t.) in rats injected with complete Freund's adjuvant (CFA) in one hindpaw. Thermal and mechanical nociceptive responses were assessed. Neurochemicals were measured by immunocytochemistry, Western blot, ELISA and RT-PCR. CFA injection increased mRNA for MrgC receptors in lumbar DRG. BAM8-22 or MSH, given i.t., generated instant short and delayed long-lasting attenuations of CFA-induced thermal hyperalgesia, but not mechanical allodynia. These effects were associated with decreased up-regulation of neuronal NOS (nNOS), CGRP and c-Fos expression in the spinal dorsal horn and/or DRG. However, i.t. administration of CTAP blocked the induction by BAM8-22 of delayed anti-hyperalgesia and inhibition of nNOS and CGRP expression in DRG. BAM8-22 also increased mRNA for MORs and pro-opiomelanocortin, along with β-endorphin content in the lumbar spinal cord and/or DRG. MrgC receptors and nNOS were co-localized in DRG neurons. Activation of MrgC receptors suppressed up-regulation of pronociceptive mediators and consequently inhibited inflammatory pain, because of the activation of up-regulated MrgC receptors and subsequent endogenous activity at MORs. The uniquely distributed MrgC receptors could be a novel target for relieving inflammatory pain. © 2013 The British Pharmacological Society.

  1. Analysis of mercerization process based on the intensity change of deconvoluted resonances of 13C CP/MAS NMR: Cellulose mercerized under cooling and non-cooling conditions

    International Nuclear Information System (INIS)

    Miura, Kento; Nakano, Takato

    2015-01-01

    The area intensity change of C1, C4, and C6 in spectrum obtained by 13 C CP/MAS NMR and the mutual relationship between their changes were examined for cellulose samples treated with various concentrations of aqueous NaOH solutions under non-cooling and cooling conditions. The area intensity of C1-up and C6-down changed cooperatively with that of C4-down which corresponds to the crystallinity of samples: “-up” and “-down” are the up- and down- field component in a splitting peak of NMR spectrum, respectively. The intensity change of C1-up starts to decrease with decreasing in that of C4-down after that of C6-down is almost complete. These changes were more clearly observed for samples treated under cooling condition. It can be suggested that their characteristic change relates closely to the change in conformation of cellulose chains by induced decrystallization and the subsequent crystallization of cellulose II, and presumed that their changes at microscopic level relate to the macroscopic morphological changes such as contraction along the length of cellulose chains and recovery along the length. - Highlight: • Samples were mercerized at various NaOH concentrations under non-cooling and cooling. • The intensity change of C1 starts immediately after that of C6 is complete. • The creation of cell-II starts when decrystallization proceeds to a certain state. • This change relates closely to the change in conformation of cellulose chains. • The above change is more clearly found for samples treated under cooling

  2. Images of the plant kingdom in the Mamluk encyclopedia Masālik al-abṣār by Ibn Faḍl Allāh al-‘Umarī (d. 1349)

    OpenAIRE

    Francesca Bellino

    2016-01-01

    This article aims at analyzing the representation of the plant kingdom in the Masālik al-abṣār fī mamālik al-amṣār, an Arabic encyclopaedia written by one the leading scholar of the Mamluk period, Šihāb al-Dīn Ibn Faḍl Allāh al-‘Umarī (1301-1349). The first part of the article offers an insight into the work of al-‘Umarī by presenting it in the framework of the encyclopaedic activities that characterize the fourteenth century. It also analyzes a number of special features of the Masālik al-ab...

  3. Out-and-back {sup 13}C-{sup 13}C scalar transfers in protein resonance assignment by proton-detected solid-state NMR under ultra-fast MAS

    Energy Technology Data Exchange (ETDEWEB)

    Barbet-Massin, Emeline; Pell, Andrew J. [University of Lyon, CNRS/ENS Lyon/UCB Lyon 1, Centre de RMN a Tres Hauts Champs (France); Jaudzems, Kristaps [Latvian Institute of Organic Synthesis (Latvia); Franks, W. Trent; Retel, Joren S. [Leibniz-Institut fuer Molekulare Pharmakologie (Germany); Kotelovica, Svetlana; Akopjana, Inara; Tars, Kaspars [Biomedical Research and Study Center (Latvia); Emsley, Lyndon [University of Lyon, CNRS/ENS Lyon/UCB Lyon 1, Centre de RMN a Tres Hauts Champs (France); Oschkinat, Hartmut [Leibniz-Institut fuer Molekulare Pharmakologie (Germany); Lesage, Anne; Pintacuda, Guido, E-mail: guido.pintacuda@ens-lyon.fr [University of Lyon, CNRS/ENS Lyon/UCB Lyon 1, Centre de RMN a Tres Hauts Champs (France)

    2013-08-15

    We present here {sup 1}H-detected triple-resonance H/N/C experiments that incorporate CO-CA and CA-CB out-and-back scalar-transfer blocks optimized for robust resonance assignment in biosolids under ultra-fast magic-angle spinning (MAS). The first experiment, (H)(CO)CA(CO)NH, yields {sup 1}H-detected inter-residue correlations, in which we record the chemical shifts of the CA spins in the first indirect dimension while during the scalar-transfer delays the coherences are present only on the longer-lived CO spins. The second experiment, (H)(CA)CB(CA)NH, correlates the side-chain CB chemical shifts with the NH of the same residue. These high sensitivity experiments are demonstrated on both fully-protonated and 100 %-H{sup N} back-protonated perdeuterated microcrystalline samples of Acinetobacter phage 205 (AP205) capsids at 60 kHz MAS.

  4. Monitoramento externo da qualidade dos exames citopatológicos cervicais realizados pelo Sistema Único de Saúde (SUS no Estado de Mato Grosso do Sul External quality control for cervical cytology exams performed in the Brazilian Public Health System of Mato Grosso do Sul State

    Directory of Open Access Journals (Sweden)

    Hilda Guimarães de Freitas

    2012-08-01

    Full Text Available OBJETIVO: Analisar a concordância de diagnósticos citopatológicos de laboratórios credenciados e os verificados no monitoramento. MÉTODOS: Foram calculados o coeficiente de concordância global e o coeficiente Kappa de Cohen de uma amostra de conveniência dos exames selecionados mensalmente pelo Sistema de Informação do Câncer do Colo do Útero (SISCOLO para monitoramento externo da qualidade (MEQ dos 15 laboratórios que realizaram exames citopatológicos para o SUS entre 2002 e 2011 no Estado do Mato Grosso do Sul (região central do Brasil. A comparação entre os valores de concordância (coeficiente de concordância global e coeficiente Kappa dos anos inicial e final foi computada por meio da variação absoluta (delta e variação percentual relativa (VPR. RESULTADOS: Foram encaminhadas para releitura 15.989 esfregaços, dos quais 48,1% apresentavam laudo normal/alteração benigna, seguidos de atipia/lesão de baixo grau (36,3%, lesão de alto grau/carcinoma/adenocarcinoma (4,2% e insatisfatórios para leitura (11,4%. O coeficiente de concordância global oscilou entre 0,2 e 1,0, sendo que o valor mediano passou de 0,7 em 2002 para 1,0 em 2011 (VPR=+36,6%. Nesse mesmo período, os valores medianos do coeficiente Kappa aumentaram de 0,5 para 0,9 (VPR=+80,8%. CONCLUSÕES: Conclui-se pela exequibilidade do MEQ dos exames citopatológicos na esfera estadual e que sua implementação resulta em melhoria nos diagnósticos realizados na rede SUS.PURPOSE: To evaluate the diagnostic agreement between the cytopathology reports issued by accredited laboratories and those obtained by quality control. METHODS: We calculated the overall agreement and Cohen's kappa coefficients of a convenience sample of smears selected monthly by the Information System of Cervical Cancer (SISCOLO for External Quality Control of the 15 laboratories that performed cytopathological PAP tests for the Brazilian Public Health System (SUS between 2002 and 2011 in

  5. Subsídios sobre práticas de monitoramento e avaliação sobre gestão governamental em Secretarias Municipais de Saúde Input on monitoring and evaluation practices of government management of Brazilian Municipal Health Departments

    Directory of Open Access Journals (Sweden)

    Alcides Silva de Miranda

    2012-04-01

    Full Text Available O que os dirigentes de Secretarias Municipais de Saúde (SMS referem e relatam acerca do monitoramento e avaliação sistemática da própria gestão governamental? O propósito desta publicação é apresentar subsídios para a formulação de hipóteses plausíveis acerca de tais processos e práticas institucionais, a partir de informações produzidas em estudo exploratório. Trata-se de estudo de casos múltiplos, com análise quanti-qualitativa sobre respostas a um questionário semiestruturado aplicado a dirigentes governamentais de uma amostra sistemática de 577 Secretarias Municipais de Saúde (10,4 % do total no Brasil, selecionadas e estratificadas por distribuição proporcional nas unidades federativas e por portes populacionais de municípios. De um modo geral, denota-se que aproximadamente metade dos respondentes utiliza informações de Monitoramento Avaliação em Saúde para subsidiar processos decisórios, planejamento e outros enfoques de gestão. Esta proporção tende a diminuir em municípios de menores portes populacionais. Há lacunas específicas e significativas nos gerenciamento financeiro, de pessoal e de situações de crises. A consubstanciação de hipóteses reforça a constatação de que estes processos encontram-se ainda em fase incipiente.What do the leaders of the Municipal Health Service (SMS report and say about the systematic monitoring and evaluation of their own government management? The purpose of this paper is to provide input for the formulation of plausible hypotheses about such institutional processes and practices based on information produced in an exploratory study. This is a multiple case study with quantitative and qualitative analysis of answers to a semi-structured questionnaire given to government officials of a systematic sample of 577 Municipal Health Services (10.4% of the total in Brazil. They were selected and stratified by proportional distribution among states and by the population

  6. Fast MAS 1H NMR Study of Water Adsorption and Dissociation on the (100) Surface of Ceria Nanocubes: A Fully Hydroxylated, Hydrophobic Ceria Surface

    Energy Technology Data Exchange (ETDEWEB)

    Gill, Lance [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States). Chemical Sciences Division; Beste, Ariana [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States). Joint Institute for Computational Sciences (JIBS); Univ. of Tennessee, Knoxville, TN (United States); Chen, Banghao [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States). Chemical Sciences Division; Li, Meijun [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States). Chemical Sciences Division; Mann, Amanda K. P. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States). Chemical Sciences Division; Overbury, Steven H. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States). Chemical Sciences Division; Hagaman, Edward W. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States). Chemical Sciences Division

    2017-03-22

    1H nuclear magnetic resonance (NMR) spectroscopy was used to study hydroxylic surface species on ceria nanocubes, a crystalline, high-surface-area CeO2 that presents mostly (100) facets. Water adsorption and desorption experiments in combination with fast magic angle spinning (MAS, 20–40 kHz) 1H NMR provide high-resolution 1H spectra that allow the observation of ten resonance bands (water or hydroxyl) on or under the (100) surface. Assignments were made using a combination of adsorption and temperature-programmed desorption, quantitative spin counting, deuterium exchange, spin–lattice (T1) and spin–spin (T2) relaxation, and DFT calculations. In air, the (100) surface exists as a fully hydroxylated surface. Water adsorption and dissociation on dry ceria surfaces occur first at oxygen vacancies, but Ce3+ centers are not required since water dissociation is barrier-less on the fully oxidized surface. Surface $-$OH functionality occurs in two resolved bands representing isolated $-$OH (1 ppm) and hydrogen-bonded $-$OH (9 ppm), the latter being dominant. Deuterium exchange of surface hydroxyls with D2O does not occur under mild or forcing conditions. Despite large differences in the T1 of surface hydroxyls and physisorbed water, surface hydroxyl T1 values are independent of the presence or absence of physisorbed water, demonstrating that the protons within these two functional group pools are not in intimate contact. These observations show that, once hydroxylated, the surface $-$OH functionality preferentially forms hydrogen bonds with surface lattice oxygen, i.e., the hydroxylated (100) surface of ceria is hydrophobic. Near this surface it is energetically more favorable for physisorbed water to hydrogen bond to itself rather than to the surface. DFT calculations support this notion. Impurity Na+ remaining in incompletely washed ceria nanocubes

  7. Expression and distribution patterns of Mas-related gene receptor subtypes A-H in the mouse intestine: inflammation-induced changes.

    Science.gov (United States)

    Avula, Leela Rani; Buckinx, Roeland; Favoreel, Herman; Cox, Eric; Adriaensen, Dirk; Van Nassauw, Luc; Timmermans, Jean-Pierre

    2013-05-01

    Mas-related gene (Mrg) receptors constitute a subfamily of G protein-coupled receptors that are implicated in nociception, and are as such considered potential targets for pain therapies. Furthermore, some Mrgs have been suggested to play roles in the regulation of inflammatory responses to non-immunological activation of mast cells and in mast cell-neuron communication. Except for MrgD, E and F, whose changed expression has been revealed during inflammation in the mouse intestine in our earlier studies, information concerning the remaining cloned mouse Mrg subtypes in the gastrointestinal tract during (patho) physiological conditions is lacking. Therefore, the present study aimed at identifying the presence and putative function of these remaining cloned Mrg subtypes (n = 19) in the (inflamed) mouse intestine. Using reverse transcriptase-PCR, quantitative-PCR and multiple immunofluorescence staining with commercial and newly custom-developed antibodies, we compared the ileum and the related dorsal root ganglia (DRG) of non-inflamed mice with those of two models of intestinal inflammation, i.e., intestinal schistosomiasis and 2,4,6-trinitrobenzene sulfonic acid-induced ileitis. In the non-inflamed ileum and DRG, the majority of the Mrg subtypes examined were sparsely expressed, showing a neuron-specific expression pattern. However, significant changes in the expression patterns of multiple Mrg subtypes were observed in the inflamed ileum; for instance, MrgA4, MrgB2and MrgB8 were expressed in a clearly increased number of enteric sensory neurons and in nerve fibers in the lamina propria, while de novo expression of MrgB10 was observed in enteric sensory neurons and in newly recruited mucosal mast cells (MMCs). The MrgB10 expressing MMCs were found to be in close contact with nerve fibers in the lamina propria. This is the first report on the expression of all cloned Mrg receptor subtypes in the (inflamed) mouse intestine. The observed changes in the expression and

  8. Effect of Ge/Si substitutions on the local geometry of Si framework sites in zeolites: A combined high resolutionsup29/supSi MAS NMR and DFT/MM study on zeolite Beta polymorph C (BEC)

    Czech Academy of Sciences Publication Activity Database

    Whittleton, Sarah R.; Vicente, A.; Fernandez, C.; Rastegar, Somayeh F.; Fishchuk, Anna V.; Sklenák, Štěpán

    2018-01-01

    Roč. 267, SEP 2018 (2018), s. 124-133 ISSN 1387-1811 R&D Projects: GA ČR(CZ) GA15-14007S Grant - others:Ga MŠk(CZ) LM2015070 Institutional support: RVO:61388955 Keywords : 29 Si MAS NMR * bec * Ge-zeolites * Germanoaluminosilicates * Zeolite Beta polymorph C Subject RIV: CF - Physical ; Theoretical Chemistry OBOR OECD: Physical chemistry Impact factor: 3.615, year: 2016

  9. ESTUDIO COMPARATIVO ENTRE DOS ESQUEMAS DE ACUPUNTURA ZUSANLI (E-36), SANYINJIAO (B-6), XUEHAI (B-10), TAICHONG (H-3) VS. MISMO ESQUEMA MAS QUANLIAO (ID-18) EN EL MANEJO DEL DOLOR Y LAS PARESTESIAS EN LA NEUROPATIA DIABETICA

    OpenAIRE

    VENEGAS CERVANTES, RAFAEL MELQUIADES

    2010-01-01

    LA NEUROPATIA DIABETICA (ND), COMPLICACION FRECUENTE DE LOS PACIENTES DIABETICOS, SE CARACTERIZA PORQUE EXISTEN ALTERACIONES EN LA PERCEPCION SOMATOSENSITIVA Y A NIVEL CIRCULATORIO (DOLOR, DISESTESIAS, PARESIAS Y PARESTESIAS). EN ESTA INVESTIGACION SE ESTUDIA EL EFECTO DE LA ACUPUNTURA, TANTO EN EL DOLOR, COMO EN LAS ALTERACIONES SENSITIVAS. PARA LO ANTERIOR SE UTILIZARON ACUPUNTOS DE EMPLEO ORDINARIO PARA LA ENFERMEDAD, HACIENDO UN COMPARATIVO CON EL MISMO ESQUEMA DE ACUPUNTOS, MAS LA ...

  10. Método da eletrorresistividade aplicado no monitoramento temporal da pluma de contaminação em área de disposição de resíduos sólidos urbanos Electrical resistivity method applied in the temporal monitoring of the contamination plume in disposal area of urban solid waste

    Directory of Open Access Journals (Sweden)

    José Ricardo Melges Bortolin

    2010-12-01

    Full Text Available Este trabalho apresenta os resultados do monitoramento temporal da pluma de contaminação do aterro controlado de Rio Claro, São Paulo, por meio do método da eletrorresistividade, que consistiu na comparação dos resultados de várias seções de imageamento elétrico, executados nos mesmo locais, nos anos de 1999 e 2008. Zonas de baixa resistividade, com valores menores ou iguais a 50 Ω.m, foram associadas à contaminação por chorume. Desse modo, foi possível identificar dois sentidos do fluxo da pluma: (1 em direção ao sul, e (2 em direção ao oeste. Nas seções de 2008, a pluma de contaminação apresentou-se mais extensa e profunda do que em 1999. De forma complementar, as sondagens elétricas verticais aferiram a profundidade do nível freático e o sentido do fluxo d'água, subsidiando a interpretação dos imageamentos.This paper shows the results of a periodical monitoring of the contamination plume of a controlled landfill in Rio Claro, São Paulo, Brazil, using electrical resistivity geophysical method. The monitoring consisted on comparing the results of several electrical sections, performed at the same location, in the years of 1999 and 2008. Low resistivity zones, with values lower than or equal to 50 Ω.m, have been associated to contamination by leachate. Thus, it was possible to identify two directions for the contamination flows: (1 toward south, and (2 toward west. In the results of 2008, the contamination plume was more extensive and profound than in 1999. The vertical electrical soundings indicated the water table depth and the water flow directions, helping the interpretation of results of the electrical profiles.

  11. Review of semiochemicals that mediate the oviposition of mosquitoes: a possible sustainable tool for the control and monitoring of Culicidae Revisão dos semioquímicos que mediam a oviposição em mosquitos: uma possível ferramenta sustentável para o monitoramento e controle de Culicidae

    Directory of Open Access Journals (Sweden)

    Mario A. Navarro-Silva

    2009-01-01

    Full Text Available The choice for suitable places for female mosquitoes to lay eggs is a key-factor for the survival of immature stages (eggs and larvae. This knowledge stands out in importance concerning the control of disease vectors. The selection of a place for oviposition requires a set of chemical, visual, olfactory and tactile cues that interact with the female before laying eggs, helping the localization of adequate sites for oviposition. The present paper presents a bibliographic revision on the main aspects of semiochemicals in regard to mosquitoes' oviposition, aiding the comprehension of their mechanisms and estimation of their potential as a tool for the monitoring and control of the Culicidae.A seleção de locais adequados pelas fêmeas de mosquitos para depositarem seus ovos é um fator chave para a sobrevivência de seus imaturos (ovos e larvas. O conhecimento das relações ecológicas implicadas neste processo é de grande importância quando se refere a vetores de agentes patogênicos. A determinação do local de oviposição pelas fêmeas grávidas envolve uma rede de mensagens químicas, visuais, olfativas e táteis que facilitam a localização de lugares adequados para depositarem seus ovos. Neste trabalho é apresentada uma revisão bibliográfica dos principais aspectos relacionados com semioquímicos presentes na oviposição dos mosquitos auxiliando no entendimento dos mecanismos de atuação dos mesmos e potencializando a aplicação destes semioquímicos como uma possível ferramenta de monitoramento e controle de Culicidae.

  12. Fluxos informacionais para o monitoramento da Convenção dos Direitos da Criança: a atuação da rede NGO Group for CRCInformation follow and the monitoring process of the convention on the rights of child by NGO Group for CRC network

    Directory of Open Access Journals (Sweden)

    Maria Guiomar da Cunha Frota

    2010-05-01

    Full Text Available O presente artigo apresenta os resultados de uma pesquisa que investiga uma rede social internacional denominada NGO Group for CRC. A rede é composta por cerca de noventa organizações não governamentais e foi criada para monitorar a implementação da Convenção dos Direitos da Criança (CRC. A CRC é o principal documento jurídico relativo aos direitos da criança, tendo sido aprovada pela totalidade dos países pertencentes à ONU, com exceção dos EUA. Pretende-se especificamente analisar o fluxo informacional que se estabelece em meio à rede, seus membros e as organizações que a ela se associam. As questões investigadas são as seguintes: 1 Em que medida o fluxo informacional torna-se parte intrínseca da estrutura em rede? 2 Como os fluxos informacionais se configuram e de que modo são apropriados e veiculados pela rede NGO Group for CRC no curso do monitoramento da implementação da Convenção dos Direitos da Criança?This paper presents the research results about the social network NGO Group for CRC which is an articulation of non governmental organizations related to children's rights. This paper analyzes the information flow inside the network, among its members and among the network organizations. The Convention on the Rights of the Child (CRC was approved in 1989 by the General Assembly of the United Nations, being ratified in its totality by the countries members, with the exception of the United States of America. The investigated questions are: 1 How is the role of the information flow in the network structure? 2 How is the information flow configured to support the implementation monitoring process of the Convention on the Rights of the Child?

  13. One-Pot Synthesis, X-Ray Diffraction and MAS NMR Spectroscopic Study of Gallosilicate Nitrate Cancrinite Na8[GaSiO4]6(NO34(H2O6

    Directory of Open Access Journals (Sweden)

    Ashok V. Borhade

    2010-01-01

    Full Text Available One-pot synthetic gallosilicate nitrate cancrinite (CAN framework topology have been synthesized under hydrothermal conditions at 100 °C. The synthesized product was characterized by, X-ray powder diffraction, IR, Raman and 29Si, 23Na MAS NMR spectroscopy, SEM and thermogravimetry. The crystal structure refinement of pure nitrate cancrinite has been carried out from X-ray data using Rietveld refinement method. Gallosilicate cancrinite Na8[GaSiO4]6(NO34(H2O6 crystalline hexagonal with space group P63 and a = 12.77981 Å (2, c = 5.20217 Å (1, (Rwp = 0.0696 Rp = 0.0527. The results by MAS NMR spectroscopy confirmed the alternating Si, Ga ordering of the gallosilicate framework for a Si/Ga ratio of 1.0. A distribution of the quadrupolar interaction of the sodium cations caused by the enclatherated water molecules and motional effects can be suggested from the 23Na MAS NMR. Thermogravimetric investigation shows the extent of nitrate entrapment, stability within the cancrinite cage and decomposition properties. SEM clearly shows the hexagonal needle shaped crystals of nitrate cancrinite.

  14. Cogeneration techniques; Les techniques de cogeneration

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    1999-10-01

    This dossier about cogeneration techniques comprises 12 parts dealing successively with: the advantages of cogeneration (examples of installations, electrical and thermal efficiency); the combustion turbine (principle, performances, types); the alternative internal combustion engines (principle, types, rotation speed, comparative performances); the different configurations of cogeneration installations based on alternative engines and based on steam turbines (coal, heavy fuel and natural gas-fueled turbines); the environmental constraints of combustion turbines (pollutants, techniques of reduction of pollutant emissions); the environmental constraints of alternative internal combustion engines (gas and diesel engines); cogeneration and energy saving; the techniques of reduction of pollutant emissions (pollutants, unburnt hydrocarbons, primary and secondary (catalytic) techniques, post-combustion); the most-advanced configurations of cogeneration installations for enhanced performances (counter-pressure turbines, massive steam injection cycles, turbo-chargers); comparison between the performances of the different cogeneration techniques; the tri-generation technique (compression and absorption cycles). (J.S.)

  15. BN interphase in composite materials with nicalon Si-C-O fibers and with vitro ceramic matrix of MAS type; L`interphase BN dans les materiaux composites a fibres Si-C-O nicalon et a matrice vitroceramique de type MAS

    Energy Technology Data Exchange (ETDEWEB)

    Ricca, N

    1994-03-14

    BN has been suggested as an interphase in silica-based glass-ceramic matrix composites with a view to use these materials in oxidizing atmospheres at medium or high temperatures. The matrix had a boron-doped MAS (MgO-Al{sub 2}O{sub 3}-SiO{sub 2}) composition and was prepared from an hydrosol precursor. Pseudo-ID composites were prepared according to a sol impregnations/calcination/hot-pressing route. Chemical and microstructural characterizations of the fiber/matrix interfacial area were conducted by mean of TEM/EELS and AES analyses. The efficiency of BN as a coupling interphase for this particular composite system was successfully demonstrated through tensile tests performed on either as-processed or aged specimens (100 hours at 1000 deg C in air or under argon). In addition, composites maintained in air at 600 deg C, 800 deg C and 900 deg C while simultaneously loaded did not fail after 150 hours or more. Thus, a BN interphase appeared to be compatible with an oxidizing environment (i.e. the oxide matrix and/or air from 600 to 1000 deg C) and should therefore successfully replace the usual carbon interphase at least for use at medium temperatures. (author)

  16. QuBiLS-MAS, open source multi-platform software for atom- and bond-based topological (2D) and chiral (2.5D) algebraic molecular descriptors computations.

    Science.gov (United States)

    Valdés-Martiní, José R; Marrero-Ponce, Yovani; García-Jacas, César R; Martinez-Mayorga, Karina; Barigye, Stephen J; Vaz d'Almeida, Yasser Silveira; Pham-The, Hai; Pérez-Giménez, Facundo; Morell, Carlos A

    2017-06-07

    In previous reports, Marrero-Ponce et al. proposed algebraic formalisms for characterizing topological (2D) and chiral (2.5D) molecular features through atom- and bond-based ToMoCoMD-CARDD (acronym for Topological Molecular Computational Design-Computer Aided Rational Drug Design) molecular descriptors. These MDs codify molecular information based on the bilinear, quadratic and linear algebraic forms and the graph-theoretical electronic-density and edge-adjacency matrices in order to consider atom- and bond-based relations, respectively. These MDs have been successfully applied in the screening of chemical compounds of different therapeutic applications ranging from antimalarials, antibacterials, tyrosinase inhibitors and so on. To compute these MDs, a computational program with the same name was initially developed. However, this in house software barely offered the functionalities required in contemporary molecular modeling tasks, in addition to the inherent limitations that made its usability impractical. Therefore, the present manuscript introduces the QuBiLS-MAS (acronym for Quadratic, Bilinear and N-Linear mapS based on graph-theoretic electronic-density Matrices and Atomic weightingS) software designed to compute topological (0-2.5D) molecular descriptors based on bilinear, quadratic and linear algebraic forms for atom- and bond-based relations. The QuBiLS-MAS module was designed as standalone software, in which extensions and generalizations of the former ToMoCoMD-CARDD 2D-algebraic indices are implemented, considering the following aspects: (a) two new matrix normalization approaches based on double-stochastic and mutual probability formalisms; (b) topological constraints (cut-offs) to take into account particular inter-atomic relations; (c) six additional atomic properties to be used as weighting schemes in the calculation of the molecular vectors; (d) four new local-fragments to consider molecular regions of interest; (e) number of lone-pair electrons in

  17. Evolution of geodesical auscultation monitoring in power plants: Foz do Areia, Segredo and Salto Caxias; Evolucao da auscultacao geodesica no monitoramento das usinas: Foz do Areia, Segredo e Salto Caxias

    Energy Technology Data Exchange (ETDEWEB)

    Soares, Marcos Alberto; Ferreira, Elizeu Santos [Companhia Paranaense de Energia (COPEL), Curitiba, PR (Brazil)], Emails: marcos.asoares@copel.com, elizeu.sf@copel.com; Faggion, Pedro Luis; Veiga, Luis Augusto Kuenig; Nadal, Carlos Aurelio; Freitas, Silvio Rogerio Correia de; Nadal, Marco Aurelio Debus; Neves, Ricardo Vilares [Universidade Federal do Parana (UFPR), Curitiba, PR (Brazil)], Emails: faggion@ufpr.br, kngveiga@ufpr.br, cnadal@ufpr.br, sfreitas@ufpr.br, marco_nadal@yahoo.com.br, ricvilar@yahoo.com.br; Boszczowski, Roberta Bomfim [Instituto de Tecnologia para o Desenvolvimento (LACTEC), Curitiba, PR (Brazil)], Email: roberta.bomfim@lactec.org.br

    2009-10-15

    The main objective of the geodetic auscultation is to obtain cartesian coordinates of points by geodetic techniques, such as differential leveling, GPS, triangulation and traverse applied in the monitoring of certain phenomena.This paper presents some results on the integration of Geodetic Auscultation with the security instrumentation; The objective of this is to determine possible points displacements in the Salto Caxias dam. This integration is intended to provide support to the technicians to set absolute displacements of the blocks since the conventional instruments provides only relative changes. Thus, it were established a monitoring network downstream of the reservoir, formed by six concrete piles, equipped with forced centering system. This network serves to perform the external monitoring of the dam and also to support a precision traverse that is conducted within the galleries. It were also performed a differential leveling on the crest of the dam. (author)

  18. Study of an optimization protocol for radiographic techniques in computerized radiology; Estudo de um protocolo de otimizacao para as tecnicas radiograficas em radiologia computadorizada

    Energy Technology Data Exchange (ETDEWEB)

    Abrantes, Marcos Eugenio Silva

    2015-07-01

    This work is designed to produce information for the improvement of image quality to deployment in a radiology department based on previous reviews of the images by questionnaires of acceptance and quality e recognition of the parameters used in chest radiographic techniques. The data collected were divided by male, female, PA and LAT thickness, body mass index, biotypes, anthropomorphic parameters and body evaluation associated with constant voltage and the additional filtration. The results show the predominance of 35 and 40 constants with additional filtration from 0.5 to 1.5 mmAl, voltage in male: (PA and LAT) 86-92 kV and 96-112 kV, female: 85-98 kV and 96-112 kV. The charge applied to the tube for males: (PA and LAT) 5-10 mA.s and 5-16 mA.s, female: (PA and LAT) 6.3-8 mA.s and 9-14 mA.s. Absorbed doses for males: (PA and PF) 0.04-0.17 mGy and 0.03-0.19 mGy and from female (PA and PF) from 0.03-0.22 mGy and 0, 04-0.17 mGy. This procedure can be used in radiology department to implement and acceptance in the quality of images. (author)

  19. La technique de la titrisation : un outil pertinent de financement des industries minières ?

    OpenAIRE

    Yves Jégourel

    2015-01-01

    La stratégie d’intégration verticale des producteurs miniers nécessite de trouver les conditions de son financement. De nombreux schémas sont pour cela envisageables et la technique de la titrisation, bien que largement stigmatisée depuis la crise financière de 2008, doit être considérée. Plusieurs conditions doivent cependant être réunies et il est peu probable que la titrisation hors-bilan s’affirme, sous sa forme actuelle, comme un des modes importants de financement des capacités de produ...

  20. Researches, development and characterization of dosimetric materials for monitoring in irradiation processes with high doses; Pesquisa, desenvolvimento e caracterizacao de materiais dosimetricos para monitoramento em processos de irradiacao com doses altas

    Energy Technology Data Exchange (ETDEWEB)

    Galante, Ana Maria Sisti

    2003-07-01

    Dosimetric materials that can be produced in Brazil with material acquired in the national market to replace the imported dosimeters used in radiation processing were developed in this work. Mixtures of potassium nitrate and sensitizers compounds as manganese dioxide, barium nitrate and potassium bromide were prepared in the pellet form. Dosimetric characteristics such as dose-response useful range, sensitivity, environmental conditions and dose rate influences were evaluated in {sup 60}Co gamma radiation fields. Dyed polymethylmethacrylate detectors were also produced and its dosimetric characteristics were evaluated. The main characteristics evaluated in this case were: dose response useful range sensitivity, environmental conditions, dose rate influences and radiation energy dependence in gamma radiation fields and accelerated electrons beam of 0.8 to 1.5 MeV. The applied analytic technique was spectrophotometry. The calibration was performed in the irradiation facilities belonging to IPEN and certified by the International Atomic Energy Agency by means of the program IDAS (International Dose Assurance Service ) using the Fricke dosimeter. The mixture of potassium nitrate and manganese dioxide presented the best results and a wide dose range between 200 and 600 kGy. The response of the developed polymethylmethacrylate detectors are similar to the imported detectors and the dose range is characteristic to each detector and depends on the dye added in its formulation. (author)

  1. Monitoramento do teor de umidade de madeiras de Pinus elliottii Engelm. E Eucalyptus grandis W. Hill ex Maiden, sob diferentes temperaturas de secagem, através do ultra-som

    Directory of Open Access Journals (Sweden)

    Leandro Calegari

    2007-01-01

    Full Text Available With the purpose of evaluating the viability of use of ultrasonic technique to estimate the wood moisture content during the drying process, samples of Pinus elliottii Engelm. and Eucalyptus grandis W. Hill ex Maiden with dimensions of 3.5 cm thick, 10 cm width and 25 cm long were submitted to drying temperatures of 20, 40 and 70ºC. A PUNDIT ultrasonic equipment with plane face transducers by 50 KHz was used to measure sound velocity in the longitudinal direction of the wood. Results indicated increase of estimated ultrasonic speed with reduction of moisture content. This relationship showed to be valid for the wood from green to the end of the drying process, and the best determination coefficients were found in the eucalypt wood (R² = 81%. Although no influence of the species in the ultrasonic speed has been observed, this one was influenced by the wood specific gravity and by the drying temperature. The effect of the specific mass was directly proportional for the pinus wood. Opposite effect was observed in eucalypt wood. The ultrasonic speed tended to decrease as drying temperature increased for both species. Results suggest that this method presents good potential for the control of the drying process.

  2. "Faz isso, faz aquilo, mas eu tô caindo...": compreendendo a Doença de Chron "Haz eso, haz aquello, mas yo estoy cayendo...": comprendiendo la enfermedad de Chron "Do this, do that, but I'm falling down...": understanding Chron's disease

    Directory of Open Access Journals (Sweden)

    Andrea Castelli

    2007-03-01

    Full Text Available Buscando compreender o significado e o impacto da doença de Chron na vida de seu portador, desenvolvemos este estudo, de natureza qualitativa, optando pela História Oral de Vida como referencial metodológico, tendo como base filosófica a corrente monista, advinda de Hipócrates, em que a prática médica tem por objeto a pessoa doente em sua totalidade, levando em conta seu temperamento e a sua história. A terapêutica deve restabelecer a harmonia da pessoa com seu ambiente e consigo mesma , trata-se de uma medicina integradora e dinâmica, que corresponde aos primórdios da medicina psicossomática. O estudo da doença de Chron, por meio da compreensão psicossomática, permitiu que analisássemos os sintomas, não como corpos estranhos a serem erradicados, mas como mensageiros de um apelo a ser compreendido. Por intermédio deles, pode ser resgatada a história de um indivíduo que, se conscientemente vivida e analisada, permite o desenvolvimento até níveis mais evoluídos de entendimento.Buscando comprender el significado y el impacto de la Enfermedad de Chron en la vida de su portador, desarrollamos este estudio, de naturaleza cualitativa, optando por la Historia Oral de Vida como referencial metodológico, y teniendo como base filosófica la corriente monista, advenida de Hipócrates, donde la práctica médica tiene por objeto a la persona enferma en su totalidad, teniendo en cuenta su temperamento y su historia. La terapéutica debe restablecer la armonía de la persona con su ambiente y consigo misma y se trata de una medicina integradora y dinámica, que corresponde a los inicios de la medicina psicosomática. El Estudio de la enfermedad de Chron, por medio de la comprensión psicosomática, permitió que analizásemos los síntomas, no como cuerpos extraños a ser erradicados, mas como mensajeros de un apelo a ser comprendido. Por intermedio de ellos, puede ser rescatada la historia de un individuo que, si conscientemente vivida

  3. Surface science techniques

    CERN Document Server

    Bracco, Gianangelo

    2013-01-01

    The book describes the experimental techniques employed to study surfaces and interfaces. The emphasis is on the experimental method. Therefore all chapters start with an introduction of the scientific problem, the theory necessary to understand how the technique works and how to understand the results. Descriptions of real experimental setups, experimental results at different systems are given to show both the strength and the limits of the technique. In a final part the new developments and possible extensions of the techniques are presented. The included techniques provide microscopic as well as macroscopic information. They cover most of the techniques used in surface science.

  4. Training techniques for industry

    International Nuclear Information System (INIS)

    Jones, D.W.

    1978-01-01

    The advantages and disadvantages of commonly used training techniques in relation to cost-effective, prevention-oriented Quality Assurance are examined. Important questions are whether training techniques teach cost effectiveness and whether the techniques are, themselves, cost effective. To answer these questions, criteria for evaluating teaching techniques for cost effectiveness were developd, and then commonly used techniques are evaluated in terms of specific training program objectives. Motivation of personnel is also considered important to the success of a training program, and methods are outlined by which recognition of the academic quality of industrial training can be used as a motivational technique

  5. Monitoring of mass flux of catalyst FCC in a Cold Pilot Unit by gamma radiation transmission; Monitoramento da taxa de fluxo do catalisador FCC em uma unidade piloto a frio por medicao de transmissao gama

    Energy Technology Data Exchange (ETDEWEB)

    Brito, Marcio Fernando Paixao de

    2014-09-01

    This paper proposes a model for monitoring the mass flow of catalyst FCC - Fluid Catalytic Cracking - in a CPU - Cold Pilot unit - due to the injection of air and solid by gamma radiation transmission. The CPU simplifies the process of FCC, which is represented by the catalyst cycle, and it was constructed of acrylic, so that the flow can be visualized. The CPU consists of riser separation chamber and return column, and simulates the riser reactor of the FCC process. The catalyst is injected into the column back to the base of the riser, an inclined tube, where the compressed air means that there fluidization along the riser. When the catalyst comes in the separation chamber, the solid phase is sent to the return column, and the gas phase exits the system through one of the four cyclones at the top of the separation chamber. The transmission gamma of measures will be made by means of three test sections that have source and detector shielded. Pressure drop in the riser measurements are made through three pressure gauges positioned on the riser. The source used was Am-241 gamma ray with energy of 60 keV, and detector used was a scintillator of NaI (Tl) of 2 {sup x} 2{sup .} Measures the mass flow of catalyst are made by varying the seal of the catalyst, and density of solid in the riser because with the combination of these measures can determine the speed of the catalyst in the riser. The results show that the transmission gamma is a suitable technique for monitoring the flow of catalyst, flow model in CPU is annular, tomography third generation is more appropriate to study the CPU and the density variation in circulation in the CPU decreases linearly with increasing air flow. (author)

  6. Phosphole complexes of Gold(I) halides: Comparison of solution and solid-state structures by a combination of solution and CP/MAS 31P NMR spectroscopy and x-ray crystallography

    International Nuclear Information System (INIS)

    Attar, S.; Nelson, J.H.; Bearden, W.H.; Alcock, N.W.; Alyea, E.C.

    1990-01-01

    A series of complexes of 1-phenyldibenzophosphole (DBP), 1-phenyl-3,4,-dimethylphosphole (DMPP), and triphenylphosphine of the type L n AuX (n = 1, L = DBP, DMPP, Ph 3 P, X = Cl, Br, I; n = 3, L = DBP, X = Cl, Br, I; n = 3, L = Ph 3 P, X = Cl; n = 4, L = DBP, DMPP, X = PF 6 ) have been prepared and characterized. The structures of (DBP)AuCl (1), (DBP) 3 AuCl (2), and (DMPP)AuCl (3) have been determined from three-dimensional x-ray data collected by counter methods. Crystal structure of the complexes is reported. The CP/MAS 31 P( 1 H) NMR spectrum of complex 1 shows two resonances in a 1:1 intensity ratio, and the CP/MAS 31 P( 1 H) NMR spectrum of complex 3 shows three resonances in a 1:1:1 intensity ratio for reasons that are not yet understood. Though the three phospholes are crystallographically inequivalent (d(AuP) = 2.359 (1), 2.382 (1), and 2.374 (2) angstrom) the molecule has effective C s symmetry as evidenced by the observation of two 31 P resonances in a 2:1 intensity ratio in its CP/MAS 31 P( 1 H) NMR spectrum. Variable-temperature 31 P( 1 H) NMR spectra obtained on solutions of LAuCl + L in various ratios were analyzed to determine the nature of the species present in solution and to gain information regarding their relative stabilities as a function of the nature of the phosphine. 79 refs., 8 figs., 9 tabs

  7. UNA DÉCADA DEL GOBIERNO DEL M.A.S. EN BOLIVIA: UN BALANCE GLOBAL / A DECADE OF GOVERNMENT OF ‘MAS’ IN BOLIVIA: A GLOBAL BALANCE

    Directory of Open Access Journals (Sweden)

    Luis Miguel Uharte Pozas

    2017-12-01

    Full Text Available This paper aims to carry out an analysis about the government experience of the Movement to Socialism (MAS in Bolivia since Evo Morales became president in 2006 to the present, identifying the main changes and conflicts that have occurred in four areas: social policy, domestic policy, foreign policy, and economy. The methodology is based on the collection of documents from various sources (public and business institutions, researchers, and recognized research centers, and interviews with various social actors (academics, politicians. We conclude that there have been substantial advances in terms of national sovereignty and economic model (overcoming neoliberalism, despite the contradictions and conflicts with sectors of internal dissent.

  8. Definição do posicionamento de sensores para monitoramento da água no solo em bananeira irrigada por diferentes sistemas de irrigação localizada Sensor placement for soil water monitoring in banana crop irrigated by drip irrigation systens

    Directory of Open Access Journals (Sweden)

    Eugênio F. Coelho

    2010-08-01

    Full Text Available O uso eficiente da água na irrigação localizada dependerá, além de outros fatores, também do correto monitoramento da água no solo. Portanto, este trabalho teve como objetivo caracterizar as zonas efetivas de comprimento de raízes e de extração de água, bem como indicar o correto posicionamento de sensores de água no solo para o manejo da irrigação por gotejamento na bananeira em fase de produção. No experimento, conduzido na Embrapa Mandioca e Fruticultura Tropical, foram estudados diferentes sistemas de irrigação localizada, diante dos seguintes tratamentos: T1 - dois emissores de 4 L h-1 por planta em uma lateral por fileira de plantas; T2 - quatro emissores de 4 L h-1 por planta em uma lateral por fileira de plantas; T3 - cinco emissores de 4 L h-1 por planta em faixa contínua com uma lateral por fileira. Pelos resultados obtidos, pode-se observar que as regiões mais adequadas para a instalação de sensores de umidade no solo nos tratamentos T1, T2 e T3 são as limitadas pelas distâncias e profundidades de 0,2 m e 0,4 m; 0,5 m e 0,35 m; 0,55 m e 0,35 m, respectivamente.The efficient use of water for drip irrigation will depend, among other factors, the correct monitoring of water in the soil profile. This work aimed to characterize root zones of effective root length and effective root water uptake and also to indicate the correct sensors location in the soil profile for drip irrigation management in banana crop during the production stage of the first cycle. The experiment was carried out at the Embrapa Cassava & Tropical Fruits, under different systems: T1 - one lateral per plant row with two 4 L h-1 emitters per plant; T2 - one lateral per plant row with four 4 L h-1 emitters per plant; T3 - one lateral per plant row as line source, with five 4 L h-1 emitters per plant. The results showed that the more appropriate regions for soil water sensor placement in treatments T1, T2 and T3, should correspond to zones limited

  9. Blindagem eletromagnética, aterramento e proteção contra surtos de tensão em equipamentos para monitoramento automático do teor de água no solo Electromagnetic shielding, grounding and protection against voltage surges in equipments for automatic soil-water measurements

    Directory of Open Access Journals (Sweden)

    Claudia F. A. Teixeira

    2004-04-01

    Full Text Available O objetivo do presente trabalho foi implementar um sistema de blindagem eletromagnética, aterramento e proteção contra surtos de tensão na instalação de instrumental para o monitoramento automático do teor de água no solo. O experimento foi instalado em Piracicaba, São Paulo, em que os equipamentos utilizados foram um testador de cabos marca Tektronix, que opera pelo princípio da reflectometria no domínio do tempo e um sistema de aquisição de dados marca Campbell Scientific Inc. (CSI, que controla e analisa as formas de onda produzidas pelo testador de cabos. A umidade volumétrica foi obtida indiretamente por meio de sensores inseridos no solo, os quais medem a constante dielétrica do mesmo. Utilizaram-se tubos galvanizados para a blindagem eletromagnética dos cabos e hastes "cooperweld", cordoalha de cobre e terminais bimetálicos para o sistema de aterramento. Para o sistema de proteção eletroeletrônica, utilizaram-se um disjuntor para a separação do circuito de alimentação, protetor de surtos, "no-breaks" e medidor de resistência de terra. Face aos resultados obtidos, pode-se concluir que o sistema proposto, ao utilizar material geralmente preexistente em locais de pesquisa agropecuária, apresentou uma proteção eficaz.The objective of this paper was to implement an electromagnetic shielding, grounding and voltage surge protection in equipments for automatic soil water monitoring. The experiment was carried out in Piracicaba, São Paulo State, Brazil, using a Tektronix Cable Tester (Model 1502 B that operates by time domain reflectometry (TDR and a datalogger (CR10X, Campbell Scientific Inc., CSI to control and analyze the waveforms produced by the cable tester. The water content was indirectly obtained by measuring the dielectric constant through probes inserted in the soil. For electromagnetic shielding the energy and signal cables were inserted in galvanized pipes, linked together by means of copper wire fixed in

  10. Metodologia de construção de um painel de indicadores para o monitoramento e a avaliação da gestão do SUS Methodology for construction of a panel of indicators for monitoring and evaluation of unified health system (SUS management

    Directory of Open Access Journals (Sweden)

    Edson Mamoru Tamaki

    2012-04-01

    Full Text Available Este estudo teve como objetivo desenvolver uma metodologia de construção de um Painel de Monitoramento e Avaliação da Gestão do Sistema Único de Saúde (SUS. O processo participativo utilizado e a sistematização realizada permitiram identificar uma estratégia efetiva para a construção de instrumentos de gestão em parceria entre pesquisadores, instituições acadêmicas e gestores do SUS. A sistematização final do Painel selecionou indicadores da gestão do SUS em termos de Demandas, Insumos, Processos, Produtos e Resultados de forma a disponibilizar um instrumento simples, ágil e útil para a avaliação em qualquer instância de gestão e mais transparente e de mais fácil comunicação com todos os interessados na tomada de decisão. Tomar a gestão do SUS como objeto destes processos e práticas em seus aspectos normativos possibilitou o diálogo entre teorias sistêmicas e aquelas que consideram a centralidade do ator social no processo de tomada de decisão.This study sought to develop methodology for the construction of a Panel for the Monitoring and Evaluation of Management of the Unified Health System (SUS. The participative process used in addition to the systematization conducted made it possible to identify an effective strategy for building management tools in partnership with researchers, academic institutions and managers of the SUS. The final systematization of the Panel selected indicators for the management of the SUS in terms of Demand, Inputs, Processes, Outputs and Outcomes in order to provide a simple, versatile and useful tool for evaluation at any level of management and more transparent and easier communication with all stakeholders in decision-making. Taking the management of the SUS as the scope of these processes and practices in all normative aspects enabled dialog between systemic theories and those which consider the centrality of the social actor in the decision-making process.

  11. Genetic monitoring of a Santa Ines herd using microsatellite markers near or linked to the sheep MHC Monitoramento genético de um rebanho da raça Santa Inês a partir de marcadores microssatélites próximos ou ligados ao MHC ovino

    Directory of Open Access Journals (Sweden)

    César Daniel Petroli

    2009-04-01

    monitoramento ao longo dos anos é desejável e deve ser implantada como ferramenta adicional visando, por exemplo, indicação de acasalamentos e descarte de animais.

  12. A importância da determinação da hemoglobina glicada no monitoramento das complicações crônicas do diabetes mellitus The importance of glycated hemoglobin determination in the management of chronic complications associated with diabetes mellitus

    Directory of Open Access Journals (Sweden)

    Andreza Fabro de Bem

    2006-06-01

    Full Text Available O diabetes é uma situação clínica muito freqüente que envolve cerca de 7% da população mundial. Por essa razão muitos esforços têm sido empregados na implementação de métodos de monitoramento e no desenvolvimento de terapias efetivas para o seu controle. A hemoglobina glicada (HbA1c é o teste mais indicado na quantificação do risco de complicações crônicas em pacientes diabéticos. O Diabetes Control and Complications Trial (DCCT e o United Kingdom Prospective Diabetes Study (UKPDS concluíram que o risco de complicações em pacientes diabéticos é diretamente proporcional ao controle glicêmico, determinado através dos níveis de HbA1c. A medida exata e precisa da HbA1c é uma questão importante para os laboratórios clínicos, sendo que vários fatores podem afetar as determinações, levando a resultados equivocados. O objetivo deste estudo é demonstrar os diferentes métodos para a quantificação da HbA1c, bem como discutir os problemas mais freqüentes de padronização dessa determinação.Diabetes is a widespread disease, involving about 7% of the entire world population. For this reason, many efforts have been devoted to the wide application of valid monitoring procedures and to the development of effective therapeutic approaches. Glycated hemoglobin (HbA1c is the pre-eminent factor for quantifying the risk of chronic complications in patients with diabetes. The Diabetes Control and Complications Trial (DCCT and United Kingdom Prospective Diabetes Study (UKPDS, demonstrated conclusively that risks for complications in patients with diabetes are directly related to glycemic control, as measured by glycated hemoglobin (HbA1c. Accurate determination of HbA1c is an important issue for clinical laboratories and several factors may affect and lead to erroneous results. The main objective of this study is to show the different methods for glycated hemoglobin quantification and to discuss the most frequent problems of

  13. Airway Clearance Techniques (ACTs)

    Medline Plus

    Full Text Available ... to loosen mucus from airway walls. See how different airway clearance techniques work to help you clear the thick, sticky mucus ... Offer their tips for fitting ACTs into daily life Airway Clearance Techniques | Webcast ... Facebook Twitter ...

  14. Nuclear techniques in industry

    International Nuclear Information System (INIS)

    Hammad, F.H.

    1994-01-01

    Nuclear techniques are utilized in almost every industry. The discussion in this paper includes discussions on tracer methods and uses nucleonic control systems technology; non-destructive testing techniques and radiation technology. 1 fig., 2 tabs

  15. Airway Clearance Techniques (ACTs)

    Medline Plus

    Full Text Available ... decisions about your health care. CF Genetics: The Basics CF Mutations Video Series Find Out More About ... of Breathing Technique Airway Clearance Techniques Autogenic Drainage Basics of Lung Care Chest Physical Therapy Coughing and ...

  16. Airway Clearance Techniques (ACTs)

    Medline Plus

    Full Text Available ... Active Cycle of Breathing Technique Airway Clearance Techniques Autogenic Drainage Basics of Lung Care Chest Physical Therapy ... clearance. Facebook Twitter Email More Related Content Medications Autogenic Drainage Positive Expiratory Pressure High-Frequency Chest Wall ...

  17. Airway Clearance Techniques (ACTs)

    Medline Plus

    Full Text Available ... a range of treatment options. Airway Clearance Active Cycle of Breathing Technique Airway Clearance Techniques Autogenic Drainage ... LEGACY GIFT Sponsor a Participant CF Climb CF Cycle for Life Great Strides Xtreme Hike Participate In ...

  18. Airway Clearance Techniques (ACTs)

    Medline Plus

    Full Text Available ... many challenges, including medical, social, and financial. By learning more about how you can manage your disease every day, you can ultimately help find a ... Cycle of Breathing Technique Airway Clearance Techniques Autogenic ...

  19. Airway Clearance Techniques (ACTs)

    Medline Plus

    Full Text Available ... Cycle of Breathing Technique Airway Clearance Techniques Autogenic Drainage Basics of Lung Care Chest Physical Therapy Coughing ... Facebook Twitter Email More Related Content Medications Autogenic Drainage Positive Expiratory Pressure High-Frequency Chest Wall Oscillation ( ...

  20. Análise do monitoramento de descargas atmosféricas na área de concessão da companhia força e luz do oeste em Guarapuava, Estado do Paraná = Analysis of the monitoring of atmospheric discharges in the area of cocession of the western força e luz company in Guarapuava, state of Paraná

    Directory of Open Access Journals (Sweden)

    Aparecido Ribeiro de Andrade

    2007-01-01

    Full Text Available Objetivando uma análise do monitoramento da incidência de descargasatmosféricas, a região de concessão da Companhia Força e Luz do Oeste (CFLO, localizada no município de Guarapuava, Estado do Paraná, foi selecionada para um estudo realizado no período de janeiro a dezembro de 2003. Após a descrição da dinâmica da entrada de massas de ar, foi possível identificar a ocorrência de descargas atmosféricas e compará-las com as interrupções de energia. Para tanto, foram criados mapas de densidade de descargas atmosféricas dentro da área de concessão da CFLO para posterior análise de sua influênciano fornecimento de energia elétrica. O monitoramento das descargas atmosféricas e a comparação da incidência desse fenômeno com a ocorrência de interrupções no fornecimento de energia elétrica possibilitaram concluir que tais eventos estão diretamenterelacionados, e que a área rural da região em estudo sofre uma interferência maior.Aiming to analyze the monitoring of the atmospheric discharges incidence, the concession area of Companhia Força e Luz do Oeste (CFLO – Western Power and Light Company, located in the district of Guarapuava, state of Paraná, was chosen for a study developed in2003, from January to December. After the air masses dynamics description, it was possible to identify the occurrence of atmospheric discharges and to compare them to the energy interruptions. To that end, atmospheric discharges density maps were created within the CFLO concession area for a later analysis of their influence in the electric energy supply. The monitoring of the atmospheric discharges and the comparison between this phenomenon and the occurrence of interruptions in the electric energy supply enabled this study. Results showed that such events are directly related, and that the rural area of the region under study underwent a major interference.

  1. Radiation scattering techniques

    International Nuclear Information System (INIS)

    Edmonds, E.A.

    1986-01-01

    Radiation backscattering techniques are useful when access to an item to be inspected is restricted to one side. These techniques are very sensitive to geometrical effects. Scattering processes and their application to the determination of voids, thickness measuring, well-logging and the use of x-ray fluorescence techniques are discussed. (U.K.)

  2. Point of Technique

    African Journals Online (AJOL)

    .

    Minimally invasive techniques are becoming popular choice for the recent times. These techniques are lowering the cost and giving the best cosmetic results. For cardiovascular surgery these techniques are much more newer and much more unknown. Open lumbar sympathectomy for certain indications is a very well ...

  3. Handling of uncertainty due to interference fringe in FT-NIR transmittance spectroscopy - Performance comparison of interference elimination techniques using glucose-water system

    Science.gov (United States)

    Beganović, Anel; Beć, Krzysztof B.; Henn, Raphael; Huck, Christian W.

    2018-05-01

    The applicability of two elimination techniques for interferences occurring in measurements with cells of short pathlength using Fourier transform near-infrared (FT-NIR) spectroscopy was evaluated. Due to the growing interest in the field of vibrational spectroscopy in aqueous biological fluids (e.g. glucose in blood), aqueous solutions of D-(+)-glucose were prepared and split into a calibration set and an independent validation set. All samples were measured with two FT-NIR spectrometers at various spectral resolutions. Moving average smoothing (MAS) and fast Fourier transform filter (FFT filter) were applied to the interference affected FT-NIR spectra in order to eliminate the interference pattern. After data pre-treatment, partial least squares regression (PLSR) models using different NIR regions were constructed using untreated (interference affected) spectra and spectra treated with MAS and FFT filter. The prediction of the independent validation set revealed information about the performance of the utilized interference elimination techniques, as well as the different NIR regions. The results showed that the combination band of water at approx. 5200 cm-1 is of great importance since its performance was superior to the one of the so-called first overtone of water at approx. 6800 cm-1. Furthermore, this work demonstrated that MAS and FFT filter are fast and easy-to-use techniques for the elimination of interference fringes in FT-NIR transmittance spectroscopy.

  4. Radiation doses during chest examinations using dose modulation techniques in multislice CT scanner

    International Nuclear Information System (INIS)

    Livingstone, Roshan S.; Pradip, Joe; Dinakran, Paul M.; Srikanth, B.

    2010-01-01

    Objectives: To evaluate the radiation dose and image quality using a manual protocol and dose modulation techniques in a 6-slice CT scanner. Materials and Methods: Two hundred and twenty-one patients who underwent contrast-enhanced CT of the chest were included in the study. For the manual protocol settings, constant tube potential (kV) and tube current-time product (mAs) of 140 kV and 120 mAs, respectively, were used. The angular and z-axis dose modulation techniques utilized a constant tube potential of 140 kV; mAs values were automatically selected by the machine. Effective doses were calculated using dose-length product (DLP) values and the image quality was assessed using the signal-to-noise (SNR) ratio values. Mean effective doses using manual protocol for patients of weights 40-60 kg, 61-80 kg, and 81 kg and above were 8.58 mSv, 8.54 mSv, and 9.07 mSv, respectively. Mean effective doses using z-axis dose modulation for patients of weights 40-60 kg, 61-80 kg, and 81 kg and above were 4.95 mSv, 6.87 mSv, and 10.24 mSv, respectively. The SNR at the region of the liver for patients of body weight of 40-60 kg was 5.1 H, 6.2 H, and 8.8 H for manual, angular, and z-axis dose modulation, respectively. Conclusion: Dose reduction of up to 15% was achieved using angular dose modulation and of up to 42% using z-axis dose modulation, with acceptable diagnostic image quality compared to the manual protocol. (author)

  5. Nuclear techniques in hydrology

    International Nuclear Information System (INIS)

    Moser, H.

    1976-01-01

    The nuclear techniques used in hydrology are usually tracer techniques based on the use of nuclides either intentionally introduced into, or naturally present in the water. The low concentrations of these nuclides, which must be detected in groundwater and surface water, require special measurement techniques for the concentrations of radioactive or of stable nuclides. The nuclear techniques can be used most fruitfully in conjunction with conventional methods for the solution of problems in the areas of hydrology, hydrogeology and glacier hydrology. Nuclear techniques are used in practice in the areas of prospecting for water, environment protection and engineering hydrogeology. (orig.) [de

  6. Specific radiography technique

    International Nuclear Information System (INIS)

    Abdul Nassir Ibrahim; Azali Muhammad; Ab. Razak Hamzah; Abd. Aziz Mohamed; Mohamad Pauzi Ismail

    2008-01-01

    Beside radiography testing using x-ray machine and gamma source, there are several technique that developed specifically to complete the testing that cannot be done with the two earlier. This technique was specific based on several factor, for the example, the advantages of neutron and electron using to show the image was unique compare to x-ray and gamma. Besides that, these special radiography techniques maybe differ in how to detect the radiation get through the object. These technique can used to inspect thin or specimen that contained radioactive material. There are several technique will discussed in this chapter such as neutron radiography, electron radiography, fluoroscopy and also autoradiography.

  7. Low current beam techniques

    Energy Technology Data Exchange (ETDEWEB)

    Saint, A; Laird, J S; Bardos, R A; Legge, G J.F. [Melbourne Univ., Parkville, VIC (Australia). School of Physics; Nishijima, T; Sekiguchi, H [Electrotechnical Laboratory, Tsukuba (Japan).

    1994-12-31

    Since the development of Scanning Transmission Microscopy (STIM) imaging in 1983 many low current beam techniques have been developed for the scanning (ion) microprobe. These include STIM tomography, Ion Beam Induced Current, Ion Beam Micromachining and Microlithography and Ionoluminense. Most of these techniques utilise beam currents of 10{sup -15} A down to single ions controlled by beam switching techniques This paper will discuss some of the low beam current techniques mentioned above, and indicate, some of their recent applications at MARC. A new STIM technique will be introduced that can be used to obtain Z-contrast with STIM resolution. 4 refs., 3 figs.

  8. Low current beam techniques

    Energy Technology Data Exchange (ETDEWEB)

    Saint, A.; Laird, J.S.; Bardos, R.A.; Legge, G.J.F. [Melbourne Univ., Parkville, VIC (Australia). School of Physics; Nishijima, T.; Sekiguchi, H. [Electrotechnical Laboratory, Tsukuba (Japan).

    1993-12-31

    Since the development of Scanning Transmission Microscopy (STIM) imaging in 1983 many low current beam techniques have been developed for the scanning (ion) microprobe. These include STIM tomography, Ion Beam Induced Current, Ion Beam Micromachining and Microlithography and Ionoluminense. Most of these techniques utilise beam currents of 10{sup -15} A down to single ions controlled by beam switching techniques This paper will discuss some of the low beam current techniques mentioned above, and indicate, some of their recent applications at MARC. A new STIM technique will be introduced that can be used to obtain Z-contrast with STIM resolution. 4 refs., 3 figs.

  9. Pulse holographic measurement techniques

    International Nuclear Information System (INIS)

    Kim, Cheol Jung; Baik, Seong Hoon; Hong, Seok Kyung; Kim, Jeong Moog; Kim, Duk Hyun

    1992-01-01

    With the development of laser, remote inspection techniques using laser have been growing on. The inspection and measurement techniques by pulse holography are well-established technique for precise measurement, and widely used in various fields of industry now. In nuclear industry, this technology is practically used because holographic inspection is remote, noncontact, and precise measurement technique. In relation to remote inspection technology in nuclear industry, state-of-the art of pulse HNDT (Holographic non-destructive testing) and holographic measurement techniques are examined. First of all, the fundamental principles as well as practical problems for applications are briefly described. The fields of pulse holography have been divided into the HNDT, flow visualization and distribution study, and other application techniques. Additionally holographic particle study, bubble chamber holography, and applications to other visualization techniques are described. Lastly, the current status for the researches and applications of pulse holography to nuclear industry which are carried out actively in Europe and USA, is described. (Author)

  10. Tautas partijas reklāmas un sabiedrisko attiecību kampaņas pirms 7. un 9. Saeimas vēlēšanām

    OpenAIRE

    Velika, Anna

    2007-01-01

    Tautas partija tika nodibināta 1998.gada maijā, īsi pirms 7.Saeimas vēlēšanām. Pateicoties harizmātiskajam līderim A.Šķēlem, masīvai reklāmas un sabiedrisko attiecību kampaņai, kā arī tautas uzticībai un cerībām jaunā partija gūst uzvaru vēlēšanās. Taču uzmanību piesaista fakts, ka šī partija, kas ir neraksturīgi pašreizējai Latvijas politiskajai skatuvei, spēj iekarot stabilu vietu gan valdībā, gan pašvaldībās, un ar profesionālu kampaņu palīdzību gūt panākumus arī divās nākamajās Saeimas vē...

  11. Structure determination of uniformly {sup 13}C, {sup 15}N labeled protein using qualitative distance restraints from MAS solid-state {sup 13}C-NMR observed paramagnetic relaxation enhancement

    Energy Technology Data Exchange (ETDEWEB)

    Tamaki, Hajime [Hokkaido University, Graduate School of Life Science (Japan); Egawa, Ayako [Osaka University, Institute for Protein Research (Japan); Kido, Kouki [Hokkaido University, Graduate School of Life Science (Japan); Kameda, Tomoshi [National Institute of Advanced Industrial Science and Technology, Biotechnology Research Institute for Drug Discovery (Japan); Kamiya, Masakatsu; Kikukawa, Takashi; Aizawa, Tomoyasu [Hokkaido University, Faculty of Advanced Life Science (Japan); Fujiwara, Toshimichi [Osaka University, Institute for Protein Research (Japan); Demura, Makoto, E-mail: demura@sci.hokudai.ac.jp [Hokkaido University, Faculty of Advanced Life Science (Japan)

    2016-01-15

    Magic angle spinning (MAS) solid-state nuclear magnetic resonance (NMR) is a powerful method for structure determination of insoluble biomolecules. However, structure determination by MAS solid-state NMR remains challenging because it is difficult to obtain a sufficient amount of distance restraints owing to spectral complexity. Collection of distance restraints from paramagnetic relaxation enhancement (PRE) is a promising approach to alleviate this barrier. However, the precision of distance restraints provided by PRE is limited in solid-state NMR because of incomplete averaged interactions and intermolecular PREs. In this report, the backbone structure of the B1 domain of streptococcal protein G (GB1) has been successfully determined by combining the CS-Rosetta protocol and qualitative PRE restraints. The derived structure has a Cα RMSD of 1.49 Å relative to the X-ray structure. It is noteworthy that our protocol can determine the correct structure from only three cysteine-EDTA-Mn{sup 2+} mutants because this number of PRE sites is insufficient when using a conventional structure calculation method based on restrained molecular dynamics and simulated annealing. This study shows that qualitative PRE restraints can be employed effectively for protein structure determination from a limited conformational sampling space using a protein fragment library.

  12. Microwave assisted saponification (MAS) followed by on-line liquid chromatography (LC)-gas chromatography (GC) for high-throughput and high-sensitivity determination of mineral oil in different cereal-based foodstuffs.

    Science.gov (United States)

    Moret, Sabrina; Scolaro, Marianna; Barp, Laura; Purcaro, Giorgia; Conte, Lanfranco S

    2016-04-01

    A high throughput, high-sensitivity procedure, involving simultaneous microwave-assisted extraction (MAS) and unsaponifiable extraction, followed by on-line liquid chromatography (LC)-gas chromatography (GC), has been optimised for rapid and efficient extraction and analytical determination of mineral oil saturated hydrocarbons (MOSH) and mineral oil aromatic hydrocarbons (MOAH) in cereal-based products of different composition. MAS has the advantage of eliminating fat before LC-GC analysis, allowing an increase in the amount of sample extract injected, and hence in sensitivity. The proposed method gave practically quantitative recoveries and good repeatability. Among the different cereal-based products analysed (dry semolina and egg pasta, bread, biscuits, and cakes), egg pasta packed in direct contact with recycled paperboard had on average the highest total MOSH level (15.9 mg kg(-1)), followed by cakes (10.4 mg kg(-1)) and bread (7.5 mg kg(-1)). About 50% of the pasta and bread samples and 20% of the biscuits and cake samples had detectable MOAH amounts. The highest concentrations were found in an egg pasta in direct contact with recycled paperboard (3.6 mg kg(-1)) and in a milk bread (3.6 mg kg(-1)). Copyright © 2015 Elsevier Ltd. All rights reserved.

  13. Ab initio study of structure and stability of thiocarbonates, thiosilicates, thionitrates, thiophosphates, thioborates and thioaluminates L2AS3 and MAS3 (L=Li, Na; M=Be, Mg; A=C, Si, N+, P+, B-, Al-)

    International Nuclear Information System (INIS)

    Charkin, D.O.; Makki, M.L.; Charkin, O.P.

    1998-01-01

    Nonempiric calculations of potential energy surfaces for the family of isoelectron molecules and ions of lithium and sodium thiosalts of the MAS 3 type atr carried out within the frames of the MP2/6-31G * +ZPE(HF/6-31G * ) and MP4SDTQ/6-31(+)G + //MP2/6-31G * +ZPE(MP2/6-31G * ) approximations. Plane structures C s with disulfide bridge S-S are found to be most preferable for thionitrates, angular structure C s with one bridge and two end sulfur atoms - for thioborate negative ions BeBS 3 , MgBS 3 and molecules B 2 S 3 , Al 2 S 3 and structures C 2v with bidentate coordination of cations and thioanion AS 3 n- - for remaining systems. Equilibrium geometric parameters and relative energies of isomers, energies of their decomposition, frequencies and IR-intensities of normal oscillations are determined, effect of electron correlation on the calculation results is analyzed. Ortho-meta-isomery in thioborates and thioaluminates, deformation and polarization of thioanions under the effect of alkali and alkaline-earth cations and trends in chomping molecular properties in various series of the L 2 AS 3 and MAS 3 salts are discussed

  14. Sistema RTP: uma técnica poderosa para o monitoramento da formação de nanotubos de carbono durante o processo por deposição de vapor químico TPR system: a powerful technique to monitor carbon nanotube formation during chemical vapour deposition

    Directory of Open Access Journals (Sweden)

    Juliana Cristina Tristão

    2010-01-01

    Full Text Available In this work, a TPR (Temperature Programmed Reduction system is used as a powerful tool to monitor carbon nanotubes production during CVD (Chemical Vapour Deposition, The experiments were carried out using catalyst precursors based on Fe-Mo supported on Al2O3 and methane as carbon source. As methane reacts on the Fe metal surface, carbon is deposited and H2 is produced. TPR is very sensitive to the presence of H2 and affords information on the temperature where catalyst is active to form different forms of carbon, the reaction kinetics, the catalyst deactivation and carbon yields.

  15. Uso da Técnica do Micro-Hematócrito para Predição do Peso Corporal e de Características Reprodutivas em Frangos de Corte Utilization of Micro-Hematocrit Technique on Body Weight and Reproductive Traits Prediction in Broiler Chickens

    Directory of Open Access Journals (Sweden)

    Millor Fernandes do Rosário

    2002-06-01

    Full Text Available O hematócrito é uma metodologia indireta utilizada no monitoramento da síndrome ascítica que poderia ser utilizada também para avaliar o peso corporal e características reprodutivas em frangos de corte. Objetivou-se com este trabalho avaliar a técnica do micro-hematócrito em relação ao peso corporal e características reprodutivas (fertilidade, eclodibilidade e nascimento visando sua utilização pelos programas de melhoramento genético. Dois grupos contrastantes foram constituídos, baseados na seleção fenotípica de 630 reprodutores de 18 genótipos para a característica hematócrito. Progênies das aves selecionadas, 74 pintos não sexados (40 do grupo de hematócrito alto e 34 do grupo baixo foram criados com manejo convencional. Os pesos corporais e os valores de hematócrito foram mensurados aos 14 e 42 dias de idade. Para avaliar as características reprodutivas, ovos de 42 matrizes (22 do grupo alto e 20 do baixo foram incubados. As médias foram estimadas utilizando-se um modelo linear com o efeito fixo do grupo genético. Os pintos do grupo baixo apresentaram as maiores médias de peso corporal (305,59 e 1387,06 g, diferindo dos pintos do grupo alto os quais apresentaram médias de peso de 243,56 e 1128,11 g aos 14 e 42 dias de idade, respectivamente. Também para o valor do hematócrito os grupos diferiram significativamente. Para as características reprodutivas, não se verificou diferenças significativas entre os grupos, sendo as médias gerais para fertilidade de 93,8 e 94,9%, para eclodibilidade de 98,2 e 93,9% e para nascimento de 89,3 e 82,4%, respectivamente, para alto e baixo hematócrito. Concluiu-se que a técnica do micro-hematócrito pode ser empregada para avaliação do peso corporal, mas não para características reprodutivas.Hematocrit is an indirect method used to monitor ascites, which might be used also on body weight and reproductive traits evalution in broiler chickens. The aim of this paper was

  16. Quality Attribute Techniques Framework

    Science.gov (United States)

    Chiam, Yin Kia; Zhu, Liming; Staples, Mark

    The quality of software is achieved during its development. Development teams use various techniques to investigate, evaluate and control potential quality problems in their systems. These “Quality Attribute Techniques” target specific product qualities such as safety or security. This paper proposes a framework to capture important characteristics of these techniques. The framework is intended to support process tailoring, by facilitating the selection of techniques for inclusion into process models that target specific product qualities. We use risk management as a theory to accommodate techniques for many product qualities and lifecycle phases. Safety techniques have motivated the framework, and safety and performance techniques have been used to evaluate the framework. The evaluation demonstrates the ability of quality risk management to cover the development lifecycle and to accommodate two different product qualities. We identify advantages and limitations of the framework, and discuss future research on the framework.

  17. Tracer techniques in microelectronics

    International Nuclear Information System (INIS)

    Flachowsky, J.; Freyer, K.

    1981-01-01

    Tracer technique and neutron activation analysis are capable of measuring impurities in semiconductor material or on the semiconductor surface in a very low concentration range. The methods, combined with autoradiography, are also suitable to determine dopant distributions in silicon. However, both techniques suffer from certain inherent experimental difficulties and/or limitations which are discussed. Methods of tracer technique practicable in the semiconductor field are described. (author)

  18. Materials characterization techniques

    National Research Council Canada - National Science Library

    Zhang, Sam; Li, L; Kumar, Ashok

    2009-01-01

    "With an emphasis on practical applications and real-world case studies, Materials Characterization Techniques presents the principles of widely used advanced surface and structural characterization...

  19. Persian fencing techniques

    Directory of Open Access Journals (Sweden)

    Manouchehr Moshtagh Khorasani

    2012-07-01

    Full Text Available There are numerous manuscripts, poems and stories that describe, specifically and in detail, the different techniques used in Persian swordsmanship. The present article explains the origins and the techniques of Persian swordsmanship. The article also describes the traditional code of conduct for Persian warriors. Additionally, it describes an array of techniques that were deployed in actual combat in Iran’s history. Some of these techniques are represented via the miniatures that are reproduced herein. This is the first article on Persian swordsmanship published in any periodical.

  20. Uranium exploration techniques

    International Nuclear Information System (INIS)

    Nichols, C.E.

    1984-01-01

    The subject is discussed under the headings: introduction (genetic description of some uranium deposits; typical concentrations of uranium in the natural environment); sedimentary host rocks (sandstones; tabular deposits; roll-front deposits; black shales); metamorphic host rocks (exploration techniques); geologic techniques (alteration features in sandstones; favourable features in metamorphic rocks); geophysical techniques (radiometric surveys; surface vehicle methods; airborne methods; input surveys); geochemical techniques (hydrogeochemistry; petrogeochemistry; stream sediment geochemistry; pedogeochemistry; emanometry; biogeochemistry); geochemical model for roll-front deposits; geologic model for vein-like deposits. (U.K.)