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Sample records for low-temperature magnetization measurements

  1. Translation balance for measuring magnetic susceptibilities at high or low temperatures (1962)

    International Nuclear Information System (INIS)

    Blaise, A.; Peuch, M.A.

    1962-01-01

    A translation balance is described for the measurement of the magnetic susceptibilities of liquids or solids in the temperature range from 1.7 to 1400 deg. K. Measurements are made within a magnetic field adjustable from 3400 to 16000 oersteds, in any desired atmosphere. Susceptibilities between 10 -8 and 10 -4 u.e.m. C.G.S., can be measured. (authors) [fr

  2. Review of modern instrumentation for magnetic measurements at high pressure and low temperature

    International Nuclear Information System (INIS)

    Wang, X.; Kamenev, K.V.

    2015-01-01

    High-pressure magnetic susceptibility experiments can provide insights into the changes in magnetic behavior and electric properties which can accompany extreme compressions of material. Instrumentation plays an important role in the experimental work in this field since 1990s. Here we present a comprehensive review of the high-pressure instrumentation development for magnetic measurement from the engineering perspective in the last 20 years. Suitable nonmagnetic materials for high pressure cell are introduced initially. Then we focus on the existing cells developed for magnetic property measurement system (MPMS) SQUID magnetometer from Quantum Design (USA). Two categories of high pressure cells for this system are discussed in detail respectively. Some high pressure cells with built-in magnetic measurement system are also reviewed

  3. Magnetic Levitation Force Measurement System at Any Low Temperatures From 20 K To 300 K

    Science.gov (United States)

    Celik, Sukru; Guner, S. Baris; Coskun, Elvan

    2015-03-01

    Most of the magnetic levitation force measurements in previous studies were performed at liquid nitrogen temperatures. For the levitation force of MgB2 and iron based superconducting samples, magnetic levitation force measurement system is needed. In this study, magnetic levitation force measurement system was designed. In this system, beside vertical force versus vertical motion, lateral and vertical force versus lateral motion measurements, the vertical force versus temperature at the fixed distance between permanent magnet PM - superconducting sample SS and the vertical force versus time measurements were performed at any temperatures from 20 K to 300 K. Thanks to these measurements, the temperature dependence, time dependence, and the distance (magnetic field) and temperature dependences of SS can be investigated. On the other hand, the magnetic stiffness MS measurements can be performed in this system. Using the measurement of MS at different temperature in the range, MS dependence on temperature can be investigated. These measurements at any temperatures in the range help to the superconductivity properties to be characterized. This work was supported by TUBTAK-the Scientific and technological research council of Turkey under project of MFAG - 110T622. This system was applied to the Turkish patent institute with the Application Number of 2013/13638 on 22/11/2013.

  4. Measurement of low-temperature specific heat

    International Nuclear Information System (INIS)

    Stewart, G.R.

    1983-01-01

    The measurement of low-temperature specific heat (LTSH) (0.1 K< T<60 K) has seen a number of breakthroughs both in design concepts and instrumentation in the last 15 years: particularly in small sample calorimetry. This review attempts to provide an overview of both large and small sample calorimetry techniques at temperatures below 60 K, with sufficient references to enable more detailed study. A comprehensive review is made of the most reliable measurements of the LTSH of 84 of the elements to illustrate briefly some of the problems of measurements and analysis, as well as to provide additional references. More detail is devoted to three special areas of low-temperature calorimetry that have seen rapid development recently: (1) measurement of the specific heat of highly radioactive samples, (2) measurement of the specific heat of materials in high magnetic fields (18 T), and (3) measurement of the specific heat of very small (100 μg) samples. The review ends with a brief discussion of the frontier research currently underway on microcalorimetry for nanogram sample weights

  5. Comparative measurements of plasma potential with ball-pen and Langmuir probe in low-temperature magnetized plasma

    International Nuclear Information System (INIS)

    Zanáška, M.; Kudrna, P.; Tichý, M.; Adámek, J.; Peterka, M.

    2015-01-01

    The ball-pen probe (BPP) is used for direct plasma potential measurements in magnetized plasma. The probe can adjust the ratio of the electron and ion saturation currents I sat − /I sat + to be close to one and therefore its I-V characteristic becomes nearly symmetric. If this is achieved, the floating potential of the BPP is close to the plasma potential. Because of its rather simple construction, it offers an attractive probe for measurements in magnetized plasma. Comparative measurements of plasma potential by BPPs of different dimensions as well as one Langmuir probe (LP) in an argon discharge plasma of a cylindrical magnetron were performed at various experimental conditions. An additional comparison by an emissive probe was also performed. All these types of probes provide similar values of plasma potential in a wide range of plasma parameters. Our results for three different BPP dimensions indicate that the BPP can be operated in a cylindrical magnetron DC argon discharge if the value of the ratio of the magnetic field and neutral gas pressure, B/p, is greater than approximately 10 mT/Pa

  6. Comparative measurements of plasma potential with ball-pen and Langmuir probe in low-temperature magnetized plasma

    Science.gov (United States)

    Zanáška, M.; Adámek, J.; Peterka, M.; Kudrna, P.; Tichý, M.

    2015-03-01

    The ball-pen probe (BPP) is used for direct plasma potential measurements in magnetized plasma. The probe can adjust the ratio of the electron and ion saturation currents Isat-/Isat+ to be close to one and therefore its I-V characteristic becomes nearly symmetric. If this is achieved, the floating potential of the BPP is close to the plasma potential. Because of its rather simple construction, it offers an attractive probe for measurements in magnetized plasma. Comparative measurements of plasma potential by BPPs of different dimensions as well as one Langmuir probe (LP) in an argon discharge plasma of a cylindrical magnetron were performed at various experimental conditions. An additional comparison by an emissive probe was also performed. All these types of probes provide similar values of plasma potential in a wide range of plasma parameters. Our results for three different BPP dimensions indicate that the BPP can be operated in a cylindrical magnetron DC argon discharge if the value of the ratio of the magnetic field and neutral gas pressure, B/p, is greater than approximately 10 mT/Pa.

  7. Comparative measurements of plasma potential with ball-pen and Langmuir probe in low-temperature magnetized plasma

    Energy Technology Data Exchange (ETDEWEB)

    Zanáška, M.; Kudrna, P.; Tichý, M. [Faculty of Mathematics and Physics, Charles University in Prague, Ke Karlovu 3, 12116 Prague 2 (Czech Republic); Adámek, J. [Institute of Plasma Physics AS CR, v.v.i., Za Slovankou 3, 18200 Prague 8 (Czech Republic); Peterka, M. [Faculty of Mathematics and Physics, Charles University in Prague, Ke Karlovu 3, 12116 Prague 2 (Czech Republic); Institute of Plasma Physics AS CR, v.v.i., Za Slovankou 3, 18200 Prague 8 (Czech Republic)

    2015-03-15

    The ball-pen probe (BPP) is used for direct plasma potential measurements in magnetized plasma. The probe can adjust the ratio of the electron and ion saturation currents I{sub sat}{sup −}/I{sub sat}{sup +} to be close to one and therefore its I-V characteristic becomes nearly symmetric. If this is achieved, the floating potential of the BPP is close to the plasma potential. Because of its rather simple construction, it offers an attractive probe for measurements in magnetized plasma. Comparative measurements of plasma potential by BPPs of different dimensions as well as one Langmuir probe (LP) in an argon discharge plasma of a cylindrical magnetron were performed at various experimental conditions. An additional comparison by an emissive probe was also performed. All these types of probes provide similar values of plasma potential in a wide range of plasma parameters. Our results for three different BPP dimensions indicate that the BPP can be operated in a cylindrical magnetron DC argon discharge if the value of the ratio of the magnetic field and neutral gas pressure, B/p, is greater than approximately 10 mT/Pa.

  8. The effect of low temperature cryocoolers on the development of low temperature superconducting magnets

    International Nuclear Information System (INIS)

    Green, Michael A.

    2000-01-01

    The commercial development of reliable 4 K cryocoolers improves the future prospects for magnets made from low temperature superconductors (LTS). The hope of the developers of high temperature superconductors (HTS) has been to replace liquid helium cooled LTS magnets with HTS magnets that operate at or near liquid nitrogen temperature. There has been limited success in this endeavor, but continued problems with HTS conductors have greatly slowed progress toward this goal. The development of cryocoolers that reliably operate below 4 K will allow magnets made from LTS conductor to remain very competitive for many years to come. A key enabling technology for the use of low temperature cryocoolers on LTS magnets has been the development of HTS leads. This report describes the characteristics of LTS magnets that can be successfully melded to low-temperature cryocoolers. This report will also show when it is not appropriate to consider the use of low-temperature cryocoolers to cool magnets made with LTS conductor. A couple of specific examples of LTS magnets where cryocoolers can be used are given

  9. Magnetic behavior of VBr2 at very low temperatures

    International Nuclear Information System (INIS)

    Arthur, J.R.; Kawarazaki, S.; Hirakawa, K.

    1985-01-01

    Vanadium dibromide, along with VCl 2 and VI 2 , has a hexagonal crystal structure (CdI 2 structure) in which the magnetic coupling of vanadium ions within the c planes is much stronger than the interplane coupling. These systems are of interest as possible examples of highly frustrated two-dimensional triangular lattice antiferromagnets. This interest is encouraged by high-temperature magnetic susceptibility measurements, which yield Weiss constants of several hundred degrees Kelvin. In fact, magnetic transitions do not occur in these substances until temperatures of less than 50 K are reached, indicating that the antiferromagnetic interactions are frustrated. A search for possible new transitions at very low temperatures was conducted with a VBr 2 single-crystal sample mounted in the dilution refrigerator neutron diffraction facility at HFIR. The crystal was not of very good quality, but three distinct magnetic reflections were observed at 4.2 K and below

  10. Low temperature magnetic structure of MnSe

    Indian Academy of Sciences (India)

    Abstract. In this paper we report low temperature neutron diffraction studies on MnSe in order to understand the anomalous behaviour of their magnetic and transport prop- erties. Our study indicates that at low temperatures MnSe has two coexisting crystal structures, high temperature NaCl and hexagonal NiAs. NiAs phase ...

  11. Low-temperature dynamics of magnetic nanoshells

    KAUST Repository

    Zhang, Bei

    2010-09-01

    Well and poorly crystallized iron oxide nanoshells (or hollow nanoparticles) were successfully fabricated using the Kirkendall effect in an oxygen and in an air environment using Fe nanoparticles. The low-field, zero-field-cooling (ZFC) and field-cooling (FC), measurements on these two samples indicated that the inter-particle interactions between the well-crystallized nanoshells were much stronger than those in the poorly crystallized nanoshell assembly. However, the memory experiments showed that there was no spin-glass phase in the well-crystallized nanoshell assembly, whereas the signature of the spin-glass phase (or the memory effect) was evident in the poorly crystallized nanoshell assembly. This result suggests that the origin of the spin-glass characteristic observed in the poorly crystallized nanoshells is the existence of the spinglass phase within those particular nanoshells. Copyright © EPLA, 2010.

  12. Low-temperature magnetic modification of sensitive biological materials

    Czech Academy of Sciences Publication Activity Database

    Pospišková, K.; Šafařík, Ivo

    2015-01-01

    Roč. 142, mar (2015), s. 184-188 ISSN 0167-577X R&D Projects: GA MŠk(CZ) LD13021 Institutional support: RVO:67179843 Keywords : magnetic iron oxides particles * microwave-assisted synthesis * low-temperature magnetic modification * immobilized enzymes Subject RIV: BO - Biophysics Impact factor: 2.437, year: 2015

  13. Determination of magnetic characteristics of nanoparticles by low-temperature calorimetry methods

    Energy Technology Data Exchange (ETDEWEB)

    Ugulava, A.; Toklikishvili, Z. [Department of Physics, I.Javakhishvili Tbilisi State University,I.Chavchavadze av. 3, 0179 Tbilisi, Georgia (United States); Chkhaidze, S., E-mail: simon.chkhaidze@tsu.ge [Department of Physics, I.Javakhishvili Tbilisi State University,I.Chavchavadze av. 3, 0179 Tbilisi, Georgia (United States); Kekutia, Sh. [V. Chavchanidze Institute of Cybernetics, at the Technical State University, S. Euli str. 5, 0186 Tbilisi, Georgia (United States)

    2017-05-15

    At low temperatures, the heat capacity of a superparamagnetic “ideal gas” determined by magnetic degrees of freedom can greatly exceed the lattice heat capacity. It is shown that in the presence of an external magnetic field, the temperature dependence of the magnetic part of the heat capacity has two maxima. The relations between the temperature at which these maxima are achieved, the magnetic moment of the nanoparticles and the magnetic anisotropy constant have been obtained. Measuring the heat capacity maxima temperatures by low-temperature calorimetry methods and using the obtained relations, we can obtain the numerical values both of the magnetic moment of nanoparticles and the magnetic anisotropy constants.

  14. Measuring Poisson Ratios at Low Temperatures

    Science.gov (United States)

    Boozon, R. S.; Shepic, J. A.

    1987-01-01

    Simple extensometer ring measures bulges of specimens in compression. New method of measuring Poisson's ratio used on brittle ceramic materials at cryogenic temperatures. Extensometer ring encircles cylindrical specimen. Four strain gauges connected in fully active Wheatstone bridge self-temperature-compensating. Used at temperatures as low as liquid helium.

  15. Low temperature magnetic characterization of EuO1-x

    Science.gov (United States)

    Rimal, Gaurab; Tang, Jinke

    EuO is a widely studied magnetic semiconductor. It is an ideal case of a Heisenberg ferromagnet as well as a model magnetic polaron system. The interesting aspect of this material is the existance of magnetic polarons in the low temperature region. We study the properties of oxygen deficient EuO prepared by pulsed laser deposition. Besides normal ferromagnetic transitions near 70K and 140K, we observe a different transition at 16K. We also observe a shift in the coercivity for field cooling versus zero field cooling. Possible mechanisms driving these behaviors will be discussed. This work was supported by the U.S. Department of Energy, Office of Basic Energy Sciences, Division of Materials Sciences and Engineering (DEFG02-10ER46728) and by the School of Energy Resources of the University of Wyoming.

  16. Postmortem magnetic resonance imaging dealing with low temperature objects

    International Nuclear Information System (INIS)

    Kobayashi, Tomoya; Shiotani, Seiji; Isobe, Tomonori

    2010-01-01

    In Japan, the medical examiner system is not widespread, the rate of autopsy is low, and many medical institutions therefore perform postmortem imaging using clinical equipment. Postmortem imaging is performed to clarify cause of death, select candidates for autopsy, make a guide map for autopsy, or provide additional information for autopsy. Findings are classified into 3 categories: cause of death and associated changes, changes induced by cardiopulmonary resuscitation, and postmortem changes. Postmortem magnetic resonance imaging shows characteristic changes in signal intensity related to low body temperature after death; they are low temperature images. (author)

  17. Magnetic resonance studies of atomic hydrogen gas at low temperatures

    International Nuclear Information System (INIS)

    Hardy, W.N.; Morrow, M.; Jochemsen, R.; Statt, B.W.; Kubik, P.R.; Marsolais, R.M.; Berlinsky, A.J.; Landesman, A.

    1980-01-01

    Using a pulsed low temperature discharge in a closed cell containing H 2 and 4 He, we have been able to store a low density (approximately 10 12 atoms/cc) gas of atomic hydrogen for periods of order one hour in zero magnetic field and T=1 K. Pulsed magnetic resonance at the 1420 MHz hyperfine transition has been used to study a number of the properties of the gas, including the recombination rate H + H + 4 He→H 2 + 4 He, the hydrogen spin-exchange relaxation rates, the diffusion coefficient of H in 4 He gas and the pressure shift of the hyperfine frequency due to the 4 He buffer gas. Here we discuss the application of hyperfine frequency shifts as a probe of the H-He potential, and as a means for determining the binding energy of H on liquid helium

  18. Low-temperature susceptibility of concentrated magnetic fluids

    Science.gov (United States)

    Pshenichnikov, Alexander F.; Lebedev, Alexander V.

    2004-09-01

    The initial susceptibility of concentrated magnetic fluids (ferrocolloids) has been experimentally investigated at low temperatures. The results obtained indicate that the interparticle dipole-dipole interactions can increase the susceptibility by several times as compared to the Langevin value. It is shown that good agreement between recent theoretical models and experimental observations can be achieved by introducing a correction for coefficients in the series expansion of susceptibility in powers of density and aggregation parameter. A modified equation for equilibrium susceptibility is offered to sum over corrections made by Kalikmanov (Statistical Physics of Fluids, Springer-Verlag, Berlin, 2001) and by B. Huke and M. Lücke (Phys. Rev. E 67, 051403, 2003). The equation gives good quantitative agreement with the experimental data in the wide range of temperature and magnetic particles concentration. It has been found that in some cases the magnetic fluid solidification occurs at temperature several tens of kelvins higher than the crystallization temperature of the carrier liquid. The solidification temperature of magnetic fluids is independent of particle concentration (i.e., magneto-dipole interparticle interactions) and dependent on the surfactant type and carrier liquid. This finding allows us to suggest that molecular interactions and generation of some large-scale structure from colloidal particles in magnetic fluids are responsible for magnetic fluid solidification. If the magnetic fluid contains the particles with the Brownian relaxation mechanism of the magnetic moment, the solidification manifests itself as the peak on the "susceptibility-temperature" curve. This fact proves the dynamic nature of the observed peak: it arises from blocking the Brownian mechanism of the magnetization relaxation.

  19. Low temperature magnetic behaviour of glass-covered magnetic microwires with gradient nanocrystalline microstructure

    Energy Technology Data Exchange (ETDEWEB)

    Serrano, I. G.; Hernando, A.; Marín, P. [Instituto de Magnetismo Aplicado, UCM-ADIF-CSIC, P.O. Box 155 las Rozas, Madrid 28230 (Spain)

    2014-01-21

    Slow nanocrystallization driving dynamics can be affected by the combination of two factors: sample residual stresses and sample geometry. This effect is evidenced at the initial stages of nanocrystallization of amorphous CoFeSiBCuNb magnetic microwires. Transmission electron microscopy observations indicate how crystallization at temperatures between 730 and 780 K results in a graded microstructure where the crystallization at the surface skin of the microwire, which remains almost amorphous, differs from that of the middle, where elongated grains are observed, and inner regions. However, samples annealed at higher temperatures present a homogeneous microstructure. The effect of gradient microstructure on magnetic properties has been also analyzed and a loss of bistable magnetic behaviour at low temperatures, from that obtained in the amorphous and fully nanocrystallized sample, has been observed and ascribed to changes in sign of magnetostriction for measuring temperatures below 100 K.

  20. Measuring Systems for Thermometer Calibration in Low-Temperature Range

    Science.gov (United States)

    Szmyrka-Grzebyk, A.; Lipiński, L.; Manuszkiewicz, H.; Kowal, A.; Grykałowska, A.; Jancewicz, D.

    2011-12-01

    The national temperature standard for the low-temperature range between 13.8033 K and 273.16 K has been established in Poland at the Institute of Low Temperature and Structure Research (INTiBS). The standard consists of sealed cells for realization of six fixed points of the International Temperature Scale of 1990 (ITS-90) in the low-temperature range, an adiabatic cryostat and Isotech water and mercury triple-point baths, capsule standard resistance thermometers (CSPRT), and AC and DC bridges with standard resistors for thermometers resistance measurements. INTiBS calibrates CSPRTs at the low-temperature fixed points with uncertainties less than 1 mK. In lower temperature range—between 2.5 K and about 25 K — rhodium-iron (RhFe) resistance thermometers are calibrated by comparison with a standard which participated in the EURAMET.T-K1.1 comparison. INTiBS offers a calibration service for industrial platinum resistance thermometers and for digital thermometers between 77 K and 273 K. These types of thermometers may be calibrated at INTiBS also in a higher temperature range up to 550°C. The Laboratory of Temperature Standard at INTiBS acquired an accreditation from the Polish Centre for Accreditation. A management system according to EN ISO/IEC 17025:2005 was established at the Laboratory and presented on EURAMET QSM Forum.

  1. Low-temperature mobility measurements on CMOS devices

    International Nuclear Information System (INIS)

    Hairpetian, A.; Gitlin, D.; Viswanathan, C.R.

    1989-01-01

    The surface channel mobility of carriers in eta- and rho-MOS transistors fabricated in a CMOS process was accurately determined at low temperatures down to 5 Κ. The mobility was obtained by an accurate measurement of the inversion charge density using a split C-V technique and the conductance at low drain voltages. The split C-V technique was validated at all temperatures using a one-dimensional Poisson solver (MOSCAP), which was modified for low-temperature application. The mobility dependence on the perpendicular electric field for different substrate bias values appears to have different temperature dependence for eta- and rho-channel devices. The electron mobility increases with a decrease in temperature at all gate voltages. On the other hand, the hole mobility exhibits a different temperature behavior depending upon whether the gate voltage corresponds to strong inversion or is near threshold

  2. Magnetic hyperthermia heating of cobalt ferrite nanoparticles prepared by low temperature ferrous sulfate based method

    Directory of Open Access Journals (Sweden)

    Tejabhiram Yadavalli

    2016-05-01

    Full Text Available A facile low temperature co-precipitation method for the synthesis of crystalline cobalt ferrite nanostructures using ferrous sulfate salt as the precursor has been discussed. The prepared samples were compared with nanoparticles prepared by conventional co-precipitation and hydrothermal methods using ferric nitrate as the precursor. X-ray diffraction studies confirmed the formation of cubic spinel cobalt ferrites when dried at 110 °C as opposed to conventional methods which required higher temperatures/pressure for the formation of the same. Field emission scanning electron microscope studies of these powders revealed the formation of nearly spherical nanostructures in the size range of 20-30 nm which were comparable to those prepared by conventional methods. Magnetic measurements confirmed the ferromagnetic nature of the cobalt ferrites with low magnetic remanance. Further magnetic hyperthermia studies of nanostructures prepared by low temperature method showed a rise in temperature to 50 °C in 600 s.

  3. Magnetic and Structural Phase Transitions in Thulium under High Pressures and Low Temperatures

    Energy Technology Data Exchange (ETDEWEB)

    Vohra, Yogesh K.; Tsoi, Georgiy M.; Samudrala, Gopi K. [UAB

    2017-10-01

    The nature of 4f electrons in many rare earth metals and compounds may be broadly characterized as being either "localized" or "itinerant", and is held responsible for a wide range of physical and chemical properties. The pressure variable has a very dramatic effect on the electronic structure of rare earth metals which in turn drives a sequence of structural and magnetic transitions. We have carried out four-probe electrical resistance measurements on rare earth metal Thulium (Tm) under high pressures to 33 GPa and low temperatures to 10 K to monitor the magnetic ordering transition. These studies are complemented by angle dispersive x-ray diffraction studies to monitor crystallographic phase transitions at high pressures and low temperatures. We observe an abrupt increase in magnetic ordering temperature in Tm at a pressure of 17 GPa on phase transition from ambient pressure hcp-phase to α-Sm phase transition. In addition, measured equation of state (EOS) at low temperatures show anomalously low thermal expansion coefficients likely linked to magnetic transitions.

  4. Magnetization jumps in nanostructured Nd–Fe–B alloy at low temperatures

    International Nuclear Information System (INIS)

    Neznakhin, D.S.; Bolyachkin, A.S.; Volegov, A.S.; Markin, P.E.; Andreev, S.V.; Kudrevatykh, N.V.

    2015-01-01

    Magnetic properties of the nanostructured isotropic alloy on the base of Nd 2 Fe 14 B type phase were investigated at low temperatures. The evaluated average grain size of this phase was much smaller than its critical single domain diameter. Hence the magnetization and demagnetization processes were expected to be performed by coherent magnetization rotation. For such coercivity type system magnetization jumps were revealed on the demagnetization hysteresis loop branch in the vicinity of the coercive force at temperatures below 4 K. It was shown that magnetization jumps have a stochastic behavior and their number strongly depends on the temperature and the mass of measured samples. High temperature spikes corresponding to magnetization discontinuities were observed. All these results allowed to propose that magnetization jumps in nanostructured magnetics with magnetization rotation reversal processes comply with the local heating model. - Highlights: • Magnetization reversals of the nanostructured Nd–Fe–B-type alloy were obtained below 4 K. • Magnetization jumps were first observed for magnetization rotation coercivity type magnets. • Staircase magnetization reversal was explained within the framework of the local heating model

  5. Measured Performance of a Low Temperature Air Source Heat Pump

    Energy Technology Data Exchange (ETDEWEB)

    Johnson, R. K. [Johnson Research LLC, Pueblo West, CO (United States)

    2013-09-01

    A 4-ton Low Temperature Heat Pump (LTHP) manufactured by Hallowell International was installed in a residence near New Haven, Connecticut and monitored over two winters of operation. After attending to some significant service issues, the heat pump operated as designed. This report should be considered a review of the dual compressor 'boosted heat pump' technology. The Low Temperature Heat Pumpsystem operates with four increasing levels of capacity (heat output) as the outdoor temperature drops. The system was shown to select capacity correctly, supplying the appropriate amount of heat to the house across the full range of outdoor temperatures. The system's Coefficient of Performance (Seasonal COP, or SCOP) over two entire winters was calculated, based on measured data, to be 3.29over the first winter and 2.68 over the second winter. A second seasonal efficiency calculation by a different method yielded a SCOP of 2.78 for the first winter and 2.83 for the second winter. This second seasonal efficiency calculation was determined by comparing measured heat pump energy use to the in situ energy use with resistance heat alone. This method is the ratio of the slopes of thedaily energy use load lines.

  6. Low temperature behavior of magnetic domains observed using a magnetic force microscope

    International Nuclear Information System (INIS)

    Chung, S. H.; Shinde, S. R.; Ogale, S. B.; Venkatesan, T.; Greene, R. L.; Dreyer, M.; Gomez, R. D.

    2001-01-01

    A commercial atomic force microscope/magnetic force microscope (MFM) was modified to cool magnetic samples down to around 100 K under a high vacuum while maintaining its routine imaging functionality. MFM images of a 120 nm thick La 0.7 Ca 0.3 MnO 3 film on a LaAlO 3 substrate at low temperature show the paramagnetic-to-ferromagnetic phase transition. Evolution of magnetic domains and magnetic ripples with decreasing temperature are also observed near the edge of a 20 nm thick patterned Co film on a Si substrate. [copyright] 2001 American Institute of Physics

  7. Low temperature Mössbauer studies on magnetic nanocomposites

    Indian Academy of Sciences (India)

    Unknown

    in the recording industry for achieving high density infor- mation storage and in the refrigeration industry ( ... by an ultra fine grain size (< 50 nm) have created a great deal of interest in recent years by virtue of their ... The reduction in size modifies the magnetic order in these materials. The magnetic nanocomposites can be ...

  8. Stored energy in fusion magnet materials irradiated at low temperatures

    International Nuclear Information System (INIS)

    Chaplin, R.L.; Kerchner, H.R.; Klabunde, C.E.; Coltman, R.R.

    1989-08-01

    During the power cycle of a fusion reactor, the radiation reaching the superconducting magnet system will produce an accumulation of immobile defects in the magnet materials. During a subsequent warm-up cycle of the magnet system, the defects will become mobile and interact to produce new defect configurations as well as some mutual defect annihilations which generate heat-the release of stored energy. This report presents a brief qualitative discussion of the mechanisms for the production and release of stored energy in irradiated materials, a theoretical analysis of the thermal response of irradiated materials, theoretical analysis of the thermal response of irradiated materials during warm-up, and a discussion of the possible impact of stored energy release on fusion magnet operation 20 refs

  9. Study of the dynamics of magnetic nano-particles within the limit of very low temperatures

    International Nuclear Information System (INIS)

    Sappey, Romain

    1997-01-01

    In this research thesis, the author first describes some aspects of the magnetism of nano-particles, and then the very-low-temperature magnetometer which has been fabricated in the laboratory during this research work. Then, he presents samples (ferrimagnetic or antiferromagnetic particle assemblies, distributed in size and diluted in such a way that a modelling in terms of superposition of independent processes could be attempted), and reports their characterisation measurements. He discusses the reliability of ZFC magnetization measurements used for the characterization of these particle assemblies. An anomaly noticed during the study of the field effect is discussed and an explanation is proposed for it. The author then reports relaxation measurements which are used to study the dynamics nature. A new measurement procedure is proposed to avoid the problem of barrier energy distribution [fr

  10. Measured Performance of a Low Temperature Air Source Heat Pump

    Energy Technology Data Exchange (ETDEWEB)

    R.K. Johnson

    2013-09-01

    A 4-ton Low Temperature Heat Pump (LTHP) manufactured by Hallowell International was installed in a residence near New Haven, Connecticut and monitored over two winters of operation. After attending to some significant service issues, the heat pump operated as designed. This report should be considered a review of the dual compressor “boosted heat pump” technology. The Low Temperature Heat Pump system operates with four increasing levels of capacity (heat output) as the outdoor temperature drops.

  11. Low temperature synthesis, magnetic and electrical properties of iron-magnesium superparamagnetic nanoalloy

    Energy Technology Data Exchange (ETDEWEB)

    Nazir, Rabia [Department of Chemistry, Quaid-i-Azam University, Islamabad 45320 (Pakistan); Mazhar, Muhammad [Department of Chemistry, Quaid-i-Azam University, Islamabad 45320 (Pakistan)], E-mail: mazhar42pk@yahoo.com; Akhtar, Muhammad Javed; Nadeem, Muhammad; Siddique, Muhammad [Physics Division, Pinstech, P.O. Nilore, Islamabad (Pakistan); Shah, Raza [HEJ Research Institute of Chemistry, University of Karachi, Karachi 75270 (Pakistan); Hasanain, S. Khurshid [Department of Physics, Quaid-i-Azam University, Islamabad 45320 (Pakistan)

    2009-06-24

    A low temperature chemical approach which beats the miscibility barrier of Fe and Mg has been designed to synthesize Fe-Mg{sub 2} nanoalloy and tested to result nanoparticles of average 30 nm size. The nanoalloy is amorphous in nature and characterized by XPRD, AFM, magnetometery, Moessbauer and impedance spectroscopies. The result of magnetic measurement suggests the sample to be superparamagnetic as evidenced by the {sup 57}Fe Moessbauer spectroscopy. The two Mg atoms occupy different positions around iron resulting in two phase system as shown by Moessbauer and impedance spectroscopies.

  12. Low temperature synthesis, magnetic and electrical properties of iron-magnesium superparamagnetic nanoalloy

    International Nuclear Information System (INIS)

    Nazir, Rabia; Mazhar, Muhammad; Akhtar, Muhammad Javed; Nadeem, Muhammad; Siddique, Muhammad; Shah, Raza; Hasanain, S. Khurshid

    2009-01-01

    A low temperature chemical approach which beats the miscibility barrier of Fe and Mg has been designed to synthesize Fe-Mg 2 nanoalloy and tested to result nanoparticles of average 30 nm size. The nanoalloy is amorphous in nature and characterized by XPRD, AFM, magnetometery, Moessbauer and impedance spectroscopies. The result of magnetic measurement suggests the sample to be superparamagnetic as evidenced by the 57 Fe Moessbauer spectroscopy. The two Mg atoms occupy different positions around iron resulting in two phase system as shown by Moessbauer and impedance spectroscopies.

  13. Low-temperature magnetization of (Ga,Mn)As semiconductors

    Czech Academy of Sciences Publication Activity Database

    Jungwirth, Tomáš; Mašek, Jan; Wang, K. Y.; Edmonds, K. W.; Sawicki, M.; Polini, M.; Sinova, J.; MacDonald, A. H.; Campion, R. P.; Zhao, L.X.; Farley, N.R.S.; Johal, T.K.; van der Laan, G.; Foxon, C. T.; Gallagher, B. L.

    2006-01-01

    Roč. 73, č. 16 (2006), 165205/1-165205/11 ISSN 1098-0121 R&D Projects: GA ČR GA202/05/0575 Grant - others:EPSRC(GB) GR/S81407/01; FENIKS(XE) EC:G5RD-CT-2001-00535; US Department of Energy(US) DE-FG03-02ER45958 Institutional research plan: CEZ:AV0Z10100521 Keywords : ferromagnetic semiconductors * magnetization Subject RIV: BM - Solid Matter Physics ; Magnetism Impact factor: 3.107, year: 2006

  14. Low temperature measurement of the vapor pressures of planetary molecules

    Science.gov (United States)

    Kraus, George F.

    1989-01-01

    Interpretation of planetary observations and proper modeling of planetary atmospheres are critically upon accurate laboratory data for the chemical and physical properties of the constitutes of the atmospheres. It is important that these data are taken over the appropriate range of parameters such as temperature, pressure, and composition. Availability of accurate, laboratory data for vapor pressures and equilibrium constants of condensed species at low temperatures is essential for photochemical and cloud models of the atmospheres of the outer planets. In the absence of such data, modelers have no choice but to assume values based on an educated guess. In those cases where higher temperature data are available, a standard procedure is to extrapolate these points to the lower temperatures using the Clausius-Clapeyron equation. Last summer the vapor pressures of acetylene (C2H2) hydrogen cyanide (HCN), and cyanoacetylene (HC3N) was measured using two different methods. At the higher temperatures 1 torr and 10 torr capacitance manometers were used. To measure very low pressures, a technique was used which is based on the infrared absorption of thin film (TFIR). This summer the vapor pressure of acetylene was measured the TFIR method. The vapor pressure of hydrogen sulfide (H2S) was measured using capacitance manometers. Results for H2O agree with literature data over the common range of temperature. At the lower temperatures the data lie slightly below the values predicted by extrapolation of the Clausius-Clapeyron equation. Thin film infrared (TFIR) data for acetylene lie significantly below the values predicted by extrapolation. It is hoped to bridge the gap between the low end of the CM data and the upper end of the TFIR data in the future using a new spinning rotor gauge.

  15. Low temperature spin-glass-like phases in magnetic nano-granular composites

    KAUST Repository

    Zhang, Bei

    2012-09-01

    It is a common understanding that the dipole-dipole interaction among the magnetic nanoparticles may result in a low-temperature spin-glass phase, which has been evidenced by observation of aging effect and memory effect. However, several studies on the nano-particles systems showed that some of the observed spin-glass-like phenomena could be due to the existence of spin-glasslike shells surrounding the ferrimagnetic cores. Therefore, it is very important to understand that how the dipole-dipole interaction induce the spin-glass phase. In order to address this issue, we have fabricated Co-SiO 2 and Fe-SiO 2 nano-granular thin films and measured the memory effect for them. Spin-glass-like phase has been observed at low temperatures. We found that, after annealing, the size of the clusters increased significantly. Based on a simple model, the dipole-dipole interaction between the clusters must be increased accordingly for the annealed samples. Interestingly, the memory effect is greatly weakened in the annealed films, which strongly suggested that the dipole-dipole interaction may not be the major factor for the formation of the low-temperature spin-glass-like phase. Copyright © 2012 American Scientific Publishers All rights reserved.

  16. Low-temperature phonoemissive tunneling rates in single molecule magnets

    Science.gov (United States)

    Liu, Yun; Garg, Anupam

    2016-03-01

    Tunneling between the two lowest energy levels of single molecule magnets with Ising type anisotropy, accompanied by the emission or absorption of phonons, is considered. Quantitatively accurate calculations of the rates for such tunneling are performed for a model Hamiltonian especially relevant to the best studied example, Fe8. Two different methods are used: high-order perturbation theory in the spin-phonon interaction and the non-Ising-symmetric parts of the spin Hamiltonian, and a novel semiclassical approach based on spin-coherent-state-path-integral instantons. The methods are found to be in good quantitative agreement with other, and consistent with previous approaches to the problem. The implications of these results for magnetization of molecular solids of these molecules are discussed briefly.

  17. Instrument for Measuring Thermal Conductivity of Materials at Low Temperatures

    Science.gov (United States)

    Fesmire, James; Sass, Jared; Johnson, Wesley

    2010-01-01

    With the advance of polymer and other non-metallic material sciences, whole new series of polymeric materials and composites are being created. These materials are being optimized for many different applications including cryogenic and low-temperature industrial processes. Engineers need these data to perform detailed system designs and enable new design possibilities for improved control, reliability, and efficiency in specific applications. One main area of interest is cryogenic structural elements and fluid handling components and other parts, films, and coatings for low-temperature application. An important thermal property of these new materials is the apparent thermal conductivity (k-value).

  18. How systems of single-molecule magnets magnetize at low temperatures

    Science.gov (United States)

    Fernández, Julio F.; Alonso, Juan J.

    2004-01-01

    We model magnetization processes that take place through tunneling in crystals of single-molecule magnets, such as Mn12 and Fe8. These processes take place when a field H is applied after quenching to very low temperatures. Magnetic dipolar interactions and spin-flipping rules are essential ingredients of the model. The results obtained follow from Monte Carlo simulations and from the stochastic model we propose for dipole field diffusion. Correlations established before quenching are shown to later drive the magnetization process. We also show that in simple cubic lattices, m∝√(t) at time t after H is applied, as observed in Fe8, but only for 1+2log10(hd/hw) time decades, where hd is some near-neighbor magnetic dipolar field, and a spin reversal can occur only if the magnetic field acting on it is within some field window (-hw,hw). However, the √(t) behavior is not universal. For bcc and fcc lattices, m∝tp, but p≃0.7. An expression for p in terms of lattice parameters is derived. At later times the magnetization levels off to a constant value. All these processes take place at approximately constant magnetic energy if the annealing energy ɛa is larger than the tunneling window’s energy width (i.e., if ɛa≳gμBhwS). Thermal processes come in only later on to drive further magnetization growth.

  19. Low-temperature magnetic properties of GdCoIn5

    Science.gov (United States)

    Betancourth, D.; Facio, J. I.; Pedrazzini, P.; Jesus, C. B. R.; Pagliuso, P. G.; Vildosola, V.; Cornaglia, Pablo S.; García, D. J.; Correa, V. F.

    2015-01-01

    A comprehensive experimental and theoretical study of the low temperature properties of GdCoIn5 was performed. Specific heat, thermal expansion, magnetization and electrical resistivity were measured in good quality single crystals down to 4He temperatures. All the experiments show a second-order-like phase transition at 30 K probably associated with the onset of antiferromagnetic order. The magnetic susceptibility shows a pronounced anisotropy below TN with an easy magnetic axis perpendicular to the crystallographic ĉ-axis. Total energy GGA+U calculations indicate a ground state with magnetic moments localized at the Gd ions and allowed a determination of the Gd-Gd magnetic interactions. Band structure calculations of the electron and phonon contributions to the specific heat together with Quantum Monte Carlo calculations of the magnetic contributions show a very good agreement with the experimental data. Comparison between experiment and calculations suggests a significant anharmonic contribution to the specific heat at high temperature (T ≳ 100 K).

  20. Advanced magneto-optical Kerr effect measurements of superconductors at low temperatures

    Directory of Open Access Journals (Sweden)

    Claudia Stahl

    2017-10-01

    Full Text Available Magneto-optical Kerr-effect (MOKE measurements of superconducting films with soft-magnetic coatings are performed at low temperatures using a laser-based MOKE set-up. An elaborate measurement scheme with internal reference allows the quantitative comparison of the temperature dependent Kerr-amplitude with the magnetic field generated by supercurrents. For this purpose, an amorphous CoFeB thin film exhibiting a large Kerr-signal is deposited directly on top of the YBCO superconductor acting as field sensing layer. It is shown that the resulting magnetic hysteresis loops of the soft-magnetic film can be used to reconstruct the electric properties of the superconductor.

  1. Low-temperature elastic properties of YbSbPt probed by ultrasound measurements

    Science.gov (United States)

    Nakanishi, Y.; Takahashi, S.; Ohyama, R.; Hasegawa, J.; Nakamura, M.; Suzuki, H.; Yoshizawa, M.

    2018-03-01

    The elastic properties of a single crystal of the half-Heusler compound YbSbPt have been investigated by means of the ultrasonic measurement. In particular, careful measurements of the temperature (T) dependent elastic constant C 11(T) was performed in the vicinity of its phase transition point near T N of 0.5 K. A clear step-like anomaly accompanied by spin-density-wave type antiferromagnetic (AFM) phase transition was found in the C 11(T) curve. The low-temperature magnetic phase diagram is proposed on the basis of the results. The phase diagram consists of, at least two main distinct phases: a low-field and high-field regime with a transition field of approximately 0.6 T at zero field. We discuss the low-temperature elastic property based on analysis of Landau-type free energy.

  2. Low-temperature magnetism of alabandite: Crucial role of surface oxidation

    Czech Academy of Sciences Publication Activity Database

    Čuda, J.; Kohout, Tomáš; Filip, J.; Tuček, J.; Kosterov, A.; Haloda, J.; Skála, Roman; Santala, E.; Medřík, I.; Zbořil, R.

    2013-01-01

    Roč. 98, 8/9 (2013), s. 1550-1556 ISSN 0003-004X R&D Projects: GA AV ČR KJB300130903 Institutional support: RVO:67985831 Keywords : alabandite (MnS) * hausmannite (Mn3O4) * magnetism * troilite (FeS) * crystallization * experimental mineralogy * ferromanganese deposit * hysteresis * low temperature * magnetic anomaly * magnetic field * manganese deposit * oxidation * remanent magnetization * stoichiometry * sulfide Subject RIV: DD - Geochemistry Impact factor: 2.059, year: 2013

  3. A New Tool for Separating the Magnetic Mineralogy of Complex Mineral Assemblages from Low Temperature Magnetic Behavior

    Directory of Open Access Journals (Sweden)

    France Lagroix

    2017-07-01

    Full Text Available One timeless challenge in rock magnetic studies, inclusive of paleomagnetism and environmental magnetism, is decomposing a sample's bulk magnetic behavior into its individual magnetic mineral components. We present a method permitting to decompose the magnetic behavior of a bulk sample experimentally and at low temperature avoiding any ambiguities in data interpretation due to heating-induced alteration. A single instrument is used to measure the temperature dependence of remanent magnetizations and to apply an isothermal demagnetization step at any temperature between 2 and 400 K. The experimental method is validated on synthetic mixtures of magnetite, hematite, goethite as well as on natural loess samples where the contributions of magnetite, goethite, hematite and maghemite are successfully isolated. The experimental protocol can be adapted to target other iron bearing minerals relevant to the rock or sediment under study. One limitation rests on the fact that the method is based on remanent magnetizations. Consequently, a quantitative decomposition of absolute concentration of individual components remains unachievable without assumptions. Nonetheless, semi-quantitative magnetic mineral concentrations were determined on synthetic and natural loess/paleosol samples in order to validate and test the method as a semi-quantitative tool in environmental magnetism studies.

  4. Characterization of low temperature metallic magnetic calorimeters having gold absorbers with implanted $^{163}$Ho ions

    CERN Document Server

    Gastaldo, L.; von Seggern, F.; Porst, J.-P.; Schäfer, S.; Pies, C.; Kempf, S.; Wolf, T.; Fleischmann, A.; Enss, C.; Herlert, A.; Johnston, K.

    2013-01-01

    For the first time we have investigated the behavior of fully micro-fabricated low temperature metallic magnetic calorimeters (MMCs) after undergoing an ion-implantation process. This experiment had the aim to show the possibility to perform a high precision calorimetric measurement of the energy spectrum following the electron capture of $^{163}$Ho using MMCs having the radioactive $^{163}$Ho ions implanted in the absorber. The implantation of $^{163}$Ho ions was performed at ISOLDE-CERN. The performance of a detector that underwent an ion-implantation process is compared to the one of a detector without implanted ions. The results show that the implantation dose of ions used in this experiment does not compromise the properties of the detector. In addition an optimized detector design for future $^{163}$Ho experiments is presented.

  5. Magnetic study of the low temperature anomalies in the underdoped PrBCO compound

    Science.gov (United States)

    Lahoubi, Mahieddine

    2018-05-01

    The low temperature anomalous magnetic properties of a non-superconducting PrBCO6+x compound in an underdoped oxygen state of concentration (x = 0.44) are characterized by paraprocess magnetic susceptibility χH(T) measurements carried out as a function of temperature T under different values of a DC magnetic field H up to 110 kOe. The derivatives dχH(T)/dT curves reveal a significant reduction with increasing H in the Néel temperature TN = 9 K of the Pr antiferromagnetic (AFM) ordering for which the transition subsists at 100 kOe. The small anomaly at T2 = 6-7 K is confirmed at 20 kOe and the previous spin reorientation attributed to this transition temperature seems to be suppressed above 60 kOe. The well defined anomaly in the vicinity of the low-critical point Tcr = 4-5 K which occurs simultaneously, is still present when the strength of H is increased up to 100 kOe. Weak field induced phase transitions are observed between T2 and TN at a low transition-field (Ht<11 kOe) in the differential magnetic susceptibility dMT(H)/dH as a function of H deduced from the isothermal magnetizations MT(H) with H up to 21 kOe, whereas a weak ferromagnetic behavior of the Pr sublattice appears below Tcr. The magnetic field effects give rise to more evidence for the Pr-Cu(2) coupling with 'exchange-frustrated AFM' interactions and ascertain the main role of the Pr sublattice whereas the Cu(2) sublattice seems to be less efficient.

  6. Influence of Magnetic Field on Electric Charge Transport in Holomiun Thin Films at Low Temperatures

    Directory of Open Access Journals (Sweden)

    Jan Dudas

    2005-01-01

    Full Text Available Holmium thin films were prepared by evaporation in ultrahigh vacuum (UHV and high precision electrical resistance measurements were performed on them as well as on holomium bulk sample in the wide temperature range from 4,2 K up to the room temperature. Electric charge transport is profoundly influenced by the magnetic structure at low temperatures and a "knee-like" resistance anomaly was observed near the transportation from paramagnetic state to basal-plane spiral structure in bulk with the Neel temperature TN=128,9 K and below ~ 122 K in thin Ho films in a thickness range from 98 nm to 215 nm. Unexpected resistance minimum at ~ 9 K and a slope´s charge of the R vs. T curve near ~ 170 K was observed in 215 nm thin film. Application of magnetic field parallel to the substrate and thin film plane for temperatures below ~ 150 K caused the decrease of resistence value with increasing magnetic flux density. Increasing suppression of the TN value up to ~ 5 K with increasing flux density value up to 5 T was observed in Ho films. 

  7. Effect of low temperature reactor irradiation on organic insulators in superconducting magnets, (4)

    International Nuclear Information System (INIS)

    Kato, Teruo; Takamura, Saburo

    1983-01-01

    In order to study effects of irradiation at low temperature on insulating materials of superconducting magnets, flexural and impact tests are carried out at 4.2K without warmup after low temperature irradiation for several fiber reinforced plastics. The used materials are glass fiber reinforced epoxies and polyimide, and carbon fiber reinforced epoxies. After irradiation of 1.1 X 10 9 rad, the reduction in flexural strength of G-10 CR is about 70% and that of G-11 CR about 25%. No change are observed in strength of glass fiber reinforced polyimide by low temperature irradiation. Other kinds of glass fiber reinforced epoxies show a reduction in strength but the flexural strength of carbon fiber reinforced epoxies increases a small by irradiation. Irradiation effect of these materials on impact value is similar to that on flexural strength. (author)

  8. Magnetization process and low-temperature thermodynamics of a spin-1/2 Heisenberg octahedral chain

    Science.gov (United States)

    Strečka, Jozef; Richter, Johannes; Derzhko, Oleg; Verkholyak, Taras; Karľová, Katarína

    2018-05-01

    Low-temperature magnetization curves and thermodynamics of a spin-1/2 Heisenberg octahedral chain with the intra-plaquette and monomer-plaquette interactions are examined within a two-component lattice-gas model of hard-core monomers, which takes into account all low-lying energy modes in a highly frustrated parameter space involving the monomer-tetramer, localized many-magnon and fully polarized ground states. It is shown that the developed lattice-gas model satisfactorily describes all pronounced features of the low-temperature magnetization process and the magneto-thermodynamics such as abrupt changes of the isothermal magnetization curves, a double-peak structure of the specific heat or a giant magnetocaloric effect.

  9. Low-temperature magnetic ordering in the perovskites Pr1-xAxCoO3 (A=Ca, Sr)

    International Nuclear Information System (INIS)

    Deac, Iosif G.; Tetean, Romulus; Balasz, Istvan; Burzo, Emil

    2010-01-01

    The magnetic and electrical properties of polycrystalline Pr 1-x A x CoO 3 cobaltites with A=Ca, Sr and 0≤x≤0.5 were studied in the temperature range 4 K≤T≤1000 K and field up to 7 T. The X-ray analyses show the presence of only one phase having monoclinic or orthorhombic symmetry. The magnetic measurements indicate that the Ca-doped samples have at low temperatures, similar properties to the frustrated magnetic materials. PrCoO 3 is a paramagnetic insulator in the range from 4 to 1000 K. The Sr-doped cobaltites exhibit two phase transitions: a paramagnetic-ferromagnetic (or magnetic phase separated state) phase transition at about 240 K and a second one at about 100 K. The magnetic measurements suggest the presence of magnetic clusters and a change in the nature of magnetic coupling between Co ions at low temperatures. A semiconducting type behavior and high negative magnetoresistance was found for the Ca-doped samples, while the Sr-doped ones were metallic and with negligible magnetoresistance. The results are analyzed in the frame of a phase separation scenario in the presence of the spin-state transitions of Co ions.

  10. Rotating structures in low temperature magnetized plasmas - Insight from particle simulations

    Directory of Open Access Journals (Sweden)

    Jean-Pierre eBoeuf

    2014-12-01

    Full Text Available The EXB configuration of various low temperature plasma devices is often responsible for the formation of rotating structures and instabilities leading to anomalous electron transport across the magnetic field. In these devices, electrons are strongly magnetized while ions are weakly or not magnetized and this leads to specific physical phenomena that are not present in fusion plasmas where both electrons and ions are strongly magnetized. In this paper we describe basic phenomena involving rotating plasma structures in simple configurations of low temperature EXB plasma devices on the basis of PIC-MCC (Particle-In-Cell Monte Carlo Collisions simulations. We focus on three examples: rotating electron vortices and rotating spokes in cylindrical magnetrons, and azimuthal electron-cyclotron drift instability in Hall thrusters. The simulations are not intended to give definite answers to the many physics issues related to low temperature EXB plasma devices but are used to illustrate and discuss some of the basic questions that need further studies.

  11. Description of the universal low-temperature measuring system

    International Nuclear Information System (INIS)

    Langfeld, R.; Maurer, C.

    1987-01-01

    There are various measuring methods for a characterization of semiconductor devices, especially for analysis of radiation effects after ion implantation. The four most important methods are: 1. Recording of voltage-current characteristics at pn-junctions or Schottky diodes. 2. Determination of the temperature dependence of the electrical resistance, e.g. of amorphous semiconductor layers, by feeding a constant voltage and measuring the current as a function of sample temperature. 3. Measurement of the resistive layer capacitance of a semiconductor diode as a function of the fed blocking voltage and determination of the doping concentration profile. 4. Time-resolved capacitance measurement after abrupt blocking-voltage alterations at pn - or Schottky diodes as a function of specimen temperature for determining defects in semiconductors, DLTS method. A measuring equipment has been set up that allows measurements being made in the temperature range between 14 K and 400 K, on up to eight specimens in one temperature test. Operating mode and handling of the computerized measuring program are described. (orig./HP) [de

  12. New type of magnetocaloric effect: Implications on low-temperature magnetic refrigeration using an Ericsson cycle

    International Nuclear Information System (INIS)

    Takeya, H.; Pecharsky, V.K.; Gschneidner, K.A. Jr.; Moorman, J.O.

    1994-01-01

    The low-temperature, high magnetic field heat capacity (1.5 to 70 K and 0 to 9.85 T), dc and ac magnetic behaviors of the compound (Gd 0.54 Er 0.46 )AlNi show that field-induced magnetic entropy change is significant and almost constant over the temperature region of ∼15 to ∼45 K. The resulting temperature dependence of the magnetocaloric effect, nearly constant over a 30+ K temperature range, is unprecedented (most magnetic materials have a caretlike shape temperature dependence). These data show that (Gd 0.54 Er 0.46 )AlNi can be used as an effective active magnetic regenerator material for an Ericsson-cycle magnetic refrigerator, and could substitute for complex composite layered materials suggested earlier

  13. Calorimetric measurements of YBa2Cu3O7-δ at low temperatures

    International Nuclear Information System (INIS)

    Schreiner, T.

    1992-01-01

    The first part of this thesis (Chap. II and III) describes the construction and functioning of an apparatus for measuring the specific heat, designed for small samples and for use in a top-loading dilution refrigerator. Automatic measurements are possible in the temperature range between 30 mK and 3 K with magnetic fields up to 12 Tesla. The accuracy of the calorimeter was verified by test measurements with copper. The second part (Chap. IV and V) presents measurements performed on an YBa 2 Cu 3 O 7-δ single crystal in the temperature range from 38 mK to 3 K and with magnetic fields up to 11.2 Tesla. Among others the nuclear contribution, the contribution of the lattice, as well as a possible linear term in the specific heat are discussed. At low temperatures and in high magnetic fields a non-exponential relaxation behavior was found, which is presumably due to a weak coupling of the nuclear moments to the lattice. (orig.)

  14. Acoustic levitator for containerless measurements on low temperature liquids

    Energy Technology Data Exchange (ETDEWEB)

    Benmore, Chris J [Argonne National Laboratory (ANL); Weber, Richard [Argonne National Laboratory (ANL); Neuefeind, Joerg C [ORNL; Rey, Charles A A [Charles Ray, Inc.

    2009-01-01

    A single-axis acoustic levitator was constructed and used to levitate liquid and solid drops at temperatures from -40 to +40 C. The levitator consisted of: (i) two acoustic transducers mounted on a rigid vertical support that was bolted to an optical breadboard, (ii) a acoustic power supply that controlled acoustic intensity, relative phase of the drive to the transducers, and could modulate the acoustic forces at frequencies up to 1kHz, (iii) a video camera, and (iv) a system for providing a stream of controlled temperature gas flow over the sample. The acoustic transducers were operated at their resonant frequency of ~ 22 kHz and could produce sound pressure levels up to 160 dB. The force applied by the acoustic field could be modulated using a frequency generator to excite oscillations in the sample. Sample temperature was controlled using a modified Cryostream Plus and measured using thermocouples and an infrared thermal imager. The levitator was installed at x-ray beamline 11 ID-C at the Advanced Photon Source and used to investigate the structure of supercooled liquids.

  15. High field magnetic anisotropy in praseodymium gallium garnet at low temperatures

    International Nuclear Information System (INIS)

    Wang Wei; Yue Yuan; Liu Gongqiang

    2011-01-01

    Research highlights: → A detailed analysis of crystal field effect is presented, and a set of new crystal field parameters is given to study the magnetic behaviors of the paramagnetic praseodymium gallium garnet (PrGaG). → The contribution of the exchange interaction between the praseodymium ions to the magnetic properties of PrGaG is further explored. Meanwhile, some characteristics of exchange interaction are revealed. → With the consideration of crystal field and exchange interaction, the available experiments are successfully fitted by our theoretical model. → Our theory suggests that PrGaG is ferromagnetic ordering at low temperatures, and the exchange interaction is anisotropic. - Abstract: In this paper, with the consideration of crystal field and exchange interaction between the rare-earth Pr 3+ ions, the magnetic anisotropy in praseodymium gallium garnet (PrGaG) in high magnetic fields and at low temperatures is theoretically analyzed. A set of relatively suitable CF parameters is obtained by studying the influence of the variations of nine CF parameters on the magnetization. However, only taking crystal field effect into account, theoretical calculations indicate that the experiments cannot be excellently interpreted. Then, the exchange interaction between Pr 3+ ion, which can be described as an effective exchange field H v = vM = vχH e = ηH e , is further considered. On the other hand, by evaluating the variation of the parameter η with the magnetic fields, our theory implies that PrGaG exhibits ferrimagnetic ordering at low temperatures, and the exchange interaction in PrGaG displays obvious anisotropy. Also, the theoretical data show better agreements with the experimental results.

  16. Characterization of low temperature metallic magnetic calorimeters having gold absorbers with implanted 163Ho ions

    Science.gov (United States)

    Gastaldo, L.; Ranitzsch, P. C.-O.; von Seggern, F.; Porst, J.-P.; Schäfer, S.; Pies, C.; Kempf, S.; Wolf, T.; Fleischmann, A.; Enss, C.; Herlert, A.; Johnston, K.

    2013-05-01

    For the first time we have investigated the behavior of fully micro-fabricated low temperature metallic magnetic calorimeters (MMCs) after undergoing an ion-implantation process. This experiment had the aim to show the possibility to perform a high precision calorimetric measurement of the energy spectrum following the electron capture of 163Ho using MMCs having the radioactive 163Ho ions implanted in the absorber. The isotope 163Ho decays through electron capture to 163Dy and features the smallest known QEC value. This peculiarity makes 163Ho a very interesting candidate to investigate the value of the electron neutrino mass by the analysis of the energy spectrum. The implantation of 163Ho ions was performed at ISOLDE-CERN. The performance of a detector that underwent an ion-implantation process is compared to the one of a detector without implanted ions. The results show that the implantation dose of ions used in this experiment does not compromise the properties of the detector. Moreover the performance of the detector prototype having the 163Ho ions implanted in the absorber is already close to the requirements needed for an experiment with sub-eV sensitivity to the electron neutrino mass. Based on these results, an optimized detector design for future 163Ho experiments is presented.

  17. Characterization of low temperature metallic magnetic calorimeters having gold absorbers with implanted 163Ho ions

    International Nuclear Information System (INIS)

    Gastaldo, L.; Ranitzsch, P.C.-O.; Seggern, F. von; Porst, J.-P.; Schäfer, S.; Pies, C.; Kempf, S.; Wolf, T.; Fleischmann, A.; Enss, C.; Herlert, A.; Johnston, K.

    2013-01-01

    For the first time we have investigated the behavior of fully micro-fabricated low temperature metallic magnetic calorimeters (MMCs) after undergoing an ion-implantation process. This experiment had the aim to show the possibility to perform a high precision calorimetric measurement of the energy spectrum following the electron capture of 163 Ho using MMCs having the radioactive 163 Ho ions implanted in the absorber. The isotope 163 Ho decays through electron capture to 163 Dy and features the smallest known Q EC value. This peculiarity makes 163 Ho a very interesting candidate to investigate the value of the electron neutrino mass by the analysis of the energy spectrum. The implantation of 163 Ho ions was performed at ISOLDE-CERN. The performance of a detector that underwent an ion-implantation process is compared to the one of a detector without implanted ions. The results show that the implantation dose of ions used in this experiment does not compromise the properties of the detector. Moreover the performance of the detector prototype having the 163 Ho ions implanted in the absorber is already close to the requirements needed for an experiment with sub-eV sensitivity to the electron neutrino mass. Based on these results, an optimized detector design for future 163 Ho experiments is presented

  18. Magnetocaloric effect of polycrystalline Sm0.5Ca0.5MnO3 compound: Investigation of low temperature magnetic state

    Science.gov (United States)

    Das, Kalipada; Banu, Nasrin; Das, I.; Dev, B. N.

    2018-06-01

    An attempt has been made to probe low temperature magnetic state of the polycrystalline Sm0.5Ca0.5MnO3 compound via magnetization and magnetocaloric studies. In the context of the earlier debatable reports on the above mentioned compound between the existence of glassy magnetic state and small ferromagnetic domains from the 'ac' susceptibility measurements, our experimental observation from magnetocaloric effect study clearly indicates the existence of ferromagnetic droplets along with certain amount of superparamagnetic component at low temperature (magnetization (even at H = 0.01 T) data do not exhibit the spin freezing nature at the low temperature which is almost a generic tendency of glassy magnetic state. Our study also highlights the competence of magnetocaloric effect as a tool to distinguish between different magnetic states of a compound.

  19. Nonlocal electrodynamics and low-temperature magnetization of clean high-κ superconductors

    International Nuclear Information System (INIS)

    Kogan, V.G.; Gurevich, A.; Cho, J.H.; Johnston, D.C.; Xu, M.; Thompson, J.R.; Martynovich, A.

    1996-01-01

    We show that magnetic properties of clean superconductors with a large Ginzburg-Landau parameter κ at low temperatures are affected by the nonlocality of the microscopic current-field relation and can be described by modified London equations. We argue that for clean materials at low temperatures, the standard London formula for the reversible magnetization in intermediate fields, M∼ln(H c2 /B), should contain the field H 0 ∼φ 0 /ρ 2 instead of H c2 ∼φ 0 /ξ 2 (T), with ρ being the nonlocality range on the order of ξ 0 , the zero-T coherence length. Since ρ depends weakly on T, the magnetization should exhibit an approximate scaling M(T,B)=X(T)Y(B) as observed in Bi- and Tl-based compounds in a broad temperature domain well below T c . Our expression for the magnetization reduces to the standard London result near T c and at any temperature for the dirty case. Implications of our results for interpretation of neutron scattering data and for procedures of extracting the penetration depth are discussed. copyright 1996 The American Physical Society

  20. Development of low temperature and high magnetic field X-ray diffraction facility

    Energy Technology Data Exchange (ETDEWEB)

    Shahee, Aga; Sharma, Shivani; Singh, K.; Lalla, N. P., E-mail: nplallaiuc82@gmail.com; Chaddah, P. [UGC-DAE Consortium for Scientific Research, University campus, Khandwa Road, Indore-452001 (India)

    2015-06-24

    The current progress of materials science regarding multifunctional materials (MFM) has put forward the challenges to understand the microscopic origin of their properties. Most of such MFMs have magneto-elastic correlations. To investigate the underlying mechanism it is therefore essential to investigate the structural properties in the presence of magnetic field. Keeping this in view low temperature and high magnetic field (LTHM) powder x-ray diffraction (XRD), a unique state-of-art facility in the country has been developed at CSR Indore. This setup works on symmetric Bragg Brentano geometry using a parallel incident x-ray beam from a rotating anode source working at 17 kW. Using this one can do structural studies at non-ambient conditions i.e. at low- temperatures (2-300 K) and high magnetic field (+8 to −8 T). The available scattering angle ranges from 5° to 115° 2θ with a resolution better than 0.1°. The proper functioning of the setup has been checked using Si sample. The effect of magnetic field on the structural properties has been demonstrated on Pr{sub 0.5}Sr{sub 0.5}MnO{sub 3} sample. Clear effect of field induced phase transition has been observed. Moreover, the effect of zero field cooled and field cooled conditions is also observed.

  1. Low-temperature nuclear magnetic resonance investigation of systems frustrated by competing exchange interactions

    Science.gov (United States)

    Roy, Beas

    NMR spectra proved the existence of a commensurate magnetic order while below 10 K, the shape of the NMR spectrum changes either due to an incommensurate magnetic order or due to spin reorientation. In summary the work presented in this thesis focusses on the NMR investigation of the magnetic properties of various compounds frustrated by the competing exchange interactions. References. [1] A. Yogi, N. Ahmad, R. Nath, A. A. Tsirlin, J. Sichelschmidt, B. Roy and Y. Furukawa, arXiv:1409.3076 (submitted to Phys. Rev. B). [2] Beas Roy, Yuji Furukawa, Ramesh Nath, David C. Johnston, J. Phys.: Conf. Ser. 320, 012048 (2011). [3] Beas Roy, Yuji Furukawa, David Johnston, Ramesh Nath, Yasuhiro Komaki, Hideto Fukazawa, and Yoh Kohori, ``Magnetic phase diagram of the two-dimensional frustrated square lattice compound BaCdVO(PO4)2 from high-pressure and low-temperature 31P-NMR study'', Paper to be submitted. [4] S. Ran, S. L. Bud'ko, D. K. Pratt, A. Kreyssig, M. G. Kim, M. J. Kramer, D. H. Ryan, W. N. Rowan-Weetaluktuk, Y. Furukawa, B. Roy, A. I. Goldman, and P. C. Canfield, Phys. Rev. B 83, 144517 (2011). [5] Y. Furukawa, B. Roy, S. Ran, S. L. Bud'ko and P. C. Canfield, Phys. Rev. B 89, 121109 (R) (2014). [6] B. Roy, Abhishek Pandey, Q. Zhang, T. W. Heitmann, D. Vaknin, D. C. Johnston, and Y. Furukawa, Phys. Rev. B 88, 174415 (2013). [7] R. Nath, K. M. Ranjith, B. Roy, D. C. Johnston, Y. Furukawa, and A. A. Tsirlin, Phys. Rev. B 90, 024431 (2014).

  2. Observation of magnetically anisotropic defects during stage I recovery in nickel after low-temperature electron irradiation

    International Nuclear Information System (INIS)

    Forsch, K.; Hemmerich, J.; Knoll, H.; Lucki, G.

    1974-01-01

    The measurement of defect-induced changes of magnetic anisotropy in a nickel single crystal after low-temperature electron irradiation was undertaken. A dynamic measuring method was used after reorienting a certain fraction of the radiation-induced defects in an external magnetic field of 5 kOe. In the temperature range of recovery stage I sub(C,D,E) (45 to 60 k) the crystallographic direction dependence of defect-induced anisotropy could be determined. The results show that in this temperature range the (100) split interstitial is mobile and able to reorient. The obtained data are further discussed with respect to existing information on magnetic after effect and resistivity annealing in electron-irradiated nickel

  3. Low-temperature magnetic study of naturally and experimentally shocked pyrrhotite

    Science.gov (United States)

    Mang, C.; Kontny, A. M.; Hecht, L.

    2011-12-01

    The most intriguing observation from the suevite unit of the 35 Ma old Chesapeake Bay impact structure (CBIS), Virginia, USA, is the occurrence of "shocked pyrrhotite", which might provide clues for a better understanding of the acquisition of shock-induced remagnetization during an impact event. A large range of differently strong deformed and melted components are mixed in the suevite and maximum shock pressures up to 35 GPa are reported (Wittmann et al. 2009). Pyrrhotite occurs as grains and grain clusters within the suevite matrix and rarely in melt fragments, and abundant lattice defects in pyrrhotite prove a shock-induced deformation. The shocked mineral is characterized by a significant loss of iron and the stoichiometric formula lies between Fe0.808S and Fe0.811S. This composition falls significantly below the Fe/S ratio of regular pyrrhotite (Fe>0.875) and is similar to the one of smythite (Fe9S11). The Curie temperature (TC) is above that of the ferrimagnetic 4C modification (320°C) and lies between 350 and 365°C. However, a transition at 30 K (Rochette et al. 1990), visible in low temperature remanence curves, confirms the presence of ferrimagnetic monoclinic 4C pyrrhotite.The present work aims at the question if all these different features observed in the natural pyrrhotite from the CBIS suevite are impact-related. Therefore we experimentally shocked a pyrrhotite ore from the Cerro de Pasco mine, Peru at 3, 5, 8, 20 and 30 GPa using a high pressure gun and high explosive devices. The obtained samples have been investigated by low-temperature AC susceptibility and remanence measurements (LT). In addition, we determined TC using AC susceptibility as function of temperature. LT experiments of the pyrrhotite ore unfortunately do not only show magnetic transition temperatures related to pure pyrrhotite but additionally of accessory magnetic mineral phases like magnetite (Fe3O4) and pyrophanite (MnTiO3). The contribution of those phases makes especially

  4. Low temperature structural transitions in dipolar hard spheres: The influence on magnetic properties

    International Nuclear Information System (INIS)

    Ivanov, A.O.; Kantorovich, S.S.; Rovigatti, L.; Tavares, J.M.; Sciortino, F.

    2015-01-01

    We investigate the structural chain-to-ring transition at low temperature in a gas of dipolar hard spheres (DHS). Due to the weakening of entropic contribution, ring formation becomes noticeable when the effective dipole–dipole magnetic interaction increases. It results in the redistribution of particles from usually observed flexible chains into flexible rings. The concentration (ρ) of DHS plays a crucial part in this transition: at a very low ρ only chains and rings are observed, whereas even a slight increase of the volume fraction leads to the formation of branched or defect structures. As a result, the fraction of DHS aggregated in defect-free rings turns out to be a non-monotonic function of ρ. The average ring size is found to be a slower increasing function of ρ when compared to that of chains. Both theory and computer simulations confirm the dramatic influence of the ring formation on the ρ-dependence of the initial magnetic susceptibility (χ) when the temperature decreases. The rings due to their zero total dipole moment are irresponsive to a weak magnetic field and drive to the strong decrease of the initial magnetic susceptibility. - Highlights: • Found structural chain-to-ring transition at low temperature sheds the light on the no-man's-land of the phase diagram of dipolar hard sphere gas. • Particle concentration plays a crucial part: at high dilution only chains and rings are observed, otherwise different branched structures occur. • The dramatic influence of the ring formation on the concentration dependence of the initial magnetic susceptibility when temperature decreases

  5. Continuous Emission Spectrum Measurement for Electron Temperature Determination in Low-Temperature Collisional Plasmas

    International Nuclear Information System (INIS)

    Liu Qiuyan; Li Hong; Chen Zhipeng; Xie Jinlin; Liu Wandong

    2011-01-01

    Continuous emission spectrum measurement is applied for the inconvenient diagnostics of low-temperature collisional plasmas. According to the physical mechanism of continuous emission, a simplified model is presented to analyze the spectrum in low temperature plasma. The validity of this model is discussed in a wide range of discharge parameters, including electron temperature and ionization degree. Through the simplified model, the continuous emission spectrum in a collisional argon internal inductively coupled plasma is experimentally measured to determine the electron temperature distribution for different gas pressures and radio-frequency powers. The inverse Abel transform is also applied for a better spatially resoluted results. Meanwhile, the result of the continuous emission spectrum measurement is compared to that of the electrostatic double probes, which indicates the effectiveness of this method. (low temperature plasma)

  6. Low temperature anomaly of light stimulated magnetization and heat capacity of the 1D diluted magnetic semiconductors

    Science.gov (United States)

    Geffe, Chernet Amente

    2018-03-01

    This article reports magnetization and specific heat capacity anomalies in one dimensional diluted magnetic semiconductors observed at very low temperatures. Based on quantum field theory double time temperature dependent Green function technique is employed to evaluate magnon dispersion and the time correlation function. It is understood that magnon-photon coupling and magnetic impurity concentration controls both, such that near absolute temperature magnetization is nearly zero and abruptly increase to saturation level with decreasing magnon-photon coupling strength. We also found out dropping of magnetic specific heat capacity as a result of increase in magnetic impurity concentration x, perhaps because of inter-band disorder that would suppress the enhancement of density of spin waves.

  7. Low temperature anomaly of light stimulated magnetization and heat capacity of the 1D diluted magnetic semiconductors

    Directory of Open Access Journals (Sweden)

    Chernet Amente Geffe

    2018-03-01

    Full Text Available This article reports magnetization and specific heat capacity anomalies in one dimensional diluted magnetic semiconductors observed at very low temperatures. Based on quantum field theory double time temperature dependent Green function technique is employed to evaluate magnon dispersion and the time correlation function. It is understood that magnon-photon coupling and magnetic impurity concentration controls both, such that near absolute temperature magnetization is nearly zero and abruptly increase to saturation level with decreasing magnon-photon coupling strength. We also found out dropping of magnetic specific heat capacity as a result of increase in magnetic impurity concentration x, perhaps because of inter-band disorder that would suppress the enhancement of density of spin waves.

  8. Low-temperature magnetic transition in troilite: A simple marker for highly stoichiometric FeS systems

    Czech Academy of Sciences Publication Activity Database

    Čuda, J.; Kohout, Tomáš; Tuček, J.; Haloda, J.; Filip, J.; Prucek, R.; Zbořil, J.

    2011-01-01

    Roč. 116, č. 11 (2011), art. B11205-B11205 ISSN 0148-0227 Institutional research plan: CEZ:AV0Z30130516 Keywords : troilite * meteorite * Mössbauer spectroscopy * low-temperature magnetic behavior * magnetic transition Subject RIV: DE - Earth Magnetism, Geodesy, Geography Impact factor: 3.021, year: 2011

  9. Cryogen free high magnetic field and low temperature sample environments for neutron scattering - latest developments

    International Nuclear Information System (INIS)

    Burgoyne, John

    2016-01-01

    Continuous progress has been made over many years now in the provision of low- and ultra-low temperature sample environments, together with new high-field superconducting magnets and increased convenience for both the user and the neutron research facility via new cooling technologies. Within Oxford Instrument's experience, this has been achieved in many cases through close collaboration with neutron scientists, and with the neutron facilities' sample environment leaders in particular. Superconducting magnet designs ranging from compact Small Angle (SANS) systems up to custom-engineered wide-angle scattering systems have been continuously developed. Recondensing, or 'zero boil-off' (ZBO), systems are well established for situations in which a high field magnet is not conducive to totally cryogen free cooling solutions, and offer a reliable route with the best trade-offs of maximum system capability versus running costs and user convenience. Fully cryogen free solutions for cryostats, dilution refrigerators, and medium-field magnets are readily available. Here we will present the latest technology developments in these options, describing the state-of-the art, the relative advantages of each, and the opportunities they offer to the neutron science community. (author)

  10. Low temperature superconductor and aligned high temperature superconductor magnetic dipole system and method for producing high magnetic fields

    Science.gov (United States)

    Gupta, Ramesh; Scanlan, Ronald; Ghosh, Arup K.; Weggel, Robert J.; Palmer, Robert; Anerella, Michael D.; Schmalzle, Jesse

    2017-10-17

    A dipole-magnet system and method for producing high-magnetic-fields, including an open-region located in a radially-central-region to allow particle-beam transport and other uses, low-temperature-superconducting-coils comprised of low-temperature-superconducting-wire located in radially-outward-regions to generate high magnetic-fields, high-temperature-superconducting-coils comprised of high-temperature-superconducting-tape located in radially-inward-regions to generate even higher magnetic-fields and to reduce erroneous fields, support-structures to support the coils against large Lorentz-forces, a liquid-helium-system to cool the coils, and electrical-contacts to allow electric-current into and out of the coils. The high-temperature-superconducting-tape may be comprised of bismuth-strontium-calcium-copper-oxide or rare-earth-metal, barium-copper-oxide (ReBCO) where the rare-earth-metal may be yttrium, samarium, neodymium, or gadolinium. Advantageously, alignment of the large-dimension of the rectangular-cross-section or curved-cross-section of the high-temperature-superconducting-tape with the high-magnetic-field minimizes unwanted erroneous magnetic fields. Alignment may be accomplished by proper positioning, tilting the high-temperature-superconducting-coils, forming the high-temperature-superconducting-coils into a curved-cross-section, placing nonconducting wedge-shaped-material between windings, placing nonconducting curved-and-wedge-shaped-material between windings, or by a combination of these techniques.

  11. Contribution to the study, by magnetic resonance, of the properties of heavily doped silicon at low temperature

    International Nuclear Information System (INIS)

    Jerome, D.

    1965-10-01

    The magnetic properties of heavily doped silicon at low temperature have been studied in a range of concentration on either side of the Mott transition. For impurity densities less than that of the transition a magnetic double resonance method allows the exchange coupling between localized donors to be measured, and in addition the existence of paramagnetic centers (pairs of neutral and ionized donors) is demonstrated. The behaviour of the spin-lattice relaxation of 29 Ci is explained in terms of the dipolar coupling between nuclei and paramagnetic centers. In the range of concentration 10 16 -10 17 impurities/cm 3 , the concentration dependent relaxation of donors is studied experimentally. A theoretical explanation is proposed for the latter mechanism, the basis of which is the presence of ionized pairs of donors. At increasing impurity concentrations the electronic delocalization increases. For the concentration of 2.5 X 10 18 P/cm 3 the hyperfine coupling is responsible for the 29 Si relaxation. It is shown that the electron density has a very large maximum near the impurities in the metallic domain of concentrations. An estimation of the impurity band width (19 deg. K) is deduced from the measurement of the paramagnetic part of the electronic susceptibility at low temperature. (author) [fr

  12. Synthesis of high saturation magnetic iron oxide nanomaterials via low temperature hydrothermal method

    Energy Technology Data Exchange (ETDEWEB)

    Bhavani, P.; Rajababu, C.H. [Department of Materials Science & Nanotechnology, Yogivemana University, Vemanapuram 516003, Kadapa (India); Arif, M.D. [Environmental Magnetism Laboratory, Indian Institute of Geomagnetism (IIG), Navi Mumbai 410218, Mumbai (India); Reddy, I. Venkata Subba [Department of Physics, Gitam University, Hyderabad Campus, Rudraram, Medak 502329 (India); Reddy, N. Ramamanohar, E-mail: manoharphd@gmail.com [Department of Materials Science & Nanotechnology, Yogivemana University, Vemanapuram 516003, Kadapa (India)

    2017-03-15

    Iron oxide nanoparticles (IONPs) were synthesized through a simple low temperature hydrothermal approach to obtain with high saturation magnetization properties. Two series of iron precursors (sulfates and chlorides) were used in synthesis process by varying the reaction temperature at a constant pH. The X-ray diffraction pattern indicates the inverse spinel structure of the synthesized IONPs. The Field emission scanning electron microscopy and high resolution transmission electron microscopy studies revealed that the particles prepared using iron sulfate were consisting a mixer of spherical (16–40 nm) and rod (diameter ~20–25 nm, length <100 nm) morphologies that synthesized at 130 °C, while the IONPs synthesized by iron chlorides are found to be well distributed spherical shapes with size range 5–20 nm. On other hand, the IONPs synthesized at reaction temperature of 190 °C has spherical (16–46 nm) morphology in both series. The band gap values of IONPs were calculated from the obtained optical absorption spectra of the samples. The IONPs synthesized using iron sulfate at temperature of 130 °C exhibited high saturation magnetization (M{sub S}) of 103.017 emu/g and low remanant magnetization (M{sub r}) of 0.22 emu/g with coercivity (H{sub c}) of 70.9 Oe{sub ,} which may be attributed to the smaller magnetic domains (d{sub m}) and dead magnetic layer thickness (t). - Highlights: • Comparison of iron oxide materials prepared with Fe{sup +2}/Fe{sup +3} sulfates and chlorides at different temperatures. • We prepared super-paramagnetic and soft ferromagnetic magnetite nanoparticles. • We report higher saturation magnetization with lower coercivity.

  13. The Use of Low Temperature Detectors for Direct Measurements of the Mass of the Electron Neutrino

    Directory of Open Access Journals (Sweden)

    A. Nucciotti

    2016-01-01

    Full Text Available Recent years have witnessed many exciting breakthroughs in neutrino physics. The detection of neutrino oscillations has proved that neutrinos are massive particles, but the assessment of their absolute mass scale is still an outstanding challenge in today particle physics and cosmology. Since low temperature detectors were first proposed for neutrino physics experiments in 1984, there has been tremendous technical progress: today this technique offers the high energy resolution and scalability required to perform competitive experiments challenging the lowest electron neutrino masses. This paper reviews the thirty-year effort aimed at realizing calorimetric measurements with sub-eV neutrino mass sensitivity using low temperature detectors.

  14. One-pot low-temperature green synthesis of magnetic graphene nanocomposite for the selective reduction of nitrobenzene

    Science.gov (United States)

    Haridas, Vijayasree; Sugunan, Sankaran; Narayanan, Binitha N.

    2018-06-01

    In the present study, a green one-pot low-temperature method is adopted for the synthesis of a novel magnetic graphene nanocomposite catalyst. Graphene preparation is performed without employing any oxidizing agents or corrosive chemicals, under mild sonication in isopropyl alcohol - water mixture. Monolayered nanoplatelets of graphene are obtained in the green solvent mixture and the composite material is found to be ferromagnetic in nature, obvious from the vibrating sample magnetometric measurements. Fe in the nanocomposite exists in two different forms i.e., α-Fe2O3 and α-FeOOH, as evident from the material characterization results. The graphene nanocomposite is found to be highly efficient in the selective reduction of nitrobenzene to aniline under solvent free reaction conditions and magnetic separation of this fine nanomaterial from the reaction mixture is successfully carried out. The catalyst is efficiently reusable till five repeated cycles.

  15. Pattern formation and filamentation in low temperature, magnetized plasmas - a numerical approach

    Science.gov (United States)

    Menati, Mohamad; Konopka, Uwe; Thomas, Edward

    2017-10-01

    In low-temperature discharges under the influence of high magnetic field, pattern and filament formation in the plasma has been reported by different groups. The phenomena present themselves as bright plasma columns (filaments) oriented parallel to the magnetic field lines at high magnetic field regime. The plasma structure can filament into different shapes from single columns to spiral and bright rings when viewed from the top. In spite of the extensive experimental observations, the observed effects lack a detailed theoretical and numerical description. In an attempt to numerically explain the plasma filamentation, we present a simplified model for the plasma discharge and power deposition into the plasma. Based on the model, 2-D and 3-D codes are being developed that solve Poisson's equation along with the fluid equations to obtain a self-consistent description of the plasma. The model and preliminary results applied to the specific plasma conditions will be presented. This work was supported by the US Dept. of Energy and NSF, DE-SC0016330, PHY-1613087.

  16. Embedding of $^{163}$Ho and $^{166m}$ Ho in the energy absorbers of low temperature metallic magnetic calorimeters

    CERN Multimedia

    The calorimetric measurement of the $^{163}$Ho electron capture spectrum is a promising tool to investigate the electron neutrino mass. A suitable method to embed the source in the detectors is the ion-implantation. This process has already been used to embed $^{163}$Ho ions in micro-fabricated low temperature metallic magnetic prototypes. The $^{163}$Ho electron capture spectrum obtained with these first prototypes is presently the most precise with an energy resolution of $\\Delta$$\\textit{E}$$_{FWHM}$ = 7.6 eV. In order to test the performance of the new generation of low temperature metallic magnetic calorimeters, we propose to perform a $^{163}$Ho ion-implantation on the new chip having two arrays consisting of 32 pixels each. An activity of about 1 Bq per pixel is required. With this new detector array we will be able to achieve a better energy resolution and to acquire a higher statistics which allows for studying the $^{163}$Ho spectral shape. We propose also to perform an ion-implantation of $^{166m}$...

  17. Competing magnetic interactions and low temperature magnetic phase transitions in composite multiferroics

    International Nuclear Information System (INIS)

    Borkar, Hitesh; Singh, V N; Kumar, Ashok; Choudhary, R J; Tomar, M; Gupta, Vinay

    2015-01-01

    Novel magnetic properties and magnetic interactions in composite multiferroic oxides Pb[(Zr 0.52 Ti 0.48 ) 0.60 (Fe 0.67 W 0.33 ) .40 ]O 3 ] 0.80 –[CoFe 2 O 4 ] 0.20 (PZTFW–CFO) have been studied from 50 to 1000 Oe field cooled (FC) and zero field cooled (ZFC) probing conditions, and over a wide range of temperatures (4–350 K). Crystal structure analysis, surface morphology, and high resolution transmission electron microscopy images revealed the presence of two distinct phases, where micro- and nano-size spinel CFO were embedded in tetragonal PZTFW matrix and applied a significant built-in compressive strain (∼0.4–0.8%). Three distinct magnetic phase transitions were observed with the subtle effect of CFO magnetic phase on PZTFW magnetic phase transitions below the blocking temperature (T B ). Temperature dependence magnetic property m(T) shows a clear evidence of spin freezing in magnetic order with lowering in thermal vibration. Chemical inhomogeneity and confinement of nanoscale ferrimagnetic phase in paramagnetic/antiferromagnetic matrix restrict the long range interaction of spin which in turn develop a giant spin frustration. A large divergence in the FC and ZFC data and broad hump in ZFC data near 200 (±10) K were observed which suggests that large magnetic anisotropy and short range order magnetic dipoles lead to the development of superparamagnetic states in composite. (paper)

  18. Development of a Proof of Concept Low Temperature Superfluid Magnetic Pump with Applications

    Science.gov (United States)

    Jahromi, Amir E.

    State of the art particle and photon detectors such as Transition Edge Sensors (TES) and Microwave Kinetic Inductance Detectors (MKID) use large arrays of sensors or detectors for space science missions. As the size of these space science detectors increases, future astrophysics missions will require sub-Kelvin coolers over larger areas. This leads to not only increased cooling power requirements, but also a requirement for distributed sub-Kelvin cooling. Development of a proof of concept Superfluid Magnetic Pump is discussed in this work. This novel low temperature, no moving part pump can replace the existing bellows-piston driven 4He or 3He- 4He mixture compressor/circulators used in various sub Kelvin refrigeration systems such as dilution, Superfluid pulse tube, or active magnetic regenerative refrigerators. Due to its superior thermal transport properties this pump can also be used as a simple circulator of sub-Lambda 4He to distribute cooling over large surface areas. The pump discussed in this work was experimentally shown to produce a maximum flow rate of 440 mg/s (averaged over cycle), 665 mg/s (peak) and produced a maximum pressure difference of 2323 Pascal. This pump worked in an "ideal" thermodynamic state: The experimental results matched with the theoretical values predicted by a computer model. Pump curves were developed to map the performance of this pump. This successful demonstration will enable this novel pump to be put to test in suitable sub Kelvin refrigeration systems. Numerical modeling of an Active Magnetic Regenerative Refrigerator (AMRR) that uses the Superfluid Magnetic Pump (SMP) to circulate liquid 3He-4He through a magnetic regenerator is presented as a potential application of such a pump.

  19. Development of a proof of concept low temperature 4He Superfluid Magnetic Pump

    Science.gov (United States)

    Jahromi, Amir E.; Miller, Franklin K.

    2017-03-01

    We describe the development and experimental results of a proof of concept Superfluid Magnetic Pump in this work. This novel low temperature, no moving part pump can replace the existing bellows-piston driven 4He or 3He-4He mixture compressor/circulators used in various sub Kelvin refrigeration systems such as dilution, Superfluid pulse tube, Stirling, or active magnetic regenerative refrigerators. Due to the superior thermal transport properties of sub-Lambda 4He this pump can also be used as a simple circulator to distribute cooling over large surface areas. Our pump was experimentally shown to produce a maximum flow rate of 440 mg/s (averaged over cycle), 665 mg/s (peak) and produced a maximum pressure difference of 2323 Pa using only the more common isotope of helium, 4He. This pump worked in an ;ideal; thermodynamic state: The experimental results matched with the theoretical values predicted by a computer model. Pump curves were developed to map the performance of this pump. This successful demonstration will enable this novel pump to be implemented in suitable sub Kelvin refrigeration systems.

  20. Low temperatures - hot topic

    Energy Technology Data Exchange (ETDEWEB)

    Anon.

    1988-09-15

    Neutrino mass measurements, next-generation double beta experiments, solar neutrino detection, searches for magnetic monopoles and the challenge of discovering what most of the Universe is made of (dark matter), not to mention axions (cosmic and solar), supersymmetric neutral particles and cosmic neutrinos. All this physics could use cryogenic techniques. Thus the second European Workshop on Low Temperature Devices for the Detection of Low Energy Neutrinos and Dark Matter, held at LAPP (Annecy) in May, covered an active and promising field.

  1. Low temperatures - hot topic

    International Nuclear Information System (INIS)

    Anon.

    1988-01-01

    Neutrino mass measurements, next-generation double beta experiments, solar neutrino detection, searches for magnetic monopoles and the challenge of discovering what most of the Universe is made of (dark matter), not to mention axions (cosmic and solar), supersymmetric neutral particles and cosmic neutrinos. All this physics could use cryogenic techniques. Thus the second European Workshop on Low Temperature Devices for the Detection of Low Energy Neutrinos and Dark Matter, held at LAPP (Annecy) in May, covered an active and promising field

  2. Magnetic ordering at low temperatures in some random superconducting and insulating compounds

    International Nuclear Information System (INIS)

    Hueser, D.

    1985-01-01

    This thesis presents the results of some investigations on the magnetic ordering phenomena in some random superconducting and insulating materials. The results are described of an investigation of the coexistence of superconductivity and random magnetic freezing in (Th,Nd)Ru 2 . On the basis of various measurements as function of temperature and external magnetic field the author found that spin glass-like freezing can occur far below the superconductivity and even that a sample may re-enter the superconducting state below a freezing temperature. Associated with the isothermal remanent magnetization of a random magnetic material he observed strong anomalies in the critical field versus temperature curves. Also a magnetic field memory effect has been found. (Auth.)

  3. Low-temperature specific heat measurements on the NdCoxFe1-xO3 system

    International Nuclear Information System (INIS)

    Bartolome, F.; Kuz'min, M.D.; Bartolome, J.; Blasco, J.; Garcia, J.

    1995-01-01

    Low-temperature specific heat measurements have been carried out on the NdCo x Fe 1-x O 3 perovskite system (x=0, 0.25, 0.5, 0.9, 1). Magnetic ordering of Nd 3+ ions have been observed in NdCoO 3 (at 1.20 K) and NdFeO 3 (at 1.05 K). The studied dilutions, unlike the pure Fe or Co compounds, do not show a magnetic order of the Nd ions due to the stronger molecular field caused by decompensation of the internal field upon the introduction of the (Co 3+ ) magnetic vacancies in the antiferromagnetically ordered Fe subsystem. The specific heat curve of the system at x=0.9 resembles spin-glass behaviour. ((orig.))

  4. Growth and Low Temperature Transport Measurements of Pure and Doped Bismuth Selenide

    DEFF Research Database (Denmark)

    Mlack, Jerome Thomas

    Se3, which is a strong spin orbit material and a topological insulator. I describe a synthesis technique and low-temperature transport measurements of nanostructures of Bi2Se3, that when annealed with palladium show evidence of superconductivity. The growth method is a catalyst-free atmospheric...... with palladium via annealing, the transport properties of the samples can be altered to exhibit superconductivity. Thin films of palladium are deposited on prefabricated Bi2Se3 nanodevices and annealed at temperatures in excess of 100 Celsius. We find that Bi2Se3 absorbs Pd under these conditions...... pressure vapor-solid growth. The growth method yields a variety of nanostructures, and materials analysis shows ordered structures of bismuth selenide in all cases. Low-temperature measurements of as-grown nanostructures indicate tunable carrier density in all samples. By doping the nanostructures...

  5. Magnetic properties of ZnFe2O4 nanoparticles produced by a low-temperature solid-state reaction method

    International Nuclear Information System (INIS)

    Li Fashen; Wang Haibo; Wang Li; Wang Jianbo

    2007-01-01

    ZnFe 2 O 4 nanoparticles with average grain size ranging from 40 to 60 nm behaving superparamagnetic at room temperature have been produced using a low-temperature solid-state reaction (LTSSR) method without ball-milling process. Abnormal magnetic properties such as S-shape hysteresis loops and non-zero magnetic moments were observed. ZnFe 2 O 4 nanoparticles were also synthesized using a NaOH coprecipitation method and a PVA sol-gel method to study the relationship between the preparation processes and the magnetic properties. Spin-glass behavior was observed in the low temperature solid-state reaction produced Zn ferrite in the zero-field cooled (ZFC) measurement. Our work proves that the various preparation methods will to some extent determine the properties of magnetic nanoparticles

  6. Multi-frequency ESR studies on a Haldane magnet in a field-induced phase at ultra-low temperatures

    International Nuclear Information System (INIS)

    Hagiwara, Masayuki; Kashiwagi, Takanari; Idutsu, Yuichi; Honda, Zentaro; Miyazaki, Hiroshi; Harada, Isao

    2010-01-01

    We report the results of multi-frequency electron spin resonance (ESR) measurements on single crystals of Ni(C 5 H 14 N 2 ) 2 N 3 (PF 6 ) which is regarded as the one-dimensional Heisenberg antiferromagnet with spin one, namely the Haldane magnet, at very low temperatures down to about 100 mK. We observed the lowest resonance branch below about 500 mK for the field along the chain direction (H||c), which was observed previously only in an inelastic neutron scattering experiment at 30 mK. We compare the resonance branch with that calculated by a phenomenological field theory, and discuss the field dependence and the temperature sensitivity of this ESR branch.

  7. Electrostatic fluctuations measured in low temperature helical plasmas with low collisionality

    International Nuclear Information System (INIS)

    Takeuchi, M.; Ikeda, R.; Ito, T.; Toi, K.; Suzuki, C.; Matsunaga, G.

    2004-01-01

    Electrostatic fluctuations have been measured by Langmuir probes from edge to core plasma region in low temperature helical plasmas which are produced by 2.45 GHz microwaves at very low field less than 0.1 T. The principal dimensionless parameters of the plasmas, that is, the normalized electron-ion collision frequency ν ei , and averaged plasma β φ and others are in the same range of them in high temperature plasmas, except the normalized gyro radius ρ s . The data on fluctuation characteristics from the dimensionally similar low temperature plasmas may give an important insight into the understanding of turbulent transport in high temperature plasmas. Dependences of fluctuation amplitudes on the radial electric field shear, ρ s and ν ei are investigated. Electrostatic fluctuations propagating in electron-diamagnetic drift direction have been observed in the plasma edge region and in ion-diamagnetic drift direction in the plasma core region. (authors)

  8. Microstructure in hardened cement pastes measured by mercury intrusion porosimetry and low temperature microcalorimetry

    DEFF Research Database (Denmark)

    Hansen, Kurt Kielsgaard; Baroghel, V.B.; Künzel, H.M.

    1996-01-01

    The present paper is presenting some of the results on microstructure from the CEC-Science Project CT91-0737 "Characterization of microstructure as a tool for prediction of moisture transfer in porous media". In the Project the microstructure for the porous media is studied by absorption isotherms......, image analysis, mercury intrusion porosimetry and low temperature microcalorimetry.The present paper is dealing with cumulated pore size distributions measured by mercury intrusion porosimetry (MIP) from two laboratories (LCPC, IBP) and low temperature microcalorimetry (CAL) from one laboratory (BKM......). The materials are five different hardened cement pastes. The materials, the preparation procedure for the samples, the experiments and the experimental results are described. Finally, the results are compared and discussed....

  9. Theoretical analysis and experimental study on breakaway torque of large-diameter magnetic liquid seal at low temperature

    Science.gov (United States)

    Zhang, Haina; Li, Decai; Wang, Qinglei; Zhang, Zhili

    2013-07-01

    The existing researches of the magnetic liquid rotation seal have been mainly oriented to the seal at normal temperature and the seal with the smaller shaft diameter less than 100 mm. However, the large-diameter magnetic liquid rotation seal at low temperature has not been reported both in theory and in application up to now. A key factor restricting the application of the large-diameter magnetic liquid rotation seal at low temperature is the high breakaway torque. In this paper, the factors that influence the breakaway torque including the number of seal stages, the injected quantity of magnetic liquid and the standing time at normal temperature are studied. Two kinds of magnetic liquid with variable content of large particles are prepared first, and a seal feedthrough with 140 mm shaft diameter is used in the experiments. All experiments are carried out in a low temperature chamber with a temperature range from 200°C to -100°C. Different numbers of seal stages are tested under the same condition to study the relation between the breakaway torque and the number of seal stages. Variable quantity of magnetic liquid is injected in the seal gap to get the relation curve of the breakaway torque and the injecting quantity of magnetic liquid. In the experiment for studying the relation between the breakaway torque and the standing time at the normal temperature, the seal feedtrough is laid at normal temperature for different period of time before it is put in the low temperature chamber. The experimental results show that the breakaway torque is proportional to the number of seal stages, the injected quantity of magnetic liquid and the standing time at the normal temperature. Meanwhile, the experimental results are analyzed and the torque formula of magnetic liquid rotation seal at low temperature is deduced from the Navier-Stokes equation on the base of the model of magnetic liquid rotation seal. The presented research can make wider application of the magnetic liquid

  10. Mössbauer spectroscopy, magnetization, magnetic susceptibility, and low temperature heat capacity of α-Na2NpO4

    International Nuclear Information System (INIS)

    Smith, Anna L; Hen, Amir; Magnani, Nicola; Colineau, Eric; Griveau, Jean-Christophe; Raison, Philippe E; Caciuffo, Roberto; Konings, Rudy J M; Sanchez, Jean-Pierre; Cheetham, Anthony K

    2016-01-01

    The physical and chemical properties at low temperatures of hexavalent disodium neptunate α-Na 2 NpO 4 are investigated for the first time in this work using Mössbauer spectroscopy, magnetization, magnetic susceptibility, and heat capacity measurements. The Np(VI) valence state is confirmed by the isomer shift value of the Mössbauer spectra, and the local structural environment around the neptunium cation is related to the fitted quadrupole coupling constant and asymmetry parameters. Moreover, magnetic hyperfine splitting is reported below 12.5 K, which could indicate magnetic ordering at this temperature. This interpretation is further substantiated by the existence of a λ-peak at 12.5 K in the heat capacity curve, which is shifted to lower temperatures with the application of a magnetic field, suggesting antiferromagnetic ordering. However, the absence of any anomaly in the magnetization and magnetic susceptibility data shows that the observed transition is more intricate. In addition, the heat capacity measurements suggest the existence of a Schottky-type anomaly above 15 K associated with a low-lying electronic doublet found about 60 cm −1 above the ground state doublet. The possibility of a quadrupolar transition associated with a ground state pseudoquartet is thereafter discussed. The present results finally bring new insights into the complex magnetic and electronic peculiarities of α-Na 2 NpO 4 . (paper)

  11. Precise electrical transport measurements by using Bridgman type pressure cell at low temperature

    Energy Technology Data Exchange (ETDEWEB)

    Oishi, Takayuki [Division of Civil and Enviromental Engineering, Kanazawa University, Kakuma-machi, Kanazawa 920-1192 (Japan); Ohashi, Masashi [Faculty of Environmental Design, Kanazawa University, Kakuma-machi, Kanazawa 920-1192 (Japan)

    2010-03-01

    We report a technique for the precise measurement of the electrical resisivity under high pressure at low temperature by using Bridgman anvils made of tungsten carbide. Quasi-hydrostatic pressure is generated up to {approx}15 GPa in the relatively large working space which allows the use of large specimens and simple experimental procedures rather than using a standard diamond anvil cell. The application is demonstrated by the measurements of the electrical resistivity of lead in order to describe the effect of pressure on the superconducting transition.

  12. Precise electrical transport measurements by using Bridgman type pressure cell at low temperature

    International Nuclear Information System (INIS)

    Oishi, Takayuki; Ohashi, Masashi

    2010-01-01

    We report a technique for the precise measurement of the electrical resisivity under high pressure at low temperature by using Bridgman anvils made of tungsten carbide. Quasi-hydrostatic pressure is generated up to ∼15 GPa in the relatively large working space which allows the use of large specimens and simple experimental procedures rather than using a standard diamond anvil cell. The application is demonstrated by the measurements of the electrical resistivity of lead in order to describe the effect of pressure on the superconducting transition.

  13. $\\mu$SR-Measurements under High Pressure and at Low Temperatures

    CERN Multimedia

    2002-01-01

    High pressure causes changes in the volume available to each atom in a solid and will therefore influence local properties like the electronic charge and spin densities and, in the case of magnetic materials, the spin ordering.\\\\ \\\\ The positive muon is known to be an interesting probe particle for the study of certain problems in magnetism. It has in fact been used for one high pressure experiment earlier in CERN, but the present experiments aim at more systematic studie For this purpose it is necessary to carry out pressure experiments at low temperatures. The new experiments use a helium gas pressure system, which covers the temperature range 10-300 K at pressures up to 14 Kbar.\\\\ \\\\ Experiments are in progress on \\item 1)~~~~Ferromagnetic metals like Fe, Co, Ni where the pressure dependence of the local magnetic field ~~~is studied at 77 K and at room temperature. \\item 2)~~~~Knight shifts in semimetals, where in the case of Sb strong variations with temperature and ~~~pressure are observed. \\end{enumerat...

  14. Low temperature magnetic properties and spin dynamics in single crystals of Cr{sub 8}Zn antiferromagnetic molecular rings

    Energy Technology Data Exchange (ETDEWEB)

    Adelnia, Fatemeh [Dipartimento di Fisica, Università degli Studi di Milano and INSTM, I-20133 Milano (Italy); Dipartimento di Fisica, Università degli Studi di Pavia and INSTM, I-27100 Pavia (Italy); Chiesa, Alessandro; Bordignon, Sara; Carretta, Stefano [Dipartimento di Fisica e Scienze della Terra, Università degli Studi di Parma, I-43124 Parma (Italy); Ghirri, Alberto; Candini, Andrea [CNR Institute Nanosciences S3, I- 41125 Modena (Italy); Cervetti, Christian [Dipartimento di Scienze Fisiche, Informatiche, Matematiche, Università di Modena e Reggio Emilia, I-41125 Modena (Italy); Evangelisti, Marco [CNR Institute Nanosciences S3, I- 41125 Modena (Italy); Dipartimento di Scienze Fisiche, Informatiche, Matematiche, Università di Modena e Reggio Emilia, I-41125 Modena (Italy); Instituto de Ciencia de Materiales de Aragón and Departamento de Física de la Materia Condensada, CSIC-Universidad de Zaragoza, 50009 Zaragoza (Spain); Affronte, Marco [CNR Institute Nanosciences S3, I- 41125 Modena (Italy); Dipartimento di Scienze Fisiche, Informatiche, Matematiche, Università di Modena e Reggio Emilia, I-41125 Modena (Italy); Sheikin, Ilya [Grenoble High Magnetic Field Laboratory, CNRS-LNCMI, 25, B.P. 166, 38042 Grenoble Cedex 9 (France); Winpenny, Richard; Timco, Grigore [The Lewis Magnetism Laboratory, The University of Manchester, M13 9PL Manchester (United Kingdom); Borsa, Ferdinando [Dipartimento di Fisica, Università degli Studi di Pavia and INSTM, I-27100 Pavia (Italy); and others

    2015-12-28

    A detailed experimental investigation of the effects giving rise to the magnetic energy level structure in the vicinity of the level crossing (LC) at low temperature is reported for the open antiferromagnetic molecular ring Cr{sub 8}Zn. The study is conducted by means of thermodynamic techniques (torque magnetometry, magnetization and specific heat measurements) and microscopic techniques (nuclear magnetic resonance line width, nuclear spin lattice, and spin-spin relaxation measurements). The experimental results are shown to be in excellent agreement with theoretical calculations based on a minimal spin model Hamiltonian, which includes a Dzyaloshinskii-Moriya interaction. The first ground state level crossing at μ{sub 0}H{sub c1} = 2.15 T is found to be an almost true LC while the second LC at μ{sub 0}H{sub c2} = 6.95 T has an anti-crossing gap of Δ{sub 12} = 0.19 K. In addition, both NMR and specific heat measurements show the presence of a level anti-crossing between excited states at μ{sub 0}H = 4.5 T as predicted by the theory. In all cases, the fit of the experimental data is improved by introducing a distribution of the isotropic exchange couplings (J), i.e., using a J strain model. The peaks at the first and second LCs in the nuclear spin-lattice relaxation rate are dominated by inelastic scattering and a value of Γ ∼ 10{sup 10} rad/s is inferred for the life time broadening of the excited state of the open ring, due to spin phonon interaction. A loss of NMR signal (wipe-out effect) is observed for the first time at LC and is explained by the enhancement of the spin-spin relaxation rate due to the inelastic scattering.

  15. Low-temperature magnetic ordering in the perovskites Pr 1-xA xCoO 3 (A=Ca, Sr)

    Science.gov (United States)

    Deac, Iosif G.; Tetean, Romulus; Balasz, Istvan; Burzo, Emil

    2010-05-01

    The magnetic and electrical properties of polycrystalline Pr 1-xA xCoO 3 cobaltites with A=Ca, Sr and 0≤ x≤0.5 were studied in the temperature range 4 K≤ T≤1000 K and field up to 7 T. The X-ray analyses show the presence of only one phase having monoclinic or orthorhombic symmetry. The magnetic measurements indicate that the Ca-doped samples have at low temperatures, similar properties to the frustrated magnetic materials. PrCoO 3 is a paramagnetic insulator in the range from 4 to 1000 K. The Sr-doped cobaltites exhibit two phase transitions: a paramagnetic-ferromagnetic (or magnetic phase separated state) phase transition at about 240 K and a second one at about 100 K. The magnetic measurements suggest the presence of magnetic clusters and a change in the nature of magnetic coupling between Co ions at low temperatures. A semiconducting type behavior and high negative magnetoresistance was found for the Ca-doped samples, while the Sr-doped ones were metallic and with negligible magnetoresistance. The results are analyzed in the frame of a phase separation scenario in the presence of the spin-state transitions of Co ions.

  16. Apparent increase in the thickness of superconducting particles at low temperatures measured by electron holography

    International Nuclear Information System (INIS)

    Hirsch, J.E.

    2013-01-01

    We predict that superconducting particles will show an apparent increase in thickness at low temperatures when measured by electron holography. This will result not from a real thickness increase, rather from an increase in the mean inner potential sensed by the electron wave traveling through the particle, originating in expansion of the electronic wavefunction of the superconducting electrons and resulting negative charge expulsion from the interior to the surface of the superconductor, giving rise to an increase in the phase shift of the electron wavefront going through the sample relative to the wavefront going through vacuum. The temperature dependence of the observed phase shifts will yield valuable new information on the physics of the superconducting state of metals. - Highlights: • A new property of superconducting particles is predicted. • Electron holography will show an apparent increase in thickness at low temperatures. • This will result from a predicted increase in the mean inner potential. • This will originate in expulsion of electrons from the interior to the surface. • This is not predicted by the conventional BCS theory of superconductivity

  17. A method of surface area measurement of fuel materials by fission gas release at low temperature

    International Nuclear Information System (INIS)

    Kaimal, K.N.G.; Naik, M.C.; Paul, A.R.; Venkateswarlu, K.S.

    1989-01-01

    The present report deals with the development of a method for surface area measurement of nuclear fuel as well as fissile doped materials by fission gas release study at low temperature. The method is based on the evaluation of knock-out release rate of fission 133 Xe from irradiated fuel after sufficient cooling to decay the short lived activity. The report also describes the fabrication of an ampoule breaker unit for such study. Knock-out release rate of 133 Xe has been studied from UO 2 powders having varying surface area 'S' ranging from 270 cm 2 /gm to 4100 cm 2 /gm at two fissioning rates 10 12 f/cm 3 . sec. and 3.2x10 10 f/cm.sec. A relation between K and A has been established and discussed in this report. (author). 6 refs

  18. Apparent increase in the thickness of superconducting particles at low temperatures measured by electron holography.

    Science.gov (United States)

    Hirsch, J E

    2013-10-01

    We predict that superconducting particles will show an apparent increase in thickness at low temperatures when measured by electron holography. This will result not from a real thickness increase, rather from an increase in the mean inner potential sensed by the electron wave traveling through the particle, originating in expansion of the electronic wavefunction of the superconducting electrons and resulting negative charge expulsion from the interior to the surface of the superconductor, giving rise to an increase in the phase shift of the electron wavefront going through the sample relative to the wavefront going through vacuum. The temperature dependence of the observed phase shifts will yield valuable new information on the physics of the superconducting state of metals. Copyright © 2013 Elsevier B.V. All rights reserved.

  19. Design and assembly of a torsion pendulum for the measurement of internal friction at low temperatures

    International Nuclear Information System (INIS)

    San Juan, J. M.; Gallego, I.; No, M. L.

    2001-01-01

    In this work we describe the assembly, operation and specifications of an inverted torsion pendulum designed to measure internal friction at low temperatures (from 4.2 K to 500 K). The high precision mechanics allow us to obtain internal friction spectra with low levels of noise from amplitudes as small as 2x10''7. The inertia components of the pendulum have been built with specific materials, so that the resonance frequency of the pendulum can be changed within two orders of magnitude (0.1-10Hz). In addition, the sample can be in situ deformed at any temperature and can be inserted into the pendulum at liquid nitrogen temperature. The operation of the pendulum, all the control p recesses and data acquisition are completely automated. (Author) 4 refs

  20. System and method for heating ferrite magnet motors for low temperatures

    Science.gov (United States)

    Reddy, Patel Bhageerath; El-Refaie, Ayman Mohamed Fawzi; Huh, Kum-Kang

    2017-07-04

    A system and method for heating ferrite permanent magnets in an electrical machine is disclosed. The permanent magnet machine includes a stator assembly and a rotor assembly, with a plurality of ferrite permanent magnets disposed within the stator assembly or the rotor assembly to generate a magnetic field that interacts with a stator magnetic field to produce a torque. A controller of the electrical machine is programmed to cause a primary field current to be applied to the stator windings to generate the stator magnetic field, so as to cause the rotor assembly to rotate relative to the stator assembly. The controller is further programmed to cause a secondary current to be applied to the stator windings to selectively generate a secondary magnetic field, the secondary magnetic field inducing eddy currents in at least one of the stator assembly and the rotor assembly to heat the ferrite permanent magnets.

  1. System and method for heating ferrite magnet motors for low temperatures

    Science.gov (United States)

    Reddy, Patel Bhageerath; El-Refaie, Ayman Mohamed Fawzi; Huh, Kum-Kang

    2018-05-08

    A system and method for heating ferrite permanent magnets in an electrical machine is disclosed. The permanent magnet machine includes a stator assembly and a rotor assembly, with a plurality of ferrite permanent magnets disposed within the stator assembly or the rotor assembly to generate a magnetic field that interacts with a stator magnetic field to produce a torque. A controller of the electrical machine is programmed to cause a primary field current to be applied to the stator windings to generate the stator magnetic field, so as to cause the rotor assembly to rotate relative to the stator assembly. The controller is further programmed to cause a secondary current to be applied to the stator windings to selectively generate a secondary magnetic field, the secondary magnetic field inducing eddy currents in at least one of the stator assembly and the rotor assembly to heat the ferrite permanent magnets.

  2. In Situ Irradiation and Measurement of Triple Junction Solar Cells at Low Intensity, Low Temperature (LILT) Conditions

    Science.gov (United States)

    Harris, R.D.; Imaizumi, M.; Walters, R.J.; Lorentzen, J.R.; Messenger, S.R.; Tischler, J.G.; Ohshima, T.; Sato, S.; Sharps, P.R.; Fatemi, N.S.

    2008-01-01

    The performance of triple junction InGaP/(In)GaAs/Ge space solar cells was studied following high energy electron irradiation at low temperature. Cell characterization was carried out in situ at the irradiation temperature while using low intensity illumination, and, as such, these conditions reflect those found for deep space, solar powered missions that are far from the sun. Cell characterization consisted of I-V measurements and quantum efficiency measurements. The low temperature irradiations caused substantial degradation that differs in some ways from that seen after room temperature irradiations. The short circuit current degrades more at low temperature while the open circuit voltage degrades more at room temperature. A room temperature anneal after the low temperature irradiation produced a substantial recovery in the degradation. Following irradiation at both temperatures and an extended room temperature anneal, quantum efficiency measurement suggests that the bulk of the remaining damage is in the (In)GaAs sub-cell

  3. Effect of impurity scattering on the low temperature magnetic penetration depth of a nonlocal and nonlinear d-wave superconductor

    International Nuclear Information System (INIS)

    Yavary, H.

    2006-01-01

    The magnetic penetration depth of a quasi-two dimensional d-wave superconductor in the presence of nonlineary, nonlocality, and impurity effects is investigated by using Green's function method. It is shown that a d-wave superconductor would inevitably avoid the violation of the Nernst theorem by creating a T 2 term in its penetration depth through a competition of nonlinear, nonlocal, and impurity effects and this system may be stable at low temperatures. I also show that in the impure sample at low temperatures, T < T * ∝ γ the impurity effect determines the temperature dependence of the penetration depth, i.e., nonlocal and nonlinear effects are completely masked by impurities

  4. Normal state resistance and low temperature magnetoresistance of superconducting cables for accelerator magnets

    International Nuclear Information System (INIS)

    Sampson, W.B.; Garber, M.; Ghosh, A.K.

    1988-01-01

    The normal state resistivity of the superconducting NbTi cable used in accelerator magnets is usually specified by the resistance per unit length at room temperature (295 K) and the residual resistance ratio (RRR). Using these resistance parameters, the amount of copper in the multifilamentary wire can be calculated. This method is consistent with the traditional etch and weigh technique, and as such is a alternative and convenient way of specifying the copper to superconductor ratio. In principle the magnetoresistance can be calculated from the RRR and the ''Kohler Plot'', for copper. In practice however, measurements of magnetoresistance for a wide variety of SSC inner cables show considerable disagreement with calculation. In this paper the magnetoresistance data on cables with RRR ranging from 50 to 175 are analyzed taking into account the conductor geometry and the effect of the small interfilamentary spacing on the resistivity of copper. 8 refs., 5 figs., 1 tab

  5. Normal and superconducting state properties of U6Fe at low temperatures and high magnetic fields

    International Nuclear Information System (INIS)

    DeLong, L.E.; Crabtree, G.W.; Hall, L.N.; Kierstead, H.; Aoki, H.; Dhar, S.K.; Gschneidner, K.A. Jr.; Junod, A.

    1985-01-01

    High purity U 6 Fe polycrystals with a resistance ratio rrr=9 at T=4 K are found to exhibit a record onset temperature (T 0 >4.0 K) to superconductivity for U materials. Our measured values of the electronic coefficient of heat capacity Csup(*)=(150+-3) mJ/mol.K 2 , the mean Debye temperature THETA(T->0)=116 K and the normalized jump in heat capacity at Tsub(c), ΔC/γsup(*)Tsub(c)=2.3+-0.1, are all in good agreement with previous work, and suggest that U 6 Fe is a strong-coupled superconductor. Resistive upper critical field measurements on high purity samples revealed a pronounced S-shaped curvature of Hsub(c2)(T) and evidence for anisotropy, similar to effects seen in UPt 3 , but not observed in lower purity U 6 Fe samples. We find Hsub(c2)(0)>10 T and transition widths ΔTsub(c)proportionalHsup(1/2) at moderate fields, followed by an abrupt increase in ΔTsub(c) for H>8 T. Our Hsub(c2) data cannot be explained by existing theoretical models. Preliminary heat capacity measurements in magnetic fields 0 6 Fe at T< or approx.110 K. (orig.)

  6. Low-temperature magnetic properties of Fe3C/iron oxide nanocomposite

    Czech Academy of Sciences Publication Activity Database

    David, Bohumil; Schneeweiss, Oldřich; Mašláň, M.; Šantavá, Eva; Morjan, I.

    2007-01-01

    Roč. 316, č. 2 (2007), s. 422-425 ISSN 0304-8853. [Joint European Magnetic Symposia /3./ (JEMS´06). San Sebastian, 26.06.2006-30.06.2006] R&D Projects: GA MŠk 1M0512 Institutional research plan: CEZ:AV0Z20410507; CEZ:AV0Z10100520 Keywords : Nanopowder * Fe3C * Mossbauer spectroscopy * Magnetic properties * AC susceptibility Subject RIV: BM - Solid Matter Physics ; Magnetism Impact factor: 1.704, year: 2007

  7. Low temperature synthesis of coiled carbon nanotubes and their magnetic properties

    Science.gov (United States)

    Krishna, Vemula Mohana; Somanathan, T.; Manikandan, E.

    2018-04-01

    In this paper, coiled like structure of carbon nanotubes (c-CNTs) have been effectively grown on bi-metal substituted α-alumina nanoparticles catalyst by chemical vapor deposition (CVD) system. Highly graphitized and dense bundles of carbon product were attained at a low temperature of 550 °C. The coiled carbon nanostructures in very longer lengths were noticed by field emission scanning electron microscope (FESEM) observation. Furthermore, high purity material was achieved, which correlates the energy dispersive x-ray spectroscopy (EDX) analysis. High resolution transmission electron microscope (HRTEM) revealed the diameter and graphitization of coiled structures. The superparamagnetic like behavior was observed at room temperature for the as-synthesized product, which was found by VSM investigation.

  8. Low-temperature magnetic properties of NpNi.sub.5./sub..

    Czech Academy of Sciences Publication Activity Database

    Hen, A.; Colineau, E.; Eloirdi, R.; Griveau, J.C.; Magnani, N.; Wilhelm, F.; Rogalev, A.; Sanchez, J.-P.; Shick, Alexander; Halevy, I.; Orion, I.; Caciuffo, R.

    2014-01-01

    Roč. 89, č. 5 (2014), "054480-1"-"054480-11" ISSN 1098-0121 R&D Projects: GA ČR(CZ) GAP204/10/0330 Institutional support: RVO:68378271 Keywords : magnetism * Mossbauer spectra * XMCD Subject RIV: BM - Solid Matter Physics ; Magnetism Impact factor: 3.736, year: 2014

  9. Photo-Hall measurements on phosphorus-doped n-type CVD diamond at low temperatures

    Czech Academy of Sciences Publication Activity Database

    Remeš, Zdeněk; Kalish, R.; Uzan-Saguy, C.; Baskin, E.; Nesládek, M.; Koizumi, S.

    2003-01-01

    Roč. 199, č. 1 (2003), s. 82-86 ISSN 0031-8965 EU Projects: European Commission(XE) HPRN-CT-1999-00139 Institutional research plan: CEZ:AV0Z1010914 Keywords : photo-Hall measurements * CVD diamonnd * phosphorus doped Subject RIV: BM - Solid Matter Physics ; Magnetism Impact factor: 0.950, year: 2003

  10. Low-temperature magnetic behavior of ball-milled copper ferrite

    DEFF Research Database (Denmark)

    Goya, G.F.; Rechenberg, H.R.; Jiang, Jianzhong

    1999-01-01

    We present a study on magnetic properties of CuFe2O4 nanoparticles, produced by high-energy ball milling. The series of samples obtained, with average particle sizes LFAN alpha d RTAN ranging from 61 nm to 9 nm, display increasing relaxation effects at room temperature. Irreversibility of the mag......We present a study on magnetic properties of CuFe2O4 nanoparticles, produced by high-energy ball milling. The series of samples obtained, with average particle sizes LFAN alpha d RTAN ranging from 61 nm to 9 nm, display increasing relaxation effects at room temperature. Irreversibility...... of the magnetization and shifts to negative fields in the hysteresis loops are observed below T-f APEQ 55 K, indicating unidirectional magnetic anisotropy in milled samples. These features could be explained by assuming the formation of a spin-disordered surface layer, which is exchange-coupled to the ferrimagnetic...

  11. Low temperature X-ray imaging of magnetic flux patterns in high temperature superconductors

    Science.gov (United States)

    Stahl, Claudia; Ruoß, Stephen; Weigand, Markus; Bechtel, Michael; Schütz, Gisela; Albrecht, Joachim

    2015-05-01

    We present X-ray magnetic circular dichroism (XMCD) microscopy results obtained at liquid nitrogen temperatures on the high-Tc superconductor YBCO (YBa2Cu3O7-δ). The magnetic flux distribution arising from electric currents in the superconductor is detected and visualized using soft-magnetic Co40Fe40B20 (CoFeB) as sensor layer and XMCD as contrast mechanism. It has been shown that the XMCD contrast in the sensor layer directly corresponds to magnetic flux distribution of the superconductor and hence can be used to image magnetic structures in superconductors [Stahl et al., Phys. Rev. B 90, 104515 (2014)]. The existing scanning UHV X-ray microscopy setup MAXYMUS at the synchrotron BESSY II in Berlin has been upgraded for that purpose: we use a nitrogen based MMR Micro Miniature Joule-Thompson Cryostat with temperature range from 75 K to 580 K. The capability of the method is demonstrated on two different superconducting samples, an optimally doped thin film and a melt-textured block.

  12. Critical current measurements of high Tc superconductors in a scanning low temperature cryostat

    International Nuclear Information System (INIS)

    Telschow, K.L.; O'Brien, T.K.

    1991-01-01

    Maintaining uniformity of properties over long distances is one of the fabrication problems encountered with the new high T c superconductors. Uniform properties are crucial in long tapes or wires with high critical current since local nonuniformities can limit the current carrying capacity of the whole piece. Transport critical currents in high T c superconductors are conventionally measured with the contact 4-point probe DC current-voltage technique. This technique requires contact with the sample and and spatially averages over the region between the two voltage contacts. Two techniques have been used to infer the critical state model. The first uses the net magnetization of a suitably shaped sample in an external magnetic field. The second combines a DC magnetic field with AC induced currents to infer spatial flux profiles. The AC magnetization technique offers an advantage in that it is noncontacting; however, it also averages the measurement over a large area and requires that the sample be shaped and positioned such that it exhibits zero demagnetizing factor. This paper describes a measurement technique and a scanning cryostat assembly that are capable of determining local critical current in a tape or wire with high resolution and without any direct sample electrical contact. A small compensated coil was used to induce AC currents in slab-shaped samples. The coil was situated near the surface on one side of the slab. With this method, the AC probe can be used as a noncontacting dissipation probe, replacing the voltage probe in the 4-point contact method, when an externally driven transport current is used, or by itself as a local critical state generator and dissipation detector. The results are shown to be meaningful even when the internal magnetic field is not uniform due to shape demagnetizing effects. 10 refs., 5 figs

  13. Scattering of magnetized electrons at the boundary of low temperature plasmas

    Science.gov (United States)

    Krüger, Dennis; Trieschmann, Jan; Brinkmann, Ralf Peter

    2018-02-01

    Magnetized technological plasmas with magnetic fields of 10-200 mT, plasma densities of 1017-1019 m-3, gas pressures of less than 1 Pa, and electron energies from a few to (at most) a few hundred electron volts are characterized by electron Larmor radii r L, that are small compared to all other length scales of the system, including the spatial scale L of the magnetic field and the collisional mean free path λ. In this regime, the classical drift approximation applies. In the boundary sheath of these discharges, however, that approximation breaks down: The sheath penetration depth of electrons (a few to some ten Debye length λ D; depending on the kinetic energy; typically much smaller than the sheath thickness of tens/hundreds of λ D) is even smaller than r L. For a model description of the electron dynamics, an appropriate boundary condition for the plasma/sheath interface is required. To develop such, the interaction of magnetized electrons with the boundary sheath is investigated using a 3D kinetic single electron model that sets the larger scales L and λ to infinity, i.e. neglects magnetic field gradients, the electric field in the bulk, and collisions. A detailed comparison of the interaction for a Bohm sheath (which assumes a finite Debye length) and a hard wall model (representing the limit {λ }{{D}}\\to 0; also called the specular reflection model) is conducted. Both models are found to be in remarkable agreement with respect to the sheath-induced drift. It is concluded that the assumption of specular reflection can be used as a valid boundary condition for more realistic kinetic models of magnetized technological plasmas.

  14. Nanocalorimeter platform for in situ specific heat measurements and x-ray diffraction at low temperature

    Science.gov (United States)

    Willa, K.; Diao, Z.; Campanini, D.; Welp, U.; Divan, R.; Hudl, M.; Islam, Z.; Kwok, W.-K.; Rydh, A.

    2017-12-01

    Recent advances in electronics and nanofabrication have enabled membrane-based nanocalorimetry for measurements of the specific heat of microgram-sized samples. We have integrated a nanocalorimeter platform into a 4.5 T split-pair vertical-field magnet to allow for the simultaneous measurement of the specific heat and x-ray scattering in magnetic fields and at temperatures as low as 4 K. This multi-modal approach empowers researchers to directly correlate scattering experiments with insights from thermodynamic properties including structural, electronic, orbital, and magnetic phase transitions. The use of a nanocalorimeter sample platform enables numerous technical advantages: precise measurement and control of the sample temperature, quantification of beam heating effects, fast and precise positioning of the sample in the x-ray beam, and fast acquisition of x-ray scans over a wide temperature range without the need for time-consuming re-centering and re-alignment. Furthermore, on an YBa2Cu3O7-δ crystal and a copper foil, we demonstrate a novel approach to x-ray absorption spectroscopy by monitoring the change in sample temperature as a function of incident photon energy. Finally, we illustrate the new insights that can be gained from in situ structural and thermodynamic measurements by investigating the superheated state occurring at the first-order magneto-elastic phase transition of Fe2P, a material that is of interest for magnetocaloric applications.

  15. Materials studies for magnetic fusion energy applications at low temperatures. VIII. Technical reports

    International Nuclear Information System (INIS)

    Reed, R.P.

    1985-05-01

    This report contains results of a research progam to produce material property data that will facilitte design and development of cryogenic structures for the superconducting magnets of magnetic fusion energy power plants and prototypes. Research results for 1984 are summarized in an initial ''Highlights of Results'' section and reported in detail in the technical papers that form the main body of this report. The technical papers are presented under four headings reflecting the main program areas: Welding, Nonmetallics, Structural Alloys, and Technology Transfer. Objectives, approaches, and achievements are summarized in an introduction to each program area

  16. Design and fabrication of sintered Nd-Fe-B magnets with a low temperature coefficient of intrinsic coercivity

    Directory of Open Access Journals (Sweden)

    Cui X.G.

    2009-01-01

    Full Text Available To decrease the temperature coefficients of sintered Nd-Fe-B magnets, the influencing factors on temperature coefficients, especially the reversible temperature coefficient β of intrinsic coercivity Hcj, were analyzed. The results showed that the absolute value of β decreased with increasing Hcj and also the ratio of microstructure parameter c to Neff, indicating that the increase of magnetocrystalline anisotropy field HA and c/Neff can effectively decrease the absolute value of β. On the basis of this analysis, a sintered Nd-Fe-B magnet with a low temperature coefficient of Hcj was fabricated through composition design, and the value of β was only -0.385%/ºC in the temperature interval of 20-150ºC.

  17. Performance of silicon PIN photodiodes at low temperatures and in high magnetic fields

    Czech Academy of Sciences Publication Activity Database

    Wauters, F.; Kraeva, I.S.; Tandecki, M.; Traykov, E.; Van Gorp, S.; Zákoucký, Dalibor; Severijns, N.

    2009-01-01

    Roč. 604, č. 3 (2009), s. 563-567 ISSN 0168-9002 Institutional research plan: CEZ:AV0Z10480505 Keywords : PIN-diode * beta-particle detection * Magnetic field Subject RIV: BG - Nuclear, Atomic and Molecular Physics, Colliders Impact factor: 1.317, year: 2009

  18. Dynamic Nuclear Polarization at low temperature and high magnetic eld for biomedical applications in Magnetic Resonance Spectroscopic Imaging

    International Nuclear Information System (INIS)

    Goutailler, Florent

    2011-01-01

    The aim of this thesis work was to design, build and optimize a large volume multi-samples DNP (Dynamic Nuclear Polarization) polarizer dedicated to Magnetic Resonance Spectroscopic Imaging applications. The experimental system is made up of a high magnetic field magnet (3,35 T) in which takes place a cryogenic system with a pumped bath of liquid helium ("4He) allowing temperatures lower than 1,2 K. A set of inserts is used for the different steps of DNP: irradiation of the sample by a microwave field (f=94 GHz and P=50 mW), polarization measurement by Nuclear Magnetic Resonance... With this system, up to three samples of 1 mL volume can be polarized to a rate of few per-cents. The system has a long autonomy of four hours, so it can be used for polarizing molecules with a long time constant of polarization. Finally, the possibility to get quasi-simultaneously, after dissolution, several samples with a high rate of polarization opens the way of new applications in biomedical imaging. (author) [fr

  19. Low-temperature DC-contact piezoelectric switch operable in high magnetic fields

    CERN Document Server

    Kaltenbacher, T; Doser, M; Kellerbauer, A; Pribyl, W

    2013-01-01

    A piezoelectric single-pole single-throw (SPST) switch has been developed, since there is no satisfying commercial low-resistance, high current DC-contact RF switch available which is operable at 4.2K and in a high magnetic field of at least 0.5T. This piezoelectric switch shows very low insertion loss of less than -0.1dB within a bandwidth of 100MHz when operated at 4.2K. The switch could also be used to mechanically disconnect and connect electrodes or electrical circuits from one another.

  20. Low-temperature DC-contact piezoelectric switch operable in high magnetic fields

    Energy Technology Data Exchange (ETDEWEB)

    Kaltenbacher, Thomas, E-mail: thomas.kaltenbacher@cern.ch [Physics and Accelerator Departments, CERN, 1211 Geneva 23 (Switzerland); Institute of Electronics, Graz University of Technology, Inffeldgasse 12, 8010 Graz (Austria); Caspers, Fritz; Doser, Michael [Physics and Accelerator Departments, CERN, 1211 Geneva 23 (Switzerland); Kellerbauer, Alban [Max Planck Institute for Nuclear Physics, Saupfercheckweg 1, 69117 Heidelberg (Germany); Pribyl, Wolfgang [Institute of Electronics, Graz University of Technology, Inffeldgasse 12, 8010 Graz (Austria)

    2013-11-21

    A piezoelectric single-pole single-throw (SPST) switch has been developed, since there is no satisfying commercial low-resistance, high current DC-contact RF switch available which is operable at 4.2 K and in a high magnetic field of at least 0.5 T. This piezoelectric switch shows very low insertion loss of less than −0.1 dB within a bandwidth of 100 MHz when operated at 4.2 K. The switch could also be used to mechanically disconnect and connect electrodes or electrical circuits from one another.

  1. Accurate solid solution range of BiMnxFe3-xO6 and low temperature magnetism

    Science.gov (United States)

    Jiang, Pengfei; Yue, Mufei; Cong, Rihong; Gao, Wenliang; Yang, Tao

    2017-11-01

    BiMnxFe3-xO6 (x = 1) represents a new type of oxide structure containing Bi3+ and competing magnetic super-exchanges. In literature, multiple magnetic states were realized at low temperatures in BiMnFe2O6, and the hypothetical parent compounds (BiMn3O6, BiFe3O6) were predicted to be different in magnetism. Herein, we performed a careful study on the syntheses of BiMnxFe3-xO6 at ambient pressure, and the solid solution range was determined to be 0.9 ≤ x ≤ 1.3 by Rietveld refinements on high-quality powder X-ray diffraction data. Due to the very similar cationic size of Mn3+ and Fe3+, and possibly the structural rigidity, there was no significant structure change in the whole range of solid solution. The magnetic behavior of BiMnxFe3-xO6 (x = 1.2, 1.22, 1.26, 1.28 and 1.3) was generally similar to BiMnFe2O6, while the relative higher concentration of Mn3+ led to the decreasing of the antiferromagnetic ordering temperature.

  2. Prospects for sub-micron solid state nuclear magnetic resonance imaging with low-temperature dynamic nuclear polarization.

    Science.gov (United States)

    Thurber, Kent R; Tycko, Robert

    2010-06-14

    We evaluate the feasibility of (1)H nuclear magnetic resonance (NMR) imaging with sub-micron voxel dimensions using a combination of low temperatures and dynamic nuclear polarization (DNP). Experiments are performed on nitroxide-doped glycerol-water at 9.4 T and temperatures below 40 K, using a 30 mW tunable microwave source for DNP. With DNP at 7 K, a 0.5 microL sample yields a (1)H NMR signal-to-noise ratio of 770 in two scans with pulsed spin-lock detection and after 80 db signal attenuation. With reasonable extrapolations, we infer that (1)H NMR signals from 1 microm(3) voxel volumes should be readily detectable, and voxels as small as 0.03 microm(3) may eventually be detectable. Through homonuclear decoupling with a frequency-switched Lee-Goldburg spin echo technique, we obtain 830 Hz (1)H NMR linewidths at low temperatures, implying that pulsed field gradients equal to 0.4 G/d or less would be required during spatial encoding dimensions of an imaging sequence, where d is the resolution in each dimension.

  3. Effect of low temperature neutron irradiation on the magnetoresistivity in stabilizer materials for a superconducting magnet

    International Nuclear Information System (INIS)

    Nakata, Kiyotomo; Tada, Naobumi; Masaoka, Isao; Takamura, Saburo.

    1985-01-01

    Magnetoresistivity changes caused by neutron irradiation at 5 K, annealing up to 300 K and cyclic irradiation are studied in copper and aluminuim stabilizer materials at 4.2 K. The radiation-induced resistivity in Al is about three times as large as that in Cu, and the resistivities in both Al and Cu are independent of the purity and the degree of cold-work of the samples. The radiation-induced magnetoresistivity of the high purity Cu with R.R.R. (R sub(298 K)/R sub(4.2 K)) of 1400 is larger than that of the impure Cu with R.R.R. of 300 and 280. The magnetoresistivities of the high purity Cu and Al with R.R.R. of 1500 increase with the magetic field. Magnetoresistivity change with the magnetic field in the irradiated Cu mostly follows Kohler's rule, and that in the irradiated Al does not follow the rule at high magnetic fields. By the annealing at 300 K after the irradiation, the radiation-induced resistivity is completely annihilated in the Al, but about 20 % of the resistivity retains in the full-annealed Cu and the retained resistivity is accumulated during the cyclic irradiation. Though the accumulated resistivity in the cold-worked Cu is smaller than that in the full-annealed one, the resistivity before irradiation in the cold-worked samples is very large. From the above results, the full-annealed Cu with R.R.R. of about 300 is considered to be the best material as a stabilizer used under irradiation. (author)

  4. Low temperature ultrahigh vacuum cross-sectional scanning tunneling microscope for luminescence measurements

    International Nuclear Information System (INIS)

    Khang, Yoonho; Park, Yeonjoon; Salmeron, Miquel; Weber, Eicke R.

    1999-01-01

    We have constructed a scanning tunneling microscope with simultaneous light collection capabilities in order to investigate the opto-electronic properties of semiconductors. The microscope has in situ sample cleavage mechanism for cross-sectional sample. In order to reach low temperature (4 K), we used a specially designed cryostat. The efficiency of light collection generated in the tip-surface junction was greatly improved by use of a small parabolic mirror with the tip located at its focal point. (c) 1999 American Institute of Physics

  5. Angular dependence of Jc for YBCO coated conductors at low temperature and very high magnetic fields

    International Nuclear Information System (INIS)

    Xu, A; Jaroszynski, J J; Kametani, F; Chen, Z; Larbalestier, D C; Viouchkov, Y L; Chen, Y; Xie, Y; Selvamanickam, V

    2010-01-01

    We present very high field angle dependent critical current density (J c ) data for three recently obtained YBa 2 Cu 3 O 7-x (YBCO) coated conductors used in the construction of high field solenoids. We find that strongly correlated pins, such as BaZrO 3 (BZO) nanorods, while yielding strong c-axis peaks at 77 K, produce almost no measurable contribution at 4 K. Raising the field from c (θ) at low fields to a marked cusp-like behavior at high fields. Transmission electron micrographs show that all samples contain a high density of stacking faults which strengthen the plane correlated pinning parallel to the ab planes produced by the intrinsic ab-plane pinning of the Cu-O charge reservoir layers.

  6. The low temperature specific heat and electrical transport, magnetic properties of Pr{sub 0.65}Ca{sub 0.35}MnO{sub 3}

    Energy Technology Data Exchange (ETDEWEB)

    Han, Zhiyong, E-mail: zyhan@cauc.edu.cn

    2017-02-01

    The magnetic properties, electrical transport properties, and low temperature specific heat of polycrystalline perovskite manganese oxide Pr{sub 0.65}Ca{sub 0.35}MnO{sub 3} have been investigated experimentally. It is found that there exists cluster glass state in the sample at low temperature besides the antiferromagnetic insulating state. With the increase of magnetic field, antiferromagnetic insulating state converts to ferromagnetic metal state and the Debye temperature decreases gradually. In addition, the low temperature electron specific heat in zero magnetic field is obviously larger than that of ordinary rare-earth manganites oxide and this phenomenon is related to the itinerant electrons in ferromagnetic cluster state and the disorder in Pr{sub 0.65}Ca{sub 0.35}MnO{sub 3}. - Highlights: • There exists cluster glass state in the sample at low temperature besides the antiferromagnetic insulating state. • With the increase of magnetic field, antiferromagnetic insulating state converts to ferromagnetic metal state. • Low temperature electron specific heat in zero magnetic field is larger than that of ordinary rare-earth manganites oxide.

  7. Low-temperature synthesis, structural and magnetic properties of self-dopant LaMnO{sub 3+δ} nanoparticles from a metal-organic polymeric precursor

    Energy Technology Data Exchange (ETDEWEB)

    Ahmad, Tokeer, E-mail: tahmad3@jmi.ac.in [Nanochemistry Laboratory, Department of Chemistry, Jamia Millia Islamia, New Delhi 110025 (India); Lone, Irfan H.; Ubaidullah, Mohd. [Nanochemistry Laboratory, Department of Chemistry, Jamia Millia Islamia, New Delhi 110025 (India); Coolhan, Kelsey [Department of Physics and Astronomy, Rowan University, 201 Mullica Hill Road, Glassboro, NJ 08028 (United States)

    2013-11-15

    Graphical abstract: Monophasic and highly crystalline Self-dopant LaMnO{sub 3+δ} nanoparticles (72 nm) have been successfully synthesized at low temperature (773 K) by metal citrate complex method based on Pechini-type reaction route which showed ferromagnetic interaction. Surface areas of LaMnO{sub 3+δ} nanoparticles were found to be 157.4 and 153 m{sup 2} g{sup −1} for the samples annealed at 773 K and 1173 K, respectively. - Highlights: • Self-dopant LaMnO{sub 3+δ} nanoparticles using Pechini-type reaction route at 773 K. • Size range varies from 72 to 80 nm. • Surface area varies from 153 to 157 m{sup 2} g{sup −1}. • Extensive characterization using sophisticated techniques. - Abstract: Self-dopant LaMnO{sub 3+δ} nanoparticles have been successfully synthesized by metal citrate complex method based on Pechini-type reaction route, at low temperature (773 K). Powder X-ray diffraction and transmission electron microscope revealed pure and nanostructured phase of LaMnO{sub 3+δ} (δ = 0.125) with an average grain size of ∼72 nm (773 K) and ∼80 nm (1173 K). DC-magnetization measurements under an applied magnetic field of H = ±60 kOe showed an increase in the magnetization with the increase of calcination temperature. Ferromagnetic nature shown by non-stoichiometric LaMnO{sub 3+δ} was verified by well-defined hysteresis loop with large remanent magnetization (M{sub r}) and coercive field (H{sub c}). Surface areas of LaMnO{sub 3+δ} nanoparticles were found to be 157.4 and 153 m{sup 2} g{sup −1} for the samples annealed at 773 K and 1173 K, respectively.

  8. Commissioning and modification of the low temperature scanning polarization microscope (TTSPM) and imaging of the local magnetic flux density distribution in superconducting niobium samples

    International Nuclear Information System (INIS)

    Gruenzweig, Matthias Sebastian Peter

    2014-01-01

    The dissertation is separated into two different parts, which will be presented in the following. Part I of the dissertation is about the commissioning and the modification of the ''low-temperature scanning polarization microscope'' which was designed in a previous dissertation of Stefan Guenon [1]. A scanning polarization microscope has certain advantages compared to conventional polarization microscopes. With a scanning polarization microscope it is easily possible to achieve a high illumination intensity, which is important to realize a high signal-to-noise ratio. Moreover, the confocal design of the scanning polarization microscope improves the resolution of the microscope by a factor of 1.4. Normally, it is not necessary to post-process the images by means of differential frame method to eliminate the contrast of non-magnetic origin. In contrast to conventional polarization microscopes the low-temperature scanning polarization microscope is able to image electronic transport properties via beam-induced voltage variation in addition to the magneto-optical effects. In this dissertation, it was possible to demonstrate the performance capability of the scanning polarization microscope at room temperature as well as at low temperatures. The investigation of the polar Kerr-effect has been carried out with a BaFe 12 O 19 -test sample whereas the measurements of the longitudinal Kerr-effect have been carried out with an in-plane magnetized acceleration sensor. Furthermore, an independent room temperature construction for out-of-plane measurements in a magnetic field up to 1 Tesla has been designed and implemented within the framework of a diploma thesis, supervised by the author of this dissertation. Using this construction, it was possible to gain experimental results regarding the interlayer exchange coupling between iron-terbium alloys (Fe 1-x Tb x ) and cobalt-platinum multilayers (vertical stroke Co/Pt vertical stroke n ). Indeed, it has been

  9. Low-temperature phase MnBi compound: A potential candidate for rare-earth free permanent magnets

    International Nuclear Information System (INIS)

    Ly, V.; Wu, X.; Smillie, L.; Shoji, T.; Kato, A.; Manabe, A.; Suzuki, K.

    2014-01-01

    Highlights: • The spin reorientation temperature of MnBi is suppressed by nanoscale grain refinement. • Hardness parameter of MnBi reaches as large as 2.8 at 580 K. • MnBi has a great potential as a hard phase in rare-earth free nanocomposite magnets. • Improving the surface passivity is a remaining task for MnBi-based permanent magnets. - Abstract: The low-temperature phase (LTP) MnBi is one of the few rare-earth free compounds that exhibit a large magnetocrystalline anisotropy energy in the order of 10 6 J/m 3 . A large coercive field (μ 0 H cj ) above 1 T can be obtained readily by reducing the crystallite size (D) through mechanical grinding (MG). The room-temperature H cj values follow a phenomenological expression μ 0 H cj = μ 0 H a (δ/D) n where the anisotropy field (μ 0 H a ) is ∼4 T, the Bloch wall width (δ) is 7 nm and the exponent (n) is about 0.7 in our study. The grain refinement upon MG is accompanied by suppression of the spin reorientation transition temperature (T SR ) from 110 K to below 50 K. The coercive field starts to exhibit positive temperature dependence approximately 50 K above T SR and the room-temperature magnetic hardening induced by MG could partially be brought about by the lowered onset of this positive temperature dependence. The suppression of T SR by MG is likely to be induced by the surface anisotropy with which the 2nd order crystal field term is enhanced. One of the shortcomings of LTP-MnBi is its poor phase stability under the ambient atmosphere. The spontaneous magnetization decreases considerably after room-temperature aging for 1 week. This is due to oxidation of Mn which leads to decomposition of the MnBi phase. Hence, the surface passivity needs to be established before this material is considered for a permanent magnet in practical uses. Another shortcoming is the limited spontaneous magnetization. The theoretical upper limit of the maximum energy product in LTP-MnBi remains only a quarter of that in Nd 2

  10. A Peltier cooling diamond anvil cell for low-temperature Raman spectroscopic measurements

    Science.gov (United States)

    Noguchi, Naoki; Okuchi, Takuo

    2016-12-01

    A new cooling system using Peltier modules is presented for a low-temperature diamond anvil cell instrument. This cooling system has many advantages: it is vibration-free, low-cost, and compact. It consists of double-stacked Peltier modules and heat sinks, where a cooled ethylene glycol-water mixture flows through a chiller. Current is applied to the Peltier modules by two programmable DC power supplies. Sample temperature can be controlled within the range 210-300 K with a precision of ±0.1 K via a Proportional-Integral-Differential (PID) control loop. A Raman spectroscopic study for the H2O ice VII-VIII transition is shown as an example of an application of the Peltier cooling diamond anvil cell system.

  11. The investigation of the magnetic after-effect in iron-alpha after neutron irradiation at low temperature

    International Nuclear Information System (INIS)

    Mensch, W.

    1986-01-01

    The present thesis investigates the magnetic after-effect for neutron irradiated, polycrystalline iron-alpha for the temperature range 10 to 400 K by means of susceptibility measurements. 24 maxima of magnetic after-effect are found, which are related to different classes of defects. (BHO)

  12. Measuring hydroperoxide chain-branching agents during n-pentane low-temperature oxidation

    KAUST Repository

    Rodriguez, Anne

    2016-06-23

    The reactions of chain-branching agents, such as HO and hydroperoxides, have a decisive role in the occurrence of autoignition. The formation of these agents has been investigated in an atmospheric-pressure jet-stirred reactor during the low-temperature oxidation of n-pentane (initial fuel mole fraction of 0.01, residence time of 2s) using three different diagnostics: time-of-flight mass spectrometry combined with tunable synchrotron photoionization, time-of-flight mass spectrometry combined with laser photoionization, and cw-cavity ring-down spectroscopy. These three diagnostics enable a combined analysis of HO, C-C, and C alkylhydroperoxides, C-C alkenylhydroperoxides, and C alkylhydroperoxides including a carbonyl function (ketohydroperoxides). Results using both types of mass spectrometry are compared for the stoichiometric mixture. Formation data are presented at equivalence ratios from 0.5 to 2 for these peroxides and of two oxygenated products, ketene and pentanediones, which are not usually analyzed during jet-stirred reactor oxidation. The formation of alkenylhydroperoxides during alkane oxidation is followed for the first time. A recently developed model of n-pentane oxidation aids discussion of the kinetics of these products and of proposed pathways for C-C alkenylhydroperoxides and the pentanediones.

  13. Low temperature magneto-dielectric measurements on BiFeO3 lightly substituted by cobalt

    International Nuclear Information System (INIS)

    Ray, J.; Biswal, A. K.; Vishwakarma, P. N.

    2015-01-01

    Dielectric and magnetodielectric measurements are done on BiFe 1−x Co x O 3 : x = 0, 0.01, and 0.02 in the temperature range 70–300 K and up to magnetic field 1.3 T. The dielectric data are well described by Haverliak–Negami expression plus an additional term for the Maxwell Wagner (MW) type relaxations, whose contribution is dominant near room temperature. The parameters obtained from the fitting of data using the above mentioned expression, suggest slowing down of relaxation and approach towards ideal Debye type relaxations, as the temperature is lowered. The dielectric relaxations obey polaronic variable range hopping model with distinct activation energies (E a ) in the extrinsic (6.67T 3/4  meV) and intrinsic (2.88T 3/4  meV) regions for the parent sample (x = 0), and thus a distinct transition from extrinsic to intrinsic behavior is seen at 215 K while lowering the temperature. This distinct transition is missing for Co substituted samples probably due to the extrinsic region values of E a (3.42T 3/4  meV and 2.42T 3/4  meV for x = 0.01 and 0.02, respectively) comparable to that of the intrinsic region (see x = 0). The magnetodielectric measurement shows positive magnetodielectricity (MD) in the intrinsic region (T < 215 K for x = 0) and negative MD in the extrinsic region (T > 215 K for x = 0). The extrinsic region is found to be dominated by MW and magnetoresistance effects, whereas MD in intrinsic regions is due to the spin reorientation transitions. The Co substitution is found to increase the extrinsic and non-Debye contributions to dielectricity, which becomes so large that no spin reorientation transitions are seen in x = 0.02 sample. The pyroelectric active region in x = 0 is found to be dominated by the diffusive behavior having contribution of the form ω −0.5

  14. Low-temperature magnetic susceptibility of the solid solutions (ErxY1-x)3Al5O12

    International Nuclear Information System (INIS)

    Bagdasarov, Kh.S.; Dodokin, A.P.; Sorokin, A.A.

    1988-01-01

    Measurements of magnetic susceptibility of erbium-yttrium alumogarnets in the 0.04-4.2 K temperature range are carried out. (Er x I 1-x ) 3 Al 5 O 12 monocrystals were grown by the method of vertical directed crystallization. The specimens were produced as 5 cm high cylinders 0.63 cm in diameter; the axis of the cylinders coincided with the (100) direction of the crystals. Magnetic susceptibility was measured by the Harsthorn bridge method at the frequency of 33 Hz. The analysis of measurement results shows that susceptibility of the investigated crystals at T >or approx. 2T N is well described by the Curie-Weiss law. Existence of threshold concentration of the magnetic component testifies to an essential role of exchange interactions in establishment of the magnetic order in Er 3 Al 5 O 12

  15. Low-temperature phase MnBi compound: A potential candidate for rare-earth free permanent magnets

    Energy Technology Data Exchange (ETDEWEB)

    Ly, V.; Wu, X.; Smillie, L. [Department of Materials Engineering, Monash University, Clayton, VIC 3800 (Australia); Shoji, T.; Kato, A.; Manabe, A. [Toyota Motor Corporation, Mishuku, Susono, Shizuoka 410-1193 (Japan); Suzuki, K., E-mail: kiyonori.suzuki@monash.edu [Department of Materials Engineering, Monash University, Clayton, VIC 3800 (Australia)

    2014-12-05

    Highlights: • The spin reorientation temperature of MnBi is suppressed by nanoscale grain refinement. • Hardness parameter of MnBi reaches as large as 2.8 at 580 K. • MnBi has a great potential as a hard phase in rare-earth free nanocomposite magnets. • Improving the surface passivity is a remaining task for MnBi-based permanent magnets. - Abstract: The low-temperature phase (LTP) MnBi is one of the few rare-earth free compounds that exhibit a large magnetocrystalline anisotropy energy in the order of 10{sup 6} J/m{sup 3}. A large coercive field (μ{sub 0}H{sub cj}) above 1 T can be obtained readily by reducing the crystallite size (D) through mechanical grinding (MG). The room-temperature H{sub cj} values follow a phenomenological expression μ{sub 0}H{sub cj} = μ{sub 0}H{sub a}(δ/D){sup n} where the anisotropy field (μ{sub 0}H{sub a}) is ∼4 T, the Bloch wall width (δ) is 7 nm and the exponent (n) is about 0.7 in our study. The grain refinement upon MG is accompanied by suppression of the spin reorientation transition temperature (T{sub SR}) from 110 K to below 50 K. The coercive field starts to exhibit positive temperature dependence approximately 50 K above T{sub SR} and the room-temperature magnetic hardening induced by MG could partially be brought about by the lowered onset of this positive temperature dependence. The suppression of T{sub SR} by MG is likely to be induced by the surface anisotropy with which the 2nd order crystal field term is enhanced. One of the shortcomings of LTP-MnBi is its poor phase stability under the ambient atmosphere. The spontaneous magnetization decreases considerably after room-temperature aging for 1 week. This is due to oxidation of Mn which leads to decomposition of the MnBi phase. Hence, the surface passivity needs to be established before this material is considered for a permanent magnet in practical uses. Another shortcoming is the limited spontaneous magnetization. The theoretical upper limit of the maximum

  16. Low-temperature measurement system based on a closed-cycle refrigerator

    Energy Technology Data Exchange (ETDEWEB)

    Tsuji, Mitsuyuki; Kawamata, Shuichi; Ishida, Takekazu; Okayasu, Satoru; Hojou, Kiichi

    2003-05-01

    We have built a new torque magnetometer with a closed-cycle helium refrigerator. The temperature can be lowered down to 1.5 K by pumping liquefied helium in sample space. The temperature can be stabilized within {+-}0.01 K by using the two-independent PID loops. A piezoresistor bridge configured with a silicon cantilever surface is used to detect a torque. A transeverse magnetic field, which is fabricated by the several pieces of the permanent magnets, can produce a field up to 10 kG in any direction. The system has complete control from a computer by coding a LabVIEW. We have demonstrated the torque curves of a single crystal YBa{sub 2}Cu{sub 4}O{sub 8} successfully even at 1.6 K.

  17. Low-temperature measurement system based on a closed-cycle refrigerator

    International Nuclear Information System (INIS)

    Tsuji, Mitsuyuki; Kawamata, Shuichi; Ishida, Takekazu; Okayasu, Satoru; Hojou, Kiichi

    2003-01-01

    We have built a new torque magnetometer with a closed-cycle helium refrigerator. The temperature can be lowered down to 1.5 K by pumping liquefied helium in sample space. The temperature can be stabilized within ±0.01 K by using the two-independent PID loops. A piezoresistor bridge configured with a silicon cantilever surface is used to detect a torque. A transeverse magnetic field, which is fabricated by the several pieces of the permanent magnets, can produce a field up to 10 kG in any direction. The system has complete control from a computer by coding a LabVIEW. We have demonstrated the torque curves of a single crystal YBa 2 Cu 4 O 8 successfully even at 1.6 K

  18. Application of SQUIDs to low temperature and high magnetic field measurements—Ultra low noise torque magnetometry

    Science.gov (United States)

    Arnold, F.; Naumann, M.; Lühmann, Th.; Mackenzie, A. P.; Hassinger, E.

    2018-02-01

    Torque magnetometry is a key method to measure the magnetic anisotropy and quantum oscillations in metals. In order to resolve quantum oscillations in sub-millimeter sized samples, piezo-electric micro-cantilevers were introduced. In the case of strongly correlated metals with large Fermi surfaces and high cyclotron masses, magnetic torque resolving powers in excess of 104 are required at temperatures well below 1 K and magnetic fields beyond 10 T. Here, we present a new broadband read-out scheme for piezo-electric micro-cantilevers via Wheatstone-type resistance measurements in magnetic fields up to 15 T and temperatures down to 200 mK. By using a two-stage superconducting-quantum interference device as a null detector of a cold Wheatstone bridge, we were able to achieve a magnetic moment resolution of Δm = 4 × 10-15 J/T at maximal field and 700 mK, outperforming conventional magnetometers by at least one order of magnitude in this temperature and magnetic field range. Exemplary de Haas-van Alphen measurement of a newly grown delafossite, PdRhO2, was used to show the superior performance of our setup.

  19. Direct measurement of the low temperature spin state transitions in La1-xSrxCoO3 (0.05 < x < 0.3)

    Science.gov (United States)

    Gulec, A.; Klie, R. F.

    2014-12-01

    Sr-doped LaCoO3 has a complex magnetic phase diagram, which is believed to be directly correlated to changes in the crystal structure and ordering of the Co3+ spin states. In this work, we study the low temperature Co3+-ion spin state transitions in Sr-doped LaCoO3 around the critical doping concentration where a metal to insulator transition has been observed using electron energy-loss spectroscopy of the O K-edge combined with the Co L-edge fine structure. We measure the local spin state of the Co3+-ions and we demonstrate that the Co3+ spin-state transition only occurs in La0.95Sr0.05CoO3 single-crystal materials in the temperature range accessible by LN2 in-situ cooling, while no structural symmetry change is observed. The presence of this low-temperature spin-state transition in La1-xSrxCoO3 (x < 0.17) has been proposed as the origin of the percolative magnetic ordering in doped LaCoO3.

  20. Low-temperature transport properties of chemical solution deposited polycrystalline La0.7Sr0.3MnO3 ferromagnetic films under a magnetic field

    International Nuclear Information System (INIS)

    Zhu, Junyu; Chen, Ying; Xu, Wenfei; Yang, Jing; Bai, Wei; Wang, Genshui; Duan, Chungang; Tang, Zheng; Tang, Xiaodong

    2011-01-01

    Polycrystalline La 0.7 Sr 0.3 MnO 3 (LSMO) films were prepared on SiO 2 /Si (001) substrates by chemical solution deposition technique. Electrical and magnetic properties of LSMO were investigated. A minimum phenomenon in resistivity is found at the low temperature ( 0.7 Sr 0.3 MnO 3 films were grown by a modified chemical solution deposition route. → High quality LSMO thin films were prepared directly onto SiO 2 /Si substrates. → Abnormality in resistivity of LSMO films at low temperatures was studied in detail. → The abnormality was mainly attributed to Kondo-like spin dependent scattering.

  1. Facility for low-temperature spin-polarized-scanning tunneling microscopy studies of magnetic/spintronic materials prepared in situ by nitride molecular beam epitaxy

    Energy Technology Data Exchange (ETDEWEB)

    Lin, Wenzhi; Foley, Andrew; Alam, Khan; Wang, Kangkang; Liu, Yinghao; Chen, Tianjiao; Pak, Jeongihm; Smith, Arthur R., E-mail: smitha2@ohio.edu [Department of Physics and Astronomy, Nanoscale and Quantum Phenomena Institute, Ohio University, Athens, Ohio 45701 (United States)

    2014-04-15

    Based on the interest in, as well as exciting outlook for, nitride semiconductor based structures with regard to electronic, optoelectronic, and spintronic applications, it is compelling to investigate these systems using the powerful technique of spin-polarized scanning tunneling microscopy (STM), a technique capable of achieving magnetic resolution down to the atomic scale. However, the delicate surfaces of these materials are easily corrupted by in-air transfers, making it unfeasible to study them in stand-alone ultra-high vacuum STM facilities. Therefore, we have carried out the development of a hybrid system including a nitrogen plasma assisted molecular beam epitaxy/pulsed laser epitaxy facility for sample growth combined with a low-temperature, spin-polarized scanning tunneling microscope system. The custom-designed molecular beam epitaxy growth system supports up to eight sources, including up to seven effusion cells plus a radio frequency nitrogen plasma source, for epitaxially growing a variety of materials, such as nitride semiconductors, magnetic materials, and their hetero-structures, and also incorporating in situ reflection high energy electron diffraction. The growth system also enables integration of pulsed laser epitaxy. The STM unit has a modular design, consisting of an upper body and a lower body. The upper body contains the coarse approach mechanism and the scanner unit, while the lower body accepts molecular beam epitaxy grown samples using compression springs and sample skis. The design of the system employs two stages of vibration isolation as well as a layer of acoustic noise isolation in order to reduce noise during STM measurements. This isolation allows the system to effectively acquire STM data in a typical lab space, which during its construction had no special and highly costly elements included, (such as isolated slabs) which would lower the environmental noise. The design further enables tip exchange and tip coating without

  2. Facility for low-temperature spin-polarized-scanning tunneling microscopy studies of magnetic/spintronic materials prepared in situ by nitride molecular beam epitaxy.

    Science.gov (United States)

    Lin, Wenzhi; Foley, Andrew; Alam, Khan; Wang, Kangkang; Liu, Yinghao; Chen, Tianjiao; Pak, Jeongihm; Smith, Arthur R

    2014-04-01

    Based on the interest in, as well as exciting outlook for, nitride semiconductor based structures with regard to electronic, optoelectronic, and spintronic applications, it is compelling to investigate these systems using the powerful technique of spin-polarized scanning tunneling microscopy (STM), a technique capable of achieving magnetic resolution down to the atomic scale. However, the delicate surfaces of these materials are easily corrupted by in-air transfers, making it unfeasible to study them in stand-alone ultra-high vacuum STM facilities. Therefore, we have carried out the development of a hybrid system including a nitrogen plasma assisted molecular beam epitaxy/pulsed laser epitaxy facility for sample growth combined with a low-temperature, spin-polarized scanning tunneling microscope system. The custom-designed molecular beam epitaxy growth system supports up to eight sources, including up to seven effusion cells plus a radio frequency nitrogen plasma source, for epitaxially growing a variety of materials, such as nitride semiconductors, magnetic materials, and their hetero-structures, and also incorporating in situ reflection high energy electron diffraction. The growth system also enables integration of pulsed laser epitaxy. The STM unit has a modular design, consisting of an upper body and a lower body. The upper body contains the coarse approach mechanism and the scanner unit, while the lower body accepts molecular beam epitaxy grown samples using compression springs and sample skis. The design of the system employs two stages of vibration isolation as well as a layer of acoustic noise isolation in order to reduce noise during STM measurements. This isolation allows the system to effectively acquire STM data in a typical lab space, which during its construction had no special and highly costly elements included, (such as isolated slabs) which would lower the environmental noise. The design further enables tip exchange and tip coating without

  3. Facility for low-temperature spin-polarized-scanning tunneling microscopy studies of magnetic/spintronic materials prepared in situ by nitride molecular beam epitaxy

    International Nuclear Information System (INIS)

    Lin, Wenzhi; Foley, Andrew; Alam, Khan; Wang, Kangkang; Liu, Yinghao; Chen, Tianjiao; Pak, Jeongihm; Smith, Arthur R.

    2014-01-01

    Based on the interest in, as well as exciting outlook for, nitride semiconductor based structures with regard to electronic, optoelectronic, and spintronic applications, it is compelling to investigate these systems using the powerful technique of spin-polarized scanning tunneling microscopy (STM), a technique capable of achieving magnetic resolution down to the atomic scale. However, the delicate surfaces of these materials are easily corrupted by in-air transfers, making it unfeasible to study them in stand-alone ultra-high vacuum STM facilities. Therefore, we have carried out the development of a hybrid system including a nitrogen plasma assisted molecular beam epitaxy/pulsed laser epitaxy facility for sample growth combined with a low-temperature, spin-polarized scanning tunneling microscope system. The custom-designed molecular beam epitaxy growth system supports up to eight sources, including up to seven effusion cells plus a radio frequency nitrogen plasma source, for epitaxially growing a variety of materials, such as nitride semiconductors, magnetic materials, and their hetero-structures, and also incorporating in situ reflection high energy electron diffraction. The growth system also enables integration of pulsed laser epitaxy. The STM unit has a modular design, consisting of an upper body and a lower body. The upper body contains the coarse approach mechanism and the scanner unit, while the lower body accepts molecular beam epitaxy grown samples using compression springs and sample skis. The design of the system employs two stages of vibration isolation as well as a layer of acoustic noise isolation in order to reduce noise during STM measurements. This isolation allows the system to effectively acquire STM data in a typical lab space, which during its construction had no special and highly costly elements included, (such as isolated slabs) which would lower the environmental noise. The design further enables tip exchange and tip coating without

  4. Deformation measurements of materials at low temperatures using laser speckle photography method

    International Nuclear Information System (INIS)

    Sumio Nakahara; Yukihide Maeda; Kazunori Matsumura; Shigeyoshi Hisada; Takeyoshi Fujita; Kiyoshi Sugihara

    1992-01-01

    The authors observed deformations of several materials during cooling down process from room temperature to liquid nitrogen temperature using the laser speckle photography method. The in-plane displacements were measured by the image plane speckle photography and the out-of-plane displacement gradients by the defocused speckle photography. The results of measurements of in-plane displacement are compared with those of FEM analysis. The applicability of laser speckle photography method to cryogenic engineering are also discussed

  5. A cryostatic setup for the low-temperature measurement of thermal diffusivity with the photothermal method

    International Nuclear Information System (INIS)

    Bertolotti, M.; Liakhou, G.; Li Voti, R.; Paoloni, S.; Sibilia, C.; Sparvieri, N.

    1995-01-01

    A cryostatic setup is described to perform photothermal deflection measurements from room temperature to 77 K. The setup uses gaseous nitrogen as a medium where the photodeflection is produced. The ability of the system to work is demonstrated presenting some measurements of thermal diffusivity of high-temperature superconductor samples and of yttrium-iron garnets with variable aluminum content. copyright 1995 American Institute of Physics

  6. Low-temperature relative reflectivity measurements of reflective and scintillating foils used in rare event searches

    Science.gov (United States)

    Langenkämper, A.; Ulrich, A.; Defay, X.; Feilitzsch, F. v.; Lanfranchi, J.-C.; Mondragón, E.; Münster, A.; Oppenheimer, C.; Potzel, W.; Roth, S.; Schönert, S.; Steiger, H.; Trinh Thi, H. H.; Wawoczny, S.; Willers, M.; Zöller, A.

    2018-03-01

    In this work we investigate the reflectivity of highly reflective multilayer polymer foils used in the CRESST experiment. The CRESST experiment searches directly for dark matter via operating scintillating CaWO4 crystals as targets for elastic dark matter-nucleon scattering. In order to suppress background events, the experiment employs the so-called phonon-light technique which is based on the simultaneous measurement of the heat signal in the main CaWO4 target crystal and of the emitted scintillation light with a separate cryogenic light detector. Both detectors are surrounded by a highly reflective and scintillating multilayer polymer foil to increase the light collection efficiency and to veto surface backgrounds. While this study is motivated by the CRESST experiment, the results are also relevant for other rare event searches using scintillating cryogenic bolometers in the field of the search of dark matter and neutrinoless double beta decay (0 νββ). In this work a dedicated experiment has been set up to determine the relative reflectivity at 300 K and 20 K of three multilayer foils ("VM2000", "VM2002", "Vikuiti") produced by the company 3M. The intensity of a light beam reflected off the foil is measured with a CCD camera. The ratio of the intensities at 300 K and 20 K corresponds to the relative reflectivity change. The measurements performed in this work show no variation of the reflectivity with temperature at a level of ∼1%.

  7. Low-temperature thermal expansion measurements in PrV2Al20

    International Nuclear Information System (INIS)

    Magata, A.; Matsumoto, Y.; Tsujimoto, M.; Tomita, T.; Sakai, A.; Nakatsuji, S.; Kiichler, R.

    2016-01-01

    We have measured thermal expansion of PrV 2 Al 20 and LaV 2 Al 20 from room temperature down to 2 K, using a capacitance dilatometer. Linear thermal expansion ΔL/L along [111] direction decreases monotonically on cooling in both materials. The extracted 4ƒ electrons contribution of the linear thermal expansion coefficient a clearly shows a broad peak at ∼ 30 K which may correspond to the crystal electric field excited state at 40 K suggested in the previous specific heat study. (paper)

  8. Thermodynamics of hydrogen adsorption in MOF-177 at low temperatures: measurements and modelling

    Energy Technology Data Exchange (ETDEWEB)

    Poirier, Eric [College of Engineering, Purdue University, West Lafayette, IN 47907 (United States); Dailly, Anne [Chemical and Environmental Sciences Laboratory, General Motors Corporation, Warren, MI 48090 (United States)], E-mail: poirierem@gmail.com, E-mail: anne.dailly@gm.com

    2009-05-20

    Hydrogen adsorption measurements and modelling for the Zn-based microporous metal-organic framework (MOF) Zn{sub 4}O(1,3,5-benzenetribenzoate){sub 2}, MOF-177, were performed over the 50-77 K and 0-40 bar ranges. The maximum excess adsorption measured under these conditions varies over about 105-70 mg g{sup -1}. An analysis of the isotherms near saturation shows that hydrogen is ultimately adsorbed in an incompressible phase whose density is comparable to that of the bulk liquid. These liquid state properties observed under supercritical conditions reveal a remarkable effect of nanoscale confinement. The entire set of adsorption isotherms can be well described using a micropore filling model. The latter is used, in particular, to determine the absolute amounts adsorbed and the adsorption enthalpy. When expressed in terms of absolute adsorption, the isotherms show considerable hydrogen storage capacities, reaching up to 125 mg g{sup -1} at 50 K and 25 bar. The adsorption enthalpies are calculated as a function of fractional filling and range from 3 to 5 kJ mol{sup -1} in magnitude, in accordance with physisorption. These results are discussed with respect to a similar analysis performed on another Zn-based MOF, Zn{sub 4}O(1,4-benzenedicarboxylate){sub 3}, IRMOF-1, presented recently. It is found that both materials adsorb hydrogen by similar mechanisms.

  9. Neutron spin echo measurements of monolayer and capillary condensed water in MCM-41 at low temperatures

    International Nuclear Information System (INIS)

    Yoshida, K; Yamaguchi, T; Kittaka, S; Bellissent-Funel, M-C; Fouquet, P

    2012-01-01

    Neutron spin echo measurements of monolayer and capillary condensed heavy water (D 2 O) confined in MCM-41 C10 (pore diameter 2.10 nm) were performed in a temperature range of 190-298 K. The intermediate scattering functions were analyzed by the Kohlrausch-Williams-Watts stretched exponential function. The relaxation times of confined D 2 O in the capillary condensed state follow remarkably well the Vogel-Fulcher-Tammann equation between 298 and 220 K, whereas below 220 K they show an Arrhenius type behavior. That is, the fragile-to-strong (FTS) dynamic crossover occurs, which has never been seen in experiments on bulk water. On the other hand, for monolayer D 2 O, the FTS dynamic crossover was not observed in the temperature range measured. The FTS dynamic crossover observed in capillary condensed water would take place in the central region of the pore, not near the pore surface. Because the tetrahedral-like water structure in the central region of the pore is more preserved than that near the pore surface, the FTS dynamic crossover would be concerned with the tetrahedral-like water structure. (paper)

  10. Thermodynamics of hydrogen adsorption in MOF-177 at low temperatures: measurements and modelling

    International Nuclear Information System (INIS)

    Poirier, Eric; Dailly, Anne

    2009-01-01

    Hydrogen adsorption measurements and modelling for the Zn-based microporous metal-organic framework (MOF) Zn 4 O(1,3,5-benzenetribenzoate) 2 , MOF-177, were performed over the 50-77 K and 0-40 bar ranges. The maximum excess adsorption measured under these conditions varies over about 105-70 mg g -1 . An analysis of the isotherms near saturation shows that hydrogen is ultimately adsorbed in an incompressible phase whose density is comparable to that of the bulk liquid. These liquid state properties observed under supercritical conditions reveal a remarkable effect of nanoscale confinement. The entire set of adsorption isotherms can be well described using a micropore filling model. The latter is used, in particular, to determine the absolute amounts adsorbed and the adsorption enthalpy. When expressed in terms of absolute adsorption, the isotherms show considerable hydrogen storage capacities, reaching up to 125 mg g -1 at 50 K and 25 bar. The adsorption enthalpies are calculated as a function of fractional filling and range from 3 to 5 kJ mol -1 in magnitude, in accordance with physisorption. These results are discussed with respect to a similar analysis performed on another Zn-based MOF, Zn 4 O(1,4-benzenedicarboxylate) 3 , IRMOF-1, presented recently. It is found that both materials adsorb hydrogen by similar mechanisms.

  11. Design of a low temperature translation balance for the measurement of paramagnetic and diamagnetic susceptibilities

    Energy Technology Data Exchange (ETDEWEB)

    Mowry, G.S.

    1979-05-01

    A modified Foex and Forrer Translation Balance has been designed for measuring the paramagnetic and diamagnetic properties of materials over the temperature range 77-300/sup 0/K. The systems' temperature range can eventually be extended to 4.2/sup 0/K. The apparatus incorporates a vertical Dewar of Standard variety in addition to a horizontal Dewar for cooling the sample holder and adjacent horizontal supports. The design also allows for the placement of a thermocouple junction in direct contact with a sample. The balance sensitivity, defined as the change in displacement per unit applied force, is 0.0044 cm/dyne. The precision of the balance is +- .5% with an accuracy of 1.5%.

  12. Internal friction measurements of Mo after low-temperature proton irradiation

    International Nuclear Information System (INIS)

    Tanimoto, H.; Mizubayashi, H.; Masuda, R.; Okuda, S.; Tagishi, Y.

    1992-01-01

    Internal friction measurements are performed in Mo after 20 MeV proton irradiation in order to clarify the behavior of self-interstitial atoms (SIA's) in Mo. In the low dose range, strong dislocation pinning suggesting the free migration of defects is observed at about 40 K and weak pinning at about 25 K. The features are very similar to those reported after neutron irradiation except that the 25 K pinning is much smaller after proton irradiation. The result suggests that the migration of free SIA's is responsible for the 40 K pinning and that of SIA-defect clusters, probably di-SIA's, formed during irradiation for the 25 K pinning. In the high dose range, the relaxation peaks are observed at about 13 and 41 K, where the close similarities are found between the present peaks and the corresponding peaks reported after neutron irradiation except that the peak height of the 41 K peak per unit concentration of Frenkel pairs (FP) tends to increase strongly with decreasing dose here. The latter fact suggests the strong interaction between SIA's. Then the smallness of the 41 K peak reported after electron irradiation with very high dose could be explained by an increased interaction between SIA's, but not by the two-dimensional migration of SIA's as proposed by Jacques and Robrock. Deformation given prior to irradiation causes a drastic decrease in the modulus defects associated with FP's (so-called bulk effect) and in the 13 K peak height. After neutron irradiation, no such effect of deformation was reported. A possible origin for this difference is discussed. (orig.)

  13. The low-temperature magnetostructure and magnetic field response of Pr0.9Ca0.1MnO3

    DEFF Research Database (Denmark)

    Tikkanen, J.; Frontzek, M.; Hergert, W.

    2016-01-01

    phase separation model of manganites to the material under discussion despite its very low Ca doping level in the context of the model. In the light of the new data, we also conclude that the low temperature magnetic moment of Pr must be ca. 300% larger than previously thought in this material, close...... calculations. Particular emphasis was placed on determining the presence of nanoscale magnetic phase separation. Previously published results of a canted A-AFM average ground state were reproduced to a good precision both experimentally and theoretically, and complemented by investigating the effects...... of an applied magnetic field of 2.7 T on the magnetostructure. Explicit evidence of nanoscale magnetic clusters in the material was obtained based on high-resolution neutron diffractograms. Along with several supporting arguments, we present this finding as a justification for extending the nanoscale magnetic...

  14. Development of a sample environment for neutron diffraction at low temperature

    International Nuclear Information System (INIS)

    Lee, Jeong Soo; Lee, Chang Hee; Choi, Yong Nam

    2000-06-01

    This report contains the development of low temperature sample environment for the neutron diffraction and its utilization techniques. With this research, a low temperature experimental facility of T=10-300 K was developed. We measured magnetic peak of La 1 .4Sr 1 .6Mn 2 O 7 due to low temperature phase transition successfully by this unit installed at the sample table of HRPD. Therefore, the research capability for various materials under the low temperature was expanded

  15. Spin-state crossover and low-temperature magnetic state in yttrium-doped Pr0.7Ca0.3CoO3

    Science.gov (United States)

    Knížek, K.; Hejtmánek, J.; Maryško, M.; Novák, P.; Šantavá, E.; Jirák, Z.; Naito, T.; Fujishiro, H.; de la Cruz, Clarina

    2013-12-01

    The structural and magnetic properties of two mixed-valence cobaltites with a formal population of 0.30 Co4+ ions per f.u., (Pr1-yYy)0.7Ca0.3CoO3 (y=0 and 0.15), have been studied down to very low temperatures by means of high-resolution neutron diffraction, SQUID magnetometry, and heat-capacity measurements. The results are interpreted within the scenario of the spin-state crossover from a room-temperature mixture of the intermediate-spin Co3+ and low-spin Co4+ (IS/LS) to the LS/LS mixture in the sample ground states. In contrast to the yttrium-free y=0 that retains the metallic-like character and exhibits ferromagnetic (FM) ordering below 55 K, the doped system y=0.15 undergoes a first-order metal-insulator transition at 132 K, during which not only the crossover to low-spin states but also a partial electron transfer from Pr3+ 4f to cobalt 3d states takes place simultaneously. Taking into account the nonmagnetic character of LS Co3+, such a valence shift electronic transition causes a magnetic dilution, formally to 0.12 LS Co4+ or 0.12 t2g hole spins per f.u., which is the reason for an insulating, highly nonuniform magnetic ground state without long-range order. Nevertheless, even in that case there exists a relatively strong molecular field distributed over all the crystal lattice. It is argued that the spontaneous FM order in y=0 and the existence of strong FM correlations in y=0.15 apparently contradict the single t2g band character of LS/LS phase. The explanation we suggest relies on a model of the defect-induced, itinerant hole-mediated magnetism, where the defects are identified with the magnetic high-spin Co3+ species stabilized near oxygen vacancies.

  16. Construction of an apparatus for nuclear orientation measurements at low temperatures. Application to neodymium-cobalt alloy

    International Nuclear Information System (INIS)

    Mayer, E.

    1965-10-01

    We describe experiments along which has been studied the anisotropy of γ radiations emitted by oriented nuclei. We have used the great hyperfine fields acting on nuclei in ferromagnetic metals so as to produce alignment at low temperature. By irradiation we obtained a few cobalt 60 nuclei in our samples which were then cooled down to 0,01 K. The anisotropic rate of the 1,33 MeV γ radiation was measured in function of the sample temperature, using as thermometer the anisotropy of γ radiation emitted by cobalt 60 nuclei in a cobalt single crystal. Cobalt 60 was lined up in a cobalt nickel alloy (40% Ni). The hyperfine field at the cobalt was measured compared to the effective field in metallic cobalt: Heff(Co Ni)/Heff(Co metal) = 0.71 ± 0.12. These results are in good agreement with specific heat measurements made previously. Cobalt 60 has been polarised in a neodymium-cobalt alloy (NdCo 5 ). The field at the cobalt in NdCo 5 has been measured compared to the field in metallic cobalt and taking the non-saturation into account we found 165000 oersteds 5 ) [fr

  17. Effect of Static and Rotating Magnetic Fields on Low-Temperature Fabrication of InGaZnO Thin-Film Transistors.

    Science.gov (United States)

    Park, Jeong Woo; Tak, Young Jun; Na, Jae Won; Lee, Heesoo; Kim, Won-Gi; Kim, Hyun Jae

    2018-05-16

    We suggest thermal treatment with static magnetic fields (SMFs) or rotating magnetic fields (RMFs) as a new technique for the activation of indium-gallium-zinc oxide thin-film transistors (IGZO TFTs). Magnetic interactions between metal atoms in IGZO films and oxygen atoms in air by SMFs or RMFs can be expected to enhance metal-oxide (M-O) bonds, even at low temperature (150 °C), through attraction of metal and oxygen atoms having their magnetic moments aligned in the same direction. Compared to IGZO TFTs with only thermal treatment at 300 °C, IGZO TFTs under an RMF (1150 rpm) at 150 °C show superior or comparable characteristics: field-effect mobility of 12.68 cm 2 V -1 s -1 , subthreshold swing of 0.37 V dec -1 , and on/off ratio of 1.86 × 10 8 . Although IGZO TFTs under an SMF (0 rpm) can be activated at 150 °C, the electrical performance is further improved in IGZO TFTs under an RMF (1150 rpm). These improvements of IGZO TFTs under an RMF (1150 rpm) are induced by increases in the number of M-O bonds due to enhancement of the magnetic interaction per unit time as the rpm value increases. We suggest that this new process of activating IGZO TFTs at low temperature widens the choice of substrates in flexible or transparent devices.

  18. The Nd-Mn exchange interaction, low temperature specific heat and magnetism of Nd{sub 2/3}Ca{sub 1/3}MnO{sub 3}

    Energy Technology Data Exchange (ETDEWEB)

    Beznosov, Anatoly [B. Verkin Institute for Low Temperature Physics and Engineering NASU, 47 Lenin Avenue, Kharkov 61103 (Ukraine); Fertman, Elena, E-mail: fertman@ilt.kharkov.ua [B. Verkin Institute for Low Temperature Physics and Engineering NASU, 47 Lenin Avenue, Kharkov 61103 (Ukraine); Desnenko, Vladimir [B. Verkin Institute for Low Temperature Physics and Engineering NASU, 47 Lenin Avenue, Kharkov 61103 (Ukraine); Kajnakova, Marcela; Feher, Alexander [Centre of Low Temperature Physics of the Faculty of Science UPJS and IEP SAS, Park Angelinum 9, 04154 Kosice (Slovakia)

    2011-10-15

    The low temperature specific heat and magnetic characteristics of Nd{sub 2/3}Ca{sub 1/3}MnO{sub 3} perovskite are studied in a wide range of magnetic fields (up to 9 T). Temperature dependent specific heat data show a broadened Schottky-like anomaly below 20 K caused by splitting of the Nd{sup 3+} ions ground-state doublet in the effective molecular field H{sub ex}, determined by exchange interaction between Nd and Mn spin systems supplemented by an applied external magnetic field. Existence of the splitting at zero magnetic field and expressed field dependence is the evidence of a strong exchange coupling between Nd and Mn magnetic subsystems. The Nd-ions magnetic ordering leads to an additional contribution to the magnetic moment of the system below 30 K, producing anomalies of the magnetic loss and field-cooled and zero-field-cooled magnetizations. The observed broadened Schottky-like anomalies are fitted for each applied magnetic field by the sum of three Schottky functions. Applied magnetic field extends the anomaly region and shifts it to higher temperatures. Splitting of the higher crystal field Kramers doublets gives an additional contribution to the heat capacity in magnetic fields. The ground state doublet g-factors g{sub ||} and g{sub perpendicular} were estimated to be 3.4 and 2.2, respectively, and H{sub ex} was estimated to be 9 T. The Nd{sup 3+} ions magnetic moment estimated from the magnetization data agrees with the value obtained from the specific heat data. - Highlights: > Low temperature specific heat of Nd{sub 2/3}Ca{sub 1/3}MnO{sub 3} has been measured in magnetic fields up to 9 T. > Schottky-like anomalies are fitted for each magnetic field by a sum of three Schottky functions. > An effective magnetic field of the Mn spin system on Nd ion has been estimated as H{sub ex}=9 T. > Nd{sup 3+} ground-state g-factors have been estimated as g{sub ||}=3.4 and g{sub perpendicular} =2.2. > Magnetic ordering of the Nd subsystem has been revealed below

  19. Magnetic properties of hydrothermally synthesized greigite (Fe3S4)- II. High- and low-temperature characteristics

    NARCIS (Netherlands)

    Dekkers, M.J.; Passier, Hilde F.; Schoonen, M.A.A.

    1999-01-01

    The magnetic behaviour of hydrothermally synthesized greigite was analysed in the temperature range from 4 K to 700 °C. Below room temperature, hysteresis parameters were determined as a function of temperature, with emphasis on the temperature range below 50 K. Saturation magnetization and

  20. Nanocalorimeter platform for in situ specific heat measurements and x-ray diffraction at low temperature

    Energy Technology Data Exchange (ETDEWEB)

    Willa, K. [Materials Science Division, Argonne National Laboratory, 9700 South Cass Avenue, Argonne, Illinois 60439, USA; Diao, Z. [Department of Physics, Stockholm University, SE-106 91 Stockholm, Sweden; Laboratory of Mathematics, Physics and Electrical Engineering, Halmstad University, P.O. Box 823, SE-301 18 Halmstad, Sweden; Campanini, D. [Department of Physics, Stockholm University, SE-106 91 Stockholm, Sweden; Welp, U. [Materials Science Division, Argonne National Laboratory, 9700 South Cass Avenue, Argonne, Illinois 60439, USA; Divan, R. [Center for Nanoscale Materials, Argonne National Laboratory, 9700 South Cass Avenue, Argonne, Illinois 60439, USA; Hudl, M. [Department of Physics, Stockholm University, SE-106 91 Stockholm, Sweden; Islam, Z. [X-ray Science Division, Argonne National Laboratory, 9700 South Cass Avenue, Argonne, Illinois 60439, USA; Kwok, W. -K. [Materials Science Division, Argonne National Laboratory, 9700 South Cass Avenue, Argonne, Illinois 60439, USA; Rydh, A. [Department of Physics, Stockholm University, SE-106 91 Stockholm, Sweden

    2017-12-01

    Recent advances in electronics and nanofabrication have enabled membrane-based nanocalorimetry for measurements of the specific heat of microgram-sized samples. We have integrated a nanocalorimeter platform into a 4.5 T split-pair vertical-field magnet to allow for the simultaneous measurement of the specific heat and x-ray scattering in magnetic fields and at temperatures as low as 4 K. This multi-modal approach empowers researchers to directly correlate scattering experiments with insights from thermodynamic properties including structural, electronic, orbital, and magnetic phase transitions. The use of a nanocalorimeter sample platform enables numerous technical advantages: precise measurement and control of the sample temperature, quantification of beam heating effects, fast and precise positioning of the sample in the x-ray beam, and fast acquisition of x-ray scans over a wide temperature range without the need for time-consuming re-centering and re-alignment. Furthermore, on an YBa2Cu3O7-delta crystal and a copper foil, we demonstrate a novel approach to x-ray absorption spectroscopy by monitoring the change in sample temperature as a function of incident photon energy. Finally, we illustrate the new insights that can be gained from in situ structural and thermodynamic measurements by investigating the superheated state occurring at the first-order magneto-elastic phase transition of Fe2P, a material that is of interest for magnetocaloric applications.

  1. Ionization and acoustical instability of a low temperature magnetized plasma in a combined (direct and alternating) electrical field

    International Nuclear Information System (INIS)

    Andropov, V.G.; Sinkevich, O.A.

    1983-01-01

    It is shown that the ionization front which moves through a gas along a magnetic field in a combined electrical field, which lies in the plane of the front, may be unstable, as a result of the development of an ionization instability in the plasma behind the front. The criterion of instability of the ionization front does not greatly differ from the criterion of instability of an infinite plasma. The ionization front in the magnetic field is stable only in an electrical field of circular polarization or in a combined field in which the direct and alternating electrical fields are orthogonal and the Joule heat liberation from them is equal. The generation of sound is possible in a magnetized plasma in an alternating electrical field orthogonal to a magnetic due to the parametric acoustical instability at the frequency of the external electrical field. 8 refs

  2. Development and testing of a new apparatus for the measurement of high-pressure low-temperature phase equilibria

    DEFF Research Database (Denmark)

    Fonseca, José M.S.; von Solms, Nicolas

    2012-01-01

    A new apparatus for the study of high-pressure phase equilibria at low temperatures using an analytical method was designed, assembled and tested. The apparatus was specially developed for the study of multi-phase equilibria in systems containing hydrocarbons, water and hydrate inhibitors, at tem...

  3. Low-temperature thermal expansion

    International Nuclear Information System (INIS)

    Collings, E.W.

    1986-01-01

    This chapter discusses the thermal expansion of insulators and metals. Harmonicity and anharmonicity in thermal expansion are examined. The electronic, magnetic, an other contributions to low temperature thermal expansion are analyzed. The thermodynamics of the Debye isotropic continuum, the lattice-dynamical approach, and the thermal expansion of metals are discussed. Relative linear expansion at low temperatures is reviewed and further calculations of the electronic thermal expansion coefficient are given. Thermal expansions are given for Cu, Al and Ti. Phenomenologic thermodynamic relationships are also discussed

  4. The low-temperature, high-magnetic-field critical current characteristics of Zr-added (Gd, Y)Ba2Cu3Ox superconducting tapes

    Energy Technology Data Exchange (ETDEWEB)

    Selvamanickam, V; Yao, Y; Chen, Y; Shi, T; Liu, Y; Khatri, ND; Liu, J; Lei, C; Galstyan, E; Majkic, G

    2012-10-26

    Critical current performances of state-of-the-art Zr-added (Gd, Y)BaCuO tapes have been investigated over a temperature range of 20-77 K, in magnetic fields up to 9 T and over a wide angular range of magnetic field orientations. The peak in critical current that is commonly observed in the field orientation perpendicular to the tape in BaZrO3 (BZO) containing superconducting tapes is found to vanish at 30 K in magnetic fields at 1-9 T. While the critical current of 15% Zr-added tapes was about 40% lower than that of 7.5% Zr-added tapes at 77 K, the pinning force values of the former were found to be 18-23% higher than those of the latter in the temperature range of 20-40 K and in magnetic fields of 3-5 T. The results from this study emphasize the importance of optimization of coated conductor fabrication processes for optimum performance not just in low magnetic fields at 77 K but also at the operating conditions of low temperatures and high magnetic fields that are of interest, especially for rotating superconducting machinery applications.

  5. The low-temperature, high-magnetic-field critical current characteristics of Zr-added (Gd,Y)Ba2Cu3Ox superconducting tapes

    International Nuclear Information System (INIS)

    Selvamanickam, V; Yao, Y; Shi, T; Liu, Y; Khatri, N D; Liu, J; Galstyan, E; Majkic, G; Chen, Y; Lei, C

    2012-01-01

    Critical current performances of state-of-the-art Zr-added (Gd, Y)BaCuO tapes have been investigated over a temperature range of 20–77 K, in magnetic fields up to 9 T and over a wide angular range of magnetic field orientations. The peak in critical current that is commonly observed in the field orientation perpendicular to the tape in BaZrO 3 (BZO) containing superconducting tapes is found to vanish at 30 K in magnetic fields at 1–9 T. While the critical current of 15% Zr-added tapes was about 40% lower than that of 7.5% Zr-added tapes at 77 K, the pinning force values of the former were found to be 18–23% higher than those of the latter in the temperature range of 20–40 K and in magnetic fields of 3–5 T. The results from this study emphasize the importance of optimization of coated conductor fabrication processes for optimum performance not just in low magnetic fields at 77 K but also at the operating conditions of low temperatures and high magnetic fields that are of interest, especially for rotating superconducting machinery applications. (paper)

  6. Neutron diffraction and low temperature magnetization study of Tb0.8Y0.2MnO3

    International Nuclear Information System (INIS)

    Chakraborty, Keka R.; Mukadam, M.; Yusuf, S.M.; Shukla, R.; Tyagi, A.K.; Kaushik, S.D.; Siruguri, V.

    2012-01-01

    Multiferroic materials possess mutually correlated magnetic and electric order parameters which are suitable for device applications but scarcity of such materials and the separation of magnetic and electric ordering temperatures are a major hindrance in technological applications. TbMnO 3 is one of the material which is reported to have higher magnetoelectric coupling. Structurally, TbMnO 3 crystallizes in orthorhombically distorted perovskite structure (space group Pbnm). For TbMnO 3 , several reports are available in the literature which further modify the magnetoelectric coupling by selective doping or reducing the particle size to nano dimensions, or preparing thin films. Here, we study the effect of Y doping at Tb site in nanoparticle form in terms of crystal structure and magnetic properties. Nanoparticles of Tb 0.8 Y 0.2 MnO 3 were synthesized using the gel combustion technique. Crystal structure of this sample is studied at 300 K using neutron diffraction

  7. Iron in the Fire: Searching for Fire's Magnetic Fingerprint using Controlled Heating Experiments, High-Resolution FORCs, IRM Coercivity Spectra, and Low-Temperature Remanence Experiments

    Science.gov (United States)

    Lippert, P. C.; Reiners, P. W.

    2014-12-01

    Evidence for recent climate-wildfire linkages underscores the need for better understanding of relationships between wildfire and major climate shifts in Earth history, which in turn offers the potential for prognoses for wildfire and human adaptations to it. In particular, what are the links between seasonality and wildfire frequency and severity, and what are the feedbacks between wildfire, landscape evolution, and biogeochemical cycles, particularly the carbon and iron cycles? A key first step in addressing these questions is recovering well-described wildfire records from a variety of paleolandscapes and paleoclimate regimes. Although charcoal and organic biomarkers are commonly used indicators of fire, taphonomic processes and time-consuming analytical preparations often preclude their routine use in some environments and in high-stratigraphic resolution paleowildfire surveying. The phenomenological relationship between fire and magnetic susceptibility can make it a useful surveying tool, but increased magnetic susceptibility in sediments is not unique to fire, and thus limits its diagnostic power. Here we utilize component-specific rock magnetic methods and analytical techniques to identify the rock magnetic fingerprint of wildfire. We use a custom-designed air furnace, a series of iron-free laboratory soils, natural saprolites and soils, and fuels from Arizona Ponderosa pine forests and grasslands to simulate wildfire in a controlled and monitored environment. Soil-ash residues and soil and fuel controls were then characterized using First Order Reversal Curve (FORC) patterns, DC backfield IRM coercivity spectra, low-temperature SIRM demagnetization behavior, and low-temperature cycling of room-temperature SIRM behavior. We will complement these magnetic analyses with high-resolution TEM of magnetic extracts. Here we summarize the systematic changes to sediment magnetism as pyrolitized organic matter is incorporated into artificial and natural soils. These

  8. Low Temperature Magnetic Transition in Meteoritic Troilites – Simple Mmarker for Highly Stoichiometric Iron(II) Sulphide Systems?

    Czech Academy of Sciences Publication Activity Database

    Kohout, Tomáš; Čuda, J.; Tuček, J.; Zbořil, R.; Haloda, J.; Filip, J.

    2010-01-01

    Roč. 91, Suppl. (2010), , GP42A-07-GP42A-07 ISSN 0096-3941. [American Geophysical Union Fall Meeting 2010. 13.12.2010-17.12.2010, San Francisco] Institutional research plan: CEZ:AV0Z30130516 Keywords : troilite * magnetism Subject RIV: BN - Astronomy, Celestial Mechanics, Astrophysics

  9. Spin valve-like magnetic tunnel diode exhibiting giant positive junction magnetoresistance at low temperature in Co2MnSi/SiO2/p-Si heterostructure

    Science.gov (United States)

    Maji, Nilay; Kar, Uddipta; Nath, T. K.

    2018-02-01

    The rectifying magnetic tunnel diode has been fabricated by growing Co2MnSi (CMS) Heusler alloy film carefully on a properly cleaned p-Si (100) substrate with the help of electron beam physical vapor deposition technique and its structural, electrical and magnetic properties have been experimentally investigated in details. The electronic- and magneto-transport properties at various isothermal conditions have been studied in the temperature regime of 78-300 K. The current-voltage ( I- V) characteristics of the junction show an excellent rectifying magnetic tunnel diode-like behavior throughout that temperature regime. The current ( I) across the junction has been found to decrease with the application of a magnetic field parallel to the plane of the CMS film clearly indicating positive junction magnetoresistance (JMR) of the heterostructure. When forward dc bias is applied to the heterostructure, the I- V characteristics are highly influenced on turning on the field B = 0.5 T at 78 K, and the forward current reduces abruptly (99.2% current reduction at 3 V) which is nearly equal to the order of the magnitude of the current observed in the reverse bias. Hence, our Co2MnSi/SiO2/p-Si heterostructure can perform in off ( I off)/on ( I on) states with the application of non-zero/zero magnetic field like a spin valve at low temperature (78 K).

  10. Experimental set-up for electrical resistivity measurements at low temperature in amorphous and crystalline metallic samples

    International Nuclear Information System (INIS)

    Rodriquez Fernandez, J.M.; Lopez Sanchez, R.J.; Gomez-Sal, J.C.

    1986-01-01

    The experimental set-up to measure the thermal variation of the electrical resistivity between 10.5 K and 300 K, has been developed. A four probe A.C. method with a synchronous-detection (lock'in) technique were the idoneous for our proposes. We have designed a new type of pressure sample-holder adopted to the CS-202 type cryostat. The measurements performed on samples already known have allowed us to determine the sensitivity of our experiments, which is Δ ρ/ρ=2x10 -4 . The measurements performed in the new Y 3 Rh 2 Si 2 compound which at 10 K has no magnetic ordering, are also presented. (author)

  11. Glass and crystallization like transitions at low temperature in Zr-Cu based glasses by internal friction measurements

    Directory of Open Access Journals (Sweden)

    Aboki A.T.

    2011-05-01

    Full Text Available Low temperature β internal friction peak evolution upon thermal cycles shows two peculiar peaks similar to high temperature internal friction peak. The modulus softening associated to these peaks suggest a phase transformation phenomenon and the relaxation time τo in order of 10-23–10-35s, close to that observed in grains boundary sliding are due to interface motions in the amorphous structure under combined thermal and mechanical energies.

  12. Low temperature measurement of thermal and mechanical properties of phenolic laminate, the pultruded polyester fiberglass and A and B epoxy putty

    International Nuclear Information System (INIS)

    Wang, S.T.; Kim, S.H.; Kim, N.S.; Cheng, R.S.; Hoffman, J.; Gonczy, J.

    1979-01-01

    Low temperature measurements were made and are reported of thermal and mechanical properties of phenolic laminate, pultruded polyester fiberglass, and A and B epoxy putty. To determine the modulus, compressive and tensile stress and strain, an Instron machine, a Tinus-Olsen testing machine, a Wheatstone bridge and strain gages were used

  13. {sup 1}H-NMR and charge transport in metallic polypyrrole at ultra-low temperatures and high magnetic fields

    Energy Technology Data Exchange (ETDEWEB)

    Jugeshwar Singh, K; Ramesh, K P; Menon, Reghu [Department of Physics, Indian Institute of Science, Bangalore 560012 (India); Clark, W G [Department of Physics and Astronomy, University of California at Los Angeles, 405 Hilgard Avenue, Los Angeles, CA 90095 (United States)], E-mail: jshwar@physics.iisc.ernet.in

    2008-11-19

    The temperature dependence of conductivity, proton spin relaxation time (T{sub 1}) and magnetoconductance (MC) in metallic polypyrrole (PPy) doped with PF{sub 6}{sup -} have been carried out at mK temperatures and high magnetic fields. At T<1 K both electron-electron interaction (EEI) and hopping contributes to conductivity. The temperature dependence of a proton T{sub 1} is classified in three regimes: (a) for T<6 K-relaxation mechanism follows a modified Korringa relation due to EEI and disorder, (b) for 6 K50 K-relaxation is due to the dipolar interaction modulated by the reorientation of the symmetric PF{sub 6} groups following the Bloembergen, Purcell and Pound (BPP) model. The data analysis shows that the Korringa ratio is enhanced by an order of magnitude. The positive and negative MC at T<250 mK is due to the contributions from weak localization and Coulomb-correlated hopping transport, respectively. The role of EEI is observed to be consistent in conductivity, T{sub 1} and MC data, especially at T<1 K.

  14. (Dy0.5Er0.5)Al2: A large magnetocaloric effect material for low-temperature magnetic refrigeration

    International Nuclear Information System (INIS)

    Gschneidner, K.A. Jr.; Takeya, H.; Moorman, J.O.; Pecharsky, V.K.

    1994-01-01

    The low-temprature heat capacity and ac and dc magnetic properties of (Dy 0.5 Er 0.5 )Al 2 have been studied as a function of magnetic fields up to ∼10 T. The magnetocaloric effect in (Dy 0.5 Er 0.5 )Al 2 is 30% larger than that of the prototype material, GdPd. Magnetic measurements show that there is no measurable magnetic hysteresis above ∼17 K. These results suggest that (Dy 0.5 Er 0.5 )Al 2 would be a significantly better magnetic refrigerant than GdPd

  15. Properties of recent IBAD-MOCVD coated conductors relevant to their high field, low temperature magnet use

    International Nuclear Information System (INIS)

    Braccini, V; Xu, A; Jaroszynski, J; Xin, Y; Larbalestier, D C; Chen, Y; Carota, G; Dackow, J; Kesgin, I; Yao, Y; Guevara, A; Shi, T; Selvamanickam, V

    2011-01-01

    BaZrO 3 (BZO) nanorods are now incorporated into production IBAD-MOCVD coated conductors. Here we compare several examples of both BZO-free and BZO-containing coated conductors using critical current (I c ) characterizations at 4.2 K over their full angular range up to fields of 31 T. We find that BZO nanorods do not produce any c-axis distortion of the critical current density J c (θ) curve at 4.2 K at any field, but also that pinning is nevertheless strongly enhanced compared to the non-BZO conductors. We also find that the tendency of the ab-plane J c (θ) peak to become cusp-like is moderated by BZO and we define a new figure of merit that may be helpful for magnet design-the OADI (off-axis double I c ), which clearly shows that BZO broadens the ab-plane peak and thus raises J c 5 0 -30 0 away from the tape plane, where the most critical approach to I c occurs in many coil designs. We describe some experimental procedures that may make critical current I c tests of these very high current tapes more tractable at 4.2 K, where I c exceeds 1000 A even for 4 mm wide tape with only 1 μm thickness of superconductor. A positive conclusion is that BZO is very beneficial for the J c characteristics at 4.2 K, just as it is at higher temperatures, where the correlated c-axis pinning effects of the nanorods are much more obvious.

  16. Properties of recent IBAD-MOCVD coated conductors relevant to their high field, low temperature magnet use

    Energy Technology Data Exchange (ETDEWEB)

    Braccini, V; Xu, A; Jaroszynski, J; Xin, Y; Larbalestier, D C [Applied Superconductivity Center, National High Magnetic Field Laboratory, 2031 E Paul Dirac Drive, Tallahassee, FL 32310 (United States); Chen, Y; Carota, G; Dackow, J [SuperPower Inc., 450 Duane Avenue, Schenectady, NY 12304 (United States); Kesgin, I; Yao, Y; Guevara, A; Shi, T; Selvamanickam, V, E-mail: braccini@asc.magnet.fsu.edu [Department of Mechanical Engineering and the Texas Center for Superconductivity at the University of Houston, 4800 Calhoun Road, Houston, TX 77204 (United States)

    2011-03-15

    BaZrO{sub 3} (BZO) nanorods are now incorporated into production IBAD-MOCVD coated conductors. Here we compare several examples of both BZO-free and BZO-containing coated conductors using critical current (I{sub c}) characterizations at 4.2 K over their full angular range up to fields of 31 T. We find that BZO nanorods do not produce any c-axis distortion of the critical current density J{sub c}({theta}) curve at 4.2 K at any field, but also that pinning is nevertheless strongly enhanced compared to the non-BZO conductors. We also find that the tendency of the ab-plane J{sub c}({theta}) peak to become cusp-like is moderated by BZO and we define a new figure of merit that may be helpful for magnet design-the OADI (off-axis double I{sub c}), which clearly shows that BZO broadens the ab-plane peak and thus raises J{sub c} 5{sup 0}-30{sup 0} away from the tape plane, where the most critical approach to I{sub c} occurs in many coil designs. We describe some experimental procedures that may make critical current I{sub c} tests of these very high current tapes more tractable at 4.2 K, where I{sub c} exceeds 1000 A even for 4 mm wide tape with only 1 {mu}m thickness of superconductor. A positive conclusion is that BZO is very beneficial for the J{sub c} characteristics at 4.2 K, just as it is at higher temperatures, where the correlated c-axis pinning effects of the nanorods are much more obvious.

  17. Spin-strain effects in the frustrated magnet Tb{sub 2}Ti{sub 2}O{sub 7} at low temperatures

    Energy Technology Data Exchange (ETDEWEB)

    Gritsenko, Y.; Wosnitza, J. [HZDR/HLD, Dresden (Germany); TUD/IFP, Dresden (Germany); Zherlitsyn, S. [HZDR/HLD, Dresden (Germany); Ruminy, M.; Fennell, T. [PSI/LNS, 5232 Villigen PSI (Switzerland); Kenzelmann, M. [PSI/LDM, 5232 Villigen PSI (Switzerland)

    2016-07-01

    Geometrically frustrated magnets have attracted much attention, due to their tendency to build unconventional ground states with exotic excitations. Tb{sub 2}Ti{sub 2}O{sub 7} possesses a pyrochlore lattice as building block of the crystallographic structure, providing a basis for geometric frustration. This cubic material features Curie-Weiss temperature of Θ{sub CW} = -19 K, but no long-range magnetic order has been detected down to 50 mK indicating a large frustration. The existence of a spin-liquid state has been suggested for Tb{sub 2}Ti{sub 2}O{sub 7}. Here, we present results of ultrasonic investigations of this material. The magnetic field was applied along the [110] direction at temperatures of 20, 150 and 300 mK. Clear anomalies were found for different acoustic modes. The temperature dependence of the sound velocity shows a softening at about 500 mK and step-like features at about 150 mK suggesting a low-temperature phase transformation. This investigation sheds new light on the role of lattice degrees of freedom and magneto-elastic interactions in this material.

  18. Influence of low-temperature nitriding on the strain-induced martensite and laser-quenched austenite in a magnetic encoder made from 304L stainless steel

    Science.gov (United States)

    Leskovšek, Vojteh; Godec, Matjaž; Kogej, Peter

    2016-01-01

    We have investigated the possibility of producing a magnetic encoder by an innovative process. Instead of turning grooves in the encoder bar for precise positioning, we incorporated the information in 304L stainless steel by transforming the austenite to martensite after bar extrusion in liquid nitrogen and marking it with a laser, which caused a local transformation of martensite back into austenite. 304L has an excellent corrosion resistance, but a low hardness and poor wear resistance, which limits its range of applications. However, nitriding is a very promising way to enhance the mechanical and magnetic properties. After low-temperature nitriding at 400 °C it is clear that both ε- and α′-martensite are present in the deformed microstructure, indicating the simultaneous stress-induced and strain-induced transformations of the austenite. The effects of a laser surface treatment and the consequent appearance of a non-magnetic phase due to the α′ → γ transformation were investigated. The EDS maps show a high concentration of nitrogen in the alternating hard surface layers of γN and α′N (expanded austenite and martensite), but no significantly higher concentration of chromium or iron was detected. The high surface hardness of this nitride layer will lead to steels and encoders with better wear and corrosion resistance. PMID:27492862

  19. Magnetic field induced low temperature upturn of magnetization in highly Ca-doped La{sub 0.1875}Ca{sub 0.8125}MnO{sub 3} polycrystalline compound

    Energy Technology Data Exchange (ETDEWEB)

    Das, Kalipada, E-mail: kalipadadasphysics@gmail.com [Indian Association for the Cultivation of Science, 2A and 2B Raja S. C. Mullick Road, Jadavpur, Kolkata 700032 (India); Dasgupta, P.; Poddar, A. [CMP Division, Saha Institute of Nuclear Physics, 1/AF, Bidhannagar, Kolkata 700 064 (India)

    2017-06-15

    Highlights: • Magnetic field induced super paramagnetic nanoclusters formation. • Magnetic field dependent change of the curvature of the magnetization. • We report the training effect in polycrystalline La{sub 0.1875}Ca{sub 0.8125}MnO{sub 3} compound. - Abstract: In our present study we have reported the magnetic properties of highly Ca-doped polycrystalline compound La{sub 0.1875}Ca{sub 0.8125}MnO{sub 3}. Along with the conventional charge ordered antiferromagnetic ground state, a small ferromagnetic phase fraction is present at the low temperature. The effect of the external magnetic field markedly modifies the ground state of the compound. Our experimental results indicate that in addition to the ferromagnetic phase fraction, another field induced super paramagnetic phase grow at low temperature (T < 50 K) above H = 10 kOe magnetic field within the charge ordered antiferromagnetic matrix. The nature of the temperature dependent magnetization curves influenced by the external applied magnetic field was observed and analyzed using Langevin theory of super paramagnetism.

  20. Local moment formation and magnetic coupling of Mn dopants in Bi2Se3: A low-temperature ferromagnetic resonance study

    Science.gov (United States)

    Savchenko, D.; Tarasenko, R.; Vališka, M.; Kopeček, J.; Fekete, L.; Carva, K.; Holý, V.; Springholz, G.; Sechovský, V.; Honolka, J.

    2018-05-01

    We compare the magnetic and electronic configuration of single Mn atoms in molecular beam epitaxy (MBE) grown Bi2Se3 thin films, focusing on electron paramagnetic (ferromagnetic) resonance (EPR and FMR, respectively) and superconducting quantum interference device (SQUID) techniques. X-ray diffraction (XRD) and electron backscatter diffraction (EBSD) reveal the expected increase of disorder with increasing concentration of magnetic guest atoms, however, Kikuchi patterns show that disorder consists majorly of μm-scale 60° twin domains in the hexagonal Bi2Se3 structure, which are promoted by the presence of single unclustered Mn impurities. Ferromagnetism below TC (5.4±0.3) K can be well described by critical scaling laws M (T) (1 - T /TC) β with a critical exponent β = (0.34 ± 0.2) , suggesting 3D Heisenberg class magnetism instead of e.g. 2D-type coupling between Mn-spins in van der Waals gap sites. From EPR hyperfine structure data we determine a Mn2+ (d5, S = 5/2) electronic configuration with a g-factor of 2.002 for -1/2 → +1/2 transitions. In addition, from the strong dependence of the low temperature FMR fields and linewidth on the field strength and orientation with respect to the Bi2Se3 (0001) plane, we derive magnetic anisotropy energies of up to K1 = -3720 erg/cm3 in MBE-grown Mn-doped Bi2Se3, reflecting the first order magneto-crystalline anisotropy of an in-plane magnetic easy plane in a hexagonal (0001) crystal symmetry. We observe an increase of K1 with increasing Mn concentration, which we interpret to be correlated to a Mn-induced in-plane lattice contraction. Across the ferromagnetic-paramagnetic transition the FMR intensity is suppressed and resonance fields converge the paramagnetic limit of Mn2+ (d5, S = 5/2).

  1. Angular dependence of J{sub c} for YBCO coated conductors at low temperature and very high magnetic fields

    Energy Technology Data Exchange (ETDEWEB)

    Xu, A; Jaroszynski, J J; Kametani, F; Chen, Z; Larbalestier, D C [Applied Superconductivity Center, National High Magnetic Field Laboratory, Florida State University, Tallahassee, FL 32310 (United States); Viouchkov, Y L [National High Magnetic Field Laboratory, Florida State University, Tallahassee, FL 32310 (United States); Chen, Y; Xie, Y; Selvamanickam, V, E-mail: aixiaxu@asc.magnet.fsu.ed [SuperPower Incorporated, 450 Duane Avenue, Schenectady, NY 12304 (United States)

    2010-01-15

    We present very high field angle dependent critical current density (J{sub c}) data for three recently obtained YBa{sub 2}Cu{sub 3}O{sub 7-x} (YBCO) coated conductors used in the construction of high field solenoids. We find that strongly correlated pins, such as BaZrO{sub 3} (BZO) nanorods, while yielding strong c-axis peaks at 77 K, produce almost no measurable contribution at 4 K. Raising the field from <5 to 30 T at 4 K causes a marked transition from a Ginzburg-Landau-like J{sub c}({theta}) at low fields to a marked cusp-like behavior at high fields. Transmission electron micrographs show that all samples contain a high density of stacking faults which strengthen the plane correlated pinning parallel to the ab planes produced by the intrinsic ab-plane pinning of the Cu-O charge reservoir layers.

  2. Low-temperature nuclear orientation

    International Nuclear Information System (INIS)

    Stone, N.J.; Postma, H.

    1986-01-01

    This book comprehensively surveys the many aspects of the low temperature nuclear orientation method. The angular distribution of radioactive emissions from nuclei oriented by hyperfine interactions in solids, is treated experimentally and theoretically. A general introductory chapter is followed by formal development of the theory of the orientation process and the anisotropic emission of decay products from oriented nuclei, applied to radioactive decay and to reactions. Five chapters on applications to nuclear physics cover experimental studies of alpha, beta and gamma emission, nuclear moment measurement and level structure information. Nuclear orientation studies of parity non-conservation and time reversal asymmetry are fully described. Seven chapters cover aspects of hyperfine interactions, magnetic and electric, in metals, alloys and insulating crystals, including ordered systems. Relaxation phenomena and the combined technique of NMR detection using oriented nuclei are treated at length. Chapters on the major recent development of on-line facilities, giving access to short lived nuclei far from stability, on the use of nuclear orientation for thermometry below 1 Kelvin and on technical aspects of the method complete the main text. Extensive appendices, table of relevant parameters and over 1000 references are included to assist the design of future experiments. (Auth.)

  3. Influence of low-temperature annealing on magnetic properties of (Nd0.625Ni0.375)85Al15 metallic glass

    International Nuclear Information System (INIS)

    Xu Feng; Wang Zhiming; Chen Guang; Jiang Jianzhong; Du Youwei

    2008-01-01

    After a review of the selection process of (Nd 0.625 Ni 0.375 ) 85 Al 15 as a metallic glass with a relatively high glass-forming ability, we investigate the influences of its phase transitions by duplicating the heating process of the isochronal thermal analysis with low-temperature annealings. The structure, thermal stability and magnetic properties are characterized. And the influences on magnetic properties are particularly discussed with emphasis. Both the annealing processes, to the glass-transition temperature and to the onset temperature of crystallization, bring about a higher coercivity of the sample and a higher freezing temperature of the spin-glass-state. For the sample annealed to the onset temperature of crystallization, the influence is quite obvious and is ascribed to the formation of ferrimagnetic Nd 7 Ni 3 phase, as detected by XRD. For the sample annealed to the glass-transition temperature, the indistinct influence is further identified with the analysis of the frequency dependence of the spin-glass-state, and it is mainly attributed to the change of the short-range order in the amorphous matrix

  4. WORKSHOP: Low temperature devices

    International Nuclear Information System (INIS)

    Anon.

    1987-01-01

    With extraterrestrial neutrinos (whether from the sun or further afield) continuing to make science news, and with the search for the so far invisible 'dark matter' of the universe a continual preoccupation, physicists from different walks of life (solid state, low temperature, particles, astrophysics) gathered at a workshop on low temperature devices for the detection of neutrinos and dark matter, held from 12-13 March at Ringberg Castle on Lake Tegernsee in the Bavarian Alps, and organized by the Max Planck Institute for Physics and Astrophysics in Munich

  5. WORKSHOP: Low temperature devices

    Energy Technology Data Exchange (ETDEWEB)

    Anon.

    1987-06-15

    With extraterrestrial neutrinos (whether from the sun or further afield) continuing to make science news, and with the search for the so far invisible 'dark matter' of the universe a continual preoccupation, physicists from different walks of life (solid state, low temperature, particles, astrophysics) gathered at a workshop on low temperature devices for the detection of neutrinos and dark matter, held from 12-13 March at Ringberg Castle on Lake Tegernsee in the Bavarian Alps, and organized by the Max Planck Institute for Physics and Astrophysics in Munich.

  6. Measurements of magnetic anisotropy in sickle cells

    International Nuclear Information System (INIS)

    Salvo Souza, L.H. de.

    1982-03-01

    Room temperature magnetic measurements in deoxigenated sickle cells showed the existence of magnetic anisotropy, Δchi=1,29 x 10 -3 . This effect was supposed paramagnetic and considered to be due to the iron atoms of the hemoglobin molecules which are one over the other, forming ordered chains inside the erythrocytes. Low temperature (liquid He - 4,2K) measurements of the magnetic anisotropy of sickle cells and normal red blood cells diluted in a cryoprotector was made to confirm the paramagnetic origin of the fenomena. For that purpose it was used a superconductor magnetometer coupled to a SQUID, developed in the 'Laboratorio do Estado Solido do Departamento de Fisica da PUC-RJ'. The results obtained seem to confirm the expected paramagnetic anisotropy and, furthermore, suggest the presence of magnetic interactions among the iron atoms in the sickle cells samples. (Author) [pt

  7. Magnetic Measurement and Magnet Tutorial, Part 3

    Energy Technology Data Exchange (ETDEWEB)

    Tanabe, Jack

    2003-07-15

    Magnetic measurements, like magnet design, is a broad subject. It is the intention of this lecture to cover only a small part of the field, regarding the characterization of the line integral field quality of multipole magnets (dipoles, quadrupoles and sextupoles) using compensated rotating coils. Other areas which are not covered are magnet mapping, AC measurements and sweeping wire measurements.

  8. Low temperature carbonization

    Energy Technology Data Exchange (ETDEWEB)

    Abbott, A A

    1934-01-10

    A process is described in which coal is passed through a distillation chamber in one retort at a comparatively low temperature, then passing the coal through a distillation chamber of a second retort subjected to a higher temperature, thence passing the coal through the distillation chamber of a third retort at a still higher temperature and separately collecting the liquid and vapors produced from each retort.

  9. Sweating at low temperature

    International Nuclear Information System (INIS)

    Chalaye, H.; Launay, J.P.

    1980-11-01

    Tests of penetration liquids normally used between 10 and 40 0 C have shown that the arrangement of operationaal conditions (penetration and revealing times) was not sufficient to maintain their sensitivity below 10 0 C, thereby confirming that this temperature is a limit below which such products cannot be employed. The results achieved with a penetrant and a tracer specially devised for low temperatures (SHERWIN B 305 + D100) are satisfactory between 0 0 C and 15 0 C [fr

  10. Thermal conductivity at very low temperature

    Energy Technology Data Exchange (ETDEWEB)

    Locatelli, M [CEA Centre d' Etudes Nucleaires de Grenoble, 38 (France). Service des Basses Temperatures

    1976-06-01

    The interest of low and very low temperatures in solid physics and especially that of thermal measurements is briefly mentioned. Some notes on the thermal conductivity of dielectrics, the method and apparatus used to measure this property at very low temperatures (T<1.5K) and some recent results of fundamental and applied research are then presented.

  11. Effects of La{sup 3+}-Zn{sup 2+} doping on the structure, magnetic, electrical, and dielectric properties of low temperature sintered Sr-hexaferrites

    Energy Technology Data Exchange (ETDEWEB)

    Peng, Long, E-mail: penglong@cuit.edu.cn [Sichuan Province Key Laboratory of Information Materials and Devices Application, College of Optoelectronic Technology, Chengdu University of Information Technology, Chengdu 610225 (China); Li, Lezhong; Zhong, Xiaoxi [Sichuan Province Key Laboratory of Information Materials and Devices Application, College of Optoelectronic Technology, Chengdu University of Information Technology, Chengdu 610225 (China); Hu, Yuebin [Chengdu Industrial Vocational and Technical College, Chengdu 610213 (China); Chen, Sanming [Sichuan Province Key Laboratory of Information Materials and Devices Application, College of Optoelectronic Technology, Chengdu University of Information Technology, Chengdu 610225 (China)

    2017-04-15

    The Sr{sub 1-x}La{sub x}Fe{sub 12-x}Zn{sub x}O{sub 19} (x=0–0.3) hexaferrites with Bi{sub 2}O{sub 3} additive were prepared by microwave sintering method at low sintering temperatures, and their crystal structure, microstructure, magnetic, electrical, and dielectric properties were studied. The results show that the pure M-type phase is obtained for the ferrites with x≤0.2. With x further increasing to 0.3, the multiphase structure is inevitably formed, where the LaFeO{sub 3} phase coexists with the M-type phase. In the single phase region, the varied magnetic, electrical, and dielectric properties with La{sup 3+}-Zn{sup 2+} doping amount are well explained by the occupancy effects of La{sup 3+} and Zn{sup 2+} in magnetoplumbite structure. It is suggested that the Zn{sup 2+} ions replace the Fe{sup 3+} ions at 4f{sub 1} site with x≤0.15, but the substitution of Zn{sup 2+} for Fe{sup 3+} occurs at 2b site preferentially when the La{sup 3+}-Zn{sup 2+} doping amount exceeds 0.15. - Highlights: • The low temperature sintered Sr{sub 1-x}La{sub x}Fe{sub 12-x}Zn{sub x}O{sub 19} (x=0–0.3) hexaferrites are successfully prepared. • The La{sup 3+}-Zn{sup 2+} ions partially substitute the Sr{sup 2+}-Fe{sup 3+} ions in a doping region of x≤0.2. • Effects of La{sup 3+}-Zn{sup 2+} doping on the magnetic, electrical and polarization properties are revealed. • The substitution of Zn{sup 2+} for Fe{sup 3+} occurs at 4f{sub 1} site and 2b site before and after x=0.15, respectively.

  12. Extremely low temperature properties of epoxy GFRP

    International Nuclear Information System (INIS)

    Kadotani, Kenzo; Nagai, Matao; Aki, Fumitake.

    1983-01-01

    The examination of fiber-reinforced plastics, that is, plastics such as epoxy, polyester and polyimide reinforced with high strength fibers such as glass, carbon, boron and steel, for extremely low temperature use began from the fuel tanks of rockets. Therafter, the trial manufacture of superconducting generators and extremely low temperature transformers and the manufacture of superconducting magnets for nuclear fusion experimental setups became active, and high performance FRPs have been adopted, of which the extremely low temperature properties have been sufficiently grasped. Recently, the cryostats made of FRPs have been developed, fully utilizing such features of FRPs as high strength, high rigidity, non-magnetic material, insulation, low heat conductivity, light weight and the freedom of molding. In this paper, the mechanical properties at extremely low temperature of the plastic composite materials used as insulators and structural materials for extremely low temperature superconducting equipment is outlined, and in particular, glass fiber-reinforced epoxy laminates are described somewhat in detail. The fracture strain of GFRP at extremely low temperature is about 1.3 times as large as that at room temperature, but at extremely low temperature, clear cracking occurred at 40% of the fracture strain. The linear thermal contraction of GFRP showed remarkable anisotropy. (Kako, I.)

  13. Elaboration and evolution in temperature of the amorphous alloy Tb65Cu35, study of short and medium range atomic order and low temperature magnetic order related to the elaboration process

    International Nuclear Information System (INIS)

    El Gadi, M.

    1986-12-01

    The thesis presents the study of the amorphous metallic alloy Tb 65 Cu 35 prepared by rapid quenching and sputtering. Differential scanning calorimetry (DSC) measurements establish the annealing procedure needed to obtain a stable amorphous state through structural relaxation. Nearest neighbour distances as determined by neutron diffraction measurements shows a high coordination for Tb atom and a relatively low one for Cu atom. In addition, small-angle neutron scattering (SANS) experiments carried out as a function of temperature show the existence of Tb bubbles with very high magnetization at low-temperature. The region between the bubbles shows composition fluctuations. The SANS measurements also indicate the coexistence of phases with compositions bordering the eutectic value and in the form of domains having sizes of a few thousand Angstroms. An unexpected result in the observation of an hundred fold increase in the intensity of low-angle magnetic scattering when the samples are hand-polished with simple sand paper. This clearly indicates the importance of sample surface state. Finally, this work establishes that samples prepared by two different techniques show identical properties [fr

  14. Low temperature destructive distillation

    Energy Technology Data Exchange (ETDEWEB)

    1938-07-05

    A process is given and apparatus is described for the destructive distillation at low temperature of coal, oil shale, and the like by subjection to the action of a stream of hot gases or superhearted steam, flowing in a closed circuit. Subsequent treatment of the distillation residues with a gas stream containing oxygen results in combustion of the carbon-containing material therein brings to a high temperature the solid residue, in which the process comprises subsequently contacting the hot solid residue with the fluid stream effecting the distillation.

  15. Automatic low-temperature calorimeter

    International Nuclear Information System (INIS)

    Malyshev, V.M.; Mil'ner, G.A.; Shibakin, V.F.; Sorkin, E.L.

    1986-01-01

    This paper describes a low-temperature adiabatic calorimeter with a range of 1.5-500K. The system for maintaining adiabatic conditions is implemented by two resitance thermometers, whose sensitivity at low temperatures is several orders higher than that of thermocouples. The calorimeter cryostat is installed in an STG-40 portable Dewar flask. The calorimeter is controlled by an Elektronika-60 microcomputer. Standard platinum and germanium thermometers were placed inside of the calorimeter to calibrate the thermometers of the calorimeter and the shield, and the specific heats of specimens of OSCh 11-4 copper and KTP-8 paste were measured to demonstrate the possibilities of the described calorimeter. Experience with the calorimeter has shown that a thorough study of the dependence of heat capacity on temperature (over 100 points for one specimen) can be performed in one or two dats

  16. Development of an optical time-resolved measurement system under high-pressure and low-temperature with a piston-cylinder pressure cell

    Science.gov (United States)

    Tsuchiya, Satoshi; Kino, Yohei; Nakagawa, Koichi; Nakagawa, Daisuke; Yamada, Jun-ichi; Toda, Yasunori

    2016-04-01

    To perform the femtosecond pump-probe spectroscopy under high pressure and low temperature, we constructed a measurement system with a piston cylinder type pressure cell installing an optical fiber bundle. The applied pressure was achieved to 6 kbar and the cell was cooled down to 15 K. Several demonstrations revealed that broadening and change of polarization of pulse (duration of ˜120 fs) owing to the dispersions in the fiber bundle are much small indicating that those have little influence on the measurement of carrier relaxation dynamics. In the measurements of κ-(BEDT-TTF)2Cu(NCS)2 under 1.3 kbar at 43 K, we have successfully detected the polarization anisotropy of the carrier relaxation dynamics and estimated the decay time in the same way as the normal measurement.

  17. Low temperature distillation

    Energy Technology Data Exchange (ETDEWEB)

    Vandegrift, J N; Postel, C

    1929-04-09

    To recover gas, oil tars, and coked residues by low temperature distillation from bituminous coals, lignites, oil shales, and the like, the raw material is fed from a hopper into a rotary retort which is zonally heated, the temperature being greatest at the discharge end. The material is heated first to a relatively low temperature, thereby removing the moisture and lighter volatiles which are withdrawn through a pipe by the suction of a pump, while the higher boiling point volatiles and fixed gases are withdrawn by suction through an outlet from the higher temperature zone. The vapors withdrawn from the opposite ends of the retort pass through separate vapor lines and condensers, and the suction in each end of the retort, caused by the pumps, is controlled by valves, which also control the location of the neutral point in the retort formed by said suction. Air and inert gas may be introduced into the retort from pipe and stack respectively through a pipe, and steam may be admitted into the high temperature zone through a pipe.

  18. Low-temperature carbonization

    Energy Technology Data Exchange (ETDEWEB)

    Strankmuller, J

    1954-01-01

    The low-temperature carbonization plant at Boehlen in Eastern Germany (the first in which Lurgi type ovens were installed) worked with a throughput of 300 tons of brown-coal briquets per day per oven since 1936, later increased to 365 tons per day. The rising demand for low-temperature tar for hydrogenation purposes led to development of a modified oven of 450 tons throughput. This was achieved by stepping up the flow of the circulating gas and air mixture from 420,000 to 560,000 cubic feet per hour and by additional rows of V-shaped deflectors across the width of the oven chamber, which break up and loosen the charge, thus reducing cooling-gas pressure and allowing a greater flow of scavenging gas. The distance traversed by each briquet is nearly doubled, and the temperature gradient is less. It is claimed that the tar and the coke from modified ovens are of comparable quality. The compressive strength of the briquets was found to have an appreciable effect on the output. Better qts the chemistry, mechanism and thermodynamics of the Fischer-Tropsch reaction and aectromagnetic radiation.

  19. Surface magnetic field measurement with magnetic shielding

    Czech Academy of Sciences Publication Activity Database

    Perevertov, Oleksiy

    2010-01-01

    Roč. 61, č. 7 (2010), 66-68 ISSN 1335-3632 Grant - others:AVČR(CZ) M100100906 Institutional research plan: CEZ:AV0Z10100520 Keywords : magnetic hysteresis * magnetic field measurement * magnetic shielding * extrapolation Subject RIV: BM - Solid Matter Physics ; Magnetism Impact factor: 0.270, year: 2010

  20. A Simple Experiment to Determine the Characteristics of an NTC Thermistor for Low-Temperature Measurement Applications

    Science.gov (United States)

    Mawire, A.

    2012-01-01

    A simple low-cost experiment for undergraduate students to determine the characteristics of a negative temperature coefficient of resistance thermistor is presented. The experiment measures the resistance-temperature and voltage-temperature characteristics of the thermistor. Results of the resistance-temperature experiment are used to determine…

  1. Current-Induced Joule Heating and Electrical Field Effects in Low Temperature Measurements on TIPS Pentacene Thin Film Transistors

    NARCIS (Netherlands)

    Nikiforov, G.O.; Venkateshvaran, D.; Mooser, S.; Meneau, A.; Strobel, T.; Kronemeijer, A.; Jiang, L.; Lee, M.J.; Sirringhaus, H.

    2016-01-01

    The channel temperature (Tch) of solution-processed 6,13-bis(triisopropylsilylethynyl)-pentacene (TIPS pentacene) thin film transistors (TFTs) is closely monitored in real time during current–voltage (I–V) measurements carried out in a He exchange gas cryostat at various base temperatures (Tb)

  2. Low-temperature positron lifetime and Doppler-broadening measurements for single-crystal nickel oxide containing cation vacancies

    International Nuclear Information System (INIS)

    Waber, J.T.; Snead, C.L. Jr.; Lynn, K.G.

    1985-01-01

    Lifetime and Doppler-broadening measurements for positron annihilation in substoichiometric nickelous oxide have been made concomitantly from liquid-helium to room temperature. The concentration of cation vacancies is readily controlled by altering the ambient oxygen pressure while annealing the crystals at 1673 0 K. It was found that neither of the three lifetimes observed or their relative intensities varied significantly with the oxygen pressure, and the bulk rate only increased slightly when the specimen was cooled from room to liquid-helium temperatures. These results are interpreted as indicating that some of the positrons are trapped by the existing cation vacancies and a smaller fraction by vacancy clusters

  3. Low-temperature thermal reduction of graphene oxide: In situ correlative structural, thermal desorption, and electrical transport measurements

    Science.gov (United States)

    Lipatov, Alexey; Guinel, Maxime J.-F.; Muratov, Dmitry S.; Vanyushin, Vladislav O.; Wilson, Peter M.; Kolmakov, Andrei; Sinitskii, Alexander

    2018-01-01

    Elucidation of the structural transformations in graphene oxide (GO) upon reduction remains an active and important area of research. We report the results of in situ heating experiments, during which electrical, mass spectrometry, X-ray photoelectron spectroscopy (XPS), Raman spectroscopy, and transmission electron microscopy (TEM) measurements were carried out correlatively. The simultaneous electrical and temperature programmed desorption measurements allowed us to correlate the onset of the increase in the electrical conductivity of GO by five orders of magnitude at about 150 °C with the maxima of the rates of desorption of H2O, CO, and CO2. Interestingly, this large conductivity change happens at an intermediate level of the reduction of GO, which likely corresponds to the point when the graphitic domains become large enough to enable percolative electronic transport. We demonstrate that the gas desorption is intimately related to (i) the changes in the chemical structure of GO detected by XPS and Raman spectroscopy and (ii) the formation of nanoscopic holes in GO sheets revealed by TEM. These in situ observations provide a better understanding of the mechanism of the GO thermal reduction.

  4. Investigation of optimal manufacturing process for freeze-dried formulations: Observation of frozen solutions by low temperature X-ray diffraction measurements

    International Nuclear Information System (INIS)

    Egawa, Hiroaki; Yonemochi, Etsuo; Terada, Katsuhide

    2005-01-01

    Freeze-drying is used for the production of sterile injections in the pharmaceutical industry. However, most pharmaceutical compounds are obtained as less stable amorphous form. Freeze crystallization by annealing is an effective method for pharmaceutical compounds that fail to crystallize in the freeze-drying process. Crystallization occurs in the frozen solution during the thermal treatment. In order to establish suitable annealing conditions efficiently, it is important to observe the crystallization process directly in the frozen solution. Recently, low temperature X-ray diffraction has been used to observe frozen solutions. In order to investigate the crystallization process kinetically, the temperature of the low temperature X-ray diffraction instrument must be accurately controlled. We calibrated the temperature of X-ray diffraction instrument by measuring eutectic temperatures of solutions for a series of compounds. Each eutectic crystal was observed in frozen solution with ice crystal below the eutectic temperature. Eutectic temperatures were detected by the decrease in diffraction intensity associated with heating from below the eutectic temperature. Good correlation was obtained between values in the literature and experimental values

  5. Hydroperoxide Measurements During Low-Temperature Gas-Phase Oxidation of n-Heptane and n-Decane

    KAUST Repository

    Rodriguez, Anne

    2017-02-13

    A wide range of hydroperoxides (C-C alkyl hydroperoxides, C-C alkenyl hydroperoxides, C ketohydroperoxides, and hydrogen peroxide (HO)), as well as ketene and diones, have been quantified during the gas-phase oxidation of n-heptane. Some of these species, as well as C alkenyl hydroperoxides and ketohydroperoxides, were also measured during the oxidation of n-decane. These experiments were performed using an atmospheric-pressure jet-stirred reactor at temperatures from 500 to 1100 K and one of three analytical methods, time-of-flight mass spectrometry combined with tunable synchrotron photoionization with a molecular beam sampling: time-of-flight mass spectrometry combined with laser photoionization with a capillary tube sampling, continuous wave cavity ring-down spectroscopy with sonic probe sampling. The experimental temperature at which the maximum mole fraction is observed increases significantly for alkyl hydroperoxides, alkenyl hydroperoxides, and then more so again for hydrogen peroxide, compared to ketohydroperoxides. The influence of the equivalence ratio from 0.25 to 4 on the formation of these peroxides has been studied during n-heptane oxidation. The up-to-date detailed kinetic oxidation models for n-heptane and for n-decane found in the literature have been used to discuss the possible pathways by which these peroxides, ketene, and diones are formed. In general, the model predicts well the reactivity of the two fuels, as well as the formation of major intermediates. (Figure Presented).

  6. Hydroperoxide Measurements During Low-Temperature Gas-Phase Oxidation of n-Heptane and n-Decane

    KAUST Repository

    Rodriguez, Anne; Herbinet, Olivier; Meng, Xiangzan; Fittschen, Christa; Wang, Zhandong; Xing, Lili; Zhang, Lidong; Battin-Leclerc, Fré dé rique

    2017-01-01

    A wide range of hydroperoxides (C-C alkyl hydroperoxides, C-C alkenyl hydroperoxides, C ketohydroperoxides, and hydrogen peroxide (HO)), as well as ketene and diones, have been quantified during the gas-phase oxidation of n-heptane. Some of these species, as well as C alkenyl hydroperoxides and ketohydroperoxides, were also measured during the oxidation of n-decane. These experiments were performed using an atmospheric-pressure jet-stirred reactor at temperatures from 500 to 1100 K and one of three analytical methods, time-of-flight mass spectrometry combined with tunable synchrotron photoionization with a molecular beam sampling: time-of-flight mass spectrometry combined with laser photoionization with a capillary tube sampling, continuous wave cavity ring-down spectroscopy with sonic probe sampling. The experimental temperature at which the maximum mole fraction is observed increases significantly for alkyl hydroperoxides, alkenyl hydroperoxides, and then more so again for hydrogen peroxide, compared to ketohydroperoxides. The influence of the equivalence ratio from 0.25 to 4 on the formation of these peroxides has been studied during n-heptane oxidation. The up-to-date detailed kinetic oxidation models for n-heptane and for n-decane found in the literature have been used to discuss the possible pathways by which these peroxides, ketene, and diones are formed. In general, the model predicts well the reactivity of the two fuels, as well as the formation of major intermediates. (Figure Presented).

  7. Operation related on-line measurements of low temperature fire side corrosion during co-combustion of biomass and oil; Driftrelaterad direktmaetning av laagtemperaturkorrosion i en braensleeldad kraftvaermeanlaeggning

    Energy Technology Data Exchange (ETDEWEB)

    Eriksson, Thomas [Studsvik Nuclear AB, Nykoeping (Sweden)

    2000-05-01

    A number of combustion plants have experienced corrosion attack on air preheaters and economisers when fired with biomass fuels. In certain plants the problems are great and reconstruction has been performed so that exposed components can be exchanged during operation. The electrochemical techniques offer on-line measurements of the changes in corrosion rate in the low temperature region in a waste incinerator. The purpose with this study was to evaluate the technique in a biomass fired boiler where the corrosion rate is considerable lower compared to a waste incinerator. Experiments were performed at the Haesselby plant, boiler 3, which was fired with pure biomass as well as a mixture of biomass and oil during the test period. It was found that the electrochemical technique is a useful tool for on-line measurements of the changes in corrosion rate in biomass fired utilities. Since the corrosion rate in the low temperature region is dependent on the boiler construction, electrochemical measurements give valuable information on the corrosion rate during optimisation of the fuel mixture, SNCR and temperature or the low temperature components. This is of special importance when introducing new fuels or fuel mixtures. Soot blowing is of prime importance for the total corrosion. During a few minutes an individual soot blower can initiate such a high corrosion rate that it represents the total corrosion. The material temperature is another important parameter. Above a certain temperature the corrosion rate is negligible. During co-combustion this temperature was found to be in the region 65-85 deg C. The influence of the SNCR with ammonia, with respect to corrosion, is dependent on the fuel mixture used. In utilities where acidic combustion products are formed, ammonia has a neutralising effect e.g. in Hoegdalen. At the Haesselby plant this neutralising effect was not found. During cocombustion with oil the ammonia forms ammoniahydrosulphate which increases the corrosion

  8. Thermoluminescent system for low temperatures

    International Nuclear Information System (INIS)

    Rosa, L.A.R. da; Caldas, L.V.E.; Leite, N.G.

    1988-09-01

    A system for measurements of the thermoluminescent glow curve, the thermoluminescent emission spectrum and the optical absorption spectrum of solid samples, from liquid nitrogen temperature up to 473 K, is reported. A specially designed temperature programmer provides a linear heating of the sample at a wide range of selectable heating rates, as also long term steady-state temperatures for annealing and isothermal decay studies. The system operates at a pressure of 1.33 x 10 -3 Pa. Presently it is being used for lithium fluoride low temperature thermoluminescent studies. (author) [pt

  9. Measurements of quadrupole magnets

    International Nuclear Information System (INIS)

    Conradie, J.L.; Fourie, D.T.; Cornell, J.C.; Lloyd, G.C.W.

    1987-01-01

    Measurements carried out on quadrupole magnets using a long asymmetric rotating coil are described. Although the method itself is fairly well-known, the introduction of microprocessors has made this once-tedious technique into a useful and simple method of evaluating quadrupole magnets. The rotating-coil device and a variety of coil sizes are now commercially available. The coil contains a large number of extremely fine wires, embedded in a carefully balanced fibre-glass rotor, resulting in a reasonable induced voltage when the coil is rotated. A digital harmonic analyser is then used to obtain the integrated multipole content of the waveform, while the coil is rotating. By integrating over time, one can average out random noise and increase the reliability and repeatability of the measurements. Because the harmonic analysis is done in real time, the method is quick, easy and accurate, and has been extended to locate the precise magnetic centre of the quadrupole magnet by adjusting its position relative to the coil axis so as to minimize the dipole content of the output waveform. Results of these measurements are compared with those obtained with an optical method using a suspension of magnetite. The observed light pattern is explained analytically. (author)

  10. Low-temperature kinetic measurements of microsecond freeze-hyperquench (MHQ) cytochrome oxidase monitored by UV-visible spectroscopy with a newly designed cuvette.

    Science.gov (United States)

    Wiertz, F G M; de Vries, S

    2006-02-01

    A special cuvette was designed to measure optical changes of MHQ (microsecond freeze-hyperquench) powder samples at temperatures below approx. 250 K. Reduced cytochrome c oxidase from Paracoccus denitrificans was reacted with O(2) for 100 micros, frozen as a powder and transferred to the cuvette. Subsequently, cytochrome oxidase was allowed to react further following stepwise increments of the temperature from 100 K up to 250 K while recording spectra between 300 and 700 nm. The temperature was raised only when no further changes in the spectra could be detected. The experiment yielded spectra of the A, P(M), F and O intermediate states. This demonstrated that the catalytic cycle of cytochrome oxidase at low temperature is similar to that at room temperature and so verifies the suitability of this method for the study of enzymes with high catalytic-centre activity.

  11. High-pressure cells for study of condensed matter by diffraction and inelastic neutron scattering at low temperatures and in strong magnetic fields

    Science.gov (United States)

    Sadykov, R. A.; Strassle, Th; Podlesnyak, A.; Keller, L.; Fak, B.; Mesot, J.

    2017-12-01

    We have developed and implemented series of new original clamp high-pressure cells for neutron diffraction and inelastic neutron scattering at low temperatures. The cells design allows one to place them in the standard cryostats or cryomagnets used on neutron sources. Some results obtained for ZnCr2Se4 are demonstrated as an example.

  12. Low Temperature Plasma Medicine

    Science.gov (United States)

    Graves, David

    2013-10-01

    Ionized gas plasmas near room temperature are used in a remarkable number of technological applications mainly because they are extraordinarily efficient at exploiting electrical power for useful chemical and material transformations near room temperature. In this tutorial address, I will focus on the newest area of low temperature ionized gas plasmas (LTP), in this case operating under atmospheric pressure conditions, in which the temperature-sensitive material is living tissue. LTP research directed towards biomedical applications such as sterilization, surgery, wound healing and anti-cancer therapy has seen remarkable growth in the last 3-5 years, but the mechanisms responsible for the biomedical effects have remained mysterious. It is known that LTP readily create reactive oxygen species (ROS) and reactive nitrogen species (RNS). ROS and RNS (or RONS), in addition to a suite of other radical and non-radical reactive species, are essential actors in an important sub-field of aerobic biology termed ``redox'' (or oxidation-reduction) biology. I will review the evidence suggesting that RONS generated by plasmas are responsible for their observed therapeutic effects. Other possible bio-active mechanisms include electric fields, charges and photons. It is common in LTP applications that synergies between different mechanisms can play a role and I will review the evidence for synergies in plasma biomedicine. Finally, I will address the challenges and opportunities for plasma physicists to enter this novel, multidisciplinary field.

  13. Low-Temperature Supercapacitors

    Science.gov (United States)

    Brandon, Erik J.; West, William C.; Smart, Marshall C.

    2008-01-01

    An effort to extend the low-temperature operational limit of supercapacitors is currently underway. At present, commercially available non-aqueous supercapacitors are rated for a minimum operating temperature of -40 C. A capability to operate at lower temperatures would be desirable for delivering power to systems that must operate in outer space or in the Polar Regions on Earth. Supercapacitors (also known as double-layer or electrochemical capacitors) offer a high power density (>1,000 W/kg) and moderate energy density (about 5 to 10 Wh/kg) technology for storing energy and delivering power. This combination of properties enables delivery of large currents for pulsed applications, or alternatively, smaller currents for low duty cycle applications. The mechanism of storage of electric charge in a supercapacitor -- at the electrical double-layer formed at a solid-electrode/liquid-electrolyte interface -- differs from that of a primary or secondary electrochemical cell (i.e., a battery) in such a manner as to impart a long cycle life (typically >10(exp 6) charge/discharge cycles).

  14. Low temperature magnetic studies on PbFe{sub 0.5}Nb{sub 0.5}O{sub 3} multiferroic

    Energy Technology Data Exchange (ETDEWEB)

    Matteppanavar, Shidaling [Department of Physics, Bangalore University, Jnanabharati Campus, Bangalore 560056 (India); Angadi, Basavaraj, E-mail: brangadi@gmail.com [Department of Physics, Bangalore University, Jnanabharati Campus, Bangalore 560056 (India); Rayaprol, Sudhindra [UGC–DAE CSR, Mumbai Centre, B.A.R.C, R-5 Shed, Mumbai 400085 (India)

    2014-09-01

    PbFe{sub 0.5}Nb{sub 0.5}O{sub 3} (PFN), a well-known A(B′{sub 1/2}B″{sub 1/2})O{sub 3} type multiferroic, was successfully synthesized in single phase by a single step solid state reaction method. The single phase PFN was characterized through XRD, microstructure through SEM, and magnetic studies were carried out through a temperature dependent vibrating sample magnetometer (VSM) and neutron diffraction (ND) measurements. PFN exhibits a cusp at around 150 K in the temperature dependent magnetic susceptibility corresponding to the Néel temperature (T{sub N1}) and another peak around 10 K (T{sub N2}) corresponding to spin-glass like transition. In the temperature dependent ND studies, a magnetic Bragg peak appears at Q=1.35 Å{sup −1} (where Q=4πsinθ/λ, is called the scattering vector) below T{sub N} (150 K) implying antiferromagnetic (AFM) ordering in the system. On the basis of Rietveld analysis of the ND data at T=2 K, the magnetic structure of PFN could be explained by a G-type antiferromagnetic structure.

  15. Measurement of grain-boundary diffusion at low temperature by the surface-accumulation method. II. Results for gold-silver system

    International Nuclear Information System (INIS)

    Hwang, J.C.M.; Pan, J.D.; Balluffi, R.W.

    1979-01-01

    Grain-boundary diffusion rates in the gold-silver system were measured at relatively low temperatures by the surface-accumulation method which was analyzed in Paper I. The specimen was a polycrystalline gold film possessing columnar grains on which a silver layer was initially deposited epitaxially on one surface. During subsequent low-temperature annealing lattice diffusion was frozen out, and diffusion then occurred along the grain boundary and free-surface short circuits. The silver, therefore, diffused into the film from the silver layer along the boundaries, eventually reaching the opposite surface where it accumulated and was measured by Auger spectroscopy. The silver layer acted as an effective constant silver source, and grain-boundary diffusivities were calculated from the accumulation data. However, the exact location of the effective constant source in the silver layer could not be determined and this led to an uncertainty in the values of the grain-boundary diffusivities of a factor of 10. Lower- and upper-bound values were therefore described by D/sub b/(lower bound) =7.8 x 10 -6 exp(-0.62eV/kT) and D/sub b/(upper bound) =7.8 x 10 -5 exp(-0.62eV/kT) cm 2 /s in the temperature range 30--269 0 C. An examination of available grain-boundary diffusion data (including the present) suggests a tendency for the observed activation energy to decrease with decreasing temperature, and this was ascribed to a spectrum of activated jumps in the grain boundary and/or a spectrum of grain-boundary types in the specimen employed. The constant source behavior was tentatively ascribed, at least in part, to a grain-boundary ''Kirkendall effect'' resulting from the faster diffusion of silver than gold. The work indicates a need for increased understanding of the details of grain-boundary diffusion in alloys

  16. The Low Temperature Microgravity Physics Experiments Project

    Science.gov (United States)

    Holmes, Warren; Lai, Anthony; Croonquist, Arvid; Chui, Talso; Eraker, J. H.; Abbott, Randy; Mills, Gary; Mohl, James; Craig, James; Balachandra, Balu; hide

    2000-01-01

    The Low Temperature Microgravity Physics Facility (LTMPF) is being developed by NASA to provide long duration low temperature and microgravity environment on the International Space Station (ISS) for performing fundamental physics investigations. Currently, six experiments have been selected for flight definition studies. More will be selected in a two-year cycle, through NASA Research Announcement. This program is managed under the Low Temperature Microgravity Physics Experiments Project Office at the Jet Propulsion Laboratory. The facility is being designed to launch and returned to earth on a variety of vehicles including the HII-A and the space shuttle. On orbit, the facility will be connected to the Exposed Facility on the Japanese Experiment Module, Kibo. Features of the facility include a cryostat capable of maintaining super-fluid helium at a temperature of 1.4 K for 5 months, resistance thermometer bridges, multi-stage thermal isolation system, thermometers capable of pico-Kelvin resolution, DC SQUID magnetometers, passive vibration isolation, and magnetic shields with a shielding factor of 80dB. The electronics and software architecture incorporates two VME buses run using the VxWorks operating system. Technically challenging areas in the design effort include the following: 1) A long cryogen life that survives several launch and test cycles without the need to replace support straps for the helium tank. 2) The minimization of heat generation in the sample stage caused by launch vibration 3) The design of compact and lightweight DC SQUID electronics. 4) The minimization of RF interference for the measurement of heat at pico-Watt level. 5) Light weighting of the magnetic shields. 6) Implementation of a modular and flexible electronics and software architecture. The first launch is scheduled for mid-2003, on an H-IIA Rocket Transfer Vehicle, out of the Tanegashima Space Center of Japan. Two identical facilities will be built. While one facility is onboard

  17. In-situ study of cascade defects in silver by simultaneous transmission electron microscopy and electrical resistivity measurements at low temperatures

    International Nuclear Information System (INIS)

    Haga, K.; King, W.E.; Merkle, K.L.; Meshii, M.

    1985-12-01

    A helium-cooled double-tilt specimen stage for transmission electron microscopy (TEM) with the capability of simultaneous electrical resistivity measurements was constructed and used to study defect-production, migration, clustering and recovery processes in ion-irradiated silver. Vacuum-evaporated thin film specimens were irradiated with 1 MeV Kr + -ions up to a dose of 4.0 x 10 10 ions/cm 2 , at T = 10 0 K in the microscope, using the HVEM-tandem accelerator ion beam interface system in the Argonne National Laboratory Electron Microscopy Center. Cascade defect formation during ion bombardment at the low temperature was directly observed both by TEM and electrical resistivity measurements. Ion bombardment created groups of defect clusters with strong strain fields which gave rise to TEM contrast. The specimen resistivity was increased by 16% during the irradiation. Subsequent microstructural changes and resistivity recovery during isochronal annealing were monitored up to room temperature. 58.3% of the irradiation induced resistivity was recovered, while significant reduction in the size of black spot defect clusters was observed by TEM. A small fraction of clusters disappeared, while no nucleation of new defect clusters was observed

  18. Magnetic Properties of the Nanocrystalline Nd-Ho-Fe-Co-B Alloy at Low Temperatures: The Influence of Time and Annealing

    Czech Academy of Sciences Publication Activity Database

    Tereshina, I. S.; Kudrevatykh, N. V.; Ivanov, L.A.; Politova, G.A.; Tereshina, Evgeniya; Gorbunov, D.I.; Doerr, M.; Rogacki, K.

    2017-01-01

    Roč. 26, č. 10 (2017), s. 4676-4680 ISSN 1059-9495 Institutional support: RVO:68378271 Keywords : hard magnetic materials * heat treatment * high magnetic field * hysteresis Subject RIV: BM - Solid Matter Physics ; Magnetism OBOR OECD: Condensed matter physics (including formerly solid state physics, supercond.) Impact factor: 1.331, year: 2016

  19. Microscopic origin of read current noise in TaO{sub x}-based resistive switching memory by ultra-low temperature measurement

    Energy Technology Data Exchange (ETDEWEB)

    Pan, Yue; Cai, Yimao, E-mail: caiyimao@pku.edu.cn; Liu, Yefan; Fang, Yichen; Yu, Muxi; Tan, Shenghu; Huang, Ru [Institute of Microelectronics, Peking University, Beijing 100871 (China)

    2016-04-11

    TaO{sub x}-based resistive random access memory (RRAM) attracts considerable attention for the development of next generation nonvolatile memories. However, read current noise in RRAM is one of the critical concerns for storage application, and its microscopic origin is still under debate. In this work, the read current noise in TaO{sub x}-based RRAM was studied thoroughly. Based on a noise power spectral density analysis at room temperature and at ultra-low temperature of 25 K, discrete random telegraph noise (RTN) and continuous average current fluctuation (ACF) are identified and decoupled from the total read current noise in TaO{sub x} RRAM devices. A statistical comparison of noise amplitude further reveals that ACF depends strongly on the temperature, whereas RTN is independent of the temperature. Measurement results combined with conduction mechanism analysis show that RTN in TaO{sub x} RRAM devices arises from electron trapping/detrapping process in the hopping conduction, and ACF is originated from the thermal activation of conduction centers that form the percolation network. At last, a unified model in the framework of hopping conduction is proposed to explain the underlying mechanism of both RTN and ACF noise, which can provide meaningful guidelines for designing noise-immune RRAM devices.

  20. Microscopic origin of read current noise in TaO_x-based resistive switching memory by ultra-low temperature measurement

    International Nuclear Information System (INIS)

    Pan, Yue; Cai, Yimao; Liu, Yefan; Fang, Yichen; Yu, Muxi; Tan, Shenghu; Huang, Ru

    2016-01-01

    TaO_x-based resistive random access memory (RRAM) attracts considerable attention for the development of next generation nonvolatile memories. However, read current noise in RRAM is one of the critical concerns for storage application, and its microscopic origin is still under debate. In this work, the read current noise in TaO_x-based RRAM was studied thoroughly. Based on a noise power spectral density analysis at room temperature and at ultra-low temperature of 25 K, discrete random telegraph noise (RTN) and continuous average current fluctuation (ACF) are identified and decoupled from the total read current noise in TaO_x RRAM devices. A statistical comparison of noise amplitude further reveals that ACF depends strongly on the temperature, whereas RTN is independent of the temperature. Measurement results combined with conduction mechanism analysis show that RTN in TaO_x RRAM devices arises from electron trapping/detrapping process in the hopping conduction, and ACF is originated from the thermal activation of conduction centers that form the percolation network. At last, a unified model in the framework of hopping conduction is proposed to explain the underlying mechanism of both RTN and ACF noise, which can provide meaningful guidelines for designing noise-immune RRAM devices.

  1. Characterization of the effects of nitrogen and hydrogen passivation on SiO2/4H-SiC interface by low temperature conductance measurements

    International Nuclear Information System (INIS)

    Wang Yiyu; Peng Zhaoyang; Shen Huajun; Tang Yachao; Liu Xinyu; Li Chengzhan; Wu Jia; Zhao Yanli; Chen Ximing; Liu Kean

    2016-01-01

    We investigate the effects of NO annealing and forming gas (FG) annealing on the electrical properties of a SiO 2 /SiC interface by low-temperature conductance measurements. With nitrogen passivation, the density of interface states (D IT ) is significantly reduced in the entire energy range, and the shift of flatband voltage, ΔV FB , is effectively suppressed to less than 0.4 V. However, very fast states are observed after NO annealing and the response frequencies are higher than 1 MHz at room temperature. After additional FG annealing, the D IT and ΔV FB are further reduced. The values of the D IT decrease to less than 10 11 cm −2 eV −1 for the energy range of E C − E T > 0.4 eV. It is suggested that the fast states in shallow energy levels originated from the N atoms accumulating at the interface by NO annealing. Though FG annealing has a limited effect on these shallow traps, hydrogen can terminate the residual Si and C dangling bonds corresponding to traps at deep energy levels and improve the interface quality further. It is indicated that NO annealing in conjunction with FG annealing will be a better post-oxidation process method for high performance SiC MOSFETs. (paper)

  2. Effect of La-CO substitution on the crystal structure and magnetic properties of low temperature sintered Sr1-xLaxFe12-xCoxO19 (x=0-0.5) ferrites

    Science.gov (United States)

    Peng, Long; Li, Lezhong; Wang, Rui; Hu, Yun; Tu, Xiaoqiang; Zhong, Xiaoxi

    2015-11-01

    The La-Co substituted Sr1-xLaxFe12-xCoxO19 (x=0-0.5) ferrites with appropriate Bi2O3 additive were prepared at a low sintering temperature of 890 °C compatible with LTCC (low temperature co-fired ceramics) systems, and the effect of La-Co substitution on their crystal structure and magnetic properties was investigated. The results show that the pure M-type phase is successfully obtained when the La-Co substitution amount x does not exceed 0.3. However, the single M-type phase structure transforms to multiphase structure with further increased x, where the α-Fe2O3 phase and La2O3 phase coexist with the M-type phase. Moreover, the saturation magnetization Ms, magnetic anisotropy field Ha, intrinsic coercivity Hci, and Curie temperature TC of the ferrites depend on the La-Co substitution amount strongly, which are suggested to be determined by the partially substitution of La3+-Co2+ ions for Sr2+-Fe3+ ions with x not higher than 0.3. It is found that the obtained Sr1-xLaxFe12-xCoxO19 (x=0.2 and 0.3) ferrites can provide improved magnetic properties (Ms>62 emu/g, Ha>1400 kA/m, and Hci>320 kA/m) as low temperature sintered M-type hexaferrites for microwave LTCC applications.

  3. Low-temperature magnetic structure of YBaCuFeO5 and the effect of partial substitution of yttrium by calcium

    DEFF Research Database (Denmark)

    Ruiz-Aragon, M.J.; Moran, E.; Amador, U.

    1998-01-01

    Two magnetic phase transitions at T-N1 approximate to 475 K (AF1 phase) and T-N2 approximate to 240 K (AF2) are observed in YBaCuFeO5. The magnetic unit cell of AFL is four times the chemical cell, a(m) = root 2a, c(m) = 2c, and the magnetic moments within one chemical cell are antiparallel to ea...

  4. New experimental perspectives for soft x-ray absorption spectroscopies at ultra-low temperatures below 50 mK and in high magnetic fields up to 7 T

    International Nuclear Information System (INIS)

    Beeck, T.; Baev, I.; Gieschen, S.; Meyer, H.; Meyer, S.; Palutke, S.; Martins, M.; Feulner, P.; Uhlig, K.; Wurth, W.

    2016-01-01

    A new ultra-low temperature experiment including a superconducting vector magnet has been developed for soft x-ray absorption spectroscopy experiments at third generation synchrotron light sources. The sample is cooled below 50 mK by a cryogen free "3He-"4He dilution refrigerator. At the same time, magnetic fields of up to ±7 T in the horizontal direction and ±0.5 T in the vertical direction can be applied by a superconducting vector magnet. The setup allows to study ex situ and in situ prepared samples, offered by an attached UHV preparation chamber with load lock. The transfer of the prepared samples between the preparation section and the dilution refrigerator is carried out under cryogenic temperatures. First commissioning studies have been carried out at the Variable Polarization XUV Beamline P04 at PETRA III and the influence of the incident photon beam to the sample temperature has been studied.

  5. Effect of Ising-type Tb.sup.3+./sup. ions on the low-temperature magnetism of La, Ca cobaltite

    Czech Academy of Sciences Publication Activity Database

    Knížek, Karel; Jirák, Zdeněk; Hejtmánek, Jiří; Veverka, Miroslav; Kaman, Ondřej; Maryško, Miroslav; Šantavá, Eva; André, G.

    2014-01-01

    Roč. 26, č. 11 (2014), "116003-1"-"116003-9" ISSN 0953-8984 R&D Projects: GA ČR(CZ) GAP204/11/0713 Institutional support: RVO:68378271 Keywords : perovskite cobaltites * neutron diffraction * magnetic ordering * Ising moments * linear specific heat Subject RIV: BM - Solid Matter Physics ; Magnetism Impact factor: 2.346, year: 2014

  6. A low-temperature scanning tunneling microscope capable of microscopy and spectroscopy in a Bitter magnet at up to 34 T.

    Science.gov (United States)

    Tao, W; Singh, S; Rossi, L; Gerritsen, J W; Hendriksen, B L M; Khajetoorians, A A; Christianen, P C M; Maan, J C; Zeitler, U; Bryant, B

    2017-09-01

    We present the design and performance of a cryogenic scanning tunneling microscope (STM) which operates inside a water-cooled Bitter magnet, which can attain a magnetic field of up to 38 T. Due to the high vibration environment generated by the magnet cooling water, a uniquely designed STM and a vibration damping system are required. The STM scan head is designed to be as compact and rigid as possible, to minimize the effect of vibrational noise as well as fit the size constraints of the Bitter magnet. The STM uses a differential screw mechanism for coarse tip-sample approach, and operates in helium exchange gas at cryogenic temperatures. The reliability and performance of the STM are demonstrated through topographic imaging and scanning tunneling spectroscopy on highly oriented pyrolytic graphite at T = 4.2 K and in magnetic fields up to 34 T.

  7. Low-temperature electron properties of Heusler alloys Fe2VAl and Fe2CrAl: Effect of annealing

    International Nuclear Information System (INIS)

    Podgornykh, S. M.; Svyazhin, A. D.; Shreder, E. I.; Marchenkov, V. V.; Dyakina, V. P.

    2007-01-01

    We present the results of measurements of low-temperature heat capacity, as well as electrical and magnetic properties of Heusler alloys Fe 2 VAl and Fe 2 CrAl prepared in different ways using various heat treatment regimes. The density of states at the Fermi level is estimated. A contribution of ferromagnetic clusters in the low-temperature heat capacity of the Fe 2 VAl alloy is detected. The change in the number and volume of clusters as a result of annealing of an alloy affects the behavior of their low-temperature heat capacity, resistivity, and magnetic properties

  8. Low-temperature phase diagram of YbBiPt

    International Nuclear Information System (INIS)

    Movshovich, R.; Lacerda, A.; Canfield, P.C.; Thompson, J.D.; Fisk, Z.

    1994-01-01

    Resistivity measurements are reported on the cubic heavy-fermion compound YbBiPt at ambient and hydrostatic pressures to ∼19 kbar and in magnetic fields to 1 T. The phase transition at T c =0.4 K is identified by a sharp rise in resistivity. That feature is used to build low-temperature H-T and P-T phase diagrams. The phase boundary in the H-T plane follows the weak-coupling BCS expression remarkably well from T c to T c /4, while small hydrostatic pressure of ∼1 kbar suppresses the low-temperature phase entirely. These effects of hydrostatic pressure and magnetic field on the phase transition are consistent with an spin-density-wave (SDW) formation in a very heavy electron band at T=0.4 K. Outside of the SDW phase at low temperature, hydrostatic pressure increases the T 2 coefficient of resistivity, signaling an increase in heavy-fermion correlations with hydrostatic pressure. The residual resistivity decreases with pressure, contrary to trends in other Yb heavy-fermion compounds

  9. Magnetic Field Measurements in Beam Guiding Magnets

    CERN Document Server

    Henrichsen, K N

    1998-01-01

    Electromagnets used as beam guiding elements in particle accelerators and colliders require very tight tole-rances on their magnetic fields and on their alignment along the particle path. This article describes the methods and equipment used for magnetic measurements in beam transport magnets. Descriptions are given of magnetic resonance techniques, various induction coil methods, Hall generator measurements, the fluxgate magnetometer as well as the recently developed method of beam based alignment. References of historical nature as well as citations of recent work are given. The present commercial availability of the different sensors and asso-ciated equipment is indicated. Finally we shall try to analyze possible future needs for developments in those fields.

  10. Experiments on Quantum Hall Topological Phases in Ultra Low Temperatures

    International Nuclear Information System (INIS)

    Du, Rui-Rui

    2015-01-01

    This project is to cool electrons in semiconductors to extremely low temperatures and to study new states of matter formed by low-dimensional electrons (or holes). At such low temperatures (and with an intense magnetic field), electronic behavior differs completely from ordinary ones observed at room temperatures or regular low temperature. Studies of electrons at such low temperatures would open the door for fundamental discoveries in condensed matter physics. Present studies have been focused on topological phases in the fractional quantum Hall effect in GaAs/AlGaAs semiconductor heterostructures, and the newly discovered (by this group) quantum spin Hall effect in InAs/GaSb materials. This project consists of the following components: 1) Development of efficient sample cooling techniques and electron thermometry: Our goal is to reach 1 mK electron temperature and reasonable determination of electron temperature; 2) Experiments at ultra-low temperatures: Our goal is to understand the energy scale of competing quantum phases, by measuring the temperature-dependence of transport features. Focus will be placed on such issues as the energy gap of the 5/2 state, and those of 12/5 (and possible 13/5); resistive signature of instability near 1/2 at ultra-low temperatures; 3) Measurement of the 5/2 gaps in the limit of small or large Zeeman energies: Our goal is to gain physics insight of 5/2 state at limiting experimental parameters, especially those properties concerning the spin polarization; 4) Experiments on tuning the electron-electron interaction in a screened quantum Hall system: Our goal is to gain understanding of the formation of paired fractional quantum Hall state as the interaction pseudo-potential is being modified by a nearby screening electron layer; 5) Experiments on the quantized helical edge states under a strong magnetic field and ultralow temperatures: our goal is to investigate both the bulk and edge states in a quantum spin Hall insulator under

  11. Numerical modelling and experimental measurements for a low-temperature district heating substation for instantaneous preparation of DHW with respect to service pipes

    International Nuclear Information System (INIS)

    Brand, Marek; Thorsen, Jan Eric; Svendsen, Svend

    2012-01-01

    Traditional district heating (DH) systems are becoming uneconomic as the number of new and renovated buildings with reduced heating requirements increases. To keep DH competitive in the future, heat losses in DH networks need to be reduced. One option is to reduce the supply temperature of DH as much as possible. This requires a review and improvement of a DH network, in-house substations, and the whole domestic hot water (DHW) supply system, with the focus on user comfort, hygiene, overall cost and energy efficiency. This paper describes some practical approaches to the implementation of low-temperature district heating (LTDH) with an entry-to-substation temperature around 50 °C. To this end we developed a numerical model for an instantaneous LTDH substation that takes into consideration the effect of service pipes. The model has been verified and can be used for the further optimization of the whole concept as well for individual components. The results show that the way that the service pipe is operated has a significant effect on waiting time for DHW, heat loss, and overall cost. Furthermore, the service pipe should be kept warm by using a bypass in order to fulfil the comfort requirements for DHW instantaneously prepared. -- Highlights: ► Describes and justifies concept of low-temperature district heating with supply temperature of 50 °C. ► Focuses on DHW preparation in low-temperature district heating in-house substations, considering comfort and Legionella. ► Verified numerical model reports on dynamic performance of an in-house substation, considering operation of service pipes. ► Bypass is needed for instantaneous type of district heating substations to fulfil comfort requirements of users. ► The model developed can be used for future optimization of low-temperature substations and whole district heating networks.

  12. Comparative study of magnetic ordering in bulk and nanoparticles of Sm0.65Ca0.35MnO3: Magnetization and electron magnetic resonance measurements

    International Nuclear Information System (INIS)

    Goveas, Lora Rita; Anuradha, K. N.; Bhagyashree, K. S.; Bhat, S. V.

    2015-01-01

    To explore the effect of size reduction to nanoscale on the hole doped Sm 0.65 Ca 0.35 MnO 3 compound, dc magnetic measurements and electron magnetic resonance (EMR) were done on bulk and nanoparticle samples in the temperature range 10 ≤ T ≤ 300 K. Magnetization measurement showed that the bulk sample undergoes a charge ordering transition at 240 K and shows a mixed magnetic phase at low temperature. However, the nanosample underwent a ferromagnetic transition at 75 K, and the charge ordered state was destabilized on size reduction down to nanoscale. The low-temperature ferromagnetic component is found to be enhanced in nanoparticles as compared to their bulk counterpart. Interestingly around room temperature, bulk particles show higher magnetization where as at low temperature nanoparticles show higher magnetization. Ferromagnetism in the bulk is due to super exchange where as ferromagnetism in nanoparticles is due to uncompensated spins of the surface layer. Temperature variation of EMR parameters correlates well with the results of magnetic measurements. The magnetic behaviour of the nanoparticles is understood in terms of the core shell scenario

  13. Comparative study of magnetic ordering in bulk and nanoparticles of Sm0.65Ca0.35MnO3: Magnetization and electron magnetic resonance measurements

    Science.gov (United States)

    Goveas, Lora Rita; Anuradha, K. N.; Bhagyashree, K. S.; Bhat, S. V.

    2015-05-01

    To explore the effect of size reduction to nanoscale on the hole doped Sm0.65Ca0.35MnO3 compound, dc magnetic measurements and electron magnetic resonance (EMR) were done on bulk and nanoparticle samples in the temperature range 10 ≤ T ≤ 300 K. Magnetization measurement showed that the bulk sample undergoes a charge ordering transition at 240 K and shows a mixed magnetic phase at low temperature. However, the nanosample underwent a ferromagnetic transition at 75 K, and the charge ordered state was destabilized on size reduction down to nanoscale. The low-temperature ferromagnetic component is found to be enhanced in nanoparticles as compared to their bulk counterpart. Interestingly around room temperature, bulk particles show higher magnetization where as at low temperature nanoparticles show higher magnetization. Ferromagnetism in the bulk is due to super exchange where as ferromagnetism in nanoparticles is due to uncompensated spins of the surface layer. Temperature variation of EMR parameters correlates well with the results of magnetic measurements. The magnetic behaviour of the nanoparticles is understood in terms of the core shell scenario.

  14. Measurements of magnetic field alignment

    International Nuclear Information System (INIS)

    Kuchnir, M.; Schmidt, E.E.

    1987-01-01

    The procedure for installing Superconducting Super Collider (SSC) dipoles in their respective cryostats involves aligning the average direction of their field with the vertical to an accuracy of 0.5 mrad. The equipment developed for carrying on these measurements is described and the measurements performed on the first few prototypes SSC magnets are presented. The field angle as a function of position in these 16.6 m long magnets is a characteristic of the individual magnet with possible feedback information to its manufacturing procedure. A comparison of this vertical alignment characteristic with a magnetic field intensity (by NMR) characteristic for one of the prototypes is also presented. 5 refs., 7 figs

  15. Technological uses of low temperature plasmas

    International Nuclear Information System (INIS)

    Lawton, J.

    1975-01-01

    Types of low temperature plasma sources considered include; arc discharge, high pressure discharge, low pressure discharge and flame. The problems of uniform heating of a gas are discussed and it is considered that the most reliable technique is the magnetically rotated arc, but expanded discharges of one kind or another are likely to be serious competitors in the future. The uses of low temperature plasma in chemistry and combustion are considered. The potential for plasma chemistry lies with processes in which the reactions occur in the plasma itself or its neighbouring gas phase, including those which require the vaporization of liquefaction of a refractory material and also highly endothermic reactions. The production of thixotropic silica and acetylene are discussed as examples of such reactions. The field of plasma and combustion including; ignition, flame ionization and soot formation, and the MHD generator, is considered. (U.K.)

  16. Magnetic measurements under pressure

    Czech Academy of Sciences Publication Activity Database

    Zentková, M.; Arnold, Zdeněk; Mihalik, M.; Mihalik, M.; Zentko, A.; Kamarád, Jiří; Mitróová, Z.; Mat`aš, S.

    2006-01-01

    Roč. 57, 8/S (2006), s. 29-32 ISSN 1335-3632 Institutional research plan: CEZ:AV0Z10100521 Keywords : hydrostatic pressure * Prussian blue analogues * AC susceptibility * intermetallic compound * ferromagnetism * errimagnetism Subject RIV: BM - Solid Matter Physics ; Magnetism

  17. Mechanical-property changes of structural composite materials after low-temperature proton irradiation: Implications for use in SSC magnet systems

    International Nuclear Information System (INIS)

    Morena, J.; Snead, C.L. Jr.; Czajkowski, C.; Skaritka, J.

    1993-01-01

    Longterm physical, mechanical, electrical, and other properties of advanced composites, plastics, and other polymer materials are greatly affected by high-energy proton, neutron, electron, and gamma radiation. The effects of high-energy particles on materials is a critical design parameter to consider when choosing polymeric structural, nonstructural, and elastomeric matrix resin systems. Polymer materials used for filled resins, laminates, seals, gaskets, coatings, insulation and other nonmetallic components must be chosen carefully, and reference data viewed with caution. Most reference data collected in the high-energy physics community to date reflects material property degradation using other than proton irradiations. In most instances, the data were collected for room-temperature irradiations, not 4.2 K or other cryogenic temperatures, and at doses less than 10 8 --10 9 Rad. Energetic proton (and the accompanying spallation-product particles) provide good simulation fidelity to the expected radiation fields predicted for the cold-mass regions of the SSC magnets, especially the corrector magnets. The authors present here results for some structural composite materials which were part of a larger irradiation-characterization of polymeric materials for SSC applications

  18. NMR study of CeTe at low temperatures

    Energy Technology Data Exchange (ETDEWEB)

    Hinderer, J. [Laboratorium fuer Festkoerperphysik, ETH Zuerich, CH-8093 Zurich (Switzerland)]. E-mail: hinderer@phys.ethz.ch; Weyeneth, S.M. [Laboratorium fuer Festkoerperphysik, ETH Zuerich, CH-8093 Zurich (Switzerland); Weller, M. [Laboratorium fuer Festkoerperphysik, ETH Zuerich, CH-8093 Zurich (Switzerland); Gavilano, J.L. [Laboratorium fuer Festkoerperphysik, ETH Zuerich, CH-8093 Zurich (Switzerland); Felder, E. [Laboratorium fuer Festkoerperphysik, ETH Zuerich, CH-8093 Zurich (Switzerland); Hulliger, F. [Laboratorium fuer Festkoerperphysik, ETH Zuerich, CH-8093 Zurich (Switzerland); Ott, H.R. [Laboratorium fuer Festkoerperphysik, ETH Zuerich, CH-8093 Zurich (Switzerland)

    2006-05-01

    We present {sup 125}Te NMR measurements on CeTe powder at temperatures between 1 and 150K and in magnetic fields between 5 and 8T. CeTe is a rocksalt-type intermetallic compound. It orders antiferromagnetically at T{sub N}{approx}2.2K with a much reduced ordered moment [H.R. Ott, J.K. Kjems, F. Hulliger, Phys. Rev. Lett. 42 20 (1979) 1378]. From our low-temperature NMR spectra we infer the presence of at least three inequivalent Te sites at low temperatures. Considering the crystal structure this result is completely unexpected. The linewidths and the Knight shifts of the individual lines are significantly different and increase substantially with decreasing temperature. They follow the temperature dependence of the magnetic susceptibility above 20K. Above T{sub N}, hyperfine fields of 1.6, 0.8 and 0.0T at the three Te sites per Bohr magneton of Ce moment are deduced from Knight shift vs. magnetic susceptibility data. These values are typical for transferred hyperfine fields via conduction electrons.

  19. Vol. 5: Low Temperature Physics

    International Nuclear Information System (INIS)

    Sitenko, A.

    1993-01-01

    Problems of modern physics and the situation with physical research in Ukraine are considered. Programme of the conference includes scientific and general problems. Its proceeding are published in 6 volumes. The papers presented in this volume refer to low-temperature physics

  20. Certification testing at low temperatures

    International Nuclear Information System (INIS)

    Noss, P.W.; Ammerman, D.J.

    2004-01-01

    Regulations governing the transport of radioactive materials require that most hypothetical accident condition tests or analyses consider the effects of the environmental temperature that most challenges package performance. For many packages, the most challenging temperature environment is the cold condition (-29 C according to U.S. regulations), primarily because the low temperature causes the highest free drop impact forces due to the higher strength of many energy-absorbing materials at this temperature. If it is decided to perform low temperature testing, it is only necessary that the relevant parts of the package have the required temperature prior to the drop. However, the details of performing a drop at low temperature can have a large influence on testing cost and technical effectiveness. The selection of the test site, the chamber and type of chilling equipment, instrumentation, and even the time of year are all important. Control of seemingly minor details such as the effect on internal pressure, placement of monitoring thermocouples, the thermal time constant of the test article, and icing of equipment are necessary to ensure a successful low temperature test. This paper will discuss these issues and offer suggestions based on recent experience

  1. Science with low temperature detectors

    International Nuclear Information System (INIS)

    Sadoulet, B.; Lawrence Berkeley National Lab., CA; California Univ., Berkeley

    1996-01-01

    The novel technique of particle detection with low temperature detectors opens a number of new scientific opportunities. We review some of these, focusing on three generic applications: far infrared bolometry taking as an example the cosmic microwave background, X-ray spectroscopy for astrophysics and biological applications, and massive calorimeters for dark matter searches and neutrino physics. (orig.)

  2. LOW TEMPERATURE CATHODE SUPPORTED ELECTROLYTES

    Energy Technology Data Exchange (ETDEWEB)

    Harlan U. Anderson

    2000-03-31

    This project has three main goals: Thin Films Studies, Preparation of Graded Porous Substrates and Basic Electrical Characterization and Testing of Planar Single Cells. During this time period substantial progress has been made in developing low temperature deposition techniques to produce dense, nanocrystalline yttrium-stabilized zirconia films on both dense oxide and polymer substrates. Progress has been made in the preparation and characterization of thin electrolytes and porous LSM substrates. Both of these tasks are essentially on or ahead of schedule. In our proposal, we suggested that the ZrO{sub 2}/Sc system needed to be considered as a candidate as a thin electrolyte. This was because microcrystalline ZrO{sub 2}/Sc has a significantly higher ionic conductivity than YSZ, particularly at the lower temperatures. As a result, some 0.5 micron thick film of ZrO{sub 2}/16% Sc on an alumina substrate (grain size 20nm) was prepared and the electrical conductivity measured as a function of temperature and oxygen activity. The Sc doped ZrO{sub 2} certainly has a higher conductivity that either 20nm or 2400nm YSZ, however, electronic conductivity dominates the conductivity for oxygen activities below 10{sup -15}. Whereas for YSZ, electronic conductivity is not a problem until the oxygen activity decreases below 10{sup -25}. These initial results show that the ionic conductivity of 20nm YSZ and 20nm ZrO{sub 2}/16% Sc are essentially the same and the enhanced conductivity which is observed for Sc doping in microcrystalline specimens is not observed for the same composition when it is nanocrystalline. In addition they show that the electronic conductivity of Sc doped ZrO{sub 2} is at least two orders of magnitude higher than that observed for YSZ. The conclusion one reaches is that for 0.5 to 1 micron thick nanocrystalline films, Sc doping of ZrO{sub 2} has no benefits compared to YSZ. As a result, electrolyte films of ZrO{sub 2}/Sc should not be considered as candidates

  3. Low temperature measurements of the heat capacity and thermodynamic functions of pseudo-malachite Cu5(PO4)2(OH)4

    International Nuclear Information System (INIS)

    Bissengaliyeva, M.R.; Gogol, D.B.; Bekturganov, N.S.

    2012-01-01

    The investigation of the heat capacity of a natural specimen of copper phosphate—pseudo-malachite Cu 5 (PO 4 ) 2 (OH) 4 in the temperature range between 4.2 K and 320 K has been carried out by the method of low-temperature adiabatic calorimetry. Tabulated values of the heat capacity and thermodynamic functions of the mineral including the changes of entropy and enthalpy and the Gibbs function of free energy have been calculated. The standard values of thermodynamic functions of pseudo-malachite at T = 298.15 K are C p,m ° =(385.43±0.41)J mole −1  K −1 , Δ 0 T S m ° =(412.16±0.61)J mole −1  K −1 , Δ 0 T H m ° =(63681.5±57.0)J mole −1 , F m ° =(198.57±0.47)J mole −1  K −1 . In the low-temperature area 0 tr = (5.772 ± 0.081) J mole −1 K −1 , ΔH tr = (29.94 ± 0.42) J mole −1 .

  4. Measuring Earth's Magnetic Field Simply.

    Science.gov (United States)

    Stewart, Gay B.

    2000-01-01

    Describes a method for measuring the earth's magnetic field using an empty toilet paper tube, copper wire, clear tape, a battery, a linear variable resistor, a small compass, cardboard, a protractor, and an ammeter. (WRM)

  5. Measurement and modeling of the low-temperature penetration-depth anomaly in high-quality MgB{sub 2} thin films

    Energy Technology Data Exchange (ETDEWEB)

    Agassi, Y.D. [Naval Surface Warfare Center, Carderock Division, Bethesda, MD 20817 (United States); Oates, D.E., E-mail: OATES@LL.MIT.EDU [MIT-Lincoln Laboratory, Lexington, MA 02420 (United States); Moeckly, B.H. [STI, Inc. Santa Barbara, CA 93111 (United States)

    2012-10-15

    Based on our measurements of intermodulation distortion in MgB{sub 2}, we have previously proposed that the {pi} energy-gap in MgB{sub 2} entails six nodal lines [Y.D. Agassi, D.E. Oates, and B.H. Moeckly, Phys. Rev. B 80 (2009) 174522]. Here we report high-precision measurements in MgB{sub 2} stripline resonators that show an increase of the penetration depth as the temperature is decreased below 5 K. This increase is consistent with the Script-Small-L = 6 symmetry of the {pi} energy gap that we have proposed. We interpret the increase as a manifestation of Andreev surface-attached states that are associated with the nodal lines of the {pi} energy gap. Penetration-depth calculations are in good agreement with our data. To reconcile the present interpretation with existing literature, we review other penetration-depth data, magnetic-impurity and tunneling experiments, and data on the paramagnetic Meissner effect. We conclude that these data do not rule out the interpretation of our experimental data based on a nodal {pi} energy gap.

  6. Comparative measurements of plasma potential with ball-pen and Langmuir probe in low-temperature magnetized plasma

    Czech Academy of Sciences Publication Activity Database

    Zanáška, M.; Adámek, Jiří; Peterka, Matěj; Kudrna, P.; Tichý, M.

    2015-01-01

    Roč. 22, č. 3 (2015), č. článku 033516. ISSN 1070-664X Institutional support: RVO:61389021 Keywords : plasma * tokamak * ball- pen probe (BPP) Subject RIV: BL - Plasma and Gas Discharge Physics OBOR OECD: Fluids and plasma physics (including surface physics) Impact factor: 2.207, year: 2015 http://scitation.aip.org/content/aip/journal/pop/22/3/10.1063/1.4916572

  7. Interesting low temperature magneto-elastic behavior of a FINEMET metglass

    Directory of Open Access Journals (Sweden)

    Md. Sarowar Hossain

    2017-11-01

    Full Text Available We here report on studies of low temperature dynamic elastic properties of an amorphous ribbon of a FINEMET alloy, with and without magnetic field. Characterization with XRD and SEM showed that the sample was partially amorphous. Magnetization study showed the system as ferromagnetic and there was no transition in resistivity, anomalous peaks in sound velocity and internal friction measurements, with a small hysteresis and strong magnetic field dependence, were found in this temperature range. After analysing the data we concluded that it was magnetic in origin. This is reported for the first time in the FINEMET system.

  8. Containment test in area of high latitude and low temperature

    International Nuclear Information System (INIS)

    Cai Jiantao; Ni Yongsheng; Jia Wutong

    2014-01-01

    The effects of high latitude and low temperature on containment test are detailed analyzed from the view of design, equipment, construct and start-up, and the solution is put forward. The major problems resolved is as below: the effects of low temperature and high wind on defect inspection of the containment surface, the effects of test load on the affiliated equipment of containment in the condition of low temperature, and the effects of low temperature on the containment leak rate measurement. Application in Hongyanhe Unit 1 showed that the proposed scheme can effectively overcome the influence of adverse weather on the containment test. (authors)

  9. An experimental study of praseodymium intermetallic compounds at low temperatures

    International Nuclear Information System (INIS)

    Greidanus, F.J.A.M.

    1982-01-01

    In this thesis the author studies the low temperature properties of praseodymium intermetallic compounds. In chapter 2 some of the techniques used for the experiments described in the subsequent chapters are discussed. A set-up to perform specific-heat experiments below 1 K and a technique for performing magnetic susceptibility measurments below 1 K, using a superconducting quantum interference device (SQUID) are described. Chapter 3 is devoted to the theory of interacting Pr 3+ ions. Both bilinear and biquadratic interactions are dealt with in a molecular-field approximation. It is shown that first as well as second-order phase transitions can occur, depending on the nature of the ground state, and on the ratio of magnetic to crystal-field interactions. In chapters 4, 5, 6 and 7 experimental results on the cubic Laves phase compounds PrRh 2 , PrIr 2 , PrPt 2 , PrRu 2 and PrNi 2 are presented. From inelastic neutron scattering experiments the crystalline electric field parameters of the above compounds are determined. In chapters 5 and 6 susceptibility, neutron-diffraction, hyperfine specific-heat, low-field magnetization, pulsed-field magnetization, specific-heat and resistivity measurements are presented. In chapter 7 the specific heat and differential susceptibility of PrNi 2 below 1 K are studied. Finally, in chapter 8 praseodymium intermetallic compounds with low-symmetry singlet ground states, and cubic compounds with magnetic doublet ground states are studied. (Auth.)

  10. AA magnet measurement team

    CERN Multimedia

    CERN PhotoLab

    1978-01-01

    Quickly improvised measurement equipment for the AA (Antiproton Accumulator) was all the tight schedule permitted, but the high motivation of the team made up for the lack of convenience. From left to right: Roy Billinge (Joint AA Project Leader, the other one was Simon van der Meer); Bruno Autin, Brian Pincott, Colin Johnson.

  11. Mechanical pumping at low temperature

    International Nuclear Information System (INIS)

    Perin, J.P.; Claudet, G.; Disdier, F.

    1995-01-01

    This novel concept consist of a mechanical pump able to run at low temperature (25K). Since gas density varies inversely with temperature, this pump would deliver much higher mass flow rate than at room temperature for a given size. Advantages of this concept are order of magnitude reduction in size, weight, when compared to a conventional pump scaled to perform the same mass flow rate at room temperature. This pump would be a solution to allow continuously tritium extraction and minimize the mass inventory. (orig.)

  12. Ammonia synthesis at low temperatures

    DEFF Research Database (Denmark)

    Rod, Thomas Holm; Logadottir, Ashildur; Nørskov, Jens Kehlet

    2000-01-01

    have been carried out to evaluate its feasibility. The calculations suggest that it might be possible to catalytically produce ammonia from molecular nitrogen at low temperatures and pressures, in particular if energy is fed into the process electrochemically. (C) 2000 American Institute of Physics.......Density functional theory (DFT) calculations of reaction paths and energies for the industrial and the biological catalytic ammonia synthesis processes are compared. The industrial catalyst is modeled by a ruthenium surface, while the active part of the enzyme is modeled by a MoFe6S9 complex...

  13. Low-temperature dynamics of magnetic nanoshells

    KAUST Repository

    Zhang, Bei; Gao, Jinhao; Xu, Bing; Zhang, Xixiang

    2010-01-01

    that there was no spin-glass phase in the well-crystallized nanoshell assembly, whereas the signature of the spin-glass phase (or the memory effect) was evident in the poorly crystallized nanoshell assembly. This result suggests that the origin of the spin-glass

  14. Wolte 5. low temperature electronics

    International Nuclear Information System (INIS)

    Balestra, F.; Dieudonne, F.; Jomaah, J.

    2002-01-01

    This book present the latest research and development results in advanced materials, technologies, devices, circuits and systems for low temperature electronics. The main themes of the papers are ranging from physics and fundamental aspects, modeling and simulation, to device and circuit design. The topics include advanced process and characterization, novel devices and cryogenic instrumentation. The papers are divided into nine sections, reflecting the main research efforts in different areas: i) deep submicron silicon MOSFETs, ii) alternative MOSFETs (SOI, innovating device architectures), iii) III-V devices, iv) other semiconductor devices (Ge devices, p-n junctions, IR sensors, semiconductor microcrystals), v) emerging devices and phenomena (nano Si-based devices, conduction and fluctuations mechanisms), vi) superconducting materials, vii) superconducting detectors, viii) superconducting devices and circuits (RSFQ, SIS mixers, metal-superconducting-semiconductor structures), ix) low temperature electronics for space applications. Six invited papers presented by internationally recognized authors, and 39 contributed papers are presented. The invited papers provide an excellent overview of today's status and progress, as well as tomorrow's challenges and trends in this important discipline for many cryogenic applications. (authors)

  15. Magnetic susceptibility measurements on Bi - Sn alloys

    International Nuclear Information System (INIS)

    Mustaffa bin Haji Abdullah

    1985-01-01

    Magnetic susceptibility measurements on eight samples of tin-rich and three samples of bismuth-rich Bi-Sn alloys were made from 85K to 300K by Faraday's method. The susceptibilities of the eight tin-rich samples are positive and greater than the susceptibility of pure tin. The values are approximately constant at low temperatures but decreasing a little bit with increasing temperature. This result is interpreted as due to the predominant contribution of the Pauli spin paramagnetic susceptibility. A small decrease in susceptibility with temperature is interpreted as due to the effect of the second order term in the expression for spin paramagnetic susceptibility. The fluctuation of the susceptibility for alloys of different composition is interpreted as due to the effect of the density of states at the Fermi levels. The three samples of bismuth-rich alloys show a transition to diamagnetic property, where the diamagnetism is increased with temperature. This result is predominant and due to the diamagnetic contribution from the ions. The increase in susceptibility with temperature is interpreted as due to an increase in the effective radii of the ions due to thermal expansion. (author)

  16. Existence and structure of rare-earth mono-carbides: study of their low-temperature magnetic properties; Existence et structure des monocarbures de terres rares. Etude de leurs proprietes magnetiques a basses temperatures

    Energy Technology Data Exchange (ETDEWEB)

    Lallement, R [Commissariat a l' Energie Atomique, Centre d' Etudes Nucleaires de Fontenay-aux-Roses, 92 (France)

    1966-07-01

    There are two types of rare earth carbides, the first one is face-centered cubic, stable at high temperature, and very hypo-stoichiometric (formula MC{sub x} with 0.35 < x < 0.65); the other is rhombohedric, stable at lower temperature, with a formula M{sub 2}C. These two carbides are magnetically ordered at low temperatures (ferro or ferri-magnetism). They are highly anisotropic. A great part of the electric and magnetic properties can be explained from the following ideas: the M{sup 3+} ions are coupled via the conduction electrons, there are more conduction electrons in the carbides than in the metals, and there is some local order around the transition temperatures. (author) [French] Nous avons mis en evidence l'existence de deux carbures de terres rares, l'un de formule MC{sub x} (0,35 < x < 0,65) de structure cubique a faces centrees, stable a haute temperature, l'autre de formule M{sub 2}C, de structure rhomhoedrique, stable a temperature moyenne. Ces deux types de carbures presentent des phenomenes d'ordre magnetique a basses temperatures (ferro ou ferrimagnetisme). Ils sont caracterises par une forte anisotropie magnetique. Une grande partie des proprietes electriques et magnetiques s'explique a partir des hypotheses suivantes: a) Les ions M{sup 3+} sont couples entre eux par l'intermediaire des electrons de conduction; b) Le nombre d'electrons de conduction dans les carbures est plus grand que dans les metaux; c) Autour des temperatures de transition se manifestent des phenomenes d'ordre local. (auteur)

  17. Single crystal growth and electrical and magnetic measurements on CeFe4Sb12

    International Nuclear Information System (INIS)

    Mori, I.; Sugawara, H.; Magishi, K.; Saito, T.; Koyama, K.; Kikuchi, D.; Tanaka, K.; Sato, H.

    2007-01-01

    We have succeeded in growing single crystals of CeFe 4 Sb 12 by a Sb-self-flux method and measured the electrical resistivity and magnetization. The residual resistivity is about two times smaller than that of polycrystalline ones, suggesting that the sample quality is highly improved. The magnetization measurements at low temperature revealed that the sample contains almost no magnetic impurities which are always observed in polycrystalline samples. The weak temperature dependence and a broad maximum around 115K in magnetic susceptibility, which is a typical feature of valence fluctuation compounds, have been observed

  18. Magnetic susceptibility and specific heat of the one-dimensional conductor (H3O) sub (1,6) Pt (C2O4)2.nH2O at low temperatures

    International Nuclear Information System (INIS)

    Raede, H.S.

    1985-01-01

    It has been shown recently that some transition metal complexes exhibit one-dimensional metallic properties. It is reported, in this context, susceptibility and specific heat measurements of polycrystalline (H 3 O) 1 , 6 Pt(C 2 O 4 ) 2 .nH 2 O in the low temperature range. It is found that the susceptibility can be described by a non-uniform Curie law with a characteristic break in the slope. The specific heat reveals no linear temperature contribution, which could be explained by a transition into a Peierls distorted state. Until 13 0 K, the heat capacity follows a T 3 -law. Deviations at higher temperatures are possibly attributed to the anisotropy of the system [pt

  19. The Low temperature CFB gasifier

    DEFF Research Database (Denmark)

    Stoholm, P.; Nielsen, Rasmus Glar; Fock, Martin W.

    2003-01-01

    %) particle separation by the hot secondary cyclone. The next LT-CFB experiment, currently under preparation, is expected to be on either municipal/industrial waste or animal manure. Eventually a 500 kW LT-CFB test plant scheduled for commission during summer 2003, and the anticipated primary LT......The Low Temperature Circulating Fluidised Bed (LT-CFB) gasification process aims at avoiding problems due to ash deposition and agglomeration when using difficult fuels such as agricultural biomass and many waste materials. This, as well as very simple gas cleaning, is achieved by pyrolysing...... the fuel at around 650?C in a CFB reaction chamber and subsequently gasifying the char at around 730oC in a slowly fluidised bubbling bed chamber located in the CFB particle recirculation path. In this paper the novel LT-CFB concept is further described together with the latest test results from the 50 k...

  20. Low Temperature Hydrogen Antihydrogen Interactions

    International Nuclear Information System (INIS)

    Armour, E. A. G.; Chamberlain, C. W.

    2001-01-01

    In view of current interest in the trapping of antihydrogen (H-bar) atoms at low temperatures, we have carried out a full four-body variational calculation to determine s-wave elastic phase shifts for hydrogen antihydrogen scattering, using the Kohn Variational Principle. Terms outside the Born-Oppenheimer approximation have been taken into account using the formalism of Kolos and Wolniewicz. As far as we are aware, this is the first time that these terms have been included in an H H-bar scattering calculation. This is a continuation of earlier work on H-H-bar interactions. Preliminary results differ substantially from those calculated using the Born-Oppenheimer approximation. A method is outlined for reducing this discrepancy and taking the rearrangement channel into account.

  1. Mechanical pumping at low temperature

    Energy Technology Data Exchange (ETDEWEB)

    Perin, J.P.; Claudet, G.; Disdier, F.

    1994-12-31

    This new concept consists of a mechanical pump able to run at low temperature (25 K). Since gas density varies inversely with temperature, the pump could deliver much higher mass flow rate than at room temperature for a given size. Advantages of this concept are reduction of an order of magnitude in size and weight when compared to a conventional pump scaled to perform the same mass flow rate at room temperature. Results obtained at 80 K and 25 K with a Holweck type molecular drag pump of 100 mm diameter and with few stages of a turbomolecular pump running at the same temperatures, are given. This pump would be a solution to allow continuous tritium extraction and minimize the mass inventory for the ITER (International Tokamak Experiment Reactor). 5 figs., 2 tabs., 4 refs.

  2. Magnetic moment measurement of magnetic nanoparticles using atomic force microscopy

    International Nuclear Information System (INIS)

    Park, J-W; Lee, E-C; Ju, H; Yoo, I S; Chang, W-S; Chung, B H; Kim, B S

    2008-01-01

    Magnetic moment per unit mass of magnetic nanoparticles was found by using the atomic force microscope (AFM). The mass of the nanoparticles was acquired from the resonance frequency shift of the particle-attached AFM probe and magnetic force measurement was also carried out with the AFM. Combining with magnetic field strength, the magnetic moment per unit mass of the nanoparticles was determined as a function of magnetic field strength. (technical design note)

  3. Magnetic properties and low-temperature large magnetocaloric effect in the antiferromagnetic HoCu{sub 0.33}Ge{sub 2} and ErCu{sub 0.25}Ge{sub 2} compounds

    Energy Technology Data Exchange (ETDEWEB)

    Gao, R.L. [School of Metallurgy and Materials Engineering, Chongqing University of Science and Technology, Chongqing 401331 (China); Xu, Z.Y., E-mail: zhyxu@nim.ac.cn [National Institute of Metrology, Beijing 100029 (China); Wang, L.C. [State Key Laboratory for Magnetism, Institute of Physics, Chinese Academy of Sciences, Beijing 100190 (China); Dong, Q.Y.; Zhang, Y. [Department of Physics, Capital Normal University, Beijing 100048 (China); Liu, F.H. [National Space Science Center, Beijing 100190 (China); Mo, Z.J. [School of material Science and Engineering, Hebei University of Technology, Tianjin 300401 (China); Niu, E. [State Key Laboratory for Magnetism, Institute of Physics, Chinese Academy of Sciences, Beijing 100190 (China); Fu, C.L.; Cai, W.; Chen, G.; Deng, X.L. [School of Metallurgy and Materials Engineering, Chongqing University of Science and Technology, Chongqing 401331 (China)

    2015-05-15

    Highlights: • Antiferromagnetic material RCu{sub x}Ge{sub 2} of high purity was prepared. • Large MCE as −10.2 J/kg K and −10.5 J/kg K for RCu{sub x}Ge{sub 2} (Ho, Er) was obtained for field change of 0–50 kOe. • The RCu{sub x}Ge{sub 2} compounds with variable x had different transition temperature which made them suitable for ‘table-like’ magnetocaloric refrigerant. - Abstract: Magnetic properties and magnetocaloric effect (MCE) of HoCu{sub 0.33}Ge{sub 2} and ErCu{sub 0.25}Ge{sub 2} compounds have been investigated. The compounds were determined to be antiferromagnetic with the Néel temperatures T{sub N} = 9 K and 3.9 K, respectively. The critical transition magnetic fields for the metamagnetic transition from antiferromagnetic to ferromagnetic state below T{sub N} were determined to be 10 kOe for HoCu{sub 0.33}Ge{sub 2} at 5 K and 6 kOe for ErCu{sub 0.25}Ge{sub 2} at 2 K. Large MCE with the maximal values of magnetic entropy changes (ΔS{sub M}) as −10.2 J/kg K at 10.5 K were found in HoCu{sub 0.33}Ge{sub 2} for field changes of 0–70 kOe and −10.5 J/kg K at 5.5 K in ErCu{sub 0.25}Ge{sub 2} for field changes of 0–50 kOe, respectively. The large ΔS{sub M} around T{sub N} as well as no hysteresis loss made RCu{sub x}Ge{sub 2} competitive candidates as low temperature magnetic refrigerant.

  4. The Low Temperature Microgravity Physics Facility Project

    Science.gov (United States)

    Chui, T.; Holmes, W.; Lai, A.; Croonquist, A.; Eraker, J.; Abbott, R.; Mills, G.; Mohl, J.; Craig, J.; Balachandra, B.; hide

    2000-01-01

    We describe the design and development of the Low Temperature Microgravity Physics Facility, which is intended to provide a unique environment of low temperature and microgravity for the scientists to perform breakthrough investigations on board the International Space Station.

  5. Low Temperature Synthesis of Magnesium Aluminate Spinel

    International Nuclear Information System (INIS)

    Lebedovskaya, E.G.; Gabelkov, S.V.; Litvinenko, L.M.; Logvinkov, D.S.; Mironova, A.G.; Odejchuk, M.A.; Poltavtsev, N.S.; Tarasov, R.V.

    2006-01-01

    The low-temperature synthesis of magnesium-aluminum spinel is carried out by a method of thermal decomposition in combined precipitated hydrates. The fine material of magnesium-aluminium spinel with average size of coherent dispersion's area 4...5 nanometers is obtained. Magnesium-aluminum spinel and initial hydrates were investigated by methods of the differential thermal analysis, the x-ray phase analysis and measurements of weight loss during the dehydration and thermal decomposition. It is established that synthesis of magnesium-aluminum spinel occurs at temperature 300 degree C by method of the x-ray phase analysis

  6. Low-temperature transport in ultra-thin tungsten films

    Energy Technology Data Exchange (ETDEWEB)

    Chiatti, Olivio [Neue Materialien, Institut fuer Physik, Humboldt-Univ. Berlin (Germany); London Centre for Nanotechnology, University College London (United Kingdom); Nash, Christopher; Warburton, Paul [London Centre for Nanotechnology, University College London (United Kingdom)

    2012-07-01

    Tungsten-containing films, fabricated by focused-ion-beam-induced chemical vapour deposition, are known to have an enhanced superconducting transition temperature compared to bulk tungsten, and have been investigated previously for film thickness down to 25 nm. In this work, by using ion-beam doses below 50 pC/{mu}m{sup 2} on a substrate of amorphous silicon, we have grown continuous films with thickness below 20 nm. The electron transport properties were investigated at temperatures down to 350 mK and in magnetic fields up to 3 T, parallel and perpendicular to the films. The films in this work are closer to the limit of two-dimensional systems and are superconducting at low temperatures. Magnetoresistance measurements yield upper critical fields of the order of 1 T, and the resulting coherence length is smaller than the film thickness.

  7. The Low-Temperature Inflection Observed in Neutron Scattering Measurements of Proteins Is Due to Methyl Rotation : Direct Evidence Using Isotope Labeling and Molecular Dynamics Simulations

    NARCIS (Netherlands)

    Wood, Kathleen; Tobias, Douglas J.; Kessler, Brigitte; Gabel, Frank; Oesterhelt, Dieter; Mulder, Frans A. A.; Zaccai, Giuseppe; Weik, Martin

    2010-01-01

    There is increasing interest in the contribution of methyl groups to the overall dynamics measured by neutron scattering experiments of proteins. In particular an inflection observed in atomic mean square displacements measured as a function of temperature on high resolution spectrometers (similar

  8. The Low Temperature CFB Gasifier

    DEFF Research Database (Denmark)

    Stoholm, P.; Nielsen, Rasmus Glar; Richardt, K.

    2004-01-01

    straw, animal manure and waste and for co-firing the product gas in existing, e.g. coal fired power plant boilers. The aim is to prevent fouling, agglomeration and high temperature corrosion caused by potassium and chlorine and other fuel components when producing electricity. So far 92 hours......The Low Temperature Circulating Fluidised Bed (LT-CFB) gasification process is described together with the 50 kW and the 500 kW test plants and latest test results. The LT-CFB process is especially developed for medium and large scale (few to >100 MW) gasification of problematic bio-fuels like...... of experiments with the 50 kW test plant with two extremely difficult types of straw has shown low char losses and high retentions of ash including e.g. potassium. Latest 27 hours of experiments with dried, high ash pig- and hen manure has further indicated the concepts high fuel flexibility. The new 500 kW test...

  9. Some examples of a differential calorimeter use for low temperature thermal effects measurement; Quelques exemples d'utilisation d'un calorimetre differentiel a puissance compensee pour des mesures d'anomalies thermiques a basses temperatures

    Energy Technology Data Exchange (ETDEWEB)

    Bochirol, L; Bonjour, E

    1967-07-01

    The principle of a differential calorimeter is briefly described. The apparatus allows a direct and continuous determination of the differential heat-capacity between a sample and a reference, in the range 20 to 600 deg. K approximately. Some examples concerning measurements at low temperatures of reversible or non reversible thermal effects are given. They show the possibilities of the apparatus and are connected with: - detection and measurements of thermal effects associated to structural transformations in elastomers at low temperatures, - measurements of Wigner energy released after neutron irradiations at 77 deg. K for: recrystallized pyro-graphites; high purity iron, aluminium. [French] On decrit brievement le principe d'un calorimetre differentiel qui permet la determination directe et continue de la difference de chaleur specifique apparente entre un echantillon et une reference, dans une gamme de temperatures s'etendant de 20 a 600 deg. K environ. On donne quelques exemples de mesure a basses temperatures d'effets thermiques reversibles ou non reversibles. Ils montrent les possibilites de l'appareillage et concernent: - la detection et la mesure d'effets thermiques associes a des transformations structurales dans des elastomeres a basse temperature, - la mesure du degagement d'energie Wigner apres des irradiations neutroniques a 77 deg. K dans: des pyrographites recristallises; du fer de haute purete et de l'aluminium. (auteurs)

  10. Temperature Measurements in the Magnetic Measurement Facility

    Energy Technology Data Exchange (ETDEWEB)

    Wolf, Zachary

    2010-12-13

    Several key LCLS undulator parameter values depend strongly on temperature primarily because of the permanent magnet material the undulators are constructed with. The undulators will be tuned to have specific parameter values in the Magnetic Measurement Facility (MMF). Consequently, it is necessary for the temperature of the MMF to remain fairly constant. Requirements on undulator temperature have been established. When in use, the undulator temperature will be in the range 20.0 {+-} 0.2 C. In the MMF, the undulator tuning will be done at 20.0 {+-} 0.1 C. For special studies, the MMF temperature set point can be changed to a value between 18 C and 23 C with stability of {+-}0.1 C. In order to ensure that the MMF temperature requirements are met, the MMF must have a system to measure temperatures. The accuracy of the MMF temperature measurement system must be better than the {+-}0.1 C undulator tuning temperature tolerance, and is taken to be {+-}0.01 C. The temperature measurement system for the MMF is under construction. It is similar to a prototype system we built two years ago in the Sector 10 alignment lab at SLAC. At that time, our goal was to measure the lab temperature to {+-}0.1 C. The system has worked well for two years and has maintained its accuracy. For the MMF system, we propose better sensors and a more extensive calibration program to achieve the factor of 10 increase in accuracy. In this note we describe the measurement system under construction. We motivate our choice of system components and give an overview of the system. Most of the software for the system has been written and will be discussed. We discuss error sources in temperature measurements and show how these errors have been dealt with. The calibration system is described in detail. All the LCLS undulators must be tuned in the Magnetic Measurement Facility at the same temperature to within {+-}0.1 C. In order to ensure this, we are building a system to measure the temperature of the

  11. Electrical measurements during magnet construction

    International Nuclear Information System (INIS)

    Sintchak, G.; Ganetis, G.; Cottingham, G.

    1989-01-01

    Throughout the construction phase of the cold mass for SSC magnets, electrical tests are made to determine that no faults in the coil structure have developed. These tests include ones designed to measure turn-to-turn voltage hold-off, hypot tests to ground, coil resistance, and instrumentation checks. These various tests will be described and the test parameters that are used will be covered. 4 figs

  12. Automation of low temperature positron annihilation spectroscopy system

    International Nuclear Information System (INIS)

    Chaturvedi, T.P.; Venkiteswaran, S.; Pujari, P.K.

    1997-01-01

    This paper describes the automation implemented in the low temperature measurements in positron annihilation spectroscopic studies. This has not only widened the scope of the positron research, but also helps achieve result with better precision. (author). 3 refs., 1 fig

  13. Measurement of H and H2 populations in-situ in a low-temperature plasma by vacuum-ultraviolet laser-absorption spectroscopy

    International Nuclear Information System (INIS)

    Schlachter, A.S.; Young, A.T.; Stutzin, G.C.; Stearns, J.W.; Doebele, H.G.; Leung, K.N.; Kunkel, W.B.

    1988-12-01

    A new technique, vacuum-ultraviolet laser-absorption spectroscopy, has been developed to quantitatively determine the absolute density of H and H 2 within a plasma. The technique is particularly well suited to measurement in a plasma, where high charged particle and photon background complicate other methods of detection. The high selectivity and sensitivity of the technique allows for the measurement of the rotational-vibrational state distribution of H 2 as well as the translational temperature of the atoms and molecules. The technique has been used to study both pulsed and continuous H/sup /minus// ion-source plasma discharges. H 2 state distributions in a multicusp ''volume'' H/sup /minus// ion- source plasma show a high degree of internal excitation, with levels up to v = 5 and J = 8 being observed. The method is applicable for a very wide range of plasma conditions. Emission measurements from excited states of H are also reported. 17 refs., 9 figs

  14. Low aperture magnetic elements measurements

    International Nuclear Information System (INIS)

    Aleksandrov, V.A.; Mikhajlichenko, A.A.; Parkhomchuk, V.V.; Seryj, A.A.; Shil'tsev, V.D.

    1991-01-01

    Two new methods of magnetic field measurements in low aperture elements are discussed. The first method uses thin magnetoresistive bismuth wire and the second-strained wire with AC. Principles of measuring used in the last technique are different from well known SLAC method of vibrating wire. Results of testing 0.38 T/mm quadrupole and VLEPP final focus test 3 T/mm lens are presented. Brief comparing of the lens axis determination precision of these methods is also discussed. 4 refs.; 8 figs

  15. Warm measurements of CBA superconducting magnets

    International Nuclear Information System (INIS)

    Engelmann, R.; Herrera, J.; Kahn, S.; Kirk, H.; Willen, E.; Yamin, P.

    1983-01-01

    We present results on magnetic field measurements of CBA dipole magnets in the warm (normal conductor) and cryogenic (superconducting) states. We apply two methods for the warm measurements, a dc and ac method. We find a good correlation between warm and cryogenic measurements which lends itself to a reliable diagnosis of magnet field errors using warm measurements early in the magnet assembly process. We further find good agreement between the two warm measurement methods, both done at low currents

  16. Material Properties at Low Temperature

    International Nuclear Information System (INIS)

    Duthil, P

    2014-01-01

    From ambient down to cryogenic temperatures, the behaviour of materials changes greatly. Mechanisms leading to variations in electrical, thermal, mechanical, and magnetic properties in pure metals, alloys, and insulators are briefly introduced from a general engineering standpoint. Data sets are provided for materials commonly used in cryogenic systems for design purposes

  17. Material Properties at Low Temperature

    CERN Document Server

    Duthil, P

    2014-07-17

    From ambient down to cryogenic temperatures, the behaviour of materials changes greatly. Mechanisms leading to variations in electrical, thermal, mechanical, and magnetic properties in pure metals, alloys, and insulators are briefly introduced from a general engineering standpoint. Data sets are provided for materials commonly used in cryogenic systems for design purposes.

  18. Material Properties at Low Temperature

    Energy Technology Data Exchange (ETDEWEB)

    Duthil, P [Orsay, IPN (France)

    2014-07-01

    From ambient down to cryogenic temperatures, the behaviour of materials changes greatly. Mechanisms leading to variations in electrical, thermal, mechanical, and magnetic properties in pure metals, alloys, and insulators are briefly introduced from a general engineering standpoint. Data sets are provided for materials commonly used in cryogenic systems for design purposes.

  19. Characterization of magnetic phase transitions in PrMn2Ge2 compound investigated by magnetization and hyperfine field measurements

    Directory of Open Access Journals (Sweden)

    B. Bosch-Santos

    2017-05-01

    Full Text Available The magnetic properties of PrMn2Ge2 compound have been investigated by perturbed γ−γ angular correlation (PAC spectroscopy using 111In(111Cd as probe nuclei as well as by magnetization measurements. This ternary intermetallic compound exhibits different magnetic structures depending on the temperature. The magnetic ordering is mainly associated with the magnetic moment of 3d-Mn sublattice but at low temperatures a magnetic contribution due to ordering of the magnetic moment from 4f-Pr sublattice appears. PAC results with 111Cd probe nuclei at Mn sites show that the temperature dependence of hyperfine field Bhf(T follows the expected behavior for the host magnetization, which could be fitted by two Brillouin functions, one for antiferromagnetic phase and the other for ferromagnetic phase, associated with the magnetic ordering of Mn ions. Magnetization measurements showed the magnetic behavior due to Mn ions highlighting the antiferromagnetic to ferromagnetic transition around 326 K and an increase in the magnetization around 36 K, which is ascribed to Pr ions ordering.

  20. R&D ERL: Magnetic measurements of the ERL magnets

    Energy Technology Data Exchange (ETDEWEB)

    Jain, A.

    2010-08-01

    The magnet system of ERL consists of G5 solenoids, 6Q12 quadrupoles with 0.58 T/m gradient, 3D60 dipoles with 0.4 T central field, 15 and 30 degree Z-bend injection line dipole/quadrupole combined function magnets, and extraction line magnets. More details about the magnets can be found in a report by G. Mahler. Field quality in all the 6Q12 quadrupoles, 3D60 dipoles and the injection line magnets has been measured with either a rotating coil, or a Hall probe mapper. This report presents the results of these magnetic measurements.

  1. Low temperature kinetics of In-Cd solid solution decomposition

    Czech Academy of Sciences Publication Activity Database

    Pal-Val, P.P.; Pal-Val, L.N.; Ostapovets, A.A.; Vaněk, Přemysl

    2008-01-01

    Roč. 137, - (2008), s. 35-42 ISSN 1012-0394 Institutional research plan: CEZ:AV0Z10100520 Keywords : low temperatures * In-based alloys * solid solutions * isothermal structure instability * Young's modulus * electrical resistivity * phase diagrams Subject RIV: BM - Solid Matter Physics ; Magnetism http://www.scientific.net/3-908451-53-1/35/

  2. Low temperature heat capacity of scandium and alloys of scandium

    Energy Technology Data Exchange (ETDEWEB)

    Tsang, T. W.E.

    1977-12-01

    The heat capacity of three electrotransport purified scandium samples has been measured from 1 to 20/sup 0/K. The resultant electronic specific heat constant and Debye temperature are 10.337 +- 0.015 mJ/gm-atom K/sup 2/ and 346.7 +- 0.8/sup 0/K respectively, and these values are believed to be truly representative of intrinsic scandium. Alloying studies have also been carried out to investigate the band structure of scandium based on the rigid band model, with zirconium to raise the electron concentration and magnesium to lower it. The results are then compared to the theoretical band structure calculations. Low temperature heat capacity measurements have also been made on some dilute Sc-Fe alloys. An anomaly is observed in the C/T vs. T/sup 2/ plot, but the C vs. T curve shows no evidence of magnetic ordering down to 1/sup 0/K, and electrical resistance measurement from 4 to 0.3/sup 0/K also indicates that no magnetic ordering took place.

  3. Low temperature heat capacity measurements of the spin-liquid states of hydrogenated and deuterated κ-(BEDT-TTF)2Cu2(CN)3

    International Nuclear Information System (INIS)

    Yamashita, S.; Yamamoto, T.; Nakazawa, Y.

    2010-01-01

    Heat capacity measurements of organic triangular lattice compound κ-(BEDT-TTF) 2 Cu 2 (CN) 3 were performed to discuss the low energy excitations from the spin-liquid ground states. Existence of the T-linear electronic coefficient with finite electronic heat capacity coefficient γ was confirmed in three different samples from different batches, although small sample dependence was observed in the absolute values of the heat capacities. Concerning the sample in which hydrogen atoms in ethylene group in BEDT-TTF molecule have been substituted by deuterons, we have observed almost similar thermodynamic behavior as the hydrogenated sample. The absence of drastic change of electronic properties of this compound is consistent with the electronic phase diagram given by Kurosaki et al. [11] (Phys. Rev. Lett. 95 (2005) 17001). The obtained data are well consistent with the previous heat capacity experiments. The existence of the γ term demonstrates that the excitations from the quantum spin-liquid states show a gapless behavior at least down to 0.7 K.

  4. Magnetic measurements inside the Omicron magnet.

    CERN Multimedia

    1977-01-01

    The multipurpose detection system (Omicron) built at the SC in the late seventies in the Proton Hall made use of the large aperture magnet (on loan from Rutherford Lab, 85 cm gap height, 1 m width, 1.8 m length, 1 Tesla peak field). See CERN Courier 17 (1977) p. 61.

  5. Characterization of the low-temperature triplet state of chlorophyll in photosystem II core complexes: Application of phosphorescence measurements and Fourier transform infrared spectroscopy.

    Science.gov (United States)

    Zabelin, Alexey A; Neverov, Konstantin V; Krasnovsky, Alexander A; Shkuropatova, Valentina A; Shuvalov, Vladimir A; Shkuropatov, Anatoly Ya

    2016-06-01

    Phosphorescence measurements at 77 K and light-induced FTIR difference spectroscopy at 95 K were applied to study of the triplet state of chlorophyll a ((3)Chl) in photosystem II (PSII) core complexes isolated from spinach. Using both methods, (3)Chl was observed in the core preparations with doubly reduced primary quinone acceptor QA. The spectral parameters of Chl phosphorescence resemble those in the isolated PSII reaction centers (RCs). The main spectral maximum and the lifetime of the phosphorescence corresponded to 955±1 nm and of 1.65±0.05 ms respectively; in the excitation spectrum, the absorption maxima of all core complex pigments (Chl, pheophytin a (Pheo), and β-carotene) were observed. The differential signal at 1667(-)/1628(+)cm(-1) reflecting a downshift of the stretching frequency of the 13(1)-keto C=O group of Chl was found to dominate in the triplet-minus-singlet FTIR difference spectrum of core complexes. Based on FTIR results and literature data, it is proposed that (3)Chl is mostly localized on the accessory chlorophyll that is in triplet equilibrium with P680. Analysis of the data suggests that the Chl triplet state responsible for the phosphorescence and the FTIR difference spectrum is mainly generated due to charge recombination in the reaction center radical pair P680(+)PheoD1(-), and the energy and temporal parameters of this triplet state as well as the molecular environment and interactions of the triplet-bearing Chl molecule are similar in the PSII core complexes and isolated PSII RCs. Copyright © 2016 Elsevier B.V. All rights reserved.

  6. Recent developments in magnet measuring techniques

    International Nuclear Information System (INIS)

    Billan, J.; Henrichsen, K.N.; Walckiers, L.

    1985-01-01

    The main problems related to magnetic measurements of particle accelerator components are discussed. Measurements of the properties of magnetic materials as well as the measurements of field distribution in the electromagnets for the Large Electron-Positron Collider (LEP) are illustrated. The fluxmeter method is extensively employed in this work. The impact of recent advances in electronic technology on measurement techniques is explained. Magnetic measurements (including the harmonic coil method) can be performed with improved accuracy applying modern technology to the classical methods. New methods for the non-destructive testing of magnetic materials and for the measurement of magnetic geometry are described. (orig.) [de

  7. Development of decay energy spectroscopy using low temperature detectors.

    Science.gov (United States)

    Jang, Y S; Kim, G B; Kim, K J; Kim, M S; Lee, H J; Lee, J S; Lee, K B; Lee, M K; Lee, S J; Ri, H C; Yoon, W S; Yuryev, Y N; Kim, Y H

    2012-09-01

    We have developed a high-resolution detection technique for measuring the energy and activity of alpha decay events using low-temperature detectors. A small amount of source material containing alpha-emitting radionuclides was enclosed in a 4π metal absorber. The energy of the alpha particles as well as that of the recoiled nuclides, low-energy electrons, and low-energy x-rays and γ-rays was converted into thermal energy of the gold absorber. A metallic magnetic calorimeter serving as a fast and sensitive thermometer was thermally attached to the metal absorber. In the present report, experimental demonstrations of Q spectroscopy were made with a new meander-type magnetic calorimeter. The thermal connection between the temperature sensor and the absorber was established with annealed gold wires. Each alpha decay event in the absorber resulted in a temperature increase of the absorber and the temperature sensor. Using the spectrum measured for a drop of (226)Ra solution in a 4π gold absorber, all of the alpha emitters in the sample were identified with a demonstration of good detector linearity. The resolution of the (226)Ra spectrum showed a 3.3 keV FWHM at its Q value together with an expected gamma escape peak at the energy shifted by its γ-ray energy. Copyright © 2012 Elsevier Ltd. All rights reserved.

  8. Comparative study of magnetic ordering in bulk and nanoparticles of Sm{sub 0.65}Ca{sub 0.35}MnO{sub 3}: Magnetization and electron magnetic resonance measurements

    Energy Technology Data Exchange (ETDEWEB)

    Goveas, Lora Rita, E-mail: loragoveas@gmail.com [Department of Physics, Dr. Ambedkar Institute of Technology, Bangalore 560056 (India); St. Joseph' s College of Arts and Science, Bangalore 560027 (India); Anuradha, K. N. [Department of Physics, Dr. Ambedkar Institute of Technology, Bangalore 560056 (India); Bhagyashree, K. S.; Bhat, S. V. [Department of Physics, Indian Institute of Science, Bangalore 560012 (India)

    2015-05-07

    To explore the effect of size reduction to nanoscale on the hole doped Sm{sub 0.65}Ca{sub 0.35}MnO{sub 3} compound, dc magnetic measurements and electron magnetic resonance (EMR) were done on bulk and nanoparticle samples in the temperature range 10 ≤ T ≤ 300 K. Magnetization measurement showed that the bulk sample undergoes a charge ordering transition at 240 K and shows a mixed magnetic phase at low temperature. However, the nanosample underwent a ferromagnetic transition at 75 K, and the charge ordered state was destabilized on size reduction down to nanoscale. The low-temperature ferromagnetic component is found to be enhanced in nanoparticles as compared to their bulk counterpart. Interestingly around room temperature, bulk particles show higher magnetization where as at low temperature nanoparticles show higher magnetization. Ferromagnetism in the bulk is due to super exchange where as ferromagnetism in nanoparticles is due to uncompensated spins of the surface layer. Temperature variation of EMR parameters correlates well with the results of magnetic measurements. The magnetic behaviour of the nanoparticles is understood in terms of the core shell scenario.

  9. Low-temperature specific heat of YMn sub 2 in the paramagnetic and antiferromagnetic phases

    Energy Technology Data Exchange (ETDEWEB)

    Fisher, R.A.; Emerson, J.P.; Phillips, N.E. (Lawrence Berkeley Lab., CA (United States)); Ballou, R.; Lelievre-Berna, E. (Centre National de la Recherche Scientifique (CNRS), 38 - Grenoble (France). Lab. Louis Neel)

    1992-07-01

    The low-temperature specific heat of YMn{sub 2} has been measured at applied pressures of 0 to 7.7 kbar. A paramagnetic state is stabilized for moderate values of the applied pressure (of the order of 1.6 kbar). A large linear term in the specific heat, which decreases regularly with increasing pressure, is observed in this phase. It is ascribed to giant spin fluctuations associated with a magnetic-non magnetic instability and a strong geometrical spin frustration.

  10. Magneto-optical Kerr-effect at low temperatures. Investigation of superconductor/ferromagnet heterostructures

    Energy Technology Data Exchange (ETDEWEB)

    Zahn, Patrick; Bayer, Jonas [Max Planck Institute for Intelligent Systems, Heisenbergstrasse 3, 70569 Stuttgart (Germany); Institute for Innovative Surfaces FINO, Aalen University, Beethovenstrasse 1, 73430 Aalen (Germany); Stahl, Claudia; Ruoss, Stephen; Graefe, Joachim; Schuetz, Gisela [Max Planck Institute for Intelligent Systems, Heisenbergstrasse 3, 70569 Stuttgart (Germany); Albrecht, Joachim [Institute for Innovative Surfaces FINO, Aalen University, Beethovenstrasse 1, 73430 Aalen (Germany)

    2016-07-01

    With XMCD microscopy it is possible to visualize the critical current density of the superconductor YBCO with high spatial resolution. Therefore, soft magnetic CoFeB is introduced as sensor layer. The magnetic stray fields of the supercurrents lead to a local reorientation of the magnetic moments in the ferromagnet, which are then imaged via X-ray microscopy. These experiments have to be carried out at the scanning X-ray microscope MAXYMUS at the synchrotron Bessy II in Berlin. For that purpose pre-characterization of the sensor is highly desirable: Magnetic interactions between the superconductor and the ferromagnetic sensor layer have been investigated at low temperatures using Kerr-effect measurements. Therefore hysteresis loops are obtained by a sophisticated magnet and field ramping setup within the NanoMOKE3 system. The results are used to optimize the ferromagnetic sensor layer for XMCD microscopy of superconductors.

  11. Magnetic field measurements and mapping techniques

    CERN Multimedia

    CERN. Geneva

    2003-01-01

    These lectures will present an overview of the most common techniques used for the measurement of magnetic field in accelerator magnets. The formalism for a harmonic description of the magnetic field will be presented, including a discussion of harmonics allowed under various types of symmetries in the magnet. The harmonic coil technique for measurement of field harmonics will be covered in depth. Using examples from recent projects, magnetic measurements will be shown to be a powerful tool for monitoring magnet production. Measurements of magnetic axis using extensions of the harmonic coil technique, as well as other techniques, such as the colloidal cell and stretched wire, will be covered. Topics of interest in superconducting magnets, such as time decay and snapback, requiring relatively fast measurements of the harmonics, will also be described.

  12. Study of the magnetic heavy fermions UCoGe and YbRh2Si2 by transport measurements

    International Nuclear Information System (INIS)

    Taupin, Mathieu

    2013-01-01

    Thermal conductivity measurements have been performed at low temperatures and under field in the superconducting ferromagnetic UCoGe and in the weak antiferromagnetic YbRh 2 S i 2. In both systems, the magnetic fluctuations have an important role in their properties, and it appeared that they contribute as a heat channel, seen by thermal conductivity at low temperatures. In UCoGe, the extra contribution due to the magnetic fluctuations have the same field dependence as the one measured by NMR, and, unexpectedly, a new heat channel appears at very low temperatures. Furthermore, thermal conductivity measurements in the superconducting state have confirmed the multi-gap superconductivity of UCoGe. XMCD measurements have also been performed in UCoGe. In YbRh 2 Si 2 , the very low temperature thermal conductivity measurements have shown that an extra contribution appears at very low temperature, which avoids to conclude de n itively about the violation or the validation of the Wiedemann-Franz law at the quantum critical point, even if the results can be interpreted supposing its validation. (author) [fr

  13. Measurement system for SSRF pulsed magnets

    International Nuclear Information System (INIS)

    Peng Chengcheng; Gu Ming; Liu Bo; Ouyang Lianhua

    2007-01-01

    This paper describes the magnetic field measurement system for pulsed magnets in SSRF. The system consists of magnetic probes, analog active integrator, oscilloscope, stepper motor and a controller. An application program based on LabVIEW has been developed as main control unit. After the magnetic field mapping of a septum magnet prototype, it is verified that the test results accord with the results of theoretical calculation and computer simulation. (authors)

  14. Recrystallization of magnesium deformed at low temperatures

    International Nuclear Information System (INIS)

    Fromageau, R.; Pastol, J.L.; Revel, G.

    1978-01-01

    The recrystallization of magnesium was studied after rolling at temperatures ranging between 248 and 373 K. For zone refined magnesium the annealing behaviour as observed by electrical resistivity measurements showed two stages at about 250 K and 400 K due respectively to recrystallization and grain growth. The activation energy associated with the recrystallization stage was 0.75 +- 0.01 eV. In less pure magnesium, with nominal purity 99.99 and 99.9%, the recrystallization stage was decomposed into two substages. Activation energies were determined in relation with deformation temperature and purity. The magnesium of intermediate purity (99.99%) behaved similarly to the lowest purity metal when it was deformed at high temperature and to the purest magnesium when the deformation was made at low temperature. This behaviour was discussed in connection with the theories of Luecke and Cahn. (Auth.)

  15. Measurements of Solar Vector Magnetic Fields

    Science.gov (United States)

    Hagyard, M. J. (Editor)

    1985-01-01

    Various aspects of the measurement of solar magnetic fields are presented. The four major subdivisions of the study are: (1) theoretical understanding of solar vector magnetic fields; (3) techniques for interpretation of observational data; and (4) techniques for data display.

  16. Measurements of Solar Vector Magnetic Fields

    International Nuclear Information System (INIS)

    Hagyard, M.J.

    1985-05-01

    Various aspects of the measurement of solar magnetic fields are presented. The four major subdivisions of the study are: (1) theoretical understanding of solar vector magnetic fields; (3) techniques for interpretation of observational data; and (4) techniques for data display

  17. Development of a highly efficient conversion electron Moessbauer spectroscopy (CEMS) detector for low temperature (<20 K) measurements and tests on Fe / (Eu{sub x}Pb{sub 1-x})Te bilayers; Desenvolvimento de um detector de alta eficiencia para espectroscopia Moessbauer de eletrons de conversao (CEMS) a baixas temperaturas (<20K) e testes em bicamadas Fe / (Eu{sub x}Pb{sub 1-x})Te

    Energy Technology Data Exchange (ETDEWEB)

    Pombo, Carlos Jose da Silva Matos

    2006-07-01

    The {sup 57}Fe Moessbauer spectroscopy is a nuclear, non-destructive technique used for the investigation of structural, magnetic and hyperfine properties of several materials. It is a powerful tool in characterizing materials in physics, metallurgy, geology and biology field areas, especially magnetic materials, alloys and minerals containing Fe. Lately, the Conversion Electron Moessbauer Spectroscopy (CEMS) is widely used in making studies on ultra-thin magnetic films, as well as other nanostructured materials. In case of magnetic nanostructures, low temperature (LT) studies are especially important due to the possibility of dealing with superparamagnetic effects. In this work it was developed a CEMS measurement system for low temperatures (<20 K) based on a solid-state electron multiplier (Channeltron{sup R}) and an optical cryostat (Model SVT-400, Janis Research Co, USA), from which the project was originally conceived at the Applied Physics / Moessbauer spectroscopy Department from University of Duisburg-Essen, Germany. The LT-CEMS system was fully built, tested and successfully applied in a preliminary characterization of Fe/(Eu{sub x}Pb{sub 1-x})Te(111) bilayers with use of a 15 angstrom, {sup 57} Fe probe layer, with reasonable results at sample temperatures as low as 8 K. (author)

  18. Radically Different Kinetics at Low Temperatures

    Science.gov (United States)

    Sims, Ian

    2014-06-01

    The use of the CRESU (Cinétique de Réaction en Ecoulement Supersonique Uniforme, or Reaction Kinetics in Uniform Supersonic Flow) technique coupled with pulsed laser photochemical kinetics methods has shown that reactions involving radicals can be very rapid at temperatures down to 10 K or below. The results have had a major impact in astrochemistry and planetology, as well as proving an exacting test for theory. The technique has also been applied to the formation of transient complexes of interest both in atmospheric chemistry and combustion. Until now, all of the chemical reactions studied in this way have taken place on attractive potential energy surfaces with no overall barrier to reaction. The F + H2 {→} HF + H reaction does possess a substantial energetic barrier ({\\cong} 800 K), and might therefore be expected to slow to a negligible rate at very low temperatures. In fact, this H-atom abstraction reaction does take place efficiently at low temperatures due entirely to tunneling. I will report direct experimental measurements of the rate of this reaction down to a temperature of 11 K, in remarkable agreement with state-of-the-art quantum reactive scattering calculations by François Lique (Université du Havre) and Millard Alexander (University of Maryland). It is thought that long chain cyanopolyyne molecules H(C2)nCN may play an important role in the formation of the orange haze layer in Titan's atmosphere. The longest carbon chain molecule observed in interstellar space, HC11N, is also a member of this series. I will present new results, obtained in collaboration with Jean-Claude Guillemin (Ecole de Chimie de Rennes) and Stephen Klippenstein (Argonne National Labs), on reactions of C2H, CN and C3N radicals (using a new LIF scheme by Hoshina and Endo which contribute to the low temperature formation of (cyano)polyynes. H. Sabbah, L. Biennier, I. R. Sims, Y. Georgievskii, S. J. Klippenstein, I. W. M. Smith, Science 317, 102 (2007). S. D. Le Picard, M

  19. Low temperature study of nonstoichiometric titanium carbide

    International Nuclear Information System (INIS)

    Tashmetov, M.Yu.

    2005-05-01

    By low temperature neutron diffraction method was studied structure in nonstoichiometric titanium carbide from room temperature up to 12K. It is found of low temperature phase in titanium carbide- TiC 0.71 . It is established region and borders of this phase. It is determined change of unit cell parameter. (author)

  20. Low-temperature plasma modelling and simulation

    NARCIS (Netherlands)

    Dijk, van J.

    2011-01-01

    Since its inception in the beginning of the twentieth century, low-temperature plasma science has become a major ¿eld of science. Low-temperature plasma sources and gas discharges are found in domestic, industrial, atmospheric and extra-terrestrial settings. Examples of domestic discharges are those

  1. High pressure apparatus for neutron scattering at low temperature

    International Nuclear Information System (INIS)

    Munakata, Koji; Uwatoko, Yoshiya; Aso, Naofumi

    2010-01-01

    Effects of pressure on the physical properties are very important for understanding highly correlated electron systems, in which pressure-induced attractive phenomena such as superconductivity and magnetically ordered non-Fermi liquid have been observed. Up to now, many scientists have developed a lot of high pressure apparatus for each purpose. The characteristic features of various materials and pressure transmitting media for use of high pressure apparatus are reported. Then, two kinds of clamp type high-pressure cell designed for low-temperature neutron diffraction measurements are shown; one is a piston cylinder type high-pressure cell which can be attached to the dilution refrigerator, and the other one is a newly-developed cubic anvil type high-pressure cell which can generate pressure above 7GPa. We also introduce the results of magnetic neutron scattering under pressure on a pressure-induced superconducting ferromagnet UGe 2 in use of the piston cylinder type clamp cell, and those on an iron arsenide superconductor SrFe 2 As 2 in use of the cubic anvil type clamp cell. (author)

  2. Accurate method of the magnetic field measurement of quadrupole magnets

    International Nuclear Information System (INIS)

    Kumada, M.; Sakai, I.; Someya, H.; Sasaki, H.

    1983-01-01

    We present an accurate method of the magnetic field measurement of the quadrupole magnet. The method of obtaining the information of the field gradient and the effective focussing length is given. A new scheme to obtain the information of the skew field components is also proposed. The relative accuracy of the measurement was 1 x 10 -4 or less. (author)

  3. Measurements of magnetic field sources in schools

    International Nuclear Information System (INIS)

    Johnson, G.B.

    1992-01-01

    The Electrical Systems Division of the Electric Power Research Institute (EPRI) has initiated several research projects to investigate magnetic field levels, their characteristics, and their sources. This paper describes measurements of magnetic field sources in schools. Magnetic field measurements were made at four schools in the service areas of two utility companies. Magnetic field measurements included profiles of the magnetic field versus distance near power lines, around the perimeter of the school buildings, and at several locations within each school. Twenty-four hour measurements were also made to record the temporal variation of the magnetic field at several locations at each school. The instrumentation, measurement techniques, and magnetic field sources identified are discussed

  4. Magnetic Field Measurements of the GOLIATH Magnet in EHN1

    CERN Document Server

    Rosenthal, Marcel; Chatzidaki, Panagiota; Margraf, Rachel; Wilkens, Henric; Bergsma, Felix; Giudici, Pierre-Ange; CERN. Geneva. ATS Department

    2018-01-01

    This note describes the measurement campaign of the magnetic field of the GOLIATH magnet conducted in 2017. It documents the applied measurement procedure and the consecutive analysis of the recorded data. The shape of the magnetic field along the beam axis is discussed and compared with a previous measurement taken in the 1980s. Overall a very good agreement of both data sets is observed. The integrated vertical magnetic field is obtained by analytical descriptions fitted to the data. Additionally, the influence of different configurations of the power converters, as for example in the case of a differ- ent powering scheme of the upper and lower coil of the GOLIATH magnet, on the magnetic field are discussed.

  5. A dynamic method for magnetic torque measurement

    Science.gov (United States)

    Lin, C. E.; Jou, H. L.

    1994-01-01

    In a magnetic suspension system, accurate force measurement will result in better control performance in the test section, especially when a wider range of operation is required. Although many useful methods were developed to obtain the desired model, however, significant error is inevitable since the magnetic field distribution of the large-gap magnetic suspension system is extremely nonlinear. This paper proposed an easy approach to measure the magnetic torque of a magnetic suspension system using an angular photo encoder. Through the measurement of the velocity change data, the magnetic torque is converted. The proposed idea is described and implemented to obtain the desired data. It is useful to the calculation of a magnetic force in the magnetic suspension system.

  6. Magnetic measurements at Lawrence Berkeley Laboratory

    International Nuclear Information System (INIS)

    Green, M.I.; Barale, P.; Callapp, L.; Case-Fortier, M.; Lerner, D.; Nelson, D.; Schermer, R.; Skipper, G.; Van Dyke, D.; Cork, C.; Halbach, K.; Hassenzahl, W.; Hoyer, E.; Marks, S.; Harten, T.; Luchini, K.; Milburn, J.; Tanabe, J.; Zucca, F.; Keller, R.; Selph, F.; Gilbert, W.; Green, M.A.; O'Neil, J.; Schafer, R.; Taylor, C.; Greiman, W.; Hall, D.; MacFarlane, J.

    1991-08-01

    Recent magnetic measurement activities at LBL have been concentrated in two separate areas, electro-magnets and permanent magnets for the Advanced Light Source (ALS), and superconducting magnets for the Superconducting Super Collider Laboratory (SSCL). A survey of the many different measurement systems is presented. These include: AC magnetic measurements of an ALS booster dipole engineering model magnet, dipole moment measurements of permanent magnet blocks for ALS wigglers and undulators, permeability measurements of samples destined for wiggler and undulator poles, harmonic error analysis of SSC one meter model dipoles and quadrupoles and five meter long SSC prototype quadrupoles, harmonic error analysis of ALS dipoles, quadrupoles, and sextupoles, precision Hall probe mapping of ALS storage ring combined function magnets, and the design of the ALS insertion device magnets mapping system. We also describe a new UNIX based data acquisition system that is being developed for the SSC. Probes used for magnetic measurements include Helmholtz coils, integral coils, point coils, and bucking harmonic analysis coils, several different types of Hall probes, and nuclear magnetic resonance magnetometers. Both analog and digital integrators are used with the coils. Some problems that occurred and their rectification is described. The mechanisms used include rotating systems with optical encoders, X-Y mapping systems with optical encoders and a laser position measuring device. 10 refs., 3 figs., 1 tab

  7. Study of room temperature Raman scattering and XPS, high temperature electrical and low temperature magnetic properties of Zn1−yLiyO (0.00 ≤y≤ 0.10) nanoparticles

    KAUST Repository

    Awan, Saif Ullah

    2015-10-15

    Multiferroics are potentially future materials in spintronics for memory and data storage applications. In this paper, a series of Li-doped nanoparticles were studied to investigate the effects of Li on the physical properties of the ZnO system. Analysis of structural micrographs and Raman spectra confirmed the wurtzite structure of doped samples. The vibrational modes of Zinc and oxygen atoms were labeled as E and E with an additional mode at 134 cm in the doped samples. We observed the presence of interstitial and substitutional Li defects from the deconvolution of Li 1s core level spectra using high resolution x-ray photoelectron spectroscopy. The approximated measured values (e.g., for y = 0.04 and 0.08 samples) for interstitial Li defects were 27% and 39%, and for substitutional Li defects were 73% and 61% respectively. For the y = 0.06 composition, dc resistivity was the highest, while the transition temperature (measured from dielectric loss) was the lowest. We observed a non-monotonic trend of saturation magnetization (obtained at 50 K) against the Li concentration. The compositions having the highest magnetic moment were those having higher interstitial Li defects and lower dc resistivity. Higher hole carrier concentrations and dielectric transition temperatures were correlated with the higher magnetization. Interstitial Li defects played a key role in stabilizing more cationic Zn vacancies. Hole carriers were the major cause of long-range ferromagnetic order in these nanoparticles.

  8. Study of room temperature Raman scattering and XPS, high temperature electrical and low temperature magnetic properties of Zn1−yLiyO (0.00 ≤y≤ 0.10) nanoparticles

    KAUST Repository

    Awan, Saif Ullah; Hasanain, S. K.; Mehmood, Zahid; Anjum, Dalaver H.; Shah, Saqlain A.; Aftab, M.; Abbas, Turab Ali

    2015-01-01

    Multiferroics are potentially future materials in spintronics for memory and data storage applications. In this paper, a series of Li-doped nanoparticles were studied to investigate the effects of Li on the physical properties of the ZnO system. Analysis of structural micrographs and Raman spectra confirmed the wurtzite structure of doped samples. The vibrational modes of Zinc and oxygen atoms were labeled as E and E with an additional mode at 134 cm in the doped samples. We observed the presence of interstitial and substitutional Li defects from the deconvolution of Li 1s core level spectra using high resolution x-ray photoelectron spectroscopy. The approximated measured values (e.g., for y = 0.04 and 0.08 samples) for interstitial Li defects were 27% and 39%, and for substitutional Li defects were 73% and 61% respectively. For the y = 0.06 composition, dc resistivity was the highest, while the transition temperature (measured from dielectric loss) was the lowest. We observed a non-monotonic trend of saturation magnetization (obtained at 50 K) against the Li concentration. The compositions having the highest magnetic moment were those having higher interstitial Li defects and lower dc resistivity. Higher hole carrier concentrations and dielectric transition temperatures were correlated with the higher magnetization. Interstitial Li defects played a key role in stabilizing more cationic Zn vacancies. Hole carriers were the major cause of long-range ferromagnetic order in these nanoparticles.

  9. Magnetic field measurements of the superEBIS superconducting magnet

    International Nuclear Information System (INIS)

    Herschcovitch, A.; Kponou, A.; Clipperton, R.; Hensel, W.; Usack, F.

    1994-01-01

    SuperEBIS was designed to have a solenoidal magnetic field of a 5 Tesla strength with a 120 cm long bore. The field was specified to be straight within 1 part in 10000 within the bore, and uniform to within 1 part in 1000 within the central 90 cm. Magnetic field measurements were performed with a computerized magnetic field measuring setup that was borrowed from W. Sampson's group. A preliminary test was made of a scheme to determine if the magnetic and mechanical axes of the solenoid coincided, and, if not, by how much

  10. Magnet measuring equipment of SC2

    CERN Multimedia

    CERN PhotoLab

    1974-01-01

    Checking the positioning of the magnet measuring equipment installed between the poles of SC2. The steel structure in front of the magnet is designed to house the rotary condenser and to shield it from the stray magnetic field of the accelerator.

  11. Magnet measuring equipment of SC2

    CERN Multimedia

    1974-01-01

    Checking the positioning of the magnet measuring equipment installed between the poles of SC2. The steel structure in front of the magnet is designed to house the rotary condenser and to shield it from the stray magnetic field of the accelerator. On the left, Marinus van Gulik. (See Photo Archive 7402005 and Annual Report 1974, p. 44.)

  12. Improved Low Temperature Performance of Supercapacitors

    Science.gov (United States)

    Brandon, Erik J.; West, William C.; Smart, Marshall C.; Gnanaraj, Joe

    2013-01-01

    Low temperature double-layer capacitor operation enabled by: - Base acetonitrile / TEATFB salt formulation - Addition of low melting point formates, esters and cyclic ethers center dot Key electrolyte design factors: - Volume of co-solvent - Concentration of salt center dot Capacity increased through higher capacity electrodes: - Zeolite templated carbons - Asymmetric cell designs center dot Continuing efforts - Improve asymmetric cell performance at low temperature - Cycle life testing Motivation center dot Benchmark performance of commercial cells center dot Approaches for designing low temperature systems - Symmetric cells (activated carbon electrodes) - Symmetric cells (zeolite templated carbon electrodes) - Asymmetric cells (lithium titanate/activated carbon electrodes) center dot Experimental results center dot Summary

  13. Low temperature Moessbauer study of amorphous Fe83B17

    International Nuclear Information System (INIS)

    Miglierini, M.; Sitek, J.

    1987-01-01

    Information about changes in magnetic structures of metallic glass Fe 83 B 17 at low temperatures has been obtained by 57 Fe Moessbauer spectroscopy in the temperature range from 295 to 77 K. The mean values of the magnetic hyperfine field have been calculated from magnetic splitting of Moessbauer spectra. The angle between the direction of magnetization and the γ-ray direction θ obtained from line intensity ratios is given as a function of temperature. The curve shows a minimum at 120 K. The influence of decreasing temperature on the magnetic structure may be caused by a change in magnetic anisotropy and a reorientation of surface spins. The main contribution to the changes in θ comes from the reorientation of surface domains

  14. LOW TEMPERATURE CATHODE SUPPORTED ELECTROLYTES

    Energy Technology Data Exchange (ETDEWEB)

    Harlan U. Anderson; Wayne Huebner; Igor Kosacki

    2001-09-30

    endeavors have lead us to a solution which we think is quite unique and should allow us to obtain flaw free dense films of thickness in the 0.5 to 5 {micro}m range at processing temperatures {le} 900{sup o}. The process involves the deposition of a slurry of nanocrystalline YSZ onto a presintered porous LSM substrate. The key element in the deposition is that the slurry contains sufficient YSZ polymer precursor to allow adhesion of the YSZ particles to each other and the surface after annealing at about 600 C. This allows the formation of a porous film of 0.5 to 5 {micro}m thick which adheres to the surface. After formation of this film, YSZ polymer precursor is allowed to impregnate the porous surface layer (capillary forces tend to confine the polymer solution in the nanoporous layer). After several impregnation/heat treatment cycles, a dense film results. Within the next few months, this process should be developed to the point that single cell measurements can be made on 0.5 to 5 {micro}m films on a LSM substrate. This type of processing allows the formation of essentially flaw free films over areas > 1 cm{sup 2}.

  15. Magnetic susceptibility measurements of σ plutonium alloys. Contribution to the study of the 5f electrons localization in the plutonium

    International Nuclear Information System (INIS)

    Meot-Reymond, S.

    1996-01-01

    Physical properties of actinide metals are essentially ruled by the 5f electrons localization. From a theoretically point of view, this localization is more important in the δ-phase than in the α-one. To compare their magnetic behaviour, low temperature magnetic susceptibility measurements have been performed and previous-resistivity data have been analysed. Experimental results and theoretical data can be conciliate by the existence of a Kondo effect in the δ-Pu phase. (author)

  16. Magnetic measurements at Lawrence Berkeley Laboratory

    International Nuclear Information System (INIS)

    Green, M.I.; Barale, P.; Callapp, L.; Case-Fortier, M.; Lerner, D.; Nelson, D.; Schermer, R.; Skipper, G.; Van Dyke, D.; Cork, C.

    1992-01-01

    Recent magnetic measurement activities at LBL have been concentrated in two separate areas, electro-magnets and permanent magnets for the Advanced Light Source (ALS), and superconducting magnets for the Superconducting Super Collider Laboratory (SSCL). In this paper a survey of the many different measurement systems is presented. These include: AC magnetic measurements of an ALS booster dipole engineering model magnet, dipole moment measurements of permanent magnet blocks for ALS wigglers and undulators, permeability measurements of samples destined for wiggler and undulator poles, harmonic error analysis of SSC one meter model dipoles and quadrupoles and five meter long SSC prototype quadrupoles, harmonic error analysis of ALS dipoles, quadrupoles, and sextupoles, precision Hall probe mapping of ALS design of the ALS insertion device magnetic mapping system. The authors also describe a new UNIX based data acquisition system that is being developed for the SSC. Probes used for magnetic measurements include Helmholtz coils, integral coils, point coils, and bucking harmonic analysis coils, several different types of Hall probes, and nuclear magnetic resonance magnetometers

  17. Low-temperature strain gauges based on silicon whiskers

    Directory of Open Access Journals (Sweden)

    Druzhinin A. A.

    2008-08-01

    Full Text Available To create low-temperature strain gauges based on p-type silicon whiskers tensoresistive characteristics of these crystals in 4,2—300 K temperature range were studied. On the basis of p-type Si whiskers with different resistivity the strain gauges for different materials operating at cryogenic temperatures with extremely high gauge factor at 4,2 K were developed, as well as strain gauges operating at liquid helium temperatures in high magnetic fields.

  18. The on-line low temperature nuclear orientation facility NICOLE

    International Nuclear Information System (INIS)

    Ohtsubo, T; Roccia, S; Gaulard, C; Stone, N J; Stone, J R; Köster, U; Nikolov, J; Veskovic, M; Simpson, G S

    2017-01-01

    We review major experiments and results obtained by the on-line low temperature nuclear orientation method at the NICOLE facility at ISOLDE, CERN since the year 2000 and highlight their general physical impact. This versatile facility, providing a large degree of controlled nuclear polarization, was used for a long-standing study of magnetic moments at shell closures in the region Z  = 28, N  = 28–50 but also for dedicated studies in the deformed region around A  ∼ 180. Another physics program was conducted to test symmetry in the weak sector and constrain weak coupling beyond V–A . Those two programs were supported by careful measurements of the involved solid state physics parameters to attain the full sensitivity of the technique and provide interesting interdisciplinary results. Future plans for this facility include the challenging idea of measuring the beta–gamma–neutron angular distributions from polarized beta delayed neutron emitters, further test of fundamental symmetries and obtaining nuclear structure data used in medical applications. The facility will also continue to contribute to both the nuclear structure and fundamental symmetry test programs. (paper)

  19. Analysis of low-temperature tar fractions

    Energy Technology Data Exchange (ETDEWEB)

    Kikkawa, S; Yamada, F

    1952-01-01

    A preliminary comparative study was made on the applicability of the methods commonly used for the type analysis of petroleum products to the low-temperature tar fractions. The usability of chromatography was also studied.

  20. Low temperature plasma technology methods and applications

    CERN Document Server

    Chu, Paul K

    2013-01-01

    Written by a team of pioneering scientists from around the world, Low Temperature Plasma Technology: Methods and Applications brings together recent technological advances and research in the rapidly growing field of low temperature plasmas. The book provides a comprehensive overview of related phenomena such as plasma bullets, plasma penetration into biofilms, discharge-mode transition of atmospheric pressure plasmas, and self-organization of microdischarges. It describes relevant technology and diagnostics, including nanosecond pulsed discharge, cavity ringdown spectroscopy, and laser-induce

  1. Low temperature humidification dehumidification desalination process

    International Nuclear Information System (INIS)

    Al-Enezi, Ghazi; Ettouney, Hisham; Fawzy, Nagla

    2006-01-01

    The humidification dehumidification desalination process is viewed as a promising technique for small capacity production plants. The process has several attractive features, which include operation at low temperature, ability to utilize sustainable energy sources, i.e. solar and geothermal, and requirements of low technology level. This paper evaluates the characteristics of the humidification dehumidification desalination process as a function of operating conditions. A small capacity experimental system is used to evaluate the process characteristics as a function of the flow rate of the water and air streams, the temperature of the water stream and the temperature of the cooling water stream. The experimental system includes a packed humidification column, a double pipe glass condenser, a constant temperature water circulation tank and a chiller for cooling water. The water production is found to depend strongly on the hot water temperature. Also, the water production is found to increase upon the increase of the air flow rate and the decrease of the cooling water temperature. The measured air and water temperatures, air relative humidity and the flow rates are used to calculate the air side mass transfer coefficient and the overall heat transfer coefficient. Measured data are found to be consistent with previous literature results

  2. Parameterization and measurements of helical magnetic fields

    International Nuclear Information System (INIS)

    Fischer, W.; Okamura, M.

    1997-01-01

    Magnetic fields with helical symmetry can be parameterized using multipole coefficients (a n , b n ). We present a parameterization that gives the familiar multipole coefficients (a n , b n ) for straight magnets when the helical wavelength tends to infinity. To measure helical fields all methods used for straight magnets can be employed. We show how to convert the results of those measurements to obtain the desired helical multipole coefficients (a n , b n )

  3. Programming the control of magnetic field measurements

    International Nuclear Information System (INIS)

    David, L.

    1998-01-01

    This paper gives a short review concerning the new NMR probe measurement control system. Then it presents the new program 'CYCLOCHAMP' attached to the magnetic field measurement which also allows to cycle the magnetic field inside the cyclotrons and to equilibrate it among the SSC sectors. (authors)

  4. Fringing field measurement of dipole magnet

    International Nuclear Information System (INIS)

    Lu Hongyou; Jiang Weisheng; Mao Naifeng; Mao Xingwang

    1985-01-01

    The fringing field of a dipole magnet with a C-type circuit and homogeneous field in the gap has been measured including the distributions of fringing fields with and without magnetic shield. The measured data was analyzed by using the concept of virtual field boundary

  5. Direct measurements of the magnetic entropy change

    DEFF Research Database (Denmark)

    Nielsen, Kaspar Kirstein; Neves Bez, Henrique; von Moos, Lars

    2015-01-01

    An experimental device that can accurately measure the magnetic entropy change, Δs, as a function of temperature, T, and magnetic field, H, is presented. The magnetic field source is in this case a set of counter-rotating concentric Halbach-type magnets, which produce a highly homogeneous applied...... to the ambient are negligible in terms of the calorimetric determination of the magnetic entropy change, while the losses cannot be ignored when correcting for the actual sample temperature. We apply the device to two different types of samples; one is commercial grade Gd, i.e., a pure second-order phase...

  6. The measurement of solar magnetic fields

    International Nuclear Information System (INIS)

    Stenflo, J.O.

    1978-01-01

    Solar activity is basically caused by the interaction between magnetic fields, solar rotation and convective motions. Detailed mapping of the Sun's rapidly varying magnetic field helps in the understanding of the mechanisms of solar activity. Observations in recent years have revealed unexpected and intriguing properties of solar magnetic fields, the explanation of which has become a challenge to plasma physicists. This review deals primarily with how the Sun's magnetic field is measured, but it also includes a brief review of the present observational picture of the magnetic field, which is needed to understand the problems of how to properly interpret the observations. 215 references. (author)

  7. Enhancement of the spectral selectivity of complex samples by measuring them in a frozen state at low temperatures in order to improve accuracy for quantitative analysis. Part II. Determination of viscosity for lube base oils using Raman spectroscopy.

    Science.gov (United States)

    Kim, Mooeung; Chung, Hoeil

    2013-03-07

    The use of selectivity-enhanced Raman spectra of lube base oil (LBO) samples achieved by the spectral collection under frozen conditions at low temperatures was effective for improving accuracy for the determination of the kinematic viscosity at 40 °C (KV@40). A collection of Raman spectra from samples cooled around -160 °C provided the most accurate measurement of KV@40. Components of the LBO samples were mainly long-chain hydrocarbons with molecular structures that were deformable when these were frozen, and the different structural deformabilities of the components enhanced spectral selectivity among the samples. To study the structural variation of components according to the change of sample temperature from cryogenic to ambient condition, n-heptadecane and pristane (2,6,10,14-tetramethylpentadecane) were selected as representative components of LBO samples, and their temperature-induced spectral features as well as the corresponding spectral loadings were investigated. A two-dimensional (2D) correlation analysis was also employed to explain the origin for the improved accuracy. The asynchronous 2D correlation pattern was simplest at the optimal temperature, indicating the occurrence of distinct and selective spectral variations, which enabled the variation of KV@40 of LBO samples to be more accurately assessed.

  8. Mechanical design and protection of superconducting magnets

    CERN Document Server

    Asner, Alfred M

    1978-01-01

    The principles of the mechanical design of superconducting magnets of concentric configuration, with iron low-temperature and room- temperature screening, are outlined. Measures for protection of such magnets against quench forces, are considered. (4 refs).

  9. A Flexible Framework for Magnetic Measurements

    CERN Document Server

    Inglese, V; Buzio, M

    2009-01-01

    The work presented in this Ph.D. thesis covers the specification, design, prototyping, and validation of a new version of a magnetic measurement control, acquisition, and data analysis software package: the Flexible Framework for Magnetic Measurements (FFMM). FFMM constitutes the software part of the new platform for magnetic measurements, including also new high-performance hardware, developed at the European Organization for Nuclear Research (CERN) in cooperation with the Department of Engineering of the University of Sannio. FFMM is conceived as a unified solution to drive all the existing and future park of measurement systems (mainly magnetic but also optical, mechanical, etc.). The effort for the series test of the LHC superconducting magnets highlighted limitations in the measurement control and acquisition programs, mainly associated with the relatively long time needed for a development iteration (the cycle of specification-programming-debugging-validation). Moreover, the software capabilities needed...

  10. Erosion–corrosion and corrosion properties of DLC coated low temperature Erosion–corrosion and corrosion properties of DLC coated low temperature

    DEFF Research Database (Denmark)

    Jellesen, Morten Stendahl; Christiansen, Thomas; Hilbert, Lisbeth Rischel

    2009-01-01

    of AISI 316 as substrate for DLC coatings are investigated. Corrosion and erosion–corrosion measurements were carried out on low temperature nitrided stainless steel AISI 316 and on low temperature nitrided stainless steel AISI 316 with a top layer of DLC. The combination of DLC and low temperature...... nitriding dramatically reduces the amount of erosion–corrosion of stainless steel under impingement of particles in a corrosive medium....

  11. Some experiments in low-temperature thermometry

    International Nuclear Information System (INIS)

    Fogle, W.E.

    1982-11-01

    A powdered cerous magnesium nitrate (CMN) temperature scale has been developed in the 0.016 to 3.8 K region which represents an interpolation between the 3 He/ 4 He (T 62 /T 58 ) vapor pressure scale and absolute temperatures in the millikelvin region as determined with a 60 Co in hcp Co nuclear orientation thermometer (NOT). Both ac and dc susceptibility thermometers were used in these experiments. The ac susceptibility of a 13 mg CMN-oil slurry was measured with a mutual inductance bridge employing a SQUID null detector while the dc susceptibility of a 3 mg slurry was measured with a SQUID/flux transformer combination. To check the internal consistency of the NOT, γ-ray intensities were measured both parallel and perpendicular to the Co crystal c-axis. The independent temperatures determined in this fashion were found to agree to within experimental error. For the CMN thermometers employed in these experiments, the susceptibility was found to obey a Curie-Weiss law with a Weiss constant of Δ = 1.05 +- 0.1 mK. The powdered CMN scale in the 0.05 to 1.0 K region was transferred to two germanium resistance thermometers for use in low-temperature specific heat measurements. The integrity of the scale was checked by examining the temperature dependence of the specific heat of high purity copper in the 0.1 to 1 K region. In more recent experiments in this laboratory, the scale was also checked by a comparison with the National Bureau of Standards cryogenic temperature scale (NBS-CTS-1). The agreement between the two scales in the 99 to 206 mK region was found to be on the order of the stated accuracy of the NBS scale

  12. Minimizing material damage using low temperature irradiation

    International Nuclear Information System (INIS)

    Craven, E.; Hasanain, F.; Winters, M.

    2012-01-01

    Scientific advancements in healthcare driven both by technological breakthroughs and an aging and increasingly obese population have lead to a changing medical device market. Complex products and devices are being developed to meet the demands of leading edge medical procedures. Specialized materials in these medical devices, including pharmaceuticals and biologics as well as exotic polymers present a challenge for radiation sterilization as many of these components cannot withstand conventional irradiation methods. The irradiation of materials at dry ice temperatures has emerged as a technique that can be used to decrease the radiation sensitivity of materials. The purpose of this study is to examine the effect of low temperature irradiation on a variety of polymer materials, and over a range of temperatures from 0 °C down to −80 °C. The effectiveness of microbial kill is also investigated under each of these conditions. The results of the study show that the effect of low temperature irradiation is material dependent and can alter the balance between crosslinking and chain scission of the polymer. Low temperatures also increase the dose required to achieve an equivalent microbiological kill, therefore dose setting exercises must be performed under the environmental conditions of use. - Highlights: ► A study is performed to quantify low temperature irradiation effects on polymer materials and BIs. ► Low temperature irradiation alters the balance of cross-linking and chain scissoning in polymers. ► Low temperatures provide radioprotection for BIs. ► Benefits of low temperatures are application specific and must be considered when dose setting.

  13. Lightning magnetic field measuring system in Bogota

    OpenAIRE

    Escobar Alvarado, Oscar Fernardo

    2013-01-01

    This thesis presents the configuration and performance of a lightning radiated electromagnetic field measuring system in Bogotá Colombia. The system is composed by both magnetic and electric field measuring systems working as separated sensors. The aim of the thesis is the design and construction of a Magnetic Field Measuring System and the implementation of a whole lightning measuring system in Bogotá. The theoretical background, design process, construction and implementation of the system ...

  14. Magnetic Field Measurements In Magnetized Plasmas Using Zeeman Broadening Diagnostics

    Science.gov (United States)

    Haque, Showera; Wallace, Matthew; Presura, Radu; Neill, Paul

    2017-10-01

    The Zeeman effect has been used to measure the magnetic field in high energy density plasmas. This method is limited when plasma conditions are such that the line broadening due to the high plasma density and temperature surpasses the Zeeman splitting. We have measured magnetic fields in magnetized laser plasmas under conditions where the Zeeman splitting was not spectrally resolved. The magnetic field strength was determined from the difference in widths of two doublet components, using an idea proposed by Tessarin et al. (2011). Time-gated spectra with one-dimensional space-resolution were obtained at the Nevada Terawatt Facility for laser plasmas created by 20 J, 1 ns Leopard laser pulses, and expanding in the azimuthal magnetic field produced by the 0.6 MA Zebra pulsed power generator. We explore the response of the Al III 4s 2S1/2 - 4p 2P1 / 2 , 3 / 2 doublet components to the external magnetic field spatially along the plasma. Radial magnetic field and electron density profiles were measured within the plasma plume. This work was supported by the DOE/OFES Grant DE-SC0008829 and DOE/NNSA contract DE-FC52-06NA27616.

  15. Materials with low DC magnetic susceptibility for sensitive magnetic measurements

    International Nuclear Information System (INIS)

    Khatiwada, R; Kendrick, R; Khosravi, M; Peters, M; Smith, E; Snow, W M; Dennis, L

    2016-01-01

    Materials with very low DC magnetic susceptibility have many scientific applications. To our knowledge however, relatively little research has been conducted with the goal to produce a totally nonmagnetic material. This phrase in our case means after spatially averaging over macroscopic volumes, it possesses an average zero DC magnetic susceptibility. We report measurements of the DC magnetic susceptibility of three different types of nonmagnetic materials at room temperature: (I) solutions of paramagnetic salts and diamagnetic liquids, (II) liquid gallium–indium alloys and (III) pressed powder mixtures of tungsten and bismuth. The lowest measured magnetic susceptibility among these candidate materials is in the order of 10 −9 cgs volume susceptibility units, about two orders of magnitude smaller than distilled water. In all cases, the measured concentration dependence of the magnetic susceptibility is consistent with that expected for the weighted sum of the susceptibilities of the separate components within experimental error. These results verify the well-known Wiedemann additivity law for the magnetic susceptibility of inert mixtures of materials and thereby realize the ability to produce materials with small but tunable magnetic susceptibility. For our particular scientific application, we are also looking for materials with the largest possible number of neutrons and protons per unit volume. The gallium–indium alloys fabricated and measured in this work possess to our knowledge the smallest ratio of volume magnetic susceptibility to nucleon number density per unit volume for a room temperature liquid, and the tungsten-bismuth pressed powder mixtures possess to our knowledge the smallest ratio of volume magnetic susceptibility to nucleon number density per unit volume for a room temperature solid. This ratio is a figure of merit for a certain class of precision experiments that search for possible exotic spin-dependent forces of Nature. (paper)

  16. Superconducting property measuring system by magnetization method

    International Nuclear Information System (INIS)

    Ikisawa, K.; Mori, T.; Takasu, N.

    1988-01-01

    Superconducting property measuring system (CMS-370B) for high temperature oxide superconductor has been developed. This system adopts magnetization measurement. The superconducting properties are able to be measured automatically and continuously changing the temperature and external magnetic field. The critical current density as a function of temperature and magnetic field of high temperature superconductor YBa 2 Cu 3 O 7-y (YBCO) has been measured. This paper reports how it was confirmed that this system having the high performance and the accuracy gave the significant contribution to the superconducting material development

  17. Ac loss measurement of SSC dipole magnets

    International Nuclear Information System (INIS)

    Delchamps, S.; Hanft, R.; Jaffery, T.; Kinney, W.; Koska, W.; Lamm, M.J.; Mazur, P.O.; Orris, D.; Ozelis, J.P.; Strait, J.; Wake, M.

    1992-09-01

    AC losses in full length and 1.5 m model SSC collider dipoles were successfully measured by the direct observation of energy flow into and out of magnets during a ramp cycle. The measurement was performed by using two double-integrating type digital volt meters (DVM's) for current and voltage measurement. Measurements were performed for six is m long ASST magnets and five 1.5 m long model magnets, inducting one 40 mm diameter magnet. There were large variations in the eddy current losses. Since these magnets use conductors with slight deviations in their internal structures and processing of the copper surface depending on the manufacturer, it is likely that there are differences in the contact resistance between strands. Correlation between the ramp rate dependence of the,quench current and the eddy current loss was evident

  18. Measurement of magnetic fluctuation induced energy transport

    International Nuclear Information System (INIS)

    Fiksel, G.; Prager, S.C.; Shen, W.; Stoneking, M.

    1993-11-01

    The local electron energy flux produced by magnetic fluctuations has been measured directly in the MST reversed field pinch (over the radial range r/a > 0.75). The flux, produced by electrons traveling parallel to a fluctuating magnetic field, is obtained from correlation between the fluctuations in the parallel heat flux and the radial magnetic field. The fluctuation induced flux is large (100 kW/cm 2 ) in the ''core'' (r/a 2 ) in the edge

  19. Measurement of the magnetic field coefficients of particle accelerator magnets

    International Nuclear Information System (INIS)

    Herrera, J.; Ganetis, G.; Hogue, R.; Rogers, E.; Wanderer, P.; Willen, E.

    1989-01-01

    An important aspect in the development of magnets to be used in particle accelerators is the measurement of the magnetic field in the beam aperture. In general it is necessary to measure the harmonic multipoles in the dipole, quadrupole, and sextupole magnets for a series of stationary currents (plateaus). This is the case for the Superconducting Super Collider (SSC) which will be ramped to high field over a long period (/approximately/1000 sec.) and then remain on the flat top for the duration of the particle collision phase. In contrast to this mode of operation, the Booster ring being constructed for the Brookhaven AGS, will have a fast ramp rate of approximately 10 Hz. The multipole fields for these Booster magnets must therefore be determined ''on the ramp.'' In this way the effect of eddy currents will be taken into account. The measurement system which we will describe in this paper is an outgrowth of that used for the SSC dipoles. It has the capability of measuring the field multipoles on both a plateau or during a fast ramp. In addition, the same basic coil assembly is used to obtain the magnetic multipoles in dipole, quadrupole, and sextupole magnets. 2 refs., 3 figs., 1 tab

  20. Basics of Low-temperature Refrigeration

    CERN Document Server

    Alekseev, A.

    2014-07-17

    This chapter gives an overview of the principles of low temperature refrigeration and the thermodynamics behind it. Basic cryogenic processes - Joule-Thomoson process, Brayton process as well as Claude process - are described and compared. A typical helium laboratory refrigerator based on Claude process is used as a typical example of a low-temperature refrigeration system. A description of the hardware components for helium liquefaction is an important part of this paper, because the design of the main hardware components (compressors, turbines, heat exchangers, pumps, adsorbers, etc.) provides the input for cost calculation, as well as enables to estimate the reliability of the plant and the maintenance expenses. All these numbers are necessary to calculate the economics of a low temperature application.

  1. Kinetics and spectroscopy of low temperature plasmas

    CERN Document Server

    Loureiro, Jorge

    2016-01-01

    This is a comprehensive textbook designed for graduate and advanced undergraduate students. Both authors rely on more than 20 years of teaching experience in renowned Physics Engineering courses to write this book addressing the students’ needs. Kinetics and Spectroscopy of Low Temperature Plasmas derives in a full self-consistent way the electron kinetic theory used to describe low temperature plasmas created in the laboratory with an electrical discharge, and presents the main optical spectroscopic diagnostics used to characterize such plasmas. The chapters with the theoretical contents make use of a deductive approach in which the electron kinetic theory applied to plasmas with basis on the electron Boltzmann equation is derived from the basic concepts of Statistical and Plasma Physics. On the other hand, the main optical spectroscopy diagnostics used to characterize experimentally such plasmas are presented and justified from the point of view of the Atomic and Molecular Physics. Low temperature plasmas...

  2. Basics of Low-temperature Refrigeration

    Energy Technology Data Exchange (ETDEWEB)

    Alekseev, A [Linde AG, Munich (Germany)

    2014-07-01

    This chapter gives an overview of the principles of low temperature refrigeration and the thermodynamics behind it. Basic cryogenic processes - Joule-Thomoson process, Brayton process as well as Claude process - are described and compared. A typical helium laboratory refrigerator based on Claude process is used as a typical example of a low-temperature refrigeration system. A description of the hardware components for helium liquefaction is an important part of this paper, because the design of the main hardware components (compressors, turbines, heat exchangers, pumps, adsorbers, etc.) provides the input for cost calculation, as well as enables to estimate the reliability of the plant and the maintenance expenses. All these numbers are necessary to calculate the economics of a low temperature application.

  3. The methods of the LHC magnets' magnetic axis location measurement

    International Nuclear Information System (INIS)

    Bottura, L.; Buzio, M.; Deferne, G.; Sievers, P.; Smirnov, N.; Villar, F.P.; Walckiers, L.

    1999-01-01

    More than 8 thousands LHC magnets of various types will be extensively measured during series magnetic test at both room and superfluid helium temperature. The precise knowledge of the magnetic axis positioning is vital for the alignment of those magnets in the tunnel. The most efficient and cost effective method with rotating pick up coil is chosen currently as a baseline for series measurement. The position of the measuring coil axis herewith is measured with a dedicated optical system. The deflection of the light beam in the air due to temperature gradient either passing through the cold bore when the magnet excited for warm measurement or through the anti-cryostat during cold measurement can reach magnitudes significantly exceeding tolerance and therefore is a critical issue. We present studies of the light deflection in 10 m long dipole at warm and cold and propose means to reduce it. The result of the dipole centring powered in Quadrupole Configured Dipole (QCD) or 'ugly quad' configuration and correlation with centring based on high order harmonics are presented as well. (authors)

  4. Low temperature monitoring system for subsurface barriers

    Science.gov (United States)

    Vinegar, Harold J [Bellaire, TX; McKinzie, II Billy John [Houston, TX

    2009-08-18

    A system for monitoring temperature of a subsurface low temperature zone is described. The system includes a plurality of freeze wells configured to form the low temperature zone, one or more lasers, and a fiber optic cable coupled to at least one laser. A portion of the fiber optic cable is positioned in at least one freeze well. At least one laser is configured to transmit light pulses into a first end of the fiber optic cable. An analyzer is coupled to the fiber optic cable. The analyzer is configured to receive return signals from the light pulses.

  5. Materials for low-temperature fuel cells

    CERN Document Server

    Ladewig, Bradley; Yan, Yushan; Lu, Max

    2014-01-01

    There are a large number of books available on fuel cells; however, the majority are on specific types of fuel cells such as solid oxide fuel cells, proton exchange membrane fuel cells, or on specific technical aspects of fuel cells, e.g., the system or stack engineering. Thus, there is a need for a book focused on materials requirements in fuel cells. Key Materials in Low-Temperature Fuel Cells is a concise source of the most important and key materials and catalysts in low-temperature fuel cells. A related book will cover key materials in high-temperature fuel cells. The two books form part

  6. Low-temperature carbonization plant for lignite

    Energy Technology Data Exchange (ETDEWEB)

    Shiotsuki, Y

    1949-01-01

    The design and operational data of a low-temperature carbonization plant for Japanese lignite are described. The retort had a vertical cylinder with a capacity of about 10 tons per day. By continuous operation, in which a part of the gas produced was circulated and burned in the lignite zone, about 40 percent semicoke and 3 to 4 percent tar were obtained. From the tar the following products were separated: Low-temperature carbonization cresol, 18.3; motor fuel, 1.00; solvent, 9.97; cresol for medical uses, 11.85; and creosote oil, 32 percent.

  7. Low temperature junction magnetoresistance properties of Co{sub 0.65}Zn{sub 0.35}Fe{sub 2}O{sub 4}/SiO{sub 2}/p-Si magnetic diode like heterostructure for spin-electronics

    Energy Technology Data Exchange (ETDEWEB)

    Panda, J.; Nath, T.K., E-mail: tnath@phy.iitkgp.ernet.in

    2016-02-29

    The magnetic heterojunction diode has been fabricated by growing Co{sub 0.65}Zn{sub 0.35}Fe{sub 2}O{sub 4} (CZFO) on well cleaned p-Si substrate using pulsed laser deposition technique, and its behavior under magnetic field is experimentally studied in details. The magnetic field dependent current–voltage characteristics (I–V) have been studied at different isothermal conditions in the range of 5–300 K. The junction shows magnetic diode like rectifying behavior at low temperature, whereas at high temperatures the junction shows nonlinear I–V characteristics. Magnetic field shows a strong effect on junction resistance (CZFO/p-Si). It is interesting that the positive junction magnetoresistance (MR) thus produced, remains very large at low temperature regime (590% at 5 K) and gradually decreases at higher temperatures. In contrast, CZFO magnetic thin film shows negative MR behavior, whereas the junction shows large positive junction magnetoresistance (JMR) behavior throughout the temperature range. The origin of JMR has been best explained by standard spin injection theory. The temperature dependent spin life time (τ) has been estimated for our heterostructure. The value of τ decreases with increasing temperature. The spin life time (183 ps), spin polarization (0.71) and spin diffusion length (375 nm) have been estimated of the heterostructure at 10 K. - Highlights: • The junction magnetoresistance (JMR) of Co{sub 0.65}Zn{sub 0.35}Fe{sub 2}O{sub 4}/SiO{sub 2}/p-Si heterojunction is studied. • Heterostructure shows rectifying magnetic diode like behavior. • The highest positive JMR (590%) has been found to be at 5 K. • The origin of observed JMR has been best explained by spin injection theory. • The spin life time, spin diffusion length and spin polarization have been estimated at 10 K.

  8. Moessbauer spectroscopy of He irradiated austenitic stainless steel SUS304 at low temperature

    International Nuclear Information System (INIS)

    Horii, Kiyomasa; Ishibashi, Tetsu; Toriyama, Tamotsu; Wakabayashi, Hidehiko; Iijima, Hiroshi; Kawasaki, Katsunori; Hayashi, Nobuyuki; Sakamoto, Isao.

    1996-01-01

    SUS 304 austenitic stainless steel causes the magnetic transition at 60 K, and the Young's modulus lowers. In addition, its composition elements have the large (n,α) reaction cross section to high energy neutrons, and helium is apt to be generated, and this is a factor that lowers the material strength. In the He-irradiated parts in austenitic stainless steel, the precursory state of martensite transformation should exist, and its effect is considered to be observable by carrying out low temperature Moessbauer spectroscopy. As to the preparation of He-irradiation samples, the SUS 304 foils used and the irradiation conditions are described. The measurement of low temperature Moessbauer spectra for the samples without irradiation and with irradiation is reported. In order to determine the magnetic transition point, the thermal scanning measurement was carried out for the samples without or with irradiation. The martensite transformation was measured by X-ray diffraction and transmission type Moessbauer spectroscopy. In order to observe the state of the sample surfaces, the measurement by internal conversion electron Moessbauer spectroscopy was performed. These results and the temperature dependence of the Moessbauer spectra for the irradiated parts are reported. (K.I.)

  9. Moessbauer spectroscopy of He irradiated austenitic stainless steel SUS304 at low temperature

    Energy Technology Data Exchange (ETDEWEB)

    Horii, Kiyomasa; Ishibashi, Tetsu; Toriyama, Tamotsu; Wakabayashi, Hidehiko; Iijima, Hiroshi [Musashi Inst. of Tech., Tokyo (Japan); Kawasaki, Katsunori; Hayashi, Nobuyuki; Sakamoto, Isao

    1996-04-01

    SUS 304 austenitic stainless steel causes the magnetic transition at 60 K, and the Young`s modulus lowers. In addition, its composition elements have the large (n,{alpha}) reaction cross section to high energy neutrons, and helium is apt to be generated, and this is a factor that lowers the material strength. In the He-irradiated parts in austenitic stainless steel, the precursory state of martensite transformation should exist, and its effect is considered to be observable by carrying out low temperature Moessbauer spectroscopy. As to the preparation of He-irradiation samples, the SUS 304 foils used and the irradiation conditions are described. The measurement of low temperature Moessbauer spectra for the samples without irradiation and with irradiation is reported. In order to determine the magnetic transition point, the thermal scanning measurement was carried out for the samples without or with irradiation. The martensite transformation was measured by X-ray diffraction and transmission type Moessbauer spectroscopy. In order to observe the state of the sample surfaces, the measurement by internal conversion electron Moessbauer spectroscopy was performed. These results and the temperature dependence of the Moessbauer spectra for the irradiated parts are reported. (K.I.)

  10. High Pressure Low Temperature X-Ray Diffraction Studies of UO2 and UN single crystals.

    Science.gov (United States)

    Antonio, Daniel; Mast, Daniel; Lavina, Barbara; Gofryk, Krzysztof

    Uranium dioxide is the most commonly used nuclear fuel material in commercial reactors, while uranium nitride also has many thermal and physical properties that make it attractive for potential use in reactors. Both have a cubic fcc lattice structure at ambient conditions and transition to antiferromagnetic order at low temperature. UO2 is a Mott insulator that orders in a complex non-collinear 3k magnetic structure at about 30 K, while UN has appreciable conductivity and orders in a simpler 1k magnetic structure below 52 K. Both compounds are characterized by strong magneto-structural interactions, understanding of which is vital for modeling their thermo-physical properties. While UO2 and UN have been extensively studied at and above room temperature, little work has been done to directly study the structure of these materials at low temperatures where magnetic interactions are dominant. In the course of our systematic studies on magneto vibrational behavior of UO2 and UN, here we present our recent results of high pressure X-Ray Diffraction (up to 35 GPa) measured below the Neel temperature using synchrotron radiation. Work supported by the Department of Energy, Office of Basic Energy Sciences, Materials Sciences, and Engineering Division.

  11. Low temperature thermophysical properties of lunar soil

    Science.gov (United States)

    Cremers, C. J.

    1973-01-01

    The thermal conductivity and thermal diffusivity of lunar fines samples from the Apollo 11 and Apollo 12 missions, determined at low temperatures as a function of temperature and various densities, are reviewed. It is shown that the thermal conductivity of lunar soil is nearly the same as that of terrestrial basaltic rock under the same temperature and pressure conditions.

  12. Neutrinos, dark matter and low temperature detectors

    International Nuclear Information System (INIS)

    Gonzalez-Mestres, L.; Perret-Gallix, D.

    1988-01-01

    The present status of cryogenic detector developments for particle physics is discussed, with emphasis on applications at the cross-disciplinary frontier between particle physics and astrophysics, where low temperature devices appear to be particularly well suited. The overwiew of results is completed by a sketch of new ideas and possible ways for further improvements. Neutrino role importance is particularly shown

  13. Low Temperature Cure Powder Coatings (LTCPC)

    Science.gov (United States)

    2010-10-01

    Dr. Glen Merfeld, General Electric Global Research evaluated and optimized the formulation, and cure and performance parameters of candidate LTCPC...Unacceptable test result = Marginal test result = Acceptable test result 80 therefore suffer from brittleness at extremely low temperatures. NASA’s

  14. Industrial Applications of Low Temperature Plasmas

    International Nuclear Information System (INIS)

    Bardsley, J N

    2001-01-01

    The use of low temperature plasmas in industry is illustrated by the discussion of four applications, to lighting, displays, semiconductor manufacturing and pollution control. The type of plasma required for each application is described and typical materials are identified. The need to understand radical formation, ionization and metastable excitation within the discharge and the importance of surface reactions are stressed

  15. Low temperature anodic bonding to silicon nitride

    DEFF Research Database (Denmark)

    Weichel, Steen; Reus, Roger De; Bouaidat, Salim

    2000-01-01

    Low-temperature anodic bonding to stoichiometric silicon nitride surfaces has been performed in the temperature range from 3508C to 4008C. It is shown that the bonding is improved considerably if the nitride surfaces are either oxidized or exposed to an oxygen plasma prior to the bonding. Both bu...

  16. Arc generators of low-temperature plasma

    International Nuclear Information System (INIS)

    Krolikowski, Cz.; Niewiedzial, R.; Siwiec, J.

    1979-01-01

    This paper is a review of works concerning investigation and use of low-temperature plasma in arc plasma generators made in Electric Power Institute of PP. There are discussed: analytical approach to a problem of volt-current and operational characteristics of DC arc plasma generators, determination of limits of their stable work and possibilities of their use to technological aims. (author)

  17. Magnetic measurements of the injector synchrotron magnets for the Advanced Photon Source

    International Nuclear Information System (INIS)

    Kim, S.H.; Carnegie, D.W.; Doose, C.L.; Hogrefe, R.; Kim, K.; Merl, R.; Turner, L.R.

    1993-01-01

    The magnetic measurement data of the dipole, quadrupole, and sextupole magnets for the Advanced Photon Source injector synchrotron are summarized. Magnet design and magnetic measurements of the field strength, field shape, and multipole coefficients are described

  18. Magnetic measurements of the injector synchrotron magnets for the advanced photon source

    Science.gov (United States)

    Kim, S. H.; Carnegie, D. W.; Doose, C. L.; Hogrefe, R.; Kim, K.; Merl, R.; Turner, L. R.

    1994-07-01

    The magnetic measurement data of the dipole, quadrupole, and sextupole magnets for the Advanced Photon Source injector synchrotron are summarized. Magnet design and magnetic measurements of the field strength, field shape, and multipole coefficients are described.

  19. The development of the high-tension wire for nuclear fusion superconductive magnet measurement

    International Nuclear Information System (INIS)

    Yoshida, Kiyoshi; Morita, Yohsuke; Yamazaki, Takanori; Watanabe, Kiyoshi; Furusawa, Ken-ichi.

    1987-01-01

    Following on tokamak critical plasma testing device JT-60, experimental fusion reactor JT-100 is being developed. The 6 kV high-tension wire has been developed for use in JT-100 under ultra-low temperature and high radiation environment. Used for superconductive magnet measurement, the wire is inserted in the vacuum vessel, being immersed within the liquid helium. As the insulating material of this wire, polyetherimido was found to be most suitable in the respects of radiation resistance and voltage-withstand property. In an electric wire covered with polyetherimido, which was made in trial, its test in voltage-withstand and bending characteristics at ultra-low temperature showed the wire to be usable for the intended purpose. (Mori, K.)

  20. On the measurement of magnetic viscosity

    Science.gov (United States)

    Serletis, C.; Efthimiadis, K. G.

    2012-08-01

    This work is an investigation of the experimental method used for measuring the magnetic viscosity in a hard ferromagnetic material, i.e. the recording of the magnetization under constant applied field and temperature, after the material has been magnetically saturated. It investigates how the experimental results are affected by the initial conditions of the method (saturation field, field change rate and field oscillation prior to its stabilization), and by minor variations of field and temperature during the recording. Based on the arising conclusions and the use of a more complex fitting function of measurements, the accuracy and repeatability of experimental results is improved.

  1. Accuracy of magnetic resonance based susceptibility measurements

    Science.gov (United States)

    Erdevig, Hannah E.; Russek, Stephen E.; Carnicka, Slavka; Stupic, Karl F.; Keenan, Kathryn E.

    2017-05-01

    Magnetic Resonance Imaging (MRI) is increasingly used to map the magnetic susceptibility of tissue to identify cerebral microbleeds associated with traumatic brain injury and pathological iron deposits associated with neurodegenerative diseases such as Parkinson's and Alzheimer's disease. Accurate measurements of susceptibility are important for determining oxygen and iron content in blood vessels and brain tissue for use in noninvasive clinical diagnosis and treatment assessments. Induced magnetic fields with amplitude on the order of 100 nT, can be detected using MRI phase images. The induced field distributions can then be inverted to obtain quantitative susceptibility maps. The focus of this research was to determine the accuracy of MRI-based susceptibility measurements using simple phantom geometries and to compare the susceptibility measurements with magnetometry measurements where SI-traceable standards are available. The susceptibilities of paramagnetic salt solutions in cylindrical containers were measured as a function of orientation relative to the static MRI field. The observed induced fields as a function of orientation of the cylinder were in good agreement with simple models. The MRI susceptibility measurements were compared with SQUID magnetometry using NIST-traceable standards. MRI can accurately measure relative magnetic susceptibilities while SQUID magnetometry measures absolute magnetic susceptibility. Given the accuracy of moment measurements of tissue mimicking samples, and the need to look at small differences in tissue properties, the use of existing NIST standard reference materials to calibrate MRI reference structures is problematic and better reference materials are required.

  2. Magnet Fiducialization with Coordinate Measuring Machines

    International Nuclear Information System (INIS)

    Friedsam, H.; Oren, W.; Pietryka, M.; SLAC

    2005-01-01

    One of the fundamental alignment problems encountered when building a particle accelerator is the transfer of a component's magnetic centerline position to external fiducials. This operation, dubbed fiducialization, is critical because it can contribute significantly to the alignment error budget. The fiducialization process requires two measurements: (1) from magnetic centerline to mechanical centerline, and (2) from mechanical centerline to external fiducials. This paper will focus on methods for observing the second measurement. Two Stanford Linear Collider (SLC) examples are presented. The object of magnet fiducialization is to relate the magnet-defined beamline position to exterior reference surfaces. To be useful for later component alignment, this relationship must be established in a manner consistent with overall positioning tolerances. The error budget for the SLC's ± 100 (micro)m component to component alignment tolerance is as follows: magnetic centerline to mechanical centerline--σ = ±30 (micro)m; mechanical centerline to fiducial marks--σ = ±50 (micro)m; and fiducial marks to adjacent components--σ = ±80 (micro)m; the TOTAL σ = ±100 (micro)m. The offset between the mechanical and magnetic centerlines of well-known magnets is generally smaller than the ±30 (micro)m measurement tolerance. It is commonly assumed to be zero without measurement. When this tiny value must be measured, extreme care is necessary to avoid obscuring the offset with measurement tool registration errors. In contrast, the mechanical centerline to fiducial measurement must be performed on every magnet. The 50 (micro)m tolerance for this operation is only slightly larger and pushes conventional surveying technology to its limit

  3. Magnet Fiducialization with Coordinate Measuring Machines

    Energy Technology Data Exchange (ETDEWEB)

    Friedsam, H.; Oren, W.; Pietryka, M.; /SLAC

    2005-08-12

    One of the fundamental alignment problems encountered when building a particle accelerator is the transfer of a component's magnetic centerline position to external fiducials. This operation, dubbed fiducialization, is critical because it can contribute significantly to the alignment error budget. The fiducialization process requires two measurements: (1) from magnetic centerline to mechanical centerline, and (2) from mechanical centerline to external fiducials. This paper will focus on methods for observing the second measurement. Two Stanford Linear Collider (SLC) examples are presented. The object of magnet fiducialization is to relate the magnet-defined beamline position to exterior reference surfaces. To be useful for later component alignment, this relationship must be established in a manner consistent with overall positioning tolerances. The error budget for the SLC's {+-} 100 {micro}m component to component alignment tolerance is as follows: magnetic centerline to mechanical centerline--{sigma} = {+-}30 {micro}m; mechanical centerline to fiducial marks--{sigma} = {+-}50 {micro}m; and fiducial marks to adjacent components--{sigma} = {+-}80 {micro}m; the TOTAL {sigma} = {+-}100 {micro}m. The offset between the mechanical and magnetic centerlines of well-known magnets is generally smaller than the {+-}30 {micro}m measurement tolerance. It is commonly assumed to be zero without measurement. When this tiny value must be measured, extreme care is necessary to avoid obscuring the offset with measurement tool registration errors. In contrast, the mechanical centerline to fiducial measurement must be performed on every magnet. The 50 {micro}m tolerance for this operation is only slightly larger and pushes conventional surveying technology to its limit.

  4. MAGNETIC FIELD MEASUREMENTS FOR FAST-CHANGING MAGNETIC FIELDS

    International Nuclear Information System (INIS)

    2004-01-01

    Several recent applications for fast ramped magnets have been found that require rapid measurement of the field quality during the ramp. (In one instance, accelerator dipoles will be ramped at 1 T/sec, with measurements needed to the accuracy typically required for accelerators.) We have built and tested a new type of magnetic field measuring system to meet this need. The system consists of 16 stationary pickup windings mounted on a cylinder. The signals induced in the windings in a changing magnetic field are sampled and analyzed to obtain the field harmonics. To minimize costs, printed circuit boards were used for the pickup windings and a combination of amplifiers and ADPs used for the voltage readout system. New software was developed for the analysis. Magnetic field measurements of a model dipole developed for the SIS200 accelerator at GSI are presented. The measurements are needed to insure that eddy currents induced by the fast ramps do not impact the field quality needed for successful accelerator operation

  5. Crustal evolution inferred from apollo magnetic measurements

    International Nuclear Information System (INIS)

    Dyal, P.; Daily, W.D.; Vanyan, L.L.

    1978-09-01

    Magnetic field and solar wind plasma density measurements were analyzed to determine the scale size characteristics of remanent fields at the Apollo 12, 15, and 16 landing sites. Theoretical model calculations of the field-plasma interaction, involving diffusion of the remanent field into the solar plasma, were compared to the data. The information provided by all these experiments shows that remanent fields over most of the lunar surface are characterized by spatial variations as small as a few kilometers. Large regions (50 to 100 km) of the lunar crust were probably uniformly magnetized during early crustal evolution. Bombardment and subsequent gardening of the upper layers of these magnetized regions left randomly oriented, smaller scale (5 to 10 km) magnetic sources close to the surface. The larger scale size fields of magnitude approximately 0.1 gammas are measured by the orbiting subsatellite experiments and the small scale sized remanent fields of magnitude approximately 100 gammas are measured by the surface experiments

  6. Low temperature {sup 57}Fe Moessbauer study of cucumber root

    Energy Technology Data Exchange (ETDEWEB)

    Kovacs, K; Kuzmann, E; Homonnay, Z; Vertes, A [Institute of Chemistry, Eoetvoes Lorand University, PO Box 32, 1512 Budapest (Hungary); Fodor, F [Department of Plant Physiology and Molecular Plant Biology, Eoetvoes Lorand University, PO Box 32, 1512 Budapest (Hungary); Machala, L, E-mail: kkriszti@chem.elte.h [Centre for Nanomaterial Research, Palacky University, Svobody 26, Olomouc 771 46 (Czech Republic)

    2010-03-01

    Iron uptake and distribution in cucumber root were studied with the help of {sup 57}Fe Moessbauer spectroscopy at low temperature applying external magnetic field. Cucumber was grown in iron sufficient modified Hoagland nutrient solution. Moessbauer spectra of the frozen roots taken at 4.2 and 1.5 K, at 5 T external magnetic field support the identification of the main iron species (Fe{sup III}-carboxylates, hydrous ferric oxides, Fe{sup III}-sulfate-hydroxide) suggested according to its Moessbauer spectra taken between 35-200 K [1]. The magnetic ordering temperature of the hydrous ferric oxide and Fe{sup III}-sulfate-hydroxide was found to be in the range of 4.2-1.5 K, which suggests the incorporation of H{sub 3}O{sup +}, PO{sub 4}{sup 3-} and citrate into these minerals.

  7. Pressure measurements in magnetic-fusion devices

    International Nuclear Information System (INIS)

    Dylla, H.F.

    1981-11-01

    Accurate pressure measurements are important in magnetic fusion devices for: (1) plasma diagnostic measurements of particle balance and ion temperature; (2) discharge cleaning optimization; (3) vacuum system performance; and (4) tritium accountability. This paper reviews the application, required accuracy, and suitable instrumentation for these measurements. Demonstrated uses of ionization-type and capacitance-diaphragm gauges for various pressure and gas-flow measurements in tokamaks are presented, with specific reference to the effects of magnetic fields on gauge performance and the problems associated with gauge calibration

  8. Measurement of gradient magnetic field temporal characteristics

    International Nuclear Information System (INIS)

    Bartusek, K.; Jflek, B.

    1994-01-01

    We describe a technique of measuring the time dependence and field distortions of magnetic fields due to eddy currents (EC) produced by time-dependent magnetic field gradients. The EC measuring technique makes use of a large volume sample and selective RF excitation pulses and free induction decay (FID) (or a spin or gradient echo) to measure the out-of-phase component of the FID, which is proportional to γδB, i.e. the amount the signal is off resonance. The measuring technique is sensitive, easy to implement and interpret, and used for determining pre-emphasis compensation parameters

  9. Pressure measurements in magnetic-fusion devices

    Energy Technology Data Exchange (ETDEWEB)

    Dylla, H.F.

    1981-11-01

    Accurate pressure measurements are important in magnetic fusion devices for: (1) plasma diagnostic measurements of particle balance and ion temperature; (2) discharge cleaning optimization; (3) vacuum system performance; and (4) tritium accountability. This paper reviews the application, required accuracy, and suitable instrumentation for these measurements. Demonstrated uses of ionization-type and capacitance-diaphragm gauges for various pressure and gas-flow measurements in tokamaks are presented, with specific reference to the effects of magnetic fields on gauge performance and the problems associated with gauge calibration.

  10. Low Temperature Surface Carburization of Stainless Steels

    Energy Technology Data Exchange (ETDEWEB)

    Collins, Sunniva R; Heuer, Arthur H; Sikka, Vinod K

    2007-12-07

    Low-temperature colossal supersaturation (LTCSS) is a novel surface hardening method for carburization of austenitic stainless steels (SS) without the precipitation of carbides. The formation of carbides is kinetically suppressed, enabling extremely high or colossal carbon supersaturation. As a result, surface carbon concentrations in excess of 12 at. % are routinely achieved. This treatment increases the surface hardness by a factor of four to five, improving resistance to wear, corrosion, and fatigue, with significant retained ductility. LTCSS is a diffusional surface hardening process that provides a uniform and conformal hardened gradient surface with no risk of delamination or peeling. The treatment retains the austenitic phase and is completely non-magnetic. In addition, because parts are treated at low temperature, they do not distort or change dimensions. During this treatment, carbon diffusion proceeds into the metal at temperatures that constrain substitutional diffusion or mobility between the metal alloy elements. Though immobilized and unable to assemble to form carbides, chromium and similar alloying elements nonetheless draw enormous amounts of carbon into their interstitial spaces. The carbon in the interstitial spaces of the alloy crystals makes the surface harder than ever achieved before by more conventional heat treating or diffusion process. The carbon solid solution manifests a Vickers hardness often exceeding 1000 HV (equivalent to 70 HRC). This project objective was to extend the LTCSS treatment to other austenitic alloys, and to quantify improvements in fatigue, corrosion, and wear resistance. Highlights from the research include the following: • Extension of the applicability of the LTCSS process to a broad range of austenitic and duplex grades of steels • Demonstration of LTCSS ability for a variety of different component shapes and sizes • Detailed microstructural characterization of LTCSS-treated samples of 316L and other alloys

  11. Magnetic resonance: safety measures and biological effects

    International Nuclear Information System (INIS)

    Gordillo, I.; Lafuente, J.; Fernandez, C.; Barbero, M.J.; Cascon, E.

    1997-01-01

    The biological effects of electromagnetic fields is currently a subject of great controversy. For this reason, magnetic resonance imaging (MRI) and spectroscopy are constantly under investigation. The source of the risk in MRI is associated with the three types of electromagnetic radiation to which the patient is exposed: the static magnetic field, variable (gradient) magnetic fields and radiofrequency fields. Each is capable of producing significant biological effects when employed at sufficient intensity. Patients exposed to risk sources are those situated within the lines of force of the magnetic field, ellipsoid lines that are arranged around the magnet, representing the strength of the surrounding field. To date, at the intensity normally utilized in MRI(<2T) and respecting the field limit recommendations established by the US Food and Drug Administration (FDA) for clinical use of this technique no adverse secondary biological effects have been reported. The known biological effects and other possible secondary effects are reviewed, and the recommended safety measures are discussed. (Author)

  12. Magnetic Field Response Measurement Acquisition System

    Science.gov (United States)

    Woodard, Stanley E.; Taylor,Bryant D.; Shams, Qamar A.; Fox, Robert L.

    2007-01-01

    This paper presents a measurement acquisition method that alleviates many shortcomings of traditional measurement systems. The shortcomings are a finite number of measurement channels, weight penalty associated with measurements, electrical arcing, wire degradations due to wear or chemical decay and the logistics needed to add new sensors. Wire degradation has resulted in aircraft fatalities and critical space launches being delayed. The key to this method is the use of sensors designed as passive inductor-capacitor circuits that produce magnetic field responses. The response attributes correspond to states of physical properties for which the sensors measure. Power is wirelessly provided to the sensing element by using Faraday induction. A radio frequency antenna produces a time-varying magnetic field used to power the sensor and receive the magnetic field response of the sensor. An interrogation system for discerning changes in the sensor response frequency, resistance and amplitude has been developed and is presented herein. Multiple sensors can be interrogated using this method. The method eliminates the need for a data acquisition channel dedicated to each sensor. The method does not require the sensors to be near the acquisition hardware. Methods of developing magnetic field response sensors and the influence of key parameters on measurement acquisition are discussed. Examples of magnetic field response sensors and the respective measurement characterizations are presented. Implementation of this method on an aerospace system is discussed.

  13. Radiation detection at very low temperature. DRTBT 1991 Aussois - Course collection

    International Nuclear Information System (INIS)

    Salce, B.; Godfrin, H.; Dumoulin, L.; Garoche, Pierre; Pannetier, B.; Equer, B.; Hubert, PH.; Urbina, C.; Lamarre, J.M.; Brison, J.P.; Lesueur, D.; Bret, J.L.; Ayela, F.; Coron, N.; Gonzalez-Mestres, L.

    1991-12-01

    This publication gather several courses which propose or address: Thermal conduction, Kapitza resistance, Metal-insulator transition, Thermal properties and specific heat at low temperature, Thermometry, Low temperature superconductors, Defects due to irradiations in solids, Semiconducting detectors, Techniques of protection of a measurement assembly at low temperatures against perturbations, Noise reduction by impedance matching converter at low temperature, Low noise electronics and measurement, Low radio-activities, SQUID and electrometer, Results and expectations related to bolometers, Infrared and sub-millimetre radiation in astrophysics, Neutrinos, dark matter and heavy ions

  14. Loss measurement and analysis for the prototype generator with HTS stator and permanent magnet rotor

    Energy Technology Data Exchange (ETDEWEB)

    Song, Peng, E-mail: songp10@mails.tsinghua.edu.cn [Applied Superconductivity Research Center, Department of Physics, Tsinghua University, Beijing 100084 (China); Qu, Timing, E-mail: tmqu@mail.tsinghua.edu.cn [Applied Superconductivity Research Center, Department of Physics, Tsinghua University, Beijing 100084 (China); Department of Mechanical Engineering, Tsinghua University, Key Laboratory for Advanced Materials Processing Technology, Ministry of Education, Beijing 100084 (China); Yu, Xiaoyu [Department of Mechanical Engineering, Tsinghua University, Key Laboratory for Advanced Materials Processing Technology, Ministry of Education, Beijing 100084 (China); Li, Longnian; Gu, Chen [Applied Superconductivity Research Center, Department of Physics, Tsinghua University, Beijing 100084 (China); Li, Xiaohang [Innova Superconductor Technology Co., Ltd., Beijing 100084 (China); Wang, Dewen; Hu, Boping [Beijing Zhong Ke San Huan Hi-Tech Co., Ltd., Beijing 100084 (China); Chen, Duxing [Department Fis, University Autonoma Barcelona, Barcelona 08193 (Spain); Han, Zhenghe [Applied Superconductivity Research Center, Department of Physics, Tsinghua University, Beijing 100084 (China)

    2013-11-15

    Highlights: •A novel prototype HTS generator with HTS armature windings was developed. •No-load loss and the iron loss at low temperature were measured. •The total loss at low temperature is much larger than the room temperature case. •The reason for no-load loss increment at low temperature is discussed. -- Abstract: A prototype HTS synchronous generator with a permanent magnet rotor and HTS armature windings was developed. The rated armature frequency is 10 Hz. The cryogenic Dewar is tightly surrounded outside the iron core. Both HTS coils and the iron core were cooled by using conduction cooling method. During the process of no-load running, the no-load loss power data were obtained through the torque measurement. The temperature evolution characteristics of the stator was measured by PT-100 temperature sensors. These results show that the no-load loss power at around 77 K are much larger than that at room temperature. The possible reason for the no-load loss increment is discussed. The ac loss power of one individual HTS coil used in this generator was also tested. Compared with the iron loss power, the ac loss power is rather small and could be neglected.

  15. Manufacturing Demonstration Facility: Low Temperature Materials Synthesis

    International Nuclear Information System (INIS)

    Graham, David E.; Moon, Ji-Won; Armstrong, Beth L.; Datskos, Panos G.; Duty, Chad E.; Gresback, Ryan; Ivanov, Ilia N.; Jacobs, Christopher B.; Jellison, Gerald Earle; Jang, Gyoung Gug; Joshi, Pooran C.; Jung, Hyunsung; Meyer, Harry M.; Phelps, Tommy

    2015-01-01

    The Manufacturing Demonstration Facility (MDF) low temperature materials synthesis project was established to demonstrate a scalable and sustainable process to produce nanoparticles (NPs) for advanced manufacturing. Previous methods to chemically synthesize NPs typically required expensive, high-purity inorganic chemical reagents, organic solvents and high temperatures. These processes were typically applied at small laboratory scales at yields sufficient for NP characterization, but insufficient to support roll-to-roll processing efforts or device fabrication. The new NanoFermentation processes described here operated at a low temperature (~60 C) in low-cost, aqueous media using bacteria that produce extracellular NPs with controlled size and elemental stoichiometry. Up-scaling activities successfully demonstrated high NP yields and quality in a 900-L pilot-scale reactor, establishing this NanoFermentation process as a competitive biomanufacturing strategy to produce NPs for advanced manufacturing of power electronics, solid-state lighting and sensors.

  16. Low temperature experiments in radiation biophysics

    International Nuclear Information System (INIS)

    Moan, J.

    1977-01-01

    The reasons for performing experiments in radiation biophysics at low temperatures, whereby electron spectra may be studied, are explained. The phenomenon of phosphorescence spectra observed in frozen aqueous solutions of tryptophan and adenosine is also described. Free radicals play an important part in biological radiation effects and may be studied by ESR spectroscopy. An ESR spectrum of T 1 bacteriophages irradiated dry at 130K is illustrated and discussed. Hydrogen atoms, which give lines on the spectrum, are believed to be those radiation products causing most biological damage in a dry system. Low temperature experiments are of great help in explaining the significance of direct and indirect effects. This is illustrated for the case of trypsin. (JIW)

  17. Dehydration of hydrated low-temperature tar

    Energy Technology Data Exchange (ETDEWEB)

    Yoshida, T

    1949-01-01

    Yoshida examined the mechanism of the dehydration of hydrated low-temperature tar with a microscope. The tar containing free carbon and coal dust is so stable that the removal of the above substances and water by a physical method is very difficult. Addition of light oil produced by fractionation of low-temperature tar facilitates the operations. Yoshida tried using the separate acid, neutral, and basic components of the light oil; the acid oil proved to be most effective. For many reasons it is convenient to use light oil as it is. In this method the quantity of light oil required is 2 to 3 times that of tar. But in supplementing the centrifugal method, the quantity of light oil needed might be only half the amount of tar.

  18. Manufacturing Demonstration Facility: Low Temperature Materials Synthesis

    Energy Technology Data Exchange (ETDEWEB)

    Graham, David E. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Moon, Ji-Won [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Armstrong, Beth L. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Datskos, Panos G. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Duty, Chad E. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Gresback, Ryan [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Ivanov, Ilia N. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Jacobs, Christopher B. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Jellison, Gerald Earle [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Jang, Gyoung Gug [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Joshi, Pooran C. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Jung, Hyunsung [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Meyer, III, Harry M. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Phelps, Tommy [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)

    2015-06-30

    The Manufacturing Demonstration Facility (MDF) low temperature materials synthesis project was established to demonstrate a scalable and sustainable process to produce nanoparticles (NPs) for advanced manufacturing. Previous methods to chemically synthesize NPs typically required expensive, high-purity inorganic chemical reagents, organic solvents and high temperatures. These processes were typically applied at small laboratory scales at yields sufficient for NP characterization, but insufficient to support roll-to-roll processing efforts or device fabrication. The new NanoFermentation processes described here operated at a low temperature (~60 C) in low-cost, aqueous media using bacteria that produce extracellular NPs with controlled size and elemental stoichiometry. Up-scaling activities successfully demonstrated high NP yields and quality in a 900-L pilot-scale reactor, establishing this NanoFermentation process as a competitive biomanufacturing strategy to produce NPs for advanced manufacturing of power electronics, solid-state lighting and sensors.

  19. Behaviour of polar crystals at low temperatures

    International Nuclear Information System (INIS)

    Drozhdin, S.N.; Novik, V.K.; Gavrilova, N.D.; Koptsik, V.A.; Popova, T.V.

    1975-01-01

    Temperature dependencies of pyrocoefficient for a wide class of various pyroactive crystals in the temperature range from 4,2 to 300 deg K were investigated. The problems to be solved were: to confirm a conclusion on the pyrocoefficient γsup(sigma) tending to zero at T → 0; to compare experimental data with conclusions of existing theories; to reveal specific features in the behaviour of both linear pyroelectrics and segnetoelectrics at low temperatures. The behaviour of the total pyrocoefficient for all crystals obeys the regularity γsup(sigma) → 0 at T → O. In the range of low temperatures the pyrocoefficient varies by the power law: γsup(sigma) approximately Tsup(α). For the majority of crystals studied α is close to 3. CdS, BeO, ZiNbO 3 and other crystals were studied

  20. Low-temperature conductivity of gadolinium sulfides

    Energy Technology Data Exchange (ETDEWEB)

    Mustafaeva, S. N., E-mail: solmust@gmail.com [Azerbaijan National Academy of Sciences, Institute of Physics (Azerbaijan); Asadov, S. M., E-mail: mirasadov@gmail.com [Azerbaijan National Academy of Sciences, Institute of Catalysis and Inorganic Chemistry (Azerbaijan)

    2016-09-15

    In samples of GdS{sub x} (x = 1.475–2) of various compositions, the conductivity temperature dependences are investigated for the case of direct current in the low-temperature region (4.2–225 K). The presence of the activation and activationless hopping mechanisms of charge transport over the band gap of the samples of GdS{sub x} phases is established. The parameters of localized states in GdS{sub x} are determined.

  1. Thermodynamic power stations at low temperatures

    Science.gov (United States)

    Malherbe, J.; Ployart, R.; Alleau, T.; Bandelier, P.; Lauro, F.

    The development of low-temperature thermodynamic power stations using solar energy is considered, with special attention given to the choice of the thermodynamic cycle (Rankine), working fluids (frigorific halogen compounds), and heat exchangers. Thermomechanical conversion machines, such as ac motors and rotating volumetric motors are discussed. A system is recommended for the use of solar energy for irrigation and pumping in remote areas. Other applications include the production of cold of fresh water from brackish waters, and energy recovery from hot springs.

  2. Crystal growth from low-temperature solutions

    International Nuclear Information System (INIS)

    Sangwal, K.

    1994-01-01

    The state of the art in crystal growth from solutions at low-temperatures has been done. The thermodynamic and kinetic parameters have been discussed in respect to different systems. The methods of crystal growth from water and organic solutions and different variants of their technical realizations have been reviewed. Also the growth by chemical reactions and gel growth have been described. The large number of examples have been shown. 21 refs, 30 figs, 3 tabs

  3. Composite Materials for Low-Temperature Applications

    Science.gov (United States)

    2008-01-01

    Composite materials with improved thermal conductivity and good mechanical strength properties should allow for the design and construction of more thermally efficient components (such as pipes and valves) for use in fluid-processing systems. These materials should have wide application in any number of systems, including ground support equipment (GSE), lunar systems, and flight hardware that need reduced heat transfer. Researchers from the Polymer Science and Technology Laboratory and the Cryogenics Laboratory at Kennedy Space Center were able to develop a new series of composite materials that can meet NASA's needs for lightweight materials/composites for use in fluid systems and also expand the plastic-additive markets. With respect to thermal conductivity and physical properties, these materials are excellent alternatives to prior composite materials and can be used in the aerospace, automotive, military, electronics, food-packaging, and textile markets. One specific application of the polymeric composition is for use in tanks, pipes, valves, structural supports, and components for hot or cold fluid-processing systems where heat flow through materials is a problem to be avoided. These materials can also substitute for metals in cryogenic and other low-temperature applications. These organic/inorganic polymeric composite materials were invented with significant reduction in heat transfer properties. Decreases of 20 to 50 percent in thermal conductivity versus that of the unmodified polymer matrix were measured. These novel composite materials also maintain mechanical properties of the unmodified polymer matrix. These composite materials consist of an inorganic additive combined with a thermoplastic polymer material. The intrinsic, low thermal conductivity of the additive is imparted into the thermoplastic, resulting in a significant reduction in heat transfer over that of the base polymer itself, yet maintaining most of the polymer's original properties. Normal

  4. Minimizing material damage using low temperature irradiation

    Science.gov (United States)

    Craven, E.; Hasanain, F.; Winters, M.

    2012-08-01

    Scientific advancements in healthcare driven both by technological breakthroughs and an aging and increasingly obese population have lead to a changing medical device market. Complex products and devices are being developed to meet the demands of leading edge medical procedures. Specialized materials in these medical devices, including pharmaceuticals and biologics as well as exotic polymers present a challenge for radiation sterilization as many of these components cannot withstand conventional irradiation methods. The irradiation of materials at dry ice temperatures has emerged as a technique that can be used to decrease the radiation sensitivity of materials. The purpose of this study is to examine the effect of low temperature irradiation on a variety of polymer materials, and over a range of temperatures from 0 °C down to -80 °C. The effectiveness of microbial kill is also investigated under each of these conditions. The results of the study show that the effect of low temperature irradiation is material dependent and can alter the balance between crosslinking and chain scission of the polymer. Low temperatures also increase the dose required to achieve an equivalent microbiological kill, therefore dose setting exercises must be performed under the environmental conditions of use.

  5. Computational Chemistry of Cyclopentane Low Temperature Oxidation

    KAUST Repository

    El Rachidi, Mariam

    2015-03-30

    Cycloalkanes are significant constituents of conventional fossil fuels, but little is known concerning their combustion chemistry and kinetics, particularly at low temperatures. This study investigates the pressure dependent kinetics of several reactions occurring during low-temperature cyclopentane combustion using theoretical chemical kinetics. The reaction pathways of the cyclopentyl + O2 adduct is traced to alkylhydroperoxide, cyclic ether, β-scission and HO2 elimination products. The calculations are carried out at the UCCSD(T)-F12b/cc-pVTZ-F12//M06-2X/6-311++G(d,p) level of theory. The barrierless entrance channel is treated using variable-reaction-coordinate transition state theory (VRC-TST) at the CASPT2(7e,6o) level of theory, including basis set, geometry relaxation and ZPE corrections. 1-D time-dependent multiwell master equation analysis is used to determine pressure-and temperature-dependent rate parameters of all investigated reactions. Tunneling corrections are included using Eckart barriers. Comparison with cyclohexane is used to elucidate the effect of ring size on the low temperature reactivity of naphthenes. The rate coefficients reported herein are suitable for use in cyclopentane and methylcyclopentane combustion models, even below ~900 K, where ignition is particularly sensitive to these pressure-dependent values.

  6. Neutron moderation at very low temperatures (1691)

    International Nuclear Information System (INIS)

    Lacaze, A.

    1961-04-01

    Starting from Harwell experiment carried out inside a low-power reactor, we intended to maintain a liquid hydrogen cell in a channel of the EL3 reactor (at Saclay) whose thermal neutrons flux is 10 14 neutrons/cm 2 /s. We tried to work out a device giving off an important beam of cold neutrons and able to operate in a way as automatic as possible during many consecutive day without a stop. Several circuits have already been achieved at very low temperatures but they brought out volumes and fluxes much lower than those we used this time. The difficulties we have met in carrying out such a device arose on the one hand from the very high energy release to which any kind of experiment is inevitably submitted when placed near the core of the reactor, on the other, hand from the very little room which is available in experimental channels of reactors. In such condition, it is necessary to use a moderator as effective as possible. This study is divided into three parts ; in the first part, we try to determine: a) conditions in which moderation takes place, hence the volume of the cell; b) materials likely to be used at low temperature and in pile; c) cooling system; hence we had to study fluid flow conditions at very low temperatures in very long ducts. The second part is devoted to the description of the device. The third part ventilates the results we have obtained. (author) [fr

  7. Low temperature surface chemistry and nanostructures

    Science.gov (United States)

    Sergeev, G. B.; Shabatina, T. I.

    2002-03-01

    The new scientific field of low temperature surface chemistry, which combines the low temperature chemistry (cryochemistry) and surface chemistry approaches, is reviewed in this paper. One of the most exciting achievements in this field of science is the development of methods to create highly ordered hybrid nanosized structures on different organic and inorganic surfaces and to encapsulate nanosized metal particles in organic and polymer matrices. We consider physical and chemical behaviour for the systems obtained by co-condensation of the components vapours on the surfaces cooled down to 4-10 and 70-100 K. In particular the size effect of both types, the number of atoms in the reactive species structure and the thickness of growing co-condensate film, on the chemical activity of the system is analysed in detail. The effect of the internal mechanical stresses on the growing interfacial co-condensate film formation and on the generation of fast (explosive) spontaneous reactions at low temperatures is discussed. The examples of unusual chemical interactions of metal atoms, clusters and nanosized particles, obtained in co-condensate films on the cooled surfaces under different conditions, are presented. The examples of highly ordered surface and volume hybrid nanostructures formation are analysed.

  8. Construction of an apparatus for nuclear orientation measurements at low temperatures. Application to neodymium-cobalt alloy; Realisation d'un appareil pour des mesures d'orientation nucleaire a basse temperature. Application a l'alliage neodyme-cobalt

    Energy Technology Data Exchange (ETDEWEB)

    Mayer, E [Commissariat a l' Energie Atomique, Grenoble (France). Centre d' Etudes Nucleaires

    1965-10-01

    We describe experiments along which has been studied the anisotropy of {gamma} radiations emitted by oriented nuclei. We have used the great hyperfine fields acting on nuclei in ferromagnetic metals so as to produce alignment at low temperature. By irradiation we obtained a few cobalt 60 nuclei in our samples which were then cooled down to 0,01 K. The anisotropic rate of the 1,33 MeV {gamma} radiation was measured in function of the sample temperature, using as thermometer the anisotropy of {gamma} radiation emitted by cobalt 60 nuclei in a cobalt single crystal. Cobalt 60 was lined up in a cobalt nickel alloy (40% Ni). The hyperfine field at the cobalt was measured compared to the effective field in metallic cobalt: Heff(Co Ni)/Heff(Co metal) = 0.71 {+-} 0.12. These results are in good agreement with specific heat measurements made previously. Cobalt 60 has been polarised in a neodymium-cobalt alloy (NdCo{sub 5}). The field at the cobalt in NdCo{sub 5} has been measured compared to the field in metallic cobalt and taking the non-saturation into account we found 165000 oersteds < Heff(NdCo{sub 5}) < 220000 oersteds. (author) [French] Nous decrivons des experiences au cours desquelles nous avons etudie l'anisotropie de rayonnements {gamma} emis par des noyaux orientes. Nous avons utilise les grands champs hyperfins agissant sur las noyaux dans les metaux ferromagnetiques pour produire l'alignement a basse temperature. Par irradiation nous avons obtenu quelques noyaux de cobalt 60 dans nos echantillons qui furent ensuite refroidis a 0,01 K. Le degre d'anisotropie du rayonnement {gamma} de 1,33 MeV fut mesure en fonction de la temperature de l'echantillon en utilisant l'anisotropie du rayonnement {gamma} de noyaux de cobalt 60 dans un monocristal de cobalt metallique utilise comme thermometre. Le cobalt 60 a ete aligne dans un alliage de cobalt-nickel (40% Ni). Le champ hyperfin au niveau du cobalt a ete mesure par rapport au champ effectif dans le cobalt metallique

  9. Device measures static friction of magnetic tape

    Science.gov (United States)

    Cole, P. T.

    1967-01-01

    Device measures the coefficient of static friction of magnetic tape over a range of temperatures and relative humidities. It uses a strain gage to measure the force of friction between a reference surface and the tape drawn at a constant velocity of approximately 0.0001 inch per second relative to the reference surface.

  10. The low temperature specific heat of Lu-Cu-Y metallic glasses

    International Nuclear Information System (INIS)

    Mohammed, K.A.; Lanchester, P.C.

    1987-01-01

    The specific heat of a series of amorphous metallic alloys of the form Lu x Cu 0.37 Y 0.36 (x=0, 0.1, 0.3 and 0.4) has been measured between 2 and 50 K, primarily in order to be able to determine the non-magnetic contributions to the specific heat in magnetic Re-Cu-Y amorphous alloys. The data at low temperature fit the simple form C p =γT+βT 3 from which values of γ and θ D (0) have been determined. Consideration is given to the error that arises if Y is used rather than Lu or La in forming non-magnetic rare earth intermetallics for purposes of determining the non-magnetic contributions to the specific heat of magnetic samples. A simple procedure is described that allows a useful improvement in accuracy in estimating non-magnetic contributions below 20 K if Y is used. The method may also be useful if only a restricted range of compositions using Lu is possible. (orig.)

  11. Low temperature specific heat of Lu-Cu-Y metallic glasses

    Energy Technology Data Exchange (ETDEWEB)

    Mohammed, K.A.; Lanchester, P.C.

    1987-02-01

    The specific heat of a series of amorphous metallic alloys of the form Lu/sub x/Cu/sub 0.37/Y/sub 0.36/ (x=0, 0.1, 0.3 and 0.4) has been measured between 2 and 50 K, primarily in order to be able to determine the non-magnetic contributions to the specific heat in magnetic Re-Cu-Y amorphous alloys. The data at low temperature fit the simple form C/sub p/=..gamma..T+..beta..T/sup 3/ from which values of ..gamma.. and theta/sub D/(0) have been determined. Consideration is given to the error that arises if Y is used rather than Lu or La in forming non-magnetic rare earth intermetallics for purposes of determining the non-magnetic contributions to the specific heat of magnetic samples. A simple procedure is described that allows a useful improvement in accuracy in estimating non-magnetic contributions below 20 K if Y is used. The method may also be useful if only a restricted range of compositions using Lu is possible.

  12. Model for the low-temperature magnetic phases observed in doped YBa2Cu3O6+x

    DEFF Research Database (Denmark)

    Andersen, N.H.; Uimin, G.

    1997-01-01

    A classical statistical model for the antiferromagnetic ordering of the Cu spins in the CuO2 planes of reduced YBa2Cu3O6+x-type materials is presented. The magnetic phases considered are the experimentally observed high-temperature antiferromagnetic (AFI) phase with ordering vector Q(I)=(1/2 1/2 0...

  13. Application of piezoceramic materials in low temperature scanning tunnel microscope

    International Nuclear Information System (INIS)

    Volodin, A.P.; Panich, A.E.

    1989-01-01

    Temperature dependences of the voltage-to-movement conversion coefficients for piezoceramic domestic materials PKR and TsTS-19 are measured using a capacitance dilatometer in the 0.4< T<300K temperature range. Anisotropy of thermal expansion of materials determined by the polarization vector is observed. Some recommendations concerning the use of the given materials in low-temperature scanning tunnel microscopes are given

  14. Low temperature specific heat anomalies in melanins and tumor melanosomes

    Energy Technology Data Exchange (ETDEWEB)

    Mizutani, U [Carnegie--Mellon Univ., Pittsburgh; Massalski, T B; McGinness, J E; Corry, P M

    1976-02-12

    Human malignant melanoma cells obtained at autopsy were used. Data indicate that melanins exhibit a large linear term (50-200 erg g/sup -1/K/sup -2/) and that they seem to undergo a phase transition as indicated by the heat capacity near 1.9/sup 0/K. A table is presented to show low temperature specific heat data for melanin samples. The measurements include two anomalies, a transition and an unusually high linear contribution. (HLW)

  15. Muonium in Al2O3 powder at low temperature

    International Nuclear Information System (INIS)

    Kiefl, R.F.; Warren, J.B.; Oram, C.J; Brewer, J.H.; Harshman, D.R.

    1982-04-01

    Measurements of muonium (μ + e - ) spin relaxation in a finely powdered sample of γ-Al 2 O 3 in a He (or Ne) atmosphere indicate that the muonium atoms escape the powder grains with a high efficiency at low temperatures (T < 30 K). The muonium spin relaxation rate is proportional to the fraction of the powder surface area not covered by adsorbed He (Ne)

  16. Electric-field-induced superconductivity detected by magnetization measurements of an electric-double-layer capacitor

    International Nuclear Information System (INIS)

    Kasahara, Yuichi; Takeuchi, Yuki; Ye, Jianting; Yuan, Hongtao; Shimotani, Hidekazu; Iwasa, Yoshihiro; Nishimura, Takahiro; Sato, Tatsuya

    2010-01-01

    We report evidence for superconductivity induced by the application of strong electric fields onto the surface of a band insulator, ZrNCl, provided by the observation of a shielding diamagnetic signal. We introduced an electric-double-layer capacitor configuration and in situ magnetization measurements at low temperatures as a method to detect the novel electric-field-induced superconducting state. The results showed excellent agreement with a previous report using a transistor configuration, demonstrating that the present technique is a novel method for investigating the nonequilibrium phase induced by electric fields. (author)

  17. CIME: last results of magnetic measurements

    International Nuclear Information System (INIS)

    Duval, M.

    1997-01-01

    This paper reports about the magnetic measurements recently finished at the CIME cyclotron. The measurements were carried out over two stages, first in January 1997 dedicated to the magnetic chart acquisition (for the main field only) and the other from 16 April to 2 June dedicated to the chart acquisition of the isochronous fields (main field + 11 correction magnetic coils). These charts have a closed enough meshing to ensure good interpolations and to define the current intensity values for any working point. This has been tested by measuring the fields calculated for a 18 O +4 beam. The results confirmed all the calculations done with TOSCA code. Calculations of current intensities for 11 isochronous coils were made by using only field response given by TOSCA for each coil and each induction level. (author)

  18. Experimental studies in solid state and low temperature physics. Progress report, 1975

    International Nuclear Information System (INIS)

    Goldman, A.M.; Weyhmann, W.V.; Zimmermann, W. Jr.

    1975-09-01

    Experimental investigations are being carried out in a broad area of low-temperature and solid-state physics which includes superconductivity, magnetism in metals and liquid and solid helium. The pair-field susceptibility of superconductors is being studied. A propagating mode in the phase of the superconducting order parameter has been found. Heat capacities of superconducting films in the vicinity of T/sub c/ are also being investigated. An investigation in the time-dependent high conductivity of dilute solid solutions of sodium in ammonia has been initiated. Nuclear orientation studies of the dilute magnetic impurity problem in metals in the 1 mK temperature region are being carried out. Refrigeration requirements for this work are being met using enhanced hyperfine nuclear cooling. Measurements of the differential osmotic pressure of 3 He/ 4 He liquid mixtures near the tricritical point have shown a peak in the ''concentration susceptibility'' at the lambda line. Data obey a simple tricritical scaling relation. The dynamics of superfluid flow through submicron pores are being studied in both pure 4 He and in 3 He/ 4 He mixtures in an apparatus provided with a 3 He refrigerator. The quantization of circulation in superfluid liquid 4 He is being investigated using the Vinen method. The low temperature heat capacity of bcc solid 3 He is being studied

  19. The significance of vector magnetic field measurements

    Science.gov (United States)

    Hagyard, M. J.

    1990-01-01

    Observations of four flaring solar active regions, obtained during 1980-1986 with the NASA Marshall vector magnetograph (Hagyard et al., 1982 and 1985), are presented graphically and characterized in detail, with reference to nearly simultaneous Big Bear Solar Observatory and USAF ASW H-alpha images. It is shown that the flares occurred where local photospheric magnetic fields differed most from the potential field, with initial brightening on either side of a magnetic-neutral line near the point of maximum angular shear (rather than that of maximum magnetic-field strength, typically 1 kG or greater). Particular emphasis is placed on the fact that these significant nonpotential features were detected only by measuring all three components of the vector magnetic field.

  20. On the measurement of magnetic viscosity

    Energy Technology Data Exchange (ETDEWEB)

    Serletis, C. [Department of Physics, Aristotle University, Thessaloniki 54124 (Greece); Efthimiadis, K.G., E-mail: kge@auth.gr [Department of Physics, Aristotle University, Thessaloniki 54124 (Greece)

    2012-08-15

    This work is an investigation of the experimental method used for measuring the magnetic viscosity in a hard ferromagnetic material, i.e. the recording of the magnetization under constant applied field and temperature, after the material has been magnetically saturated. It investigates how the experimental results are affected by the initial conditions of the method (saturation field, field change rate and field oscillation prior to its stabilization), and by minor variations of field and temperature during the recording. Based on the arising conclusions and the use of a more complex fitting function of measurements, the accuracy and repeatability of experimental results is improved. - Highlights: Black-Right-Pointing-Pointer Magnetic viscosity is affected by initial measurement conditions. Black-Right-Pointing-Pointer Minor field deviations prior to its stabilization cause large changes in viscosity. Black-Right-Pointing-Pointer Viscosity is strongly dependent on the field change rate from saturation to the measurement field. Black-Right-Pointing-Pointer Small changes in field and temperature during the experiment can lead to false measurements. Black-Right-Pointing-Pointer Errors in measurements can be eliminated through the use of a proper fitting function.

  1. Absolute method of measuring magnetic susceptibility

    Science.gov (United States)

    Thorpe, A.; Senftle, F.E.

    1959-01-01

    An absolute method of standardization and measurement of the magnetic susceptibility of small samples is presented which can be applied to most techniques based on the Faraday method. The fact that the susceptibility is a function of the area under the curve of sample displacement versus distance of the magnet from the sample, offers a simple method of measuring the susceptibility without recourse to a standard sample. Typical results on a few substances are compared with reported values, and an error of less than 2% can be achieved. ?? 1959 The American Institute of Physics.

  2. Spin-state crossover and low-temperature magnetic state in yttrium-doped Pr.sub.0.7./sub.Ca.sub.0.3./sub.CoO.sub.3./sub..

    Czech Academy of Sciences Publication Activity Database

    Knížek, Karel; Hejtmánek, Jiří; Maryško, Miroslav; Novák, Pavel; Šantavá, Eva; Jirák, Zdeněk; Naito, T.; Fujishiro, H.; de la Cruz, C.

    2013-01-01

    Roč. 88, DEC (2013), "224412-1"-"224412-8" ISSN 1098-0121 R&D Projects: GA ČR(CZ) GAP204/11/0713 Institutional support: RVO:68378271 Keywords : cobaltites * mixed valence * spin state Subject RIV: BM - Solid Matter Physics ; Magnetism Impact factor: 3.664, year: 2013 http://prb.aps.org/abstract/PRB/v88/i22/e224412

  3. Low temperature photoresponse of monolayer tungsten disulphide

    Directory of Open Access Journals (Sweden)

    Bingchen Cao

    2014-11-01

    Full Text Available High photoresponse can be achieved in monolayers of transition metal dichalcogenides. However, the response times are inconveniently limited by defects. Here, we report low temperature photoresponse of monolayer tungsten disulphide prepared by exfoliation and chemical vapour deposition (CVD method. The exfoliated device exhibits n-type behaviour; while the CVD device exhibits intrinsic behaviour. In off state, the CVD device has four times larger ratio of photoresponse for laser on/off and photoresponse decay–rise times are 0.1 s (limited by our setup, while the exfoliated device has few seconds. These findings are discussed in terms of charge trapping and localization.

  4. Low-temperature preparation of pyrolytic carbon

    International Nuclear Information System (INIS)

    Kidd, R.W.; Seifert, D.A.; Browning, M.F.

    1984-01-01

    Previous studies have demonstrated that nuclear waste forms coated with chemical vapor deposited pyrolytic carbon (PyC) at about 1273 K can provide ground water leach protection. To minimize the release during coating of volatile material from the waste forms and permit the coating of waste forms with a low softening point, a study was initiated to develop parameters for the catalytic deposition of PyC at low temperatures. The parameters surveyed in a fluidized-bed coater were deposition temperatures, carbon precursors, catalyst, diluent gas, concentration, and pressure

  5. Investigations of Low Temperature Time Dependent Cracking

    Energy Technology Data Exchange (ETDEWEB)

    Van der Sluys, W A; Robitz, E S; Young, B A; Bloom, J

    2002-09-30

    The objective of this project was to investigate metallurgical and mechanical phenomena associated with time dependent cracking of cold bent carbon steel piping at temperatures between 327 C and 360 C. Boiler piping failures have demonstrated that understanding the fundamental metallurgical and mechanical parameters controlling these failures is insufficient to eliminate it from the field. The results of the project consisted of the development of a testing methodology to reproduce low temperature time dependent cracking in laboratory specimens. This methodology was used to evaluate the cracking resistance of candidate heats in order to identify the factors that enhance cracking sensitivity. The resultant data was integrated into current available life prediction tools.

  6. Ionometric determination of fluorides at low temperatures

    International Nuclear Information System (INIS)

    Kostyukova, I.S.; Ennan, A.A.; Dzerzhko, E.K.; Leivikova, A.A.

    1995-01-01

    A method for determining fluoride ions in solution at low temperatures using a solid-contact fluorine-selective electrode (FSE) has been developed. The effect of temperature (60 to -15 degrees C) on the calibration slope, potential equilibrium time, and operational stability is studied; the effect of an organic additive (cryoprotector) on the calibration slope is also studied. The temperature relationships obtained for the solid-contact FSEs allow appropriate corrections to be applied to the operational algorithm of the open-quotes Ftoringclose quotes hand-held semiautomatic HF gas analyzer for the operational temperature range of -16 to 60 degrees C

  7. Low-temperature centrifugal helium compressor

    International Nuclear Information System (INIS)

    Kawada, M.; Togo, S.; Akiyama, Y.; Wada, R.

    1974-01-01

    A centrifugal helium compressor with gas bearings, which can be operated at the temperature of liquid nitrogen, has been investigated. This compressor has the advantages that the compression ratio should be higher than the room temperature operation and that the contamination of helium could be eliminated. The outer diameter of the rotor is 112 mm. The experimental result for helium gas at low temperature shows a flow rate of 47 g/s and a compression ratio of 1.2 when the inlet pressure was 1 ata and the rotational speed 550 rev/s. The investigation is now focused on obtaining a compression ratio of 1.5. (author)

  8. Low-temperature creep of austenitic stainless steels

    Science.gov (United States)

    Reed, R. P.; Walsh, R. P.

    2017-09-01

    Plastic deformation under constant load (creep) in austenitic stainless steels has been measured at temperatures ranging from 4 K to room temperature. Low-temperature creep data taken from past and unreported austenitic stainless steel studies are analyzed and reviewed. Creep at cryogenic temperatures of common austenitic steels, such as AISI 304, 310 316, and nitrogen-strengthened steels, such as 304HN and 3116LN, are included. Analyses suggests that logarithmic creep (creep strain dependent on the log of test time) best describe austenitic stainless steel behavior in the secondary creep stage and that the slope of creep strain versus log time is dependent on the applied stress/yield strength ratio. The role of cold work, strain-induced martensitic transformations, and stacking fault energy on low-temperature creep behavior is discussed. The engineering significance of creep on cryogenic structures is discussed in terms of the total creep strain under constant load over their operational lifetime at allowable stress levels.

  9. Mechanical behavior and fatigue in polymeric composites at low temperatures

    International Nuclear Information System (INIS)

    Katz, Y.; Bussiba, A.; Mathias, H.

    1986-01-01

    Advanced fiber reinforced polymeric composite materials are often suggested as structural materials at low temperature. In this study, graphite epoxy and Kevlar-49/epoxy systems were investigated. Fatigue behavior was emphasized after establishing the standard monotonic mechanical properties, including fracture resistance parameters at 77, 190, and 296 K. Tension-tension fatigue crack propagation testing was carried out at nominal constant stress intensity amplitudes using precracked compact tensile specimens. The crack tip damage zone was measured and tracked by an electro-potential device, opening displacement gage, microscopic observation, and acoustic emission activity recording. Fractograhic and metallographic studies were performed with emphasis on fracture morphology and modes, failure processes, and description of sequential events. On the basis of these experimental results, the problem of fatigue resistance, including low temperature effects, is analyzed and discussed. The fundamental concepts of fatigue in composites are assessed, particularly in terms of fracture mechanics methods

  10. Mechanical equipment for magnet measurement and alignment

    International Nuclear Information System (INIS)

    Harvey, A.

    1992-05-01

    The mechanical equipment for measuring and aligning (or fiducializing) magnets is described by reference to devices designed and built by a number of laboratories. Some of these are now available commercially. The descriptions are supplemented by a list of representative sources of hardware

  11. Nitrous oxide emissions at low temperatures

    International Nuclear Information System (INIS)

    Martikainen, P.J.

    2002-01-01

    Microbial processes in soil are generally stimulated by temperature, but at low temperatures there are anomalies in the response of microbial activities. Soil physical-chemical characteristics allow existence of unfrozen water in soil also at temperatures below zero. Therefore, some microbial activities, including those responsible for nitrous oxide (N 2 0) production, can take place even in 'frozen' soil. Nitrous oxide emissions during winter are important even in boreal regions where they can account for more than 50% of the annual emissions. Snow pack therefore has great importance for N 2 0 emissions, as it insulates soil from the air allowing higher temperatures in soil than in air, and possible changes in snoav cover as a result of global warming would thus affect the N 2 0 emission from northern soils. Freezing-thawing cycles highly enhance N 2 0 emissions from soil, probably because microbial nutrients, released from disturbed soil aggregates and lysed microbial cells, support microbial N 2 0 production. However, the overall interactions between soil physics, chemistry, microbiology and N 2 0 production at low temperatures, including effects of freezing-thawing cycles, are still poorly known. (au)

  12. Efficient prepreg recycling at low temperatures

    Science.gov (United States)

    Pannkoke, Kord; Oethe, Marcus; Busse, Jürgen

    When manufacturing fibre reinforced plastics engineers are still confronted with a lack of experience concerning efficient recycling methods for prepreg cutting waste. Normally, the prepregs are cured and subsequently milled to use them as a filler material for polymers. However, this method is expensive and it is difficult to find applications for the milled FRP. An alternative method to recycle CFRP prepregs will be presented in this paper. Cutting the uncured prepreg waste was done by means of a saw mill which was cooled down to low temperatures. Working temperatures of -30°C are sufficient to harden the uncured resin and to achieve cuttable prepregs. Furthermore, post-curing during the cutting process is avoided with this technique. The result is a `cotton'-like matted structure with random fibre orientation and fibre length distribution. Subsequent curing was done by means of a press and an autoclave, respectively. It will be shown by means of tension and bending tests that low-temperature cutting of uncured prepregs is a way to partly conserve the high valuation of FRP during recycling. Furthermore, it offers possibilities for various applications.

  13. Extreme low temperature tolerance in woody plants

    Directory of Open Access Journals (Sweden)

    George Richard Strimbeck

    2015-10-01

    Full Text Available Woody plants in boreal to arctic environments and high mountains survive prolonged exposure to temperatures below -40˚C and minimum temperatures below -60˚C, and laboratory tests show that many of these species can also survive immersion in liquid nitrogen at -196˚C. Studies of biochemical changes that occur during acclimation, including recent proteomic and metabolomic studies, have identified changes in carbohydrate and compatible solute concentrations, membrane lipid composition, and proteins, notably dehydrins, that may have important roles in survival at extreme low temperature. Consideration of the biophysical mechanisms of membrane stress and strain lead to the following hypotheses for cellular and molecular mechanisms of survival at extreme low temperature: 1. Changes in lipid composition stabilize membranes at temperatures above the lipid phase transition temperature (-20 to 30˚C, preventing phase changes that result in irreversible injury. 2. High concentrations of oligosaccharides promote vitrification or high viscosity in the cytoplasm in freeze-dehydrated cells, which would prevent deleterious interactions between membranes. 3. Dehydrins bind membranes and further promote vitrification or act stearically to prevent membrane-membrane interactions.

  14. Computational Chemistry of Cyclopentane Low Temperature Oxidation

    KAUST Repository

    El Rachidi, Mariam; Zá dor, Judit; Sarathy, Mani

    2015-01-01

    reactions occurring during low-temperature cyclopentane combustion using theoretical chemical kinetics. The reaction pathways of the cyclopentyl + O2 adduct is traced to alkylhydroperoxide, cyclic ether, β-scission and HO2 elimination products. The calculations are carried out at the UCCSD(T)-F12b/cc-pVTZ-F12//M06-2X/6-311++G(d,p) level of theory. The barrierless entrance channel is treated using variable-reaction-coordinate transition state theory (VRC-TST) at the CASPT2(7e,6o) level of theory, including basis set, geometry relaxation and ZPE corrections. 1-D time-dependent multiwell master equation analysis is used to determine pressure-and temperature-dependent rate parameters of all investigated reactions. Tunneling corrections are included using Eckart barriers. Comparison with cyclohexane is used to elucidate the effect of ring size on the low temperature reactivity of naphthenes. The rate coefficients reported herein are suitable for use in cyclopentane and methylcyclopentane combustion models, even below ~900 K, where ignition is particularly sensitive to these pressure-dependent values.

  15. Multichannel simultaneous magnetic induction measurement system (MUSIMITOS)

    International Nuclear Information System (INIS)

    Steffen, Matthias; Leonhardt, Steffen; Heimann, Konrad; Bernstein, Nina

    2008-01-01

    Non-contact heart and lung activity monitoring would be a desirable supplement to conventional monitoring techniques. Based on the potential of non-contact magnetic induction measurements, requirements for an adequate monitoring system were estimated. This formed the basis for the development of the presented extendable multichannel simultaneous magnetic induction measurement system (MUSIMITOS). Special focus was given to the dynamic behaviour and simultaneous multichannel measurements, so that the system allows for up to 14 receiver coils working simultaneously at 6 excitation frequencies. Moreover, a real-time software concept for online signal processing visualization in combination with a fast software demodulation is presented. Finally, first steps towards a clinical application are pointed out and technical performance as well as first in vivo measurements are presented. This paper covers some aspects previously presented in Steffen and Leonhardt (2007 Proc. 13th Int. Conf. on Electrical Bioimpedance and the 8th Conf. on Electrical Impedance Tomography, Graz 2007)

  16. Measurement accuracy in shielded magnetic fields

    International Nuclear Information System (INIS)

    Bottauscio, Oriano; Chiampi, Mario; Crotti, Gabriella; Zucca, Mauro

    2005-01-01

    The measurement error due to both the probe size averaging effect and the coil arrangement is investigated when magnetic field measurements are performed in close proximity to different planar shields. The analysis is carried on through a hybrid FEM/BEM model which employs the 'thin shield' technique. Ferromagnetic, pure conductive and multilayer screens are taken into consideration and an estimation of the errors for concentric and non-concentric coil probes is given. The numerical results are validated by experiments

  17. Magnetic field measurements in xi Bootis A

    International Nuclear Information System (INIS)

    Boesgaard, A.M.; Chesley, D.; Preston, G.W.

    1975-01-01

    Four Zeeman spectrograms from Lick Observatory of xi Boo A and two of iota Peg at 2 A mm -1 have been measured to determine if a weak magnetic field is present in xi Boo A. The results indicate that the field is too weak to be measured by this technique on these spectrograms, although remeasurements of spectrograms from Mauna Kea at 3.4 A mm -1 still give a positive field of 170 gauss. (U.S.)

  18. Low-Temperature Co-Fired Unipoled Multilayer Piezoelectric Transformers.

    Science.gov (United States)

    Gao, Xiangyu; Yan, Yongke; Carazo, Alfredo Vazquez; Dong, Shuxiang; Priya, Shashank

    2018-03-01

    The reliability of piezoelectric transformers (PTs) is dependent upon the quality of fabrication technique as any heterogeneity, prestress, or misalignment can lead to spurious response. In this paper, unipoled multilayer PTs were investigated focusing on high-power composition and co-firing profile in order to provide low-temperature synthesized high-quality device measured in terms of efficiency and power density. The addition of 0.2 wt% CuO into Pb 0.98 Sr 0.02 (Mg 1/3 Nb 2/3 ) 0.06 (Mn 1/3 Nb 2/3 ) 0.06 (Zr 0.48 Ti 0.52 ) 0.88 O 3 (PMMnN-PZT) reduces the co-firing temperature from 1240 °C to 930 °C, which allows the use of Ag/Pd inner electrode instead of noble Pt inner electrode. Low-temperature synthesized material was found to exhibit excellent piezoelectric properties ( , , %, pC/N, and °C). The performance of the PT co-fired with Ag/Pd electrode at 930 °C was similar to that co-fired at 1240 °C with Pt electrode (25% reduction in sintering temperature). Both high- and low-temperature synthesized PTs demonstrated 5-W output power with >90% efficiency and 11.5 W/cm 3 power density.

  19. New developments in low temperature physics New developments in low temperature physics

    Science.gov (United States)

    Hallock, Bob; Paalanenn, Mikko

    2009-04-01

    Below you will find part of the activity report to the IUPAP General Assembly, October 2008, by the present and previous Chairmen of C5. It provides an overview of the most important and recent developments in low temperature physics, much in line with the program of LT25. For the field of experimental low temperature physics, the ability to conduct research has been damaged by the dramatic increase in the price of liquid helium. In the USA, for example, the price of liquid helium has approximately doubled over the past two years. This has led to a reduction in activity in many laboratories as the funding agencies have not quickly increased support in proportion. The increase in price of liquid helium has accelerated interest in the development and use of alternative cooling systems. In particular, pulse-tube coolers are now available that will allow cryostats with modest cooling needs to operate dilution refrigerators without the need for repeated refills of liquid helium from external supply sources. Solid helium research has seen a dramatic resurgence. Torsional oscillator experiments have been interpreted to show that solid helium may undergo a transition to a state in which some of the atoms in the container do not follow the motion of the container, e.g. may be 'supersolid'. The observation is robust, but the interpretation is controversial. The shear modulus of solid helium undergoes a similar signature with respect to temperature. Experiments that should be expected to cause helium to flow give conflicting results. Theory predicts that a perfect solid cannot show supersolid behavior, but novel superfluid-like behavior should be seen in various defects that can exist in the solid, and vorticity may play a significant role. And, recently there have been reports of unusual mass decoupling in films of pure 4He on graphite surfaces as well as 3He- 4He mixture films on solid hydrogen surfaces. These may be other examples of unusual superfluid-like behavior. There

  20. Self-contained high-pressure chambers for study on the Moessbauer effect at low temperatures

    International Nuclear Information System (INIS)

    Stepanov, G.N.

    1980-01-01

    Designs of two high-pressure chambers intended for studying the Moessbauer effect at low temperatures are described. The high-pressure chamber of the Bridgman anvil type is made of non magnetic materials and intended for operation at helium temperatures. The chamber employs a superconducting pressure gage. A sample and superconducting pressure gage are surrounded with a liquid medium of a high pressure at a room temperature. Measurements of the pressure were taken during heating the chamber in the vapours of liquid helium according to the known dependence of the lead superconducting transition temperature on pressure. The other high-pressure chamber of the piston-to-cylinder type can be used to study the Moessbauer effect at temperatures ranging from 4 to 300 K. Pressure in the chamber is measured by means of the superconducting pressure gage. The maximum pressure obtained in the chamber constitutes 25 kbar

  1. Field measuring probe for SSC magnets

    International Nuclear Information System (INIS)

    Ganetis, G.; Herrera, J.; Hogue, R.; Skaritka, J.; Wanderer, P.; Willen, E.

    1987-01-01

    The field probe developed for measuring the field in SSC dipole magnets is an adaptation of the rotating tangential coil system in use at Brookhaven for several years. Also known as the MOLE, it is a self-contained room-temperature mechanism that is pulled through the aperture of the magnet with regular stops to measure the local field. Several minutes are required to measure the field at each point. The probe measures the multipole components of the field as well as the field angle relative to gravity. The sensitivity of the coil and electronics is such that the field up to the full 6.6 T excitation of the magnet as well as the field when warm with only 0.01 T excitation can be measured. Tethers are attached to both ends of the probe to carry electrical connections and to supply dry nitrogen to the air motors that rotate the tangential windings as well as the gravity sensor. A small computer is attached to the probe for control and for data collection, analysis and storage

  2. Programming Enhancements for Low Temperature Thermal Decomposition Workstation

    Energy Technology Data Exchange (ETDEWEB)

    Igou, R.E.

    1998-10-01

    This report describes a new control-and-measurement system design for the Oak Ridge Y-12 Plant's Low Temperature Thermal Decomposition (LTTD) process. The new design addresses problems with system reliability stemming from equipment obsolescence and addresses specific functional improvements that plant production personnel have identified, as required. The new design will also support new measurement techniques, which the Y-12 Development Division has identified for future operations. The new techniques will function in concert with the original technique so that process data consistency is maintained.

  3. Programming Enhancements for Low Temperature Thermal Decomposition Workstation

    International Nuclear Information System (INIS)

    Igou, R.E.

    1998-01-01

    This report describes a new control-and-measurement system design for the Oak Ridge Y-12 Plant's Low Temperature Thermal Decomposition (LTTD) process. The new design addresses problems with system reliability stemming from equipment obsolescence and addresses specific functional improvements that plant production personnel have identified, as required. The new design will also support new measurement techniques, which the Y-12 Development Division has identified for future operations. The new techniques will function in concert with the original technique so that process data consistency is maintained

  4. Low temperature distillation of coal, shale, etc

    Energy Technology Data Exchange (ETDEWEB)

    1938-08-12

    A process is disclosed for the low temperature distillation of solid carbonaceous fuels, such as coal, lignite, shale or the like, which comprises feeding or supplying the comminuted fuel in the form of a layer of shallow depth to drying and distilling zones in succession moving the fuel forward through the zones, submitting it to progressively increasing nonuniform heating therein by combustion gases supplied to the distillation zone and traveling thence to the drying zone, the gases heating the distillation zone indirectly and the drying zone both indirectly and then directly such that the fuel retains its solid discrete form during substantially the whole of its travel through the drying and distillation zones, subjecting the fuel for a portion of its travel to a zigzag ploughing and propelling movement on a heated sole, and increasing the heating so as to cause fusion of the fuel immediately prior to its discharge from the distillation zone.

  5. On Low-temperature Polyamorphous transformations

    International Nuclear Information System (INIS)

    Bakay, A.S.

    2006-01-01

    A theory of polyamorphous transformations in glasses is constructed in the framework of a model of heterophase fluctuations with allowance for the fact that a glass inherits the short- and intermediate-range order from the liquid. A multicomponent order parameter describing the concentration of fluctuons with different types of short-range order is introduced, along with the concepts of isoconfigurational and non-isoconfigurational transitions in the glass. Taking the nonergodicity, nonequilibrium, and multiplicity of structural states of a glass into account leads to a kinetic criterion of observability of polyamorphism of a glass. As an example, a theory is constructed for the low-temperature first-order phase transition in an orientational glass based on doped fullerite. The relaxation processes of this system are described, including the subsystem of tunneling states. The possibility of a hierarchy of polyamorphous transformations in a glass is discussed

  6. Shock waves in helium at low temperatures

    International Nuclear Information System (INIS)

    Liepmann, H.W.; Torczynski, J.R.

    1986-01-01

    Results are reported from studies of the properties of low temperature He-4 using shock waves as a probe. Ideal shock tube theory is used to show that sonic speeds of Mach 40 are attainable in He at 300 K. Viscosity reductions at lower temperatures minimize boundary layer effects at the side walls. A two-fluid model is described to account for the phase transition which He undergoes at temperatures below 2.2 K, after which the quantum fluid (He II) and the normal compressed superfluid (He I) coexist. Analytic models are provided for pressure-induced shocks in He I and temperature-induced shock waves (called second sound) which appear in He II. The vapor-fluid interface of He I is capable of reflecting second and gasdynamic sound shocks, which can therefore be used as probes for studying phase transitions between He I and He II. 17 references

  7. Preparation of silver nanoparticles at low temperature

    Energy Technology Data Exchange (ETDEWEB)

    Mishra, Mini, E-mail: mishramini5@gmail.com [Centre of Environmental Science, Department of Botany, University of Allahabad, Allahabad, U.P. (India); Chauhan, Pratima, E-mail: mangu167@yahoo.co.in [Department of Physics, University of Allahabad, Allahabad U.P. (India)

    2016-04-13

    Silver from ancient time is used as antimicrobial agent in the bulk form but now with the advancement in nanotechnology silver in the form of nanoparticles shown potential effect against microbes which make us easy to fight with many diseases plants and animals. In this work silver nanoparticles were synthesized by chemical routes using sodium borohydride as reducing agent at low temperature. The particles were characterized through UV-Visible spectroscopy as well as X-Ray Diffraction. The UV-visible spectra of silver nanoparticles exhibited absorption at 425 cm; the crystallite size of the particles is between 19nm to 39nm. EDAX graph shows two peaks of silver and oxygen. Water absorbed by silver nanoparticles was removed by the calcinations.

  8. Preparation of silver nanoparticles at low temperature

    International Nuclear Information System (INIS)

    Mishra, Mini; Chauhan, Pratima

    2016-01-01

    Silver from ancient time is used as antimicrobial agent in the bulk form but now with the advancement in nanotechnology silver in the form of nanoparticles shown potential effect against microbes which make us easy to fight with many diseases plants and animals. In this work silver nanoparticles were synthesized by chemical routes using sodium borohydride as reducing agent at low temperature. The particles were characterized through UV-Visible spectroscopy as well as X-Ray Diffraction. The UV-visible spectra of silver nanoparticles exhibited absorption at 425 cm; the crystallite size of the particles is between 19nm to 39nm. EDAX graph shows two peaks of silver and oxygen. Water absorbed by silver nanoparticles was removed by the calcinations.

  9. Desalination by very low temperature nuclear heat

    International Nuclear Information System (INIS)

    Saari, Risto

    1977-01-01

    A new sea water desalination method has been developed: Nord-Aqua Vacuum Evaporation, which utilizes waste heat at a very low temperature. The requisite vacuum is obtained by the aid of a barometric column and siphon, and the dissolved air is removed from the vacuum by means of water flows. According to test results from a pilot plant, the process is operable if the waste heat exists at a temperature 7degC higher than ambient. The pumping energy which is then required is 9 kcal/kg, or 1.5% of the heat of vaporization of water. Calculations reveal that the method is economically considerably superior to conventional distilling methods. (author)

  10. Low temperature distillation of powdered materials

    Energy Technology Data Exchange (ETDEWEB)

    1929-04-11

    In the low temperature distillation of powdered material such as coal, brown coal, or oil shale, dust carried by the gases and vapors is precipitated by supplying liquid hydrocarbons to the effluent gases, for example, to a dust remover through which the distillates pass. The material is supplied through a hopper and moved through a retort by a worm feed, and is discharged into a sump. Scavenging gases such as steam may be introduced through a pipe. Two conveyor worms moving in opposite directions are provided in an outlet conduit which may be surrounded by a cooling jacket. Heavy hydrocarbons condense on the walls of the conduit and on the conveyor worms and serve as dust catchers for the distillates, the lighted volatiles escaping through an outlet. The high boiling point oils flow back to and are cracked in the retort. Oils such as tar oils may be sprayed into the conduit or directly adjacent the entry of the material from feeding hopper.

  11. Installation for low temperature vapor explosion experiment

    International Nuclear Information System (INIS)

    Nilsuwankosit, Sunchai; Archakositt, Urith

    2000-01-01

    A preparation for the experiment on the low temperature vapor explosion was planned at the department of Nuclear Technology, Chulalongkorn University, Thailand. The objective of the experiment was to simulate the interaction between the molten fuel and the volatile cooling liquid without resorting to the high temperature. The experiment was expected to involve the injection of the liquid material at a moderate temperature into the liquid material with the very low boiling temperature in order to observe the level of the pressurization as a function of the temperatures and masses of the applied materials. For this purpose, the liquid nitrogen and the water were chosen as the coolant and the injected material for this experiment. Due to the size of the installation and the scale of the interaction, only lumped effect of various parameters on the explosion was expected from the experiment at this initial stage. (author)

  12. Biomedical applications using low temperature plasma technology

    International Nuclear Information System (INIS)

    Dai Xiujuan; Jiang Nan

    2006-01-01

    Low temperature plasma technology and biomedicine are two different subjects, but the combination of the two may play a critical role in modern science and technology. The 21 st century is believed to be a biotechnology century. Plasma technology is becoming a widely used platform for the fabrication of biomaterials and biomedical devices. In this paper some of the technologies used for material surface modification are briefly introduced. Some biomedical applications using plasma technology are described, followed by suggestions as to how a bridge between plasma technology and biomedicine can be built. A pulsed plasma technique that is used for surface functionalization is discussed in detail as an example of this kind of bridge or combination. Finally, it is pointed out that the combination of biomedical and plasma technology will be an important development for revolutionary 21st century technologies that requires different experts from different fields to work together. (authors)

  13. Low-temperature geothermal resources of Washington

    Energy Technology Data Exchange (ETDEWEB)

    Schuster, J.E. [Washington State Dept. of Natural Resources, Olympia, WA (United States). Div. of Geology and Earth Resources; Bloomquist, R.G. [Washington State Energy Office, Olympia, WA (United States)

    1994-06-01

    This report presents information on the location, physical characteristics, and water chemistry of low-temperature geothermal resources in Washington. The database includes 941 thermal (>20C or 68F) wells, 34 thermal springs, lakes, and fumaroles, and 238 chemical analyses. Most thermal springs occur in the Cascade Range, and many are associated with stratovolcanoes. In contrast, 97 percent of thermal wells are located in the Columbia Basin of southeastern Washington. Some 83.5 percent are located in Adams, Benton, Franklin, Grant, Walla Walla, and Yakima Counties. Yakima County, with 259 thermal wells, has the most. Thermal wells do not seem to owe their origin to local sources of heat, such as cooling magma in the Earth`s upper crust, but to moderate to deep circulation of ground water in extensive aquifers of the Columbia River Basalt Group and interflow sedimentary deposits, under the influence of a moderately elevated (41C/km) average geothermal gradient.

  14. Low-temperature glycerolysis of avocado oil

    Science.gov (United States)

    Satriana, Arpi, Normalina; Supardan, Muhammad Dani; Gustina, Rizka Try; Mustapha, Wan Aida Wan

    2018-04-01

    Glycerolysis can be a useful technique for production of mono- and diacylglycerols from triacylglycerols present in avocado oil. In the present work, the effect of catalyst and co-solvent concentration on low-temperature glycerolysis of avocado oil was investigated at 40oC of reaction temperature. A hydrodynamic cavitation system was used to enhance the miscibility of the oil and glycerol phases. NaOH and acetone were used as catalyst and co-solvent, respectively. The experimental results showed that the catalyst and co-solvent concentration affected the glycerolysis reaction rate. The catalyst concentration of 1.5% and co-solvent concentration of 300% were the optimised conditions. A suitable amount of NaOH and acetone must be added to achieve an optimum of triacylglycerol conversion.

  15. Low Temperature Waste Immobilization Testing Vol. I

    Energy Technology Data Exchange (ETDEWEB)

    Russell, Renee L.; Schweiger, Michael J.; Westsik, Joseph H.; Hrma, Pavel R.; Smith, D. E.; Gallegos, Autumn B.; Telander, Monty R.; Pitman, Stan G.

    2006-09-14

    The Pacific Northwest National Laboratory (PNNL) is evaluating low-temperature technologies to immobilize mixed radioactive and hazardous waste. Three waste forms—alkali-aluminosilicate hydroceramic cement, “Ceramicrete” phosphate-bonded ceramic, and “DuraLith” alkali-aluminosilicate geopolymer—were selected through a competitive solicitation for fabrication and characterization of waste-form properties. The three contractors prepared their respective waste forms using simulants of a Hanford secondary waste and Idaho sodium bearing waste provided by PNNL and characterized their waste forms with respect to the Toxicity Characteristic Leaching Procedure (TCLP) and compressive strength. The contractors sent specimens to PNNL, and PNNL then conducted durability (American National Standards Institute/American Nuclear Society [ANSI/ANS] 16.1 Leachability Index [LI] and modified Product Consistency Test [PCT]) and compressive strength testing (both irradiated and as-received samples). This report presents the results of these characterization tests.

  16. A Magnetic Resonance Measurement Technique for Rapidly Switched Gradient Magnetic Fields in a Magnetic Resonance Tomograph

    Directory of Open Access Journals (Sweden)

    K. Bartušek

    2003-01-01

    Full Text Available This paper describes a method for measuring of the gradient magnetic field in Nuclear Magnetic Resonance (NMR tomography, which is one of the modern medical diagnostic methods. A very important prerequisite for high quality imaging is a gradient magnetic field in the instrument with exactly defined properties. Nuclear magnetic resonance enables us to measure the pulse gradient magnetic field characteristics with high accuracy. These interesting precise methods were designed, realised, and tested at the Institute of Scientific Instruments (ISI of the Academy of Sciences of the Czech Republic. The first of them was the Instantaneous Frequency (IF method, which was developed into the Instantaneous Frequency of Spin Echo (IFSE and the Instantaneous Frequency of Spin Echo Series (IFSES methods. The above named methods are described in this paper and their a comparison is also presented.

  17. Development of magnetic calorimeters for absolute activity measurement; Developpement de calorimetres magnetiques pour la mesure absolue d'activite

    Energy Technology Data Exchange (ETDEWEB)

    Loidl, M.; Leblanc, E.; Rodrigues, M.; Qasimi, A.; Bouchard, J.; Censier, B.; Branger, T.; Lacour, D. [CEA Saclay, LNE-LNHB, Lab. National Henri Becquerel, LIST, 91 - Gif-sur-Yvette (France)

    2009-07-01

    We have developed a prototype magnetic calorimeter, operated at very low temperature, for absolute activity measurement of low energy emitting radionuclides. A weighed source of {sup 55}Fe has been enclosed inside the detector absorber assuring a high detection efficiency. The result of a preliminary activity measurement carried out with this prototype is compatible with a measurement by liquid scintillation counting. Apart from the high detection efficiency, this approach is particularly interesting since it introduces a new method into a field where only few measuring techniques are available. (authors)

  18. Review of MFTF yin-yang magnet displacement and magnetic field measurements and calculations

    International Nuclear Information System (INIS)

    Hanson, C.L.; Myall, J.O.; Wohlwend, J.W.

    1983-01-01

    During the recent testing of the MFTF yin-yang magnet, measurements of coil position, structural case strain, and magnetic field were made to verify calculated values. Measurements to detect magnet movement were taken throughout cooldown and during the operation of the magnet. The magnetic field at the mirror points was measured by Hall-effect probes. The magnet position, structural case strain, and magnetic field measurements indicated a reasonably close correlation with calculated values. Information obtained from the yin-yang test has been very useful in setting realistic mechanical alignment values for the new MFTF-B magnet system

  19. The magnet measurement facility for the Advanced Photon Source

    International Nuclear Information System (INIS)

    Kim, S.H.; Doose, C.; Hogrefe, R.; Kim, K.; Merl, R.

    1993-01-01

    A magnet measurement facility has been developed to measure the prototype and production magnets for the Advance Photon Source. The measurement facility is semi-automatic in measurement control and data analysis. One dipole system and three rotating coil measurement systems for quadrupole and sextupole magnets and corresponding probe coils are described

  20. Field measurement of dipole magnets for TARN

    International Nuclear Information System (INIS)

    Hori, T.; Noda, A.; Hattori, T.; Fujino, T.; Yoshizawa, M.

    1980-05-01

    Eight dipole magnets of window-frame type with zero field gradient have been fabricated for TARN. Various characteristics of the field were examined by a measuring system with a Hall and an NMR probes. The accuracy of the measurement was better than 1 x 10 -4 at the maximum field strength of --9 kG, and the uniformity of the field in the radial direction was better than +-2 x 10 -4 over the whole useful aperture. The deviations both of the field strengths and of the effective lengths among the eight magnets are smaller than +-2 x 10 -3 . The sextupole component of the field and the variation of the effective length over the beam orbits contribute to chromaticities of the ring as the amount of -1.59 and 0.93 in the horizontal and vertical directions, respectively. (author)

  1. Measurement of myocardial perfusion using magnetic resonance

    DEFF Research Database (Denmark)

    Fritz-Hansen, T.; Jensen, L.T.; Larsson, H.B.

    2008-01-01

    Cardiac magnetic resonance imaging (MRI) has evolved rapidly. Recent developments have made non-invasive quantitative myocardial perfusion measurements possible. MRI is particularly attractive due to its high spatial resolution and because it does not involve ionising radiation. This paper reviews...... myocardial perfusion imaging with MR contrast agents: methods, validation and experiences from clinical studies. Unresolved issues still restrict the use of these techniques to research although clinical applications are within reach Udgivelsesdato: 2008/12/8...

  2. Microchip-calorimetry of organic charge transfer complex which shows superconductivity at low temperatures

    Energy Technology Data Exchange (ETDEWEB)

    Muraoka, Yuki [Department of Chemistry, Graduate School of Science, Osaka University, Machikaneyama 1-1, Toyonaka, Osaka 560-0043 (Japan); Yamashita, Satoshi [RIKEN, Hirosawa 2-1, Wako, Saitama 351-0198 (Japan); Yamamoto, Takashi [Department of Chemistry, Graduate School of Science, Osaka University, Machikaneyama 1-1, Toyonaka, Osaka 560-0043 (Japan); Nakazawa, Yasuhiro, E-mail: nakazawa@chem.sci.osaka-u.ac.jp [Department of Chemistry, Graduate School of Science, Osaka University, Machikaneyama 1-1, Toyonaka, Osaka 560-0043 (Japan); Institute for Molecular Science, Nishigonaka 38, Myodaiji, Okazaki 444-8585 (Japan)

    2012-03-20

    Highlights: Black-Right-Pointing-Pointer Organic charge transfer salt of {kappa}-(BEDT-TTF){sub 2}Cu[N(CN){sub 2}]Br shows superconductivity. Black-Right-Pointing-Pointer We succeeded to detect thermal anomaly microchip device TCG3880. Black-Right-Pointing-Pointer Development details of the calorimeter and the detection system is presented. Black-Right-Pointing-Pointer The magnetic fields dependence shows typical character of layered superconductor. - Abstract: We carried out thermodynamic measurements of organic charge transfer complex of {kappa}-(BEDT-TTF){sub 2}Cu[N(CN){sub 2}]Br, where BEDT-TTF is bis(ethylenedithio)tetrathiafulvalene by TCG3880 chip device in order to examine capability of the chip calorimeter at low temperature region and under magnetic fields. TCG3880 chip is mounted on a {sup 3}He cryostat available in combination with a superconductive magnet up to 7 T. Thermal anomalies related to the glass-like freezing of ethylene groups of BEDT-TTF molecules and the superconductive transition were observed. A frequency dependence of the thermal anomaly of the glass formation and a magnetic fields dependence of the thermal anomaly of the superconductive transition are reported. The results presented in this work demonstrate that the TCG3880 is quite useful for thermodynamic investigations of the organic charge transfer complex with much reduced sample quantity as compared with those of relaxation and adiabatic calorimetry.

  3. Thermal conductivity of yttrium iron garnet at low temperatures

    International Nuclear Information System (INIS)

    Joshi, Y.P.; Sing, D.P.

    1979-01-01

    An analysis of the low-temperature thermal conductivity of yttrium iron garnet is presented giving consideration to the fact that in a conventional conductivity experiment the magnon temperature gradient inside a magnetic insulator need not be necessarily equal to the phonon temperature gradient. Consequently the effective conductivity can be less than the algebraic sum of the phonon and magnon intrinsic conductivities, depending on the magnon-phonon thermal relaxation rate. This relaxation rate has been distinguished from the individual phonon and magnon relaxation rates and an expression is derived for it. Theoretical calculations of the effective conductivity are found to be in good agreement with experimental results. The contribution of magnons to the effective conductivity is observed to be small at all temperatures below the conductivity maximum. (author)

  4. Low-temperature structural phase transition in synthetic libethenite Cu2PO4OH

    International Nuclear Information System (INIS)

    Belik, Alexei A.; Naumov, Pance; Kim, Jungeun; Tsuda, Shunsuke

    2011-01-01

    Low-temperature structural properties of the synthetic mineral libethenite Cu 2 PO 4 OH were investigated by single-crystal X-ray diffraction, synchrotron X-ray powder diffraction, specific heat measurements, and Raman spectroscopy. A second-order structural phase transition from the Pnnm symmetry (a=8.0553(8) A, b=8.3750(9) A, c=5.8818(6) A at 180 K) to the P2 1 /n symmetry (a=8.0545(8) A, b=8.3622(9) A, c=5.8755(6) A, β=90.0012(15) at 120 K) was found at 160 K during cooling. At 120 K, the monoclinic angle is 90.0012(15) from single crystal X-ray data vs 90.083(1) from powder X-ray diffraction data. The P2 1 /n-to-Pnnm transition may be a general feature of the adamite-type compounds, M 2 XO 4 OH. - Graphical Abstract: Fragments of experimental synchrotron X-ray powder diffraction patterns of Cu 2 PO 4 OH between 100 and 280 K. Arrows show additional reflections that appear below 160 K in the monoclinic P2 1 /n phase. Highlights: → A low-temperature phase transition was found in the mineral libethenite Cu 2 PO 4 OH. → No magnetic anomalies and weak specific heat anomalies are detected. → Phase transition is of the second order. → Libethenite may exemplify a general feature of the adamite-type compounds.

  5. Low temperature magneto-morphological characterisation of coronene and the resolution of previously observed unexplained phenomena

    Science.gov (United States)

    Potticary, Jason; Boston, Rebecca; Vella-Zarb, Liana; Few, Alex; Bell, Christopher; Hall, Simon R.

    2016-12-01

    The polyaromatic hydrocarbon coronene has been the molecule of choice for understanding the physical properties of graphene for over a decade. The modelling of the latter by the former was considered to be valid, as since it was first synthesised in 1932, the physical behaviour of coronene has been determined extremely accurately. We recently discovered however, an unforeseen polymorph of coronene, which exists as an enantiotrope with the previously observed crystal structure. Using low-temperature magnetisation and crystallographic measurements, we show here for the first time that the electronic and magnetic properties of coronene depend directly on the temperature at which it is observed, with hysteretic behaviour exhibited between 300 K and 100 K. Furthermore we determine that this behaviour is a direct result of the appearance and disappearance of the newly-discovered polymorph during thermal cycling. Our results not only highlight the need for theoretical models of graphene to take into account this anomalous behaviour at low temperatures, but also explain puzzling experimental observations of coronene dating back over 40 years.

  6. Finding the magnetic size distribution of magnetic nanoparticles from magnetization measurements via the iterative Kaczmarz algorithm

    Energy Technology Data Exchange (ETDEWEB)

    Schmidt, Daniel, E-mail: frank.wiekhorst@ptb.de; Eberbeck, Dietmar; Steinhoff, Uwe; Wiekhorst, Frank

    2017-06-01

    The characterization of the size distribution of magnetic nanoparticles is an important step for the evaluation of their suitability for many different applications like magnetic hyperthermia, drug targeting or Magnetic Particle Imaging. We present a new method based on the iterative Kaczmarz algorithm that enables the reconstruction of the size distribution from magnetization measurements without a priori knowledge of the distribution form. We show in simulations that the method is capable of very exact reconstructions of a given size distribution and, in that, is highly robust to noise contamination. Moreover, we applied the method on the well characterized FeraSpin™ series and obtained results that were in accordance with literature and boundary conditions based on their synthesis via separation of the original suspension FeraSpin R. It is therefore concluded that this method is a powerful and intuitive tool for reconstructing particle size distributions from magnetization measurements. - Highlights: • A new method for the size distribution fit of magnetic nanoparticles is proposed. • Employed Kaczmarz algorithm does not need a priori input or eigenwert regularization. • The method is highly robust to noise contamination. • Size distributions are reconstructed from simulated and measured magnetization curves.

  7. Magnetic measurements on Tl-2212 and Bi-2212 single crystals: a comparative study

    Energy Technology Data Exchange (ETDEWEB)

    Oussena, M. (Physics Dept., Univ. of Southampton (United Kingdom)); Porter, S. (Physics Dept., Univ. of Southampton (United Kingdom)); Volkozub, A. (Physics Dept., Univ. of Southampton (United Kingdom)); De Groot, P.A.J. (Physics Dept., Univ. of Southampton (United Kingdom)); Lanchester, P.C. (Physics Dept., Univ. of Southampton (United Kingdom)); Ogborne, D. (Physics Dept., Univ. of Southampton (United Kingdom) Chemistry Dept., Univ. of Southampton (United Kingdom)); Weller, M.T. (Physics Dept., Univ. of Southampton (United Kingdom) Chemistry Dept., Univ. of Southampton (United Kingdom)); Balakrishnan, G. (Physics Dept., Univ. of Southampton (United Kingdom) Physics Dept., Univ. of Warwick, Coventry (United Kingdom)); Paul, D.McK. (Physics Dept., Univ. of Southampton (United Kingdom) Physics Dept., Univ. of Warwick, Coventry (United Kingdom))

    1994-02-01

    We have compared the magnetic behaviour of two identically shaped single crystals, Tl[sub 2]Ba[sub 2]CaCu[sub 2]O[sub 8] and Bi[sub 2]Sr[sub 2]CaCu[sub 2]O[sub 8]. The critical current density is found to decrease more rapidly with temperature in Bi-2212 although it is the highest in this material at low temperatures (T < 10K). I-V characteristic curves have been obtained from measurements of magnetic sweep rate dependencies of the hysteresis loops. We have found that the characteristic temperature at which flux motion becomes important is significantly higher in Tl-2212 than in Bi-2212. Hence the Tl-2212 has a larger effective pinning. (orig.)

  8. Magnetic measurements on Tl-2212 and Bi-2212 single crystals: a comparative study

    International Nuclear Information System (INIS)

    Oussena, M.; Porter, S.; Volkozub, A.; De Groot, P.A.J.; Lanchester, P.C.; Ogborne, D.; Weller, M.T.; Balakrishnan, G.; Paul, D.McK.

    1994-01-01

    We have compared the magnetic behaviour of two identically shaped single crystals, Tl 2 Ba 2 CaCu 2 O 8 and Bi 2 Sr 2 CaCu 2 O 8 . The critical current density is found to decrease more rapidly with temperature in Bi-2212 although it is the highest in this material at low temperatures (T < 10K). I-V characteristic curves have been obtained from measurements of magnetic sweep rate dependencies of the hysteresis loops. We have found that the characteristic temperature at which flux motion becomes important is significantly higher in Tl-2212 than in Bi-2212. Hence the Tl-2212 has a larger effective pinning. (orig.)

  9. Magnetic field measurement in the analyzing magnet of NIS spectrometer

    Science.gov (United States)

    Avramenko, S. A.; Afanas'ev, S. V.; Voloshina, I. G.; Dolgii, S. A.; Yusupov, A. Yu.; Kalmykov, A. V.; Makoveev, V. K.; Nikolaevskii, G. P.; Ostrovskii, I. V.; Perepelkin, E. E.; Peresedov, V. F.; Plyashkevich, S. N.; Rossiiskaya, N. S.; Salmin, R. A.; Spodarets, V. K.; Strokovskii, E. A.; Yudin, I. P.

    2006-12-01

    The main goals of the Nucleon Intrinsic Strangeness experiment (NIS) are the search for the effects of hidden polarized strangeness in the nucleon and the exploration and study of exotic baryons (pentaquarks) in NN reactions. The setup is located in the Laboratory of High Energies at the Joint Institute for Nuclear Research in channel 4V of the Nuclotron extracted beam with the energy between 1 and 4 GeV. The 1SP-40-4V electromagnet of the spectrometer has the external dimensions 3.20 × 3.26 × 4.48 m and the aperture 2.74 × 0.68 m. The magnetic field measurement was performed using the three-component Hall magnetometer in the computer-controlled automated mode. The volume of measurements was 1.03 × 0.60 × 3.92 m. The description of the measuring equipment and measurement procedure is given. The results of the measurements are used for the Monte Carlo computer modeling of the experiment. These results will be used in the analysis of physical data after their acquisition.

  10. A low temperature aluminizing treatment of hot work tool steel

    Energy Technology Data Exchange (ETDEWEB)

    Matijevic, B., E-mail: bozidar.matijevic@fsb.hr [University of Zagreb, Faculty of Mechanical Engineering and Naval Architecture, Zagreb (Croatia)

    2010-07-01

    Conventional aluminizing processes by pack cementation are typically carried out at elevated temperatures. A low temperature powder aluminizing technology was applied to hot tool steel H13. The aluminizing treating temperature was from 550 to 620°C. Effects of temperature and time on the microstructure and phase evolution were investigated. Also, the intermetallic layer thickness was measured in the aluminized layer of a steel substrate. The cross-sectional microstructures, the aluminized layer thickness and the oxide layer were studied. Scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDX), glow discharge optical spectroscopy (GDOS) were applied to observe the cross-sections and the distribution of elements. (author)

  11. A LOW TEMPERATURE ALUMINIZING TREATMENT OF HOT WORK TOOL STEEL

    OpenAIRE

    Matijević, Božidar

    2013-01-01

    Conventional aluminizing processes by pack cementation are typically carried out at elevated temperatures. A low temperature powder aluminizing technology was applied to the X40CrMoV5-1 hot tool steel. The aluminizing temperature was from 550 °C to 620 °C. Effects of temperature and time on the microstructure and phase evolution were investigated. Also, the intermetallic layer thickness was measured in the aluminized layer of a steel substrate. The cross-sectional microstructures, the alumini...

  12. A low temperature aluminizing treatment of hot work tool steel

    International Nuclear Information System (INIS)

    Matijevic, B.

    2010-01-01

    Conventional aluminizing processes by pack cementation are typically carried out at elevated temperatures. A low temperature powder aluminizing technology was applied to hot tool steel H13. The aluminizing treating temperature was from 550 to 620°C. Effects of temperature and time on the microstructure and phase evolution were investigated. Also, the intermetallic layer thickness was measured in the aluminized layer of a steel substrate. The cross-sectional microstructures, the aluminized layer thickness and the oxide layer were studied. Scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDX), glow discharge optical spectroscopy (GDOS) were applied to observe the cross-sections and the distribution of elements. (author)

  13. Anomalous low-temperature desorption from preirradiated rare gas solids

    International Nuclear Information System (INIS)

    Savchenko, E.V.; Gumenchuk, G.B.; Yurtaeva, E.M.; Belov, A.G.; Khyzhniy, I.V.; Frankowski, M.; Beyer, M.K.; Smith-Gicklhorn, A.M.; Ponomaryov, A.N.; Bondybey, V.E.

    2005-01-01

    The role for the exciton-induced defects in the stimulation of anomalous low-temperature desorption of the own lattice atoms from solid Ar and Ne preirradiated by an electron beam is studied. The free electrons from shallow traps-structural defects-was monitored by the measurements of a yield of the thermally induced exoelectron emission (TSEE). The reaction of recombination of self-trapped holes with electrons is considered as a source of energy needed for the desorption of atoms from the surface of preirradiated solids. A key part of the exciton-induced defects in the phenomenon observed is demonstrated

  14. The anomalous low temperature resistivity of thermally evaporated α-Mn thin film

    International Nuclear Information System (INIS)

    Ampong, F.K.; Boakye, F.; Nkum, R.K.

    2010-01-01

    Electrical resistivity measurements have been carried out on thermally evaporated α-Mn thin film between 300 and 1.4 K using the van der Pauw four probe technique. The film was grown on a glass substrate held at a temperature of 373 K, in an ambient pressure of 5x10 -6 Torr. The results show a resistance minimum, a notable characteristic of α-Mn but at a (rather high) temperature of 194±1 K. Below the resistivity maximum which corresponds to 70 K, the resistivity drops by only 0.02 μΩm indicating a rather short range magnetic ordering. The low temperature results show a tendency towards saturation of the resistivity as the temperature approaches zero suggesting a Kondo scattering.

  15. The anomalous low temperature resistivity of thermally evaporated alpha-Mn thin film

    Energy Technology Data Exchange (ETDEWEB)

    Ampong, F.K., E-mail: kampxx@yahoo.co [Department of Physics, Kwame Nkrumah University of Science and Technology, Kumasi (Ghana); Boakye, F.; Nkum, R.K. [Department of Physics, Kwame Nkrumah University of Science and Technology, Kumasi (Ghana)

    2010-08-15

    Electrical resistivity measurements have been carried out on thermally evaporated alpha-Mn thin film between 300 and 1.4 K using the van der Pauw four probe technique. The film was grown on a glass substrate held at a temperature of 373 K, in an ambient pressure of 5x10{sup -6} Torr. The results show a resistance minimum, a notable characteristic of alpha-Mn but at a (rather high) temperature of 194+-1 K. Below the resistivity maximum which corresponds to 70 K, the resistivity drops by only 0.02 muOMEGAm indicating a rather short range magnetic ordering. The low temperature results show a tendency towards saturation of the resistivity as the temperature approaches zero suggesting a Kondo scattering.

  16. Active carbons from low temperature conversion chars

    International Nuclear Information System (INIS)

    Adebowale, K.O.; Bayer, E.

    2002-05-01

    Hulls obtained from the fruits of five tropical biomass have been subjected to low temperature conversion process and their chars activated by partial physical gasification to produce active carbons. The biomass are T. catappa, B. nitida, L leucophylla, D. regia and O. martiana. The bulk densities of the samples ranged from 0.32 g.cm 3 to 0.52 g.cm 3 . Out of the samples T. catappa recorded the highest cellulose content (41.9 g.100g -1 ), while O. martiana contained the highest lignin content (40.7 g.100g -1 ). The ash of the samples were low (0.5 - 4.4%). The percentage of char obtained after conversion were high (33.7% - 38.6%). Active carbons obtained from T. catappa, D. regia and O. martiana, recorded high methylene blue numbers and iodine values. They also displayed good micro- and mesostructural characteristics. Micropore volume (V micro ) was between 0.33cm 3 .g -1 - 0.40cm 3 .g -1 , while the mesopore volume(V meso ) was between 0.05 cm 3 .g -1 - 0.07 cm 3 .g -1 . The BET specific surface exceeds 1000 m 2 .g -1 . All these values compared favourably with high grade commercial active carbons. (author)

  17. Low Temperature Catalyst for NH3 Removal

    Science.gov (United States)

    Monje, Oscar; Melendez, Orlando

    2013-01-01

    Air revitalization technologies maintain a safe atmosphere inside spacecraft by the removal of C02, ammonia (NH3), and trace contaminants. NH3 onboard the International Space Station (ISS) is produced by crew metabolism, payloads, or during an accidental release of thermal control refrigerant. Currently, the ISS relies on removing NH3 via humidity condensate and the crew wears hooded respirators during emergencies. A different approach to cabin NH3 removal is to use selective catalytic oxidation (SCO), which builds on thermal catalytic oxidation concepts that could be incorporated into the existing TCCS process equipment architecture on ISS. A low temperature platinum-based catalyst (LTP-Catalyst) developed at KSC was used for converting NH3 to H20 and N2 gas by SCO. The challenge of implementing SCO is to reduce formation of undesirable byproducts like NOx (N20 and NO). Gas mixture analysis was conducted using FTIR spectrometry in the Regenerable VOC Control System (RVCS) Testbed. The RVCS was modified by adding a 66 L semi-sealed chamber, and a custom NH3 generator. The effect of temperature on NH3 removal using the LTP-Catalyst was examined. A suitable temperature was found where NH3 removal did not produce toxic NO, (NO, N02) and N20 formation was reduced.

  18. Pyrocatechol from low-temperature tar

    Energy Technology Data Exchange (ETDEWEB)

    Lowenstein-Lom, W

    1950-01-01

    A method for production and purification of pyrocatechol (I) from low-temperature carbonization effluents was described. Phenosolvan, a mixture of isobutyl, butyl, and amyl acetates, was used for extraction of I from the effluent. After removing most of the solvent by distillation, the separation was completed by batch vacuum distillation at 25 to 50 millimeter Hg. The 4th fraction, containing I 49.2, I homologues 31.1, o-cresol 6.8, xylenols 7.3, and higher boiling material and residue 5.6 percent, was treated in a purification pilot plant, which was described. This fraction was dissolved in an equal weight of C/sub 6/H/sub 6/, then cooled. I was crystallized out in a vacuum crystallizer, centrifuged, and washed with C/sub 6/H/sub 6/, dried in a rotating-plate drier and taken to storage. The purified I melted 100/sup 0/ to 102/sup 0/ and contained 4 to 8 percent homologues or other impurities. A further recrystallization raised its purity to 99.2 percent. Plant capacities and production costs are given.

  19. Enhanced Design Alternative I: Low Temperature Design

    International Nuclear Information System (INIS)

    MacNeil, K.

    1999-01-01

    The purpose of this document is to evaluate Enhanced Design Alternative (EDA) 1, the low temperature repository design concept (CRWMS M and O 1999a). This technical document will provide supporting information for Site Recommendation (SR) and License Application (LA). Preparation of this evaluation will be in accordance with the technical document preparation plan (TDPP), (CRWMS M and O 1999b). EDA 1, one of five EDAs, was evolved from evaluation of a series of design features and alternatives developed during the first phase of the License Application Design Selection (LADS) process. Low, medium, and high temperature concepts were developed from the design features and alternatives prepared during Phase 1 of the LADS effort (CRWMS M and O 1999a). EDA 1 will first be evaluated against a single Screening Criterion, outlined in CRWMS M and O 1999a, which addresses post-closure performance of the repository. The performance of the repository is defined quantitatively as the peak radiological dose rate to an average individual of a critical group at a distance of 20 km from the repository site within 10,000 years. To satisfy this criterion the peak dose rate must not exceed the anticipated regulatory level of 25 mrem/yr within 10,000 years. If the EDA meets the screening criterion, the EDA will be further evaluated against the LADS Phase 2 Evaluation Criteria contained in CRWMS M and O 1999a

  20. Low temperature nitrogen chemistry. Final report

    Energy Technology Data Exchange (ETDEWEB)

    Glarborg, P.; Dam-Johansen, K.; Kristensen, P.G.; Alzueta, M.; Roejel, H.

    1997-04-01

    The results of a two tasks program on Natural Gas Reburning are reported. The work involved an experimental and theoretical study of the reburning and hybrid reburning/SNCR chemistry in the 1000-1500 K range. The interactions between hydrocarbon and nitrogen chemistry under fuel-rich conditions were investigated in order to assess the NO{sub x} reduction potential of low temperature reburning. The effect of reburn fuel(carbon monoxide, methane, acetylene, ethylene, ethane, and methane/ethane mixture), temperature, stoichiometry, reactant dilution, reaction time, and inlet NO level were studied. The results indicate a significant NO reduction potential even below 1400 K, but extrapolation to practical conditions are complicated by inadequate knowledge of the detailed chemistry as well as of the effect of mixing. The possibilities of enhancing the conversion to N{sub 2} instead of NO by adding selective reducing agents (hybrid reburning/SNCR) were evaluated. Our results indicate little synergistic effect between reburn and SNCR. The most simple configuration, where the selective reducing agent is injected together with the burnout air, is not expected to be effective, unless the N-agent is injected in form of an aqueous solution. A chemical kinetic model for reburning and reburn/SNCR is listed and can be obtained by e-mail from pgl(commerical at)kt.dtu.dk.(au) 145 refs.

  1. Active carbons from low temperature conversion chars

    Energy Technology Data Exchange (ETDEWEB)

    Adebowale, K O [Department of Chemistry, University of lbadan, lbadan (Nigeria); Abdus Salam International Centre for Theoretical Physics, Trieste (Italy); Bayer, E [Universitaet Tuebingen, Institut fuer Organische Chemie, Forschungstelle Nukleinsaeure- und Peptidchemie, Tuebingen (Germany)

    2002-05-01

    Hulls obtained from the fruits of five tropical biomass have been subjected to low temperature conversion process and their chars activated by partial physical gasification to produce active carbons. The biomass are T. catappa, B. nitida, L leucophylla, D. regia and O. martiana. The bulk densities of the samples ranged from 0.32 g.cm{sup 3} to 0.52 g.cm{sup 3}. Out of the samples T. catappa recorded the highest cellulose content (41.9 g.100g{sup -1}), while O. martiana contained the highest lignin content (40.7 g.100g{sup -1}). The ash of the samples were low (0.5 - 4.4%). The percentage of char obtained after conversion were high (33.7% - 38.6%). Active carbons obtained from T. catappa, D. regia and O. martiana, recorded high methylene blue numbers and iodine values. They also displayed good micro- and mesostructural characteristics. Micropore volume (V{sub micro}) was between 0.33cm{sup 3}.g{sup -1} - 0.40cm{sup 3}.g{sup -1}, while the mesopore volume(V{sub meso}) was between 0.05 cm{sup 3}.g{sup -1} - 0.07 cm{sup 3}.g{sup -1}. The BET specific surface exceeds 1000 m{sup 2}.g{sup -1}. All these values compared favourably with high grade commercial active carbons. (author)

  2. Radiation detection at very low temperature. DRTBT 1992 -Londe-Les-Maures - Course collection

    International Nuclear Information System (INIS)

    Bellefon, A. de; Serra, Guy; Broniatowski, A.; Giraud-Heraud, Y.; Bruere Dawson, R.; Waysand, G.; Maneval, J.P.; Jacquier, B.; Leotin, J.; Chapellier, M.; Beaudin, G.; Encrenaz, P.; Gheudin, M.; Lamarre, J.M.; Ravex, A.; Godfrin, H.; Bret, J.L.; Gianese, Chr.; Torre, J.P.; Marcillac, P. de; Benoit, A.; Jegoudez, G.; Pari, P.

    1992-09-01

    The contributions addressed various themes: Cooled sensors, what are they for? (Search for rare events; Astrophysics, X rays and infrared, Spectrometry in nuclear physics); Cooled sensors (Bolometer physics, Bolometers for photometry, Bolometers for particle detection, Superconducting sensors, Other types of bolometers, Low temperature luminescence, Photo-conductors and photovoltaic BIB, Ionisation at very low temperature, Heterodyne detection); Problems related to the signal (Photometry and external measurement noise, Line, amplification and signal processing), Pulse measurement (Line and amplification, Signal processing), Cryogenics (Cryogenic machines, Very low temperature cryogenics, Noise and environment). Nota: contributions are printed in a different order than they are listed in the table of contents

  3. Warm magnetic measurements of MCBCs: comparison between the results obtained with the Quadrupole Industrial Magnetic Measurement and the Corrector Industrial Magnetic Measurement systems

    CERN Document Server

    Remondino, Vittorio; Catalan-Lasheras, N

    2005-01-01

    MCBCs modules are first magnetically measured at Tesla using a second-generation Corrector Industrial Magnetic Measurement (CIMM). After assembly into the SSS quadrupoles, measurements are repeated at CERN using the Quadrupole Industrial Magnetic Measurement (QIMM) system. In this note, we compare the measurements provided by the two systems. In all the 18 cases examined, the correlation found is excellent. The consistency of the results obtained indicates that both systems are effective, that modules are correctly measured by the firm personnel and that magnetic characteristics of the modules do not change during their assembly in cold masses.

  4. Review of MFTF yin-yang magnet displacement and magnetic field measurements and calculations

    International Nuclear Information System (INIS)

    Hanson, C.L.; Myall, J.O.; Wohlwend, J.W.

    1983-01-01

    During the recent testing of the MFTF yin-yang magnet, measurements of coil position, structural case strain, and magnetic field were made to verify calculated values. Measurements to detect magnet movement were taken throughout cooldown and during the operation of the magnet. The magnetic field at the mirror points was measured by Hall-effect probes. The magnet position, structural case strain, and magntic field measurements indicated a reasonably close correlation with calculated values. Information obtained from the yin-yang test has been very useful in setting realistic mechanical alignment values for the new MFTF-B magnet system

  5. Effect of low temperature on reservoir water and mechanical control measure%水库低温水的生态影响及工程对策研究

    Institute of Scientific and Technical Information of China (English)

    张士杰; 刘昌明; 谭红武; 李国强

    2011-01-01

    Thermal stratification of reservoirs is a critical ecological factor for regulating direct and indirect effects of temperature on reservoir productivity. In particular, low temperature reservoir waters have adverse effects on agricultural/aquatic ecology. Selective water withdrawal from different reservoir depths is used to manage water demand for different uses. In China, stoplog gate are constructed in large reservoirs to regulate water temperatures for crop irrigation and fish breeding. When water is withdrawn from different reservoir depths, flow patterns, stratification and therefore water quality in the reservoir are altered. Vertical 1-D or 2-D water temperature models were applied to analyze the effects of selective water withdrawal on thermal structure and release water temperature in reservoirs. In this study, thermal stratification and the related seasonal variations in reservoirs were simulated. The effects of two different water withdrawal schemes on water release temperature were analyzed using the MIKE-3 numerical simulation model. Based on the model simulation, stoplog gates effectively improved low temperature water conditions. The predicted thermal stratification and water temperature profiles were noticeably influenced by withdrawal schemes. There were significant differences in the regulation effects of water withdrawal on release temperature between single-layer entry and stoplog gate. From March to September, water temperature was higher by 2~4 °C in stoplog gate than in single-layer entry scheme. The water release temperature of stoplog gate scheme reached 18.4 °C in May, which was the required water temperature for fish spawning. It was therefore concluded that stoplog gate was a more suitable engineered structure. It was not only ecologically friendly, but also effectively improved water temperature, mitigated ecological effects, and ensured coordinated environmental protection and socio-economic efficiency.%大型水库低温水下泄

  6. Development of a magnetic measurement device for thin ribbon samples

    International Nuclear Information System (INIS)

    Sato, Yuta; Todaka, Takashi; Enokizono, Masato

    2008-01-01

    This paper presents a magnetic measurement device for thin ribbon samples, which are produced by rapid cooling technique. This device enables us to measure magnetic properties easily by only inserting a ribbon sample into a sample holder. The sample holder was made by bakelite to fix any width sample. A long solenoid coil was used to generate a uniform magnetic field and the sample holder was placed at the mid part of the solenoid. The magnetic field strength was measured using a shunt resistor and the magnetic flux density and magnetization in sample ribbons were evaluated by using search coils. The accuracy of measurement was verified with an amorphous metal ribbon sample. Next, we have measured magnetic properties of some magnetic shape memory alloys, which have different compositions. The measured results are compared and we clarified the effect of Sm contents on the magnetic properties

  7. Magnetic field measuring system for remapping the ORIC magnetic field

    International Nuclear Information System (INIS)

    Mosko, S.W.; Hudson, E.D.; Lord, R.S.; Hensley, D.C.; Biggerstaff, J.A.

    1977-01-01

    The Holifield Heavy Ion Research Facility will integrate a new 25 MV tandem electrostatic acccelerator into the existing cyclotron laboratory which includes the Oak Ridge Isochronous Cyclotron (ORIC). Computations of ion paths for beam injection from the new tandem into ORIC require field mapping in the regions traversed by the beam. Additional field data is also desired for the higher levels (approx.19 kG) now used for most heavy ion beams. The magnetic field measurement system uses 39 flip coil/current integrator sets with computer controlled data scanning. The coils are spaced radially at 1 inch intervals in an arm which can be rotated azimuthally in 2 degree increments. The entire flip coil assembly can be shifted to larger radii to measure fields beyond the pole boundary. Temperature stabilization of electronic circuitry permits a measurement resolution of +-1 gauss over a dynamic range of +-25,000 gauss. The system will process a scan of 8000 points in about one hour

  8. Low temperature and neutron physics studies

    International Nuclear Information System (INIS)

    Shull, C.G.

    1989-01-01

    A search for a novel coupling interaction between the Pendelloesung periodicity which is formed in a diffracting crystal and the Larmor precession of neutrons in a magnetic field has been carried out. This interaction is expected to exhibit a resonant behavior when the two spatial periodicities become matched upon scanning the magnetic field being applied to the crystal. Observations on a diffracting, perfect crystal of silicon with neutrons of wavelength 1 Angstrom show the expected resonant action but some discrepancy between the observed magnitude of the resonance effects remains for interpretation. 16 refs

  9. Biodegradation of magnetic nanoparticles evaluated from Moessbauer and magnetization measurements

    Energy Technology Data Exchange (ETDEWEB)

    Mischenko, I., E-mail: IlyaMischenko@rambler.ru; Chuev, M. [Russian Academy of Sciences, Institute of Physics and Technology (Russian Federation); Cherepanov, V.; Polikarpov, M.; Panchenko, V. [National Research Centre ' Kurchatov Institute' (Russian Federation)

    2013-04-15

    In order to extract a quantitative information about characteristics of the magnetic nanoparticles injected into a living organism it is necessary to define a model of the magnetic dynamics for fitting self-consistently the whole set of the experimental data, specifically, the evolution of Moessbauer spectral shape with temperature and external magnetic field as well as the magnetization curves. We have developed such a model and performed such an analysis of the temperature- and magnetic field-dependent spectra and magnetization curves of nanoparticles injected into mice. This allowed us to reliably evaluate changes in the characteristics of the residual particles and their chemical transformation to paramagnetic ferritin-like forms in different mouse organs as a function of time. Actually, the approach makes it possible to quantitatively characterize biodegradation and biotransformation of magnetic nanoparticles delivered in a body.

  10. Fluxgate Magnetic Sensor and Its Application for Current Measurement

    International Nuclear Information System (INIS)

    Mitra-Djamal

    2007-01-01

    Conventionally electric current can be measured by connecting the instrument serially on the circuit. This method has disadvantage because its disturb the measured current flow. By using a magnetic sensor, current can be measured without disturbing the current flow, because it just measures the magnetic field of the measured current. This paper shows the use of fluxgate magnetic sensor for current measurement. It is shown that the sensor can measure widely range of current with resolution ≤ 2 %. (author)

  11. Low-temperature thermal properties of yttrium and lutetium dodecaborides

    International Nuclear Information System (INIS)

    Czopnik, A; Shitsevalova, N; Pluzhnikov, V; Krivchikov, A; Paderno, Yu; Onuki, Y

    2005-01-01

    The heat capacity (C p ) and dilatation (α) of YB 12 and LuB 12 are studied. C p of the zone-melted YB 12 tricrystal is measured in the range 2.5-70 K, of the zone-melted LuB 12 single crystal in the range 0.6-70 K, and of the LuB 12 powder sample in the range 4.3-300 K; α of the zone-melted YB 12 tricrystal and LuB 12 single crystals is measured in the range 5-200 K. At low temperatures a negative thermal expansion (NTE) is revealed for both compounds: for YB 12 at 50-70 K, for LuB 12 at 10-20 K and 60-130 K. Their high-temperature NTE is a consequence of nearly non-interacting freely oscillating metal ions (Einstein oscillators) in cavities of a simple cubic rigid Debye lattice formed by B 12 cage units. The Einstein temperatures are ∼254 and ∼164 K, and the Debye temperatures are ∼1040 K and ∼1190 K for YB 12 and LuB 12 respectively. The LuB 12 low-temperature NTE is connected with an induced low-energy defect mode. The YB 12 superconducting transition has not been detected up to 2.5 K

  12. NTD germanium: a novel material for low-temperature bolometers

    International Nuclear Information System (INIS)

    Haller, E.E.; Palaio, N.P.; Rodder, M.; Hansen, W.L.; Kreysa, E.

    1982-06-01

    Six samples of ultra-pure (absolute value N/sub A/ - N/sub D/ absolute value less than or equal to 10 11 cm -3 ), single-crystal germanium have been neutron transmutation doped with neutron doses between 7.5 x 10 16 and 1.88 x 10 18 cm -2 . After thermal annealing at 400 0 C for six hours in a pure argon atmosphere, the samples have been characterized with Hall effect and resistivity measurements between 300 and 0.3 K. Our results show that the resistivity in the low temperature, hopping conduction regime can be approximated with rho = rho 0 exp(Δ/T). The three more heavily doped samples show values for rho 0 and Δ ranging from 430 to 3.3 Ω cm and from 4.9 to 2.8 K, respectively. The excellent reproducibility of neutron transmutation doping and the values of rho 0 and Δ make NTD Ge a prime candidate for the fabrication of low temperature, low noise bolometers. The large variation in the tabulated values of the thermal neutron cross sections for the different germanium isotopes makes it clear that accurate measurements of these cross-sections for well defined neutron energy spectra would be highly desirable

  13. Field measurement for large bending magnets

    International Nuclear Information System (INIS)

    Lazzaro, A.; Cappuzzello, F.; Cunsolo, A.; Cavallaro, M.; Foti, A.; Orrigo, S.E.A.; Rodrigues, M.R.D.; Winfield, J.S.

    2008-01-01

    The results of magnetic field measurements of the large bending magnet of the MAGNEX spectrometer are presented. The experimental values are used to build an Enge function by the least-squares method. The resulting field is compared to the measured one, showing too large deviation for application to ray reconstruction techniques. Similarly, the experimental values are compared with results from a three-dimensional finite elements calculation. Again the deviations between measured and calculated field are too large for a direct application of the latter to ray reconstruction, while its reliability is sufficient for analysis purposes. In particular, it has been applied to study the effect of the inaccuracies in the probe location and orientation on the precision of field reconstruction, and to establish the requirements for the field interpolation. These inaccuracies are found to be rather important, especially for the transversal components of the field, with the consequence that their effect on the reconstructed field should be minimized by special interpolation algorithms

  14. Planar permanent magnet multipoles: Measurements and configurations

    International Nuclear Information System (INIS)

    Cremer, T.; Tatchyn, R.

    1995-05-01

    Biplanar arrays of N rectangular permanent magnet (PM) blocks can be used to generate high quality N-pole fields in close proximity to the array axis. In applications featuring small-diameter charged particle beams, N-poles of adequate quality can be realized at relatively low cost using small volumes of PM material. In this paper we report on recent measurements performed on planar PM multipoles, and discuss techniques for improving the field quality of such devices at distances appreciably far away from the axis. Applications to hybrid/PM insertion device designs for linac-driven Free Electron Laser (FEL) operation in the x-ray range are described

  15. Low temperature delayed recombinationand trap tunneling

    Czech Academy of Sciences Publication Activity Database

    Mihóková, Eva; Schulman, L. S.

    2015-01-01

    Roč. 27, č. 7 (2015), 1-8 ISSN 0953-8984 Grant - others:AVČR(CZ) M100101212 Institutional support: RVO:68378271 Keywords : scintillator * tunneling * traps Subject RIV: BM - Solid Matter Physics ; Magnetism Impact factor: 2.209, year: 2015

  16. Magnetic measurements for RFP experiment on STP-3(M)

    International Nuclear Information System (INIS)

    Nagata, Akiyoshi; Tamaru, Takeshi; Arimoto, Hideki; Yamada, Shuichi; Sato, Koichi.

    1984-03-01

    Magnetic measurements are arranged for RFP experiment on STP-3(M). Magnetic measurements will be applied to investigate the discharge parameters, F(field reversal ratio) - theta(pinch parameter) diagram, the physical mechanism of flux enhancement and the toroidal and poloidal mode numbers due to the MHD instability. Theoretical considerations and instrumental techniques for magnetic measurements are described in detail. (author)

  17. Design principles for prototype and production magnetic measurements of superconducting magnets

    International Nuclear Information System (INIS)

    Brown, B.C.

    1989-02-01

    The magnetic field strength and shape for SSC superconducting magnets will determine critical properties of the accelerator systems. This paper will enumerate the relations between magnetic field properties and magnet material selection and assembly techniques. Magnitudes of various field errors will be explored along with operating parameters which can affect them. Magnetic field quality requirements will be compared to available measuring techniques and the relation between magnetic field measurements and other quality control efforts will be discussed. This will provide a framework for designing a complete magnet measurement plan for the SSC project. 17 refs., 1 fig., 5 tabs

  18. Low temperature magnetic properties of NdCu2

    International Nuclear Information System (INIS)

    Hillberg, M.; Wagener, W.; Melo, M.A.C. de; Klauss, H.H.; Litterst, F.J.; Loewenhaupt, W.

    1997-01-01

    μSR experiments on NdCu 2 give evidence for short range order below 25 K above T N =6.5 K. No signal was detected between 16 K and 1.2 K where neutron scattering reveals an incommensurate spin structure. Below 1.2 K the μSR signal is recovered and shows a rotation with 22 MHz. This is interpreted with a squaring up of Nd spins accompanied by a decrease of magnon excitations which is reflected in a decrease of damping of the muon signal

  19. Low temperature magnetic structure of MnSe

    Indian Academy of Sciences (India)

    Author Affiliations. J B C Efrem D'sa1 P A Bhobe1 K R Priolkar1 A Das2 P S R Krishna2 P R Sarode1 R B Prabhu1. Department of Physics, Goa University, Taleigao Plateau, Goa 403 206, India; Solid State Physics Division, Bhabha Atomic Research Centre, Mumbai 400 085, India ...

  20. Effect of low temperature annealing on magneto-caloric effect of Ni–Mn–Sn–Al ferromagnetic shape memory alloy

    Energy Technology Data Exchange (ETDEWEB)

    Agarwal, Sandeep [Haldia Institute of Technology, Haldia 721657, West Bengal (India); LCMP, Department of Condensed Matter Physics and Material Sciences, S.N. Bose National Centre for Basic Sciences, JD Block, Salt Lake, Kolkata 700098 (India); Stern-Taulats, Enric; Mañosa, Lluís [Departament d’Estructura i Constituents de la Matèria, Facultat de Física, Universitat de Barcelona, 08028 Barcelona, Catalonia (Spain); Mukhopadhyay, P.K., E-mail: pkm@bose.res.in [LCMP, Department of Condensed Matter Physics and Material Sciences, S.N. Bose National Centre for Basic Sciences, JD Block, Salt Lake, Kolkata 700098 (India)

    2015-08-25

    Highlights: • Magnetic properties of the system changed after secondary heat treatment. • MCE was enhanced after Al was partially replaced with Sn in Ni–Mn–Al system. • Suitable heat treatment further increased overall MCE in the sample. • Change in magnetic properties occurred due to change in atomic ordering. - Abstract: We studied the effect of low temperature annealing on the atomic ordering and consequent changes in the magnetization and magnetocaloric effect of the sample. The annealing at lower temperatures initially decreased the magnetization and magnetocaloric effect in the sample, but at higher annealing temperatures both increased. The changes in magnetization and magnetocaloric effect arise from the change in atomic ordering. We have shown that post quenching heat treatment offers easy way of optimizing the alloy for magnetocaloric effect. In order to verify that there was no overestimation in the measurement of magnetocaloric effect we also performed an infield calorimetric measurements and compared them with those from the magnetization measurements. We did not find remarkable difference between them.

  1. Measuring the Earth's Magnetic Field in a Laboratory

    Science.gov (United States)

    Cartacci, A.; Straulino, S.

    2008-01-01

    Two methods for measuring the Earth's magnetic field are described. In the former, according to Gauss, the Earth's magnetic field is compared with that of a permanent magnet; in the latter, a well-known method, the comparison is made with the magnetic field generated by a current. As all the used instruments are available off the shelf, both…

  2. Low temperature thermal expansion of liquid Helium-4

    International Nuclear Information System (INIS)

    Berthold, J.E.

    1976-01-01

    Results of a measurement of the thermal expansion of liquid He-4 are presented along the saturated vapor pressure curve at low temperatures (0.1 - 0.6 0 K). The thermal expansion is related to the low momentum region of the He-4 excitation spectrum, and the results of this measurement are analyzed to gain information concerning deviations from linearity in the phonon region of the spectrum. The data is also compared with theoretical predictions of Alrich and Bhatt and McMillan and with the thermal expansion measurement of Van Degrift. In addition a discussion of previous experimental evidence on the shape of the low momentum region of the dispersion relation is presented

  3. Chemical yields from low-temperature pyrolysis of CCA-treated wood

    Science.gov (United States)

    Qirong Fu; Dimitris Argyropolous; Lucian Lucia; David Tilotta; Stan Lebow

    2009-01-01

    Low-temperature pyrolysis offers a feasible option for wood-waste management and the recovery of a variety of useful chemicals. The effect of chromated copper arsenate (CCA) wood preservative on the yield and composition of various pyrolysis products was investigated in the present research. A novel quantitative 31P nuclear magnetic resonance (...

  4. Low-temperature localization in the transport properties of self-doped

    Indian Academy of Sciences (India)

    ... such as electron–electron, Kondo, electron–phonon and electron–magnon are found to be strongly influenced by the applied magnetic field. The results suggest that interplay between electron–electron and Kondo-like scatterings lead to the localization in the temperature dependence of resistivity at low temperature.

  5. Low temperature gamma sterilization of a bioresorbable polymer, PLGA

    Science.gov (United States)

    Davison, Lisa; Themistou, Efrosyni; Buchanan, Fraser; Cunningham, Eoin

    2018-02-01

    Medical devices destined for insertion into the body must be sterilised before implantation to prevent infection or other complications. Emerging biomaterials, for example bioresorbable polymers, can experience changes in their properties due to standard industrial sterilization processes. Gamma irradiation is one of the most reliable, large scale sterilization methods, however it can induce chain scission, cross-linking or oxidation reactions in polymers. sterilization at low temperature or in an inert atmosphere has been reported to reduce the negative effects of gamma irradiation. The aim of this study was to investigate the impact of low temperature sterilization (at -80 °C) when compared to sterilization at ambient temperature (25 °C) both in inert atmospheric conditions of nitrogen gas, on poly(lactide co-glycolide) (PLGA). PLGA was irradiated at -80 and 25 °C at 40 kGy in a nitrogen atmosphere. Samples were characterised using differential scanning calorimetry (DSC), tensile test, Fourier transform infrared (FTIR) spectroscopy, proton nuclear magnetic resonance (1H NMR) spectroscopy and gel permeation chromatography (GPC). The results showed that the molecular weight was significantly reduced as was the glass transition temperature, an indication of chain scission. FTIR showed small changes in chemical structure in the methyl and carbonyl groups after irradiation. Glass transition temperature was significantly different between irradiation at -80 °C and irradiation at 25 °C, however this was a difference of only 1 °C. Ultimately, the results indicate that the sterilization temperature used does not affect PLGA when carried out in a nitrogen atmosphere.

  6. Ruthenium(V) oxides from low-temperature hydrothermal synthesis

    Energy Technology Data Exchange (ETDEWEB)

    Hiley, Craig I.; Walton, Richard I. [Department of Chemistry, University of Warwick, Coventry (United Kingdom); Lees, Martin R. [Department of Physics, University of Warwick, Coventry (United Kingdom); Fisher, Janet M.; Thompsett, David [Johnson Matthey Technology Centre, Reading (United Kingdom); Agrestini, Stefano [Max-Planck Institut, CPfS, Dresden (Germany); Smith, Ronald I. [ISIS Neutron and Muon Source, Rutherford Appleton Laboratory, Harwell Oxford, Didcot (United Kingdom)

    2014-04-22

    Low-temperature (200 C) hydrothermal synthesis of the ruthenium oxides Ca{sub 1.5}Ru{sub 2}O{sub 7}, SrRu{sub 2}O{sub 6}, and Ba{sub 2}Ru{sub 3}O{sub 9}(OH) is reported. Ca{sub 1.5}Ru{sub 2}O{sub 7} is a defective pyrochlore containing Ru{sup V/VI}; SrRu{sub 2}O{sub 6} is a layered Ru{sup V} oxide with a PbSb{sub 2}O{sub 6} structure, whilst Ba{sub 2}Ru{sub 3}O{sub 9}(OH) has a previously unreported structure type with orthorhombic symmetry solved from synchrotron X-ray and neutron powder diffraction. SrRu{sub 2}O{sub 6} exhibits unusually high-temperature magnetic order, with antiferromagnetism persisting to at least 500 K, and refinement using room temperature neutron powder diffraction data provides the magnetic structure. All three ruthenates are metastable and readily collapse to mixtures of other oxides upon heating in air at temperatures around 300-500 C, suggesting they would be difficult, if not impossible, to isolate under conventional high-temperature solid-state synthesis conditions. (copyright 2014 WILEY-VCH Verlag GmbH and Co. KGaA, Weinheim)

  7. Low-temperature thermal conductivity of terbium-gallium garnet

    International Nuclear Information System (INIS)

    Inyushkin, A. V.; Taldenkov, A. N.

    2010-01-01

    Thermal conductivity of paramagnetic Tb 3 Ga 5 O 12 (TbGG) terbium-gallium garnet single crystals is investigated at temperatures from 0.4 to 300 K in magnetic fields up to 3.25 T. A minimum is observed in the temperature dependence κ(T) of thermal conductivity at T min = 0.52 K. This and other singularities on the κ(T) dependence are associated with scattering of phonons from terbium ions. The thermal conductivity at T = 5.1 K strongly depends on the magnetic field direction relative to the crystallographic axes of the crystal. Experimental data are considered using the Debye theory of thermal conductivity taking into account resonance scattering of phonons from Tb 3+ ions. Analysis of the temperature and field dependences of the thermal conductivity indicates the existence of a strong spin-phonon interaction in TbGG. The low-temperature behavior of the thermal conductivity (field and angular dependences) is mainly determined by resonance scattering of phonons at the first quasi-doublet of the electron spectrum of Tb 3+ ion.

  8. Low temperature irradiation facility at Kyoto University Reactor (KUR)

    International Nuclear Information System (INIS)

    Atobe, Kozo; Okada, Moritami; Yoshida, Hiroyuki; Kodaka, Hisao; Miyata, Kiyomi.

    1977-01-01

    A new refrigeration system has been substituted to the low temperature irradiation facility at KUR instead of the previous one, since April in 1975. The model 1204 CTi He liquifier was designed to be modified for the refrigerator with the capacity of 30 watts at 10 K. The refrigeration capacity of 38 watts at 10 K was defined using a special cryostat and transfer-tubes, and the lowest temperature of about 18 K was measured using the irradiation loop without reactor operation. The reconstructed facility enables us to hold the many specimens simultaneously in the sample chamber of the irradiation loop at about 25 K during reactor operation of 5 MW. The irradiation dose has been reached about 6.6 x 10 16 n sub(f)/cm 2 and 6.1 x 10 17 n sub(th)/cm 2 with the normal reactor operation cycle of up to 77 hours. The stable operation condition of the machine and the special safety system for the refrigeration system enable us to maintain easily the facility with a constant operation condition for such a long time irradiation. Many kinds of low temperature neutron irradiation experiments are carried out using the facility, which techniques are partially reported. (auth.)

  9. Field measurements for low-aperture magnetic elements

    International Nuclear Information System (INIS)

    Mikhajlichenko, A.A.

    1989-01-01

    The method of the field measurements with help of bismuth wire in low aperture magnetic elements is revised. The quadrupole with permanent magnets was tested. It has aperture diameter about 4 mm and length 40 mm. Gradient about 38 kOe/cm was measured. The accuracy of the magnetic axis position definition is better than 1 μm. This method is a good kandidate for linear colider low aperture magnetic elements measurements. 7 refs.; 6 figs

  10. Determination of Henry’s law constant of light hydrocarbon gases at low temperatures

    International Nuclear Information System (INIS)

    Mohebbi, V.; Naderifar, A.; Behbahani, R.M.; Moshfeghian, M.

    2012-01-01

    Highlights: ► Henry’s constants of light hydrocarbon gases are reported at low temperatures. ► Solubility of iso-butane in water at low temperatures (275 K to 293 K) was measured. ► An expression of Krichevsky–Kasarnovsky equation is reported. - Abstract: The solubility of i-butane in water at the low temperatures was measured (274 K to 293 K). Additionally, Henry’s law constants of light hydrocarbons (methane, ethane, propane, i-butane, and n-butane) in water at the low temperatures are reported. A modified equation based on Krichevsky–Kasarnovsky equation is proposed to consider the effect of pressure and temperature on the equation parameters. Results show that Henry’s law constant of the selected components depends on temperature. It is deduced that pressure has a considerable effect on Henry’s law constant for methane, ethane, and propane, whereas this dependency for butanes is negligible.

  11. Magnetic Measurements of Storage Ring Magnets for the APS Upgrade Project

    Energy Technology Data Exchange (ETDEWEB)

    Doose, C.; Dejus, R.; Jaski, M.; Jansma, W.; Collins, J.; Donnelly, A.; Liu, J.; Cease, H.; Decker, G.; Jain, A.; DiMarco, J.

    2017-06-01

    Extensive prototyping of storage ring magnets is ongoing at the Advanced Photon Source (APS) in support of the APS Multi-Bend Achromat (MBA) upgrade project (APS-U) [1]. As part of the R&D activities four quadrupole magnets with slightly different geometries and pole tip materials, and one sextupole magnet with vanadium permendur (VP) pole tips were designed, built and tested. Magnets were measured individually using a rotating coil and a Hall probe for detailed mapping of the magnetic field. Magnets were then assembled and aligned relative to each other on a steel support plate and concrete plinth using precision machined surfaces to gain experience with the alignment method chosen for the APS-U storage ring magnets. The required alignment of magnets on a common support structure is 30 μm rms. Measurements of magnetic field quality, strength and magnet alignment after subjecting the magnets and assemblies to different tests are presented.

  12. Highly anisotropic SmCo5 nanoflakes by surfactant-assisted ball milling at low temperature

    International Nuclear Information System (INIS)

    Liu, Lidong; Zhang, Songlin; Zhang, Jian; Ping Liu, J.; Xia, Weixing; Du, Juan; Yan, Aru; Yi, Jianhong; Li, Wei; Guo, Zhaohui

    2015-01-01

    Surfactant-assisted ball milling (SABM) has been shown to be a promising method for preparing rare earth-transition metal (RE-TM) nanoflakes and nanoparticles. In this work, we prepared SmCo 5 nanoflakes by SABM at low temperature, and 2-methyl pentane and trioctylamine were specially selected as solvent and surfactant, respectively, due to their low melting points. The effects of milling temperature on the morphology, microstructure and magnetic performance of SmCo 5 nanoflakes were investigated systematically. Comparing with the samples milled at room temperature, the SmCo 5 nanoflakes prepared at low temperature displayed more homogeneous morphology and lower oxygen content. Remarkably, better crystallinity, better grain alignment and larger remanence ratio were shown in the samples milled at low temperature, which resulted from the distinct microstructure caused by low milling temperature. The differences in structural evolution between the SmCo 5 nanoflakes milled at room temperature and low temperature, including the formation of nanocrystalline, grain boundary sliding, grain rotation, et al., were discussed. It was found that lowering the temperature of SABM was a powerful method for the fabrication of RE-TM nanoflakes, which showed better hard magnetic properties and lower oxygen content. This was important for the preparation of high-performance sintered magnets, bonded magnets and nanocomposite magnets. - Highlights: • We prepare SmCo 5 nanoflakes by surfactant-assisted ball milling at low temperature. • Better grain alignment and higher remanence ratio are achieved. • The oxygen content is reduced by lowering the milling temperature. • A distinct microstructural evolution caused by low milling temperature is clarified

  13. Inconsistent effects of developmental temperatureacclimation on low-temperature performance andmetabolism in Drosophila melanogaster

    DEFF Research Database (Denmark)

    Kristensen, Torsten Nygaard; Overgaard, Johannes; Hoffmann, Ary A

    2012-01-01

    Question: Does acclimation to developmental temperature consistently affect metabolismand low-temperature performance when measured in different laboratory and field assays? Hypothesis: Developmental acclimation reflecting naturally fluctuating thermal conditionsconsistently increases different...... conditions in the field, while constant cool rearingconditions led to high cold resistance. The fluctuating- and low-temperature rearing conditionsresulted in a similar metabolic profile, while the 24C rearing profile was distinct and showeda lack of plasticity. The effects of developmental acclimation...

  14. PHASE GRADIENT METHOD OF MAGNETIC FIELD MEASUREMENTS IN ELECTRIC VEHICLES

    Directory of Open Access Journals (Sweden)

    N. G. Ptitsyna

    2013-01-01

    Full Text Available Operation of electric and hybrid vehicles demands real time magnetic field control, for instance, for fire and electromagnetic safety. The article deals with a method of magnetic field measurements onboard electric cars taking into account peculiar features of these fields. The method is based on differential methods of measurements, and minimizes the quantity of magnetic sensors.

  15. Ultrathin magnetic structures II measurement techniques and novel magnetic properties

    CERN Document Server

    Heinrich, Bretislav

    2006-01-01

    The ability to understand and control the unique properties of interfaces has created an entirely new field of magnetism, with profound impact in technology and serving as the basis for a revolution in electronics. Our understanding of the physics of magnetic nanostructures has also advanced significantly. This rapid development has generated a need for a comprehensive treatment that can serve as an introduction to the field for those entering it from diverse fields, but which will also serve as a timely overview for those already working in this area. The four-volume work Ultra-Thin Magnetic

  16. Measuring magnetic field vector by stimulated Raman transitions

    International Nuclear Information System (INIS)

    Wang, Wenli; Wei, Rong; Lin, Jinda; Wang, Yuzhu; Dong, Richang; Zou, Fan; Chen, Tingting

    2016-01-01

    We present a method for measuring the magnetic field vector in an atomic fountain by probing the line strength of stimulated Raman transitions. The relative line strength for a Λ-type level system with an existing magnetic field is theoretically analyzed. The magnetic field vector measured by our proposed method is consistent well with that by the traditional bias magnetic field method with an axial resolution of 6.1 mrad and a radial resolution of 0.16 rad. Dependences of the Raman transitions on laser polarization schemes are also analyzed. Our method offers the potential advantages for magnetic field measurement without requiring additional bias fields, beyond the limitation of magnetic field intensity, and extending the spatial measurement range. The proposed method can be widely used for measuring magnetic field vector in other precision measurement fields.

  17. Quantum Simulations of Low Temperature High Energy Density Matter

    National Research Council Canada - National Science Library

    Voth, Gregory

    2004-01-01

    .... Using classical molecular dynamics simulations to evaluate these equilibrium properties would predict qualitatively incorrect results for low temperature solid hydrogen, because of the highly quantum...

  18. Geochemical Controls on Nuclear Magnetic Resonance Measurements

    International Nuclear Information System (INIS)

    Knight, Rosemary; Prasad, Manika; Keating, Kristina

    2003-01-01

    OAK-B135 Our research objectives are to determine, through an extensive set of laboratory experiments, the effect of the specific mineralogic form of iron and the effect of the distribution of iron on proton nuclear magnetic resonance (NMR) relaxation mechanisms. In the first nine months of this project, we have refined the experimental procedures to be used in the acquisition of the laboratory NMR data; have ordered, and conducted preliminary measurements on, the sand samples to be used in the experimental work; and have revised and completed the theoretical model to use in this project. Over the next year, our focus will be on completing the first phase of the experimental work where the form and distribution of the iron in the sands in varied

  19. Anomalous thermal property behaviour of uranium at low temperatures

    International Nuclear Information System (INIS)

    Sandenaw, T.A.

    1975-01-01

    Low temperature heat capacity curves are presented for polycrystalline 235 U and 238 U metals in different microstructural states and of different purities. Thermal conductivity versus temperature curves are shown for low-purity, polycrystalline 238 U in the temperature range between approximately 80 and 373 0 K for metal having undergone varied fabrication procedures. Published information suggests that there will be no structural modification in very pure uranium below room temperature. The influence of impurities on low temperature transitions may be through their effects on dislocation formation. Thermal conductivity and heat capacity runs started at approximately 80 0 K, after holding specimens at the temperature of boiling liquid nitrogen, do not give results which match up with runs started below 36 to 43 0 K. Result of measurements started at approximately 80 0 K indicate that an ordering mechanism is predominating, with microstructure rather than purity being the important factor. This can be explained if ordering at approximately 80 0 K is through lattice imperfections remaining from prior specimen processing. The drop off in heat capacity appearing above 36 0 K in the C/sub p/ versus T curves of 235 U and 238 U suggest the possibility of: (1) heat evolution from a developing antiphase structure or (2) heat evolution similar to that noted with a quenched martensite. Physical property changes in 238 U at 250 to 270 0 K and at 325 to 350 0 K seem to be related to the heat evolution which starts at 36 0 K during adiabatic heat capacity measurements. The data from heat capacity and thermal conductivity measurements are analyzed to help explain the significance of the sometimes very slight physical property changes observed at 36 to 43, approximately 80, 250 to 270 and 325 to 350 0 K in uranium metal. (U.S.)

  20. Magnetic susceptibility measurement using 2D magnetic resonance imaging

    Czech Academy of Sciences Publication Activity Database

    Marcon, P.; Bartušek, Karel; Burdkova, M.; Dokoupil, Zdeněk

    2011-01-01

    Roč. 22, č. 10 (2011), 105702:1-8 ISSN 0957-0233 R&D Projects: GA ČR GAP102/11/0318; GA MŠk ED0017/01/01 Institutional research plan: CEZ:AV0Z20650511 Keywords : magnetic flux density * magnetic susceptibility * MRI * MR signal * reaction field Subject RIV: JA - Electronics ; Optoelectronics, Electrical Engineering Impact factor: 1.494, year: 2011