Instrumental neutron activation analysis of soil sample

International Nuclear Information System (INIS)

Abdul Khalik Haji Wood.

1983-01-01

This paper describes the analysis of soil samples collected from 5 different location around Sungai Lui, Kajang, Selangor, Malaysia. These sample were taken at 22-24 cm from the top of the ground and were analysed using the techniques of Instrumental Neutron Activation Analysis (INAA). The analysis on soil sample taken above 22-24 cm level were done in order to determine if there is any variation in elemental contents at different sampling levels. The results indicate a wide variation in the contents of the samples. About 30 elements have been analysed. The major ones are Na, I, Cl, Mg, Al, K, Ti, Ca and Fe. Trace elements analysed were Ba, Sc, V, Cr, Mn, Ga, As, Zn, Br, Rb, Co, Hf, Zr, Th, U, Sb, Cs, Ce, Sm, Eu, Tb, Dy, Yb, Lu and La. (author)

Astrobiology Sample Analysis Program (ASAP) for Advanced Life Detection Instrumentation Development and Calibration

Science.gov (United States)

Glavin, Daniel; Brinkerhoff, Will; Dworkin, Jason; Eigenbrode, Jennifer; Franz, Heather; Mahaffy, Paul; Stern, Jen; Blake, Daid; Sandford, Scott; Fries, marc;

Sparse feature learning for instrument identification: Effects of sampling and pooling methods.

Science.gov (United States)

Han, Yoonchang; Lee, Subin; Nam, Juhan; Lee, Kyogu

2016-05-01

Feature learning for music applications has recently received considerable attention from many researchers. This paper reports on the sparse feature learning algorithm for musical instrument identification, and in particular, focuses on the effects of the frame sampling techniques for dictionary learning and the pooling methods for feature aggregation. To this end, two frame sampling techniques are examined that are fixed and proportional random sampling. Furthermore, the effect of using onset frame was analyzed for both of proposed sampling methods. Regarding summarization of the feature activation, a standard deviation pooling method is used and compared with the commonly used max- and average-pooling techniques. Using more than 47 000 recordings of 24 instruments from various performers, playing styles, and dynamics, a number of tuning parameters are experimented including the analysis frame size, the dictionary size, and the type of frequency scaling as well as the different sampling and pooling methods. The results show that the combination of proportional sampling and standard deviation pooling achieve the best overall performance of 95.62% while the optimal parameter set varies among the instrument classes.

Development and Application of the Lincoln Adherence Instrument Record for Assessing Client Adherence to Advice in Dog Behavior Consultations and Success

Directory of Open Access Journals (Sweden)

Lisanna Lamb

2018-03-01

Full Text Available Adherence to the advice of medical practitioners is critical to successful treatment outcomes and has been much researched in human health, but is less well studied in the veterinary and clinical animal behavior fields. Given that the management of behavior problems often requires substantial change in established client behavior, it is likely that adherence is a substantive issue affecting success. However, little is known about the relationships between relevant factors, and there is no established way of assessing these. Therefore, the aim of this study was to develop an instrument for coding factors likely to impinge on pet owner adherence to behavior advice and validate its utility through the identification of the factors appearing to relate most closely to a successful treatment outcome in a sample population from our clinic. Potential factors affecting adherence were identified from human health and animal behavior studies, and a survey instrument developed with items matched to these factors. Forty-two dog owners who had attended the University of Lincoln Animal Behavior Clinic over a 2-year period provided data used in the analysis. The assessment of treatment outcome success by clients and clinicians was correlated, but clinicians tended to overestimate success by half a point on a 5-point scale. Eleven items relating to adherence were found to correlate with client ratings of treatment success in a univariate analysis, with three of these remaining in an ordinal logistic regression model. These three related to trust in the advice given by the clinician, concern over distress caused to the pet in the longer term and the perceived recommendation of treatment measures that had failed. By further examining the relationship between all of these factors in a hierarchical cluster analysis, we were able to postulate ways in which we might be able to improve client adherence and thus treatment success. This provides a model for the

Development and Application of the Lincoln Adherence Instrument Record for Assessing Client Adherence to Advice in Dog Behavior Consultations and Success.

Science.gov (United States)

Lamb, Lisanna; Affenzeller, Nadja; Hewison, Lynn; McPeake, Kevin James; Zulch, Helen; Mills, Daniel S

2018-01-01

Adherence to the advice of medical practitioners is critical to successful treatment outcomes and has been much researched in human health, but is less well studied in the veterinary and clinical animal behavior fields. Given that the management of behavior problems often requires substantial change in established client behavior, it is likely that adherence is a substantive issue affecting success. However, little is known about the relationships between relevant factors, and there is no established way of assessing these. Therefore, the aim of this study was to develop an instrument for coding factors likely to impinge on pet owner adherence to behavior advice and validate its utility through the identification of the factors appearing to relate most closely to a successful treatment outcome in a sample population from our clinic. Potential factors affecting adherence were identified from human health and animal behavior studies, and a survey instrument developed with items matched to these factors. Forty-two dog owners who had attended the University of Lincoln Animal Behavior Clinic over a 2-year period provided data used in the analysis. The assessment of treatment outcome success by clients and clinicians was correlated, but clinicians tended to overestimate success by half a point on a 5-point scale. Eleven items relating to adherence were found to correlate with client ratings of treatment success in a univariate analysis, with three of these remaining in an ordinal logistic regression model. These three related to trust in the advice given by the clinician, concern over distress caused to the pet in the longer term and the perceived recommendation of treatment measures that had failed. By further examining the relationship between all of these factors in a hierarchical cluster analysis, we were able to postulate ways in which we might be able to improve client adherence and thus treatment success. This provides a model for the application of the instrument

Autonomous site selection and instrument positioning for sample acquisition

Science.gov (United States)

Shaw, A.; Barnes, D.; Pugh, S.

The European Space Agency Aurora Exploration Program aims to establish a European long-term programme for the exploration of Space, culminating in a human mission to space in the 2030 timeframe. Two flagship missions, namely Mars Sample Return and ExoMars, have been proposed as recognised steps along the way. The Exomars Rover is the first of these flagship missions and includes a rover carrying the Pasteur Payload, a mobile exobiology instrumentation package, and the Beagle 2 arm. The primary objective is the search for evidence of past or present life on mars, but the payload will also study the evolution of the planet and the atmosphere, look for evidence of seismological activity and survey the environment in preparation for future missions. The operation of rovers in unknown environments is complicated, and requires large resources not only on the planet but also in ground based operations. Currently, this can be very labour intensive, and costly, if large teams of scientists and engineers are required to assess mission progress, plan mission scenarios, and construct a sequence of events or goals for uplink. Furthermore, the constraints in communication imposed by the time delay involved over such large distances, and line-of-sight required, make autonomy paramount to mission success, affording the ability to operate in the event of communications outages and be opportunistic with respect to scientific discovery. As part of this drive to reduce mission costs and increase autonomy the Space Robotics group at the University of Wales, Aberystwyth is researching methods of autonomous site selection and instrument positioning, directly applicable to the ExoMars mission. The site selection technique used builds on the geometric reasoning algorithms used previously for localisation and navigation [Shaw 03]. It is proposed that a digital elevation model (DEM) of the local surface, generated during traverse and without interaction from ground based operators, can be

Factors affecting genotyping success in giant panda fecal samples.

Science.gov (United States)

Zhu, Ying; Liu, Hong-Yi; Yang, Hai-Qiong; Li, Yu-Dong; Zhang, He-Min

2017-01-01

Fecal samples play an important role in giant panda conservation studies. Optimal preservation conditions and choice of microsatellites for giant panda fecal samples have not been established. In this study, we evaluated the effect of four factors (namely, storage type (ethanol (EtOH), EtOH -20 °C, 2-step storage medium, DMSO/EDTA/Tris/salt buffer (DETs) and frozen at -20 °C), storage time (one, three and six months), fragment length, and repeat motif of microsatellite loci) on the success rate of microsatellite amplification, allelic dropout (ADO) and false allele (FA) rates from giant panda fecal samples. Amplification success and ADO rates differed between the storage types. Freezing was inferior to the other four storage methods based on the lowest average amplification success and the highest ADO rates ( P panda fecal preservation in microsatellite studies, and EtOH and the 2-step storage medium should be chosen on priority for long-term storage. We recommend candidate microsatellite loci with longer repeat motif to ensure greater genotyping success for giant panda fecal studies.

The psychometric evaluation and predictors for two subjective career success instruments / Audine Marlé du Toit

OpenAIRE

Du Toit, Audine Marlé

2014-01-01

Subjective career success has been the focus of research for a number of years. The term refers to the individual’s personal perception of how successful he/she is in a career. In many qualitative studies subjective career success is found to be a multi-dimensional construct. Although there are quantitative instruments that measure subjective career success, they do not measure the construct on multiple dimensions. The first objective of this study was to determine the validity...

Analysis of atmospheric particulate samples via instrumental neutron activation analysis

International Nuclear Information System (INIS)

Greenberg, R.R.

1990-01-01

Instrumental neutron activation analysis (INAA) is a powerful analytical technique for the elemental characterization of atmospheric particulate samples. It is a true multielement technique with adequate sensitivity to determine 30 to 40 elements in a sample of atmospheric particulate material. Its nondestructive nature allows sample reanalysis by the same or a different analytical technique. In this paper as an example of the applicability of INAA to the study of atmospheric particulate material, a study of the emissions from municipal incinerators is described

Portable Instrument to Measure CDOM Light Absorption in Aquatic Systems: WPI Success Story

Science.gov (United States)

2001-01-01

World Precision Instruments, Inc. (WPI), of Sarasota, FL, in collaboration with NASA's John C. Stennis Space Center, has developed an innovative instrument to accurately measure Colored Dissolved Organic Matter (CDOM) absorption in the field. This successful collaboration has culminated in an exciting new device, called the UltraPath, now commercially available through WPI. Traditional methods of measuring absorption of dissolved materials require special handling and storage prior to measurement. Use of laboratory spectrophotometers as the measuring devices have proven time consuming, cumbersome, and delicate to handle. The UltraPath provides a low-cost, highly sensitive, rugged, portable system that is capable of high sensitivity measurements in widely divergent waters.

Factors affecting genotyping success in giant panda fecal samples

Directory of Open Access Journals (Sweden)

Ying Zhu

2017-05-01

Full Text Available Fecal samples play an important role in giant panda conservation studies. Optimal preservation conditions and choice of microsatellites for giant panda fecal samples have not been established. In this study, we evaluated the effect of four factors (namely, storage type (ethanol (EtOH, EtOH −20 °C, 2-step storage medium, DMSO/EDTA/Tris/salt buffer (DETs and frozen at −20 °C, storage time (one, three and six months, fragment length, and repeat motif of microsatellite loci on the success rate of microsatellite amplification, allelic dropout (ADO and false allele (FA rates from giant panda fecal samples. Amplification success and ADO rates differed between the storage types. Freezing was inferior to the other four storage methods based on the lowest average amplification success and the highest ADO rates (P < 0.05. The highest microsatellite amplification success was obtained from either EtOH or the 2-step storage medium at three storage time points. Storage time had a negative effect on the average amplification of microsatellites and samples stored in EtOH and the 2-step storage medium were more stable than the other three storage types. We only detected the effect of repeat motif on ADO and FA rates. The lower ADO and FA rates were obtained from tri- and tetra-nucleotide loci. We suggest that freezing should not be used for giant panda fecal preservation in microsatellite studies, and EtOH and the 2-step storage medium should be chosen on priority for long-term storage. We recommend candidate microsatellite loci with longer repeat motif to ensure greater genotyping success for giant panda fecal studies.

Finite-sample instrumental variables inference using an asymptotically pivotal statistic

NARCIS (Netherlands)

Bekker, P; Kleibergen, F

2003-01-01

We consider the K-statistic, Kleibergen's (2002, Econometrica 70, 1781-1803) adaptation of the Anderson-Rubin (AR) statistic in instrumental variables regression. Whereas Kleibergen (2002) especially analyzes the asymptotic behavior of the statistic, we focus on finite-sample properties in, a

Risk factors for cesarean section and instrumental vaginal delivery after successful external cephalic version

NARCIS (Netherlands)

de Hundt, Marcella; Vlemmix, Floortje; Bais, Joke M. J.; de Groot, Christianne J.; Mol, Ben Willem; Kok, Marjolein

2016-01-01

Aim of this article is to examine if we could identify factors that predict cesarean section and instrumental vaginal delivery in women who had a successful external cephalic version. We used data from a previous randomized trial among 25 hospitals and their referring midwife practices in the

Robotic, MEMS-based Multi Utility Sample Preparation Instrument for ISS Biological Workstation, Phase I

Data.gov (United States)

National Aeronautics and Space Administration — This project will develop a multi-functional, automated sample preparation instrument for biological wet-lab workstations on the ISS. The instrument is based on a...

Guidelines for Successful Use and Communication of Instrument Heritage in Early Mission Development with a Focus on Spectrometers

Science.gov (United States)

Baker, Elizabeth E.

2012-01-01

Heritage is important for both cost and risk related issues and as such, it is heavily discussed in NASA proposal evaluations. If used and communicated efficiently, heritage can lower both the perception of risk and the associated costs. Definitions of heritage vary between engineering, cost, and scientific communities, but when applied appropriately, heritage provides a benefit to the proposed mission. By making an instrument at least once before, the cost of producing it again can be reduced. The time and effort needed to develop the instrument concept and test the product represent an expense that can be lowered through the use of a previously built and developed instrument. This same thought can be applied when using a flight spare or build-to-print model of the heritage instrument. The lowered perception of risk is a result of the confidence gained in the instrument through successful use in the target environment. This is extremely important in early mission development to the evaluation board. This analysis will use JPL-managed proposals from 2003 to 2011, including Discovery, New Frontiers, and Mars Scout missions. Through the examination of these proposals and their associated debriefs, a set of guidelines have been created for successful use and communication of instrument heritage in early mission development

Evaluation of multivariate calibration models transferred between spectroscopic instruments

DEFF Research Database (Denmark)

Eskildsen, Carl Emil Aae; Hansen, Per W.; Skov, Thomas

2016-01-01

In a setting where multiple spectroscopic instruments are used for the same measurements it may be convenient to develop the calibration model on a single instrument and then transfer this model to the other instruments. In the ideal scenario, all instruments provide the same predictions for the ......In a setting where multiple spectroscopic instruments are used for the same measurements it may be convenient to develop the calibration model on a single instrument and then transfer this model to the other instruments. In the ideal scenario, all instruments provide the same predictions...... for the same samples using the transferred model. However, sometimes the success of a model transfer is evaluated by comparing the transferred model predictions with the reference values. This is not optimal, as uncertainties in the reference method will impact the evaluation. This paper proposes a new method...... for calibration model transfer evaluation. The new method is based on comparing predictions from different instruments, rather than comparing predictions and reference values. A total of 75 flour samples were available for the study. All samples were measured on ten near infrared (NIR) instruments from two...

Theory of sampling: four critical success factors before analysis.

Science.gov (United States)

Wagner, Claas; Esbensen, Kim H

2015-01-01

Food and feed materials characterization, risk assessment, and safety evaluations can only be ensured if QC measures are based on valid analytical data, stemming from representative samples. The Theory of Sampling (TOS) is the only comprehensive theoretical framework that fully defines all requirements to ensure sampling correctness and representativity, and to provide the guiding principles for sampling in practice. TOS also defines the concept of material heterogeneity and its impact on the sampling process, including the effects from all potential sampling errors. TOS's primary task is to eliminate bias-generating errors and to minimize sampling variability. Quantitative measures are provided to characterize material heterogeneity, on which an optimal sampling strategy should be based. Four critical success factors preceding analysis to ensure a representative sampling process are presented here.

Sampled data spectroscopy (SDS): A new technology for radiation instrumentation

International Nuclear Information System (INIS)

Odell, D.M.C.

1992-01-01

A new instrumentation architecture for radiation spectroscopy is in the early stages of development at Savannah River. Based upon the same digital sampling techniques used in sonar and radar, sampled data spectroscopy (SDS) has produced Na(I)/PMT spectra with resolution comparable to conventional PHA systems. This work has laid the foundation for extending SDS techniques to solid state detector applications as well. Two-dimensional SDS processes raw, unintegrated detector output pulses to produce both energy and shape information that is used to construct a conventional energy spectrum. System advantages include zero electronic deadtime to support very high count rates, elimination of pulse pile-up peaks, high noise immunity, and digital system stability and reliability. Small size and low power requirements make 2-D SDS anideal technology for portable instrumentation and remote monitoring applications. Applications of potential interest at Savannah River include on-the-spot spill analysis, real-time waste stream monitoring, and personnel and area monitoring below background levels. A three-dimensional sampled data architecture is also being developed. Relying on image analysis and enhancement techniques, 3-D SDS identifies spectral peaks without determining the energy of any individual detector pulses. These techniques also open up a new avenue of exploration for reducing or removing Compton effects from the spectra of single detector systems. The intended application for this technique is waste characterization where lower energy isotopes are often obscured by the Compton scattering from dominant isotopes such as Csl37

Elemental analysis of soil and hair sample by instrumental neutron activation analysis

International Nuclear Information System (INIS)

Chung, Yong Sam; Quraishi, Shamshad Begum; Moon, Jong Hwa; Kim, Sun Ha; Baek, Sung Yeoil; Kang, Sang Hoon; Lim, Jong Myoung; Cho, Hyun Je; Kim, Young Jin

2004-03-01

Myanmar soil sample was analyzed by using the instrumental neutron activation analysis. The elemental concentrations in the sample, altogether 34 elements, Al As, Ba, Ce, Co, Cr, Cs, Eu, Fe, Ga, Gd, Hf, Ir, K, La, Lu, Mn, Na, Nd, Rb, Sb, Sc, Se, Sm, Th, Ti, V, Yb, Zn and Zr were determined. The concentration of 17 elements (Al, Au, Br, Ca, Cl, Cr, Cu, Co, Fe, Hg, K, Na, Mn, Mg, Sb, Se, Zn) in human hair samples were determined by INAA For quality control of analytical method, certified reference material was used

Elemental analysis of soil and hair sample by instrumental neutron activation analysis

Energy Technology Data Exchange (ETDEWEB)

Chung, Yong Sam; Quraishi, Shamshad Begum; Moon, Jong Hwa; Kim, Sun Ha; Baek, Sung Yeoil; Kang, Sang Hoon; Lim, Jong Myoung; Cho, Hyun Je; Kim, Young Jin

2004-03-01

Myanmar soil sample was analyzed by using the instrumental neutron activation analysis. The elemental concentrations in the sample, altogether 34 elements, Al As, Ba, Ce, Co, Cr, Cs, Eu, Fe, Ga, Gd, Hf, Ir, K, La, Lu, Mn, Na, Nd, Rb, Sb, Sc, Se, Sm, Th, Ti, V, Yb, Zn and Zr were determined. The concentration of 17 elements (Al, Au, Br, Ca, Cl, Cr, Cu, Co, Fe, Hg, K, Na, Mn, Mg, Sb, Se, Zn) in human hair samples were determined by INAA For quality control of analytical method, certified reference material was used.

Instrument developments for chemical and physical characterization, mapping and sampling of extreme environments (Antarctic sub ice environment)

Science.gov (United States)

Vogel, S. W.; Powell, R. D.; Griffith, I.; Lawson, T.; Schiraga, S.; Ludlam, G.; Oen, J.

2009-12-01

A number of instrumentation is currently under development designed to enable the study of subglacial environments in Antarctica through narrow kilometer long boreholes. Instrumentation includes: - slim line Sub-Ice ROV (SIR), - Geochemical Instrumentation Package for Sub Ice Environments (GIPSIE) to study geochemical fluxes in water and across the sediment water interface (CO2, CH4, dO, NH4, NO3, Si, PO4, pH, redox, T, H2, HS, O2, N2O, CTD, particle size, turbidity, color camera, current meter and automated water sampler) with real-time telemetry for targeted sampling, - long term energy-balance mooring system, - active source slide hammer sediment corer, and - integration of a current sensor into the ITP profiler. The instrumentation design is modular and suitable for remote operated as well as autonomous long-term deployment. Of interest to the broader science community is the development of the GIPSIE and efforts to document the effect of sample recovery from depth on the sample chemistry. The GIPSIE is a geochemical instrumentation package with life stream telemetry, allowing for user controlled targeted sampling of water column and the water sediment interphase for chemical and biological work based on actual measurements and not a preprogrammed automated system. The porewater profiler (pH, redox, T, H2, HS, O2, N2O) can penetrate the upper 50 cm of sediment and penetration is documented with real time video. Associated with GIPSIE is an on-site lab set-up, utilizing a set of identical sensors. Comparison between the insitu measurements and measurements taken onsite directly after samples are recovered from depth permits assessing the effect of sample recovery on water and sediment core chemistry. Sample recovery related changes are mainly caused by changes in the pressure temperature field and exposure of samples to atmospheric conditions. Exposure of anaerobic samples to oxygen is here a specific concern. Recovery from depth effects in generally p

Comparison of three sampling instruments, Cytobrush, Curette and OralCDx, for liquid-based cytology of the oral mucosa.

Science.gov (United States)

Reboiras-López, M D; Pérez-Sayáns, M; Somoza-Martín, J M; Antúnez-López, J R; Gándara-Vila, P; Gayoso-Diz, P; Gándara-Rey, J M; García-García, A

2012-01-01

Exfoliative cytology of the oral cavity is a simple and noninvasive technique that permits the study of epithelial cells. Liquid-based cytology is an auxiliary diagnostic tool for improving the specificity and sensitivity of conventional cytology. The objective of our study was to compare the quality of normal oral mucosa cytology samples obtained using three different instruments, Cytobrush®, dermatological curette and Oral CDx® for liquid-based cytology. One hundred four cytological samples of oral cavity were analyzed. Samples were obtained from healthy volunteer subjects using all three instruments. The clinical and demographic variables were age, sex and smoking habits. We analyzed cellularity, quality of the preparation and types of cells in the samples. All preparations showed appropriate preparation quality. In all smears analyzed, cells were distributed uniformly and showed no mucus, bleeding, inflammatory exudate or artifacts. We found no correlation between the average number of cells and the type of instrument. The samples generally consisted of two types of cells: superficial and intermediate. No differences were found among the cytological preparations of these three instruments. We did not observe basal cells in any of the samples analyzed.

The neutron instrument simulation package, NISP

International Nuclear Information System (INIS)

Seeger, P.A.; Daemen, L.L.

2004-01-01

The Neutron Instrument Simulation Package (NISP) performs complete source-to-detector simulations of neutron instruments, including neutrons that do not follow the expected path. The original user interface (MC( ) Web) is a web-based application, http://strider.lansce.lanl.gov/NISP/Welcome.html. This report describes in detail the newer standalone Windows version, NISP( ) Win. Instruments are assembled from menu-selected elements, including neutron sources, collimation and transport elements, samples, analyzers, and detectors. Magnetic field regions may also be specified for the propagation of polarized neutrons including spin precession. Either interface writes a geometry file that is used as input to the Monte Carlo engine (MC( ) Run) in the user's computer. Both the interface and the engine rely on a subroutine library, MCLIB. The package is completely open source. New features include capillary optics, temperature dependence of Al and Be, revised source files for ISIS, and visualization of neutron trajectories at run time. Also, a single-crystal sample type has been successfully imported from McStas (with more generalized geometry), demonstrating the capability of including algorithms from other sources, and NISP( ) Win may render the instrument in a virtual reality file. Results are shown for two instruments under development.

Psychometric Properties of a Screening Instrument for Domestic Violence in a Sample of Iranian Women

Science.gov (United States)

Azadarmaki, Taghi; Kassani, Aziz; Menati, Rostam; Hassanzadeh, Jafar; Menati, Walieh

2016-01-01

Background Domestic violence against women is regarded as an important health problem among women and a serious concern in issues related to human rights. To date, a few screening tools for domestic violence exist for Iranian married women, but they assess only some of the domestic violence components. Objectives The present study aimed to design and determine the validity and reliability of a screening instrument for domestic violence in a sample of Iranian women. Materials and Methods The present study was a cross-sectional psychometric evaluation conducted on 350 married women in Ilam, Iran, in 2014. The samples were selected through multistage sampling and the main method was cluster sampling. A 20-item, self-administered questionnaire was validated by exploratory factor analysis (EFA) and confirmatory factor analysis (CFA). An Eigen value > 1 and a loading factor > 0.3 for each component were considered as indices for extracting domestic violence components. Reliability was calculated by test-retest and Cronbach’s alpha. Also, the content validity index (CVI) and content validity ratio (CVR) were used to measure content validity. The data were analyzed using SPSS-13 and LISREL 8.8 software programs. Results The self-administered instrument was completed by 334 women. The CFA and EFA methods confirmed embedding items and the three-factor structure of the instrument including psychological, physical, and sexual violence, which explained 66% of the total variance of the domestic violence. The ICC and Cronbach’s alpha coefficients were > 0.7 for the components of the questionnaire. The test-retest also revealed strong correlations for each of the domestic violence components (r > 0.6). Conclusions The used instrument for measuring domestic violence had desirable validity and reliability and can be used as a suitable instrument in health and social researches in the local population. PMID:27331052

Determination of trace elements in fisheries samples by instrumental neutron and photon activation analysis

International Nuclear Information System (INIS)

Chattopadhyay, A.; Ellis, K.M.; Nimalasiri Desilva, K.

1979-01-01

An instrumental neutron activation analysis (INAA) method has been developed for the simultaneous determination of trace concentrations of up to 23 elements in fisheries samples. The INAA method consists of irradiations of wet and lyophilized cod muscle and liver samples for three different periods at a flux density of 5x10 11 n.cm -2 .s -1 and subsequent measurements after four different decay periods using high-resolution Ge(Li) gamma-ray spectrometry. Concentrations of several essential and toxic elements have been determined. Loss of certain elements during lyophilization has been studied. Elemental distribution in muscles and livers as a function of the age of fish has been investigated. Precision and accuracy of the INAA method have been evaluated by analysing replicate samples, National Bureau of Standards' bovine liver standard reference material, and an intercalibration fish flour sample provided by the International Council for the Exploration of the Sea. A few fish samples have also been analysed by an alternative method, namely instrumental photon activation analysis (IPAA). Elemental concentrations determined by both INAA and IPAA methods are reported here. (author)

A model for estimating the minimum number of offspring to sample in studies of reproductive success.

Science.gov (United States)

Anderson, Joseph H; Ward, Eric J; Carlson, Stephanie M

2011-01-01

Molecular parentage permits studies of selection and evolution in fecund species with cryptic mating systems, such as fish, amphibians, and insects. However, there exists no method for estimating the number of offspring that must be assigned parentage to achieve robust estimates of reproductive success when only a fraction of offspring can be sampled. We constructed a 2-stage model that first estimated the mean (μ) and variance (v) in reproductive success from published studies on salmonid fishes and then sampled offspring from reproductive success distributions simulated from the μ and v estimates. Results provided strong support for modeling salmonid reproductive success via the negative binomial distribution and suggested that few offspring samples are needed to reject the null hypothesis of uniform offspring production. However, the sampled reproductive success distributions deviated significantly (χ(2) goodness-of-fit test p value reproductive success distribution at rates often >0.05 and as high as 0.24, even when hundreds of offspring were assigned parentage. In general, reproductive success patterns were less accurate when offspring were sampled from cohorts with larger numbers of parents and greater variance in reproductive success. Our model can be reparameterized with data from other species and will aid researchers in planning reproductive success studies by providing explicit sampling targets required to accurately assess reproductive success.

Control of the positional relationship between a sample collection instrument and a surface to be analyzed during a sampling procedure using a laser sensor

Science.gov (United States)

Van Berkel, Gary J [Clinton, TN; Kertesz, Vilmos [Knoxville, TN

2012-02-21

A system and method utilizes distance-measuring equipment including a laser sensor for controlling the collection instrument-to-surface distance during a sample collection process for use, for example, with mass spectrometric detection. The laser sensor is arranged in a fixed positional relationship with the collection instrument, and a signal is generated by way of the laser sensor which corresponds to the actual distance between the laser sensor and the surface. The actual distance between the laser sensor and the surface is compared to a target distance between the laser sensor and the surface when the collection instrument is arranged at a desired distance from the surface for sample collecting purposes, and adjustments are made, if necessary, so that the actual distance approaches the target distance.

Trace DNA Sampling Success from Evidence Items Commonly Encountered in Forensic Casework.

Science.gov (United States)

Dziak, Renata; Peneder, Amy; Buetter, Alicia; Hageman, Cecilia

2018-05-01

Trace DNA analysis is a significant part of a forensic laboratory's workload. Knowing optimal sampling strategies and item success rates for particular item types can assist in evidence selection and examination processes and shorten turnaround times. In this study, forensic short tandem repeat (STR) casework results were reviewed to determine how often STR profiles suitable for comparison were obtained from "handler" and "wearer" areas of 764 items commonly submitted for examination. One hundred and fifty-five (155) items obtained from volunteers were also sampled. Items were analyzed for best sampling location and strategy. For casework items, headwear and gloves provided the highest success rates. Experimentally, eyeglasses and earphones, T-shirts, fabric gloves and watches provided the highest success rates. Eyeglasses and latex gloves provided optimal results if the entire surfaces were swabbed. In general, at least 10%, and up to 88% of all trace DNA analyses resulted in suitable STR profiles for comparison. © 2017 American Academy of Forensic Sciences.

Provenance study of obsidian samples by using portable and conventional X ray fluorescence spectrometers. Performance comparison of both instrumentations

International Nuclear Information System (INIS)

Cristina Vazquez

2012-01-01

The potentiality of portable instrumentation lies on the possibility of the in situ determinations. Sampling, packaging and transport of samples from the site to the laboratory are avoided and the analysis becomes non destructive at all. However, detection limits for light elements are, in most cases, a limitation for quantification purposes. In this work a comparison between the results obtained with an X ray fluorescence spectrometer laboratory based and a portable instrument is performed. A set of 76 obsidian archaeological specimens from northwest Patagonia, Argentina was used to carry out the study. Samples were collected in the area of the middle and high basin of the Limay River. The analytical information obtained with both instrumentations was complemented with Principal Component Analysis in order to define groups and identify provenance sources. The information from both instruments allows arriving to the same conclusion about sample provenance and mobility of hunter-gatherer groups. Three groups of sources were identified in both cases matching with the geographical information. Also, same sets of outlier samples or not associated to these sources were found. Artifact samples were associated mainly to the closest sources, but some of them are related to sources located more than three hundred kilometers, evidencing the large mobility of the hunter-gatherers by the obsidian interchange. No significant differences between concentrations values obtained by laboratory based instrument and portable one were found. (author)

Moving your laboratories to the field – Advantages and limitations of the use of field portable instruments in environmental sample analysis

Energy Technology Data Exchange (ETDEWEB)

Gałuszka, Agnieszka, E-mail: Agnieszka.Galuszka@ujk.edu.pl [Geochemistry and the Environment Division, Institute of Chemistry, Jan Kochanowski University, 15G Świętokrzyska St., 25-406 Kielce (Poland); Migaszewski, Zdzisław M. [Geochemistry and the Environment Division, Institute of Chemistry, Jan Kochanowski University, 15G Świętokrzyska St., 25-406 Kielce (Poland); Namieśnik, Jacek [Department of Analytical Chemistry, Chemical Faculty, Gdańsk University of Technology (GUT), 11/12 G. Narutowicz St., 80-233 Gdańsk (Poland)

2015-07-15

The recent rapid progress in technology of field portable instruments has increased their applications in environmental sample analysis. These instruments offer a possibility of cost-effective, non-destructive, real-time, direct, on-site measurements of a wide range of both inorganic and organic analytes in gaseous, liquid and solid samples. Some of them do not require the use of reagents and do not produce any analytical waste. All these features contribute to the greenness of field portable techniques. Several stationary analytical instruments have their portable versions. The most popular ones include: gas chromatographs with different detectors (mass spectrometer (MS), flame ionization detector, photoionization detector), ultraviolet–visible and near-infrared spectrophotometers, X-ray fluorescence spectrometers, ion mobility spectrometers, electronic noses and electronic tongues. The use of portable instruments in environmental sample analysis gives a possibility of on-site screening and a subsequent selection of samples for routine laboratory analyses. They are also very useful in situations that require an emergency response and for process monitoring applications. However, quantification of results is still problematic in many cases. The other disadvantages include: higher detection limits and lower sensitivity than these obtained in laboratory conditions, a strong influence of environmental factors on the instrument performance and a high possibility of sample contamination in the field. This paper reviews recent applications of field portable instruments in environmental sample analysis and discusses their analytical capabilities. - Highlights: • Field portable instruments are widely used in environmental sample analysis. • Field portable instruments are indispensable for analysis in emergency response. • Miniaturization of field portable instruments reduces resource consumption. • In situ analysis is in agreement with green analytical chemistry

Moving your laboratories to the field – Advantages and limitations of the use of field portable instruments in environmental sample analysis

International Nuclear Information System (INIS)

Gałuszka, Agnieszka; Migaszewski, Zdzisław M.; Namieśnik, Jacek

2015-01-01

The recent rapid progress in technology of field portable instruments has increased their applications in environmental sample analysis. These instruments offer a possibility of cost-effective, non-destructive, real-time, direct, on-site measurements of a wide range of both inorganic and organic analytes in gaseous, liquid and solid samples. Some of them do not require the use of reagents and do not produce any analytical waste. All these features contribute to the greenness of field portable techniques. Several stationary analytical instruments have their portable versions. The most popular ones include: gas chromatographs with different detectors (mass spectrometer (MS), flame ionization detector, photoionization detector), ultraviolet–visible and near-infrared spectrophotometers, X-ray fluorescence spectrometers, ion mobility spectrometers, electronic noses and electronic tongues. The use of portable instruments in environmental sample analysis gives a possibility of on-site screening and a subsequent selection of samples for routine laboratory analyses. They are also very useful in situations that require an emergency response and for process monitoring applications. However, quantification of results is still problematic in many cases. The other disadvantages include: higher detection limits and lower sensitivity than these obtained in laboratory conditions, a strong influence of environmental factors on the instrument performance and a high possibility of sample contamination in the field. This paper reviews recent applications of field portable instruments in environmental sample analysis and discusses their analytical capabilities. - Highlights: • Field portable instruments are widely used in environmental sample analysis. • Field portable instruments are indispensable for analysis in emergency response. • Miniaturization of field portable instruments reduces resource consumption. • In situ analysis is in agreement with green analytical chemistry

Career-success scale – a new instrument to assess young physicians' academic career steps

OpenAIRE

Buddeberg-Fischer, B; Stamm, M; Buddeberg, C; Klaghofer, R

2008-01-01

Abstract Background Within the framework of a prospective cohort study of Swiss medical school graduates, a Career-Success Scale (CSS) was constructed in a sample of young physicians choosing different career paths in medicine. Furthermore the influence of personality factors, the participants' personal situation, and career related factors on their career success was investigated. Methods 406 residents were assessed in terms of career aspired to, and their career progress. The Career-Success...

Geosciences research: development of techniques and instruments for investigation geological environments

International Nuclear Information System (INIS)

1993-01-01

In order to understand the geological environment in Japan, new investigation techniques have been developed. These include: 1) Geological techniques for fracture characterization, 2) Nondestructive investigation techniques for detailed geological structure, 3) Instruments for hydraulic characterization, 4) Instruments for hydrochemical characterization. Results so far obtained are: 1) Fractures can be classified by their patterns, 2) The applicability and limitations of conventional geophysical methods were defined, 3) Instruments for measuring very low permeability were successfully developed, 4) Instruments for sampling formation water without changing in-situ conditions were developed. (author)

Instrumental analysis by gamma spectrometry of low level caesium-137 in marine samples

International Nuclear Information System (INIS)

Figueira, R.C.L.; Silva, L.R.N.; Figueiredo, A.M.G.; Cunha, I.I.L.

1998-01-01

An instrumental method for the analysis of low levels of 137 Cs in marine samples consists in calibrating the detector, determining the counting efficiency of the detector, accumulative counts of background and sample and smoothing the 661.6 keV photopeak. The methodology was applied to reference samples containing low levels of 137 Cs, showing a good accuracy. It was further applied to sediment samples from the southern coast of Brazil. The levels obtained ranged between 1.0 and 1.8 Bq.kg -1 , and the lower limit of detection and minimum detectable concentration values were 10 mBq and 0.28 Bq.kg -1 , respectively. (author)

A compact time-of-flight SANS instrument optimised for measurements of small sample volumes at the European Spallation Source

Energy Technology Data Exchange (ETDEWEB)

Kynde, Søren, E-mail: kynde@nbi.ku.dk [Niels Bohr Institute, University of Copenhagen (Denmark); Hewitt Klenø, Kaspar [Niels Bohr Institute, University of Copenhagen (Denmark); Nagy, Gergely [SINQ, Paul Scherrer Institute (Switzerland); Mortensen, Kell; Lefmann, Kim [Niels Bohr Institute, University of Copenhagen (Denmark); Kohlbrecher, Joachim, E-mail: Joachim.kohlbrecher@psi.ch [SINQ, Paul Scherrer Institute (Switzerland); Arleth, Lise, E-mail: arleth@nbi.ku.dk [Niels Bohr Institute, University of Copenhagen (Denmark)

2014-11-11

The high flux at European Spallation Source (ESS) will allow for performing experiments with relatively small beam-sizes while maintaining a high intensity of the incoming beam. The pulsed nature of the source makes the facility optimal for time-of-flight small-angle neutron scattering (ToF-SANS). We find that a relatively compact SANS instrument becomes the optimal choice in order to obtain the widest possible q-range in a single setting and the best possible exploitation of the neutrons in each pulse and hence obtaining the highest possible flux at the sample position. The instrument proposed in the present article is optimised for performing fast measurements of small scattering volumes, typically down to 2×2×2 mm{sup 3}, while covering a broad q-range from about 0.005 1/Å to 0.5 1/Å in a single instrument setting. This q-range corresponds to that available at a typical good BioSAXS instrument and is relevant for a wide set of biomacromolecular samples. A central advantage of covering the whole q-range in a single setting is that each sample has to be loaded only once. This makes it convenient to use the fully automated high-throughput flow-through sample changers commonly applied at modern synchrotron BioSAXS-facilities. The central drawback of choosing a very compact instrument is that the resolution in terms of δλ/λ obtained with the short wavelength neutrons becomes worse than what is usually the standard at state-of-the-art SANS instruments. Our McStas based simulations of the instrument performance for a set of characteristic biomacromolecular samples show that the resulting smearing effects still have relatively minor effects on the obtained data and can be compensated for in the data analysis. However, in cases where a better resolution is required in combination with the large simultaneous q-range characteristic of the instrument, we show that this can be obtained by inserting a set of choppers.

Evaluation of Rock Powdering Methods to Obtain Fine-grained Samples for CHEMIN, a Combined XRD/XRF Instrument

Science.gov (United States)

Chipera, S. J.; Vaniman, D. T.; Bish, D. L.; Sarrazin, P.; Feldman, S.; Blake, D. F.; Bearman, G.; Bar-Cohen, Y.

2004-01-01

A miniature XRD/XRF (X-ray diffraction / X-ray fluorescence) instrument, CHEMIN, is currently being developed for definitive mineralogic analysis of soils and rocks on Mars. One of the technical issues that must be addressed to enable remote XRD analysis is how best to obtain a representative sample powder for analysis. For powder XRD analyses, it is beneficial to have a fine-grained sample to reduce preferred orientation effects and to provide a statistically significant number of crystallites to the X-ray beam. Although a two-dimensional detector as used in the CHEMIN instrument will produce good results even with poorly prepared powder, the quality of the data will improve and the time required for data collection will be reduced if the sample is fine-grained and randomly oriented. A variety of methods have been proposed for XRD sample preparation. Chipera et al. presented grain size distributions and XRD results from powders generated with an Ultrasonic/Sonic Driller/Corer (USDC) currently being developed at JPL. The USDC was shown to be an effective instrument for sampling rock to produce powder suitable for XRD. In this paper, we compare powder prepared using the USDC with powder obtained with a miniaturized rock crusher developed at JPL and with powder obtained with a rotary tungsten carbide bit to powders obtained from a laboratory bench-scale Retsch mill (provides benchmark mineralogical data). These comparisons will allow assessment of the suitability of these methods for analysis by an XRD/XRF instrument such as CHEMIN.

Breeding snow: an instrumented sample holder for simultaneous tomographic and thermal studies

International Nuclear Information System (INIS)

Pinzer, B; Schneebeli, M

2009-01-01

To study the recrystallization processes during temperature gradient metamorphism of snow, we developed a sample holder that allows applying well-defined and stable thermal gradients to a snow sample while it is scanned in an x-ray micro-tomograph. To this end, both the thermal insulation of the sample as well as image contrast and resolution of the tomography had to be optimized. We solved this conflict by using thin aluminum cylinders in combination with highly insulating foam. This design is light, does not corrupt image quality and provides very good thermal decoupling from the environment. The sample holder was instrumented to measure the effective conductivity of the snow sample and calibrated using five materials of known conductivity. Finite element simulations were consistent with the calibration measurements and gave insight into the internal temperature and heat flux fields. With this setup, geometric and thermal evolution of snow under realistic thermal boundary conditions like alternating temperature gradients can be measured

Developing a theoretical model and questionnaire survey instrument to measure the success of electronic health records in residential aged care.

Science.gov (United States)

Yu, Ping; Qian, Siyu

2018-01-01

Electronic health records (EHR) are introduced into healthcare organizations worldwide to improve patient safety, healthcare quality and efficiency. A rigorous evaluation of this technology is important to reduce potential negative effects on patient and staff, to provide decision makers with accurate information for system improvement and to ensure return on investment. Therefore, this study develops a theoretical model and questionnaire survey instrument to assess the success of organizational EHR in routine use from the viewpoint of nursing staff in residential aged care homes. The proposed research model incorporates six variables in the reformulated DeLone and McLean information systems success model: system quality, information quality, service quality, use, user satisfaction and net benefits. Two variables training and self-efficacy were also incorporated into the model. A questionnaire survey instrument was designed to measure the eight variables in the model. After a pilot test, the measurement scale was used to collect data from 243 nursing staff members in 10 residential aged care homes belonging to three management groups in Australia. Partial least squares path modeling was conducted to validate the model. The validated EHR systems success model predicts the impact of the four antecedent variables-training, self-efficacy, system quality and information quality-on the net benefits, the indicator of EHR systems success, through the intermittent variables use and user satisfaction. A 24-item measurement scale was developed to quantitatively evaluate the performance of an EHR system. The parsimonious EHR systems success model and the measurement scale can be used to benchmark EHR systems success across organizations and units and over time.

Low power data acquisition unit for autonomous geophysical instrumentation

Science.gov (United States)

Prystai, Andrii

2017-04-01

The development of an autonomous instrumentation for field research is always a challenge which needs knowledge and application of recent advances in technology and components production. Using this information a super-low power, low-cost, stand-alone GPS time synchronized data acquisition unit was created. It comprises an extended utilization of the microcontroller modules and peripherals and special firmware with flexible PLL parameters. The present report is devoted to a discussion of synchronization mode of data sampling in autonomous field instruments with possibility of GPS random breaks. In the result the achieved sampling timing accuracy is better than ± 60 ns without phase jumps and distortion plus fixed shift depending on the sample rate. The main application of the system is for simultaneous measurement of several channels from magnetic and electric sensors in field conditions for magneto-telluric instruments. First utilization of this system was in the new developed versions of LEMI-026 magnetometer and LEMI-423 field station, where it was applied for digitizing of up to 6 analogue channels with 32-bit resolution in the range ± 2.5V, digital filtration (LPF) and maximum sample rate 4kS/s. It is ready for record in 5 minutes after being turned on. Recently, this system was successfully utilized with the drone-portable magnetometers destined for the search of metallic objects, like UXO, in rural areas, research of engineering underground structure and for mapping ore bodies. The successful tests of drone-portable system were made and tests results are also discussed.

Cost-Utility Analysis of Pedicle Screw Removal After Successful Posterior Instrumented Fusion in Thoracolumbar Burst Fractures.

Science.gov (United States)

Lee, Han-Dong; Jeon, Chang-Hoon; Chung, Nam-Su; Seo, Young-Wook

2017-08-01

A cost-utility analysis (CUA). The aim of this study was to determine the cost-effectiveness of pedicle screw removal after posterior fusion in thoracolumbar burst fractures. Pedicle screw instrumentation is a standard fixation method for unstable thoracolumbar burst fracture. However, removal of the pedicle screw after successful fusion remains controversial because the clinical benefits remain unclear. CUA can help clinicians make appropriate decisions about optimal health care for pedicle screw removal after successful fusion in thoracolumbar burst fractures. We conducted a single-center, retrospective, longitudinal matched-cohort study of prospectively collected outcomes. In total, 88 consecutive patients who had undergone pedicle screw instrumentation for thoracolumbar burst fracture with successful fusion confirmed by computed tomography (CT) were used in this study. In total, 45 patients wanted to undergo implant removal surgery (R group), and 43 decided not to remove the implant (NR group). A CUA was conducted from the health care perspective. The direct costs of health care were obtained from the medical bill of each patient. Changes in health-related quality of life (HRQoL) scores, validated by Short Form 6D, were used to calculate quality-adjusted life-years (QALYs). Total costs and gained QALY were calculated at 1 year (1 year) and 2 years (2 years) compared with baseline. Results are expressed as an incremental cost-effectiveness ratio (ICER). Different discount rates (0%, 3%, and 5%) were applied to both cost and QALY for sensitivity analysis. Baseline patient variables were similar between the two groups (all P > 0.05). The additional benefits of implant removal (0.201 QALY at 2 years) were achieved with additional costs ($2541 at 2 years), equating to an ICER of $12,641/QALY. On the basis of the different discount rates, the robustness of our study's results was also determined. Implant removal after successful fusion in a thoracolumbar burst

Estimation of Sensitive Proportion by Randomized Response Data in Successive Sampling

Directory of Open Access Journals (Sweden)

Bo Yu

2015-01-01

Full Text Available This paper considers the problem of estimation for binomial proportions of sensitive or stigmatizing attributes in the population of interest. Randomized response techniques are suggested for protecting the privacy of respondents and reducing the response bias while eliciting information on sensitive attributes. In many sensitive question surveys, the same population is often sampled repeatedly on each occasion. In this paper, we apply successive sampling scheme to improve the estimation of the sensitive proportion on current occasion.

The development of an automatic sample-changer and control instrumentation for isotope-source neutron-activation analysis

International Nuclear Information System (INIS)

Andeweg, A.H.; Watterson, J.I.W.

1983-01-01

An automatic sample-changer was developed at the Council for Mineral Technology for use in isotope-source neutron-activation analysis. Tests show that the sample-changer can transfer a sample of up to 3 kg in mass over a distance of 3 m within 5 s. In addition, instrumentation in the form of a three-stage sequential timer was developed to control the sequence of irradiation transfer and analysis

Instrument and method for X-ray diffraction, fluorescence, and crystal texture analysis without sample preparation

Science.gov (United States)

Gendreau, Keith (Inventor); Martins, Jose Vanderlei (Inventor); Arzoumanian, Zaven (Inventor)

2010-01-01

An X-ray diffraction and X-ray fluorescence instrument for analyzing samples having no sample preparation includes a X-ray source configured to output a collimated X-ray beam comprising a continuum spectrum of X-rays to a predetermined coordinate and a photon-counting X-ray imaging spectrometer disposed to receive X-rays output from an unprepared sample disposed at the predetermined coordinate upon exposure of the unprepared sample to the collimated X-ray beam. The X-ray source and the photon-counting X-ray imaging spectrometer are arranged in a reflection geometry relative to the predetermined coordinate.

Sampling and instrumentation requirements for long-range D and D activities at INEL

International Nuclear Information System (INIS)

Ahlquist, A.J.

1985-01-01

Assistance was requested to help determine sampling and instrumentation requirements for the long-range decontamination and decommissioning activities at the Idaho National Engineering Laboratory. Through a combination of literature review, visits to other DOE contractors, and a determination of the needs for the INEL program, a draft report has been prepared that is now under review. The final report should be completed in FY 84

Determination of gold and silver in geological standard samples MGI by instrument neutron activation analysis

International Nuclear Information System (INIS)

Lu Huijiuan; Zhou; Yunlu

1987-01-01

Gold and silver in geological standard samples MGI were determined by instrument neutron activation analysis. The various interferences of nuclides were considered. Corrected factors of the geometry in different positions have been determined. Using the geological standard sample MGM and radiochemical separation neutron activation method as reference, the reliability of this method is proved. Gold content in samples is 0.4-0.009 g/t, silver content is 9-0.3 g/t. Standard deviation is less than 3.5%, the precision of the measurement is 4.8-11.6%

Determination of phosphorus in wheat grass samples by instrumental neutron activation analysis

International Nuclear Information System (INIS)

Kulkarni, S.D.; Rajurkar, N.S.; Acharya, R.; Nair, A.G.C.; Reddy, A.V.R.

2005-01-01

An instrumental neutron activation analysis (INAA) method using β-counting was used to determine phosphorus in wheat grass; grown in three different conditions. The phosphorus concentration was found to be in the range of 950-23000 mg/g in the samples grown in different conditions. The accuracy of the method was evaluated by determining phosphorus in three reference materials and the % deviations were within 10%. Reliability of the method was checked by following the half-life of the 32 P. (author)

Analysis of medicinal plants and soil sample from Haridwar region by instrumental neutron activation analysis

International Nuclear Information System (INIS)

Maharia, R.S.; Dutta, R.K.; Acharya, R.; Reddy, A.V.R.

2009-01-01

Samples of leaves and stems of four medicinal plants namely Kalmegh, Amaltas, Moalshri, and Arusa were analysed by Instrumental Neutron Activation Analysis. Soil from same location was analyzed. Though concentrations of many elements were determined in the plant samples, results of selected elements namely Na, K, Mn, Fe, Co, Cr, Zn and As are discussed in this paper. The results show that all medicinal plants analyzed have lower elemental contents except Zn compared to the soil. (author)

Wide-range bipolar pulse conductance instrument employing current and voltage modes with sampled or integrated signal acquisition

Energy Technology Data Exchange (ETDEWEB)

Calhoun, R K; Holler, F J [Kentucky Univ., Lexington, KY (United States). Dept. of Chemistry; Geiger, jr, R F; Nieman, T A [Illinois Univ., Urbana, IL (United States). Dept. of Chemistry; Caserta, K J [Procter and Gamble Co., Cincinnati, OH (United States)

1991-11-05

An instrument for measuring solution conductance using the bipolar pulse technique is described. The instrument is capable of measuring conductances in the range of 5x10{sup -9}-10{Omega}{sup -1} with 1% accuracy or better in as little as 32 {mu}s. Accuracy of 0.001-0.01% is achievable over the range 1x10{sup -6}-1{Omega}{sup -1}. Circuitry and software are described that allow the instrument to adjust automatically the pulse height, pulse duration, excitation mode (current or voltage pulse) and data acquisition mode (sampled or integrated) to acquire data of optimum accuracy and precision. The urease-catalyzed decomposition of urea is used to illustrate the versality of the instrument, and other applications are cited. (author). 60 refs.; 7 figs.; 2 tabs.

Evaluation applications of instrument calibration research findings in psychology for very small samples

Science.gov (United States)

Fisher, W. P., Jr.; Petry, P.

2016-11-01

Many published research studies document item calibration invariance across samples using Rasch's probabilistic models for measurement. A new approach to outcomes evaluation for very small samples was employed for two workshop series focused on stress reduction and joyful living conducted for health system employees and caregivers since 2012. Rasch-calibrated self-report instruments measuring depression, anxiety and stress, and the joyful living effects of mindfulness behaviors were identified in peer-reviewed journal articles. Items from one instrument were modified for use with a US population, other items were simplified, and some new items were written. Participants provided ratings of their depression, anxiety and stress, and the effects of their mindfulness behaviors before and after each workshop series. The numbers of participants providing both pre- and post-workshop data were low (16 and 14). Analysis of these small data sets produce results showing that, with some exceptions, the item hierarchies defining the constructs retained the same invariant profiles they had exhibited in the published research (correlations (not disattenuated) range from 0.85 to 0.96). In addition, comparisons of the pre- and post-workshop measures for the three constructs showed substantively and statistically significant changes. Implications for program evaluation comparisons, quality improvement efforts, and the organization of communications concerning outcomes in clinical fields are explored.

Microwave-Assisted Sample Treatment in a Fully Automated Flow-Based Instrument: Oxidation of Reduced Technetium Species in the Analysis of Total Technetium-99 in Caustic Aged Nuclear Waste Samples

International Nuclear Information System (INIS)

Egorov, Oleg B.; O'Hara, Matthew J.; Grate, Jay W.

2004-01-01

An automated flow-based instrument for microwave-assisted treatment of liquid samples has been developed and characterized. The instrument utilizes a flow-through reaction vessel design that facilitates the addition of multiple reagents during sample treatment, removal of the gaseous reaction products, and enables quantitative removal of liquids from the reaction vessel for carryover-free operations. Matrix modification and speciation control chemistries that are required for the radiochemical determination of total 99Tc in caustic aged nuclear waste samples have been investigated. A rapid and quantitative oxidation procedure using peroxydisulfate in acidic solution was developed to convert reduced technetium species to pertechnetate in samples with high content of reducing organics. The effectiveness of the automated sample treatment procedures has been validated in the radiochemical analysis of total 99Tc in caustic aged nuclear waste matrixes from the Hanford site

Instrumental analysis of low level of Cs-137 in marine samples by gamma spectrometry; Analise instrumental de baixos niveis de Cs-137 em amostras marinhas por espectrometria gama

Energy Technology Data Exchange (ETDEWEB)

Figueira, Rubens C.L.; Silva, Luiz R.N.; Figueiredo, Ana M.G.; Cunha, Ieda I.L. [Instituto de Pesquisas Energeticas e Nucleares (IPEN), Sao Paulo, SP (Brazil). Supervisao de Radioquimica

1997-12-31

An instrumental method for low level Cs-137 analysis in marine samples is presented. The method consists in the detector calibration, as well as, determination of detector counting efficiency, accumulative counting of both background and sample and smoothing of 661.6 keV photopeak. The methodology was applied in reference samples and in sediments samples of south Brazilian coast 11 refs., 6 figs., 4 tabs.; e-mail: figueira at net.ipen.br

Digibaro pressure instrument onboard the Phoenix Lander

Science.gov (United States)

Harri, A.-M.; Polkko, J.; Kahanpää, H. H.; Schmidt, W.; Genzer, M. M.; Haukka, H.; Savijarv1, H.; Kauhanen, J.

2009-04-01

The Phoenix Lander landed successfully on the Martian northern polar region. The mission is part of the National Aeronautics and Space Administration's (NASA's) Scout program. Pressure observations onboard the Phoenix lander were performed by an FMI (Finnish Meteorological Institute) instrument, based on a silicon diaphragm sensor head manufactured by Vaisala Inc., combined with MDA data processing electronics. The pressure instrument performed successfully throughout the Phoenix mission. The pressure instrument had 3 pressure sensor heads. One of these was the primary sensor head and the other two were used for monitoring the condition of the primary sensor head during the mission. During the mission the primary sensor was read with a sampling interval of 2 s and the other two were read less frequently as a check of instrument health. The pressure sensor system had a real-time data-processing and calibration algorithm that allowed the removal of temperature dependent calibration effects. In the same manner as the temperature sensor, a total of 256 data records (8.53 min) were buffered and they could either be stored at full resolution, or processed to provide mean, standard deviation, maximum and minimum values for storage on the Phoenix Lander's Meteorological (MET) unit.The time constant was approximately 3s due to locational constraints and dust filtering requirements. Using algorithms compensating for the time constant effect the temporal resolution was good enough to detect pressure drops associated with the passage of nearby dust devils.

Sample preparation in foodomic analyses.

Science.gov (United States)

Martinović, Tamara; Šrajer Gajdošik, Martina; Josić, Djuro

2018-04-16

Representative sampling and adequate sample preparation are key factors for successful performance of further steps in foodomic analyses, as well as for correct data interpretation. Incorrect sampling and improper sample preparation can be sources of severe bias in foodomic analyses. It is well known that both wrong sampling and sample treatment cannot be corrected anymore. These, in the past frequently neglected facts, are now taken into consideration, and the progress in sampling and sample preparation in foodomics is reviewed here. We report the use of highly sophisticated instruments for both high-performance and high-throughput analyses, as well as miniaturization and the use of laboratory robotics in metabolomics, proteomics, peptidomics and genomics. This article is protected by copyright. All rights reserved. This article is protected by copyright. All rights reserved.

Instrumental neutron activation analysis of rib bone samples and of bone reference materials

International Nuclear Information System (INIS)

Saiki, M.; Takata, M.K.; Kramarski, S.; Borelli, A.

2000-01-01

The instrumental neutron activation analysis method was used for the determination of trace elements in rib bone samples taken from autopsies of accident victims. The elements Br, Ca, Cl, Cr, Fe, Mg, Mn, Na, P, Sr, Rb and Zn were determined in cortical tissues by using short and long irradiations with thermal neutron flux of the IEA-R1m nuclear reactor. The reference materials NIST SRM 1400 Bone Ash and NIST SRM 1486 Bone Meal were also analyzed in order to evaluate the precision and the accuracy of the results. It was verified that lyophilization is the most convenient process for drying bone samples since it does not cause any element losses. Comparisons were made between the results obtained for rib samples and the literature values as well as between the results obtained for different ribs from a single individual and for bones from different individuals. (author)

Farewell to the Earth and the Moon -ESA's Mars Express successfully tests its instruments

Science.gov (United States)

2003-07-01

The routine check-outs of Mars Express's instruments and of the Beagle-2 lander, performed during the last weeks, have been very successful. "As in all space missions little problems have arisen, but they have been carefully evaluated and solved. Mars Express continues on its way to Mars performing beautifully", comments Chicarro. The views of the Earth/Moon system were taken on 3 July 2003 by Mars Express's High Resolution Stereo Camera (HRSC), when the spacecraft was 8 million kilometres from Earth. The image taken shows true colours; the Pacific Ocean appears in blue, and the clouds near the Equator and in mid to northern latitudes in white to light grey. The image was processed by the Instrument Team at the Institute of Planetary Research of DLR, Berlin (Germany). It was built by combining a super resolution black and white HRSC snap-shot image of the Earth and the Moon with colour information obtained by the blue, green, and red sensors of the instrument. “The pictures and the information provided by the data prove the camera is working very well. They provide a good indication of what to expect once the spacecraft is in its orbit around Mars, at altitudes of only 250-300 kilometres: very high resolution images with brilliant true colour and in 3D,” says the Principal Investigator of the HRSC, Gerhard Neukum, of the Freie Universität of Berlin (Germany). This camera will be able to distinguish details of up to 2 metres on the Martian surface. Another striking demonstration of Mars Express's instruments high performance are the data taken by the OMEGA spectrometer. Once at Mars, this instrument will provide the best map of the molecular and mineralogical composition of the whole planet, with 5% of the planetary surface in high resolution. Minerals and other compounds such as water will be charted as never before. As the Red Planet is still too far away, the OMEGA team devised an ingenious test for their instrument: to detect the Earth’s surface

Determination of sodium in biological samples by instrumental neutron activation analysis

International Nuclear Information System (INIS)

Parwate, D.V.; Garg, A.N.

1981-01-01

Sodium is one of the most essential elements needed for metabolic processes amongst human beings. It is consumed in the form of sodium chloride but it is also present in edible plant leaves. Sodium is mostly analyzed by flame photometric method, a destructive and time consuming technique. Sodium has been determined in some green leave vegetables samples-palak, radish, khatta palak (ambat chuka), chaulai leaves, chauli bean covers and its seeds by instrumental neutron activation analysis. The method involves irradiation of samples with thermal neutrons from 241 Am-Be source and counting 24 Na activity (half life 15 hr) from the reaction 23 Na(n,γ) 24 Na. Activity due to 1.37 MeV photopeak was counted with a NaI(Tl) crystal coupled to gamma ray spectrometer. Green leaves of the vegetables were thoroughly washed, dried at constant temperature and powdered. Bowen's Kale powder was used as standard for measuring sodium abundances. About 2g each of samples and the standard were packed in polythene vials. They were irradiated for 24 hrs, delayed by 1 hr and then counted for 20 mts. It is found that radish leaves are most enriched in sodium (14.0 +-0.45%) amongst four leave samples analyzed. For three different parts of chaulai leaves, bean covers and seeds, sodium contents are 1.38%, 1820 and 1010 ppm. Palak contains 2.84 +-0.29% while khatta palak contains only 4210 +- 830 ppm sodium. All values reported here are for dry weight samples and are means of three replicate measurements with standard deviation. (author)

A comparative study of sample dissolution techniques and plasma-based instruments for the precise and accurate quantification of REEs in mineral matrices

International Nuclear Information System (INIS)

Whitty-Léveillé, Laurence; Turgeon, Keven; Bazin, Claude; Larivière, Dominic

2017-01-01

The recent commercialisation of inductively coupled plasma tandem mass spectrometric (ICP-MS/MS) instruments has provided analytical chemists with a new tool to properly quantify atomic composition in a variety of matrices with minimal sample preparation. In this article, we report on our assessment of the compatibility of 3 sample preparation techniques (open-vessel acid digestion, microwave digestion and alkaline fusion) for the quantification of rare earth elements (REEs) in mineral matrices. The combination of the high digestion temperatures (1050 °C) and using LiBO_2 as a flux was the most effective strategy for the digestion of all rare earth elements in mineral matrices and was compatible with ICP-MS/MS measurements. We also assessed the analytical performances of ICP-MS/MS against other plasma-based instrumentation (microwave induced plasma and inductively coupled plasma atomic emission spectroscopy (MIP-AES and ICP-AES, respectively) and single quadrupole inductively coupled plasma mass spectrometry (ICP-MS). The comparative study showed that the concentrations obtained by ICP-MS/MS are in excellent agreement with the certified reference material values, and much more suited than the other analytical techniques tested for the quantification of REEs, which exhibited low detectability and/or spectral interferences for some elements/isotopes. Finally, the ruggedness of the analytical protocol proposed which combines a rapid sample dissolution step performed by an automated fusion unit and an ICP-MS/MS as a detector was established using various certified mineral matrices containing variable levels of REEs. - Highlights: • Three types of digestion methods were tested. • Four types of analytical techniques were compared. • Elimination of the spectral interferences encountered in ICP-MS was achieved by the use of Tandem ICP-MS. • Robustness of the analytical procedure was successfully evaluate on four types of certified reference material.

A comparative study of sample dissolution techniques and plasma-based instruments for the precise and accurate quantification of REEs in mineral matrices

Energy Technology Data Exchange (ETDEWEB)

Whitty-Léveillé, Laurence; Turgeon, Keven [Département de génie des mines, de la métallurgie et des matériaux, Université Laval, Québec, QC (Canada); Département de chimie, Université Laval, Québec, QC (Canada); Bazin, Claude [Département de génie des mines, de la métallurgie et des matériaux, Université Laval, Québec, QC (Canada); Larivière, Dominic, E-mail: dominic.lariviere@chm.ulaval.ca [Département de chimie, Université Laval, Québec, QC (Canada)

2017-04-08

The recent commercialisation of inductively coupled plasma tandem mass spectrometric (ICP-MS/MS) instruments has provided analytical chemists with a new tool to properly quantify atomic composition in a variety of matrices with minimal sample preparation. In this article, we report on our assessment of the compatibility of 3 sample preparation techniques (open-vessel acid digestion, microwave digestion and alkaline fusion) for the quantification of rare earth elements (REEs) in mineral matrices. The combination of the high digestion temperatures (1050 °C) and using LiBO{sub 2} as a flux was the most effective strategy for the digestion of all rare earth elements in mineral matrices and was compatible with ICP-MS/MS measurements. We also assessed the analytical performances of ICP-MS/MS against other plasma-based instrumentation (microwave induced plasma and inductively coupled plasma atomic emission spectroscopy (MIP-AES and ICP-AES, respectively) and single quadrupole inductively coupled plasma mass spectrometry (ICP-MS). The comparative study showed that the concentrations obtained by ICP-MS/MS are in excellent agreement with the certified reference material values, and much more suited than the other analytical techniques tested for the quantification of REEs, which exhibited low detectability and/or spectral interferences for some elements/isotopes. Finally, the ruggedness of the analytical protocol proposed which combines a rapid sample dissolution step performed by an automated fusion unit and an ICP-MS/MS as a detector was established using various certified mineral matrices containing variable levels of REEs. - Highlights: • Three types of digestion methods were tested. • Four types of analytical techniques were compared. • Elimination of the spectral interferences encountered in ICP-MS was achieved by the use of Tandem ICP-MS. • Robustness of the analytical procedure was successfully evaluate on four types of certified reference material.

Accounting for the thermal neutron flux depression in voluminous samples for instrumental neutron activation analysis

International Nuclear Information System (INIS)

Overwater, R.M.W.; Hoogenboom, J.E.

1994-01-01

At the Delft University of Technology Interfaculty Reactor Institute, a facility has been installed to irradiate cylindrical samples with diameters up to 15 cm and weights up to 50 kg for instrumental neutron activation analysis (INAA) purposes. To be able to do quantitative INAA on voluminous samples, it is necessary to correct for gamma-ray absorption, gamma-ray scattering, neutron absorption, and neutron scattering in the sample. The neutron absorption and the neutron scattering are discussed. An analytical solution is obtained for the diffusion equation in the geometry of the irradiation facility. For samples with known composition, the neutron flux--as a function of position in the sample--can be calculated directly. Those of unknown composition require additional flux measurements on which least-squares fitting must be done to obtain both the thermal neutron diffusion coefficient D s and the diffusion length L s of the sample. Experiments are performed to test the theory

Fatty Acid Detection in Mars-Analogous Rock Samples with the TMAH Wet Chemistry Experiment on the Sample Analysis at Mars (SAM) Instrument

Science.gov (United States)

Williams, A. J.; Eigenbrode, J. L.; Wilhelm, M. B.; Johnson, S. S.; Craft, K.; O'Reilly, S.; Lewis, J. M. T.; Williams, R.; Summons, R. E.; Benison, K. C.; Mahaffy, P. R.

2017-12-01

The Curiosity rover is exploring sedimentary rock sequences in Gale Crater for evidence of habitability and searching for organic compounds using the Sample Analysis at Mars (SAM) instrument suite. SAM includes a gas chromatograph mass spectrometer (GC-MS) and pyrolysis ovens. SAM has the ability to perform wet chemistry experiments, one of which uses tetramethylammonium hydroxide (TMAH) thermochemolysis to liberate bound lipids, making them sufficiently volatile for detection by GC-MS. To determine the effectiveness of the SAM-like TMAH experiment on fatty acid methyl ester (FAME) biomarker identification, rock and sediment samples were collected from a variety of Mars analog environments including iron oxides from a modern mineral precipitate and older surface gossan at Iron Mountain, CA, as well as modern acid salt and neutral lake sediments with mixed iron oxides and clays from Western Australia; siliceous sinter from recently inactive and modern near-vent Icelandic hot springs deposits; modern carbonate ooids from The Bahamas, and organic-rich shale from Germany. Samples underwent pyrolysis with TMAH. Fatty acids were analyzed by pyro-GC-MS using a SAM-like heating ramp (35°C/min) as well as a 500°C flash on a Frontier pyrolyzer and Agilent GC-MS instrument. Results reveal that FAMEs were detectable with the TMAH experiment in nearly all samples. Low molecular weight (MW) C6:0-C10:0 FAMEs were present in all samples, medium MW C11:0-C18:2 FAMEs were present in select samples, and high MW (HMW) C20:0-C30:0 FAMEs were present in the shale sample. Many of these samples exhibited an even-over-odd carbon number preference, indicating biological production. These experiments demonstrate that TMAH thermochemolysis with SAM-like pyro-GC-MS is effective in fatty acid analysis from natural Mars-analog samples that vary in mineralogy, age, and microbial community input. HMW FAMEs are not detected in iron-dominated samples, and may not be detectable at low

Use of an Ultrasonic/Sonic Driller/Corer to Obtain Sample Powder for CHEMIN, a Combined XRD/XRF Instrument

Science.gov (United States)

Chipera, S. J.; Bish, D. L.; Vaniman, D. T.; Sherrit, S.; Bar-Cohen, Y.; Sarrazin, P.; Blake, D. F.

2003-01-01

A miniature CHEMIN XRD/XRF (X-Ray Diffraction/X-Ray Fluourescence) instrument is currently being developed for definitive mineralogic analysis of soils and rocks on Mars. One of the technical issues that must be addressed in order to enable XRD analysis on an extraterrestrial body is how best to obtain a representative sample powder for analysis. For XRD powder diffraction analyses, it is beneficial to have a fine-grained sample to reduce preferred orientation effects and to provide a statistically significant number of crystallites to the X-ray beam. Although a 2-dimensional detector as used in the CHEMIN instrument will produce good results with poorly prepared powders, the quality of the data will improve if the sample is fine-grained and randomly oriented. An Ultrasonic/Sonic Driller/Corer (USDC) currently being developed at JPL is an effective mechanism of sampling rock to produce cores and powdered cuttings. It requires low axial load (XRD/XRF spectrometer such as CHEMIN, powders obtained from the JPL ultrasonic drill were analyzed and the results were compared to carefully prepared powders obtained using a laboratory bench scale Retsch mill.

Improved technical success and radiation safety of adrenal vein sampling using rapid, semi-quantitative point-of-care cortisol measurement.

Science.gov (United States)

Page, Michael M; Taranto, Mario; Ramsay, Duncan; van Schie, Greg; Glendenning, Paul; Gillett, Melissa J; Vasikaran, Samuel D

2018-01-01

Objective Primary aldosteronism is a curable cause of hypertension which can be treated surgically or medically depending on the findings of adrenal vein sampling studies. Adrenal vein sampling studies are technically demanding with a high failure rate in many centres. The use of intraprocedural cortisol measurement could improve the success rates of adrenal vein sampling but may be impracticable due to cost and effects on procedural duration. Design Retrospective review of the results of adrenal vein sampling procedures since commencement of point-of-care cortisol measurement using a novel single-use semi-quantitative measuring device for cortisol, the adrenal vein sampling Accuracy Kit. Success rate and complications of adrenal vein sampling procedures before and after use of the adrenal vein sampling Accuracy Kit. Routine use of the adrenal vein sampling Accuracy Kit device for intraprocedural measurement of cortisol commenced in 2016. Results Technical success rate of adrenal vein sampling increased from 63% of 99 procedures to 90% of 48 procedures ( P = 0.0007) after implementation of the adrenal vein sampling Accuracy Kit. Failure of right adrenal vein cannulation was the main reason for an unsuccessful study. Radiation dose decreased from 34.2 Gy.cm 2 (interquartile range, 15.8-85.9) to 15.7 Gy.cm 2 (6.9-47.3) ( P = 0.009). No complications were noted, and implementation costs were minimal. Conclusions Point-of-care cortisol measurement during adrenal vein sampling improved cannulation success rates and reduced radiation exposure. The use of the adrenal vein sampling Accuracy Kit is now standard practice at our centre.

Measuring Sulfur Isotope Ratios from Solid Samples with the Sample Analysis at Mars Instrument and the Effects of Dead Time Corrections

Science.gov (United States)

Franz, H. B.; Mahaffy, P. R.; Kasprzak, W.; Lyness, E.; Raaen, E.

2011-01-01

The Sample Analysis at Mars (SAM) instrument suite comprises the largest science payload on the Mars Science Laboratory (MSL) "Curiosity" rover. SAM will perform chemical and isotopic analysis of volatile compounds from atmospheric and solid samples to address questions pertaining to habitability and geochemical processes on Mars. Sulfur is a key element of interest in this regard, as sulfur compounds have been detected on the Martian surface by both in situ and remote sensing techniques. Their chemical and isotopic composition can belp constrain environmental conditions and mechanisms at the time of formation. A previous study examined the capability of the SAM quadrupole mass spectrometer (QMS) to determine sulfur isotope ratios of SO2 gas from a statistical perspective. Here we discuss the development of a method for determining sulfur isotope ratios with the QMS by sampling SO2 generated from heating of solid sulfate samples in SAM's pyrolysis oven. This analysis, which was performed with the SAM breadboard system, also required development of a novel treatment of the QMS dead time to accommodate the characteristics of an aging detector.

The Contribution of Counseling Providers to the Success or Failure of Marriages

Science.gov (United States)

Ansah-Hughes, Winifred

2015-01-01

This study is an investigation into the contribution of counseling providers to the success or failure of marriages. The purposive and the simple random sampling methods were used to select eight churches and 259 respondents (married people) in the Techiman Municipality. The instrument used to collect data was a 26-item questionnaire including a…

What are the keys to successful adrenal venous sampling (AVS) in patients with primary aldosteronism?

Science.gov (United States)

Young, William F; Stanson, Anthony W

2009-01-01

Adrenal venous sampling (AVS) is the criterion standard to distinguish between unilateral and bilateral adrenal disease in patients with primary aldosteronism. The keys to successful AVS include appropriate patient selection, careful patient preparation, focused technical expertise, defined protocol, and accurate data interpretation. The use of AVS should be based on patient preferences, patient age, clinical comorbidities, and the clinical probability of finding an aldosterone-producing adenoma. AVS is optimally performed in the fasting state in the morning. AVS is an intricate procedure because the right adrenal vein is small and may be difficult to locate - the success rate depends on the proficiency of the angiographer. The key factors that determine the successful catheterization of both adrenal veins are experience, dedication and repetition. With experience, and focusing the expertise to 1 or 2 radiologists at a referral centre, the AVS success rate can be as high as 96%. A centre-specific, written protocol is mandatory. The protocol should be developed by an interested group of endocrinologists, radiologists and laboratory personnel. Safeguards should be in place to prevent mislabelling of the blood tubes in the radiology suite and to prevent sample mix-up in the laboratory.

Determination of uranium and thorium in rock samples from Harargaj Anticline by instrumental neutron activation analysis

International Nuclear Information System (INIS)

Rahman, M.; Molla, N.I.; Sharif, A.K.M.; Basunia, S.; Islam, S.; Miah, R.U.; Hossain, S.M.; Chowdhury, M.I.; Bhuiyan, A.D.; Stegnar, P.

1993-01-01

Uranium and thorium were determined in geological materials such as radioactive rock samples collected from the Harargaj Anticline in Moulavi Bazar. The pure instrumental neutron activation analysis (INAA) technique was used in qualitative and quantitative analysis of the rock samples for U and Th. The samples were properly prepared together with their standards and simultaneously irradiated in a neutron flux of the order of 10 12 n*cm -2 *s -1 using the TRIGA MARK II research reactor facility at the AERE, Savar, Dhaka. After activation the samples were subjected to γ-ray spectrometry using a high purity germanium detection system. As a result of the analysis, U and Th could be determined. The data are consistent with the values reported by the ground radiometric survey group for some of the samples. (author) 7 refs.; 1 fig.; 2 tabs

Instrumentation

International Nuclear Information System (INIS)

Muehllehner, G.; Colsher, J.G.

1982-01-01

This chapter reviews the parameters which are important to positron-imaging instruments. It summarizes the options which various groups have explored in designing tomographs and the methods which have been developed to overcome some of the limitations inherent in the technique as well as in present instruments. The chapter is not presented as a defense of positron imaging versus single-photon or other imaging modality, neither does it contain a description of various existing instruments, but rather stresses their common properties and problems. Design parameters which are considered are resolution, sampling requirements, sensitivity, methods of eliminating scattered radiation, random coincidences and attenuation. The implementation of these parameters is considered, with special reference to sampling, choice of detector material, detector ring diameter and shielding and variations in point spread function. Quantitation problems discussed are normalization, and attenuation and random corrections. Present developments mentioned are noise reduction through time-of-flight-assisted tomography and signal to noise improvements through high intrinsic resolution. Extensive bibliography. (U.K.)

Apical instrumentation in endodontic therapy

Directory of Open Access Journals (Sweden)

Kurniasri Darliana

2007-07-01

Full Text Available Cleaning and shaping of the root canal as the foundation for successful endodontic therapy. Cleaning of the root canal as the removal of all the contents of the root canal systems before and during shaping. Mechanical cleaning as the most important part of the root canal therapy. Instrumentation of the apical region has long been considered to be an essential component in the cleaning and shaping process. The apical area as the critical zone for instrumentation. The apical portion of the root canal system can retain microorganisms that could potentially cause periradicular inflammation. The nickel-titanium rotary instrumentation system to facilitate the cleaning and shaping process. Larger instrumentation sizes not only allow proper irrigation but also significantly decrease remaining bacteria in the canal system. How the larger apical sizes preparation must be achieved to clinical success. This paper will describe the major factors impacting the selection of final apical size, the factors are the anatomy of the apical constriction, root canal diameter, apical instrumentation, and bacteria in dentin tubuli.

Designing Successful Next-Generation Instruments to Detect the Epoch of Reionization

Science.gov (United States)

Thyagarajan, Nithyanandan; Hydrogen Epoch of Reionization Array (HERA) team, Murchison Widefield Array (MWA) team

2018-01-01

The Epoch of Reionization (EoR) signifies a period of intense evolution of the Inter-Galactic Medium (IGM) in the early Universe caused by the first generations of stars and galaxies, wherein they turned the neutral IGM to be completely ionized by redshift ≥ 6. This important epoch is poorly explored to date. Measurement of redshifted 21 cm line from neutral Hydrogen during the EoR is promising to provide the most direct constraints of this epoch. Ongoing experiments to detect redshifted 21 cm power spectrum during reionization, including the Murchison Widefield Array (MWA), Precision Array for Probing the Epoch of Reionization (PAPER), and the Low Frequency Array (LOFAR), appear to be severely affected by bright foregrounds and unaccounted instrumental systematics. For example, the spectral structure introduced by wide-field effects, aperture shapes and angular power patterns of the antennas, electrical and geometrical reflections in the antennas and electrical paths, and antenna position errors can be major limiting factors. These mimic the 21 cm signal and severely degrade the instrument performance. It is imperative for the next-generation of experiments to eliminate these systematics at their source via robust instrument design. I will discuss a generic framework to set cosmologically motivated antenna performance specifications and design strategies using the Precision Radio Interferometry Simulator (PRISim) -- a high-precision tool that I have developed for simulations of foregrounds and the instrument transfer function intended primarily for 21 cm EoR studies, but also broadly applicable to interferometer-based intensity mapping experiments. The Hydrogen Epoch of Reionization Array (HERA), designed in-part based on this framework, is expected to detect the 21 cm signal with high significance. I will present this framework and the simulations, and their potential for designing upcoming radio instruments such as HERA and the Square Kilometre Array (SKA).

The use of the hybrid K-edge densitometer for routine analysis of safeguards verification samples of reprocessing input liquor

International Nuclear Information System (INIS)

Ottmar, H.; Eberle, H.

1991-01-01

Following successful tests of a hybrid K-edge instrument at TUI Karlsruhe and the routine use of a K-edge densitometer for safeguards verification at the same laboratory, the Euratom Safeguards Directorate of the Commission of the European Communities decided to install the first such instrument into a large industrial reprocessing plant for the routine verification of samples taken from the input accountancy tanks. This paper reports on the installation, calibration, sample handling procedure and the performance of this instrument after one year of routine operation

Strategies for Successfully Teaching Students with ADD or ADHD in Instrumental Lessons

Science.gov (United States)

Melago, Kathleen A.

2014-01-01

Teachers can easily encounter students with Attention Deficit Disorder (ADD) or Attention Deficit Hyperactivity Disorder (ADHD) in the instrumental lesson setting. Applicable to instrumental lesson settings in the public or private schools, private studios, or college studios, this article focuses on specific strategies ranging from the…

Predicting Academic Success and Psychological Wellness in a Sample of Canadian Undergraduate Students

Science.gov (United States)

Chow, Henry P. H.

2010-01-01

Introduction: University students need to cope with a complex new life role and to achieve academic success. This article explores the academic performance and psychological well-being among university students in a western Canadian city. Method: Using a convenience sample, a total of 501 undergraduate students in Regina, Saskatchewan took part in…

Rare earths analysis of rock samples by instrumental neutron activation analysis, internal standard method

International Nuclear Information System (INIS)

Silachyov, I.

2016-01-01

The application of instrumental neutron activation analysis for the determination of long-lived rare earth elements (REE) in rock samples is considered in this work. Two different methods are statistically compared: the well established external standard method carried out using standard reference materials, and the internal standard method (ISM), using Fe, determined through X-ray fluorescence analysis, as an element-comparator. The ISM proved to be the more precise method for a wide range of REE contents and can be recommended for routine practice. (author)

Design and development of a highly sensitive, field portable plasma source instrument for on-line liquid stream monitoring and real-time sample analysis

International Nuclear Information System (INIS)

Duan, Yixiang; Su, Yongxuan; Jin, Zhe; Abeln, Stephen P.

2000-01-01

The development of a highly sensitive, field portable, low-powered instrument for on-site, real-time liquid waste stream monitoring is described in this article. A series of factors such as system sensitivity and portability, plasma source, sample introduction, desolvation system, power supply, and the instrument configuration, were carefully considered in the design of the portable instrument. A newly designed, miniature, modified microwave plasma source was selected as the emission source for spectroscopy measurement, and an integrated small spectrometer with a charge-coupled device detector was installed for signal processing and detection. An innovative beam collection system with optical fibers was designed and used for emission signal collection. Microwave plasma can be sustained with various gases at relatively low power, and it possesses high detection capabilities for both metal and nonmetal pollutants, making it desirable to use for on-site, real-time, liquid waste stream monitoring. An effective in situ sampling system was coupled with a high efficiency desolvation device for direct-sampling liquid samples into the plasma. A portable computer control system is used for data processing. The new, integrated instrument can be easily used for on-site, real-time monitoring in the field. The system possesses a series of advantages, including high sensitivity for metal and nonmetal elements; in situ sampling; compact structure; low cost; and ease of operation and handling. These advantages will significantly overcome the limitations of previous monitoring techniques and make great contributions to environmental restoration and monitoring. (c)

Instrumentation

International Nuclear Information System (INIS)

Umminger, K.

2008-01-01

A proper measurement of the relevant single and two-phase flow parameters is the basis for the understanding of many complex thermal-hydraulic processes. Reliable instrumentation is therefore necessary for the interaction between analysis and experiment especially in the field of nuclear safety research where postulated accident scenarios have to be simulated in experimental facilities and predicted by complex computer code systems. The so-called conventional instrumentation for the measurement of e. g. pressures, temperatures, pressure differences and single phase flow velocities is still a solid basis for the investigation and interpretation of many phenomena and especially for the understanding of the overall system behavior. Measurement data from such instrumentation still serves in many cases as a database for thermal-hydraulic system codes. However some special instrumentation such as online concentration measurement for boric acid in the water phase or for non-condensibles in steam atmosphere as well as flow visualization techniques were further developed and successfully applied during the recent years. Concerning the modeling needs for advanced thermal-hydraulic codes, significant advances have been accomplished in the last few years in the local instrumentation technology for two-phase flow by the application of new sensor techniques, optical or beam methods and electronic technology. This paper will give insight into the current state of instrumentation technology for safety-related thermohydraulic experiments. Advantages and limitations of some measurement processes and systems will be indicated as well as trends and possibilities for further development. Aspects of instrumentation in operating reactors will also be mentioned.

Cross-cultural feigning assessment: A systematic review of feigning instruments used with linguistically, ethnically, and culturally diverse samples.

Science.gov (United States)

Nijdam-Jones, Alicia; Rosenfeld, Barry

2017-11-01

The cross-cultural validity of feigning instruments and cut-scores is a critical concern for forensic mental health clinicians. This systematic review evaluated feigning classification accuracy and effect sizes across instruments and languages by summarizing 45 published peer-reviewed articles and unpublished doctoral dissertations conducted in Europe, Asia, and North America using linguistically, ethnically, and culturally diverse samples. The most common psychiatric symptom measures used with linguistically, ethnically, and culturally diverse samples included the Structured Inventory of Malingered Symptomatology, the Miller Forensic Assessment of Symptoms Test, and the Minnesota Multiphasic Personality Inventory (MMPI). The most frequently studied cognitive effort measures included the Word Recognition Test, the Test of Memory Malingering, and the Rey 15-item Memory test. The classification accuracy of these measures is compared and the implications of this research literature are discussed. (PsycINFO Database Record (c) 2017 APA, all rights reserved).

PlanetVac: Sample Return with a Puff of Gas

Science.gov (United States)

Zacny, K.; Mueller, R.; Betts, B. H.

2014-12-01

PlanetVac is a regolith sample acquisition mission concept that uses compressed gas to blow material from the surface up a pneumatic tube and directly into a sample return container. The PlanetVac sampling device is built into the lander legs to eliminate cost and complexity associated with robotic arms and scoops. The pneumatic system can effectively capture fine and coarse regolith, including small pebbles. It is well suited for landed missions to Mars, asteroids, or the Moon. Because of the low pressures on all those bodies, the technique is extremely efficient. If losses are kept to minimum, 1 gram of compressed gas could efficiently lift 6000 grams of soil. To demonstrate this approach, the PlanetVac lander with four legs and two sampling tubes has been designed, integrated, and tested. Vacuum chamber testing was performed using two well-known planetary regolith simulants: Mars Mojave Simulant (MMS) and lunar regolith simulant JSC-1A. One of the two sampling systems was connected to a mockup of an earth return rocket while the second sampling system was connected to a lander deck mounted instrument (clear box for easy viewing). The tests included a drop from a height of approximately 50 cm onto the bed of regolith, deployment of sampling tubes into the regolith, pneumatic acquisition of sample into an instrument (sample container) and the rocket, and the launch of the rocket. The demonstration has been successful and can be viewed here: https://www.youtube.com/watch?v=DjJXvtQk6no. In most of the tests, 20 grams or more of sample was delivered to the 'instrument' and approximately 5 grams of regolith was delivered into a sampling chamber within the rocket. The gas lifting efficiency was calculated to be approximately 1000:1; that is 1 gram of gas lofted 1000 grams of regolith. Efficiencies in lower gravity environments are expected to be much higher. This successful, simple and lightweight sample capture demonstration paves the way to using such sampling system

Psychometric Evaluation of an Instrument for Measuring Organizational Climate for Quality: Evidence From a National Sample of Infection Preventionists.

Science.gov (United States)

Pogorzelska-Maziarz, Monika; Nembhard, Ingrid M; Schnall, Rebecca; Nelson, Shanelle; Stone, Patricia W

2016-09-01

In recent years, there has been increased interest in measuring the climate for infection prevention; however, reliable and valid instruments are lacking. This study tested the psychometric properties of the Leading a Culture of Quality for Infection Prevention (LCQ-IP) instrument measuring the infection prevention climate in a sample of 972 infection preventionists from acute care hospitals. An exploratory principal component analysis showed that the instrument had structural validity and captured 4 factors related to the climate for infection prevention: Psychological Safety, Prioritization of Quality, Supportive Work Environment, and Improvement Orientation. LCQ-IP exhibited excellent internal consistency, with a Cronbach α of .926. Criterion validity was supported with overall LCQ-IP scores, increasing with the number of evidence-based prevention policies in place (P = .047). This psychometrically sound instrument may be helpful to researchers and providers in assessing climate for quality related to infection prevention. © The Author(s) 2015.

The Comparative Study Of Saprophytic Fungi In Air Canal, Air, Hospital Instruments And Clinical Samples From Patients With Bone Marrow Transplantation

Directory of Open Access Journals (Sweden)

Hashemi S J

2004-08-01

Full Text Available Background: Bone Marrow Transplantation is one of the most important therapeutic methods in much malignant and nonmalignant disease. Patients with Bone Marrow Transplantation (BMT following radiotherapy and chemotherapy will suffer from immuno-suppression. Therefore they are susceptible to get saprophytic fungi infection that sometimes are killer. Materials and Methods: The purpose of this cross-sectional survey is isolation of saprophytic fungi from patients with BMT and wards space and instruments. Therefore sampling from ventilator system (HEPA filter and common filter, air canal, air, hospital instruments and clinical samples (nasal discharge, sputum, urine were done and cultured in sabouro dextrose agar with choloramphenicol (SC. In assessing total frequency from 4838 plates of wards space and instruments, 985 fungi colonies includes 21 genus were isolated. Results and Conclusion: Most fungi colonies present were Penicillium , Aspergillus and Cladosporium and low present were Trichoderma ,Stereptomyses, Chrysosporium, Rhizopus.

Plans for Selection and In-Situ Investigation of Return Samples by the Supercam Instrument Onboard the Mars 2020 Rover

Science.gov (United States)

Wiens, R. C.; Maurice, S.; Mangold, N.; Anderson, R.; Beyssac, O.; Bonal, L.; Clegg, S.; Cousin, A.; DeFlores, L.; Dromart, G.; Fisher, W.; Forni, O.; Fouchet, T.; Gasnault, O.; Grotzinger, J.; Johnson, J.; Martinez-Frias, J.; McLennan, S.; Meslin, P.-Y.; Montmessin, F.; Poulet, F.; Rull, F.; Sharma, S.

2018-04-01

The SuperCam instrument onboard Rover 2020 still provides a complementary set of analyses with IR reflectance and Raman spectroscopy for mineralogy, LIBS for chemistry, and a color imager in order to investigate in-situ samples to return.

Health physics instrument manual

International Nuclear Information System (INIS)

Gupton, E.D.

1978-08-01

The purpose of this manual is to provide apprentice health physics surveyors and other operating groups not directly concerned with radiation detection instruments a working knowledge of the radiation detection and measuring instruments in use at the Laboratory. The characteristics and applications of the instruments are given. Portable instruments, stationary instruments, personnel monitoring instruments, sample counters, and miscellaneous instruments are described. Also, information sheets on calibration sources, procedures, and devices are included. Gamma sources, beta sources, alpha sources, neutron sources, special sources, a gamma calibration device for badge dosimeters, and a calibration device for ionization chambers are described

Estimating Sampling Biases and Measurement Uncertainties of AIRS-AMSU-A Temperature and Water Vapor Observations Using MERRA Reanalysis

Science.gov (United States)

Hearty, Thomas J.; Savtchenko, Andrey K.; Tian, Baijun; Fetzer, Eric; Yung, Yuk L.; Theobald, Michael; Vollmer, Bruce; Fishbein, Evan; Won, Young-In

2014-01-01

We use MERRA (Modern Era Retrospective-Analysis for Research Applications) temperature and water vapor data to estimate the sampling biases of climatologies derived from the AIRS/AMSU-A (Atmospheric Infrared Sounder/Advanced Microwave Sounding Unit-A) suite of instruments. We separate the total sampling bias into temporal and instrumental components. The temporal component is caused by the AIRS/AMSU-A orbit and swath that are not able to sample all of time and space. The instrumental component is caused by scenes that prevent successful retrievals. The temporal sampling biases are generally smaller than the instrumental sampling biases except in regions with large diurnal variations, such as the boundary layer, where the temporal sampling biases of temperature can be +/- 2 K and water vapor can be 10% wet. The instrumental sampling biases are the main contributor to the total sampling biases and are mainly caused by clouds. They are up to 2 K cold and greater than 30% dry over mid-latitude storm tracks and tropical deep convective cloudy regions and up to 20% wet over stratus regions. However, other factors such as surface emissivity and temperature can also influence the instrumental sampling bias over deserts where the biases can be up to 1 K cold and 10% wet. Some instrumental sampling biases can vary seasonally and/or diurnally. We also estimate the combined measurement uncertainties of temperature and water vapor from AIRS/AMSU-A and MERRA by comparing similarly sampled climatologies from both data sets. The measurement differences are often larger than the sampling biases and have longitudinal variations.

Successful Adrenal Venous Sampling by Non-experts with Reference to CT Images

International Nuclear Information System (INIS)

Morita, Satoru; Yamazaki, Hiroshi; Sonoyama, Yasuyuki; Nishina, Yu; Ichihara, Atsuhiro; Sakai, Shuji

2016-01-01

PurposeTo establish technical success rates and safety of adrenal venous sampling (AVS) performed by non-experts with reference to CT images.Materials and Methods104 AVS procedures with adrenocorticotropic hormone stimulation were performed for patients with suspected primary aldosteronism. One of three radiology residents with 2nd, 5th, and 5th grade experience undertook the procedure under the guidance of an experienced, board-certified interventional radiologist with reference to contrast-enhanced CT images obtained in 102 cases. Successful catheterization of the adrenal veins was assessed using three criteria: an adrenal venous cortisol concentration of more than 200 μg/dL (criterion A); an adrenal vein/inferior vena cava cortisol ratio of more than 5:1 (criterion B); and an adrenal vein/inferior vena cava cortisol ratio of more than 10:1 (criterion C).ResultsThe operators were aware of the anatomy of the left adrenal veins in 102 cases (98 %) and of the right adrenal veins in 99 cases (95 %) prior to the procedure. CT identified the correct position of the right adrenal vein orifice in 82 of 99 cases (83 %). The overall technical success rates for AVS from the right adrenal vein according to criteria A, B, and C, were 96, 96, and 94 %, respectively. Those for the left adrenal vein were 97, 98, and 94 %, respectively. No significant differences in success rates were observed between the operators (p = 0.922–0.984). No major complications, including adrenal vein rupture, were observed.ConclusionsWhen CT images are used to guide AVS, the procedure can be performed successfully and safely even by non-experts.

Successful Adrenal Venous Sampling by Non-experts with Reference to CT Images

Energy Technology Data Exchange (ETDEWEB)

Morita, Satoru, E-mail: i@imodey.com; Yamazaki, Hiroshi; Sonoyama, Yasuyuki; Nishina, Yu [Tokyo Women’s Medical University Hospital, Department of Diagnostic Imaging and Nuclear Medicine (Japan); Ichihara, Atsuhiro [Tokyo Women’s Medical University Hospital, Department of Medicine II, Endocrinology and Hypertension (Japan); Sakai, Shuji [Tokyo Women’s Medical University Hospital, Department of Diagnostic Imaging and Nuclear Medicine (Japan)

2016-07-15

PurposeTo establish technical success rates and safety of adrenal venous sampling (AVS) performed by non-experts with reference to CT images.Materials and Methods104 AVS procedures with adrenocorticotropic hormone stimulation were performed for patients with suspected primary aldosteronism. One of three radiology residents with 2nd, 5th, and 5th grade experience undertook the procedure under the guidance of an experienced, board-certified interventional radiologist with reference to contrast-enhanced CT images obtained in 102 cases. Successful catheterization of the adrenal veins was assessed using three criteria: an adrenal venous cortisol concentration of more than 200 μg/dL (criterion A); an adrenal vein/inferior vena cava cortisol ratio of more than 5:1 (criterion B); and an adrenal vein/inferior vena cava cortisol ratio of more than 10:1 (criterion C).ResultsThe operators were aware of the anatomy of the left adrenal veins in 102 cases (98 %) and of the right adrenal veins in 99 cases (95 %) prior to the procedure. CT identified the correct position of the right adrenal vein orifice in 82 of 99 cases (83 %). The overall technical success rates for AVS from the right adrenal vein according to criteria A, B, and C, were 96, 96, and 94 %, respectively. Those for the left adrenal vein were 97, 98, and 94 %, respectively. No significant differences in success rates were observed between the operators (p = 0.922–0.984). No major complications, including adrenal vein rupture, were observed.ConclusionsWhen CT images are used to guide AVS, the procedure can be performed successfully and safely even by non-experts.

The Opera Instrument: An Advanced Curation Development for Mars Sample Return Organic Contamination Monitoring

Science.gov (United States)

Fries, M. D.; Fries, W. D.; McCubbin, F. M.; Zeigler, R. A.

2018-01-01

Mars Sample Return (MSR) requires strict organic contamination control (CC) and contamination knowledge (CK) as outlined by the Mars 2020 Organic Contamination Panel (OCP). This includes a need to monitor surficial organic contamination to a ng/sq. cm sensitivity level. Archiving and maintaining this degree of surface cleanliness may be difficult but has been achieved. MSR's CK effort will be very important because all returned samples will be studied thoroughly and in minute detail. Consequently, accurate CK must be collected and characterized to best interpret scientific results from the returned samples. The CK data are not only required to make accurate measurements and interpretations for carbon-depleted martian samples, but also to strengthen the validity of science investigations performed on the samples. The Opera instrument prototype is intended to fulfill a CC/CK role in the assembly, cleaning, and overall contamination history of hardware used in the MSR effort, from initial hardware assembly through post-flight sample curation. Opera is intended to monitor particulate and organic contamination using quartz crystal microbalances (QCMs), in a self-contained portable package that is cleanroom-compliant. The Opera prototype is in initial development capable of approximately 100 ng/sq. cm organic contamination sensitivity, with additional development planned to achieve 1 ng/sq. cm. The Opera prototype was funded by the 2017 NASA Johnson Space Center Innovation Charge Account (ICA), which provides funding for small, short-term projects.

Governance as an instrument of successful organizational integration.

Science.gov (United States)

Lozon, Jeffrey C; Vernon, Sarah E

2002-01-01

In July 1997 the Health Services Restructuring Commission (HSRC) issued a formal direction to the Wellesley Central Hospital to relinquish the operation and management of its programs and services to St. Michael's Hospital. This event propelled staff and volunteers into four years of unrelenting efforts to bring together the mission, vision, values, human resources, clinical programs and broad communities of these two very unique and long-standing organizations. Looking back, the result was arguably one of the most successful hospital mergers in the province at that time. A number of factors were responsible for this outcome. The tremendous value of a strong and integrated governance team clearly stands out as one of the most pivotal success factors. This article examines the principles and structures that guided the governance team and St. Michael's Hospital to a stronger and more vibrant future.

Development of the Potassium-Argon Laser Experiment (KArLE) Instrument for In Situ Geochronology

Science.gov (United States)

Cohen, Barbara A.; Li, Z.-H.; Miller, J. S.; Brinckerhoff, W. B.; Clegg, S. M.; Mahaffy, P. R.; Swindle, T. D.; Wiens, R. C.

2012-01-01

Absolute dating of planetary samples is an essential tool to establish the chronology of geological events, including crystallization history, magmatic evolution, and alteration. Traditionally, geochronology has only been accomplishable on samples from dedicated sample return missions or meteorites. The capability for in situ geochronology is highly desired, because it will allow one-way planetary missions to perform dating of large numbers of samples. The success of an in situ geochronology package will not only yield data on absolute ages, but can also complement sample return missions by identifying the most interesting rocks to cache and/or return to Earth. In situ dating instruments have been proposed, but none have yet reached TRL 6 because the required high-resolution isotopic measurements are very challenging. Our team is now addressing this challenge by developing the Potassium (K) - Argon Laser Experiment (KArLE) under the NASA Planetary Instrument Definition and Development Program (PIDDP), building on previous work to develop a K-Ar in situ instrument [1]. KArLE uses a combination of several flight-proven components that enable accurate K-Ar isochron dating of planetary rocks. KArLE will ablate a rock sample, determine the K in the plasma state using laser-induced breakdown spectroscopy (LIBS), measure the liberated Ar using quadrupole mass spectrometry (QMS), and relate the two by the volume of the ablated pit using an optical method such as a vertical scanning interferometer (VSI). Our preliminary work indicates that the KArLE instrument will be capable of determining the age of several kinds of planetary samples to +/-100 Myr, sufficient to address a wide range of geochronology problems in planetary science.

Innovative instrumentation

International Nuclear Information System (INIS)

Anon.

1983-01-01

At this year's particle physics conference at Brighton, a parallel session was given over to instrumentation and detector development. While this work is vital to the health of research and its continued progress, its share of prime international conference time is limited. Instrumentation can be innovative three times — first when a new idea is outlined, secondly when it is shown to be feasible, and finally when it becomes productive in a real experiment, amassing useful data rather than operational experience. Hyams' examples showed that it can take a long time for a new idea to filter through these successive stages, if it ever makes it at all

Innovative instrumentation

Energy Technology Data Exchange (ETDEWEB)

Anon.

1983-11-15

At this year's particle physics conference at Brighton, a parallel session was given over to instrumentation and detector development. While this work is vital to the health of research and its continued progress, its share of prime international conference time is limited. Instrumentation can be innovative three times — first when a new idea is outlined, secondly when it is shown to be feasible, and finally when it becomes productive in a real experiment, amassing useful data rather than operational experience. Hyams' examples showed that it can take a long time for a new idea to filter through these successive stages, if it ever makes it at all.

Instrumental aspects

Directory of Open Access Journals (Sweden)

Qureshi Navid

2017-01-01

Full Text Available Every neutron scattering experiment requires the choice of a suited neutron diffractometer (or spectrometer in the case of inelastic scattering with its optimal configuration in order to accomplish the experimental tasks in the most successful way. Most generally, the compromise between the incident neutron flux and the instrumental resolution has to be considered, which is depending on a number of optical devices which are positioned in the neutron beam path. In this chapter the basic instrumental principles of neutron diffraction will be explained. Examples of different types of experiments and their respective expectable results will be shown. Furthermore, the production and use of polarized neutrons will be stressed.

Coherent diffraction microscopy at SPring-8: instrumentation, data acquisition and data analysis

International Nuclear Information System (INIS)

Xu, Rui; Salha, Sara; Raines, Kevin S.; Jiang, Huaidong; Chen, Chien-Chun; Takahashi, Yukio; Kohmura, Yoshiki; Nishino, Yoshinori; Song, Changyong; Ishikawa, Tetsuya; Miao, Jianwei

2011-01-01

An instrumentation and data analysis review of coherent diffraction microscopy at SPring-8 is given. This work will be of interest to those who want to apply coherent diffraction imaging to studies of materials science and biological samples. Since the first demonstration of coherent diffraction microscopy in 1999, this lensless imaging technique has been experimentally refined by continued developments. Here, instrumentation and experimental procedures for measuring oversampled diffraction patterns from non-crystalline specimens using an undulator beamline (BL29XUL) at SPring-8 are presented. In addition, detailed post-experimental data analysis is provided that yields high-quality image reconstructions. As the acquisition of high-quality diffraction patterns is at least as important as the phase-retrieval procedure to guarantee successful image reconstructions, this work will be of interest for those who want to apply this imaging technique to materials science and biological samples

Instrument Modeling and Synthesis

Science.gov (United States)

Horner, Andrew B.; Beauchamp, James W.

During the 1970s and 1980s, before synthesizers based on direct sampling of musical sounds became popular, replicating musical instruments using frequency modulation (FM) or wavetable synthesis was one of the “holy grails” of music synthesis. Synthesizers such as the Yamaha DX7 allowed users great flexibility in mixing and matching sounds, but were notoriously difficult to coerce into producing sounds like those of a given instrument. Instrument design wizards practiced the mysteries of FM instrument design.

Development of an Electronic Portfolio System Success Model: An Information Systems Approach

Science.gov (United States)

Balaban, Igor; Mu, Enrique; Divjak, Blazenka

2013-01-01

This research has two main goals: to develop an instrument for assessing Electronic Portfolio (ePortfolio) success and to build a corresponding ePortfolio success model using DeLone and McLean's information systems success model as the theoretical framework. For this purpose, we developed an ePortfolio success measurement instrument and structural…

Instrumentation for in situ sampling and analysis of compounds of interest to Astrobiology in the lower atmosphere and surface of Titan

Science.gov (United States)

Holland, Paul M.; Kojiro, Daniel R.; Stimac, Robert; Kaye, William; Takeuchi, Nori

2006-01-01

Instrumentation for exploration of the solar system will require new enabling technology for in situ sample acquisition and analysis of pre-biotic chemistry in extreme planetary environments, such as that encountered at the surface of Titan. The potential use of balloon aero-rovers for Titan places special emphasis on the importance of miniaturization, low power and low usage of consumables. To help meet this need, we are developing a miniature gas chromatograph coupled with a new Mini-Cell ion mobility spectrometer (GC-IMS), and one of us (PMH) has begun development work on a miniaturized cryogenic inlet system with sampling probes for Titan. This instrumentation, and its approach for meeting measurement needs for the analysis of prebiotic chemistry on Titan, will be discussed.

Raman Life Detection Instrument Development for Icy Worlds

Science.gov (United States)

Thomson, Seamus; Allen, A'Lester; Gutierrez, Daniel; Quinn, Richard C.; Chen, Bin; Koehne, Jessica E.

2017-01-01

The objective of this project is to develop a compact, high sensitivity Raman sensor for detection of life signatures in a flow cell configuration to enable bio-exploration and life detection during future mission to our Solar Systems Icy Worlds. The specific project objectives are the following: 1) Develop a Raman spectroscopy liquid analysis sensor for biosignatures; 2) Demonstrate applicability towards a future Enceladus or other Icy Worlds missions; 3) Establish key parameters for integration with the ARC Sample Processor for Life on Icy Worlds (SPLIce); 4) Position ARC for a successful response to upcoming Enceladus or other Icy World mission instrument opportunities.

Validating an instrument for measuring brand equity of CSR driven organizations in Malaysia

Directory of Open Access Journals (Sweden)

Singh Dara Singh Karpal

2017-06-01

Full Text Available The objective of this study is to develop and propose a valid and reliable instrument to measure brand equity of CSR driven organizations in Malaysia. An instrument to measure brand equity was constructed with adaptations from two key sources, namely Yew Leh and Lee (2011 and Yoo and Donthu (2001. As such the study only focuses on the development and validation of an instrument to measure brand equity of CSR driven organizations. The usable sample population included 909 respondents from 12 states of West Malaysia which were selected using a quota sampling plan. Confirmatory factor analysis (CFA and reliability analysis were carried out to test and validate the proposed brand equity instrument containing four components (brand awareness, brand association, perceived quality and brand loyalty with a total of 13 items. Results from the CFA and reliability analysis indicated that all the items representing the four components were valid and can be used to measure the brand equity of organizations that are practicing CSR. The study tried to set an empirical basis for brand equity and CSR related research which could be used by future researchers in different industries and geographical locations. The study also implies the need for organizations to assess the success of their CSR efforts through the use of the proposed instrument in order to gauge whether all their CSR efforts translate to improved brand equity.

Final report, Ames Mobile Laboratory Project: The development and operation of instrumentation in a mobile laboratory for in situ, real-time screening and characterization of soils using the laser ablation sampling technique

International Nuclear Information System (INIS)

Anderson, M.S.; Braymen, S.D.

1995-01-01

The main focus of the Ames Laboratory's Technology Integration Program, TIP, from May 1991 through December 1994 was the development, fabrication, and demonstration of a mobile instrumentation laboratory incorporating rapid in situ sampling systems for safe, rapid, and cost effective soil screening/characterization. The Mobile Demonstration Laboratory for Environmental Screening Technologies, MDLEST, containing the analysis instrumentation, along with surface and subsurface sampling probe prototypes employing the laser ablation sampling technique were chosen to satisfy the particular surface and subsurface soil characterization needs of the various Department of Energy facilities for determining the extent of heavy metal and radionuclide contamination. The MDLEST, a 44 foot long 5th wheel trailer, is easily configured for the analysis instrumentation and sampling system required for the particular site work. This mobile laboratory contains all of the utilities needed to satisfy the operating requirements of the various instrumentation installed. These utilities include, an electric generator, a chilled water system, process gases, a heating/air conditioning system, and computer monitoring and automatic operating systems. Once the MDLEST arrives at the job site, the instrumentation is aligned and calibration is completed, sampling and analysis operations begin. The sample is acquired, analyzed and the results reported in as little as 10 minutes. The surface sampling probe is used in two modes to acquire samples for analysis. It is either set directly on the ground over the site to be sampled, in situ sampling, or in a special fixture used for calibrating the sampling analysis system with standard soil samples, having the samples brought to the MDLEST. The surface sampling probe was used to in situ sample a flat concrete surface (nondestructively) with the ablated sample being analyzed by the instrumentation in the MDLEST

Performance of BATAN-SANS instrument

Energy Technology Data Exchange (ETDEWEB)

Ikram, Abarrul; Insani, Andon [National Nuclear Energy Agency, P and D Centre for Materials Science and Technology, Serpong (Indonesia)

2003-03-01

SANS data from some standard samples have been obtained using BATAN-SANS instrument in Serpong. The experiments were performed for various experimental set-ups that involve different detector positions and collimator lengths. This paper describes the BATAN-SANS instrument briefly as well as the data taken from those experiments and followed with discussion of the results concerning the performance and calibration of the instrument. The standard samples utilized in these experiments include porous silica, polystyrene-poly isoprene, silver behenate, poly ball and polystyrene-poly (ethylene-alt-propylene). Even though the results show that BATAN-SANS instrument is in good shape, but rooms for improvements are still widely open especially for the velocity selector and its control system. (author)

Integrating Nephelometer Instrument Handbook

Energy Technology Data Exchange (ETDEWEB)

Uin, J. [Brookhaven National Lab. (BNL), Upton, NY (United States)

2016-03-01

The Integrating Nephelometer (Figure 1) is an instrument that measures aerosol light scattering. It measures aerosol optical scattering properties by detecting (with a wide angular integration – from 7 to 170°) the light scattered by the aerosol and subtracting the light scattered by the carrier gas, the instrument walls and the background noise in the detector (zeroing). Zeroing is typically performed for 5 minutes every day at midnight UTC. The scattered light is split into red (700 nm), green (550 nm), and blue (450 nm) wavelengths and captured by three photomultiplier tubes. The instrument can measure total scatter as well as backscatter only (from 90 to 170°) (Heintzenberg and Charlson 1996; Anderson et al. 1996; Anderson and Ogren 1998; TSI 3563 2015) At ARM (Atmospheric Radiation Measurement), two identical Nephelometers are usually run in series with a sample relative humidity (RH) conditioner between them. This is possible because Nephelometer sampling is non-destructive and the sample can be passed on to another instrument. The sample RH conditioner scans through multiple RH values in cycles, treating the sample. This kind of setup allows to study how aerosol particles’ light scattering properties are affected by humidification (Anderson et al. 1996). For historical reasons, the two Nephelometers in this setup are labeled “wet” and “dry”, with the “dry” Nephelometer usually being the one before the conditioner and sampling ambient air (the names are switched for the MAOS measurement site due to the high RH of the ambient air).

Prediction of autosomal STR typing success in ancient and Second World War bone samples.

Science.gov (United States)

Zupanič Pajnič, Irena; Zupanc, Tomaž; Balažic, Jože; Geršak, Živa Miriam; Stojković, Oliver; Skadrić, Ivan; Črešnar, Matija

2017-03-01

Human-specific quantitative PCR (qPCR) has been developed for forensic use in the last 10 years and is the preferred DNA quantification technique since it is very accurate, sensitive, objective, time-effective and automatable. The amount of information that can be gleaned from a single quantification reaction using commercially available quantification kits has increased from the quantity of nuclear DNA to the amount of male DNA, presence of inhibitors and, most recently, to the degree of DNA degradation. In skeletal remains samples from disaster victims, missing persons and war conflict victims, the DNA is usually degraded. Therefore the new commercial qPCR kits able to assess the degree of degradation are potentially able to predict the success of downstream short tandem repeat (STR) typing. The goal of this study was to verify the quantification step using the PowerQuant kit with regard to its suitability as a screening method for autosomal STR typing success on ancient and Second World War (WWII) skeletal remains. We analysed 60 skeletons excavated from five archaeological sites and four WWII mass graves from Slovenia. The bones were cleaned, surface contamination was removed and the bones ground to a powder. Genomic DNA was obtained from 0.5g of bone powder after total demineralization. The DNA was purified using a Biorobot EZ1 device. Following PowerQuant quantification, DNA samples were subjected to autosomal STR amplification using the NGM kit. Up to 2.51ng DNA/g of powder were extracted. No inhibition was detected in any of bones analysed. 82% of the WWII bones gave full profiles while 73% of the ancient bones gave profiles not suitable for interpretation. Four bone extracts yielded no detectable amplification or zero quantification results and no profiles were obtained from any of them. Full or useful partial profiles were produced only from bone extracts where short autosomal (Auto) and long degradation (Deg) PowerQuant targets were detected. It is

Cytological Sampling Versus Forceps Biopsy During Percutaneous Transhepatic Biliary Drainage and Analysis of Factors Predicting Success

Energy Technology Data Exchange (ETDEWEB)

Tapping, C. R.; Byass, O. R.; Cast, J. E. I., E-mail: james.cast@hey.nhs.uk [Hull Royal Infirmary, Department of Radiology (United Kingdom)

2012-08-15

Purpose: To assess the accuracy of cytological sampling and forceps biopsy in obstructing biliary lesions and to identify factors predictive of success. Methods: Consecutive patients (n = 119) with suspected malignant inoperable obstructive jaundice treated with percutaneous transhepatic biliary drainage during 7 years were included (60 male; mean age 72.5 years). All patients underwent forceps biopsy plus cytological sampling by washing the forceps device in cytological solution. Patient history, procedural and pathological records, and clinical follow-up were reviewed. Statistical analysis included chi-square test and multivariate regression analysis. Results: Histological diagnosis after forceps biopsy was more successful than cytology: Sensitivity was 78 versus 61%, and negative predictive value was 30 versus 19%. Cytology results were never positive when the forceps biopsy was negative. The cytological sample was negative and forceps sample positive in 2 cases of cholangiocarcinoma, 16 cases of pancreatic carcinoma, and 1 case of benign disease. Diagnostic accuracy was predicted by low bilirubin (p < 0.001), aspartate transaminase (p < 0.05), and white cell count (p {<=} 0.05). Conclusions: This technique is safe and effective and is recommended for histological diagnosis during PTBD in patients with inoperable malignant biliary strictures. Diagnostic yield is greater when bilirubin levels are low and there is no sepsis; histological diagnosis by way of forceps biopsy renders cytological sampling unnecessary.

Instrument validation system of general application

International Nuclear Information System (INIS)

Filshtein, E.L.

1990-01-01

This paper describes the Instrument Validation System (IVS) as a software system which has the capability of evaluating the performance of a set of functionally related instrument channels to identify failed instruments and to quantify instrument drift. Under funding from Combustion Engineering (C-E), the IVS has been developed to the extent that a computer program exists whose use has been demonstrated. The initial development work shows promise for success and for wide application, not only to power plants, but also to industrial manufacturing and process control. Applications in the aerospace and military sector are also likely

Instrumentation for studying binder burnout in an immobilized plutonium ceramic wasteform

Energy Technology Data Exchange (ETDEWEB)

Mitchell, M; Pugh, D; Herman, C

2000-04-21

The Plutonium Immobilization Program produces a ceramic wasteform that utilizes organic binders. Several techniques and instruments were developed to study binder burnout on full size ceramic samples in a production environment. This approach provides a method for developing process parameters on production scale to optimize throughput, product quality, offgas behavior, and plant emissions. These instruments allow for offgas analysis, large-scale TGA, product quality observation, and thermal modeling. Using these tools, results from lab-scale techniques such as laser dilametry studies and traditional TGA/DTA analysis can be integrated. Often, the sintering step of a ceramification process is the limiting process step that controls the production throughput. Therefore, optimization of sintering behavior is important for overall process success. Furthermore, the capabilities of this instrumentation allows better understanding of plant emissions of key gases: volatile organic compounds (VOCs), volatile inorganics including some halide compounds, NO{sub x}, SO{sub x}, carbon dioxide, and carbon monoxide.

SQUID-based Nondestructive Testing Instrument of Dished Niobium Sheets for SRF Cavities

International Nuclear Information System (INIS)

Q. S. Shu; I. Ben-Zvi; G. Cheng; I. M. Phipps; J. T. Susta; P. Kneisel; G. Myneni; J. Mast; R. Selim

2007-01-01

Currently available technology can only inspect flat sheets and allow the elimination of defective flat sheets before the expensive forming and machining of the SRF cavity half-cells, but it does not eliminate the problem of remaining or uncovered surface impurities after partial chemical etching of the half-cells, nor does it detect any defects that may have been added during the fabrication of the half-cells. AMAC has developed a SQUID scanning system based on eddy current technique that allows the scanning of curved Nb samples that are welded to make superconducting RF cavity half-cells. AMAC SQUID scanning system successfully located the defects (Ta macro particles about 100 mm diameter) in a flat Nb sample (top side) and was able to also locate the defects in a cylindrical surface sample (top side). It is more significant that the system successfully located the defects on the backside of the flat sample and curved sample or 3-mm from the top surface. The 3-D SQUID-based Nondestructive instrument will be further optimized and improved in making SRF cavities and allow inspection and detection during cavity manufacturing for achieving highest accelerating fields

A statistical approach to instrument calibration

Science.gov (United States)

Robert R. Ziemer; David Strauss

1978-01-01

Summary - It has been found that two instruments will yield different numerical values when used to measure identical points. A statistical approach is presented that can be used to approximate the error associated with the calibration of instruments. Included are standard statistical tests that can be used to determine if a number of successive calibrations of the...

The design and implementation of the Dynamic Ionosphere Cubesat Experiment (DICE) science instruments

Science.gov (United States)

Burr, Steven Reed

Dynamic Ionosphere Cubesat Experiment (DICE) is a satellite project funded by the National Science Foundation (NSF) to study the ionosphere, more particularly Storm Enhanced Densities (SED) with a payload consisting of plasma diagnostic instrumentation. Three instruments onboard DICE include an Electric Field Probe (EFP), Ion Langmuir Probe (ILP), and Three Axis Magnetometer (TAM). The EFP measures electric fields from +/-8V and consists of three channels a DC to 40Hz channel, a Floating Potential Probe (FPP), and an spectrographic channel with four bands from 16Hz to 512Hz. The ILP measures plasma densities from 1x104 cm--3 to 2x107 cm--3. The TAM measures magnetic field strength with a range +/-0.5 Gauss with a sensitivity of 2nT. To achieve desired mission requirements careful selection of instrument requirements and planning of the instrumentation design to achieve mission success. The analog design of each instrument is described in addition to the digital framework required to sample the science data at a 70Hz rate and prepare the data for the Command and Data Handing (C&DH) system. Calibration results are also presented and show fulfillment of the mission and instrumentation requirements.

Aethalometer™ Instrument Handbook

Energy Technology Data Exchange (ETDEWEB)

Sedlacek, Arthur J. [Brookhaven National Lab. (BNL), Upton, NY (United States)

2016-04-01

The Aethalometer is an instrument that provides a real-time readout of the concentration of “Black” or “Elemental” carbon aerosol particles (BC or E) in an air stream (see Figure 1 and Figure 2). It is a self-contained instrument that measures the rate of change of optical transmission through a spot on a filter where aerosol is being continuously collected and uses the information to calculate the concentration of optically absorbing material in the sampled air stream. The instrument measures the transmitted light intensities through the “sensing” portion of the filter, on which the aerosol spot is being collected, and a “reference” portion of the filter as a check on the stability of the optical source. A mass flowmeter monitors the sample air flow rate. The data from these three measurements is used to determine the mean BC content of the air stream.

Language profiles in young children with autism spectrum disorder: A community sample using multiple assessment instruments.

Science.gov (United States)

Nevill, Rose; Hedley, Darren; Uljarević, Mirko; Sahin, Ensu; Zadek, Johanna; Butter, Eric; Mulick, James A

2017-11-01

This study investigated language profiles in a community-based sample of 104 children aged 1-3 years who had been diagnosed with autism spectrum disorder using Diagnostic and Statistical Manual of Mental Disorders (5th ed.) diagnostic criteria. Language was assessed with the Mullen scales, Preschool Language Scale, fifth edition, and Vineland-II parent-report. The study aimed to determine whether the receptive-to-expressive language profile is independent from the assessment instrument used, and whether nonverbal cognition, early communicative behaviors, and autism spectrum disorder symptoms predict language scores. Receptive-to-expressive language profiles differed between assessment instruments and reporters, and Preschool Language Scale, fifth edition profiles were also dependent on developmental level. Nonverbal cognition and joint attention significantly predicted receptive language scores, and nonverbal cognition and frequency of vocalizations predicted expressive language scores. These findings support the administration of multiple direct assessment and parent-report instruments when evaluating language in young children with autism spectrum disorder, for both research and in clinical settings. Results also support that joint attention is a useful intervention target for improving receptive language skills in young children with autism spectrum disorder. Future research comparing language profiles of young children with autism spectrum disorder to children with non-autism spectrum disorder developmental delays and typical development will add to our knowledge of early language development in children with autism spectrum disorder.

Economic instruments for environmental policy making in Ontario

International Nuclear Information System (INIS)

Barg, S.; Duraiappah, A.; Van Exan, S.

2000-01-01

The conditions and approaches required for a successful implementation of economic instruments in Ontario are reviewed. The advantages and disadvantages of economic instruments are discussed, as are some design issues. Some best practices and practical experiences from Canada, the United States, and Europe are examined through the use of nine specific case studies. Each one highlights a different environmental challenge, such as energy efficiency, air pollution, water pollution, waste management along with the solutions that were implemented. The situations described were not all successful, but there is much to be learned from unsuccessful episodes. Lessons learned from the review of the case studies were presented. The points to ponder when using economic instruments in Ontario were highlighted. The command and control policy instrument must be kept in context when considering economic instruments. The reasons that underline the preference of the economic theory for economic instruments are discussed. The different types of economic instruments are described, and the considerations related to the design and comparison of economic instruments is briefly discussed. The authors concluded with several points to ponder: there are a number of options available, details must not be neglected, consultation with the interested parties is important, there is a need for frequent reassessment, and using a number of instruments is helpful. 55 refs., tabs., figs

Serendipity: Genesis of the Electrochemical Instrumentation at Princeton Applied Research Corporation

Science.gov (United States)

Flato, J. B.

2007-01-01

Princeton Applied Research Corporation (PAR) was a small electronic instrument company in early 1960s but once they entered electrochemistry they were very successful. Since then they have developed and designed successful instruments with their tremendous knowledge and have made great contribution to the field of analytical chemistry.

DEVELOPMENT OF AN ON-LINE, REAL-TIME ALPHA RADIATION MEASURING INSTRUMENT FOR LIQUID STREAMS

International Nuclear Information System (INIS)

Unknown

1999-01-01

The US Department of Energy (DOE) has expressed a need for an on-line, real-time instrument for assaying alpha-emitting radionuclides (uranium and the transuranics) in effluent waters leaving DOE sites to ensure compliance with regulatory limits. Due to the short range of alpha particles in water (approximately40 Im), it is necessary now to intermittently collect samples of water and send them to a central laboratory for analysis. A lengthy and costly procedure is used to separate and measure the radionuclides from each sample. Large variations in radionuclide concentrations in the water may go undetected due to the sporadic sampling. Even when detected, the reading may not be representative of the actual stream concentration. To address these issues, the Advanced Technologies Group of Thermo Power Corporation (a Thermo Electron company) is developing a real-time, field-deployable alpha monitor based on a solid-state silicon wafer semiconductor (US Patent 5,652,013 and pending, assigned to the US Department of Energy). The Thermo Water Alpha Monitor will serve to monitor effluent water streams (Subsurface Contaminants Focus Area) and will be suitable for process control of remediation as well as decontamination and decommissioning (D and D) operations, such as monitoring scrubber or rinse water radioactivity levels (Mixed Waste, Plutonium, and D and D Focus Area). It would be applicable for assaying other liquids, such as oil, or solids after proper preconditioning. Rapid isotopic alpha air monitoring is also possible using this technology. This report details the program's accomplishments to date. Most significantly, the Alpha Monitoring Instrument was successfully field demonstrated on water 100X below the Environmental Protection Agency's proposed safe drinking water limit--down to under 1 pCi/1. During the Field Test, the Alpha Monitoring Instrument successfully analyzed isotopic uranium levels on a total of five different surface water, process water, and

Determination of elemental concentrations in environmental plant samples by instrumental neutron activation analysis

International Nuclear Information System (INIS)

Datta, J.; Chowdhury, D.P.; Verma, R.; Reddy, A.V.R.

2012-01-01

The intake of leafy vegetables in daily diet is very important to meet our nutritional needs. Vegetables provide the essential elements which are necessary and recommended for human growth. However, due to rapid industrialization and urbanization our environment becomes polluted and this affects the normal growth of agricultural products and composition of environmental species. The elemental concentrations present in the environmental samples are good indicators to assess the toxicological levels due to pollution affects. In the present work we have analysed several vegetable plant samples by instrumental neutron activation analysis to determine the elemental concentrations at major, minor and trace levels. The leafy vegetables like spinach, red leafy vegetable, pui, gourd leaf, lettuce and katoua were chosen as these are extensively consumed by local people in eastern part of India. We have determined 15 elements in the above mentioned vegetable samples and some of these are essential elements and some are toxic elements. It was found that Na and K were present as major elements, Fe and Zn as minor elements and As, Ce, Cr, Co, La, Mo, Rb, Sc, Sm, Sr as trace elements. The concentration level of Cr was found to be higher than that of recommended value certified by WHO and National environment quality control for human consumption. The validation of our analytical results have been performed by the Z-score tests through the determination of concentrations of the elements of interest in certified reference materials. (author)

The Sensors and Instrumentation Knowledge Transfer Network

International Nuclear Information System (INIS)

Cooper, P

2009-01-01

The Sensors and Instrumentation KTN has established itself as the UK's national network in sensors and instrumentation, developing a community of over 2,250 member organisations. This paper describes the background to Knowledge Transfer Networks (KTNs) and the changes that are happening to KTNs at a national level, before describing the market size, activities and successes of the Sensors and Instrumentation KTN. The paper concludes by describing the merger between the Sensors and Instrumentation KTN and four other KTNs to create a new KTN, with a working title of the Electronics, Sensors and Photonics KTN.

Cavity-enhanced quantum-cascade laser-based instrument for carbon monoxide measurements.

Science.gov (United States)

Provencal, Robert; Gupta, Manish; Owano, Thomas G; Baer, Douglas S; Ricci, Kenneth N; O'Keefe, Anthony; Podolske, James R

2005-11-01

An autonomous instrument based on off-axis integrated cavity output spectroscopy has been developed and successfully deployed for measurements of carbon monoxide in the troposphere and tropopause onboard a NASA DC-8 aircraft. The instrument (Carbon Monoxide Gas Analyzer) consists of a measurement cell comprised of two high-reflectivity mirrors, a continuous-wave quantum-cascade laser, gas sampling system, control and data-acquisition electronics, and data-analysis software. CO measurements were determined from high-resolution CO absorption line shapes obtained by tuning the laser wavelength over the R(7) transition of the fundamental vibration band near 2172.8 cm(-1). The instrument reports CO mixing ratio (mole fraction) at a 1-Hz rate based on measured absorption, gas temperature, and pressure using Beer's Law. During several flights in May-June 2004 and January 2005 that reached altitudes of 41,000 ft (12.5 km), the instrument recorded CO values with a precision of 0.2 ppbv (1-s averaging time) and an accuracy limited by the reference CO gas cylinder (uncertainty < 1.0%). Despite moderate turbulence and measurements of particulate-laden airflows, the instrument operated consistently and did not require any maintenance, mirror cleaning, or optical realignment during the flights.

Instruments for Water Quality Monitoring

Science.gov (United States)

Ballinger, Dwight G.

1972-01-01

Presents information regarding available instruments for industries and agencies who must monitor numerous aquatic parameters. Charts denote examples of parameters sampled, testing methods, range and accuracy of test methods, cost analysis, and reliability of instruments. (BL)

The Search for Organic Compounds of Martian Origin in Gale Crater by the Sample Analysis at Mars (SAM) Instrument on Curiosity

Science.gov (United States)

Glavin, Daniel; Freissinet, Caroline; Mahaffy, Paul; Miller, Kristen; Eigenbrode, Jennifer; Summons, Roger; Archer, Douglas, Jr.; Brunner, Anna; Martin, Mildred; Buch, Arrnaud;

Success and failure rates of tumor genotyping techniques in routine pathological samples with non-small-cell lung cancer.

Science.gov (United States)

Vanderlaan, Paul A; Yamaguchi, Norihiro; Folch, Erik; Boucher, David H; Kent, Michael S; Gangadharan, Sidharta P; Majid, Adnan; Goldstein, Michael A; Huberman, Mark S; Kocher, Olivier N; Costa, Daniel B

2014-04-01

Identification of some somatic molecular alterations in non-small-cell lung cancer (NSCLC) has become evidence-based practice. The success and failure rate of using commercially available tumor genotyping techniques in routine day-to-day NSCLC pathology samples is not well described. We sought to evaluate the success and failure rate of EGFR mutation, KRAS mutation, and ALK FISH in a cohort of lung cancers subjected to routine clinical tumor genotype. Clinicopathologic data, tumor genotype success and failure rates were retrospectively compiled and analyzed from 381 patient-tumor samples. From these 381 patients with lung cancer, the mean age was 65 years, 61.2% were women, 75.9% were white, 27.8% were never smokers, 73.8% had advanced NSCLC and 86.1% had adenocarcinoma histology. The tumor tissue was obtained from surgical specimens in 48.8%, core needle biopsies in 17.9%, and as cell blocks from aspirates or fluid in 33.3% of cases. Anatomic sites for tissue collection included lung (49.3%), lymph nodes (22.3%), pleura (11.8%), bone (6.0%), brain (6.0%), among others. The overall success rate for EGFR mutation analysis was 94.2%, for KRAS mutation 91.6% and for ALK FISH 91.6%. The highest failure rates were observed when the tissue was obtained from image-guided percutaneous transthoracic core-needle biopsies (31.8%, 27.3%, and 35.3% for EGFR, KRAS, and ALK tests, respectively) and bone specimens (23.1%, 15.4%, and 23.1%, respectively). In specimens obtained from bone, the failure rates were significantly higher for biopsies than resection specimens (40% vs. 0%, p=0.024 for EGFR) and for decalcified compared to non-decalcified samples (60% vs. 5.5%, p=0.021 for EGFR). Tumor genotype techniques are feasible in most samples, outside small image-guided percutaneous transthoracic core-needle biopsies and bone samples from core biopsies with decalcification, and therefore expansion of routine tumor genotype into the care of patients with NSCLC may not require special

Microdialysis sampling for investigations of bioavailability and bioequivalence of topically administered drugs: current state and future perspectives

DEFF Research Database (Denmark)

Holmgaard, R; Nielsen, J B; Benfeldt, E

2010-01-01

of instrumentation, calibration and experimental procedures are discussed along with the analytical considerations necessary for successful sampling. Clinical MD studies in the skin are reviewed with emphasis on pharmacokinetic studies of topically applied drugs with or without impairment of skin barrier function...

Hanford double shell tank corrosion monitoring instrument trees

International Nuclear Information System (INIS)

Nelson, J.L.

1995-03-01

High-level nuclear wastes at the Hanford site are stored underground in carbon steel double-shell and single-shell tanks - (DSTs and SSTS). Westinghouse Hanford Company is considering installation of a prototype corrosion monitoring instrument tree in at least one DST in the summer of 1995. The instrument tree will have the ability to detect and discriminate between uniform corrosion, stress corrosion cracking (SCC), and pitting. Additional instrument trees will follow in later years. Proof-of-technology testing is currently underway for the use of commercially available electric field pattern (EFP) analysis and electrochemical noise (EN) corrosion monitoring equipment. Creative use and combinations of other existing technologies is also being considered. Successful demonstration of these technologies will be followed by the development of a Hanford specific instrument tree. The first instrument tree will incorporate one of these technologies. Subsequent trees may include both technologies, as well as a more standard assembly of corrosion coupons. Successful development of these trees will allow their application to single shell tanks and the transfer of technology to other U.S. Department of Energy (DOE) sites

Development of Real-Time Coal Monitoring Instrument

Energy Technology Data Exchange (ETDEWEB)

Rajan Gurjar, Ph.D.

2010-06-17

Relying on coal for energy requires optimizing the extraction of heat content from various blends of coal fuel and reducing harmful constituents and byproducts. Having a real-time measurement instrument provides relevant information about toxic constituents released in the atmosphere from burning coal and optimizes the performance of a power plant. A few commercial instruments exist and have been in operation for more than a decade. However, most of these instruments are based on radioactive sources and are bulky, expensive and time-consuming. The proposed instrument is based on the Laser Induced Breakdown Spectroscopy (LIBS). The advantage of LIBS is that it is a standoff instrument, does not require sample preparation and provides precise information about sample constituents.

Risk Management Affecting IS/IT Project Success Through Communicative Action

NARCIS (Netherlands)

de Bakker, K.F.C.; Boonstra, A.; Wortmann, J.C.

Project risk management is defined in the literature as being instrumental action based on rational problem solving. Research indicates limited positive effects of an exclusive focus of instrumental action on project success. This article proposes to extend this instrumental view through

Quantification of chlorine in zirconium oxide and biological samples by instrumental NAA utilizing PCF of Dhruva reactor

International Nuclear Information System (INIS)

Shinde, Amol D.; Reddy, A.V.R.; Acharya, R.; Balaji Rao, Y.

2012-01-01

Recently studies on chlorine contents in various samples are being pursued due to its corrosive nature. Chlorine present at trace level in various finished products as well as powder is used as a raw material for production of different types of zircaloys used as structural materials in nuclear technology. As a part of quality assurance program, it is necessary to quantify chlorine accurately with suitable and simple technique. In the present work we have applied instrumental neutron activation analysis (INAA) utilizing its short-lived activation product ( 38 Cl, 37 min, 1642 and 2168 keV) for its estimation. Pneumatic Carrier Facility (PCF) of Dhruva reactor, BARC was used sample irradiation of zirconium oxide dry powder, synthetic wax and IAEA RMs 1515 (Apple leaves) and Lichen 336. (author)

A Comparison of Multivariate and Pre-Processing Methods for Quantitative Laser-Induced Breakdown Spectroscopy of Geologic Samples

Science.gov (United States)

Anderson, R. B.; Morris, R. V.; Clegg, S. M.; Bell, J. F., III; Humphries, S. D.; Wiens, R. C.

2011-01-01

The ChemCam instrument selected for the Curiosity rover is capable of remote laser-induced breakdown spectroscopy (LIBS).[1] We used a remote LIBS instrument similar to ChemCam to analyze 197 geologic slab samples and 32 pressed-powder geostandards. The slab samples are well-characterized and have been used to validate the calibration of previous instruments on Mars missions, including CRISM [2], OMEGA [3], the MER Pancam [4], Mini-TES [5], and Moessbauer [6] instruments and the Phoenix SSI [7]. The resulting dataset was used to compare multivariate methods for quantitative LIBS and to determine the effect of grain size on calculations. Three multivariate methods - partial least squares (PLS), multilayer perceptron artificial neural networks (MLP ANNs) and cascade correlation (CC) ANNs - were used to generate models and extract the quantitative composition of unknown samples. PLS can be used to predict one element (PLS1) or multiple elements (PLS2) at a time, as can the neural network methods. Although MLP and CC ANNs were successful in some cases, PLS generally produced the most accurate and precise results.

Psychometric Validation of the Parental Bonding Instrument in a UK Population–Based Sample Role of Gender and Association With Mental Health in Mid-Late Life

NARCIS (Netherlands)

M.K. Xu (Kate); A. J. S. Morin (Alexandre); H. W. Marsh (Herbert); M. Richards (Martin); P. B. Jones (Peter)

2016-01-01

markdownabstractThe factorial structure of the Parental Bonding Instrument (PBI) has been frequently studied in diverse samples but no study has examined its psychometric properties from large, population-based samples. In particular, important questions have not been addressed such as the

40+ Years of Instrumentation for the La Silla Paranal Observatory

Science.gov (United States)

D'Odorico, S.

2018-03-01

As ESO Period 100 comes to a close, I look back at the development of ESO's instrumentation programme over more than 40 years. Instrumentation and detector activities were initially started by a small group of designers, engineers, technicians and astronomers while ESO was still at CERN in Geneva in the late 1970s. They have since led to the development of a successful suite of optical and infrared instruments for the La Silla Paranal Observatory, as testified by the continuous growth in the number of proposals for observing time and in the publications based on data from ESO telescopes. The instrumentation programme evolved significantly with the VLT and most instruments were developed by national institutes in close cooperation with ESO. This policy was a cornerstone of the VLT programme from the beginning and a key to its success.

Evolved Gas Measurements Planned for the Lower Layers of the Gale Crater Mound with the Sample Analysis at Mars Instrument Suite

Science.gov (United States)

Mahaffy, Paul; Brunner, Anna; McAdam, Amy; Franz, Heather; Conrad, Pamela; Webster, Chris; Cabane, Michel

2009-01-01

The lower mound strata of Gale Crater provide a diverse set of chemical environments for exploration by the varied tools of the Curiosity Rover of the Mars Science Laboratory (MSL) Mission. Orbital imaging and spectroscopy clearly reveal distinct layers of hydrated minerals, sulfates, and clays with abundant evidence of a variety of fluvial processes. The three instruments of the MSL Sample Analysis at aMars (SAM) investigation, the Quadrupole Mass Spectrometer (QMS), the Tunable Laser Spectrometer (TLS), and the Gas Chromatograph (GC) are designed to analyze either atmospheric gases or volatiles thermally evolved or chemically extracted from powdered rock or soil. The presence or absence of organic compounds in these layers is of great interest since such an in situ search for this type of record has not been successfully implemented since the mid-60s Viking GCMS experiments. However, regardless of the outcome of the analysis for organics, the abundance and isotopic composition of thermally evolved inorganic compounds should also provide a rich data set to complement the mineralogical and elemental information provided by other MSL instruments. In addition, these evolved gas analysis (EGA) experiments will help test sedimentary models proposed by Malin and Edgett (2000) and then further developed by Milliken et al (2010) for Gale Crater. In the SAM EGA experiments the evolution temperatures of H2O, CO2, SO2, O2, or other simple compounds as the samples are heated in a helium stream to 1000 C provides information on mineral types and their associations. The isotopic composition of O, H, C, and S can be precisely determined in several evolved compounds and compared with the present day atmosphere. Such SAM results might be able to test mineralogical evidence of changing sedimentary and alteration processes over an extended period of time. For example, Bibring et al (2006) have suggested such a major shift from early nonacidic to later acidic alteration. We will

Robotic thin layer chromatography instrument for synthetic chemistry

International Nuclear Information System (INIS)

Corkan, L.A.; Lindsey, J.S.

1990-01-01

One of our long-term goals is to develop robotic workstations for automated synthetic chemistry. Toward that goal we have constructed a 2nd generation instrument for performing TLC analysis. TLC has important advantages (over HPLC and GC) in analysis of crude reaction samples and parallel sample development. The TLC instrument consist of four dedicated stations for (1) plate dispensing, (2) sample application, (3) plate development, and (4) plate densitometry. A robot is used to move plates among stations. The combination of fixed automation and robotics gives high sample throughout (up to 10 samples per hour). A second robot performs reaction chemistry and feeds samples to the TLC instrument, thus enabling TLC analysis at the same time as synthetic reactions proceed on the workstation

Astronomical Instrumentation System Markup Language

Science.gov (United States)

Goldbaum, Jesse M.

2016-05-01

The Astronomical Instrumentation System Markup Language (AISML) is an Extensible Markup Language (XML) based file format for maintaining and exchanging information about astronomical instrumentation. The factors behind the need for an AISML are first discussed followed by the reasons why XML was chosen as the format. Next it's shown how XML also provides the framework for a more precise definition of an astronomical instrument and how these instruments can be combined to form an Astronomical Instrumentation System (AIS). AISML files for several instruments as well as one for a sample AIS are provided. The files demonstrate how AISML can be utilized for various tasks from web page generation and programming interface to instrument maintenance and quality management. The advantages of widespread adoption of AISML are discussed.

Instrument to collect fogwater for chemical analysis

OpenAIRE

Jacob, Daniel J.; Waldman, Jed M.; Haghi, Mehrdad; Hoffmann, Michael R.; Flagan, Richard C.

1985-01-01

An instrument is presented which collects large samples of ambient fogwater by impaction of droplets on a screen. The collection efficiency of the instrument is determined as a function of droplet size, and it is shown that fog droplets in the range 3–100-µm diameter are efficiently collected. No significant evaporation or condensation occurs at any stage of the collection process. Field testing indicates that samples collected are representative of the ambient fogwater. The instrument may ea...

Policy instruments for pollution control in developing countries.

Science.gov (United States)

Eskeland, G S; Jimenez, E

1992-07-01

Economic development in developing countries must be accomplished in a manner that does not harm the environment with pollution. Pollution harms human health and productivity. Thus appropriate strategies must be developed that promote growth, reduce poverty, and protect the environment. A review of the current literature is performed with attention paid to cost-effective interventions i.e., comparisons of regulatory and fiscal instruments that can reduce pollution. Both direct instruments (like effluent charges, tradable permits, deposit refund systems, emission regulations and regulatory agency funding for purification, cleanup, waste disposal, and enforcement) and indirect instruments (like input/output taxes and subsidies, substitution subsidies, abatement inputs, regulation of equipment and processes, and development of clean technologies) are examined. Examples are used to show how indirect instruments can be successful when monitoring and enforcement is too costly. A careful examination of distributive concerns illustrate how the effect on the poor may need particular consideration and how groups with vested interests can help evaluate the probable success of such interventions.

Instrumentation for tropospheric aerosol characterization

Energy Technology Data Exchange (ETDEWEB)

Shi, Z.; Young, S.E.; Becker, C.H.; Coggiola, M.J. [SRI International, Menlo Park, CA (United States); Wollnik, H. [Giessen Univ. (Germany)

1997-12-31

A new instrument has been developed that determines the abundance, size distribution, and chemical composition of tropospheric and lower stratospheric aerosols with diameters down to 0.2 {mu}m. In addition to aerosol characterization, the instrument also monitors the chemical composition of the ambient gas. More than 25.000 aerosol particle mass spectra were recorded during the NASA-sponsored Subsonic Aircraft: Contrail and Cloud Effects Special Study (SUCCESS) field program using NASA`s DC-8 research aircraft. (author) 7 refs.

Instrumentation for tropospheric aerosol characterization

Energy Technology Data Exchange (ETDEWEB)

Shi, Z; Young, S E; Becker, C H; Coggiola, M J [SRI International, Menlo Park, CA (United States); Wollnik, H [Giessen Univ. (Germany)

1998-12-31

A new instrument has been developed that determines the abundance, size distribution, and chemical composition of tropospheric and lower stratospheric aerosols with diameters down to 0.2 {mu}m. In addition to aerosol characterization, the instrument also monitors the chemical composition of the ambient gas. More than 25.000 aerosol particle mass spectra were recorded during the NASA-sponsored Subsonic Aircraft: Contrail and Cloud Effects Special Study (SUCCESS) field program using NASA`s DC-8 research aircraft. (author) 7 refs.

The sample handling system for the Mars Icebreaker Life mission: from dirt to data.

Science.gov (United States)

Davé, Arwen; Thompson, Sarah J; McKay, Christopher P; Stoker, Carol R; Zacny, Kris; Paulsen, Gale; Mellerowicz, Bolek; Glass, Brian J; Willson, David; Bonaccorsi, Rosalba; Rask, Jon

2013-04-01

The Mars Icebreaker Life mission will search for subsurface life on Mars. It consists of three payload elements: a drill to retrieve soil samples from approximately 1 m below the surface, a robotic sample handling system to deliver the sample from the drill to the instruments, and the instruments themselves. This paper will discuss the robotic sample handling system. Collecting samples from ice-rich soils on Mars in search of life presents two challenges: protection of that icy soil--considered a "special region" with respect to planetary protection--from contamination from Earth, and delivery of the icy, sticky soil to spacecraft instruments. We present a sampling device that meets these challenges. We built a prototype system and tested it at martian pressure, drilling into ice-cemented soil, collecting cuttings, and transferring them to the inlet port of the SOLID2 life-detection instrument. The tests successfully demonstrated that the Icebreaker drill, sample handling system, and life-detection instrument can collectively operate in these conditions and produce science data that can be delivered via telemetry--from dirt to data. Our results also demonstrate the feasibility of using an air gap to prevent forward contamination. We define a set of six analog soils for testing over a range of soil cohesion, from loose sand to basalt soil, with angles of repose of 27° and 39°, respectively. Particle size is a key determinant of jamming of mechanical parts by soil particles. Jamming occurs when the clearance between moving parts is equal in size to the most common particle size or equal to three of these particles together. Three particles acting together tend to form bridges and lead to clogging. Our experiments show that rotary-hammer action of the Icebreaker drill influences the particle size, typically reducing particle size by ≈ 100 μm.

Possible Detection of Perchlorates by the Sample Analysis at Mars (SAM) Instrument: Comparison with Previous Missions

Science.gov (United States)

Navarro-Gonzalex, Rafael; Sutter, Brad; Archer, Doug; Ming, Doug; Eigenbrode, Jennifer; Franz, Heather; Glavin, Daniel; McAdam, Amy; Stern, Jennifer; McKay, Christopher;

A GC Instrument Simulator

Science.gov (United States)

Armitage, D. Bruce

1999-02-01

This simulator was developed to help students beginning the study of gas chromatographic instruments to understand their operation. It is not meant to teach chromatographic theory. The instrument simulator is divided into 5 sections. One is for sample preparation. Another is used to manage carrier gases and choose a detector and column. The third sets the conditions for either isothermal or programmed temperature operation. A fourth section models manual injections, and the fifth is the autosampler. The operator has a choice among 6 columns of differing diameters and packing polarities and a choice of either isothermal or simple one-stage temperature programming. The simulator can be operated in either single-sample mode or as a 10-sample autosampler. The integrator has two modes of operation, a "dumb" mode in which only the retention time, area of the peak, and percentage area are listed and a "smart" mode that also lists the components' identities. The identities are obtained from a list of names and retention times created by the operator. Without this list only the percentages and areas are listed. The percentages are based on the areas obtained from the chromatogram and not on the actual percentages assigned during sample preparation. The data files for the compounds used in the simulator are ASCII files and can be edited easily to add more compounds than the 11 included with the simulator. A maximum of 10 components can be used in any one sample. Sample mixtures can be made on a percent-by-volume basis, but not by mass of sample per volume of solvent. A maximum of 30 compounds can be present in any one file, but the number of files is limited only by the operating system. (I suggest that not more than 20 compounds be used in any one file, as scrolling through large numbers of compounds is annoying to say the least.) File construction and layout are discussed in detail in the User's Manual. Chromatograms are generated by calculating a retention time based on

On Representative Spaceflight Instrument and Associated Instrument Sensor Web Framework

Science.gov (United States)

Kizhner, Semion; Patel, Umeshkumar; Vootukuru, Meg

2007-01-01

Sensor Web-based adaptation and sharing of space flight mission resources, including those of the Space-Ground and Control-User communication segment, could greatly benefit from utilization of heritage Internet Protocols and devices applied for Spaceflight (SpaceIP). This had been successfully demonstrated by a few recent spaceflight experiments. However, while terrestrial applications of Internet protocols are well developed and understood (mostly due to billions of dollars in investments by the military and industry), the spaceflight application of Internet protocols is still in its infancy. Progress in the developments of SpaceIP-enabled instrument components will largely determine the SpaceIP utilization of those investments and acceptance in years to come. Likewise SpaceIP, the development of commercial real-time and instrument colocated computational resources, data compression and storage, can be enabled on-board a spacecraft and, in turn, support a powerful application to Sensor Web-based design of a spaceflight instrument. Sensor Web-enabled reconfiguration and adaptation of structures for hardware resources and information systems will commence application of Field Programmable Arrays (FPGA) and other aerospace programmable logic devices for what this technology was intended. These are a few obvious potential benefits of Sensor Web technologies for spaceflight applications. However, they are still waiting to be explored. This is because there is a need for a new approach to spaceflight instrumentation in order to make these mature sensor web technologies applicable for spaceflight. In this paper we present an approach in developing related and enabling spaceflight instrument-level technologies based on the new concept of a representative spaceflight Instrument Sensor Web (ISW).

A simple, inexpensive device for nucleic acid amplification without electricity-toward instrument-free molecular diagnostics in low-resource settings.

Directory of Open Access Journals (Sweden)

Paul LaBarre

2011-05-01

Full Text Available Molecular assays targeted to nucleic acid (NA markers are becoming increasingly important to medical diagnostics. However, these are typically confined to wealthy, developed countries; or, to the national reference laboratories of developing-world countries. There are many infectious diseases that are endemic in low-resource settings (LRS where the lack of simple, instrument-free, NA diagnostic tests is a critical barrier to timely treatment. One of the primary barriers to the practicality and availability of NA assays in LRS has been the complexity and power requirements of polymerase chain reaction (PCR instrumentation (another is sample preparation.In this article, we investigate the hypothesis that an electricity-free heater based on exothermic chemical reactions and engineered phase change materials can successfully incubate isothermal NA amplification assays. We assess the heater's equivalence to commercially available PCR instruments through the characterization of the temperature profiles produced, and a minimal method comparison. Versions of the prototype for several different isothermal techniques are presented.We demonstrate that an electricity-free heater based on exothermic chemical reactions and engineered phase change materials can successfully incubate isothermal NA amplification assays, and that the results of those assays are not significantly different from ones incubated in parallel in commercially available PCR instruments. These results clearly suggest the potential of the non-instrumented nucleic acid amplification (NINA heater for molecular diagnostics in LRS. When combined with other innovations in development that eliminate power requirements for sample preparation, cold reagent storage, and readout, the NINA heater will comprise part of a kit that should enable electricity-free NA testing for many important analytes.

Determination of selenium in food matrices by replicate sample neutron activation analysis

International Nuclear Information System (INIS)

Ventura, M.G.; Freitas, M.C.; Ventura, M.G.; Pacheco, A.M.G.

2009-01-01

The replicate sample instrumental neutron activation method was optimized and used for the determination of selenium in foodstuffs. The method was reliable, yielding accurate results. Lower detections limits were obtained after each successive irradiation. Different irradiation conditions were used depending on the type of sample. For samples with higher selenium contents (meat, fish, eggs), the measured selenium in the first replicate is in all cases larger than the detection limit, but a better accuracy was obtained with a larger number of replicates (2-3 replicates). For samples with extremely low selenium contents (vegetable samples), at least seven replicates were necessary to obtain a concentration value two times larger than the detection limit. (author)

The Influence of Innovation and Entrepreneurial Self-Efficacy to Digital Startup Success

Directory of Open Access Journals (Sweden)

Agnes Dessyana

2017-08-01

Full Text Available Establishing and developing a startup business is not easy. Startup success depend on various aspects, such as financial,business model, and learning organizations. Personalities factor of founders have a contribution in business development, especially entrepreneurial self-efficacy (ESE and innovation. But, in Indonesia, there is still no psychological study who see the contribution of those factors on business success in digital startup. This study aimed to understand how both factors influence startup digital. The sample is 64 founders. The research instrument is ESE, KAI, and Business Success questionnaire (Kirton in Riyanti, 2003; Chen et al, 1998; Kaplan & Norton, 2006. Multiple-regression analyses reveal ESE and innovation contributes 20.8% to business success. ESE regression coefficient is 0.200 (P 0.05. This means, ESE has significant positive effect, while innovation has a positive relationship but insignificant. Interventions in the form of booklets that inform how to increase ESE. The booklet is already conducted trials on five founders.

Detecting Organic Compounds Released from Iron Oxidizing Bacteria using Sample Analysis at Mars (SAM) Like Instrument Protocols

Science.gov (United States)

Glavin, D. P.; Popa, R.; Martin, M. G.; Freissinet, C.; Fisk, M. R.; Dworkin, J. P.; Mahaffy, P. R.

2012-01-01

Mars is a planet of great interest for Astrobiology since its past environmental conditions are thought to have been favourable for the emergence life. At present, the Red Planet is extremely cold and dry and the surface is exposed to intense UV and ionizing radiation, conditions generally considered to be incompatible with life as we know it on Earth. It was proposed that the shallow subsurface of Mars, where temperatures can be above freezing and liquid water can exist on rock surfaces, could harbor chemolithoautotrophic bacteria such as the iron oxidizing microorganism Pseudomonas sp. HerB. The Mars Science Laboratory (MSL) mission will provide the next opportunity to carry out in situ measurements for organic compounds of possible biological origin on Mars. One instrument onboard MSL, called the Sample Analysis at Mars (SAM) instrument suite, will carry out a broad and sensitive search for organic compounds in surface samples using either high temperature pyrolysis or chemical extraction followed by gas chromatography mass spectrometry. We present gas chromatograph mass spectrometer (GC/MS) data on crushed olivine rock powders that have been inoculated with Pseudomonas sp. HerB at different concentrations ranging from approx 10(exp 2) to 10(exp 7) cells per gram. The inoculated olivine samples were heated under helium carrier gas flow at 500 C and the pyrolysis products concentrated using a SAM-like hydrocarbon trap set at -20 C followed by trap heating and analysis by GC/Ms. In addition, the samples were also extracted using a low temperature "one-pot" chemical extraction technique using N-methyl, N-(tert-butyldimethylsilyl) trifluoroacetamide (MTBSTFA) as the silylating agent prior to GC/MS analysis. We identified several aldehydes, thiols, and alkene nitriles after pyrolysis GC/MS analysis of the bacteria that were not found in the olivine control samples that had not been inoculated with bacteria. The distribution of pyrolysis products extracted from the

Finite-sample instrumental variables Inference using an Asymptotically Pivotal Statistic

NARCIS (Netherlands)

Bekker, P.; Kleibergen, F.R.

2001-01-01

The paper considers the K-statistic, Kleibergen’s (2000) adaptation ofthe Anderson-Rubin (AR) statistic in instrumental variables regression.Compared to the AR-statistic this K-statistic shows improvedasymptotic efficiency in terms of degrees of freedom in overidentifiedmodels and yet it shares,

Robotic thin layer chromatography instrument for synthetic chemistry

International Nuclear Information System (INIS)

Corkan, L.A.; Haynes, E.; Kline, S.; Lindsey, J.S.

1991-01-01

We have constructed a second generation instrument for performing automated thin layer chromatography (TLC), The TLC instrument Consists of four dedicated stations for (1) plate dispensing, (2) sample application, (3) plate development, and (4) densitometry. A robot is used to move TLC plates among stations. The TLC instrument functions either as a stand-alone unit or as one analytical module in a robotic workstation for synthetic chemistry. An integrated hardware and software architecture enables automatic TLC analysis of samples produced concurrently from synthetic reactions in progress on the workstation. The combination of fixed automation and robotics gives a throughput of 12 TLC samples per hour. From these results a blueprint has emerged for an advanced automated TLC instrument with far greater throughput and analytical capabilities

Journey towards active lifestyle and successful ageing among ...

African Journals Online (AJOL)

A research instrument tagged 'Active Lifestyle and Successful Ageing among Pensioners' (ALASAAP) was the main instrument used for the research. Data was analysed using Pearson product correlation moment and multiple regression. The results of the study revealed active lifestyle as a strong positive relationship with ...

Planning instruments to control urban growth

DEFF Research Database (Denmark)

Jørgensen, Gertrud; Nielsen, Thomas Alexander Sick

2010-01-01

It is challenging to plan and control urban development in peri-urban areas. But if no planning is done, the result will often be unsustainable, including widespread, dispersed and uncoordinated urban growth. Spatial planning based on zoning remains the most important planning instrument and its...... success depend on regional coordination. Incentive based instruments may contrbute to growth management, but only few examples are available and their effects on urban growth patterns yet to be seen....

Marketing instruments of foreign trade promotion

Directory of Open Access Journals (Sweden)

Bjelić Predrag

2011-01-01

Full Text Available Instruments of promotion as a part of marketing mix are usually associated with companies but more and more countries use this instrument in order to boost their exports. These foreign trade promotion instruments are now popular in many countries in the world since their use is not opposed to any World Trade Organization rules. Marketing instruments of trade promotions are the most important. They include National Exhibitions and National labels of origin and quality. In order to coordinate the application of these instruments countries have established national bodies for trade promotion. Many studies in the past had argued that national Agencies established to promote export did not had any real success, but recent studies indicate that they could have a significant impact on country export promotion. The result of this rise in impact of national export promotion agencies is due to international effort spearheaded by International Trade Center. The aim of this paper is to point out types and methods of marketing instruments application in trade promotion and to present the effectiveness of these instruments applications.

Finite-sample instrumental variables inference using an asymptotically pivotal statistic

NARCIS (Netherlands)

Bekker, Paul A.; Kleibergen, Frank

2001-01-01

The paper considers the K-statistic, Kleibergen’s (2000) adaptation of the Anderson-Rubin (AR) statistic in instrumental variables regression. Compared to the AR-statistic this K-statistic shows improved asymptotic efficiency in terms of degrees of freedom in overidenti?ed models and yet it shares,

Instrument to collect fogwater for chemical analysis

Energy Technology Data Exchange (ETDEWEB)

Jacob, D.J.; Waldman, J.M.; Haghi, M.; Hoffmann, M.R.; Flagan, R.C.

1985-06-01

An instrument is presented which collects large samples of ambient fogwater by impaction of droplets on a screen. The collection efficiency of the instrument is determined as a function of droplet size, and it is shown that fog droplets in the range 3--100-..mu..m diameter are efficiently collected. No significant evaporation or condensation occurs at any stage of the collection process. Field testing indicates that samples collected are representative of the ambient fogwater. The instrument may easily be automated, and is suitable for use in routine air quality monitoring programs.

Instrument to collect fogwater for chemical analysis

Science.gov (United States)

Jacob, Daniel J.; Waldman, Jed M.; Haghi, Mehrdad; Hoffmann, Michael R.; Flagan, Richard C.

1985-06-01

An instrument is presented which collects large samples of ambient fogwater by impaction of droplets on a screen. The collection efficiency of the instrument is determined as a function of droplet size, and it is shown that fog droplets in the range 3-100-μm diameter are efficiently collected. No significant evaporation or condensation occurs at any stage of the collection process. Field testing indicates that samples collected are representative of the ambient fogwater. The instrument may easily be automated, and is suitable for use in routine air quality monitoring programs.

Low-Dimensional Feature Representation for Instrument Identification

Science.gov (United States)

Ihara, Mizuki; Maeda, Shin-Ichi; Ikeda, Kazushi; Ishii, Shin

For monophonic music instrument identification, various feature extraction and selection methods have been proposed. One of the issues toward instrument identification is that the same spectrum is not always observed even in the same instrument due to the difference of the recording condition. Therefore, it is important to find non-redundant instrument-specific features that maintain information essential for high-quality instrument identification to apply them to various instrumental music analyses. For such a dimensionality reduction method, the authors propose the utilization of linear projection methods: local Fisher discriminant analysis (LFDA) and LFDA combined with principal component analysis (PCA). After experimentally clarifying that raw power spectra are actually good for instrument classification, the authors reduced the feature dimensionality by LFDA or by PCA followed by LFDA (PCA-LFDA). The reduced features achieved reasonably high identification performance that was comparable or higher than those by the power spectra and those achieved by other existing studies. These results demonstrated that our LFDA and PCA-LFDA can successfully extract low-dimensional instrument features that maintain the characteristic information of the instruments.

Cross-instrument Analysis Correlation Software

Energy Technology Data Exchange (ETDEWEB)

2017-06-28

This program has been designed to assist with the tracking of a sample from one analytical instrument to another such as SEM, microscopes, micro x-ray diffraction and other instruments where particular positions/locations on the sample are examined, photographed, etc. The software is designed to easily enter the position of fiducials and locations of interest such that in a future session in the same of different instrument the positions of interest can be re-found through using the known location fiducials in the current and reference session to transform the point into the current sessions coordinate system. The software is dialog box driven guiding the user through the necessary data entry and program choices. Information is stored in a series of text based extensible markup language (XML) files.

Simultaneous multi-element determination in different seed samples of Dodonaea viscosa hopseed using instrumental neutron activation analysis

International Nuclear Information System (INIS)

El-Sweify, Fatma H.; El-Amir, Mahmoud A.; Mostafa, Mohamed; Ramadan, Hala E.; Rashad, Ghada M.

2016-01-01

Instrumental neutron activation analysis technique (INAA) was applied for nondestructive multi-element analysis of seed samples of the plant Dodonaea viscosa hopseed. This plant is distributed all over Egypt, because of its suitable properties. The samples were collected from some bushes grown at different sites in some governorates, in July of each year during the period from 2004 to 2011. The determined elements are: Co, Cs, Eu, Fe, Hg, Ni, Rb, Sc, Se, Sr and Zn, under the chosen irradiation and cooling times. The content of some elements has been compared with data obtained from previous work on analysis of various kinds of seeds. The influence of some parameters on the determined elemental content is discussed. Standard reference materials IAEA-155 and IAEA-V-10 were used to assure quality control, accuracy and precision of the technique.

Simultaneous multi-element determination in different seed samples of Dodonaea viscosa hopseed using instrumental neutron activation analysis

Energy Technology Data Exchange (ETDEWEB)

El-Sweify, Fatma H.; El-Amir, Mahmoud A.; Mostafa, Mohamed; Ramadan, Hala E.; Rashad, Ghada M. [Atomic Energy Authority, Cairo (Egypt). Hot Lab. Center

2016-07-01

Instrumental neutron activation analysis technique (INAA) was applied for nondestructive multi-element analysis of seed samples of the plant Dodonaea viscosa hopseed. This plant is distributed all over Egypt, because of its suitable properties. The samples were collected from some bushes grown at different sites in some governorates, in July of each year during the period from 2004 to 2011. The determined elements are: Co, Cs, Eu, Fe, Hg, Ni, Rb, Sc, Se, Sr and Zn, under the chosen irradiation and cooling times. The content of some elements has been compared with data obtained from previous work on analysis of various kinds of seeds. The influence of some parameters on the determined elemental content is discussed. Standard reference materials IAEA-155 and IAEA-V-10 were used to assure quality control, accuracy and precision of the technique.

Lessons Learned From the Analysis of the SAFOD Downhole Instrument Package.

Science.gov (United States)

Johnson, Wade; Mencin, David; Mattioli, Glen

2013-04-01

In September of 2008 a downhole instrument package (DIP) consisting of a string of seismometers and tilt meters in isolated pressure vessels (PODs) was installed in the SAFOD main borehole. This package was designed to protect the sensors from the corrosive borehole environment and to operate for two years. The SAFOD borehole is not sealed at the bottom allowing borehole gasses and fluids infiltratration. Previous short-term installations of instruments in the SAFOD main borehole had also failed as a result of corrosion of the wireline cable head. The average failure time for these installations was two weeks. The use of stainless steel tubing connected to the pressure vessels through gas tight fittings was designed to block borehole fluid and gas infiltration of the individual instruments within the PODs. Unfortunately, the DIP completely failed within a month of its installation. In October of 2010, the DIP was removed from the borehole and a failure analysis was performed. This analysis involved to following steps: 1. Analysis of data to understand timeline of failure 2. Remove instrument safely, maintaining integrity of spliced section and documenting any external clues. Test instrument at surface 3. Open PODs in a way that allows for sampling and avoids damaging instruments. 4. Chemical analysis of fluids recovered from splices and PODs. 5. Instrument failure analysis by the instrument manufacturers. The analysis found that there were several design flaws in the DIP. This included the use of motor oil to take up air space in the individual PODs, use of a large number of gas tight seals, lack of internal seals, poorly done solder joints, use of non-temperature rated sensors, and lack of management oversight. The lessons learned from the attempts to instrument the SAFOD borehole are critical to the success of future deep borehole projects.

Atomic absorption instrument functional description

International Nuclear Information System (INIS)

Bystroff, R.I.; Boyle, W.G. Jr.; Barton, G.W. Jr.

1976-01-01

This report describes a proposed system for automating atomic absorption analysis. The system consists of two atomic absorption instruments and an automatic sampler that can be attached to either instrument. A computer program controls the sampling and gathers data. The program then uses the data to perform bookkeeping, data processing, and report writing

Evaluation of sediment sampling devices and methods used in the NKS/EKO-1 project

Energy Technology Data Exchange (ETDEWEB)

Ilus, E. [Finnish Centre for Radiation and Nuclear Safety (Finland)

1996-10-01

The radioactive fallout caused by nuclear weapons tests in the 1960s and the accident at the Chernobyl NPP in 1986 has created useful markers in the sediments of many Nordic waters. These have been successfully used not only in radioecological studies but also in limnological and marine research dealing with sedimentation processes and rates. To be able to study sedimentation and processes in sediments, it is essential to obtain reliable samples from sediments. False conclusions are an obvious risk if the studies are based on biased field samples. More strictly,, it is unreasonable to perform exacting and expensive analyses if the samples themselves are unreliable or of poor quality. The instruments best suited for quantitative sampling of soft-bottom sediments appear to be those based on the coring principle. Box corers can be reliably used for bulk sampling of coherent sediments and some silty and sandy sediments. Many factors speak in favour of large diameters/areas of the corer orifices. It is not possible, however, to increase the tube diameter without negative impact to the corer`s handiness and increasing difficulty in handling and slicing of the cores. Despite the large variety of sampling instruments and many sources of error involved in the use of different instruments, it is most important to know and account for the disadvantages and to work as carefully as possible towards minimizing errors and obtaining undisturbed, reliable samples. (EG).

Evaluation of sediment sampling devices and methods used in the NKS/EKO-1 project

International Nuclear Information System (INIS)

Ilus, E.

1996-01-01

The radioactive fallout caused by nuclear weapons tests in the 1960s and the accident at the Chernobyl NPP in 1986 has created useful markers in the sediments of many Nordic waters. These have been successfully used not only in radioecological studies but also in limnological and marine research dealing with sedimentation processes and rates. To be able to study sedimentation and processes in sediments, it is essential to obtain reliable samples from sediments. False conclusions are an obvious risk if the studies are based on biased field samples. More strictly,, it is unreasonable to perform exacting and expensive analyses if the samples themselves are unreliable or of poor quality. The instruments best suited for quantitative sampling of soft-bottom sediments appear to be those based on the coring principle. Box corers can be reliably used mainly for bulk sampling of coherent sediments and some silty and sandy sediments. Many factors speak in favour of relatively large diameters/areas of the corer orifices. It is not possible, however, to increase the tube diameter endlessly without negative impact to the corer's handiness and increasing difficulty in handling and slicing of the cores. Despite the large variety of sampling instruments and many sources of error involved in the use of different instruments, it is most important to know and account for the disadvantages and to work as carefully as possible towards minimizing errors and obtaining undisturbed, reliable samples. (EG)

Standard practice for instrumented indentation testing

CERN Document Server

American Society for Testing and Materials. Philadelphia

2007-01-01

1.1 This practice defines the basic steps of Instrumented Indentation Testing (IIT) and establishes the requirements, accuracies, and capabilities needed by an instrument to successfully perform the test and produce the data that can be used for the determination of indentation hardness and other material characteristics. IIT is a mechanical test that measures the response of a material to the imposed stress and strain of a shaped indenter by forcing the indenter into a material and monitoring the force on, and displacement of, the indenter as a function of time during the full loading-unloading test cycle. 1.2 The operational features of an IIT instrument, as well as requirements for Instrument Verification Annex A1), Standardized Reference Blocks (Annex A2) and Indenter Requirements (Annex A3) are defined. This practice is not intended to be a complete purchase specification for an IIT instrument. 1.3 With the exception of the non-mandatory Appendix X4, this practice does not define the analysis necessary...

Satellite-instrument system engineering best practices and lessons

Science.gov (United States)

Schueler, Carl F.

2009-08-01

This paper focuses on system engineering development issues driving satellite remote sensing instrumentation cost and schedule. A key best practice is early assessment of mission and instrumentation requirements priorities driving performance trades among major instrumentation measurements: Radiometry, spatial field of view and image quality, and spectral performance. Key lessons include attention to technology availability and applicability to prioritized requirements, care in applying heritage, approaching fixed-price and cost-plus contracts with appropriate attention to risk, and assessing design options with attention to customer preference as well as design performance, and development cost and schedule. A key element of success either in contract competition or execution is team experience. Perhaps the most crucial aspect of success, however, is thorough requirements analysis and flowdown to specifications driving design performance with sufficient parameter margin to allow for mistakes or oversights - the province of system engineering from design inception to development, test and delivery.

Central banks' use in East Asia of money market instruments in the conduct of monetary policy

OpenAIRE

Robert F. Emery

1992-01-01

The paper examines the greater use in the past decade of money market instruments in the conduct of monetary policy by the central banks, or their equivalent, in six of the main East Asian developing economies. Some of these economies have been successful in using various money market instruments to control liquidity, while others have been much less successful. A common theme in the case of the successful economies has been one of employing money market instruments that have yields based on ...

Modularized Parallel Neutron Instrument Simulation on the TeraGrid

International Nuclear Information System (INIS)

Chen, Meili; Cobb, John W.; Hagen, Mark E.; Miller, Stephen D.; Lynch, Vickie E.

2007-01-01

In order to build a bridge between the TeraGrid (TG), a national scale cyberinfrastructure resource, and neutron science, the Neutron Science TeraGrid Gateway (NSTG) is focused on introducing productive HPC usage to the neutron science community, primarily the Spallation Neutron Source (SNS) at Oak Ridge National Laboratory (ORNL). Monte Carlo simulations are used as a powerful tool for instrument design and optimization at SNS. One of the successful efforts of a collaboration team composed of NSTG HPC experts and SNS instrument scientists is the development of a software facility named PSoNI, Parallelizing Simulations of Neutron Instruments. Parallelizing the traditional serial instrument simulation on TeraGrid resources, PSoNI quickly computes full instrument simulation at sufficient statistical levels in instrument de-sign. Upon SNS successful commissioning, to the end of 2007, three out of five commissioned instruments in SNS target station will be available for initial users. Advanced instrument study, proposal feasibility evaluation, and experiment planning are on the immediate schedule of SNS, which pose further requirements such as flexibility and high runtime efficiency on fast instrument simulation. PSoNI has been redesigned to meet the new challenges and a preliminary version is developed on TeraGrid. This paper explores the motivation and goals of the new design, and the improved software structure. Further, it describes the realized new features seen from MPI parallelized McStas running high resolution design simulations of the SEQUOIA and BSS instruments at SNS. A discussion regarding future work, which is targeted to do fast simulation for automated experiment adjustment and comparing models to data in analysis, is also presented

Proceedings of the 38th international instrumentation symposium

International Nuclear Information System (INIS)

Richter, S.H.; Smith, E.A.

1991-01-01

This volume covers the proceedings of a symposium on instrumentation within the Aerospace and Test Measurement Divisions of the Instrument Society of America. Topics covered included: PC control in turbine engine testing, energy measurement of high proton beams, instrumentation for sampling related to the US clean Air Act, and instrumentation for monitoring in-reactor severe fuel damage tests

Research and development of thermal-fluid measuring instrument

International Nuclear Information System (INIS)

Tuzla, K.; Chen, J.C.

1991-01-01

The goal of this program is to develop an instrument to measure the time-fraction of liquid contact in the transition and film boiling regimes for flow within a vertical tube. The work was carried out at Lehigh University between February 15, 1989 to February 15, 1991. The instrument to measure time-fraction of liquid contact was successfully developed and tested

Developing a workplace resilience instrument.

Science.gov (United States)

Mallak, Larry A; Yildiz, Mustafa

2016-05-27

Resilience benefits from the use of protective factors, as opposed to risk factors, which are associated with vulnerability. Considerable research and instrument development has been conducted in clinical settings for patients. The need existed for an instrument to be developed in a workplace setting to measure resilience of employees. This study developed and tested a resilience instrument for employees in the workplace. The research instrument was distributed to executives and nurses working in the United States in hospital settings. Five-hundred-forty completed and usable responses were obtained. The instrument contained an inventory of workplace resilience, a job stress questionnaire, and relevant demographics. The resilience items were written based on previous work by the lead author and inspired by Weick's [1] sense-making theory. A four-factor model yielded an instrument having psychometric properties showing good model fit. Twenty items were retained for the resulting Workplace Resilience Instrument (WRI). Parallel analysis was conducted with successive iterations of exploratory and confirmatory factor analyses. Respondents were classified based on their employment with either a rural or an urban hospital. Executives had significantly higher WRI scores than nurses, controlling for gender. WRI scores were positively and significantly correlated with years of experience and the Brief Job Stress Questionnaire. An instrument to measure individual resilience in the workplace (WRI) was developed. The WRI's four factors identify dimensions of workplace resilience for use in subsequent investigations: Active Problem-Solving, Team Efficacy, Confident Sense-Making, and Bricolage.

Comparison of fine particle measurements from a direct-reading instrument and a gravimetric sampling method.

Science.gov (United States)

Kim, Jee Young; Magari, Shannon R; Herrick, Robert F; Smith, Thomas J; Christiani, David C

2004-11-01

Particulate air pollution, specifically the fine particle fraction (PM2.5), has been associated with increased cardiopulmonary morbidity and mortality in general population studies. Occupational exposure to fine particulate matter can exceed ambient levels by a large factor. Due to increased interest in the health effects of particulate matter, many particle sampling methods have been developed In this study, two such measurement methods were used simultaneously and compared. PM2.5 was sampled using a filter-based gravimetric sampling method and a direct-reading instrument, the TSI Inc. model 8520 DUSTTRAK aerosol monitor. Both sampling methods were used to determine the PM2.5 exposure in a group of boilermakers exposed to welding fumes and residual fuel oil ash. The geometric mean PM2.5 concentration was 0.30 mg/m3 (GSD 3.25) and 0.31 mg/m3 (GSD 2.90)from the DUSTTRAK and gravimetric method, respectively. The Spearman rank correlation coefficient for the gravimetric and DUSTTRAK PM2.5 concentrations was 0.68. Linear regression models indicated that log, DUSTTRAK PM2.5 concentrations significantly predicted loge gravimetric PM2.5 concentrations (p gravimetric PM2.5 concentrations was found to be modified by surrogate measures for seasonal variation and type of aerosol. PM2.5 measurements from the DUSTTRAK are well correlated and highly predictive of measurements from the gravimetric sampling method for the aerosols in these work environments. However, results from this study suggest that aerosol particle characteristics may affect the relationship between the gravimetric and DUSTTRAK PM2.5 measurements. Recalibration of the DUSTTRAK for the specific aerosol, as recommended by the manufacturer, may be necessary to produce valid measures of airborne particulate matter.

Development of Interactive Monitoring System for Neutron Scattering Instrument

Energy Technology Data Exchange (ETDEWEB)

So, Ji Yong [Korea Atomic Energy Research Institute, Daejeon (Korea, Republic of)

2015-10-15

Neutron scattering instruments in HANARO research reactor have been contributed to various fields of basic science and material engineering. These instruments are open to publics and researchers can apply beam-time and do experiments with instrument scientists. In most cases, these instruments run for several weeks without stopping, and therefore instrument scientist wants to see the instrument status and receive information if the instruments have some problem. This is important for the safety. However, it is very hard to get instrument information outside of instruments. Access from external site is strongly forbidden in the institute due to the network safety, I developed another way to send instrument status information using commercial short messaging service(SMS). In this presentation, detailed features of this system will be shown. As a prototype, this system is being developed for the single instrument: Disk-chopper time-of-flight instruments (DC-TOF). I have successfully developed instruments and operate for several years. This information messaging system can be used for other neutron scattering instruments.

Density dependence and climate effects in Rocky Mountain elk: an application of regression with instrumental variables for population time series with sampling error.

Science.gov (United States)

Creel, Scott; Creel, Michael

2009-11-01

1. Sampling error in annual estimates of population size creates two widely recognized problems for the analysis of population growth. First, if sampling error is mistakenly treated as process error, one obtains inflated estimates of the variation in true population trajectories (Staples, Taper & Dennis 2004). Second, treating sampling error as process error is thought to overestimate the importance of density dependence in population growth (Viljugrein et al. 2005; Dennis et al. 2006). 2. In ecology, state-space models are used to account for sampling error when estimating the effects of density and other variables on population growth (Staples et al. 2004; Dennis et al. 2006). In econometrics, regression with instrumental variables is a well-established method that addresses the problem of correlation between regressors and the error term, but requires fewer assumptions than state-space models (Davidson & MacKinnon 1993; Cameron & Trivedi 2005). 3. We used instrumental variables to account for sampling error and fit a generalized linear model to 472 annual observations of population size for 35 Elk Management Units in Montana, from 1928 to 2004. We compared this model with state-space models fit with the likelihood function of Dennis et al. (2006). We discuss the general advantages and disadvantages of each method. Briefly, regression with instrumental variables is valid with fewer distributional assumptions, but state-space models are more efficient when their distributional assumptions are met. 4. Both methods found that population growth was negatively related to population density and winter snow accumulation. Summer rainfall and wolf (Canis lupus) presence had much weaker effects on elk (Cervus elaphus) dynamics [though limitation by wolves is strong in some elk populations with well-established wolf populations (Creel et al. 2007; Creel & Christianson 2008)]. 5. Coupled with predictions for Montana from global and regional climate models, our results

Turbidity threshold sampling: Methods and instrumentation

Science.gov (United States)

Rand Eads; Jack Lewis

2001-01-01

Traditional methods for determining the frequency of suspended sediment sample collection often rely on measurements, such as water discharge, that are not well correlated to sediment concentration. Stream power is generally not a good predictor of sediment concentration for rivers that transport the bulk of their load as fines, due to the highly variable routing of...

Search for Chemical Biomarkers on Mars Using the Sample Analysis at Mars Instrument Suite on the Mars Science Laboratory

Science.gov (United States)

Glavin, D. P.; Conrad, P.; Dworkin, J. P.; Eigenbrode, J.; Mahaffy, P. R.

2011-01-01

One key goal for the future exploration of Mars is the search for chemical biomarkers including complex organic compounds important in life on Earth. The Sample Analysis at Mars (SAM) instrument suite on the Mars Science Laboratory (MSL) will provide the most sensitive measurements of the organic composition of rocks and regolith samples ever carried out in situ on Mars. SAM consists of a gas chromatograph (GC), quadrupole mass spectrometer (QMS), and tunable laser spectrometer to measure volatiles in the atmosphere and released from rock powders heated up to 1000 C. The measurement of organics in solid samples will be accomplished by three experiments: (1) pyrolysis QMS to identify alkane fragments and simple aromatic compounds; pyrolysis GCMS to separate and identify complex mixtures of larger hydrocarbons; and (3) chemical derivatization and GCMS extract less volatile compounds including amino and carboxylic acids that are not detectable by the other two experiments.

An instrument for real time detection of contamination in space environmental tests chambers

Science.gov (United States)

Richmond, R. G.; Harmon, H. N.

1972-01-01

An instrument for in situ vacuum detection of surface reflectance changes at 1216A was designed. Using successive reflections, this instrument is more sensitive as an indicator of reflectance changes than similar instruments having only a single reflection. The selection of each component of the instrument and its operational performance is discussed.

Iron Quadrangle, Brazil. Elemental concentration determined by k0-instrumental neutron activation analysis. Part 1. Soil samples

International Nuclear Information System (INIS)

Menezes, M.A.B.C.; Palmieri, H.E.L.; Leonel, L.V.; Nalini, H.A.Jr.; Jacimovic, R.

2006-01-01

The Iron Quadrangle, Minas Gerais, Brazil, is rich in mineral occurrences and is considered one of the richest mineral-bearing regions in the world. Most investigations in this region have dealt with the determination of arsenic and mercury but so far few studies have been carried out aiming at determining other important elements. Having in mind the potential risk caused by mineral activities, this study was developed in order to assess the potential influence of the soil on foodstuffs. The soil samples were collected from three sites inside and outside the Iron Quadrangle. The samples were analyzed at the Laboratory for Neutron Activation Analysis, CDTN/CNEN by the k 0 -instrumental neutron activation analysis. This paper reports the elemental concentration determined in soil and emphasises the elements cited in the Brazilian environmental legislation for soil. This work also confirms the high elemental concentration of several minerals, however, it is difficult to distinguish the contamination from anthropogenic activities from the natural occurrence. (author)

Cassette-based in-situ TEM sample inspection in the dual-beam FIB

International Nuclear Information System (INIS)

Kendrick, A B; Moore, T M; Zaykova-Feldman, L; Amador, G; Hammer, M

2008-01-01

A novel method is presented, combining site-specific TEM sample preparation and in-situ STEM analysis in a dual-beam microscope (FIB/SEM) fitted with a chamber mounted nano-manipulator. TEM samples are prepared using a modified in-situ, lift-out method, whereby the samples are thinned and oriented for immediate in-situ STEM analysis using the tilt, translation, and rotation capabilities of a FIB/SEM sample stage, a nano-manipulator, and a novel cassette. This cassette can provide a second tilt axis, orthogonal to the stage tilt axis, so that the STEM image contrast can be optimized to reveal the structural features of the sample (true STEM imaging in the FIB/SEM). The angles necessary for stage rotation and probe shaft rotation are calculated based on the position of the nano-manipulator relative to the stage and door and the stage tilt angle. A FIB/SEM instrument, equipped with a high resolution scanning electron column, can provide sufficiently high image resolution to enable many failure analysis and process control applications to be successfully carried out without requiring the use of a separate dedicated TEM/STEM instrument. The benefits of this novel approach are increased throughput and reduced cost per sample. Comparative analysis of different sample preparation methods is provided, and the STEM images obtained are shown.

Neutron scattering instrumentation. A guide to future directions

International Nuclear Information System (INIS)

Crawford, R.K.

2001-01-01

Many of the neutron scattering instruments being designed or built now are the first generation of pulsed source instruments to provide nearly optimal scattering angle coverage with good spatial resolution in a single setting of the instrument while making full use of modern optics to maximize the useful flux on the sample. Spectacular gains have resulted from such optimization, but in most of these cases there is little room for further large improvements. However, other types of pulsed source instruments are currently less well optimized, and there is room for significant improvements in these types of pulsed source instruments. Several examples will illustrate these points. In the longer term, we can expect source strengths to continue to increase, but only slowly. However, we can expect new science and new ways of doing experiments to emerge. Many of these changes will be driven by enhancements in sample environment capabilities leading to more innovative sample conditions and to efficient parametric studies. Kinetic studies and parametric studies will take on much greater roles with the high data rates now available. Implications of these trends will be discussed. (author)

Instruments to measure behavioural and psychological symptoms of dementia.

Science.gov (United States)

van der Linde, Rianne M; Stephan, Blossom C M; Dening, Tom; Brayne, Carol

2014-03-01

Reliable and valid measurement of behavioural and psychological symptoms of dementia (BPSD) is important for research and clinical practice. Here we provide an overview of the different instruments and discuss issues involved in the choice of the most appropriate instrument to measure BPSD in research. A list of BPSD instruments was generated. For each instrument Pubmed and SCOPUS were searched for articles that reported on their use or quality. Eighty-three instruments that are used to measure BPSD were identified. Instruments differ in length and detail, whether the interview is with participants, informants or by observation, the target sample and the time frames for use. Reliability and validity is generally good, but reported in few independent samples. When choosing a BPSD instrument for research the research question should be carefully scrutinised and the symptoms of interest, population, quality, detail, time frame and practical issues should be considered. Copyright © 2014 John Wiley & Sons, Ltd.

The upgraded cold neutron triple-axis spectrometer FLEXX – enhanced capabilities by new instrumental options

Directory of Open Access Journals (Sweden)

Habicht Klaus

2015-01-01

Full Text Available The upgrade of the cold neutron triple axis spectrometer FLEXX, a work-horse instrument for inelastic neutron scattering matching the sample environment capabilities at Helmholtz-Zentrum Berlin, has been successfully accomplished. Experiments confirmed an order of magnitude gain in flux now allowing for intensity demanding options to be fully exploited at FLEXX. In this article, we describe the layout and design of two newly available FLEXX instrument options in detail. The new Heusler analyzer gives an increase of the detected polarized neutron flux due to its superior focusing properties, significantly improving the feasibility of future polarized and neutron resonance spin echo experiments. The MultiFLEXX option provides simultaneous access to large regions in wavevector and energy space for inelastic excitations thus adding mapping capabilities to the spectrometer.

Software for simulation and design of neutron scattering instrumentation

DEFF Research Database (Denmark)

Bertelsen, Mads

designed using the software. The Union components uses a new approach to simulation of samples in McStas. The properties of a sample are split into geometrical and material, simplifying user input, and allowing the construction of complicated geometries such as sample environments. Multiple scattering...... from conventional choices. Simulation of neutron scattering instrumentation is used when designing instrumentation, but also to understand instrumental effects on the measured scattering data. The Monte Carlo ray-tracing package McStas is among the most popular, capable of simulating the path of each...... neutron through the instrument using an easy to learn language. The subject of the defended thesis is contributions to the McStas language in the form of the software package guide_bot and the Union components.The guide_bot package simplifies the process of optimizing neutron guides by writing the Mc...

Field portable low temperature porous layer open tubular cryoadsorption headspace sampling and analysis part I: Instrumentation.

Science.gov (United States)

Bruno, Thomas J

2016-01-15

Building on the successful application in the laboratory of PLOT-cryoadsorption as a means of collecting vapor (or headspace) samples for chromatographic analysis, in this paper a field portable apparatus is introduced. This device fits inside of a briefcase (aluminum tool carrier), and can be easily transported by vehicle or by air. The portable apparatus functions entirely on compressed air, making it suitable for use in locations lacking electrical power, and for use in flammable and explosive environments. The apparatus consists of four aspects: a field capable PLOT-capillary platform, the supporting equipment platform, the service interface between the PLOT-capillary and the supporting equipment, and the necessary peripherals. Vapor sampling can be done with either a hand piece (containing the PLOT capillary) or with a custom fabricated standoff module. Both the hand piece and the standoff module can be heated and cooled to facilitate vapor collection and subsequent vapor sample removal. The service interface between the support platform and the sampling units makes use of a unique counter current approach that minimizes loss of cooling and heating due to heat transfer with the surroundings (recuperative thermostatting). Several types of PLOT-capillary elements and sampling probes are described in this report. Applications to a variety of samples relevant to forensic and environmental analysis are discussed in a companion paper. Published by Elsevier B.V.

A systematic review of motivational values and conservation success in and around protected areas.

Science.gov (United States)

Cetas, Elijah R; Yasué, Maï

2017-02-01

In conservation projects in and around protected areas (PAs), a suite of policy instruments are used to promote conservation behavior in local people. Few studies have related psychological research on motivational values to conservation in PAs. We conducted a systematic review of 120 peer-reviewed articles to assess the relative frequencies of policy instruments that aimed to foster intrinsic versus extrinsic motivations to conserve. We examined how the type of motivation engendered by the instrument (i.e., intrinsic or extrinsic motivation and based on the description of how the project was designed and implemented) influenced the ecological, economic, and social success of the project. We assessed the success of the project in only the case studies that included a quantitative or qualitative analysis of success. Projects designed to foster at least one intrinsically motivating instrument were 3 times more likely to meet socioeconomic or ecological goals. Although certain types of instruments such as payments or fines tended to be based on extrinsic motivators more often than education or monitoring programs, several successful projects involving payments or fines were linked to intrinsic motivation in the local community. Thus, our results suggest that rather than debating the relative merits of specific types of policy instruments, conservationists may have more success by focusing on how different motivators, suited to specific contexts, can better empower local communities to conserve. Broadly, our results suggest the current emphasis on social justice and well-being of local communities is a positive step toward protecting the world's remaining biodiversity. © 2016 Society for Conservation Biology.

Tritium instrumentation for a fusion reactor power plant

International Nuclear Information System (INIS)

Shank, K.E.; Easterly, C.E.

1976-09-01

A review of tritium instrumentation is presented. This includes a discussion of currently available in-plant instrumentation and methods required for sampling stacks, monitoring process streams and reactor coolants, analyzing occupational work areas for air and surface contamination, and personnel monitoring. Off-site instrumentation and collection techniques are also presented. Conclusions are made concerning the adequacy of existing instrumentation in relation to the monitoring needs for fusion reactors

Nucleonic instruments from VUPJT Tesla

International Nuclear Information System (INIS)

Smola, J.

1986-01-01

The instruments currently produced by Tesla Premysleni are listed and briefly characterized. They include a low level alpha-beta counter, an automatic low level alpha-beta counter, detection units for environmental sample counting, instruments for measuring specific activity of liquids and radon concentration in water, a radioactive aerosol meter, dose ratemeters, portable alpha-beta indicators for surface contamintion monitoring, neutron monitors, single-, two- and three-channel spectrometric units. (M.D.)

THE EFFECT OF HARD AND SOFT FACTORS ON THE SUCCESS OF A COMPANY

Directory of Open Access Journals (Sweden)

Peter Bóna

2015-06-01

Full Text Available What makes a company successful? What kind of instruments may it use to achieve outstanding results? Instruments necessary for effective operation depend remarkably on the current age and the environment surrounding the organisation. Various ages have had their different keys to success. This key has become more and more complex and complicated due to the continuous acceleration of world economy and the fact that distances have become negligible. The aim of this study is to explore, whether companies having an interest in the processing industry use hard or soft success factors as a key to achieve success. In order to do that, the research will identify the possible success factors first. Henceforward it will reveal the effect of the resulting factors on success by logistic regression, which will be examined via the balance scorecard by complementing the four classic aspects – as one of the pioneers – with a fifth one, i.e. sustainability. Thus it will become visible, to what extent strategic, structural, cultural and leadership success factors influence the performance of a company to reach excellence in accordance with the expectations of the owners, the customers, the employees and the social sphere. The results of the research will thereby show the unravelled correlations between the successful operation of a company and the instruments indicating hard and soft success affecting it.

Laser sampling

International Nuclear Information System (INIS)

Gorbatenko, A A; Revina, E I

2015-01-01

The review is devoted to the major advances in laser sampling. The advantages and drawbacks of the technique are considered. Specific features of combinations of laser sampling with various instrumental analytical methods, primarily inductively coupled plasma mass spectrometry, are discussed. Examples of practical implementation of hybrid methods involving laser sampling as well as corresponding analytical characteristics are presented. The bibliography includes 78 references

Digital readout alpha survey instrument

International Nuclear Information System (INIS)

Jacobs, M.E.

1976-01-01

A prototype solid-state digital readout alpha particle survey instrument has been designed and constructed. The meter incorporates a Ludlum alpha scintillator as a detector, digital logic circuits for control and timing, and a Digilin counting module with reflective liquid crystal display. The device is used to monitor alpha radiation from a surface. Sample counts are totalized over 10-second intervals and displayed digitally in counts per minute up to 19,999. Tests over source samples with counts to 15,600 cpm have shown the device to be rapid, versatile and accurate. The instrument can be fabricated in one man-week and requires about $835 in material costs. A complete set of drawings is included

Non-process instrumentation surveillance and test reduction

International Nuclear Information System (INIS)

Ferrell, R.; LeDonne, V.; Donat, T.; Thomson, I.; Sarlitto, M.

1993-12-01

Analysis of operating experience, instrument failure modes, and degraded instrument performance has led to a reduction in Technical Specification surveillance and test requirements for nuclear power plant process instrumentation. These changes have resulted in lower plant operations and maintenance (O ampersand M) labor costs. This report explores the possibility of realizing similar savings by reducing requirements for non-process instrumentation. The project team reviewed generic Technical Specifications for the four major US nuclear steam supply system (NSSS) vendors (Westinghouse, General Electric, Combustion Engineering, and Babcock ampersand Wilcox) to identify nonprocess instrumentation for which surveillance/test requirements could be reduced. The team surveyed 10 utilities to identify specific non-process instrumentation at their plants for which requirements could be reduced. The team evaluated utility analytic approaches used to justify changes in surveillance/test requirements for process equipment to determine their applicability to non-process instrumentation. The report presents a prioritized list of non-process instrumentation systems suitable for surveillance/test requirements reduction. The top three systems in the list are vibration monitors, leak detection monitors, and chemistry monitors. In general, most non-process instrumentation governed by Technical Specification requirements are candidates for requirements reduction. If statistical requirements are somewhat relaxed, the analytic approaches previously used to reduce requirements for process instrumentation can be applied to non-process instrumentation. The report identifies as viable the technical approaches developed and successfully used by Southern California Edison, Arizona Public Service, and Boston Edison

Laser light scattering instrument advanced technology development

Science.gov (United States)

Wallace, J. F.

1993-01-01

The objective of this advanced technology development (ATD) project has been to provide sturdy, miniaturized laser light scattering (LLS) instrumentation for use in microgravity experiments. To do this, we assessed user requirements, explored the capabilities of existing and prospective laser light scattering hardware, and both coordinated and participated in the hardware and software advances needed for a flight hardware instrument. We have successfully breadboarded and evaluated an engineering version of a single-angle glove-box instrument which uses solid state detectors and lasers, along with fiber optics, for beam delivery and detection. Additionally, we have provided the specifications and written verification procedures necessary for procuring a miniature multi-angle LLS instrument which will be used by the flight hardware project which resulted from this work and from this project's interaction with the laser light scattering community.

Personal assistance, income and employment: the spinal injuries survey instrument (SISI) and its application in a sample of people with quadriplegia.

Science.gov (United States)

Rowell, D; Connelly, L B

2008-06-01

Our aim was to ascertain what effect access to personal care package (PCP) has on the labour market activities of people who have a spinal cord injury (SCI). We developed a new instrument called the spinal injuries survey instrument (SISI). The SISI is a 35-item instrument, which contains items on health, education, employment, along with measures of personal assistance, mobility and psychological attribution style. The SISI was administered, with the Short Form 36 (SF-36) health status instrument, to 250 people with an SCI. The response rate was 72%. A retrospective, matched case-control sampling approach matched individuals who received a PCP, with a cohort who did not. The matching criteria included the site and severity of spinal lesion, age and gender. Although data on the reliability of the instrument are currently lacking, our empirical results are consistent with other studies: (1) mean annual health care costs (AUD$8741) are comparable with Walsh's estimates (2) SF-36 data support Kreuter's contention that mental health is resilient to SCI and (3) a post-injury employment rate of 29.7% corroborates Murphy et al. We present additional data describing income, educational attainment and family support. Our discussion borrows a conceptualization of disability by Sen, that includes both an 'earning handicap' (an impediment to earn income) and a 'conversion handicap' (an impediment to the enjoyment of income). Our application of the SISI provides evidence of both. The labour income of people with quadriplegia is AUD$10,007 per annum, while diminished health status, increased out-of-pocket health expenditure and loss of time suggest a conversion handicap.

Catching Stardust and Bringing it Home: The Astronomical Importance of Sample Return

Science.gov (United States)

Brownlee, D.

2002-12-01

The return of lunar samples by the Apollo program provided the first opportunity to perform detailed laboratory studies of ancient solid materials from a known astronomical body. The highly detailed study of the samples, using the best available laboratory instruments and techniques, revolutionized our understanding of the Moon and provided fundamental insight into the remarkable and violent processes that occur early in the history of moons and terrestrial planets. This type of astronomical paleontology is only possible with samples and yet the last US sample return was made by Apollo 17- over thirty years ago! The NASA Stardust mission, began a new era of sample missions with its 1999 launch to retrieve samples from the short period comet Wild 2. Genesis (a solar wind collector) was launched in 2001, the Japanese MUSES-C asteroid sample return mission will launch in 2003 and Mars sample return missions are under study. All of these missions will use sophisticated ground-based instrumentation to provide types of information that cannot be obtained by astronomical and spacecraft remote sensing methods. In the case of Stardust, the goal is to determine the fundamental nature of the initial solid building blocks of solar systems at atomic-scale spatial resolution. The samples returned by the mission will be samples from the Kuiper Belt region and they are probably composed of submicron silicate and organic materials of both presolar and nebular origin. Unlocking the detailed records contained in the elemental, chemical, isotopic and mineralogical composition of these tiny components can only be appropriately explored with full power, precision and flexibility of laboratory instrumentation. Laboratory instrumentation has the advantage that is state-of-the-art and is not limited by serious considerations of power, mass, cost or even reliability. The comparison of the comet sample, accumulated beyond Neptune, with asteroidal meteorites that accumulated just beyond the

Instrument for Study of Microbial Thermal Inactivation

Science.gov (United States)

Dickerson, R. W.; Read, R. B.

1968-01-01

An instrument was designed for the study of thermal inactivation of microorganisms using heating times of less than 1 sec. The instrument operates on the principle of rapid automatic displacement of the microorganism to and from a saturated steam atmosphere, and the operating temperature range is 50 to 90 C. At a temperature of 70 C, thermometric lag (time required to respond to 63.2% of a step change) of the fluid sample containing microorganisms was 0.12 sec. Heating time required to heat the sample to within 0.1 C of the exposure temperature was less than 1 sec, permitting exposure periods as brief as 1 sec, provided the proper corrections are made for the lethal effect of heating. The instrument is most useful for heat exposure periods of less than 5 min, and, typically, more than 500 samples can be processed for microbial inactivation determinations within an 8-hr period. Images Fig. 2 Fig. 3 Fig. 4 Fig. 5 Fig. 7 Fig. 8 PMID:4874466

Determination of the total amount of organically bound chlorine, bromine and iodine in environmental samples by instrumental neutron activation analysis

Energy Technology Data Exchange (ETDEWEB)

Gether, J; Lunde, G [Central Institute for Industrial Research, Oslo (Norway); Steinnes, E [Institutt for Atomenergi, Kjeller (Norway)

1979-07-01

The determination of chlorine, bromine and iodine present as non-polar, hydrophobic hydrocarbons in environmental samples is reported. The organohalogen compounds are seprated from water into an organic phase by on-site liquid-liquid extraction, and form biological material by procedures based on lipid phase extraction and codistillation. After removal of inorganic halides by washing with water and concentration of the sample by evaporation of the solvent, the resulting extracts are analyzed for their chlorine, bromine and iodine contents by instrumental neutron activation analysus. Strict attention is paid to the possibility of contamination in every step of the procedure. Background values in routine analysis are approximately 100-200 ng of chlorine, <5 ng of bromine and <3 ng of iodine.

Methods and instrumentation for quantitative microchip capillary electrophoresis

NARCIS (Netherlands)

Revermann, T.

2007-01-01

The development of novel instrumentation and analytical methodology for quantitative microchip capillary electrophoresis (MCE) is described in this thesis. Demanding only small quantities of reagents and samples, microfluidic instrumentation is highly advantageous. Fast separations at high voltages

Teaching Strategies and Gender in Higher Education Instrumental Studios

Science.gov (United States)

Zhukov, Katie

2012-01-01

This study investigates instrumental music teaching strategies in higher education settings, in order to identify those employed and their frequency and context of use. An instrument- and gender-balanced sample of 24 lessons from five institutions was analysed using a researcher-designed observational instrument. The results reveal the…

Well scintillation counter with automatic sample changing and data processing: an inexpensive instrument incorporating consumer products

International Nuclear Information System (INIS)

Dudley, R.A.; Figdor, H.C.; Keroe, E.A.; Morris, A.C. Jr.; Mutz, O.J.

1977-01-01

An automatic well scintillation-counting system suitable for in vitro assays with 125 I has been designed with the express purpose of allowing effective operation and maintenance in laboratories in developing countries. The system incorporates comparatively simple components, notably two consumer products: A Kodak Carousel slide projector as sample changer and a Hewlett-Packard HP-97 programmable printing calculator as system controller and data processor. The instrument can accomodate 80 counting vials of demensions 12 mm diameter x 75 mm, or 40 vials of 16 mm diameter x 100 mm. The calculator provides on-line control and data reduction with the mediation of an interface somewhat resembling that required between a scaler and a printer. Its program capacity is adequate for fairly complicated on-line operations, including, interpolation from a standard curve in logit-log space, calculation of error in hormone concentration, and termination of counting when the counting error is rediced to a prescribed fraction of the composite of other random assay errors (as stored in the calculator's memory). This system is inexpensive, robust, and capable of being operated manually if automatic accessories fail. It could be improved in several ways, particularly by providing for operation from batteries and, no doubt in the immediate future, substitution of the next generation of cheaper and more powerful calculators. The instrument may be cost-effective in any small to medium-sized laboratory. (orig.) [de

Evaluating manta ray mucus as an alternative DNA source for population genetics study: underwater-sampling, dry-storage and PCR success

Science.gov (United States)

Maxwell, Elisabeth A.; Marshall, Andrea D.; Christensen, Ana B.

2015-01-01

Sharks and rays are increasingly being identified as high-risk species for extinction, prompting urgent assessments of their local or regional populations. Advanced genetic analyses can contribute relevant information on effective population size and connectivity among populations although acquiring sufficient regional sample sizes can be challenging. DNA is typically amplified from tissue samples which are collected by hand spears with modified biopsy punch tips. This technique is not always popular due mainly to a perception that invasive sampling might harm the rays, change their behaviour, or have a negative impact on tourism. To explore alternative methods, we evaluated the yields and PCR success of DNA template prepared from the manta ray mucus collected underwater and captured and stored on a Whatman FTA™ Elute card. The pilot study demonstrated that mucus can be effectively collected underwater using toothbrush. DNA stored on cards was found to be reliable for PCR-based population genetics studies. We successfully amplified mtDNA ND5, nuclear DNA RAG1, and microsatellite loci for all samples and confirmed sequences and genotypes being those of target species. As the yields of DNA with the tested method were low, further improvements are desirable for assays that may require larger amounts of DNA, such as population genomic studies using emerging next-gen sequencing. PMID:26413431

In situ analysis of Mars soil sample with the sam gcms instrumentation onboard Curiosity : interpretation and comparison of measurements done at Rocknest and Yelloknife bay sites

Science.gov (United States)

Szopa, Cyril; Coll, Patrice; Cabane, Michel; Coscia, David; Buch, Arnaud; Francois, Pascaline; Millan, Maeva; Teinturier, Sammy; Navarro-Gonzales, Rafael; Glavin, Daniel; Freissinet, Caro; Steele, Andrew; Eigenbrode, Jen; Mahaffy, Paul

2014-05-01

The characterisation of the chemical and mineralogical composition of regolith samples collected with the Curiosity rover is a primary objective of the SAM experiment. These data should provide essential clues on the past habitability of Gale crater. Amongst the SAM suite of instruments [1], SAM-GC (Gas Chromatograph) is devoted to identify and quantify volatiles evolved from the thermal (heating up to about 900°C)/chemical (derivatization procedure) treatment of any soil sample collected by the Curiosity rover. With the aim to search for potential organic molecules outgassed from the samples, a SAM-GC analytical channel composed of thermal-desorption injector and a MXT-CLP chromatographic column was chosen to achieve all the measurements done up today, as it was designed for the separation of a wide range of volatile organic molecules. Three solid samples have been analyzed with GCMS, one sand sample collected at the Rocknest site, and two rock samples (John Klein and Cumberland respectively) collected at the Yellowknife Bay site using the Curiosity driller. All the measurements were successful and they produced complex chromatograms with both detectors used for SAM GC, i.e. a thermal conductivity detector and the SAM quandrupole mass spectrometer. Their interpretation already revealed the presence of an oxychlorine phase present in the sample which is at the origin of chlorohydrocarbons clearly identified [2] but this represents only a fraction of the GCMS signal recorded [3,4]. This work presents a systematic comparison of the GCMS measurements done for the different samples collected, supported by reference data obtained in laboratory with different spare models of the gas chromatograph, with the aim to bring new elements of interpretation of the SAM measurements. References: [1] Mahaffy, P. et al. (2012) Space Sci Rev, 170, 401-478. [2] Glavin, D. et al. (2013), JGR. [3] Leshin L. et al. (2013), Science, [4] Ming D. et al. (2013), Science, 32, 64

Associative symmetry in the pigeon after successive matching-to-sample training.

Science.gov (United States)

Frank, Andrea J; Wasserman, Edward A

2005-09-01

If an organism is explicitly taught an A-->B association, then might it also spontaneously learn the symmetrical B-->A association? Little evidence attests to such "associative symmetry" in nonhuman animals. We report for the first time a clear case of associative symmetry in the pigeon. Experiment 1 used a successive go/no go matching-to-sample procedure, which showed all of the training and testing stimuli in one location and intermixed arbitrary and identity matching trials. We found symmetrical responding that was as robust during testing (B-->A) as during training (A-->B). In Experiment 2, we trained different pigeons using only arbitrary matching trials before symmetry testing. No symmetrical responding was found. In Experiment 3, we trained other pigeons with only arbitrary matching trials and then tested for symmetry. When these pigeons, too, did not exhibit symmetrical responding, we retrained them with intermixed identity and arbitrary matching trials. Less robust symmetrical responding was obtained here than in Experiment 1. Collectively, these results suggest that identity matching may have to be learned concurrently with arbitrary matching from the outset of training for symmetry to emerge.

Nuclear reactor instrumentation

International Nuclear Information System (INIS)

Duncombe, E.; McGonigal, G.

1976-01-01

Reference is made to the instrumentation of liquid metal cooled fast reactors. In order to ensure the safe operation of such reactors it is necessary to constantly monitor the coolant flowing through the fuel assemblies for temperature and rate of flow, requiring a large number of sensors. An improved and simplified arrangement is claimed in which the fuel assemblies feed a fraction of coolant to three instrument units arranged to sense the temperature and rate of flow of samples of coolant. Each instrument unit comprises a sleeve housing a sensing unit and has a number of inlet ducts arranged for receiving coolant from a fuel assembly together with a single outlet. The sensing unit has three thermocouple hot junctions connected in series, the hot junctions and inlet ducts being arranged in pairs. Electromagnetic windings around an inductive core are arranged to sense variation in flow of liquid metal by flux distortion. Fission product sensing means may also be provided. Full constructional details are given. (U.K.)

Factors Driving Learner Success in Online Professional Development

Directory of Open Access Journals (Sweden)

Phu Vu

2014-07-01

Full Text Available This study examined factors that contributed to the success of online learners in an online professional development course. Research instruments included an online survey and learners’ activity logs in an online professional development course for 512 in-service teachers. The findings showed that there were several factors affecting online learners’ success in online professional development. In addition, there were also significant differences between successful and unsuccessful online learners in terms of course login frequency and learning activities viewed.

Scientific instruments, scientific progress and the cyclotron

International Nuclear Information System (INIS)

Baird, David; Faust, Thomas

1990-01-01

Philosophers speak of science in terms of theory and experiment, yet when they speak of the progress of scientific knowledge they speak in terms of theory alone. In this article it is claimed that scientific knowledge consists of, among other things, scientific instruments and instrumental techniques and not simply of some kind of justified beliefs. It is argued that one aspect of scientific progress can be characterized relatively straightforwardly - the accumulation of new scientific instruments. The development of the cyclotron is taken to illustrate this point. Eight different activities which promoted the successful completion of the cyclotron are recognised. The importance is in the machine rather than the experiments which could be run on it and the focus is on how the cyclotron came into being, not how it was subsequently used. The completed instrument is seen as a useful unit of scientific progress in its own right. (UK)

The Successful Diagnosis and Typing of Systemic Amyloidosis Using A Microwave-Assisted Filter-Aided Fast Sample Preparation Method and LC/MS/MS Analysis.

Directory of Open Access Journals (Sweden)

Weiyi Sun

Full Text Available Laser microdissection followed by mass spectrometry has been successfully used for amyloid typing. However, sample contamination can interfere with proteomic analysis, and overnight digestion limits the analytical throughput. Moreover, current quantitative analysis methods are based on the spectrum count, which ignores differences in protein length and may lead to misdiagnoses. Here, we developed a microwave-assisted filter-aided sample preparation (maFASP method that can efficiently remove contaminants with a 10-kDa cutoff ultrafiltration unit and can accelerate the digestion process with the assistance of a microwave. Additionally, two parameters (P- and D-scores based on the exponentially modified protein abundance index were developed to define the existence of amyloid deposits and those causative proteins with the greatest abundance. Using our protocol, twenty cases of systemic amyloidosis that were well-typed according to clinical diagnostic standards (training group and another twenty-four cases without subtype diagnoses (validation group were analyzed. Using this approach, sample preparation could be completed within four hours. We successfully subtyped 100% of the cases in the training group, and the diagnostic success rate in the validation group was 91.7%. This maFASP-aided proteomic protocol represents an efficient approach for amyloid diagnosis and subtyping, particularly for serum-contaminated samples.

The Successful Diagnosis and Typing of Systemic Amyloidosis Using A Microwave-Assisted Filter-Aided Fast Sample Preparation Method and LC/MS/MS Analysis.

Science.gov (United States)

Sun, Weiyi; Sun, Jian; Zou, Lili; Shen, Kaini; Zhong, Dingrong; Zhou, Daobin; Sun, Wei; Li, Jian

2015-01-01

Laser microdissection followed by mass spectrometry has been successfully used for amyloid typing. However, sample contamination can interfere with proteomic analysis, and overnight digestion limits the analytical throughput. Moreover, current quantitative analysis methods are based on the spectrum count, which ignores differences in protein length and may lead to misdiagnoses. Here, we developed a microwave-assisted filter-aided sample preparation (maFASP) method that can efficiently remove contaminants with a 10-kDa cutoff ultrafiltration unit and can accelerate the digestion process with the assistance of a microwave. Additionally, two parameters (P- and D-scores) based on the exponentially modified protein abundance index were developed to define the existence of amyloid deposits and those causative proteins with the greatest abundance. Using our protocol, twenty cases of systemic amyloidosis that were well-typed according to clinical diagnostic standards (training group) and another twenty-four cases without subtype diagnoses (validation group) were analyzed. Using this approach, sample preparation could be completed within four hours. We successfully subtyped 100% of the cases in the training group, and the diagnostic success rate in the validation group was 91.7%. This maFASP-aided proteomic protocol represents an efficient approach for amyloid diagnosis and subtyping, particularly for serum-contaminated samples.

Regulatory requirements and quality assurance of radiation monitoring instruments

International Nuclear Information System (INIS)

Narasimharao, K.L.; Sharma, Ranjit

2005-01-01

The successful utilisation of radiation sources in the fields of medicine and industry requires the accurate measurement of activity, exposure rate and dose. Many varieties of instruments are in use for measurement of these parameters and new ones are being developed. The criteria for the design of the radiation monitoring instrument include the type and intensity of the radiation, purpose of measurement and ruggedness of the instrument. Quality and reliability of radiation monitoring instruments ensure that individuals are adequately protected. Accuracy, response time and ruggedness are required to be as per the approved/ prescribed guidelines. Regulatory authorities outline the design and performance criteria for radiation monitoring instruments and prescribe the recommendations of international agencies such as IAEA, ICRU and ISO for radiological measurement assurance programme. National Standards Laboratories all over the world prescribe procedures for calibration of various radiation monitoring instruments. The instruments should be calibrated as per these guidelines and should be traceable to national standards. The calibration traceable to national/ international standards and documentation as well as limits stipulated by the competent authority ensures the expected performance of the instrument. (author)

Psychometric Validation of the Parental Bonding Instrument in a U.K. Population-Based Sample: Role of Gender and Association With Mental Health in Mid-Late Life.

Science.gov (United States)

Xu, Man K; Morin, Alexandre J S; Marsh, Herbert W; Richards, Marcus; Jones, Peter B

2016-08-01

The factorial structure of the Parental Bonding Instrument (PBI) has been frequently studied in diverse samples but no study has examined its psychometric properties from large, population-based samples. In particular, important questions have not been addressed such as the measurement invariance properties across parental and offspring gender. We evaluated the PBI based on responses from a large, representative population-based sample, using an exploratory structural equation modeling method appropriate for categorical data. Analysis revealed a three-factor structure representing "care," "overprotection," and "autonomy" parenting styles. In terms of psychometric measurement validity, our results supported the complete invariance of the PBI ratings across sons and daughters for their mothers and fathers. The PBI ratings were also robust in relation to personality and mental health status. In terms of predictive value, paternal care showed a protective effect on mental health at age 43 in sons. The PBI is a sound instrument for capturing perceived parenting styles, and is predictive of mental health in middle adulthood. © The Author(s) 2016.

Design and Implementation of Data Collection Instruments for Neonatology Research

Directory of Open Access Journals (Sweden)

Monica G. HĂŞMĂŞANU

2014-12-01

Full Text Available im: The aim of our research was to design and implement data collection instruments to be use in context of an observational prospective clinical study with follow-up conducted on new born with intrauterine growth restriction. Methods: The structure of the data collection forms (paper based and electronic based was first identified and for each variable the best type to accomplish the research aim was established. The code for categorical variables has also been decided as well as the units of measurements for quantitative variables. In respect of good practice, a set of confounding factors (as gender, date of birth, etc. have also been identified and integrated in data collection instruments. Data-entry validation rules were implemented for each variable to reduce data input errors when the electronic data collection instrument was created. Results: Two data collection instruments have been developed and successfully implemented: a paper-based form and an electronic data collection instrument. The developed forms included demographics, neonatal complications (as hypoglycemia, hypocalcemia, etc., biochemical data at birth and follow-up, immunological data, as well as basal and follow-up echocardiographic data. Data-entry validation criteria have been implemented in electronic data collection instrument to assure validity and precision when paper-based data are translated in electronic form. Furthermore, to assure subject’s confidentiality a careful attention was given to HIPPA identifiers when electronic data collection instrument was developed. Conclusion: Data collection instruments were successfully developed and implemented as an a priori step in a clinical research for assisting data collection and management in a case of an observational prospective study with follow-up visits.

Social-philosophical practices of success

Directory of Open Access Journals (Sweden)

S. R. Karpenko

2017-01-01

Is social-philosophical experts of success represent the complicated system of various world outlook, speech, mental factors and events in life of the various professional, age and subcultural bunches producing assessments under different visual angles, from positions of various social installations and identity in what the social philosophy of success expresses. In the course of forming social an expert (both in daily, and in an institutional discourse are shaped also theoretical ideas success: instrumental, is social-philosophical, is social-psychological, world outlook, historical and cultural, etc., characterising thereby various systems of a social discourse. Examination is social-philosophical the success expert shows the real complexity and ambiguity of the given appearance. Besides the presented typology constructed as the most approximate abstract plan, in each separate case probably build-up of typological models according to a principle ad hoc. It looks quite justified, considering that circumstance that representations about success and the successful person are constantly transformed and acquire new performances. Efficiency of the further examinations of a discourse and a success expert will depend on accepting of new heuristic approaches, capable to consider multidimensionality and ambiguity of the given phenomenon.

How Musical Instrumentation Affects Perceptual Identification of Musical Genres

OpenAIRE

Brene, Sofia; Thome, Carl

2014-01-01

A listening experiment was conducted to investigate which musical instruments are the most important for defining certain musical genres. 66 participants genre classified a series of audio samples, with the same songs recurring both with full instrumentation and partial instrumentation. The report used the collected genre classifications to clarify therelationship between certain musical genres and song instrumentation. A numericalanalysis of the classifications, in the context of genre tradi...

Sampling and analytical methodologies for instrumental neutron activation analysis of airborne particulate matter

International Nuclear Information System (INIS)

1992-01-01

The IAEA supports a number of projects having to do with the analysis of airborne particulate matter by nuclear techniques. Most of this work involves the use of activation analysis in its various forms, particularly instrumental neutron activation analysis (INAA). This technique has been widely used in many different countries for the analysis of airborne particulate matter, and there are already many publications in scientific journals, books and reports describing such work. The present document represents an attempt to summarize the most important features of INAA as applied to the analysis of airborne particulate matter. It is intended to serve as a set of guidelines for use by participants in the IAEA's own programmes, and other scientists, who are not yet fully experienced in the application of INAA to airborne particulate samples, and who wish either to make a start on using this technique or to improve their existing procedures. The methodologies for sampling described in this document are of rather general applicability, although they are presented here in a way that takes account of the particular requirements arising from the use of INAA as the analytical technique. The analytical part of the document, however, is presented in a form that is applicable only to INAA. (Subsequent publications in this series are expected to deal specifically with other nuclear related techniques such as energy dispersive X ray fluorescence (ED-XRF) and particle induced X ray emission (PIXE) analysis). Although the methods and procedures described here have been found through experience to yield acceptable results, they should not be considered mandatory. Any other procedure used should, however, be chosen to be capable of yielding results at least of equal quality to those described

Sampling and analytical methodologies for instrumental neutron activation analysis of airborne particulate matter

Energy Technology Data Exchange (ETDEWEB)

NONE

1992-12-01

The IAEA supports a number of projects having to do with the analysis of airborne particulate matter by nuclear techniques. Most of this work involves the use of activation analysis in its various forms, particularly instrumental neutron activation analysis (INAA). This technique has been widely used in many different countries for the analysis of airborne particulate matter, and there are already many publications in scientific journals, books and reports describing such work. The present document represents an attempt to summarize the most important features of INAA as applied to the analysis of airborne particulate matter. It is intended to serve as a set of guidelines for use by participants in the IAEA's own programmes, and other scientists, who are not yet fully experienced in the application of INAA to airborne particulate samples, and who wish either to make a start on using this technique or to improve their existing procedures. The methodologies for sampling described in this document are of rather general applicability, although they are presented here in a way that takes account of the particular requirements arising from the use of INAA as the analytical technique. The analytical part of the document, however, is presented in a form that is applicable only to INAA. (Subsequent publications in this series are expected to deal specifically with other nuclear related techniques such as energy dispersive X ray fluorescence (ED-XRF) and particle induced X ray emission (PIXE) analysis). Although the methods and procedures described here have been found through experience to yield acceptable results, they should not be considered mandatory. Any other procedure used should, however, be chosen to be capable of yielding results at least of equal quality to those described.

Determination of concentrations of chromium and other elements in soil and plant samples from leather tanning area by Instrumental Neutron Activation Analysis

International Nuclear Information System (INIS)

Rohit Kumar; Rai, A.K.; Alamelu, D.; Acharya, R.

2014-01-01

Chromium, one of the toxic elements, along with other elements has been determined in samples of soil and plant (leaves and seeds) from Jajmau Area, Kanpur district, India, which is irrigated with effluent waste water from leather tanning industries. Soil and plant samples were collected from these areas and analyzed by Instrumental Neutron Activation Analysis (INAA) using high flux reactor neutrons and high resolution gamma-ray spectrometry. Concentrations of fifteen elements in soil and five elements in plant samples were determined by relative method. Chromium concentrations were found to be in range of 45-3,900 mg kg -1 in soil samples and 14-83 mg kg -1 in plant samples. This study showed that Cr is present in significant amounts, in the soil as well as in the plant samples, near to the leather tanning area. As a part of quality control work, IAEA reference material (RM) SL-3 and NIST standard reference material (SRM) 1645 were analyzed and the quality of the results has been evaluated by calculating % deviations from recommended/literature/certified values. (author)

Musical instruments in the 21st century identities, configurations, practices

CERN Document Server

Campo, Alberto; Egermann, Hauke; Hardjowirogo, Sarah-Indriyati; Weinzierl, Stefan

2017-01-01

By exploring the many different types and forms of contemporary musical instruments, this book contributes to a better understanding of the conditions of instrumentality in the 21st century. Providing insights from science, humanities and the arts, authors from a wide range of disciplines discuss the following questions: · What are the conditions under which an object is recognized as a musical instrument? · What are the actions and procedures typically associated with musical instruments? · What kind of (mental and physical) knowledge do we access in order to recognize or use something as a musical instrument? · How is this knowledge being shaped by cultural conventions and temporal conditions? · How do algorithmic processes 'change the game' of musical performance, and as a result, how do they affect notions of instrumentality? · How do we address the question of instrumental identity within an instrument's design process? · What properties can be used to differentiate successful and unsuccessful ins...

Evolved Gas Analyses of the Murray Formation in Gale Crater, Mars: Results of the Curiosity Rover's Sample Analysis at Mars (SAM) Instrument

Science.gov (United States)

Sutter, B.; McAdam, A. C.; Rampe, E. B.; Thompson, L. M.; Ming, D. W.; Mahaffy, P. R.; Navarro-Gonzalez, R.; Stern, J. C.; Eigenbrode, J. L.; Archer, P. D.

2017-01-01

The Sample Analysis at Mars (SAM) instrument aboard the Mars Science Laboratory rover has analyzed 13 samples from Gale Crater. All SAM-evolved gas analyses have yielded a multitude of volatiles (e.g., H2O, SO2, H2S, CO2, CO, NO, O2, HCl) [1- 6]. The objectives of this work are to 1) Characterize recent evolved SO2, CO2, O2, and NO gas traces of the Murray formation mudstone, 2) Constrain sediment mineralogy/composition based on SAM evolved gas analysis (SAM-EGA), and 3) Discuss the implications of these results relative to understanding the geological history of Gale Crater.

'Intelligent' approach to radioimmunoassay sample counting employing a microprocessor controlled sample counter

International Nuclear Information System (INIS)

Ekins, R.P.; Sufi, S.; Malan, P.G.

1977-01-01

The enormous impact on medical science in the last two decades of microanalytical techniques employing radioisotopic labels has, in turn, generated a large demand for automatic radioisotopic sample counters. Such instruments frequently comprise the most important item of capital equipment required in the use of radioimmunoassay and related techniques and often form a principle bottleneck in the flow of samples through a busy laboratory. It is therefore particularly imperitive that such instruments should be used 'intelligently' and in an optimal fashion to avoid both the very large capital expenditure involved in the unnecessary proliferation of instruments and the time delays arising from their sub-optimal use. The majority of the current generation of radioactive sample counters nevertheless rely on primitive control mechanisms based on a simplistic statistical theory of radioactive sample counting which preclude their efficient and rational use. The fundamental principle upon which this approach is based is that it is useless to continue counting a radioactive sample for a time longer than that required to yield a significant increase in precision of the measurement. Thus, since substantial experimental errors occur during sample preparation, these errors should be assessed and must be releted to the counting errors for that sample. It is the objective of this presentation to demonstrate that the combination of a realistic statistical assessment of radioactive sample measurement, together with the more sophisticated control mechanisms that modern microprocessor technology make possible, may often enable savings in counter usage of the order of 5-10 fold to be made. (orig.) [de

Subnanogram proteomics: Impact of LC column selection, MS instrumentation and data analysis strategy on proteome coverage for trace samples

Energy Technology Data Exchange (ETDEWEB)

Zhu, Ying; Zhao, Rui; Piehowski, Paul D.; Moore, Ronald J.; Lim, Sujung; Orphan, Victoria J.; Paša-Tolić, Ljiljana; Qian, Wei-Jun; Smith, Richard D.; Kelly, Ryan T.

2018-04-01

One of the greatest challenges for mass spectrometry (MS)-based proteomics is the limited ability to analyze small samples. Here we investigate the relative contributions of liquid chromatography (LC), MS instrumentation and data analysis methods with the aim of improving proteome coverage for sample sizes ranging from 0.5 ng to 50 ng. We show that the LC separations utilizing 30-µm-i.d. columns increase signal intensity by >3-fold relative to those using 75-µm-i.d. columns, leading to 32% increase in peptide identifications. The Orbitrap Fusion Lumos mass spectrometer significantly boosted both sensitivity and sequencing speed relative to earlier generation Orbitraps (e.g., LTQ-Orbitrap), leading to a ~3× increase in peptide identifications and 1.7× increase in identified protein groups for 2 ng tryptic digests of bacterial lysate. The Match Between Runs algorithm of open-source MaxQuant software further increased proteome coverage by ~ 95% for 0.5 ng samples and by ~42% for 2 ng samples. The present platform is capable of identifying >3000 protein groups from tryptic digestion of cell lysates equivalent to 50 HeLa cells and 100 THP-1 cells (~10 ng total proteins), respectively, and >950 proteins from subnanogram bacterial and archaeal cell lysates. The present ultrasensitive LC-MS platform is expected to enable deep proteome coverage for subnanogram samples, including single mammalian cells.

Sample positioning effects in x-ray spectrometry

International Nuclear Information System (INIS)

Carpenter, D.

Instrument error due to variation in sample position in a crystal x-ray spectrometer can easily exceed the total instrumental error. Lack of reproducibility in sample position in the x-ray optics is the single largest source of system error. The factors that account for sample positioning error are described, and many of the details of flat crystal x-ray optics are discussed

Instrumental activation analysis of molybdenites

International Nuclear Information System (INIS)

Geisler, M.; Schelhorn, H.

1981-01-01

Na, K, Sc, Cr, Fe, Co, Se, Rb, Ag, Cs, Ba, La, Ce, Eu, Yb, Hf, W, Re, and Th have been determined in 6 molybdenite samples by instrumental activation analysis. The samples were of different origin and showed K, Sc, W, and Re values with differences of more than two orders of magnitude, whereas Sc values were within one order of magnitude

Quantification and handling of sampling errors in instrumental measurements: a case study

DEFF Research Database (Denmark)

Andersen, Charlotte Møller; Bro, R.

2004-01-01

in certain situations, the effect of systematic errors is also considerable. The relevant errors contributing to the prediction error are: error in instrumental measurements (x-error), error in reference measurements (y-error), error in the estimated calibration model (regression coefficient error) and model...

Novel seismic instrumentation for nuclear power plants

International Nuclear Information System (INIS)

Bolleter, W.; Savary, C.

1998-01-01

Conforming to the latest issues of the Nuclear Regulatory Commission Regulatory Guide, a novel hardware and software solution for seismic instrumentation is presented. Both instrumentation and PC-based data evaluation software for post-earthquake actions are type-tested and approved by the German TUeV. Reference installations replacing obsolete analog instrumentation were successfully completed and are presented. The instrumentation consists of highly linear, solid-state capacitive accelerometers as well as digital recorders storing the signals from the sensors in situ. These recorders are linked in a star-topology network to a central unit that permanently communicates with them via fiber-optic cable or current-loop links. The central unit is responsible for alerting and synchronizes all recorders which otherwise act autonomously. Data evaluation is handled by a PC-based software package. It includes automatic data evaluation after earthquakes (batch mode), interactive data evaluation software for detailed data analysis, and software tools for remote operation, maintenance and data storage. (author)

Microfluidic Apps for off-the-shelf instruments.

Science.gov (United States)

Mark, Daniel; von Stetten, Felix; Zengerle, Roland

2012-07-21

Within the last decade a huge increase in research activity in microfluidics could be observed. However, despite several commercial success stories, microfluidic chips are still not sold in high numbers in mass markets so far. Here we promote a new concept that could be an alternative approach to commercialization: designing microfluidic chips for existing off-the-shelf instruments. Such "Microfluidic Apps" could significantly lower market entry barriers and provide many advantages: developers of microfluidic chips make use of existing equipment or platforms and do not have to develop instruments from scratch; end-users can profit from microfluidics without the need to invest in new equipment; instrument manufacturers benefit from an expanded customer base due to the new applications that can be implemented in their instruments. Microfluidic Apps could be considered as low-cost disposables which can easily be distributed globally via web-shops. Therefore they could be a door-opener for high-volume mass markets.

Use of the Aromascan(TM) Instrument for Nonsubjective Evaluation of Rodent Spaceflight Hardware

Science.gov (United States)

Scribner, K. A.; Steele, M. K.; Hinds, W. E.; Dalton, Bonnie P. (Technical Monitor)

1997-01-01

This report describes the verification and utilization of the AromaScan(TM) (Hollis, NH) instrument for the ground-based evaluation of odor containment by various spaceflight habitats developed at NASA's Ames Research Center (ARC). The AromaScan(TM) instrument is an electronic odor detection system consisting of 32 polymer sensors that respond differentially to 10 different chemical groups present in an air sample. The AromaScan(TM) system also includes neural network software for constructing a database of known odors, against which an unknown odor can be compared. At present, the standard method for characterizing rodent odor containment during the development and testing of spaceflight hardware is the use of a human odor assessment panel. However, this can be a very time consuming and costly process, and the results are inherently subjective. The AromaScan(TM) system should produce more consistent and objective results, as well as a cost savings in the long term. To test and verify the AromaScan(TM) instrument, daily air samples will be collected from the exhaust port of rodent habitats, during experiment development tests, then injected into the instrument and used to create a database of recognizable odors. Human sniff tests will be performed in conjunction with the AromaScan(TM) analysis, and the results will be correlated. We will then teach the neural network to differentiate between an acceptable and an unacceptable odor profile, as defined by the human sniff test, and to be able to accurately identify an odor that would not pass a sniff panel. The results of our efforts will be to verify that the AromaScan(TM) system is a valuable alternative to human sniff panel assessments for the early iterative process of designing and testing rodent waste filters for spaceflight. Acceptance by a human panel will remain one of the final criteria for successful rodent habitat development.

A measurement instrument for bone mineral content of adult and children

International Nuclear Information System (INIS)

Liu Shaofang

1996-01-01

The γ radiation source was used in bone mineral content measurement analysis of adult and children and a new instrument is developed successfully. It's precision is +2%. The advantage of this instrument is light, cheap and reliable. It can be used widely in medical science and clinic for diagnosis on certain diseases and research work

Evaluating manta ray mucus as an alternative DNA source for population genetics study: underwater-sampling, dry-storage and PCR success

Directory of Open Access Journals (Sweden)

Tom Kashiwagi

2015-08-01

Full Text Available Sharks and rays are increasingly being identified as high-risk species for extinction, prompting urgent assessments of their local or regional populations. Advanced genetic analyses can contribute relevant information on effective population size and connectivity among populations although acquiring sufficient regional sample sizes can be challenging. DNA is typically amplified from tissue samples which are collected by hand spears with modified biopsy punch tips. This technique is not always popular due mainly to a perception that invasive sampling might harm the rays, change their behaviour, or have a negative impact on tourism. To explore alternative methods, we evaluated the yields and PCR success of DNA template prepared from the manta ray mucus collected underwater and captured and stored on a Whatman FTA™ Elute card. The pilot study demonstrated that mucus can be effectively collected underwater using toothbrush. DNA stored on cards was found to be reliable for PCR-based population genetics studies. We successfully amplified mtDNA ND5, nuclear DNA RAG1, and microsatellite loci for all samples and confirmed sequences and genotypes being those of target species. As the yields of DNA with the tested method were low, further improvements are desirable for assays that may require larger amounts of DNA, such as population genomic studies using emerging next-gen sequencing.

[Treatment of a fractured endodontical instrument in the root canal].

Science.gov (United States)

Schipper, M; Peters, L B

2015-12-01

A 53-year-old woman with continuing pain coming from a lower first molar was diagnosed with apical periodontitis, with a retained fractured instrument in the root canal. There are a variety of treatment options for dealing with a corpus alienum in a root canal. In this case it was decided to treat the tooth endodontically, and leave the fractured instrument fragment in situ. The selection of this treatment option was made on the basis of knowledge of the original diagnosis and the success rates of the various treatment options as described in the relevant literature, weighed against the possible risks and their effects on the prognosis. This suggested that the use of a dental operating microscope has a positive impact on the success rates of endodontic treatment The prognosis for endodontic treatment when a fractured instrument fragment is left within the root canal, as in this case, is not significantly reduced. The presence of preoperative periapical pathology, however, is a more clinically significant prognostic indicator.

Subsurface Sampling and Sensing Using Burrowing Moles

Science.gov (United States)

Stoker, C. R.; Richter, L.; Smith, W. H.

2004-01-01

Finding evidence for life on Mars will likely require accessing the subsurface since the Martian surface is both hostile to life and to preservation of biosignatures due to the cold dry conditions, the strong W environment, and the presence of strong oxidants. Systems are needed to probe beneath the sun and oxidant baked surface of Mars and return samples to the surface for analysis or to bring the instrument sensing underground. Recognizing this need, the European Space Agency incorporated a small subsurface penetrometer or Mole onto the Beagle 2 Mars lander. Had the 2003 landing been successful, the Mole would have collected samples from 1-1.5 m depth and delivered them to an organic analysis instrument on the surface. The de- vice called the Planetary Underground Tool (PLUTO), also measured soil mechanical and thermophysical properties. Constrained by the small mass and volume allowance of the Beagle lander, the PLUTO mole was a slender cylinder only 2 cm diameter and 28 cm long equipped with a small sampling device designed to collect samples and bring them to the surface for analysis by other instrument. The mass of the entire system including deployment mechanism and tether was 1/2 kg. sensor package underground to make in situ measurements. The Mars Underground Mole (MUM) is a larger Mole based on the PLUTO design but incorporating light collection optics that interface to a fiber optic cable in the tether that transmits light to a combined stimulated emission Raman Spectrometer and Short Wave Infrared (SWIR) reflectance Spectrometer with sensitivity from 0.7 to 2.5 micrometers. This instrument is called the Dual Spectral Sensor and uses a Digital Array Scanning Interferometer as the sensor technology, a type of fourier transform interferometer that uses fixed element prisms and thus is highly rugged compared to a Michaelson interferometer. Due to the size limitations of an on-Mole instrument compartment, and the availability of a tether, the sensor head

Year 2000 experience with safeguards instruments

International Nuclear Information System (INIS)

Coffing, J.

1999-01-01

Presentation covers the following items concerning the experiences with safeguards instruments related to Y2K issues: initial Y2K evaluation process; improvement of Y2K testing procedure, policy of the Aquila Technologies Group, Inc. The results concerning Y2K evaluation are presented as designed in the manufacturing process in order to assure success

A Method for Choosing the Best Samples for Mars Sample Return.

Science.gov (United States)

Gordon, Peter R; Sephton, Mark A

2018-05-01

Success of a future Mars Sample Return mission will depend on the correct choice of samples. Pyrolysis-FTIR can be employed as a triage instrument for Mars Sample Return. The technique can thermally dissociate minerals and organic matter for detection. Identification of certain mineral types can determine the habitability of the depositional environment, past or present, while detection of organic matter may suggest past or present habitation. In Mars' history, the Theiikian era represents an attractive target for life search missions and the acquisition of samples. The acidic and increasingly dry Theiikian may have been habitable and followed a lengthy neutral and wet period in Mars' history during which life could have originated and proliferated to achieve relatively abundant levels of biomass with a wide distribution. Moreover, the sulfate minerals produced in the Theiikian are also known to be good preservers of organic matter. We have used pyrolysis-FTIR and samples from a Mars analog ferrous acid stream with a thriving ecosystem to test the triage concept. Pyrolysis-FTIR identified those samples with the greatest probability of habitability and habitation. A three-tier scoring system was developed based on the detection of (i) organic signals, (ii) carbon dioxide and water, and (iii) sulfur dioxide. The presence of each component was given a score of A, B, or C depending on whether the substance had been detected, tentatively detected, or not detected, respectively. Single-step (for greatest possible sensitivity) or multistep (for more diagnostic data) pyrolysis-FTIR methods informed the assignments. The system allowed the highest-priority samples to be categorized as AAA (or A*AA if the organic signal was complex), while the lowest-priority samples could be categorized as CCC. Our methods provide a mechanism with which to rank samples and identify those that should take the highest priority for return to Earth during a Mars Sample Return mission. Key Words

DEVELOPMENT OF AN ON-LINE, REAL-TIME ALPHA RADIATION MEASURING INSTRUMENT FOR LIQUID STREAMS

International Nuclear Information System (INIS)

Unknown

1999-01-01

Thermo Power Corporation has proven the technical viability of an on-line, real-time alpha radionuclide instrument for aqueous sample analysis through laboratory and initial field tests of the instrument. The instrument has been shown to be isotonically sensitive to extremely low (ten parts per trillion, or femto Curies per liter) levels of a broad range of radioisotopes. Performance enhancement and other scaling data obtained during the course of this investigation have shown that on-line, real-time operation is possible, with a sub 30-minute response time analyzing 20 ppb (30 pCi/1) natural uranium. Now that these initial field tests in Oak Ridge, Tennessee have been successfully completed, Thermo Power plans to conduct comprehensive field tests of the instrument. The purpose of these endurance tests will be to determine the endurance characteristics of the Thermo Alpha Monitor for Water when it is used by non-Thermo Power personnel in a series of one or more extended field tests. Such endurance testing is the vital next step towards the commercialization of the Alpha Monitor. Subsequently, it will be possible to provide the DOE with an instrument that has the capability of obtaining rapid feedback about the concentrations of alpha-emitting isotope contamination in effluent water streams (Subsurface Contaminants Focus Area). It will also be useful for process control of remediation and D and D operations such as monitoring scrubber/rinse water radioactivity levels (Mixed Waste, Plutonium and D and D Focus Areas)

University of Houston Undergraduate Student Instrumentation Projects

Science.gov (United States)

Bering, E. A., III; Talbot, R. W.; Hampton, D. L.; Molders, N.; Millan, R. M.; Halford, A. J.; Dunbar, B.; Morris, G. A.; Prince, J.; Gamblin, R.; Ehteshami, A.; Lehnen, J. N.; Greer, M.; Porat, I.; Alozie, M.; Behrend, C. C.; Bias, C.; Fenton, A.; Gunawan, B.; Harrison, W.; Martinez, A.; Mathur, S.; Medillin, M.; Nguyen, T.; Nguyen, T. V.; Nowling, M.; Perez, D.; Pham, M.; Pina, M.; Thomas, G.; Velasquez, B.; Victor, L.

2017-12-01

The Undergraduate Student Instrumentation Project (USIP) is a NASA program to engage undergraduate students in rigorous scientific research, for the purposes of innovation and developing the next generation of professionals for an array of fields. The program is student led and executed from initial ideation to research to the design and deployment of scientific payloads. The University of Houston has been selected twice to participate in the USIP programs. The first program (USIP_UH I) ran from 2013 to 2016. USIP_UH II started in January of 2016, with funding starting at the end of May. USIP_UH I (USIP_UH II) at the University of Houston was (is) composed of eight (seven) research teams developing six (seven), distinct, balloon-based scientific instruments. These instruments will contribute to a broad range of geophysical sciences from Very Low Frequency recording and Total Electron Content to exobiology and ozone profiling. USIP_UH I had 12 successful launches with 9 recoveries from Fairbanks, AK in March 2015, and 4 piggyback flights with BARREL 3 from Esrange, Kiruna, Sweden in August, 2015. USIP_UH II had 8 successful launches with 5 recoveries from Fairbanks, AK in March 2017, 3 piggyback flights with BARREL 4 from Esrange, Kiruna, Sweden in August, 2016, and 1 flight each from CSBF and UH. The great opportunity of this program is capitalizing on the proliferation of electronics miniaturization to create new generations of scientific instruments that are smaller and lighter than ever before. This situation allows experiments to be done more cheaply which ultimately allows many more experiments to be done.

Instrumentation for chemical and radiochemical monitoring in nuclear power plants

International Nuclear Information System (INIS)

Nordmann, F.; Ballard, G.

2009-01-01

This article details the instrumentation implemented in French nuclear power plants for the monitoring of chemical and radiochemical effluents with the aim of limiting their environmental impact. It describes the controls performed with chemical automata for the search for drifts, anomalies or pollution in a given circuit. The operation principles of the different types of chemical automata are explained as well as the manual controls performed on samples manually collected. Content: 1 - general considerations; 2 - objectives of the chemical monitoring: usefulness of continuous monitoring with automata, transmission to control rooms and related actions, redundancy of automata; 3 - instrumentation and explanations for the main circuits: principle of chemical automata monitoring, instrumentation of the main primary circuit, instrumentation of the main secondary circuit, instrumentation of the tertiary circuit, preparation of water makeup (demineralized water), other loops, instrumentation for effluents and environment monitoring, measurement principles of chemical automata, control and maintenance of chemical automata; 4 - manual controls after sampling; 5 - radiochemical monitoring: automatized radiochemical measurements, manual radiochemical measurements; 6 - conclusion

Structural Model of the Effect of Psychological Capital on Success with Due to the Mediating Role of Commitment and Satisfaction

OpenAIRE

M Golparvar; Z Mirzaie

2016-01-01

This research was administered with the aim of investigating structural model of the effect of psychological capital on career success with due to the mediating role of satisfaction and commitment among employees of Telecom Company. Research statistical population was male and female employees of Telecom in Isfahan city, who among them two hundred and eighty five persons were selected using convenience sampling. Research instruments were Nguyen et al. Psychological Capital questionnaire, Nabi...

An Undergraduate Student Instrumentation Project (USIP) to Develop New Instrument Technology to Study the Auroral Ionosphere and Stratospheric Ozone Layer Using Ultralight Balloon Payloads

Science.gov (United States)

Nowling, M.; Ahmad, H.; Gamblin, R.; Guala, D.; Hermosillo, D.; Pina, M.; Marrero, E.; Canales, D. R. J.; Cao, J.; Ehteshami, A.; Bering, E. A., III; Lefer, B. L.; Dunbar, B.; Bias, C.; Shahid, S.

2015-12-01

This project is currently engaging twelve undergraduate students in the process of developing new technology and instrumentation for use in balloon borne geospace investigations in the auroral zone. Motivation stems from advances in microelectronics and consumer electronic technology. Given the technological innovations over the past 20 years it now possible to develop new instrumentation to study the auroral ionosphere and stratospheric ozone layer using ultralight balloon payloads for less than 6lbs and $3K per payload. The University of Houston Undergraduate Student Instrumentation Project (USIP) team has built ten such payloads for launch using 1500 gm latex weather balloons deployed in Houston, TX, Fairbanks, AK, and as well as zero pressure balloons launched from northern Sweden. The latex balloon project will collect vertical profiles of wind velocity, temperature, electrical conductivity, ozone, and odd nitrogen. This instrument payload will also produce profiles of pressure, electric field, and air-earth electric current. The zero pressure balloons will obtain a suite of geophysical measurements including: DC electric field, electric field and magnetic flux, optical imaging, total electron content of ionosphere via dual-channel GPS, X-ray detection, and infrared/UV spectroscopy. Students flew payloads with different combinations of these instruments to determine which packages are successful. Data collected by these instruments will be useful in understanding the nature of electrodynamic coupling in the upper atmosphere and how the global earth system is changing. Twelve out of the launched fifteen payloads were successfully launched and recovered. Results and best practices learned from lab tests and initial Houston test flights will be discussed.

Improved analytical sensitivity for uranium and plutonium in environmental samples: Cavity ion source thermal ionization mass spectrometry

International Nuclear Information System (INIS)

Ingeneri, Kristofer; Riciputi, L.

2001-01-01

Following successful field trials, environmental sampling has played a central role as a routine part of safeguards inspections since early 1996 to verify declared and to detect undeclared activity. The environmental sampling program has brought a new series of analytical challenges, and driven a need for advances in verification technology. Environmental swipe samples are often extremely low in concentration of analyte (ng level or lower), yet the need to analyze these samples accurately and precisely is vital, particularly for the detection of undeclared nuclear activities. Thermal ionization mass spectrometry (TIMS) is the standard method of determining isotope ratios of uranium and plutonium in the environmental sampling program. TIMS analysis typically employs 1-3 filaments to vaporize and ionize the sample, and the ions are mass separated and analyzed using magnetic sector instruments due to their high mass resolution and high ion transmission. However, the ionization efficiency (the ratio of material present to material actually detected) of uranium using a standard TIMS instrument is low (0.2%), even under the best conditions. Increasing ionization efficiency by even a small amount would have a dramatic impact for safeguards applications, allowing both improvements in analytical precision and a significant decrease in the amount of uranium and plutonium required for analysis, increasing the sensitivity of environmental sampling

Some comments on combusting flows and instrumentation for two-phase flows

International Nuclear Information System (INIS)

Whitelaw, J.H.

1985-01-01

Measurements of the velocity characteristics of combusting flows have been reported over the past 15 years and have Encompassed an extensive range of flows configurations. Difficulties in applying instrumentation and interpreting results are, however, still experienced and this presentation describes two experiments which are useful examples of successful applications. The first is concerned with a gas-turbine combustion chamber which involves limited optical access with high heat release but does not require measurement accuracy such as that of, for example, external aerodynamic flows. The second combines laser velocimetry with digitally compensated thermocouples to provide detailed information of a premixed, bluff-body stabilized flame and involves conditionally sampled results so as to determine the separate flow characteristics of products and reactants

Large sample NAA facility and methodology development

International Nuclear Information System (INIS)

Roth, C.; Gugiu, D.; Barbos, D.; Datcu, A.; Aioanei, L.; Dobrea, D.; Taroiu, I. E.; Bucsa, A.; Ghinescu, A.

2013-01-01

A Large Sample Neutron Activation Analysis (LSNAA) facility has been developed at the TRIGA- Annular Core Pulsed Reactor (ACPR) operated by the Institute for Nuclear Research in Pitesti, Romania. The central irradiation cavity of the ACPR core can accommodate a large irradiation device. The ACPR neutron flux characteristics are well known and spectrum adjustment techniques have been successfully applied to enhance the thermal component of the neutron flux in the central irradiation cavity. An analysis methodology was developed by using the MCNP code in order to estimate counting efficiency and correction factors for the major perturbing phenomena. Test experiments, comparison with classical instrumental neutron activation analysis (INAA) methods and international inter-comparison exercise have been performed to validate the new methodology. (authors)

Rotary mode system initial instrument calibration

International Nuclear Information System (INIS)

Johns, B.R.

1994-01-01

The attached report contains the vendor calibration procedures used for the initial instrument calibration of the rotary core sampling equipment. The procedures are from approved vendor information files

An 'intelligent' approach to radioimmunoassay sample counting employing a microprocessor-controlled sample counter

International Nuclear Information System (INIS)

Ekins, R.P.; Sufi, S.; Malan, P.G.

1978-01-01

The enormous impact on medical science in the last two decades of microanalytical techniques employing radioisotopic labels has, in turn, generated a large demand for automatic radioisotopic sample counters. Such instruments frequently comprise the most important item of capital equipment required in the use of radioimmunoassay and related techniques and often form a principle bottleneck in the flow of samples through a busy laboratory. It is therefore imperative that such instruments should be used 'intelligently' and in an optimal fashion to avoid both the very large capital expenditure involved in the unnecessary proliferation of instruments and the time delays arising from their sub-optimal use. Most of the current generation of radioactive sample counters nevertheless rely on primitive control mechanisms based on a simplistic statistical theory of radioactive sample counting which preclude their efficient and rational use. The fundamental principle upon which this approach is based is that it is useless to continue counting a radioactive sample for a time longer than that required to yield a significant increase in precision of the measurement. Thus, since substantial experimental errors occur during sample preparation, these errors should be assessed and must be related to the counting errors for that sample. The objective of the paper is to demonstrate that the combination of a realistic statistical assessment of radioactive sample measurement, together with the more sophisticated control mechanisms that modern microprocessor technology make possible, may often enable savings in counter usage of the order of 5- to 10-fold to be made. (author)

Evolved Gas Measurements Planned for the Lower Layers of the Gale Crater Mound with the Sample Analysis at Mars Instrument Suite

Science.gov (United States)

Mahaffy, P. R.; Franz, H.; McAdam, A.; Conrad, P. G.; Brunner, A.; Cabane, M.; Webster, C. R.

2011-12-01

The lower mound strata of Gale Crater provide a diverse set of chemical environments for exploration by the varied tools of the Curiosity Rover of the Mars Science Laboratory (MSL) Mission. Orbital imaging and spectroscopy clearly reveal distinct layers of hydrated minerals, sulfates, and clays with abundant evidence of a variety of fluvial processes. The three instruments of the MSL Sample Analysis at Mars (SAM) investigation, the Quadrupole Mass Spectrometer (QMS), the Tunable Laser Spectrometer (TLS), and the Gas Chromatograph (GC) are designed to analyze either atmospheric gases or volatiles thermally evolved or chemically extracted from powdered rock or soil. The presence or absence of organic compounds in these layers is of great interest since such an in situ search for this type of record has not been successfully implemented since the mid-70s Viking GCMS experiments. However, regardless of the outcome of the analysis for organics, the abundance and isotopic composition of thermally evolved inorganic compounds should also provide a rich data set to complement the mineralogical and elemental information provided by other MSL instruments. In addition, these evolved gas analysis (EGA) experiments will help test sedimentary models proposed by Malin and Edgett (2000) and then further developed by Milliken et al (2010) for Gale Crater. In the SAM EGA experiments the evolution temperatures of H2O, CO2, SO2, O2, or other simple compounds as the samples are heated in a helium stream to 1000C provides information on mineral types and their associations. The isotopic composition of O, H, C, and S can be precisely determined in several evolved compounds and compared with the present day atmosphere. Such SAM results might be able to test mineralogical evidence of changing sedimentary and alteration processes over an extended period of time. For example, Bibring et al (2006) have suggested such a major shift from early nonacidic to later acidic alteration. We will

A new time-of-flight instrument for quantitative surface analysis

International Nuclear Information System (INIS)

Veryovkin, Igor V.; Calaway, Wallis F.; Moore, Jerry F.; Pellin, Michael J.; Burnett, Donald S.

2004-01-01

A new generation of time-of-flight mass spectrometers that implement ion sputtering and laser desorption for probing solid samples and can operate in regimes of laser post-ionization secondary neutral mass spectrometry and secondary ion mass spectrometry is being developed at Argonne National Laboratory. These new instruments feature novel ion optical systems for efficient extraction of ions from large laser post-ionization volumes and for lossless transport of these ions to detectors. Another feature of this design is a new in-vacuum all-reflecting optical microscope with 0.5-μm resolution. Advanced ion and light optics and three ion sources, including a liquid metal ion gun (focusable to 50 nm) and a low energy ion gun, give rise to an instrument capable of quantitative analyses of samples for the most challenging applications, such as determining elemental concentrations in shallow implants at ultra-trace levels (for example, solar wind samples delivered by NASA Genesis mission) and analyzing individual sub-micrometer particles on a sample stage (such as, interstellar dust delivered by NASA Stardust mission). Construction of a prototype instrument has been completed and testing is underway. A more advanced instrument of similar design is under construction. The overall design of the new instrument and the innovations that make it unique are outlined. Results of the first tests to characterize its analytical capabilities are presented also

Neutron beam instruments at Harwell

International Nuclear Information System (INIS)

Baston, A.H.; Harris, D.H.C.

1978-11-01

A list and brief descriptions are given of the neutron beam facilities for U.K. scientists at Harwell and in academic institutions, available under an agreement between the Science Research Council and AERE (Harwell). The list falls under the following headings: reactor instruments (single crystal diffractometers, powder diffractometers, triple axis spectrometers, time-of-flight cold neutron twin rotor spectrometer, beryllium filter spectrometer, MARX spectrometer, Harwell small-angle scattering spectrometer); LINAC instruments (total scattering spectrometer, back scattering spectrometer, active sample spectrometer, inelastic rotor spectrometer, constant Q spectrometer); ancillary equipment (cryostats, superconducting magnets, electromagnets, furnaces). (U.K.)

Sample Preparation Report of the Fourth OPCW Confidence Building Exercise on Biomedical Sample Analysis

Energy Technology Data Exchange (ETDEWEB)

Udey, R. N. [Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States); Corzett, T. H. [Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States); Alcaraz, A. [Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States)

2014-07-03

Following the successful completion of the 3rd biomedical confidence building exercise (February 2013 – March 2013), which included the analysis of plasma and urine samples spiked at low ppb levels as part of the exercise scenario, another confidence building exercise was targeted to be conducted in 2014. In this 4th exercise, it was desired to focus specifically on the analysis of plasma samples. The scenario was designed as an investigation of an alleged use of chemical weapons where plasma samples were collected, as plasma has been reported to contain CWA adducts which remain present in the human body for several weeks (Solano et al. 2008). In the 3rd exercise most participants used the fluoride regeneration method to analyze for the presence of nerve agents in plasma samples. For the 4th biomedical exercise it was decided to evaluate the analysis of human plasma samples for the presence/absence of the VX adducts and aged adducts to blood proteins (e.g., VX-butyrylcholinesterase (BuChE) and aged BuChE adducts using a pepsin digest technique to yield nonapeptides; or equivalent). As the aging of VX-BuChE adducts is relatively slow (t1/2 = 77 hr at 37 °C [Aurbek et al. 2009]), soman (GD), which ages much more quickly (t1/2 = 9 min at 37 °C [Masson et al. 2010]), was used to simulate an aged VX sample. Additional objectives of this exercise included having laboratories assess novel OP-adducted plasma sample preparation techniques and analytical instrumentation methodologies, as well as refining/designating the reporting formats for these new techniques.

Development of quality control and instrumentation performance metrics for diffuse optical spectroscopic imaging instruments in the multi-center clinical environment

Science.gov (United States)

Keene, Samuel T.; Cerussi, Albert E.; Warren, Robert V.; Hill, Brian; Roblyer, Darren; Leproux, AnaÑ--s.; Durkin, Amanda F.; O'Sullivan, Thomas D.; Haghany, Hosain; Mantulin, William W.; Tromberg, Bruce J.

2013-03-01

Instrument equivalence and quality control are critical elements of multi-center clinical trials. We currently have five identical Diffuse Optical Spectroscopic Imaging (DOSI) instruments enrolled in the American College of Radiology Imaging Network (ACRIN, #6691) trial located at five academic clinical research sites in the US. The goal of the study is to predict the response of breast tumors to neoadjuvant chemotherapy in 60 patients. In order to reliably compare DOSI measurements across different instruments, operators and sites, we must be confident that the data quality is comparable. We require objective and reliable methods for identifying, correcting, and rejecting low quality data. To achieve this goal, we developed and tested an automated quality control algorithm that rejects data points below the instrument noise floor, improves tissue optical property recovery, and outputs a detailed data quality report. Using a new protocol for obtaining dark-noise data, we applied the algorithm to ACRIN patient data and successfully improved the quality of recovered physiological data in some cases.

Microcontroller-based system for estimate of calcium in serum samples.

Science.gov (United States)

Neelamegam, Periyaswmy; Jamaludeen, Abdul Sheriff; Ragendran, Annamalai; Murugrananthan, Krishanamoorthy

2010-01-01

In this study, a microcontroller-based control unit was designed and constructed for the estimation of serum calcium in blood samples. The proposed optoelectronic instrument used a red light emitting diode (LED) as a light source and photodiode as a sensor. The performance of the system was compared with that of a commercial instrument in measuring calcium ion. The quantitative analysis of calcium in a catalyst using arsenazo III as colorimetric reagent was used to test the device. The calibration curve for calcium binding with arsenazo III was drawn to check the range of linearity, which was between 0.1 to 4.5 mM L⁻¹. The limit of detection (LOD) is 0.05 mM L⁻¹. Absorbance changes over the pH range of 2-12 were determined to optimize the assay, with maximum absorption at pH 9.0. Interferences in absorbance from monovalent (K+ and Na+) and divalent (Mg²+) cations were also studied. The results show that the system works successfully.

Intercomparison of aerosol instruments: number concentration

International Nuclear Information System (INIS)

Knutson, E.O.; Sinclair, D.; Tu, K.W.; Hinchliffe, L.; Franklin, H.

1982-05-01

An intercomparison of aerosol instruments conducted February 23-27, 1981, at the Environmental Measurements Laboratory (EML) focused on five instruments: the Pollak and TSI condensation nucleus counters; the Active Scattering Aerosol Spectrometer (ASAS-X); and two aerosol electrometers. Test aerosols of sodium chloride and ammonium fluorescein generated by nebulization/electrostatic classification were used to obtain 195 lines of comparison data. Concentrations measured by the ASAS-X and the TSI aerosol electrometer averaged respectively 1.388 and 1.581 times that measured by the Pollak. These ratios were very stable during the week and there was little effect of particle size or material. Most other comparisons were equally stable. However, a review of past work at EML and elsewhere led to the disturbing conclusion that these ratios may change from year to year, or from season to season. A filter sample was taken from microscopy, concurrent with readings from the ASAS-X and the TSI condensation nucleus counters. In this sample, the two instruments differed by 20%. Within its 20% uncertainty, the filter result matched both the TSI and ASAS-X readings

Waste minimization methods for treating analytical instrumentation effluents at the source

International Nuclear Information System (INIS)

Ritter, J.A.; Barnhart, C.

1995-01-01

The primary goal of this project was to reduce the amount of hazardous waste being generated by the Savannah River Siste Defense Waste Processing Technology-analytical Laboratory (DWPT-AL). A detailed characterization study was performed on 12 of the liquid effluent streams generated within the DWPT-AL. Two of the streams were not hazardous, and are now being collected separately from the 10 hazardous streams. A secondary goal of the project was to develop in-line methods using primarily adsorption/ion exchange columns to treat liquid effluent as it emerges from the analytical instrument as a slow, dripping flow. Samples from the 10 hazardous streams were treated by adsorption in an experimental apparatus that resembled an in-line or at source column apparatus. The layered adsorbent bed contained activated carbon and ion exchange resin. The column technique did not work on the first three samples of the spectroscopy waste stream, but worked well on the next three samples which were treated in a different column. It was determined that an unusual form of mercury was present in the first three samples. Similarly, two samples of a combined waste stream were rendered nonhazardous, but the last two samples contained acetylnitrile that prevented analysis. The characteristics of these streams changed from the initial characterization study; therefore, continual, in-deptch stream characterization is the key to making this project successful

W-026, health physics instrumentation operational test report

International Nuclear Information System (INIS)

Hackworth, M.F.

1998-01-01

This report documents the testing of the Health Physics Instrumentation associated with phase 2 and 3 start-up of Project W-026, WRAP. The Health Physics Instrumentation includes: Alpha and Beta Continuous Air Monitors (CAMS), Personnel Contamination Monitors (PCMs), Gamma Area Radiation Monitors (ARMs), Criticality Monitors, Alpha and Beta Smear Sample Counters, Portable Friskers, and Operator Breathing Zone Air Samplers. This OTR will cover only the Health Physics Instrumentation that was tested under the Operational test Plan for Health Physics Instrumentation (Phase 2 and 3). That instrumentation included: Alpha CAMS, Beta CAMs and ARMs located in rooms 107 and 113 of 2336-W. The remaining Health Physics Instrumentation that will be used for phase 2 and 3 start-up is tested during calibrations. These calibrations are outside the scope of the Operational Test Plan

Effect of Instrumentation Techniques, Irrigant Solutions and Artificial accelerated Aging on Fiberglass Post Bond Strength to Intraradicular Dentin.

Science.gov (United States)

Santana, Fernanda Ribeiro; Soares, Carlos José; Silva, Júlio Almeida; Alencar, Ana Helena Gonçalves; Renovato, Sara Rodrigues; Lopes, Lawrence Gonzaga; Estrela, Carlos

2015-07-01

To evaluate the effect of instrumentation techniques, irrigant solutions and specimen aging on fiberglass posts bond strength to intraradicular dentine. A total of 120 bovine teeth were prepared and randomized into control and experimental groups resulting from three study factors (instrumentation techniques, irrigant solutions, specimen aging). Posts were cemented with RelyX U100. Samples were submitted to push-out test and failure mode was evaluated under a confocal microscope. In specimens submitted to water artificial aging, nickel-titanium rotary instruments group presented higher bond strength values in apical third irrigated with NaOCl or chlorhexi-dine. Irrigation with NaOCl resulted in higher bond strength than ozonated water. Artificial aging resulted in significant bond strength increase. Adhesive cement-dentin failure was prevalent in all the groups. Root canal preparation with NiTi instruments associated with NaOCl irrigation and ethylenediaminetetra acetic acid (EDTA) increased bond strength of fiberglass posts cemented with self-adhesive resin cement to intraradicular dentine. Water artificial aging significantly increased post-Clinical significance: The understanding of factors that may influence the optimal bond between post-cement and cement-dentin are essential to the success of endodontically treated tooth restoration.

Instrumental neutron activation analysis of environmental samples from a region with prevalence of population disabilities in the North Gondar, Ethiopia

International Nuclear Information System (INIS)

Bitewlign, T.A.; Addis Ababa University, Addis Ababa; Chaubey, A.K.; Beyene, G.A.; Melikegnaw, T.H.; Mizera, Jiri; Czech Academy of Sciences, Prague; Kamenik, Jan; Krausova, Ivana; Kucera, Jan

2017-01-01

Instrumental neutron activation analysis (INAA) of soil, coal, water, and crops from the village of Awdarda in the North Gondar, Ethiopia, where the residents suffer from various disabilities, was performed in an attempt to elucidate the existing health problems. More than forty elements were determined in the samples analyzed. Comparison of our results with literature values indicates highly elevated contents of terrigenous elements in Awdarda cereals, possibly due to contamination by excavation and indoor combustion of local coal-bearing sediments. Impact is discussed of the elevated aluminium and the rare earth elements levels in crops on the health problems. (author)

Study of phosphors determination in biological samples

International Nuclear Information System (INIS)

Oliveira, Rosangela Magda de.

1994-01-01

In this paper, phosphors determination by neutron activation analysis in milk and bone samples was studied employing both instrumental and radiochemical separation methods. The analysis with radiochemistry separation consisted of the simultaneous irradiation of the samples and standards during 30 minutes, dissolution of the samples, hold back carrier, addition precipitation of phosphorus with ammonium phosphomolibdate (A.M.P.) and phosphorus-32 by counting by using Geiger-Mueller detector. The instrumental analysis consisted of the simultaneous irradiation of the samples and standards during 30 minutes, transfer of the samples into a counting planchet and measurement of the beta radiation emitted by phosphorus-32, after a suitable decay period. After the phosphorus analysis methods were established they were applied to both commercial milk and animal bone samples, and data obtained in the instrumental and radiochemical separation methods for each sample, were compared between themselves. In this work, it became possible to obtain analysis methods for phosphorus that can be applied independently of the sample quantity available, and the phosphorus content in the samples or interference that can be present in them. (author). 51 refs., 7 figs., 4 tabs

Endotoxins in surgical instruments of hip arthroplasty

Directory of Open Access Journals (Sweden)

Vania Regina Goveia

2016-06-01

Full Text Available Abstract OBJECTIVE To investigate endotoxins in sterilized surgical instruments used in hip arthroplasties. METHOD A descriptive exploratory study conducted in a public teaching hospital. Six types of surgical instruments were selected, namely: acetabulum rasp, femoral rasp, femoral head remover, chisel box, flexible bone reamer and femoral head test. The selection was based on the analysis of the difficulty in removing bone and blood residues during cleaning. The sample was made up of 60 surgical instruments, which were tested for endotoxins in three different stages. The EndosafeTM Gel-Clot LAL (Limulus Amebocyte Lysate method was used. RESULT There was consistent gel formation with positive analysis in eight instruments, corresponding to 13.3%, being four femoral rasps and four bone reamers. CONCLUSION Endotoxins in quantity ≥0.125 UE/mL were detected in 13.3% of the instruments tested.

Use of Instrumental Neutron Activation Analysis for Determination of Some Trace Elements of Biological Importance in Different Jute(Corchorus Capsularis) Seed Samples

International Nuclear Information System (INIS)

Metwally, E.; Abd-El-Khalik, H.; El-Sweify, F.H.; El-Sweify, A.H.H.

2004-01-01

Instrumental neutron activation analysis technique was used to determine some trace elements in seeds of jute (corchorus capsularis). The seed samples were obtained from Agricultural Research Center (ARC), Giza, (EG). The analyzed seed samples were produced from cultivation of three different strains, namely: St. DC 1105, st. JRC 7447 and St. PADMA. These strains were imported from Bangladesh. The jute plant was cultivated in sandy soil in Ismailaya research station farm at may on two seasons 1999 and 2000. The plant was irrigated with water from Ismailaya canal. The study was carried out to compare the influence of applying different kinds of fertilizers of different rates, i.e. mineral fertilizer and biofertilizer, on the uptake of some biologically important trace elements and to determine their concentration in the analyzed jute seed samples. These elements were; Co,Cr,Fe,Zn and others eight elements were analyzed quantitatively

Automated cellular sample preparation using a Centrifuge-on-a-Chip.

Science.gov (United States)

Mach, Albert J; Kim, Jae Hyun; Arshi, Armin; Hur, Soojung Claire; Di Carlo, Dino

2011-09-07

The standard centrifuge is a laboratory instrument widely used by biologists and medical technicians for preparing cell samples. Efforts to automate the operations of concentration, cell separation, and solution exchange that a centrifuge performs in a simpler and smaller platform have had limited success. Here, we present a microfluidic chip that replicates the functions of a centrifuge without moving parts or external forces. The device operates using a purely fluid dynamic phenomenon in which cells selectively enter and are maintained in microscale vortices. Continuous and sequential operation allows enrichment of cancer cells from spiked blood samples at the mL min(-1) scale, followed by fluorescent labeling of intra- and extra-cellular antigens on the cells without the need for manual pipetting and washing steps. A versatile centrifuge-analogue may open opportunities in automated, low-cost and high-throughput sample preparation as an alternative to the standard benchtop centrifuge in standardized clinical diagnostics or resource poor settings.

Psychometrics of the preschooler physical activity parenting practices instrument among a Latino sample.

Science.gov (United States)

O'Connor, Teresia M; Cerin, Ester; Hughes, Sheryl O; Robles, Jessica; Thompson, Deborah I; Mendoza, Jason A; Baranowski, Tom; Lee, Rebecca E

2014-01-15

Latino preschoolers (3-5 year old children) have among the highest rates of obesity. Low levels of physical activity (PA) are a risk factor for obesity. Characterizing what Latino parents do to encourage or discourage their preschooler to be physically active can help inform interventions to increase their PA. The objective was therefore to develop and assess the psychometrics of a new instrument: the Preschooler Physical Activity Parenting Practices (PPAPP) among a Latino sample, to assess parenting practices used to encourage or discourage PA among preschool-aged children. Cross-sectional study of 240 Latino parents who reported the frequency of using PA parenting practices. 95% of respondents were mothers; 42% had more than a high school education. Child mean age was 4.5 (±0.9) years (52% male). Test-retest reliability was assessed in 20%, 2 weeks later. We assessed the fit of a priori models using Confirmatory factor analyses (CFA). In a separate sub-sample (35%), preschool-aged children wore accelerometers to assess associations with their PA and PPAPP subscales. The a-priori models showed poor fit to the data. A modified factor structure for encouraging PPAPP had one multiple-item scale: engagement (15 items), and two single-items (have outdoor toys; not enroll in sport-reverse coded). The final factor structure for discouraging PPAPP had 4 subscales: promote inactive transport (3 items), promote screen time (3 items), psychological control (4 items) and restricting for safety (4 items). Test-retest reliability (ICC) for the two scales ranged from 0.56-0.85. Cronbach's alphas ranged from 0.5-0.9. Several sub-factors correlated in the expected direction with children's objectively measured PA. The final models for encouraging and discouraging PPAPP had moderate to good fit, with moderate to excellent test-retest reliabilities. The PPAPP should be further evaluated to better assess its associations with children's PA and offers a new tool for measuring PPAPP

Algorithms for a hand-held miniature x-ray fluorescence analytical instrument

International Nuclear Information System (INIS)

Elam, W.T.; Newman, D.; Ziemba, F.

1998-01-01

The purpose of this joint program was to provide technical assistance with the development of a Miniature X-ray Fluorescence (XRF) Analytical Instrument. This new XRF instrument is designed to overcome the weaknesses of spectrometers commercially available at the present time. Currently available XRF spectrometers (for a complete list see reference 1) convert spectral information to sample composition using the influence coefficients technique or the fundamental parameters method. They require either a standard sample with composition relatively close to the unknown or a detailed knowledge of the sample matrix. They also require a highly-trained operator and the results often depend on the capabilities of the operator. In addition, almost all existing field-portable, hand-held instruments use radioactive sources for excitation. Regulatory limits on such sources restrict them such that they can only provide relatively weak excitation. This limits all current hand-held XRF instruments to poor detection limits and/or long data collection times, in addition to the licensing requirements and disposal problems for radioactive sources. The new XRF instrument was developed jointly by Quantrad Sensor, Inc., the Naval Research Laboratory (NRL), and the Department of Energy (DOE). This report describes the analysis algorithms developed by NRL for the new instrument and the software which embodies them

JURISDICTION, COMPETENT JUDICIAL AUTHORITIES AND PROCEEDINGS UNDER REGULATION (EU NO 650/2012 ON SUCCESSION

Directory of Open Access Journals (Sweden)

Paula Poretti

2016-01-01

Full Text Available Novelties in the field of matters of succession brought by implementation of Regulation (EU No 650/2012 of the European Parliament and of the Council of 4 July 2012 on jurisdiction, applicable law, recognition and enforcement of decisions and acceptance and enforcement of authentic instruments in matters of succession and on the creation of a European Certificate of Succession are disscused in the paper. Especial emphasis is on jurisdiction, competent judicial authority and proceedings under Regulation on succession. In this sense, in the first part of the paper detailed analysis of provisions of Commission Implementing Regulation (EU No 1329/2014 of 9 December 2014 establishing the Forms referred to in Regulation (EU No 650/2012 of the European Parliament and of the Council on jurisdiction, applicable law, recognition and enforcement of decisions and acceptance and enforcement of authentic instruments in matters of succession and on the creation of a European Certificate of Succession and provisions of Croatian Law on implementation of Regulation (EU No 650/2012 of the European Parliament and of the Council on jurisdiction, applicable law, recognition and enforcement of decisions and acceptance and enforcement of authentic instruments in matters of succession and on the creation of a European Certificate of Succession is provided. In the second part of the paper case C404/14 Matoušková v. Republic of Czech is presented and difficulties in determining whether the case at issue falls within the scope of Regulation (EC No 2201/2003 or Regulation No 650/2012 on succession which could occur in matters of succession with cross-border implications are reffered to.

Novel Sample-handling Approach for XRD Analysis with Minimal Sample Preparation

Science.gov (United States)

Sarrazin, P.; Chipera, S.; Bish, D.; Blake, D.; Feldman, S.; Vaniman, D.; Bryson, C.

2004-01-01

Sample preparation and sample handling are among the most critical operations associated with X-ray diffraction (XRD) analysis. These operations require attention in a laboratory environment, but they become a major constraint in the deployment of XRD instruments for robotic planetary exploration. We are developing a novel sample handling system that dramatically relaxes the constraints on sample preparation by allowing characterization of coarse-grained material that would normally be impossible to analyze with conventional powder-XRD techniques.

Development of an automatic sampling device for the continuous measurement of atmospheric carbonyls compounds

International Nuclear Information System (INIS)

Perraud, V.

2007-12-01

Two sampling strategies were studied to develop an automatic instrument for the continuous measurement of atmospheric carbonyl compounds. Because of its specificity towards carbonyls compounds, sampling by using a transfer of gaseous phase in a liquid phase associated with a simultaneous chemical derivatization of the trapped compounds was first studied. However, this method do not allow a quantitative sampling of all studied carbonyl compounds, nor a continuous measurement in the field. To overcome the difficulties, a second strategy was investigated: the cryogenic adsorption onto solid adsorbent followed by thermodesorption and a direct analysis by GC/MS. Collection efficiency using different solid adsorbents was found greater than 95% for carbonyl compounds consisting of 1 to 7 carbons. This work is a successful first step towards the realization of the automatic sampling device for a continuous measurement of atmospheric carbonyls compounds. (author)

Using instrumental leadership to manage change.

Science.gov (United States)

Lesic, S A

1999-01-01

Effective leadership is the key factor in directing and influencing change in an organization. In today's healthcare environment, leaders have less time to make decisions that will ensure their organization's survival, a fact that has forced them to recreate the way they do business and be cognizant of ways to remain competitive. In the environment of change, a new type of leader is needed--the instrumental leader--one who combines the charismatic traits of envisioning, energizing and enabling with the three key facilitating behaviors of controlling, structuring and rewarding. To these attributes the instrumental leader adds critical thinking, problem solving and a feedback mechanism. Leaders who focus on employees as individuals and on the organization as a whole will achieve greater success. Today's leader must share a picture of the intended reality with the organization's staff, constituents and the community. Those most affected by oncoming change must be included in future planning. A shared vision is, however, an ongoing process, with communication crucial for its success. At some point in the change process, leaders must spend time building teams, clarifying behaviors and administering rewards and punishments. Part of this process involves energizing and aligning employees who will find ways to implement the shared new vision. The instrumental leader understands the need for teams that will form the backbone of the integrated system. Creating objective measures for performance, based on the new shared vision, demonstrates the organization's values better than communication or vision alone. Additional training or dialogue may better clarify the organization's expectations of employees.

Risk Implications of Energy Policy Instruments

DEFF Research Database (Denmark)

Kitzing, Lena

papers and a working paper), based on a combination of micro-economic and policy analysis. Financial theory is used for the quantitative analysis of investment problems under uncertainty, including mean-variance portfolio theory, real option analysis, Monte Carlo simulations and time series analysis...... show, both qualitatively and quantitatively, that policy makers cannot neglect risk implications when designing RES support instruments without compromising either on effectiveness or cost-efficiency of energy policy. The central research questions are: how can risk implications of RES policy...... instruments be integrated into policy design, so that the policies provide adequate investment incentives? And can the consideration of such risk implications in policy design make overall energy policy more successful? These questions are answered in seven research papers (four journal papers, two conference...

Recent developments in nuclear instruments

International Nuclear Information System (INIS)

Vaidya, P.P.

2004-01-01

Full text : Nuclear Instrumentation is a field of vital importance for DAE. It has important applications in many areas of interest such as Reactor Monitoring and control, Accelerator based research, Laser and nuclear physics experiments, Health and environmental monitoring, Astrophysics experiments etc. It is a specialized field involving expertise in detection of radioactivity down to the level of few events per minute as well as processing and analysis of signals which can be as small as few hundred micro volts embedded in noise. Some applications involve digitizing and processing these signals with 0.001% accuracy and timing accuracies of a fraction of nano sec. Rapid developments in semiconductor related technologies have influenced the field of nuclear instrumentation. Development of FPGA's and ASIC's have made it possible to develop miniaturized smart and portable instruments for field applications. Advancements in field of computers, communications and various field buses have been successfully utilized for smart, portable and DSP based instrumentation. Smart sensor with detector and front-end electronics on a single silicon chip is now a reality. These instruments are also made intelligent by addition of fuzzy logic, artificial neural networks and expert systems. Electronics Division of BARC has made significant contribution to the field of nuclear instrumentation to achieve self-reliance in this area. This has also led to development of several new methods, which have been published in international journals and appreciated worldwide. As a step towards achieving complete self-reliance a programme for development of FPGA's, HMC's and ASIC's has been undertaken and is being followed with special emphasis. This also includes development of detector and front- end electronics on a single chip. This talk brings out details of these developments and describes the 'state of art' work done in India

Modular time division multiplexer: Efficient simultaneous characterization of fast and slow transients in multiple samples

Science.gov (United States)

Kim, Stephan D.; Luo, Jiajun; Buchholz, D. Bruce; Chang, R. P. H.; Grayson, M.

2016-09-01

A modular time division multiplexer (MTDM) device is introduced to enable parallel measurement of multiple samples with both fast and slow decay transients spanning from millisecond to month-long time scales. This is achieved by dedicating a single high-speed measurement instrument for rapid data collection at the start of a transient, and by multiplexing a second low-speed measurement instrument for slow data collection of several samples in parallel for the later transients. The MTDM is a high-level design concept that can in principle measure an arbitrary number of samples, and the low cost implementation here allows up to 16 samples to be measured in parallel over several months, reducing the total ensemble measurement duration and equipment usage by as much as an order of magnitude without sacrificing fidelity. The MTDM was successfully demonstrated by simultaneously measuring the photoconductivity of three amorphous indium-gallium-zinc-oxide thin films with 20 ms data resolution for fast transients and an uninterrupted parallel run time of over 20 days. The MTDM has potential applications in many areas of research that manifest response times spanning many orders of magnitude, such as photovoltaics, rechargeable batteries, amorphous semiconductors such as silicon and amorphous indium-gallium-zinc-oxide.

Using Longitudinal Scales Assessment for Instrumental Music Students

Science.gov (United States)

Simon, Samuel H.

2014-01-01

In music education, current assessment trends emphasize student reflection, tracking progress over time, and formative as well as summative measures. This view of assessment requires instrumental music educators to modernize their approaches without interfering with methods that have proven to be successful. To this end, the Longitudinal Scales…

CHOMIK -Sampling Device of Penetrating Type for Russian Phobos Sample Return Mission

Science.gov (United States)

Seweryn, Karol; Grygorczuk, Jerzy; Rickmann, Hans; Morawski, Marek; Aleksashkin, Sergey; Banaszkiewicz, Marek; Drogosz, Michal; Gurgurewicz, Joanna; Kozlov, Oleg E.; Krolikowska-Soltan, Malgorzata; Sutugin, Sergiej E.; Wawrzaszek, Roman; Wisniewski, Lukasz; Zakharov, Alexander

Measurements of physical properties of planetary bodies allow to determine many important parameters for scientists working in different fields of research. For example effective heat conductivity of the regolith can help with better understanding of processes occurring in the body interior. Chemical and mineralogical composition gives us a chance to better understand the origin and evolution of the moons. In principle such parameters of the planetary bodies can be determined based on three different measurement techniques: (i) in situ measurements (ii) measurements of the samples in laboratory conditions at the Earth and (iii) remote sensing measurements. Scientific missions which allow us to perform all type of measurements, give us a chance for not only parameters determination but also cross calibration of the instruments. Russian Phobos Sample Return (PhSR) mission is one of few which allows for all type of such measurements. The spacecraft will be equipped with remote sensing instruments like: spectrometers, long wave radar and dust counter, instruments for in-situ measurements -gas-chromatograph, seismometer, thermodetector and others and also robotic arm and sampling device. PhSR mission will be launched in November 2011 on board of a launch vehicle Zenit. About a year later (11 months) the vehicle will reach the Martian orbit. It is anticipated that it will land on Phobos in the beginning of 2013. A take off back will take place a month later and the re-entry module containing a capsule that will hold the soil sample enclosed in a container will be on its way back to Earth. The 11 kg re-entry capsule with the container will land in Kazakhstan in mid-2014. A unique geological penetrator CHOMIK dedicated for the Phobos Sample Return space mis-sion will be designed and manufactured at the Space Mechatronics and Robotics Laboratory, Space Research Centre Polish Academy of Sciences (SRC PAS) in Warsaw. Functionally CHOMIK is based on the well known MUPUS

Solution assay instrument operations manual

International Nuclear Information System (INIS)

Li, T.K.; Marks, T.; Parker, J.L.

1983-09-01

An at-line solution assay instrument (SAI) has been developed and installed in a plutonium purification and americium recovery process area in the Los Alamos Plutonium Processing Facility. The instrument was designed for accurate, timely, and simultaneous nondestructive analysis of plutonium and americium in process solutions that have a wide range of concentrations and americium/plutonium ratios and for routine operation by process technicians who lack instrumentation background. The SAI, based on transmission-corrected, high-resolution gamma-ray spectroscopy, has two measurement stations attached to a single multichannel analyzer/computer system. To ensure the quality of assay results, the SAI has an internal measurement control program, which requires daily and weekly check runs and monitors key aspects of all assay runs. For a 25-ml sample, the assay precision is 5 g/l within a 2000-s count time

ANL small-sample calorimeter system design and operation

International Nuclear Information System (INIS)

Roche, C.T.; Perry, R.B.; Lewis, R.N.; Jung, E.A.; Haumann, J.R.

1978-07-01

The Small-Sample Calorimetric System is a portable instrument designed to measure the thermal power produced by radioactive decay of plutonium-containing fuels. The small-sample calorimeter is capable of measuring samples producing power up to 32 milliwatts at a rate of one sample every 20 min. The instrument is contained in two packages: a data-acquisition module consisting of a microprocessor with an 8K-byte nonvolatile memory, and a measurement module consisting of the calorimeter and a sample preheater. The total weight of the system is 18 kg

Nuclear electronic instrument systems using the Harwell 6000 series

International Nuclear Information System (INIS)

Seymour, F.D.; Snelling, G.F.; Hawthorn, I.

1980-01-01

This report describes some of the more recent equipment designed by the Systems Instrumentation Unit (AERE, Harwell), in the Harwell 6000 modular format. The units include: Laboratory Instruments (alpha monitors, beta-gamma detectors, spectrometers, automatic sample changer systems, automated counting laboratory systems, low power systems). Environmental Monitors (nuclear plant monitor, air monitor, sea bed monitor). Process Instruments (plutonium waste control, x-ray fluorescence monitor, process monitor, beam current monitor, effluent monitors). (U.K.)

The personality profile of a successful sales representative in the liquor industry

Directory of Open Access Journals (Sweden)

J. C. D. Augustyn

1988-05-01

Full Text Available From a study of the relevant literature it is clear that in general characteristics of sales representatives, and their personality profile in particular, have not been clearly identified. The objective of this study was to seek clarification of this issue. Two instruments were used in the investigation; namely, the South African Personality Questionnaire and the Thurstone Temperament Schedule. These instruments were administered to 45 sales representatives in the liquor industry and it was established that successful and less successful sales representatives could be statistically differentiated in terms of personality profile. Opsomming Uit die relevante literatuur blyk dit duidelik dat die kenmerke van die verkoopsverteenwoordiger in die algemeen en sypersoonlikheidsprofiel in die besonder nie duidelik ornlyn is nie. Die doelwit van hierdie studie was om groter duidelikheid in die verband te verkry. Twee instrumente is in die ondersoek gebruik nl. die Suid-Afrikaanse Persoonlikheidsvraelys en die Thurstone Temperament Schedule. Hierdie instrumente is geadministreer aan 'n steekproefvan 45 verkoopsverteenwoordigers in die drankbedryf en daar is bevind dat suksesvolle en minder suksesvolle verkoopsverteenwoordigers statisties gedifferensieer kan word in terme van hul persoonlikheidsprofiele.

Neutrons and music: Imaging investigation of ancient wind musical instruments

Science.gov (United States)

Festa, G.; Tardino, G.; Pontecorvo, L.; Mannes, D. C.; Senesi, R.; Gorini, G.; Andreani, C.

2014-10-01

A set of seven musical instruments and two instruments cares from the 'Fondo Antico della Biblioteca del Sacro Convento' in Assisi, Italy, were investigated through neutron and X-ray imaging techniques. Historical and scientific interests around ancient musical instruments motivate an intense research effort for their characterization using non-destructive and non-invasive techniques. X-ray and neutron tomography/radiography were applied to the study of composite material samples containing wood, hide and metals. The study was carried out at the NEUTRA beamline, PSI (Paul Scherrer Institute, Switzerland). Results of the measurements provided new information on the composite and multi-scale structure, such as: the internal structure of the samples, position of added materials like metals, wood fiber displays, deformations, presence of adhesives and their spatial distribution and novel insight about construction methods to guide the instruments' restoration process.

Calibration through on-line monitoring of instruments channels

International Nuclear Information System (INIS)

James, R.W.

1996-01-01

Plant technical specifications require periodic calibration of instrument channels, and this has traditionally meant calibration at fixed time intervals for nearly all instruments. Experience has shown that unnecessarily frequent calibrations reduce channel availability and reliability, impact outage durations, and increase maintenance costs. An alternative approach to satisfying existing requirements for periodic calibration consists of on-line monitoring and quantitative comparison of instrument channels during operation to identify instrument degradation and failure. A Utility Working Group has been formed by EPRI to support the technical activities necessary to achieve generic NRC acceptance of on-line monitoring of redundant instrument channels as a basis for determining when to perform calibrations. A topical report proposing NRC acceptance of this approach was submitted in August 1995, and the Working Group is currently resolving NRC technical questions. This paper describes the proposed approach and the current status of the topical report with regard to NRC review. While these activities will not preclude utilities from continuing to use existing calibration approaches, successful acceptance of this performance-based approach will allow utilities to substantially reduce the number of calibrations which are performed. Concurrent benefits will include reduced I ampersand C impact on outage durations and improved sensitivity to instrument channel performance

Mercury and gold concentrations of highly polluted environmental samples determined using prompt gamma-ray analysis and instrument neutron activation analysis

Science.gov (United States)

Osawa, Takahito; Hatsukawa, Yuichi; Appel, Peter W. U.; Matsue, Hideaki

2011-04-01

The authors have established a method of determining mercury and gold in severely polluted environmental samples using prompt gamma-ray analysis (PGA) and instrumental neutron activation analysis (INAA). Since large amounts of mercury are constantly being released into the environment by small-scale gold mining in many developing countries, the mercury concentration in tailings and water has to be determined to mitigate environmental pollution. Cold-vapor atomic absorption analysis, the most pervasive method of mercury analysis, is not suitable because tailings and water around mining facilities have extremely high mercury concentrations. On the other hand, PGA can determine high mercury concentrations in polluted samples as it has an appropriate level of sensitivity. Moreover, gold concentrations can be determined sequentially by using INAA after PGA. In conclusion, the analytical procedure established in this work using PGA and INAA is the best way to evaluate the degree of pollution and the tailing resource value. This method will significantly contribute to mitigating problems in the global environment.

Mercury and gold concentrations of highly polluted environmental samples determined using prompt gamma-ray analysis and instrument neutron activation analysis

International Nuclear Information System (INIS)

Osawa, Takahito; Hatsukawa, Yuichi; Appel, Peter W.U.; Matsue, Hideaki

2011-01-01

The authors have established a method of determining mercury and gold in severely polluted environmental samples using prompt gamma-ray analysis (PGA) and instrumental neutron activation analysis (INAA). Since large amounts of mercury are constantly being released into the environment by small-scale gold mining in many developing countries, the mercury concentration in tailings and water has to be determined to mitigate environmental pollution. Cold-vapor atomic absorption analysis, the most pervasive method of mercury analysis, is not suitable because tailings and water around mining facilities have extremely high mercury concentrations. On the other hand, PGA can determine high mercury concentrations in polluted samples as it has an appropriate level of sensitivity. Moreover, gold concentrations can be determined sequentially by using INAA after PGA. In conclusion, the analytical procedure established in this work using PGA and INAA is the best way to evaluate the degree of pollution and the tailing resource value. This method will significantly contribute to mitigating problems in the global environment.

Elemental analysis in bed sediment samples of Karnafuli estuarine zone in the Bay of Bengal by instrumental neutron activation analysis

International Nuclear Information System (INIS)

Molla, N.I.; Hossain, S.M.; Basunia, S.; Miah, R.U.; Rahman, M.; Sikder, D.H.; Chowdhury, M.I.

1997-01-01

The concentration of rare earths and other elements have been determined in the bed sediment samples of Karnafuli estuarine zone in the Bay of Bengal by instrumental neutron activation analysis (INAA). The samples and the standards soil-5, soil-7, coal fly ash and pond sediment were prepared and simultaneously irradiated for short and long time at the TRIGA Mark-II research reactor facility of Atomic Energy Research Establishment, Savar, Dhaka. The maximum thermal neutron flux was of the order of 10 13 n x cm -2 x s -1 . After irradiation the radioactivity of the product nuclides was measured by using a high resolution high purity germanium detector system. Analysis of γ-ray spectra and quantitative analysis of the elemental concentration were done via the software GANAAS. It has been possible to determine the concentration level of 27 elements including the rare earths La, Ce, Sm, Eu, Tb, Dy and Yb and uranium and thorium. (author)

Method to deterministically study photonic nanostructures in different experimental instruments.

Science.gov (United States)

Husken, B H; Woldering, L A; Blum, C; Vos, W L

2009-01-01

We describe an experimental method to recover a single, deterministically fabricated nanostructure in various experimental instruments without the use of artificially fabricated markers, with the aim to study photonic structures. Therefore, a detailed map of the spatial surroundings of the nanostructure is made during the fabrication of the structure. These maps are made using a series of micrographs with successively decreasing magnifications. The graphs reveal intrinsic and characteristic geometric features that can subsequently be used in different setups to act as markers. As an illustration, we probe surface cavities with radii of 65 nm on a silica opal photonic crystal with various setups: a focused ion beam workstation; a scanning electron microscope (SEM); a wide field optical microscope and a confocal microscope. We use cross-correlation techniques to recover a small area imaged with the SEM in a large area photographed with the optical microscope, which provides a possible avenue to automatic searching. We show how both structural and optical reflectivity data can be obtained from one and the same nanostructure. Since our approach does not use artificial grids or markers, it is of particular interest for samples whose structure is not known a priori, like samples created solely by self-assembly. In addition, our method is not restricted to conducting samples.

Effects of thermal deformation on optical instruments for space application

Science.gov (United States)

Segato, E.; Da Deppo, V.; Debei, S.; Cremonese, G.

2017-11-01

Optical instruments for space missions work in hostile environment, it's thus necessary to accurately study the effects of ambient parameters variations on the equipment. In particular optical instruments are very sensitive to ambient conditions, especially temperature. This variable can cause dilatations and misalignments of the optical elements, and can also lead to rise of dangerous stresses in the optics. Their displacements and the deformations degrade the quality of the sampled images. In this work a method for studying the effects of the temperature variations on the performance of imaging instrument is presented. The optics and their mountings are modeled and processed by a thermo-mechanical Finite Element Model (FEM) analysis, then the output data, which describe the deformations of the optical element surfaces, are elaborated using an ad hoc MATLAB routine: a non-linear least square optimization algorithm is adopted to determine the surface equations (plane, spherical, nth polynomial) which best fit the data. The obtained mathematical surface representations are then directly imported into ZEMAX for sequential raytracing analysis. The results are the variations of the Spot Diagrams, of the MTF curves and of the Diffraction Ensquared Energy due to simulated thermal loads. This method has been successfully applied to the Stereo Camera for the BepiColombo mission reproducing expected operative conditions. The results help to design and compare different optical housing systems for a feasible solution and show that it is preferable to use kinematic constraints on prisms and lenses to minimize the variation of the optical performance of the Stereo Camera.

Solvent Front Position Extraction procedure with thin-layer chromatography as a mode of multicomponent sample preparation for quantitative analysis by instrumental technique.

Science.gov (United States)

Klimek-Turek, A; Sikora, E; Dzido, T H

2017-12-29

A concept of using thin-layer chromatography to multicomponent sample preparation for quantitative determination of solutes followed by instrumental technique is presented. Thin-layer chromatography (TLC) is used to separate chosen substances and their internal standard from other components (matrix) and to form a single spot/zone containing them at the solvent front position. The location of the analytes and internal standard in the solvent front zone allows their easy extraction followed by quantitation by HPLC. Copyright © 2017 Elsevier B.V. All rights reserved.

Instruments to assess stigmatization in dermatology.

Science.gov (United States)

Dimitrov, Dimitre; Szepietowski, Jacek C

2017-11-03

Stigmatization is the assignment of negative perceptions to an individual because of a perceived difference from the population at large. Skin conditions are frequently the reason of social rejection with a consequent negative influence on the personal and social life of patients. The aim of the current study was to review the available instruments that can be successfully utilized to measure the stigmatization level among dermatological patients. We performed our search on PubMed up to November 2016 and utilized combinations of key phrases containing such words as stigmatization, skin, dermatology, names of various skin conditions (psoriasis, vitiligo, acne, etc.), measurement. The search found a considerable number of articles - 548. After filtering them through a precise selection process, 58 articles remained. We concentrated only on the methodological aspects to assess stigmatization in various dermatoses. The review ascertained that there exist numerous instruments in the form of questionnaires. They were utilized in various researches in order to assess the stigmatization level in patients with skin problems. We divided them into two main groups: dermatology specific instruments (6 questionnaires) and dermatosis/disease specific ones (8 questionnaires). It is recommended to use dermatology-specific instruments to compare the stigmatization level in various skin conditions. They can be utilized as well as a first line tools to study the feeling of stigmatization in specific skin diseases; however, where it is possible, they should be supplemented with the disease-specific instrument for deeper analysis of both qualities of life and stigmatization.

Neutron activation analysis of geochemical samples

International Nuclear Information System (INIS)

Rosenberg, R.; Zilliacus, R.; Kaistila, M.

1983-06-01

The present paper will describe the work done at the Technical Research Centre of Finland in developing methods for the large-scale activation analysis of samples for the geochemical prospecting of metals. The geochemical prospecting for uranium started in Finland in 1974 and consequently a manually operated device for the delayed neutron activation analysis of uranium was taken into use. During 1974 9000 samples were analyzed. The small capacity of the analyzer made it necessary to develop a completely automated analyzer which was taken into use in August 1975. Since then 20000-30000 samples have been analyzed annually the annual capacity being about 60000 samples when running seven hours per day. Multielemental instrumental neutron activation analysis is used for the analysis of more than 40 elements. Using instrumental epithermal neutron activation analysis 25-27 elements can be analyzed using one irradiation and 20 min measurement. During 1982 12000 samples were analyzed for mining companies and Geological Survey of Finland. The capacity is 600 samples per week. Besides these two analytical methods the analysis of lanthanoids is an important part of the work. 11 lanthanoids have been analyzed using instrumental neutron activation analysis. Radiochemical separation methods have been developed for several elements to improve the sensitivity of the analysis

Endotoxins in surgical instruments of hip arthroplasty

OpenAIRE

Goveia, Vania Regina; Mendoza, Isabel Yovana Quispe; Guimarães, Gilberto Lima; Ercole, Flavia Falci; Couto, Bráulio Roberto Gonçalves Marinho; Leite, Edna Marilea Meireles; Stoianoff, Maria Aparecida Resende; Ferreira, José Antonio Guimarães

2016-01-01

Abstract OBJECTIVE To investigate endotoxins in sterilized surgical instruments used in hip arthroplasties. METHOD A descriptive exploratory study conducted in a public teaching hospital. Six types of surgical instruments were selected, namely: acetabulum rasp, femoral rasp, femoral head remover, chisel box, flexible bone reamer and femoral head test. The selection was based on the analysis of the difficulty in removing bone and blood residues during cleaning. The sample was made up of 60...

Developing and testing an instrument to measure the presence of conditions for successful implementation of quality improvement collaboratives.

Science.gov (United States)

Dückers, Michel L A; Wagner, Cordula; Groenewegen, Peter P

2008-08-11

In quality improvement collaboratives (QICs) teams of practitioners from different health care organizations are brought together to systematically improve an aspect of patient care. Teams take part in a series of meetings to learn about relevant best practices, quality methods and change ideas, and share experiences in making changes in their own local setting. The purpose of this study was to develop an instrument for measuring team organization, external change agent support and support from the team's home institution in a Dutch national improvement and dissemination programme for hospitals based on several QICs. The exploratory methodological design included two phases: a) content development and assessment, resulting in an instrument with 15 items, and b) field testing (N = 165). Internal consistency reliability was tested via Cronbach's alpha coefficient. Principal component analyses were used to identify underlying constructs. Tests of scaling assumptions according to the multi trait/multi-item matrix, were used to confirm the component structure. Three components were revealed, explaining 65% of the variability. The components were labelled 'organizational support', 'team organization' and 'external change agent support'. One item not meeting item-scale criteria was removed. This resulted in a 14 item instrument. Scale reliability ranged from 0.77 to 0.91. Internal item consistency and divergent validity were satisfactory. On the whole, the instrument appears to be a promising tool for assessing team organization and internal and external support during QIC implementation. The psychometric properties were good and warrant application of the instrument for the evaluation of the national programme and similar improvement programmes.

Developing and testing an instrument to measure the presence of conditions for successful implementation of quality improvement collaboratives

Directory of Open Access Journals (Sweden)

Wagner Cordula

2008-08-01

Full Text Available Abstract Background In quality improvement collaboratives (QICs teams of practitioners from different health care organizations are brought together to systematically improve an aspect of patient care. Teams take part in a series of meetings to learn about relevant best practices, quality methods and change ideas, and share experiences in making changes in their own local setting. The purpose of this study was to develop an instrument for measuring team organization, external change agent support and support from the team's home institution in a Dutch national improvement and dissemination programme for hospitals based on several QICs. Methods The exploratory methodological design included two phases: a content development and assessment, resulting in an instrument with 15 items, and b field testing (N = 165. Internal consistency reliability was tested via Cronbach's alpha coefficient. Principal component analyses were used to identify underlying constructs. Tests of scaling assumptions according to the multi trait/multi-item matrix, were used to confirm the component structure. Results Three components were revealed, explaining 65% of the variability. The components were labelled 'organizational support', 'team organization' and 'external change agent support'. One item not meeting item-scale criteria was removed. This resulted in a 14 item instrument. Scale reliability ranged from 0.77 to 0.91. Internal item consistency and divergent validity were satisfactory. Conclusion On the whole, the instrument appears to be a promising tool for assessing team organization and internal and external support during QIC implementation. The psychometric properties were good and warrant application of the instrument for the evaluation of the national programme and similar improvement programmes.

Alternative concepts for design of air monitoring instruments: In-line and open face reference samplers and a new method of demonstrating alpha CAM performance

International Nuclear Information System (INIS)

Rodgers, J.C.; McFarland, A.R.

1993-01-01

Over the past several years Los Alamos, Texas A ampersand M University and Canberra Instruments have been collaborating on the development of advanced continuous air monitoring and air sampling concepts and technology. We have successfully completed the design of an alpha CAM which embodies a number of innovations in the way radon progeny background interference is controlled and compensated, and in the way data processing, alarm generation, and data communication are handled

Comparison of instrumental neutron activation analysis and instrumental charged-particle activation analysis for determining of Zn-68 abundance

International Nuclear Information System (INIS)

Rafii, H.; Mirzaei, M.; Aslani, G.R.; Kamali-Dehghan, M.; Rajamand, A-A.; Rahiminejad, A.; Mirzajani, N.; Sardari, D.; Shahabi, I.; Majidi, F.

2004-01-01

Gallium-67 has found important applications in nuclear medicine since last decades. The bombardment of enriched zinc-68 by proton beams in cyclotron is the most suitable method for the carrier-free production of this radionuclide. Any traces and isotopic impurities of the target cause serious radiological hazards because of their associated induced radioactivities. Trace analysis and Zn-68 content determination of the target material before any bombardment and chemical separation provide a valuable assessment of desired product. The elemental abundance evaluation of enriched isotopes is generally carried out by inductively coupled plasma-mass spectrometry method, ICP-Ms Instrumental neutron activation analysis and instrumental charged particle activation analysis. International neutron activation analysis and instrumental charged- particle activation analysis, looks be an alternative nuclear method for determining the abundance evaluation of enriched Zn-68 enrichment in two different samples has been studied by mean of international neutron activation analysis and instrumental charged- particle activation analysis . One sample was purchased from a French company, cortecnet, and the other was separated by an electromagnetic system in the Ions source department of our center, NRCAM. The neutron or proton irradiation was took place respectively in miniature neutron source reactor of Esfahan by flux of (1 to 5) 10 11 n/cm 2 .sec for 30 min and in Cyclon30 by 19 MeV proton beams of 100μA current for 12 min. The produced radioactivity was measured by HpGe detector for determination of trace impurities and evaluation of Zn-68 content in the samples. The result shows a good agreement with the reported ones by their producers and their low derivation of about ± indicates that the international neutron activation analysis and instrumental charged- particle activation analysis are relatively precise and rapid and each one can be used as a supplemental method for analyzing

XRF analysis of mineralised samples

International Nuclear Information System (INIS)

Ahmedali, T.

2002-01-01

Full text: Software now supplied by instrument manufacturers has made it practical and convenient for users to analyse unusual samples routinely. Semiquantitative scanning software can be used for rapid preliminary screening of elements ranging from Carbon to Uranium, prior to assigning mineralised samples to an appropriate quantitative analysis routine. The general quality and precision of analytical results obtained from modern XRF spectrometers can be significantly enhanced by several means: a. Modifications in preliminary sample preparation can result in less contamination from crushing and grinding equipment. Optimised techniques of actual sample preparation can significantly increase precision of results. b. Employment of automatic data recording balances and the use of catch weights during sample preparation reduces technician time as well as weighing errors. * c. Consistency of results can be improved significantly by the use of appropriate stable drift monitors with a statistically significant content of the analyte d. A judicious selection of kV/mA combinations, analysing crystals, primary beam filters, collimators, peak positions, accurate background correction and peak overlap corrections, followed by the use of appropriate matrix correction procedures. e. Preventative maintenance procedures for XRF spectrometers and ancillary equipment, which can also contribute significantly to reducing instrument down times, are described. Examples of various facets of sample processing routines are given from the XRF spectrometer component of a multi-instrument analytical university facility, which provides XRF data to 17 Canadian universities. Copyright (2002) Australian X-ray Analytical Association Inc

40 CFR 92.117 - Gas meter or flow instrumentation calibration, particulate measurement.

Science.gov (United States)

2010-07-01

... 40 Protection of Environment 20 2010-07-01 2010-07-01 false Gas meter or flow instrumentation... ENGINES Test Procedures § 92.117 Gas meter or flow instrumentation calibration, particulate measurement. (a) Sampling for particulate emissions requires the use of gas meters or flow instrumentation to...

Instrumentational complexity of music genres and why simplicity sells.

Directory of Open Access Journals (Sweden)

Gamaliel Percino

Full Text Available Listening habits are strongly influenced by two opposing aspects, the desire for variety and the demand for uniformity in music. In this work we quantify these two notions in terms of instrumentation and production technologies that are typically involved in crafting popular music. We assign an 'instrumentational complexity value' to each music style. Styles of low instrumentational complexity tend to have generic instrumentations that can also be found in many other styles. Styles of high complexity, on the other hand, are characterized by a large variety of instruments that can only be found in a small number of other styles. To model these results we propose a simple stochastic model that explicitly takes the capabilities of artists into account. We find empirical evidence that individual styles show dramatic changes in their instrumentational complexity over the last fifty years. 'New wave' or 'disco' quickly climbed towards higher complexity in the 70s and fell back to low complexity levels shortly afterwards, whereas styles like 'folk rock' remained at constant high instrumentational complexity levels. We show that changes in the instrumentational complexity of a style are related to its number of sales and to the number of artists contributing to that style. As a style attracts a growing number of artists, its instrumentational variety usually increases. At the same time the instrumentational uniformity of a style decreases, i.e. a unique stylistic and increasingly complex expression pattern emerges. In contrast, album sales of a given style typically increase with decreasing instrumentational complexity. This can be interpreted as music becoming increasingly formulaic in terms of instrumentation once commercial or mainstream success sets in.

Instrumentational Complexity of Music Genres and Why Simplicity Sells

Science.gov (United States)

Percino, Gamaliel; Klimek, Peter; Thurner, Stefan

2014-01-01

Listening habits are strongly influenced by two opposing aspects, the desire for variety and the demand for uniformity in music. In this work we quantify these two notions in terms of instrumentation and production technologies that are typically involved in crafting popular music. We assign an ‘instrumentational complexity value’ to each music style. Styles of low instrumentational complexity tend to have generic instrumentations that can also be found in many other styles. Styles of high complexity, on the other hand, are characterized by a large variety of instruments that can only be found in a small number of other styles. To model these results we propose a simple stochastic model that explicitly takes the capabilities of artists into account. We find empirical evidence that individual styles show dramatic changes in their instrumentational complexity over the last fifty years. ‘New wave’ or ‘disco’ quickly climbed towards higher complexity in the 70s and fell back to low complexity levels shortly afterwards, whereas styles like ‘folk rock’ remained at constant high instrumentational complexity levels. We show that changes in the instrumentational complexity of a style are related to its number of sales and to the number of artists contributing to that style. As a style attracts a growing number of artists, its instrumentational variety usually increases. At the same time the instrumentational uniformity of a style decreases, i.e. a unique stylistic and increasingly complex expression pattern emerges. In contrast, album sales of a given style typically increase with decreasing instrumentational complexity. This can be interpreted as music becoming increasingly formulaic in terms of instrumentation once commercial or mainstream success sets in. PMID:25551631

Instrumentational complexity of music genres and why simplicity sells.

Science.gov (United States)

Percino, Gamaliel; Klimek, Peter; Thurner, Stefan

2014-01-01

Listening habits are strongly influenced by two opposing aspects, the desire for variety and the demand for uniformity in music. In this work we quantify these two notions in terms of instrumentation and production technologies that are typically involved in crafting popular music. We assign an 'instrumentational complexity value' to each music style. Styles of low instrumentational complexity tend to have generic instrumentations that can also be found in many other styles. Styles of high complexity, on the other hand, are characterized by a large variety of instruments that can only be found in a small number of other styles. To model these results we propose a simple stochastic model that explicitly takes the capabilities of artists into account. We find empirical evidence that individual styles show dramatic changes in their instrumentational complexity over the last fifty years. 'New wave' or 'disco' quickly climbed towards higher complexity in the 70s and fell back to low complexity levels shortly afterwards, whereas styles like 'folk rock' remained at constant high instrumentational complexity levels. We show that changes in the instrumentational complexity of a style are related to its number of sales and to the number of artists contributing to that style. As a style attracts a growing number of artists, its instrumentational variety usually increases. At the same time the instrumentational uniformity of a style decreases, i.e. a unique stylistic and increasingly complex expression pattern emerges. In contrast, album sales of a given style typically increase with decreasing instrumentational complexity. This can be interpreted as music becoming increasingly formulaic in terms of instrumentation once commercial or mainstream success sets in.

Development and Preliminary Tests of an Open-Path Airborne Diode Laser Absorption Instrument for Carbon Dioxide

Science.gov (United States)

Diskin, Glenn S.; DiGangi, Joshua P.; Yang, Melissa; Slate, Thomas A.; Rana, Mario

2015-01-01

Carbon dioxide (CO2) is well known for its importance as an atmospheric greenhouse gas, with many sources and sinks around the globe. Understanding the fluxes of carbon into and out of the atmosphere is a complex and daunting challenge. One tool applied by scientists to measure the vertical flux of CO2 near the surface uses the eddy covariance technique, most often from towers but also from aircraft flying specific patterns over the study area. In this technique, variations of constituents of interest are correlated with fluctuations in the local vertical wind velocity. Measurement requirements are stringent, particularly with regard to precision, sensitivity to small changes, and temporal sampling rate. In addition, many aircraft have limited payload capability, so instrument size, weight, and power consumption are also important considerations. We report on the development and preliminary application of an airborne sensor for the measurement of atmospheric CO2. The instrument, modeled on the successful DLH (Diode Laser Hygrometer) series of instruments, has been tested in the laboratory and on the NASA DC-8 aircraft. Performance parameters such as accuracy, precision, sensitivity, specificity, and temporal response are discussed in the context of typical atmospheric variability and suitability for flux measurement applications. On-aircraft, in-flight data have been obtained and are discussed as well. Performance of the instrument has been promising, and continued flight testing is planned during 2016.

The Multicultural Personality Questionnaire : A multidimensional instrument of multicultural effectiveness

NARCIS (Netherlands)

Van der Zee, KI; Van Oudenhoven, JP

2000-01-01

In today's global business environment, executive work is becoming more international in orientation. Several skills and traits may underlie executive success in an inter national environment. The Multicultural Personality Questionnaire was developed as a multidimensional instrument aimed at

Structural Model of the Effect of Psychological Capital on Success with Due to the Mediating Role of Commitment and Satisfaction

Directory of Open Access Journals (Sweden)

M Golparvar

2016-09-01

Full Text Available This research was administered with the aim of investigating structural model of the effect of psychological capital on career success with due to the mediating role of satisfaction and commitment among employees of Telecom Company. Research statistical population was male and female employees of Telecom in Isfahan city, who among them two hundred and eighty five persons were selected using convenience sampling. Research instruments were Nguyen et al. Psychological Capital questionnaire, Nabi Job Success (career success Questionnaire, Spector Job Satisfaction Questionnaire and Speier and Venkatesh Organizational Commitment Questionnaire. Data were analyzed using structural equation modeling. Results of structural equation modeling revealed thatin aseriesof sequential relationships, there is a significant effect from psychological capital also on job satisfaction and organizational commitment and there is a significant effect also from job satisfaction and organizational commitment on job success (career success. The results also showed that psychological capital impact on career success was indirectly through job satisfaction and organizational commitment. Overall, the results of this study showed that job satisfaction and organizational commitment were mediating variables in the relationship between psychological capital and career success.

Fabrication of Non-instrumented capsule for DUPIC simulated fuel irradiation test in HANARO

Energy Technology Data Exchange (ETDEWEB)

Kim, B.G.; Kang, Y.H.; Park, S.J.; Shin, Y.T. [Korea Atomic Energy Research Institute, Taejon (Korea)

1999-10-01

In order to develope DUPIC nuclear fuel, the irradiation test for simulated DUPIC fuel was planed using a non-instrumented capsule in HANARO. Because DUPIC fuel is highly radioactive material the non-instrumented capsule for an irradiation test of simulated DUPIC fuel in HANARO was designed to remotely assemble and disassemble in hot cell. And then, according to the design requirements the non-instrumented DUPIC capsule was successfully manufactured. Also, the manufacturing technologies of the non-instrumented capsule for irradiating the nuclear fuel in HANARO were established, and the basic technology for the development of the instrumented capsule technology was accumulated. This report describes the manufacturing of the non-instrumented capsule for simulated DUPIC fuel. And, this report will be based to develope the instrumented capsule, which will be utilized to irradiate the nuclear fuel in HANARO. 26 refs., 4 figs. (Author)

Successful aging in centenarians: myths and reality.

Science.gov (United States)

Motta, M; Bennati, E; Ferlito, L; Malaguarnera, M; Motta, L

2005-01-01

The term "successful aging" appeared in the first issue of "The Gerontologist" in 1961. During the successive years, this expression has changed its meaning. Nowadays, successful aging means "absence of diseases and disabilities, maintenance of high levels of physical and cognitive abilities, preservation of the social and productive activities". It has become a common opinion that the centenarians may represent the prototypes of the successful aging. This motivated our work to study the clinical, psychical, and functional aspects in a centenarian group, verifying the real autonomy, instrumental capacities, and working abilities. Our study pool consisted of 602 centenarians, who were also subjects of then epidemiological studies of the Italian Multicenter Studies on Centenarians (IMUSCE). All subjects underwent a clinical-anamnestic evaluation, cognitive-functional tests by means of the mini mental state examination (MMSE), the independence index in activities of daily living (ADL), the instrumental activities of daily living (IADL) scale. The centenarians were classified in three groups, according to the criteria elaborated previously by us, based on their psychophysical status and autonomy, as follows. Group A: centenarians in good health status; Group B: centenarians in an intermediate health status. Group C: centenarians in bad health status. Group A represented 20.0% of the total pool, Group B amounted to 33.4%, and the Group C was 46.6%. The centenarians of Group A presented normal ADL values, and 47.9% of them were autosufficient in all functions; 5.7% of them were independent in all IADL items. These data confirm that the centenarians of Group A are free of invalidating chronic diseases, are autonomous, maintain good physical and cognitive capacities, however, have not maintained any social or productive activities. Therefore, they cannot be considered as prototypes of successful aging.

Quality Assurance for Space Instruments Built with COTS

DEFF Research Database (Denmark)

Guldager, Peter Buch; Thuesen, Gøsta Guldbæk; Jørgensen, John Leif

2005-01-01

be changed at any time and have major consequences to the components ability to survive the space environment. A safe way to protect to components, which are not Latch-Up immune, is to protect the components with a Latch-Up protection circuit. A strict control has to be established, when procuring COTS......Instruments for space can be built with COTS. However no radiation data are available for COTS, so the only way to ensure that the components can survive the space environment is to irradiate each component. Samples from each Lot have to be irradiated, because the manufac-turing process can...... component, testing and manufacturing the instrument before the instrument is qualified for space. By having a strict control with instrument built with COTS, it is possible to manufacture a reliable instrument as with Rad-Hard components....

Testing of Environmental Satellite Bus-Instrument Interfaces Using Engineering Models

Science.gov (United States)

Gagnier, Donald; Hayner, Rick; Nosek, Thomas; Roza, Michael; Hendershot, James E.; Razzaghi, Andrea I.

2004-01-01

This paper discusses the formulation and execution of a laboratory test of the electrical interfaces between multiple atmospheric scientific instruments and the spacecraft bus that carries them. The testing, performed in 2002, used engineering models of the instruments and the Aura spacecraft bus electronics. Aura is one of NASA s Earth Observatory System missions. The test was designed to evaluate the complex interfaces in the command and data handling subsystems prior to integration of the complete flight instruments on the spacecraft. A problem discovered during the flight integration phase of the observatory can cause significant cost and schedule impacts. The tests successfully revealed problems and led to their resolution before the full-up integration phase, saving significant cost and schedule. This approach could be beneficial for future environmental satellite programs involving the integration of multiple, complex scientific instruments onto a spacecraft bus.

Instrument development continues in Oak Ridge

International Nuclear Information System (INIS)

Ekkebus, Allen E.

2012-01-01

Peer review panels composed of 80 external scientists recently visited Oak Ridge National Laboratory (ORNL) to review almost 700 proposals for experiments on 23 instruments at the Spallation Neutron Source (SNS) and High Flux Isotope Reactor (HFIR). These were proposed for the time period from January-June 2012. About 40% of the proposals were approved for beam time and 20% were placed on an alternate list if time becomes available. The Hybrid Spectrometer HYSPEC at SNS began its commissioning in September 2011. HYSPEC is otpimized for studying low energy dynamics in single-crystal samples using a broad variety of sample environments, and is equipped with a polarization analysis capability. It is expected to be available for users on a limited basis in the second half of 2012. The detector tank of CORELLI has been installed on beamline 9 at SNS. Now that the tank is in place, banks of neutron detectors and boron carbide shielding will be installed around the interior. CORELLI is optimized to probe complex disorder in crystalline materials through diffuse scattering from single-crystal samples. It will begin commissioning in 2014. CORELLI is one of four instruments being developed under the SING II (SNS Instruments Next Generation II) project. The others are the Macromolecular Neutron Diffractometer (MANDI), the Vibrational Spectrometer (VISION, scheduled to begin commissioning in 2012), and the Time of Flight Ultra Small Angle Neutron Scattering Instrument (TOF-USANS). The single crystal neutron diffractometer IMAGINE, was deliverd to HFIR in October 2011. Preliminary testing has been carried out. IMAGINE will provide atomic resolution information on chemical, organic, metallo-organic and protein single crystals that will enable their chemical, physical and biological structure and function to be understood. This instrument will benefit scientists with interests in pharmaceuticals, minerals and other inorganic crystals, small molecules, molecular organo

Software quality assurance plan for void fraction instrument

International Nuclear Information System (INIS)

Gimera, M.

1994-01-01

Waste Tank SY-101 has been the focus of extensive characterization work over the past few years. The waste continually generates gases, most notably hydrogen, which are periodically released from the waste. Gas can be trapped in tank waste in three forms: as void gas (bubbles), dissolved gas, or absorbed gas. Void fraction is the volume percentage of a given sample that is comprised of void gas. The void fraction instrument (VFI) acquires the data necessary to calculate void fraction. This document covers the product, Void Fraction Data Acquisition Software. The void fraction software being developed will have the ability to control the void fraction instrument hardware and acquire data necessary to calculate the void fraction in samples. This document provides the software quality assurance plan, verification and validation plan, and configuration management plan for developing the software for the instrumentation that will be used to obtain void fraction data from Tank SY-101

Instrumentation for collecting and measuring radon and its daughters

International Nuclear Information System (INIS)

Essling, M.A.; Hengde, W.; Markun, F.; Toohey, R.E.; Rundo, J.; Miranda, J.E. Jr.

1982-01-01

A new sampling can is described for collecting an air sample for determination of its radon content. Instruments which are employed for the continuous monitoring of radon or its daughters in houses are described and their performances discussed

[Evaluation of Medical Instruments Cleaning Effect of Fluorescence Detection Technique].

Science.gov (United States)

Sheng, Nan; Shen, Yue; Li, Zhen; Li, Huijuan; Zhou, Chaoqun

2016-01-01

To compare the cleaning effect of automatic cleaning machine and manual cleaning on coupling type surgical instruments. A total of 32 cleaned medical instruments were randomly sampled from medical institutions in Putuo District medical institutions disinfection supply center. Hygiena System SUREII ATP was used to monitor the ATP value, and the cleaning effect was evaluated. The surface ATP values of the medical instrument of manual cleaning were higher than that of the automatic cleaning machine. Coupling type surgical instruments has better cleaning effect of automatic cleaning machine before disinfection, the application is recommended.

Human Resource Outsourcing Success

OpenAIRE

Hasliza Abdul-Halim; Elaine Ee; T. Ramayah; Noor Hazlina Ahmad

2014-01-01

The existing literature on partnership seems to take the relationship between partnership quality and outsourcing success for granted. Therefore, this article aims at examining the role of service quality in strengthening the relationship between partnership quality and human resource (HR) outsourcing success. The samples were obtained from 96 manufacturing organizations in Penang, Malaysia. The results showed that par...

National standard and code compliance for electrical equipment installed in hazardous locations for the void fraction instrument

International Nuclear Information System (INIS)

Bussell, J.H.; Martin, J.D.; Stokes, T.I.

1994-01-01

The hazardous area classification is evaluated and defined for the void fraction instrument (VFI). The void fraction instrument is an instrument that is used to measure gas bubble concentration in tank waste. It is a 18.3 meter (60-foot) long pipe with swivel sampling head. The assembly is lowered into tank waste via an available riser and waste sample is obtained. The sample is obtained and the sample chamber is pressurized from a fixed volume chamber. The pressure is then measured and then the VFI is moved to the next sample elevation

Improved Instrument for Detecting Water and Ice in Soil

Science.gov (United States)

Buehler, Martin; Chin, Keith; Keymeulen, Didler; McCann, Timothy; Seshadri, Suesh; Anderson, Robert

2009-01-01

An instrument measures electrical properties of relatively dry soils to determine their liquid water and/or ice contents. Designed as a prototype of instruments for measuring the liquid-water and ice contents of lunar and planetary soils, the apparatus could also be utilized for similar purposes in research and agriculture involving terrestrial desert soils and sands, and perhaps for measuring ice buildup on aircraft surfaces. This instrument is an improved version of the apparatus described in Measuring Low Concentrations of Liquid Water and Ice in Soil (NPO-41822), NASA Tech Briefs, Vol. 33, No. 2 (February 2009), page 22. The designs of both versions are based on the fact that the electrical behavior of a typical soil sample is well approximated by a network of resistors and capacitors in which resistances decrease and capacitances increase (and the magnitude and phase angle of impedance changes accordingly) with increasing water content. The previous version included an impedance spectrometer and a jar into which a sample of soil was placed. Four stainless-steel screws at the bottom of the jar were used as electrodes of a fourpoint impedance probe connected to the spectrometer. The present instrument does not include a sample jar and can be operated without acquiring or handling samples. Its impedance probe consists of a compact assembly of electrodes housed near the tip of a cylinder. The electrodes protrude slightly from the cylinder (see Figure 1). In preparation for measurements, the cylinder is simply pushed into the ground to bring the soil into contact with the electrodes.

Inspector-instrument interface in portable NDA instrumentation

International Nuclear Information System (INIS)

Halbig, J.K.; Klosterbuer, S.F.

1981-01-01

Recent electronics technology advances make it possible to design sophisticated instruments in small packages for convenient field implementation. An inspector-instrument interface design that allows communication of procedures, responses, and results between the instrument and user is presented. This capability has been incorporated into new spent-fuel instrumentation and a battery-powered multichannel analyzer

Inspector-instrument interface in portable NDA instrumentation

International Nuclear Information System (INIS)

Halbig, J.K.; Klosterbuer, S.F.

1981-01-01

Recent electronics technology advances make it possible to design sophisticated instruments in small packages for convenient field implementation. This report describes an inspector-instrument interface design which allows communication of procedures, responses, and results between the instrument and user. The interface has been incorporated into new spent-fuel instrumentation and a battery-powered multichannel analyzer

Development of thermocouple re-instrumentation technique for irradiated fuel rod. Techniques for making center hole into UO2 pellets and thermocouple re-instrumentation to fuel rod

International Nuclear Information System (INIS)

Shimizu, Michio; Saito, Junichi; Oshima, Kunio

1995-07-01

The information on FP gas pressure and centerline temperature of fuel pellets during power transient is important to study the pellet clad interaction (PCI) mechanism of high burnup LWR fuel rods. At the Department of JMTR, a re-instrumentation technique of FP gas pressure gage for an irradiated fuel rod was developed in 1990. Furthermore, a thermocouple re-instrumentation technique was successfully developed in 1994. Two steps were taken to carry out the development program of the thermocouple re-instrumentation technique. In the first step, a drilling technique was developed for making a center hole of the irradiated fuel pellets. Various drilling tests were carried out using dummy of fuel rods consisted of Ba 2 FeO 3 pellets and Zry-2 cladding. On this work it is important to keep the pellets just the state cracked at a power reactor. In these tests, the technique to fix the pellets by frozen CO 2 was used during the drilling work. Also, diamond drills were used to make the center hole. These tests were completed successfully. A center hole, 54mm depth and 2.5mm diameter, was realized by these methods. The second step of this program is the in-pile demonstration test on an irradiated fuel rod instrumented dually a thermocouple and FP gas pressure gage. The demonstration test was carried out at the JMTR in 1995. (author)

Project management for complex ground-based instruments: MEGARA plan

Science.gov (United States)

García-Vargas, María. Luisa; Pérez-Calpena, Ana; Gil de Paz, Armando; Gallego, Jesús; Carrasco, Esperanza; Cedazo, Raquel; Iglesias, Jorge

2014-08-01

The project management of complex instruments for ground-based large telescopes is a challenge itself. A good management is a clue for project success in terms of performance, schedule and budget. Being on time has become a strict requirement for two reasons: to assure the arrival at the telescope due to the pressure on demanding new instrumentation for this first world-class telescopes and to not fall in over-costs. The budget and cash-flow is not always the expected one and has to be properly handled from different administrative departments at the funding centers worldwide distributed. The complexity of the organizations, the technological and scientific return to the Consortium partners and the participation in the project of all kind of professional centers working in astronomical instrumentation: universities, research centers, small and large private companies, workshops and providers, etc. make the project management strategy, and the tools and procedures tuned to the project needs, crucial for success. MEGARA (Multi-Espectrógrafo en GTC de Alta Resolución para Astronomía) is a facility instrument of the 10.4m GTC (La Palma, Spain) working at optical wavelengths that provides both Integral-Field Unit (IFU) and Multi-Object Spectrograph (MOS) capabilities at resolutions in the range R=6,000-20,000. The project is an initiative led by Universidad Complutense de Madrid (Spain) in collaboration with INAOE (Mexico), IAA-CSIC (Spain) and Universidad Politécnica de Madrid (Spain). MEGARA is being developed under contract with GRANTECAN.

Key to Language Learning Success

Directory of Open Access Journals (Sweden)

Oktavian Mantiri

2015-01-01

Full Text Available This paper looks at the important elements of language learning and teaching i.e. the role of teachers as well as the attitude and motivation of learners. Teachers undoubtedly play crucial roles in students’ language learning outcome which could ignite or diminish students’ motivation. Positive attitudes and motivation – instrumental or integrative and intrinsic or extrinsic – are key to successful learning. Therefore it is paramount for language teachers as well as learners to know these roles and nurture the best possible ways where language teaching and learning will thrive. This paper also suggested that both stake-holders should be open to holistic approach of language learning and that other factors such as the environment could play an important part in language teaching and learning success.

Using a graphical programming language to write CAMAC/GPIB instrument drivers

Science.gov (United States)

Zambrana, Horacio; Johanson, William

1991-01-01

To reduce the complexities of conventional programming, graphical software was used in the development of instrumentation drivers. The graphical software provides a standard set of tools (graphical subroutines) which are sufficient to program the most sophisticated CAMAC/GPIB drivers. These tools were used and instrumentation drivers were successfully developed for operating CAMAC/GPIB hardware from two different manufacturers: LeCroy and DSP. The use of these tools is presented for programming a LeCroy A/D Waveform Analyzer.

In Situ Analysis of Mars Soil and Rocks Sample with the Sam Gcms Instrumentation Onboard Curiosity : Interpretation and Comparison of Measurements Done during the First Martian Year of Curiosity on Mars

Science.gov (United States)

Szopa, C.; Coll, P. J.; Cabane, M.; Buch, A.; Coscia, D.; Millan, M.; Francois, P.; Belmahadi, I.; Teinturier, S.; Navarro-Gonzalez, R.; Glavin, D. P.; Freissinet, C.; Steele, A.; Eigenbrode, J. L.; Mahaffy, P. R.

2014-12-01

The characterisation of the chemical and mineralogical composition of solid surface samples collected with the Curiosity rover is a primary objective of the SAM experiment. These data should provide essential clues on the past habitability of Gale crater. Amongst the SAM suite of instruments [1], SAM-GC (Gas Chromatograph) is devoted to identify and quantify volatiles evolved from the thermal (heating up to about 900°C)/chemical (derivatization procedure) treatment of any soil sample collected by the Curiosity rover. With the aim to search for potential organic molecules outgassed from the samples, SAM-GC analytical channels composed of thermal-desorption injector, and a MXT-CLP or a MXT-Q chromatographic column was chosen to achieve all the measurements done up today, with the aim to separate of a wide range of volatile inorganic and organic molecules. Four solid samples have been analyzed with GCMS, one sand sample collected at the Rocknest site, two rock samples (John Klein and Cumberland respectively) collected at the Yellowknife Bay site using the Curiosity driller, and one rock sample collected at the Kimberly site. All the measurements were successful and they produced complex chromatograms with both detectors used for SAM GC, i.e. a thermal conductivity detector and the SAM quandrupole mass spectrometer. Their interpretation already revealed the presence of an oxychlorine phase present in the sample which is at the origin of chlorohydrocarbons clearly identified [2] but this represents only a fraction of the GCMS signal recorded [3,4]. This work presents a systematic comparison of the GCMS measurements done for the different samples collected, supported by reference data obtained in laboratory with different spare models of the gas chromatograph, with the aim to bring new elements of interpretation of the SAM measurements. References: [1] Mahaffy, P. et al. (2012) Space Sci Rev, 170, 401-478. [2] Glavin, D. et al. (2013), JGR. [3] Leshin L. et al. (2013

Microbial Habitability in Gale Crater: Sample Analysis at Mars (SAM) Instrument Detection of Microbial Essential Carbon and Nitrogen

Science.gov (United States)

Sutter, B.; Ming, D. W.; Eigenbrode, J. E.; Steele, A.; Stern, J. C.; Gonzalez, R. N.; McAdam, A. C.; Mahaffy, P. R.

2016-01-01

Chemical analyses of Mars soils and sediments from previous landed missions have demonstrated that Mars surface materials possessed major (e.g., P, K, Ca, Mg, S) and minor (e.g., Fe, Mn, Zn, Ni, Cl) elements essential to support microbial life. However, the detection of microbial essential organic-carbon (C) and nitrate have been more elusive until the Mars Science Laboratory (MSL) rover mission. Nitrate and organic-C in Gale Crater, Mars have been detected by the Sample Analysis at Mars (SAM) instrument onboard the MSL Curiosity rover. Eolian fines and drilled sedimentary rock samples were heated in the SAM oven from approximately 30 to 860 degrees Centigrade where evolved gases (e.g., nitrous oxide (NO) and CO2) were released and analyzed by SAM’s quadrupole mass spectrometer (MS). The temperatures of evolved NO was assigned to nitrate while evolved CO2 was assigned to organic-C and carbonate. The CO2 releases in several samples occurred below 450 degrees Centigrade suggesting organic-C dominated in those samples. As much as 7 micromoles NO3-N per gram and 200 micromoles CO2-C per gram have been detected in the Gale Crater materials. These N and C levels coupled with assumed microbial biomass (9 x 10 (sup -7) micrograms per cell) C (0.5 micrograms C per micrograms cell) and N (0.14 micrograms N per micrograms cell) requirements, suggests that less than 1 percent and less than 10 percent of Gale Crater C and N, respectively, would be required if available, to accommodate biomass requirements of 1 by 10 (sup 5) cells per gram sediment. While nitrogen is the limiting nutrient, the potential exists that sufficient N and organic-C were present to support limited heterotrophic microbial populations that may have existed on ancient Mars.

Service quality in banking: developing and testing measurement instrument with Latvian sample data

Directory of Open Access Journals (Sweden)

Jelena Titko

2013-01-01

Full Text Available The paper highlights the importance of managing service quality in banking that can positively affect customer satisfaction. The goal of the given study is to develop an instrument for measuring service quality perceived by Latvian banks’ retail customers and to determine the most important contributors to customer satisfaction. To achieve this purpose, randomly selected customers of Latvian banks were surveyed, using the authors’ developed questionnaire. The proposed instrument was tested for reliability and validity, using techniques of confirmatory factor analysis. Exploratory factor analysis yielded five service quality dimensions (factors that allowed constructing customer satisfaction factor model EPICA: E – expenses, P – product, I – image, C – competence and emotional intellect, A – access. The subsequent correlation analysis revealed that the strongest relationship is between customer satisfaction and C factor. The results of the current research are crucially important for Latvian banks’ executives because the majority of previous studies in the related field offered measurement scales adequate for measuring service quality in other industries. Besides, the proposed questionnaire is exclusively developed for Latvia and considers Latvian banking sector specifics.

Research on seamless development of surgical instruments based on biological mechanisms using CAD and 3D printer.

Science.gov (United States)

Yamamoto, Ikuo; Ota, Ren; Zhu, Rui; Lawn, Murray; Ishimatsu, Takakazu; Nagayasu, Takeshi; Yamasaki, Naoya; Takagi, Katsunori; Koji, Takehiko

2015-01-01

In the area of manufacturing surgical instruments, the ability to rapidly design, prototype and test surgical instruments is critical. This paper provides a simple case study of the rapid development of two bio-mechanism based surgical instruments which are ergonomic, aesthetic and were successfully designed, prototyped and conceptually tested in a very short period of time.

Feedback to Managers, Volume II: A Review and Comparison of Sixteen Multi-Rater Feedback Instruments.

Science.gov (United States)

Van Velsor, Ellen; Leslie, Jean Brittain

"Feedback to Managers" is a two-volume report. Volume 2 compares 16 of the better feedback instruments available. The following are the instruments: (1) ACUMEN Group Feedback; (2) BENCHMARKS; (3) the Campbell Leadership Index; (4) COMPASS: the Managerial Practices Survey; (5) the Executive Success Profile; (6) Leader Behavior Analysis…

How Sample Size Affects a Sampling Distribution

Science.gov (United States)

Mulekar, Madhuri S.; Siegel, Murray H.

2009-01-01

If students are to understand inferential statistics successfully, they must have a profound understanding of the nature of the sampling distribution. Specifically, they must comprehend the determination of the expected value and standard error of a sampling distribution as well as the meaning of the central limit theorem. Many students in a high…

VINCI: the VLT Interferometer commissioning instrument

Science.gov (United States)

Kervella, Pierre; Coudé du Foresto, Vincent; Glindemann, Andreas; Hofmann, Reiner

2000-07-01

The Very Large Telescope Interferometer (VLTI) is a complex system, made of a large number of separated elements. To prepare an early successful operation, it will require a period of extensive testing and verification to ensure that the many devices involved work properly together, and can produce meaningful data. This paper describes the concept chosen for the VLTI commissioning instrument, LEONARDO da VINCI, and details its functionalities. It is a fiber based two-way beam combiner, associated with an artificial star and an alignment verification unit. The technical commissioning of the VLTI is foreseen as a stepwise process: fringes will first be obtained with the commissioning instrument in an autonomous mode (no other parts of the VLTI involved); then the VLTI telescopes and optical trains will be tested in autocollimation; finally fringes will be observed on the sky.

Detection of Reduced Nitrogen Compounds at Rocknest Using the Sample Analysis At Mars (SAM) Instrument on the Mars Science Laboratory (MSL)

Science.gov (United States)

Stern, J. C.; Steele, A.; Brunner, A.; Coll, P.; Eigenbrode, J.; Franz, H. B.; Freissinet, C.; Glavin, D.; Jones, J. H.; Navarro-Gonzalez, R.;

Mode of delivery following successful external cephalic version: comparison with spontaneous cephalic presentations at delivery.

Science.gov (United States)

Kuppens, Simone M I; Hutton, Eileen K; Hasaart, Tom H M; Aichi, Nassira; Wijnen, Henrica A; Pop, Victor J M

2013-10-01

To compare the obstetric outcomes of pregnant women after successful external cephalic version (ECV) (cases) with a large group of pregnant women with a spontaneously occurring cephalic fetal position at delivery (controls). We conducted a retrospective matched cohort study in a teaching hospital in the Netherlands. Delivery outcomes of women with a successful ECV were compared with those of women with spontaneously occurring cephalic presentations, controlling for maternal age, parity, gestational age at delivery, and onset of labour (spontaneous or induced). Exclusion criteria were a history of Caesarean section, delivery at < 35 weeks, and elective Caesarean section. The primary outcome was the prevalence of Caesarean section and instrumental delivery in both groups; secondary outcomes were the characteristics of cases requiring intervention such as Caesarean section or instrumental delivery. Women who had a successful ECV had a significantly higher Caesarean section rate than the women in the control group (33/220 [15%] vs. 62/1030 [6.0 %]; P < 0.001). There was no difference in the incidence of instrumental delivery (20/220 [9.1%] vs. 103/1030 [10%]). Comparison of characteristics of women in the cases group showed that nulliparity, induction of labour, and occiput posterior presentation were associated with Caesarean section and instrumental deliveries. Compared with delivery of spontaneous cephalic presenta-tions, delivery of cephalic presenting babies following successful ECV is associated with an increased rate of Caesarean section, especially in nulliparous women and women whose labour is induced.

Using an Instrumented Drone to Probe Dust Devils on Oregon’s Alvord Desert

Directory of Open Access Journals (Sweden)

Brian Jackson

2018-01-01

Full Text Available Dust devils are low-pressure, small (many to tens of meters convective vortices powered by surface heating and rendered visible by lofted dust. Dust devils occur ubiquitously on Mars, where they may dominate the supply of atmospheric dust, and since dust contributes significantly to Mars’ atmospheric heat budget, dust devils probably play an important role in its climate. The dust-lifting capacity of a devil likely depends sensitively on its structure, particularly the wind and pressure profiles, but the exact dependencies are poorly constrained. Thus, the exact contribution to Mars’ atmosphere remains unresolved. Analog studies of terrestrial devils have provided some insights into dust devil dynamics and properties but have been limited to near-surface (few meters or relatively high altitude (hundreds of meters sampling. Automated aerial vehicles or drones, combined with miniature, digital instrumentation, promise a novel and uniquely powerful platform from which to sample dust devils at a wide variety of altitudes. In this article, we describe a pilot study using an instrumented quadcopter on an active field site in southeastern Oregon, which (to our knowledge has not previously been surveyed for dust devils. We present preliminary results from the encounters, including stereo image analysis and encounter footage collected onboard the drone. In spite of some technical difficulties, we show that a quadcopter can successfully navigate in an active dust devil, while collecting time-series data about the dust devil’s structure.

Fuel cell-based instrumentation for ethanol determination in alcoholic beverages, fermentations, and biofluids

Energy Technology Data Exchange (ETDEWEB)

Parry, K W

1988-01-01

The main aim of this project was to devise an alternative method for ethanol assay, employing an electrochemical fuel cell sensor. Thus, the early part of this thesis describes the work carried out in the development of a new analytical technique for this purpose. This work resulted in the production of a successful prototype unit which has led to the development of a commercial instrument, vis., the Lion Drinks Alcolmeter (DA-1) available from Lion Laboratories Ltd. The problem of determining the ethanol content of a fermenting liquor at any point during a fermentation process was also broached and a novel technique combining a flow dilution system, dynamic headspace analysis and a fuel cell sensor was developed. This procedure, suitably automated, will enable the ethanolic content of a fermenting beverage to be determined at any stage during a fermentation, the results obtained in this manner being in excellent agreement with those obtained gas chromatographically. Methods of extending the linear working range of a fuel cell-based sampling system are reported in the hope that the encouraging results obtained may initiate further progress in this field. Finally, the sensing system used in this work has also been utilized with an alternative sampling procedure for the determination of ethanol in biological fluids, mainly for clinical and forensic applications. This work has also led to the production of a commercial instrument, viz. the Lion AE-D3 Alcolmeter.

An integrated and accessible sample data library for Mars sample return science

Science.gov (United States)

Tuite, M. L., Jr.; Williford, K. H.

2015-12-01

Over the course of the next decade or more, many thousands of geological samples will be collected and analyzed in a variety of ways by researchers at the Jet Propulsion Laboratory (California Institute of Technology) in order to facilitate discovery and contextualize observations made of Mars rocks both in situ and here on Earth if samples are eventually returned. Integration of data from multiple analyses of samples including petrography, thin section and SEM imaging, isotope and organic geochemistry, XRF, XRD, and Raman spectrometry is a challenge and a potential obstacle to discoveries that require supporting lines of evidence. We report the development of a web-accessible repository, the Sample Data Library (SDL) for the sample-based data that are generated by the laboratories and instruments that comprise JPL's Center for Analysis of Returned Samples (CARS) in order to facilitate collaborative interpretation of potential biosignatures in Mars-analog geological samples. The SDL is constructed using low-cost, open-standards-based Amazon Web Services (AWS), including web-accessible storage, relational data base services, and a virtual web server. The data structure is sample-centered with a shared registry for assigning unique identifiers to all samples including International Geo-Sample Numbers. Both raw and derived data produced by instruments and post-processing workflows are automatically uploaded to online storage and linked via the unique identifiers. Through the web interface, users are able to find all the analyses associated with a single sample or search across features shared by multiple samples, sample localities, and analysis types. Planned features include more sophisticated search and analytical interfaces as well as data discoverability through NSF's EarthCube program.

Development and evaluation of the Korean Health Literacy Instrument.

Science.gov (United States)

Kang, Soo Jin; Lee, Tae Wha; Paasche-Orlow, Michael K; Kim, Gwang Suk; Won, Hee Kwan

2014-01-01

The purpose of this study is to develop and validate the Korean Health Literacy Instrument, which measures the capacity to understand and use health-related information and make informed health decisions in Korean adults. In Phase 1, 33 initial items were generated to measure functional, interactive, and critical health literacy with prose, document, and numeracy tasks. These items included content from health promotion, disease management, and health navigation contexts. Content validity assessment was conducted by an expert panel, and 11 items were excluded. In Phase 2, the 22 remaining items were administered to a convenience sample of 292 adults from community and clinical settings. Exploratory factor and item difficulty and discrimination analyses were conducted and four items with low discrimination were deleted. In Phase 3, the remaining 18 items were administered to a convenience sample of 315 adults 40-64 years of age from community and clinical settings. A confirmatory factor analysis was performed to test the construct validity of the instrument. The Korean Health Literacy Instrument has a range of 0 to 18. The mean score in our validation study was 11.98. The instrument exhibited an internal consistency reliability coefficient of 0.82, and a test-retest reliability of 0.89. The instrument is suitable for screening individuals who have limited health literacy skills. Future studies are needed to further define the psychometric properties and predictive validity of the Korean Health Literacy Instrument.

Fetal scalp blood sampling during labor

DEFF Research Database (Denmark)

Chandraharan, Edwin; Wiberg, Nana

2014-01-01

Fetal cardiotocography is characterized by low specificity; therefore, in an attempt to ensure fetal well-being, fetal scalp blood sampling has been recommended by most obstetric societies in the case of a non-reassuring cardiotocography. The scientific agreement on the evidence for using fetal...... scalp blood sampling to decrease the rate of operative delivery for fetal distress is ambiguous. Based on the same studies, a Cochrane review states that fetal scalp blood sampling increases the rate of instrumental delivery while decreasing neonatal acidosis, whereas the National Institute of Health...... and Clinical Excellence guideline considers that fetal scalp blood sampling decreases instrumental delivery without differences in other outcome variables. The fetal scalp is supplied by vessels outside the skull below the level of the cranial vault, which is likely to be compressed during contractions...

Metering instrument of quality factor Q of gravitational wave antenna

International Nuclear Information System (INIS)

Jia-yan, C.; Tong-ren, G.

1982-01-01

The quality factor, Q, of gravitational wave antenna depends on the material property as well as external conditions, such as temperature, residual pressure in vacuum tank, support type, additional loss from transducer on antenna, etc. In order to find out the relationship between the antenna Q and external conditions automatical operating in succession is required. The authors have designed and made a metering instrument for quality factor Q. The metering instrument of Q can measure Q of the metal cylinder and other bar of higher Q. It can give data of the measurement at regular intervals as desired. It can measure accurately the longitudinal fundamental mode frequency of the cylinder with a digital frequency meter record oscillating signal from metering instrument. Because the metering instrument excites free-vibration of the cylinder with free-running type and keep up the stationary amplitude for a long time. (Auth.)

What Do Companies in the Processing Industry do in Order to Achieve Success?

Directory of Open Access Journals (Sweden)

Peter BONA

2015-04-01

Full Text Available Borders of countries and continents have become more and more blurred by now, while distances have turned out to be less important. Markets of continents or countries are not separated anymore therefore competition between companies has gotten fiercer and much faster than earlier. What kind of instruments may companies in the processing industry use to maintain their existence and to remain competitive in the fragile system following the economic crisis in 2008? This research aims at finding out how the effects of components belonging to the concept of strategic management system influence outstanding achievement and success. It primarily analyses, in what ways instruments considered being the most determinative, i.e. strategic a structural success factors affect the processing industry. In order to do that the research defines the factors having an influence. Thereafter it explains successful operation of companies with factors emerging via the use of regression models. It uses the balance scorecard as a tool for success criteria describing success. The research tackles the issue of sustainability with a high priority in this system as a success component: the fifth perspective among the other four classic ones. Thus the results of the research will show how strategic and structural success factors can make a company successful and the satisfaction of which groups of interest they affect the most.

Derivative financial instruments and nonprofit health care providers.

Science.gov (United States)

Stewart, Louis J; Owhoso, Vincent

2004-01-01

This article examines the extent of derivative financial instrument use among US nonprofit health systems and the impact of these financial instruments on their cash flows, reported operating results, and financial risks. Our examination is conducted through a case study of New Jersey hospitals and health systems. We review the existing literature on interest rate derivative instruments and US hospitals and health systems. This literature describes the design of these derivative financial instruments and the theoretical benefits of their use by large health care provider organizations. Our contribution to the literature is to provide an empirical evaluation of derivative financial instruments usage among a geographically limited sample of US nonprofit health systems. We reviewed the audited financial statements of the 49 community hospitals and multi-hospital health systems operating in the state of New Jersey. We found that 8 percent of New Jersey's nonprofit health providers utilized interest rate derivatives with an aggregate principle value of $229 million. These derivative users combine interest rate swaps and caps to lower the effective interest costs of their long-term debt while limiting their exposure to future interest rate increases. In addition, while derivative assets and liabilities have an immaterial balance sheet impact, derivative related gains and losses are a material component of their reported operating results. We also found that derivative usage among these four health systems was responsible for generating positive cash flows in the range of 1 percent to 2 percent of their total 2001 cash flows from operations. As a result of our admittedly limited samples we conclude that interest rate swaps and caps are effective risk management tools. However, we also found that while these derivative financial instruments are useful hedges against the risks of issuing long-term financing instruments, they also expose derivative users to credit, contract

Comparison of textural atributes of selected meat sausages using instrumental analysis

OpenAIRE

Vladimír Vietoris; Ľubomír Lopašovský; Peter Zajác; Jozef Čurlej; Jozef Čapla

2013-01-01

The aim of the study was to compare textural atributes of selected meat sausages using instrumental analysis. For this purpose, seven different meat sausage samples were treated by instrumental analysis, by the use of Warner-Bratzler probe,  to find differences for two selected textural parameter firmness and work of shear. As expected, various values of mentioned atributes were obtained for different samples tested in fresh stage and after storage under controlled conditions (48 hrs., 30 °...

Continuous high-temperature surveillance instrumentation for Dresden-2 hydrogen water chemistry program

International Nuclear Information System (INIS)

Fleming, M.F.; Mitchell, R.A.; Nelson, J.L.

1987-01-01

The objective of this program (under EPRI Contract RP1930-11) is to install and operate a high-temperature surveillance instrumentation system capable of monitoring the length of cracks in boiling water reactor (BWR) piping during plant operation. The ability to measure crack growth in BWR power plant piping welds is important to rapidly identify the effectiveness of repairs (such as the Hydrogen Water Chemistry Program). The feasibility of a system capable of continuous ultrasonic instrumentation at 600 0 F (288 0 C) was successfully demonstrated at the Dresden-2 suction line known as N1B. This intergranular stress corrosion cracking (IGSCC) surveillance instrumentation is sound in principal, because it survived on N1B for a time period of more than nine months from April 1985 to January 1986 (the last time data were recorded). The redesigned low-profile transducer system used for this system operated successfully for the same nine-month time period. This low profile transducer fits in the two-inch space normally occupied by insulation. As a result of poor routing of the coaxial cables running from the low-profile transducer to the electrical feed-throughs between the drywell and containment, these cables melted. Other instrument cables nearby were not damaged

From theory based policy evaluation to SMART Policy Design: Lessons learned from 20 ex-post evaluations of energy efficiency instruments

International Nuclear Information System (INIS)

Harmelink, Mirjam; Harmsen, Robert; Nilsson, Lars

2007-01-01

This article presents the results of an in-depth ex-post analysis of 20 energy efficiency policy instruments applied across different sectors and countries. Within the AID-EE project, we reconstructed and analysed the implementation process of energy efficiency policy instruments with the aim to identify key factors behind successes and failures. The analysis was performed using a uniform methodology called 'theory based policy evaluation'. With this method the whole implementation process is assessed with the aim to identify: (i) the main hurdles in each step of the implementation process, (ii) key success factors for different types of instruments and (iii) the key indicators that need to be monitored to enable a sound evaluation of the energy efficiency instruments. Our analysis shows that: Energy efficiency policies often lack quantitative targets and clear timeframes; Often policy instruments have multiple and/or unclear objectives; The need for monitoring information does often not have priority in the design phase; For most instruments, monitoring information is collected on a regular basis. However, this information is often insufficient to determine the impact on energy saving, cost-effectiveness and target achievement of an instrument; Monitoring and verification of actual energy savings have a relatively low priority for most of the analyzed instruments. There is no such thing as the 'best' policy instrument. However, typical circumstances in which to apply different types of instruments and generic characteristics that determine success or failure can be identified. Based on the assessments and the experience from applying theory based policy evaluation ex-post, we suggest that this should already be used in the policy formulation and design phase of instruments. We conclude that making policy theory an integral and mandated part of the policy process would facilitate more efficient and effective energy efficiency instruments

An Exploratory Factor Analysis and Reliability Analysis of the Student Online Learning Readiness (SOLR) Instrument

Science.gov (United States)

Yu, Taeho; Richardson, Jennifer C.

2015-01-01

The purpose of this study was to develop an effective instrument to measure student readiness in online learning with reliable predictors of online learning success factors such as learning outcomes and learner satisfaction. The validity and reliability of the Student Online Learning Readiness (SOLR) instrument were tested using exploratory factor…

Design of a TFT-LCD Based Digital Automobile Instrument

Directory of Open Access Journals (Sweden)

Yunsong Xu

2014-01-01

instrument and gives an introduction to the sampling circuits and interfaces related to these signals. Following this is the functional categorizing of the circuit modules, such as video buffer circuit, CAN bus interface circuit, and TFT-LCD drive circuit. Additionally, the external EEPROM stores information of the vehicle for history data query, and the external FLASH enables the display of high quality figures. On the whole, the accomplished automobile instrument meets the requirements of automobile instrument markets with its characters of low cost, favorable compatibility, friendly interfaces, and easy upgrading.

Development and validation of an instrument to measure nurse educator perceived confidence in clinical teaching.

Science.gov (United States)

Nguyen, Van N B; Forbes, Helen; Mohebbi, Mohammadreza; Duke, Maxine

2017-12-01

Teaching nursing in clinical environments is considered complex and multi-faceted. Little is known about the role of the clinical nurse educator, specifically the challenges related to transition from clinician, or in some cases, from newly-graduated nurse to that of clinical nurse educator, as occurs in developing countries. Confidence in the clinical educator role has been associated with successful transition and the development of role competence. There is currently no valid and reliable instrument to measure clinical nurse educator confidence. This study was conducted to develop and psychometrically test an instrument to measure perceived confidence among clinical nurse educators. A multi-phase, multi-setting survey design was used. A total of 468 surveys were distributed, and 363 were returned. Data were analyzed using exploratory and confirmatory factor analyses. The instrument was successfully tested and modified in phase 1, and factorial validity was subsequently confirmed in phase 2. There was strong evidence of internal consistency, reliability, content, and convergent validity of the Clinical Nurse Educator Skill Acquisition Assessment instrument. The resulting instrument is applicable in similar contexts due to its rigorous development and validation process. © 2017 The Authors. Nursing & Health Sciences published by John Wiley & Sons Australia, Ltd.

On-line calibration of process instrumentation channels in nuclear power plants

Energy Technology Data Exchange (ETDEWEB)

Hashemian, H.M.; Farmer, J.P. [Analysis and Measurement Services Corp., Knoxville, TN (United States)

1995-04-01

An on-line instrumentation monitoring system was developed and validated for use in nuclear power plants. This system continuously monitors the calibration status of instrument channels and determines whether or not they require manual calibrations. This is accomplished by comparing the output of each instrument channel to an estimate of the process it is monitoring. If the deviation of the instrument channel from the process estimate is greater than an allowable limit, then the instrument is said to be {open_quotes}out of calibration{close_quotes} and manual adjustments are made to correct the calibration. The success of the on-line monitoring system depends on the accuracy of the process estimation. The system described in this paper incorporates both simple intercomparison techniques as well as analytical approaches in the form of data-driven empirical modeling to estimate the process. On-line testing of the calibration of process instrumentation channels will reduce the number of manual calibrations currently performed, thereby reducing both costs to utilities and radiation exposure to plant personnel.

An instrument design and sample strategy for measuring soil respiration in the coastal temperate rain forest

Science.gov (United States)

Nay, S. M.; D'Amore, D. V.

2009-12-01

The coastal temperate rainforest (CTR) along the northwest coast of North America is a large and complex mosaic of forests and wetlands located on an undulating terrain ranging from sea level to thousands of meters in elevation. This biome stores a dynamic portion of the total carbon stock of North America. The fate of the terrestrial carbon stock is of concern due to the potential for mobilization and export of this store to both the atmosphere as carbon respiration flux and ocean as dissolved organic and inorganic carbon flux. Soil respiration is the largest export vector in the system and must be accurately measured to gain any comprehensive understanding of how carbon moves though this system. Suitable monitoring tools capable of measuring carbon fluxes at small spatial scales are essential for our understanding of carbon dynamics at larger spatial scales within this complex assemblage of ecosystems. We have adapted instrumentation and developed a sampling strategy for optimizing replication of soil respiration measurements to quantify differences among spatially complex landscape units of the CTR. We start with the design of the instrument to ease the technological, ergonomic and financial barriers that technicians encounter in monitoring the efflux of CO2 from the soil. Our sampling strategy optimizes the physical efforts of the field work and manages for the high variation of flux measurements encountered in this difficult environment of rough terrain, dense vegetation and wet climate. Our soil respirometer incorporates an infra-red gas analyzer (LiCor Inc. LI-820) and an 8300 cm3 soil respiration chamber; the device is durable, lightweight, easy to operate and can be built for under $5000 per unit. The modest unit price allows for a multiple unit fleet to be deployed and operated in an intensive field monitoring campaign. We use a large 346 cm2 collar to accommodate as much micro spatial variation as feasible and to facilitate repeated measures for tracking

The high resolution optical instruments for the Pleiades HR Earth observation satellites

Science.gov (United States)

Gaudin-Delrieu, Catherine; Lamard, Jean-Luc; Cheroutre, Philippe; Bailly, Bruno; Dhuicq, Pierre; Puig, Olivier

2017-11-01

Coming after the SPOT satellites series, PLEIADESHR is a CNES optical high resolution satellite dedicated to Earth observation, part of a larger optical and radar multi-sensors system, ORFEO, which is developed in cooperation between France and Italy for dual Civilian and Defense use. The development of the two PLEIADES-HR cameras was entrusted by CNES to Thales Alenia Space. This new generation of instrument represents a breakthrough in comparison with the previous SPOT instruments owing to a significant step in on-ground resolution, which approaches the capabilities of aerial photography. The PLEIADES-HR instrument program benefits from Thales Alenia Space long and successful heritage in Earth observation from space. The proposed solution benefits from an extensive use of existing products, Cannes Space Optics Centre facilities, unique in Europe, dedicated to High Resolution instruments. The optical camera provides wide field panchromatic images supplemented by 4 multispectral channels with narrow spectral bands. The optical concept is based on a four mirrors Korsch telescope. Crucial improvements in detector technology, optical fabrication and electronics make it possible for the PLEIADES-HR instrument to achieve the image quality requirements while respecting the drastic limitations of mass and volume imposed by the satellite agility needs and small launchers compatibility. The two flight telescopes were integrated, aligned and tested. After the integration phase, the alignment, mainly based on interferometric measurements in vacuum chamber, was successfully achieved within high accuracy requirements. The wave front measurements show outstanding performances, confirmed, after the integration of the PFM Detection Unit, by MTF measurements on the Proto-Flight Model Instrument. Delivery of the proto flight model occurred mi-2008. The FM2 Instrument delivery is planned Q2-2009. The first optical satellite launch of the PLEIADES-HR constellation is foreseen

Local density measurement of additive manufactured copper parts by instrumented indentation

Science.gov (United States)

Santo, Loredana; Quadrini, Fabrizio; Bellisario, Denise; Tedde, Giovanni Matteo; Zarcone, Mariano; Di Domenico, Gildo; D'Angelo, Pierpaolo; Corona, Diego

2018-05-01

Instrumented flat indentation has been used to evaluate local density of additive manufactured (AM) copper samples with different relative density. Indentations were made by using tungsten carbide (WC) flat pins with 1 mm diameter. Pure copper powders were used in a selective laser melting (SLM) machine to produce samples to test. By changing process parameters, samples density was changed from the relative density of 63% to 71%. Indentation tests were performed on the xy surface of the AM samples. In order to make a correlation between indentation test results and sample density, the indentation pressure at fixed displacement was selected. Results show that instrumented indentation is a valid technique to measure density distribution along the geometry of an SLM part. In fact, a linear trend between indentation pressure and sample density was found for the selected density range.

Characterization of a traceable profiler instrument for areal roughness measurement

International Nuclear Information System (INIS)

Thomsen-Schmidt, P

2011-01-01

A two-dimensional profiler instrument was designed and realized at the PTB (Physikalisch-Technische Bundesanstalt). The main function of the instrument is to provide traceable results in the field of roughness measurement. It is equipped with a linear moving stylus which is guided by precision air bearings. The moving part of the stylus has weight around 1 g and is carried by a magnetic field. The contacting force of the tip onto the surface under test is controlled by a small voice coil actuator in a closed control loop. Vertical movements of the stylus are captured by two different, completely independent measurement systems, covering a range of 100 µm. The first one is an interferometer, which provides a traceable signal, and the second one is an inductive measurement system. The signal from the inductive measurement system is calibrated by the interferometer. The sample under test is carried within the x–y-plane by a linear guided table with low noise air bearings. These air bearings are preloaded by vacuum and a constant gap is achieved by gas pressure controllers. Both axes of the table are driven by linear voice coil actuators and their movement in the plane is measured by linear encoders. The sample carrier is equipped with two axes tilt compensation, by which the sample under test can be levelled automatically using the measurement system of the stylus. Real-time data acquisition, manual handling and automated procedures are managed by a programmable controller and proprietary software written in LabVIEW. After measurement, data from the system can be directly transferred into the smd- or sdf-format. Results of measurements on different samples to characterize the metrological behaviour of the instrument will be reported. To characterize the uncertainty of the instrument, a model is applied, which is in accordance with approved rules for contact stylus instruments

Disturbance induced by surface preparation on instrumented indentation test

International Nuclear Information System (INIS)

Li, Yugang; Kanouté, Pascale; François, Manuel

2015-01-01

Surface preparation, which may induce considerable sample disturbance, plays an important role in instrumented indentation test (IIT). In this study, the sample disturbance (mainly divided into residual stresses and plastic strain) induced by the surface preparation process of instrumented indentation test specimens were investigated with both experimental tests and numerical simulations. Grazing incidence X-ray diffractions (GIXRD) and uniaxial tensile tests were conducted for characterizing the residual stresses and high plastic strain in the top surface layers of a carefully mechanically polished indentation sample, which, in the present work, is made of commercially pure titanium. Instrumented indentation tests and the corresponding finite element simulations were performed as well. For comparison, a reference sample (carefully mechanically polished & electrolytically polished) which represents the raw material was prepared and tested. Results showed that a careful mechanical polishing procedure can effectively reduce the level of residual stresses induced by this process. However, the high plastic strain in the surface region imposed by the polishing process is significant. The induced plastic strain can affect a depth up to 5 µm, which is deeper than the maximum penetration depth h max (3 µm) used for the instrumented indentation tests. In the near surface layer (in the range of depth about 350 nm), the plastic strain levels are fairly high. In the very top layer, the plastic strain was even estimated to reach more than 60%. The simultaneous use of indentation tests and numerical simulations showed that the existence of high plastic strain in the surface region will make the load vs depth (P–h) curve shift upwards, the contact hardness (H) increase and the contact stiffness (S) decrease

Disturbance induced by surface preparation on instrumented indentation test

Energy Technology Data Exchange (ETDEWEB)

Li, Yugang, E-mail: yugang.li@utt.fr [Université de Technologie de Troyes (UTT), ICD-LASMIS, UMR CNRS 6281, 12, rue Marie Curie-CS 42060, 10010 Troyes Cedex (France); Kanouté, Pascale, E-mail: pascale.kanoute@onera.fr [Université de Technologie de Troyes (UTT), ICD-LASMIS, UMR CNRS 6281, 12, rue Marie Curie-CS 42060, 10010 Troyes Cedex (France); The French Aerospace Lab (ONERA), DMSM/MCE, 29 avenue de la Division Leclerc-BP 72, F-92322 Chatillon Cedex (France); François, Manuel, E-mail: manuel.francois@utt.fr [Université de Technologie de Troyes (UTT), ICD-LASMIS, UMR CNRS 6281, 12, rue Marie Curie-CS 42060, 10010 Troyes Cedex (France)

2015-08-26

Surface preparation, which may induce considerable sample disturbance, plays an important role in instrumented indentation test (IIT). In this study, the sample disturbance (mainly divided into residual stresses and plastic strain) induced by the surface preparation process of instrumented indentation test specimens were investigated with both experimental tests and numerical simulations. Grazing incidence X-ray diffractions (GIXRD) and uniaxial tensile tests were conducted for characterizing the residual stresses and high plastic strain in the top surface layers of a carefully mechanically polished indentation sample, which, in the present work, is made of commercially pure titanium. Instrumented indentation tests and the corresponding finite element simulations were performed as well. For comparison, a reference sample (carefully mechanically polished & electrolytically polished) which represents the raw material was prepared and tested. Results showed that a careful mechanical polishing procedure can effectively reduce the level of residual stresses induced by this process. However, the high plastic strain in the surface region imposed by the polishing process is significant. The induced plastic strain can affect a depth up to 5 µm, which is deeper than the maximum penetration depth h{sub max} (3 µm) used for the instrumented indentation tests. In the near surface layer (in the range of depth about 350 nm), the plastic strain levels are fairly high. In the very top layer, the plastic strain was even estimated to reach more than 60%. The simultaneous use of indentation tests and numerical simulations showed that the existence of high plastic strain in the surface region will make the load vs depth (P–h) curve shift upwards, the contact hardness (H) increase and the contact stiffness (S) decrease.

Overview: Field instrumentation - A Mikado's dream

International Nuclear Information System (INIS)

Spittler, T.M.

1992-01-01

The Mikado of Gilbert ampersand Sullivan fame held out as an open-quotes object all sublimeclose quotes which he hoped to open-quotes achieve in timeclose quotes the fitting of the punishment to the crime. Like that potentate, I too have long held the hope of finding instrumentation which is ideally suited to measurement of environmental contaminants in the field. Today, at least one of us has had that dream fulfilled. For years, those of us interested in field analysis have had to apply time consuming and cumbersome methods to relatively simple and often short-term environmental measurement problems. Meanwhile, we watched the literature and perused the product blurbs in hopes of finding the ideal tools for on-site, real time analysis. Of course, that search will always go forward as better instruments are developed. Today we can finally point to many pieces of equipment that are on the market and which provide high quality data in real time for a number of the most important environmental contaminants. Furthermore, the sensitivity of some of these field instruments exceeds that of conventional lab instrumentation. Coupled with innovative techniques for sample preparation and proper quality control, field instrumentation can often go a long way to solving problems in rapid detection, quantitation, and positive identification

In Situ Identification of Mineral Resources with an X-Ray-Optical "Hands-Lens" Instrument

Science.gov (United States)

Marshall, J.; Koppel, L.; Bratton, C.; Metzger, E.; Hecht, M.

1999-09-01

The recognition of material resources on a planetary surface requires exploration strategies not dissimilar to those employed by early field geologists who searched for ore deposits primarily from surface clues. In order to determine the location of mineral ores or other materials, it will be necessary to characterize host terranes at regional or subregional scales. This requires geographically broad surveys in which statistically significant numbers of samples are rapidly scanned from a roving platform. To enable broad-scale, yet power-conservative planetary-surface exploration, we are developing an instrument that combines x-ray diffractometry (XRD), x-ray fluorescence spectrometry (XRF), and optical capabilities; the instrument can be deployed at the end of a rover's robotic arm, without the need for sample capture or preparation. The instrument provides XRD data for identification of mineral species and lithological types; diffractometry of minerals is conducted by ascertaining the characteristic lattice parameters or "d-spacings" of mineral compounds. D-spacings of 1.4 to 25 angstroms can be determined to include the large molecular structures of hydrated minerals such as clays. The XRF data will identify elements ranging from carbon (Atomic Number = 6) to elements as heavy as barium (Atomic Number = 56). While a sample is being x-rayed, the instrument simultaneously acquires an optical image of the sample surface at magnifications from lx to at least 50x (200x being feasible, depending on the sample surface). We believe that imaging the sample is extremely important as corroborative sample-identification data (the need for this capability having been illustrated by the experience of the Pathfinder rover). Very few geologists would rely on instrument data for sample identification without having seen the sample. Visual inspection provides critical recognition data such as texture, crystallinity, granularity, porosity, vesicularity, color, lustre, opacity, and

Instrumentation renewal at the FIR 1 research reactor in Finland

International Nuclear Information System (INIS)

Bars, Bruno; Kall, Leif

1982-01-01

The Finnish TRIGA Mark II reactor (FIR 1 100 kW, later 250 kW steady state power and pulsing capability up to 250 MW) has been in operation for 20 years. The reactor is the only research reactor in Finland and is an important research training and service facility, which obviously will be operated for 10...20 years ahead. The mechanical parts of the reactor are in good shape. Some minor modifications have previously been made in the instrumentation. However, the original instrumentation could hardly have been used for 10...20 years ahead without extensive modifications and modernization. After a careful evaluation and planning process the whole reactor instrumentation was renewed in 1981 at a cost of about 400 000 dollar. The renewal was carried out in cooperation with the Central Research Institute for Physics (KFKI) at the Hungarian Academy of Sciences, which delivered the nuclear part of the instrumentation and with the Finnish company Valmet Oy Instrument Works, which delivered the conventional instrumentation, including the automatic power control system and the control console. The instrumentation, which is located in-a new isolated control room is based on modern industrial standard modular units with standardized signal ranges, electronic testing possibilities, galvanically isolated outputs etc. The instrument renewal project was brought successfully to completion in November 1981 after only about 10 working days of shut down time. The reactor is now in routine operation and the experiences gained from the new instrumentation are excellent. (author)

Musical Sound, Instruments, and Equipment

Science.gov (United States)

Photinos, Panos

2017-12-01

'Musical Sound, Instruments, and Equipment' offers a basic understanding of sound, musical instruments and music equipment, geared towards a general audience and non-science majors. The book begins with an introduction of the fundamental properties of sound waves, and the perception of the characteristics of sound. The relation between intensity and loudness, and the relation between frequency and pitch are discussed. The basics of propagation of sound waves, and the interaction of sound waves with objects and structures of various sizes are introduced. Standing waves, harmonics and resonance are explained in simple terms, using graphics that provide a visual understanding. The development is focused on musical instruments and acoustics. The construction of musical scales and the frequency relations are reviewed and applied in the description of musical instruments. The frequency spectrum of selected instruments is explored using freely available sound analysis software. Sound amplification and sound recording, including analog and digital approaches, are discussed in two separate chapters. The book concludes with a chapter on acoustics, the physical factors that affect the quality of the music experience, and practical ways to improve the acoustics at home or small recording studios. A brief technical section is provided at the end of each chapter, where the interested reader can find the relevant physics and sample calculations. These quantitative sections can be skipped without affecting the comprehension of the basic material. Questions are provided to test the reader's understanding of the material. Answers are given in the appendix.

MSL Chemistry and Mineralogy X-Ray Diffraction X-Ray Fluorescence (CheMin) Instrument

Science.gov (United States)

Zimmerman, Wayne; Blake, Dave; Harris, William; Morookian, John Michael; Randall, Dave; Reder, Leonard J.; Sarrazin, Phillipe

2013-01-01

This paper provides an overview of the Mars Science Laboratory (MSL) Chemistry and Mineralogy Xray Diffraction (XRD), X-ray Fluorescence (XRF) (CheMin) Instrument, an element of the landed Curiosity rover payload, which landed on Mars in August of 2012. The scientific goal of the MSL mission is to explore and quantitatively assess regions in Gale Crater as a potential habitat for life - past or present. The CheMin instrument will receive Martian rock and soil samples from the MSL Sample Acquisition/Sample Processing and Handling (SA/SPaH) system, and process it utilizing X-Ray spectroscopy methods to determine mineral composition. The Chemin instrument will analyze Martian soil and rocks to enable scientists to investigate geophysical processes occurring on Mars. The CheMin science objectives and proposed surface operations are described along with the CheMin hardware with an emphasis on the system engineering challenges associated with developing such a complex instrument.

A critical appraisal of instruments to measure outcomes of interprofessional education.

Science.gov (United States)

Oates, Matthew; Davidson, Megan

2015-04-01

Interprofessional education (IPE) is believed to prepare health professional graduates for successful collaborative practice. A range of instruments have been developed to measure the outcomes of IPE. An understanding of the psychometric properties of these instruments is important if they are to be used to measure the effectiveness of IPE. This review set out to identify instruments available to measure outcomes of IPE and collaborative practice in pre-qualification health professional students and to critically appraise the psychometric properties of validity, responsiveness and reliability against contemporary standards for instrument design. Instruments were selected from a pool of extant instruments and subjected to critical appraisal to determine whether they satisfied inclusion criteria. The qualitative and psychometric attributes of the included instruments were appraised using a checklist developed for this review. Nine instruments were critically appraised, including the widely adopted Readiness for Interprofessional Learning Scale (RIPLS) and the Interdisciplinary Education Perception Scale (IEPS). Validity evidence for instruments was predominantly based on test content and internal structure. Ceiling effects and lack of scale width contribute to the inability of some instruments to detect change in variables of interest. Limited reliability data were reported for two instruments. Scale development and scoring protocols were generally reported by instrument developers, but the inconsistent application of scoring protocols for some instruments was apparent. A number of instruments have been developed to measure outcomes of IPE in pre-qualification health professional students. Based on reported validity evidence and reliability data, the psychometric integrity of these instruments is limited. The theoretical test construction paradigm on which instruments have been developed may be contributing to the failure of some instruments to detect change in

SASSI: Subsystems for Automated Subsurface Sampling Instruments, Phase I

Data.gov (United States)

National Aeronautics and Space Administration — Future robotic planetary exploration missions will benefit greatly from the ability to capture rock and/or regolith core samples that deliver the stratigraphy of the...

NESSE - New Standards in Sample Environment

International Nuclear Information System (INIS)

Schober, H.; Lelievre-Berna, E.

2011-01-01

The actual sample environment equipments suite has been designed for instruments built a few decades ago. Since then, we have considerably improved the ILL instruments and the experiments are slowed down by the performance of the sample environment. We propose to establish a new standard that will permit to exploit the new-generation instruments and to develop the environments not presently available for investigating novel scientific challenges. Not only we need reliable equipments covering very large ranges of temperature, pressure, magnetic and electric fields, we must also be able to change the physical parameters much more rapidly as well as exchanging samples automatically. Further to these needs, there are many scientific challenges that cannot be investigated without specific equipment presently unavailable at ILL. For example, among many subjects, high-pressure gas-handling systems are required to improve the storage of hydrogen; specific pressure cells would contribute to the optimization of the food distribution and ultra-high temperature furnaces would allow us to investigate the preparation process of ceramics, cement and refracting materials

Instrumentation

International Nuclear Information System (INIS)

Prieur, G.; Nadi, M.; Hedjiedj, A.; Weber, S.

1995-01-01

This second chapter on instrumentation gives little general consideration on history and classification of instrumentation, and two specific states of the art. The first one concerns NMR (block diagram of instrumentation chain with details on the magnets, gradients, probes, reception unit). The first one concerns precision instrumentation (optical fiber gyro-meter and scanning electron microscope), and its data processing tools (programmability, VXI standard and its history). The chapter ends with future trends on smart sensors and Field Emission Displays. (D.L.). Refs., figs

determination of thiobencarb in water samples by gas

African Journals Online (AJOL)

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The proposed method was successfully applied to analysis of thiobencarb in the ... The principle of competitive immunoassay is based on a specific competitive reaction between ... be performed by instrumental techniques. Homogeneous ...

SALSA-A new instrument for strain imaging in engineering materials and components

International Nuclear Information System (INIS)

Pirling, Thilo; Bruno, Giovanni; Withers, Philip J.

2006-01-01

Residual stresses are very hard to predict and if undetected can lead to premature failure or unexpected behaviour of engineering materials or components. This paper describes the operation of a new residual strain-mapping instrument, Strain Analyser for Large and Small scale engineering Applications (SALSA), recently commissioned at the public user facility, the Institut Laue-Langevin in Grenoble, France. A unique feature of this neutron diffraction instrument is the sample manipulator, which is the first of its kind, allowing precise scanning of large and heavy (<500 kg) samples along any trajectory involving translations, tilts and rotations. Other notable features of the instrument are also described

Instrumentation for Structure Measurements on Highly Non-equilibrium Materials

Energy Technology Data Exchange (ETDEWEB)

Weber, Richard [Argonne National Laboratory (ANL); Benmore, Chris J [Argonne National Laboratory (ANL); Neuefeind, Joerg C [ORNL; Wilding, Martin C [ORNL

2011-01-01

Containerless techniques (levitation) completely eliminate contact with the sample. This unique sample environment allows deep supercooling of many liquids and avoids contamination of high temperature melts. Recent experiments at the APS high energy beamline 11 ID-C used aerodynamic levitation with laser beam heating and acoustic levitation with cryogenic cooling. By using these two methods, liquids were studied over much of the temperature range from -40 to +2500 C. This paper briefly describes the instrumentation and its use with an -Si area detector that allows fast, in-situ measurements. Use of the instruments is illustrated with examples of measurements on molten oxides and aqueous materials.

The Basic Design Report of the 40M SANS Instrument

Energy Technology Data Exchange (ETDEWEB)

Han, Young Soo; Lee, Chang Hee; Hwang, Dong Gil; Kim, Hak Rho [Korea Atomic Energy Research Institute, Daejeon (Korea, Republic of); Kim, Tae Hwan; Choi, Sung Min [Korea Advanced Institute of Science and Technology, Daejeon (Korea, Republic of)

2006-04-15

The HANARO cold neutron research facility project was launched on July 1, 2003. A state of the art SANS instrument was selected as a top-priority instrument by an instrument selection committee, which consisted of domestic users and HANARO personnel. An instrument development team and an international and domestic instrument advisory team were formulated. The guide and the instrument simulation were performed using Vitess software and the optimum basic design was completed based on the simulation results and the international advisory team reviews. The optimum design of the guide for the 40M SANS instrument was completed and the optimum basic design of the 40M the SANS instrument was also completed based on the Vitess simulation results. The Q range of the instrument will cover from 0.0008 to 1.0 A-1 and the maximum flux at a sample position can reach about 5.5x10 7 n/cm2sec. The simulation results and the basic design product will be used for the detailed design and the construction of the SANS instrument. The simulation results could be applied to the development of the other instrument.

Performing T-tests to Compare Autocorrelated Time Series Data Collected from Direct-Reading Instruments.

Science.gov (United States)

O'Shaughnessy, Patrick; Cavanaugh, Joseph E

2015-01-01

Industrial hygienists now commonly use direct-reading instruments to evaluate hazards in the workplace. The stored values over time from these instruments constitute a time series of measurements that are often autocorrelated. Given the need to statistically compare two occupational scenarios using values from a direct-reading instrument, a t-test must consider measurement autocorrelation or the resulting test will have a largely inflated type-1 error probability (false rejection of the null hypothesis). A method is described for both the one-sample and two-sample cases which properly adjusts for autocorrelation. This method involves the computation of an "equivalent sample size" that effectively decreases the actual sample size when determining the standard error of the mean for the time series. An example is provided for the one-sample case, and an example is given where a two-sample t-test is conducted for two autocorrelated time series comprised of lognormally distributed measurements.

Problems in instrumentation for S-odorant emissions

International Nuclear Information System (INIS)

Hall, H.J.

1974-01-01

Instrumentation to measure sulfur-containing odorants in stack emissions is much more difficult than in the ambient atmosphere, and must be matched to the specific source: key components aside from H 2 S are methyl mercaptan in paper mills, COS/CS 2 in a refinery Claus plant, and SO 2 /SO 3 in a combustion stack. Satisfactory operation for a period of six months was not achieved by any instrument in this service, in a lab and field evaluation of eight instruments of three types commercially available as of 1971. The effects of interferent gases H 2 O, SO 2 , CO 2 /CO and particulates which are diluted in ambient samples are greatly aggravated in stack gases, where the ratio of odorant to interferent may be 1:1000 or less, due to the very great sensitivity of human receptors to S-odorants. The most serious problem proved to be the analysis for odorless carbonyl sulfide, which is commonly formed where S compounds are oxidized in a reducing atmosphere. This COS has been undetected or mistaken for odorous H 2 S in most analyses. A field instrument for the general case would provide exactly simultaneous readings at five minute intervals or less for the five components H 2 S, SO 2 , COS, CSH, and total S, or their equivalent. This may be simplified to four components or less only when the composition of the sample gas is positively known

Human Resource Outsourcing Success

Directory of Open Access Journals (Sweden)

Hasliza Abdul-Halim

2014-07-01

Full Text Available The existing literature on partnership seems to take the relationship between partnership quality and outsourcing success for granted. Therefore, this article aims at examining the role of service quality in strengthening the relationship between partnership quality and human resource (HR outsourcing success. The samples were obtained from 96 manufacturing organizations in Penang, Malaysia. The results showed that partnership quality variables such as trust, business understanding, and communication have significant positive impact on HR outsourcing success, whereas in general, service quality was found to partially moderate these relationships. Therefore, comprehending the HR outsourcing relationship in the context of service quality may assist the organizations to accomplish HR outsourcing success by identifying areas of expected benefits and improvements.

Design of analytical instrumentation with D-T sealed neutron generators

International Nuclear Information System (INIS)

Qiao Yahua; Wu Jizong; Zheng Weiming; Liu Quanwei; Zhang Min

2008-01-01

Analytical instrumentation with D-T sealed neutron generators source activation, The 14 MeV D-T sealed neutron tube with 10 9 n · s -1 neutron yield is used as generator source. The optimal structure of moderator and shield was achieved by MC computing.The instrumentation's configuration is showed. The instrumentation is made up of the SMY-DT50.8-2.1 sealed neutron tube and the high-voltage power supply system, which center is the sealed neutron generators. 6 cm Pb and 20 cm polythene is chosen as moderator, Pb, polythene and 10 cm boron-PE was chosen as shield .The sample box is far the source from 9 cm, the measurement system were made up of HPGe detector and the sample transforming system. After moderator and shield, the thermal neutron fluence rate at the point of sample is 0.93 × 10 6 n · s -1 cm -2 , which is accorded with design demand, and the laboratory and surroundings reaches the safety standard of the dose levels. (authors)

Validation of method in instrumental NAA for food products sample

International Nuclear Information System (INIS)

Alfian; Siti Suprapti; Setyo Purwanto

2010-01-01

NAA is a method of testing that has not been standardized. To affirm and confirm that this method is valid. it must be done validation of the method with various sample standard reference materials. In this work. the validation is carried for food product samples using NIST SRM 1567a (wheat flour) and NIST SRM 1568a (rice flour). The results show that the validation method for testing nine elements (Al, K, Mg, Mn, Na, Ca, Fe, Se and Zn) in SRM 1567a and eight elements (Al, K, Mg, Mn, Na, Ca, Se and Zn ) in SRM 1568a pass the test of accuracy and precision. It can be conclude that this method has power to give valid result in determination element of the food products samples. (author)

Instrumentation

Energy Technology Data Exchange (ETDEWEB)

Decreton, M

2001-04-01

SCK-CEN's research and development programme on instrumentation involves the assessment and the development of sensitive measurement systems used within a radiation environment. Particular emphasis is on the assessment of optical fibre components and their adaptability to radiation environments. The evaluation of ageing processes of instrumentation in fission plants, the development of specific data evaluation strategies to compensate for ageing induced degradation of sensors and cable performance form part of these activities. In 2000, particular emphasis was on in-core reactor instrumentation applied to fusion, accelerator driven and water-cooled fission reactors. This involved the development of high performance instrumentation for irradiation experiments in the BR2 reactor in support of new instrumentation needs for MYRRHA, and for diagnostic systems for the ITER reactor.

Instrumentation

International Nuclear Information System (INIS)

Decreton, M.

2001-01-01

SCK-CEN's research and development programme on instrumentation involves the assessment and the development of sensitive measurement systems used within a radiation environment. Particular emphasis is on the assessment of optical fibre components and their adaptability to radiation environments. The evaluation of ageing processes of instrumentation in fission plants, the development of specific data evaluation strategies to compensate for ageing induced degradation of sensors and cable performance form part of these activities. In 2000, particular emphasis was on in-core reactor instrumentation applied to fusion, accelerator driven and water-cooled fission reactors. This involved the development of high performance instrumentation for irradiation experiments in the BR2 reactor in support of new instrumentation needs for MYRRHA, and for diagnostic systems for the ITER reactor

Development of a Computerized Multifunctional Form and Position Measurement Instrument

International Nuclear Information System (INIS)

Liu, P; Tian, W Y

2006-01-01

A model machine of multifunctional form and position measurement instrument controlled by a personal computer has been successfully developed. The instrument is designed in rotary table type with a high precision air bearing and the radial rotation error of the rotary table is 0.08 μm. Since a high precision vertical sliding carriage supported by an air bearing is used for the instrument, the straightaway motion error of the carriage is 0.3 μm/200 mm and the parallelism error of the motion of the carriage relative to the rotation axis of the rotary table is 0.4 μm/200 mm. The mathematical models have been established for assessing planar and spatial straightness, flatness, roundness, cylindricity, and coaxality errors. By radial deviation measurement, the instrument can accurately measure form and position errors of such workpieces as shafts, round plates and sleeves of medium or small dimensions with the tolerance grades mostly used in industry

Challenges and achievements of instrumentation for failed fuel identification in PFBR

International Nuclear Information System (INIS)

Upadhyay, Chandra Kant; Sivaramakrishna, M.; Nageswaran, A.; Nagaraj, C.P.; Madhusoodanan, K.; Krishnakumar, B.

2010-01-01

Failed fuel identification system is provided to locate and remove the failed fuel sub assembly. It comprises of selector valve mechanism to sample the flow from each assembly and associated instrumentation to detect the activity in the sample, indicating the clad failure of the respective subassembly. The development includes sampling pump, its power supply, motor to rotate the selector valve, encoder, brake, gear box, neutron detectors and Instrumentation and Control for all these with interlocks and related logic. These systems are expected to work under many physical constraints and in harsh environmental conditions, such as high temperature. This paper discusses the various challenges and achievements towards this system design. (author)

Three instruments for positron annihilation spectroscopy (PAS)

International Nuclear Information System (INIS)

Ivanov, E.A.; Plostinaru, D.; Catana, D.; Racolta, P.M.; Vata, I.

2003-01-01

The instruments presented here and dedicated to positron annihilation spectroscopy, PAS, are: 1. High Resolution Life Time Spectrometer (LTS) with time resolution τ = 260 ps, based on large BaF 2 scintillators; 2. Doppler Broadening Spectrometer (DBS) having a 1.6 keV resolution at 514 keV; 3. Positronium Life Time - Perturbed Angular Distribution Spectrometer ( PLT-PAD); positronium life time, in samples under high vacuum in magnetic field, is measured for time intervals up to 500 ns. Results of measurements are shown to illustrate performances of the instruments. (authors)

Development Instruments Through Confirmatory Factor Analysis (CFA in Appropriate Intensity Assessment

Directory of Open Access Journals (Sweden)

Ari Saptono

2017-06-01

Full Text Available The research aims to develop the valid and reliable measurement instruments of entrepreneurship intention in vocational secondary school students. Multi stage random sampling was used as the technique to determine sample (300 respondents. The research method used research and development with confirmatory factor analysis (CFA. Result of confirmatory factor analysis (CFA at the second order with robust maximum likelihood method shows that valid and reliable instrument with the acquisition value of loading factor is more than 0.5 (> 0,5 and a significance value of t is more than 1,96 (> 1,96. Reliability test results shows that the value of the combined construct reliability (CR of 0.97and a variance value extract (VE to 0.52 is greater than the limit of acceptance CR ≥ 0.70 and VE ≥ 0.50. The conclusion of the measurement instruments of entrepreneurship intention with three dimensions and 31 items met the standards of validity and reliability in accordance with the instrument development process.

Neutrons and music: Imaging investigation of ancient wind musical instruments

Energy Technology Data Exchange (ETDEWEB)

Festa, G., E-mail: giulia.festa@roma2.infn.it [Università degli Studi di Roma Tor Vergata (Italy); Università degli Studi di Milano-Bicocca (Italy); Consiglio Nazionale delle Ricerche-IPCF, Messina (Italy); Tardino, G. [BauArt Basel, Basel (Switzerland); Pontecorvo, L. [Conservatorio di Cosenza – Cosenza Conservatory (Italy); Mannes, D.C. [Paul Scherrer Institut, Villigen (Switzerland); Senesi, R. [Università degli Studi di Roma Tor Vergata (Italy); Consiglio Nazionale delle Ricerche-IPCF, Messina (Italy); Gorini, G. [Università degli Studi di Milano-Bicocca (Italy); Andreani, C. [Università degli Studi di Roma Tor Vergata (Italy); Consiglio Nazionale delle Ricerche-IPCF, Messina (Italy)

2014-10-01

A set of seven musical instruments and two instruments cares from the ‘Fondo Antico della Biblioteca del Sacro Convento’ in Assisi, Italy, were investigated through neutron and X-ray imaging techniques. Historical and scientific interests around ancient musical instruments motivate an intense research effort for their characterization using non-destructive and non-invasive techniques. X-ray and neutron tomography/radiography were applied to the study of composite material samples containing wood, hide and metals. The study was carried out at the NEUTRA beamline, PSI (Paul Scherrer Institute, Switzerland). Results of the measurements provided new information on the composite and multi-scale structure, such as: the internal structure of the samples, position of added materials like metals, wood fiber displays, deformations, presence of adhesives and their spatial distribution and novel insight about construction methods to guide the instruments’ restoration process.

Neutrons and music: Imaging investigation of ancient wind musical instruments

International Nuclear Information System (INIS)

Festa, G.; Tardino, G.; Pontecorvo, L.; Mannes, D.C.; Senesi, R.; Gorini, G.; Andreani, C.

2014-01-01

A set of seven musical instruments and two instruments cares from the ‘Fondo Antico della Biblioteca del Sacro Convento’ in Assisi, Italy, were investigated through neutron and X-ray imaging techniques. Historical and scientific interests around ancient musical instruments motivate an intense research effort for their characterization using non-destructive and non-invasive techniques. X-ray and neutron tomography/radiography were applied to the study of composite material samples containing wood, hide and metals. The study was carried out at the NEUTRA beamline, PSI (Paul Scherrer Institute, Switzerland). Results of the measurements provided new information on the composite and multi-scale structure, such as: the internal structure of the samples, position of added materials like metals, wood fiber displays, deformations, presence of adhesives and their spatial distribution and novel insight about construction methods to guide the instruments’ restoration process

INAA of human and animal whole blood samples by short term reactor irradiation. [Au, Br, Cd, Ce, Cl, Cr, Cu, Fe, Hg, K, La, Mn, Na, P, Sc, Zn

Energy Technology Data Exchange (ETDEWEB)

Samudralwar, D L; Garg, A N

1986-11-03

Instrumental neutron activation analysis was employed for the determination of 15 major, minor and trace elements in human and animal blood samples. Dry whole blood samples along with NBS and IAEA standards were irradiated for 5 min, 1 h, 5 h and 10 h with reactor thermal neutrons and counted using high resolution ..gamma..-spectrometry at successive intervals. Data for a new IAEA proposed CRM Mixed Human Diet (H-9) is reported. 28 references, 4 tables.

Thermo Scientific Ozone Analyzer Instrument Handbook

Energy Technology Data Exchange (ETDEWEB)

Springston, S. R. [Brookhaven National Lab. (BNL), Upton, NY (United States)

2016-03-01

The primary measurement output from the Thermo Scientific Ozone Analyzer is the concentration of the analyte (O3) reported at 1-s resolution in units of ppbv in ambient air. Note that because of internal pneumatic switching limitations the instrument only makes an independent measurement every 4 seconds. Thus, the same concentration number is repeated roughly 4 times at the uniform, monotonic 1-s time base used in the AOS systems. Accompanying instrument outputs include sample temperatures, flows, chamber pressure, lamp intensities and a multiplicity of housekeeping information. There is also a field for operator comments made at any time while data is being collected.

Standardization of portable assay instrumentation: the neutron-coincidence tree

International Nuclear Information System (INIS)

Menlove, H.O.

1983-01-01

Standardization of portable neutron assay instrumentation has been achieved by using the neutron coincidence technique as a common basis for a wide range of instruments and applications. The electronics originally developed for the High-Level Neutron Coincidence Counter has been adapted to both passive- and active-assay instrumentation for field verification of bulk plutonium, inventory samples, pellets, powders, nitrates, high-enriched uranium, and materials-testing-reactor, light-water-reactor, and mixed-oxide fuel assemblies. The family of detectors developed at Los Alamos National Laboratory and their performance under in-field conditions are described. 16 figures, 3 tables

DNA Profiling Success Rates from Degraded Skeletal Remains in Guatemala.

Science.gov (United States)

Johnston, Emma; Stephenson, Mishel

2016-07-01

No data are available regarding the success of DNA Short Tandem Repeat (STR) profiling from degraded skeletal remains in Guatemala. Therefore, DNA profiling success rates relating to 2595 skeletons from eleven cases at the Forensic Anthropology Foundation of Guatemala (FAFG) are presented. The typical postmortem interval was 30 years. DNA was extracted from bone powder and amplified using Identifiler and Minifler. DNA profiling success rates differed between cases, ranging from 50.8% to 7.0%, the overall success rate for samples was 36.3%. The best DNA profiling success rates were obtained from femur (36.2%) and tooth (33.7%) samples. DNA profiles were significantly better from lower body bones than upper body bones (p = <0.0001). Bone samples from males gave significantly better profiles than samples from females (p = <0.0001). These results are believed to be related to bone density. The findings are important for designing forensic DNA sampling strategies in future victim recovery investigations. © 2016 American Academy of Forensic Sciences.

Electronic instrumentation system for pulsed neutron measurements

International Nuclear Information System (INIS)

Burda, J.; Igielski, A.; Kowalik, W.

1982-01-01

An essential point of pulsed neutron measurement of thermal neutron parameters for different materials is the registration of the thermal neutron die-away curve after a fast neutron bursts have been injected into the system. An electronic instrumentation system which is successfully applied for pulsed neutron measurements is presented. An important part of the system is the control unit which has been designed and built in the Laboratory of Neutron Parameters of Materials. (author)

Modification of ion chromatograph for analyses of radioactive samples

International Nuclear Information System (INIS)

Curfman, L.L.; Johnson, S.J.

1979-01-01

In ion chromatographic analysis, the sample is injected through a sample loop onto an analytical column where separation occurs. The sample then passes through a suppressor column to remove or neutralize background ions. A flow-through conductivity cell is used as a detector. Depending upon column and eluent selection, ion chromatography can be used for anion or cation analyses. Ion chromatography has proven to be a versatile analytical tool for the analysis of anions in Hanford waste samples. These radioactive samples range from caustic high salt solutions to hydrochloric acid dissolutions of insoluble sludges. Instrument modifications which provide safe and convenient handling of these samples without lengthening analysis time or altering instrument performance are described

High resolution tomographic instrument development

International Nuclear Information System (INIS)

1992-01-01

Our recent work has concentrated on the development of high-resolution PET instrumentation reflecting in part the growing importance of PET in nuclear medicine imaging. We have developed a number of positron imaging instruments and have the distinction that every instrument has been placed in operation and has had an extensive history of application for basic research and clinical study. The present program is a logical continuation of these earlier successes. PCR-I, a single ring positron tomograph was the first demonstration of analog coding using BGO. It employed 4 mm detectors and is currently being used for a wide range of biological studies. These are of immense importance in guiding the direction for future instruments. In particular, PCR-II, a volume sensitive positron tomograph with 3 mm spatial resolution has benefited greatly from the studies using PCR-I. PCR-II is currently in the final stages of assembly and testing and will shortly be placed in operation for imaging phantoms, animals and ultimately humans. Perhaps the most important finding resulting from our previous study is that resolution and sensitivity must be carefully balanced to achieve a practical high resolution system. PCR-II has been designed to have the detection characteristics required to achieve 3 mm resolution in human brain under practical imaging situations. The development of algorithms by the group headed by Dr. Chesler is based on a long history of prior study including his joint work with Drs. Pelc and Reiderer and Stearns. This body of expertise will be applied to the processing of data from PCR-II when it becomes operational

High resolution tomographic instrument development

Energy Technology Data Exchange (ETDEWEB)

1992-08-01

Our recent work has concentrated on the development of high-resolution PET instrumentation reflecting in part the growing importance of PET in nuclear medicine imaging. We have developed a number of positron imaging instruments and have the distinction that every instrument has been placed in operation and has had an extensive history of application for basic research and clinical study. The present program is a logical continuation of these earlier successes. PCR-I, a single ring positron tomograph was the first demonstration of analog coding using BGO. It employed 4 mm detectors and is currently being used for a wide range of biological studies. These are of immense importance in guiding the direction for future instruments. In particular, PCR-II, a volume sensitive positron tomograph with 3 mm spatial resolution has benefited greatly from the studies using PCR-I. PCR-II is currently in the final stages of assembly and testing and will shortly be placed in operation for imaging phantoms, animals and ultimately humans. Perhaps the most important finding resulting from our previous study is that resolution and sensitivity must be carefully balanced to achieve a practical high resolution system. PCR-II has been designed to have the detection characteristics required to achieve 3 mm resolution in human brain under practical imaging situations. The development of algorithms by the group headed by Dr. Chesler is based on a long history of prior study including his joint work with Drs. Pelc and Reiderer and Stearns. This body of expertise will be applied to the processing of data from PCR-II when it becomes operational.

High resolution tomographic instrument development

Energy Technology Data Exchange (ETDEWEB)

1992-01-01

Our recent work has concentrated on the development of high-resolution PET instrumentation reflecting in part the growing importance of PET in nuclear medicine imaging. We have developed a number of positron imaging instruments and have the distinction that every instrument has been placed in operation and has had an extensive history of application for basic research and clinical study. The present program is a logical continuation of these earlier successes. PCR-I, a single ring positron tomograph was the first demonstration of analog coding using BGO. It employed 4 mm detectors and is currently being used for a wide range of biological studies. These are of immense importance in guiding the direction for future instruments. In particular, PCR-II, a volume sensitive positron tomograph with 3 mm spatial resolution has benefited greatly from the studies using PCR-I. PCR-II is currently in the final stages of assembly and testing and will shortly be placed in operation for imaging phantoms, animals and ultimately humans. Perhaps the most important finding resulting from our previous study is that resolution and sensitivity must be carefully balanced to achieve a practical high resolution system. PCR-II has been designed to have the detection characteristics required to achieve 3 mm resolution in human brain under practical imaging situations. The development of algorithms by the group headed by Dr. Chesler is based on a long history of prior study including his joint work with Drs. Pelc and Reiderer and Stearns. This body of expertise will be applied to the processing of data from PCR-II when it becomes operational.

ALADIN - Advanced Laue Diffraction Instruments using Neutrons

International Nuclear Information System (INIS)

Lemee-Cailleau, M.H.; Ouladdiaf, B.; McIntyre, G.J.

2011-01-01

Laue diffraction techniques have proven to be very attractive to a broad user community interested in obtaining detailed structural information on very small single-crystal samples or needing data collection speeds comparable to those available with the powder diffraction technique. However our experience has clearly demonstrated the negative effect of up-stream monochromatic instruments on the quality of Laue data. In order to obtain Laue diffraction data with a statistical accuracy similar to that achieved on a monochromatic instrument (neutron or X-rays), the project ALADIN (for Advanced Laue Diffraction Instruments using Neutrons) aims to: -) construct a Laue-dedicated thermal neutron guide, with m=2 super-mirror coating, providing access to the desirable wavelength bandwidth; -) installation of one of the ILL Laue diffractometers (VIVALDI or CYCLOPS) on this new guide. (authors)

Small-angle neutron scattering instrument at MINT

International Nuclear Information System (INIS)

Mohd Ali Sufi; Yusof Abdullah; Razali Kassim; Hamid; Shahidan Radiman; Mohammad Deraman; Abdul Ghaffar Ramli

1996-01-01

The Small Angle Neutron Scattering (SANS) Instrument has been developed at Malaysian Institute for Nuclear Technology Research (MINT) for studying structural properties of materials on the length scale 1 nm to 100 nm. This is the length scale which is relevant for many topics within soft condensed matter, like polymers, colloids, biological macromolecules, etc. The SANS is a complementary technique to X-ray and electron scattering. However, while these later techniques give information on structures near surface, SANS concerns the structure of the bulk. Samples studied by SANS technique are typically bulk materials of the sizes mm's to cm's, or materials dissolved in a liquid. This paper described the general characteristics of SANS instrument as well as the experimental formulation in neutron scattering. The preliminary results obtained by this instrument are shown

Instrument for Real-Time Digital Nucleic Acid Amplification on Custom Microfluidic Devices.

Directory of Open Access Journals (Sweden)

David A Selck

Full Text Available Nucleic acid amplification tests that are coupled with a digital readout enable the absolute quantification of single molecules, even at ultralow concentrations. Digital methods are robust, versatile and compatible with many amplification chemistries including isothermal amplification, making them particularly invaluable to assays that require sensitive detection, such as the quantification of viral load in occult infections or detection of sparse amounts of DNA from forensic samples. A number of microfluidic platforms are being developed for carrying out digital amplification. However, the mechanistic investigation and optimization of digital assays has been limited by the lack of real-time kinetic information about which factors affect the digital efficiency and analytical sensitivity of a reaction. Commercially available instruments that are capable of tracking digital reactions in real-time are restricted to only a small number of device types and sample-preparation strategies. Thus, most researchers who wish to develop, study, or optimize digital assays rely on the rate of the amplification reaction when performed in a bulk experiment, which is now recognized as an unreliable predictor of digital efficiency. To expand our ability to study how digital reactions proceed in real-time and enable us to optimize both the digital efficiency and analytical sensitivity of digital assays, we built a custom large-format digital real-time amplification instrument that can accommodate a wide variety of devices, amplification chemistries and sample-handling conditions. Herein, we validate this instrument, we provide detailed schematics that will enable others to build their own custom instruments, and we include a complete custom software suite to collect and analyze the data retrieved from the instrument. We believe assay optimizations enabled by this instrument will improve the current limits of nucleic acid detection and quantification, improving our

High-resolution space-time characterization of convective rain cells: implications on spatial aggregation and temporal sampling operated by coarser resolution instruments

Science.gov (United States)

Marra, Francesco; Morin, Efrat

2017-04-01

Forecasting the occurrence of flash floods and debris flows is fundamental to save lives and protect infrastructures and properties. These natural hazards are generated by high-intensity convective storms, on space-time scales that cannot be properly monitored by conventional instrumentation. Consequently, a number of early-warning systems are nowadays based on remote sensing precipitation observations, e.g. from weather radars or satellites, that proved effective in a wide range of situations. However, the uncertainty affecting rainfall estimates represents an important issue undermining the operational use of early-warning systems. The uncertainty related to remote sensing estimates results from (a) an instrumental component, intrinsic of the measurement operation, and (b) a discretization component, caused by the discretization of the continuous rainfall process. Improved understanding on these sources of uncertainty will provide crucial information to modelers and decision makers. This study aims at advancing knowledge on the (b) discretization component. To do so, we take advantage of an extremely-high resolution X-Band weather radar (60 m, 1 min) recently installed in the Eastern Mediterranean. The instrument monitors a semiarid to arid transition area also covered by an accurate C-Band weather radar and by a relatively sparse rain gauge network ( 1 gauge/ 450 km2). Radar quantitative precipitation estimation includes corrections reducing the errors due to ground echoes, orographic beam blockage and attenuation of the signal in heavy rain. Intense, convection-rich, flooding events recently occurred in the area serve as study cases. We (i) describe with very high detail the spatiotemporal characteristics of the convective cores, and (ii) quantify the uncertainty due to spatial aggregation (spatial discretization) and temporal sampling (temporal discretization) operated by coarser resolution remote sensing instruments. We show that instantaneous rain intensity

SHARK-NIR: from K-band to a key instrument, a status update

Science.gov (United States)

Farinato, Jacopo; Bacciotti, Francesca; Baffa, Carlo; Baruffolo, Andrea; Bergomi, Maria; Bongiorno, Angela; Carbonaro, Luca; Carolo, Elena; Carlotti, Alexis; Centrone, Mauro; Close, Laird; De Pascale, Marco; Dima, Marco; D'Orazi, Valentina; Esposito, Simone; Fantinel, Daniela; Farisato, Giancarlo; Gaessler, Wolfgang; Giallongo, Emanuele; Greggio, Davide; Guyon, Olivier; Hinz, Philip; Lisi, Franco; Magrin, Demetrio; Marafatto, Luca; Mohr, Lars; Montoya, Manny; Pedichini, Fernando; Pinna, Enrico; Puglisi, Alfio; Ragazzoni, Roberto; Salasnich, Bernardo; Stangalini, Marco; Vassallo, Daniele; Verinaud, Christophe; Viotto, Valentina

2016-07-01

SHARK-NIR channel is one of the two coronagraphic instruments proposed for the Large Binocular Telescope, in the framework of the call for second generation instruments, issued in 2014. Together with the SHARK-VIS channel, it will offer a few observing modes (direct imaging, coronagraphic imaging and coronagraphic low resolution spectroscopy) covering a wide wavelength domain, going from 0.5μm to 1.7μm. Initially proposed as an instrument covering also the K-band, the current design foresees a camera working from Y to H bands, exploiting in this way the synergy with other LBT instruments such as LBTI, which is actually covering wavelengths greater than L' band, and it will be soon upgraded to work also in K band. SHARK-NIR has been undergoing the conceptual design review at the end of 2015 and it has been approved to proceed to the final design phase, receiving the green light for successive construction and installation at LBT. The current design is significantly more flexible than the previous one, having an additional intermediate pupil plane that will allow the usage of coronagraphic techniques very efficient in term of contrast and vicinity to the star, increasing the instrument coronagraphic performance. The latter is necessary to properly exploit the search of giant exo-planets, which is the main science case and the driver for the technical choices of SHARK-NIR. We also emphasize that the LBT AO SOUL upgrade will further improve the AO performance, making possible to extend the exo-planet search to target fainter than normally achieved by other 8-m class telescopes, and opening in this way to other very interesting scientific scenarios, such as the characterization of AGN and Quasars (normally too faint to be observed) and increasing considerably the sample of disks and jets to be studied. Finally, we emphasize that SHARK-NIR will offer XAO direct imaging capability on a FoV of about 15"x15", and a simple coronagraphic spectroscopic mode offering spectral

Automatic HTS force measurement instrument

International Nuclear Information System (INIS)

Sanders, S.T.; Niemann, R.C.

1999-01-01

A device is disclosed for measuring the levitation force of a high temperature superconductor sample with respect to a reference magnet includes a receptacle for holding several high temperature superconductor samples each cooled to superconducting temperature. A rotatable carousel successively locates a selected one of the high temperature superconductor samples in registry with the reference magnet. Mechanism varies the distance between one of the high temperature superconductor samples and the reference magnet, and a sensor measures levitation force of the sample as a function of the distance between the reference magnet and the sample. A method is also disclosed. 3 figs

Measurement equivalence of the food related lifestyle instrument (FRL) in Ireland and Great Britain

DEFF Research Database (Denmark)

O´Sullivan, C.; Scholderer, Joachim; Cowan, Cathal

2005-01-01

The food-related lifestyle instrument (FRL) is tested for cross-cultural validity. Representative consumer samples from the UK 1998 ( N = 1000) and Ireland 2001 (N = 1024) are compared using multi-sample confirmatory factor analysis with structured means. The results suggest that, in all five FRL...... domains, the measurement characteristics of the survey instrument were completely invariant across the two cultures. No indication was found of any bias. Regarding future applications of the FRL, it can be concluded that the instrument has identical measurement characteristics when applied to consumer...

Improved sample size determination for attributes and variables sampling

International Nuclear Information System (INIS)

Stirpe, D.; Picard, R.R.

1985-01-01

Earlier INMM papers have addressed the attributes/variables problem and, under conservative/limiting approximations, have reported analytical solutions for the attributes and variables sample sizes. Through computer simulation of this problem, we have calculated attributes and variables sample sizes as a function of falsification, measurement uncertainties, and required detection probability without using approximations. Using realistic assumptions for uncertainty parameters of measurement, the simulation results support the conclusions: (1) previously used conservative approximations can be expensive because they lead to larger sample sizes than needed; and (2) the optimal verification strategy, as well as the falsification strategy, are highly dependent on the underlying uncertainty parameters of the measurement instruments. 1 ref., 3 figs

Aerothermal Instrumentation Loads To Implement Aeroassist Technology in Future Robotic and Human Missions to MARS and Other Locations Within the Solar System

Science.gov (United States)

Parmar, Devendra S.; Shams, Qamar A.

2002-01-01

The strategy of NASA to explore space objects in the vicinity of Earth and other planets of the solar system includes robotic and human missions. This strategy requires a road map for technology development that will support the robotic exploration and provide safety for the humans traveling to other celestial bodies. Aeroassist is one of the key elements of technology planning for the success of future robot and human exploration missions to other celestial bodies. Measurement of aerothermodynamic parameters such as temperature, pressure, and acceleration is of prime importance for aeroassist technology implementation and for the safety and affordability of the mission. Instrumentation and methods to measure such parameters have been reviewed in this report in view of past practices, current commercial availability of instrumentation technology, and the prospects of improvement and upgrade according to the requirements. Analysis of the usability of each identified instruments in terms of cost for efficient weight-volume ratio, power requirement, accuracy, sample rates, and other appropriate metrics such as harsh environment survivability has been reported.

Aggregated particles caused by instrument artifact

Directory of Open Access Journals (Sweden)

A. M. Pierce

2018-04-01

Full Text Available Previous studies have indicated that superaggregates, clusters of aggregates of soot primary particles, can be formed in large-scale turbulent fires. Due to lower effective densities, higher porosity, and lower aerodynamic diameters, superaggregates may pass through inlets designed to remove particles  <  2.5 µm in aerodynamic diameter (PM2.5. Ambient particulate matter samples were collected at Peavine Peak, NV, USA (2515 m northwest of Reno, NV, USA from June to November 2014. The Teledyne Advanced Pollution Instrumentation (TAPI 602 BetaPlus particulate monitor was used to collect PM2.5 on two filter types. During this time, aggregated particles  >  2.5 µm in aerodynamic diameter were collected on 36 out of 158 sample days. On preliminary analysis, it was thought that these aggregated particles were superaggregates, depositing past PM10 (particles  <  10 µm in aerodynamic diameter pre-impactors and PM2.5 cyclones. However, further analysis revealed that these aggregated particles were dissimilar to superaggregates observed in previous studies, both in morphology and in elemental composition. To determine if the aggregated particles were superaggregates or an instrument artifact, samples were investigated for the presence of certain elements, the occurrence of fires, high relative humidity and wind speeds, as well as the use of generators on site. Samples with aggregated particles, referred to as aggregates, were analyzed using a scanning electron microscope for size and shape and energy dispersive X-ray spectroscopy was used for elemental analysis. It was determined, based on the high amounts of aluminum present in the aggregate samples, that a sampling artifact associated with the sample inlet and prolonged, high wind events was the probable reason for the observed aggregates.

Considerations on measurements of radioactivity in biological samples

International Nuclear Information System (INIS)

Mascanzoni, D.

1986-01-01

Radioactivity in biological samples and particularly in foodstuffs can be measured with several procedures, depending on the type of sample and radiation. In case of a radioactive fallout like the one from Chernobyl 1986, contamination in biological samples varies with time, being high immediately after the accident and decreasing successively with time. During the first stage, accurate measurements of gamma-emission should be made with high-resolution instruments, like HPGe-detectors coupled to multichannel analyzers in order to be able to assess the fallout's composition and separate the different nuclides. Even portable GM-counters and NaI(Tl)-detectors can be used, but they provide very limited information and the resolution of NaI(Tl) is too poor to make them suitable for other than survey purposes. In this case, they can be used for monitoring the activity in a certain area, or scanning a large amount of samples. After some months, when the activity has decayed and only a few nuclides are still active, the most important parameter is not resolution any longer, but sensitivity, since the content of radionuclides has decreased. At this stage NaI(Tl)-detectors assume greater importance and their sensitivity can permit the detection of low activity levels in relatively short time. The laboratory procedures for sample handling and preparation is also very important: established routines concentrated upon reducing the risk of contamination and minimizing sources of error must be used

A preliminary study on identification of Thai rice samples by INAA and statistical analysis

Science.gov (United States)

Kongsri, S.; Kukusamude, C.

2017-09-01

This study aims to investigate the elemental compositions in 93 Thai rice samples using instrumental neutron activation analysis (INAA) and to identify rice according to their types and rice cultivars using statistical analysis. As, Mg, Cl, Al, Br, Mn, K, Rb and Zn in Thai jasmine rice and Sung Yod rice samples were successfully determined by INAA. The accuracy and precision of the INAA method were verified by SRM 1568a Rice Flour. All elements were found to be in a good agreement with the certified values. The precisions in term of %RSD were lower than 7%. The LODs were obtained in range of 0.01 to 29 mg kg-1. The concentration of 9 elements distributed in Thai rice samples was evaluated and used as chemical indicators to identify the type of rice samples. The result found that Mg, Cl, As, Br, Mn, K, Rb, and Zn concentrations in Thai jasmine rice samples are significantly different but there was no evidence that Al is significantly different from concentration in Sung Yod rice samples at 95% confidence interval. Our results may provide preliminary information for discrimination of rice samples and may be useful database of Thai rice.

LAMMA 500 principle and technical description of the instrument

International Nuclear Information System (INIS)

Vogt, H.; Heinen, H.J.; Meier, S.; Wechsung, R.

1981-01-01

The Laser Microprobe Mass Analyzer LAMMA 500 originally had been designed for the analysis of biomedical samples, especially thin sections, with high lateral resolution and extreme detection sensitivity. The principle of LAMMA is based on the excitation of a microvolume of the sample to an ionized state by a focused laser beam. The analytical information is derived from mass spectrometry of these ions. It is obvious that all elements of the periodic table and their isotopes can be detected. Various applications have demonstrated that besides element detection the instrument can also be used for the detection of organic and inorganic compounds. A detailed description of the LAMMA 500 instrument is given. (orig./RB)

Evaluation of surface characteristics of rotary nickel-titanium instruments produced by different manufacturing methods.

Science.gov (United States)

Inan, U; Gurel, M

2017-02-01

Instrument fracture is a serious concern in endodontic practice. The aim of this study was to investigate the surface quality of new and used rotary nickel-titanium (NiTi) instruments manufactured by the traditional grinding process and twisting methods. Total 16 instruments of two rotary NiTi systems were used in this study. Eight Twisted Files (TF) (SybronEndo, Orange, CA, USA) and 8 Mtwo (VDW, Munich, Germany) instruments were evaluated. New and used of 4 experimental groups were evaluated using an atomic force microscopy (AFM). New and used instruments were analyzed on 3 points along a 3 mm. section at the tip of the instrument. Quantitative measurements according to the topographical deviations were recorded. The data were statistically analyzed with paired samples t-test and independent samples t-test. Mean root mean square (RMS) values for new and used TF 25.06 files were 10.70 ± 2.80 nm and 21.58 ± 6.42 nm, respectively, and the difference between them was statistically significant (P instruments produced by twisting method (TF 25.06) had better surface quality than the instruments produced by traditional grinding process (Mtwo 25.06 files).

Falsification Testing of Instrumental Variables Methods for Comparative Effectiveness Research.

Science.gov (United States)

Pizer, Steven D

2016-04-01

To demonstrate how falsification tests can be used to evaluate instrumental variables methods applicable to a wide variety of comparative effectiveness research questions. Brief conceptual review of instrumental variables and falsification testing principles and techniques accompanied by an empirical application. Sample STATA code related to the empirical application is provided in the Appendix. Comparative long-term risks of sulfonylureas and thiazolidinediones for management of type 2 diabetes. Outcomes include mortality and hospitalization for an ambulatory care-sensitive condition. Prescribing pattern variations are used as instrumental variables. Falsification testing is an easily computed and powerful way to evaluate the validity of the key assumption underlying instrumental variables analysis. If falsification tests are used, instrumental variables techniques can help answer a multitude of important clinical questions. © Health Research and Educational Trust.

Determination of silver, gold, zinc and copper in mineral samples by various techniques of instrumental neutron activation analysis

International Nuclear Information System (INIS)

Rodriguez R, N. I.; Rios M, C.; Pinedo V, J. L.; Yoho, M.; Landsberger, S.

2015-09-01

Using the method of instrumental neutron activation analysis, mineral exploration samples were analyzed in order to determine the concentrations of silver, gold, zinc and copper; these minerals being the main products of benefit of Tizapa and Cozamin mines. Samples were subjected to various techniques, where the type of radiation and counting methods were chosen based on the specific isotopic characteristics of each element. For calibration and determination of concentrations the comparator method was used, certified standards were subjected to the same conditions of irradiation and measurement that the prospecting samples. The irradiations were performed at the research reactor TRIGA Mark II of the University of Texas at Austin. The silver concentrations were determined by Cyclical Epithermal Neutron Activation Analysis. This method in combination with the transfer pneumatic system allowed a good analytical precision and accuracy in prospecting for silver, from photo peak measurement 657.7 keV of short half-life radionuclide 110 Ag. For the determination of gold and zinc, Epithermal Neutron Activation Analysis was used, the photo peaks analyzed corresponded to the energies 411.8 keV of radionuclide 199 Au and 438.6 keV of metastable radionuclide 69m Zn. On the other hand, copper quantification was based on the photo peak analysis of 1039.2 keV produced by the short half-life radionuclide 66 Cu, by Thermal Neutron Activation Analysis. The photo peaks measurement corresponding to gold, zinc and copper was performed using a Compton suppression system, which allowed an improvement in the signal to noise relationship, so that better detection limits and low uncertainties associated with the results were obtained. Comparing elemental concentrations the highest values in silver, zinc and copper was for samples of mine Tizapa. Regarding gold values were found in the same range for both mines. To evaluate the precision and accuracy of the methods used, various geological

Performance acceptance test of a portable instrument to detect uranium in water at the DOE Advanced Waste Water Treatment Plant, Fernald, Ohio

International Nuclear Information System (INIS)

Anderson, M.S.; Weeks, S.J.

1997-01-01

The Eppendorf-Biotronik Model IC 2001-2, a portable field ruggedized ion chromatography instrument, was rigorously tested at the DOE Advanced Waste Water Treatment Plant, Fernald, Ohio. This instrument rapidly detected the uranium concentration in water, and has a detection limit in the low ppb range without using the sample concentrating feature. The test set of samples analyzed included: ''Real World'' water samples from the AWWT containing uranium concentrations in the 9--110 ppb range, a sample blank, and a performance evaluation sample. The AWWT samples contained sets of both raw water and acid-preserved water samples. Selected samples were analyzed in quadruplicate to asses the instrument's precision, and these results were compared with the results from an off-site confirmatory laboratory to assess the instrument's accuracy. Additional comparisons with on-site laboratory instruments, Chemcheck KPA-11 and Scintrex UA-3 are reported. Overall, the Eppendorf-Biotronik IC 2001-2 performed exceptionally well providing a detection limit in the low ppb region (< 10 ppb) and giving rapid (< 5 minutes) accurate and reproducible analytical results for the AWWT, ''real world'', water samples with uranium concentrations in the region of interest (10--40 ppb). The per sample operating cost for this instrument is equivalent to the per sample cost for the currently used KPA. The time required to analyze a sample and provide a result is approximately the same for the CI 2001-2, KPA, and Scintrex instruments

Recycled material-based science instruments to support science education in rural area at Central Sulawesi District of Indonesia

Science.gov (United States)

Ali, M.; Supriyatman; Saehana, S.

2018-03-01

It has been successfully designing low cost of science experiment from recycled materials. The science instruments were produced to explain expansion concept and hydrostatic pressure inside the liquid. Science instruments were calibrated and then validated. It was also implemented in science learning.

Radionuclide determination in environmental samples by inductively coupled plasma mass spectrometry

International Nuclear Information System (INIS)

Lariviere, Dominic; Taylor, Vivien F.; Evans, R. Douglas; Cornett, R. Jack

2006-01-01

The determination of naturally occurring and anthropogenic radionuclides in the environment by inductively coupled plasma mass spectrometry has gained recognition over the last fifteen years, relative to radiometric techniques, as the result of improvement in instrumental performance, sample introduction equipment, and sample preparation. With the increase in instrumental sensitivity, it is now possible to measure ultratrace levels (fg range) of many radioisotopes, including those with half-lives between 1 and 1000 years, without requiring very complex sample pre-concentration schemes. However, the identification and quantification of radioisotopes in environmental matrices is still hampered by a variety of analytical issues such as spectral (both atomic and molecular ions) and non-spectral (matrix effect) interferences and instrumental limitations (e.g., abundance sensitivity). The scope of this review is to highlight recent analytical progress and issues associated with the determination of radionuclides by inductively coupled plasma mass spectrometry. The impact of interferences, instrumental limitations (e.g., degree of ionization, abundance sensitivity, detection limits) and low sample-to-plasma transfer efficiency on the measurement of radionuclides by inductively coupled plasma mass spectrometry will be described. Solutions that overcome these issues will be discussed, highlighting their pros and cons and assessing their impact on the measurement of environmental radioactivity. Among the solutions proposed, mass and chemical resolution through the use of sector-field instruments and chemical reactions/collisions in a pressurized cell, respectively, will be described. Other methods, such as unique sample introduction equipment (e.g., laser ablation, electrothermal vaporisation, high efficiency nebulization) and instrumental modifications/optimizations (e.g., instrumental vacuum, radiofrequency power, guard electrode) that improve sensitivity and performance

The OCO-3 Mission: Science Objectives and Instrument Performance

Science.gov (United States)

Eldering, A.; Basilio, R. R.; Bennett, M. W.

2017-12-01

The Orbiting Carbon Observatory 3 (OCO-3) will continue global CO2 and solar-induced chlorophyll fluorescence (SIF) using the flight spare instrument from OCO-2. The instrument is currently being tested, and will be packaged for installation on the International Space Station (ISS) (launch readiness in early 2018.) This talk will focus on the science objectives, updated simulations of the science data products, and the outcome of recent instrument performance tests. The low-inclination ISS orbit lets OCO-3 sample the tropics and sub-tropics across the full range of daylight hours with dense observations at northern and southern mid-latitudes (+/- 52º). The combination of these dense CO2 and SIF measurements provides continuity of data for global flux estimates as well as a unique opportunity to address key deficiencies in our understanding of the global carbon cycle. The instrument utilizes an agile, 2-axis pointing mechanism (PMA), providing the capability to look towards the bright reflection from the ocean and validation targets. The PMA also allows for a snapshot mapping mode to collect dense datasets over 100km by 100km areas. Measurements over urban centers could aid in making estimates of fossil fuel CO2 emissions. Similarly, the snapshot mapping mode can be used to sample regions of interest for the terrestrial carbon cycle. In addition, there is potential to utilize data from ISS instruments ECOSTRESS (ECOsystem Spaceborne Thermal Radiometer Experiment on Space Station) and GEDI (Global Ecosystem Dynamics Investigation), which measure other key variables of the control of carbon uptake by plants, to complement OCO-3 data in science analysis. In 2017, the OCO-2 instrument was transformed into the ISS-ready OCO-3 payload. The transformed instrument was thoroughly tested and characterized. Key characteristics, such as instrument ILS, spectral resolution, and radiometric performance will be described. Analysis of direct sun measurements taken during testing

Increased Science Instrumentation Funding Strengthens Mars Program

Science.gov (United States)

Graham, Lee D.; Graff, T. G.

2012-01-01

As the strategic knowledge gaps mature for the exploration of Mars, Mars sample return (MSR), and Phobos/Deimos missions, one approach that becomes more probable involves smaller science instrumentation and integrated science suites. Recent technological advances provide the foundation for a significant evolution of instrumentation; however, the funding support is currently too small to fully utilize these advances. We propose that an increase in funding for instrumentation development occur in the near-term so that these foundational technologies can be applied. These instruments would directly address the significant knowledge gaps for humans to Mars orbit, humans to the Martian surface, and humans to Phobos/ Deimos. They would also address the topics covered by the Decadal Survey and the Mars scientific goals, objectives, investigations and priorities as stated by the MEPAG. We argue that an increase of science instrumentation funding would be of great benefit to the Mars program as well as the potential for human exploration of the Mars system. If the total non-Earth-related planetary science instrumentation budget were increased 100% it would not add an appreciable amount to the overall NASA budget and would provide the real potential for future breakthroughs. If such an approach were implemented in the near-term, NASA would benefit greatly in terms of science knowledge of the Mars, Phobos/Deimos system, exploration risk mitigation, technology development, and public interest.

Radioisotope instruments

CERN Document Server

Cameron, J F; Silverleaf, D J

1971-01-01

International Series of Monographs in Nuclear Energy, Volume 107: Radioisotope Instruments, Part 1 focuses on the design and applications of instruments based on the radiation released by radioactive substances. The book first offers information on the physical basis of radioisotope instruments; technical and economic advantages of radioisotope instruments; and radiation hazard. The manuscript then discusses commercial radioisotope instruments, including radiation sources and detectors, computing and control units, and measuring heads. The text describes the applications of radioisotop

Emotional support, instrumental support, and gambling participation among Filipino Americans.

Science.gov (United States)

Kim, Isok; Kim, Wooksoo; Nochajski, Thomas H

2014-08-01

Using representative survey data of Filipino Americans in Honolulu and San Francisco (SF) (N = 2,259), we examined the roles of emotional support and instrumental support on gambling participation. With considerable difference in gambling environments between two regions, we conducted two sets of hierarchical regression analyses for Honolulu sample, which has restricted gambling laws, and SF sample, which has legal gambling environment, and compared the effects of two types of social support on gambling participation. The results indicated that emotional support was positively and instrumental support was negatively associated with gambling participation among Filipino Americans in Honolulu. However, neither type of social support was significantly associated with gambling participation among Filipino Americans living in SF. This study highlights the differing roles and effects of instrumental and emotional support on gambling where gambling is restricted. It also suggests that gambling behaviors of Filipino Americans are subject to situation- and environment-specific factors.

The Influence of Mineralogy on Recovering Organic Acids from Mars Analogue Materials Using the One-Pot Derivatization Experiment on the Sample Analysis at Mars(SAM) Instrument Suite

Science.gov (United States)

Stalport, Fabien; Glavin, Daniel P.; Eigenbrode, J. L.; Bish, D.; Blake, D.; Coll, P.; Szopa, C.; Buch, A.; McAdam, A.; Dworkin, J. P.;

Soil analysis. Modern instrumental technique

International Nuclear Information System (INIS)

Smith, K.A.

1993-01-01

This book covers traditional methods of analysis and specialist monographs on individual instrumental techniques, which are usually not written with soil or plant analysis specifically in mind. The principles of the techniques are combined with discussions of sample preparation and matrix problems, and critical reviews of applications in soil science and related disciplines. Individual chapters are processed separately for inclusion in the appropriate data bases

The Coherent X-ray Imaging (CXI) Instrument at the Linac Coherent Light Source (LCLS)

International Nuclear Information System (INIS)

Boutet, Sebastien

2011-01-01

The Linac Coherent Light Source (LCLS) has become the first ever operational hard X-ray Free Electron Laser in 2009. It will operate as a user facility capable of delivering unique research opportunities in multiple fields of science. The LCLS and the LCLS Ultrafast Science Instruments (LUSI) construction projects are developing instruments designed to make full use of the capabilities afforded by the LCLS beam. One such instrument is being designed to utilize the LCLS coherent beam to image with high resolution any sub-micron object. This instrument is called the Coherent X-ray Imaging (CXI) instrument. This instrument will provide a flexible optical system capable of tailoring key beam parameters for the users. A suite of shot-to-shot diagnostics will also be provided to characterize the beam on every pulse. The provided instrumentation will include multi-purpose sample environments, sample delivery and a custom detector capable of collecting 2D data at 120 Hz. In this article, the LCLS will be briefly introduced along with the technique of Coherent X-ray Diffractive Imaging (CXDI). A few examples of scientific opportunities using the CXI instrument will be described. Finally, the conceptual layout of the instrument will be presented along with a description of the key requirements for the overall system and specific devices required.

Reference Proteome Extracts for Mass Spec Instrument Performance Validation and Method Development

Science.gov (United States)

Rosenblatt, Mike; Urh, Marjeta; Saveliev, Sergei

2014-01-01

Biological samples of high complexity are required to test protein mass spec sample preparation procedures and validate mass spec instrument performance. Total cell protein extracts provide the needed sample complexity. However, to be compatible with mass spec applications, such extracts should meet a number of design requirements: compatibility with LC/MS (free of detergents, etc.)high protein integrity (minimal level of protein degradation and non-biological PTMs)compatibility with common sample preparation methods such as proteolysis, PTM enrichment and mass-tag labelingLot-to-lot reproducibility Here we describe total protein extracts from yeast and human cells that meet the above criteria. Two extract formats have been developed: Intact protein extracts with primary use for sample preparation method development and optimizationPre-digested extracts (peptides) with primary use for instrument validation and performance monitoring

Elemental and isotopic characterization of Japanese and Philippine polished rice samples using instrumental neutron activation analysis and isotope ratio mass spectrometry

International Nuclear Information System (INIS)

Pabroa, Preciosa Corazon B.; Sucgang, Raymond J.; Mendoza, Norman dS.; Ebihara, Mitsuru

2011-01-01

Rice is a staple food for most Asian countries such as the Philippines and Japan and as such its elemental and isotopic content are of interest to the consumers. Its elemental content may reflect the macro nutrient reduction during milling or probable toxic elements uptake. Three Japanese and four Philippine polished rice samples in his study mostly came from rice bought from supermarkets.These rice samples were washed, dried and ground to fine powder. Instrumental neutron activation analysis (INAA), a very sensitive non-destructive multi-element analytical technique, was used for the elemental analysis of the samples and isotope-ratio mass spectrometry (IRMS) was used to obtain the isotopic signatures of the samples. Results show that compared with the unpolished rice standard NIES CRM10b, the polished Japanese and Philippine rice sampled show reduced concentrations of elements by as much as 1/3 to 1/10 of Mg, Mn, K and Na. Levels of Ca and Zn are not greatly affected. Arsenic is found in all the Japanese rice tested at an average concentration of 0.103 μg/g and three out of four of the Philippine rice at an average concentration of 0.070 μg/g. Arsenic contamination may have been introduced from the fertilizer used in rice fields. Higher levels of Br are seen in two of the Philippine rice at 14 and 34 μg/g with the most probable source being the pesticide methyl bromide. Isotopic ratio of ae 13 C show signature of a C3 plant with possible narrow distinguishable signature of Japanese rice within -27.5 to -28.5 while Philippine rice within -29 to -30. More rice samples will be analyzed to gain better understanding of isotopic signatures to distinguish inter-varietal and/or geographical differences. Elemental composition of soil samples of rice samples sources will be determined for better understanding of uptake mechanisms. (author)

Analysis of in-core coolant temperatures of FFTF instrumented fuels tests at full power

International Nuclear Information System (INIS)

Hoth, C.W.

1981-01-01

Two full size highly instrumented fuel assemblies were inserted into the core of the Fast Flux Test Facility in December of 1979. The major objectives of these instrumented tests are to provide verification of the FFTF core conditions and to characterize temperature patterns within FFTF driver fuel assemblies. A review is presented of the results obtained during the power ascents and during irradiation at a constant reactor power of 400 MWt. The results obtained from these instrumented tests verify the conservative nature of the design methods used to establish core conditions in FFTF. The success of these tests also demonstrates the ability to design, fabricate, install and irradiate complex, instrumented fuel tests in FFTF using commercially procured components

Performance on cognitive tests, instrumental activities of daily living and depressive symptoms of a community-based sample of elderly adults in Rio de Janeiro, Brazil

Science.gov (United States)

Lima, Christina Martins Borges; Alves, Heloisa Veiga Dias; Mograbi, Daniel Correa; Pereira, Flávia Furtado; Fernandez, Jesus Landeira; Charchat-Fichman, Helenice

2017-01-01

Objective To describe the performance on basic cognitive tasks, instrumental activities of daily living, and depressive symptoms of a community-based sample of elderly adults in Rio de Janeiro (Brazil) who participated in multiple physical, social, and cognitive activities at government-run community centers. Methods A total of 264 educated older adults (> 60 years of age of both genders) were evaluated by the Brief Cognitive Screening Battery (BCSB), Lawton's and Pfeffer's activities of daily living indexes, and the Geriatric Depressive Scale (GDS). Results The mean age of the sample was 75.7 years. The participants had a mean of 9.3 years of formal education. With the exception of the Clock Drawing Test (CDT), mean scores on the cognitive tests were consistent with the values in the literature. Only 6.4% of the sample had some kind of dependence for activities of daily living. The results of the Geriatric Depression Scale (GDS-15) indicated mild symptoms of depression in 16.8% of the sample Conclusion This study provided important demographic, cognitive, and functional characteristics of a specific community-based sample of elderly adults in Rio de Janeiro, Brazil. PMID:29213494

Performance on cognitive tests, instrumental activities of daily living and depressive symptoms of a community-based sample of elderly adults in Rio de Janeiro, Brazil

Directory of Open Access Journals (Sweden)

Christina Martins Borges Lima

Full Text Available ABSTRACT Objective: To describe the performance on basic cognitive tasks, instrumental activities of daily living, and depressive symptoms of a community-based sample of elderly adults in Rio de Janeiro (Brazil who participated in multiple physical, social, and cognitive activities at government-run community centers. Methods: A total of 264 educated older adults (> 60 years of age of both genders were evaluated by the Brief Cognitive Screening Battery (BCSB, Lawton's and Pfeffer's activities of daily living indexes, and the Geriatric Depressive Scale (GDS . Results: The mean age of the sample was 75.7 years. The participants had a mean of 9.3 years of formal education. With the exception of the Clock Drawing Test (CDT, mean scores on the cognitive tests were consistent with the values in the literature. Only 6.4% of the sample had some kind of dependence for activities of daily living. The results of the Geriatric Depression Scale (GDS-15 indicated mild symptoms of depression in 16.8% of the sample. Conclusion: This study provided important demographic, cognitive, and functional characteristics of a specific community-based sample of elderly adults in Rio de Janeiro, Brazil.

Successful Working Memory Processes and Cerebellum in an Elderly Sample: A Neuropsychological and fMRI Study.

Directory of Open Access Journals (Sweden)

Elkin O Luis

Full Text Available Imaging studies help to understand the evolution of key cognitive processes related to aging, such as working memory (WM. This study aimed to test three hypotheses in older adults. First, that the brain activation pattern associated to WM processes in elderly during successful low load tasks is located in posterior sensory and associative areas; second, that the prefrontal and parietal cortex and basal ganglia should be more active during high-demand tasks; third, that cerebellar activations are related to high-demand cognitive tasks and have a specific lateralization depending on the condition.We used a neuropsychological assessment with functional magnetic resonance imaging and a core N-back paradigm design that was maintained across the combination of four conditions of stimuli and two memory loads in a sample of twenty elderly subjects.During low-loads, activations were located in the visual ventral network. In high loads, there was an involvement of the basal ganglia and cerebellum in addition to the frontal and parietal cortices. Moreover, we detected an executive control role of the cerebellum in a relatively symmetric fronto-parietal network. Nevertheless, this network showed a predominantly left lateralization in parietal regions associated presumably with an overuse of verbal storage strategies. The differential activations between conditions were stimuli-dependent and were located in sensory areas.Successful WM processes in the elderly population are accompanied by an activation pattern that involves cerebellar regions working together with a fronto-parietal network.

Evolution of Perceived Cohesion and Efficacy over the Season and their Relation to Success Expectations in Soccer Teams.

Science.gov (United States)

Marcos, Francisco Miguel Leo; Sánchez-Miguel, Pedro Antonio; Sánchez-Oliva, David; Alonso, Diana Amado; García-Calvo, Tomás

2012-10-01

The main goal of the study is to examine the evolution of players' perception of cohesion and efficacy over the season and their relation with success expectations. The research sample comprised 146 male soccer players, aged between 15 and 19 years (M = 16.96, SD = .76). Diverse instruments were used to measure cohesion, perceived efficacy, and success expectations. The most noteworthy results show that players whose expectations do not match the team's final performance will experience a negative evolution of their levels of perceived cohesion and efficacy, whereas players whose expectations at the start of the season match the team's final performance in the classification will maintain their degree of perceived cohesion and efficacy. The main conclusion of the study is that coaches and sport psychologists should attempt to clarify the players' basic goals of the season to create expectations that match what is expected from the team.

Instrument calls and real-time code for laboratory automation

International Nuclear Information System (INIS)

Taber, L.; Ames, H.S.; Yamauchi, R.K.; Barton, G.W. Jr.

1978-01-01

These programs are the result of a joint Lawrence Livermore Laboratory and Environmental Protection Agency project to automate water quality laboratories. They form the interface between the analytical instruments and the BASIC language programs for data reduction and analysis. They operate on Data General NOVA 840's at Cincinnati and Chicago and on a Data General ECLIPSE C330 at Livermore. The operating system consists of unmodified RDOS, Data General's disk operating system, and Data General's multiuser BASIC modified to provide the instrument CALLs and other functions described. Instruments automated at various laboratories include Technicon AutoAnalyzers, atomic absorption spectrophotometers, total organic carbon analyzers, an emission spectrometer, an electronic balance, sample changers, and an optical spectrophotometer. Other instruments may be automated using these same CALLs, or new CALLs may be written as described

Pointers, Lessons Learned, and Rules of Thumb for Successful Vibro-Acoustic Data Acquisition

Science.gov (United States)

Rossoni, Peter

1998-01-01

This presentation contains helpful pointers for successful vibroacoustic data acquisition in the following three areas: Instrumentation, Vibration Control and Pyro-shock data acquisition and analysis. A helpful bibliography is provided.

76 FR 52314 - Application(s) for Duty-Free Entry of Scientific Instruments

Science.gov (United States)

2011-08-22

... invite comments on the question of whether instruments of equivalent scientific value, for the purposes...: Projekt Messtechnik, Germany. Intended Use: The SPSx will be used to monitor the water-solid interaction... instrument monitors water-solid interactions by taking gravimetric measurement of samples continuously using...