WorldWideScience

Sample records for in-738lc in-939 nimonic

  1. Investigation of the thermal expansion behaviour and elastic properties of superalloys in vacuum and at temperatures between 20deg C and 1300deg C. [IN100; IN617; IN713; IN 738LC; IN 738LC DS; IN800 H; IN907; IN939; Nimonic 75; Nimonic 90; Udimet 500; Udimet 720; MA 6000 DS; MA 754; MAR M247; MAR M002 mod; CMSX 2; CMSX 6; B1914 DS; X3CrNi18 9; X22CrMoV12. 1; FSX414]. Untersuchungen ueber das thermische Ausdehnungsverhalten und die elastischen Eigenschaften von Superlegierungen zwischen 20deg C und 1300deg C unter Vakuum

    Energy Technology Data Exchange (ETDEWEB)

    Klose, P.L.M.

    1987-07-24

    In this paper, a comprising survey on the thermal and elastic behaviour of 20 high-temperature alloys is given. Besides Ni base forge and cast alloys (especially IN 738 LC and CMSX 6), the measurements were carried out in vacuum maximally up to 1300deg C with directionally solidified and monocrystalline superalloys as well as with cobalt base, iron base and Ni-Fe-Cr alloys. The creep strain at increased temperatures and the hot-isostatic re-compaction were also considered in the investigations. Dynamic and static measurement methods as for example the resonance method, the ultrasonic pulse transit-time measurement as well as the four-point bending tests and compression tests were used for the determination of the elastic properties. The determination of the expansion behaviour was carried out dilatometrically. It can be concluded from this study that the elastic anisotropy influences considerably the mechanical and thermal properties of the materials investigated. (orig./MM).

  2. The characteristics of serrated flow in superalloy IN738LC

    Energy Technology Data Exchange (ETDEWEB)

    Sharghi-Moshtaghin, Reza [Department of Materials Science and Engineering, Sharif University of Technology, Azadi Avenue, Tehran (Iran, Islamic Republic of); Department of Materials Science and Engineering, Case Western Reserve University, Cleveland, OH 44106 (United States)], E-mail: rxs270@case.edu; Asgari, Sirous [Department of Materials Science and Engineering, Sharif University of Technology, Azadi Avenue, Tehran (Iran, Islamic Republic of)

    2008-07-15

    Serrated flow was investigated in superalloy IN738LC, a nickel-base {gamma}' age-hardened alloy. In this material serrated flow appeared between 350 and 450 deg. C and strain rate of (8.77 x 10{sup -5} to 8.77 x 10{sup -3}) s{sup -1}. Activation energy for this process was calculated to be 0.69-0.86 eV which is in good agreement with the values reported for similar alloys. Results show that the diffusion rate of substitutional solute atoms at this temperature range is too low to cause this effect. This suggests that the interaction of solute atoms and moving dislocation is responsible for the observed serrated flow in this alloy.

  3. Structure dependence of the dynamic Young modulus, G modulus and the attenuation in high temperature forged alloys and cast alloys. Final report. [IN 100; IN 617; IN 713LC; IN 738LC; IN 738 LC DS; IN 800 H; IN 907; IN 939; Nimonic 75; Nimonic 90; Udimet 500; Udimet 720; MA 6000 DS; MA 754; MAR M247; MAR M002 mod; CMSX 2; CMSX 6; B1914 DS; X3CrNi18 9; X22CrMoV12 1; FSX414]. Gefuegeabhaengigkeit des dynamischen E-Moduls, G-Moduls und der Daempfung bei hochwarmfesten Schmiede- und Gusslegierungen. Abschlussbericht

    Energy Technology Data Exchange (ETDEWEB)

    Klose, P.; Kuhn, A.H.

    1987-01-01

    This work consists of two parts. The first part reports on the measurement of the elastic properties and the thermal expansion coefficients of selected, technically important high temperature alloys (as e.g. cast alloys and forged alloys, directionally solidified alloys, single crystals) in the temperature range of 20deg C to 1200deg C. The orientation dependence and the structure dependence of these characteristics are of special interest especially in this study. The second part reports on investigations of selected materials with regard to the quantitative relationships between the elastic properties of single-phase single crystals and multiphase single crystals, directionally solidified alloys as well as polycrystals without und with texture, in the temperature range of 20deg C to 1200deg C. The limiting value concept and the phase mixing rules are used for the evaluation. (orig./MM) With 133 figs., 18 tabs., 322 refs.

  4. Kinetics and Microstructural Investigation of High-Temperature Oxidation of IN-738LC Super Alloy

    Science.gov (United States)

    Hamidi, S.; Rahimipour, M. R.; Eshraghi, M. J.; Hadavi, S. M. M.; Esfahani, H.

    2017-02-01

    The present study was carried out to investigate the kinetics and the surface chemistry of the oxide layers formed on the IN-738LC super alloy during high-temperature oxidation at 950 °C in air from 1 to 260 h. Oxidation kinetics were studied by mass gain measurement. The oxide layers were characterized by field emission scanning electron microscope, elemental distribution map, energy-dispersive spectroscopy as well as x-ray diffractometry (XRD). The oxidation kinetics followed the parabolic law. The XRD analysis revealed that the oxide scale contained mainly NiO, Ni (Cr, Al)2O4, Al2O3, TiO2 and Cr2O3. The oxide structure, from the top surface down to the substrate, was clarified by elemental map distribution studies as Ni-Ti oxides, Cr-Ti oxides, Cr2O3 oxide band, Ni-Co-Cr-W oxide and finally a blocky Al2O3 region. The oxidation scales were composed of three distinct layers of the outer and mid layers enriched by TiO2 and Cr2O3, NiCr2O4 oxide, respectively, and the innermost layer was composed of Al2O3 and matrix alloy. The depleted gamma prime layer was formed under the oxidation scales due to the impoverishment of Al and Ti which were induced by the formation of Al2O3 and TiO2.

  5. Formation and Characterization of Titanium Modified Aluminide Coatings on IN738LC

    Institute of Scientific and Technical Information of China (English)

    Mohammad Moradi; Fakhreddin Ashrafizadeh

    2004-01-01

    Up to now, the aluminide coatings used to protect industrial components at high temperature and corrosive environments have been modified by Pt, Cr, Si and Ni. In this investigation, aluminide coatings were modified by titanium and the microstructural feature and formation mechanism were evaluated. The coatings were formed on a Ni-based superalloy(IN738LC) by a two stage process including titanizing at first and aluminizing thereafter. Pack cementation titanizing performed at temperatures 950℃ and 1050℃ in several mixtures of Ti, Al2O3 and NH4Cl. At the second stage,aluminum diffused into surface of the specimens by an industrial aluminizing process known as Elcoatl01(4 hrs at 1050℃C). The modified coatings were characterized by means of standard optical microscopy, scanning electron microscopy,energy dispersive spectroscopy and X-Ray diffraction methods. The results show that Ti in the coatings is mainly present in the form of TiNi and Al67CrsTi25. Titanium modified coatings grew with a mechanism similar to simple aluminizing; this includes inward diffusion of Al from the pack to the substrate and then outward diffusion of Ni from the substrate to the coating. The advantages and characteristics of this two-stage modified coating is discussed and the process parameters are proposed to obtain a coating of optimum microstructure.

  6. Evaluation of hot corrosion protection of Cr-Al and CoNiCrAlY on IN-738LC

    Energy Technology Data Exchange (ETDEWEB)

    Khajavi, M.R. [Niroo Research Institute - Chemistry and Materials Research Center - Metallurgy Dept. End of Pounak-e-Bakhtari, P.O.Box 14665-517, Post Code 1468617151, Blvd., Shahrak-e-Gharb, Tehran (Iran)]|[Shiraz University - Materials Science and Engineering Department, Engineering School, Shiraz University, Shiraz (Iran); Pasha, A. [Niroo Research Institute - Chemistry and Materials Research Center - Metallurgy Dept. End of Pounak-e-Bakhtari, P.O.Box 14665-517, Post Code 1468617151, Blvd., Shahrak-e-Gharb, Tehran (Iran); Shariat, M.H. [Shiraz University - Materials Science and Engineering Department, Engineering School, Shiraz University, Shiraz (Iran)

    2004-07-01

    A program was conducted to evaluate the relative corrosion resistance of CoNiCrAlY and Chromium modified Aluminide on IN738-LC, used for turbine blades. The corrosion experiments were performed in a laboratory tube furnace. The microstructure of coatings was characterized by using optical and scanning electron microscopy techniques. The results indicated that at a temperature of 800 deg. C the CoNiCrAlY is more protective than Cr-Al coating. (authors)

  7. Inelastic analysis of the deformation behaviour of internally cooled IN 738 LC turbine blades using the microstructural dependent constitutive equations; Inelastische Analyse des Verformungsverhaltens einer innengekuehlten Gasturbinenschaufel aus dem Werkstoff IN 738 LC unter Verwendung des strukturabhaengigen Werkstoffmodells

    Energy Technology Data Exchange (ETDEWEB)

    Beckmoeller, S.; Schubert, F.; Penkalla, H.J.; Nickel, H.; Breitbach, G.

    1994-06-01

    To enhance the high temperature potential of Superalloys for applications in stationary gas turbines a new concept is required for the prediction of the service life of the blades with an improved method for inelastic analysis. The applicability of the microstructural dependent constitutive equations, which has been developed at the IWE of the KFA, are discussed for a structural analysis of an internally cooled IN 738 LC turbine blade. For the multiaxial confirmation of the model tension-torsion experiments and experiments with precision casted internally cooled model turbine blades were carried out. The blades were exposed to temperature transients and tension stresses to simulate the centrifugal forces. For the mathematical analysis the constitutive equations were implemented into the Finite Elemente Code ABAQUS. A two dimensional mesh was used. At first, the temperature distribution in the blade was calculated based on the temperatures measured at certain points during the experiments. After the temperature distribution was known, it was possible to calculate the stresses and inelastic strains at every point of the model structure. The comparison of the experiments with the calculations, using the constitutive equations of Penkalla, showed a good conformity. For the life time prediction by experiments with short holding times, an elastic analysis could be used. But for experiments with long holding times creep is more dominant and has to be considered. (orig.) [Deutsch] Fuer die optimale Nutzung der Eigenschaften neuer hochwarmfester Superlegierungen reicht die herkoemmliche Auslegung dann nicht mehr aus, wenn ein Bauteil komplizierten Temperatur- und Belastungszyklen ausgesetzt ist. Die Beurteilung des Betriebsverhaltens und der Lebensdauer solcher Bauteile bedarf neuer Konzepte. Ein solches Bauteil ist die innengekuehlte Turbinenschaufel einer modernen stationaeren Gasturbine. Im Rahmen dieser Arbeit wurde die Anwendbarkeit des strukturabhaengigen

  8. Tailoring the texture of IN738LC processed by selective laser melting (SLM) by specific scanning strategies

    Energy Technology Data Exchange (ETDEWEB)

    Geiger, Fabian [General Electric Switzerland GmbH – GE Power, CH-5401 Baden (Switzerland); Kunze, Karsten, E-mail: karsten.kunze@scopem.ethz.ch [ETH Zurich, Scientific Center of Optical and Electron Microscopy (ScopeM), CH-8093 Zürich (Switzerland); Etter, Thomas [General Electric Switzerland GmbH – GE Power, CH-5401 Baden (Switzerland)

    2016-04-20

    Selective laser melting (SLM) is an emerging technology of additive manufacturing, which is used to directly produce metallic parts from thin powder layers. This study aims at correlating laser scanning strategies with the resulting textures and corresponding anisotropy of the elastic behavior of bulk materials. Tensile test specimens made of the γ’-containing Ni-base superalloy IN738LC were built with the loading direction oriented either parallel (z-specimens) or perpendicular to the build-up direction (xy-specimens). Their bulk mechanical properties were determined at room temperature and at 850 °C. Specimens were investigated in the ‘as-built’ condition and after recrystallization heat treatment. SEM-based electron backscatter diffraction (EBSD) was applied to measure their crystallographic preferred orientations (texture) and to correlate the anisotropy of Young's modulus with the texture of the material. It is shown that the applied laser scanning strategies allow to tailor the crystallographic texture locally. The possibility to switch from transverse anisotropic to transverse isotropic properties and reverse is demonstrated for triple layered tensile samples. A recrystallization heat treatment reduces the degree of crystallographic texture and thus the elastic anisotropy by abundant annealing twinning. Predictions of Young's modulus calculated from the measured textures compare well with the data from tensile tests.

  9. High-Temperature Friction and Wear Studies of Nimonic 80A and Nimonic 90 Against Nimonic 75 Under Dry Sliding Conditions

    OpenAIRE

    Khajuria, G.; Wani, Mohammad Farooq

    2017-01-01

    The present research focuses on dry sliding friction and wear behaviour of Nimonic 80A and Nimonic 90 against Nimonic 75 at high temperature up to 1023 K. The influence of temperature, sliding distance and normal load on friction and wear behaviour of Nimonic 80A and Nimonic 90 against Nimonic 75 was studied using pin (Nimonic 75)-on-disc (Nimonic 80A and Nimonic 90). Lower wear and lower friction of superalloys was observed at high temperatures, as compared to room temperature. Surface morph...

  10. Microstructure of helium-implanted Nimonic PE16

    Energy Technology Data Exchange (ETDEWEB)

    Czyrska-Filemonowicz, A.; Gadalla, A.A.; Kesternich, W.; Weckermann, B.

    1987-09-01

    Transmission electron microsocpy has been used to investigate the microstructure in Nimonic PE16 after room temperature a-implementation followed by subsequent annealing. Helium bubble formation in the matrix, at dislocations, at grain boundaries and at precipitates of ..gamma..', M/sub 23/C/sub 6/, and MC type has been studied.

  11. Recovery of creep properties of the nickel-base superalloy nimonic 105

    CSIR Research Space (South Africa)

    Girdwood, RB

    1996-01-01

    Full Text Available -crept samples and creep recovery quantitatively assessed. Microstructural damage occurring during the creep of Nimonic 105 was studied. Creep strength is lost by the coarsening of the precipitate and grain boundary carbides. The Theta Projection Concept relates...

  12. Selection of criteria for interchangeability verification of special alloys on the example of nimonic

    Directory of Open Access Journals (Sweden)

    Егор Павлович Дымко

    2016-06-01

    Full Text Available Research of nimonic long-term strength, which allows determining its value at different temperatures and the test of time are conducted on the basis of mathematical simulation. Criterion for interchangeability verification of special alloys on the example of nimonic is proposed. This criterion is based on a parametric description of the test property depending on the Lagrange multiplier and allows finding its suboptimal values in the investigated range of input variables

  13. Thermophysical properties of the Ni-based alloy Nimonic 80A up to 2400 K

    Institute of Scientific and Technical Information of China (English)

    B. Wilthan; R. Tanzer; W. Schiitzenh(o)fer; G. Pottlacher

    2006-01-01

    Nimonic 80A is a nickel-chromium alloy which is strengthened by additions of titanium and aluminium. The alloy is used for high temperature, high strength applications. Wire shaped Nimonic 80A samples are resistively volume heated as part of a fast capacitor discharge circuit. Time resolved measurements with sub-μs resolution of current through the specimen are performed with a Pearson probe, voltage drop across the specimen is measured with knife-edge contacts and ohmic voltage dividers and the radiance temperature of the sample with a pyrometer. These measurements allow to determine heat of fusion as well as heat capacity and electrical resistivity at initial geometry of Nimonic 80A as a function of temperature in the solid and in the liquid phase up to 2400 K.

  14. TEM and SANS investigation of age hardened Nimonic PE16 after cyclic loading at room temperature

    Energy Technology Data Exchange (ETDEWEB)

    Sundararaman, M.; Chen, W.; Wahi, R.P.; Wiedenmann, A.; Wagner, W.; Petry, W. (Bhabha Atomic Research Centre, Bombay (India) Berlin, Technische Universitaet, (Germany) Hahn-Meitner-Institut Berlin GmbH, (Germany) Paul Scherrer Institut, Villigen (Switzerland) Institut Max von Laue - Paul Langevin, Grenoble (France))

    1992-05-01

    A nickel-base superalloy Nimonic PE16 shows softening when subjected to low cycle fatigue (LCF) at room temperature. In this work, small-angle neutron scattering (SANS) and transmission electron microscopy (TEM) were used to study the morphology of gamma-prime precipitates in the Nimonic PE16 after LCF at room temperature. In TEM dark-field images using superlattice reflections, deformation bands free of gamma-prime precipitates in the Nimonic PE16 after LCF at room temperature. In TEM dark-field images using superlattice reflections, deformation bands free of gamma-prime precipitates are observed. SANS measurements allowed the characterization of the disappeared precipitates with regard to their average size, size distribution and volume fraction by comparing the scattered intensities of loaded and unloaded specimens. An analysis of the results shows that the gamma-prime precipitates within the deformation bands have completely dissolved and not just disordered or cut to sizes smaller than the TEM resolution limit. 14 refs.

  15. Evaluation of Optimum Cutting Parameters In Turning of NIMONIC 75 using RSM

    Directory of Open Access Journals (Sweden)

    P Subhash

    2013-08-01

    Full Text Available Nickel based superalloys pose a real threat to industries when it comes to machining, due to their strength and hardness. Despite of this disadvantage, they are in high demand just because of their excellent performance at high temperature. NIMONIC 75 is one of such alloys which exhibits all the essential properties of a superalloy and has hardness less than INCONEL 718. This paper investigates the effect of AlTiN coated cemented carbide tool and various cutting parameters – speed, feed and depth of cut – on the surface integrity of NIMONIC 75 under dry machining condition using response surface methodology (RSM. Since no data related to machining of NIMNIC75 is available so far, so to find the initial values of each parameter preliminary experiments had to be conducted. These preliminary experiments showed that the value of surface roughness is less between the speeds from 100 m/min to 250 m/min and feed rate from 0.02 mm/rev. to 0.04 mm/rev. The final result shows the significance of each machining parameter individually on the surface integrity and a model to predict the value of surface roughness between that particular range of cutting parameters.

  16. Trim cut machining and surface integrity analysis of Nimonic 80A alloy using wire cut EDM

    Directory of Open Access Journals (Sweden)

    Amitesh Goswami

    2017-02-01

    Full Text Available This present work deals with the features of trim cut wire EDM machining of Nimonic 80A in terms of machining parameters, to predict material removal rate (MRR, surface roughness (Ra, wire wear ratio (WWR and microstructure analysis. Trim cut is performed after rough cut to remove the rough layer deposited after machining due to melting and re-solidification of the eroded metal from workpiece as well as from wire electrode. Taguchi’s design of experiments methodology has been used for planning and designing the experiments. The relative significance of various factors has also been evaluated and analyzed using ANOVA. The results clearly indicate trim cut potential for high surface finish compared to rough cut machining.

  17. Numerical simulation for determination of limit strains of a cold rolled and solution treated Nimonic C-263 alloy sheet

    Indian Academy of Sciences (India)

    K Ankamma; P V R Ravindra Reddy; S Nagarjuna; G Chandra Mohan Reddy; M Komaraiah; N Eswara Prasad

    2011-06-01

    Nimonic alloys are Ni-base superalloys used for several high temperature applications, notable among them are the components in space vehicles, rocket engines, submarines, nuclear reactors, chemical processing vessels and heat exchange tubing as they exhibit excellent mechanical strength and creep resistance at high temperatures. Hence, evaluation of their formability characteristics is of utmost importance to make them into several useful components. Limit strains or forming limit curve is one of the parameters that indicates the formability, especially the drawability of sheet metal for deep drawing applications. In this paper, the limit strains of Nimonic C-263 alloy is investigated and presented using an explicit finite element code LSDYNA 3D. The material properties and the material model are evaluated by conducting tensile tests. The limit strains obtained from the simulation are verified by the analytical equations developed using vertex theory. The results tally within ±10% error.

  18. Effect of Machining Parameters on Surface Integrity in Machining Nimonic C-263 Super Alloy Using Whisker-Reinforced Ceramic Insert

    Science.gov (United States)

    Ezilarasan, C.; Senthil kumar, V. S.; Velayudham, A.

    2013-06-01

    Whisker-reinforced ceramic inserts were used to conduct turning trials on nimonic C-263 super alloy to study the effect of different combinations of cutting parameters on surface integrity (roughness, microhardness, and residual stress) by employing energy dispersive spectroscopy, scanning electron microscopy, x-ray diffraction, and Vicker's microhardness test. Abrasion, adhesion and diffusion were found to be the main tool wear mechanisms in turning nimonic C-263 alloy. Based on characterization of surface roughness, a combination of 190 m/min cutting speed and 0.102 mm/rev feed rate was found to be the critical condition for turning nimonic C-263 alloy. Microhardness varied between 550 and 690 HV at the feed rates of 0.102-0.143 mm/rev for a cutting speed of 250 m/min after 9 min of turning. A tensile residual stress of 725-850 MPa on the machined surface was recorded at the preceding combination of cutting parameters. Cutting speed and cutting time had a dominant effect on the magnitude of the residual stress. No evidence of thermal relaxation and reduction in the degree of work hardening was noted during machining at high cutting speed.

  19. The role of particle ripening on the creep acceleration of Nimonic 263 superalloy

    Directory of Open Access Journals (Sweden)

    Angella Giuliano

    2014-01-01

    Full Text Available Physically based constitutive equations need to incorporate the most relevant microstructural features of materials to adequately describe their mechanical behaviour. To accurately model the creep behaviour of precipitation hardened alloys, the value and the evolution of strengthening particle size are important parameters to be taken into account. In the present work, creep tests have been run on virgin and overaged (up to 3500 h at 800 ∘C Nimonic 263, a polycrystalline nickel base superalloy used for combustion chambers of gas turbines. The experimental results suggest that the reinforcing particle evolution is not the main reason for the creep acceleration that seems to be better described by a strain correlated damage, such as the accumulation of mobile dislocations or the grain boundary cavitation. The coarsened microstructure, obtained by overageing the alloy at high temperature before creep testing, mainly influences the initial stage of the creep, resulting in a higher minimum creep rate and a corresponding reduction of the creep resistance.

  20. Picosecond Laser Shock Peening of Nimonic 263 at 1064 nm and 532 nm Wavelength

    Directory of Open Access Journals (Sweden)

    Sanja Petronic

    2016-02-01

    Full Text Available The paper presents a study on the surface modifications of nickel based superalloy Nimonic 263 induced by laser shock peening (LSP process. The process was performed by Nd3+:Yttrium Aluminium Garnet (YAG picosecond laser using the following parameters: pulse duration 170 ps; repetition rate 10 Hz; pulse numbers of 50, 100 and 200; and wavelength of 1064 nm (with pulse energy of 2 mJ, 10 mJ and 15 mJ and 532 nm (with pulse energy of 25 mJ, 30 mJ and 35 mJ. The following response characteristics were analyzed: modified surface areas obtained by the laser/material interaction were observed by scanning electron microscopy; elemental composition of the modified surface was evaluated by energy-dispersive spectroscopy (EDS; and Vickers microhardness tests were performed. LSP processing at both 1064 nm and 532 nm wavelengths improved the surface structure and microhardness of a material. Surface morphology changes of the irradiated samples were determined and surface roughness was calculated. These investigations are intended to contribute to the study on the level of microstructure and mechanical properties improvements due to LSP process that operate in a picosecond regime. In particular, the effects of laser wavelength on the microstructural and mechanical changes of a material are studied in detail.

  1. Optimization in wire-cut EDM of Nimonic-80A using Taguchi's approach and utility concept

    Directory of Open Access Journals (Sweden)

    Amitesh Goswami

    2014-12-01

    Full Text Available In the present study a multi response optimization method using utility concept is proposed for wire electrical discharge machining (WEDM of Nimonic-80A alloy. The machining characteristics that are being investigated are material removal rate (MRR and surface roughness (SR along with surface topography of the machined surface. The study makes use of experimentation planned and executed as per Taguchi's robust design methodology. The Investigation indicated that material removal rate and surface roughness increases with increase in pulse-on time and decreases with increase in pulse-off time. Significant interactions have been found between pulse-on time (Ton and pulse-off time (Toff, pulse-on time (Ton and peak current (IP, pulse-off time (Toff and peak current (IP for material removal rate; and pulse-on time (Ton and peak current (IP for surface roughness. Multi-response optimization with utility concept provides the collective optimization of both responses for improving the mean of the process.

  2. Application of EBSD in the study of dynamic recrystallization mechanisms in Nimonic 80A%EBSD在Nimonic80A动态再结晶机制研究中的应用

    Institute of Scientific and Technical Information of China (English)

    吴洁琼; 陈科; 陈杏芳; 田胜; 沈治; 张澜庭; 单爱党

    2011-01-01

    本文采用背散射电子衍射(EBSD)技术对镍基高温合金Nimonic 80A在不同温度下热压变形后的微观结构进行表征.基于对动态再结晶过程关键参数-再结晶体积百分含量(volume fraction of DRX)、晶界取向差分布(misorientation angle distribution)和孪晶界含量(fraction of twin boundaries)的量化分析,实现对动态再结晶机制的辨别.充分发挥了EBSD大面积定量分析的优点,展示了其在量化分析金属材料动态再结晶机制中的优势.%Electron backscatter diffraction ( EBSD) was applied to characterize the microstructures of Nimonic 80A deformed at elevated temperature. Based on quantitative analyses of key dynamic recrystallization (DRX) parameters, including volume fraction of DRX, misorientation angle distribution, and fraction of twin boundaries, DRX mechanisms occurring during the hot working were studied and successfully identified for different hot-working temperatures. With the advantage of fast indexing for large-area quantitative analyses, EBSD was demonstrated by this work to have a high potential in the study of DRX mechanisms in metals.

  3. Prediction of the Hot Compressive Deformation Behavior for Superalloy Nimonic 80A by BP-ANN Model

    Directory of Open Access Journals (Sweden)

    Guo-zheng Quan

    2016-02-01

    Full Text Available In order to predict hot deformation behavior of superalloy nimonic 80A, a back-propagational artificial neural network (BP-ANN and strain-dependent Arrhenius-type model were established based on the experimental data from isothermal compression tests on a Gleeble-3500 thermo-mechanical simulator at temperatures ranging of 1050–1250 °C, strain rates ranging of 0.01–10.0 s−1. A comparison on a BP-ANN model and modified Arrhenius-type constitutive equation has been implemented in terms of statistical parameters, involving mean value of relative (μ, standard deviation (w, correlation coefficient (R and average absolute relative error (AARE. The μ -value and w -value of the improved Arrhenius-type model are 3.0012% and 2.0533%, respectively, while their values of the BP-ANN model are 0.0714% and 0.2564%, respectively. Meanwhile, the R-value and ARRE-value for the improved Arrhenius-type model are 0.9899 and 3.06%, while their values for the BP-ANN model are 0.9998 and 1.20%. The results indicate that the BP-ANN model can accurately track the experimental data and show a good generalization capability to predict complex flow behavior. Then, a 3D continuous interaction space for temperature, strain rate, strain and stress was constructed based on the expanded data predicted by a well-trained BP-ANN model. The developed 3D continuous space for hot working parameters articulates the intrinsic relationships of superalloy nimonic 80A.

  4. Numerical simulation for the determination of the limit drawing ratio of a cold rolled and solution treated Nimonic C-263 alloy sheet

    Energy Technology Data Exchange (ETDEWEB)

    Ankamma, Kandula; Chandra Mohan Reddy, Gangireddy [Mahatma Gandhi Institute of Technology, Hyderabad (India). Mechanil Engineering Dept.; Rama Ravindra Reddy, Pidugu Venkata [Chaitanya Bharathi Institute of Technology, Hyderabad (India). Mechanical Engineering Dept.; Nagarjuna, Settivari [Defence Metallurgical Research Lab., Hyderabad (India); Komaraiah, Methuku [Malla Reddy College of Engineering and Technology, Secunderabad (India); Eswara Prasad, Namburi [Regional Centre for Military Airworthiness (Materials), Hyderabad (India)

    2011-03-15

    Nimonic alloys are Ni-based superalloys used for several high temperature applications, notable among them are components in space vehicles, rocket engines, submarines, nuclear reactors, chemical processing vessels and heat exchange tubing, as they exhibit excellent mechanical strength and creep resistance at high temperatures. Hence, evaluation of their formability characteristics is of the utmost importance in making them into several useful components. The limit drawing ratio is one of the parameters that indicate the formability, especially the drawability of sheet material for deep drawing applications. In this paper, the limit drawing ratio of Nimonic C-263 alloy is investigated and presented using an explicit finite element code LSDYNA-3D. The material properties and the material model are evaluated through tensile testing. (orig.)

  5. Influence of laser alloying with boron and niobium on microstructure and properties of Nimonic 80A-alloy

    Science.gov (United States)

    Makuch, N.; Piasecki, A.; Dziarski, P.; Kulka, M.

    2015-12-01

    Ni-base superalloys were widely used in aeronautics, chemical and petrochemical industries due to their high corrosion resistance, high creep and rupture strength at high temperature. However, these alloys were not considered for applications in which conditions of appreciable mechanical wear were predominant. The diffusion boriding provided suitable protection against wear. Unfortunately, this process required long duration and high temperature. In this study, instead of the diffusion process, the laser alloying with boron and niobium was used in order to produce the hard and wear resistant layer on Nimonic 80A-alloy. The laser-alloying was carried out as a two-step process. First, the external cylindrical surface of specimens was pre-placed with a paste containing boron and niobium. Then, the pre-placed coating and the thin surface layer of the substrate were re-melted by a laser beam. The high laser beam power (P=1.56 kW) and high averaging irradiance (E=49.66 kW/cm2) provided the thick laser re-melted zone. The laser-borided layers were significantly thicker (470 μm) in comparison with the layers obtained as a consequence of the diffusion boriding. Simultaneously, the high overlapping of multiple laser tracks (86%) caused that the laser-alloyed layer was uniform in respect of the thickness. The produced layer consisted of nickel borides (Ni3B, Ni2B, Ni4B3, NiB), chromium borides (CrB, Cr2B), niobium borides (NbB2, NbB) and Ni-phase. The presence of hard borides caused the increase in microhardness up to 1000 HV in the re-melted zone. However, the measured values were lower than those-characteristic of niobium borides, chromium borides and nickel borides. The presence of the soft Ni-phase in re-melted zone was the reason for such a situation. After laser alloying, the significant increase in abrasive wear resistance was also observed. The mass wear intensity factor, as well as the relative mass loss of the laser-alloyed specimens, was over 10 times smaller in

  6. Thermophysical properties of Incoloy 800 and five additional FeNiCr-base high temperature alloys in comparison with the nickel-base alloy Nimonic 86 between 20 and 1000deg C

    Energy Technology Data Exchange (ETDEWEB)

    Richter, F. (Mannesmann-Forschungsinstitut GmbH, Duisburg (Germany, F.R.))

    1991-05-01

    The most important physical properties of the following high temperature alloys have been determined in the temperature range between 20 and 1000deg C: Incoloy 800, Incoloy 800 H, Incoloy 802, Incoloy 802 Nb, Manaurite 36 X, IN 519 and Nimonic 86. It is shown that these materials differ only a little in some of the properties. These properties include thermal expansion, thermal conductivity and thermal diffusivity. Owing to a substantially higher nickel content, the density of the nickel-base alloy Nimonic 86 differs significantly from that of the other materials investigated. The differences in the elastic properties of the materials are to be attributed to the differences in their crystallographic texture. Incoly 800 was very highly textured compared to other materials. The temperature dependence of the coefficient of linear thermal expansion and electrical resistivity of these materials is different from the normal behaviour of pure metals and alloys. The discrepancies observed are attributable to short range ordering processes in the case of Nimonic 86 and to temperature-induced electron transitons in the case of the other materials investigated, as known for austenitic Cr-Ni steels. (orig.).

  7. Analysis and description of the long-term creep behaviour of high-temperature gas turbine materials. Ermittlung und Beschreibung des Langzeitkriechverhaltens hochwarmfester Gasturbinenwerkstoffe

    Energy Technology Data Exchange (ETDEWEB)

    Bartsch, H.

    1985-05-14

    On a series of standard high-temperature gas turbine materials, creep tests were accomplished with the aim to obtain improved data on the long-term creep behaviour. The tests were carried out in the range of the main application temperatures of the materials and in the range of low stresses and elongations similar to operation conditions. They lasted about 5000 to 16000 h at maximum. At all important temperatures additional annealing tests lasting up to about 10000 h were carried out for the determination of a material-induced structure contraction. Thermal tension tests were effected for the description of elastoplastic short-time behaviour. As typical selection of materials the nickel investment casting alloys IN-738 LC, IN-939 and Udimet 500 for industrial turbine blades, IN-100 for aviation turbine blades and IN-713 C for integrally cast wheels of exhaust gas turbochargers were investigated, and also the nickel forge alloy Inconel 718 for industrial and aviation turbine disks and Nimonic 101 for industrial turbine blades and finally the cobalt alloy FSC 414 for guide blades and heat accumulation segments of industrial gas turbines. The creep tests were started on long-period individual creep testing machines with high strain measuring accuracy and economically continued on long-period multispecimen creep testing machines with long duration of test. The test results of this mixed test method were first subjected to a conventional evaluation in logarithmic time yield and creep diagrams which besides creep strength curves provided creep stress limit curves down to 0.2% residual strain.

  8. In-plane anisotropy in tensile deformation and its influence on the drawability of Nimonic C–263 alloy sheets

    Indian Academy of Sciences (India)

    K Ankamma; D V V Satyanarayana; G Chandramohan Reddy; M Komaraiah; N Eswara Prasad

    2011-04-01

    An effort has been made to comprehensively evaluate and rationalize the in-plane anisotropy in tensile properties and the effect of aging on the nature of deformation (strain hardening behaviour) and formability characteristics, especially the limit drawing ratio and forming limit diagram. Despite weak crystallographic texture and excellent ductility and high work hardening exponents, the alloy sheets of C-263 exhibit significant extent of in-plane anisotropy in its tensile properties and yield loci. The absolute magnitudes of yield stress and the exact nature of anisotropy that can be predicted from the tensile part of the yield locus need to be employed with caution. This is because when the magnitudes of the yield stresses, obtained from yield locus are more than 5 times higher as compared to the yield and ultimate tensile strength values and the nature and degree of in-plane anisotropy under tensile loading matches with that of only the compressive yield stresses of yield locus. The alloy sheet, due to weak crystallographic texture and relatively high strengths, is found to be far more suitable for structural applications, rather than for deep drawing applications, which was reflected in low limit drawing ratio values (1.34 for CR+ST and 1.23 for peak aged conditions). Further, the study conducted reveals that the safer forming limits in strain space is higher for CR+ST condition; while, the safer forming limits in stress space are higher for peak aged (CR+ST+1073 K/8 h) condition. Finally, detailed studies are outlined to arrive at suitable microstructural and textural characteristics that provide significantly enhanced drawability in the Nimonic C-263 alloy sheets.

  9. Atomic investigation of the dissolution of the [gamma]'-phase of the Nimonic PE16 alloy under irradiation with 300 keV Ni[sup +]-ions. Atomare Untersuchung der Aufloesung der [gamma]'-Phase der Nimonic PE16-Legierung unter Bestrahlung mit 300 keV Ni[sup +]-Ionen

    Energy Technology Data Exchange (ETDEWEB)

    Camus, E.

    1993-01-01

    The dissolution mechanism of the [gamma]' phase of the nickel base alloy Nimonic PE16 upon irradiation with [sup 58]Ni[sup +] ions of 300 keV energy is studied using field ion microscopy with atom probe. At room temperature, it is shown that the precipitates dissolve within 10 dpa. A smoothed [gamma]/[gamma]' interface is observed, the composition of the [gamma]' precipitates is affected by the irradiation, their size and number density remaining constant. These observations can be explained by a dissolution mechanism being described by a diffusion-controlled transport process determined by the concentration gradients. At higher temperatures the precipitates dissolve in an disordered state as well as in an ordered state. It means that the observed radiation-induced transition is of first order. A statistical model, which permits to deduce the radiation-induced diffusion coefficients from the measured depth profiles, is presented. At room temperature, a value of D[sub mix]/K = 0.75 nm[sup 2]dpa[sup -1] for the diffusion coefficient normalized to the displacement rate is found. This figure confirms that cascade mixing is responsible for the dissolution of the [gamma]' phase. At higher temperatures a more sluggish dissolution is observed. (orig.)

  10. Relation of Engine Turbine-blade Life to Stress-rupture Properties of the Alloys, Stellite 21, Hastelloy B, Cast S-816, Forged S-816, X-40, Nimonic 80, Refractaloy 26, N-155, and Inconel X

    Science.gov (United States)

    Garrett, F B; Yaker, C

    1951-01-01

    An investigation was conducted to relate the engine performance of the heat-resistant alloys, Stellite 21, Hastelloy B, cast S-816, forged S-816, X-40, Nimonic 80, Refractory 26, N-155, and Iconel X to their stress-rupture properties. The engine test consisted of the repetition of a 20-minute cycle, 15 minutes at rated speed and approximately 5 minutes at idle. The results of the investigation indicated a direct correlation between stress-rupture life and blade life for the relatively low-strength alloys. The stress-rupture life and blade life for the relatively high-strength alloys did not correlate because of the effects of the vibratory stresses and the corrosive-gas atmosphere.

  11. An experimental investigation and statistical modelling for trim cutting operation in WEDM of Nimonic-90

    Directory of Open Access Journals (Sweden)

    Vinod Kumar

    2015-09-01

    Full Text Available Trim cutting operation in wire electrical discharge machining (WEDM is considered as a probable solution to improve surface characteristics and geometrical accuracy by removing very small amount of work materials from the surface obtained after a rough cutting operation. In this study, an attempt has been made to model the surface roughness and dimensional shift in trim cutting operations in WEDM process through response surface methodology (RSM. Four process parameters; namely pulse-on time (Ton, servo voltage (SV, wire depth (Wd and Dielectric flow rate (FR have been considered as input parameters in trim cutting operations for modelling. Desirability function has been employed to optimize multi performance characteristics. Increasing the value of Ton, Wd and FR increases the surface roughness and dimensional shift but increasing SV decreases both surface roughness and dimensional shift. Quadratic models have been proposed for both the performance characteristics. In present experimentation, thickness of recast layer was observed in the range of 6μm to 12μm for low to high value of discharge parameters.

  12. A survey on dietary intake in 939 pregnant women%939例孕妇妊娠期膳食营养摄入状况调查

    Institute of Scientific and Technical Information of China (English)

    曹晓辉; 孙丽洲

    2012-01-01

    目的 了解孕期妇女膳食营养素摄入情况.方法 常规产检的孕妇939例,年龄(28.1士3.4)岁,孕前体重(54.42±7.17) kg,体重指数(20.76±2.57) kg/m2.于建围产期保健卡时(孕24-28周)采用24 h膳食回顾法调查孕妇的膳食状况,分析其膳食营养素摄入情况.结果 收集到孕中期膳食调查表605份,24 h总能量摄入为(2208.8±592.1)kJ,为推荐摄入量的(96.04±25.74)%;收集到孕晚期膳食调查表334份,24 h总能量摄入为(2106.0±554.1)kJ,为推荐摄入量的(91.57±24.09)%;孕妇孕中晚期各餐次能量摄入分配不合理.微量元素多来源于植物性,动物性的来源较少.结论 妊娠期妇女的膳食丰富多样,但晚期总能量摄入偏低,各种膳食营养素水平摄入不均,需加强孕期妇女的营养指导.%To investigate the dietary intake of pregnant women. Methods The dietary status of 939 pregnant women was investigated with a 24-h dietary recall method in a period of 24 to 28 weeks of gestation,who aged (28. 1 + 3. 4) years old,weighted (54. 42 + 7. 17) kg and had a mean BMI of (20. 76 + 2. 57) kg/m2. The dietary intake was analyzed. Results A total of 605 cases returned the dietary questionnaires in the second trimester. The total energy intake was (2208. 8 + 592. 1) kj,which accounted for (96. 04 + 25. 74)% of the recommended intake. In the third trimester of pregnancy, 334 cases returned the dietary questionnaires and total energy intake of (2106. 0 + 554.1) kj was calculated, which accounted for (91.57 + 24.09)% of the recommended intake. The distribution of energy intake among the meals was not rational in pregnant women. The majority' of trace elements in the pregnants were got from plants rather than animal sources. Conclusion The diets of pregnant women are varied. But the dietary intake of them is rather lower in the late gestation trimester and the guidance of dietary for pregnant women should be intensified.

  13. Life prediction of advanced materials for gas turbine application

    Energy Technology Data Exchange (ETDEWEB)

    Zamrik, S.Y.; Ray, A.; Koss, D.A.

    1995-12-31

    Emphasis is placed on life characterization based on low cycle fatigue under isothermal conditions and thermomechanical fatigue. Microstructure of failed coated and uncoated specimens is being analyzed. IN 738 LC is the material; the coating is either overlay (NiCoCrAly) or NiAl-based aluminide.

  14. Influence of different etchants on the representation of microstructures in nickel alloys; Einfluss verschiedener Aetzmittel auf die Gefuegedarstellung in Nickellegierungen

    Energy Technology Data Exchange (ETDEWEB)

    Speicher, Magdalena; Scheck, Rudi; Maile, Karl [Stuttgart Univ. (Germany). Materialpruefungsanstalt

    2016-04-15

    This work presents a comparison of selected nickel alloys of the same condition which were treated by means of specifically chosen etching techniques. Microstructures on microscope images of wrought Alloy 617, a casting variant of Alloy 625, a polycrystalline casting alloy IN-738 LC, as well as of a monocrystalline superalloy CM 247 LC SX, respectively, are juxtaposed and evaluated. This approach allows for a comprehensive optical microscopy characterization of the characteristic microstructural features.

  15. Isothermal Oxidation Comparison of Three Ni-Based Superalloys

    Science.gov (United States)

    Mallikarjuna, H. T.; Richards, N. L.; Caley, W. F.

    2017-05-01

    Ni-based superalloys are used for high-temperature components of gas turbines in both industrial and aerospace applications due to their ability to maintain dimensional stability under conditions of high stress and strain. The oxidation resistance of these alloys often dictates their service lifetime. This study focuses on the isothermal oxidation behavior of three Ni-based superalloys, namely, polycrystalline cast IN738LC, single-crystal N5, and a ternary Ni-Fe-Cr (TAS) powder metallurgy alloy. The isothermal oxidation tests were conducted at 900 °C in the static air up to 1000 h, and the specific aspects studied were the oxidation behavior of these chromia-forming and alumina-forming alloys that are used extensively in industry. In particular, the behavior of oxide scale growth and subsurface changes were analyzed in detail using various techniques such as SEM, EDS, and AFM. From the isothermal oxidation kinetics, the oxidation rate constant, k p, was calculated for each alloy and found to be; k p = 2.79 × 10-6 mg2 cm-4 s-1 for IN738LC, k p = 1.42 × 10-7 mg2 cm-4 s-1 for N5 and k p = 1.62 × 10-7 mg2 cm-4 s-1 for TAS. Based on a microstructural analysis, IN738LC exhibited a continuous dense outer scale of Cr2O3 and discontinuous inner scale of Al2O3, whereas N5 and TAS showed a dense outer scale of Al2O3 alone. The results suggested that the N5 and PM-TAS alloys are more oxidation resistant than the IN738LC under these conditions.

  16. Comparison of measured and calculated thermophysical properties of nickel super-alloys

    Directory of Open Access Journals (Sweden)

    A. Kalup

    2016-07-01

    Full Text Available Three real grades of nickel super-alloys (IN 713LC, IN 738LC and IN 792-5A were investigated and values of temperatures of phase transformations and latent heats of melting were obtained. All investigated quantities are very important for thermodynamic and kinetic modelling. Moreover, these data are also valuable for a lot of software used for technological processes modelling. Experimental values were obtained using Differential Thermal Analysis (DTA measurements. Calculations were performed using Thermo-Calc 3.1 software with the use of three different databases (SSOL5, TTNI8 and TCNI6. Comparison and discussion of experimental and calculated data was performed.

  17. EB-PVDによる遮熱コーティングの残留応力のX線評価

    OpenAIRE

    鈴木, 賢治; 和田, 国彦; 松原, 秀彰; 菖蒲, 敬久; 川村, 昌志; 田中, 啓介; SUZUKI, Kenji; Wada, Kunihiko; Matsubara, Hideaki; Shobu, Takahisa; Kawamura. Masashi; Tanaka, Keisuke

    2007-01-01

    The Ni-based superalloy IN738LC was used as the substrate material, and CoNiCrAIY powder was pressureless plasma-sprayed on the substrate as the bond coating. Zirconia was coated as the top coating by the electron beam-physical vapor deposition (EB-PVD) method. In the EB-PVD process, the specimens were kept at 1223K and rotated with 5rpm, 10rpm and 20rpm. According to the microscopic observation and the result of the pole figures, the top coalings had a columnar structure, which was made by t...

  18. Fatigue lifespan of a mobile blade gas turbine with ceramic coating; Vida util por fatiga de un alabe movil de turbina de gas con recubrimiento ceramico

    Energy Technology Data Exchange (ETDEWEB)

    Garcia Illescas, Rafael; Z. Mazur Czerwiec, Zdzislaw; Islas Mungarro, Ricardo [Instituto de Investigaciones Electricas, Cuernavaca, Morelos (Mexico)]. E-mail: rgi@iie.org.mx; mazur@iie.org.mx; rick_iie@terra.com.mx

    2010-11-15

    Fatigue analysis of a gas turbine moving blade made of IN738LC was carried out in order to evaluate useful life time. The life estimation was done from a previous 3D linear finite element analysis where thermal and mechanical stress calculation at high temperatures was done during steady and transient state i.e. normal start ups and shutdowns. Several load histories with different stresses and strains in the blade were used for different cooling conditions including a thermal barrier coating in comparison with to simple blade without such coating. The important effect of high temperatures on the blade material and stress calculations is shown. The analysis is focused on two different critical zones in the blade: the leading edge at the middle of the height and a cooling channel surface, where high stresses were found in numerical analysis as well as in reality. Finally, the benefit of the presence of a thermal barrier coating in the blade life is shown. [Spanish] Se realizo el analisis de fatiga de un alabe movil de turbina de gas fabricado de IN738LC a fin de evaluar su vida util. La estimacion de vida fue realizada a partir de simulaciones lineales de esfuerzos termomecanicos por elemento finito en 3D a altas temperaturas y durante el arranque y paro normal. Se utilizaron diversos historiales de carga, esfuerzos y deformaciones del alabe para diferentes configuraciones de enfriamiento incluyendo el recubrimiento ceramico tipo barrera termica en comparacion con los resultados sin incluir dicho recubrimiento. Se presenta el efecto importante de las temperaturas elevadas en las propiedades de fatiga del material del alabe y en sus esfuerzos. El analisis se centra en dos puntos de interes identificados como criticos: borde de entrada y un canal de enfriamiento, en donde esfuerzos elevados fueron encontrados tanto numericamente como en la realidad. Finalmente se muestra el beneficio del recubrimiento tipo barrera termica en la vida del alabe.

  19. Corrosion behavior of Ni-base superalloys in a hot molten salt

    Energy Technology Data Exchange (ETDEWEB)

    Cho, Soo Haeng; Kang, Dae Seong; Hong, Sun Seok; Hur, Jin Mok; Lee, Han Soo [Korea Atomic Energy Research Institute, Daejeon (Korea, Republic of)

    2008-09-15

    The electrolytic reduction of spent oxide fuel involves the liberation of oxygen in a molten LiCl electrolyte, which results in a chemically aggressive environment that is too corrosive for typical structural materials. So, it is essential to choose the optimum material for the process equipment handling molten salt. In this study, corrosion behavior of Inconel 713LC, Inconel MA 754, Nimonic 80A and Nimonic 90 in the molten salt LiCl-Li{sub 2}O under an oxidizing atmosphere was investigated at 650 .deg. C for 72-216 hrs. Inconel 713LC alloy showed the highest corrosion resistance among the examined alloys. Corrosion products of Inconel 713LC were Cr{sub 2}O{sub 3}, NiCr{sub 2}O{sub 4} and NiO, and those of Inconel MA 754 were Cr{sub 2}O{sub 3} and Li{sub 2}Ni{sub 8}O{sub 10} while Cr{sub 2}O{sub 3}, LiFeO{sub 2}, (Cr, Ti){sub 2}O{sub 3} and Li{sub 2}Ni{sub 8}O{sub 10} were produced from Nimonic 80A. Also, corrosion products of Nimonic 90 were found to be Cr{sub 2}O{sub 3}, (Cr, Ti){sub 2}O{sub 3}, LiAlO{sub 2} and CoCr{sub 2}O{sub 4}. Inconel 713LC showed local corrosion behavior and Inconel MA 754, Nimonic 80A, Nimonic 90 showed uniform corrosion behavior.

  20. Mechanical characteristics and swelling of austenitic Fe-Cr-Mn steels irradiated in the SM-2 and BOR-60 reactors. [0. 4C-12Cr-19Mn-2Ni-Mo-N; 0. 4C-12Cr-14Mn-5Ni-Mo-2Al-B; 0. 4C-17Cr-17Mn-Cu-Mo-Nb-N; Fe-Cr-Ni steel: 0. 8C-16Cr-15Ni-3Mo-Nb; 316; 304

    Energy Technology Data Exchange (ETDEWEB)

    Shamardin, V.K.; Bulanova, T.M.; Neustroev, V.S. (Lenin (V.I.) Research Inst. of Atomic Reactors, Dimitrovgrad (USSR)); Ivanov, L.I.; Djomina, E.V.; Platov, Yu.M. (AN SSSR, Moscow (USSR). A.A. Baikov Inst. of Metallurgy)

    Three types of austenitic Fe-Cr-Mn stainless steels were irradiated simultaneously with Fe-Cr-Ni austenitic steel at temperatures from 400 to 800deg C in the mixed spectrum of the high flux SM-2 reactor to 10 dpa and 700 appm of He and in the BOR-60 reactor to 60 dpa without He generation. The paper presents the swelling and mechanical properties of steels irradiated in the BOR-60 and SM-2 as a function of the concentration of transmuted He and the value of atomic displacement. (orig.).

  1. Pre-oxidation and its effect on reducing high-temperature corrosion of superheater tubes during biomass firing

    DEFF Research Database (Denmark)

    Okoro, Sunday Chukwudi; Kvisgaard, M.; Montgomery, Melanie

    2017-01-01

    -oxidised Al and Ti-containing alloys (Kanthal APM and Nimonic 80A, respectively) was investigated under laboratory conditions mimicking biomass firing. The alloys were pre-oxidised at 900°C for 1 week. Afterwards, pre-oxidised samples, and virgin non-pre-oxidised samples as reference, were coated...

  2. Development of the Work Intention Inventory Short-Form

    Science.gov (United States)

    Nimon, Kim; Zigarmi, Drea

    2015-01-01

    The Work Intention Inventory (WII: Zigarmi, Nimon, Houson, Witt, & Diehl, 2012) was designed to assess five measures of work intention. Measuring employee intentions is important to consider when evaluating outcomes associated with employee engagement or work passion as research indicates intentions are strong predictors of behavior. Following…

  3. Microstructure stability: Optimisation of 263 Ni-based superalloy

    Directory of Open Access Journals (Sweden)

    Crozet Coraline

    2014-01-01

    Full Text Available To reduce CO2 emissions on coal-fired power plant, A-ultra supercritical (A-USC power plant whose steam conditions exceed 700 °C are being developed. At these elevated temperatures, the use of Ni-base superalloys becomes necessary. In this context and within the European project NextGenPower, focus is made on commercial Nimonic C-263 as a candidate material for turbine rotors. Nimonic C-263 is known to have low sensitivity to segregation, high workability and high weldability which are major properties for the manufacture of large shafts. Long-term creep strength is also required for this application and unfortunately Nimonic C-263 shows η-phase precipitation after long-time exposure between 700 °C–900 °C which is detrimental for long-term creep properties. The composition of Nimonic C-263 was thus optimised to overcome the formation of η-phase. Trial tests were made in order to study the effect of hardening contribution elements on microstructural and mechanical properties. Then, a 500 mm diameter forged rotor was made from optimised 263 alloy and shows promising properties.

  4. Investigation of Creep Feed Grinding Parameters and Heat treatment Effects on the Nickel-base Superalloys

    Institute of Scientific and Technical Information of China (English)

    Hasan Jamshidi; Sayed Ali Sadough Vanini; Alireza Attari

    2004-01-01

    The Nickel base Superalloys are the most famous complicated and useable of Superalloys to make hot zone components of the gas turbines. The complicated dimensional tolerances, specially at the root of the blade show importance of grinding processes at the production of blades root. The prediction of the effect of machining parameters on the soundness of component surface strengthening for reaching to a suitable surface finishing and avoiding from crack formation at the work part during machining operation often is not easy and feasible so needs to more industrial investigation.This research is about frame 5 blade designed by GE and made from Superalloy IN738LC has been investigated. The formation of a plastically deformed and heat affected zone during grinding of Superalloy IN738LC with a high depth of cut but slow work speed (creep feed grinding) was investigated. Parameters such as work speed, depth of cut and radial dressing speed have been considered as variables and their effects have been studied. During experimental performed, the voltage and current of motor measured and power and special energy calculated.Some samples heat-treated (of the 1176℃ for 1 hr under neutral argon gas and cooling rate of 15℃/min up to 537℃ and then air cooling) to study grains recrystallization. Other samples have been created from the roots of blades and then coated by Nickel to measure boundary layer micro-hardness. The results show that increasing work speed leads to increasing the use power. Increasing the depth of cut, by increasing material removal rate, and the radial dressing speed, by decreasing power, lead to decreasing special energy. The temperature created by grinding lead to decreasing plastic deformation and boundary layer formation. When the radial dressing speed changes from 1 to 0.6 μm/rev and other parameters are kept unchanged the roughness of surface increases and the special energy decreases. Sufficient dressing is very essential in limiting the width

  5. Life prediction methodology for thermal-mechanical fatigue and elevated temperature creep design

    Science.gov (United States)

    Annigeri, Ravindra

    Nickel-based superalloys are used for hot section components of gas turbine engines. Life prediction techniques are necessary to assess service damage in superalloy components resulting from thermal-mechanical fatigue (TMF) and elevated temperature creep. A new TMF life model based on continuum damage mechanics has been developed and applied to IN 738 LC substrate material with and without coating. The model also characterizes TMF failure in bulk NiCoCrAlY overlay and NiAl aluminide coatings. The inputs to the TMF life model are mechanical strain range, hold time, peak cycle temperatures and maximum stress measured from the stabilized or mid-life hysteresis loops. A viscoplastic model is used to predict the stress-strain hysteresis loops. A flow rule used in the viscoplastic model characterizes the inelastic strain rate as a function of the applied stress and a set of three internal stress variables known as back stress, drag stress and limit stress. Test results show that the viscoplastic model can reasonably predict time-dependent stress-strain response of the coated material and stress relaxation during hold times. In addition to the TMF life prediction methodology, a model has been developed to characterize the uniaxial and multiaxial creep behavior. An effective stress defined as the applied stress minus the back stress is used to characterize the creep recovery and primary creep behavior. The back stress has terms representing strain hardening, dynamic recovery and thermal recovery. Whenever the back stress is greater than the applied stress, the model predicts a negative creep rate observed during multiple stress and multiple temperature cyclic tests. The model also predicted the rupture time and the remaining life that are important for life assessment. The model has been applied to IN 738 LC, Mar-M247, bulk NiCoCrAlY overlay coating and 316 austenitic stainless steel. The proposed model predicts creep response with a reasonable accuracy for wide range of

  6. Oxidation resistance of Al2O3-nanostructured/CSZ composite compared to conventional CSZ and YSZ thermal barrier coatings

    Science.gov (United States)

    Keyvani, A.; Bahamirian, M.

    2016-10-01

    Thermal barrier coatings are widely used in combustion sections of turbine engines, however, their main disadvantage is the spallation from the bond coat, occurring due to oxidation and formation of thermally grown oxide (TGO). In this paper, the oxidation resistance of yttria stabilized zirconia (YSZ), ceria stabilized zirconia (CSZ), and Al2O3-nanostructured/CSZ composite coatings have been studied and compared with each other. Samples were heated in air at 1100 °C using an electrical furnace. Three types of the top coats were applied by thermal spray technique on IN738LC base metal. Scanning electron microscopy was used to study the microstructure of the coatings before and after the oxidation. The experimental results showed that Al2O3-nanostructured/CSZ composite coating exhibits considerably better oxidation resistance compared to conventional YSZ and CSZ coatings. The microstructural analysis indicated a smaller growth of TGO in the Al2O3-nanostructured/CSZ composite coating, improving the oxidation resistance of the coating.

  7. Misfit in Inconel-Type Superalloy

    Directory of Open Access Journals (Sweden)

    Pavel Strunz

    2013-01-01

    Full Text Available An important parameter for the characterization of microstructural changes in nickel base superalloys is the misfit - the relative difference between lattice parameters of γ matrix and γ′ precipitates. The misfit in IN738LC superalloy was examined at POLDI time-of-flight (TOF neutron diffractometer both at room temperature and in situ at elevated temperatures using a high-temperature furnace. A careful out-of-furnace measurement yielded the lattice parameters of both γ and γ′ phase at room temperature (aγ=3.58611(10 Å, aγ′=3.58857(17 Å as well as the misfit (equal to 6.9(6×10-4. The in situ measurement at elevated temperatures provided the temperature dependence of the lattice parameters of γ (up to 1120°C and γ′ (up to 1000°C. Using these data, the evolution of the misfit with temperature was calculated. The misfit decreases with increasing temperature until it reaches zero value at a temperature around 800°C. Above 800°C, it becomes negative.

  8. Materials for Advanced Ultrasupercritical Steam Turbines Task 3: Materials for Non-Welded Rotors, Buckets, and BoltingMaterials for Advanced Ultrasupercritical Steam Turbines

    Energy Technology Data Exchange (ETDEWEB)

    Saha, Deepak

    2015-09-15

    The primary objective of the task was to characterize the materials suitable for mechanically coupled rotor, buckets and bolting operating with an inlet temperature of 760°C (1400°F). A previous study DOE-FC26-05NT42442, identified alloys such as Haynes®282®, Nimonic 105, Inconel 740, Waspaloy, Nimonic 263, and Inconel 617 as potential alloys that met the requirements for the necessary operating conditions. Of all the identified materials, Waspaloy has been widely utilized in the aviation industry in the form of disk and other smaller forgings, and sufficient material properties and vendor experience exist, for the design and manufacture of large components. The European program characterizing materials for A-USC conditions are evaluating Nimonic 263 and Inconel 617 for large components. Inconel 740 has been studied extensively as a part of the boiler consortium and is code approved. Therefore, the consortium focused efforts in the development of material properties for Haynes®282® and Nimonic 105 to avoid replicative efforts and provide material choices/trade off during the detailed design of large components. Commercially available Nimonic 105 and Haynes®282® were evaluated for microstructural stability by long term thermal exposure studies. Material properties requisite for design such as tensile, creep / rupture, low cycle fatigue, high cycle fatigue, fatigue crack growth rate, hold-time fatigue, fracture toughness, and stress relaxation are documented in this report. A key requisite for the success of the program was a need demonstrate the successful scale up of the down-selected alloys, to large components. All property evaluations in the past were performed on commercially available bar/billet forms. Components in power plant equipment such as rotors and castings are several orders in magnitude larger and there is a real need to resolve the scalability issue. Nimonic 105 contains high volume fraction y’ [>50%], and hence the alloy is best suited

  9. KCl-induced high temperature corrosion of selected commercial alloys. Part II: alumina and silica-formers

    DEFF Research Database (Denmark)

    Kiamehr, Saeed; Dahl, Kristian Vinter; Montgomery, Melanie

    2016-01-01

    ). It was observed that alloying with aluminum did not lead to the formation of protective alumina for the studied alloys. The silicon containing stainless steel 153MA showed an analogous performance to low silicon austenitic stainless steels of similar chromium and nickel contents. For alloy HR160, a potassium......-chromium-silicon-oxygen containing layer forms as the innermost corrosion product. The layer was uniformly distributed over the surface and appears to render some protection as this alloy exhibited the best performance among the investigated alloys. To reveal further aspects of the corrosion mechanism, Nimonic 80A was exposed...

  10. Influence of preoxidation on high temperature corrosion of a Ni-based alloy under conditions relevant to biomass firing

    DEFF Research Database (Denmark)

    Okoro, Sunday Chukwudi; Montgomery, Melanie; Jappe Frandsen, Flemming

    2017-01-01

    of preoxidized layers formed on a commercial Cr-Ti-Al-containing Ni-based alloy (Nimonic 80A) to withstand biomass-induced corrosion was investigated. Preoxidation treatments at 900 °C in O2 and O2 + 10 vol% H2O, respectively, were conducted before samples were exposed to conditions that mimicked biomass firing...... attack and formed porous non-protective oxides containing the alloying elements, Ni, Cr, Ti and Al. The influence of the preoxidation layers on the corrosion mechanism is discussed....

  11. Correlation and contingency analysis of atom probe data: Diffusion-controlled dissolution of precipitates

    Energy Technology Data Exchange (ETDEWEB)

    Camus, E. (Hahn-Meitner-Institut Berlin GmbH (Germany)); Abromeit, C. (Hahn-Meitner-Institut Berlin GmbH (Germany))

    1994-05-01

    A statistical analysis of atom probe data is developed for evaluating the evolution of local composition fluctuations in concentrated alloys. The model allows the calculation of theoretical correlation and contingency coefficients for a presumed alloy microstructure taking into account the instrumental parameters, i.e. aperture size, block size and detector efficiency. A comparison of theoretical coefficients with those obtained from measured concentration profiles gives access to physically relevant parameters. The analysis is applied to the diffusion-controlled dissolution of spherical precipitates in the technical alloy Nimonic PE16 under ion irradiation. (orig.)

  12. Determination of elastic modulus in nickel alloy from ultrasonic measurements

    Indian Academy of Sciences (India)

    Nikhat Parveen; G V S Murthy

    2011-04-01

    Elastic constants relate technological, structural and safety aspects to various materials phenomena and to their fundamental interatomic forces. Hence, they are of fundamental importance in almost all engineering applications. Thus its determination is of utmost importance. The aim of the present investigation is to study the behaviour of elastic constants and the variation on heat treatment in a nickel base super alloy Nimonic 263 by ultrasonic velocity measurements. From the present study it is evident that the elastic moduli of the material are very sensitive to any minor compositional changes, resulting due to the formation of intermetallic phases on heat treatment and can be effectively monitored by ultrasonic.

  13. High temperature corrosion by combustion gases produced by burning liquid fuels containing sulphur, sodium and vanadium.

    OpenAIRE

    Khan, Fazlur Rahman

    1980-01-01

    High temperature corrosion, at 730° C, by combustion gases produced by burning liquid fuels in a laboratory combustor has been investigated. A selected range of steels and alloys (mild steel, stainless steel type 347, Nimonic N90, N105, and IN657) have been tested in the combustion gases using fuels containing varying amounts of impurities in the range of 0 - 6% sulphur, 0 - 60 ppm sodium, and 0 - 300 ppm vanadium. On the basis of the comprehensive results a computer programme was written t...

  14. Analysis of zirconium and nickel based alloys and zirconium oxides by relative and internal monostandard neutron activation analysis methods

    Energy Technology Data Exchange (ETDEWEB)

    Shinde, Amol D.; Acharya, Raghunath; Reddy, Annareddy V. R. [Bhabha Atomic Research Centre, Mumbai (India)

    2017-04-15

    The chemical characterization of metallic alloys and oxides is conventionally carried out by wet chemical analytical methods and/or instrumental methods. Instrumental neutron activation analysis (INAA) is capable of analyzing samples nondestructively. As a part of a chemical quality control exercise, Zircaloys 2 and 4, nimonic alloy, and zirconium oxide samples were analyzed by two INAA methods. The samples of alloys and oxides were also analyzed by inductively coupled plasma optical emission spectroscopy (ICP-OES) and direct current Arc OES methods, respectively, for quality assurance purposes. The samples are important in various fields including nuclear technology. Samples were neutron irradiated using nuclear reactors, and the radioactive assay was carried out using high-resolution gamma-ray spectrometry. Major to trace mass fractions were determined using both relative and internal monostandard (IM) NAA methods as well as OES methods. In the case of alloys, compositional analyses as well as concentrations of some trace elements were determined, whereas in the case of zirconium oxides, six trace elements were determined. For method validation, British Chemical Standard (BCS)-certified reference material 310/1 (a nimonic alloy) was analyzed using both relative INAA and IM-NAA methods. The results showed that IM-NAA and relative INAA methods can be used for nondestructive chemical quality control of alloys and oxide samples.

  15. Evaluation of the Low Heat Input Process for Weld Repair of Nickel-Base Superalloys

    Science.gov (United States)

    Durocher, J.; Richards, N. L.

    2011-10-01

    The repair of turbine blades and vanes commonly involves gas tungsten arc welding or an equivalent process, but unfortunately these components are often susceptible to heat-affected zone (HAZ) cracking during the weld repair process. This is a major problem especially in cast alloys due to their coarse-grain size and where the (Al + Ti) contents is in excess of 3-4%; vacuum brazing is also used but mainly on low stress non-rotating components such as vanes. Micro-welding has the potential to deposit small amounts of filler at low heat input levels with minimum HAZ and thus is an attractive process for depositing a quality weld. As with conventional fusion processes, the filler alloy is deposited by the generation of a low power arc between a consumable electrode and the substrate. The low heat input of this process offers unique advantages over more common welding processes such as gas tungsten arc, plasma arc, laser, and electron beam welding. In this study, the low heat input characteristic of micro-welding has been used to simulate weld repair using Inconel (IN) (Inconel and IN are trademarks of INCO Alloys International) 625, Rene (Rene is a trademark of General Electric Company) 41, Nimonic (Nimonic is a trademark of INCO Alloys International) 105 and Inconel 738LC filler alloys, to a cast Inconel 738LC substrate. The effect of micro-welding process parameters on the deposition rate, coating quality, and substrate has been investigated.

  16. Mitral annular calcification and incident ischemic stroke in treated hypertensive patients

    DEFF Research Database (Denmark)

    De Marco, Marina; Gerdts, Eva; Casalnuovo, Giuseppina;

    2013-01-01

    ). Methods Baseline and follow-up clinical and echocardiographic parameters were assessed in 939 hypertensive patients with electrocardiogram (ECG) LVH participating in the Losartan Intervention for Endpoint reduction in hypertension (LIFE) echocardiography substudy (66±7 years; 42% women; 11% with diabetes...

  17. Environmental aspects on LCF-life of Ni-base superalloys during long term operation; Miljoeinverkan paa LCF-egenskaper vid laanga drifttider hos superlegeringar

    Energy Technology Data Exchange (ETDEWEB)

    Moverare, Johan; Leijon, Gunnar; Palmert, Frans

    2012-02-15

    The applicability of fine grain polycrystalline nickel base superalloys in gas or steam turbine applications is often limited by their susceptibility to fast intergranular cracking during fatigue in combination with extended hold times at high temperatures and high tensile stresses. This effect is further enhanced in corrosive environments even at moderate temperatures such as 400-600 deg In this study the negative effect of SO{sub 2} + water vapour on the low cycle fatigue resistance of three different nickel based superalloys (Nimonic 901, Inconel 718 and 718 plus) has been studied at 450 deg and 550 deg. A negative effect was found on both the crack initiation and crack propagation process. The effect increases with increasing temperature and is likely to be influenced by both the chemical composition and the grain size of the material. The negative effect of water vapour + SO{sub 2} is manifested by a decreased resistance to cyclic plastic deformation and a transition from transcrystalline to intercrystalline fracture behaviour. In Nimonic 901 this negative effect increases with the degree of plastic deformation. For lower mechanical strain amplitudes where the number of cycles and the total exposure time is increased the environmental impact is reduced. Similar trends can also be noticed for the other alloys. The surface corrosion in air and in SO{sub 2} + water vapour are found to be rather similar in this study and it is therefore concluded that the surface scale can remain adherent and protective if the strains on the oxide scale are low. However, for LCF tests with higher strain ranges, the oxide scale will rupture preferably at the grain boundaries and intergranular microcracks will initiate which promotes inward diffusion of embritteling elements such as oxygen and sulphur. Inconel 718 seems to be more sensitive to SO{sub 2} + water vapour than Nimonic 901 when tested at 450. The overall resistance to LCF is however still higher in Inconel 718 for the

  18. Environmental aspects on LCF-life of Ni-base superalloys during long term operation; Miljoeinverkan paa LCF-egenskaper vid laanga drifttider hos superlegeringar

    Energy Technology Data Exchange (ETDEWEB)

    Moverare, Johan; Leijon, Gunnar; Palmert, Frans

    2012-02-15

    The applicability of fine grain polycrystalline nickel base superalloys in gas or steam turbine applications is often limited by their susceptibility to fast intergranular cracking during fatigue in combination with extended hold times at high temperatures and high tensile stresses. This effect is further enhanced in corrosive environments even at moderate temperatures such as 400-600 deg In this study the negative effect of SO{sub 2} + water vapour on the low cycle fatigue resistance of three different nickel based superalloys (Nimonic 901, Inconel 718 and 718 plus) has been studied at 450 deg and 550 deg. A negative effect was found on both the crack initiation and crack propagation process. The effect increases with increasing temperature and is likely to be influenced by both the chemical composition and the grain size of the material. The negative effect of water vapour + SO{sub 2} is manifested by a decreased resistance to cyclic plastic deformation and a transition from transcrystalline to intercrystalline fracture behaviour. In Nimonic 901 this negative effect increases with the degree of plastic deformation. For lower mechanical strain amplitudes where the number of cycles and the total exposure time is increased the environmental impact is reduced. Similar trends can also be noticed for the other alloys. The surface corrosion in air and in SO{sub 2} + water vapour are found to be rather similar in this study and it is therefore concluded that the surface scale can remain adherent and protective if the strains on the oxide scale are low. However, for LCF tests with higher strain ranges, the oxide scale will rupture preferably at the grain boundaries and intergranular microcracks will initiate which promotes inward diffusion of embritteling elements such as oxygen and sulphur. Inconel 718 seems to be more sensitive to SO{sub 2} + water vapour than Nimonic 901 when tested at 450. The overall resistance to LCF is however still higher in Inconel 718 for the

  19. Mechanical Properties and Fracture Behaviour of LMD Produced 2.4682 and Wrought 2.4630 Dissimilar Welds

    Science.gov (United States)

    Dahmen, Martin; Göbel, Marco

    A bearing made of Stellite 31 (2.4682) has to be welded onto a housing of Nimonic 75 (2.4630) by autogenous laser beam welding. The bearing part is produced by laser metal deposition (LMD), the housing consists of wrought sheet metal. An investigation is undertaken in order to study the effect of the anisotropy of the LMD part on the weld quality. Tensile specimens were produced and tested under varying load directions and test temperatures, and application of different weld heat treatments. The fractured specimens were analysed by metallography and fractography. Tensile tests at room temperature show a dependency of the fracture location and the mode of failure on the load direction with respect to the layer direction in conjunction with the heat treatment. At elevated temperature of 750° all specimens broke in the base material of 2.4630 in ductile fracture mode. Strength measured supersedes the values of either of the base materials.

  20. Proceedings from the Conference on Critical Issues in the Development of High Temperature Structural Materials Held in Kona, Hawaii on March 7-14, 1993,

    Science.gov (United States)

    1993-01-14

    INCONEL . X-750.650VC , RENM 88. 85&C O NIMONIc 9n o. , 5%’ SUDIMET 718 . 550’C 10- A286. 5S50C o Ni•.I * a Hf. 600*C I0 ’ 0 IC-221.,S0C " ~10-7z 10"o 101...10). High temperature yield strength of the XD® Ti-Al is not a great deal different than that of an alloy such as Inconel 713C but the density is about...the very slow transport of SL through the Ti 5 Si 3 to the Ti substrate and the slow dissolution of Si into the TL. In experimental oxidation studies

  1. The shape effects of nanoparticles suspended in HFE-7100 over wedge with entropy generation and mixed convection

    Science.gov (United States)

    Ellahi, R.; Hassan, M.; Zeeshan, A.; Khan, Ambreen A.

    2016-06-01

    The flow of mixed convection nanofluid over wedge under the effects of porous medium is investigated. The HFE-7100 Engineered Fluid having Nimonic 80a metal nanoparticles of spherical and non-spherical shapes with different sizes is used. The particle shape effects on Bejan number and entropy generation are taken into account. The system of partial differential equations is first written in terms of ordinary differential equations using adequate similarity transformations and then solved analytically. Analytical solutions of the resulting equations are obtained for the velocity and temperature profiles. Simultaneous effects of porous medium, particle volume friction, mixed convection parameter, and angle of wedge in the presence of different shapes nanoparticles are demonstrated graphically. Effects of particle concentrations, sizes on wall stress, heat transfer coefficient of Skin friction, and Nusselt are discussed in the form of tables.

  2. A non-contacting instrument for direct stress mapping

    Science.gov (United States)

    Oliver, David E.

    An instrument called SPATE (stress pattern analysis by measurement of thermal emission) developed for noncontact measurements of stress in structures and components under cyclic load or vibration is described. The method is based on the phenomenon called the thermoelastic or Kelvin effect, whereby cyclic changes in the volume or pressure in a material produce cyclic temperature changes that are proportional to stress. The temperature changes measured by SPATE are totally reversible and are independent of heating due to material hysteresis damping. Two instrument was used to test structural materials including steels, aluminum alloys, a magnesium alloy, titanium, Nimonic 90, copper, brass, silicon nitride, Hylox 961, plexiglass, epoxy, polyester, rubber, Kevlar, wood, brick, concrete, 'live' bone, glass, boron, and various composites. The results of SPATE test on a stage-one turbine blade (tested at 9224 Hz) and a notched aluminum plate loaded in tension at 20 Hz are presented together with a diagram of the SPATE equipment.

  3. Investigation into the high temperature wear properties of alloys contacting against different counterfaces

    Energy Technology Data Exchange (ETDEWEB)

    Wood, P.D.; Datta, P.K.; Burnell-Gray, J.S. [Northumbria Univ., Newcastle (United Kingdom). Surface Eng. Res. Group; Wood, N.

    1997-12-31

    Wear tests have been conducted on a reciprocating high temperature rig at 750 C and a load of 7N using a stellite 6 and incoloy 800 counterface. The ODS alloys (MA956, PM2000 and PM2000SD) all showed poor wear resistance and the absence of glaze formation when worn against Incoloy 800. Glaze formation occurred when the ODS alloys were tested againststellite 6 providing very good wear protection. Nimonic 80A tested under similar conditions exhibited good wear resistance against Incoloy 800 (presence of glazes) and poor wear resistance against stellite 6 (absence of glazes). Titanium aluminide showed very good wear resistance when tested against incoloy 800 and stellite 6. In both cases, the glaze and underlying oxide particles were entirely formed from the counterface material. These results show the strong influence of the counterface materials on the formation of wear resistant glazes. (orig.) 5 refs.

  4. Disordering and dissolution of [gamma][prime] precipitates under ion irradiation

    Energy Technology Data Exchange (ETDEWEB)

    Bourdeau, F.; Camus, E.; Abromeit, C.; Wollenberger, H. (Hahn-Meitner-Institut Berlin GmbH, Glienicker Stragese 100, D-14109 Berlin (Germany))

    1994-12-01

    The stability of the [gamma][prime] phase of the nickel-base alloy Nimonic PE16 under irradiation with Ni[sup +] ions of 300-keV energy is studied by means of transmission electron microscopy. The disordering of the [gamma][prime] phase could be followed as a function of fluence. The main finding is the observation of weak but measurable superlattice reflections between 0.1 and 1 dpa after irradiation at room temperature. The superlattice reflections disappear in two steps. Their intensities decrease considerably within a fluence of 0.1 dpa, while weak intensities are observed up to a fluence of 1 dpa. These reflections disappear completely after a fluence of 2 dpa. The results are discussed within a model which considers both disordering and dissolution of precipitates under cascade producing irradiation.

  5. Cobalt: A vital element in the aircraft engine industry

    Science.gov (United States)

    Stephens, J. R.

    1981-01-01

    Recent trends in the United States consumption of cobalt indicate that superalloys for aircraft engine manufacture require increasing amounts of this strategic element. Superalloys consume a lion's share of total U.S. cobalt usage which was about 16 million pounds in 1980. In excess of 90 percent of the cobalt used in this country was imported, principally from the African countries of Zaire and Zambia. Early studies on the roles of cobalt as an alloying element in high temperature alloys concentrated on the simple Ni-Cr and Nimonic alloy series. The role of cobalt in current complex nickel base superalloys is not well defined and indeed, the need for the high concentration of cobalt in widely used nickel base superalloys is not firmly established. The current cobalt situation is reviewed as it applies to superalloys and the opportunities for research to reduce the consumption of cobalt in the aircraft engine industry are described.

  6. Creep rupture behavior of candidate materials for nuclear process heat applications

    Energy Technology Data Exchange (ETDEWEB)

    Schubert, F.; te Heesen, E.; Bruch, U.; Cook, R.; Diehl, H.; Ennis, P.J.; Jakobeit, W.; Penkalla, H.J.; Ullrich, G.

    1984-08-01

    Creep and stress rupture properties are determined for the candidate materials to be used in hightemperature gas-cooled reactor (HTGR) components. The materials and test methods are briefly described based on experimental results of test durations of about20000 h. The medium creep strengths of the alloys Inconel-617, Hastelloy-X, Nimonic-86, Hastelloy-S, Manaurite-36X, IN-519, and Incoloy-800H are compared showing that Inconel-617 has the best creep rupture properties in the temperature range above 800/sup 0/C. The rupture time of welded joints is in the lower range of the scatterband of the parent metal. The properties determined in different simulated HTGR atmospheres are within the scatterband of the properties obtained in air. Extrapolation methods are discussed and a modified minimum commitment method is favored.

  7. Aleación superficial de superaleaciones base níquel mediante láser

    Directory of Open Access Journals (Sweden)

    Rodríguez, G. P.

    1998-04-01

    Full Text Available Ni based superalloys present a high oxidation resistance at high temperature as well as good mechanical properties. But new tecnhology developments forcé to research in this materials to improve their properties at high temperature. In this work, two Ni based superalloys (Nimonic 80A and Inconel 600 were surface alloyed with aluminium using a high power laser. SEM and EDX were used to study the microstructure of the obtained coatings. Alloyed specimens were tested at 1.273 K between 24 and 250 h. Results showed the generation of a protective and continuous coating of alumina on the laser treated specimens surface that can improve oxidation resistance.

    Las superaleaciones base níquel presentan una elevada resistencia a la oxidación a alta temperatura, así como excelentes propiedades mecánicas. Los nuevos desarrollos tecnológicos (condiciones cada vez más agresivas obligan a una casi continua modificación de dichas aleaciones. En el presente trabajo, dos superaleaciones base níquel (Nimonic 80A e Inconel 600 se alean superficialmente con aluminio utilizando un láser de alta potencia. Se estudia la microestructura de la capas obtenidas mediante SEM y EDX. Se realizan ensayos de oxidación a 1.273 K sobre las probetas aleadas y sobre el material base durante tiempos variables entre 24 y 250 h. Los resultados indican la formación de una capa protectora de alúmina sobre las probetas aleadas que puede incrementar la resistencia a la oxidación.

  8. Development of service-relevant materials data and economic quality assurance and machining procedures for gas turbine blades. Final report; Entwicklung betriebsrelevanter Werkstoffkennwerte und wirtschaftlicher Qualitaetssicherungs- und Bearbeitungsverfahren fuer GT-Schaufeln. Schlussbericht

    Energy Technology Data Exchange (ETDEWEB)

    Buergel, R.; Rechtenbacher, H.

    1994-01-01

    In the frame of the reported project, together with the programme partners, optimization of service relevant properties as well as modification of manufacturing procedures for the forged alloy Nimonic 101 were achieved. These results are directly implementable into serial production and cause improved service reliability and economic benefit. For the forged alloy Udimet 720 materials data were generated in accordance with the programme plan. The final evaluation for this alloy will be performed by the project partner Siemens-KWU. The qualification of fine-grained investment cast blades of IN 792 for large rear=stage blading is not yet fully completed. Three major questions are lacking final answers: - Does a stress rupture strength advantage exist over the forged alloy Udimet 720/coarse/grained? - Can a high cycle fatigue strength as high as that for Udimet 720/coarse-grained be met reproducibly? - Does the investment cast blades offer a cost advantage over the forged ones - technical qualification assumed? The programme helped significantly in preparing the right answers to these questions. (orig.) [Deutsch] Im Rahmen des berichteten Teilvorhabens ist es in Zusammenarbeit mit den Projektpartnern gelungen, fuer die Schmiedelegierung Nimonic 101 die betriebsrelevanten Eigenschaften zu optimieren, sowie die Schaufelherstellung so zu modifizieren, dass die Betriebszuverlaessigkeit verbessert wird. Diese Ergebnisse sind direkt in die Serienfertigung implementierbar und damit wirtschaftlich nutzbar. Fuer die Schmiedelegierung Udimet 720 wurden im Rahmen des Projektverbundes Werkstoffkennwerte ermittelt. Die Gesamtauswertung fuer diesen Werkstoff erfolgt von Projektpartner Siemens-KWU. Das Bild zur Qualifikation feinkoerniger Feingussschaufeln ist noch nicht restlos klar. Drei wesentliche, noch abschliessend zu beantwortende Fragen sind: - Ergibt sich ein Zeitstandfestigkeitsvorteil gegenueber der Schmiedelegierung Udimet 720/Grobkorn? - Laesst sich reproduzierbar eine

  9. The Possible Climatic Impact in China of Iceland's Eldgja Eruption Inferred from Historical Sources

    Energy Technology Data Exchange (ETDEWEB)

    Fei, Jie [State Key Laboratory of Loess and Quaternary Geology, Institute of Earth Environment, Chinese Academy of Sciences, Xi' an, 710075 (China); Zhou, Jie [Graduate School, Chinese Academy of Sciences, Beijing, 100039 (China)

    2006-06-15

    Based on Chinese historical sources, the possible climatic impact in China of the prolonged Eldgja eruption starting around 934 AD was investigated. An extremely hot summer was reported in 934 AD; hundreds of people died of the intense heat of this summer in Luoyang, the capital of the Later Tang Empire (923-936 AD). Snowless (and possibly also mild) winters probably occurred successively following the Eldgja eruption until 938 AD. In 939 AD, cold weather set in abruptly and lasted for about 3 years; whereas peak cooling occurred in 939AD. In the summer of 939 AD, it snowed in the southeast of the Inner Mongolia Plateau (about 40-44N, 113-123E). From 939AD to 941 AD, hard winters occurred successively in China. Worse, unprecedented drought and plague of locusts broke out in 942 AD and persisted in 943 AD. More than several hundred thousand people were starved to death. This catastrophe was at least partly responsible for the collapse of the Later Jin Dynasty in China. By comparison with the tree-ring evidence and uncovered European historical evidence, the spatial response to the Eldgja eruption appeared to be complex, whereas hemispheric or global cooling occurred in 939-942 AD.

  10. Hot Corrosion of Coated Single Crystal Superalloys

    Energy Technology Data Exchange (ETDEWEB)

    Simms, N. J.; Encinas-Oropesa, A.; Nicholls, J.R. [Cranfield University, Power Generation Technology Centre, Cranfield, Beds, MK43 0AL (United Kingdom)

    2004-07-01

    Gas turbines are at the heart of many modern power systems, with combined cycle power generation utilising natural gas being an effective way of reducing environmental emissions compared to conventional pulverized coal fired plants. The development of gas turbine technology has been focused on increasing its efficiency. However, the lives of the hot gas path components within these gas turbines are also critical to the viability of the power systems. Single crystal superalloys have been developed for use with clean fuel/air but are now being used in industrial gas turbines that may need to run with dirtier fuel/air. Indeed, gas turbine based power systems are being evaluated in which solid fuels (e.g. coal and/or biomass) are gasified to produce fuel gases, which introduces the potential for significant corrosive and erosive damage to gas turbine blades and vanes. The performance of these materials, with coatings, has to be determined before they can be used with confidence in dirtier fuel environments. This paper reports results from a series of laboratory tests carried out using the 'deposit replenishment' technique to investigate the sensitivity of candidate materials to exposure conditions anticipated in such gas turbines. The materials investigated have included CMSX-4 and SC{sup 2}-B (both bare and with Pt-Al and Amdry 997 coatings) as well as conventional nickel based superalloys such as IN738LC for comparison. The exposure conditions within the laboratory tests have covered ranges of SO{sub x} (50 and 500 vpm) and HCl (0 and 500 vpm) in air, as well as 4/1 (Na/K){sub 2}SO{sub 4} deposits, with deposition fluxes of 1.5, 5 and 15 {mu}g/cm{sup 2}/h, for periods of up to 500 hours at 700 and 900 deg. C. Data on the performance of materials has been obtained using dimensional metrology: pre-exposure contact measurements and post-exposure measurements of features on polished cross-sections. These measurement methods allow distributions of damage data to

  11. Materials for Advanced Ultrasupercritical Steam Turbines Task 4: Cast Superalloy Development

    Energy Technology Data Exchange (ETDEWEB)

    Thangirala, Mani

    2015-09-30

    The Steam Turbine critical stationary structural components are high integrity Large Shell and Valve Casing heavy section Castings, containing high temperature steam under high pressures. Hence to support the development of advanced materials technology for use in an AUSC steam turbine capable of operating with steam conditions of 760°C (1400°F) and 35 Mpa (5000 psia), Casting alloy selection and evaluation of mechanical, metallurgical properties and castability with robust manufacturing methods are mandated. Alloy down select from Phase 1 based on producability criteria and creep rupture properties tested by NETL-Albany and ORNL directed the consortium to investigate cast properties of Haynes 282 and Haynes 263. The goals of Task 4 in Phase 2 are to understand a broader range of mechanical properties, the impact of manufacturing variables on those properties. Scale up the size of heats to production levels to facilitate the understanding of the impact of heat and component weight, on metallurgical and mechanical behavior. GE Power & Water Materials and Processes Engineering for the Phase 2, Task 4.0 Castings work, systematically designed and executed casting material property evaluation, multiple test programs. Starting from 15 lbs. cylinder castings to world’s first 17,000 lbs. poured weight, heavy section large steam turbine partial valve Haynes 282 super alloy casting. This has demonstrated scalability of the material for steam Turbine applications. Activities under Task 4.0, Investigated and characterized various mechanical properties of Cast Haynes 282 and Cast Nimonic 263. The development stages involved were: 1) Small Cast Evaluation: 4 inch diam. Haynes 282 and Nimonic 263 Cylinders. This provided effects of liquidus super heat range and first baseline mechanical data on cast versions of conventional vacuum re-melted and forged Ni based super alloys. 2) Step block castings of 300 lbs. and 600 lbs. Haynes 282 from 2 foundry heats were evaluated which

  12. Materials for advanced ultrasupercritical steam turbines

    Energy Technology Data Exchange (ETDEWEB)

    Purgert, Robert [Energy Industries Of Ohio Inc., Independence, OH (United States); Shingledecker, John [Energy Industries Of Ohio Inc., Independence, OH (United States); Saha, Deepak [Energy Industries Of Ohio Inc., Independence, OH (United States); Thangirala, Mani [Energy Industries Of Ohio Inc., Independence, OH (United States); Booras, George [Energy Industries Of Ohio Inc., Independence, OH (United States); Powers, John [Energy Industries Of Ohio Inc., Independence, OH (United States); Riley, Colin [Energy Industries Of Ohio Inc., Independence, OH (United States); Hendrix, Howard [Energy Industries Of Ohio Inc., Independence, OH (United States)

    2015-12-01

    The U.S. Department of Energy (DOE) and the Ohio Coal Development Office (OCDO) have sponsored a project aimed at identifying, evaluating, and qualifying the materials needed for the construction of the critical components of coal-fired power plants capable of operating at much higher efficiencies than the current generation of supercritical plants. This increased efficiency is expected to be achieved principally through the use of advanced ultrasupercritical (A-USC) steam conditions. A limiting factor in this can be the materials of construction for boilers and for steam turbines. The overall project goal is to assess/develop materials technology that will enable achieving turbine throttle steam conditions of 760°C (1400°F)/35MPa (5000 psi). This final technical report covers the research completed by the General Electric Company (GE) and Electric Power Research Institute (EPRI), with support from Oak Ridge National Laboratory (ORNL) and the National Energy Technology Laboratory (NETL) – Albany Research Center, to develop the A-USC steam turbine materials technology to meet the overall project goals. Specifically, this report summarizes the industrial scale-up and materials property database development for non-welded rotors (disc forgings), buckets (blades), bolting, castings (needed for casing and valve bodies), casting weld repair, and casting to pipe welding. Additionally, the report provides an engineering and economic assessment of an A-USC power plant without and with partial carbon capture and storage. This research project successfully demonstrated the materials technology at a sufficient scale and with corresponding materials property data to enable the design of an A-USC steam turbine. The key accomplishments included the development of a triple-melt and forged Haynes 282 disc for bolted rotor construction, long-term property development for Nimonic 105 for blading and bolting, successful scale-up of Haynes 282 and Nimonic 263 castings using

  13. Determination of service relevant materials data on specimens from gas turbine blades. Final report; Ermittlung betriebsrelevanter Werkstoffkennwerte an Proben aus GT-Schaufeln. Schlussbericht

    Energy Technology Data Exchange (ETDEWEB)

    Pickert, U.

    1994-01-01

    This joint program `Manufacturing of large GT-blades` ran in the frame of the project `AG-TURBO, High Temperature Gas Turbine` and dealt with the highly dynamicly stressed blades of the last rows of stationary gas turbines. The aim of this joint program was to improve properties of common Ni-base superalloys for forged and cast blades and to establish a design database. During the program a great progress was made regarding large forged blades from Nimonic 101 and Udimet 720 due to optimizing the manufacturing and heat treatment process. One has succeed in forgeing large blades with very low residual stresses and suitable mechanical properties. The obtained knowledge was immediately transfered to serial production. In case of fine grain precision cast blades from IN 792 not all problems could be solved. So no success was made to improve significantly the dynamic fatigue strength of mechanically grain refined (MKF) blades comparing to conventionally cast ones. The same is worth for the metallurgical grain refined (CCF) blades. The very good fatigue strength results from test slabs could not be transfered to blades. So there is a remaining open question how to get reproducible good fatigue properties in fine grain cast blades. However the basis of material knowledge for cast alloys could be exceeded a lot during the course of this program. (orig.) [Deutsch] Ziel dieses Vorhabens war in Zusammenarbeit mit den Projektpartnern die Erarbeitung von Methoden zur Herstellung optimierter Schaufeln aus Ni-Basis Schmiede- und Feingusslegierungen fuer die Endstufen grosser Industriegasturbinen und die Erstellung einer Beurteilungsmatrix bezueglich deren betriebrelevanten mechanischen Eigenschaften. Hierdurch sollte die Auslegungssicherheit und Betriebszuverlaessigkeit erheblich gesteigert werden, um verlaessliche Gasturbinen fuer den Kombiprozess mit Dampfturbinen bauen zu koennen. So ist es im Rahmen dieses Verbundprojektes gelungen, durch Optimierung des Schmiede- und

  14. The effect of variations of cobalt content on the cyclic oxidation resistance of selected Ni-base superalloys

    Science.gov (United States)

    Barrett, Charles A.

    1987-01-01

    Cobalt levels were systematically varied in the Ni-base turbine alloys U-700 (cast), U-700m (PM/HIP), Waspaloy, Mar-M-247, In-738, Nimonic-115, U-720, and SX-R-150. the cobalt levels ranged from 0 wt pct to the nominal commercial content in each alloy. the alloys were tested in cyclic oxidation in static air at 1000, 1100 and 1150 C for 500, 200, and 100 hr, respectively. An oxidation attack parameter, Ka, derived from the specific weight change versus time data was used to evaluate the oxidation behavior of the alloys along with X-ray diffraction analysis of the surface oxides. The alloys tend to form either Cr2O3/chromite spinel or Al2O3/aluminate spinel depending on the Cr/Al ratio in the alloys. Alloys with a ratio of 3.5 or higher tend to favor the Cr oxides while those under 3.0 form mostly Al oxides. In general the Al2O3/aluminate spinel forming alloys have the better oxidation resistance. Increased cobalt content lowers the scaling resistance of the higher Cr allys while a 5.0 wt pct Co content is optimum for the Al controlling alloys. The refractory metals, particularly Ta, appear beneficial to both types of oxides, perhaps due to the formation of the omnipresent trirutile Ni(Ta, Cb, Mo, W)2O6. Both scales break down as increasing amounts of NiO are formed.

  15. Mechanical properties and microstructure changes after long-term aging at 700℃ for a nickel-base superalloy

    Institute of Scientific and Technical Information of China (English)

    Shuangqun Zhao; Jianxin Dong; Xishan Xie

    2003-01-01

    Mechanical properties and microstructure changes have been investigated on a new nickel-base superalloy after long-term aging at 700℃. It is found that the major precipitates of the tested alloy are MC, M23C6, M6C and γ' in the course of long-term aging at 700℃. The carbides maintain good thermal stability with the aging time up to 5008 h. The growth rate of gamma prime precipitates is relatively high in the early aging period and then slows down. The coarsening behavior of gamma prime follows a diffusion-controlled growth procedure. The room temperature Rockwell hardness of the alloy aged at 700℃ increases slightly at the initial stage of aging, but it decreases with the prolonged time. It mainly depends on the size of gamma prime. In comparison with Nimonic lloy 263, the new alloy characterizes with higher tensile and stress-rupture strengths at high temperatures. The new nickel-base superalloy offers a combination of microstructure stability, strength, ductility and toughness at 700℃.

  16. Monte Carlo simulations of the NIMROD diffractometer

    Energy Technology Data Exchange (ETDEWEB)

    Botti, A. [University of Roma TRE, Rome (Italy)]. E-mail: botti@fis.uniroma3.it; Ricci, M.A. [University of Roma TRE, Rome (Italy); Bowron, D.T. [ISIS-Rutherford Appleton Laboratory, Chilton (United Kingdom); Soper, A.K. [ISIS-Rutherford Appleton Laboratory, Chilton (United Kingdom)

    2006-11-15

    The near and intermediate range order diffractometer (NIMROD) has been selected as a day one instrument on the second target station at ISIS. Uniquely, NIMROD will provide continuous access to particle separations ranging from the interatomic (<1A) to the mesoscopic (<300A). This instrument is mainly designed for structural investigations, although the possibility of putting a Fermi chopper (and corresponding NIMONIC chopper) in the incident beam line, will potentially allow the performance of low resolution inelastic scattering measurements. The performance characteristics of the TOF diffractometer have been simulated by means of a series of Monte Carlo calculations. In particular, the flux as a function of the transferred momentum Q as well as the resolution in Q and transferred energy have been estimated. Moreover, the possibility of including a honeycomb collimator in order to achieve better resolution has been tested. Here, we want to present the design of this diffractometer that will bridge the gap between wide- and small-angle neutron scattering experiments.

  17. Dissolution of ordered precipitates under ion irradiation

    Energy Technology Data Exchange (ETDEWEB)

    Camus, E.; Bourdeau, F.; Abromeit, C.; Wanderka, N.; Wollenberger, H. [Hahn-Meitner-Institut Berlin GmbH (Germany)

    1995-09-01

    The stability of the ordered {gamma}{prime} precipitates under 300-keV Ni{sup +} irradiation was investigated between room temperature and 623 K. The two competing mechanisms of destabilization by cascade producing irradiation, i.e. disordering and dissolution of the {gamma}{prime} precipitates in Nimonic PE16 alloy, has been studied separately by electron microscopy and field-ion microscopy with atom probe. At high temperatures, the precipitates are stable. At intermediate temperatures, the precipitates dissolve by ballistic mixing into the matrix, but the interface is restored by the radiation-enhanced atomic jumps. The order in the precipitates remains stable. At low temperatures, the precipitates are dissolved by atomic mixing. The dissolution proceeds in a diffusional manner with a diffusion coefficient normalized by the displacement rate D/K = 0.75 nm{sup 2}dpa{sup {minus}1}. The precipitates become disordered by a fluence of 0.1 dpa, whereas precipitate dissolution needs much higher fluences.

  18. Tensile and Creep Property Characterization of Potential Brayton Cycle Impeller and Duct Materials

    Science.gov (United States)

    Gabb, Timothy P.; Gayda, John

    2006-01-01

    This paper represents a status report documenting the work on creep of superalloys performed under Project Prometheus. Cast superalloys have potential applications in space as impellers within closed-loop Brayton cycle nuclear power generation systems. Likewise wrought superalloys are good candidates for ducts and heat exchangers transporting the inert working gas in a Brayton-based power plant. Two cast superalloys, Mar-M247LC and IN792, and a NASA GRC powder metallurgy superalloy, LSHR, are being screened to compare their respective capabilities for impeller applications. Several wrought superalloys including Hastelloy X, (Haynes International, Inc., Kokomo, IN), Inconel 617, Inconel 740, Nimonic 263, and Incoloy MA956 (Special Metals Corporation, Huntington, WV) are also being screened to compare their capabilities for duct applications. These proposed applications would require sufficient strength and creep resistance for long term service at temperatures up to 1200 K, with service times to 100,000 h or more. Conventional tensile and creep tests were performed at temperatures up to 1200 K on specimens extracted from the materials. Initial microstructure evaluations were also undertaken.

  19. Creep Property Characterization of Potential Brayton Cycle Impeller and Duct Materials

    Science.gov (United States)

    Gabb, Timothy P.; Gayda, john; Garg, Anita

    2007-01-01

    Cast superalloys have potential applications in space as impellers within closed-loop Brayton cycle nuclear power generation systems. Likewise wrought superalloys are good candidates for ducts and heat exchangers transporting the inert working gas in a Brayton-based power plant. Two cast superalloys, Mar-M247LC and IN792, and a NASA GRC powder metallurgy superalloy, LSHR, have been screened to compare their respective capabilities for impeller applications. Mar-M247LC has been selected for additional long term evaluations. Initial tests in helium indicate this inert environment may debit long term creep resistance of this alloy. Several wrought superalloys including Hastelloy(Registered TradeMark) X, Inconel(Registered TradeMark) 617, Inconel(Registered TradeMark) 740, Nimonic(Registered TradeMark) 263, Incoloy(Registered TradeMark) MA956, and Haynes 230 are also being screened to compare their capabilities for duct applications. Haynes 230 has been selected for additional long term evaluations. Initial tests in helium are just underway for this alloy. These proposed applications would require sufficient strength and creep resistance for long term service at temperatures up to 1200 K, with service times to 100,000 h or more. Therefore, long term microstructural stability is also being screened.

  20. Static Structural and Modal Analysis of Gas Turbine Blade

    Science.gov (United States)

    Ranjan Kumar, Ravi; Pandey, K. M., Prof.

    2017-08-01

    Gas turbine is one of the most versatile items of turbo machinery nowadays. It is used in different modes such as power generation, oil and gas, process plants, aviation, domestic and related small industries. This paper is based on the problems concerning blade profile selection, material selection and turbine rotor blade vibration that seriously impact the induced stress-deformation and structural functioning of developmental gas turbine engine. In this paper for generating specific power by rotating blade at specific RPM, blade profile and material has been decided by static structural analysis. Gas turbine rotating blade RPM is decided by Modal Analysis so that the natural frequency of blade should not match with the excitation frequency. For the above blade profile has been modeled in SOLIDWORKS and analysis has been done in ANSYS WORKBENCH 14. Existing NACA6409 profile has been selected as base model and then it is modified by bending it through 72.5° and 145°. Hence these three different blade profiles have been analyzed for three different materials viz. Super Alloy X, Nimonic 80A and Inconel 625 at three different speed viz. 20000, 40000 and 60000RPM. It is found that NACA6409 with 72.5° bent gives best result for all material at all speed. Among all the material Inconel 625 gives best result. Hence Blade of Inconel 625 having 72.5° bent profile is the best combination for all RPM.

  1. 棘轮-蠕变交互作用下汽轮机汽缸紧固螺栓失效研究

    Institute of Scientific and Technical Information of China (English)

    张淼; 袁新勇

    2013-01-01

    机组负荷变动和调峰过程中,汽缸的紧固螺栓在非零平均应力的交变载荷作用下会产生棘轮-蠕变行为,因此,对螺栓在棘轮-蠕变过程中损伤的发展进行研究具有重要意义。对镍基合金Nimonic 80A材料进行了550℃下单轴棘轮-蠕变试验,并在有限元软件Ansys中嵌入基于AbdelKarim-Ohno运动硬化准则的用户自定义程序,模拟了螺栓的棘轮-蠕变过程。模拟得到的宏观变形量与试验结果一致,在棘轮-蠕变交互作用下,螺栓螺杆处的损伤发展速度大于应力集中的螺纹处,并在此发生断裂。

  2. 2015欧洲粉末冶金大会的金属增材制造:高温合金、粉末雾化、喷墨和激光金属沉积工艺的进展%Metal AM at Euro PM2015:superalloys,powder atomization and advances in inkjet and LMD processes

    Institute of Scientific and Technical Information of China (English)

    David Whittaker

    2016-01-01

    In the part two of report on technical advances in metal AM at the Euro PM2015 congress,Reims, France,October 4-7 2015,Dr David Whittaker reported on six further papers presented at the conference very well attended metal AM sessions. These papers cover the heat treatment of IN939 superalloy parts,the production of Ni718 superalloy powder,advances in inkjet-based metal AM and the production of gears by laser metal deposi-tion (LMD).%2015欧洲粉末冶金会议于2015年10月4—7日在法国兰斯(Reims)举行。本届大会报告的第二部分是关于金属增材制造的进展,David博士就会议中有关金属增材制造的6篇论文作了报告。这些论文涵盖了IN939高温合金制件的热处理、Ni718高温合金粉末的生产、喷墨金属增材制造和激光金属沉积(LMD)生产齿轮的进展。

  3. Thermo-mechanical fatigue behaviour of the near-{gamma}-titanium aluminide alloy TNB-V5 under uniaxial and multiaxial loading

    Energy Technology Data Exchange (ETDEWEB)

    Brookes, Stephen Peter

    2009-12-19

    -strain history. The effects of TMF on the microstructure were also investigated. For all types of tests intergranular fracture is predominant. Failure is strongly influenced by environmental conditions. This study compares TMF results of TiAl with previous TMF investigations on the nickel-based alloys IN 738 and Nimonic 90. IN 738 shows similar TMF behaviour to {gamma}-TiAl in that uniaxial IP loading has the longest fatigue lifetimes. Nimonic 90 shows the opposite behaviour to both of these alloys. A lifetime model developed for this near-{gamma}-TiAl alloy, successfully describes all temperaturestrain TMF loading conditions over the test temperature range, with the use of a single loading parameter. The loading parameter is based on the plastic work per cycle, and is not only dependant on the mean tensile stress but also on the maximum principal stress. The loading parameter responds to various strain-temperature-paths differently. It describes the lifetime relation between uniaxial IP and OP loading, axial and torsional loading and the hold period effect. (orig.)

  4. Processing of Advanced Cast Alloys for A-USC Steam Turbine Applications

    Science.gov (United States)

    Jablonski, Paul D.; Hawk, Jeffery A.; Cowen, Christopher J.; Maziasz, Philip J.

    2012-02-01

    The high-temperature components within conventional supercritical coal-fired power plants are manufactured from ferritic/martensitic steels. To reduce greenhouse-gas emissions, the efficiency of pulverized coal steam power plants must be increased to as high a temperature and pressure as feasible. The proposed steam temperature in the DOE/NETL Advanced Ultra Supercritical power plant is high enough (760°C) that ferritic/martensitic steels will not work for the majority of high-temperature components in the turbine or for pipes and tubes in the boiler due to temperature limitations of this class of materials. Thus, Ni-based superalloys are being considered for many of these components. Off-the-shelf forged nickel alloys have shown good promise at these temperatures, but further improvements can be made through experimentation within the nominal chemistry range as well as through thermomechanical processing and subsequent heat treatment. However, cast nickel-based superalloys, which possess high strength, creep resistance, and weldability, are typically not available, particularly those with good ductility and toughness that are weldable in thick sections. To address those issues related to thick casting for turbine casings, for example, cast analogs of selected wrought nickel-based superalloys such as alloy 263, Haynes 282, and Nimonic 105 have been produced. Alloy design criteria, melt processing experiences, and heat treatment are discussed with respect to the as-processed and heat-treated microstructures and selected mechanical properties. The discussion concludes with the prospects for full-scale development of a thick section casting for a steam turbine valve chest or rotor casing.

  5. Materials Performance in USC Steam Portland

    Energy Technology Data Exchange (ETDEWEB)

    G.R. Holcomb; J. Tylczak; R. Hu

    2011-04-26

    Goals of the U.S. Department of Energy's Advanced Power Systems Initiatives include power generation from coal at 60% efficiency, which requires steam conditions of up to 760 C and 340 atm, co-called advanced ultrasupercritical (A-USC) steam conditions. A limitation to achieving the goal is a lack of cost-effective metallic materials that can perform at these temperatures and pressures. Some of the more important performance limitations are high-temperature creep strength, fire-side corrosion resistance, and steam-side oxidation resistance. Nickel-base superalloys are expected to be the materials best suited for steam boiler and turbine applications above about 675 C. Specific alloys of interest include Haynes 230 and 282, Inconel 617, 625 and 740, and Nimonic 263. Further validation of a previously developed chromia evaporation model is shown by examining the reactive evaporation effects resulting from exposure of Haynes 230 and Haynes 282 to moist air environments as a function of flow rate and water content. These two alloys differ in Ti and Mn contents, which may form outer layers of TiO{sub 2} or Cr-Mn spinels. This would in theory decrease the evaporation of Cr{sub 2}O{sub 3} from the scale by decreasing the activity of chromia at the scale surface, and be somewhat self-correcting as chromia evaporation concentrates the Ti and Mn phases. The apparent approximate chromia activity was found for each condition and alloy that showed chromia evaporation kinetics. As expected, it was found that increasing the gas flow rate led to increased chromia evaporation and decreased chromia activity. However, increasing the water content in moist air increased the evaporation, but results were mixed with its effect on chromia activity.

  6. Small-scale mechanical characterization of viscoelastic adhesive systems

    Science.gov (United States)

    Shean, T. A. V.

    Aero engine hot end components are often covered with ceramic Thermal Barrier Coatings (TBCs). Laser drilling in the TBC coated components can be a source of service life TBC degradation and spallation. The present study aims to understand the mechanisms of TBC delamination and develop techniques to drill holes without damaging the TBC, Nimonic 263 workpieces coated with TBC are used in the experiments. Microwave non-destructive testing (NDT) is employed to monitor the integrity of the coating /substrate interfaces of the post-laser drilled materials. A numerical modelling technique is used to investigate the role of melt ejection on TBC delamination. The model accounts for the vapour and the assist gas flow effects in the process. Broadly, melt ejection induced mechanical stresses for the TBC coating / bond coating and thermal effects for the bond coating / substrate interfaces are found the key delamination mechanisms. Experiments are carried out to validate the findings from the model. Various techniques that enable laser drilling without damaging the TBC are demonstrated. Twin jet assisted acute angle laser drilling is one successful technique that has been analysed using the melt ejection simulation. Optimisation of the twin jet assisted acute angle laser drilling process parameters is carried out using Design of Experiments (DoE) and statistical modelling approaches. Finally, an industrial case study to develop a high speed, high quality laser drilling system for combustor cans is described. Holes are drilled by percussion and trepan drilling in TBC coated and uncoated Haynes 230 workpieces. The production rate of percussion drilling is significantly higher than the trepan drilling, however metallurgical hole quality and reproducibility is poor. A number of process parameters are investigated to improve these characteristics. Gas type and gas pressure effects on various characteristics of the inclined laser drilled holes are investigated through theoretical

  7. Laser drilling of thermal barrier coated jet-engine components

    Science.gov (United States)

    Sezer, H. K.

    Aero engine hot end components are often covered with ceramic Thermal Barrier Coatings (TBCs). Laser drilling in the TBC coated components can be a source of service life TBC degradation and spallation. The present study aims to understand the mechanisms of TBC delamination and develop techniques to drill holes without damaging the TBC, Nimonic 263 workpieces coated with TBC are used in the experiments. Microwave non-destructive testing (NDT) is employed to monitor the integrity of the coating /substrate interfaces of the post-laser drilled materials. A numerical modelling technique is used to investigate the role of melt ejection on TBC delamination. The model accounts for the vapour and the assist gas flow effects in the process. Broadly, melt ejection induced mechanical stresses for the TBC coating / bond coating and thermal effects for the bond coating / substrate interfaces are found the key delamination mechanisms. Experiments are carried out to validate the findings from the model. Various techniques that enable laser drilling without damaging the TBC are demonstrated. Twin jet assisted acute angle laser drilling is one successful technique that has been analysed using the melt ejection simulation. Optimisation of the twin jet assisted acute angle laser drilling process parameters is carried out using Design of Experiments (DoE) and statistical modelling approaches. Finally, an industrial case study to develop a high speed, high quality laser drilling system for combustor cans is described. Holes are drilled by percussion and trepan drilling in TBC coated and uncoated Haynes 230 workpieces. The production rate of percussion drilling is significantly higher than the trepan drilling, however metallurgical hole quality and reproducibility is poor. A number of process parameters are investigated to improve these characteristics. Gas type and gas pressure effects on various characteristics of the inclined laser drilled holes are investigated through theoretical

  8. Materials for Advanced Ultrasupercritical Steam Turbines Task 4: Cast Superalloy Development

    Energy Technology Data Exchange (ETDEWEB)

    Thangirala, Mani

    2015-09-30

    The Steam Turbine critical stationary structural components are high integrity Large Shell and Valve Casing heavy section Castings, containing high temperature steam under high pressures. Hence to support the development of advanced materials technology for use in an AUSC steam turbine capable of operating with steam conditions of 760°C (1400°F) and 35 Mpa (5000 psia), Casting alloy selection and evaluation of mechanical, metallurgical properties and castability with robust manufacturing methods are mandated. Alloy down select from Phase 1 based on producability criteria and creep rupture properties tested by NETL-Albany and ORNL directed the consortium to investigate cast properties of Haynes 282 and Haynes 263. The goals of Task 4 in Phase 2 are to understand a broader range of mechanical properties, the impact of manufacturing variables on those properties. Scale up the size of heats to production levels to facilitate the understanding of the impact of heat and component weight, on metallurgical and mechanical behavior. GE Power & Water Materials and Processes Engineering for the Phase 2, Task 4.0 Castings work, systematically designed and executed casting material property evaluation, multiple test programs. Starting from 15 lbs. cylinder castings to world’s first 17,000 lbs. poured weight, heavy section large steam turbine partial valve Haynes 282 super alloy casting. This has demonstrated scalability of the material for steam Turbine applications. Activities under Task 4.0, Investigated and characterized various mechanical properties of Cast Haynes 282 and Cast Nimonic 263. The development stages involved were: 1) Small Cast Evaluation: 4 inch diam. Haynes 282 and Nimonic 263 Cylinders. This provided effects of liquidus super heat range and first baseline mechanical data on cast versions of conventional vacuum re-melted and forged Ni based super alloys. 2) Step block castings of 300 lbs. and 600 lbs. Haynes 282 from 2 foundry heats were evaluated which

  9. Corrosion-resistant nickel-base alloys for gas turbines

    Energy Technology Data Exchange (ETDEWEB)

    Schultz, J.W.; Hulsizer, W.R.

    1976-08-01

    Laboratory corrosion screening procedures used during the past ten years in developing nickel-base superalloys for gas turbine applications are described. Hot salt corrosion tests have included crucible and salt shower exposures. Reproducible techniques were established and alloy composition effects defined, leading to development of M313, IN-587, a IN-792. Correlations have been made with corrosion results in burner rigs, and engine experience confirming anticipated behavior is now becoming available. During this work a number of limitations of these accelerated laboratory tests were uncovered; these are discussed. Finally, brief descriptions of the states of development of alloy MA 755E (an oxide dispersion-strengthened superalloy) and IN-939 (a cast 23 percent chromium superalloy) are outlined as examples of advanced corrosion resistant, high strength materials of the future.

  10. Phase Transformations in Cast Duplex Stainless Steels

    Energy Technology Data Exchange (ETDEWEB)

    Kim, Yoon-Jun [Iowa State Univ., Ames, IA (United States)

    2004-01-01

    Duplex stainless steels (DSS) constitute both ferrite and austenite as a matrix. Such a microstructure confers a high corrosion resistance with favorable mechanical properties. However, intermetallic phases such as σ and χ can also form during casting or high-temperature processing and can degrade the properties of the DSS. This research was initiated to develop time-temperature-transformation (TTT) and continuous-cooling-transformation (CCT) diagrams of two types of cast duplex stainless steels, CD3MN (Fe-22Cr-5Ni-Mo-N) and CD3MWCuN (Fe-25Cr-7Ni-Mo-W-Cu-N), in order to understand the time and temperature ranges for intermetallic phase formation. The alloys were heat treated isothermally or under controlled cooling conditions and then characterized using conventional metallographic methods that included tint etching, and also using electron microscopy (SEM, TEM) and wavelength dispersive spectroscopy (WDS). The kinetics of intermetallic-phase (σ + χ) formation were analyzed using the Johnson-Mehl-Avrami (MA) equation in the case of isothermal transformations and a modified form of this equation in the case of continuous cooling transformations. The rate of intermetallic-phase formation was found to be much faster in CD3MWCuN than CD3MN due mainly to differences in the major alloying contents such as Cr, Ni and Mo. To examine in more detail the effects of these elements of the phase stabilities; a series of eight steel castings was designed with the Cr, Ni and Mo contents systematically varied with respect to the nominal composition of CD3MN. The effects of varying the contents of alloying additions on the formation of intermetallic phases were also studied computationally using the commercial thermodynamic software package, Thermo-Calc. In general, σ was stabilized with increasing Cr addition and χ by increasing Mo addition. However, a delicate balance among Ni and other minor elements such as N and Si also exists. Phase equilibria in DSS can be affected by

  11. Clean cast steel technology. Determination of transformation diagrams for duplex stainless steel

    Energy Technology Data Exchange (ETDEWEB)

    Chumbley, S. L. [Iowa State Univ., Ames, IA (United States)

    2005-09-01

    Duplex stainless steels (DSS) constitute both ferrite and austenite as a matrix. Such a microstructure confers a high corrosion resistance with favorable mechanical properties. However, intermetallic phases such as sigma ( can also form during casting or high-temperature processing and can degrade the properties of the DSS. This research was initiated to develop time-temperature-transformation (TTT) and continuous-cooling- transformation (CCT) diagrams of two types of cast duplex stainless steels, CD3MN (Fe 22Cr-5Ni-Mo-N) and CD3MWCuN (Fe-25Cr-7Ni-Mo-W-Cu-N), in order to understand the time and temperature ranges for intermetallic phase formation. The alloys were heat treated isothermally or under controlled cooling conditions and then characterized using conventional metallographic methods that included tint etching, and also using electron microscopy (SEM, TEM) and wavelength dispersive spectroscopy (WDS). The kinetics of intermetallic-phase ( formation were analyzed using the Johnson-Mehl-Avrami (JMA) equation in the case of isothermal transformations and a modified form of this equation in the case of continuous cooling transformations, The rate of intermetallic-phase formation was found to be much faster in CD3MWCuN than CD3MN due mainly to differences in the major alloying contents such as Cr, Ni and Mo. To examine in more detail the effects of these elements of the phase stabilities, a series of eight steel castings was designed with the Cr, Ni and Mo contents systematically varied with respect to the nominal composition of CD3MN. The effects of varying the contents of alloying additions on the formation of intermetallic phases were also studied computationally using the commercial thermodynamic software package, Thermo-Calc. In general, was stabilized with increasing Cr addition and by increasing Mo addition. However, a delicate balance among Ni and other minor elements such as N and Si also exists. Phase equilibria in DSS can be affected by local

  12. Prediction of forming limit strains of thin foils using shim

    Science.gov (United States)

    Joshi, Sanket Vivek; Bade, Rohit A.; Narasimhan, K.

    2013-12-01

    Thin foils of metallic alloys find utility in metallic thermal protection systems, such as honeycomb structures. Understanding the formability of these thin foils becomes imperative so as to design accurate tooling and also to ensure mechanical robustness of the honeycomb structures during service. It has been found that, obtaining the precise limit strains of these foils directly using the conventional limiting dome test tooling is difficult, because of the excessive draw in and wrinkling that occurs during the punch travel, resulting in erroneous measurement or prediction of limit strains. To address this issue, the blank over blank stacking methodology was developed, which helped keep the draw-in and wrinkling at negligible and thus acceptable levels. Although the blank over blank stacking methodology offers a way to predict and measure limit strains, the same may not be accurate enough due to the effect the substrate properties may impose on the thin foil. To avoid this effect, a different methodology has been proposed herein, which uses a shim stacked over the blank to avoid draw in of these foil blanks and thus help accurate clamping of the blank between the die and blank holder. It is thus understood that either a critical local or global increase in the thickness of the blank material in and around the draw bead is essential to obtain effective clamping of foil and to avoid draw-in and wrinkling. Although, miniaturized hemispherical dome tests may be beneficial for obtaining limit strains as far as foils are concerned, the methodologies proposed herein provide a route to obtaining the same using available equipment, thus saving resources and time involved in development of new miniaturized testing devices. The forming limit strains of thin foils of IN 718 (inconel) alloy having a thickness of 50μm, C263 (nimonic) alloy having a thickness of 100μm and CP Ti (commercially pure titanium) having a thickness of 200μm have been predicted using this methodology

  13. Phase Transformations in Cast Duplex Stainless Steels

    Energy Technology Data Exchange (ETDEWEB)

    Yoon-Jun Kim

    2004-12-19

    Duplex stainless steels (DSS) constitute both ferrite and austenite as a matrix. Such a microstructure confers a high corrosion resistance with favorable mechanical properties. However, intermetallic phases such as {sigma} and {chi} can also form during casting or high-temperature processing and can degrade the properties of the DSS. This research was initiated to develop time-temperature-transformation (TTT) and continuous-cooling-transformation (CCT) diagrams of two types of cast duplex stainless steels, CD3MN (Fe-22Cr-5Ni-Mo-N) and CD3MWCuN (Fe-25Cr-7Ni-Mo-W-Cu-N), in order to understand the time and temperature ranges for intermetallic phase formation. The alloys were heat treated isothermally or under controlled cooling conditions and then characterized using conventional metallographic methods that included tint etching, and also using electron microscopy (SEM, TEM) and wavelength dispersive spectroscopy (WDS). The kinetics of intermetallic-phase ({sigma} + {chi}) formation were analyzed using the Johnson-Mehl-Avrami (MA) equation in the case of isothermal transformations and a modified form of this equation in the case of continuous cooling transformations. The rate of intermetallic-phase formation was found to be much faster in CD3MWCuN than CD3MN due mainly to differences in the major alloying contents such as Cr, Ni and Mo. To examine in more detail the effects of these elements of the phase stabilities; a series of eight steel castings was designed with the Cr, Ni and Mo contents systematically varied with respect to the nominal composition of CD3MN. The effects of varying the contents of alloying additions on the formation of intermetallic phases were also studied computationally using the commercial thermodynamic software package, Thermo-Calc. In general, {sigma} was stabilized with increasing Cr addition and {chi} by increasing Mo addition. However, a delicate balance among Ni and other minor elements such as N and Si also exists. Phase equilibria in

  14. Systemic inflammation and cerebral palsy risk in extremely preterm infants.

    Science.gov (United States)

    Kuban, Karl C K; O'Shea, T Michael; Allred, Elizabeth N; Paneth, Nigel; Hirtz, Deborah; Fichorova, Raina N; Leviton, Alan

    2014-12-01

    The authors hypothesized that among extremely preterm infants, elevated concentrations of inflammation-related proteins in neonatal blood are associated with cerebral palsy at 24 months. In 939 infants born before 28 weeks gestation, the authors measured blood concentrations of 25 proteins on postnatal days 1, 7, and 14 and evaluated associations between elevated protein concentrations and cerebral palsy diagnosis. Protein elevations within 3 days of birth were not associated with cerebral palsy. Elevations of tumor necrosis factor-α, tumor necrosis factor-α-receptor-1, interleukin-8, and intercellular adhesion molecule-1 on at least 2 days were associated with diparesis. Recurrent-persistent elevations of interleukin-6, E-selectin, or insulin-like growth factor binding protein-1 were associated with hemiparesis. Diparesis and hemiparesis were more likely among infants who had at least 4 of 9 protein elevations that previously have been associated with cognitive impairment and microcephaly. Repeated elevations of inflammation-related proteins during the first 2 postnatal weeks are associated with increased risk of cerebral palsy.

  15. Simulation of Ni-Based Super-Alloy and Optimizing of Its Mechanical Properties in a Near-Shaped Turbine Blade Part

    Directory of Open Access Journals (Sweden)

    Mohammd Reza Alizadeh

    2015-01-01

    Full Text Available This paper presents simulation of a Ni-based super-alloy during filling of a near-shaped turbine blade part to optimize its mechanical properties. Since geometrical shape of the airfoil is so complicated, a simple near-shaped part was made by plexiglass to water modeling. Condition and parameters of water modeling were obtained from the Procast software simulation. The flow pattern of the transparent systems, recorded by a high speed video camera, was analyzed. Air bubble amounts were quantitatively measured by an image analysis software. Quantified results were used to compare two systems in terms of ability to prevent bubble formation and entrainment. Both water modeling and computer simulating methods indicated that highest turbulences in bottom- and top-poured systems form in first initially pouring times. According to the water modeling results amount of bubble values was 40 and 18 percent for top-poured and bottom-poured systems, respectively. Then the Ni-base super-alloy IN939 is poured by investment casting in bottom- and top-poured systems and compared with each other. The results stated that bottom-poured system had higher mechanical properties compared to top-poured one. Ultimate tensile strength for the former was 820 MPa while for the part which was cast by bottom-poured system it was 850 MPa.

  16. Microstructural response to heat affected zone cracking of prewelding heat-treated Inconel 939 superalloy

    Energy Technology Data Exchange (ETDEWEB)

    Gonzalez, M.A., E-mail: mgonzalez@comimsa.com.mx [Facultad de Ingenieria Mecanica y Electrica (FIME-UANL), Av. Universidad s/n. Ciudad Universitaria, C.P.66451 San Nicolas de los Garza, N.L. (Mexico); Martinez, D.I., E-mail: dorairma@yahoo.com [Facultad de Ingenieria Mecanica y Electrica (FIME-UANL), Av. Universidad s/n. Ciudad Universitaria, C.P.66451 San Nicolas de los Garza, N.L. (Mexico); Perez, A., E-mail: betinperez@hotmail.com [Facultad de Ingenieria Mecanica y Electrica (FIME-UANL), Av. Universidad s/n. Ciudad Universitaria, C.P.66451 San Nicolas de los Garza, N.L. (Mexico); Guajardo, H., E-mail: hguajardo@frisa.com [FRISA Aerospace, S.A. de C.V., Valentin G. Rivero No. 200, Col. Los Trevino, C.P. 66150, Santa Caterina N.L. (Mexico); Garza, A., E-mail: agarza@comimsa.com [Corporacion Mexicana de Investigacion en Materiales S.A. de C.V. (COMIMSA), Ciencia y Tecnologia No.790, Saltillo 400, C.P. 25295 Saltillo Coah. (Mexico)

    2011-12-15

    The microstructural response to cracking in the heat-affected zone (HAZ) of a nickel-based IN 939 superalloy after prewelding heat treatments (PWHT) was investigated. The PWHT specimens showed two different microstructures: 1) spherical ordered {gamma} Prime precipitates (357-442 nm), with blocky MC and discreet M{sub 23}C{sub 6} carbides dispersed within the coarse dendrites and in the interdendritic regions; and 2) ordered {gamma} Prime precipitates in 'ogdoadically' diced cube shapes and coarse MC carbides within the dendrites and in the interdendritic regions. After being tungsten inert gas welded (TIG) applying low heat input, welding speed and using a more ductile filler alloy, specimens with microstructures consisting of spherical {gamma} Prime precipitate particles and dispersed discreet MC carbides along the grain boundaries, displayed a considerably improved weldability due to a strong reduction of the intergranular HAZ cracking associated with the liquation microfissuring phenomena. - Highlights: Black-Right-Pointing-Pointer Homogeneous microstructures of {gamma} Prime spheroids and discreet MC carbides of Ni base superalloys through preweld heat treatments. Black-Right-Pointing-Pointer {gamma} Prime spheroids and discreet MC carbides reduce the intergranular HAZ liquation and microfissuring of Nickel base superalloys. Black-Right-Pointing-Pointer Microstructure {gamma} Prime spheroids and discreet blocky type MC carbides, capable to relax the stress generated during weld cooling. Black-Right-Pointing-Pointer Low welding heat input welding speeds and ductile filler alloys reduce the HAZ cracking susceptibility.

  17. Experimental Design for Evaluation of Co-extruded Refractory Metal/Nickel Base Superalloy Joints

    Energy Technology Data Exchange (ETDEWEB)

    ME Petrichek

    2005-12-16

    Prior to the restructuring of the Prometheus Program, the NRPCT was tasked with delivering a nuclear space reactor. Potential NRPCT nuclear space reactor designs for the Prometheus Project required dissimilar materials to be in contact with each other while operating at extreme temperatures under irradiation. As a result of the high reactor core temperatures, refractory metals were the primary candidates for many of the reactor structural and cladding components. They included the tantalum-base alloys ASTAR-811C and Ta-10W, the niobium-base alloy FS-85, and the molybdenum base alloys Moly 41-47.5 Rhenium. The refractory metals were to be joined to candidate nickel base alloys such as Haynes 230, Alloy 617, or Nimonic PE 16 either within the core if the nickel-base alloys were ultimately selected to form the outer core barrel, or at a location exterior to the core if the nickel-base alloys were limited to components exterior to the core. To support the need for dissimilar metal joints in the Prometheus Project, a co-extrusion experiment was proposed. There are several potential methods for the formation of dissimilar metal joints, including explosive bonding, friction stir welding, plasma spray, inertia welding, HIP, and co-extrusion. Most of these joining methods are not viable options because they result in the immediate formation of brittle intermetallics. Upon cooling, intermetallics form in the weld fusion zone between the joined metals. Because brittle intermetallics do not form during the initial bonding process associated with HIP, co-extrusion, and explosive bonding, these three joining procedures are preferred for forming dissimilar metal joints. In reference to a Westinghouse Astronuclear Laboratory report done under a NASA sponsored program, joints that were fabricated between similar materials via explosive bonding had strengths that were directly affected by the width of the diffusion barrier. It was determined that the diffusion zone should not exceed

  18. Microstructural Evolution and Creep-Rupture Behavior of Fusion Welds Involving Alloys for Advanced Ultrasupercritical Power Generation

    Science.gov (United States)

    Bechetti, Daniel H., Jr.

    Projections for large increases in the global demand for electric power produced by the burning of fossil fuels, in combination with growing environmental concerns surrounding these fuel sources, have sparked initiatives in the United States, Europe, and Asia aimed at developing a new generation of coal fired power plant, termed Advanced Ultrasupercritical (A-USC). These plants are slated to operate at higher steam temperatures and pressures than current generation plants, and in so doing will offer increased process cycle efficiency and reduced greenhouse gas emissions. Several gamma' precipitation strengthened Ni-based superalloys have been identified as candidates for the hottest sections of these plants, but the microstructural instability and poor creep behavior (compared to wrought products) of fusion welds involving these alloys present significant hurdles to their implementation and a gap in knowledge that must be addressed. In this work, creep testing and in-depth microstructural characterization have been used to provide insight into the long-term performance of these alloys. First, an investigation of the weld metal microstructural evolution as it relates to creep strength reductions in A-USC alloys INCONELRTM 740, NIMONICRTM 263 (INCONEL and NIMONIC are registered trademarks of Special Metals Corporation), and HaynesRTM 282RTM (Haynes and 282 are registered trademarks of Haynes International) was performed. gamma'-precipitate free zones were identified in two of these three alloys, and their development was linked to the evolution of phases that precipitate at the expense of gamma'. Alloy 282 was shown to avoid precipitate free zone formation because the precipitates that form during long term aging in this alloy are poor in the gamma'-forming elements. Next, the microstructural evolution of INCONELRTM 740H (a compositional variant of alloy 740) during creep was investigated. Gleeble-based interrupted creep and creep-rupture testing was used to

  19. Evaluation of Kerosene Fuelled Scramjet Combustor using a Combination of Cooled and Uncooled Struts

    Directory of Open Access Journals (Sweden)

    C. Chandrasekhar

    2014-01-01

    Full Text Available The scramjet combustor a vital component of scramjet engine has been designed by employing fuel injection struts. Several experimental studies have been carried out to evaluate the propulsive performance and structural integrity of the in-stream fuel injection struts in the connect-pipe test facility. As the mission objective of hypersonic demonstrator is to flight test the scramjet engine for 20 s duration, in-stream fuel injection struts which are designed as heat sink devices encounter hostile flow field conditions especially in terms of high thermal and high convective loads in the scramjet combustor. To circumvent these adverse conditions, materials like Niobium C-103 and W-Ni-Fe alloys have been used for the construction of struts and a number of tests have been carried out to evaluate the survivability of the in-stream fuel injection struts in the scramjet combustor. The results thus obtained show that the erosion of leading edges of the Stage-II fuel injection struts in the initial phase and subsequently puncturing of the fuel injection manifold after 10-12 s of the test are noticed, while the other stages of the struts are found to be intact. This deteriorating leading edges of Stage-II struts with respect to time, affect the overall propulsive performance of the combustor. To mitigate this situation, Stage-II struts have been designed as cooled structure and other Stages of struts are designed as un-cooled structure. Material of construction of struts used is Nimonic C-263 alloy. This paper highlights the results of the static test of the scramjet combustor, which has been carried out at a combustor entry Mach number of 2.0, total temperature of 2000 K, with an overall kerosene fuel equivalence ratio of 1.0 and for the supersonic combustion duration of 20 s. Low back pressure has been created at the exit of the scramjet combustor using ejector system to avoid flow separation.Visual inspection of the fuel injection struts after the test

  20. Development and Validation of a Preprocedural Risk Score to Predict Access Site Complications After Peripheral Vascular Interventions Based on the Vascular Quality Initiative Database

    Directory of Open Access Journals (Sweden)

    Daniel Ortiz

    2016-01-01

    Full Text Available Purpose: Access site complications following peripheral vascular intervention (PVI are associated with prolonged hospitalization and increased mortality. Prediction of access site complication risk may optimize PVI care; however, there is no tool designed for this. We aimed to create a clinical scoring tool to stratify patients according to their risk of developing access site complications after PVI. Methods: The Society for Vascular Surgery’s Vascular Quality Initiative database yielded 27,997 patients who had undergone PVI at 131 North American centers. Clinically and statistically significant preprocedural risk factors associated with in-hospital, post-PVI access site complications were included in a multivariate logistic regression model, with access site complications as the outcome variable. A predictive model was developed with a random sample of 19,683 (70% PVI procedures and validated in 8,314 (30%. Results: Access site complications occurred in 939 (3.4% patients. The risk tool predictors are female gender, age > 70 years, white race, bedridden ambulatory status, insulin-treated diabetes mellitus, prior minor amputation, procedural indication of claudication, and nonfemoral arterial access site (model c-statistic = 0.638. Of these predictors, insulin-treated diabetes mellitus and prior minor amputation were protective of access site complications. The discriminatory power of the risk model was confirmed by the validation dataset (c-statistic = 0.6139. Higher risk scores correlated with increased frequency of access site complications: 1.9% for low risk, 3.4% for moderate risk and 5.1% for high risk. Conclusions: The proposed clinical risk score based on eight preprocedural characteristics is a tool to stratify patients at risk for post-PVI access site complications. The risk score may assist physicians in identifying patients at risk for access site complications and selection of patients who may benefit from bleeding avoidance

  1. Bloodstream Amyloid-beta (1-40) Peptide, Cognition, and Outcomes in Heart Failure.

    Science.gov (United States)

    Bayes-Genis, Antoni; Barallat, Jaume; de Antonio, Marta; Domingo, Mar; Zamora, Elisabet; Vila, Joan; Subirana, Isaac; Gastelurrutia, Paloma; Pastor, M Cruz; Januzzi, James L; Lupón, Josep

    2017-03-06

    In the brain, amyloid-beta generation participates in the pathophysiology of cognitive disorders; in the bloodstream, the role of amyloid-beta is uncertain but may be linked to sterile inflammation and senescence. We explored the relationship between blood levels of amyloid-beta 1-40 peptide (Aβ40), cognition, and mortality (all-cause, cardiovascular, and heart failure [HF]-related) in ambulatory patients with HF. Bloodstream Aβ40 was measured in 939 consecutive patients with HF. Cognition was evaluated with the Pfeiffer questionnaire (adjusted for educational level) at baseline and during follow-up. Multivariate Cox regression analyses and measurements of performance (discrimination, calibration, and reclassification) were used, with competing risk for specific causes of death. Over 5.1 ± 2.9 years, 471 patients died (all-cause): 250 from cardiovascular causes and 131 HF-related. The median Aβ40 concentration was 519.1 pg/mL [Q1-Q3: 361.8-749.9 pg/mL]. The Aβ40 concentration correlated with age, body mass index, renal dysfunction, and New York Heart Association functional class (all P < .001). There were no differences in Aβ40 in patients with and without cognitive impairment at baseline (P = .97) or during follow-up (P = .20). In multivariable analysis, including relevant clinical predictors and N-terminal pro-B-type natriuretic peptide, Aβ40 remained significantly associated with all-cause death (HR, 1.22; 95%CI, 1.10-1.35; P < .001) and cardiovascular death (HR, 1.18; 95%CI, 1.03-1.36; P = .02), but not with HF-related death (HR, 1.13; 95%CI, 0.93-1.37; P = .22). Circulating Aβ40 improved calibration and patient reclassification. Blood levels of Aβ40 are not associated with cognitive decline in HF. Circulating Aβ40 was predictive of mortality and may indicate systemic aging. Copyright © 2017 Sociedad Española de Cardiología. Published by Elsevier España, S.L.U. All rights reserved.

  2. Karakterizacija vakuum plazma naprskane kobalt-nikal-hrom-aluminijum-itrijum prevlake

    Directory of Open Access Journals (Sweden)

    Mihailo R. Mrdak

    2013-12-01

    prevlake za ispitivanje mikrotvrdoće i za procenu mikrostrukture u deponovanom stanju su napravljene od čelika Č.4171 (X15Cr13 EN10027 u termički neobrađenom stanju dimenzija 70x20x1,5mm (Turbojet Engine - Standard Practices Manual (PN 582005, 2002, Pratt & Whitney, East Hartford, USA. Uzorci za ispitivanje mikrostrukture prevlake na oksidaciju na 1100°C su napravljeni od legure NIMONIC 80A dimenzija 70x20x1,5mm (Turbojet Engine - Standard Practices Manual (PN 582005, 2002, Pratt & Whitney, East Hartford, USA. Osnove za ispitivanje čvrstoće spoja su takođe napravljene od čelika Č.4171(X15Cr13EN10027 u termički neobrađenom stanju dimenzija Ø25x50 mm (Turbojet Engine - Standard Practices Manual (PN 582005, 2002, Pratt & Whitney, East Hartford, USA. Ispitivanje mikrotvrdoće,čvrstoće spoja i mikrostrukture Procena mehaničkih osobina slojeva je urađena ispitivanjem mikrotvrdoće metodom HV0.3 i čvrstoće spoja ispitivanjem na zatezanje. Merenje mikrotvrdoće je izvršeno u pravcu duž lamela, u sredini i na krajevima uzoraka. Izvršeno je pet očitavanja vrednosti, koje su usrednjene. Metoda ispitivanja čvrstoće spoja je metoda ispitivanja na zatezanje. Ispitivanje je urađeno na sobnoj temperaturi sa brzinom zatezanja 1cm/60s. Za svaku grupu uzoraka su ispitane po tri epruvete. Morfologija čestica praha urađena je metodom SEM. Mikrostruktura slojeva u deponovanom stanju posle nagrizanja je ispitana tehnikom svetlosne mikroskopije. Prevlaka najboljih mehaničkih karakteristika, koja je termički tretirana na oksidaciju na 1100°C u trajanju od 240 sati ispitana je na skening elektronskom mikroskopu (SEM. Nagrizanje prevlake je rađeno elektrolitički sa 10% oksalne kiseline H2C2O4 x2H2O. Depozicija praha Depozicija praha izvršena je na niskom pritisku u vakuumu sa mešavinom plazma-gasova Ar-H2. Vakuum plazma sprej (VPS sistem firme Plasma Technik AG je projektovan za zaštitu vazduhoplovnh delova izloženih kombinaciji prekomerne oksidacije i vrele