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Sample records for icp source experiments

  1. LLNL large-area inductively coupled plasma (ICP) source: Experiments

    International Nuclear Information System (INIS)

    Richardson, R.A.; Egan, P.O.; Benjamin, R.D.

    1995-05-01

    We describe initial experiments with a large (76-cm diameter) plasma source chamber to explore the problems associated with large-area inductively coupled plasma (ICP) sources to produce high density plasmas useful for processing 400-mm semiconductor wafers. Our experiments typically use a 640-nun diameter planar ICP coil driven at 13.56 MHz. Plasma and system data are taken in Ar and N 2 over the pressure range 3-50 mtorr. RF inductive power was run up to 2000W, but typically data were taken over the range 100-1000W. Diagnostics include optical emission spectroscopy, Langmuir probes, and B probes as well as electrical circuit measurements. The B and E-M measurements are compared with models based on commercial E-M codes. Initial indications are that uniform plasmas suitable for 400-mm processing are attainable

  2. ICP experiments more durable pavements

    International Nuclear Information System (INIS)

    Carta Petrolera

    1994-01-01

    A new asphalts technology that will make more durable the pavement in the highways and roads of the cities of Colombia investigates the Colombian Institute of the Petroleum ICP. The project that will have important incidence in the solution of one of the main problems in the roads of cities like Bogota, is only one of the 35 investigation programs and application of new technologies that with relationship to the sector of the hydrocarbons and its influence branches the ICP advances. The investigation looks for to elevate the current average of useful life of the pavements, with that it would be reached a standard that has the developed countries in this field

  3. ICP MS selection of radiopure materials for the GERDA experiment

    Science.gov (United States)

    di Vacri, M. L.; Nisi, S.; Cattadori, C.; Janicsko, J.; Lubashevskiy, A.; Smolnikov, A.; Walter, M.

    2015-08-01

    The GERDA (GERmanium Detector Array) experiment, located in the Gran Sasso Underground Laboratory (LNGS, Italy) aims to search for neutrinoless double beta (0νββ) decay of the 76Ge isotope. Both an ultra-low radioactivity background environment and active techniques to abate the residual background are required to reach the background index (of 10-3 counts/keV kg y) at the Qββ. In order to veto and suppress those events that partially deposit energy in Ge detectors, the readout of liquid argon (LAr) scintillation light (SL) has been implemented for the second GERDA experimental Phase. A double veto system has been designed and constructed using highly radiopure materials (scintillating fibers, wavelength shifters, polymeric foils, reflective foils). This work describes the study of lead, thorium and uranium ultra-trace content, performed at the LNGS Chemistry Laboratory by High Resolution Mass Spectrometry (HR ICP MS), for the selection of all materials involved in the construction of the veto system

  4. ICP MS selection of radiopure materials for the GERDA experiment

    Energy Technology Data Exchange (ETDEWEB)

    Di Vacri, M. L., E-mail: divacrim@lngs.infn.it [INFN, Laboratori Nazionali del Gran Sasso, via G.Acitelli 22, 67100 Assergi (Italy); Dipartimento di Scienze Fisiche e Chimiche, University of L’Aquila, via Vetoio, 67100 L’Aquila (Italy); Nisi, S., E-mail: nisi@lngs.infn.it [INFN, Laboratori Nazionali del Gran Sasso, via G.Acitelli 22, 67100 Assergi (AQ) (Italy); Cattadori, C., E-mail: cattadori@lngs.infn.it [INFN Sezione di Milano Bicocca, Milano (Italy); Janicsko, J. [TUM Munich (Germany); Lubashevskiy, A. [MPIK, Heidelberg (Germany); JINR, Dubna (Russian Federation); Smolnikov, A. [MPIK, Heidelberg (Germany); Walter, M. [Physik-Institut, Universitat Zurich, 8057 Zurich (Switzerland)

    2015-08-17

    The GERDA (GERmanium Detector Array) experiment, located in the Gran Sasso Underground Laboratory (LNGS, Italy) aims to search for neutrinoless double beta (0νββ) decay of the {sup 76}Ge isotope. Both an ultra-low radioactivity background environment and active techniques to abate the residual background are required to reach the background index (of 10{sup −3} counts/keV kg y) at the Q{sub ββ}. In order to veto and suppress those events that partially deposit energy in Ge detectors, the readout of liquid argon (LAr) scintillation light (SL) has been implemented for the second GERDA experimental Phase. A double veto system has been designed and constructed using highly radiopure materials (scintillating fibers, wavelength shifters, polymeric foils, reflective foils). This work describes the study of lead, thorium and uranium ultra-trace content, performed at the LNGS Chemistry Laboratory by High Resolution Mass Spectrometry (HR ICP MS), for the selection of all materials involved in the construction of the veto system.

  5. A 2D semi-analytical model for Faraday shield in ICP source

    International Nuclear Information System (INIS)

    Zhang, L.G.; Chen, D.Z.; Li, D.; Liu, K.F.; Li, X.F.; Pan, R.M.; Fan, M.W.

    2016-01-01

    Highlights: • In this paper, a 2D model of ICP with faraday shield is proposed considering the complex structure of the Faraday shield. • Analytical solution is found to evaluate the electromagnetic field in the ICP source with Faraday shield. • The collision-free motion of electrons in the source is investigated and the results show that the electrons will oscillate along the radial direction, which brings insight into how the RF power couple to the plasma. - Abstract: Faraday shield is a thin copper structure with a large number of slits which is usually used in inductive coupled plasma (ICP) sources. RF power is coupled into the plasma through these slits, therefore Faraday shield plays an important role in ICP discharge. However, due to the complex structure of the Faraday shield, the resulted electromagnetic field is quite hard to evaluate. In this paper, a 2D model is proposed on the assumption that the Faraday shield is sufficiently long and the RF coil is uniformly distributed, and the copper is considered as ideal conductor. Under these conditions, the magnetic field inside the source is uniform with only the axial component, while the electric field can be decomposed into a vortex field generated by changing magnetic field together with a gradient field generated by electric charge accumulated on the Faraday shield surface, which can be easily found by solving Laplace's equation. The motion of the electrons in the electromagnetic field is investigated and the results show that the electrons will oscillate along the radial direction when taking no account of collision. This interesting result brings insight into how the RF power couples into the plasma.

  6. Impact of plasma tube wall thickness on power coupling in ICP sources

    International Nuclear Information System (INIS)

    Nawaz, Anuscheh; Herdrich, Georg

    2009-01-01

    The inductively heated plasma source at the Institute of Space Systems was investigated with respect to the wall thickness of the plasma tube using an air plasma. For this, the wall thickness of the quartz tube was reduced in steps from 2.5 to 1.25 mm. The significance of reducing the wall thickness was analyzed with respect to both the maximum allowable tube cooling power and the coupling efficiency. While the former results from thermal stresses in the tube's wall, the latter results from a minimization of magnetic field losses near the coil turns of the inductively coupled plasma (ICP) source. Analysis of the thermal stress could be validated by experimental data, i.e. the measurement of the tube cooling power when the respective tube structure failed. The coupling efficiency could be assessed qualitatively by simplified models, and the experimental data recorded show that coupling was improved far more than predicted.

  7. Study on performance of a simultaneous spectrometer of ICP emission source for the determination of the major elements in rocks

    International Nuclear Information System (INIS)

    Vieira, M.D.

    1987-01-01

    The optimization of operational parameters of a simultaneous spectrometer coupled to an ICP excitation source in order to establish an analytical method for the simultaneous determination of the major elements in rocks is studied. The mutual spectral interferences, calibration curves for the acid and saline matrix and the internal standard method with ytrium are analyzed. (M.J.C.) [pt

  8. Method validation in plasma source optical emission spectroscopy (ICP-OES) - From samples to results

    International Nuclear Information System (INIS)

    Pilon, Fabien; Vielle, Karine; Birolleau, Jean-Claude; Vigneau, Olivier; Labet, Alexandre; Arnal, Nadege; Adam, Christelle; Camilleri, Virginie; Amiel, Jeanine; Granier, Guy; Faure, Joel; Arnaud, Regine; Beres, Andre; Blanchard, Jean-Marc; Boyer-Deslys, Valerie; Broudic, Veronique; Marques, Caroline; Augeray, Celine; Bellefleur, Alexandre; Bienvenu, Philippe; Delteil, Nicole; Boulet, Beatrice; Bourgarit, David; Brennetot, Rene; Fichet, Pascal; Celier, Magali; Chevillotte, Rene; Klelifa, Aline; Fuchs, Gilbert; Le Coq, Gilles; Mermet, Jean-Michel

    2017-01-01

    Even though ICP-OES (Inductively Coupled Plasma - Optical Emission Spectroscopy) is now a routine analysis technique, requirements for measuring processes impose a complete control and mastering of the operating process and of the associated quality management system. The aim of this (collective) book is to guide the analyst during all the measurement validation procedure and to help him to guarantee the mastering of its different steps: administrative and physical management of samples in the laboratory, preparation and treatment of the samples before measuring, qualification and monitoring of the apparatus, instrument setting and calibration strategy, exploitation of results in terms of accuracy, reliability, data covariance (with the practical determination of the accuracy profile). The most recent terminology is used in the book, and numerous examples and illustrations are given in order to a better understanding and to help the elaboration of method validation documents

  9. Experience with synchrotron radiation sources

    International Nuclear Information System (INIS)

    Krinsky, S.

    1987-01-01

    The development of synchrotron radiation sources is discussed, emphasizing characteristics important for x-ray microscopy. Bending magnets, wigglers and undulators are considered as sources of radiation. Operating experience at the national Synchrotron Light Source on the VUV and XRAY storage rings is reviewed, with particular consideration given to achieved current and lifetime, transverse bunch dimensions, and orbit stability. 6 refs., 3 figs

  10. Experiences in the ICP-MS analysis of geological and environmental samples

    International Nuclear Information System (INIS)

    Kallio, E.

    1994-01-01

    Inductively coupled plasma mass spectrometry (ICP-MS) has been used at the Geological Survey of Finland since 1991. Applied to determination of trace and ultra trace elements in water, sediments, biological samples and rocks. The strength of the technique lies in the ability to determine isotope ratios, and elements that are difficult or expensive to determine by other techniques, e.g. platinum group elements (PGEs), rare earths elements (REEs) and toxic metals (As, Be, Cd, Hg, Pb, Tl, U). An important part of the analysis is the pretreatment of the samples before the measurement. This paper gives an overview of the methods used at the Geological Survey. (orig.). (5 refs.)

  11. In situ quantification of Br and Cl in minerals and fluid inclusions by LA-ICP-MS: a powerful tool to identify fluid sources

    Science.gov (United States)

    Hammerli, Johannes; Rusk, Brian; Spandler, Carl; Emsbo, Poul; Oliver, Nicholas H.S.

    2013-01-01

    Bromine and chlorine are important halogens for fluid source identification in the Earth's crust, but until recently we lacked routine analytical techniques to determine the concentration of these elements in situ on a micrometer scale in minerals and fluid inclusions. In this study, we evaluate the potential of in situ Cl and Br measurements by LA-ICP-MS through analysis of a range of scapolite grains with known Cl and Br concentrations. We assess the effects of varying spot sizes, variable plasma energy and resolve the contribution of polyatomic interferences on Br measurements. Using well-characterised natural scapolite standards, we show that LA-ICP-MS analysis allows measurement of Br and Cl concentrations in scapolite, and fluid inclusions as small as 16 μm in diameter and potentially in sodalite and a variety of other minerals, such as apatite, biotite, and amphibole. As a demonstration of the accuracy and potential of Cl and Br analyses by LA-ICP-MS, we analysed natural fluid inclusions hosted in sphalerite and compared them to crush and leach ion chromatography Cl/Br analyses. Limit of detection for Br is ~8 μg g−1, whereas relatively high Cl concentrations (> 500 μg g−1) are required for quantification by LA-ICP-MS. In general, our LA-ICP-MS fluid inclusion results agree well with ion chromatography (IC) data. Additionally, combined cathodoluminescence and LA-ICP-MS analyses on natural scapolites within a well-studied regional metamorphic suite in South Australia demonstrate that Cl and Br can be quantified with a ~25 μm resolution in natural minerals. This technique can be applied to resolve a range of hydrothermal geology problems, including determining the origins of ore forming brines and ore deposition processes, mapping metamorphic and hydrothermal fluid provinces and pathways, and constraining the effects of fluid–rock reactions and fluid mixing.

  12. Lead isotope ratios in lichen samples evaluated by ICP-ToF-MS to assess possible atmospheric pollution sources in Havana, Cuba.

    Science.gov (United States)

    Alvarez, Alfredo Montero; Estévez Alvarez, Juan R; do Nascimento, Clístenes Williams Araújo; González, Iván Pupo; Rizo, Oscar Díaz; Carzola, Lázaro Lima; Torres, Roberto Ayllón; Pascual, Jorge Gómez

    2017-01-01

    Epiphytic lichens, collected from 119 sampling sites grown over "Roistonea Royal Palm" trees, were used to assess the spatial distribution pattern of lead (Pb) and identify possible pollution sources in Havana (Cuba). Lead concentrations in lichens and topsoils were determined by flame atomic absorption spectrophotometry and inductively coupled plasma (ICP) atomic emission spectrometry, respectively, while Pb in crude oils and gasoline samples were measured by ICP-time of flight mass spectrometry (ICP-ToF-MS). Lead isotopic ratios measurements for lichens, soils, and crude oils were obtained by ICP-ToF-MS. We found that enrichment factors (EF) reflected a moderate contamination for 71% of the samples (EF > 10). The 206 Pb/ 207 Pb ratio values for lichens ranged from 1.17 to 1.20 and were a mixture of natural radiogenic and industrial activities (e.g., crude oils and fire plants). The low concentration of Pb found in gasoline (leaded gasoline is no longer used in Cuba.

  13. Application of ICP-MS and AMS for determination of Pu- and U-isotope ratios for source identification

    Energy Technology Data Exchange (ETDEWEB)

    Skipperud, L. (Norwegian Univ. of Life Sciences, Isotope Lab.. Dept. of Plant and Environmental Sciences, AAs (Norway))

    2010-03-15

    the Pu-240/Pu-239 ratio offers a reliable way of distinguishing weapon's grade sources from global fallout. Since these two isotopes are not separated easily by conventional alfa spectrometry techniques, mass spectrometry is required for an assessment of the isotope ratios. Because of the low levels of plutonium in the Arctic area, plutonium concentrations and 240/239 ratios have been determined using accelerator mass spectrometry (AMS), which has proved a useful and reliable method for analysis of plutonium. ICP-MS has proven to be a good tool together with traditional alfa spectrometry when it comes to analysing plutonium and its isotope ratios in more contaminated areas. (author)

  14. Patients experience of source isolation

    DEFF Research Database (Denmark)

    Johansen, Kamilla; Pedersen, Didde; Kragbak, Nina

    2014-01-01

    , Nursing education in Århus, Hedeager 2, 8200 Aarhus N, Denmark. Background: Medical treatment and care of patients with infections may include source isolation of the patient, to avoid spreading of the infection. However, isolation is a potential physiological and psychological stress factor...... of the patients perspectives of being isolated to identify areas of potential interest for developing new caring strategies to minimize the negative side effects of isolation. Methods: Literature was systematically searched in CINAHL, Nursing Reference Center, Social Care Online, SveMed+, The Cochrane Library...... of Care: The patients felt abandoned and forgotten by the nurses, because of fewer visits and time limited communication. This led to emotions such as frustrations, insecurity and neglect. While isolated the patients felt it difficult to achieve contact and have an optimal relation with the nurses...

  15. Views and experiences of using integrated care pathways (ICPs) for caring for people in the last days to hours of life: results from a cross-sectional survey of UK professionals.

    Science.gov (United States)

    Collins, K A; Hughes, P M; Ibbotson, R; Foy, G; Brooks, D

    2016-09-01

    To determine the views and experiences of health and social care professionals on using integrated care pathways (ICPs)for caring for people in the last days to hours of life. Online cross-sectional questionnaire survey of UK professionals working in UK primary and secondary care settings. 1331 professionals returned completed questionnaires. Ninety-three per cent (1138/1228) of respondents used the Liverpool Care Pathway (LCP) or local variant. Eighty-eight (1089/1234) felt ICPs enabled professionals to provide better care for individuals and their families/carers. ICPs were viewed as promoting patient-centred holistic care, improving pain and symptom control, providing guidance and standards and improving communication with patients/families. Sixty-two per cent (770/1234) had no concerns regarding the use of ICPs. Areas of concern included incorrect use and implementation of the ICP, poor communication with families, junior level staff making decisions and insufficient education and support. There was strong support for using ICPs for caring for people in the last days to hours of life. ICPs were viewed as supporting high-quality patient-centred holistic care. Given the recommendations of the More Care Less Pathway report, those that develop the guidance and support that replace the LCP need to incorporate the aspects of this that have resulted in the benefits seen by professionals within this survey, but also learn from the instances where ICPs have failed to prevent poor care, or worse, have contributed to it. Published by the BMJ Publishing Group Limited. For permission to use (where not already granted under a licence) please go to http://www.bmj.com/company/products-services/rights-and-licensing/

  16. Materials performance experience at spallation neutron sources

    Energy Technology Data Exchange (ETDEWEB)

    Sommer, W.F. [Los Alamos National Laboratory, NM (United States)

    1995-10-01

    There is a growing, but not yet substantial, data base for materials performance at spallation neutron sources. Specially designed experiments using medium energy protons (650 MeV) have been conducted at the Proton Irradiation Experiment (PIREX) facility at the Swiss Nuclear Institute accelerator (SIN). Specially designed experiments using 760-800 MeV copper target have been completed at the Los Alamos Spallation Radiation Effects Facility (LASREF) at Los Alamos Meson Physics Facility (LAMPF). An extensive material testing program was initiated at LASREF in support of the German spallation neutron source (SNQ) project, before it terminated in 1985.

  17. Neutron source characterization for materials experiments

    International Nuclear Information System (INIS)

    Greenwood, L.R.

    1982-01-01

    Data are presented from HFIR-CTR32, EBRII-X287, and the Omega West Reactor. An important new source of damage in nickel arises from the 340 keV 56 Fe recoil from the 59 Ni(n,α) reaction used to produce high helium levels in materials irradiations in a thermal spectrum. The status of all other experiments is summarized

  18. Study of characterizations of aerosols in a dust storm source region and its influence on Beijing by NAA and ICP-MS

    International Nuclear Information System (INIS)

    Song Yan; Chai Zhifang; Xu Diandou; Feng Weiyue; Ouyang Hong; Mao Xueying

    2005-01-01

    Dust storms have caused many problems in the environment, health and climate. For decades, dust storms have occurred frequently in various regions of China. The dust aerosols not only affected the local atmosphere, but also contaminated the atmosphere of the circumjacent regions. Further, they could affect Korea, Japan and even USA via long-range transportation. Many researches related to Chinese dust storms have been reported, however, there are few reports on the chemical components and characters of dust aerosols at their sources. Data on chemical properties of dust storm in the dust source region can help people understand the characteristics of dust storms and their influence on local and other regions. Duolun county (42 degree 13' N, 116 degree 25' E) lies in the southeast of Inner Mongolia, China, in the south of Hunshandake sands (one of the four famous sands in China). Because it is located at windward of Beijing, the dust aerosols can affect Beijing quickly when dust storm occurs. Hence, the study of chemical compositions and elemental abundance patterns of atmospheric particulate matters at Duolun is imperative to understand its influence on Beijing's atmospheric quality. In this work, TSP and PM2.5 samples were collected in Beijing and Duolun, Inner Mongolia, China, in April and May of 2002. Monthly arithmetic averages of the mass concentrations indicated that the pollution of atmospheric particulate matter's (APM) in Duolun was very serious, especially in April. The chemical compositions of total 163 samples were analyzed by INAA and ICP-MS and their origins were identified through Enrichment Factor and Principal Component Analysis. The results showed that the main source of Duolun aerosols was soil dust, and coal combustion constituted the important anthropogenic contribution. The dust events in April and changes of local meteorological conditions were the main reasons for the differences of APM characteristics between April and May. The

  19. Equilibrium of the kink source experiment

    International Nuclear Information System (INIS)

    Marklin, G.

    1985-01-01

    The kink source experiment (KSX) was conceived of as a method of injecting helicity into a spheromak making special use of the m = 1 helical Taylor state. It has a Z pinch as a helicity generating source, connected to a flux conserver through an entrance region. Since the entrance region is a long (length > diameter) cyclinder, the magnetic field should be close to the helical Taylor state, which is the minimum energy configuration of a magnetized plasma in an infinite cylinder with no net flux. This paper will be concerned with modeling the actual fields in the entrance region of the KSX using zero-beta ideal MHD equilibrium theory

  20. Heavy ion source support gas mixing experiments

    International Nuclear Information System (INIS)

    Hudson, E.D.; Mallory, M.L.

    1977-01-01

    Experiments on mixing an easily ionized support gas with the primary ion source gas have produced large beam enhancements for high charge state light ions (masses less than or equal to 20). In the Oak Ridge Isochronous Cyclotron (ORIC), the beam increase has been a factor of 5 or greater, depending on ion species and charge state. Approximately 0.1 cc/min of the easily ionized support gas (argon, krypton, or xenon) is supplied to the ion source through a separate gas line and the primary gas flow is reduced by approximately 30 percent. The proposed mechanism for increased intensity is as follows: The heavier support gas ionizes readily to a higher charge state, providing increased cathode heating. The increased heating permits a reduction in primary gas flow (lower pressure) and the subsequent beam increase

  1. Obsidian provenance studies in archaeology: A comparison between PIXE, ICP-AES and ICP-MS

    International Nuclear Information System (INIS)

    Bellot-Gurlet, Ludovic; Poupeau, Gerard; Salomon, Joseph; Calligaro, Thomas; Moignard, Brice; Dran, Jean-Claude; Barrat, Jean-Alix; Pichon, Laurent

    2005-01-01

    Elemental composition fingerprinting by PIXE technique is very attractive for obsidian provenance studies as it may proceed in a non-destructive mode, even if a more complete elemental characterization can be obtained by ICP-MS and/or ICP-AES. Only few studies have compared results obtained by both methods for solid rock samples. In this work, elemental compositions were determined by ICP-MS/-AES for international geochemical standards and by ICP-MS/-AES and PIXE for inter-laboratory reference obsidians. In addition 49 obsidian source samples and artefacts were analysed by both ICP-MS/-AES and PIXE. Instrumental work and measurement quality control performed for obsidian chemical characterization, underline that PIXE and ICP-MS/-AES provide reproducible, accurate and comparable measurements. In some volcanic districts the limited number of elements dosed by PIXE is sufficient for the discrimination of the potential raw sources of obsidians. Therefore, PIXE can be an advantageous substitute to ICP-MS/-AES techniques for provenance studies

  2. ICP (ITER Collaborative Platform)

    Energy Technology Data Exchange (ETDEWEB)

    Capuano, C.; Carayon, F.; Patel, V. [ITER, 13 - St. Paul-Lez Durance (France)

    2009-07-01

    The ITER organization has the necessity to manage a massive amount of data and processes. Each team requires different process and databases often interconnected with those of others teams. ICP is the current central ITER repository of structured and unstructured data. All data in ICP is served and managed via a web interface that provides global accessibility with a common user friendly interface. This paper will explain the model used by ICP and how it serves the ITER project by providing a robust and agile platform. ICP is developed in ASP.NET using MSSQL Server for data storage. It currently houses 15 data driven applications, 150 different types of record, 500 k objects and 2.5 M references. During European working hours the system averages 150 concurrent users and 20 requests per second. ICP connects to external database applications to provide a single entry point to ITER data and a safe shared storage place to maintain this data long-term. The Core model provides an easy to extend framework to meet the future needs of the Organization. ICP follows a multi-tier architecture, providing logical separation of process. The standard three-tier architecture is expanded, with the data layer separated into data storage, data structure, and data access components. The business or applications logic layer is broken up into a common business functionality layer, a type specific logic layer, and a detached work-flow layer. Finally the presentation tier comprises a presentation adapter layer and an interface layer. Each layer is built up from small blocks which can be combined to create a wide range of more complex functionality. Each new object type developed gains access to a wealth of existing code functionality, while also free to adapt and extend this. The hardware structure is designed to provide complete redundancy, high availability and to handle high load. This document is composed of an abstract followed by the presentation transparencies. (authors)

  3. Operating experience with existing light sources

    International Nuclear Information System (INIS)

    Barton, M.Q.

    1985-01-01

    It is instructive to consider what an explosive growth there has been in the development of light sources using synchrotron radiation. This is well illustrated by the list of facilities given in Table I. In many cases, synchrotron light facilities have been obtained by tacking on parasitic beam lines to rings that were built for high energy physics. Of the twenty-three facilities in this table, however, eleven were built explicitely for this synchrotron radiation. Another seven have by now been converted for use as dedicated facilities leaving only five that share time with high energy physics. These five parasitically operated facilities are still among our best sources of hard x-rays, however, and their importance to the fields of science where these x-rays are needed must be emphasized. While the number of facilities in this table is impressive, it is even more impressive to add up the total number of user beam lines. Most of these rings are absolutely surrounded by beam lines and finding real estate on the experimental floor of one of these facilities for adding a new experiment looks about as practical as adding a farm in the middle of Manhattan. Nonetheless, the managers of these rings seem to have an attitude of ''always room for one more'' and new experimental beam lines do appear. This situation is necessary because the demand for beam time has exploded at an even faster rate than the development of the facilities. The field is not only growing, it can be expected to continue to grow for some time. Some of the explicit plans for future development will be discussed in the companion paper by Lee Teng

  4. ICP-MS Workshop

    Energy Technology Data Exchange (ETDEWEB)

    Carman, April J. [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Eiden, Gregory C. [Pacific Northwest National Lab. (PNNL), Richland, WA (United States)

    2014-11-01

    This is a short document that explains the materials that will be transmitted to LLNL and DNN HQ regarding the ICP-MS Workshop held at PNNL June 17-19th. The goal of the information is to pass on to LLNL information regarding the planning and preparations for the Workshop at PNNL in preparation of the SIMS workshop at LLNL.

  5. Application of on-line HPLC-ICP-MS for the determination of the nuclide abundances of lanthanides produced via spallation reactions in an irradiated tantalum target of a spallation neutron source

    International Nuclear Information System (INIS)

    Kerl, W.; Becker, J.S.; Dietze, H.J.

    1998-01-01

    An analytical procedure has been developed for the determination of spallation nuclides in an irradiated tantalum target using HPLC coupled on-line to ICP-MS after dissolution and separation of the tantalum matrix. Pieces of tantalum were taken from different locations of the irradiated tantalum target which had been used as the target material in a spallation neutron source. Tantalum was dissolved in a HNO 3 /HF mixture and the tantalum matrix was separated by liquid-liquid extraction so that only the spallation nuclides were left in the sample solutions. The major fraction of the spallation nuclides in the tantalum target are lanthanide metals in the μg g -1 concentration range determined in the present study. Additional reaction products are formed by the irradiation of trace impurities in the original tantalum target. The nuclide abundances of the lanthanide metals measured in the tantalum target differ significantly from the natural isotopic composition so that a lot of isobaric interferences of long-lived radionuclides and stable isotopes in the mass spectrum are to be expected. Therefore, all the lanthanide metals had to be separated chemically prior to their mass spectrometric determination. The separation of all rare earth elements was performed by ion chromatography on-line to ICP-MS. The nuclide abundances of each lanthanide were determined using a sensitive double-focusing sector field inductively coupled plasma mass spectrometer. The nuclide abundances of the lanthanides in the irradiated tantalum target calculated theoretically and the experimental results obtained by on-line HPLC-ICP-MS proved to be in good agreement. (orig.)

  6. UHE point source survey at Cygnus experiment

    International Nuclear Information System (INIS)

    Lu, X.; Yodh, G.B.; Alexandreas, D.E.; Allen, R.C.; Berley, D.; Biller, S.D.; Burman, R.L.; Cady, R.; Chang, C.Y.; Dingus, B.L.; Dion, G.M.; Ellsworth, R.W.; Gilra, M.K.; Goodman, J.A.; Haines, T.J.; Hoffman, C.M.; Kwok, P.; Lloyd-Evans, J.; Nagle, D.E.; Potter, M.E.; Sandberg, V.D.; Stark, M.J.; Talaga, R.L.; Vishwanath, P.R.; Zhang, W.

    1991-01-01

    A new method of searching for UHE point source has been developed. With a data sample of 150 million events, we have surveyed the sky for point sources over 3314 locations (1.4 degree <δ<70.4 degree). It was found that their distribution is consistent with a random fluctuation. In addition, fifty two known potential sources, including pulsars and binary x-ray sources, were studied. The source with the largest positive excess is the Crab Nebula. An excess of 2.5 sigma above the background is observed in a bin of 2.3 degree by 2.5 degree in declination and right ascension respectively

  7. New application and future of ICP-MS

    International Nuclear Information System (INIS)

    Masuda, Kimihiko

    1994-01-01

    By ICP-MS, since high sensibility, multi-element rapid analysis and isotope ratio analysis can be carried out, the position as the analysis for ultra-minute amount of elements has been established. Further recently, sample feeder system has been developed, and the multi-collector type device for the purpose of high resolution type isotope ratio analysis has appeared, so the range of its application is spreading more and more. In this report, the examples of application which were able to be attained accompanying the development of these devices are introduced, and the development of the ICP-MS hereafter is described. At present, about 1000 apparatuses are in operation in the world, and the application spread to the fields of semiconductors and materials, earth science, environment, atomic energy and so on. The ICP-MS was developed for the purpose of easily carrying out spectral analysis with high sensibility by using argon ICP as the ion source and doing ion detection which is more efficient than light detection, and has lower background. The progress and the present status of the ICP-MS are reported. As the latest examples of application of the ICP-MS, the analysis of iron by quadrupole type ICP-MS, the small region measurement of solids by laser abrasion, ultra-minute amount analysis by high resolution ICP-MS, the isotope ratio measurement of lead by multi-collector type ICP-MS are reported. (K.I.)

  8. Aging, source memory, and the experience of "remembering".

    Science.gov (United States)

    Kuhlmann, Beatrice G; Boywitt, C Dennis

    2016-07-01

    In a previous study, we found source memory for perceptual features to differentiate between younger but not older adults' reports of recollective ("remember"; R) and "know" (K) experiences. In two experiments with younger (17-30 years) and older (64-81 years) participants, we examined whether memory for meaningful speaker sources would accompany older adults' recollective experience. Indeed, memory for male and female speakers (but not partial memory for gender; Experiment 1) as well as bound memory for speakers and their facial expressions (Experiment 2) distinguished between both younger and older adults' RK reports. Thus, memory for some sources forms a common basis for younger and older adults' retrieval experience. Nonetheless, older adults still showed lower objective source memory and lower subjective source-attribution confidence than younger adults when reporting recollective experiences, suggesting that source memory is less relevant to their retrieval experience than for younger adults.

  9. Results of LA-ICP-MS sulfide mapping from Algoma-type BIF gold systems with implications for the nature of mineralizing fluids, metal sources, and deposit models

    Science.gov (United States)

    Gourcerol, B.; Kontak, D. J.; Thurston, P. C.; Petrus, J. A.

    2018-01-01

    Quantitative laser ablation inductively coupled plasma-mass spectrometry (LA-ICP-MS) element distribution maps combined with traverse mode analyses have been acquired on various sulfides (pyrite, pyrrhotite, arsenopyrite) from three Canadian Algoma-type BIF-hosted gold deposits ( 4 Moz Au Meadowbank, ≥ 2.8 Moz Au Meliadine district, 6 Moz Au Musselwhite). These data, in conjunction with detailed petrographic and SEM-EDS observations, provide insight into the nature and relative timing of gold events, the presence and implication of trace element zoning regarding crystallization processes, and elemental associations that fingerprint gold events. Furthermore, the use of an innovative method of processing the LA-ICP-MS data in map and traverse modes, whereby the results are fragmented into time-slice data, to generate various binary plots (Ag versus Ni) provides a means to identify elemental associations (Te, Bi) not otherwise apparent. This integrated means of treating geochemical data, along with petrography, allows multiple gold events and remobilization processes to be recognized and their elemental associations determined. The main gold event in each of these deposits is characterized by the coupling of an As-Se-Te-Ag element association coincident with intense stratabound sulfide-replacement of the Fe-rich host rock. Additionally, the data indicate presence of a later remobilization event, which upgraded the Au tenor, as either non-refractory or refractory type, along fracture networks due to the ingress of subsequent base metal-bearing metamorphic fluids (mainly a Pb-Bi association). Furthermore, the data reveal a stratigraphic influence, as reflected in the elemental associations and the elemental enrichments observed and the nature of the sulfide phase hosting the gold mineralization (arsenopyrite versus pyrite).

  10. Conditioning experience for spent radium sources

    International Nuclear Information System (INIS)

    Kang, I. S.; Shon, J. S.; Kim, K. J.; Min, D. K.

    2001-01-01

    In order to avoid accidents that could be resulted from improper storage of spent radium sources, it is necessary to condition and store them safely. The program for safe conditioning of spent radium sources by IAEA has been established to assist the developing countries. The main object of this paper is to apply the technology that was adapted by IAEA for the conditioning the national inventory of Ra-226 sources in member states, as a part of IAEA's project with the Korean expert team. This paper is the result that the Korean expert team carried out spent radium conditioning, under the project title 'Radium Conditioning in Myanmar(INT4131-06646C)'. The whole inventory of spent radium sources 1,429.5mCi, was safely conditioned by the Korean expert team according to the manual under the supervision of IAEA's technical officer and the control of Myanmar authority on behalf of Myanmar. These sources were encapsuled and welded into 27 small capsules and 3 large capsules, and conditioned in 3 lead shields, producing 3 concrete-shielded drums. The inventories were distributed into 3 shielding devices, holding 500mCi, 459.5mCi, and 470mCi

  11. Practical guide to ICP-MS: a tutorial for beginners

    National Research Council Canada - National Science Library

    Thomas, Robert

    2013-01-01

    ... for those with limited knowledge of the technique. Written by an insider with more than 20 years experience in product development, customer support, and technical marketing for an ICP-MS instrument vendor, the book highlights this powerful ultra...

  12. Preliminary experiments with a cusp-field ion source

    International Nuclear Information System (INIS)

    Bickes, R.W. Jr.; O'Hagan, J.B.

    1980-12-01

    Preliminary experiments with a cusp field ion source have been completed. Measurements were made of the total ion current and mass and energy distributions as a function of source operating conditions and cusp field geometry. These experiments have indicated that a cusp field source may be used in the Sandia Neutron Generator for Cancer Therapy and may permit the incorporation of a simplified unpumped accelerator design. Suggestions for future work are briefly outlined

  13. Precise and accurate isotope ratio measurements by ICP-MS.

    Science.gov (United States)

    Becker, J S; Dietze, H J

    2000-09-01

    The precise and accurate determination of isotope ratios by inductively coupled plasma mass spectrometry (ICP-MS) and laser ablation ICP-MS (LA-ICP-MS) is important for quite different application fields (e.g. for isotope ratio measurements of stable isotopes in nature, especially for the investigation of isotope variation in nature or age dating, for determining isotope ratios of radiogenic elements in the nuclear industry, quality assurance of fuel material, for reprocessing plants, nuclear material accounting and radioactive waste control, for tracer experiments using stable isotopes or long-lived radionuclides in biological or medical studies). Thermal ionization mass spectrometry (TIMS), which used to be the dominant analytical technique for precise isotope ratio measurements, is being increasingly replaced for isotope ratio measurements by ICP-MS due to its excellent sensitivity, precision and good accuracy. Instrumental progress in ICP-MS was achieved by the introduction of the collision cell interface in order to dissociate many disturbing argon-based molecular ions, thermalize the ions and neutralize the disturbing argon ions of plasma gas (Ar+). The application of the collision cell in ICP-QMS results in a higher ion transmission, improved sensitivity and better precision of isotope ratio measurements compared to quadrupole ICP-MS without the collision cell [e.g., for 235U/238U approximately 1 (10 microg x L(-1) uranium) 0.07% relative standard deviation (RSD) vs. 0.2% RSD in short-term measurements (n = 5)]. A significant instrumental improvement for ICP-MS is the multicollector device (MC-ICP-MS) in order to obtain a better precision of isotope ratio measurements (with a precision of up to 0.002%, RSD). CE- and HPLC-ICP-MS are used for the separation of isobaric interferences of long-lived radionuclides and stable isotopes by determination of spallation nuclide abundances in an irradiated tantalum target.

  14. Conventional sources of fast neutrons in 'cold fusion' experiments

    International Nuclear Information System (INIS)

    Cribier, M.; Spiro, M.; Favier, J.

    1989-04-01

    In 'cold fusion' experiments with heavy water a source of neutrons is the dissociation of deuterium induced by alpha particles emitted by natural occurring radioisotopes. We evaluate the rate of fast neutron emission as a function of the concentration of U, Th, Rn in contact with deuterium and discuss the possibility that the neutrons claimed to have been observed in 'cold fusion' experiments could be due to this conventional source

  15. Radioactive source simulation for half-life experiment

    International Nuclear Information System (INIS)

    Wanitsuksombut, Warapon; Decthyothin, Chanti

    1999-01-01

    A simulation of radioactivity decay by using programmable light source with a few minutes half-life is suggested. A photodiode with digital meter label in cps is use instead of radiation detector. Both light source and photodiode are installed in a black box to avoid surrounding room light. The simulation set can also demonstrate Inverse Square Law experiment of radiation penetration. (author)

  16. Neutron calibration sources in the Daya Bay experiment

    Energy Technology Data Exchange (ETDEWEB)

    Liu, J., E-mail: jianglai.liu@sjtu.edu.cn [Department of Physics, Shanghai Jiao Tong University, Shanghai (China); Kellogg Radiation Laboratory, California Institute of Technology, Pasadena, CA (United States); Carr, R. [Kellogg Radiation Laboratory, California Institute of Technology, Pasadena, CA (United States); Dwyer, D.A. [Kellogg Radiation Laboratory, California Institute of Technology, Pasadena, CA (United States); Lawrence Berkeley National Laboratory, Berkeley, CA (United States); Gu, W.Q. [Department of Physics, Shanghai Jiao Tong University, Shanghai (China); Li, G.S., E-mail: lgs1029@sjtu.edu.cn [Department of Physics, Shanghai Jiao Tong University, Shanghai (China); McKeown, R.D. [Kellogg Radiation Laboratory, California Institute of Technology, Pasadena, CA (United States); Department of Physics, College of William and Mary, Williamsburg, VA (United States); Qian, X. [Kellogg Radiation Laboratory, California Institute of Technology, Pasadena, CA (United States); Brookhaven National Laboratory, Upton, NY (United States); Tsang, R.H.M. [Kellogg Radiation Laboratory, California Institute of Technology, Pasadena, CA (United States); Department of Physics and Astronomy, University of Alabama, Tuscaloosa, AL 35487 (United States); Wu, F.F. [Kellogg Radiation Laboratory, California Institute of Technology, Pasadena, CA (United States); Zhang, C. [Kellogg Radiation Laboratory, California Institute of Technology, Pasadena, CA (United States); Brookhaven National Laboratory, Upton, NY (United States)

    2015-10-11

    We describe the design and construction of the low rate neutron calibration sources used in the Daya Bay Reactor Anti-neutrino Experiment. Such sources are free of correlated gamma-neutron emission, which is essential in minimizing induced background in the anti-neutrino detector. The design characteristics have been validated in the Daya Bay anti-neutrino detector.

  17. Neutron calibration sources in the Daya Bay experiment

    International Nuclear Information System (INIS)

    Liu, J.; Carr, R.; Dwyer, D.A.; Gu, W.Q.; Li, G.S.; McKeown, R.D.; Qian, X.; Tsang, R.H.M.; Wu, F.F.; Zhang, C.

    2015-01-01

    We describe the design and construction of the low rate neutron calibration sources used in the Daya Bay Reactor Anti-neutrino Experiment. Such sources are free of correlated gamma-neutron emission, which is essential in minimizing induced background in the anti-neutrino detector. The design characteristics have been validated in the Daya Bay anti-neutrino detector

  18. ICPES World Congress 2003

    Directory of Open Access Journals (Sweden)

    Chu-Pak Lau

    2002-04-01

    Full Text Available The XII World Congress on Cardiac Pacing and Electrophysiology is co-organised by the International Cardiac Pacing & Electrophysiology Society (ICPES and the Hong Kong College of Cardiology (HKCC. It will take place at the Hong Kong Convention and Exhibition Centre on February 19-22, 2003. The World Congress has been organized in various countries, including USA, France, The Netherlands, Japan, Canada, Austria, Israel, Argentina and Germany. The coming Congress is going to be held in the centre of Asia where East meets West – Hong Kong, which is now a Special Administrative Region of China since 1997. Hong Kong continues to enjoy a high degree of autonomy, and has remained an important center of finance, information technology, tourism, trade and exchange in Asia. In addition, it enjoys increasing interaction with the rapidly developing Mainland China. Developed with the assistance of a broadly represented International Scientific Advisory Committee, the scientific programme will feature 11 major topics - “Electrophysiology”, “Catheter Ablation”, “Pacing”, “Defibrillation”, “Pharmacology”, “Hybrid Therapy”, “Pediatric Arrhythmias”, “Arrhythmias for Allied Professionals”, “Genetics & Gene Therapy”, “ECG, Noninvasive Evaluation & Risk Stratification” and “Implantable Monitoring Devices”. It includes Plenary Sessions, Core Sessions, Expert Sessions, Featured Symposia, Live Demonstration, Teaching Courses, Abstract Presentations and Poster Sessions.

  19. Experiments on a 14.5 GHz ECR source

    International Nuclear Information System (INIS)

    Hill, C.E.; Langbein, K.

    1996-01-01

    The 14.5 GHz ECR4 source supplied to CERN in the framework of the Heavy Ion Facility collaboration provided Pb 27+ operational beams to a new custom built linac in 1994. This source, which operates in the pulsed 'afterglow' mode, quickly met its design specification of 80 eμA and now provides currents >100 eμA regularly. Early source tests showed the existence of extremely stable modes of operation. In the search for higher intensities a number of experiments have been performed on plasma gas composition, RF power matching, extraction, beam pulse compression and a biased dynode. The results of these tests will be presented along with further ideas to improve source performance. (author)

  20. Fundamental-mode sources in approach to critical experiments

    International Nuclear Information System (INIS)

    Goda, J.; Busch, R.

    2000-01-01

    An equivalent fundamental-mode source is an imaginary source that is distributed identically in space, energy, and angle to the fundamental-mode fission source. Therefore, it produces the same neutron multiplication as the fundamental-mode fission source. Even if two source distributions produce the same number of spontaneous fission neutrons, they will not necessarily contribute equally toward the multiplication of a given system. A method of comparing the relative importance of source distributions is needed. A factor, denoted as g* and defined as the ratio of the fixed-source multiplication to the fundamental-mode multiplication, is used to convert a given source strength to its equivalent fundamental-mode source strength. This factor is of interest to criticality safety as it relates to the 1/M method of approach to critical. Ideally, a plot of 1/M versus κ eff is linear. However, since 1/M = (1 minus κ eff )/g*, the plot will be linear only if g* is constant with κ eff . When g* increases with κ eff , the 1/M plot is said to be conservative because the critical mass is underestimated. However, it is possible for g* to decrease with κ eff yielding a nonconservative 1/M plot. A better understanding of g* would help predict whether a given approach to critical will be conservative or nonconservative. The equivalent fundamental-mode source strength g*S can be predicted by experiment. The experimental method was tested on the XIX-1 core on the Fast Critical Assembly at the Japan Atomic Energy Research Institute. The results showed a 30% difference between measured and calculated values. However, the XIX-1 reactor had significant intermediate-energy neutrons. The presence of intermediate-energy neutrons may have made the cross-section set used for predicted values less than ideal for the system

  1. Quantification of "2"3"2Th, "2"3"4U, "2"3"5U and "2"3"8U in river mollusks by magnetic sector mass spectrometry with inductively coupled plasma source (Icp-SFMS)

    International Nuclear Information System (INIS)

    Arevalo R, D. L.; Hernandez M, H.; Romero G, E. T.; Lara A, N.; Alfaro de la T, M. C.

    2016-09-01

    The present work deals with the methodology established for the quantification of "2"3"2Th, "2"3"4U, "2"3"8U and "2"3"5U in the shell of gastropod mollusks collected in the rivers Valles, Coy and Axtla of San Luis Potosi, Mexico, which belong to the Panuco River basin; these rivers have as main source of pollution the discharge of municipal sewage, waste from small industries, agricultural and cattle residues and from natural sources. Conventional methods for measuring radio-nuclides are confronted with certain conditions related to the requirement in measurement, basically in the characterization that is related to the concepts of precision and accuracy. The analysis of the gastropod mollusk shell was performed by the Icp-SFMS technique; the main advantages of this technique lie in the isotope quantification capacity, the high precision and the low limits of detection, in this study are very important because these elements are in concentrations between ppb and ppt. This technique allowed the analysis of the samples having a complex matrix by the presence CaCO_3 minimizing the interferences thanks to the ionization efficiency of the Ar plasma. For the species Pachychilus monachus were found concentrations of "2"3"2Th of 0.16-5.37 μg/g and of total U of 0.101-4.081 μg/g being this species where the highest values of total U were found. For Thiara (melanoids) tuberculata the lowest values were found among the different species ("2"3"2Th 0.61-3.61 μg/g and total U 0.006-0.042 μg/g), for Pachychilus suturalis, values of "2"3"2Th of 0.58-6.4 μg/g and for Pachychilus sp. were found between 0.26-7.62 μg/g and for total U values between 0.28-3.33 μg/g. The method offers several advantages: speed, good precision, low values of quantification limits and high sensitivity in the measurement of radio-nuclides and heavy metals. (Author)

  2. Open-source sensors system for doing simple physics experiments

    Directory of Open Access Journals (Sweden)

    César Llamas Bello

    2018-04-01

    Full Text Available An open-source platform to be used in high school or university laboratories has been developed. The platform permits the performance of dynamics experiments in a simple and affordable way, combining measurements of different sensors in the platform. The sensors are controlled by an Arduino microcontroller, which can be wirelessly accessed with smartphones or tablets. The platform constitutes an economical sensing alternative to commercial configurations and can easily be extended by including new sensors that broaden the range of covered experiments.

  3. Experiments planned to be made with the synchrotron radiation source

    International Nuclear Information System (INIS)

    Matz, W.

    1993-01-01

    For this working meeting, various research groups from the Land Sachsen and from the neighbouring countries Poland and the Czech Republic have been invited in order to present their materials research programmes or task-specific experiments intended to be carried out with the synchrotron radiation source to be installed in the near future. The proceedings volume in hand presents the discussion papers, which have been directly reproduced from the original foils. (orig.) [de

  4. Confined discharge plasma sources for Z-pinch experiments

    International Nuclear Information System (INIS)

    Hinshelwood, D.D.; Goodrich, P.J.; Mehlman, G.; Scherrer, V.E.; Stephanakis, S.J.; Young, F.C.

    1989-01-01

    The authors report their investigation Z-pinch implosions on the NRL Gamble II generator using metallic sources of sodium and aluminum, and non-metallic source of sodium (NaF), magnesium (MgF 2 ), and aluminum (Al 2 0 3 ). For 1 MA driving currents, peak Κ-shell radiated powers of about 100 GW and energies of about 1.5 kj have been obtained with both pure aluminum and NaF implosions. The aluminum results are comparable to those in previous Gamble II experiments with aluminum wire arrays. Confined discharge sources have been used to generate tens of GW in the Na Heα pump line and flourescence of the neon has been observed. The effects of nozzle shape and size, chamber diameter, amount of fuse material, and confined discharge current have been investigated in Gamble II implosion experiments. These studies indicate that confined discharge sources are capable of supplying significantly more material than required for implosions at the 1 MA level, so that this technique could be extended to higher current generators

  5. Toepassing ICP-AES op het RIKILT

    NARCIS (Netherlands)

    Ruig, de W.G.

    1980-01-01

    Rapportage over de toepassing van ICP-AES op het RIKILT. Bij ICP-AES worden twee manieren van lichtemissie detectie toegepast nl. simultaan en sequentieel. De voor- en nadelen van ICP-AES t.o.v. AAS worden op een rij gezet.

  6. LEVIS lithium ion source experiments on PBFA-II

    International Nuclear Information System (INIS)

    Renk, T.J.; Tisone, G.C.; Adams, R.G.; Lopez, M.; Clark, B.F.; Schroeder, J.; Bailey, J.E.; Filuk, A.B.; Carlson, A.L.

    1992-01-01

    PBFA-II is a pulsed power generator designed to apply up to a 25 MV, 20 ns pulse to a focusing 15 cm-radius Applied-B ion diode for inertial confinement fusion applications. Several different approaches have been pursued to produce a high-purity (> 90%), high-current density (5--10 kA/cm 2 ) singly ionized lithium ion source for acceleration in this diode. In addition to having high source purity, such a source should be active, i.e. the ions should be produced before the power pulse arrives, to provide better electrical coupling from the accelerator to the diode. In the LEVIS (Laser EVaporation Ion Source) process, energy from two lasers impinges on a thin (500 nm) lithium or lithium-bearing film on an insulating substrate. The authors will discuss a new series of LEVIS experiments, with a number of improvements: (1) the laser distribution cone was redesigned, resulting in a more uniform illumination of the 4 cm-tall Li-producing surface; (2) the anode surface is being slow-heated to 120--150 C to help drive off contaminants; and (3) they have expanded the number of source and beam diagnostics

  7. Sodium Bicarbonate for Control of ICP: A Systematic Review.

    Science.gov (United States)

    Zeiler, Frederick A; Sader, Nicholas; West, Michael; Gillman, Lawrence M

    2018-01-01

    Our goal was to perform a systematic review of the literature on the use of intravenous sodium bicarbonate for intracranial pressure (ICP) reduction in patients with neurologic illness. Data sources: articles from MEDLINE, BIOSIS, EMBASE, Global Health, Scopus, Cochrane Library, the International Clinical Trials Registry Platform (inception to April 2015), reference lists of relevant articles, and gray literature were searched. 2 reviewers independently extracted data including population characteristics and treatment characteristics. The strength of evidence was adjudicated using both the Oxford and Grading of Recommendation Assessment Development and Education methodology. Our search strategy produced a total 559 citations. Three original articles were included in the review. There were 2 prospective studies, 1 randomized control trial and 1 single arm, and 1 retrospective case report.Across all studies there were a total of 19 patients studied, with 31 episodes of elevated ICP being treated. Twenty-one of those episodes were treated with sodium bicarbonate infusion, with the remaining 10 treated with hypertonic saline in a control model. All elevated ICP episodes treated with sodium bicarbonate solution demonstrated a significant drop in ICP, without an elevation of serum partial pressure of carbon dioxide. No significant complications were described. There currently exists Oxford level 4, Grading of Recommendation Assessment Development and Education D evidence to support an ICP reduction effect with intravenous sodium bicarbonate in TBI. No comments on its impact in other neuropathologic states, or on patient outcomes, can be made at this time.

  8. Quality control of Al alloy by ICP-MS

    International Nuclear Information System (INIS)

    Zahran, N.F.; Amr, M.A.; Helal, A.I.; Waly, S.A.; Afifi, Y.K.

    2000-01-01

    Laser ablation sample introduction system in combination with an inductive coupled plasma mass spectrometer (ICP-MS) is used for the investigation of elemental distribution of Al alloy. The samples are ablated by an ultraviolet laser beam at 266 nm with an energy of 4mJ/shot at a repetition rate of 20 Hz. Samples are digested using HNO 3 in a microwave system and analyzed in a solution form by ICP-MS. The quantification of the analytical results is carried out using multielement solution. Quantitative data from the solution samples are used as a standard data for the laser ablation technique. The effect of Aluminum as a matrix is studied. High-resolution mass spectrometer is used to identify the Aluminum polyatomic ions in the ICP-ion source

  9. Air pollution studies using PIXE and ICP methods

    International Nuclear Information System (INIS)

    Stihi, Claudia; Bancuta, Anca; Popescu, I V; Virgolici, M; Cimpoca, V; Gugiu, M; Vlaicu, Gh

    2006-01-01

    In the present work the moss biomonitoring technique and the combination of two analytical techniques - Particle Induced X-ray Emission (PIXE) and Inductively Coupled Plasma (ICP) - were applied for assessing environmental situation from the point of view of air polluting along the transect from north to south of the Dambovita County. PIXE analysis at the Tandem Accelerator FN-8 of the National Institute of Nuclear Physics - Horia Hulubei of Magurele, Bucharest, allowed determination of P, S, Cl, K, Ca, Mn, Fe, Ni, Cu, Zn, As, Sr, Cd and Pb in samples. ICP analyses were made using a Baird ICP2070 - Sequential Plasma Spectrometer in Targoviste and we determined in samples the concentration of Li, B, Na, and Mg together with Cd and Pb. The obtained results will permit to determine the regional extent of heavy metals and toxic elements atmospheric pollution and to identify specially affected areas and local sources of

  10. Patient experience of source isolation: lessons for clinical practice.

    Science.gov (United States)

    Barratt, Ruth Linda; Shaban, Ramon; Moyle, Wendy

    2011-10-01

    Methicillin-resistant Staphylococcus aureus (MRSA) is now the leading antimicrobial-resistant organism of concern to clinicians worldwide. Preventing and controlling the increase and spread of MRSA within the health-care environment is therefore an important function of the infection control team. The prevention and control of MRSA requires strict use of both Standard and Additional Precautions, which include good hand hygiene practices, judicious antimicrobial prescribing, and source isolation. While few would dispute the need for these precautions for preventing the spread of MRSA and other infections, their use may result in adverse physical and psychological effects for the patient. In an age of quality and safety of health care, ensuring infection control practice such as source isolation and contact precautions adhere to fundamental human rights is paramount. This paper presents a review of the literature on the patient experience of source isolation for MRSA or other infectious diseases. The review yielded five major interconnected themes: (1) psychological effects of isolation; (2) coping with isolation; (3) social isolation; (4) communication and information provision; and (5) physical environment and quality of care. It found that the experience of isolation by patients has both negative and positive elements. Isolation may result in detrimental psychological effects including anxiety, stress and depression, but may also result in the patient receiving less or substandard care. However, patients may also benefit from the quietness and privacy of single rooms. Nurses and other healthcare workers must look for ways to improve the experience of isolation and contact precautions of patients in source isolation. Opportunities exist in particular in improving the environment and the patient's self-control of the situation and in providing adequate information.

  11. A scandium calibration source for the SNO+ experiment

    Energy Technology Data Exchange (ETDEWEB)

    Boeltzig, Axel; Barros, Nuno; Krueger, Felix; Krosigk, Belina von; Lozza, Valentina; Neumann, Laura; Petzoldt, Johannes; Soerensen, Arnd; Zuber, Kai [TU Dresden (Germany)

    2013-07-01

    The SNO+ experiment is the successor of SNO (Sudbury Neutrino Observatory), for which the detector will be filled with liquid scintillator. Located 2 km underground (equivalent to a shielding of about 6 km of water) in a mine near Sudbury, Canada, SNO+ will be a low-background experiment studying different aspects of neutrinos. The SNO+ detector calibration is scheduled to begin in mid-2013 with a water-filled detector and in 2014 filled with liquid scintillator. One of the sources designated for this calibration will use the γ rays following the beta decay of {sup 48}Sc. The sum of their energies is 3.333 MeV for the main decay branch, which is close to Q=3.371 MeV for the neutrino-less double beta decay of {sup 150}Nd that SNO+ plans to investigate. Due to the {sup 48}Sc half-life of 43.67 h, the source has to be produced shortly before the calibration via (n,p) reactions on {sup 48}Ti. Safety, radiopurity and cleanliness are further important issues for its application. The current status of the source development will be presented.

  12. Experiments with radioactive samples at the Advanced Photon Source

    International Nuclear Information System (INIS)

    Veluri, V. R.; Justus, A.; Glagola, B.; Rauchas, A.; Vacca, J.

    2000-01-01

    The Advanced Photon Source (APS) at Argonne National Laboratory is a national synchrotron-radiation light source research facility. The 7 GeV electron Storage Ring is currently delivering intense high brilliance x-ray beams to a total of 34 beamlines with over 120 experiment stations to members of the international scientific community to carry out forefront basic and applied research in several scientific disciplines. Researchers come to the APS either as members of Collaborative Access Teams (CATs) or as Independent Investigators (IIs). Collaborative Access Teams comprise large number of investigators from universities, industry, and research laboratories with common research objectives. These teams are responsible for the design, construction, finding, and operation of beamlines. They are the owners of their experimental enclosures (''hutches'') designed and built to meet their specific research needs. Fig. 1 gives a plan view of the location of the Collaborative Access Teams by Sector and Discipline. In the past two years, over 2000 individual experiments were conducted at the APS facility. Of these, about 60 experiments involved the use of radioactive samples, which is less than 3% of the total. However, there is an increase in demand for experiment stations to accommodate the use of radioactive samples in different physical forms embedded in various matrices with activity levels ranging from trace amounts of naturally occurring radionuclides to MBq (mCi) quantities including transuranics. This paper discusses in some detail the steps in the safety review process for experiments involving radioactive samples and how ALARA philosophy is invoked at each step and implemented

  13. Optimization of atomic beam sources for polarization experiments

    Energy Technology Data Exchange (ETDEWEB)

    Gaisser, Martin; Nass, Alexander; Stroeher, Hans [IKP, Forschungszentrum Juelich (Germany)

    2013-07-01

    For experiments with spin-polarized protons and neutrons a dense target is required. In current atomic beam sources an atomic hydrogen or deuterium beam is expanded through a cold nozzle and a system of sextupole magnets and RF-transition units selects a certain hyperfine state. The achievable flux seems to be limited to about 10{sup 17} particles per second with a high nuclear polarization. A lot of experimental and theoretical effort has been undertaken to understand all effects and to increase the flux. However, improvements have remained marginal. Now, a Monte Carlo simulation based on the DSMC part of the open source C++ library OpenFOAM is set up in order to get a better understanding of the flow and to optimize the various elements. It is intended to include important effects like deflection from magnetic fields, recombination on the walls and spin exchange collisions in the simulation and make quantitative predictions of changes in the experimental setup. The goal is to get a tool that helps to further increase the output of an atomic beam source. So far, a new binary collision model, magnetic fields, RF-transition units and a tool to measure the collision age are included. The next step will be to couple the whole simulation with an optimization algorithm implementing Adaptive Simulated Annealing (ASA) in order to automatically optimize the atomic beam source.

  14. Detail design of the beam source for the SPIDER experiment

    International Nuclear Information System (INIS)

    Marcuzzi, D.; Agostinetti, P.; Dalla Palma, M.; Degli Agostini, F.; Pavei, M.; Rizzolo, A.; Tollin, M.; Trevisan, L.

    2010-01-01

    The ITER Neutral Beam Test Facility (PRIMA-Padova Research on Injector Megavolt Accelerated) is planned to be built at Consorzio RFX (Padova, Italy). PRIMA includes two experimental devices: a full size plasma source with low voltage extraction called SPIDER (Source for Production of Ion of Deuterium Extracted from RF plasma) and a full size neutral beam injector at full beam power called MITICA (Megavolt ITER Injector Concept Advancement). SPIDER is the first experimental device to be built and operated, aiming at testing the extraction of a negative ion beam (made of H - and in a later stage D - ions) from an ITER size ion source. The main requirements of this experiment are a H - /D - current of approximately 70 A/50 A and an energy of 100 keV. This paper presents an overview of the SPIDER beam source design, with a particular focus on the main design choices, aiming at reaching the best compromise between physics, optics, thermo-mechanical, cooling, assembly and electrical requirements.

  15. Characterisation of Supra- and Infratentorial ICP Profiles.

    Science.gov (United States)

    Moyse, Emmanuel; Ros, Maxime; Marhar, Fouad; Swider, Pascal; Schmidt, Eric Albert

    2016-01-01

    In pathophysiology and clinical practice, the intracranial pressure (ICP) profiles in the supratentorial and infratentorial compartments are unclear. We know that the pressure within the skull is unevenly distributed, with demonstrated ICP gradients. We recorded and characterised the supra- and infratentorial ICP patterns to understand what drives the transtentorial ICP gradient.A 70-year-old man was operated on for acute cerebellar infarction. One supratentorial probe and one cerebellar probe were implanted. Both signals were recorded concurrently and analysed off-line. We calculated mean ICP, ICP pulse amplitude, respiratory waves, slow waves and the RAP index of supra- and infratentorial ICP signals. Then, we measured transtentorial difference and performed correlation analysis for every index.Supratentorial ICP mean was 8.5 mmHg lower than infratentorial ICP, but the difference lessens for higher values. Both signals across the tentorium showed close correlation. Supra- and infratentorial pulse amplitude, respiratory waves and slow waves also showed a high degree of correlation. The compensatory reserve (RAP) showed good correlation. In this case report, we demonstrate that the mean value of ICP is higher in the posterior fossa, with a strong correlation across the tentorium. All other ICP-derived parameters display a symmetrical profile.

  16. Experience with first aid in radiation sources accidents

    International Nuclear Information System (INIS)

    Klener, V.

    1979-01-01

    More than 20 years of experience at the Radiation Hygiene Centre of the Prague Institute of Hygiene and Epidemiology with prevention of accidents involving sources of radiation and the Centre's participation in providing medical aid in such accidents are described. A list is given of major types of accidents over the past decade. Prevalent were accidents involving sealed gamma sources, resulting in excessive local irradiation with serious skin damage or injury to some of the deeper structures of the hands, requiring plastic operation. Chromosomal picture investigation allows the estimation of the equivalent body dose which only reached higher values in a single case recorded (1.5 Gy = 150 rad). Organisational measures are described for emergencies and the task is shown by radiation hygiene departments attached to regional hygiene stations. The present system is capable of providing adequate, prompt and effective assistance. (author)

  17. Interpretation of the TRADE In-Pile source multiplication experiments

    International Nuclear Information System (INIS)

    Mercatali, Luigi; Carta, Mario; Peluso, Vincenzo

    2006-01-01

    Within the framework of the neutronic characterization of the TRIGA RC-1 reactor in support to the TRADE (TRiga Accelerator Driven Experiment) program, the interpretation of the subcriticality level measurements performed in static regime during the TRADE In-Pile experimental program is presented. Different levels of subcriticality have been measured using the MSA (Modified Source Approximated) method by the insertion of a standard fixed radioactive source into different core positions. Starting from a reference configuration, fuel elements were removed: control rods were moved outward as required for the coupling experiments envisioned with the proton accelerator and fission chambers were inserted in order to measure subcritical count rates. A neutron-physics analysis based on the modified formulation of the source multiplication method (MSM) has been carried out, which requires the systematic solution for each experimental configuration of the homogeneous, both in the forward and adjoint forms, and inhomogeneous Boltzmann equations. By means of such a methodology calculated correction factors to be applied to the MSA measured reactivities were produced in order to take into account spatial and energetic effects creating changes in the detector efficiencies and effective source with respect to the calibration configuration. The methodology presented has been tested against a large number of experimental states. The measurements have underlined the sensitivity of the MSA measured reactivities to core geometry changes and control rod perturbations; the efficiency of MSM factors to dramatically correct for this sensitivity is underlined, making of this technique a relevant methodology in view of the incoming US RACE program to be performed in TRIGA reactors

  18. Experiences with on-site power sources at KCB

    Energy Technology Data Exchange (ETDEWEB)

    Heijnen, B. M.A. [Borssele Nuclear Power Station, N.V. P.Z.E.M., Postbus 48, 4330 AA Middleburg (Netherlands)

    1986-02-15

    The design of the nuclear power station is of the late sixties. The experiences with the on-site power sources, signal processing and some of the resulting modifications of the design of the power plant are mentioned. In order to let the design satisfy as much as possible present ideas about safety, it was decided to realize a total new and Independent decay heat removal System. With this system a second independent on-site power System is at disposal in case of accident situations. (author)

  19. Calibration experiments of neutron source identification and detection in soil

    International Nuclear Information System (INIS)

    Gorin, N. V.; Lipilina, E. N.; Rukavishnikov, G. V.; Shmakov, D. V.; Ulyanov, A. I.

    2007-01-01

    In the course of detection of fissile materials in soil, series of calibration experiments were carried out on in laboratory conditions on an experimental installation, presenting a mock-up of an endless soil with various heterogeneous bodies in it, fissile material, measuring boreholes. A design of detecting device, methods of neutrons detection are described. Conditions of neutron background measuring are given. Soil density, humidity, chemical composition of soil was measured. Sensitivity of methods of fissile materials detection and identification in soil was estimated in the calibration experiments. Minimal detectable activity and the distance at which it can be detected were defined. Characteristics of neutron radiation in a borehole mock-up were measured; dependences of method sensitivities from water content in soil, source-detector distance and presence of heterogeneous bodies were examined. Possibility of direction detection to a fissile material as neutron source from a borehole using a collimator is shown. Identification of fissile material was carried out by measuring the gamma-spectrum. Mathematical modeling was carried out using the PRIZMA code (Developed in RFNC-VNIITF) and MCNP code (Developed in LANL). Good correlation of calculational and experimental values was shown. The methodic were shown to be applicable in the field conditions

  20. Optimization of atomic beam sources for polarization experiments

    Energy Technology Data Exchange (ETDEWEB)

    Gaisser, Martin; Nass, Alexander; Stroeher, Hans [IKP, Forschungszentrum Juelich (Germany)

    2012-07-01

    For experiments with spinpolarized protons and neutrons a dense target is required. In current atomic beam sources an atomic hydrogen or deuterium beam is expanded through a cold nozzle and a system of sextupole magnets and RF-transition units selects a certain hyperfine state. The achievable flux seems to be limited to about 10{sup 17} particles per second with a high nuclear polarization. A lot of experimental and theoretical effort has been undertaken to understand all effects and to increase the flux. However, improvements have remained marginal. Now, a Monte Carlo simulation based on the DSMC part of the open source C++ library OpenFOAM is set up in order to get a better understanding of the flow and to optimize the various elements. The goal is to include important effects like deflection from a magnetic field, recombination on the walls and spin exchange collisions in the simulation and make quantitative predictions of changes in the experimental setup. The goal is to get a tool that helps to further increase the output of an atomic beam source.

  1. Multielemental analysis of Korean geological reference samples by INAA, ICP-AES and ICP-MS

    International Nuclear Information System (INIS)

    Naoki Shirai; Hiroki Takahashi; Yuta Yokozuka; Mitsuru Ebihara; Meiramkhan Toktaganov; Shun Sekimoto

    2015-01-01

    Six Korean geological reference samples (KB-1, KGB-1, KT-1, KD-1, KG-1 and KG-2) prepared by Korea Institutes of Geoscience and Mineral Resources were analyzed by using INAA, ICP-AES and ICP-MS. Some elements could be determined by both INAA and non-INAA methods (ICP-AES and ICP-MS), and these data are consistent with each other. This study confirms that a combination of ICP-AES and ICP-MS is comparable to INAA in determining a wide range of major, minor and trace elements in geological materials. (author)

  2. Source term experiments project (STEP): aerosol characterization system

    International Nuclear Information System (INIS)

    Schlenger, B.J.; Dunn, P.F.

    1985-01-01

    A series of four experiments has been conducted at Argonne National Laboratory's TREAT Reactor. These experiments, which are sponsored by an international consortium organized by the Electric Power Research Institute, are designed to investigate the source term, i.e., the type, quantity and timing of release of radioactive fission products from a light water reactor to the environment in the event of a severe accident in which the core is insufficiently cooled. The STEP tests have been designed to provide some of the necessary data regarding the magnitude and release rates of volatile fission products from degraded fuel pins, their physical and chemical characteristics, and aerosol formation and transport phenomena of those fission products that condense to form particles in the cooler regions of the reactor beyond the core. These are inpile experiments, whereby the test fuels are heated in a nuclear test reactor by neutron induced fission and subsequent cladding oxidation in steam environments that simulate as closely as practical predicted severe reactor accident conditions. The test sequences cover a range of pressure and fuel heatup rate, and include the effect of Ag/In/Cd control rod material. 1 ref., 8 figs., 1 tab

  3. Uranium spectra in the ICP

    Energy Technology Data Exchange (ETDEWEB)

    Ghazi, A.A.; Qamar, S.; Atta, M.A. (Khan (A.Q.) Research Labs., Rawalpindi (Pakistan))

    1994-05-01

    Uranium spectra have been studied by inductively coupled plasma atomic emission spectroscopy (ICP-AES). In total, 8361 uranium lines were observed in the wavelength range of 235-500 nm. This article is an electronic publication in Spectrochimica Acta Electronica (SAE), the electronic section of Spectrochimica Acta Part B (SAB). The hard copy text is accompanied by a disk with data files and test files for an IBM-compatible computer. The main article discusses the scientific aspects of the subject and explains the purpose of the data files. (Author).

  4. Uranium spectra in the ICP

    International Nuclear Information System (INIS)

    Ghazi, A.A.; Qamar, S.; Atta, M.A.

    1994-01-01

    Uranium spectra have been studied by inductively coupled plasma atomic emission spectroscopy (ICP-AES). In total, 8361 uranium lines were observed in the wavelength range of 235-500 nm. This article is an electronic publication in Spectrochimica Acta Electronica (SAE), the electronic section of Spectrochimica Acta Part B (SAB). The hard copy text is accompanied by a disk with data files and test files for an IBM-compatible computer. The main article discusses the scientific aspects of the subject and explains the purpose of the data files. (Author)

  5. HTGR nuclear heat source component design and experience

    International Nuclear Information System (INIS)

    Peinado, C.O.; Wunderlich, R.G.; Simon, W.A.

    1982-05-01

    The high-temperature gas-cooled reactor (HTGR) nuclear heat source components have been under design and development since the mid-1950's. Two power plants have been designed, constructed, and operated: the Peach Bottom Atomic Power Station and the Fort St. Vrain Nuclear Generating Station. Recently, development has focused on the primary system components for a 2240-MW(t) steam cycle HTGR capable of generating about 900 MW(e) electric power or alternately producing high-grade steam and cogenerating electric power. These components include the steam generators, core auxiliary heat exchangers, primary and auxiliary circulators, reactor internals, and thermal barrier system. A discussion of the design and operating experience of these components is included

  6. Aluminum as a source of background in low background experiments

    Energy Technology Data Exchange (ETDEWEB)

    Majorovits, B., E-mail: bela@mppmu.mpg.de [MPI fuer Physik, Foehringer Ring 6, 80805 Munich (Germany); Abt, I. [MPI fuer Physik, Foehringer Ring 6, 80805 Munich (Germany); Laubenstein, M. [Laboratori Nazionali del Gran Sasso, INFN, S.S.17/bis, km 18 plus 910, I-67100 Assergi (Italy); Volynets, O. [MPI fuer Physik, Foehringer Ring 6, 80805 Munich (Germany)

    2011-08-11

    Neutrinoless double beta decay would be a key to understanding the nature of neutrino masses. The next generation of High Purity Germanium experiments will have to be operated with a background rate of better than 10{sup -5} counts/(kg y keV) in the region of interest around the Q-value of the decay. Therefore, so far irrelevant sources of background have to be considered. The metalization of the surface of germanium detectors is in general done with aluminum. The background from the decays of {sup 22}Na, {sup 26}Al, {sup 226}Ra and {sup 228}Th introduced by this metalization is discussed. It is shown that only a special selection of aluminum can keep these background contributions acceptable.

  7. Basic experiment on scattering type level gauge using neutron source

    International Nuclear Information System (INIS)

    Kumazaki, Hiroshi; Fukuchi, Ryoichi; Horiguchi, Yasuhiro

    1984-01-01

    The level gauges using sealed radiation sources have been utilized for pulp and chemical industries, however, for those gauges, transmission type gamma sources are used, which require considerably large radioactivity, and it hinders the spread to medium and small enterprises. Recently, Cf-252 has become easily available, and various He-3 counters are on the market, consequently, the scattering type level gauges combining them have been examined. With the level gauges of this type, the judgement of level can be made sufficiently with the Cf-252 below 3.7 x 10 6 Bq, therefore, if the practical instruments are made, they seem to spread into medium and small enterprises because of the safety and the chief handling radiation being unnecessary. For the purpose of developing and manufacturing for trial this scattering type level gauge, the basic experiment was carried out to examine the effects of the change of salt content and the thickness of vessels and the effect of scattering materials. The possibility of the on-off operation as level gauges was also examined. The experimental method and the results are reported. The count considerably decreased with increasing salt content. Scattering materials worked effectively to increase the count. (Kako, I.)

  8. The influence of laser pulse duration and energy on ICP-MS signal intensity, elemental fractionation, and particle size distribution in NIR fs-LA-ICP-MS

    Science.gov (United States)

    Diwakar, Prasoon K.; Harilal, Sivanandan S.; LaHaye, Nicole L.; Hassanein, Ahmed; Kulkarni, Pramod

    2015-01-01

    Laser parameters, typically wavelength, pulse width, irradiance, repetition rate, and pulse energy, are critical parameters which influence the laser ablation process and thereby influence the LA-ICP-MS signal. In recent times, femtosecond laser ablation has gained popularity owing to the reduction in fractionation related issues and improved analytical performance which can provide matrix-independent sampling. The advantage offered by fs-LA is due to shorter pulse duration of the laser as compared to the phonon relaxation time and heat diffusion time. Hence the thermal effects are minimized in fs-LA. Recently, fs-LA-ICP-MS demonstrated improved analytical performance as compared to ns-LA-ICP-MS, but detailed mechanisms and processes are still not clearly understood. Improvement of fs-LA-ICP-MS over ns-LA-ICP-MS elucidates the importance of laser pulse duration and related effects on the ablation process. In this study, we have investigated the influence of laser pulse width (40 fs to 0.3 ns) and energy on LA-ICP-MS signal intensity and repeatability using a brass sample. Experiments were performed in single spot ablation mode as well as rastering ablation mode to monitor the Cu/Zn ratio. The recorded ICP-MS signal was correlated with total particle counts generated during laser ablation as well as particle size distribution. Our results show the importance of pulse width effects in the fs regime that becomes more pronounced when moving from femtosecond to picosecond and nanosecond regimes. PMID:26664120

  9. ICP27-dependent resistance of herpes simplex virus type 1 to leptomycin B is associated with enhanced nuclear localization of ICP4 and ICP0

    International Nuclear Information System (INIS)

    Lengyel, Joy; Strain, Anna K.; Perkins, Keith D.; Rice, Stephen A.

    2006-01-01

    It was previously shown that herpes simplex virus type 1 (HSV-1) is sensitive to leptomycin B (LMB), an inhibitor of nuclear export factor CRM1, and that a single methionine to threonine change at residue 50 (M50T) of viral immediate-early (IE) protein ICP27 can confer LMB resistance. In this work, we show that deletion of residues 21-63 from ICP27 can also confer LMB resistance. We further show that neither the M50T mutation nor the presence of LMB affects the nuclear shuttling activity of ICP27, suggesting that another function of ICP27 determines LMB resistance. A possible clue to this function emerged when it was discovered that LMB treatment of HSV-1-infected cells dramatically enhances the cytoplasmic accumulation of two other IE proteins, ICP0 and ICP4. This effect is completely dependent on ICP27 and is reversed in cells infected with LMB-resistant mutants. Moreover, LMB-resistant mutations in ICP27 enhance the nuclear localization of ICP0 and ICP4 even in the absence of LMB, and this effect can be discerned in transfected cells. Thus, the same amino (N)-terminal region of ICP27 that determines sensitivity to LMB also enhances ICP27's previously documented ability to promote the cytoplasmic accumulation of ICP4 and ICP0. We speculate that ICP27's effects on ICP4 and ICP0 may contribute to HSV-1 LMB sensitivity

  10. 3D printing for cyclonic spray chambers in ICP spectrometry

    OpenAIRE

    Geertsen , Valérie; Barruet , Elodie; Tache , Olivier

    2015-01-01

    International audience; Additive manufacturing (AM) or 3D-printing is an increasingly widespread technique which is often described as a source for rapid prototyping whereas it is a manufacturing process in itself. It is a new tool for instrumental research laboratories which can now easily manufacture by themselves a large variety of devices. This article describes its application to ICP introduction system spray chambers. We undertake to print and study cyclone spray chambers by combining a...

  11. Relating stick-slip friction experiments to earthquake source parameters

    Science.gov (United States)

    McGarr, Arthur F.

    2012-01-01

    Analytical results for parameters, such as static stress drop, for stick-slip friction experiments, with arbitrary input parameters, can be determined by solving an energy-balance equation. These results can then be related to a given earthquake based on its seismic moment and the maximum slip within its rupture zone, assuming that the rupture process entails the same physics as stick-slip friction. This analysis yields overshoots and ratios of apparent stress to static stress drop of about 0.25. The inferred earthquake source parameters static stress drop, apparent stress, slip rate, and radiated energy are robust inasmuch as they are largely independent of the experimental parameters used in their estimation. Instead, these earthquake parameters depend on C, the ratio of maximum slip to the cube root of the seismic moment. C is controlled by the normal stress applied to the rupture plane and the difference between the static and dynamic coefficients of friction. Estimating yield stress and seismic efficiency using the same procedure is only possible when the actual static and dynamic coefficients of friction are known within the earthquake rupture zone.

  12. Romanian experience on safety and security of radiation sources

    International Nuclear Information System (INIS)

    Botgros, Madalina; Coroianu, Anton; Negreanu, Mircea

    2008-01-01

    Romania has established the first administrative structure for controlling the deployment of the nuclear activities in 1961 and the first Romanian nuclear law was published in 1974. In the present, it is in force the Law no. 111, published in 1996 and republished in 2003. Moreover, there are available facilities and services to the persons authorized to manage radioactive sources. The regulation for safety and security of radioactive sources was amended two times in order to implement the international recommendations for setting up the national system for accounting and control of radiation sources and to coordinate the recovery activities. As part of national control programme, the national inventory of sources and devices is updated permanently, when issuing a new authorization, when modifying an existing one, or when renewing an authorization system and records in the database. The government responsibility for the orphan sources is stated in the law on radioactive waste management and decommissioning fund. There is a protocol between CNCAN, Ministry of Internal and Ministry of Health and Family regarding the co-operation in the case of finding orphan sources. When a radiation source is spent, it becomes radioactive waste that has to be disposed off properly. Depending on the case, the holder of a spent source has the possibility either to return the radioactive source to its manufacturer for regeneration or to transfer it to the Radioactive Waste Treatment Facility. (author)

  13. Management of financial sources for innovative development: foreign countries experience

    Directory of Open Access Journals (Sweden)

    Dyba O. M.

    2016-12-01

    Full Text Available Authors have analyzed and synthesized the main features of financial sources management for innovative development in development economies of foreign countries. The article describes the peculiarities of above mentioned type of management, using the examples of such countries as Germany, USA and Japan, which represent different kinds of economy and society. The main sources for innovative development financing are highlighted within the national economies conditions. The authors proposed the generalized models of financial sources management for innovative development. The information will be useful for Ukrainian model of financial sources management development.

  14. ICP/AES radioactive sample analyses at Pacific Northwest Laboratory

    International Nuclear Information System (INIS)

    Matsuzaki, C.L.; Hara, F.T.

    1986-03-01

    Inductively coupled argon plasma atomic emission spectroscopy (ICP/AES) analyses of radioactive materials at Pacific Northwest Laboratory (PNL) began about three years ago upon completion of the installation of a modified Applied Research Laboratory (ARL) 3560. Funding for the purchase and installation of the ICP/AES was provided by the Nuclear Waste Materials Characterization Center (MCC) established at PNL by the Department of Energy in 1979. MCC's objective is to ensure that qualified materials data are available on waste materials. This paper is divided into the following topics: (1) Instrument selection considerations; (2) initial installation of the simultaneous system with the source stand enclosed in a 1/2'' lead-shielded glove box; (3) retrofit installation of the sequential spectrometer; and (4) a brief discussion on several types of samples analyzed. 1 ref., 7 figs., 1 tab

  15. Operational experience with the BNL magnetron H- source

    International Nuclear Information System (INIS)

    Witkover, R.L.

    1983-01-01

    A magnetron H - source with a grooved cathode has been in operation at the BNL Linac for over 18 months. The source has run at 5 pps with a 600 μsec pulse width for periods as long as 5 months. Its development and performance will be discussed

  16. A Stroboscopic Light Source for Experiments in Mechanics

    Science.gov (United States)

    Mayer, V. V.; Varaksina, E. I.

    2017-01-01

    We propose to attach a small stroboscopic light source to a moving object and connect the source to a pulse generator with the help of insulated thin flexible multi-cored wires. Students can assemble such a device independently in a school laboratory. The device can be used to obtain trajectories with time marks in students' research projects in…

  17. Going to the Source: Research Paper Writing Experience.

    Science.gov (United States)

    Rooney, Theresa

    2000-01-01

    First years students' experiences and knowledge about research paper writing were studied to investigate how strongly the process writing movement has influenced instructional practice, and how appropriately students have been prepared for their college experience. Finds that many of the students arrived at college without the experience of…

  18. On the possibility of the multiple inductively coupled plasma and helicon plasma sources for large-area processes

    Energy Technology Data Exchange (ETDEWEB)

    Lee, Jin-Won; Lee, Yun-Seong, E-mail: leeeeys@kaist.ac.kr; Chang, Hong-Young [Low-temperature Plasma Laboratory, Department of Physics, Korea Advanced Institute of Science and Technology, Daejeon 305-701 (Korea, Republic of); An, Sang-Hyuk [Agency of Defense Development, Yuseong-gu, Daejeon 305-151 (Korea, Republic of)

    2014-08-15

    In this study, we attempted to determine the possibility of multiple inductively coupled plasma (ICP) and helicon plasma sources for large-area processes. Experiments were performed with the one and two coils to measure plasma and electrical parameters, and a circuit simulation was performed to measure the current at each coil in the 2-coil experiment. Based on the result, we could determine the possibility of multiple ICP sources due to a direct change of impedance due to current and saturation of impedance due to the skin-depth effect. However, a helicon plasma source is difficult to adapt to the multiple sources due to the consistent change of real impedance due to mode transition and the low uniformity of the B-field confinement. As a result, it is expected that ICP can be adapted to multiple sources for large-area processes.

  19. Quantification of {sup 232}Th, {sup 234}U, {sup 235}U and {sup 238}U in river mollusks by magnetic sector mass spectrometry with inductively coupled plasma source (Icp-SFMS); Cuantificacion de {sup 232}Th, {sup 234}U, {sup 235}U y {sup 238}U en moluscos de rios por espectrometria de masas de sector magnetico con fuente de plasma acoplado inductivamente (ICP-SFMS)

    Energy Technology Data Exchange (ETDEWEB)

    Arevalo R, D. L.; Hernandez M, H.; Romero G, E. T.; Lara A, N. [ININ, Carretera Mexico-Toluca s/n, 52750 Ocoyoacac, Estado de Mexico (Mexico); Alfaro de la T, M. C., E-mail: arevalo0591@hotmail.com [Universidad Autonoma de San Luis Potosi, Dr. Salvador Nava s/n, Zona Universitaria, 78290 San Luis Potosi, SLP (Mexico)

    2016-09-15

    The present work deals with the methodology established for the quantification of {sup 232}Th, {sup 234}U, {sup 238}U and {sup 235}U in the shell of gastropod mollusks collected in the rivers Valles, Coy and Axtla of San Luis Potosi, Mexico, which belong to the Panuco River basin; these rivers have as main source of pollution the discharge of municipal sewage, waste from small industries, agricultural and cattle residues and from natural sources. Conventional methods for measuring radio-nuclides are confronted with certain conditions related to the requirement in measurement, basically in the characterization that is related to the concepts of precision and accuracy. The analysis of the gastropod mollusk shell was performed by the Icp-SFMS technique; the main advantages of this technique lie in the isotope quantification capacity, the high precision and the low limits of detection, in this study are very important because these elements are in concentrations between ppb and ppt. This technique allowed the analysis of the samples having a complex matrix by the presence CaCO{sub 3} minimizing the interferences thanks to the ionization efficiency of the Ar plasma. For the species Pachychilus monachus were found concentrations of {sup 232}Th of 0.16-5.37 μg/g and of total U of 0.101-4.081 μg/g being this species where the highest values of total U were found. For Thiara (melanoids) tuberculata the lowest values were found among the different species ({sup 232}Th 0.61-3.61 μg/g and total U 0.006-0.042 μg/g), for Pachychilus suturalis, values of {sup 232}Th of 0.58-6.4 μg/g and for Pachychilus sp. were found between 0.26-7.62 μg/g and for total U values between 0.28-3.33 μg/g. The method offers several advantages: speed, good precision, low values of quantification limits and high sensitivity in the measurement of radio-nuclides and heavy metals. (Author)

  20. Production of iridium-192 radiation sources: Indian Experience

    International Nuclear Information System (INIS)

    Sastry, K.V.S.; Kolhe, O.T.; Nagarja, P.S.; Paramr, Y.D.

    2002-01-01

    Board of Radiation and Isotope Technology (BRIT), a unit under the Department of Atomic Energy is fabricating and supplying Ir-192 industrial radiography sources for various models of radiography cameras for use in the industry for non-destructive testing. Basically these sources are fabricated by encapsulating the required quantity of the activity in stainless steel 316 L capsules using Tungsten Inert gas welding process and crimping/attaching to the respective pigtail assemblies of the radiography cameras. The inactive iridium pellets are irradiated in the DHRUVA reactor at a flux on 1.8 X 10 14 n/cm 2 /sec. The performance classification of these source encapsulation for various conditions of normal and accidental nature are tested by subjecting the prototype sources as per the standard laid down by the regulatory authority, Atomic Energy Regulatory Board, in India. The sources are fabricated as per the national and international standards. Activity of the sources varies from 37O GBq (10 Ci ) to 2.96 TBq (80 Ci ) source strength depending on the requirement of the user. The specific activity of the Ir-192 sources supplied is around 7.4 TBq/gm (200 Ci/gm ). Quality control /Assurance for the manufacture of the source begins from the procurement of the raw material and ends with the finished source. Ir- 192 in the form of -0.3 mm diameter (0.1 mm dia wire of Ir-25 % and Pt-75% sheathed in pure platinum of 0.1 mm thick) is being supplied for use in the treatment of cancer of cervix, tongue etc. by brachytherapy. This is supplied in lengths of 50 cm / 100 cm with 37 - 185 GBq/cm ( 1-5 mCi/cm) activity. Annually 925 TBq (25 kCi) of Ir-192 for industrial radiography and about 60 meters of wire for brachytherapy are being fabricated and supplied. Because of the quality of these sources BRIT not only caters to the Indian industry but also is able to export sources to the third world countries. (Author)

  1. Experience with qualification examinations of workers handling ionizing radiation sources

    International Nuclear Information System (INIS)

    Skokanova, K.

    1976-01-01

    The organization is described of examinations which have to be passed by supervising staff and workers using radioactive ionizing radiation sources. The requirements are listed of the examination in which these workers have to prove their professional knowledge and skills. The said examinations significantly contribute to the establishment of a system of safeguards at workplaces using ionizing radiation sources and may help economize operations at these workplaces

  2. Management of Spent and Disused Radiation Sources - The Zambian Experience

    International Nuclear Information System (INIS)

    Chabala, F.

    2002-01-01

    Zambia like all other countries in the world is faced with environmental problems brought about by a variety of human activities. In Zambia the major environmental issues as identified by Nation Environmental Action Plan (NEAP) of 1994 are water pollution, poor sanitation, land degradation, air pollution, poor waste management, misuse of chemicals, wildlife depletion and deforestation. Zambian has been using a lot of radioactive materials in its various industries. The country has taken several projects with help of external partners. These partners however left these projects in the hands of the Zambians without developing their capacities to manage these radioactive sources. The Government recognized the need to manage these sources and passed legislation governing the management of radioactive materials. The first act of Parliament on Radiation Protection work was passed in 1975 to legislate the use of ionizing radiation. However, because of financial constraints the Country is facing, these regulations have remained unimplemented. Fortunately the international Community has been working in partnership with the Zambian Government in the Management of Radioactive Material. Therefore this paper will present the following aspects of radioactive waste management in Zambia: review Existing Legislation in Zambia regarding management of spent/radioactive sources; capacity building in the field of management of radioactive waste; management of spent and disused radiation sources; existing disposal systems in Zambia regarding spent/orphaned sources; existing stocks of radioactive sources in the Zambian industries

  3. Metal RIE 2: Unaxis SHUTTLELINE ICP

    Data.gov (United States)

    Federal Laboratory Consortium — Description:CORAL Name: Unaxis ICP EtcherChlorine-based system utilizing Boron Trichloride and Chlorine to etch metals and III-V group materials on planar substrates...

  4. The Design of a Fire Source in Scale-Model Experiments with Smoke Ventilation

    DEFF Research Database (Denmark)

    Nielsen, Peter Vilhelm; Brohus, Henrik; la Cour-Harbo, H.

    2004-01-01

    The paper describes the design of a fire and a smoke source for scale-model experiments with smoke ventilation. It is only possible to work with scale-model experiments where the Reynolds number is reduced compared to full scale, and it is demonstrated that special attention to the fire source...... (heat and smoke source) may improve the possibility of obtaining Reynolds number independent solutions with a fully developed flow. The paper shows scale-model experiments for the Ofenegg tunnel case. Design of a fire source for experiments with smoke ventilation in a large room and smoke movement...

  5. Strengthening the control on radioactive sources - Cernavoda NPP operating experience

    International Nuclear Information System (INIS)

    Daian, I.; Simionov, V.

    2005-01-01

    This paper presents the national legal frame governing the radioactive source management, legislative requirements introduced during last years and current status of controlled radioactive sources program at Cernavoda NPP. Romania has only one nuclear power plant, Cernavoda NPP, equipped with five PHWR - CANDU-6 Canadian type reactors - with a 700 MW(e) gross capacity each, in different implementation stages. The legal representative of the nuclear power production sector in Romania is 'Nuclearelectrica' S.A. National Company (SNN). SNN is a governmental company controlled by the Ministry of Industry and Trade. The company has headquarters in Bucharest and three subsidiaries: - CNE-PROD Cernavoda (CNE-PROD), operating the Cernavoda NPP - Unit 1; - CNE-INVEST Cernavoda, in charge with the completion of Unit 2 and with the preservation of Units 3,4,5; - Nuclear Fuel Plant in Pitesti (FCN). Unit 1 is in commercial operation since December 2, 1996, Unit 2 is under construction (80% completed) and Units 3, 4, 5 are under preservation. The operation of Cernavoda NPP implies use of radioactive sources that may present a significant risk to health, property and the environment when control is lost. Within the last years CNCAN issued new regulations stating clear responsibilities for the different institutions involved in radioactive materials control programs. To manage radioactive sources in a safe way CNE-PROD established and revised the Controlled Radioactive Sources Program, as part of Station Radiation Protection Regulation, ensuring strict recording of the radioactive sources and their usage, ensuring physical and radiological security, protecting the personnel, members of the public and the environment from the hazards of ionizing radiation during the life cycle of the plant, including decommissioning. (authors)

  6. Strengthening the control on radioactive sources - Cernavoda NPP operating experience

    International Nuclear Information System (INIS)

    Daian, I.; Simionov, V.

    2005-01-01

    Full text: This paper presents the national legal frame governing the radioactive source management, legislative requirements introduced during last years and current status of controlled radioactive sources program at Cernavoda NPP. Romania has only one nuclear power plant, Cernavoda NPP, equipped with five PHWR - CANDU-6 Canadian type reactors - with a 700 MW(e) gross capacity each, in different implementation stages. The legal representative of the nuclear power production sector in Romania is 'Nuclearelectrica' S.A. National Company (SNN). SNN is a governmental company controlled by the Ministry of Industry and Trade. The company has headquarters in Bucharest and three subsidiaries: - CNE-PROD Cernavoda (CNE-PROD), operating the Cernavoda NPP - Unit 1; - CNE-INVEST Cernavoda, in charge with the completion of Unit 2 and with the preservation of Units 3,4,5; - Nuclear Fuel Plant in Pitesti (FCN). Unit 1 is in commercial operation since December 2, 1996, Unit 2 is under construction (80% completed) and Units 3, 4, 5 are under preservation. The operation of Cernavoda NPP implies use of radioactive sources that may present a significant risk to health, property and the environment when control is lost. Within the last years CNCAN issued new regulations stating clear responsibilities for the different institutions involved in radioactive materials control programs. To manage radioactive sources in a safe way CNE-PROD established and revised the Controlled Radioactive Sources Program, as part of Station Radiation Protection Regulation, ensuring strict recording of the radioactive sources and their usage, ensuring physical and radiological security, protecting the personnel, members of the public and the environment from the hazards of ionizing radiation during the life cycle of the plant. (authors)

  7. Comparative study for toxic elements determination in air particulate reference material by INAA, CCT-ICP-MS, and ICP-MS

    International Nuclear Information System (INIS)

    Lim, J.M.; Lee, J.H.; Kim, K.H.; Moon, J.H.; Chung, Y.S.

    2005-01-01

    Although toxic elements are minor components in the atmospheric environment, they play a significant role as important marker for atmospheric science such as risk assessment, long-range transfer study, and source apportionment. Therefore, the techniques, which allow accurate and fast elemental analysis with a minimum pre-treatment, are very important. INAA has a main advantage of non-destruction of air particulate samples, while inductively Coupled plasma with mass spectrometry (ICP-MS) encounters the most significant difficulties in pre-treatment (digestion, fusion, and dilution) and polyatomic spectral interferences for interest toxic elements, Although INAA is still reference method, a number of factors (disadvantages of cost, complexity of the instruments, and scarcity of nuclear reactor) limit its applications. To date, the use of collision cell technology ICP-MS (CCT-ICP-MS) is recommended instead of typical ICP-MS for the analysis of the toxic elements; this is because CCT-ICP-MS technique prevents polyatomic spectral interferences despite of contamination and volatile effects. In this study, a number of toxic elements in reference material, NIST SRM 2783 (air particulate on filter media) were determined by INAA, CCT-ICP-MS, and ICP-MS. For both ICP methods, the filters were decomposed by microwave digestion with 5mL nitric acid. The analytical results by three methods were compared with certificated data; the INAA results showed the most accurate and precise data sets for all target elements among three methods. In detail, the deviation between analytical results and SRM's by INAA fell below 10% for all elements excluding As (14%), while those by CCT-ICP-MS were about 20%. For ICP-MS, the result does not agree with certificated data for several elements, because polyatomic spectral interference (due to 40 Ar 35 Cl, 40 Ar 23 Na, and 35 Cl 16 O) generate positive error of analytical result for As, Cu, and V. Based on our result, INAA is still one of the most

  8. Study on the RF power necessary to ignite plasma for the ICP test facility at HUST

    Energy Technology Data Exchange (ETDEWEB)

    Yue, Haikun [School of Electronic Information and Communications, Huazhong University of Science and Technology, Wuhan (China); State Key Laboratory of Advanced Electromagnetic Engineering and Technology, Huazhong University of Science and Technology, Wuhan (China); Li, Dong; Wang, Chenre; Li, Xiaofei; Chen, Dezhi; Liu, Kaifeng; Zhou, Chi; Pan, Ruimin [State Key Laboratory of Advanced Electromagnetic Engineering and Technology, Huazhong University of Science and Technology, Wuhan (China)

    2015-10-15

    An Radio-Frequency (RF) Inductively Coupled Plasma (ICP) ion source test facility has been successfully developed at Huazhong University of Science and Technology (HUST). As part of a study on hydrogen plasma, the influence of three main operation parameters on the RF power necessary to ignite plasma was investigated. At 6 Pa, the RF power necessary to ignite plasma influenced little by the filament heating current from 5 A to 9 A. The RF power necessary to ignite plasma increased rapidly with the operation pressure decreasing from 8 Pa to 4 Pa. The RF power necessary to ignite plasma decreased with the number of coil turns from 6 to 10. During the experiments, plasma was produced with the electron density of the order of 10{sup 16}m{sup -3} and the electron temperature of around 4 eV. (copyright 2015 WILEY-VCH Verlag GmbH and Co. KGaA, Weinheim)

  9. Blending in gravitational microlensing experiments : source confusion and related systematics

    NARCIS (Netherlands)

    Smith, Martin C.; Wozniak, Przemyslaw; Mao, Shude; Sumi, Takahiro

    2007-01-01

    Gravitational microlensing surveys target very dense stellar fields in the local group. As a consequence, the microlensed source stars are often blended with nearby unresolved stars. The presence of 'blending' is a cause of major uncertainty when determining the lensing properties of events towards

  10. Students' Source Misuse in Language Classrooms: Sharing Experiences

    Science.gov (United States)

    Fazel, Ismaeil; Kowkabi, Nasrin

    2013-01-01

    In this article we first provide a brief discussion of what is generally referred to as "student plagiarism," which we prefer to call "source misuse" or "inappropriate textual borrowing," and then provide some of the factors that may contribute to this problem in language classes. Moreover, we provide our views and…

  11. The Relationships among Sources of Teacher Pedagogical Beliefs, Teaching Experiences, and Student Outcomes

    Directory of Open Access Journals (Sweden)

    Morteza Mellati

    2015-03-01

    Full Text Available Teachers’ beliefs are derived from various sources such as experiences and personality (Kennedy, 1997; Donaghue, 2003; Ellis, 2008, childhood learning experiences (Rokeach, 1968, teaching experiences (Zeichner and Tabachnick, 1981, and folk pedagogy (Bruner, 1996. The relationship of these sources and learners’ outcomes are under question; therefore, this study investigated the relationships among sources of teacher pedagogical beliefs, teaching experiences, and student outcomes. The researchers classified these sources into two categories “Experienced Pedagogical Beliefs” and “Educational Pedagogical Beliefs”. To conduct this study, 150 Iranian ELT instructors had been chosen randomly. Their students’ scores were also used in data analysis. A beliefs’ questionnaire and interview were employed to elicit instructors’ sources of pedagogical beliefs. The results suggested that a significant proportion of the total variations in learners’ outcomes were predicted by teachers’ sources of pedagogical beliefs and teachers’ teaching experiences. The implications for improving the quality of teacher education programs were also discussed.

  12. Crustal melting and recycling: geochronology and sources of Variscan syn-kinematic anatectic granitoids of the Tormes Dome (Central Iberian Zone). A U-Pb LA-ICP-MS study

    Science.gov (United States)

    López-Moro, F. J.; López-Plaza, M.; Gutiérrez-Alonso, G.; Fernández-Suárez, J.; López-Carmona, A.; Hofmann, M.; Romer, R. L.

    2018-04-01

    In this study, we report U-Pb Laser Ablation ICP-MS zircon and ID-TIMS monazite ages for peraluminous granitoid plutons (biotite ± muscovite ± cordierite ± sillimanite) in the Tormes Dome, one of the gneiss-cored domes located in the Central Iberian Zone of the Variscan belt of northern Spain. Textural domains in zircon, interpreted to represent the magmatic crystallization of the granitoids (and one monazite fraction in the Ledesma pluton) yielded ages around 320 Ma, in agreement with other geochronological studies in the region. This age is interpreted to date the timing of decompression crustal melting driven by the extensional collapse of the orogenic belt in this domain of the Variscan chain of western Europe. In addition, there are several populations of inherited (xenocrystic) zircon: (1) Carboniferous zircon crystals (ca. 345 Ma) as well as one of the monazite fractions in the coarse-grained facies of the Ledesma pluton that also yielded an age of ca. 343 Ma. (2) Devonian-Silurian zircon xenocrysts with scattered ages between ca. 390 and 432 Ma. (3) Middle Cambrian-Ordovician (ca. 450-511 Ma). (4) Ediacaran-Cryogenian zircon ages (ca. 540-840 Ma). (5) Mesoproterozoic to Archaean zircon (900-2700 Ma). The abundance of Carboniferous-inherited zircon shows that crustal recycling/cannibalization may often happen at a fast pace in orogenic scenarios with only short lapses of quiescence. In our case study, it seems plausible that a "crustal layer" of ca. 340 Ma granitoids/migmatites was recycled, partially or totally, only 15-20 My after its emplacement.

  13. Development of a helicon ion source: Simulations and preliminary experiments

    Science.gov (United States)

    Afsharmanesh, M.; Habibi, M.

    2018-03-01

    In the present context, the extraction system of a helicon ion source has been simulated and constructed. Results of the ion source commissioning at up to 20 kV are presented as well as simulations of an ion beam extraction system. Argon current of more than 200 μA at up to 20 kV is extracted and is characterized with a Faraday cup and beam profile monitoring grid. By changing different ion source parameters such as RF power, extraction voltage, and working pressure, an ion beam with current distribution exhibiting a central core has been detected. Jump transition of ion beam current emerges at the RF power near to 700 W, which reveals that the helicon mode excitation has reached this power. Furthermore, measuring the emission line intensity of Ar ii at 434.8 nm is the other way we have used for demonstrating the mode transition from inductively coupled plasma to helicon. Due to asymmetrical longitudinal power absorption of a half-helix helicon antenna, it is used for the ion source development. The modeling of the plasma part of the ion source has been carried out using a code, HELIC. Simulations are carried out by taking into account a Gaussian radial plasma density profile and for plasma densities in range of 1018-1019 m-3. Power absorption spectrum and the excited helicon mode number are obtained. Longitudinal RF power absorption for two different antenna positions is compared. Our results indicate that positioning the antenna near to the plasma electrode is desirable for the ion beam extraction. The simulation of the extraction system was performed with the ion optical code IBSimu, making it the first helicon ion source extraction designed with the code. Ion beam emittance and Twiss parameters of the ellipse emittance are calculated at different iterations and mesh sizes, and the best values of the mesh size and iteration number have been obtained for the calculations. The simulated ion beam extraction system has been evaluated using optimized parameters such

  14. Tritium source-related systematic uncertainties of the KATRIN experiment

    Energy Technology Data Exchange (ETDEWEB)

    Seitz-Moskaliuk, Hendrik [Karlsruher Institut fuer Technologie, Institut fuer experimentelle Kernphysik, Hermann-von-Helmholtz-Platz 1, 76344 Eggenstein-Leopoldshafen (Germany); Collaboration: KATRIN-Collaboration

    2016-07-01

    KATRIN will perform a direct, kinematics-based measurement of the neutrino mass with a sensitivity of 200 meV (90 % C. L.) reached after 3 years of measurement time. The neutrino mass is obtained by determining the shape of the spectrum of tritium β decay electrons close to the endpoint of 18.6 keV with a spectrometer of MAC-E filter type. To achieve the planned sensitivity, the systematic measurement uncertainties have to be carefully controlled and evaluated. Main sources of systematics are the MAC-E filter on the one hand and the source and transport section (STS) on the other hand. Most of the operational parameters of KATRIN have to be stable at or even below the per mille level and have to meet further strict requirements. This talk reviews the KATRIN systematics with a special focus on the STS. Early commissioning measurements to determine the main systematics are introduced.

  15. Science experiments via telepresence at a synchrotron radiation source facility

    International Nuclear Information System (INIS)

    Warren, J. E.; Diakun, G.; Bushnell-Wye, G.; Fisher, S.; Thalal, A.; Helliwell, M.; Helliwell, J. R.

    2008-01-01

    The application of a turnkey communication system for telepresence at station 9.8 of the Synchrotron Radiation Source, Daresbury, is described and demonstrated, including its use for inter-continental classroom instruction and user training. Station 9.8 is one of the most oversubscribed and high-throughput stations at the Synchrotron Radiation Source, Daresbury, whereby awarded experimental time is limited, data collections last normally no longer than an hour, user changeover is normally every 24 h, and familiarity with the station systems can be low. Therefore time lost owing to technical failures on the station has a dramatic impact on productivity. To provide 24 h support, the application of a turnkey communication system has been implemented, and is described along with additional applications including its use for inter-continental classroom instruction, user training and remote participation

  16. Radiological Protection Experience with natural sources of radiation

    International Nuclear Information System (INIS)

    Quindos, L. S.; Fernandez, P. L.; Vinuela, J.; Arteche, J.; Sainz, G.; Gomez, J.; Matarranz

    2003-01-01

    During the last twenty five years the research Radon Group of the Medical Physics Unit of the University of Cantabria has been involved in projects concerning the measurement of natural radiation, in special that coming from radon gas. At this moment we have available for this field a lot of information in different formats, as paper, video and CD, interesting not only for public in general but also for professionals interested in the evaluation of doses coming from natural sources of radiation. (Author)

  17. Experiments with a Dudnikov-type H source

    International Nuclear Information System (INIS)

    Allison, P.W.

    1977-01-01

    Operating characteristics of the ion source described were previously reported. It uses a Penning discharge to produce H ions by the surface-plasma principles and was constructed according to the design details presented by Dudnikov. Arc power must be held relatively constant at about 50 watts to maintain stable operation, and this occurs for an indicated cathode temperature of 500 0 C. Within this limitation the source may be operated continuously at 2 mA or pulsed at over 100 mA, as measured with a Faraday cup at the exit of a 90 0 , n = 0.85, 8-cm radius focusing magnet which also provides the magnetic field for the arc region. Recent work concentrated on studying the beam-noise behavior and on measuring the emittance. Emittance was found to vary widely depending on operating conditions, but it is comparable with the values reported by Dereviankin et al for a noisy, beam extracted from their source of this design

  18. Source term experiments project (STEP): aerosol characterization system

    International Nuclear Information System (INIS)

    Schlenger, B.J.; Dunn, P.F.

    1985-01-01

    A series of four experiments is being conducted at Argonne National Laboratory's TREAT Reactor. They have been designed to provide some of the necessary data regarding magnitude and release rates of fission products from degraded fuel pins, physical and chemical characteristics of released fission products, and aerosol formation and transport phenomena. These are in-pile experiments, whereby the test fuel is heated by neutron induced fission and subsequent clad oxidation in steam environments that simulate as closely as practical predicted reactor accident conditions. The test sequences cover a range of pressure and fuel heatup rate, and include the effect of Ag/In/Cd control rod material

  19. Comparison between INAA and ICP-OES: analysis of Sudanese medicinal plants

    International Nuclear Information System (INIS)

    Sheikhaldin, Elsadig Abdelmoniem

    2014-07-01

    The aim of this study was to provide elemental concentrations in medicinal plants and mainly to compare the two different determination methods (INAA and ICP-OES after wet digestion) elemental analysis of 14 Sudanese medicinal plants was carried out using INAA and ICP-OES techniques. The selection of reported elements was done according to intersection of elements determined by both techniques. This intersecting element list contained Ca, K, Fe, Mn, Mg, Sr, Zn, Cu, Co, and Cr. INAA correlated well with ICP-OES measurements of the same plants as long as concentrations were sufficiently above LoQ. Correlation coefficients (R 2 ) in this case is close to 1. Generally, INAA results tended to be higher compared to ICP-OES. The performance and possible source of errors of both techniques was discussed also with respect to measurements of certified reference materials. INAA provided the advantage of having both, faster and non destructive sample preparation than ICP-OES. Therefore, INAA may be technique of choice for Ca, K, Zn, and Mg elements specifically when samples are needed for further investigations. Regarding the low concentrations e.g for Cr, Ni or Cu, ICP-OES is the superior technique over INAA due to the sufficiently low limits of determination and thus gaining more detectable results at low concentrations. (author)

  20. Optimisation and application of ICP-MS and alpha-spectrometry for determination of isotopic ratios of depleted uranium and plutonium in samples collected in Kosovo

    OpenAIRE

    Boulyga, S. F.; Testa, C.; Desideri, D.; Becker, J. S.

    2001-01-01

    The determination of environmental contamination with natural and artificial actinide isotopes and evaluation of their source requires precise isotopic determination of actinides, above all uranium and plutonium. This can be achieved by alpha spectrometry or by inductively coupled plasma mass spectrometry (ICP-MS) after chemical separation of actinides. The performance of a sector-field ICP-MS (ICP-SFMS) coupled to a low-flow micronebulizer with a membrane desolvation unit, "Aridus'', was stu...

  1. Source Security Program in the Philippines: a lost source search experience

    International Nuclear Information System (INIS)

    Romallosa, Kristine M.; Salabit, Maria T.; Caseria, Estrella; Valdezco, Eulinia

    2008-01-01

    The Philippine Nuclear Research Institute (PNRI), the national agency in the licensing and regulations of radioactive materials in the country, is strengthening its capabilities in the security of radioactive sources. Part of this program is the PNRI's participation in the Regional Security of Radioactive Sources (RSRS) Project of the Australian Nuclear Science and Technology Organization (ANSTO). The project has provided equipment and methods training, assistance in the development of PNRI's own training program and support for actual orphan source search activities. On May 2007, a source search for the two lost Cs-137 level gauges of a steel manufacturing company was conducted by the PNRI and ANSTO. The source search are the: a) Development of instrument and source search training for the team, the National Training Workshop on Orphan Source Searches which was organized and conducted as a result of train-the-trainors fellowship under the RSRS project; and b) Planning and implementation of the lost source search activity. The conduct of the actual search on warehouses, product yard, canals, dust storage, steel making building, scrap yards and nearby junk shops of the steel plant took one week. The week-long search did not find the lost sources. However, naturally occurring radioactive materials identified to be Thorium, were found on sands, bricks and sack piles that are stored and/or generally present in the warehouses, yard and steel making building. The search activity had therefore cleared the facility of the lost source and its corresponding hazards. The NORM found present in the plant's premises on the other hand brought the attention of the management of the needed measures to ensure safety of the staff from possible hazards of these materials. Currently, the course syllabus that was developed is continuously enhanced to accommodate the training needs of the PNRI staff particularly for the emergency response and preparedness. This component of the source

  2. Source theory analysis of electron--positron annihilation experiments

    International Nuclear Information System (INIS)

    Schwinger, J.

    1975-01-01

    The phenomenological viewpoint already applied to deep inelastic scattering is extended to the discussion of electron-positron annihilation experiments. Some heuristic arguments lead to simple forms for the pion differential cross section that are in reasonable accord with the published experimental data in the energy interval 3 to 4.8 GeV

  3. Sources of Funds for Nigerian Companies: Experience of the food ...

    African Journals Online (AJOL)

    This paper analyzes some of the experiences of operators in the Food and Beverage Industry in Nigeria. It examines the evolution of capital structure and discusses the implications for corporate performance of the observed mode of financing. LBS Management Review Vol.5(1) 2000: 33-47 ...

  4. Open Source Software Development with Your Mother Language : Intercultural Collaboration Experiment 2002

    DEFF Research Database (Denmark)

    Nomura, Saeko; Ishida, Saeko; Jensen, Mika Yasuoka

    2002-01-01

    ”Open Source Software Development with Your Mother Language: Intercultural Collaboration Experiment 2002,” 10th International Conference on Human – Computer Interaction (HCII2003), June 2003, Crete, Greece.......”Open Source Software Development with Your Mother Language: Intercultural Collaboration Experiment 2002,” 10th International Conference on Human – Computer Interaction (HCII2003), June 2003, Crete, Greece....

  5. Dual-source CT cardiac imaging: initial experience

    International Nuclear Information System (INIS)

    Johnson, Thorsten R.C.; Nikolaou, Konstantin; Wintersperger, Bernd J.; Rist, Carsten; Buhmann, Sonja; Reiser, Maximilian F.; Becker, Christoph R.; Leber, Alexander W.; Ziegler, Franz von; Knez, Andreas

    2006-01-01

    The relation of heart rate and image quality in the depiction of coronary arteries, heart valves and myocardium was assessed on a dual-source computed tomography system (DSCT). Coronary CT angiography was performed on a DSCT (Somatom Definition, Siemens) with high concentration contrast media (Iopromide, Ultravist 370, Schering) in 24 patients with heart rates between 44 and 92 beats per minute. Images were reconstructed over the whole cardiac cycle in 10% steps. Two readers independently assessed the image quality with regard to the diagnostic evaluation of right and left coronary artery, heart valves and left ventricular myocardium for the assessment of vessel wall changes, coronary stenoses, valve morphology and function and ventricular function on a three point grading scale. The image quality ratings at the optimal reconstruction interval were 1.24±0.42 for the right and 1.09±0.27 for the left coronary artery. A reconstruction of diagnostic systolic and diastolic images is possible for a wide range of heart rates, allowing also a functional evaluation of valves and myocardium. Dual-source CT offers very robust diagnostic image quality in a wide range of heart rates. The high temporal resolution now also makes a functional evaluation of the heart valves and myocardium possible. (orig.)

  6. Collision experiment on highly ionized ions using vacuum spark source

    International Nuclear Information System (INIS)

    Takagi, S.; Ohtani, S.; Kadota, K.; Fujita, J.

    1982-03-01

    Cross sections for one-electron capture by Fe 6 + in H 2 are measured below 10 keV by using a vacuum spark ion source. It is found that the cross sections show little dependence on the collision energy and this value is about 6 x 10 - 15 cm 2 . This ion source, which has no electrode for ion extraction, can produce ions from several hundreds eV to several tens of keV and the maximum charge state of 16 in Fe at 125J discharge energy. With ion selection system of 2.7 m time-of-flight and an electrostatic analyzer of 1% resolving power, 10 2 - 10 3 ions/pulse are obtained. Because of poor reproducibility of ion beam, charge-transferred ions and unreacted ions are measured simultaneously with a microchannel plate which has two anodes behind. By utilizing the feature of pulsed ion beam and this ion selection system, it is possible to obtain cross sections for various charge states of ions simultaneously. (author)

  7. Preparation of calibration materials for microanalysis of Ti minerals by direct fusion of synthetic and natural materials: experience with LA-ICP-MS analysis of some important minor and trace elements in ilmenite and rutile.

    Science.gov (United States)

    Odegård, M; Mansfeld, J; Dundas, S H

    2001-08-01

    Calibration materials for microanalysis of Ti minerals have been prepared by direct fusion of synthetic and natural materials by resistance heating in high-purity graphite electrodes. Synthetic materials were FeTiO3 and TiO2 reagents doped with minor and trace elements; CRMs for ilmenite, rutile, and a Ti-rich magnetite were used as natural materials. Problems occurred during fusion of Fe2O3-rich materials, because at atmospheric pressure Fe2O3 decomposes into Fe3O4 and O2 at 1462 degrees C. An alternative fusion technique under pressure was tested, but the resulting materials were characterized by extensive segregation and development of separate phases. Fe2O3-rich materials were therefore fused below this temperature, resulting in a form of sintering, without conversion of the materials into amorphous glasses. The fused materials were studied by optical microscopy and EPMA, and tested as calibration materials by inductively coupled plasma mass spectrometry, equipped with laser ablation for sample introduction (LA-ICP-MS). It was demonstrated that calibration curves based on materials of rutile composition, within normal analytical uncertainty, generally coincide with calibration curves based on materials of ilmenite composition. It is, therefore, concluded that LA-ICP-MS analysis of Ti minerals can with advantage be based exclusively on calibration materials prepared for rutile, thereby avoiding the special fusion problems related to oxide mixtures of ilmenite composition. It is documented that sintered materials were in good overall agreement with homogeneous glass materials, an observation that indicates that in other situations also sintered mineral concentrates might be a useful alternative for instrument calibration, e.g. as alternative to pressed powders.

  8. The COHERENT Experiment at the Spallation Neutron Source

    Energy Technology Data Exchange (ETDEWEB)

    Elliott, Steven Ray [Los Alamos National Laboratory (LANL), Los Alamos, NM (United States)

    2015-09-30

    The COHERENT collaboration's primary objective is to measure coherent elastic neutrino- nucleus scattering (CEvNS) using the unique, high-quality source of tens-of-MeV neutrinos provided by the Spallation Neutron Source (SNS) at Oak Ridge National Laboratory (ORNL). In spite of its large cross section, the CEvNS process has never been observed, due to tiny energies of the resulting nuclear recoils which are out of reach for standard neutrino detectors. The measurement of CEvNS has now become feasible, thanks to the development of ultra-sensitive technology for rare decay and weakly-interacting massive particle (dark matter) searches. The CEvNS cross section is cleanly predicted in the standard model; hence its measurement provides a standard model test. It is relevant for supernova physics and supernova-neutrino detection, and enables validation of dark-matter detector background and detector-response models. In the long term, precision measurement of CEvNS will address questions of nuclear structure. COHERENT will deploy multiple detector technologies in a phased approach: a 14-kg CsI[Na] scintillating crystal, 15 kg of p-type point-contact germanium detectors, and 100 kg of liquid xenon in a two-phase time projection chamber. Following an extensive background measurement campaign, a location in the SNS basement has proven to be neutron-quiet and suitable for deployment of the COHERENT detector suite. The simultaneous deployment of the three COHERENT detector subsystems will test the N=2 dependence of the cross section and ensure an unambiguous discovery of CEvNS. This document describes concisely the COHERENT physics motivations, sensitivity and plans for measurements at the SNS to be accomplished on a four-year timescale.

  9. Analysis of impurities in uranium oxide by ICP-MS

    International Nuclear Information System (INIS)

    Paul, M.; Hager, J.

    1989-01-01

    The method offers detection limits of less than 0.1 μg/g in solid samples and a wide linear dynamic working range and allows a fast sample throughput. The poster summarizes recent authors' experience with the analysis of high purity uranium oxide. The samples are analyzed using both conventional solution analysis and solid sampling method, using a new powerful laser sampling system attached to the ICP mass spectrometer. The total analysis time required for one uranium oxide sample is about 4 minutes including sample handling, data acquisition and processing. The results achieved from semiquantitative and quantitative analysis applying both techniques are in good agreement with the reference values. (author)

  10. Environmental application of XRF, ICP-AES and INAA on biological matrix

    International Nuclear Information System (INIS)

    Zararsiz, A.; Dogangun, A.; Tuncel, S.

    2004-01-01

    Full text: It is very important to determine trace quantities of metals in different matrices with high accuracy since the metals are used as markers for different sources in air pollution studies. In this study, the analytical capabilities of XRF, ICP-AES and INM techniques on a biological matrix namely lichens, which are widely used as bio monitoring organisms for the pollutants mapping in the atmosphere, were tested. Lichen samples were collected in Aegean Region of Turkey where pollution is an important issue. 9 elements were determined by XRF, 14 elements by ICP-AES and 13 elements by INM. Quality assurance was achieved using lichen SRM (IAEA-336) and Orchard leaves SRM (NIST- 1571). Produced data are subjected to statistical tests, like t-test, Q-test in order to determine the accuracy and precision of each technique. A recommendation list of the proper analytical technique is obtained for determination of each specific element considering analytical capabilities of ICP-AES, XRF and INM. As a result we can recommend that the first choice for Cd, Cu, Mg is ICP-AES, for In, K, Rb is INAA, for Br is XRF, if the concentrations are not close to the detection limit of XRF. For V, Cr, AI, Na, Fe ICP-AES and INM are both well, for Pb ICP-AES and XRF are both well, if the concentrations are not close to the detection limit of XRF, for Mn and Ca INM, XRF and ICP-AES are all give similar results for this type of biological matrix

  11. CLEAR: Prospects for a low threshold neutrino experiment at the Spallation Neutron Source

    International Nuclear Information System (INIS)

    Scholberg, Kate

    2008-01-01

    A low-threshold neutrino scattering experiment at a high intensity stopped-pion neutrino source has the potential to measure coherent neutral current neutrino-nucleus elastic scattering. A promising prospect for the measurement of this process is a proposed noble-liquid-based experiment, dubbed CLEAR (Coherent Low Energy A (Nuclear) Recoils), at the Spallation Neutron Source. This poster will describe the CLEAR proposal and its physics reach.

  12. Study on Huizhou architecture of point cloud registration based on optimized ICP algorithm

    Science.gov (United States)

    Zhang, Runmei; Wu, Yulu; Zhang, Guangbin; Zhou, Wei; Tao, Yuqian

    2018-03-01

    In view of the current point cloud registration software has high hardware requirements, heavy workload and moltiple interactive definition, the source of software with better processing effect is not open, a two--step registration method based on normal vector distribution feature and coarse feature based iterative closest point (ICP) algorithm is proposed in this paper. This method combines fast point feature histogram (FPFH) algorithm, define the adjacency region of point cloud and the calculation model of the distribution of normal vectors, setting up the local coordinate system for each key point, and obtaining the transformation matrix to finish rough registration, the rough registration results of two stations are accurately registered by using the ICP algorithm. Experimental results show that, compared with the traditional ICP algorithm, the method used in this paper has obvious time and precision advantages for large amount of point clouds.

  13. Some aspects of ICP-AES analysis of high purity rare earths

    International Nuclear Information System (INIS)

    Murty, P.S.; Biswas, S.S.

    1991-01-01

    Inductively coupled plasma atomic emission spectrometry (ICP-AES) is a technique capable of giving high sensitivity in trace elemental analysis. While the technique possesses high sensitivity, it lacks high selectivity. Selectivity is important where substances emitting complex spectra are to be analysed for trace elements. Rare earths emit highly complex spectra in a plasma source and the determination of adjacent rare earths in a high purity rare earth matrix, with high sensitivity, is not possible due to the inadequate selectivity of ICP-AES. One approach that has yielded reasonably good spectral selectivity in the high purity rare earth analysis by ICP-AES is by employing a combination of wavelength modulation techniques and high resolution echelle grating. However, it was found that by using a high resolution monochromator senstitivities either comparable to or better than those reported by the wavelength modulation technique could be obtained. (author). 2 refs., 2 figs., 2 tabs

  14. Estimation of metal ions during the dissolution of corrosion product oxides by ICP-AES

    International Nuclear Information System (INIS)

    Sathyaseelan, V.S.; Mittal, Vinit Kumar; Velmurugan, S.

    2012-01-01

    Inductively coupled plasma atomic emission spectroscopy (ICP-AES) is one of the several techniques, which is being widely used for both qualitative and quantitative estimation of various elements. Determination of metals in wine, arsenic in food, trace elements in soil, nutrient levels in agricultural soils, trace elements bound to protein, motor oil analysis etc. are the examples of its application. ICP-AES utilizes plasma as the atomization and excitation source. The plasma temperature in the analytical zone ranges from 5000-8000 K. This high temperature assures that most of the compounds in the samples are completely atomized. Advantages of ICP-AES are high sensitivity and linear dynamic range, multi-element capability, low chemical interference and a stable and reproducible signal. The typical limits of detection for some of the elements like Mg, Sr, Ca, Li, Cu etc are well below 1 μg L -1

  15. A qualitative exploration of the wilderness experience as a source of spiritual inspiration

    Science.gov (United States)

    Laura M. Fredrickson; Dorothy H. Anderson

    1999-01-01

    On-site observations, personal field journals, and in-depth interviews were used to examine qualitative aspects of the wilderness experience as a source of spiritual inspiration. Two groups of women kept personal journal accounts of their daily 'lived-experience' during one of two outdoor recreation trips; five participants went to the Boundary Waters Canoe...

  16. psiTurk: An open-source framework for conducting replicable behavioral experiments online.

    Science.gov (United States)

    Gureckis, Todd M; Martin, Jay; McDonnell, John; Rich, Alexander S; Markant, Doug; Coenen, Anna; Halpern, David; Hamrick, Jessica B; Chan, Patricia

    2016-09-01

    Online data collection has begun to revolutionize the behavioral sciences. However, conducting carefully controlled behavioral experiments online introduces a number of new of technical and scientific challenges. The project described in this paper, psiTurk, is an open-source platform which helps researchers develop experiment designs which can be conducted over the Internet. The tool primarily interfaces with Amazon's Mechanical Turk, a popular crowd-sourcing labor market. This paper describes the basic architecture of the system and introduces new users to the overall goals. psiTurk aims to reduce the technical hurdles for researchers developing online experiments while improving the transparency and collaborative nature of the behavioral sciences.

  17. Breaking through the uncertainty ceiling in LA-ICP-MS U-Pb geochronology

    Science.gov (United States)

    Horstwood, M.

    2016-12-01

    Sources of systematic uncertainty associated with session-to-session bias are the dominant contributor to the 2% (2s) uncertainty ceiling that currently limits the accuracy of LA-ICP-MS U-Pb geochronology. Sources include differential downhole fractionation (LIEF), `matrix effects' and ablation volume differences, which result in irreproducibility of the same reference material across sessions. Current mitigation methods include correcting for LIEF mathematically, using matrix-matched reference materials, annealing material to reduce or eliminate radiation damage effects and tuning for robust plasma conditions. Reducing the depth and volume of ablation can also mitigate these problems and should contribute to the reduction of the uncertainty ceiling. Reducing analysed volume leads to increased detection efficiency, reduced matrix-effects, eliminates LIEF, obviates ablation rate differences and reduces the likelihood of intercepting complex growth zones with depth, thereby apparently improving material homogeneity. High detection efficiencies (% level) and low sampling volumes (20um box, 1-2um deep) can now be achieved using MC-ICP-MS such that low volume ablations should be considered part of the toolbox of methods targeted at improving the reproducibility of LA-ICP-MS U-Pb geochronology. In combination with other strategies these improvements should be feasible on any ICP platform. However, reducing the volume of analysis reduces detected counts and requires a change of analytical approach in order to mitigate this. Appropriate strategies may include the use of high efficiency cell and torch technologies and the optimisation of acquisition protocols and data handling techniques such as condensing signal peaks, using log ratios and total signal integration. The tools required to break the 2% (2s) uncertainty ceiling in LA-ICP-MS U-Pb geochronology are likely now known but require a coherent strategy and change of approach to combine their implementation and realise

  18. Note: A versatile radio-frequency source for cold atom experiments

    Energy Technology Data Exchange (ETDEWEB)

    Li, Na; Wu, Yu-Ping; Min, Hao; Yang, Tao; Jiang, Xiao, E-mail: jiangx@ustc.edu.cn [Hefei National Laboratory for Physical Sciences at Microscale and Department of Modern Physics, University of Science and Technology of China, Hefei, Anhui 230026 (China); CAS Center for Excellence and Synergetic Innovation Center in Quantum Information and Quantum Physics, University of Science and Technology of China, Hefei, Anhui 230026 (China)

    2016-08-15

    A radio-frequency (RF) source designed for cold atom experiments is presented. The source uses AD9858, a direct digital synthesizer, to generate the sine wave directly, up to 400 MHz, with sub-Hz resolution. An amplitude control circuit consisting of wideband variable gain amplifier and high speed digital to analog converter is integrated into the source, capable of 70 dB off isolation and 4 ns on-off keying. A field programmable gate array is used to implement a versatile frequency and amplitude co-sweep logic. Owing to modular design, the RF sources have been used on many cold atom experiments to generate various complicated RF sequences, enriching the operation schemes of cold atoms, which cannot be done by standard RF source instruments.

  19. Quantification of pharmaceutical peptides in human plasma by LC-ICP-MS sulfur detection

    DEFF Research Database (Denmark)

    Møller, Laura Hyrup; Macherius, André; Hansen, Thomas Hesselhøj

    2016-01-01

    A method for quantification of a pharmaceutical peptide in human plasma was developed using gradient elution LC-ICP-MS. A membrane desolvation (MD) system was applied to remove organic solvents from the eluent prior to the detection as SO+ in the dynamic reaction cell (DRC) of the ICP-DRC-MS inst......A method for quantification of a pharmaceutical peptide in human plasma was developed using gradient elution LC-ICP-MS. A membrane desolvation (MD) system was applied to remove organic solvents from the eluent prior to the detection as SO+ in the dynamic reaction cell (DRC) of the ICP......-DRC-MS instrument and subsequent quantification by post-column isotope dilution (IDA). Plasma proteins were precipitated prior to analysis. Analytical figures of merit including linearity, precision, LOD, LOQ and accuracy were considered satisfactory for analysis of plasma samples. The selectivity of the developed...... method was demonstrated for five pharmaceutically relevant peptides: desmopressin, penetratin, substance P, PTH (1-34) and insulin. Preliminary experiments on an ICP-MS/MS system using oxygen to reduce the effect of organic solvents were also performed to compare sensitivity. The results of the study...

  20. Analytical applications of ICP-FTS

    International Nuclear Information System (INIS)

    Faires, L.M.; Palmer, B.A.; Cunningham, P.T.

    1986-01-01

    The Analytical Chemistry Group of the Chemistry Division at Los Alamos National Laboratory has been investigating the analytical utility of the inductively coupled plasma (ICP) - Fourier transform spectrometer (FTS) combination. While a new state-of-the-art FTS facility is under construction at Los Alamos, preliminary data has been obtained on the one-meter FTS at the National Solar Observatory at Kitt Peak, Arizona. This paper presents an update of the Los Alamos FTS facility, which is expected to be completed in 1986, and presents data showing the analytical potential of an ICP-FTS system. Some of the potential problems of the multiplex disadvantage are discussed, and the advantages of the high resolution obtainable with the FTS are illustrated

  1. Enhanced ICP for the Registration of Large-Scale 3D Environment Models: An Experimental Study

    Directory of Open Access Journals (Sweden)

    Jianda Han

    2016-02-01

    Full Text Available One of the main applications of mobile robots is the large-scale perception of the outdoor environment. One of the main challenges of this application is fusing environmental data obtained by multiple robots, especially heterogeneous robots. This paper proposes an enhanced iterative closest point (ICP method for the fast and accurate registration of 3D environmental models. First, a hierarchical searching scheme is combined with the octree-based ICP algorithm. Second, an early-warning mechanism is used to perceive the local minimum problem. Third, a heuristic escape scheme based on sampled potential transformation vectors is used to avoid local minima and achieve optimal registration. Experiments involving one unmanned aerial vehicle and one unmanned surface vehicle were conducted to verify the proposed technique. The experimental results were compared with those of normal ICP registration algorithms to demonstrate the superior performance of the proposed method.

  2. Initial operating experience and recent development on the TRIUMF optically pumped polarized H- ion source

    International Nuclear Information System (INIS)

    Schmor, P.W.; Law, W.M.; Levy, C.D.P.; McDonald, M.

    1988-01-01

    A polarized H - ion source using optical pumping techniques has been developed at TRIUMF. This source was used to demonstrate (on an ion source test stand) the feasibility of producing 10- μA of ∼ 60% polarized H - ion beam in a dc mode suitable for injection into the TRIUMF cyclotron. The source has been installed in a 300 kV high voltage terminal connected to the cyclotron via a recently constructed beam transport line. A polarization of 80% is anticipated near the end of 1988 after the installation of a superconducting solenoid to the source. In this paper the authors describe the initial operating experience, recent developments, and the future plans for the TRIUMF optically pumped polarized ion source

  3. Dosimetry experience of 192IR sources used In HDR brachytherapy for cervical cancer

    International Nuclear Information System (INIS)

    Daci, Lulzime; Myrku, Rodina Cela

    2013-01-01

    planning system and afterloading units for all sources was done and was correctly calculated. A verification with other chambers has been done and also has given very good results. An IAEA external audit has acknowledged the good experience. (Author)

  4. Analysis of I-Br-Cl in single fluid inclusions by LA-ICP-MS

    Science.gov (United States)

    Giehl, C.; Fusswinkel, T.; Beermann, O.; Garbe-Schönberg, D.; Scholten, L.; Wagner, T.

    2017-12-01

    Halogens are excellent tracers of hydrothermal fluid sources and in-situ LA-ICP-MS analysis of Cl and Br in single fluid inclusions has provided fundamentally new insight into hydrothermal fluid flow and ore formation. There is mounting evidence that enrichment and depletion of Br relative to Cl may be caused by a number of processes beyond seawater evaporation and halite dissolution which cannot be discriminated on the basis of Br/Cl ratios alone. Expanding the analytical capabilities of fluid inclusion LA-ICP-MS analysis to include iodine would allow to discern between selective and coupled enrichment processes of Cl, Br and I, even in geologically complex samples that are inaccessible to bulk extraction techniques. We present iodine concentration data determined by LA-ICP-MS analysis of synthetic fluid inclusions, using the Sca17 scapolite reference material for external standardization (Seo et al., 2011). Iodine concentrations in Sca17 were determined using the Durango apatite standard. Four starting solutions containing I (0.3, 1.5, 27, 78 µg/g), Br (941, 1403, 2868, 4275 µg/g), Na (30.7, 94.7 mg/g), and Cl (50, 137 mg/g) (analyzed by ICP-OES and ICP-MS at CAU Kiel) were prepared by dissolving reagent grade chemical powders in ultra-pure water. Spherical inclusions (up to 40 µm) were synthesized from the starting solutions in pre-cracked, HF-treated synthetic quartz crystals which were placed in gold capsules and equilibrated at 600°C, 100/200 MPa in cold seal pressure vessels. Fluid inclusion LA-ICP-MS analysis (University of Helsinki) yielded average I concentrations in excellent agreement with the starting solutions (27.3 µg/g ± 14 %RSD for the 27 µg/g solution and 77.6 µg/g ± 8.3 %RSD for the 78 µg/g solution). Average Br and I concentrations deviate less than 10 % from solution concentration values. For the low I concentration solutions, the synthetic inclusions were too small to detect I. Thus, given suitable standard materials and sufficient

  5. Li+ alumino-silicate ion source development for the Neutralized Drift Compression Experiment (NDCX)

    Energy Technology Data Exchange (ETDEWEB)

    Roy, Prabir K.; Greenway, Wayne G.; Kwan, Joe W.; Seidl, Peter A.; Waldron, William L.; Wu, James K.

    2010-10-01

    We report results on lithium alumino-silicate ion source development in preparation for warmdense-matter heating experiments on the new Neutralized Drift Compression Experiment (NDCXII). The practical limit to the current density for a lithium alumino-silicate source is determined by the maximum operating temperature that the ion source can withstand before running into problems of heat transfer, melting of the alumino-silicate material, and emission lifetime. Using small prototype emitters, at a temperature of ~;;1275 oC, a space-charge-limited Li+ beam current density of J ~;;1 mA/cm2 was obtained. The lifetime of the ion source was ~;;50 hours while pulsing at a rate of 0.033 Hz with a pulse duration of 5-6 mu s.

  6. Li+ alumino-silicate ion source development for the Neutralized Drift Compression Experiment (NDCX)

    International Nuclear Information System (INIS)

    Roy, Prabir K.; Greenway, Wayne G.; Kwan, Joe W.; Seidl, Peter A.; Waldron, William L.; Wu, James K.

    2010-01-01

    We report results on lithium alumino-silicate ion source development in preparation for warm-dense-matter heating experiments on the new Neutralized Drift Compression Experiment (NDCX-II). The practical limit to the current density for a lithium alumino-silicate source is determined by the maximum operating temperature that the ion source can withstand before running into problems of heat transfer, melting of the alumino-silicate material, and emission lifetime. Using small prototype emitters, at a temperature of ∼1275 C, a space-charge-limited Li + beam current density of J ∼1 mA/cm 2 was obtained. The lifetime of the ion source was ∼50 hours while pulsing at a rate of 0.033 Hz with a pulse duration of 5-6 (micro) s.

  7. ICP-AES method for metals in air. Pt 2 - analysis; final report on project R48113

    International Nuclear Information System (INIS)

    Taylor, C.; Howe, A.

    2002-04-01

    An ICP-AES instrument operating procedure has been drafted and incorporated in ISO 15202-3 Workplace air - Determination of metals and metalloids in airborne particulate matter by inductively coupled plasma atomic emission spectrometry: Part 3 - Analysis. It is expected that this International Standard will be published during 2003. The performance of the analytical method described ISO 15202-3 was evaluated by carrying out laboratory experiments to determine analytical precision. The uncertainty associated with analytical variability was then combined with other sources of uncertainty arising from the sampling method described in ISO 15202-1. A first draft of a proposed new MDHS on Metals and metalloids in workplace air by Inductively Coupled Plasma Atomic Emission Spectrometry has been prepared based on ISO 15202-1, ISO 15202-2 and ISO 15202-3. It is expected that this will be published in late 2002 or early 2003

  8. Determination of rare earth elements in red mud by ICP-MS

    International Nuclear Information System (INIS)

    Kumar, Sanjukta A.; Suvarna, S.; Kiran Kumar, G.

    2017-01-01

    Red mud or red sludge is a highly alkaline waste product composed mainly of iron oxide that is generated in the industrial production of aluminum from bauxite. With about 77 million tons of this hazardous material being produced annually, red mud poses a serious disposal problem in the mining industry. Discharge of red mud is hazardous environmentally because of its alkalinity. Many studies have been conducted to develop uses of red mud. An estimated 2 to 3 million tones are used annually in the production of cement, road construction and as a source for iron. Potential applications include the production of low cost concrete, application to sandy soils to improve phosphorus cycling, amelioration of soil acidity, landfill capping and carbon sequestration. Red mud contains a large amount of iron along with appreciable concentrations of many strategic elements such as rare earth elements and therefore can be a source of valuable secondary raw material. This necessitates the elemental characterization of red mud. This paper presents an effective dissolution procedure using a mixture of phosphoric acid and nitric acid for red mud followed by determination of rare earth elements by ICP-MS. The method was validated by spike recovery experiments. The recoveries were found within 98 to 102 %. The relative standard deviation (RSD) of the method was found to be within 5 %

  9. Operating experience of upgraded radio frequency source at 76 MHz coupled to heavy ion RFQ

    International Nuclear Information System (INIS)

    Pande, Manjiri; Shiju, A.; Patel, N.R.; Shrotriya, S.D.; Bhagwat, P.V.

    2015-01-01

    A heavy ion radio frequency quadrupole (RFQ) accelerator has been developed at BARC (BARC). A RF source which was designed and developed at 76 MHz earlier, has been upgraded and coupled to heavy ion RFQ successfully. The DC bias supplies of this source have been replaced with new supplies having high efficiency and well filteration against RF interference (RFI). The driver of main power amplifier has been replaced with indigenously designed and developed unit. The earlier introduced microcontroller based interlock experienced RF noise issues. So, this circuit has been modified with the new circuit. With these modifications, the performance of the RF source was improved. Additionally, a separate low power RF source of around 100 + Watt was designed, developed and integrated with RFQ for its RF conditioning. This paper describes the details of up gradation of technologies implemented and coupling experience of this RF source with heavy ion RFQ. (author)

  10. The calculation and experiment verification of geometry factors of disk sources and detectors

    International Nuclear Information System (INIS)

    Shi Zhixia; Minowa, Y.

    1993-01-01

    In alpha counting the efficiency of counting system is most frequently determined from the counter response to a calibrated source. Whenever this procedure is used, however, question invariably arise as to the integrity of the standard source, or indeed the validity of the primary calibration. As a check, therefore, it is often helped to be able to calculate the disintegration rate from counting rate data. The conclusion are: 1. If the source is thin enough the error E is generally less than 5%. It is acceptable in routine measurement. When the standard source lacks for experiment we can use the geometry factor calculated instead of measured efficiency. 2. The geometry factor calculated can be used to correct the counter system, study the effect of each parameters and identify those parameters needing careful control. 3. The method of overlapping area of the source and the projection of the detector is very believable, simple and convenient for calculating geometry. (5 tabs.)

  11. Data acquisition and experiment control system for high-data-rate experiments at the National Synchrotron Light Source

    International Nuclear Information System (INIS)

    Alberi, J.L.; Stubblefield, F.W.

    1981-11-01

    A data acquisition and experiment control system for experiments at the Biology Small-Angle X-ray Scattering Station at the National Synchrotron Light Source has been developed based on a multiprocessor, functionally distributed architecture. The system controls an x-ray monochromator and spectrometer and acquires data from any one of three position-sensitive x-ray detectors. The average data rate from the position-sensitive detector is approx. 10 6 events/sec. Data is stored in a one megaword histogramming memory. The experiments at this Station require that x-ray diffraction patterns be correlated with timed stimuli at the sample. Therefore, depending on which detector is in use, up to 10 3 time-correlated diffraction patterns may be held in the system memory simultaneously. The operation of the system is functionally distributed over four processors communicating via a multiport memory

  12. Advancing Explosion Source Theory through Experimentation: Results from Seismic Experiments Since the Moratorium on Nuclear Testing

    Science.gov (United States)

    Bonner, J. L.; Stump, B. W.

    2011-12-01

    On 23 September 1992, the United States conducted the nuclear explosion DIVIDER at the Nevada Test Site (NTS). It would become the last US nuclear test when a moratorium ended testing the following month. Many of the theoretical explosion seismic models used today were developed from observations of hundreds of nuclear tests at NTS and around the world. Since the moratorium, researchers have turned to chemical explosions as a possible surrogate for continued nuclear explosion research. This talk reviews experiments since the moratorium that have used chemical explosions to advance explosion source models. The 1993 Non-Proliferation Experiment examined single-point, fully contained chemical-nuclear equivalence by detonating over a kiloton of chemical explosive at NTS in close proximity to previous nuclear explosion tests. When compared with data from these nearby nuclear explosions, the regional and near-source seismic data were found to be essentially identical after accounting for different yield scaling factors for chemical and nuclear explosions. The relationship between contained chemical explosions and large production mining shots was studied at the Black Thunder coal mine in Wyoming in 1995. The research led to an improved source model for delay-fired mining explosions and a better understanding of mining explosion detection by the International Monitoring System (IMS). The effect of depth was examined in a 1997 Kazakhstan Depth of Burial experiment. Researchers used local and regional seismic observations to conclude that the dominant mechanism for enhanced regional shear waves was local Rg scattering. Travel-time calibration for the IMS was the focus of the 1999 Dead Sea Experiment where a 10-ton shot was recorded as far away as 5000 km. The Arizona Source Phenomenology Experiments provided a comparison of fully- and partially-contained chemical shots with mining explosions, thus quantifying the reduction in seismic amplitudes associated with partial

  13. Theory for beam-plasma millimeter-wave radiation source experiments

    International Nuclear Information System (INIS)

    Rosenberg, M.; Krall, N.A.

    1989-01-01

    This paper reports on theoretical studies for millimeter-wave plasma source experiments. In the device, millimeter-wave radiation is generated in a plasma-filled waveguide driven by counter-streaming electron beams. The beams excite electron plasma waves which couple to produce radiation at twice the plasma frequency. Physics topics relevant to the high electron beam current regime are discussed

  14. OpenSesame: An Open-source, Graphical Experiment Builder for the Social Sciences

    NARCIS (Netherlands)

    Mathot, S.; Schreij, D.B.B.; Theeuwes, J.

    2012-01-01

    In the present article, we introduce OpenSesame, a graphical experiment builder for the social sciences. OpenSesame is free, open-source, and cross-platform. It features a comprehensive and intuitive graphical user interface and supports Python scripting for complex tasks. Additional functionality,

  15. Open-Source Low-Cost Wireless Potentiometric Instrument for pH Determination Experiments

    Science.gov (United States)

    Jin, Hao; Qin, Yiheng; Pan, Si; Alam, Arif U.; Dong, Shurong; Ghosh, Raja; Deen, M. Jamal

    2018-01-01

    pH determination is an essential experiment in many chemistry laboratories. It requires a potentiometric instrument with extremely low input bias current to accurately measure the voltage between a pH sensing electrode and a reference electrode. In this technology report, we propose an open-source potentiometric instrument for pH determination…

  16. The Self-Taught Career Musician: Investigating Learning Sources and Experiences

    Science.gov (United States)

    Watson, Leah

    2016-01-01

    This article reports early findings from a qualitative study of 10 full-time musicians who are self-taught, to investigate their learning biographies. The aim is to identify, define and explore learning sources and experiences across the musician's learning biography. Conducted in Melbourne, Australia, the musicians were recruited through snowball…

  17. Modelling of an experiment for the study of neutron spallation source at JINR

    International Nuclear Information System (INIS)

    Kumawat, Harphool; Goyal, Uttam; Kumar, V.; Barashenkov, V.S.

    2002-01-01

    Intense neutron spallation source (INSS) is a necessary requirement of accelerator driven sub-critical systems. INSS are proposed to be generated using the high current proton beams. Some studies are conducted for the neutron flux, transmutation rates and energy gains and a larger number of related experiments are being planned

  18. ICP analysis of zinc and zamak alloys

    International Nuclear Information System (INIS)

    Gomez Coedo, A.; Dorado Lopez, M.T.

    1987-01-01

    A study was carried out on the possibilities of inductively coupled plasma emission spectrometry (ICP) in the determination of Cu, Cd, Fe, Pb, Sn, Al and Mg in zinc-base materials using direct sample solutions. A selection of analytical lines is made, on account of both their sensitivity and the corresponding study of spectral interferences; measurable minimum contents and calibrated terms are also established, to conduce therefore to a complete methodology which allows determination of the mentioned elements within the contents established on the specifications of these materials. (author)

  19. Microfabricated hollow microneedle array using ICP etcher

    Science.gov (United States)

    Ji, Jing; Tay, Francis E. H.; Miao, Jianmin

    2006-04-01

    This paper presents a developed process for fabrication of hollow silicon microneedle arrays. The inner hollow hole and the fluidic reservoir are fabricated in deep reactive ion etching. The profile of outside needles is achieved by the developed fabrication process, which combined isotropic etching and anisotropic etching with inductively coupled plasma (ICP) etcher. Using the combination of SF6/O2 isotropic etching chemistry and Bosch process, the high aspect ratio 3D and high density microneedle arrays are fabricated. The generated needle external geometry can be controlled by etching variables in the isotropic and anisotropic cases.

  20. Microfabricated hollow microneedle array using ICP etcher

    International Nuclear Information System (INIS)

    Ji Jing; Tay, Francis E H; Miao Jianmin

    2006-01-01

    This paper presents a developed process for fabrication of hollow silicon microneedle arrays. The inner hollow hole and the fluidic reservoir are fabricated in deep reactive ion etching. The profile of outside needles is achieved by the developed fabrication process, which combined isotropic etching and anisotropic etching with inductively coupled plasma (ICP) etcher. Using the combination of SF 6 /O 2 isotropic etching chemistry and Bosch process, the high aspect ratio 3D and high density microneedle arrays are fabricated. The generated needle external geometry can be controlled by etching variables in the isotropic and anisotropic cases

  1. Microfabricated hollow microneedle array using ICP etcher

    Energy Technology Data Exchange (ETDEWEB)

    Ji Jing [Mechanical Engineering National University of Singapore, 119260, Singapore (Singapore); Tay, Francis E H [Mechanical Engineering National University of Singapore, 119260, Singapore (Singapore); Miao Jianmin [MicroMachines Center, School of Mechanical and Aerospace Engineering, Nanyang Technological University, 50 Nanyang Avenue, 639798 (Singapore)

    2006-04-01

    This paper presents a developed process for fabrication of hollow silicon microneedle arrays. The inner hollow hole and the fluidic reservoir are fabricated in deep reactive ion etching. The profile of outside needles is achieved by the developed fabrication process, which combined isotropic etching and anisotropic etching with inductively coupled plasma (ICP) etcher. Using the combination of SF{sub 6}/O{sub 2} isotropic etching chemistry and Bosch process, the high aspect ratio 3D and high density microneedle arrays are fabricated. The generated needle external geometry can be controlled by etching variables in the isotropic and anisotropic cases.

  2. The Importance of a Thermal Manikin as Source and Obstacle in Full-Scale Experiments

    DEFF Research Database (Denmark)

    Nielsen, Peter V.

    The thermal manikin is normally introduced at indoor environmental measurements to obtain detailed information on thermal comfort and air quality around a person. This paper deals with the opposite situation where manikins are introduced as sources and obstacles in order to obtain reasonable...... boundary conditions in experiments with the indoor environment. In other words, how will people influence the surroundings instead of how will the surroundings influence people? The use of thermal manikins in an experiment will of course take both situations into account, however, in some experiments...

  3. THE Q/U IMAGING EXPERIMENT: POLARIZATION MEASUREMENTS OF RADIO SOURCES AT 43 AND 95 GHz

    Energy Technology Data Exchange (ETDEWEB)

    Huffenberger, K. M. [Department of Physics, Florida State University, P.O. Box 3064350, Tallahassee, FL 32306-4350 (United States); Araujo, D.; Zwart, J. T. L. [Department of Physics and Columbia Astrophysics Laboratory, Columbia University, New York, NY 10027 (United States); Bischoff, C.; Buder, I. [Kavli Institute for Cosmological Physics, Department of Physics, Enrico Fermi Institute, The University of Chicago, Chicago, IL 60637 (United States); Chinone, Y.; Hasegawa, M. [High Energy Accelerator Research Organization (KEK), 1-1 Oho, Tsukuba, Ibaraki 305-0801 (Japan); Cleary, K. [Cahill Center for Astronomy and Astrophysics, California Institute of Technology, 1200 E. California Blvd M/C 249-17, Pasadena, CA 91125 (United States); Kusaka, A. [Physics Division, Lawrence Berkeley National Laboratory, 1 Cyclotron Road, Berkeley, CA 94720 (United States); Monsalve, R. [School of Earth and Space Exploration, Arizona State University, 781 E. Terrace Road, Tempe, AZ 85287 (United States); Næss, S. K. [Department of Astrophysics, University of Oxford, Keble Road, Oxford, OX1 3RH (United Kingdom); Newburgh, L. B. [Dunlap Institute, University of Toronto, 50 St. George Street, Toronto, ON M5S 3H4 (Canada); Reeves, R. [CePIA, Departamento de Astronomía, Universidad de Concepción (Chile); Ruud, T. M.; Eriksen, H. K. [Institute of Theoretical Astrophysics, University of Oslo, P.O. Box 1029 Blindern, NO-0315 Oslo (Norway); Wehus, I. K.; Gaier, T. [Jet Propulsion Laboratory, California Institute of Technology, 4800 Oak Grove Drive, Pasadena, CA 91109 (United States); Dickinson, C. [Jodrell Bank Centre for Astrophysics, Alan Turing Building, School of Physics and Astronomy, The University of Manchester, Oxford Road, Manchester M13 9PL (United Kingdom); Gundersen, J. O., E-mail: huffenbe@physics.fsu.edu [Department of Physics, University of Miami, 1320 Campo Sano Drive, Coral Gables, FL 33146 (United States); Collaboration: QUIET Collaboration; and others

    2015-06-10

    We present polarization measurements of extragalactic radio sources observed during the cosmic microwave background polarization survey of the Q/U Imaging Experiment (QUIET), operating at 43 GHz (Q-band) and 95 GHz (W-band). We examine sources selected at 20 GHz from the public, >40 mJy catalog of the Australia Telescope (AT20G) survey. There are ∼480 such sources within QUIET’s four low-foreground survey patches, including the nearby radio galaxies Centaurus A and Pictor A. The median error on our polarized flux density measurements is 30–40 mJy per Stokes parameter. At signal-to-noise ratio > 3 significance, we detect linear polarization for seven sources in Q-band and six in W-band; only 1.3 ± 1.1 detections per frequency band are expected by chance. For sources without a detection of polarized emission, we find that half of the sources have polarization amplitudes below 90 mJy (Q-band) and 106 mJy (W-band), at 95% confidence. Finally, we compare our polarization measurements to intensity and polarization measurements of the same sources from the literature. For the four sources with WMAP and Planck intensity measurements >1 Jy, the polarization fractions are above 1% in both QUIET bands. At high significance, we compute polarization fractions as much as 10%–20% for some sources, but the effects of source variability may cut that level in half for contemporaneous comparisons. Our results indicate that simple models—ones that scale a fixed polarization fraction with frequency—are inadequate to model the behavior of these sources and their contributions to polarization maps.

  4. Opportunities of Gallium Sage experiment with artificial neutrino sources for investigation of neutrino to sterile states

    International Nuclear Information System (INIS)

    Gavrin, V.N.; Gorbachiev, V.V.; Veretenkin, E.P.

    2011-01-01

    The unexpectedly low capture rate of neutrino in Ga source experiments in SAGE and GALLEX can be explained assuming electron neutrino transitions to sterile states with a mass-squared difference ∼ 1eV 2 . To test this oscillation hypothesis, we propose to place a very intense 51 Cr source at the center of a 50 tonne target of gallium metal that is divided into two zones and to measure the neutrino capture rate in each zone. The Experiment has the potential to test neutrino oscillation transitions with mass-squared difference Δm 2 > 0.5 eV 2 . An optimized SAGE setup and 3 MCi source of 51 Cr would provide a sensitivity to electron neutrino disappearance of a few percent.

  5. ICP curve morphology and intracranial flow-volume changes

    DEFF Research Database (Denmark)

    Unnerbäck, Mårten; Ottesen, Johnny T.; Reinstrup, Peter

    2018-01-01

    proposed to shape the ICP curve. This study tested the hypothesis that the ICP curve correlates to intracranial volume changes. METHODS: Cine phase contrast magnetic resonance imaging (MRI) examinations were performed in neuro-intensive care patients with simultaneous ICP monitoring. The MRI was set......BACKGROUND: The intracranial pressure (ICP) curve with its different peaks has been extensively studied, but the exact physiological mechanisms behind its morphology are still not fully understood. Both intracranial volume change (ΔICV) and transmission of the arterial blood pressure have been...

  6. Beam experiments with the Grenoble test electron cyclotron resonance ion source at iThemba LABS

    Energy Technology Data Exchange (ETDEWEB)

    Thomae, R., E-mail: rthomae@tlabs.ac.za; Conradie, J.; Fourie, D.; Mira, J.; Nemulodi, F. [iThemba LABS, P.O. Box 722, Somerset West 7130 (South Africa); Kuechler, D.; Toivanen, V. [CERN, BE/ABP/HSL, 1211 Geneva 23 (Switzerland)

    2016-02-15

    At iThemba Laboratory for Accelerator Based Sciences (iThemba LABS) an electron cyclotron ion source was installed and commissioned. This source is a copy of the Grenoble Test Source (GTS) for the production of highly charged ions. The source is similar to the GTS-LHC at CERN and named GTS2. A collaboration between the Accelerators and Beam Physics Group of CERN and the Accelerator and Engineering Department of iThemba LABS was proposed in which the development of high intensity argon and xenon beams is envisaged. In this paper, we present beam experiments with the GTS2 at iThemba LABS, in which the results of continuous wave and afterglow operation of xenon ion beams with oxygen as supporting gases are presented.

  7. Neutron and gamma ray streaming experiments at the fast neutron source reactor 'YAYOI'

    International Nuclear Information System (INIS)

    Oka, Yoshiaki; Yanagisawa, Ichiro; Akiyama, Masatsugu; An, Shigehiro

    1979-07-01

    Neutron and gamma ray streaming experiments were performed in the ducts and cavities that were located in the heavy concrete shields of the fast neutron source reactor YAYOI of University of Tokyo. The configurations have the feature that the streaming through the ducts are occurred following the scattering in the cavity. The axes of the ducts are perpendicular to the source radiation from the core. The spectrum of the source was modified by putting a plug in the beam hole of the core. An aluminum plug and the plug which contains paraffin were used. The decay in the ducts, however, hardly depends on the source spectrum. The decay in the ducts is nearly exponential. (author)

  8. Sodium source development for pulsed power driven, photopumped NA/NE x-ray laser experiments

    International Nuclear Information System (INIS)

    Burkhalter, P.G.; Cooperstein, G.; Mosher, D.; Ottinger, P.F.; Scherrer, V.E.; Stephanakis, S.J.; Young, F.C.; Hinshelwood, D.D.; Mehlman, G.; Welch, B.L.; Jones, W.D.

    1988-01-01

    A sodium plasma source is being developed for a resonant photopumping x-ray laser scheme in which the 11A 1s 2 - 1s2rho 1 P 1 line in heliumlike Na X is used to pump the Ne IX n=4 singlet level. In their experiment the NRL Gamble II generator is used to produce two z-pinch plasmas in a side-by-side geometry. The sodium plasma is produced on axis and conducts the full 1 MA machine current. A fraction of this current returns through a neon gas puff located 5 cm from the sodium. This separation is determined by the need to prevent the plasmas from mixing and the need to have each plasma's azimuthal magnetic field as symmetric as possible. A minimum separation is desirable to increase coupling efficiency. To improve the pump source, a more confined source of pure sodium involving a coaxial plasma gun is being developed. They are currently studying both the operation of this source on a test stand and implosions of the resulting plasma on Gamble II. In initial experiments aluminum is substituted for sodium. Test stand diagnostics include photodiodes, witness plates, and current monitors designed to investigate the early motion of the annular plasma. Results from test stand and Gamble II experiments with both aluminum and sodium, as well as sodium handling techniques, are presented

  9. DESIGN OF LABORATORY EXPERIMENTS TO STUDY PHOTOIONIZATION FRONTS DRIVEN BY THERMAL SOURCES

    International Nuclear Information System (INIS)

    Drake, R. P.; Keiter, P. A.; Davis, J. S.; Patterson, C. R; Hazak, G.; Frank, A.; Blackman, E. G.; Busquet, Michel

    2016-01-01

    This paper analyzes the requirements of a photoionization-front experiment that could be driven in the laboratory, using thermal sources to produce the necessary flux of ionizing photons. It reports several associated conclusions. Such experiments will need to employ the largest available facilities, capable of delivering many kJ to MJ of energy to an X-ray source. They will use this source to irradiate a volume of neutral gas, likely of N, on a scale of a few mm to a few cm, increasing with source energy. For a gas pressure of several to ten atmospheres at room temperature, and a source temperature near 100 eV, one will be able to drive a photoionization front through a system of tens to hundreds of photon mean free paths. The front should make the familiar transition from the so-called R-Type to D-Type as the radiation flux diminishes with distance. The N is likely to reach the He-like state. Preheating from the energetic photons appears unlikely to become large enough to alter the essential dynamics of the front beyond some layer near the surface. For well-chosen experimental conditions, competing energy transport mechanisms are small.

  10. Design of 6 Mev linear accelerator based pulsed thermal neutron source: FLUKA simulation and experiment

    Energy Technology Data Exchange (ETDEWEB)

    Patil, B.J., E-mail: bjp@physics.unipune.ac.in [Department of Physics, University of Pune, Pune 411 007 (India); Chavan, S.T.; Pethe, S.N.; Krishnan, R. [SAMEER, IIT Powai Campus, Mumbai 400 076 (India); Bhoraskar, V.N. [Department of Physics, University of Pune, Pune 411 007 (India); Dhole, S.D., E-mail: sanjay@physics.unipune.ac.in [Department of Physics, University of Pune, Pune 411 007 (India)

    2012-01-15

    The 6 MeV LINAC based pulsed thermal neutron source has been designed for bulk materials analysis. The design was optimized by varying different parameters of the target and materials for each region using FLUKA code. The optimized design of thermal neutron source gives flux of 3 Multiplication-Sign 10{sup 6}ncm{sup -2}s{sup -1} with more than 80% of thermal neutrons and neutron to gamma ratio was 1 Multiplication-Sign 10{sup 4}ncm{sup -2}mR{sup -1}. The results of prototype experiment and simulation are found to be in good agreement with each other. - Highlights: Black-Right-Pointing-Pointer The optimized 6 eV linear accelerator based thermal neutron source using FLUKA simulation. Black-Right-Pointing-Pointer Beryllium as a photonuclear target and reflector, polyethylene as a filter and shield, graphite as a moderator. Black-Right-Pointing-Pointer Optimized pulsed thermal neutron source gives neutron flux of 3 Multiplication-Sign 10{sup 6} n cm{sup -2} s{sup -1}. Black-Right-Pointing-Pointer Results of the prototype experiment were compared with simulations and are found to be in good agreement. Black-Right-Pointing-Pointer This source can effectively be used for the study of bulk material analysis and activation products.

  11. DESIGN OF LABORATORY EXPERIMENTS TO STUDY PHOTOIONIZATION FRONTS DRIVEN BY THERMAL SOURCES

    Energy Technology Data Exchange (ETDEWEB)

    Drake, R. P.; Keiter, P. A.; Davis, J. S.; Patterson, C. R [Climate and Space Science, University of Michigan, Ann Arbor, MI 48109 (United States); Hazak, G. [Physics Department, Nuclear Research Center-Negev (Israel); Frank, A.; Blackman, E. G. [Physics and Astronomy, University of Rochester, Rochester, NY 14611 (United States); Busquet, Michel, E-mail: rpdrake@umich.edu [ARTEP Incorporated, Ellicot City, MD 21042 (United States)

    2016-12-20

    This paper analyzes the requirements of a photoionization-front experiment that could be driven in the laboratory, using thermal sources to produce the necessary flux of ionizing photons. It reports several associated conclusions. Such experiments will need to employ the largest available facilities, capable of delivering many kJ to MJ of energy to an X-ray source. They will use this source to irradiate a volume of neutral gas, likely of N, on a scale of a few mm to a few cm, increasing with source energy. For a gas pressure of several to ten atmospheres at room temperature, and a source temperature near 100 eV, one will be able to drive a photoionization front through a system of tens to hundreds of photon mean free paths. The front should make the familiar transition from the so-called R-Type to D-Type as the radiation flux diminishes with distance. The N is likely to reach the He-like state. Preheating from the energetic photons appears unlikely to become large enough to alter the essential dynamics of the front beyond some layer near the surface. For well-chosen experimental conditions, competing energy transport mechanisms are small.

  12. Training of human resources on radiation protection and safe use of radiation sources. Argentine experience

    International Nuclear Information System (INIS)

    Biaggio, Alfredo L.; Nasazzi, Nora B.; Arias, Cesar

    2004-01-01

    Argentina has a long experience in Radiation Protection training since 25 years ago. In the present work we analyse those variable and non variable training aspects according to scientific development, increasing radiation source diversity (including new concepts like orphan sources and security), mayor concern about patient in Radiation Protection, previous exposures, etc. We comment what we consider the main steps in the training of Radiation Protection specialists, like university degree, post graduate education distinguishing between formative and informative contents and on the job training. Moreover, we point out the trainees aptitudes and attitudes to be developed in order to work properly in this interdisciplinary field. (author)

  13. Concerns about Quadrupole ICP-MS Lead Isotopic Data and Interpretations in the Environment and Health Fields

    Directory of Open Access Journals (Sweden)

    Brian Gulson

    2018-04-01

    Full Text Available There has been a massive increase in recent years of the use of lead (Pb isotopes in attempts to better understand sources and pathways of Pb in the environment and in man or experimental animals. Unfortunately, there have been many cases where the quality of the isotopic data, especially that obtained by quadrupole inductively coupled plasma mass spectrometry (Q-ICP-MS, are questionable, resulting in questionable identification of potential sources, which, in turn, impacts study interpretation and conclusions. We present several cases where the isotopic data have compromised interpretation because of the use of only the major isotopes 208Pb/206Pb and 207Pb/206Pb, or their graphing in other combinations. We also present some examples comparing high precision data from thermal ionization (TIMS or multi-collector plasma mass spectrometry (MC-ICP-MS to illustrate the deficiency in the Q-ICP-MS data. In addition, we present cases where Pb isotopic ratios measured on Q-ICP-MS are virtually impossible for terrestrial samples. We also evaluate the Pb isotopic data for rat studies, which had concluded that Pb isotopic fractionation occurs between different organs and suggest that this notion of biological fractionation of Pb as an explanation for isotopic differences is not valid. Overall, the brief review of these case studies shows that Q-ICP-MS as commonly practiced is not a suitable technique for precise and accurate Pb isotopic analysis in the environment and health fields.

  14. Non-rigid isometric ICP: A practical registration method for the analysis and compensation of form errors in production engineering

    KAUST Repository

    Sacharow, Alexei

    2011-12-01

    The unprecedented success of the iterative closest point (ICP) method for registration in geometry processing and related fields can be attributed to its efficiency, robustness, and wide spectrum of applications. Its use is however quite limited as soon as the objects to be registered arise from each other by a transformation significantly different from a Euclidean motion. We present a novel variant of ICP, tailored for the specific needs of production engineering, which registers a triangle mesh with a second surface model of arbitrary digital representation. Our method inherits most of ICP\\'s practical advantages but is capable of detecting medium-strength bendings i.e. isometric deformations. Initially, the algorithm assigns to all vertices in the source their closest point on the target mesh and then iteratively establishes isometry, a process which, very similar to ICP, requires intermediate re-projections. A NURBS-based technique for applying the resulting deformation to arbitrary instances of the source geometry, other than the very mesh used for correspondence estimation, is described before we present numerical results on synthetic and real data to underline the viability of our approach in comparison with others. © 2011 Elsevier Ltd. All rights reserved.

  15. Concerns about Quadrupole ICP-MS Lead Isotopic Data and Interpretations in the Environment and Health Fields.

    Science.gov (United States)

    Gulson, Brian; Kamenov, George D; Manton, William; Rabinowitz, Michael

    2018-04-11

    There has been a massive increase in recent years of the use of lead (Pb) isotopes in attempts to better understand sources and pathways of Pb in the environment and in man or experimental animals. Unfortunately, there have been many cases where the quality of the isotopic data, especially that obtained by quadrupole inductively coupled plasma mass spectrometry (Q-ICP-MS), are questionable, resulting in questionable identification of potential sources, which, in turn, impacts study interpretation and conclusions. We present several cases where the isotopic data have compromised interpretation because of the use of only the major isotopes 208 Pb/ 206 Pb and 207 Pb/ 206 Pb, or their graphing in other combinations. We also present some examples comparing high precision data from thermal ionization (TIMS) or multi-collector plasma mass spectrometry (MC-ICP-MS) to illustrate the deficiency in the Q-ICP-MS data. In addition, we present cases where Pb isotopic ratios measured on Q-ICP-MS are virtually impossible for terrestrial samples. We also evaluate the Pb isotopic data for rat studies, which had concluded that Pb isotopic fractionation occurs between different organs and suggest that this notion of biological fractionation of Pb as an explanation for isotopic differences is not valid. Overall, the brief review of these case studies shows that Q-ICP-MS as commonly practiced is not a suitable technique for precise and accurate Pb isotopic analysis in the environment and health fields.

  16. Design of an intense ion source and LEBT for Jinping Underground Nuclear Astrophysics experiments

    International Nuclear Information System (INIS)

    Wu, Q.; Sun, L.T.; Cui, B.Q.; Lian, G.; Yang, Y.; Ma, H.Y.; Tang, X.D.; Zhang, X.Z.; Zhang, Z.M.; Liu, W.P.

    2016-01-01

    The ongoing Jinping Underground Nuclear Astrophysics experiment (JUNA) will take the advantage of the ultralow background in China Jinping Underground Laboratory (CJPL), high current accelerator driven by on an ECR source and highly sensitive detector to study directly a number of important reactions for the first time within their relevant stellar energy range. A 2.45 GHz ECR ion source is one of its key components to provide 10 emA H + , 10 emA He + and 2.0 emA He 2+ beams for the study of (p,γ), (p,α), (α,p) and (α,γ) reactions in the first phase of the JUNA project. Ion beam is extracted from the source with energies up to 50 kV/q. The following low energy beam transport (LEBT) system transports and matches the ion beam from the exit of ion source to the acceleration tube (AT). The design status of the ECR ion source and LEBT system for the JUNA project are presented. The potential risks of the ion source are also discussed and analysed.

  17. K+ ion source for the heavy ion Induction Linac System Experiment ILSE

    International Nuclear Information System (INIS)

    Eylon, S.; Henestroza, E.; Chupp, W.W.; Yu, S.

    1993-05-01

    Low emittance singly charged potassium thermionic ion sources are being developed for the ILSE injector. The ILSE, now under study at LBL, will address the physics issues of particle beams in a heavy ion fusion driver scenario. The K + ion beam is emitted thermionically into a diode gap from alumina-silicate layers (zeolite) coated uniformly on a porous tungsten cup. The Injector diode design requires a large diameter (4in. to 7in.) source able to deliver high current (∼800 mA) low emittance (E n < .5 π mm-mr) beam. The SBTE (Single Beam Test Experiment) 120 keV gun was redesigned and modified with the aid of diode optics calculations using the EGUN code to enable the extraction of high currents of about 90 mA out of a one-inch diameter source. We report on the 1in. source fabrication technique and performance, including total current and current density profile measurements using Faraday cups, emittance and phase space profile measurements using the double slit scanning technique, and life time measurements. Furthermore, we shall report on the extension of the fabricating technique to large diameter sources (up to 7in.), measured ion emission performance, measured surface temperature uniform heating power considerations for large sources

  18. K+ ion source for the heavy ion induction linac system experiment ILSE

    International Nuclear Information System (INIS)

    Eylon, S.; Henestroza, E.; Chupp, W.W.; Yu, S.

    1993-01-01

    Low emittance singly charged potassium thermionic ion sources are being developed for the ILSE injector. The ILSE, now under study at LBL, will address the physics issues of particle beams in a heavy ion fusion driver scenario. The K + ion beam is emitted thermionically into a diode gap from alumino-silicate layers (zeolite) coated uniformly on a porous tungsten cup. The Injector diode design requires a large diameter (4 inches to 7 inches) source able to deliver high current (∼ 800 mA) low emittance (E n < .5 π mm-mr) beam. The SBTE (Single Beam Test Experiment) 120 keV gun was redesigned and modified with the aid of diode optics calculations using the EGUN code to enable the extraction of high currents of about 90 mA out of a one-inch diameter source. The authors report on the 1 inch source fabrication technique and performance, including total current and current density profile measurements using Faraday cups, emittance and phase space profile measurements using the double slit scanning technique, and life time measurements. Furthermore, they shall report on the extension of the fabricating technique to large diameter sources (up to 7 inches), measured ion emission performance, measured surface temperature uniformity and heating power considerations for large sources

  19. Design of an intense ion source and LEBT for Jinping Underground Nuclear Astrophysics experiments

    Energy Technology Data Exchange (ETDEWEB)

    Wu, Q., E-mail: wuq@impcas.ac.cn [Institute of Modern Physics (IMP), Chinese Academy of Sciences, Lanzhou 730000 (China); Sun, L.T., E-mail: sunlt@impcas.ac.cn [Institute of Modern Physics (IMP), Chinese Academy of Sciences, Lanzhou 730000 (China); Cui, B.Q.; Lian, G. [China Institute of Atomic Energy, Beijing 102413 (China); Yang, Y.; Ma, H.Y.; Tang, X.D.; Zhang, X.Z.; Zhang, Z.M. [Institute of Modern Physics (IMP), Chinese Academy of Sciences, Lanzhou 730000 (China); Liu, W.P. [China Institute of Atomic Energy, Beijing 102413 (China)

    2016-09-11

    The ongoing Jinping Underground Nuclear Astrophysics experiment (JUNA) will take the advantage of the ultralow background in China Jinping Underground Laboratory (CJPL), high current accelerator driven by on an ECR source and highly sensitive detector to study directly a number of important reactions for the first time within their relevant stellar energy range. A 2.45 GHz ECR ion source is one of its key components to provide 10 emA H{sup +}, 10 emA He{sup +} and 2.0 emA He{sup 2+} beams for the study of (p,γ), (p,α), (α,p) and (α,γ) reactions in the first phase of the JUNA project. Ion beam is extracted from the source with energies up to 50 kV/q. The following low energy beam transport (LEBT) system transports and matches the ion beam from the exit of ion source to the acceleration tube (AT). The design status of the ECR ion source and LEBT system for the JUNA project are presented. The potential risks of the ion source are also discussed and analysed.

  20. Determination of actinides using ICP-SFMS

    International Nuclear Information System (INIS)

    Nygren, Ulrika

    2006-01-01

    Interest in the determination of the actinides using ICP-MS has steadily increased with the development of systems capable of more sensitive and precise measurements. However, the analysis of less abundant actinides such as Pu and Am is not straightforward due to the need for chemical separation of these elements prior to determination. In many applications of mass-spectrometric actinide analysis, isotope ratio measurements are important, either for the analysis of the isotopic composition of, e.g., U or Pu in the sample, or for quantitative determinations using isotope dilution mass spectrometry. In order to achieve high precision and accuracy in an isotope ratio measurement, corrections for instrumentally induced systematic errors, e.g., due to dead-time and mass bias, need to be considered. In this thesis, different aspects of actinide analysis using ICP-SFMS have been addressed. In Papers I and III, separation procedures based on solid phase extraction for Pu, Am and U were developed and evaluated with respect to chemical yield and separation from elements causing spectral interferences. Applications of the analytical procedures developed comprised measurement of the 240 Pu/ 2 3 9Pu ratio in environmental reference materials, and age determination of Pu based on the 241 Pu/ 241 Am and 240 Pu/ 236 U ratios. In the application of different separation procedures for Pu, previously unidentified spectral interferences were discovered. In Paper II, these interferences were identified as lanthanide phosphate ions and the composition and formation of these species with respect to different instrumental parameters were further examined. Due to the importance of precise and accurate isotope ratio determination, a thorough investigation of the instrumental dead time of an ICP-SFMS system was performed. The dead time was evaluated via both isotope ratio and electronic measurements of the output from the detector amplifier. It was found that the overall uncertainty in ratio

  1. Disruption simulation experiment using high-frequency rastering electron beam as the heat source

    International Nuclear Information System (INIS)

    Yamazaki, S.; Seki, M.

    1987-01-01

    The disruption is a serious event which possibly reduces the lifetime of plasm interactive components, so the effects of the resulting high heat flux on the wall materials must be clearly identified. The authors performed disruption simulation experiments to investigate melting, evaporation, and crack initiation behaviors using an electron beam facility as the heat source. The facility was improved with a high-frequency beam rastering system which provided spatially and temporally uniform heat flux on wider test surfaces. Along with the experiments, thermal and mechanical analyses were also performed. A two-dimensional disruption thermal analysis code (DREAM) was developed for the analyses

  2. An Open-Source, Low-Cost Robot for Performing Reactive Liquid Handling Experiments

    DEFF Research Database (Denmark)

    Nejatimoharrami, Farzad; Faina, Andres; Støy, Kasper

    vessels in the middle, and 3) a camera as the sensing system at the bottom, providing a view of the experiment. From the raw camera image experiment specific data such as droplet size, position, speed, number, color, and shape are calculated. The computer vision system has an accuracy of 4% for droplet......Bot's application domain is extendable owing to a modular design of hardware, and open source software. Evobot's modular design enables support for different modules, e.g. syringe modules for liquid handling, grippers to reposition reaction vessels or dispose of them, sensor modules including temperature, pH, etc...

  3. Li+ alumino-silicate ion source development for the Neutralized Drift Compression Experiment (NDCX-II)

    International Nuclear Information System (INIS)

    Roy, P.K.; Greenway, W.; Kwan, J.W.; Seidl, P.A.; Waldron, W.

    2011-01-01

    To heat targets to electron-volt temperatures for the study of warm dense matter with intense ion beams, low mass ions, such as lithium, have an energy loss peak (dE/dx) at a suitable kinetic energy. The Heavy Ion Fusion Sciences (HIFS) program at Lawrence Berkeley National Laboratory will carry out warm dense matter experiments using Li + ion beam with energy 1.2-4 MeV in order to achieve uniform heating up to 0.1-1 eV. The accelerator physics design of Neutralized Drift Compression Experiment (NDCX-II) has a pulse length at the ion source of about 0.5 (micro)s. Thus for producing 50 nC of beam charge, the required beam current is about 100 mA. Focusability requires a normalized (edge) emittance ∼2 π-mm-mrad. Here, lithium aluminosilicate ion sources, of β-eucryptite, are being studied within the scope of NDCX-II construction. Several small (0.64 cm diameter) lithium aluminosilicate ion sources, on 70%-80% porous tungsten substrate, were operated in a pulsed mode. The distance between the source surface and the mid-plane of the extraction electrode (1 cm diameter aperture) was 1.48 cm. The source surface temperature was at 1220 C to 1300 C. A 5-6 (micro)s long beam pulsed was recorded by a Faraday cup (+300 V on the collector plate and -300 V on the suppressor ring). Figure 1 shows measured beam current density (J) vs. V 3/2 . A space-charge limited beam density of ∼1 mA/cm 2 was measured at 1275 C temperature, after allowing a conditioning time of about ∼ 12 hours. Maximum emission limited beam current density of (ge) 1.8mA/cm 2 was recorded at 1300 C with 10-kV extractions. Figure 2 shows the lifetime of two typical sources with space-charge limited beam current emission at a lower extraction voltage (1.75 kV) and at temperature of 1265 ± 7 C. These data demonstrate a constant, space-charge limited beam current for 20-50 hours. The lifetime of a source is determined by the loss of lithium from the alumino-silicate material either as ions or as neutral

  4. An experiment to measure the electron neutrino mass using a cryogenic tritium source

    International Nuclear Information System (INIS)

    Fackler, O.; Jeziorski, B.; Kolos, W.; Monkhorst, H.; Mugge, M.; Sticker, H.; Szalewicz, K.; White, R.M.; Woerner, R.

    1985-01-01

    An experiment has been performed to determine the electron neutrino mass with the precision of a few eV by measuring the tritium beta decay energy distribution near the endpoint. Key features of the experiment are a 2 eV resolution electrostatic spectrometer and a high-activity frozen tritium source. It is important that the source have electronic wavefunctions which can be accurately calculated. These calculations have been made for tritium and the HeT + daughter ion and allow determination of branching fractions to 0.1% and energy of the excited states to 0.1 eV. The excited final molecular state calculations and the experimental apparatus are discussed. 4 refs., 5 figs

  5. Experience with the Open Source based implementation for ATLAS Conditions Data Management System

    CERN Document Server

    Amorim, A; Oliveira, C; Pedro, L; Barros, N

    2003-01-01

    Conditions Data in high energy physics experiments is frequently seen as every data needed for reconstruction besides the event data itself. This includes all sorts of slowly evolving data like detector alignment, calibration and robustness, and data from detector control system. Also, every Conditions Data Object is associated with a time interval of validity and a version. Besides that, quite often is useful to tag collections of Conditions Data Objects altogether. These issues have already been investigated and a data model has been proposed and used for different implementations based in commercial DBMSs, both at CERN and for the BaBar experiment. The special case of the ATLAS complex trigger that requires online access to calibration and alignment data poses new challenges that have to be met using a flexible and customizable solution more in the line of Open Source components. Motivated by the ATLAS challenges we have developed an alternative implementation, based in an Open Source RDBMS. Several issues...

  6. Integrated care pathways for airway diseases (AIRWAYS-ICPs)

    NARCIS (Netherlands)

    Bousquet, J.; Addis, A.; Adcock, I.; Agache, I.; Agusti, A.; Alonso, A.; Annesi-Maesano, I.; Anto, J. M.; Bachert, C.; Baena-Cagnani, C. E.; Bai, C.; Baigenzhin, A.; Barbara, C.; Barnes, P. J.; Bateman, E. D.; Beck, L.; Bedbrook, A.; Bel, E. H.; Benezet, O.; Bennoor, K. S.; Benson, M.; Bernabeu-Wittel, M.; Bewick, M.; Bindslev-Jensen, C.; Blain, H.; Blasi, F.; Bonini, M.; Bonini, S.; Boulet, L. P.; Bourdin, A.; Bourret, R.; Bousquet, P. J.; Brightling, C. E.; Briggs, A.; Brozek, J.; Buhl, R.; Bush, A.; Caimmi, D.; Calderon, M.; Calverley, P.; Camargos, P. A.; Camuzat, T.; Canonica, G. W.; Carlsen, K. H.; Casale, T. B.; Cazzola, M.; Cepeda Sarabia, A. M.; Cesario, A.; Chen, Y. Z.; Chkhartishvili, E.; Chavannes, N. H.; Chiron, R.; Chuchalin, A.; Chung, K. F.; Cox, L.; Crooks, G.; Crooks, M. G.; Cruz, A. A.; Custovic, A.; Dahl, R.; Dahlen, S. E.; de Blay, F.; Dedeu, T.; Deleanu, D.; Demoly, P.; Devillier, P.; Didier, A.; Dinh-Xuan, A. T.; Djukanovic, R.; Dokic, D.; Douagui, H.; Dubakiene, R.; Eglin, S.; Elliot, F.; Emuzyte, R.; Fabbri, L.; Fink Wagner, A.; Fletcher, M.; Fokkens, W. J.; Fonseca, J.; Franco, A.; Frith, P.; Furber, A.; Gaga, M.; Garcés, J.; Garcia-Aymerich, J.; Gamkrelidze, A.; Gonzales-Diaz, S.; Gouzi, F.; Guzmán, M. A.; Haahtela, T.; Harrison, D.; Hayot, M.; Heaney, L. G.; Heinrich, J.; Hellings, P. W.; Hooper, J.; Humbert, M.; Hyland, M.; Iaccarino, G.; Jakovenko, D.; Jardim, J. R.; Jeandel, C.; Jenkins, C.; Johnston, S. L.; Jonquet, O.; Joos, G.; Jung, K. S.; Kalayci, O.; Karunanithi, S.; Keil, T.; Khaltaev, N.; Kolek, V.; Kowalski, M. L.; Kull, I.; Kuna, P.; Kvedariene, V.; Le, L. T.; Lodrup Carlsen, K. C.; Louis, R.; MacNee, W.; Mair, A.; Majer, I.; Manning, P.; de Manuel Keenoy, E.; Masjedi, M. R.; Melen, E.; Melo-Gomes, E.; Menzies-Gow, A.; Mercier, G.; Mercier, J.; Michel, J. P.; Miculinic, N.; Mihaltan, F.; Milenkovic, B.; Molimard, M.; Momas, I.; Montilla-Santana, A.; Morais-Almeida, M.; Morgan, M.; N'Diaye, M.; Nafti, S.; Nekam, K.; Neou, A.; Nicod, L.; O'Hehir, R.; Ohta, K.; Paggiaro, P.; Palkonen, S.; Palmer, S.; Papadopoulos, N. G.; Papi, A.; Passalacqua, G.; Pavord, I.; Pigearias, B.; Plavec, D.; Postma, D. S.; Price, D.; Rabe, K. F.; Radier Pontal, F.; Redon, J.; Rennard, S.; Roberts, J.; Robine, J. M.; Roca, J.; Roche, N.; Rodenas, F.; Roggeri, A.; Rolland, C.; Rosado-Pinto, J.; Ryan, D.; Samolinski, B.; Sanchez-Borges, M.; Schünemann, H. J.; Sheikh, A.; Shields, M.; Siafakas, N.; Sibille, Y.; Similowski, T.; Small, I.; Sola-Morales, O.; Sooronbaev, T.; Stelmach, R.; Sterk, P. J.; Stiris, T.; Sud, P.; Tellier, V.; To, T.; Todo-Bom, A.; Triggiani, M.; Valenta, R.; Valero, A. L.; Valiulis, A.; Valovirta, E.; van Ganse, E.; Vandenplas, O.; Vasankari, T.; Vestbo, J.; Vezzani, G.; Viegi, G.; Visier, L.; Vogelmeier, C.; Vontetsianos, T.; Wagstaff, R.; Wahn, U.; Wallaert, B.; Whalley, B.; Wickman, M.; Williams, D. M.; Wilson, N.; Yawn, B. P.; Yiallouros, P. K.; Yorgancioglu, A.; Yusuf, O. M.; Zar, H. J.; Zhong, N.; Zidarn, M.; Zuberbier, T.

    2014-01-01

    The objective of Integrated Care Pathways for Airway Diseases (AIRWAYS-ICPs) is to launch a collaboration to develop multi-sectoral care pathways for chronic respiratory diseases in European countries and regions. AIRWAYS-ICPs has strategic relevance to the European Union Health Strategy and will

  7. Integrated care pathways for airway diseases (AIRWAYS-ICPs)

    NARCIS (Netherlands)

    Bousquet, J.; Addis, A.; Adcock, I.; Agache, I.; Agusti, A.; Alonso, A.; Annesi-Maesano, I.; Anto, J. M.; Bachert, C.; Baena-Cagnani, C. E.; Bai, C.; Baigenzhin, A.; Barbara, C.; Barnes, P. J.; Bateman, E. D.; Beck, L.; Bedbrook, A.; Bel, E. H.; Benezet, O.; Bennoor, K. S.; Benson, M.; Bernabeu-Wittel, M.; Bewick, M.; Bindslev-Jensen, C.; Blain, H.; Blasi, F.; Bonini, M.; Bonini, S.; Boulet, L. P.; Bourdin, A.; Bourret, R.; Bousquet, P. J.; Brightling, C. E.; Briggs, A.; Brozek, J.; Buh, R.; Bush, A.; Caimmi, D.; Calderon, M.; Calverley, P.; Camargos, P. A.; Camuzat, T.; Canonica, G. W.; Carlsen, K. H.; Casale, T. B.; Cazzola, M.; Sarabia, A. M. Cepeda; Cesario, A.; Chen, Y. Z.; Chkhartishvili, E.; Chavannes, N. H.; Chiron, R.; Chuchalin, A.; Chung, K. F.; Cox, L.; Crooks, G.; Crooks, M. G.; Cruz, A. A.; Custovic, A.; Dahl, R.; Dahlen, S. E.; De Blay, F.; Dedeu, T.; Deleanu, D.; Demoly, P.; Devillier, P.; Didier, A.; Dinh-Xuan, A. T.; Djukanovic, R.; Dokic, D.; Douagui, H.; Dubakiene, R.; Eglin, S.; Elliot, F.; Emuzyte, R.; Fabbri, L.; Wagner, A. Fink; Fletcher, M.; Fokkens, W. J.; Fonseca, J.; Franco, A.; Frith, P.; Furber, A.; Gaga, M.; Garces, J.; Garcia-Aymerich, J.; Gamkrelidze, A.; Gonzales-Diaz, S.; Gouzi, F.; Guzman, M. A.; Haahtela, T.; Harrison, D.; Hayot, M.; Heaney, L. G.; Heinrich, J.; Hellings, P. W.; Hooper, J.; Humbert, M.; Hyland, M.; Iaccarino, G.; Jakovenko, D.; Jardim, J. R.; Jeandel, C.; Jenkins, C.; Johnston, S. L.; Jonquet, O.; Joos, G.; Jung, K. S.; Kalayci, O.; Karunanithi, S.; Keil, T.; Khaltaev, N.; Kolek, V.; Kowalski, M. L.; Kull, I.; Kuna, P.; Kvedariene, V.; Le, L. T.; Carlsen, K. C. Lodrup; Louis, R.; MacNee, W.; Mair, A.; Majer, I.; Manning, P.; Keenoy, E. de Manuel; Masjedi, M. R.; Meten, E.; Melo-Gomes, E.; Menzies-Gow, A.; Mercier, G.; Mercier, J.; Michel, J. P.; Miculinic, N.; Mihaltan, F.; Milenkovic, B.; Molimard, M.; Mamas, I.; Montilla-Santana, A.; Morais-Almeida, M.; Morgan, M.; N'Diaye, M.; Nafti, S.; Nekam, K.; Neou, A.; Nicod, L.; O'Hehir, R.; Ohta, K.; Paggiaro, P.; Palkonen, S.; Palmer, S.; Papadopoulos, N. G.; Papi, A.; Passalacqua, G.; Pavord, I.; Pigearias, B.; Plavec, D.; Postma, D. S.; Price, D.; Rabe, K. F.; Pontal, F. Radier; Redon, J.; Rennard, S.; Roberts, J.; Robine, J. M.; Roca, J.; Roche, N.; Rodenas, F.; Roggeri, A.; Rolland, C.; Rosado-Pinto, J.; Ryan, D.; Samolinski, B.; Sanchez-Borges, M.; Schunemann, H. J.; Sheikh, A.; Shields, M.; Siafakas, N.; Sibille, Y.; Similowski, T.; Small, I.; Sola-Morales, O.; Sooronbaev, T.; Stelmach, R.; Sterk, P. J.; Stiris, T.; Sud, P.; Tellier, V.; To, T.; Todo-Bom, A.; Triggiani, M.; Valenta, R.; Valero, A. L.; Valiulis, A.; Valovirta, E.; Van Ganse, E.; Vandenplas, O.; Vasankari, T.; Vestbo, J.; Vezzani, G.; Viegi, G.; Visier, L.; Vogelmeier, C.; Vontetsianos, T.; Wagstaff, R.; Wahn, U.; Wallaert, B.; Whalley, B.; Wickman, M.; Williams, D. M.; Wilson, N.; Yawn, B. P.; Yiallouros, P. K.; Yorgancioglu, A.; Yusuf, O. M.; Zar, H. J.; Zhong, N.; Zidarn, M.; Zuberbier, T.

    The objective of Integrated Care Pathways for Airway Diseases (AIRWAYS-ICPs) is to launch a collaboration to develop multi-sectoral care pathways for chronic respiratory diseases in European countries and regions. AIRWAYS-ICPs has strategic relevance to the European Union Health Strategy and will

  8. Operational experiences of the spallation neutron source superconducting linac and power ramp-up

    International Nuclear Information System (INIS)

    Kim, Sang-Ho

    2009-01-01

    The spallation neutron source (SNS) is a second generation pulsed neutron source and designed to provide a 1-GeV, 1.44-MW proton beam to a mercury target for neutron production. Since the commissioning of the accelerator complex in 2006, the SNS has started its operation for neutron production and beam power ramp-up has been in progress toward the design goal. All subsystems of the SNS were designed and developed for substantial improvements compared to existing accelerators because the design beam power is almost an order of magnitude higher compared to existing neutron facilities and the achievable neutron scattering performance will exceed present sources by more than a factor of 20 to 100. In this paper, the operational experiences with the SNS Superconducting Linac (SCL), Power Ramp-up Plan to reach the design goal and the Power Upgrade Plan (PUP) will be presented including machine, subsystem and beam related issues.

  9. Reactor physics experiments in PURNIMA sub critical facility coupled with 14 MeV neutron source

    International Nuclear Information System (INIS)

    Kumar, Rajeev; Degweker, S.B.; Patel, Tarun; Bishnoi, Saroj; Adhikari, P.S.

    2011-01-01

    Accelerator Driven Sub-critical Systems (ADSS) are attracting increasing worldwide attention due to their superior safety characteristics and their potential for burning actinide and fission product waste and energy production. A number of countries around the world have drawn up roadmaps/programs for development of ADSS. Indian interest in ADSS has an additional dimension, which is related to the planned utilization of our large thorium reserves for future nuclear energy generation. A programme for development of ADSS is taken up at the Bhabha Atomic Research Centre (BARC) in India. This includes R and D activities for high current proton accelerator development, target development and Reactor Physics studies. As part of the ADSS Reactor Physics research programme, a sub-critical facility is coming up in BARC which will be coupled with an existing D-D/D-T neutron generator. Two types of cores are planned. In one of these, the sub-critical reactor assembly consists of natural uranium moderated by high density polyethylene (HDP) and reflected by BeO. The other consists of natural uranium moderated by light water. The maximum neutron yield of the neutron source with tritium target is around 10 10 neutron per sec. Various reactor physics experiments like measurement of the source strength, neutron flux distribution, buckling estimation and sub-critical source multiplication are planned. Apart from this, measurement of the total fission power and neutron spectrum will also be carried out. Mainly activation detectors will be used in all in-core neutron flux measurement. Measurement of the degree of sub-criticality by various deterministic and noise methods is planned. Helium detectors with advanced data acquisition card will be used for the neutron noise experiments. Noise characteristics of ADSS are expected to be different from that of traditional reactors due to the non-Poisson statistical features of the source. A new theory incorporating these features has been

  10. Support systems for optics in the experiment stations at the Advanced Photon Source

    International Nuclear Information System (INIS)

    Barraza, J.; Shu, D.; Kuzay, T.M.

    1994-01-01

    Support systems have been designed for optics in the experiment stations of the Advanced Photon Source at Argonne National Laboratory. These systems utilize modular precision positioning slides and stages arranged in 3-point kinematic mount fashion for optimum mechanical stability. Through the use of novel configurations, these systems can achieve large linear motions, six degree-of-freedom motion, and large load capacities without sacrificing valuable experimental station space. This paper will discuss the designs and specifications of the positioning systems developed

  11. The solar neutrino problem after the GALLEX artificial neutrino source experiment

    International Nuclear Information System (INIS)

    Vignaud, D.

    1995-01-01

    Using an intense 51 Cr artificial neutrino source (more than 60 PBq), the GALLEX solar neutrino collaboration has recently checked that its radiochemical detector was fully efficient for the detection of solar neutrinos. After this crucial result, the status of the solar neutrino problem is reviewed, with emphasis on how neutrino oscillations may explain (through the MSW effect) the different deficits observed in the four existing experiments. (author). 25 refs., 5 figs., 1 tab

  12. Development of on-line electrochemical sample pretreatment methods for the analysis of thallium and uranium by ICP-MS

    International Nuclear Information System (INIS)

    Zhou, F.; Van Berkel, G.J.; Morton, S.J.; Duckworth, D.C.; Adeniyi, W.K.; Keller, J.M.

    1995-01-01

    Anodic and adsorptive stripping voltammetry (AWV and AdSV, respectively) were performed on-line with a mercury thin-film electrode (MTFE) to effect the selective accumulation and detection of thallium and uranium, respectively. ASV-ICP-MS experiments using thallium as the test element were performed to characterize the behavior of the on-line system for low level and quantitative determinations. Excellent linearity in response was demonstrated for thallium standards ranging from 0.25 ng/L to 50 microg/L. The 1.0 pg/L detection limit calculated from this data for thallium (3σ/sensitivity) was 400 times lower than that of conventional ICP-MS. The ability to overcome sample matrix effects in quantitative determinations was demonstrated by the analysis of an undiluted synthetic urine sample. AdSV-ICP-MS experiments were performed using uranium as the test element to demonstrate the utility of this method for the determination of radiologically important elements. A uranium(VI)-cupferron complex was used to effect adsorptive accumulation of uranium from a 10 microg/L standard solution onto the MTFE. The uranium was chemically stripped from the electrode for subsequent downstream detection by the ICP-MS. The quantitative nature of this method and a modest enhancement of signal levels (∼X10) over those levels obtained with conventional ICP-MS for samples in the microgram/liter concentration range were demonstrated. Modifications to the current system to provide low flow rate operation will allow further optimization of the ASV-ICP-MS and AdSV-ICP-MS combinations

  13. Summary of mirror experiments relevant to beam-plasma neutron source

    International Nuclear Information System (INIS)

    Molvik, A.W.

    1988-01-01

    A promising design for a deuterium-tritium (DT) neutron source is based on the injection of neutral beams into a dense, warm plasma column. Its purpose is to test materials for possible use in fusion reactors. A series of designs have evolved, from a 4-T version to an 8-T version. Intense fluxes of 5--10 MW/m 2 is achieved at the plasma surface, sufficient to complete end-of-life tests in one to two years. In this report, we review data from earlier mirror experiments that are relevant to such neutron sources. Most of these data are from 2XIIB, which was the only facility to ever inject 5 MW of neutral beams into a single mirror call. The major physics issues for a beam-plasma neutron source are magnetohydrodynamic (MHD) equilibrium and stability, microstability, startup, cold-ion fueling of the midplane to allow two-component reactions, and operation in the Spitzer conduction regime, where the power is removed to the ends by an axial gradient in the electron temperature T/sub e/. We show in this report that the conditions required for a neutron source have now been demonstrated in experiments. 20 refs., 15 figs., 3 tabs

  14. Operational experience of SST1 NBI control system with prototype Ion source

    International Nuclear Information System (INIS)

    Patel, V B; Patel, P J; Singh, N P; Tripathi, V; Thakkar, D; Gupta, L N; Prahlad, V; Sharma, S K; Bandyopadyay, M; Chakraborty, A K; Baruah, U K; Mattoo, S K; Patel, G B; Onali, Raja

    2010-01-01

    This paper presents operational experience of integrated control of the arc-filament and High-voltage power supply of Steady State Tokamak (SST)-1 NBI system using Versa Module Europa (VME) system on prototype Ion source. The control algorithm is implemented on the VxWorks operating system using 'C' language. This paper also describes the operating sequence and controls on power supply system. Discharge and Filament power supplies are controlled in such a way so that necessary discharge current can be available in Ion Source. The discharge current is controlled by manipulating the filament current. Close loop control is implemented on each filament power supply with feedback from Discharge Current to control the overall discharge inside the ion source. Necessary actions for shut OFF and subsequent Turn ON are also taken during breakdowns between the Grids of the ion source. Total numbers of breakdowns are also monitored. Shot is terminated, if the breakdown count is higher than the set value. This control system can be programmed to restart High-voltage power supply within 5mS after breakdown occurs. This control system is capable to handle the all types of dynamics in the system. This paper also presents results of experiment.

  15. Forensic discrimination of aluminum foil by SR-XRF and ICP-AES

    International Nuclear Information System (INIS)

    Kasamatsu, Masaaki; Suzuki, Yasuhiro; Suzuki, Shinichi; Miyamoto, Naoki; Watanabe, Seiya; Shimoda, Osamu; Takatsu, Masahisa; Nakanishi, Toshio

    2010-01-01

    The application of synchrotron radiation X-ray fluorescence spectrometry (SR-XRF) was investigated for the forensic discrimination of aluminum foil by comparisons of the elemental components. Small fragments (1 x 1 mm) were taken from 4 kinds of aluminum foils produced by different manufactures and used for measurements of the XRF spectrum at BL37XU of SPring-8. A comparison of the XRF spectra was effective for the discrimination of aluminum foils from different sources, because significant differences were observed in the X-ray peak intensities of Fe, Cu, Zn, Ga, Zr and Sn. These elements, except for Zr and Sn in the aluminum foils and NIST SRM1258 (Aluminium Alloy 6011), were also determined by inductively coupled plasma atomic emission spectrometry (ICP-AES). The observed values of Fe, Cu, Zn and Ga in NIST standard samples by ICP-AES showed satisfactorily good agreements with the certified or information values with relative standard deviations from 1.1% for Zn to 6.7% for Ga. The observed values for the aluminum foils by ICP-AES were compared with those by SR-XRF. Correlation coefficients from 0.997 for Cu/Fe to 0.999 for Zn/Fe and Ga/Fe were obtained between the ratio of the elemental concentration by ICP-AES and normalized the X-ray intensity by SR-XRF. This result demonstrates that a comparison of the normalized X-ray intensity is nearly as effective for the discrimination of aluminum foils as quantitative analysis by ICP-AES. Comparisons of the analytical results by SR-XRF allow the discrimination of all aluminum foils using only a 1 mm 2 fragment with no destruction of the samples. (author)

  16. Energy Spectra of Abundant Cosmic-ray Nuclei in Sources, According to the ATIC Experiment

    Energy Technology Data Exchange (ETDEWEB)

    Panov, A. D.; Sokolskaya, N. V.; Zatsepin, V. I., E-mail: panov@dec1.sinp.msu.ru [Moscow State University, Skobeltsyn Institute of Nuclear Physics, Moscow, 119991 (Russian Federation)

    2017-03-01

    One of the main results of the ATIC (Advanced Thin Ionization Calorimeter) experiment is a collection of energy spectra of abundant cosmic-ray nuclei: protons, He, C, O, Ne, Mg, Si, and Fe measured in terms of energy per particle in the energy range from 50 GeV to tens of teraelectronvolts. In this paper, the ATIC energy spectra of abundant primary nuclei are back-propagated to the spectra in sources in terms of magnetic rigidity using a leaky-box approximation of three different GALPROP-based diffusion models of propagation that fit the latest B/C data of the AMS-02 experiment. It is shown that the results of a comparison of the slopes of the spectra in sources are weakly model dependent; therefore the differences of spectral indices are reliable data. A regular growth of the steepness of spectra in sources in the range of magnetic rigidity of 50–1350 GV is found for a charge range from helium to iron. This conclusion is statistically reliable with significance better than 3.2 standard deviations. The results are discussed and compared to the data of other modern experiments.

  17. Soil analyses by ICP-MS (Review)

    International Nuclear Information System (INIS)

    Yamasaki, Shin-ichi

    2000-01-01

    Soil analyses by inductively coupled plasma mass spectrometry (ICP-MS) are reviewed. The first half of the paper is devoted to the development of techniques applicable to soil analyses, where diverse analytical parameters are carefully evaluated. However, the choice of soil samples is somewhat arbitrary, and only a limited number of samples (mostly reference materials) are examined. In the second half, efforts are mostly concentrated on the introduction of reports, where a large number of samples and/or very precious samples have been analyzed. Although the analytical techniques used in these reports are not necessarily novel, valuable information concerning such topics as background levels of elements in soils, chemical forms of elements in soils and behavior of elements in soil ecosystems and the environment can be obtained. The major topics discussed are total elemental analysis, analysis of radionuclides with long half-lives, speciation, leaching techniques, and isotope ratio measurements. (author)

  18. Sources

    International Nuclear Information System (INIS)

    Duffy, L.P.

    1991-01-01

    This paper discusses the sources of radiation in the narrow perspective of radioactivity and the even narrow perspective of those sources that concern environmental management and restoration activities at DOE facilities, as well as a few related sources. Sources of irritation, Sources of inflammatory jingoism, and Sources of information. First, the sources of irritation fall into three categories: No reliable scientific ombudsman to speak without bias and prejudice for the public good, Technical jargon with unclear definitions exists within the radioactive nomenclature, and Scientific community keeps a low-profile with regard to public information. The next area of personal concern are the sources of inflammation. This include such things as: Plutonium being described as the most dangerous substance known to man, The amount of plutonium required to make a bomb, Talk of transuranic waste containing plutonium and its health affects, TMI-2 and Chernobyl being described as Siamese twins, Inadequate information on low-level disposal sites and current regulatory requirements under 10 CFR 61, Enhanced engineered waste disposal not being presented to the public accurately. Numerous sources of disinformation regarding low level radiation high-level radiation, Elusive nature of the scientific community, The Federal and State Health Agencies resources to address comparative risk, and Regulatory agencies speaking out without the support of the scientific community

  19. Ophthalmodynamometry for ICP prediction and pilot test on Mt. Everest.

    Science.gov (United States)

    Querfurth, Henry W; Lieberman, Philip; Arms, Steve; Mundell, Steve; Bennett, Michael; van Horne, Craig

    2010-11-01

    A recent development in non-invasive techniques to predict intracranial pressure (ICP) termed venous ophthalmodynamometry (vODM) has made measurements in absolute units possible. However, there has been little progress to show utility in the clinic or field. One important application would be to predict changes in actual ICP during adaptive responses to physiologic stress such as hypoxia. A causal relationship between raised intracranial pressure and acute mountain sickness (AMS) is suspected. Several MRI studies report that modest physiologic increases in cerebral volume, from swelling, normally accompany subacute ascent to simulated high altitudes. 1) Validate and calibrate an advanced, portable vODM instrument on intensive patients with raised intracranial pressure and 2) make pilot, non-invasive ICP estimations of normal subjects at increasing altitudes. The vODM was calibrated against actual ICP in 12 neurosurgical patients, most affected with acute hydrocephalus and monitored using ventriculostomy/pressure transducers. The operator was blinded to the transducer read-out. A clinical field test was then conducted on a variable data set of 42 volunteer trekkers and climbers scaling Mt. Everest, Nepal. Mean ICPs were estimated at several altitudes on the ascent both across and within subjects. Portable vODM measurements increased directly and linearly with ICP resulting in good predictability (r = 0.85). We also found that estimated ICP increases normally with altitude (10 ± 3 mm Hg; sea level to 20 ± 2 mm Hg; 6553 m) and that AMS symptoms did not correlate with raised ICP. vODM technology has potential to reliably estimate absolute ICP and is portable. Physiologic increases in ICP and mild-mod AMS are separate responses to high altitude, possibly reflecting swelling and vasoactive instability, respectively.

  20. Ophthalmodynamometry for ICP prediction and pilot test on Mt. Everest

    Directory of Open Access Journals (Sweden)

    Bennett Michael

    2010-11-01

    Full Text Available Abstract Background A recent development in non-invasive techniques to predict intracranial pressure (ICP termed venous ophthalmodynamometry (vODM has made measurements in absolute units possible. However, there has been little progress to show utility in the clinic or field. One important application would be to predict changes in actual ICP during adaptive responses to physiologic stress such as hypoxia. A causal relationship between raised intracranial pressure and acute mountain sickness (AMS is suspected. Several MRI studies report that modest physiologic increases in cerebral volume, from swelling, normally accompany subacute ascent to simulated high altitudes. Objectives 1 Validate and calibrate an advanced, portable vODM instrument on intensive patients with raised intracranial pressure and 2 make pilot, non-invasive ICP estimations of normal subjects at increasing altitudes. Methods The vODM was calibrated against actual ICP in 12 neurosurgical patients, most affected with acute hydrocephalus and monitored using ventriculostomy/pressure transducers. The operator was blinded to the transducer read-out. A clinical field test was then conducted on a variable data set of 42 volunteer trekkers and climbers scaling Mt. Everest, Nepal. Mean ICPs were estimated at several altitudes on the ascent both across and within subjects. Results Portable vODM measurements increased directly and linearly with ICP resulting in good predictability (r = 0.85. We also found that estimated ICP increases normally with altitude (10 ± 3 mm Hg; sea level to 20 ± 2 mm Hg; 6553 m and that AMS symptoms did not correlate with raised ICP. Conclusion vODM technology has potential to reliably estimate absolute ICP and is portable. Physiologic increases in ICP and mild-mod AMS are separate responses to high altitude, possibly reflecting swelling and vasoactive instability, respectively.

  1. Experience and Lessons Learned from Conditioning of Spent Sealed Sources in Singapore - 13107

    Energy Technology Data Exchange (ETDEWEB)

    Hong, Dae-Seok; Kang, Il-Sik; Jang, Kyung-Duk; Jang, Won-Hyuk [Korea Atomic Energy Research Institute, 1045 Daedeokdaero, Yuseong, Daejeon (Korea, Republic of); Hoo, Wee-Teck [National Environment Agency, 40 Scotts Road 228231 (Singapore)

    2013-07-01

    In 2010, IAEA requested KAERI (Korea Atomic Energy Research Institute) to support Singapore for conditioning spent sealed sources. Those that had been used for a lightning conductor, check source, or smoke detector, various sealed sources had been collected and stored by the NEA (National Environment Agency) in Singapore. Based on experiences for the conditioning of Ra-226 sources in some Asian countries since 2000, KAERI sent an expert team to Singapore for the safe management of spent sealed sources in 2011. As a result of the conditioning, about 575.21 mCi of Am-241, Ra-226, Co-60, and Sr-90 were safely conditioned in 3 concrete lining drums with the cooperation of the KAERI expert team, the IAEA supervisor, the NEA staff and local laborers in Singapore. Some lessons were learned during the operation: (1) preparations by a local authority are very helpful for an efficient operation, (2) a preliminary inspection by an expert team is helpful for the operation, (3) brief reports before and after daily operation are useful for communication, and (4) a training opportunity is required for the sustainability of the expert team. (authors)

  2. Development of a compact laser-produced plasma soft X-ray source for radiobiology experiments

    Energy Technology Data Exchange (ETDEWEB)

    Adjei, Daniel, E-mail: nana.adjeidan@gmail.com [Institute of Optoelectronics, Military University of Technology, 2, Kaliskiego Str., 00-908 Warsaw (Poland); Radiation Protection Institute, Ghana Atomic Energy Commission, P.O. Box LG 80, Legon, Accra (Ghana); Ayele, Mesfin Getachew; Wachulak, Przemyslaw; Bartnik, Andrzej; Wegrzynski, Łukasz; Fiedorowicz, Henryk [Institute of Optoelectronics, Military University of Technology, 2, Kaliskiego Str., 00-908 Warsaw (Poland); Vyšín, Luděk [Institute of Physics, Czech Academy of Sciences, Na Slovance 2, 182 21 Prague 8 (Czech Republic); Faculty of Nuclear Sciences and Engineering Physics, Czech Technical University in Prague, Břehová 7, 115 19 Prague 1 (Czech Republic); Wiechec, Anna; Lekki, Janusz; Kwiatek, Wojciech M. [Institute of Nuclear Physics, Polish Academy of Sciences, 152, Radzikowskiego Str., 31-342 Cracow (Poland); Pina, Ladislav [Faculty of Nuclear Sciences and Engineering Physics, Czech Technical University in Prague, Břehová 7, 115 19 Prague 1 (Czech Republic); Davídková, Marie [Institute of Nuclear Physics, Czech Academy of Sciences, Řež (Czech Republic); Juha, Libor [Institute of Physics, Czech Academy of Sciences, Na Slovance 2, 182 21 Prague 8 (Czech Republic)

    2015-12-01

    A desk-top laser-produced plasma (LPP) source of soft X-rays (SXR) has been developed for radiobiology research. The source is based on a double-stream gas puff target, irradiated with the focused beam of a commercial Nd:YAG laser. The source has been optimized to get a maximum photon emission from LPP in the X-ray “water window” spectral wavelength range from 2.3 nm (i.e., an absorption edge of oxygen) to 4.4 nm (i.e., an absorption edge of carbon) (280–540 eV in photon energy units) by using argon gas-puff target and spectral filtering by free-standing thin foils. The present source delivers nanosecond pulses of soft X-rays at a fluence of about 4.2 × 10{sup 3} photons/μm{sup 2}/pulse on a sample placed inside the vacuum chamber. In this paper, the source design, radiation output characterization measurements and initial irradiation experiments are described. The source can be useful in addressing observations related to biomolecular, cellular and organisms’ sensitivity to pulsed radiation in the “water window”, where carbon atoms absorb X-rays more strongly than the oxygen, mostly present in water. The combination of the SXR source and the radiobiology irradiation layout, reported in this article, make possible a systematic investigation of relationships between direct and indirect action of ionizing radiation, an increase of a local dose in carbon-rich compartments of the cell (e.g., lipid membranes), an experimental estimation of a particular role of the Auger effect (in particular in carbon atoms) in the damage to biological systems, and the study of ionization/excitation-density (LET – Linear Energy Transfer) and dose-rate effects in radiobiology.

  3. Observation of {gamma}-sources using a new reconstruction technique in the CLUE experiment

    Energy Technology Data Exchange (ETDEWEB)

    Bartoli, B.; Bastieri, D.; Bigongiari, C.; Biral, R.; Ciocci, M.A.; Cresti, M.; Dokoutchaeva, V.; Kartashov, D.; Liello, F.; Malakhov, N.; Mariotti, M.; Marsella, G.; Menzione, A.; Paoletti, R.; Peruzzo, L.; Piccioli, A.; Pegna, R.; Rosso, F.; Saggion, A.; Sartori, G.; Sbarra, C.; Scribano, A.; Smogailov, E.; Stamerra, A.; Turini, N

    2001-04-01

    The CLUE experiment, located in La Palma island at 2200 m a.s.l., is an array of 3x3 telescope, detecting the UV (190 - 230 nm) Cherenkov light produced by atmospheric showers. Since atmospheric absorption in the UV range is higher than in the visible range, CLUE cannot apply existing algorithms normally used in IACT experiments to determine primary cosmic ray direction. In this paper we present a new method developed by CLUE. The algorithm performances were evaluated using simulated showers. Using the new technique, preliminary results of last two years observational campaigns on the Crab Nebula and on Markarian 421 are presented, showing a clear signal on both sources. The CLUE experiment collected also data with the telescopes aiming directly at the Moon: we expect improvements also on the Moon Shadow measurement adopting the new method.

  4. Observation of γ-sources using a new reconstruction technique in the CLUE experiment

    International Nuclear Information System (INIS)

    Bartoli, B.; Bastieri, D.; Bigongiari, C.; Biral, R.; Ciocci, M.A.; Cresti, M.; Dokoutchaeva, V.; Kartashov, D.; Liello, F.; Malakhov, N.; Mariotti, M.; Marsella, G.; Menzione, A.; Paoletti, R.; Peruzzo, L.; Piccioli, A.; Pegna, R.; Rosso, F.; Saggion, A.; Sartori, G.; Sbarra, C.; Scribano, A.; Smogailov, E.; Stamerra, A.; Turini, N.

    2001-01-01

    The CLUE experiment, located in La Palma island at 2200 m a.s.l., is an array of 3x3 telescope, detecting the UV (190 - 230 nm) Cherenkov light produced by atmospheric showers. Since atmospheric absorption in the UV range is higher than in the visible range, CLUE cannot apply existing algorithms normally used in IACT experiments to determine primary cosmic ray direction. In this paper we present a new method developed by CLUE. The algorithm performances were evaluated using simulated showers. Using the new technique, preliminary results of last two years observational campaigns on the Crab Nebula and on Markarian 421 are presented, showing a clear signal on both sources. The CLUE experiment collected also data with the telescopes aiming directly at the Moon: we expect improvements also on the Moon Shadow measurement adopting the new method

  5. ICP-MS measurement of natural radioactivity at LNGS

    Science.gov (United States)

    Nisi, S.; Copia, L.; Dafinei, I.; di Vacri, M. L.

    2017-10-01

    Rare events search experiments, like those dedicated to the direct evidence of dark matter or neutrinoless double beta decay, are among the most exciting challenges of modern physics. The sensitivity of such experiments is driven by the background, which depends substantially on the radiopurity of the materials used for the experimental apparatus. Cutting edge measurement techniques are needed for a fast, sensitive and efficient screening of these materials and the certification of their production. Trace element measurements of high sensitivity and quick execution are mandatory also in other fields like tracing the geographical origin of food, temporal and geographical assignment of cultural heritage or monitoring environmental radioactivity. This work is an overview of the inorganic mass spectrometry facility available at Gran Sasso National Laboratory (LNGS) for radiopure material screening and is especially focused on its ICP-MS instrumentation. Analytical methods developed to achieve lowest detection limits in different types of matrix, like metals, polymers, crystals and composite materials, are also indicated. Detection limits of 10-18gg-1 for 226Ra, 10-14gg-1 for U and Th and 10-12gg-1 for K are attained through dedicated operation conditions of the instrumentation. Details are given on the results obtained for different experiments ongoing or under construction at LNGS.

  6. Studies of an inductively coupled negative hydrogen ion radio frequency source through simulations and experiments

    International Nuclear Information System (INIS)

    Bandyopadhyay, M.

    2004-01-01

    In the frame work of a development project for ITER neutral beam injection system a radio frequency (RF) driven negative hydrogen (H-/D-) ion source, (BATMAN ion source) is developed which is designed to produce several 10s of ampere of H-/D- beam current. This PhD work has been carried out to understand and optimize BATMAN ion source. The study has been done with the help of computer simulations, modeling and experiments. The complete three dimensional Monte-Carlo computer simulation codes have been developed under the scope of this PhD work. A comprehensive description about the volume production and the surface production of H- ions is presented in the thesis along with the study results obtained from the simulations, modeling and the experiments. One of the simulations is based on the volume production of H- ions, where it calculates the density profile of the vibrationally excited H2 molecules, the density profile of H- ions and the transport probability of those H- ions along the source axis towards the grid. The other simulation studies the transport of those H- ions which are produced on the surface of the plasma grid. It is expected that if there is a plasma flow in the source, the transport of plasma components (molecules and ions) would be influenced. Experimentally it is observed that there is a convective plasma flow exists in the ion source. A transverse magnetic filter field which is present near the grid inside the ion source reduces the flow velocity. Negative ions and electrons have the same sign of charge; therefore the electrons are co-extracted with the negative ions through the grid system, which is not desirable. It is observed that a magnetic field near the grid, magnetized the electrons and therefore reduce the co-extracted electron current. It is also observed experimentally that if the plasma grid is biased positively with respect to the source body, the electron density near the plasma grid is reduced and therefore the co

  7. Determination of total selenium and Se-77 in isotopically enriched human samples by ICP-dynamic reaction cell-MS

    DEFF Research Database (Denmark)

    Sloth, Jens Jørgen; Larsen, Erik Huusfeldt; Bügel, Susanne H.

    2003-01-01

    and the digested faecal samples were diluted using an aqueous diluent containing 0.5% Triton X-100, 2% nitric acid and 3% methanol. Selenium was detected as Se-76, Se-77 and Se-80 by ICP- DRC- MS. Selenium originating from the natural isotope abundance yeast and other selenium sources from the diet was determined...

  8. Data Release Report for Source Physics Experiment 1 (SPE-1), Nevada National Security Site

    Energy Technology Data Exchange (ETDEWEB)

    Townsend, Margaret [NSTec; Mercadente, Jennifer [NSTec

    2014-04-28

    The first Source Physics Experiment shot (SPE-1) was conducted in May 2011. The explosive source was a ~100-kilogram TNT-equivalent chemical set at a depth of 60 meters. It was recorded by an extensive set of instrumentation that includes sensors both at near-field (less than 100 meters) and far-field (more than 100 meters) distances. The near-field instruments consisted of three-component accelerometers deployed in boreholes around the shot and a set of singlecomponent vertical accelerometers on the surface. The far-field network comprised a variety of seismic and acoustic sensors, including short-period geophones, broadband seismometers, three-component accelerometers, and rotational seismometers at distances of 100 meters to 25 kilometers. This report coincides with the release of these data for analysts and organizations that are not participants in this program. This report describes the first Source Physics Experiment and the various types of near-field and far-field data that are available.

  9. Skyline: an open source document editor for creating and analyzing targeted proteomics experiments.

    Science.gov (United States)

    MacLean, Brendan; Tomazela, Daniela M; Shulman, Nicholas; Chambers, Matthew; Finney, Gregory L; Frewen, Barbara; Kern, Randall; Tabb, David L; Liebler, Daniel C; MacCoss, Michael J

    2010-04-01

    Skyline is a Windows client application for targeted proteomics method creation and quantitative data analysis. It is open source and freely available for academic and commercial use. The Skyline user interface simplifies the development of mass spectrometer methods and the analysis of data from targeted proteomics experiments performed using selected reaction monitoring (SRM). Skyline supports using and creating MS/MS spectral libraries from a wide variety of sources to choose SRM filters and verify results based on previously observed ion trap data. Skyline exports transition lists to and imports the native output files from Agilent, Applied Biosystems, Thermo Fisher Scientific and Waters triple quadrupole instruments, seamlessly connecting mass spectrometer output back to the experimental design document. The fast and compact Skyline file format is easily shared, even for experiments requiring many sample injections. A rich array of graphs displays results and provides powerful tools for inspecting data integrity as data are acquired, helping instrument operators to identify problems early. The Skyline dynamic report designer exports tabular data from the Skyline document model for in-depth analysis with common statistical tools. Single-click, self-updating web installation is available at http://proteome.gs.washington.edu/software/skyline. This web site also provides access to instructional videos, a support board, an issues list and a link to the source code project.

  10. The source of monoenergetic electrons for the monitoring of spectrometer in the KATRIN neutrino experiment

    CERN Document Server

    Slezák, Martin

    The international project KATRIN (KArlsruhe TRItium Neutrino experiment) is a next-generation tritium $\\beta$-decay experiment. It is designed to measure the electron anti-neutrino mass by means of a unique electron spectrometer with sensitivity of 0.2 eV/c$^2$. This is an improvement of one order of magnitude over the last results. Important part of the measurement will rest in continuous precise monitoring of high voltage of the KATRIN main spectrometer. The monitoring will be done by means of conversion electrons emitted from a solid source based on $^{83}$Rb decay. Properties of several of these sources are studied in this thesis by means of the semiconductor $\\gamma$-ray spectroscopy. Firstly, measurement of precise energy of the 9.4 keV nuclear transition observed in $^{83}$Rb decay, from which the energy of conversion electrons is derived, is reported. Secondly, measurement of activity distribution of the solid sources by means of the Timepix detector is described. Finally, a report on measurement of r...

  11. sources

    Directory of Open Access Journals (Sweden)

    Shu-Yin Chiang

    2002-01-01

    Full Text Available In this paper, we study the simplified models of the ATM (Asynchronous Transfer Mode multiplexer network with Bernoulli random traffic sources. Based on the model, the performance measures are analyzed by the different output service schemes.

  12. LA-ICP-MS of magnetite: Methods and reference materials

    Science.gov (United States)

    Nadoll, P.; Koenig, A.E.

    2011-01-01

    Magnetite (Fe3O4) is a common accessory mineral in many geologic settings. Its variable geochemistry makes it a powerful petrogenetic indicator. Electron microprobe (EMPA) analyses are commonly used to examine major and minor element contents in magnetite. Laser ablation ICP-MS (LA-ICP-MS) is applicable to trace element analyses of magnetite but has not been widely employed to examine compositional variations. We tested the applicability of the NIST SRM 610, the USGS GSE-1G, and the NIST SRM 2782 reference materials (RMs) as external standards and developed a reliable method for LA-ICP-MS analysis of magnetite. LA-ICP-MS analyses were carried out on well characterized magnetite samples with a 193 nm, Excimer, ArF LA system. Although matrix-matched RMs are sometimes important for calibration and normalization of LA-ICP-MS data, we demonstrate that glass RMs can produce accurate results for LA-ICP-MS analyses of magnetite. Cross-comparison between the NIST SRM 610 and USGS GSE-1G indicates good agreement for magnetite minor and trace element data calibrated with either of these RMs. Many elements show a sufficiently good match between the LA-ICP-MS and the EMPA data; for example, Ti and V show a close to linear relationship with correlation coefficients, R2 of 0.79 and 0.85 respectively. ?? 2011 The Royal Society of Chemistry.

  13. Attenuation Model Using the Large-N Array from the Source Physics Experiment

    Science.gov (United States)

    Atterholt, J.; Chen, T.; Snelson, C. M.; Mellors, R. J.

    2017-12-01

    The Source Physics Experiment (SPE) consists of a series of chemical explosions at the Nevada National Security Site. SPE seeks to better characterize the influence of subsurface heterogeneities on seismic wave propagation and energy dissipation from explosions. As a part of this experiment, SPE-5, a 5000 kg TNT equivalent chemical explosion, was detonated in 2016. During the SPE-5 experiment, a Large-N array of 996 geophones (half 3-component and half z-component) was deployed. This array covered an area that includes loosely consolidated alluvium (weak rock) and weathered granite (hard rock), and recorded the SPE-5 explosion as well as 53 weight drops. We use these Large-N recordings to develop an attenuation model of the area to better characterize how geologic structures influence source energy partitioning. We found a clear variation in seismic attenuation for different rock types: high attenuation (low Q) for alluvium and low attenuation (high Q) for granite. The attenuation structure correlates well with local geology, and will be incorporated into the large simulation effort of the SPE program to validate predictive models. (LA-UR-17-26382)

  14. Computer simulation of ICP spectra: A new tool for the study of excitation, emission, and line overlap

    International Nuclear Information System (INIS)

    Blades, M.W.; Burton, L.L.

    1986-01-01

    It is well known that the relatively high temperature of ICP sources provides an excitation environment relatively free from dissociation and vaporization interferences and, in addition, produces intense analyte line spectra and hence high analytical sensitivity. However, this feature also introduces the potential for spectral overlaps from sample concomitants. The degree to which an analyte spectral line intensity can be corrected for interfering spectral overlaps depends on many factors including spectrometer resolution, sample composition and ICP operating conditions. The authors have been using a computer program to assist them in the study of ICP analyte emission spectra. This program is being used to study the spectral distribution of line intensity information and also to do detailed investigations on spectral overlaps in complex sample mixtures. As input data the program uses tabulated wavelengths, transition probabilities (gA values), partition functions, excitation energies of the transitions, ionization energy, temperature, and Doppler and Stark linewidths

  15. Metronome LKM: An open source virtual keyboard driver to measure experiment software latencies.

    Science.gov (United States)

    Garaizar, Pablo; Vadillo, Miguel A

    2017-10-01

    Experiment software is often used to measure reaction times gathered with keyboards or other input devices. In previous studies, the accuracy and precision of time stamps has been assessed through several means: (a) generating accurate square wave signals from an external device connected to the parallel port of the computer running the experiment software, (b) triggering the typematic repeat feature of some keyboards to get an evenly separated series of keypress events, or (c) using a solenoid handled by a microcontroller to press the input device (keyboard, mouse button, touch screen) that will be used in the experimental setup. Despite the advantages of these approaches in some contexts, none of them can isolate the measurement error caused by the experiment software itself. Metronome LKM provides a virtual keyboard to assess an experiment's software. Using this open source driver, researchers can generate keypress events using high-resolution timers and compare the time stamps collected by the experiment software with those gathered by Metronome LKM (with nanosecond resolution). Our software is highly configurable (in terms of keys pressed, intervals, SysRq activation) and runs on 2.6-4.8 Linux kernels.

  16. Long-term operation experience with 2 ECR ion sources and planned extensions at HIT

    International Nuclear Information System (INIS)

    Winkelmann, T.; Cee, R.; Haberer, T.; Naas, B.; Peters, A.

    2012-01-01

    The HIT (Heidelberg Ion Beam Therapy Center) is the first treatment facility at a hospital in Europe where patients can be treated with protons and carbon ions. Since the commissioning starting in 2006 two 14.5 GHz electron cyclotron resonance ion sources are routinely used to produce a variety of ion beams from protons up to oxygen. The operating time is 330 days per year, our experience after three years of continuous operation will be presented. In the future a helium beam for patient treatment is requested, therefore a third ion source will be integrated. This third ECR source with a newly designed extraction system and a spectrometer line will be installed at a test-bench to commission and validate this section. Different test settings are foreseen to study helium operation as well as enhanced parameter sets for proton and carbon beams in combination with a modified beam transport line for higher transmission efficiency. An outlook to the possible integration scheme of the new ion source into the production facility will be discussed. The paper is followed by the associated poster. (authors)

  17. A tunable, linac based, intense, broad-band THz source forpump-probe experiments

    Energy Technology Data Exchange (ETDEWEB)

    Schmerge, J. [SLAC National Accelerator Lab., Menlo Park, CA (United States); Adolphsen, C. [SLAC National Accelerator Lab., Menlo Park, CA (United States); Corbett, J. [SLAC National Accelerator Lab., Menlo Park, CA (United States); Dolgashev, V. [SLAC National Accelerator Lab., Menlo Park, CA (United States); Durr, H. [SLAC National Accelerator Lab., Menlo Park, CA (United States); Fazio, M. [SLAC National Accelerator Lab., Menlo Park, CA (United States); Fisher, A. [SLAC National Accelerator Lab., Menlo Park, CA (United States); Frisch, J. [SLAC National Accelerator Lab., Menlo Park, CA (United States); Gaffney, K. [SLAC National Accelerator Lab., Menlo Park, CA (United States); Guehr, M. [SLAC National Accelerator Lab., Menlo Park, CA (United States); Hastings, J. [SLAC National Accelerator Lab., Menlo Park, CA (United States); Hettel, B. [SLAC National Accelerator Lab., Menlo Park, CA (United States); Hoffmann, M. [SLAC National Accelerator Lab., Menlo Park, CA (United States); Hogan, M. [SLAC National Accelerator Lab., Menlo Park, CA (United States); Holtkamp, N. [SLAC National Accelerator Lab., Menlo Park, CA (United States); Huang, X. [SLAC National Accelerator Lab., Menlo Park, CA (United States); Huang, Z. [SLAC National Accelerator Lab., Menlo Park, CA (United States); Kirchmann, P. [SLAC National Accelerator Lab., Menlo Park, CA (United States); LaRue, J. [SLAC National Accelerator Lab., Menlo Park, CA (United States); Limborg, C. [SLAC National Accelerator Lab., Menlo Park, CA (United States); Lindenberg, A. [SLAC National Accelerator Lab., Menlo Park, CA (United States); Loos, H. [SLAC National Accelerator Lab., Menlo Park, CA (United States); Maxwell, T. [SLAC National Accelerator Lab., Menlo Park, CA (United States); Nilsson, A. [SLAC National Accelerator Lab., Menlo Park, CA (United States); Raubenheimer, T. [SLAC National Accelerator Lab., Menlo Park, CA (United States); Reis, D. [SLAC National Accelerator Lab., Menlo Park, CA (United States); Ross, M. [SLAC National Accelerator Lab., Menlo Park, CA (United States); Shen, Z. -X. [SLAC National Accelerator Lab., Menlo Park, CA (United States); Stupakov, G. [SLAC National Accelerator Lab., Menlo Park, CA (United States); Tantawi, S. [SLAC National Accelerator Lab., Menlo Park, CA (United States); Tian, K. [SLAC National Accelerator Lab., Menlo Park, CA (United States); Wu, Z. [SLAC National Accelerator Lab., Menlo Park, CA (United States); Xiang, D. [SLAC National Accelerator Lab., Menlo Park, CA (United States); Yakimenko, V. [SLAC National Accelerator Lab., Menlo Park, CA (United States)

    2015-02-02

    We propose an intense THz source with tunable frequency and bandwidth that can directly interact with the degrees of freedom that determine the properties of materials and thus provides a new tool for controlling and directing these ultrafast processes as well as aiding synthesis of new materials with new functional properties. This THz source will broadly impact our understanding of dynamical processes in matter at the atomic-scale and in real time. Established optical pumping schemes using femtosecond visible frequency laser pulses for excitation are extended into the THz frequency regime thereby enabling resonant excitation of bonds in correlated solid state materials (phonon pumping), to drive low energy electronic excitations, to trigger surface chemistry reactions, and to all-optically bias a material with ultrashort electric fields or magnetic fields. A linac-based THz source can supply stand-alone experiments with peak intensities two orders of magnitude stronger than existing laser-based sources, but when coupled with atomic-scale sensitive femtosecond x-ray probes it opens a new frontier in ultrafast science with broad applications to correlated materials, interfacial and liquid phase chemistry, and materials in extreme conditions.

  18. The French Experience Regarding Peer Reviews to Improve the Safety and Security of Radioactive Sources

    International Nuclear Information System (INIS)

    Lachaume, J.-L.; Bélot, G.

    2015-01-01

    France has a 50 year history of control over radioactive sources. Convinced that peer reviews may be helpful to improve any regulatory system, France decided to experience a ‘full scope’ Integrated Regulatory Review Service mission in 2006 and its follow-up mission in 2009, including a review of the implementation of the Code of Conduct. The reviews, interviews and observations performed during these missions enabled the experts to have a thorough knowledge of the French system and to highlight its strengths and ways for improvements. Following these reviews, France decided to rely on its good practices, extend them as much as possible and to define, implement and address an action plan to improve its regulatory control over radioactive sources, while maintaining the prime responsibility on the operators. While good practices in the tracking of sources were maintained and slight evolutions were conducted in the safety regulations, licensing process, and inspection and enforcement actions, the major outcome of these reviews will obviously consist of the entrustment of the French Nuclear Safety Authority with the role of the regulatory authority for the security of radioactive sources and the implementation of dedicated provisions. (author)

  19. Locating the Source of Atmospheric Contamination Based on Data From the Kori Field Tracer Experiment

    Directory of Open Access Journals (Sweden)

    Piotr Kopka

    2015-01-01

    Full Text Available Accidental releases of hazardous material into the atmosphere pose high risks to human health and the environment. Thus it would be valuable to develop an emergency reaction system which can recognize the probable location of the source based only on concentrations of the released substance as reported by a network of sensors. We apply a methodology combining Bayesian inference with Sequential Monte Carlo (SMC methods to the problem of locating the source of an atmospheric contaminant. The input data for this algorithm are the concentrations of a given substance gathered continuously in time. We employ this algorithm to locating a contamination source using data from a field tracer experiment covering the Kori nuclear site and conducted in May 2001. We use the second-order Closure Integrated PUFF Model (SCIPUFF of atmospheric dispersion as the forward model to predict concentrations at the sensors' locations. We demonstrate that the source of continuous contamination may be successfully located even in the very complicated, hilly terrain surrounding the Kori nuclear site. (original abstract

  20. Association of glass fragments by their trace elemental content using ICP-MS and LA-ICP-MS in the analysis scheme

    Science.gov (United States)

    Almirall, Jose R.; Montero, Shirly; Furton, Kenneth G.

    2002-08-01

    The importance of glass as evidence of association between a crime event and a suspect has been recognized for some time. Glass is a fragile material that is often found at the scenes of crimes such as burglaries, hit-and-run accidents and violent crime offenses. The physical and chemical properties of glass can be used to differentiate between possible sources and as evidence of association between two fragments of glass thought to originate from the same source. Refractive index (RI) comparisons have been used for this purpose but due to the improved control over glass manufacturing processes, RI values often cannot differentiate glasses, even if the glass originates from different sources. Elemental analysis methods such as NAA, XRF, ICP-AES, and Inductively Coupled Plasma Mass Spectrometry (ICP-MS) have also been used for the comparison of trace elemental compositions and these techniques have been shown to provide an improvement in the discrimination of glass fragments over RI comparisons alone. The multi-element capability and the sensitivity of ICP-MS combined with the simplified sample introduction of laser ablation prior to ion detection provides for an excellent and relatively non-destructive technique for elemental analysis of glass fragments. The methodology for solution analysis (digestion procedure) and solid sample analysis (laser ablation) of glass is reported and the analytical results are compared. An isotope dilution method is also reported as a high precision technique for elemental analysis of glass fragments. The optimum sampling parameters for laser ablation, for semi-quantitative analysis and element ratio comparisons are also presented. Finally, the results of a case involving the breaking of 15 vehicle windows in an airport parking lot and the association of a suspect to the breakings by the glass fragments found on his person are also presented.

  1. Optimization of a fluorescence X-ray source and background studies for a prospective CNNS experiment

    Energy Technology Data Exchange (ETDEWEB)

    Zoeller, Andreas; Ciemniak, Christian; Feilitzsch, Franz von; Guetlein, Achim; Haag, Nils; Hofmann, Martin; Isaila, Christian; Lanfranchi, Jean-Come; Oberauer, Lothar; Pfister, Sebastian; Potzel, Walter; Roth, Sabine; Schoenert, Stefan; Sivers, Moritz von; Strauss, Raimund [Technische Universitaet Muenchen, Physik-Department, E15 (Germany); Lachenmaier, Tobias [Eberhard Karls Universitaet, Tuebingen (Germany)

    2011-07-01

    Coherent Neutrino Nucleus Scattering (CNNS) is predicted by the Standard Model but hasn't been measured yet. A good background discrimination and shielding is essential for the achievement of a prospective experiment. We show the results of simulations for background discrimination and suppression using a myon veto system in combination with a shielding around a cryostat. With CNNS, the expected nuclear recoil energy for reactor anti-neutrinos is in the range of source within this energy region is necessary. Two different methods to create fluorescence are discussed and measured energy spectra will be shown. Finally results of an improved fluorescence x-ray source with nine clearly separated energy lines between {proportional_to}1 keV and 6.5 keV are shown.

  2. Particle generation methods applied in large-scale experiments on aerosol behaviour and source term studies

    International Nuclear Information System (INIS)

    Swiderska-Kowalczyk, M.; Gomez, F.J.; Martin, M.

    1997-01-01

    In aerosol research aerosols of known size, shape, and density are highly desirable because most aerosols properties depend strongly on particle size. However, such constant and reproducible generation of those aerosol particles whose size and concentration can be easily controlled, can be achieved only in laboratory-scale tests. In large scale experiments, different generation methods for various elements and compounds have been applied. This work presents, in a brief from, a review of applications of these methods used in large scale experiments on aerosol behaviour and source term. Description of generation method and generated aerosol transport conditions is followed by properties of obtained aerosol, aerosol instrumentation used, and the scheme of aerosol generation system-wherever it was available. An information concerning aerosol generation particular purposes and reference number(s) is given at the end of a particular case. These methods reviewed are: evaporation-condensation, using a furnace heating and using a plasma torch; atomization of liquid, using compressed air nebulizers, ultrasonic nebulizers and atomization of liquid suspension; and dispersion of powders. Among the projects included in this worked are: ACE, LACE, GE Experiments, EPRI Experiments, LACE-Spain. UKAEA Experiments, BNWL Experiments, ORNL Experiments, MARVIKEN, SPARTA and DEMONA. The aim chemical compounds studied are: Ba, Cs, CsOH, CsI, Ni, Cr, NaI, TeO 2 , UO 2 Al 2 O 3 , Al 2 SiO 5 , B 2 O 3 , Cd, CdO, Fe 2 O 3 , MnO, SiO 2 , AgO, SnO 2 , Te, U 3 O 8 , BaO, CsCl, CsNO 3 , Urania, RuO 2 , TiO 2 , Al(OH) 3 , BaSO 4 , Eu 2 O 3 and Sn. (Author)

  3. Deriving profiles of incident and scattered neutrons for TOF experiments with the spallation sources

    International Nuclear Information System (INIS)

    Watanabe, Hidehiro

    1993-01-01

    A formula that closely matches the incident profile of epi-thermal and thermal neutrons for time of flight experiments carried out with a spallation neutron source and moderator scheme is derived based on the slowing-down and diffusing-out processes in a moderator. This analytical description also enables us to predict burst-function profiles; these profiles are verified by a comparison with a diffraction pattern. The limits of the analytical model are discussed through the predictable peak position shift brought about by the slowing-down process. (orig.)

  4. Experience with low-alpha lattices at the Diamond Light Source

    Directory of Open Access Journals (Sweden)

    I. P. S. Martin

    2011-04-01

    Full Text Available In this paper we present the experience at Diamond Light Source in the design, implementation, and operation of low momentum compaction factor lattices for the generation of short x-ray pulses and coherent THz radiation. The effects of higher-order terms in the expansion of the momentum compaction factor on beam dynamics are reviewed from a theoretical point of view, and the details of both high- and low-emittance solutions at Diamond are discussed. Measurements taken to characterize the lattices under a variety of machine conditions are presented, along with the practical limitations that exist as the momentum compaction factor is made to approach zero.

  5. Experience with the source evaluation board method of procuring technical components for the Fermilab Main Injector

    International Nuclear Information System (INIS)

    Harding, D.J.; Collins, J.P.; Kobliska, G.R.; Chester, N.S.; Pewitt, E.G.; Fowler, W.B.

    1993-01-01

    Fermilab has adopted the Source Evaluation Board (SEB) method for procuring certain major technical components of the Fermilab Main Injector. The SEB procedure is designed to ensure the efficient and effective expenditure of Government funds at the same time that it optimizes the opportunity for attainment of project objectives. A qualitative trade-off is allowed between price and technical factors. The process involves a large amount of work and is only justified for a very limited number of procurements. Fermilab has gained experience with the SEB process in awarding subcontracts for major subassemblies of the Fermilab Main Injector dipoles

  6. Exploding metal film active anode source experiments on the LION extractor ion diode

    International Nuclear Information System (INIS)

    Rondeau, G.D.; Bordonaro, G.J.; Greenly, J.B.; Hammer, D.A.

    1989-01-01

    In this paper the authors report results using an extractor geometry magnetically insulated ion diode on the 0.5 TW LION accelerator. Experiments with an exploding metal film active anode plasma source (EMFAAPS) have shown that intense beams with significantly improved turn-on time compared to epoxy-filled-groove anodes can be produced. A new geometry, in which a plasma switch is used to provide the current path that explodes the thin film anode, has improved the ion efficiency (to typically 70%) compared with the previous scheme in which an electron collector on the anode provided this current. Leakage electron current is reduced when no collector is used

  7. [Enhancement effect of double-beam laser processed aqueous solution on ICP emission spectrum].

    Science.gov (United States)

    Chen, Jin-zhong; Xu, Li-jing; Su, Hong-xin; Li, Xu; Wang, Shu-fang

    2015-01-01

    In order to change the physical properties of aqueous solution and improve the radiation intensity of the ICP emission spectrum, the effects of different laser power density and irradiation time on the surface tension and viscosity of aqueous solution were investigated by using near infrared laser at 976 nm and CO2 laser at 10. 6 µm to irradiate aqueous solution orthogonally, then the enhancement of ICP spectral intensity with processed solution was discussed. The results showed that the surface tension and viscosity of aqueous solution reduced by 42. 13% and 14. 03% compared with the untreated, and the atomization efficiency increased by 51.26% at the laser power density 0. 265 7 W . cm-2 of 976 nm and 0. 206 9 W . cm-2 of CO2 laser with 40 min irradiation time. With the optimized aqueous solution introduced into the ICP source, the spectral line intensity of sample elements As, Cd, Cr, Hg and Pb was enhanced by 46.29%, 94. 65%, 30. 76%, 33.07% and 94. 58% compared to the untreated aqueous solution, while the signal-to-background ratio increased by 43. 84%, 85. 35%, 28. 71%, 34. 37% and 90. 91%, respectively. Plasma temperature and electron density also increased by 5. 94% and 1. 18% respectively. It is obvious that the method of double-beam laser orthogonal irradiation on solution can reduce the surface tension and viscosity of aqueous solution significantly, and raise the radiationintensity of ICP source, and will provide a better condition for detecting the trace heavy metal elements in water samples.

  8. Fuel plate stability experiments and analysis for the Advanced Neutron Source

    International Nuclear Information System (INIS)

    Swinson, W.F.; Battiste, R.L.; Luttrell, C.R.; Yahr, G.T.

    1992-01-01

    The planned Advanced Neutron Source (ANS) and several existing reactors use closely spaced arrays of involute shaped fuel-plates which are cooled by water flowing through the channels between the plates. There is concern that at certain coolant flow velocities adjacent plates may deflect and touch, with resulting failure of the plates. Experiments have been conducted at the Oak Ridge National Laboratory to examine this potential phenomenon. Results of the experiments and comparison with analytical predictions are reported in this paper. The tests were conducted using full scale epoxy plate models of the aluminum/uranium silicide ANS involute shaped fuel plates. Use of epoxy plates and model theory allowed lower flow velocities and pressures to explore the potential failure mechanism. Plate deflections and channel pressures as function of the flow velocity are examined. Comparisons with mathematical models are noted. 12 refs

  9. Fuel plate stability experiments and analysis for the Advanced Neutron Source

    International Nuclear Information System (INIS)

    Swinson, W.F.; Battiste, R.L.; Luttrell, C.R.; Yahr, G.T.

    1993-05-01

    The planned reactor for the Advanced Neutron Source (ANS) will use closely spaced arrays of involute-shaped fuel plates that will be cooled by water flowing through the channels between the plates. There is concern that at certain coolant flow velocities, adjacent plates may deflect and touch, with resulting failure of the plates. Experiments have been conducted at the Oak Ridge National Laboratory to examine this potential phenomenon. Results of the experiments and comparison with analytical predictions are reported. The tests were conducted using full-scale epoxy plate models of the aluminum/uranium silicide ANS involute-shaped fuel plates. Use of epoxy plates and model theory allowed lower flow velocities and pressures to explore the potential failure mechanism. Plate deflections and channel pressures as functions of the flow velocity are examined. Comparisons with mathematical models are noted

  10. Advisory Committee on human radiation experiments. Supplemental Volume 2a, Sources and documentation appendices. Final report

    International Nuclear Information System (INIS)

    1995-01-01

    This large document provides a catalog of the location of large numbers of reports pertaining to the charge of the Presidential Advisory Committee on Human Radiation Research and is arranged as a series of appendices. Titles of the appendices are Appendix A- Records at the Washington National Records Center Reviewed in Whole or Part by DoD Personnel or Advisory Committee Staff; Appendix B- Brief Descriptions of Records Accessions in the Advisory Committee on Human Radiation Experiments (ACHRE) Research Document Collection; Appendix C- Bibliography of Secondary Sources Used by ACHRE; Appendix D- Brief Descriptions of Human Radiation Experiments Identified by ACHRE, and Indexes; Appendix E- Documents Cited in the ACHRE Final Report and other Separately Described Materials from the ACHRE Document Collection; Appendix F- Schedule of Advisory Committee Meetings and Meeting Documentation; and Appendix G- Technology Note

  11. Advisory Committee on human radiation experiments. Supplemental Volume 2a, Sources and documentation appendices. Final report

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    1995-01-01

    This large document provides a catalog of the location of large numbers of reports pertaining to the charge of the Presidential Advisory Committee on Human Radiation Research and is arranged as a series of appendices. Titles of the appendices are Appendix A- Records at the Washington National Records Center Reviewed in Whole or Part by DoD Personnel or Advisory Committee Staff; Appendix B- Brief Descriptions of Records Accessions in the Advisory Committee on Human Radiation Experiments (ACHRE) Research Document Collection; Appendix C- Bibliography of Secondary Sources Used by ACHRE; Appendix D- Brief Descriptions of Human Radiation Experiments Identified by ACHRE, and Indexes; Appendix E- Documents Cited in the ACHRE Final Report and other Separately Described Materials from the ACHRE Document Collection; Appendix F- Schedule of Advisory Committee Meetings and Meeting Documentation; and Appendix G- Technology Note.

  12. An open source/real-time atomic force microscope architecture to perform customizable force spectroscopy experiments.

    Science.gov (United States)

    Materassi, Donatello; Baschieri, Paolo; Tiribilli, Bruno; Zuccheri, Giampaolo; Samorì, Bruno

    2009-08-01

    We describe the realization of an atomic force microscope architecture designed to perform customizable experiments in a flexible and automatic way. Novel technological contributions are given by the software implementation platform (RTAI-LINUX), which is free and open source, and from a functional point of view, by the implementation of hard real-time control algorithms. Some other technical solutions such as a new way to estimate the optical lever constant are described as well. The adoption of this architecture provides many degrees of freedom in the device behavior and, furthermore, allows one to obtain a flexible experimental instrument at a relatively low cost. In particular, we show how such a system has been employed to obtain measures in sophisticated single-molecule force spectroscopy experiments [Fernandez and Li, Science 303, 1674 (2004)]. Experimental results on proteins already studied using the same methodologies are provided in order to show the reliability of the measure system.

  13. NEAR FIELD MODELING OF SPE1 EXPERIMENT AND PREDICTION OF THE SECOND SOURCE PHYSICS EXPERIMENTS (SPE2)

    Energy Technology Data Exchange (ETDEWEB)

    Antoun, T; Xu, H; Vorobiev, O; Lomov, I

    2011-10-20

    Motion along joints and fractures in the rock has been proposed as one of the sources of near-source shear wave generation, and demonstrating the validity of this hypothesis is a focal scientific objective of the source physics experimental campaign in the Climax Stock granitic outcrop. A modeling effort has been undertaken by LLNL to complement the experimental campaign, and over the long term provide a validated computation capability for the nuclear explosion monitoring community. The approach involves performing the near-field nonlinear modeling with hydrodynamic codes (e.g., GEODYN, GEODYN-L), and the far-field seismic propagation with an elastic wave propagation code (e.g., WPP). the codes will be coupled together to provide a comprehensive source-to-sensor modeling capability. The technical approach involves pre-test predictions of each of the SPE experiments using their state of the art modeling capabilities, followed by code improvements to alleviate deficiencies identified in the pre-test predictions. This spiral development cycle wherein simulations are used to guide experimental design and the data from the experiment used to improve the models is the most effective approach to enable a transition from the descriptive phenomenological models in current use to the predictive, hybrid physics models needed for a science-based modeling capability for nuclear explosion monitoring. The objective of this report is to describe initial results of non-linear motion predictions of the first two SPE shots in the Climax Stock: a 220-lb shot at a depth of 180 ft (SPE No.1), and a 2570-lb shot at a depth of 150 ft (SPE No.2). The simulations were performed using the LLNL ensemble granite model, a model developed to match velocity and displacement attenuation from HARDHAT, PILE DRIVER, and SHOAL, as well as Russian and French nuclear test data in granitic rocks. This model represents the state of the art modeling capabilities as they existed when the SPE campaign was

  14. Fundamental and applied measurements in ICP MS

    International Nuclear Information System (INIS)

    Carter, Julian Robert

    2002-01-01

    Fundamental and applied aspects of ICP-MS have been investigated to gain an increased understanding of the technique and improve on its analytical capabilities. Dissociation temperatures of polyatomic ions were calculated using a double-focusing sector instrument, to obtain more reliable mass spectral data with controlled vapour introduction via a Dreschel bottle to allow accurate calculation of the ingredients in the plasma. The equilibrium temperature for the plasma, operated at 1280 W calculated using CO + and C 2 + as the thermometric probes, was c.a. 5800 - 7400 K, while using ArO + and ArC + as the thermometric probes the temperature calculated was c.a. 2000 - 7000 K. Calculated dissociation temperatures were used to elucidate the site of formation of these ions. Results confirmed that strongly bound ions such as CO + and C 2 + were formed in the plasma whereas weakly bound ions such as ArO + and ArC + were formed in the interface region due to gross deviation of the calculated temperatures from those expected for a system in thermal equilibrium. The use of helium gas in a hexapole collision cell attenuated the signals of ArH + Ar + , ArO + , ArC + , ArCl + and Ar 2 + allowing improved determination of 39 K + , 40 Ca + , 56 Fe + , 52 Cr + , 75 As + and 80 Se + in standard solutions. The use of the hexapole collision cell also resulted in an enhancement of analyte signals due to the thermalisation of the ion beam. The ion kinetic energy of ions sampled from the plasma and those sampled from the skimmer cone were determined using a modified lens stack to assess the significance for memory effects of material deposited on the skimmer cone. The most probable kinetic energy of Be + ions sampled from the skimmer cone was found to be 2.4 eV, which was considerably lower than the most probable kinetic energy of Be + ions sampled from the plasma, which was found to be 9.5 eV. The low kinetic energy of the ions deposited on the skimmer cone means they will only

  15. Fundamental and applied measurements in ICP MS

    Energy Technology Data Exchange (ETDEWEB)

    Carter, Julian Robert

    2002-07-01

    Fundamental and applied aspects of ICP-MS have been investigated to gain an increased understanding of the technique and improve on its analytical capabilities. Dissociation temperatures of polyatomic ions were calculated using a double-focusing sector instrument, to obtain more reliable mass spectral data with controlled vapour introduction via a Dreschel bottle to allow accurate calculation of the ingredients in the plasma. The equilibrium temperature for the plasma, operated at 1280 W calculated using CO{sup +} and C{sub 2}{sup +} as the thermometric probes, was c.a. 5800 - 7400 K, while using ArO{sup +} and ArC{sup +} as the thermometric probes the temperature calculated was c.a. 2000 - 7000 K. Calculated dissociation temperatures were used to elucidate the site of formation of these ions. Results confirmed that strongly bound ions such as CO{sup +} and C{sub 2}{sup +} were formed in the plasma whereas weakly bound ions such as ArO{sup +} and ArC{sup +} were formed in the interface region due to gross deviation of the calculated temperatures from those expected for a system in thermal equilibrium. The use of helium gas in a hexapole collision cell attenuated the signals of ArH{sup +} Ar{sup +}, ArO{sup +}, ArC{sup +}, ArCl{sup +} and Ar{sub 2}{sup +} allowing improved determination of {sup 39}K{sup +}, {sup 40}Ca{sup +}, {sup 56}Fe{sup +}, {sup 52}Cr{sup +}, {sup 75}As{sup +} and {sup 80}Se{sup +} in standard solutions. The use of the hexapole collision cell also resulted in an enhancement of analyte signals due to the thermalisation of the ion beam. The ion kinetic energy of ions sampled from the plasma and those sampled from the skimmer cone were determined using a modified lens stack to assess the significance for memory effects of material deposited on the skimmer cone. The most probable kinetic energy of Be{sup +} ions sampled from the skimmer cone was found to be 2.4 eV, which was considerably lower than the most probable kinetic energy of Be{sup +} ions

  16. LMFBR source term experiments in the Fuel Aerosol Simulant Test (FAST) facility

    International Nuclear Information System (INIS)

    Petrykowski, J.C.; Longest, A.W.

    1985-01-01

    The transport of uranium dioxide (UO 2 ) aerosol through liquid sodium was studied in a series of ten experiments in the Fuel Aerosol Simulant Test (FAST) facility at Oak Ridge National Laboratory (ORNL). The experiments were designed to provide a mechanistic basis for evaluating the radiological source term associated with a postulated, energetic core disruptive accident (CDA) in a liquid metal fast breeder reactor (LMFBR). Aerosol was generated by capacitor discharge vaporization of UO 2 pellets which were submerged in a sodium pool under an argon cover gas. Measurements of the pool and cover gas pressures were used to study the transport of aerosol contained by vapor bubbles within the pool. Samples of cover gas were filtered to determine the quantity of aerosol released from the pool. The depth at which the aerosol was generated was found to be the most critical parameter affecting release. The largest release was observed in the baseline experiment where the sample was vaporized above the sodium pool. In the nine ''undersodium'' experiments aerosol was generated beneath the surface of the pool at depths varying from 30 to 1060 mm. The mass of aerosol released from the pool was found to be a very small fraction of the original specimen. It appears that the bulk of aerosol was contained by bubbles which collapsed within the pool. 18 refs., 11 figs., 4 tabs

  17. A new blanket tritium recovery experiment with intense DT neutron source at JAEA/FNS

    Energy Technology Data Exchange (ETDEWEB)

    Ochiai, Kentaro, E-mail: ochiai.kentaro@jaea.go.jp [Japan Atomic Energy Agency, 2-166 Omotedate Obuchi, Rokkasho, Aomori 039-3212 (Japan); Edao, Yuki [Japan Atomic Energy Agency, 2-4 Shirane Shirakata, Tokai, Ibaraki 319-1195 (Japan); Hoshino, Tsuyoshi [Japan Atomic Energy Agency, 2-166 Omotedate Obuchi, Rokkasho, Aomori 039-3212 (Japan); Kawamura, Yoshinori [Japan Atomic Energy Agency, 801-1 Mukoyama, Naka, Ibaraki 311-0193 (Japan); Ohta, Masayuki; Kwon, Saerom; Konno, Chikara [Japan Atomic Energy Agency, 2-4 Shirane Shirakata, Tokai, Ibaraki 319-1195 (Japan)

    2016-11-01

    Highlights: • For detail investigation of the tritium recovery performance on the fusion reactor blanket, we have started a new blanket tritium recovery experiment with ionization chamber at JAEA/FNS. • A new improved container was provided for the appropriate tritium measurement by IC and also utilized for the enhancement of TPR in the new container. The TPR was calculated with a calculation code MCNP5 and some typical nuclear data libraries and then the radioactivity of the tritium recovery with LSC corresponded with that of calculation. • The tritium release curves by the IC outputs are similar to those by the LSC output. However, it was indicated that the quantitative measurement by IC needed further improvement for the tritium recovery. - Abstract: We have performed the tritium release experiment on the fusion reactor blanket at JAEA/FNS since 2009, and then clarified the ratio of tritium release and the recovered tritium chemical form. In order to acquire the detailed tritium recovery performances, we have started a new blanket tritium recovery experiment with ionization chamber (IC) at JAEA/FNS. For the appropriate tritium measurement with IC, we improved the experimental container and carried out with an intense DT neutron source at JAEA/FNS. From our new experiment, the tritium recovery radioactivity from the LSC measurement corresponds with the calculation within 6%. However, it was pointed out that further improvement in the quantitative tritium measurement by IC method was needed.

  18. Source-space EEG neurofeedback links subjective experience with brain activity during effortless awareness meditation.

    Science.gov (United States)

    van Lutterveld, Remko; Houlihan, Sean D; Pal, Prasanta; Sacchet, Matthew D; McFarlane-Blake, Cinque; Patel, Payal R; Sullivan, John S; Ossadtchi, Alex; Druker, Susan; Bauer, Clemens; Brewer, Judson A

    2017-05-01

    Meditation is increasingly showing beneficial effects for psychiatric disorders. However, learning to meditate is not straightforward as there are no easily discernible outward signs of performance and thus no direct feedback is possible. As meditation has been found to correlate with posterior cingulate cortex (PCC) activity, we tested whether source-space EEG neurofeedback from the PCC followed the subjective experience of effortless awareness (a major component of meditation), and whether participants could volitionally control the signal. Sixteen novice meditators and sixteen experienced meditators participated in the study. Novice meditators were briefly trained to perform a basic meditation practice to induce the subjective experience of effortless awareness in a progressively more challenging neurofeedback test-battery. Experienced meditators performed a self-selected meditation practice to induce this state in the same test-battery. Neurofeedback was provided based on gamma-band (40-57Hz) PCC activity extracted using a beamformer algorithm. Associations between PCC activity and the subjective experience of effortless awareness were assessed by verbal probes. Both groups reported that decreased PCC activity corresponded with effortless awareness (Pneurofeedback to link an objective measure of brain activity with the subjective experience of effortless awareness, and suggest potential utility of this paradigm as a tool for meditation training. Copyright © 2016 Elsevier Inc. All rights reserved.

  19. Assessment of In Situ Time Resolved Shock Experiments at Synchrotron Light Sources*

    Science.gov (United States)

    Belak, J.; Ilavsky, J.; Hessler, J. P.

    2005-07-01

    Prior to fielding in situ time resolved experiments of shock wave loading at the Advanced Photon Source, we have performed feasibility experiments assessing a single photon bunch. Using single and poly-crystal Al, Ti, V and Cu shock to incipient spallation on the gas gun, samples were prepared from slices normal to the spall plane of thickness 100-500 microns. In addition, single crystal Al of thickness 500 microns was shocked to incipient spallation and soft recovered using the LLNL e-gun mini-flyer system. The e-gun mini-flyer impacts the sample target producing a 10's ns flat-top shock transient. Here, we present results for imaging, small-angle scattering (SAS), and diffraction. In particular, there is little SAS away from the spall plane and significant SAS at the spall plane, demonstrating the presence of sub-micron voids. * Use of the Advanced Photon Source was supported by the U. S. Department of Energy, Office of Science, Office of Basic Energy Sciences, under Contract No. W-31-109-Eng-38 and work performed under the auspices of the U.S. Department of Energy by University of California, Lawrence Livermore National Laboratory under Contract W-7405-Eng-48.

  20. Memory sources of dreams: the incorporation of autobiographical rather than episodic experiences.

    Science.gov (United States)

    Malinowski, Josie E; Horton, Caroline L

    2014-08-01

    The present study aimed to explore autobiographical memories (long-lasting memories about the self) and episodic memories (memories about discrete episodes or events) within dream content. We adapted earlier episodic memory study paradigms and reinvestigated the incorporation of episodic memory sources into dreams, operationalizing episodic memory as featuring autonoetic consciousness, which is the feeling of truly re-experiencing or reliving a past event. Participants (n = 32) recorded daily diaries and dream diaries, and reported on wake-dream relations for 2 weeks. Using a new scale, dreams were rated for their episodic richness, which categorized memory sources of dreams as being truly episodic (featuring autonoetic consciousness), autobiographical (containing segregated features of experiences that pertained to waking life) or otherwise. Only one dream (0.5%) was found to contain an episodic memory. However, the majority of dreams (>80%) were found to contain low to moderate incorporations of autobiographical memory features. These findings demonstrate the inactivity of intact episodic memories, and emphasize the activity of autobiographical memory and processing within dreams. Taken together, this suggests that memories for personal experiences are experienced fragmentarily and selectively during dreaming, perhaps in order to assimilate these memories into the autobiographical memory schema. © 2014 European Sleep Research Society.

  1. A polarized hydrogen/deuterium atomic beam source for internal target experiments

    International Nuclear Information System (INIS)

    Szczerba, D.; Buuren, L.D. van; Brand, J.F.J. van den; Bulten, H.J.; Ferro-Luzzi, M.; Klous, S.; Kolster, H.; Lang, J.; Mul, F.; Poolman, H.R.; Simani, M.C.

    2000-01-01

    A high-brightness hydrogen/deuterium atomic beam source is presented. The apparatus, previously used in electron scattering experiments with tensor-polarized deuterium (Ferro-Luzzi et al., Phys. Rev. Lett. 77 (1996) 2630; van den Brand et al., Phys. Rev. Lett. 78 (1997) 1235; Zhou et al., Phys. Rev. Lett. 82 (1998) 687; Bouwhuis et al., Phys. Rev. Lett. 82 (1999) 3755), was configured as a source for internal target experiments to measure single- and double-polarization observables, with either polarized hydrogen or vector/tensor polarized deuterium. The atomic beam intensity was enhanced by a factor of ∼2.5 by optimizing the Stern-Gerlach focusing system using high tip-field (∼1.5 T) rare-earth permanent magnets, and by increasing the pumping speed in the beam-formation chamber. Fluxes of (5.9±0.2)x10 16 1 H/s were measured in a diameter 12 mmx122 mm compression tube with its entrance at a distance of 27 cm from the last focusing element. The total output flux amounted to (7.6±0.2)x10 16 1 H/s

  2. ICP-AES analysis of trace elements in serum from animals fed with irradiated food

    International Nuclear Information System (INIS)

    Huang Zongzhi; Zhou Hongdi

    1986-01-01

    A method of trace element analysis by ICP-AES in serum from animals fed with irradiated food is described. In order to demonstrate that irradiated food is suitable for human consumption, it is necessary to perform an experiment of animal feeding with these food before use for human. Trace element analysis in animal serum could provide an actual evidence for further human consumption study. 53 serum samples of the rats fed with irradiated food were obtained. After ashed and solved, ICP-AES analysis has been used for determining 20 trace elements in specimen solution. The detection limitation is in the range of 10 -2 -10 -3 ppm for different elements. The recovery of elements is from 70.08% to 98.28%. The relative standard deviation is found to be 0.71% to 11.52%

  3. Residents’ Preferences for Household Kitchen Waste Source Separation Services in Beijing: A Choice Experiment Approach

    Directory of Open Access Journals (Sweden)

    Yalin Yuan

    2014-12-01

    Full Text Available A source separation program for household kitchen waste has been in place in Beijing since 2010. However, the participation rate of residents is far from satisfactory. This study was carried out to identify residents’ preferences based on an improved management strategy for household kitchen waste source separation. We determine the preferences of residents in an ad hoc sample, according to their age level, for source separation services and their marginal willingness to accept compensation for the service attributes. We used a multinomial logit model to analyze the data, collected from 394 residents in Haidian and Dongcheng districts of Beijing City through a choice experiment. The results show there are differences of preferences on the services attributes between young, middle, and old age residents. Low compensation is not a major factor to promote young and middle age residents accept the proposed separation services. However, on average, most of them prefer services with frequent, evening, plastic bag attributes and without instructor. This study indicates that there is a potential for local government to improve the current separation services accordingly.

  4. Plasma jet source parameter optimisation and experiments on injection into Globus-M spherical tokamak

    International Nuclear Information System (INIS)

    Gusev, V.K.; Petrov, Yu.V.; Sakharov, N.V.; Semenov, A.A.; Voronin, A.V.

    2005-01-01

    Results of theoretical and experimental research on the plasma sources and injection of plasma and gas jet produced by the modified source into tokamak Globus-M are presented. An experimental test stand was developed for investigation of intense plasma jet generation. Optimisation of pulsed coaxial accelerator parameters by means of analytical calculations is performed with the aim of achieving the highest flow velocity at limited coaxial electrode length and discharge current. The optimal parameters of power supply to generate a plasma jet with minimal impurity contamination and maximum flow velocity were determined. A comparison of experimental and calculation results is made. Plasma jet parameters are measured, such as: impurity species content, pressure distribution across the jet, flow velocity, plasma density, etc. Experiments on the interaction of a higher kinetic energy plasma jet with the magnetic field and plasma of the Globus-M tokamak were performed. Experimental results on plasma and gas jet injection into different Globus-M discharge phases are presented and discussed. Results are presented on the investigation of plasma jet injection as the source for discharge breakdown, plasma current startup and initial density rise. (author)

  5. Preparation of a Strong Thin Polonium Source And Preliminary Experiments on the Yield of (α,n) Reactions

    International Nuclear Information System (INIS)

    Broda, E.

    1945-01-01

    This report was written by E. Broda and P. K. Wright at the Cavendish Laboratory (Cambridge) in July 1945 and is about the preparation of a strong thin polonium source and preliminary experiments on the yield of (alpha,n) reactions. This report includes the experiment description, the discussion of the results and consist of 4 parts: (1) the electrode position of polonium under different conditions (2) a standard procedure for preparation of strong thin Po sources (3) a simple method for the recovery of RaD from complex mixtures (4) some preliminary experiments with a Po source. (nowak)

  6. Preparation of a Strong Thin Polonium Source And Preliminary Experiments on the Yield of (α,n) Reactions

    Energy Technology Data Exchange (ETDEWEB)

    Broda, E.

    1945-07-01

    This report was written by E. Broda and P. K. Wright at the Cavendish Laboratory (Cambridge) in July 1945 and is about the preparation of a strong thin polonium source and preliminary experiments on the yield of (alpha,n) reactions. This report includes the experiment description, the discussion of the results and consist of 4 parts: (1) the electrode position of polonium under different conditions (2) a standard procedure for preparation of strong thin Po sources (3) a simple method for the recovery of RaD from complex mixtures (4) some preliminary experiments with a Po source. (nowak)

  7. Heat Transfer by Thermo-capillary Convection -Sounding Rocket COMPERE Experiment SOURCE

    Science.gov (United States)

    Dreyer, Michael; Fuhrmann, Eckart

    The sounding rocket COMPERE experiment SOURCE was successfully flown on MASER 11, launched in Kiruna (ESRANGE), May 15th, 2008. SOURCE has been intended to partly ful-fill the scientific objectives of the European Space Agency (ESA) Microgravity Applications Program (MAP) project AO-2004-111 (Convective boiling and condensation). Three parties of principle investigators have been involved to design the experiment set-up: ZARM for thermo-capillary flows, IMFT (Toulouse, France) for boiling studies, EADS Astrium (Bremen, Ger-many) for depressurization. The topic of this paper is to study the effect of wall heat flux on the contact line of the free liquid surface and to obtain a correlation for a convective heat trans-fer coefficient. The experiment has been conducted along a predefined time line. A preheating sequence at ground was the first operation to achieve a well defined temperature evolution within the test cell and its environment inside the rocket. Nearly one minute after launch, the pressurized test cell was filled with the test liquid HFE-7000 until a certain fill level was reached. Then the free surface could be observed for 120 s without distortion. Afterwards, the first depressurization was started to induce subcooled boiling, the second one to start saturated boiling. The data from the flight consists of video images and temperature measurements in the liquid, the solid, and the gaseous phase. Data analysis provides the surface shape versus time and the corresponding apparent contact angle. Computational analysis provides information for the determination of the heat transfer coefficient in a compensated gravity environment where a flow is caused by the temperature difference between the hot wall and the cold liquid. The paper will deliver correlations for the effective contact angle and the heat transfer coefficient as a function of the relevant dimensionsless parameters as well as physical explanations for the observed behavior. The data will be used

  8. Surface Deformation by Thermo-capillary Convection -Sounding Rocket COMPERE Experiment SOURCE

    Science.gov (United States)

    Fuhrmann, Eckart; Dreyer, Michael E.

    The sounding rocket COMPERE experiment SOURCE was successfully flown on MASER 11, launched in Kiruna (ESRANGE), May 15th, 2008. SOURCE has been intended to partly ful-fill the scientific objectives of the European Space Agency (ESA) Microgravity Applications Program (MAP) project AO-2004-111 (Convective boiling and condensation). Three parties of principle investigators have been involved to design the experiment set-up: ZARM for thermo-capillary flows, IMFT (Toulouse, France) for boiling studies, EADS Astrium (Bremen, Ger-many) for depressurization. The scientific aims are to study the effect of wall heat flux on the contact line of the free liquid surface and to obtain a correlation for a convective heat transfer coefficient. The experiment has been conducted along a predefined time line. A preheating sequence at ground was the first operation to achieve a well defined temperature evolution within the test cell and its environment inside the rocket. Nearly one minute after launch, the pressurized test cell was filled with the test liquid HFE-7000 until a certain fill level was reached. Then the free surface could be observed for 120 s without distortion. Afterwards, the first depressurization was started to induce subcooled boiling, the second one to start saturated boiling. The data from the flight consists of video images and temperature measurements in the liquid, the solid, and the gaseous phase. Data analysis provides the surface shape versus time and the corresponding apparent contact angle. Computational analysis provides information for the determination of the heat transfer coefficient in a compensated gravity environment where a flow is caused by the temperature difference between the hot wall and the cold liquid. Correlations for the effective contact angle and the heat transfer coefficient shall be delivered as a function of the relevant dimensionsless parameters. The data will be used for benchmarking of commercial CFD codes and the tank design

  9. Tracer simulation using a global general circulation model: Results from a midlatitude instantaneous source experiment

    International Nuclear Information System (INIS)

    Mahlman, J.D.; Moxim, W.J.

    1978-01-01

    An 11-level general circulation model with seasonal variation is used to perform an experiment on the dispersion of passive tracers. Specially constructed time-dependent winds from this model are used as input to a separate tracer model. The methodologies employed to construct the tracer model are described.The experiment presented is the evolution of a hypothetical instantaneous source of tracer on 1 Janaury with maximum initial concentration at 65 mb, 36 0 N, 180 0 E. The tracer is assumed to have no sources or sinks in the stratosphere, but is subject to removal processes in the lower troposphere.The experimental results reveal a number of similarities to observed tracer behavior, including the average poleward-downward slope of mixing ratio isopleths, strong tracer gradients across the tropopause, intrusion of tracer into the Southern Hemisphere lower stratosphere, and the long-term interhemispheric exchange rate. The model residence times show behavior intermediate to those exhibited for particulate radioactive debris and gaseous C 14 O 2 . This suggests that caution should be employed when either radioactive debris or C 14 O 2 data are used to develop empirical models for prediction of gaseous tracers which are efficiently removed in the troposphere.In this experiment, the tracer mixing ratio and potential vorticity evolve to very high correlations. Mechanisms for this correlation are discussed. The zonal mean tracer balances exhibit complex behavior among the various transport terms. At early stages, the tracer evolution is dominated by eddy effects. Later, a very large degree of self-cancellation between mean cell and eddy effects is observed. During seasonal transitions, however, this self-cancellation diminishes markedly, leading to significant changes in the zonal mean tracer distribution. A possible theoretical explanation is presented

  10. NEDE: an open-source scripting suite for developing experiments in 3D virtual environments.

    Science.gov (United States)

    Jangraw, David C; Johri, Ansh; Gribetz, Meron; Sajda, Paul

    2014-09-30

    As neuroscientists endeavor to understand the brain's response to ecologically valid scenarios, many are leaving behind hyper-controlled paradigms in favor of more realistic ones. This movement has made the use of 3D rendering software an increasingly compelling option. However, mastering such software and scripting rigorous experiments requires a daunting amount of time and effort. To reduce these startup costs and make virtual environment studies more accessible to researchers, we demonstrate a naturalistic experimental design environment (NEDE) that allows experimenters to present realistic virtual stimuli while still providing tight control over the subject's experience. NEDE is a suite of open-source scripts built on the widely used Unity3D game development software, giving experimenters access to powerful rendering tools while interfacing with eye tracking and EEG, randomizing stimuli, and providing custom task prompts. Researchers using NEDE can present a dynamic 3D virtual environment in which randomized stimulus objects can be placed, allowing subjects to explore in search of these objects. NEDE interfaces with a research-grade eye tracker in real-time to maintain precise timing records and sync with EEG or other recording modalities. Python offers an alternative for experienced programmers who feel comfortable mastering and integrating the various toolboxes available. NEDE combines many of these capabilities with an easy-to-use interface and, through Unity's extensive user base, a much more substantial body of assets and tutorials. Our flexible, open-source experimental design system lowers the barrier to entry for neuroscientists interested in developing experiments in realistic virtual environments. Copyright © 2014 Elsevier B.V. All rights reserved.

  11. Investigating microearthquake finite source attributes with IRIS Community Wavefield Demonstration Experiment in Oklahoma

    Science.gov (United States)

    Fan, Wenyuan; McGuire, Jeffrey J.

    2018-05-01

    An earthquake rupture process can be kinematically described by rupture velocity, duration and spatial extent. These key kinematic source parameters provide important constraints on earthquake physics and rupture dynamics. In particular, core questions in earthquake science can be addressed once these properties of small earthquakes are well resolved. However, these parameters of small earthquakes are poorly understood, often limited by available datasets and methodologies. The IRIS Community Wavefield Experiment in Oklahoma deployed ˜350 three component nodal stations within 40 km2 for a month, offering an unprecedented opportunity to test new methodologies for resolving small earthquake finite source properties in high resolution. In this study, we demonstrate the power of the nodal dataset to resolve the variations in the seismic wavefield over the focal sphere due to the finite source attributes of a M2 earthquake within the array. The dense coverage allows us to tightly constrain rupture area using the second moment method even for such a small earthquake. The M2 earthquake was a strike-slip event and unilaterally propagated towards the surface at 90 per cent local S- wave speed (2.93 km s-1). The earthquake lasted ˜0.019 s and ruptured Lc ˜70 m by Wc ˜45 m. With the resolved rupture area, the stress-drop of the earthquake is estimated as 7.3 MPa for Mw 2.3. We demonstrate that the maximum and minimum bounds on rupture area are within a factor of two, much lower than typical stress drop uncertainty, despite a suboptimal station distribution. The rupture properties suggest that there is little difference between the M2 Oklahoma earthquake and typical large earthquakes. The new three component nodal systems have great potential for improving the resolution of studies of earthquake source properties.

  12. Inductively coupled plasma mass spectrometry (ICP-MS)

    International Nuclear Information System (INIS)

    Shimamura, Tadashi

    1997-01-01

    The period of investigation for the previous general remarks on the progress of ICP-MS was from January, 1991 to September, 1993. In the investigation of this time, for the object of the Chemical Abstracts from January, 1994 to September, 1996, retrieval was carried out by using the STN International. As the key words, ICP-MS, Inductively Coupled Plasma Mass Spectrometry or Inductively Coupled Plasma Mass Spectrometer was used. The number of hit was 373 in 1994, 462 in 1995, and 356 as of September, 1996, 1191 in total. The cumulative number of the papers from 1980 to 1996 is shown. It is known how rapidly the ICP-MS has pervaded as the means of analysis. In order to cope with the enormous number of papers, this time, it was decided to do the review by limiting to the papers which were published in the main journals deeply related to analytical chemistry. As to the tendency in the last three years, it is summarized as how to overcome the spectrum interference and matrix effect in the ICP-MS and the trend of using the ICP-MS as the high sensitivity detector for separation techniques. The technical basic research of the ICP-MS on spectrum interference, sample introduction method and others and the analysis of living body samples are reported. (K.I.)

  13. A new integral experiment on copper with DT neutron source at JAEA/FNS

    Energy Technology Data Exchange (ETDEWEB)

    Kwon, Saerom, E-mail: kwon.saerom@jaea.go.jp; Sato, Satoshi; Ohta, Masayuki; Ochiai, Kentaro; Konno, Chikara

    2016-11-01

    Highlights: • Integral experiment on copper with DT neutron was performed under small influence of background neutrons which were efficiently absorbed in the Li{sub 2}O layers. • The experimental analyses were carried out using MCNP5-1.40 and the recent nuclear data libraries. • The underestimation issue of the reaction rates related to lower energy neutrons is focused on. • The combination of the {sup 63}Cu data in JEFF-3.2 and {sup 65}Cu data in JENDL-4.0 gave the best C/E. • The specific cross section data of copper should be reassessed. - Abstract: In order to validate copper nuclear data, an integral experiment on copper with the DT neutron source at JAEA/FNS had been performed over 20 years ago. The experiment had showed that ratios of the calculated values to the experimental ones (C/Es) related to lower energy neutrons had been drastically smaller than unity. In order to reveal reasons of the small C/Es, we newly performed the integral experiment on copper with the DT neutron source at JAEA/FNS. A quasi-cylindrical copper assembly of 315 mm in radius and 608 mm in depth was covered with Li{sub 2}O blocks of 51 mm in thickness for the front and side parts and 153 mm in thickness for the rear part to exclude background neutrons which might affect the measured data. We measured reaction rates with 5 activation foils and fission rates with 2 micro fission chambers at the center of the assembly. The experiment was analyzed by using MCNP5-1.40 with the recent nuclear data libraries, ENDF/B-VII.1, JEFF-3.2 and JENDL-4.0. As a result, the C/E of the reaction rate of the {sup 197}Au(n,γ){sup 198}Au reaction improved by 10% from the previous result and the combination of the {sup 63}Cu data in JEFF-3.2 and {sup 65}Cu data in JENDL-4.0 increased the C/E by more 10% because of the resonance data of the {sup 63}Cu in JEFF-3.2. Moreover, the calculated result with the {sup 63}Cu data in JEFF-3.2 and {sup 65}Cu data in JENDL-4.0 with 10% larger elastic

  14. High-precision isotopic characterization of USGS reference materials by TIMS and MC-ICP-MS

    Science.gov (United States)

    Weis, Dominique; Kieffer, Bruno; Maerschalk, Claude; Barling, Jane; de Jong, Jeroen; Williams, Gwen A.; Hanano, Diane; Pretorius, Wilma; Mattielli, Nadine; Scoates, James S.; Goolaerts, Arnaud; Friedman, Richard M.; Mahoney, J. Brian

    2006-08-01

    The Pacific Centre for Isotopic and Geochemical Research (PCIGR) at the University of British Columbia has undertaken a systematic analysis of the isotopic (Sr, Nd, and Pb) compositions and concentrations of a broad compositional range of U.S. Geological Survey (USGS) reference materials, including basalt (BCR-1, 2; BHVO-1, 2), andesite (AGV-1, 2), rhyolite (RGM-1, 2), syenite (STM-1, 2), granodiorite (GSP-2), and granite (G-2, 3). USGS rock reference materials are geochemically well characterized, but there is neither a systematic methodology nor a database for radiogenic isotopic compositions, even for the widely used BCR-1. This investigation represents the first comprehensive, systematic analysis of the isotopic composition and concentration of USGS reference materials and provides an important database for the isotopic community. In addition, the range of equipment at the PCIGR, including a Nu Instruments Plasma MC-ICP-MS, a Thermo Finnigan Triton TIMS, and a Thermo Finnigan Element2 HR-ICP-MS, permits an assessment and comparison of the precision and accuracy of isotopic analyses determined by both the TIMS and MC-ICP-MS methods (e.g., Nd isotopic compositions). For each of the reference materials, 5 to 10 complete replicate analyses provide coherent isotopic results, all with external precision below 30 ppm (2 SD) for Sr and Nd isotopic compositions (27 and 24 ppm for TIMS and MC-ICP-MS, respectively). Our results also show that the first- and second-generation USGS reference materials have homogeneous Sr and Nd isotopic compositions. Nd isotopic compositions by MC-ICP-MS and TIMS agree to within 15 ppm for all reference materials. Interlaboratory MC-ICP-MS comparisons show excellent agreement for Pb isotopic compositions; however, the reproducibility is not as good as for Sr and Nd. A careful, sequential leaching experiment of three first- and second-generation reference materials (BCR, BHVO, AGV) indicates that the heterogeneity in Pb isotopic compositions

  15. Potassium Stable Isotopic Compositions Measured by High-Resolution MC-ICP-MS

    Science.gov (United States)

    Morgan, Leah E.; Lloyd, Nicholas S.; Ellam, Robert M.; Simon, Justin I.

    2012-01-01

    -standard bracketing. As cold plasma conditions can amplify matrix effects, experiments were conducted to test the matrix tolerance of measurements; the use of clean, matrix-matched samples and standards is critical. Limitations of the cold-plasma high-resolution MC-ICP-MS methodology with respect to matrix tolerance are discussed and compared with the limitations of TIMS methodologies.

  16. HAW simulation experiments with cobalt-60 radiation sources in the Asse salt mine

    International Nuclear Information System (INIS)

    Rothfuchs, T.; Wieczorek, K.; Feddersen, H.K.

    1986-01-01

    The report describes the experimental work and the measured data of the joint German-American project for the HAW simulation experiment with cobalt-60 radiation sources in the Asse salt mine, covering the period up to the end of the third quarter 1986. The experiment is intended to yield information on the synergistic effects of heat and ionizing radiation on the salt rock under representative waste repository conditions. The investigations aim at the migration, release, and radiolytic decomposition of the water and gas components in the rock salt, and at the thermally induced strain and deformation processes. In addition, corrosion tests are planned to be made on various container test materials, and analyses of salt rock core samples for assessing the effect of heat and radiation on the rock. The report in hand presents all data obtained during the experiment. The results of the subsequent evaluation and verification studies will be presented in another report, the programme being given in an annex to the report in hand. (orig./RB) [de

  17. Rotatable spin-polarized electron source for inverse-photoemission experiments

    International Nuclear Information System (INIS)

    Stolwijk, S. D.; Wortelen, H.; Schmidt, A. B.; Donath, M.

    2014-01-01

    We present a ROtatable Spin-polarized Electron source (ROSE) for the use in spin- and angle-resolved inverse-photoemission (SR-IPE) experiments. A key feature of the ROSE is a variable direction of the transversal electron beam polarization. As a result, the inverse-photoemission experiment becomes sensitive to two orthogonal in-plane polarization directions, and, for nonnormal electron incidence, to the out-of-plane polarization component. We characterize the ROSE and test its performance on the basis of SR-IPE experiments. Measurements on magnetized Ni films on W(110) serve as a reference to demonstrate the variable spin sensitivity. Moreover, investigations of the unoccupied spin-dependent surface electronic structure of Tl/Si(111) highlight the capability to analyze complex phenomena like spin rotations in momentum space. Essentially, the ROSE opens the way to further studies on complex spin-dependent effects in the field of surface magnetism and spin-orbit interaction at surfaces

  18. Quantification of immobilized Candida antarctica lipase B (CALB) using ICP-AES combined with Bradford method.

    Science.gov (United States)

    Nicolás, Paula; Lassalle, Verónica L; Ferreira, María L

    2017-02-01

    The aim of this manuscript was to study the application of a new method of protein quantification in Candida antarctica lipase B commercial solutions. Error sources associated to the traditional Bradford technique were demonstrated. Eight biocatalysts based on C. antarctica lipase B (CALB) immobilized onto magnetite nanoparticles were used. Magnetite nanoparticles were coated with chitosan (CHIT) and modified with glutaraldehyde (GLUT) and aminopropyltriethoxysilane (APTS). Later, CALB was adsorbed on the modified support. The proposed novel protein quantification method included the determination of sulfur (from protein in CALB solution) by means of Atomic Emission by Inductive Coupling Plasma (AE-ICP). Four different protocols were applied combining AE-ICP and classical Bradford assays, besides Carbon, Hydrogen and Nitrogen (CHN) analysis. The calculated error in protein content using the "classic" Bradford method with bovine serum albumin as standard ranged from 400 to 1200% when protein in CALB solution was quantified. These errors were calculated considering as "true protein content values" the results of the amount of immobilized protein obtained with the improved method. The optimum quantification procedure involved the combination of Bradford method, ICP and CHN analysis. Copyright © 2016 Elsevier Inc. All rights reserved.

  19. Early mortality experience in a large military cohort and a comparison of mortality data sources

    Directory of Open Access Journals (Sweden)

    Smith Besa

    2010-05-01

    Full Text Available Abstract Background Complete and accurate ascertainment of mortality is critically important in any longitudinal study. Tracking of mortality is particularly essential among US military members because of unique occupational exposures (e.g., worldwide deployments as well as combat experiences. Our study objectives were to describe the early mortality experience of Panel 1 of the Millennium Cohort, consisting of participants in a 21-year prospective study of US military service members, and to assess data sources used to ascertain mortality. Methods A population-based random sample (n = 256,400 of all US military service members on service rosters as of October 1, 2000, was selected for study recruitment. Among this original sample, 214,388 had valid mailing addresses, were not in the pilot study, and comprised the group referred to in this study as the invited sample. Panel 1 participants were enrolled from 2001 to 2003, represented all armed service branches, and included active-duty, Reserve, and National Guard members. Crude death rates, as well as age- and sex-adjusted overall and age-adjusted, category-specific death rates were calculated and compared for participants (n = 77,047 and non-participants (n = 137,341 based on data from the Social Security Administration Death Master File, Department of Veterans Affairs (VA files, and the Department of Defense Medical Mortality Registry, 2001-2006. Numbers of deaths identified by these three data sources, as well as the National Death Index, were compared for 2001-2004. Results There were 341 deaths among the participants for a crude death rate of 80.7 per 100,000 person-years (95% confidence interval [CI]: 72.2,89.3 compared to 820 deaths and a crude death rate of 113.2 per 100,000 person-years (95% CI: 105.4, 120.9 for non-participants. Age-adjusted, category-specific death rates highlighted consistently higher rates among study non-participants. Although there were advantages and

  20. Operating experience relating to on-site electric power sources. Proceedings of a Specialist Meeting

    International Nuclear Information System (INIS)

    1986-02-01

    The reliability of on-site electric power sources of nuclear power plants usually consisting of diesel generators, gas turbine generators and DC power sources, has been a matter of concern during reactor operations. The frequent recurrence and the important consequences of failures relating to on-site electric power sources have led to a general consensus that they form one of the most significant features influencing the total performance of the safety Systems. This has also been confirmed by surveys performed on the incidents reported through the NEA Incident Reporting System (IRS). Accordingly, a recommendation to organise a Specialist Meeting on the subject was made at the third annual meeting of CSNI Principal Working Group No. 1 (Operating Experience and Human Factors). At the 12. meeting of the CSNI held in November 1984. the Committee endorsed the proposal and accepted an offer by the United Kingdom to host and organise the Specialist Meeting. The Specialist Meeting, sponsored by the CSNI, was held in London, United Kingdom from 16 to 18 October 1985. It was hosted by H.M. Nuclear Installations Inspectorate of the Health and Safety Executive. The purpose of the meeting was to promote the exchange of Information on operating experience relating to on-site electric power sources and to look for measures to further improve their reliability In the areas of design, operation and licensing. The meeting was organised by a Programme Group which included nominated members of CSNI PWG No. 1. the Programme Group met in May and June 1985 in Paris to agree on the programme and practical arrangements for the meeting. As a result of the review of the abstracts which had been contributed in response to the Call for Papers, 28 papers were accepted for presentation during the meeting. Approximately 60 delegates from 13 Member countries, and the NEA Secretariat, attended the meeting. Session summaries prepared by the respective session chairmen are Included prior to the

  1. Operating experience relating to on-site electric power sources. Proceedings of a Specialist Meeting

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    1986-02-15

    The reliability of on-site electric power sources of nuclear power plants usually consisting of diesel generators, gas turbine generators and DC power sources, has been a matter of concern during reactor operations. The frequent recurrence and the important consequences of failures relating to on-site electric power sources have led to a general consensus that they form one of the most significant features influencing the total performance of the safety Systems. This has also been confirmed by surveys performed on the incidents reported through the NEA Incident Reporting System (IRS). Accordingly, a recommendation to organise a Specialist Meeting on the subject was made at the third annual meeting of CSNI Principal Working Group No. 1 (Operating Experience and Human Factors). At the 12. meeting of the CSNI held in November 1984. the Committee endorsed the proposal and accepted an offer by the United Kingdom to host and organise the Specialist Meeting. The Specialist Meeting, sponsored by the CSNI, was held in London, United Kingdom from 16 to 18 October 1985. It was hosted by H.M. Nuclear Installations Inspectorate of the Health and Safety Executive. The purpose of the meeting was to promote the exchange of Information on operating experience relating to on-site electric power sources and to look for measures to further improve their reliability In the areas of design, operation and licensing. The meeting was organised by a Programme Group which included nominated members of CSNI PWG No. 1. the Programme Group met in May and June 1985 in Paris to agree on the programme and practical arrangements for the meeting. As a result of the review of the abstracts which had been contributed in response to the Call for Papers, 28 papers were accepted for presentation during the meeting. Approximately 60 delegates from 13 Member countries, and the NEA Secretariat, attended the meeting. Session summaries prepared by the respective session chairmen are Included prior to the

  2. The new atomic act. Radiation exposure from radon and natural radiation sources in workplaces and the experience of surveillance

    International Nuclear Information System (INIS)

    Sinaglova, R.

    2018-01-01

    In this presentation the new atomic act approved in the Czech republic is analyzed from the point of view of irradiation from radon and natural radiation sources in workplaces. Experience of supervision are also discussed. (authors)

  3. Comparison of elemental quantity by PIXE and ICP-MS and/or ICP-AES for NIST standards

    International Nuclear Information System (INIS)

    Saitoh, K.; Sera, K.; Gotoh, T.; Nakamura, M.

    2002-01-01

    Urban particulate matter (SRM 1648), Buffalo River sediment (SRM 2704) and pine needle (SRM 1575) standard reference materials prepared by the National Institute of Standards and Technology (NIST, USA) were analyzed by three multi-element analysis methods, i.e., particle induced X-ray emission (PIXE), inductively coupled plasma-mass spectrometry (ICP-MS) and inductively coupled plasma-atomic emission spectrometry (ICP-AES); values determined by those analysis methods were compared with certified and/or non-certified values of NIST samples. Values determined by PIXE were 70-120% relative to certified and/or non-certified values of NIST samples except for Co in the urban particulate matter, for V and Co in Buffalo River sediment and for Ni and Br in the pine needles samples. In particular, Al, K, Ca, Cr, Mn, Fe, Cu, Zn and Pb were 85-110% in all samples. On the other hand, Na and Fe values determined by ICP-MS were very much different from the certified values in all samples, but the other elements were 70-120%. As for ICP-AES, all elements except for Na were 80-100% in all samples. Comparing the values determined by PIXE and those determined by ICP-MS and/or ICP-AES, there was a slight difference between the samples, but the range was 75-120% except for Na, V, Fe and Co determined by ICP-MS and Na determined by ICP-AES, which was generally consistent with PIXE

  4. A Comparison between Predicted and Observed Atmospheric States and their Effects on Infrasonic Source Time Function Inversion at Source Physics Experiment 6

    Science.gov (United States)

    Aur, K. A.; Poppeliers, C.; Preston, L. A.

    2017-12-01

    The Source Physics Experiment (SPE) consists of a series of underground chemical explosions at the Nevada National Security Site (NNSS) designed to gain an improved understanding of the generation and propagation of physical signals in the near and far field. Characterizing the acoustic and infrasound source mechanism from underground explosions is of great importance to underground explosion monitoring. To this end we perform full waveform source inversion of infrasound data collected from the SPE-6 experiment at distances from 300 m to 6 km and frequencies up to 20 Hz. Our method requires estimating the state of the atmosphere at the time of each experiment, computing Green's functions through these atmospheric models, and subsequently inverting the observed data in the frequency domain to obtain a source time function. To estimate the state of the atmosphere at the time of the experiment, we utilize the Weather Research and Forecasting - Data Assimilation (WRF-DA) modeling system to derive a unified atmospheric state model by combining Global Energy and Water Cycle Experiment (GEWEX) Continental-scale International Project (GCIP) data and locally obtained sonde and surface weather observations collected at the time of the experiment. We synthesize Green's functions through these atmospheric models using Sandia's moving media acoustic propagation simulation suite (TDAAPS). These models include 3-D variations in topography, temperature, pressure, and wind. We compare inversion results using the atmospheric models derived from the unified weather models versus previous modeling results and discuss how these differences affect computed source waveforms with respect to observed waveforms at various distances. Sandia National Laboratories is a multi-mission laboratory managed and operated by National Technology and Engineering Solutions of Sandia LLC, a wholly owned subsidiary of Honeywell International Inc. for the U.S. Department of Energy's National Nuclear

  5. ICP measurement accuracy: the effect of temperature drift. Design of a laboratory test for assessment of ICP transducers.

    Science.gov (United States)

    Morgalla, M H; Mettenleiter, H; Katzenberger, T

    1999-01-01

    Intracranial pressure (ICP) monitoring has become the mainstay of multimodal neuromonitoring of comatous patients after head injury. In the presence of rising ICP and faced with pressures, difficult to control, aggressive measures, such as hypothermia may be used. The ICP readings should not be influenced by temperature changes. A laboratory test was designed to simulate temperature variations between 20 degrees C and 45 degrees C at different pressure levels under physiological conditions. Five types of transducers were examined: Epidyn Braun Melsungen, ICT/B-Titan Gaeltec, Camino-OLM-110-4B, Codman MicroSensor ICP-Transducer, Neurovent ICP transducer Rehau Ag+Co. Tests were performed at 6 different pressure levels between 0 mmHg and 50 mmHg. The results show very low drifts of less than 0.15 mmHg degree C-1 for Codman, Epidyn and Neurovent. Gaeltec and Camino exhibited higher drifts of 0.18 mmHg and 0.2 mmHg degree C-1 respectively. Within the temperature range from 35 degrees C to 42 degrees C all probes tested show insignificant temperature drift. Whether these results also apply to other types of transducers needs further evaluation. Problems and requirements related to the design of a laboratory test for the in vitro assessment of ICP transducers are discussed in detail.

  6. Aerosol-Cloud Interactions During Puijo Cloud Experiments - The effects of weather and local sources

    Science.gov (United States)

    Komppula, Mika; Portin, Harri; Leskinen, Ari; Romakkaniemi, Sami; Brus, David; Neitola, Kimmo; Hyvärinen, Antti-Pekka; Kortelainen, Aki; Hao, Liqing; Miettinen, Pasi; Jaatinen, Antti; Ahmad, Irshad; Lihavainen, Heikki; Laaksonen, Ari; Lehtinen, Kari E. J.

    2013-04-01

    The Puijo measurement station has provided continuous data on aerosol-cloud interactions since 2006. The station is located on top of the Puijo observation tower (306 m a.s.l, 224 m above the surrounding lake level) in Kuopio, Finland. The top of the tower is covered by cloud about 15 % of the time, offering perfect conditions for studying aerosol-cloud interactions. With a twin-inlet setup (total and interstitial inlets) we are able to separate the activated particles from the interstitial (non-activated) particles. The continuous twin-inlet measurements include aerosol size distribution, scattering and absorption. In addition cloud droplet number and size distribution are measured continuously with weather parameters. During the campaigns the twin-inlet system was additionally equipped with aerosol mass spectrometer (AMS) and Single Particle Soot Photometer (SP-2). This way we were able to define the differences in chemical composition of the activated and non-activated particles. Potential cloud condensation nuclei (CCN) in different supersaturations were measured with two CCN counters (CCNC). The other CCNC was operated with a Differential Mobility Analyzer (DMA) to obtain size selected CCN spectra. Other additional measurements included Hygroscopic Tandem Differential Mobility Analyzer (HTDMA) for particle hygroscopicity. Additionally the valuable vertical wind profiles (updraft velocities) are available from Halo Doppler lidar during the 2011 campaign. Cloud properties (droplet number and effective radius) from MODIS instrument onboard Terra and Aqua satellites were retrieved and compared with the measured values. This work summarizes the two latest intensive campaigns, Puijo Cloud Experiments (PuCE) 2010 & 2011. We study especially the effect of the local sources on the cloud activation behaviour of the aerosol particles. The main local sources include a paper mill, a heating plant, traffic and residential areas. The sources can be categorized and identified

  7. Power Law Distributions in the Experiment for Adjustment of the Ion Source of the NBI System

    International Nuclear Information System (INIS)

    Han Xiaopu; Hu Chundong

    2005-01-01

    The experiential adjustment process in an experiment on the ion source of the neutral beam injector system for the HT-7 Tokamak is reported in this paper. With regard to the data obtained in the same condition, in arranging the arc current intensities of every shot with a decay rank, the distributions of the arc current intensity correspond to the power laws, and the distribution obtained in the condition with the cryo-pump corresponds to the double Pareto distribution. Using the similar study method, the distributions of the arc duration are close to the power laws too. These power law distributions are formed rather naturally instead of being the results of purposeful seeking

  8. First results from the Los Alamos plasma source ion implantation experiment

    International Nuclear Information System (INIS)

    Rej, D.J.; Faehl, R.J.; Gribble, R.J.; Henins, I.; Kodali, P.; Nastasi, M.; Reass, W.A.; Tesmer, J.; Walter, K.C.; Wood, B.P.; Conrad, J.R.; Horswill, N.; Shamim, M.; Sridharan, K.

    1993-01-01

    A new facility is operational at Los Alamos to examine plasma source ion implantation on a large scale. Large workpieces can be treated in a 1.5-m-diameter, 4.6-m-long plasma vacuum chamber. Primary emphasis is directed towards improving tribological properties of metal surfaces. First experiments have been performed at 40 kV with nitrogen plasmas. Both coupons and manufactured components, with surface areas up to 4 m 2 , have been processed. Composition and surface hardness of implanted materials are evaluated. Implant conformality and dose uniformity into practical geometries are estimated with multidimensional particle-in-cell computations of plasma electron and ion dynamics, and Monte Carlo simulations of ion transport in solids

  9. Advisory Committee on human radiation experiments. Final report, Supplemental Volume 2. Sources and documentation

    International Nuclear Information System (INIS)

    1995-01-01

    This volume and its appendixes supplement the Advisory Committee's final report by reporting how we went about looking for information concerning human radiation experiments and intentional releases, a description of what we found and where we found it, and a finding aid for the information that we collected. This volume begins with an overview of federal records, including general descriptions of the types of records that have been useful and how the federal government handles these records. This is followed by an agency-by-agency account of the discovery process and descriptions of the records reviewed, together with instructions on how to obtain further information from those agencies. There is also a description of other sources of information that have been important, including institutional records, print resources, and nonprint media and interviews. The third part contains brief accounts of ACHRE's two major contemporary survey projects (these are described in greater detail in the final report and another supplemental volume) and other research activities. The final section describes how the ACHRE information-nation collections were managed and the records that ACHRE created in the course of its work; this constitutes a general finding aid for the materials deposited with the National Archives. The appendices provide brief references to federal records reviewed, descriptions of the accessions that comprise the ACHRE Research Document Collection, and descriptions of the documents selected for individual treatment. Also included are an account of the documentation available for ACHRE meetings, brief abstracts of the almost 4,000 experiments individually described by ACHRE staff, a full bibliography of secondary sources used, and other information

  10. Advisory Committee on human radiation experiments. Final report, Supplemental Volume 2. Sources and documentation

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    1995-01-01

    This volume and its appendixes supplement the Advisory Committee`s final report by reporting how we went about looking for information concerning human radiation experiments and intentional releases, a description of what we found and where we found it, and a finding aid for the information that we collected. This volume begins with an overview of federal records, including general descriptions of the types of records that have been useful and how the federal government handles these records. This is followed by an agency-by-agency account of the discovery process and descriptions of the records reviewed, together with instructions on how to obtain further information from those agencies. There is also a description of other sources of information that have been important, including institutional records, print resources, and nonprint media and interviews. The third part contains brief accounts of ACHRE`s two major contemporary survey projects (these are described in greater detail in the final report and another supplemental volume) and other research activities. The final section describes how the ACHRE information-nation collections were managed and the records that ACHRE created in the course of its work; this constitutes a general finding aid for the materials deposited with the National Archives. The appendices provide brief references to federal records reviewed, descriptions of the accessions that comprise the ACHRE Research Document Collection, and descriptions of the documents selected for individual treatment. Also included are an account of the documentation available for ACHRE meetings, brief abstracts of the almost 4,000 experiments individually described by ACHRE staff, a full bibliography of secondary sources used, and other information.

  11. Fission Product Transport and Source Terms in HTRs: Experience from AVR Pebble Bed Reactor

    Directory of Open Access Journals (Sweden)

    Rainer Moormann

    2008-01-01

    Full Text Available Fission products deposited in the coolant circuit outside of the active core play a dominant role in source term estimations for advanced small pebble bed HTRs, particularly in design basis accidents (DBA. The deposited fission products may be released in depressurization accidents because present pebble bed HTR concepts abstain from a gas tight containment. Contamination of the circuit also hinders maintenance work. Experiments, performed from 1972 to 88 on the AVR, an experimental pebble bed HTR, allow for a deeper insight into fission product transport behavior. The activity deposition per coolant pass was lower than expected and was influenced by fission product chemistry and by presence of carbonaceous dust. The latter lead also to inconsistencies between Cs plate out experiments in laboratory and in AVR. The deposition behavior of Ag was in line with present models. Dust as activity carrier is of safety relevance because of its mobility and of its sorption capability for fission products. All metal surfaces in pebble bed reactors were covered by a carbonaceous dust layer. Dust in AVR was produced by abrasion in amounts of about 5 kg/y. Additional dust sources in AVR were ours oil ingress and peeling of fuel element surfaces due to an air ingress. Dust has a size of about 1  m, consists mainly of graphite, is partly remobilized by flow perturbations, and deposits with time constants of 1 to 2 hours. In future reactors, an efficient filtering via a gas tight containment is required because accidents with fast depressurizations induce dust mobilization. Enhanced core temperatures in normal operation as in AVR and broken fuel pebbles have to be considered, as inflammable dust concentrations in the gas phase.

  12. Integral migration and source term experiments on cement and bitumen waste forms

    International Nuclear Information System (INIS)

    Ewart, F.T.; Howse, R.M.; Sharpe, B.M.; Smith, A.J.; Thomason, H.P.; Williams, S.J.; Young, M.

    1986-01-01

    This is the final report of a programme of research which formed a part of the CEC joint research project into radionuclide migration in the geosphere (MIRAGE). This study addressed the aspects of integral migration and source term. The integral migration experiment simulated, in the laboratory, the intrusion of water into the repository, the leaching of radionuclides from two intermediate level wasteforms and the subsequent migration through the geosphere. The simulation consisted of a source of natural ground water which flowed over a sample of wasteform, at a controlled redox potential, and then through backfill and geological material packed in columns. The two wasteforms used here were cemented waste from the WAK plant at Karlsruhe, W. Germany and bitumenised intermediate concentrates from the Marcoule plant in France. The soluble fission products such as caesium wire rapidly released from the cemented waste but the actinides, and technetium in the reduced state, were retained in the wasteform. The release of all nuclides from the bitumenised waste was very low. (author)

  13. Integral migration and source-term experiments on cement and bitumen waste forms

    International Nuclear Information System (INIS)

    Ewart, F.T.; Howse, R.M.; Sharpe, B.M.; Smith, A.J.; Thomason, H.P.; Williams, S.J.; Young, M.

    1986-01-01

    This is the final report of a programme of research which formed a part of the CEC joint research project into radionuclide migration in the geosphere (MIRAGE). This study addressed the aspects of integral migration and source term. The integral migration experiment simulated, in the laboratory, the intrusion of water into the repository, the leaching of radionuclides from two intermediate-level waste-forms and the subsequent migration through the geosphere. The simulation consisted of a source of natural ground water which flowed over a sample of waste-form, at a controlled redox potential, and then through backfill and geological material packed in columns. The two waste forms used here were cemented waste from the WAK plant at Karlsruhe in the Federal Republic of Germany and bitumenized intermediate concentrates from the Marcoule plant in France. The soluble fission products such as caesium were rapidly released from the cemented waste but the actinides, and technetium in the reduced state, were retained in the waste-form. The released of all nuclides from the bitumenized waste was very low

  14. Advanced light source vacuum policy and vacuum guidelines for beamlines and experiment endstations

    International Nuclear Information System (INIS)

    Hussain, Z.

    1995-08-01

    The purpose of this document is to: (1) Explain the ALS vacuum policy and specifications for beamlines and experiment endstations. (2) Provide guidelines related to ALS vacuum policy to assist in designing beamlines which are in accordance with ALS vacuum policy. This document supersedes LSBL-116. The Advanced Light Source is a third generation synchrotron radiation source whose beam lifetime depends on the quality of the vacuum in the storage ring and the connecting beamlines. The storage ring and most of the beamlines share a common vacuum and are operated under ultra-high-vacuum (UHV) conditions. All endstations and beamline equipment must be operated so as to avoid contamination of beamline components, and must include proper safeguards to protect the storage ring vacuum from an accidental break in the beamline or endstation vacuum systems. The primary gas load during operation is due to thermal desorption and electron/photon induced desorption of contaminants from the interior of the vacuum vessel and its components. The desorption rates are considerably higher for hydrocarbon contamination, thus considerable emphasis is placed on eliminating these sources of contaminants. All vacuum components in a beamline and endstation must meet the ALS vacuum specifications. The vacuum design of both beamlines and endstations must be approved by the ALS Beamline Review Committee (BRC) before vacuum connections to the storage ring are made. The vacuum design is first checked during the Beamline Design Review (BDR) held before construction of the beamline equipment begins. Any deviation from the ALS vacuum specifications must be approved by the BRC prior to installation of the equipment on the ALS floor. Any modification that is incorporated into a vacuum assembly without the written approval of the BRC is done at the user's risk and may lead to rejection of the whole assembly

  15. Latest experience on insertion devices at the National Synchrotron Light Source-II

    International Nuclear Information System (INIS)

    Tanabe, Toshiya; Cappadoro, Peter; Corwin, Todd

    2016-01-01

    National Synchrotron Light Source-II (NSLS-II) is the latest storage ring of 3 GeV energy with the horizontal emittance of the electron beam being 0.9 nm.rad. Nine In-Vacuum Undulators (IVUs) are utilized at the NSLS-II as of February 2016. All IVUs have a unique side window derived from the experience from the CHESS facility in Cornell University. An R and D activity called 'Vacuum Seal Test' was conducted to ensure the viability of aluminum wire seal. Another R and D activity to develop a measurement system for Cryogenic Permanent Magnet Undulator (CPMU) was also performed. Other in-air devices, namely damping wigglers (DWs) and elliptically polarizing undulators (EPUs) utilize extruded aluminum chambers with Non-Evaporable Getter (NEG) coating. The beam-based integral estimates were obtained from the virtual kicks at the upstream and downstream of the undulator that best fit the measured orbit distortion in a model lattice with Tracy. In some cases, there are fairly large discrepancies between magnetic measurement data and observed integrals by the beam. Beam studies were carried out to explain the discrepancies mentioned earlier. The latest experiences on ID development and commissioning are discussed in conjunction with related activities in the world. (author)

  16. Optimal beam sources for Stark decelerators in collision experiments: a tutorial review

    International Nuclear Information System (INIS)

    Vogels, Sjoerd N.; Gao, Zhi; Meerakker, Sebastiaan Y.T. van de

    2015-01-01

    With the Stark deceleration technique, packets of molecules with a tunable velocity, a narrow velocity spread, and a high state purity can be produced. These tamed molecular beams find applications in high resolution spectroscopy, cold molecule trapping, and controlled scattering experiments. The quality and purity of the packets of molecules emerging from the decelerator critically depend on the specifications of the decelerator, but also on the characteristics of the molecular beam pulse with which the decelerator is loaded. We consider three frequently used molecular beam sources, and discuss their suitability for molecular beam deceleration experiments, in particular with the application in crossed beam scattering in mind. The performance of two valves in particular, the Nijmegen Pulsed Valve and the Jordan Valve, is illustrated by decelerating ND 3 molecules in a 2.6 meter-long Stark decelerator. We describe a protocol to characterize the valve, and to optimally load the pulse of molecules into the decelerator. We characterize the valves regarding opening time duration, optimal valve-to-skimmer distance, mean velocity, velocity spread, state purity, and relative intensity. (orig.)

  17. Elevated source SF6-tracer dispersion experiments in the Copenhagen area. Preliminary results II

    International Nuclear Information System (INIS)

    Gryning, S.E.; Lyck, E.

    1980-01-01

    The results from 10 experiments, performed in neutral to unstable meteorological conditions, are reported from an ongoing series of elevated-source, urban-scale tracer dispersion experiments in the Copenhagen area. The tracer is released at a height of 115 m from the TV-tower in GLADSAXE, a suburb of Copenhagen, with tracer sampling units positioned at ground-level in 1 to 3 crosswind series, 2 to 6 km downwind of the tower. The lateral dispersion parameter, sigma(y), was estimated from the measured tracer concentration distribution and compared with values of sigma(y), computed by 1) methods based on wind variance measured during the experiments and 2) methods based on a stability classification of the atmospheric conditions. The wind-variance based methods proved superior in predicting the variation of sigma(y) compared with the stability based methods. Moreover, some of the former methods produced significantly biased estimates of sigma(y). The measured tracer concentration distributions were also crosswind integrated, chi(CWI). Estimates of chi(CWI) were computed using sigma (z) -values derived from the aforementioned computations assuming a Gaussian-type vertical tracer concentration distribution. A comparison is measured and calculated values of chi(CWI) showed no significant differences in the ability of the methods to predict the variation of chi(CWI). Only one method, the EPA, came out with a mean fractional error outside the range +-20% which constitutes the uncertainty in the absolute tracer concentration associated with the calibration of the gas chromatograph for tracer analysis

  18. Site Characterization of the Source Physics Experiment Phase II Location Using Seismic Reflection Data

    Science.gov (United States)

    Sexton, E. A.; Snelson, C. M.; Chipman, V.; Emer, D. F.; White, R. L.; Emmitt, R.; Wright, A. A.; Drellack, S.; Huckins-Gang, H.; Mercadante, J.; Floyd, M.; McGowin, C.; Cothrun, C.; Bonal, N.

    2013-12-01

    An objective of the Source Physics Experiment (SPE) is to identify low-yield nuclear explosions from a regional distance. Low-yield nuclear explosions can often be difficult to discriminate among the clutter of natural and man-made explosive events (e.g., earthquakes and mine blasts). The SPE is broken into three phases. Phase I has provided the first of the physics-based data to test the empirical models that have been used to discriminate nuclear events. The Phase I series of tests were placed within a highly fractured granite body. The evolution of the project has led to development of Phase II, to be placed within the opposite end member of geology, an alluvium environment, thereby increasing the database of waveforms to build upon in the discrimination models. Both the granite and alluvium sites have hosted nearby nuclear tests, which provide comparisons for the chemical test data. Phase III of the SPE is yet to be determined. For Phase II of the experiment, characterization of the location is required to develop the geologic/geophysical models for the execution of the experiment. Criteria for the location are alluvium thickness of approximately 170 m and a water table below 170 m; minimal fracturing would be ideal. A P-wave mini-vibroseis survey was conducted at a potential site in alluvium to map out the subsurface geology. The seismic reflection profile consisted of 168 geophone stations, spaced 5 m apart. The mini-vibe was a 7,000-lb peak-force source, starting 57.5 m off the north end of the profile and ending 57.5 m past the southern-most geophone. The length of the profile was 835 m. The source points were placed every 5 m, equally spaced between geophones to reduce clipping. The vibroseis sweep was from 20 Hz down to 180 Hz over 8 seconds, and four sweeps were stacked at each shot location. The shot gathers show high signal-to-noise ratios with clear first arrivals across the entire spread and the suggestion of some shallow reflectors. The data were

  19. Experiment on search for neutron-antineutron oscillations using a projected UCN source at the WWR-M reactor

    Science.gov (United States)

    Fomin, A. K.; Serebrov, A. P.; Zherebtsov, O. M.; Leonova, E. N.; Chaikovskii, M. E.

    2017-01-01

    We propose an experiment on search for neutron-antineutron oscillations based on the storage of ultracold neutrons (UCN) in a material trap. The sensitivity of the experiment mostly depends on the trap size and the amount of UCN in it. In Petersburg Nuclear Physics Institute (PNPI) a high-intensity UCN source is projected at the WWR-M reactor, which must provide UCN density 2-3 orders of magnitude higher than existing sources. The results of simulations of the designed experimental scheme show that the sensitivity can be increased by ˜ 10-40 times compared to sensitivity of previous experiment depending on the model of neutron reflection from walls.

  20. Production and characterization of a custom-made {sup 228}Th source with reduced neutron source strength for the Borexino experiment

    Energy Technology Data Exchange (ETDEWEB)

    Maneschg, W., E-mail: werner.maneschg@mpi-hd.mpg.de [Max Planck Institut fuer Kernphysik, Saupfercheckweg 1, D-69117 Heidelberg (Germany); Baudis, L. [Physik Institut der Universitaet Zuerich, Winterthurerstrasse 190, CH-8057 Zuerich (Switzerland); Dressler, R. [Paul Scherrer Institut, CH-5232 Villigen (Switzerland); Eberhardt, K. [Institut fuer Kernchemie, Universitaet Mainz, Fritz-Strassmann-Weg 2, D-55128 Mainz (Germany); Eichler, R. [Paul Scherrer Institut, CH-5232 Villigen (Switzerland); Keller, H. [Institut fuer Kernchemie, Universitaet Mainz, Fritz-Strassmann-Weg 2, D-55128 Mainz (Germany); Lackner, R. [Max Planck Institut fuer Kernphysik, Saupfercheckweg 1, D-69117 Heidelberg (Germany); Praast, B. [Institut fuer Kernchemie, Universitaet Mainz, Fritz-Strassmann-Weg 2, D-55128 Mainz (Germany); Santorelli, R. [Physik Institut der Universitaet Zuerich, Winterthurerstrasse 190, CH-8057 Zuerich (Switzerland); Schreiner, J. [Max Planck Institut fuer Kernphysik, Saupfercheckweg 1, D-69117 Heidelberg (Germany); Tarka, M. [Physik Institut der Universitaet Zuerich, Winterthurerstrasse 190, CH-8057 Zuerich (Switzerland); Wiegel, B.; Zimbal, A. [Physikalisch-Technische Bundesanstalt, Bundesallee 100, D-38116 Braunschweig (Germany)

    2012-07-11

    A custom-made {sup 228}Th source of several MBq activities was produced for the Borexino experiment to study the external background of the detector. The aim was to reduce the unwanted neutron emission produced via ({alpha},n) reactions in ceramics typically used for commercial {sup 228}Th sources. For this purpose a ThCl{sub 4} solution was chemically converted into ThO{sub 2} and embedded in a gold foil. The paper describes the production of the custom-made source and its characterization by means of {gamma}-activity, dose rate and neutron source strength measurements. From {gamma}-spectroscopic measurements it was deduced that activity transfer from the initial solution to the final source was >91% (at 68% C.L.) and the final activity was (5.41{+-}0.30) MBq. The dose rate was measured with two dosimeters yielding 12.1 mSv/h and 14.3 mSv/h in 1 cm distance. The neutron source strength of the 5.41 MBq {sup 228}Th source was determined to be (6.59{+-}0.85) s{sup -1}.

  1. Laser ablation ICP-MS for quantitative biomedical applications

    International Nuclear Information System (INIS)

    Konz, Ioana; Fernandez, Beatriz; Fernandez, M.L.; Pereiro, Rosario; Sanz-Medel, Alfredo

    2012-01-01

    LA-ICP-MS allows precise, relatively fast, and spatially resolved measurements of elements and isotope ratios at trace and ultratrace concentration levels with minimal sample preparation. Over the past few years this technique has undergone rapid development, and it has been increasingly applied in many different fields, including biological and medical research. The analysis of essential, toxic, and therapeutic metals, metalloids, and nonmetals in biomedical tissues is a key task in the life sciences today, and LA-ICP-MS has proven to be an excellent complement to the organic MS techniques that are much more commonly employed in the biomedical field. In order to provide an appraisal of the fast progress that is occurring in this field, this review critically describes new developments for LA-ICP-MS as well as the most important applications of LA-ICP-MS, with particular emphasis placed on the quantitative imaging of elements in biological tissues, the analysis of heteroatom-tagged proteins after their separation and purification by gel electrophoresis, and the analysis of proteins that do not naturally have ICP-MS-detectable elements in their structures, thus necessitating the use of labelling strategies. (orig.)

  2. Determination of the structure and composition of Au-Ag bimetallic spherical nanoparticles using single particle ICP-MS measurements performed with normal and high temporal resolution.

    Science.gov (United States)

    Kéri, Albert; Kálomista, Ildikó; Ungor, Ditta; Bélteki, Ádám; Csapó, Edit; Dékány, Imre; Prohaska, Thomas; Galbács, Gábor

    2018-03-01

    In this study, the information that can be obtained by combining normal and high resolution single particle ICP-MS (spICP-MS) measurements for spherical bimetallic nanoparticles (BNPs) was assessed. One commercial certified core-shell Au-Ag nanoparticle and three newly synthesized and fully characterized homogenous alloy Au-Ag nanoparticle batches of different composition were used in the experiments as BNP samples. By scrutinizing the high resolution spICP-MS signal time profiles, it was revealed that the width of the signal peak linearly correlates with the diameter of nanoparticles. It was also observed that the width of the peak for same-size nanoparticles is always significantly larger for Au than for Ag. It was also found that it can be reliably determined whether a BNP is of homogeneus alloy or core-shell structure and that, in the case of the latter, the core comprises of which element. We also assessed the performance of several ICP-MS based analytical methods in the analysis of the quantitative composition of bimetallic nanoparticles. Out of the three methods (normal resolution spICP-MS, direct NP nebulization with solution-mode ICP-MS, and solution-mode ICP-MS after the acid dissolution of the nanoparticles), the best accuracy and precision was achieved by spICP-MS. This method allows the determination of the composition with less than 10% relative inaccuracy and better than 3% precision. The analysis is fast and only requires the usual standard colloids for size calibration. Combining the results from both quantitative and structural analyses, the core diameter and shell thickness of core-shell particles can also be calculated. Copyright © 2017 Elsevier B.V. All rights reserved.

  3. Time-Dependent S{sub N} Calculations Describing Pulsed Source Experiments at the FRO Reactor

    Energy Technology Data Exchange (ETDEWEB)

    Bergstrom, A.; Kockum, J.; Soderberg, S. [Research Institute of National Defence, Stockholm (Sweden)

    1968-04-15

    In view of the difficulties in describing pulsed source experiments quantitatively in assemblies consisting of a fast core and a light reflector, a time-dependent S{sub N} code has been applied to this type of assembly. The code, written for the IBM 7090 computer, divides time into short intervals and computes the flux in spherical geometry for each interval using the Carlson S{sub N} scheme. The source term is obtained by extrapolation from two earlier time-intervals. Several problems in connection with the discretization of the time, space and energy dimensions are discussed. For the sub-critical assembly studied the treatment of the lower energy-groups is decisive for the numerical stability. A 22-group cross-section set with a low energy cut-off at 0.04 eV obtained with the SPENG programme has been used. The time intervals are varied continuously and are set proportional to the inverse of the maximum logarithmic time-derivative of the space and energy-dependent flux with the further restriction that they are not allowed to increase above a predetermined value. In a typical case, the intervals vary between 10{sup -9} and 10{sup -8} sec. The memory of the computer is fully exploited when 22 energy groups and 46 radial points are used. The computing time for each time-interval is about 6 sec. The code has been applied to a 3.5% sub-critical assembly consisting of a 20% enriched, spherical uranium metal core with a thick copper reflector and the calculations have been compared to experiments with good agreement. The calculations show that spectral equilibrium below 10 keV is not reached until times long compared to the usual measuring times and that the exponential decay finally reached is entirely determined by reflector properties at almost thermal energies. It is also shown that the simple one- and two-region models are inadequate in this case and that no time-independent prompt neutron life-time can be obtained from the measurements. (author)

  4. Chemical characterization of airborne particulate matter in ambient air of Nagoya, Japan, as studied by the multielement determination with ICP-AES and ICP-MS

    International Nuclear Information System (INIS)

    Fukai, Taku; Kobayashi, Tatsuya; Sakaguchi, Masahiro; Aoki, Masanori; Saito, Tsuyoshi; Fujimori, Eiji; Haraguchi, Hiroki

    2007-01-01

    The multielement determination of PM 10 (airborne particulate matter smaller than 10 μm) samples, which was collected by a high volume air sampler at the urban site of Nagoya City, was carried out by inductively coupled plasma atomic emission spectrometry (ICP-AES) and inductively coupled plasma mass spectrometry (ICP-MS). The present analytical method was validated by analyzing urban particulate matter standard reference material of NIST SRM 1648. The analytical data for ca. 30 elements in PM 10 samples collected during a period from 8 September to 9 October, 2003, were obtained in the concentration range from sub-μg g -1 to several-10 mg g -1 , but the data for 18 elements among ca. 30 elements were available for the characterization of PM 10 samples in ambient air, because of problems caused by the filter blanks. Then, the trends concerning the distributions of diverse elements in PM 10 samples were analyzed based on the enrichment factors and size distribution factors. The lithophile and siderophile elements were distributed more than 50% in coarse particle fraction (>2.1 μm), which was derived mainly from natural sources, such as soils and crustal minerals. On the other hand, chalcophile elements were distributed more than 50% in fine particle fraction ( 10 samples as well as their mining influence factors (MIFs) suggested their wide use in industrial productions. (author)

  5. Applications of ICP-MS in marine analytical chemistry

    Energy Technology Data Exchange (ETDEWEB)

    McLaren, J W; Siu, K W.M.; Lam, J W; Willie, S N; Maxwell, P S; Palepu, A; Koether, M; Berman, S S [National Research Council of Canada, Ottawa, ON (Canada). Analytical Chemistry Section

    1990-07-01

    The versatility of ICP-MS in marine analytical chemistry is illustrated with applications to the multielement trace analysis of two recently released marine reference materials, the coastal seawater CASS-2 and the non-defatted lobster hepatopancreas tissue LUTS-1, and to the determination of tributyltin and dibutyltin in the harbour sediment reference material PACS-1 by HPLC-ICP-MS. Seawater analyses were performed after separation of the trace elements either by adsorption on immobilized 8-hydroxyquinoline or by reductive coprecipitation with iron and palladium. Simultaneous determination of seven trace elements in LUTS-1, including mercury, by isotope dilution ICP-MS, was achieved after dissolution by microwave digestion with nitric acid and hydrogen peroxide. Butyltin species in PACS-1 were separated by cation exchange HPLC of an extract of the sediment; method detection limits for tributyltin and dibutyltin in sediment samples are estimated to be 5 ng Sn/g and 12 ng Sn/g, respectively. (orig.).

  6. Analysis of nanoparticles using the ICAP Q ICP-MS

    DEFF Research Database (Denmark)

    Kutscher, Daniel; McSheehy-Ducos, Shona; Lindemann, Torsten

    2014-01-01

    The analysis of Nanoparticles (NPs) has become one of the hot topics in analytical chemistry. However, detailed knowledge about potential risks or hazards is still unavailable. Two approaches have been developed in recent years using ICP-MS as a detection system: hyphenation of an appropriate...... separation technique like Field-Flow-Fractionation (FFF), or direct analysis using spICP-MS. The separation of particles and particle mixtures using FFF is based on the differing mobilities of different particle sizes in a laminar liquid flow. FFF is compatible for particle sizes in the low nm to low μm...... range and is thus perfectly suited for the separation of different NPs. Combined with other detection systems such as dynamic light scattering, it can provide also additional information about the particles of interest, like shape. In comparison, spICP-MS is able to analyze NPs directly based...

  7. ICP-MS analysis for long-lived radionuclides

    International Nuclear Information System (INIS)

    Roos, P.

    2010-01-01

    Full text: Inductively coupled plasma mass spectrometry (ICP-MS) is an attractive alternative for the analysis of radioisotopes having a half-life in the order of several hundred years and above. The technique should not be considered a replacement for radiometric measurements of these isotopes but merely an alternative. Similarly to radiometric techniques like alpha and beta spectrometry most analysis of 'low-level' concentrations by ICP-MS requires chemical isolation of the element in question. For 'ultra-low-level' concentrations this clean-up of the sample is usually even more necessary than for the alternative radiometric techniques. The presentation gives an overview of advantages and disadvantages in using ICP-MS and compares it to relevant radiometric alternatives. (author)

  8. StimSync: open-source hardware for behavioral and MRI experiments.

    Science.gov (United States)

    Rorden, Christopher; Hanayik, Taylor

    2014-04-30

    Many neuroscience experiments rely on presenting stimuli and measuring participants' responses to these events. Often computer screens, speakers and keyboards are sufficient. However, these devices are not appropriate for some situations. For example, some studies present tactile or olfactory stimuli or brain stimulation. Likewise, keyboard buttons are not appropriate for use with vocal responses, small animals or individuals with motor impairments. We describe StimSync, which simulates USB keyboard inputs, allowing use with most experimental software. StimSync can measure button presses, optical signals from magnetic resonance imaging systems, changes in ambient light (e.g. synchronizing intracranial electrography), and auditory events (a voice key). In addition to the USB keyboard mode (necessarily millisecond precision), StimSync can also be set to provide higher precision timing. This feature can be used to validate timing, ensuring event synchronization (e.g. auditory events, visual events, brain stimulation). In addition to recording inputs, StimSync provides seven digital outputs for controlling external devices. Finally, StimSync can record analog inputs; we illustrate how this can be used to evaluate the rise time for computer displays. We observed outputs with a mean latency of 2.1ms (sd=0.17ms) and USB inputs with a mean latency of 2ms (sd=0.54ms). StimSync statistically outperforms two professional solutions and numerically outperforms other devices described in the literature. StimSync (http://www.mccauslandcenter.sc.edu/CRNL/tools/stimsync) provides an open-source solution for controlling and validating neuroscience experiments. In addition to sharing the design, we have produced a batch of devices to demonstrate the market for professional implementations. Copyright © 2014. Published by Elsevier B.V.

  9. PhysioSpace: relating gene expression experiments from heterogeneous sources using shared physiological processes.

    Directory of Open Access Journals (Sweden)

    Michael Lenz

    Full Text Available Relating expression signatures from different sources such as cell lines, in vitro cultures from primary cells and biopsy material is an important task in drug development and translational medicine as well as for tracking of cell fate and disease progression. Especially the comparison of large scale gene expression changes to tissue or cell type specific signatures is of high interest for the tracking of cell fate in (trans- differentiation experiments and for cancer research, which increasingly focuses on shared processes and the involvement of the microenvironment. These signature relation approaches require robust statistical methods to account for the high biological heterogeneity in clinical data and must cope with small sample sizes in lab experiments and common patterns of co-expression in ubiquitous cellular processes. We describe a novel method, called PhysioSpace, to position dynamics of time series data derived from cellular differentiation and disease progression in a genome-wide expression space. The PhysioSpace is defined by a compendium of publicly available gene expression signatures representing a large set of biological phenotypes. The mapping of gene expression changes onto the PhysioSpace leads to a robust ranking of physiologically relevant signatures, as rigorously evaluated via sample-label permutations. A spherical transformation of the data improves the performance, leading to stable results even in case of small sample sizes. Using PhysioSpace with clinical cancer datasets reveals that such data exhibits large heterogeneity in the number of significant signature associations. This behavior was closely associated with the classification endpoint and cancer type under consideration, indicating shared biological functionalities in disease associated processes. Even though the time series data of cell line differentiation exhibited responses in larger clusters covering several biologically related patterns, top scoring

  10. Measurement of inclusion size by laser ablation ICP mass spectrometry

    International Nuclear Information System (INIS)

    Karasev, Andrey V.; Suito, Hideaki

    2004-01-01

    By using laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS), the measurement of particle size has been made for one component oxide (Al 2 O 3 and MgO) and multicomponent oxide (12CaO·7Al 2 O 3 and CaO-Al 2 O 3 -MgO) located on surface of iron or glass sample. The method of particle size estimation by LA-ICP-MS has been developed coupled with a new method of making samples with particles. The size calibration lines for Al 2 O 3 , MgO and CaO particles have been obtained. The results of particle size measurement by LA-ICP-MS are compared with those by SEM and single-particle optical sensing (SPOS) methods. It was confirmed that LA-ICP-MS has the perspective to be used for the quick measurement of inclusion composition and size in metal and other materials. The size frequency distributions of Al 2 O 3 particles measured by LA-ICP-MS in iron samples with particles agree reasonably well with those by SEM and SPOS in the range of particle diameter from 2 to 20 μm. The size of Al 2 O 3 , MgO and complex oxide (12CaO·7Al 2 O 3 and CaO-Al 2 O 3 -MgO) particles measured by LA-ICP-MS is in good agreement with that by SEM in the range of particle diameter from 10 to 40 μm. (author)

  11. PIXE and ICP-AES comparison in evaluating the efficiency of metal extraction and analysis in aerosol samples

    Energy Technology Data Exchange (ETDEWEB)

    Rugi, F.; Becagli, S.; Ghedini, C.; Marconi, M.; Severi, M.; Traversi, R.; Udisti, R. [Dep. of Chemistry, University of Florence, Sesto F.no (Fl) (Italy); Calzolai, G.; Chiari, M.; Lucarelli, F.; Nava, S. [Dep. of Physics and Astronomy , University of Florence and INFN, Sesto F. no (Fl) (Italy)

    2013-07-01

    Full text: A recent EU regulation (EN 149022005) requests the quantification of selected metals in the atmospheric particulate by mineralization with H{sub 2}0{sub 2} and HN0{sub 3} in microwave oven.This method might possibly conflict with the determination of the total metal content. In fact, the more the aerosol is enriched in crustal elements the more the difference in the two methods are expected, since the H{sub 2}0{sub 2}+ HN0{sub 3}, extraction is not reliable for metals in silicate form. In order to evaluate the extracted fraction, PIXE and ICP-AES measurements were carried out on the two halves of a series of PM10 and PM2.5 samples collected on Teflon filters in an urban site in the surrounding of Florence (Italy). An ICP-AES (Inductively Coupled Plasma -Atomic Emission Spectroscopy) method was optimized by an ultrasound nebuliser (CETAC 5000 AT+), in order to improve reproducibility and detection limit. In these conditions, it was possible quantifying AI, As, Cr, Cu, Fe, Mn, Ni, Pb and Vatsub-ppb levels. PIXE analysis using the external beam set-up at LABEC and a 3 MeV proton beam was carried out in order to measure the total elemental content of the metals. By comparing the ICP-AES and the PIXE results, a preliminary evaluation of the efficiency of the H{sub 2}0{sub 2} and HN0{sub 3} extraction method was performed. The obtained results (the mean values for the ICP-AES/PIXE ratio are reported in Table 1) show that the extraction procedure following the EN 14902 directive allows quantitative recoveries (80-120%, including the analytical uncertainties)for the majority of the analysed metals, especially for those mainly emitted by anthropic sources. This result points out that anthropic metals are present in the atmosphere as relatively available species (free metals, labile complexes, carbonates, oxides). On the contrary, lower recoveries were obtained for AI (mean value around 75%), a metal that has a relevant crustal fraction. Percentage of recovery of

  12. Inductively coupled plasma source mass spectrometry

    International Nuclear Information System (INIS)

    Price Russ, G. III

    1993-01-01

    Inductively coupled plasma source mass spectrometry (ICP-MS) is a relatively new (5 y commercial availability) technique for simultaneously determining the concentration and isotopic composition of a large number of elements at trace levels. The principle advantages of ICP-MS are the ability to measure essentially all the metallic elements at concentrations as low as 1 part in 10 12 by weight, to analyse aqueous samples directly, to determine the isotopic composition of essentially all the metallic elements, and to analyse samples rapidly (minutes). The history of the development of ICP-MS and discussions of a variety of applications have been discussed in detail in Date and Gray (1988). Koppenaal (1988, 1990) has reviewed the ICP-MS literature. In that ICP-MS is a relatively new and still evolving technique, this chapter will discuss potential capability more than proven performance. (author). 24 refs

  13. Seismic Imaging of the Source Physics Experiment Site with the Large-N Seismic Array

    Science.gov (United States)

    Chen, T.; Snelson, C. M.; Mellors, R. J.

    2017-12-01

    The Source Physics Experiment (SPE) consists of a series of chemical explosions at the Nevada National Security Site. The goal of SPE is to understand seismic wave generation and propagation from these explosions. To achieve this goal, we need an accurate geophysical model of the SPE site. A Large-N seismic array that was deployed at the SPE site during one of the chemical explosions (SPE-5) helps us construct high-resolution local geophysical model. The Large-N seismic array consists of 996 geophones, and covers an area of approximately 2 × 2.5 km. The array is located in the northern end of the Yucca Flat basin, at a transition from Climax Stock (granite) to Yucca Flat (alluvium). In addition to the SPE-5 explosion, the Large-N array also recorded 53 weight drops. Using the Large-N seismic array recordings, we perform body wave and surface wave velocity analysis, and obtain 3D seismic imaging of the SPE site for the top crust of approximately 1 km. The imaging results show clear variation of geophysical parameter with local geological structures, including heterogeneous weathering layer and various rock types. The results of this work are being incorporated in the larger 3D modeling effort of the SPE program to validate the predictive models developed for the site.

  14. ICP-MS and elemental tags for the life sciences

    Energy Technology Data Exchange (ETDEWEB)

    Giesen, Charlotte

    2012-08-07

    Inductively coupled plasma mass spectrometry (ICP-MS) has been applied for the analysis of biomolecules due to its high sensitivity, wide linear dynamic range, and multielement capabilities. However, outside the elemental MS community the potential of this technique, e.g. for life sciences applications, is not yet fully exploited. Thus, the development of ICP-MS-based (immuno) assays for a wide range of medical (cancer diagnostics, cisplatin toxicity studies), biochemical (DNA microarray, single cell analysis), and environmental (analysis of comestible goods) applications was accomplished by utilization of chemical labels. Laser ablation (LA)-ICP-MS was employed for the direct analysis of solid samples like microarrays and thin tissue sections. An immunoassay was developed for ochratoxin A (OTA) determination in wine, and ICP-MS detection was compared to conventional photometry by gold nanoparticle tagging and horseradish peroxidase, respectively. Detection limits of the assay were optimized to 0.003 {mu}g L{sup -1}, and the quantification range was 0.01-1 {mu}g L{sup -1} for both methods. For LA-ICP-MS-based DNA microarray detection, gold nanoparticle tags were specifically introduced via a streptavidin-biotin linkage. In immunohistochemistry (IHC), up to 20 tumor markers are routinely evaluated for one patient and thus, a common analysis results in a series of time consuming staining procedures. Hence, LA-ICP-MS was elaborated as a detection tool for a novel, multiplexed IHC analysis of tissue sections. Different lanthanides were employed for the simultaneous detection of up to three tumor markers (Her 2, CK 7, and MUC 1) in a breast cancer tissue. Additionally, iodine was employed as a labeling reagent, and a new LA-ICP-MS method for single cell and cell nucleus imaging was developed at 4 {mu}m laser spot size. Iodine was also applied as a new internal standard for tissue samples. Moreover, Pt-protein complexes separated by an optimized 1D and 2D gel

  15. Flame experiments at the advanced light source: new insights into soot formation processes.

    Science.gov (United States)

    Hansen, Nils; Skeen, Scott A; Michelsen, Hope A; Wilson, Kevin R; Kohse-Höinghaus, Katharina

    2014-05-26

    The following experimental protocols and the accompanying video are concerned with the flame experiments that are performed at the Chemical Dynamics Beamline of the Advanced Light Source (ALS) of the Lawrence Berkeley National Laboratory(1-4). This video demonstrates how the complex chemical structures of laboratory-based model flames are analyzed using flame-sampling mass spectrometry with tunable synchrotron-generated vacuum-ultraviolet (VUV) radiation. This experimental approach combines isomer-resolving capabilities with high sensitivity and a large dynamic range(5,6). The first part of the video describes experiments involving burner-stabilized, reduced-pressure (20-80 mbar) laminar premixed flames. A small hydrocarbon fuel was used for the selected flame to demonstrate the general experimental approach. It is shown how species' profiles are acquired as a function of distance from the burner surface and how the tunability of the VUV photon energy is used advantageously to identify many combustion intermediates based on their ionization energies. For example, this technique has been used to study gas-phase aspects of the soot-formation processes, and the video shows how the resonance-stabilized radicals, such as C3H3, C3H5, and i-C4H5, are identified as important intermediates(7). The work has been focused on soot formation processes, and, from the chemical point of view, this process is very intriguing because chemical structures containing millions of carbon atoms are assembled from a fuel molecule possessing only a few carbon atoms in just milliseconds. The second part of the video highlights a new experiment, in which an opposed-flow diffusion flame and synchrotron-based aerosol mass spectrometry are used to study the chemical composition of the combustion-generated soot particles(4). The experimental results indicate that the widely accepted H-abstraction-C2H2-addition (HACA) mechanism is not the sole molecular growth process responsible for the formation

  16. Pollutant Source Tracking (PST) Technical Guidance

    Science.gov (United States)

    2011-12-01

    in the context of heavy metals (lead, copper), is considered to be a minor process contribution to the source fingerprint. 3.7 RAPID SCREENING...limits (summarized in Table 2) support the use of ICP-AES (ICP-OES) for heavy metal determination in soils , sediments, wastewater and other matrices...are included here. Isotopic ratios of stable isotopes of the metal of interest can be used for source identification and apportionment in complex

  17. Determination of rhenium traces in river water by Q-ICP-MS and HR-ICP-MS

    International Nuclear Information System (INIS)

    Uchida, S.; Tagami, K.; Saito, M.

    2003-01-01

    A simple separation method was applied to determine rhenium in river water using Q-ICP-MS and HR-ICP-MS. Re was concentrated from 420-925 ml river water using a TEVA resin minicolumn. Such extraction using a resin could separate Re from most sample matrices and trace elements. Almost 100% recovery was found throughout the method as determined with radioactive multitracers. The HR-ICP-MS was also used for the direct determination because of its low detection limit for Re (0.007 pg/ml). The Re concentration in the river water samples ranged from 0.9 to 6.5 pg/ml and the three analysis results showed good agreement with each other. (author)

  18. Implementing Open Source Platform for Education Quality Enhancement in Primary Education: Indonesia Experience

    Science.gov (United States)

    Kisworo, Marsudi Wahyu

    2016-01-01

    Information and Communication Technology (ICT)-supported learning using free and open source platform draws little attention as open source initiatives were focused in secondary or tertiary educations. This study investigates possibilities of ICT-supported learning using open source platform for primary educations. The data of this study is taken…

  19. Spectroscopic investigations of ceramic materials using ICP-OES with modern vaporisation systems

    International Nuclear Information System (INIS)

    Reisch, M.U.; Mazurkiewicz, M.; Nickel, H.

    1990-10-01

    The object of this work was to study the evaporation and excitation process in the analysis of ceramic powders by the direct insertion of the samples into an inductively coupled plasma (ICP) as well as by external electrothermal evaporation. The evaporation rates were monitored by using 59 Fe and 115 Cd radiaoactive isotopes. The influence of various parameters such as the geometrical conditions, the carrier gas injection and the flow characteristics have been investigated. These methods have the advantage of easy preparation, no dilution and short experiment durations. The influence of different thermochemical additives as well as third elements, matrix compositions and grain size of the powders was determined. (orig.) [de

  20. Comparison of residual NAPL source removal techniques in 3D metric scale experiments

    Science.gov (United States)

    Atteia, O.; Jousse, F.; Cohen, G.; Höhener, P.

    2017-07-01

    This study compared four treatment techniques for the removal of a toluene/n-decane as NAPL (Non Aqueous Phase Liquid) phase mixture in identical 1 cubic meter tanks filled with different kind of sand. These four treatment techniques were: oxidation with persulfate, surfactant washing with Tween80®, sparging with air followed by ozone, and thermal treatment at 80 °C. The sources were made with three lenses of 26 × 26 × 6.5 cm, one having a hydraulic conductivity similar to the whole tank and the two others a value 10 times smaller. The four techniques were studied after conditioning the tanks with tap water during approximately 80 days. The persulfate treatment tests showed average removal of the contaminants but significant flux decrease if density effects are considered. Surfactant flushing did not show a highly significant increase of the flux of toluene but allowed an increased removal rate that could lead to an almost complete removal with longer treatment time. Sparging removed a significant amount but suggests that air was passing through localized gas channels and that the removal was stagnating after removing half of the contamination. Thermal treatment reached 100% removal after the target temperature of 80 °C was kept during more than 10 d. The experiments emphasized the generation of a high-spatial heterogeneity in NAPL content. For all the treatments the overall removal was similar for both n-decane and toluene, suggesting that toluene was removed rapidly and n-decane more slowly in some zones, while no removal existed in other zones. The oxidation and surfactant results were also analyzed for the relation between contaminant fluxes at the outlet and mass removal. For the first time, this approach clearly allowed the differentiation of the treatments. As a conclusion, experiments showed that the most important differences between the tested treatment techniques were not the global mass removal rates but the time required to reach 99% decrease in

  1. Integration of relational and textual biomedical sources. A pilot experiment using a semi-automated method for logical schema acquisition.

    Science.gov (United States)

    García-Remesal, M; Maojo, V; Billhardt, H; Crespo, J

    2010-01-01

    Bringing together structured and text-based sources is an exciting challenge for biomedical informaticians, since most relevant biomedical sources belong to one of these categories. In this paper we evaluate the feasibility of integrating relational and text-based biomedical sources using: i) an original logical schema acquisition method for textual databases developed by the authors, and ii) OntoFusion, a system originally designed by the authors for the integration of relational sources. We conducted an integration experiment involving a test set of seven differently structured sources covering the domain of genetic diseases. We used our logical schema acquisition method to generate schemas for all textual sources. The sources were integrated using the methods and tools provided by OntoFusion. The integration was validated using a test set of 500 queries. A panel of experts answered a questionnaire to evaluate i) the quality of the extracted schemas, ii) the query processing performance of the integrated set of sources, and iii) the relevance of the retrieved results. The results of the survey show that our method extracts coherent and representative logical schemas. Experts' feedback on the performance of the integrated system and the relevance of the retrieved results was also positive. Regarding the validation of the integration, the system successfully provided correct results for all queries in the test set. The results of the experiment suggest that text-based sources including a logical schema can be regarded as equivalent to structured databases. Using our method, previous research and existing tools designed for the integration of structured databases can be reused - possibly subject to minor modifications - to integrate differently structured sources.

  2. Determination of neptunium in soil by ICP-MS

    International Nuclear Information System (INIS)

    Ayranov, M.; Kraehenbuehl, U.

    2005-01-01

    A fast and simple method for the determination of 237 Np in soil is presented. The borate fusion decreases the sample pre-treatment time and a TEVA extraction chromatography separates neptunium from uranium and the interfering matrix components. A comparison of the sensitivities of alpha spectrometry and sector field ICP-MS for determination of 237 Np is presented. (orig.)

  3. Air ICP uses for instantaneous monitoring of airborne pollutants

    International Nuclear Information System (INIS)

    Thouzeau, F.; Birolleau, J.C.; Fieni, J.M.; Bergey, C.

    1987-01-01

    Recently the development of a pure AIR-ICP which breathes in and excites the analysed air without sample dilution, allowed the application of this technique to the real time analysis of airborne metallic pollutants. First results obtained on airborne Beryllium in a laboratory and a test-site apparatus are presented in this paper

  4. Some practical applications of an ICP-MS instrument

    International Nuclear Information System (INIS)

    Meddings, B.; Ng, R.

    1987-01-01

    An early model commercial ICP-MS instrument (PlasmaQuad from VG Isotopes Limited) was acquired more than two years ago. As a typical analytical laboratory in the metallurgical field, the application of the ICP-MS technique to real sample analysis is the authors prime concern. The process of introducing this state-of-the-art instrument into routine analysis will be described. The modifications and limitations necessary to achieve acceptable precision under normal working conditions will be outlined. In most cases, practical problems can be circumvented with some sacrifice in analytical performance in the area of detection limits and dynamic range. In this presentation, specific applications of the ICP-MS technique in the authors laboratory will be discussed. These include trace analysis on high purity metals such as copper, aluminum, cobalt, nickel etc., on refinery feed samples such as nickel sulfate, mixed cobalt and nickel sulfide, cobalt cathode, samarium oxide etc., on alloys such as cobalt-samarium magnetic materials, nickel or cobalt based alloys used in turbine blades etc. Other applications such as the determination of uranium in phosphate rock, trace analysis on fertilizers, water samples and high purity acids will also be mentioned. The solutions to the practical problems encountered in these applications will be discussed. The analytical power of the ICP-MS technique for real sample analysis will be assessed

  5. Quality and Safety of Home ICP Monitoring Compared with In-Hospital Monitoring

    DEFF Research Database (Denmark)

    Andresen, Morten; Juhler, Marianne; Munch, Tina Nørgaard

    2012-01-01

    Introduction: Intracranial pressure (ICP) monitoring is usually conducted in-hospital using stationary devices. Modern mobile ICP monitoring systems present new monitoring possibilities more closely following the patients' daily life. We reviewed patient safety, quality of technical data...

  6. Molecular Characterization of Prostate Cancer Cell Oncolysis by Herpes Simplex Virus ICP0 Mutants

    National Research Council Canada - National Science Library

    Mossman, Karen

    2006-01-01

    .... Briefly, the goals of the proposal were to characterize the oncolytic capacity of Herpes simplex virus type 1 ICP0 mutants in prostate cancer cells given the relationship between ICP0 and two tumor...

  7. Geology of the Source Physics Experiment Site, Climax Stock, Nevada National Security Site

    Energy Technology Data Exchange (ETDEWEB)

    Townsend, M., Prothro, L. B., Obi, C.

    2012-03-15

    A test bed for a series of chemical explosives tests known as Source Physics Experiments (SPE) was constructed in granitic rock of the Climax stock, in northern Yucca Flat at the Nevada National Security Site in 2010-2011. These tests are sponsored by the U.S. Department of Energy, National Nuclear Security Administration's National Center for Nuclear Security. The test series is designed to study the generation and propagation of seismic waves, and will provide data that will improve the predictive capability of calculational models for detecting and characterizing underground explosions. Abundant geologic data are available for the area, primarily as a result of studies performed in conjunction with the three underground nuclear tests conducted in the Climax granite in the 1960s and a few later studies of various types. The SPE test bed was constructed at an elevation of approximately 1,524 meters (m), and consists of a 91.4-centimeter (cm) diameter source hole at its center, surrounded by two rings of three 20.3-cm diameter instrument holes. The inner ring of holes is positioned 10 m away from the source hole, and the outer ring of holes is positioned 20 m from the source hole. An initial 160-m deep core hole was drilled at the location of the source hole that provided information on the geology of the site and rock samples for later laboratory testing. A suite of geophysical logs was run in the core hole and all six instruments holes to obtain matrix and fracture properties. Detailed information on the character and density of fractures encountered was obtained from the borehole image logs run in the holes. A total of 2,488 fractures were identified in the seven boreholes, and these were ranked into six categories (0 through 5) on the basis of their degree of openness and continuity. The analysis presented here considered only the higher-ranked fractures (ranks 2 through 5), of which there were 1,215 (approximately 49 percent of all fractures identified

  8. Simulation and beam line experiments for the superconducting ECR ion source VENUS

    International Nuclear Information System (INIS)

    Todd, Damon S.; Leitner, Daniela; Grote, David P.; Lyneis, ClaudeM.

    2007-01-01

    The particle-in-cell code Warp has been enhanced to incorporate both two- and three-dimensional sheath extraction models giving Warp the capability of simulating entire ion beam transport systems including the extraction of beams from plasma sources. In this article we describe a method of producing initial ion distributions for plasma extraction simulations in electron cyclotron resonance (ECR) ion sources based on experimentally measured sputtering on the source biased disc. Using this initialization method, we present preliminary results for extraction and transport simulations of an oxygen beam and compare them with experimental beam imaging on a quartz viewing plate for the superconducting ECR ion source VENUS

  9. Data Release Report for Source Physics Experiments 2 and 3 (SPE-2 and SPE-3) Nevada National Security Site

    Energy Technology Data Exchange (ETDEWEB)

    Townsend, Margaret [National Security Technologies, LLC, Las Vegas, NV (United States). Nevada Test Site; Obi, Curtis [National Security Technologies, LLC, Las Vegas, NV (United States). Nevada Test Site

    2015-01-26

    The second Source Physics Experiment shot (SPE-2) was conducted in Nevada on October 25, 2011, at 1900:00.011623 Greenwich Mean Time (GMT). The explosive source was 997 kilograms (kg) trinitrotoluene (TNT) equivalent of sensitized heavy ammonium fuel oil (SHANFO) detonated at a depth of 45.7 meters (m). The third Source Physics Experiment shot (SPE-3) was conducted in Nevada on July 24, 2012, at 1800:00.44835 GMT. The explosive source was 905 kg TNT equivalent of SHANFO detonated at a depth of 45.8 m. Both shots were recorded by an extensive set of instrumentation that includes sensors both at near-field (less than 100 m) and far-field (100 m or greater) distances. The near-field instruments consisted of three-component accelerometers deployed in boreholes at 15, 46, and 55 m depths around the shot and a set of single-component vertical accelerometers on the surface. The far-field network was composed of a variety of seismic and acoustic sensors, including short-period geophones, broadband seismometers, three-component accelerometers, and rotational seismometers at distances of 100 m to 25 kilometers. This report coincides with the release of these data for analysts and organizations that are not participants in this program. This report describes the second and third Source Physics Experiment shots and the various types of near-field and far-field data that are available.

  10. How Students Describe the Sources of Their Emotional and Motivational Experiences during the Learning Process: A Qualitative Approach

    Science.gov (United States)

    Jarvenoja, Hanna; Jarvela, Sanna

    2005-01-01

    The aim of the study reported in this paper was to consider the sources of emotional and motivational experiences of secondary school students (N=18), 12-15 years old, during computer-supported collaborative learning projects. We chose the concept of volition to frame the analysis of the various kinds of descriptions the students give of their…

  11. Solid electron sources for the energy scale monitoring in the KATRIN experiment

    CERN Document Server

    Zbořil, Miroslav; Vénos, D

    The KArlsruhe TRItium Neutrino (KATRIN) experiment represents a next-generation tritium $\\beta$-decay experiment designed to perform a high precision direct measurement of the electron anti-neutrino mass m($\

  12. Multielement determination of major-to-ultratrace elements in salmon egg by ICP-AES and ICP-MS

    Energy Technology Data Exchange (ETDEWEB)

    Matsuura, Hirotaka; Haraguchi, Hiroki [Nagoya Univ., Graduate School of Engineering, Dept. of Applied Chemistry, Nagoya, Aichi (Japan)

    2002-04-01

    The multielement determination of major-to-ultratrace elements in salmon egg was carried out by ICP-AES and ICP-MS. First, salmon eggs (30 eggs used) were digested with conc. nitric acid and 60% perchloric acid by heating almost to dryness repeatedly. Finally, the residues of salmon eggs were dissolved in 1 M nitric acid and the sample solutions were analyzed by ICP-AES and ICP-MS. About 40 elements could be determined over the concentration range in 9 orders of magnitude. The concentrations of bio-essential elements, such as Zn, Fe, and Cu, in salmon egg were 10-100 times higher than those in human blood serum. In addition, the major-to-ultratrace elements in cell cytoplasm and cell membrane were separately determined in a similar manner to those in whole egg cell. The concentrations of most bio-essential elements were higher in cell cytoplasm than in cell membrane, while those of Fe and Cu were higher in cell membrane than in cell cytoplasm of salmon egg. (author)

  13. Analyzing Korean consumers’ latent preferences for electricity generation sources with a hierarchical Bayesian logit model in a discrete choice experiment

    International Nuclear Information System (INIS)

    Byun, Hyunsuk; Lee, Chul-Yong

    2017-01-01

    Generally, consumers use electricity without considering the source the electricity was generated from. Since different energy sources exert varying effects on society, it is necessary to analyze consumers’ latent preference for electricity generation sources. The present study estimates Korean consumers’ marginal utility and an appropriate generation mix is derived using the hierarchical Bayesian logit model in a discrete choice experiment. The results show that consumers consider the danger posed by the source of electricity as the most important factor among the effects of electricity generation sources. Additionally, Korean consumers wish to reduce the contribution of nuclear power from the existing 32–11%, and increase that of renewable energy from the existing 4–32%. - Highlights: • We derive an electricity mix reflecting Korean consumers’ latent preferences. • We use the discrete choice experiment and hierarchical Bayesian logit model. • The danger posed by the generation source is the most important attribute. • The consumers wish to increase the renewable energy proportion from 4.3% to 32.8%. • Korea's cost-oriented energy supply policy and consumers’ preference differ markedly.

  14. Study of X-ray and gamma ray sources observed by the SIGNE (Prognoz 6 Satellite) experiment in the regions of the galactic center and anticenter

    International Nuclear Information System (INIS)

    Violes, F.

    1981-12-01

    Characteristics of the SIGNE II MP 6 experiment are reported and procedures to obtain the fluxes detected from all the sources are described. We next present deconvolution method used to isolate the galactic center sources. In the last chapter we present and discuss the photon spectra of the sources observed by the SIGNE II MP 6 experiment [fr

  15. Introducing wet aerosols into the static high sensitivity ICP (SHIP)

    Energy Technology Data Exchange (ETDEWEB)

    Scheffer, Andy; Engelhard, Carsten; Sperling, Michael; Buscher, Wolfgang [University of Muenster, Institute of Inorganic and Analytical Chemistry, Muenster (Germany)

    2007-08-15

    A demountable design of the static high sensitivity ICP (SHIP) for optical emission spectrometry is presented, and its use as an excitation source with the introduction of wet aerosols was investigated. Aerosols were produced by standard pneumatic sample introduction systems, namely a cross flow nebulizer, Meinhard nebulizer and PFA low flow nebulizer, which have been applied in conjunction with a double pass and a cyclonic spray chamber. The analytical capabilities of these sample introduction systems in combination with the SHIP system were evaluated with respect to the achieved sensitivity. It was found that a nebulizer tailored for low argon flow rates (0.3-0.5 L min{sup -1}) is best suited for the low flow plasma (SHIP). An optimization of all gas flow rates of the SHIP system with the PFA low flow nebulizer was carried out in a two-dimensional way with the signal to background ratio (SBR) and the robustness as optimization target parameters. Optimum conditions for a torch model with 1-mm injector tube were 0.25 and 0.36 L min{sup -1} for the plasma gas and the nebulizer gas, respectively. A torch model with a 2-mm injector tube was optimized to 0.4 L min{sup -1} for the plasma gas and 0.44 L min{sup -1} for the nebulizer gas. In both cases the SHIP system saves approximately 95% of the argon consumed by conventional inductively coupled plasma systems. The limits of detection were found to be in the low microgram per litre range and below for many elements, which was quite comparable to those of the conventional setup. Furthermore, the short-term stability and the wash out behaviour of the SHIP were investigated. Direct comparison with the conventional setup indicated that no remarkable memory effects were caused by the closed design of the torch. The analysis of a NIST SRM 1643e (Trace Elements in Water) with the SHIP yielded recoveries of 97-103% for 13 elements, measured simultaneously. (orig.)

  16. A comparison between PIXE and ICP-AES measurements of metals in aerosol particulate collected in urban and marine sites in Italy

    Energy Technology Data Exchange (ETDEWEB)

    Traversi, R.; Becagli, S. [Department of Chemistry “Ugo Schiff”, University of Florence, Via della Lastruccia 3, I-50019 Sesto F.no, Florence (Italy); Calzolai, G.; Chiari, M.; Giannoni, M. [Department of Physics and Astronomy, University of Florence and I.N.F.N., Florence, Via G. Sansone 1, I-50019 Sesto F.no, Florence (Italy); Lucarelli, F., E-mail: lucarelli@fi.infn.it [Department of Physics and Astronomy, University of Florence and I.N.F.N., Florence, Via G. Sansone 1, I-50019 Sesto F.no, Florence (Italy); Nava, S. [Department of Physics and Astronomy, University of Florence and I.N.F.N., Florence, Via G. Sansone 1, I-50019 Sesto F.no, Florence (Italy); Rugi, F.; Severi, M.; Udisti, R. [Department of Chemistry “Ugo Schiff”, University of Florence, Via della Lastruccia 3, I-50019 Sesto F.no, Florence (Italy)

    2014-01-01

    PIXE and ICP-AES techniques are largely used in atmospheric aerosol studies. Since PIXE is able to provide the total elemental concentrations, while ICP-AES results depend on the extraction conditions, parallel PIXE and ICP-AES measurements of Fe, Al, Cu, Pb, Mn, Cr, Ni, V, As on PM10 and PM2.5 samples were compared. Two extraction procedures were applied to samples from 5 sites at different anthropization level in Italy: a “weak” extraction (HNO{sub 3} at pH = 1.5) and a “strong” extraction (micro-wave oven in HNO{sub 3} and H{sub 2}O{sub 2} – following EU rules). The amount of the metal extracted in the different conditions resulted to be strongly dependent on the sampling site, on the main sources of the particle (crustal or anthropic) containing the metal and on the sampled size class.

  17. Experience and problems of the automated measuring and sorting of sealed radiation sources

    International Nuclear Information System (INIS)

    Shmidt, G.

    1979-01-01

    It has been shown that with the help of a serial device for samples changing and a mini-computer with a suitable software it is possible to organize the radioactivity measuring and sorting of sealed gamma-sources with activity in the microcuri region. Application of the computer permits to rise accuracy of the data on the radiation sources radioactivity, sorted according to the preset activity level groups and, in the casa of necessity, to perform the activity measurements with lower error. The method listed, gives the working-time economy of nearly 4 hours in measuring and sorting of some 500 sealed radiation sources [ru

  18. Analysis of marine samples by neutron-induced prompt gamma-ray technique and ICP-MS

    International Nuclear Information System (INIS)

    Yonezawa, C.; Matsue, H.; McKay, K.; Povinec, P.

    2001-01-01

    Multi-element and isotopic analyses of oils and marine environmental samples were carried out to estimate a contamination source using a 'finger printing' method. Elemental analyses were carried out using neutron-induced prompt gamma-ray analysis (PGA), instrumental neutron activation analysis (INAA) at the Japan Atomic Institute, Tokai-mura, Japan (JAERI) and ICP-MS in the IAEA Marine Environment Laboratory, Monaco (MEL). Fifteen elements including light elements, H, B, N, Si and Ca, which cannot be determined by INAA and ICP-MS, were determined by PGA. A total of 47 elements were determined in the present study. The potential of PGA for the determination of isotopic ratios was tested by measuring 34 S/ 32 S ratios in oils. The evaluation of historical records of marine environmental conditions using annual bands in coral samples was also investigated. (author)

  19. Reflection processing of the large-N seismic data from the Source Physics Experiment (SPE)

    Energy Technology Data Exchange (ETDEWEB)

    Paschall, Olivia C. [Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

    2016-07-18

    The purpose of the SPE is to develop a more physics-based model for nuclear explosion identification to understand the development of S-waves from explosion sources in order to enhance nuclear test ban treaty monitoring.

  20. Observations of variable and transient X-ray sources with the Ariel V Sky Survey Experiment

    International Nuclear Information System (INIS)

    Pounds, K.A.; Cooke, B.A.; Ricketts, M.J.; Turner, M.J.; Peacock, A.; Eadie, G.

    1976-01-01

    Results obtained during the first six months in orbit of Aerial V with the Leicester Sky Survey are reviewed. Among 80 sources found by a scan of the Milky Way, 16 are new, and 11 UHURU sources in the scanned region are not detected. Some of these sources may be transient. The light curve of Cen X-3 in a binary cycle shows a dip between phase 0.5 and 0.75, and a secondary maximum at the centre of the dip. The dip and the maximum get progressively weaker in the succeeding cycles. These features are interpreted in terms of the stellar wind accretion model. Cyg X-1 observation for 14 days gives a broad minimum around superior conjunction. Four bright transient sources of nova-like light curves have been observed. The light curves and the spectra are given for TrA X-1 (A1524-62) and Tau X-T (A0535+26). (Auth.)

  1. The feeling of fluent perception: a single experience from multiple asynchronous sources.

    Science.gov (United States)

    Wurtz, Pascal; Reber, Rolf; Zimmermann, Thomas D

    2008-03-01

    Zeki and co-workers recently proposed that perception can best be described as locally distributed, asynchronous processes that each create a kind of microconsciousness, which condense into an experienced percept. The present article is aimed at extending this theory to metacognitive feelings. We present evidence that perceptual fluency-the subjective feeling of ease during perceptual processing-is based on speed of processing at different stages of the perceptual process. Specifically, detection of briefly presented stimuli was influenced by figure-ground contrast, but not by symmetry (Experiment 1) or the font (Experiment 2) of the stimuli. Conversely, discrimination of these stimuli was influenced by whether they were symmetric (Experiment 1) and by the font they were presented in (Experiment 2), but not by figure-ground contrast. Both tasks however were related with the subjective experience of fluency (Experiments 1 and 2). We conclude that subjective fluency is the conscious phenomenal correlate of different processing stages in visual perception.

  2. QEMSCAN+LA-ICP-MS: a 'big data' generator for sedimentary provenance analysis

    Science.gov (United States)

    Vermeesch, Pieter; Rittner, Martin; Garzanti, Eduardo

    2017-04-01

    Sedimentary provenance may be traced by 'fingerprinting' sediments with chemical, mineralogical or isotopic means. Normally, each of these provenance proxies is characterised on a separate aliquot of the same sample. For example, the chemical composition of the bulk sample may be analysed by X-ray fluorescence (XRF) on one aliquot, framework petrography on another, heavy mineral analysis on a density separate of a third split, and zircon U-Pb dating on a further density separate of the heavy mineral fraction. The labour intensity of this procedure holds back the widespread application of multi-method provenance studies. We here present a new method to solve this problem and avoid mineral separation by coupling a QEMSCAN electron microscope to an LA-ICP-MS instrument and thereby generate all four aforementioned provenance datasets as part of the same workflow. Given a polished hand specimen, a petrographic thin section, or a grain mount, the QEMSCAN+LA-ICP-MS method produces chemical and mineralogical maps from which the X-Y coordinates of the datable mineral are extracted. These coordinates are subsequently passed on to the laser ablation system for isotopic and, hence, geochronological analysis. In the process of finding all the zircons in a sediment grain mount, the QEMSCAN yields the compositional and mineralogical compositions as byproducts. We have applied the new QEMSCAN+LA-ICP-MS instrument suite to over 100 samples from three large sediment routing systems: (1) the Tigris-Euphrates river catchments and Rub' Al Khali desert in Arabia; (2) the Nile catchment in northeast Africa and (3) desert and beach sands between the Orange and Congo rivers in southwest Africa. These studies reveal (1) that Rub' Al Khali sand is predominantly derived from the Arabian Shield and not from Mesopotamia; (2) that the Blue Nile is the principal source of Nile sand; and (3) that Orange River sand is carried northward by longshore drift nearly 1,800km from South Africa to southern

  3. Experiments with planar inductive ion source meant for creation ofH+ Beams

    Energy Technology Data Exchange (ETDEWEB)

    Vainionpaa, J.H.; Kalvas, T.; Hahto, S.K.; Reijonen, J.

    2007-02-07

    In this article the effect of different engineering parameters of an rf-driven ion sources with external spiral antenna and quartz disk rf-window are studied. Paper consists of three main topics: The effect of source geometry on the operation gas pressure, the effect of source materials and magnetic confinement on extracted current density and ion species and the effect of different antenna geometries on the extracted current density. The operation gas pressure as a function of the plasma chamber diameter, was studied. This was done with three cylindrical plasma chambers with different inner diameters. The chamber materials were studied using two materials, aluminum and alumina (AlO{sub 2}). The removable 14 magnet multicusp confinement arrangement enabled us to compare the effects of the two wall materials with and without the magnetic confinement. Highest proton fraction of {approx} 8% at 2000 W of rf-power and at pressure of 1.3 Pa was measured using AlO{sub 2} plasma chamber and no multicusp confinement. For all the compared ion sources at 1000W of rf-power, source with multicusp confinement and AlO2 plasma chamber yields highest current density of 82.7 mA/cm{sup 2} at operation pressure of 4 Pa. From the same source highest measured current density of 143 mA/cm{sup 2} at 1.3 Pa and 2200W of rf-power was achieved. Multicusp confinement increased the maximum extracted current up to factor of two. Plasma production with different antenna geometries was also studied. Antenna tests were performed using same source geometry as in source material study with AlO{sub 2} plasma chamber and multicusp confinement. The highest current density was achieved with 4.5 loop solenoid antenna with 6 cm diameter. Slightly lower current density with lower pressure was achieved using tightly wound 3 loop spiral antenna with 3.3 cm ID and 6 cm OD.

  4. The regulatory control over radiation sources: the Brazilian experience and some lessons learned from industrial applications

    International Nuclear Information System (INIS)

    Costa, E.L.C.; Gomes, J.D.R.L.; Gomes, R.S.; Costa, M.L.L.; Thomé, Z.D.; Instituto Militar de Engenharia

    2017-01-01

    This study gives an overview of the activities of the National Commission of Nuclear Energy (CNEN), as the Brazilian nuclear regulatory authority. These activities are described, especially those related to management of orphan sources and radioactive material in scrap metal considering the actions already put into place by CNEN during the licensing and controlling of radioactive sources in the industry and other facilities. In Brazil, there is not yet an effective system for controlling the scrap metal and recycling industry, thus a coordinated approach to achieve a harmonized and effective response with the involvement of third parties is needed, especially the metal industries and ores facilities. These practices call for stringent regulatory control, in order to reduce the occurrence of orphan sources, and consequently, radioactive material appearing in scrap metal. Some challenges of managing the national radiation sources register systems will be discussed, in order to cover effectively all the radiation source history (in a 'from the cradle to the grave' basis), and the dynamic maintenance and update of these data. The main industrial applications considered in this work are those dealing with constant movement of sources all over the country, with geographical issues to be considered in the managing and controlling actions, such as gammagraphy and well-logging. This study aims to identify and promote good practices to prevent inadvertent diversion of radioactive material, taking into account existing international recommendations and some lessons learned in national level. (author)

  5. The regulatory control over radiation sources: the Brazilian experience and some lessons learned from industrial applications

    Energy Technology Data Exchange (ETDEWEB)

    Costa, E.L.C.; Gomes, J.D.R.L.; Gomes, R.S.; Costa, M.L.L.; Thomé, Z.D., E-mail: evaldo@cnen.gov.br, E-mail: jlopes@cnen.gov.br, E-mail: rogeriog@cnen.gov.br, E-mail: mara@cnen.gov.br, E-mail: zielithome@gmail.com [Comissao Nacional de Energia Nuclear (CNEN), Rio de Janeiro, RJ (Brazil). Diretoria de Radioproteção e Segurança Nuclear; Instituto Militar de Engenharia (IME), Rio de Janeiro, RJ (Brazil). Seção de Engenharia Nuclear

    2017-11-01

    This study gives an overview of the activities of the National Commission of Nuclear Energy (CNEN), as the Brazilian nuclear regulatory authority. These activities are described, especially those related to management of orphan sources and radioactive material in scrap metal considering the actions already put into place by CNEN during the licensing and controlling of radioactive sources in the industry and other facilities. In Brazil, there is not yet an effective system for controlling the scrap metal and recycling industry, thus a coordinated approach to achieve a harmonized and effective response with the involvement of third parties is needed, especially the metal industries and ores facilities. These practices call for stringent regulatory control, in order to reduce the occurrence of orphan sources, and consequently, radioactive material appearing in scrap metal. Some challenges of managing the national radiation sources register systems will be discussed, in order to cover effectively all the radiation source history (in a 'from the cradle to the grave' basis), and the dynamic maintenance and update of these data. The main industrial applications considered in this work are those dealing with constant movement of sources all over the country, with geographical issues to be considered in the managing and controlling actions, such as gammagraphy and well-logging. This study aims to identify and promote good practices to prevent inadvertent diversion of radioactive material, taking into account existing international recommendations and some lessons learned in national level. (author)

  6. Feasibility of performing neutrino experiments at an intense source of strangeness

    International Nuclear Information System (INIS)

    Carlini, R.D.; Stephenson, G.J. Jr.

    1983-01-01

    Several very important low energy neutrino experiments have been identified and discussed by Kayser and Rosen in these proceedings. We address the possibility of performing some of these experiments in the environment of a kaon factory. To carry out specific analyses, we draw upon the design of existing BNL detectors, the design of experiments that are proposed for an 800 MeV proton driven facility at Los Alamos, and the use of the code NUBEAM developed at CERN. Since in most cases we have not optimized, this is a conservative estimate. We find that many of the desired experiments can be performed with facilities now under discussion

  7. Progress in the Development of a High Power Helicon Plasma Source for the Materials Plasma Exposure Experiment

    Energy Technology Data Exchange (ETDEWEB)

    Goulding, Richard Howell [ORNL; Caughman, John B. [ORNL; Rapp, Juergen [ORNL; Biewer, Theodore M. [ORNL; Bigelow, Tim S. [ORNL; Campbell, Ian H. [ORNL; Caneses Marin, Juan F. [ORNL; Donovan, David C. [ORNL; Kafle, Nischal [ORNL; Martin, Elijah H. [ORNL; Ray, Holly B. [ORNL; Shaw, Guinevere C. [ORNL; Showers, Melissa A. [ORNL

    2017-09-01

    Proto-MPEX is a linear plasma device being used to study a novel RF source concept for the planned Material Plasma Exposure eXperiment (MPEX), which will address plasma-materials interaction (PMI) for nuclear fusion reactors. Plasmas are produced using a large diameter helicon source operating at a frequency of 13.56 MHz at power levels up to 120 kW. In recent experiments the helicon source has produced deuterium plasmas with densities up to ~6 × 1019 m–3 measured at a location 2 m downstream from the antenna and 0.4 m from the target. Previous plasma production experiments on Proto-MPEX have generated lower density plasmas with hollow electron temperature profiles and target power deposition peaked far off axis. The latest experiments have produced flat Te profiles with a large portion of the power deposited on the target near the axis. This and other evidence points to the excitation of a helicon mode in this case.

  8. Evaluation of the inorganic selenium biotransformation in selenium-enriched yogurt by HPLC-ICP-MS.

    Science.gov (United States)

    Alzate, Adriana; Cañas, Benito; Pérez-Munguía, Sandra; Hernández-Mendoza, Hector; Pérez-Conde, Concepción; Gutiérrez, Ana Maria; Cámara, Carmen

    2007-11-28

    Selenium is an essential element in the human diet. Interestingly, there has been an increased consumption of dietary supplements containing this element in the form of either inorganic or organic compounds. The effect of using selenium as a dietary supplement in yogurt has been evaluated. For this purpose, different concentrations of inorganic Se (ranging from 0.2 to 5000 microg g(-1)) have been added to milk before the fermentation process. Biotransformation of inorganic Se into organic species has been carefully evaluated by ion-exchange, reversed-phase, or size-exclusion chromatography, coupled to inductively coupled plasma mass spectrometry (ICP-MS). Yogurt fermentation in the presence of up to 2 microg g(-1) of Se(IV) produces a complete incorporation of this element into proteins as has been demonstrated applying a dialysis procedure. Analysis by SEC-ICP-MS showed that most of them have a molecular mass in the range of 30-70 kDa. Species determination after enzymatic hydrolysis has allowed the identification of Se-cystine using two different chromatographic systems. The biotransformation process that takes place during yogurt fermentation is very attractive because yogurt can act as a source of selenium supplementation.

  9. Localization of short-range acoustic and seismic wideband sources: Algorithms and experiments

    Science.gov (United States)

    Stafsudd, J. Z.; Asgari, S.; Hudson, R.; Yao, K.; Taciroglu, E.

    2008-04-01

    We consider the determination of the location (source localization) of a disturbance source which emits acoustic and/or seismic signals. We devise an enhanced approximate maximum-likelihood (AML) algorithm to process data collected at acoustic sensors (microphones) belonging to an array of, non-collocated but otherwise identical, sensors. The approximate maximum-likelihood algorithm exploits the time-delay-of-arrival of acoustic signals at different sensors, and yields the source location. For processing the seismic signals, we investigate two distinct algorithms, both of which process data collected at a single measurement station comprising a triaxial accelerometer, to determine direction-of-arrival. The direction-of-arrivals determined at each sensor station are then combined using a weighted least-squares approach for source localization. The first of the direction-of-arrival estimation algorithms is based on the spectral decomposition of the covariance matrix, while the second is based on surface wave analysis. Both of the seismic source localization algorithms have their roots in seismology; and covariance matrix analysis had been successfully employed in applications where the source and the sensors (array) are typically separated by planetary distances (i.e., hundreds to thousands of kilometers). Here, we focus on very-short distances (e.g., less than one hundred meters) instead, with an outlook to applications in multi-modal surveillance, including target detection, tracking, and zone intrusion. We demonstrate the utility of the aforementioned algorithms through a series of open-field tests wherein we successfully localize wideband acoustic and/or seismic sources. We also investigate a basic strategy for fusion of results yielded by acoustic and seismic arrays.

  10. High temperature liquid chromatography hyphenated with ESI-MS and ICP-MS detection for the structural characterization and quantification of halogen containing drug metabolites

    International Nuclear Information System (INIS)

    Vlieger, Jon S.B. de; Giezen, Mark J.N.; Falck, David; Tump, Cornelis; Heuveln, Fred van; Giera, Martin; Kool, Jeroen; Lingeman, Henk; Wieling, Jaap; Honing, Maarten; Irth, Hubertus; Niessen, Wilfried M.A.

    2011-01-01

    Highlights: → Hyphenation of high temperature liquid chromatography to ICP-MS and ESI-MS. → Structural characterization of kinase inhibitor metabolites with high resolution MS n experiments. → Quantification of drug metabolites with ICP-MS based on Iodine detection. → Significant changes in ESI-MS response after small structural changes. - Abstract: In this paper we describe the hyphenation of high temperature liquid chromatography with ICP-MS and ESI-MS for the characterization of halogen containing drug metabolites. The use of temperature gradients up to 200 deg. C enabled the separation of metabolites with low organic modifier content. This specific property allowed the use of detection methods that suffer from (significant) changes in analyte response factors as a function of the organic modifier content such as ICP-MS. Metabolites of two kinase inhibitors (SB-203580-Iodo and MAPK inhibitor VIII) produced by bacterial cytochrome P450 BM3 mutants and human liver microsomes were identified based on high resolution MS n data. Quantification was done using their normalized and elemental specific response in the ICP-MS. The importance of these kinds of quantification strategies is stressed by the observation that the difference of the position of one oxygen atom in a structure can greatly affect its response in ESI-MS and UV detection.

  11. Integrated care pathways for airway diseases (AIRWAYS-ICPs)

    DEFF Research Database (Denmark)

    Bousquet, J; Addis, A; Adcock, I

    2014-01-01

    The objective of Integrated Care Pathways for Airway Diseases (AIRWAYS-ICPs) is to launch a collaboration to develop multi-sectoral care pathways for chronic respiratory diseases in European countries and regions. AIRWAYS-ICPs has strategic relevance to the European Union Health Strategy...... and will add value to existing public health knowledge by: 1) proposing a common framework of care pathways for chronic respiratory diseases, which will facilitate comparability and trans-national initiatives; 2) informing cost-effective policy development, strengthening in particular those on smoking...... and environmental exposure; 3) aiding risk stratification in chronic disease patients, using a common strategy; 4) having a significant impact on the health of citizens in the short term (reduction of morbidity, improvement of education in children and of work in adults) and in the long-term (healthy ageing); 5...

  12. Imaging of Selenium by Laser Ablation Inductively Coupled Plasma Mass Spectrometry (LA-ICP-MS) in 2-D Electrophoresis Gels and Biological Tissues.

    Science.gov (United States)

    Cruz, Elisa Castañeda Santa; Susanne Becker, J; Sabine Becker, J; Sussulini, Alessandra

    2018-01-01

    Selenium and selenoproteins are important components of living organisms that play a role in different biological processes. Laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS) is a powerful analytical technique that has been employed to obtain distribution maps of selenium in biological tissues in a direct manner, as well as in selenoproteins, previously separated by their molecular masses and isoelectric points using two-dimensional polyacrylamide gel electrophoresis (2-D PAGE). In this chapter, we present the protocols to perform LA-ICP-MS imaging experiments, allowing the distribution visualization and determination of selenium and/or selenoproteins in biological systems.

  13. Fundamental studies of interferences in ICP-MS

    Energy Technology Data Exchange (ETDEWEB)

    Rowley, L.K

    2000-11-01

    Methods of temperature measurement by mass spectrometry have been critically reviewed. It was concluded that the most appropriate method depended critically on the availability of fundamental data, hence a database of fundamental spectroscopic constants, for diatomic ions which cause interferences in ICP-MS, was compiled. The equilibration temperature, calculated using the different methods and using various diatomic ions as the thermometric probes, was between c.a. 400 - 10,000 K in the central channel, and between c.a. 600 - 16,000 K when the plasma was moved 1.8 mm off-centre. The wide range in temperature reflected the range of temperature measurement methods and uncertainty in the fundamental data. Optical studies using a fibre optic connected to a monochromator were performed in order to investigate the presence of interferences both in the plasma and the interface region of the ICP-MS, and the influence of a shielded torch on these interferences. It was possible to determine the presence of some species in the plasma, such as the strongly bound metal oxides, however, no species other than OH were detected in the interface region of the ICP-MS. The OH rotational temperature within the interface region of the ICP-MS was calculated to be between 2,000 - 4,000 K. The effect of sampling depth, operating power, radial position and solvent loading, with and without the shielded torch, on the dissociation temperature of a variety of polyatomic interferences was investigated. These calculated temperatures were then used to elucidate the site of formation for different polyatomic interferences. Results confirmed that strongly bound ions such as MO{sup +} were formed in the plasma, whereas weakly bound ions such as ArO{sup +} were formed in the interface region due to gross deviation of the calculated temperatures from those expected for a system in thermal equilibrium. (author)

  14. Experiments and simulations for the dynamics of cesium in negative hydrogen ion sources for ITER N-NBI

    Energy Technology Data Exchange (ETDEWEB)

    Gutser, Raphael

    2010-07-21

    The injection of fast neutral particles (NBI) into a fusion plasma is an important method for plasma heating and current drive. A source for negative deuterium ions delivering an 1 MeV beam that is accelerated to a specific energy and neutralized by a gas target is required for the ITER-NBI. Cesium seeding is required to extract high negative ion current densities from these sources. The optimization of the cesium homogeneity and control are major objectives to achieve the source requirements imposed by ITER. Within the scope of this thesis, the Monte Carlo based numerical transport simulation CsFlow3D was developed, which is the first computer model that is capable of simulating the flux and the accumulation of cesium on the surfaces of negative-ion sources. Basic studies that support the code development were performed at a dedicated experiment at the University of Augsburg. Input parameters of the ad- and desorption of cesium at ion source relevant conditions were taken from systematic measurements with a quartz micro balance, while the injection rate of the cesium oven at the ion source was determined by surface ionization detection. This experimental setup was used for further investigations of the work function of cesium-coated samples during plasma exposure. (orig.)

  15. Proceedings of the meeting of 'the MR light source experiments', held on March 6 and 7, 1996

    International Nuclear Information System (INIS)

    Ohsumi, Kazumasa; Fukuma, Hitoshi; Kamada, Susumu

    1996-10-01

    The program using TRISTAN main ring (MR) at High Energy Physics Laboratory as a high luminescent radiation source was finished with predetermined results on December 27, 1995. Reconstruction of the MR to the high luminescent radiation source and some application research using it were a joint research of the MR super high luminescent radiation program promoting team and TRISTAN accelerator research department. Development of radiation science is development of luminescence, and can be called to be a scientific and technical system aiming at 'the luminescence on the radiation luminescence in the world even for a moment. By confirming performances of the MR for accelerator and obtaining many results after application experiments, an application research on the 3rd generation light source for high luminescence radiation could be started faster. Furthermore, it seems to contribute on a standpoint of future program to develop a superhigh luminescent light source (coherent X ray source) called the 4th generation radiation source. In this book, the following 21 reports were described; 1) Review on Mr radiation application project, 2) Design of accelerator, 3) Operation and performance of the accelerator, 4) Measurement of dynamic apparture in MR radiation lattice, Emittance measurement using radiation visible portion, and so forth. (G.K.)

  16. Experiments and simulations for the dynamics of cesium in negative hydrogen ion sources for ITER N-NBI

    International Nuclear Information System (INIS)

    Gutser, Raphael

    2010-01-01

    The injection of fast neutral particles (NBI) into a fusion plasma is an important method for plasma heating and current drive. A source for negative deuterium ions delivering an 1 MeV beam that is accelerated to a specific energy and neutralized by a gas target is required for the ITER-NBI. Cesium seeding is required to extract high negative ion current densities from these sources. The optimization of the cesium homogeneity and control are major objectives to achieve the source requirements imposed by ITER. Within the scope of this thesis, the Monte Carlo based numerical transport simulation CsFlow3D was developed, which is the first computer model that is capable of simulating the flux and the accumulation of cesium on the surfaces of negative-ion sources. Basic studies that support the code development were performed at a dedicated experiment at the University of Augsburg. Input parameters of the ad- and desorption of cesium at ion source relevant conditions were taken from systematic measurements with a quartz micro balance, while the injection rate of the cesium oven at the ion source was determined by surface ionization detection. This experimental setup was used for further investigations of the work function of cesium-coated samples during plasma exposure. (orig.)

  17. Time-Dependent Moment Tensors of the First Four Source Physics Experiments (SPE) Explosions

    Science.gov (United States)

    Yang, X.

    2015-12-01

    We use mainly vertical-component geophone data within 2 km from the epicenter to invert for time-dependent moment tensors of the first four SPE explosions: SPE-1, SPE-2, SPE-3 and SPE-4Prime. We employ a one-dimensional (1D) velocity model developed from P- and Rg-wave travel times for Green's function calculations. The attenuation structure of the model is developed from P- and Rg-wave amplitudes. We select data for the inversion based on the criterion that they show consistent travel times and amplitude behavior as those predicted by the 1D model. Due to limited azimuthal coverage of the sources and the mostly vertical-component-only nature of the dataset, only long-period, diagonal components of the moment tensors are well constrained. Nevertheless, the moment tensors, particularly their isotropic components, provide reasonable estimates of the long-period source amplitudes as well as estimates of corner frequencies, albeit with larger uncertainties. The estimated corner frequencies, however, are consistent with estimates from ratios of seismogram spectra from different explosions. These long-period source amplitudes and corner frequencies cannot be fit by classical P-wave explosion source models. The results motivate the development of new P-wave source models suitable for these chemical explosions. To that end, we fit inverted moment-tensor spectra by modifying the classical explosion model using regressions of estimated source parameters. Although the number of data points used in the regression is small, the approach suggests a way for the new-model development when more data are collected.

  18. Coupled Hydrodynamic and Wave Propagation Modeling for the Source Physics Experiment: Study of Rg Wave Sources for SPE and DAG series.

    Science.gov (United States)

    Larmat, C. S.; Delorey, A.; Rougier, E.; Knight, E. E.; Steedman, D. W.; Bradley, C. R.

    2017-12-01

    This presentation reports numerical modeling efforts to improve knowledge of the processes that affect seismic wave generation and propagation from underground explosions, with a focus on Rg waves. The numerical model is based on the coupling of hydrodynamic simulation codes (Abaqus, CASH and HOSS), with a 3D full waveform propagation code, SPECFEM3D. Validation datasets are provided by the Source Physics Experiment (SPE) which is a series of highly instrumented chemical explosions at the Nevada National Security Site with yields from 100kg to 5000kg. A first series of explosions in a granite emplacement has just been completed and a second series in alluvium emplacement is planned for 2018. The long-term goal of this research is to review and improve current existing seismic sources models (e.g. Mueller & Murphy, 1971; Denny & Johnson, 1991) by providing first principles calculations provided by the coupled codes capability. The hydrodynamic codes, Abaqus, CASH and HOSS, model the shocked, hydrodynamic region via equations of state for the explosive, borehole stemming and jointed/weathered granite. A new material model for unconsolidated alluvium materials has been developed and validated with past nuclear explosions, including the 10 kT 1965 Merlin event (Perret, 1971) ; Perret and Bass, 1975). We use the efficient Spectral Element Method code, SPECFEM3D (e.g. Komatitsch, 1998; 2002), and Geologic Framework Models to model the evolution of wavefield as it propagates across 3D complex structures. The coupling interface is a series of grid points of the SEM mesh situated at the edge of the hydrodynamic code domain. We will present validation tests and waveforms modeled for several SPE tests which provide evidence that the damage processes happening in the vicinity of the explosions create secondary seismic sources. These sources interfere with the original explosion moment and reduces the apparent seismic moment at the origin of Rg waves up to 20%.

  19. Rural population and renewable energy sources: Experiences of the Republic of Serbia

    Directory of Open Access Journals (Sweden)

    Pucar Mila

    2006-01-01

    Full Text Available During the last decade of the twentieth century the use of green (renewable energy has become the imperative not only in developed countries worldwide, but also in poorer countries like Asia and Africa. The change from traditional to renewable energy sources carries valuable improvements in environmental protection and economic efficacy. This paper through individual examples, explores the possibility of replacing traditional with renewable energy sources such as solar, wind, geothermal, energy of small hydroelectric power plants, etc. worldwide and in rural Serbian communities.

  20. Methods of computer experiment in gamma-radiation technologies using new radiation sources

    CERN Document Server

    Bratchenko, M I; Rozhkov, V V

    2001-01-01

    Presented id the methodology of computer modeling application for physical substantiation of new irradiation technologies and irradiators design work flow. Modeling tasks for irradiation technologies are structured along with computerized methods of their solution and appropriate types of software. Comparative analysis of available packages for Monte-Carlo modeling of electromagnetic processes in media is done concerning their application to irradiation technologies problems. The results of codes approbation and preliminary data on gamma-radiation absorbed dose distributions for nuclides of conventional sources and prospective Europium-based gamma-sources are presented.

  1. Environmental 222Rn as a background source in the solar neutrino experiment GALLEX

    International Nuclear Information System (INIS)

    Wojcik, M.

    1996-01-01

    The radiochemical neutrino experiment GALLEX is described. Its aim is to measure the flux of low energy solar neutrinos. In this experiment it is essential to suppress strongly the background of environmental origin, like charged cosmic rays, neutrons and gamma rays. In low-level radioactivity measurements performed in deep underground laboratory where flux of charged comic rays is strongly reduced, radon (Rn) exhaled from rock or concrete walls forms a most important strong, time-dependent background component. In this work the impact of Rn on the GALLEX experiment has been discussed and attempts to recognize and minimize its influence on the counter background were described. 63 refs, 22 figs, 11 tabs

  2. Environmental {sup 222}Rn as a background source in the solar neutrino experiment GALLEX

    Energy Technology Data Exchange (ETDEWEB)

    Wojcik, M. [Uniwersytet Jagiellonski, Cracow (Poland). Inst. Fizyki; BOREXINO

    1996-12-31

    The radiochemical neutrino experiment GALLEX is described. Its aim is to measure the flux of low energy solar neutrinos. In this experiment it is essential to suppress strongly the background of environmental origin, like charged cosmic rays, neutrons and gamma rays. In low-level radioactivity measurements performed in deep underground laboratory where flux of charged comic rays is strongly reduced, radon (Rn) exhaled from rock or concrete walls forms a most important strong, time-dependent background component. In this work the impact of Rn on the GALLEX experiment has been discussed and attempts to recognize and minimize its influence on the counter background were described. 63 refs, 22 figs, 11 tabs.

  3. Environmental {sup 222}Rn as a background source in the solar neutrino experiment GALLEX

    Energy Technology Data Exchange (ETDEWEB)

    Wojcik, M [Uniwersytet Jagiellonski, Cracow (Poland). Inst. Fizyki; BOREXINO,

    1997-12-31

    The radiochemical neutrino experiment GALLEX is described. Its aim is to measure the flux of low energy solar neutrinos. In this experiment it is essential to suppress strongly the background of environmental origin, like charged cosmic rays, neutrons and gamma rays. In low-level radioactivity measurements performed in deep underground laboratory where flux of charged comic rays is strongly reduced, radon (Rn) exhaled from rock or concrete walls forms a most important strong, time-dependent background component. In this work the impact of Rn on the GALLEX experiment has been discussed and attempts to recognize and minimize its influence on the counter background were described. 63 refs, 22 figs, 11 tabs.

  4. Possible interferences of mercury sulfur compounds with ethylated and methylated mercury species using HPLC-ICP-MS

    International Nuclear Information System (INIS)

    Wilken, R.D.; Nitschke, F.; Falter, R.

    2003-01-01

    The HPLC-ICP-MS coupling technique is able to separate and detect methyl, ethyl and inorganic mercury isotopes specifically. An identification of ethyl mercury(+) is not possible when the widely used sodium tetraethylborate derivatisation method in combination with GC-AFS/AAS or ICP-MS techniques is performed because it contains ethyl groups. An unidentified compound with the same retention time as ethyl mercury was found in the HPLC chromatograms of industrial sewage samples and humic-rich soils of microcosm experiments after applying water vapour distillation. We also observed such unidentified peaks in samples of heavily contaminated sites in Eastern Germany, separated by HPLC fractionation only. In the experiments described, different mercury sulfur adducts were synthesised and tested for their retention times in the HPLC-ICP-MS system. It was found that the compound CH 3 -S-Hg + showed the same retention time as the ethyl mercury standard. It is therefore possible that ethyl mercury detected in chromatography by comparison of the retention time could also be due to an adduct of a sulfur compound and a mercury species. CH 3 -S-Hg + should be tested in other chromatographic mercury speciation methods for this effect. This work can also be regarded as a contribution to the discussion of artificially occurring methyl mercury in sediments during sample preparation. (orig.)

  5. Simultaneous usage of pinhole and penumbral apertures for imaging small scale neutron sources from inertial confinement fusion experiments.

    Science.gov (United States)

    Guler, N; Volegov, P; Danly, C R; Grim, G P; Merrill, F E; Wilde, C H

    2012-10-01

    Inertial confinement fusion experiments at the National Ignition Facility are designed to understand the basic principles of creating self-sustaining fusion reactions by laser driven compression of deuterium-tritium (DT) filled cryogenic plastic capsules. The neutron imaging diagnostic provides information on the distribution of the central fusion reaction region and the surrounding DT fuel by observing neutron images in two different energy bands for primary (13-17 MeV) and down-scattered (6-12 MeV) neutrons. From this, the final shape and size of the compressed capsule can be estimated and the symmetry of the compression can be inferred. These experiments provide small sources with high yield neutron flux. An aperture design that includes an array of pinholes and penumbral apertures has provided the opportunity to image the same source with two different techniques. This allows for an evaluation of these different aperture designs and reconstruction algorithms.

  6. Operational Experience with Radioactive Source Calibration of the CMS Hadron Endcap Calorimeter Wedges with Phase I Upgrade Electronics

    CERN Document Server

    Bilki, Burak

    2017-01-01

    The Phase I Upgrade of the CMS Hadron Endcap Calorimeters consists of new photodetectors and front-end electronics. The upgrade will allow the elimination of the high amplitude noise and drifting response of the Hybrid Photo-Diodes, at the same time enabling the mitigation of the radiation damage of the scintillators and the wavelength shifting fibers with a larger spectral acceptance of the Silicon Photomultipliers. The upgrade will also allow increasing the longitudinal segmentation of the readout to be beneficial for pile-up mitigation and recalibration due to depth-dependent radiation damage. As a realistic operational exercise, the responses of the Hadron Endcap Calorimeter wedges were calibrated with a 60Co radioactive source both with current and upgrade electronics. The exercise provided significant experience towards the full upgrade during the Year End Technical Stop 2017-2018. Here we describe the instrumentation details and the operational experiences related to the sourcing exercise.

  7. Rotating dust ring in an RF discharge coupled with a dc-magnetron sputter source. Experiment and simulation

    International Nuclear Information System (INIS)

    Matyash, K; Froehlich, M; Kersten, H; Thieme, G; Schneider, R; Hannemann, M; Hippler, R

    2004-01-01

    During an experiment involving coating of dust grains trapped in an RF discharge using a sputtering dc-magnetron source, a rotating dust ring was observed and investigated. After the magnetron was switched on, the dust cloud levitating above the RF electrode formed a ring rotating as a rigid body. Langmuir probe diagnostics were used for the measurement of plasma density and potential. It was discovered that the coupling of the dc-magnetron source to the RF discharge causes steep radial gradients in electron density and plasma potential. The rotation of the dust ring is attributed to the azimuthal component of the ion drag force, which appears due to the azimuthal drift of the ions caused by crossed radial electric and axial magnetic fields. In order to get more insight into the mechanism of dust ring rotation, a Particle-in-Cell simulation of a rotating dust cloud was performed. The results of the experiment and simulation are presented and discussed

  8. Rotating dust ring in an RF discharge coupled with a dc-magnetron sputter source. Experiment and simulation

    Energy Technology Data Exchange (ETDEWEB)

    Matyash, K [Institut fuer Niedertemperaturplasmaphysik Greifswald, Fr.-L.-Jahn-Strasse 19, 17489 Greifswald (Germany); Froehlich, M [Institut fuer Physik, Ernst-Moritz-Arndt-Universitaet Greifswald, Domstrasse 10a, 17487 Greifswald (Germany); Kersten, H [Institut fuer Niedertemperaturplasmaphysik Greifswald, Fr.-L.-Jahn-Strasse 19, 17489 Greifswald (Germany); Thieme, G [Institut fuer Physik, Ernst-Moritz-Arndt-Universitaet Greifswald, Domstrasse 10a, 17487 Greifswald (Germany); Schneider, R [Max-Planck-Institut fuer Plasmaphysik, Teilinstitut Greifswald, Wendelsteinstrasse 1, 17489 Greifswald (Germany); Hannemann, M [Institut fuer Niedertemperaturplasmaphysik Greifswald, Fr.-L.-Jahn-Strasse 19, 17489 Greifswald (Germany); Hippler, R [Institut fuer Physik, Ernst-Moritz-Arndt-Universitaet Greifswald, Domstrasse 10a, 17487 Greifswald (Germany)

    2004-10-07

    During an experiment involving coating of dust grains trapped in an RF discharge using a sputtering dc-magnetron source, a rotating dust ring was observed and investigated. After the magnetron was switched on, the dust cloud levitating above the RF electrode formed a ring rotating as a rigid body. Langmuir probe diagnostics were used for the measurement of plasma density and potential. It was discovered that the coupling of the dc-magnetron source to the RF discharge causes steep radial gradients in electron density and plasma potential. The rotation of the dust ring is attributed to the azimuthal component of the ion drag force, which appears due to the azimuthal drift of the ions caused by crossed radial electric and axial magnetic fields. In order to get more insight into the mechanism of dust ring rotation, a Particle-in-Cell simulation of a rotating dust cloud was performed. The results of the experiment and simulation are presented and discussed.

  9. Validation Study for an Atmospheric Dispersion Model, Using Effective Source Heights Determined from Wind Tunnel Experiments in Nuclear Safety Analysis

    Directory of Open Access Journals (Sweden)

    Masamichi Oura

    2018-03-01

    Full Text Available For more than fifty years, atmospheric dispersion predictions based on the joint use of a Gaussian plume model and wind tunnel experiments have been applied in both Japan and the U.K. for the evaluation of public radiation exposure in nuclear safety analysis. The effective source height used in the Gaussian model is determined from ground-level concentration data obtained by a wind tunnel experiment using a scaled terrain and site model. In the present paper, the concentrations calculated by this method are compared with data observed over complex terrain in the field, under a number of meteorological conditions. Good agreement was confirmed in near-neutral and unstable stabilities. However, it was found to be necessary to reduce the effective source height by 50% in order to achieve a conservative estimation of the field observations in a stable atmosphere.

  10. Deep penetration in pure sodium experiments using the HARMONIE source reactor

    International Nuclear Information System (INIS)

    Trapp, J.P.; Calamand, D.; Salvatores, M.

    1984-09-01

    The presente note is a documentation of the neutron propagation experiments in sodium, performed on HARMONIE. Details are given on the geometrical specifications, experimental results and calculation, one and two dimensional, results

  11. Data Release Report for Source Physics Experiments 2 and 3 (SPE-2 and SPE-3) Nevada National Security Site

    Energy Technology Data Exchange (ETDEWEB)

    Townsend, Margaret [National Security Technologies, LLC. (NSTec), Las Vegas, NV (United States); Obi, Curtis [National Security Technologies, LLC. (NSTec), Las Vegas, NV (United States)

    2015-04-30

    The second Source Physics Experiment shot (SPE-2) was conducted in Nevada on October 25, 2011, at 1900:00.011623 Greenwich Mean Time (GMT). The explosive source was 997 kilograms (kg) trinitrotoluene (TNT) equivalent of sensitized heavy ammonium fuel oil (SHANFO) detonated at a depth of 45.7 meters (m). The third Source Physics Experiment shot (SPE-3) was conducted in Nevada on July 24, 2012, at 1800:00.44835 GMT. The explosive source was 905 kg TNT equivalent of SHANFO detonated at a depth of 45.8 m. Both shots were recorded by an extensive set of instrumentation that includes sensors both at near-field (less than 100 m) and far-field (100 m or greater) distances. The near-field instruments consisted of three-component accelerometers deployed in boreholes at 15, 46, and 55 m depths around the shot and a set of single-component vertical accelerometers on the surface. The far-field network was composed of a variety of seismic and acoustic sensors, including short-period geophones, broadband seismometers, three-component accelerometers, and rotational seismometers at distances of 100 m to 25 kilometers. This report coincides with the release of these data for analysts and organizations that are not participants in this program. This report describes the second and third Source Physics Experiment shots and the various types of near-field and farfield data that are available.This revised document includes reports on baseline shift corrections for the SPE-2 and SPE-3 shots that were missing from the original January 2015 version.

  12. Design of interferometer system for Keda Torus eXperiment using terahertz solid-state diode sources

    International Nuclear Information System (INIS)

    Xie, Jinlin; Wang, Haibo; Li, Hong; Lan, Tao; Liu, Adi; Liu, Wandong; Yu, Changxuan; Ding, Weixing

    2014-01-01

    A solid-state source based terahertz (THz) interferometer diagnostic system has been designed and characterized for the Keda Torus eXperiment (KTX). The THz interferometer utilizes the planar diodes based frequency multiplier (X48) to provide the probing beam at fixed frequency 0.650 THz, and local oscillator is provided by an independent solid-state diode source with tunable frequency (0.650 THz +/− 10 MHz). Both solid-state sources have approximately 1 mW power. The planar-diode mixers optimized for high sensitivity, ∼750 mV/mW, are used in the heterodyne detection system, which permits multichannel interferometer on KTX with a low phase noise. A sensitivity of e l> min = 4.5 × 10 16 m −2 and a temporal resolution of 0.2 μs have been achieved during the initial bench test

  13. Performance of a high-precision calorimeter for the measurement of the antineutrino-source strength in the SOX experiment

    Energy Technology Data Exchange (ETDEWEB)

    Altenmueller, Konrad [Technische Universitaet Muenchen (Germany); Collaboration: BOREXINO-Collaboration

    2016-07-01

    A calorimeter was developed to measure the thermal power and thus the antineutrino-generation rate of a {sup 144}Ce - {sup 144}Pr antineutrino-source with < 1% overall accuracy for the SOX experiment. SOX is searching for neutrino oscillations at short baselines with the Borexino detector to investigate the existence of eV-scale sterile neutrinos. The calorimeter design is based on a copper heat exchanger with integrated water lines for the heat extraction, mounted around the source. A high precision measurement is possible thanks to an elaborate thermal insulation. In this talk, the design of the calorimeter is reviewed and results of calibration measurements are presented. The thermal insulation of the system was examined and heat losses were quantified. The methods to reconstruct the source power and the decay rate from measurements are described.

  14. Overview of multi-element monolithic germanium detectors for XAFS experiments at diamond light source

    International Nuclear Information System (INIS)

    Chatterji, S.; Dennis, G. J.; Dent, A.; Diaz-Moreno, S.; Cibin, G.; Tartoni, N.; Helsby, W. I.

    2016-01-01

    An overview of multi-element monolithic germanium detectors being used at the X-ray absorption spectroscopy (XAS) beam lines at Diamond Light Source (DLS) is being reported. The hardware details and a summary of the performance of these detectors have also been provided. Recent updates about various ongoing projects being worked on to improve the performance of these detectors are summarized.

  15. Short-term power sources for tokamaks and other physical experiments

    Czech Academy of Sciences Publication Activity Database

    Zajac, Jaromír; Žáček, František; Brettschneider, Zbyněk; Lejsek, V.

    2007-01-01

    Roč. 82, č. 4 (2007), s. 369-379 ISSN 0920-3796 Institutional research plan: CEZ:AV0Z20430508 Keywords : Tokamak * Impulse power sources * Energy accumulation Subject RIV: JA - Electronics ; Optoelectronics, Electrical Engineering Impact factor: 1.058, year: 2007 http://www.sciencedirect.com/science/journal/09203796

  16. Overview of multi-element monolithic germanium detectors for XAFS experiments at diamond light source

    Energy Technology Data Exchange (ETDEWEB)

    Chatterji, S.; Dennis, G. J.; Dent, A.; Diaz-Moreno, S.; Cibin, G.; Tartoni, N. [Diamond Light Source Ltd, Oxfordshire (United Kingdom); Helsby, W. I. [STFC Daresbury Laboratory, Warrington (United Kingdom)

    2016-07-27

    An overview of multi-element monolithic germanium detectors being used at the X-ray absorption spectroscopy (XAS) beam lines at Diamond Light Source (DLS) is being reported. The hardware details and a summary of the performance of these detectors have also been provided. Recent updates about various ongoing projects being worked on to improve the performance of these detectors are summarized.

  17. Financial Regulations and the Diversification of Funding Sources in Higher Education Institutions: Selected European Experiences

    Science.gov (United States)

    Stachowiak-Kudla, Monika; Kudla, Janusz

    2017-01-01

    The paper addresses the problem of the financial regulations' impact on the share of private financing in higher education institutions (HEIs). The authors postulate the trade-off between the size and stability of public financing and the regulations fostering stability of HEIs' funds. If the public sources are insufficient then the regulations…

  18. Source apportionment of fine organic aerosol in Mexico City during the MILAGRO experiment 2006

    Directory of Open Access Journals (Sweden)

    E. A. Stone

    2008-03-01

    Full Text Available Organic carbon (OC comprises a large fraction of fine particulate matter (PM2.5 in Mexico City. Daily and select 12-h PM2.5 samples were collected in urban and peripheral sites in Mexico City from 17–30 March 2006. Samples were analyzed for OC and elemental carbon (EC using thermal-optical filter-based methods. Real-time water-soluble organic carbon (WSOC was collected at the peripheral site. Organic compounds, particularly molecular markers, were quantified by soxhlet extraction with methanol and dichloromethane, derivitization, and gas chromatography with mass spectrometric detection (GCMS. A chemical mass balance model (CMB based on molecular marker species was used to determine the relative contribution of major sources to ambient OC. Motor vehicles, including diesel and gasoline, consistently accounted for 49% of OC in the urban area and 32% on the periphery. The daily contribution of biomass burning to OC was highly variable, and ranged from 5–26% at the urban site and 7–39% at the peripheral site. The remaining OC unapportioned to primary sources showed a strong correlation with WSOC and was considered to be secondary in nature. Comparison of temporally resolved OC showed that contributions from primary aerosol sources during daylight hours were not significantly different from nighttime. This study provides quantitative understanding of the important sources of OC during the MILAGRO 2006 field campaign.

  19. Mitigation of Cognitive Bias with a Serious Game: Two Experiments Testing Feedback Timing and Source

    Science.gov (United States)

    Dunbar, Norah E.; Jensen, Matthew L.; Miller, Claude H.; Bessarabova, Elena; Lee, Yu-Hao; Wilson, Scott N.; Elizondo, Javier; Adame, Bradley J.; Valacich, Joseph; Straub, Sara; Burgoon, Judee K.; Lane, Brianna; Piercy, Cameron W.; Wilson, David; King, Shawn; Vincent, Cindy; Schuetzler, Ryan M.

    2017-01-01

    One of the benefits of using digital games for education is that games can provide feedback for learners to assess their situation and correct their mistakes. We conducted two studies to examine the effectiveness of different feedback design (timing, duration, repeats, and feedback source) in a serious game designed to teach learners about…

  20. Regulatory control of natural ionizing sources in Lithuania: Experience based on indoor radon monitoring

    International Nuclear Information System (INIS)

    Mastauskas, A.; Morkunas, G.

    1997-01-01

    The situation in legislation of protection against risks from natural sources of ionizing radiation in Lithuania is described. The requirements of new standards came into conflict with the real situation which has not been evaluated before implementation of these standards. On the basis of recommendations of ICRP Publication 60 and results of indoor radon survey new action levels are being established. (author)

  1. Mechanistic formulation of a lineal-quadratic-linear (LQL) model: Split-dose experiments and exponentially decaying sources

    International Nuclear Information System (INIS)

    Guerrero, Mariana; Carlone, Marco

    2010-01-01

    Purpose: In recent years, several models were proposed that modify the standard linear-quadratic (LQ) model to make the predicted survival curve linear at high doses. Most of these models are purely phenomenological and can only be applied in the particular case of acute doses per fraction. The authors consider a mechanistic formulation of a linear-quadratic-linear (LQL) model in the case of split-dose experiments and exponentially decaying sources. This model provides a comprehensive description of radiation response for arbitrary dose rate and fractionation with only one additional parameter. Methods: The authors use a compartmental formulation of the LQL model from the literature. They analytically solve the model's differential equations for the case of a split-dose experiment and for an exponentially decaying source. They compare the solutions of the survival fraction with the standard LQ equations and with the lethal-potentially lethal (LPL) model. Results: In the case of the split-dose experiment, the LQL model predicts a recovery ratio as a function of dose per fraction that deviates from the square law of the standard LQ. The survival fraction as a function of time between fractions follows a similar exponential law as the LQ but adds a multiplicative factor to the LQ parameter β. The LQL solution for the split-dose experiment is very close to the LPL prediction. For the decaying source, the differences between the LQL and the LQ solutions are negligible when the half-life of the source is much larger than the characteristic repair time, which is the clinically relevant case. Conclusions: The compartmental formulation of the LQL model can be used for arbitrary dose rates and provides a comprehensive description of dose response. When the survival fraction for acute doses is linear for high dose, a deviation of the square law formula of the recovery ratio for split doses is also predicted.

  2. ICP-MS determination of boron: method optimization during preparation of graphite reference material for boron

    International Nuclear Information System (INIS)

    Granthali, S.K.; Shailaja, P.P.; Mainsha, V.; Venkatesh, K.; Kallola, K.S.; Sanjukta, A.K.

    2017-01-01

    Graphite finds widespread use in nuclear reactors as moderator, reflector, and fuel fabricating components because of its thermal stability and integrity. The manufacturing process consists of various mixing, moulding and baking operations followed by heat-treatment between 2500 °C and 3000 °C. The high temperature treatment is required to drive the amorphous carbon-to-graphite phase transformation. Since synthetic graphite is processed at high temperature, impurity concentrations in the precursor carbon get significantly reduced due to volatilization. However boron may might partly gets converted into boron carbide at high temperatures in the carbon environment of graphite and remains stable (B_4C: boiling point 3500 °C) in the matrix. Literature survey reveals the use of various methods for determination of boron. Previously we have developed a method for determination of boron in graphite electrodes using inductively coupled plasma mass spectrometry (ICP-MS). The method involves removal of graphite matrix by ignition of the sample at 800°C in presence of saturated barium hydroxide solution to prevent the loss of boron. Here we are reporting a modification in the method by using calcium carbonate in place of barium hydroxide and using beryllium (Be) as an internal standard, which resulted in a better precession. The method was validated by spike recovery experiments as well as using another technique viz. Inductively Coupled Plasma Optical Emission Spectrometry (ICP-OES). The modified method was applied in evaluation of boron concentration in the graphite reference material prepared

  3. Timeframe Dependent Fragment Ions Observed in In-Source Decay Experiments with β-Casein Using MALDI MS.

    Science.gov (United States)

    Sekiya, Sadanori; Nagoshi, Keishiro; Iwamoto, Shinichi; Tanaka, Koichi; Takayama, Mitsuo

    2015-09-01

    The fragment ions observed with time-of-flight (TOF) and quadrupole ion trap (QIT) TOF mass spectrometers (MS) combined with matrix-assisted laser desorption/ionization in-source decay (MALDI-ISD) experiments of phosphorylated analytes β-casein and its model peptide were compared from the standpoint of the residence timeframe of analyte and fragment ions in the MALDI ion source and QIT cell. The QIT-TOF MS gave fragment c-, z'-, z-ANL, y-, and b-ions, and further degraded fragments originating from the loss of neutrals such as H(2)O, NH(3), CH(2)O (from serine), C2H4O (from threonine), and H(3)PO(4), whereas the TOF MS merely showed MALDI source-generated fragment c-, z'-, z-ANL, y-, and w-ions. The fragment ions observed in the QIT-TOF MS could be explained by the injection of the source-generated ions into the QIT cell or a cooperative effect of a little internal energy deposition, a long residence timeframe (140 ms) in the QIT cell, and specific amino acid effects on low-energy CID, whereas the source-generated fragments (c-, z'-, z-ANL, y-, and w-ions) could be a result of prompt radical-initiated fragmentation of hydrogen-abundant radical ions [M + H + H](+) and [M + H - H](-) within the 53 ns timeframe, which corresponds to the delayed extraction time. The further degraded fragment b/y-ions produced in the QIT cell were confirmed by positive- and negative-ion low-energy CID experiments performed on the source-generated ions (c-, z'-, and y-ions). The loss of phosphoric acid (98 u) from analyte and fragment ions can be explained by a slow ergodic fragmentation independent of positive and negative charges.

  4. Timeframe Dependent Fragment Ions Observed in In-Source Decay Experiments with β-Casein Using MALDI MS

    Science.gov (United States)

    Sekiya, Sadanori; Nagoshi, Keishiro; Iwamoto, Shinichi; Tanaka, Koichi; Takayama, Mitsuo

    2015-09-01

    The fragment ions observed with time-of-flight (TOF) and quadrupole ion trap (QIT) TOF mass spectrometers (MS) combined with matrix-assisted laser desorption/ionization in-source decay (MALDI-ISD) experiments of phosphorylated analytes β-casein and its model peptide were compared from the standpoint of the residence timeframe of analyte and fragment ions in the MALDI ion source and QIT cell. The QIT-TOF MS gave fragment c-, z'-, z-ANL, y-, and b-ions, and further degraded fragments originating from the loss of neutrals such as H2O, NH3, CH2O (from serine), C2H4O (from threonine), and H3PO4, whereas the TOF MS merely showed MALDI source-generated fragment c-, z'-, z-ANL, y-, and w-ions. The fragment ions observed in the QIT-TOF MS could be explained by the injection of the source-generated ions into the QIT cell or a cooperative effect of a little internal energy deposition, a long residence timeframe (140 ms) in the QIT cell, and specific amino acid effects on low-energy CID, whereas the source-generated fragments (c-, z'-, z-ANL, y-, and w-ions) could be a result of prompt radical-initiated fragmentation of hydrogen-abundant radical ions [M + H + H]+ and [M + H - H]- within the 53 ns timeframe, which corresponds to the delayed extraction time. The further degraded fragment b/y-ions produced in the QIT cell were confirmed by positive- and negative-ion low-energy CID experiments performed on the source-generated ions (c-, z'-, and y-ions). The loss of phosphoric acid (98 u) from analyte and fragment ions can be explained by a slow ergodic fragmentation independent of positive and negative charges.

  5. Source of single photons and interferometry with one photon. From the Young's slit experiment to the delayed choice

    International Nuclear Information System (INIS)

    Jacques, V.

    2007-11-01

    This manuscript is divided in two independent parts. In the first part, we study the wave-particle duality for a single photon emitted by the triggered photoluminescence of a single NV color center in a diamond nano-crystal. We first present the realization of a single-photon interference experiment using a Fresnel's bi-prism, in a scheme equivalent to the standard Young's double-slit textbook experiment. We then discuss the complementarity between interference and which-path information in this two-path interferometer. We finally describe the experimental realization of Wheeler's delayed-choice Gedanken experiment, which is a fascinating and subtle illustration of wave-particle duality. The second part of the manuscript is devoted to the efficiency improvement of single-photon sources. We first describe the implementation of a new single-photon source based on the photoluminescence of a single nickel-related defect center in diamond. The photophysical properties of such defect make this single-photon source well adapted to open-air quantum cryptography. We finally demonstrate an original method that leads to an improvement of single-molecule photo stability at room temperature. (author)

  6. Battery-powered pulsed high density inductively coupled plasma source for pre-ionization in laboratory astrophysics experiments.

    Science.gov (United States)

    Chaplin, Vernon H; Bellan, Paul M

    2015-07-01

    An electrically floating radiofrequency (RF) pre-ionization plasma source has been developed to enable neutral gas breakdown at lower pressures and to access new experimental regimes in the Caltech laboratory astrophysics experiments. The source uses a customized 13.56 MHz class D RF power amplifier that is powered by AA batteries, allowing it to safely float at 3-6 kV with the electrodes of the high voltage pulsed power experiments. The amplifier, which is capable of 3 kW output power in pulsed (<1 ms) operation, couples electrical energy to the plasma through an antenna external to the 1.1 cm radius discharge tube. By comparing the predictions of a global equilibrium discharge model with the measured scalings of plasma density with RF power input and axial magnetic field strength, we demonstrate that inductive coupling (rather than capacitive coupling or wave damping) is the dominant energy transfer mechanism. Peak ion densities exceeding 5 × 10(19) m(-3) in argon gas at 30 mTorr have been achieved with and without a background field. Installation of the pre-ionization source on a magnetohydrodynamically driven jet experiment reduced the breakdown time and jitter and allowed for the creation of hotter, faster argon plasma jets than was previously possible.

  7. ICP-AES determination of trace elements in carbon steel

    International Nuclear Information System (INIS)

    Sengupta, Arijit; Rajeswari, B.; Kadam, R.M.; Babu, Y.; Godbole, S.V.

    2010-01-01

    Full text: Carbon steel, a combination of the elements iron and carbon, can be classified into four types as mild, medium, high and very high depending on the carbon content which varies from 0.05% to 2.1%. Carbon steel of different types finds application in medical devices, razor blades, cutlery and spring. In the nuclear industry, it is used in feeder pipes in the reactor. A strict quality control measure is required to monitor the trace elements, which have deleterious effects on the mechanical properties of the carbon steel. Thus, it becomes imperative to check the purity of carbon steel as a quality control measure before it is used in feeder pipes in the reactor. Several methods have been reported in literature for trace elemental determination in high purity iron. Some of these include neutron activation analysis, atomic absorption spectrometry and atomic emission spectrometry. Inductively coupled plasma atomic emission spectrometry (ICP-AES) is widely recognized as a sensitive technique for the determination of trace elements in various matrices, its major advantages being good accuracy and precision, high sensitivity, multi-element capability, large linear dynamic range and relative freedom from matrix effects. The present study mainly deals with the direct determination of trace elements in carbon steel using ICP-AES. An axially viewing ICP spectrometer having a polychromator with 35 fixed analytical channels and limited sequential facility to select any analytical line within 2.2 nm of a polychromator line was used in these studies. Iron, which forms one of the main constituents of carbon steel, has a multi electronic configuration with line rich emission spectrum and, therefore, tends to interfere in the determination of trace impurities in carbon steel matrix. Spectral interference in ICP-AES can be seriously detrimental to the accuracy and reliability of trace element determinations, particularly when they are performed in the presence of high

  8. Separation techniques for the clean-up of radioactive mixed waste for ICP-AES/ICP-MS analysis

    International Nuclear Information System (INIS)

    Swafford, A.M.; Keller, J.M.

    1993-01-01

    Two separation techniques were investigated for the clean-up of typical radioactive mixed waste samples requiring elemental analysis by Inductively Coupled Plasma-Atomic Emission Spectroscopy (ICP-AES) or Inductively Coupled Plasma-Mass Spectrometry (ICP-MS). These measurements frequently involve regulatory or compliance criteria which include the determination of elements on the EPA Target Analyte List (TAL). These samples usually consist of both an aqueous phase and a solid phase which is mostly an inorganic sludge. Frequently, samples taken from the waste tanks contain high levels of uranium and thorium which can cause spectral interferences in ICP-AES or ICP-MS analysis. The removal of these interferences is necessary to determine the presence of the EPA TAL elements in the sample. Two clean-up methods were studied on simulated aqueous waste samples containing the EPA TAL elements. The first method studied was a classical procedure based upon liquid-liquid extraction using tri-n- octylphosphine oxide (TOPO) dissolved in cyclohexane. The second method investigated was based on more recently developed techniques using extraction chromatography; specifically the use of a commercially available Eichrom TRU·Spec trademark column. Literature on these two methods indicates the efficient removal of uranium and thorium from properly prepared samples and provides considerable qualitative information on the extraction behavior of many other elements. However, there is a lack of quantitative data on the extraction behavior of elements on the EPA Target Analyte List. Experimental studies on these two methods consisted of determining whether any of the analytes were extracted by these methods and the recoveries obtained. Both methods produced similar results; the EPA target analytes were only slightly or not extracted. Advantages and disadvantages of each method were evaluated and found to be comparable

  9. Spectral emission from the alkali inductively-coupled plasma: Theory and experiment

    Directory of Open Access Journals (Sweden)

    R. Bazurto

    2018-04-01

    Full Text Available The weakly-ionized, alkali inductively-coupled plasma (ICP has a long history as the light source for optical pumping. Today, its most significant application is perhaps in the rubidium atomic frequency standard (RAFS, arguably the workhorse of atomic timekeeping in space, where it is crucial to the RAFS’ functioning and performance (and routinely referred to as the RAFS’ “rf-discharge lamp”. In particular, the photon flux from the lamp determines the signal-to-noise ratio of the device, and variations in ICP brightness define the long-term frequency stability of the atomic clock as a consequence of the ac-Stark shift (i.e., the light-shift. Given the importance of Rb atomic clocks to diverse satellite navigation systems (e.g., GPS, Galileo, BeiDou – and thereby the importance of alkali ICPs to these systems – it is somewhat surprising to find that the physical processes occurring within the discharge are not well understood. As a consequence, researchers do not understand how to improve the spectral emission from the lamp except at a trial-and-error level, nor do they fully understand the nonlinear mechanisms that result in ICP light instability. Here, we take a first step in developing an intuitive, semi-quantitative model of the alkali rf-discharge lamp, and we perform a series of experiments to validate the theory’s predictions.

  10. Spectral emission from the alkali inductively-coupled plasma: Theory and experiment

    Science.gov (United States)

    Bazurto, R.; Huang, M.; Camparo, J.

    2018-04-01

    The weakly-ionized, alkali inductively-coupled plasma (ICP) has a long history as the light source for optical pumping. Today, its most significant application is perhaps in the rubidium atomic frequency standard (RAFS), arguably the workhorse of atomic timekeeping in space, where it is crucial to the RAFS' functioning and performance (and routinely referred to as the RAFS' "rf-discharge lamp"). In particular, the photon flux from the lamp determines the signal-to-noise ratio of the device, and variations in ICP brightness define the long-term frequency stability of the atomic clock as a consequence of the ac-Stark shift (i.e., the light-shift). Given the importance of Rb atomic clocks to diverse satellite navigation systems (e.g., GPS, Galileo, BeiDou) - and thereby the importance of alkali ICPs to these systems - it is somewhat surprising to find that the physical processes occurring within the discharge are not well understood. As a consequence, researchers do not understand how to improve the spectral emission from the lamp except at a trial-and-error level, nor do they fully understand the nonlinear mechanisms that result in ICP light instability. Here, we take a first step in developing an intuitive, semi-quantitative model of the alkali rf-discharge lamp, and we perform a series of experiments to validate the theory's predictions.

  11. Method for separation of Cs from acid solution dissolving radionuclides and microanalysis of solution with ICP-AES

    International Nuclear Information System (INIS)

    Kanazawa, Toru; Hidaka, Akihide; Kudo, Tamotsu; Nakamura, Takehiko; Fuketa, Toyoshi

    2004-06-01

    The VEGA (Verification Experiments of radionuclides Gas/Aerosol release) program is being performed at JAERI to understand mechanisms of radionuclides release from irradiated fuel during severe accidents. As a part of evaluation in the program, the mass balances of released and deposited FP (Fission Products) onto the test apparatus are estimated from gamma ray measurement for acid solution leached from the apparatus, but short-life nuclides are difficult to be measured because those in the VEGA fuel have been mostly depleted due to cooling for several years. Moreover, the radionuclides without emitting gamma rays and very small quantity of elements cannot be quantified by gamma ray measurement. Therefore, a microanalysis by ICP-AES (Inductively Coupled Plasma - Atomic Emission Spectrometry) for the acid solution leached from VEGA apparatuses is being applied to evaluate the released and deposited masses for those elements. Since Cs-134 and -137, which are major FP dissolved in the solution, have high intensity of gamma ray spectrum, they have to be removed from the solution before the microanalysis in order to avoid contamination of ICP system and to decrease exposure to gamma ray. In this report, methods for separation of Cs from acid solution were reviewed and the applicability of them to the ICP-AES analysis was discussed. The method for Cs separation using the inorganic ion exchanger, AMP (Ammonium Molybdate Phosphate) was applied to the solutions of cold and hot test and the effectiveness was examined. The results showed that more than 99.9% of Cs could be removed from the test solutions, and once removed Sb by AMP was recovered by using a complexing agent such as citric acid. Next, the method was applied to an acid solution leached from VEGA-3 apparatus, and ICP-AES analysis was performed for it. The analysis showed that amount of U, Sr and Zr were successfully quantified. Most of elements to be analyzed were measurable except for Sb, Ag and Sn, although

  12. IMPULSE Highlights for recent experiments at the Advanced Photon Source (2/9-2/18 2014)

    Energy Technology Data Exchange (ETDEWEB)

    Jensen, Brian J. [Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

    2014-03-18

    This report is a presentation, with slides noting, Over 40 experiments were completed during this run using X-ray imaging on the IMPULSE system at Sector 32 IDB; Summary of new experiments: Idealized sphere compaction – Capture progression of dynamic densification through an idealized system on 0.500 mm borosilicate glass spheres (Slide 1); Detonator and EBW Imaging Experiments on IMPULSE – First time HE was intentionally detonated at APS (Slide 2); Spall and high strain rate crack nucleation/propagation in PMMA – PCI data is providing new and unique insights for model validation (Slide 3); Fiber composite for armor applications was studied under ballistic impact of Dyneema (Collaboration with Army Research Laboratory) (Slide 4). Summary of on-going experiments; Crack propagation in vitreous carbon – observed crack motion and caustic; Jet formation experiments on large grain cerium to examine phase dependent strength; Ballistic impact of Comp-B and TNT to examine thermo-mechanical response in-situ with various penetrator geometries to vary shear concentration. Other efforts: IMPULSE system moved and installed in Sector 35 (DCS). This includes the 4-frame X-ray detection system, 4- channel PDV, and other gun diagnostics; New remotely operated mobile IMPULSE structure in fabrication – to be delivered to APS in April; 4 Mini-VISAR Systems and 4-channel PDV installed in DCS instrumentation room with all associated diagnostics.

  13. Development of ICP-MS and ICP-OES methods for determination of gadolinium in samples related to hospital waste water treatment

    Czech Academy of Sciences Publication Activity Database

    Bendakovská, L.; Krejčovská, A.; Černohorský, T.; Zelenková, Jana

    2016-01-01

    Roč. 70, č. 9 (2016), s. 1155-1165 ISSN 0366-6352 Institutional support: RVO:67985874 Keywords : gadolinium * rare-earth elements * bioaccumulation * gadolinium anomaly * inductively coupled plasma mass spectrometry (ICP-MS) * inductively coupled plasma optical emission spectrometry (ICP-OES) Subject RIV: BK - Fluid Dynamics Impact factor: 1.258, year: 2016

  14. Development of a Supersonic Atomic Oxygen Nozzle Beam Source for Crossed Beam Scattering Experiments

    Science.gov (United States)

    Sibener, S. J.; Buss, R. J.; Lee, Y. T.

    1978-05-01

    A high pressure, supersonic, radio frequency discharge nozzle beam source was developed for the production of intense beams of ground state oxygen atoms. An efficient impedance matching scheme was devised for coupling the radio frequency power to the plasma as a function of both gas pressure and composition. Techniques for localizing the discharge directly behind the orifice of a water-cooled quartz nozzle were also developed. The above combine to yield an atomic oxygen beam source which produces high molecular dissociation in oxygen seeded rare gas mixtures at total pressures up to 200 torr: 80 to 90% dissociation for oxygen/argon mixtures and 60 to 70% for oxygen/helium mixtures. Atomic oxygen intensities are found to be greater than 10{sup 17} atom sr{sup -1} sec{sup -1}. A brief discussion of the reaction dynamics of 0 + IC1 ..-->.. I0 + C1 is also presented.

  15. Magnox fuel inventories. Experiment and calculation using a point source model

    International Nuclear Information System (INIS)

    Nair, S.

    1978-08-01

    The results of calculations of Magnox fuel inventories using the point source code RICE and associated Magnox reactor data set have been compared with experimental measurements for the actinide isotopes 234 , 235 , 236 , 238 U, 238 , 239 , 240 , 241 , 242 Pu, 241 , 243 Am and 242 , 244 Cm and the fission product isotopes 142 , 143 , 144 , 145 , 146 , 150 Nd, 95 Zr, 134 , 137 Cs, 144 Ce and daughter 144 Pr produced in four samples of spent Magnox fuel spanning the burnup range 3000 to 9000 MWd/Te. The neutron emissions from a further two samples were also measured and compared with RICE predictions. The results of the comparison were such as to justify the use of the code RICE for providing source terms for environmental impact studies, for the isotopes considered in the present work. (author)

  16. The UMLS Knowledge Source Server: an experience in Web 2.0 technologies.

    Science.gov (United States)

    Thorn, Karen E; Bangalore, Anantha K; Browne, Allen C

    2007-10-11

    The UMLS Knowledge Source Server (UMLSKS), developed at the National Library of Medicine (NLM), makes the knowledge sources of the Unified Medical Language System (UMLS) available to the research community over the Internet. In 2003, the UMLSKS was redesigned utilizing state-of-the-art technologies available at that time. That design offered a significant improvement over the prior version but presented a set of technology-dependent issues that limited its functionality and usability. Four areas of desired improvement were identified: software interfaces, web interface content, system maintenance/deployment, and user authentication. By employing next generation web technologies, newer authentication paradigms and further refinements in modular design methods, these areas could be addressed and corrected to meet the ever increasing needs of UMLSKS developers. In this paper we detail the issues present with the existing system and describe the new system's design using new technologies considered entrants in the Web 2.0 development era.

  17. Operational experience with the TRIUMF optically pumped polarized H- ion source

    International Nuclear Information System (INIS)

    Schmor, P.W.; Buchmann, L.; Jayamanna, K.; Levy, C.D.P.; McDonald, M.; Ruegg, R.

    1991-05-01

    The initial goal of a polarized proton beam extracted from the TRIUMF cyclotron, having a current of 5 μA with 60% polarization, has been achieved with the development of the optically pumped polarized H - ion source. This beam is now being used to produce an intense secondary beam of polarized neutrons for the TRIUMF experimental program. Much of the recent development effort has addressed the reliability requirements for routine operation. This paper describes the results with emphasis on the laser stabilization subsystem, the modifications to the electron cyclotron resonance proton ion source (ECRIS), the sodium charge exchange cells and the development of a low energy polarimeter. Also discussed are the developments which should lead to a higher polarization. (Author) 7 refs

  18. Practical Experiences of Building an IPFIX Based Open Source Botnet Detector

    Directory of Open Access Journals (Sweden)

    Mark Graham

    2016-03-01

    Full Text Available The academic study of flow-based malware detection has primarily focused on NetFlow v5 and v9. In 2013 IPFIX was ratified as the flow export standard. As part of a larger project to develop protection methods for Cloud Service Providers from botnet threats, this paper considers the challenges involved in designing an open source IPFIX based botnet detection function. This paper describes how these challenges were overcome and presents an open source system built upon Xen hypervisor and Open vSwitch that is able to display botnet traffic within Cloud Service Provider-style virtualised environments. The system utilises Euler property graphs to display suspect “botnests”. The conceptual framework presented provides a vendor-neutral, real-time detection mechanism for monitoring botnet communication traffic within cloud architectures and the Internet of Things.

  19. Synchronized and configurable source of electrical pulses for x-ray pump-probe experiments

    International Nuclear Information System (INIS)

    Strachan, J. P.; Chembrolu, V.; Yu, X. W.; Tyliszczak, T.; Acremann, Y.

    2007-01-01

    A method is described for the generation of software tunable patterns of nanosecond electrical pulses. The bipolar, high repetition rate (up to 250 MHz), fast rise time (<30 ps), square pulses are suitable for applications such as the excitation sequence in dynamic pump-probe experiments. Synchronization with the time structure of a synchrotron facility is possible as well as fine control of the relative delay in steps of 10 ps. The pulse generator described here is used to excite magnetic nanostructures with current pulses. Having an excitation system which can match the high repetition rate of a synchrotron allows for utilization of the full x-ray flux and is needed in experiments which require a large photon flux. The fast rise times allow for picosecond time resolution in pump-probe experiments. All pulse pattern parameters are configurable by software

  20. Time-resolved far-infrared experiments at the National Synchrotron Light Source. Final report

    International Nuclear Information System (INIS)

    Tanner, D.B.; Reitze, D.H.; Carr, G.L.

    1999-01-01

    A facility for time-resolved infrared and far-infrared spectroscopy has been built and commissioned at the National Synchrotron Light Source. This facility permits the study of time dependent phenomena over a frequency range from 2-8000cm -1 (0.25 meV-1 eV). Temporal resolution is approximately 200 psec and time dependent phenomena in the time range out to 100 nsec can be investigated

  1. Carbon Rod Radiant Source for Blast/Fire Interaction Experiments: Proof of Concept and Design.

    Science.gov (United States)

    1980-08-30

    traction motors , such as are used by Los Alamos Scientific Laboratory for unique pulse powered fields/beams, and a powerful low cost homopolar generator...tapping a high voltage AC transmission line (those used in the electroplating industry appear to have the right specifications), and homopolar -type...flywheel) generators. The AC rectification to DC was eliminated due to the very limited peak power available at Camp Parks. The one homopolar power source

  2. Sheath physics and materials science results from recent plasma source ion implantation experiments

    International Nuclear Information System (INIS)

    Conrad, J.R.; Radtke, J.L.; Dodd, R.A.; Worzala, F.J.

    1987-01-01

    Plasma Source Ion Implantation (PSII) is a surface modification technique which has been optimized for ion-beam processing of materials. PSII departs radically from conventional implantation by circumventing the line of sight restriction inherent in conventional ion implantation. The authors used PSII to implant cutting tools and dies and have demonstrated substantial improvements in lifetime. Recent results on plasma physics scaling laws, microstructural, mechanical, and tribological properties of PSII-implanted materials are presented

  3. Prototype of an angular-selective photoelectron calibration source for the KATRIN experiment

    Czech Academy of Sciences Publication Activity Database

    Valerius, K.; Hein, H.; Baumeister, H.; Beck, M.; Bokeloh, K.; Bonn, J.; Gluck, F.; Ortjohann, H.W.; Ostrick, B.; Zbořil, Miroslav; Weinheimer, Ch.

    2011-01-01

    Roč. 6, - (2011), P01002/1-P01002/11 ISSN 1748-0221 R&D Projects: GA MŠk LA318; GA MŠk LC07050 Institutional research plan: CEZ:AV0Z10480505 Keywords : Spectrometers * Photoemission * Detector alignment and calibration methods (lasers, sources, particle-beams) Subject RIV: BG - Nuclear, Atomic and Molecular Physics, Colliders Impact factor: 1.869, year: 2011

  4. DrSPINE - New approach to data reduction and analysis for neutron spin echo experiments from pulsed and reactor sources

    International Nuclear Information System (INIS)

    Zolnierczuk, P.A.; Ohl, M.; Holderer, O.; Monkenbusch, M.

    2015-01-01

    Neutron spin echo (NSE) method at a pulsed neutron source presents new challenges to the data reduction and analysis as compared to the instruments installed at reactor sources. The main advantage of the pulsed source NSE is the ability to resolve the neutron wavelength and collect neutrons over a wider bandwidth. This allows us to more precisely determine the symmetry phase and measure the data for several Q-values at the same time. Based on the experience gained at the SNS NSE - the first, and to date the only one, NSE instrument installed at a pulsed spallation source, we propose a novel and unified approach to the NSE data processing called DrSPINE. The goals of the DrSPINE project are: -) exploit better symmetry phase determination due to the broader bandwidth at a pulsed source; -) take advantage of larger Q coverage for TOF instruments; -) use objective statistical criteria to get the echo fits right; -) provide robust reduction with report generation; -) incorporate absolute instrument calibration; and -) allow for background subtraction. The software must be able to read the data from various instruments, perform data integrity, consistency and compatibility checks and combine the data from compatible sets, partial scans, etc. We chose to provide a console-based interface with the ability to process macros (scripts) for batch evaluation. And last and not the least, a good software package has to provide adequate documentation. DrSPINE software is currently under development

  5. Insights into the Galactic Cosmic-ray Source from the TIGER Experiment

    Science.gov (United States)

    Link, Jason T.; Barbier, L. M.; Binns, W. R.; Christian, E. R.; Cummings, J. R.; Geier, S.; Israel, M. H.; Lodders, K.; Mewaldt,R. A.; Mitchell, J. W.; hide

    2009-01-01

    We report results from 50 days of data accumulated in two Antarctic flights of the Trans-Iron Galactic Element Recorder (TIGER). With a detector system composed of scintillators, Cherenkov detectors, and scintillating optical fibers, TIGER has a geometrical acceptance of 1.7 sq m sr and a charge resolution of 0.23 cu at Iron. TIGER has obtained abundance measurements of some of the rare galactic cosmic rays heavier than iron, including Zn, Ga, Ge, Se, and Sr, as well as the more abundant lighter elements (down to Si). The heavy elements have long been recognized as important probes of the nature of the galactic cosmic-ray source and accelerator. After accounting for fragmentation of cosmic-ray nuclei as they propagate through the Galaxy and the atmosphere above the detector system, the TIGER source abundances are consistent with a source that is a mixture of about 20% ejecta from massive stars and 80% interstellar medium with solar system composition. This result supports a model of cosmic-ray origin in OB associations previously inferred from ACE-CRIS data of more abundant lighter elements. These TIGER data also support a cosmic-ray acceleration model in which elements present in interstellar grains are accelerated preferentially compared with those found in interstellar gas.

  6. Real-time analysis, visualization, and steering of microtomography experiments at photon sources

    International Nuclear Information System (INIS)

    Laszeski, G. von; Insley, J.A.; Foster, I.; Bresnahan, J.; Kesselman, C.; Su, M.; Thiebaux, M.; Rivers, M.L.; Wang, S.; Tieman, B.; McNulty, I.

    2000-01-01

    A new generation of specialized scientific instruments called synchrotron light sources allow the imaging of materials at very fine scales. However, in contrast to a traditional microscope, interactive use has not previously been possible because of the large amounts of data generated and the considerable computation required translating this data into a useful image. The authors describe a new software architecture that uses high-speed networks and supercomputers to enable quasi-real-time and hence interactive analysis of synchrotron light source data. This architecture uses technologies provided by the Globus computational grid toolkit to allow dynamic creation of a reconstruction pipeline that transfers data from a synchrotron source beamline to a preprocessing station, next to a parallel reconstruction system, and then to multiple visualization stations. Collaborative analysis tools allow multiple users to control data visualization. As a result, local and remote scientists can see and discuss preliminary results just minutes after data collection starts. The implications for more efficient use of this scarce resource and for more effective science appear tremendous

  7. First results from experiment in South China Sea using marine controlled source electromagnetic

    Science.gov (United States)

    Li, Yuan; Wang, Lipeng; Deng, Ming

    2016-04-01

    We concentrated on the use of marine controlled-source electromagnetic (CSEM) sounding with a horizontal electric dipole source towed close to the seafloor and receivers anchored on the seafloor. We applied the CSEM method in South China Sea for the first time in 2014, which not only test the application of our instrument, but also test our data processing method. Electromagnetic fields transmitted by a towed electric dipole source in deep sea were measured by a linear array of six seafloor receivers, positioned 600 meter (m) apart. Our results provided two highly resistivity layers beneath the survey line and the gas hydrate saturation profile associated with the anomalous resistivity. In the letter, we discussed some anomalous layers during the interpretation steps. The most plausible explanation of the first resistivity layer anomalies is that large amounts of gas hydrate have accumulated at 200 m depth below the seep sites, and the second layers is considerable volumes of gas hydrate have accumulated the seafloor at survey line according to the conceptual model, during the resistivity compared with other evidence like seismic and well data from the same survey. We should try other observation like heat flow, geochemical or other evidence to test the statement in the future.

  8. Radioactive contamination of foods from fallout as a source of error in some animal experiments

    Energy Technology Data Exchange (ETDEWEB)

    Clayton, C G

    1957-01-01

    Radioactivity in control animals since 1956 has increased so as to vitiate experiments. The activity of foods used was measured. The counts are given for rat cubes, milk, peas, sugar, flour, cabbage, carrot, cauliflower, salt, semolina, and water. The high count of the cabbage is probably from /sup 137/Cs present as 4 micromicrocuries/g.

  9. Feasibility of perfluorocarbon tracers (PFTs) in atmospheric source-receptor experiments

    International Nuclear Information System (INIS)

    Dietz, R.N.; Senum, G.I.

    1984-03-01

    A brief description of the perfluorocarbon tracer (PFT) system, which includes the tracers and the release equipment, the air samplers and the analyzers, is presented along with details on the research needs to provide a viable system for MATEX-scenario experiments. The present family of 2 viable PFTs needs to be increased to 5 to 6. Given the present precision of the analysis system, a one year long tracer experiment consisting of 4 hour releases every 60 hours from 5 different sites would require nearly 150 metric tons of PFTs at a cost of $15,000,000. Shortcomings in the programmable sampler include the pump, the sampling sequence control flexibility, data storage and retrieval, and the lack of remote communication capability; sampler adsorbent studies are also needed. The analytical system, including the catalyst processing bed, the chromatography column resolution, and the linearity of the detector, is in need of significant improvement. A higher resolution analysis system could significantly reduce analysis time but, more importantly, reduce tracer requirements more than 10-fold, for a cost savings potential of more than $13,000,000. A model is presented to demonstrate the feasibility of tracer material balances. Assessment of earlier long-range tracer experiments indicates the need for possibly 400 ground sampling sites requiring $8 to $14 million worth of samplers for a one-year tracer experiment. As many as six aircraft would be needed to conduct airborne model validation and material balance studies for each tracer plume

  10. Elemental analysis of oum er rbia moroccan river-water Using icp-aes and chromatography

    International Nuclear Information System (INIS)

    Zahry, F.; Bounakhla, M.; Labraimi, M.; Moutte, J.; Bilal, E.

    2001-01-01

    The analysis of water and suspended particulate matter (SPM) from Oum er Rbia Moroccan river for the content of 22 elements has been performed utilizing ICP-AES and chromatography methods. MPS samples were dissolved in nitric acid. The element analyzed are : Na, Mg, Al, Si, P, S, Cl, K, Ca, Ti, V, Cr, Mn, Fe, Co, Ni, Cu, Zn, Br, Ba and Pb. The detection limits are sufficient for most of the elements to be determined. Results were assessed for the accuracy by the analysis of a multi-elemental standard. The results for most of the elements obtained were accurate to about 2-15%. The objective of the analysis were to determine the geochemical areas on this river, to explain the mechanisms of sediment transport and nevertheless, to assess the pollution of the river by human activities. 48 samples were collected along the river, between its source in meddle atlas and the Atlantic ocean at Azemour city

  11. Uranium isotopes determination in urine samples using alpha spectrometry and ICP-MS

    Energy Technology Data Exchange (ETDEWEB)

    Rosa, Mychelle M.L.; Maihara, Vera A. [Instituto de Pesquisas Energeticas e Nucleares (IPEN/CNEN-SP), Sao Paulo, SP (Brazil); Tine, Fernanda D.; Santos, Sandra M.C.; Bonifacio, Rodrigo L.; Taddei, Maria HelenaT. [Comissao Nacional de Energia Nuclear (LAPOC/CNEN-MG), Pocos de Caldas, MG (Brazil). Laboratorio de Pocos de Caldas

    2015-07-01

    The action of determining the concentration of uranium isotopes in biological samples, 'in vitro' bioassay, is an indirect method for evaluating the incorporation and quantification of these radionuclides internally deposited. When incorporated, these radionuclides tend to be disposed through excretion, with urine being the main source of data because it can be easily collected and analyzed. The most widely used methods for determination of uranium isotopes ({sup 234}U, {sup 235}U and {sup 238}U) are Alpha Spectrometry and ICP-MS. This work presents a comparative study for the determination of uranium isotopes using these two methodologies in real samples from occupationally exposed workers. In order to validate the methodology, a sample of the intercomparison exercise organized by PROCORAD (Association pour la Promotion du Controle de Qualite des Analyses de Biologie Medicale em Radiotoxicologie) was used, and the results were statistically compared applying the Student's t-test. (author)

  12. Determination of platinum group metals by ICP-AES in environmental samples after preconcentration

    International Nuclear Information System (INIS)

    Vlasankova, R.; Sommer, L.

    1999-01-01

    Platinum group metal (PGM) may have toxic properties and their presence in the environment represent danger for human health. With the introduction of automobile catalytic converters containing PGM, the emission of these noble metals into atmosphere has increased. Platinum, palladium and rhodium are used in this catalytic converters to decrease toxic emissions of carbon monoxide, unburnt hydrocarbons and nitrogen oxides in vehicles exhaust gases. These catalysts are mobile sources of PGM into the environment. Thus, increased platinum concentrations have been found in various objects of environment because of the massive introduction of such catalytic converters are present. The preconcentration and separation of PGM and their determination by ICP-AES in environmental samples are described

  13. Uranium isotopes determination in urine samples using alpha spectrometry and ICP-MS

    International Nuclear Information System (INIS)

    Rosa, Mychelle M.L.; Maihara, Vera A.; Tine, Fernanda D.; Santos, Sandra M.C.; Bonifacio, Rodrigo L.; Taddei, Maria HelenaT.

    2015-01-01

    The action of determining the concentration of uranium isotopes in biological samples, 'in vitro' bioassay, is an indirect method for evaluating the incorporation and quantification of these radionuclides internally deposited. When incorporated, these radionuclides tend to be disposed through excretion, with urine being the main source of data because it can be easily collected and analyzed. The most widely used methods for determination of uranium isotopes ( 234 U, 235 U and 238 U) are Alpha Spectrometry and ICP-MS. This work presents a comparative study for the determination of uranium isotopes using these two methodologies in real samples from occupationally exposed workers. In order to validate the methodology, a sample of the intercomparison exercise organized by PROCORAD (Association pour la Promotion du Controle de Qualite des Analyses de Biologie Medicale em Radiotoxicologie) was used, and the results were statistically compared applying the Student's t-test. (author)

  14. Determination of trace and toxic elements in Koran rice CRM by INAA, ICP and AAS

    International Nuclear Information System (INIS)

    Yong Sam Chung; Young Ju Chung; Kyung Haeng Cho; Joung Hae Lee

    1997-01-01

    Trace and toxic elements in Certified Reference Material (CRM) made of Korean rice at the Korea Research Institute of Standards and Science have been analyzed by Instrumental Neutron Activation Analysis (INAA). Data intercomparison from the measurement with those of Atomic Absorption Spectrometry (AAS) and Induced Coupled Plasma Spectrometry (ICPS) has been studied. The powdered samples were sterilized at 1.5 x 10 6 rad in the bottles using a 60 Co source after sieving and spiking to specific elements such as As, Cd, Cr, Cu and Hg and then the homogeneity of samples was assessed. Rice flour (SRM 1568a) and standard solutions made by the National Institute of Standards Technology (NIST) were used to construct the calibration curves for the INAA and the chemical methods, respectively. The uncertainties and concentration of constituent elements were determined and the possibility of their use for analytical quality control was considered. (author)

  15. Small Works, Big Stories. Methodological approaches to photogrammetry through crowd-sourcing experiences

    Directory of Open Access Journals (Sweden)

    Seren Griffiths

    2015-12-01

    Full Text Available A recent digital public archaeology project (HeritageTogether sought to build a series of 3D ditigal models using photogrammetry from crowd-sourced images. The project saw over 13000 digital images being donated, and resulted in models of some 78 sites, providing resources for researchers, and condition surveys. The project demonstrated that digital public archaeology does not stop at the 'trowel's edge', and that collaborative post-excavation analysis and generation of research processes are as important as time in the field. We emphasise in this contribution that our methodologies, as much as our research outputs, can be fruitfully co-produced in public archaeology projects.

  16. EXPERIENCES FROM THE SOURCE-TERM ANALYSIS OF A LOW AND INTERMEDIATE LEVEL RADWASTE DISPOSAL FACILITY

    International Nuclear Information System (INIS)

    Park, Jin Beak; Park, Joo-Wan; Lee, Eun-Young; Kim, Chang-Lak

    2003-01-01

    Enhancement of a computer code SAGE for evaluation of the Korean concept for a LILW waste disposal facility is discussed. Several features of source term analysis are embedded into SAGE to analyze: (1) effects of degradation mode of an engineered barrier, (2) effects of dispersion phenomena in the unsaturated zone and (3) effects of time dependent sorption coefficient in the unsaturated zone. IAEA's Vault Safety Case (VSC) approach is used to demonstrate the ability of this assessment code. Results of MASCOT are used for comparison purposes. These enhancements of the safety assessment code, SAGE, can contribute to realistic evaluation of the Korean concept of the LILW disposal project in the near future

  17. Experiment of bias probe method at NIRS-18 GHz ECR ion source

    Energy Technology Data Exchange (ETDEWEB)

    Jincho, Kaoru; Yamamoto, Mitsugu; Okada, Takanori; Takasugi, Wataru; Sakuma, Tetsuya; Miyoshi, Tomohiro [Accelerator Engineering Corp., Chiba (Japan); Kitagawa, Atsushi; Muramatsu, Masayuki [National Inst. of Radiological Sciences, Chiba (Japan); Biri, Sandor [Institute of Nuclear Research (ATOMKI), Debrecen (Hungary)

    2000-11-01

    An 18 GHz ECR ion source (NIRS-HEC) has been developed to produce highly charged heavy ions from Ar to Xe. In order to increase the beam intensity of highly charged ion, we tried a technique of supplying cold electrons into the ECR plasma. In this paper, enhancement of the beam intensity is discussed in detail. The bias voltage is applied on the probe to repel cold electrons which flow from a plasma. The output beam current is 130 e{mu}A for Ar{sup 11+}. (J.P.N.)

  18. Experiment of bias probe method at NIRS-18 GHz ECR ion source

    International Nuclear Information System (INIS)

    Jincho, Kaoru; Yamamoto, Mitsugu; Okada, Takanori; Takasugi, Wataru; Sakuma, Tetsuya; Miyoshi, Tomohiro; Kitagawa, Atsushi; Muramatsu, Masayuki; Biri, Sandor

    2000-01-01

    An 18 GHz ECR ion source (NIRS-HEC) has been developed to produce highly charged heavy ions from Ar to Xe. In order to increase the beam intensity of highly charged ion, we tried a technique of supplying cold electrons into the ECR plasma. In this paper, enhancement of the beam intensity is discussed in detail. The bias voltage is applied on the probe to repel cold electrons which flow from a plasma. The output beam current is 130 eμA for Ar 11+ . (J.P.N.)

  19. Open-Source Development Experiences in Scientific Software: The HANDE Quantum Monte Carlo Project

    Directory of Open Access Journals (Sweden)

    J. S. Spencer

    2015-11-01

    Full Text Available The HANDE quantum Monte Carlo project offers accessible stochastic algorithms for general use for scientists in the field of quantum chemistry. HANDE is an ambitious and general high-performance code developed by a geographically-dispersed team with a variety of backgrounds in computational science. In the course of preparing a public, open-source release, we have taken this opportunity to step back and look at what we have done and what we hope to do in the future. We pay particular attention to development processes, the approach taken to train students joining the project, and how a flat hierarchical structure aids communication.

  20. Construction, commissioning and operational experience of the Advanced Photon Source (APS) linear accelerator

    International Nuclear Information System (INIS)

    White, M.; Arnold, N.; Berg, W.

    1996-01-01

    The Advanced Photon Source linear accelerator system consists of a 200 MeV, 2856 MHz S-Band electron linac and a 2-radiation-thick tungsten target followed by a 450 MeV positron linac. The linac system has operated 24 hours per day for the past year to support accelerator commissioning and beam studies and to provide beam for the user experimental program. It achieves the design goal for positron current of 8 mA and produces electron energies up to 650 MeV without the target in place. The linac is described and its operation and performance are discussed

  1. Construction, commissioning and operational experience of the Advanced Photon Source (APS) linear accelerator

    International Nuclear Information System (INIS)

    White, M.; Arnold, N.; Berg, W.; Cours, A.; Fuja, R.; Grelick, A. E.; Sereno, N.; Wesolowski, W.; Ko, K.; Qian, Y.L.; Russell, T.

    1996-01-01

    The Advanced Photon Source linear accelerator system consists of a 200-MeV, 2856-MHz S-band electron linac and a 2-radiation-thick tungsten target followed by a 450-MeV positron linac. The linac system has operated 24 hours per day for the past year to support accelerator commissioning and beam studies and to provide beam for the user experimental program. It achieves the design goal for positron current of 8 mA and produces electron energies up to 650 MeV without the target in place. The linac is described and its operation and performance are discussed. (author)

  2. X-ray holographic microscopy experiments at the Brookhaven synchrotron light source

    International Nuclear Information System (INIS)

    Howells, M.R.; Iarocci, M.; Kenney, J.; Kirz, J.; Rarback, H.

    1983-01-01

    Soft x-ray holographic microscopy is discussed from an experimental point of view. Three series of measurements have been carried out using the Brookhaven 750 MeV storage ring as an x-ray source. Young slits fringes, Gabor (in line) holograms and various data pertaining to the soft x-ray performance of photographic plates are reported. The measurements are discussed in terms of the technique for recording them and the experimental limitations in effect. Some discussion is also given of the issues involved in reconstruction using visible light

  3. Circular arc fuel plate stability experiments and analyses for the advanced neutron source

    International Nuclear Information System (INIS)

    Swinson, W.F.; Battiste, R.L.; Yahr, G.T.

    1995-08-01

    The thin fuel plates planned for the Advanced Neutron Source are to be cooled by forcing heavy water at high velocity, 25 m/s, through thin cooling channels on each side of each plate. Because the potential for structural failure of the plates is a design concern, considerable effort has been expended in assessing this potential. As part of this effort, experimental flow tests and analyses to evaluate the structural response of circular arc plates have been conducted, and the results are given in this report

  4. Novel uses of a wide beam saddle field ion source for producing targets used in nuclear physics experiments at the Argonne National Laboratory ATLAS facility

    International Nuclear Information System (INIS)

    Greene, J.P.; Thomas, G.E.

    1996-01-01

    The wide beam ion sputter source has several unique characteristics which make it very useful for producing, reducing the thickness or cleaning the surface of targets needed for nuclear physics experiments. A discussion of these techniques as well as the sputter source characteristics will be given. Sputter yields obtained utilizing the source are presented for a variety of materials common to nuclear target production

  5. Preliminary design of experiment ALVAND 1 and low beta plasma source

    International Nuclear Information System (INIS)

    Anvari, A.; Azodi, H.; Naraghi, M.; Taherzadeh, M.; Torabi-Fard, A.

    1975-12-01

    The ultimate goal of a two years program, namely ''ALVAND PROJECT'' and problems concerned with the achievement of controlled thermonuclear reactions in Iran is covered. The report consists of six sections. The introduction deals with the advantages of a linear theta pinch and its comparison with toroidal and mirror devices. Attention has been paid to two important properties of the ALVAND 1 device, namely, its property of carrying out important missions in support of high beta controlled thermonuclear research and also its acting as a source for developing different diagnostic apparatus and excercising different measurement techniques. Expected plasma parameters for ALVAND 1 are given in the third section. In the fourth section the low beta plasma source and the important diagnostic techniques that may be developed are discussed. References are given in the fifth section. The calculation of the minimum required radius of a toroidal theta pinch reactor has been given in an appendix, which covers at the same time 2 schematic figures. Finally a program schedule is presented in section six

  6. Water privatization, water source, and pediatric diarrhea in Bolivia: epidemiologic analysis of a social experiment.

    Science.gov (United States)

    Tornheim, Jeffrey A; Morland, Kimberly B; Landrigan, Philip J; Cifuentes, Enrique

    2009-01-01

    Water and sanitation services are fundamental to the prevention of pediatric diarrhea. To enhance both access to water and investment, some argue for the privatization of municipal water networks. Water networks in multiple Bolivian cities were privatized in the 1990s, but contracts ended following popular protests citing poor access. A population-based retrospective cohort study was conducted in two Bolivian cities. Data were collected on family water utilization and sanitation practices and on the prevalence of diarrhea among 596 children. Drinking from an outdoor water source (OR, 2.08; 95%CI, 1.25-3.44) and shorter in-home water boiling times (OR, 1.99; 95%CI, 1.19-3.34) were associated with prevalence of diarrhea. Increased prevalence was also observed for children from families using private versus public water services, using off-network water from cistern trucks, or not treating their water in-home. Results suggest that water source, water provider, and in-home water treatment are important predictors of pediatric diarrhea.

  7. Coherence properties of third and fourth generation X-ray sources. Theory and experiment

    Energy Technology Data Exchange (ETDEWEB)

    Singer, Andrej

    2013-06-15

    Interference effects are among the most fascinating optical phenomena. For instance, the butterflies and soap bubbles owe their beautiful colors to interference effects. They appear as a result of the superposition principle, valid in electrodynamics due to the linearity of the wave equation. If two waves interfere, the total radiation field is a sum of these two fields and depends strongly on the relative phases between these fields. While the oscillation frequency of individual fields is typically too large to be observed by a human eye or other detection systems, the phase differences between these fields manifest themselves as relatively slowly varying field strength modulations. These modulations can be detected, provided the oscillating frequencies of the superposed fields are similar. As such, the interference provides a superb measure of the phase differences of optical light, which may carry detailed information about a source or a scattering object. The ability of waves to interfere depends strongly on the degree of correlation between these waves, i.e. their mutual coherence. Until the middle of the 20th century, the coherence of light available to experimentalists was poor. A significant effort had to be made to extend the degree of coherence, which made the electromagnetic field determination using of the interference principle very challenging. Coherence is the defining feature of a laser, whose invention initiated a revolutionary development of experimental techniques based on interference, such as holography. Important contributions to this development were also provided by astronomists, as due to enormous intergalactic distances the radiation from stars has a high transverse coherence length at earth. With the construction of third generation synchrotron sources, partially coherent X-ray sources have become feasible. New areas of research utilizing highly coherent X-ray beams have emerged, including X-ray photon correlation spectroscopy (XPCS), X

  8. Coherence properties of third and fourth generation X-ray sources. Theory and experiment

    International Nuclear Information System (INIS)

    Singer, Andrej

    2013-06-01

    Interference effects are among the most fascinating optical phenomena. For instance, the butterflies and soap bubbles owe their beautiful colors to interference effects. They appear as a result of the superposition principle, valid in electrodynamics due to the linearity of the wave equation. If two waves interfere, the total radiation field is a sum of these two fields and depends strongly on the relative phases between these fields. While the oscillation frequency of individual fields is typically too large to be observed by a human eye or other detection systems, the phase differences between these fields manifest themselves as relatively slowly varying field strength modulations. These modulations can be detected, provided the oscillating frequencies of the superposed fields are similar. As such, the interference provides a superb measure of the phase differences of optical light, which may carry detailed information about a source or a scattering object. The ability of waves to interfere depends strongly on the degree of correlation between these waves, i.e. their mutual coherence. Until the middle of the 20th century, the coherence of light available to experimentalists was poor. A significant effort had to be made to extend the degree of coherence, which made the electromagnetic field determination using of the interference principle very challenging. Coherence is the defining feature of a laser, whose invention initiated a revolutionary development of experimental techniques based on interference, such as holography. Important contributions to this development were also provided by astronomists, as due to enormous intergalactic distances the radiation from stars has a high transverse coherence length at earth. With the construction of third generation synchrotron sources, partially coherent X-ray sources have become feasible. New areas of research utilizing highly coherent X-ray beams have emerged, including X-ray photon correlation spectroscopy (XPCS), X

  9. ICP magnetic sector multiple collector mass spectrometry and the precise measurement of isotopic compositions using nebulization of solutions and laser ablation of solids

    International Nuclear Information System (INIS)

    Halliday, A.N.; Lee, D-C.; Christensen, J.N.; Yi, W.; Hall, C.M.; Jones, C.E.; Teagle, D.A.H.; Freedman, P.A.

    1996-01-01

    Inductively-coupled plasma (ICP) sources offer considerable advantages over thermal sources because the high ionization efficiency facilitates measurements of relatively high sensitivity for elements such as Hf or Sn, which can be difficult to measure precisely with thermal ionization mass spectrometry (TIMS). The mass discrimination (bias) is larger than for TIMS, favours the heavier ions, and decreases in magnitude with increasing mass. However, in contrast to TIMS, this discrimination is largely independent of the chemical or physical properties of the element or the duration of the analysis. This has been demonstrated to high precision with a double focussing multiple collector magnetic sector mass spectrometer with an ICP source. The principle of this instrument is briefly described. The potential of the instrument for high precision isotopic measurements of a very broad range of elements, using solution aspiration or laser ablation, is indicated. 15 refs

  10. Positive matrix factorization and trajectory modelling for source identification: A new look at Indian Ocean Experiment ship observations

    Science.gov (United States)

    Bhanuprasad, S. G.; Venkataraman, Chandra; Bhushan, Mani

    The sources of aerosols on a regional scale over India have only recently received attention in studies using back trajectory analysis and chemical transport modelling. Receptor modelling approaches such as positive matrix factorization (PMF) and the potential source contribution function (PSCF) are effective tools in source identification of urban and regional-scale pollution. In this work, PMF and PSCF analysis is applied to identify categories and locations of sources that influenced surface concentrations of aerosols in the Indian Ocean Experiment (INDOEX) domain measured on-board the research vessel Ron Brown [Quinn, P.K., Coffman, D.J., Bates, T.S., Miller, T.L., Johnson, J.E., Welton, E.J., et al., 2002. Aerosol optical properties during INDOEX 1999: means, variability, and controlling factors. Journal of Geophysical Research 107, 8020, doi:10.1029/2000JD000037]. Emissions inventory information is used to identify sources co-located with probable source regions from PSCF. PMF analysis identified six factors influencing PM concentrations during the INDOEX cruise of the Ron Brown including a biomass combustion factor (35-40%), three industrial emissions factors (35-40%), primarily secondary sulphate-nitrate, balance trace elements and Zn, and two dust factors (20-30%) of Si- and Ca-dust. The identified factors effectively predict the measured submicron PM concentrations (slope of regression line=0.90±0.20; R2=0.76). Probable source regions shifted based on changes in surface and elevated flows during different times in the ship cruise. They were in India in the early part of the cruise, but in west Asia, south-east Asia and Africa, during later parts of the cruise. Co-located sources include coal-fired electric utilities, cement, metals and petroleum production in India and west Asia, biofuel combustion for energy and crop residue burning in India, woodland/forest burning in north sub-Saharan Africa and forest burning in south-east Asia. Significant findings

  11. Chemical Explosion Experiments to Improve Nuclear Test Monitoring - Developing a New Paradigm for Nuclear Test Monitoring with the Source Physics Experiments (SPE)

    International Nuclear Information System (INIS)

    Snelson, Catherine M.; Abbott, Robert E.; Broome, Scott T.; Mellors, Robert J.; Patton, Howard J.; Sussman, Aviva J.; Townsend, Margaret J.; Walter, William R.

    2013-01-01

    A series of chemical explosions, called the Source Physics Experiments (SPE), is being conducted under the auspices of the U.S. Department of Energy's National Nuclear Security Administration (NNSA) to develop a new more physics-based paradigm for nuclear test monitoring. Currently, monitoring relies on semi-empirical models to discriminate explosions from earthquakes and to estimate key parameters such as yield. While these models have been highly successful monitoring established test sites, there is concern that future tests could occur in media and at scale depths of burial outside of our empirical experience. This is highlighted by North Korean tests, which exhibit poor performance of a reliable discriminant, mb:Ms (Selby et al., 2012), possibly due to source emplacement and differences in seismic responses for nascent and established test sites. The goal of SPE is to replace these semi-empirical relationships with numerical techniques grounded in a physical basis and thus applicable to any geologic setting or depth

  12. First experience with single-source dual-energy computed tomography in six patients with acute arthralgia: a feasibility experiment using joint aspiration as a reference

    Energy Technology Data Exchange (ETDEWEB)

    Diekhoff, Torsten; Kiefer, Tobias; Hamm, Bernd; Hermann, Kay-Geert A. [Charite - Universitaetsmedizin Berlin Campus Mitte, Humboldt-Universitaet zu Berlin, Freie Universitaet Berlin, Department of Radiology, Berlin (Germany); Ziegeler, Katharina; Feist, Eugen [Charite - Universitaetsmedizin Berlin Campus Mitte, Humboldt-Universitaet zu Berlin, Freie Universitaet Berlin, Department of Rheumatology and Clinical Immunology, Berlin (Germany); Mews, Juergen [Toshiba Medical Systems Europe, BV, Zoetermeer (Netherlands)

    2015-11-15

    Dual-energy computed tomography (DECT) is an emerging imaging technique for examining patients with suspected gout. Single-source dual-energy CT (S-DECT) is a new way of obtaining DECT information on conventional CT scanners rather than using special dual-source CT systems. We tested the feasibility of S-DECT (320-row CT; Aquilion ONE, Toshiba Medical Systems, Otawara, Japan) in 6 patients (5 men, 1 woman; mean age 61.3, range 48 to 69 years) with acute arthralgia and suspected gout, and compared the S-DECT findings with the results of joint aspiration. Three patients had a diagnosis of gouty arthritis with negatively birefringent crystals in synovial fluid, in addition to gouty tophi in S-DECT. Three patients had no detectable crystals by polarization microscopy and no tophi on DECT. Their final diagnoses were rheumatoid arthritis, activated osteoarthritis, and septic arthritis in one case each. This initial experience suggests that S-DECT might be a valuable alternative to dual-source CT. Hence, more patients may benefit from its additional diagnostic abilities in the future. (orig.)

  13. First experience with single-source dual-energy computed tomography in six patients with acute arthralgia: a feasibility experiment using joint aspiration as a reference

    International Nuclear Information System (INIS)

    Diekhoff, Torsten; Kiefer, Tobias; Hamm, Bernd; Hermann, Kay-Geert A.; Ziegeler, Katharina; Feist, Eugen; Mews, Juergen

    2015-01-01

    Dual-energy computed tomography (DECT) is an emerging imaging technique for examining patients with suspected gout. Single-source dual-energy CT (S-DECT) is a new way of obtaining DECT information on conventional CT scanners rather than using special dual-source CT systems. We tested the feasibility of S-DECT (320-row CT; Aquilion ONE, Toshiba Medical Systems, Otawara, Japan) in 6 patients (5 men, 1 woman; mean age 61.3, range 48 to 69 years) with acute arthralgia and suspected gout, and compared the S-DECT findings with the results of joint aspiration. Three patients had a diagnosis of gouty arthritis with negatively birefringent crystals in synovial fluid, in addition to gouty tophi in S-DECT. Three patients had no detectable crystals by polarization microscopy and no tophi on DECT. Their final diagnoses were rheumatoid arthritis, activated osteoarthritis, and septic arthritis in one case each. This initial experience suggests that S-DECT might be a valuable alternative to dual-source CT. Hence, more patients may benefit from its additional diagnostic abilities in the future. (orig.)

  14. Toward a Mechanistic Source Term in Advanced Reactors: A Review of Past U.S. SFR Incidents, Experiments, and Analyses

    Energy Technology Data Exchange (ETDEWEB)

    Bucknor, Matthew; Brunett, Acacia J.; Grabaskas, David

    2016-04-17

    In 2015, as part of a Regulatory Technology Development Plan (RTDP) effort for sodium-cooled fast reactors (SFRs), Argonne National Laboratory investigated the current state of knowledge of source term development for a metal-fueled, pool-type SFR. This paper provides a summary of past domestic metal-fueled SFR incidents and experiments and highlights information relevant to source term estimations that were gathered as part of the RTDP effort. The incidents described in this paper include fuel pin failures at the Sodium Reactor Experiment (SRE) facility in July of 1959, the Fermi I meltdown that occurred in October of 1966, and the repeated melting of a fuel element within an experimental capsule at the Experimental Breeder Reactor II (EBR-II) from November 1967 to May 1968. The experiments described in this paper include the Run-Beyond-Cladding-Breach tests that were performed at EBR-II in 1985 and a series of severe transient overpower tests conducted at the Transient Reactor Test Facility (TREAT) in the mid-1980s.

  15. Madagascar: open-source software project for multidimensional data analysis and reproducible computational experiments

    Directory of Open Access Journals (Sweden)

    Sergey Fomel

    2013-11-01

    Full Text Available The Madagascar software package is designed for analysis of large-scale multidimensional data, such as those occurring in exploration geophysics. Madagascar provides a framework for reproducible research. By “reproducible research” we refer to the discipline of attaching software codes and data to computational results reported in publications. The package contains a collection of (a computational modules, (b data-processing scripts, and (c research papers. Madagascar is distributed on SourceForge under a GPL v2 license https://sourceforge.net/projects/rsf/. By October 2013, more than 70 people from different organizations around the world have contributed to the project, with increasing year-to-year activity. The Madagascar website is http://www.ahay.org/.

  16. CHRONOS architecture: Experiences with an open-source services-oriented architecture for geoinformatics

    Science.gov (United States)

    Fils, D.; Cervato, C.; Reed, J.; Diver, P.; Tang, X.; Bohling, G.; Greer, D.

    2009-01-01

    CHRONOS's purpose is to transform Earth history research by seamlessly integrating stratigraphic databases and tools into a virtual on-line stratigraphic record. In this paper, we describe the various components of CHRONOS's distributed data system, including the encoding of semantic and descriptive data into a service-based architecture. We give examples of how we have integrated well-tested resources available from the open-source and geoinformatic communities, like the GeoSciML schema and the simple knowledge organization system (SKOS), into the services-oriented architecture to encode timescale and phylogenetic synonymy data. We also describe on-going efforts to use geospatially enhanced data syndication and informally including semantic information by embedding it directly into the XHTML Document Object Model (DOM). XHTML DOM allows machine-discoverable descriptive data such as licensing and citation information to be incorporated directly into data sets retrieved by users. ?? 2008 Elsevier Ltd. All rights reserved.

  17. Radiation Tolerance Qualification Tests of the Final Source Interface Unit for the ALICE Experiment

    CERN Document Server

    Dénes, E; Futó, E; Kerék, A; Kiss, T; Molnár, J; Novák, D; Soós, C; Tölyhi, T; Van de Vyvre, P

    2007-01-01

    The ALICE Detector Data Link (DDL) is a high-speed optical link designed to interface the readout electronics of ALICE sub-detectors to the DAQ computers. The Source Interface Unit (SIU) of the DDL will operate in radiation environment. Previous tests showed that a configuration loss of SRAM-based FPGA devices may happen and the frequency of undetected data errors in the FPGA user memory area is also not acceptable. Therefore, we redesigned the SIU card using another FPGA based on flash technology. In order to detect bit errors in the user memory we added parity check logic to the design. The new SIU has been extensively tested using neutron and proton irradiation to verify its radiation tolerance. In this paper we summarize the design changes, introduce the final design, and the results of the radiation tolerance measurements on the final card.

  18. Critical experiments in support of the CNPS [Compact Nuclear Power Source] program

    International Nuclear Information System (INIS)

    Hansen, G.E.; Audas, J.H.; Martin, E.R.; Pederson, R.A.; Spriggs, G.D.; White, R.H.

    1988-01-01

    Zero-power static and kinetic measurements have been made on a mock-up of the Compact Nuclear Power Source (CNPS), a graphite moderated, graphite reflected, U(19.9% 235 U) fueled reactor design. Critical configurations were tracked from a first clean configuration (184 most central fuel channels filled and all control rod and heat pipe channels empty) to a fully loaded configuration (all 492 fuel channels filled, core-length stainless steel pipe in the twelve heat-pipe channels, and approximately half-core-length boron carbide in the outer 4 control rod channels. Reactor physics data such as material worths and neutron lifetime are presented only for the clean and fully loaded configurations

  19. Finnish experiences of health monitoring: local, regional, and national data sources for policy evaluation

    Directory of Open Access Journals (Sweden)

    Katri Kilpeläinen

    2016-02-01

    Full Text Available Background: Finland has a long tradition of gathering information about the health and welfare of the adult population. Design: Surveys and administrative registers form the basis for national and local health monitoring in Finland. Results: Different data sources are used in Finland to develop key indicators, which can be used to evaluate how the national health policy targets have been met in different parts of the country and in different population subgroups. Progress has been shown in chronic disease risk factors, such as smoking reduction. However, some health policy targets have not been met. Socioeconomic health differences, for example, have remained large compared with other European countries. Conclusion: Although data availability for key health indicators is good in Finland, there is a need for wider and more comprehensive use of this information by political decision-makers and healthcare professionals.

  20. Sources of Escherichia coli O157 and experiences over the past 15 years in Sheffield, UK.

    Science.gov (United States)

    Chapman, P A

    2000-01-01

    In the first documented outbreak of HC caused by Escherichia coli O157, which occurred in the North-west USA in 1982, there was a strong association between infection and prior consumption of ground beef from a chain of fast food restaurants. Foods of bovine origin, including beef, milk and dairy products, have since been implicated in many outbreaks of infection world-wide. Investigations during the course of outbreaks, or at random, have shown that cattle are a major reservoir of E. coli O157. E. coli O157 was isolated from cattle at slaughter in Sheffield in 1987, this being the first isolation from cattle in the UK. Following a cluster of cases in May/June 1992, an abattoir study showed the organism to be present in 4% of cattle at slaughter and on up to a third of carcasses from rectal swab-positive animals. E. coli O157 was isolated from a food source (unpasteurized milk), for the first time in the UK, in Sheffield in May 1993. During surveillance in 1995-6, E. coli O157 was isolated from 15.7% of cattle, with a monthly prevalence which varied from 5 to 37%. E. coli O157 was also isolated from 2.2% of sheep. During surveillance in 1996, E. coli O157 was isolated from 5.9% of samples of lamb products and from 1.5% of samples of beef products, despite the prevalence in cattle being much higher than in sheep. Work is in progress to try to explain this higher prevalence in lamb products. During 1997 in Sheffield, the only cases of E. coli O157 for which a confirmed source was established were associated with direct animal contact on farm visits. During on-farm investigations of these cases, E. coli O157 was isolated from faecal samples from adult cattle, calves, three different breeds of sheep, two different breeds of pigs, goats and a pony.

  1. Sputtering in a glow discharge ion source - pressure dependence: theory and experiment

    International Nuclear Information System (INIS)

    Mason, R.S.; Pichilingi, Melanie

    1994-01-01

    A simplified theoretical expression has been developed for a glow discharge to show how the average cathode erosion rate (expressed as the number of atoms per ion of the total bombarding flux) varies with primary sputter yield, pressure, 'diffusion length' and sputtered atom 'stopping' cross section. An inverse pressure dependence is predicted which correlates well with experiment in the 2 and He, tend to converge. It is suggested that this could be due to a change in the mechanism to self-sputtering. Under constant conditions, the erosion rates of different cathode materials still correlate quite well with the differences in their primary sputter yields. (author)

  2. Elemental Analysis in Biological Matrices Using ICP-MS.

    Science.gov (United States)

    Hansen, Matthew N; Clogston, Jeffrey D

    2018-01-01

    The increasing exploration of metallic nanoparticles for use as cancer therapeutic agents necessitates a sensitive technique to track the clearance and distribution of the material once introduced into a living system. Inductively coupled plasma mass spectrometry (ICP-MS) provides a sensitive and selective tool for tracking the distribution of metal components from these nanotherapeutics. This chapter presents a standardized method for processing biological matrices, ensuring complete homogenization of tissues, and outlines the preparation of appropriate standards and controls. The method described herein utilized gold nanoparticle-treated samples; however, the method can easily be applied to the analysis of other metals.

  3. Subcriticality determination by a new time-domain correlation experiment with a 252Cf neutron source

    International Nuclear Information System (INIS)

    Nishina, K.; Yamane, Y.; Ishiguro, S.; Miyoshi, Y.; Suzaki, T.; Kobayahi, I.

    1985-01-01

    As a candidate for the on-site subcriticality-monitoring method, a new time-domain correlation experiment is proposed. Hinted by the Cf-252 detector method of Mihalczo, three covariances are taken between the count of three detectors; namely an ionization chamber with Cf-252 coating, and two He-3 proportional counters. A ratio Q is formed from the three quantities such that it does not depend either on detector efficiencies or counting gate duration T, and then related to reactivity. A formulation is given deriving a theoretical expression for this Q, with the effect of higher spatial modes included. Experiments were carried out with a loading at Tank-type Critical Assembly of Japan Atomic Energy Research Institute, which is a slightly-enriched, and light-water moderated system. With fundamental mode approximation adopted in the data processing, reasonable agreements are observed between the present method and the reactivity scale that has been calibrated by water-level variety. The possibility of the present method is to be investigated further beyond the range of 7$ reported

  4. Elemental speciation in biomolecules by LC-ICP-MS with magnetic sector and collision cell instruments

    Energy Technology Data Exchange (ETDEWEB)

    Wang, Jin [Iowa State Univ., Ames, IA (United States)

    1999-11-08

    A methodology that can monitor and identify inorganic elements in biological and environmental systems was developed. Size exclusion chromatography (SEC) separates biomolecules, which are then nebulized by a microconcentric nebulizer. The resulting aerosol is desolved and introduced into either a high resolution ICP-MS device or a quadrupole device with a collision cell. Because of the high sensitivity and spectral resolution and high sample introduction efficiency, many unusual or difficult elements, such as Cr, Se, Cd and U, can be observed at ambient levels bound to proteins in human serum. These measurements are made in only a few minutes without preliminary isolation and preconcentration steps. Serum samples can be titrated with spikes of various elements to determine which proteins bind a given metal and oxidation state. Experiments concerning the effects of breaking disulfide linkages and denaturation on metal binding in proteins were also investigated. Elemental distribution in liver extract was also obtained.

  5. Elemental speciation in biomolecules by LC-ICP-MS with magnetic sector and collision cell instruments

    International Nuclear Information System (INIS)

    Wang, Jin

    1999-01-01

    A methodology that can monitor and identify inorganic elements in biological and environmental systems was developed. Size exclusion chromatography (SEC) separates biomolecules, which are then nebulized by a microconcentric nebulizer. The resulting aerosol is desolved and introduced into either a high resolution ICP-MS device or a quadrupole device with a collision cell. Because of the high sensitivity and spectral resolution and high sample introduction efficiency, many unusual or difficult elements, such as Cr, Se, Cd and U, can be observed at ambient levels bound to proteins in human serum. These measurements are made in only a few minutes without preliminary isolation and preconcentration steps. Serum samples can be titrated with spikes of various elements to determine which proteins bind a given metal and oxidation state. Experiments concerning the effects of breaking disulfide linkages and denaturation on metal binding in proteins were also investigated. Elemental distribution in liver extract was also obtained

  6. Radiation physics of high power spallation targets. State of the art simulation methods and experiments, the 'European Spallation Source' (ESS)

    International Nuclear Information System (INIS)

    Filges, D.; Cloth, P.; Neef, R.D.; Schaal, H.

    1998-01-01

    Particle transport and nuclear interactions of planned high power spallation targets with GeV proton beams can be simulated using widely developed Monte Carlo transport methods. This includes available high energy radiation transport codes and systems for low energy, earlier developed for reactor physics and fusion technology. Monte Carlo simulation codes and applied methods are discussed. The capabilities of the world-wide existing state-of-the-art computer code systems are demonstrated. Results of computational studies for the 'European Spallation Source' (ESS) mercury high power target station are given. The needs for spallation related data and planned experiments are shown. (author)

  7. The Biopsychology-Toolbox: a free, open-source Matlab-toolbox for the control of behavioral experiments.

    Science.gov (United States)

    Rose, Jonas; Otto, Tobias; Dittrich, Lars

    2008-10-30

    The Biopsychology-Toolbox is a free, open-source Matlab-toolbox for the control of behavioral experiments. The major aim of the project was to provide a set of basic tools that allow programming novices to control basic hardware used for behavioral experimentation without limiting the power and flexibility of the underlying programming language. The modular design of the toolbox allows portation of parts as well as entire paradigms between different types of hardware. In addition to the toolbox, this project offers a platform for the exchange of functions, hardware solutions and complete behavioral paradigms.

  8. Advanced plasma flow simulations of cathodic-arc and ferroelectric plasma sources for neutralized drift compression experiments

    Directory of Open Access Journals (Sweden)

    Adam B. Sefkow

    2008-07-01

    Full Text Available Large-space-scale and long-time-scale plasma flow simulations are executed in order to study the spatial and temporal evolution of plasma parameters for two types of plasma sources used in the neutralized drift compression experiment (NDCX. The results help assess the charge neutralization conditions for ion beam compression experiments and can be employed in more sophisticated simulations, which previously neglected the dynamical evolution of the plasma. Three-dimensional simulations of a filtered cathodic-arc plasma source show the coupling efficiency of the plasma flow from the source to the drift region depends on geometrical factors. The nonuniform magnetic topology complicates the well-known general analytical considerations for evaluating guiding-center drifts, and particle-in-cell simulations provide a self-consistent evaluation of the physics in an otherwise challenging scenario. Plasma flow profiles of a ferroelectric plasma source demonstrate that the densities required for longitudinal compression experiments involving ion beams are provided over the drift length, and are in good agreement with measurements. Simulations involving azimuthally asymmetric plasma creation conditions show that symmetric profiles are nevertheless achieved at the time of peak on-axis plasma density. Also, the ferroelectric plasma expands upstream on the thermal expansion time scale, and therefore avoids the possibility of penetration into the acceleration gap and transport sections, where partial neutralization would increase the beam emittance. Future experiments on NDCX will investigate the transverse focusing of an axially compressing intense charge bunch to a sub-mm spot size with coincident focal planes using a strong final-focus solenoid. In order to fill a multi-tesla solenoid with the necessary high-density plasma for beam charge neutralization, the simulations predict that supersonically injected plasma from the low-field region will penetrate and

  9. Experience with copper oxide production in antiproton source components at Fermi National Accelerator Laboratory

    International Nuclear Information System (INIS)

    Ader, Christine R.; Harms, Elvin R. Jr; Morgan, James P.

    2000-01-01

    The Antiproton (Pbar) Source at Fermi National Accelerator Laboratory is a facility comprised of a target station, two rings called the Debuncher and Accumulator and the transport lines between those rings and the remainder of the particle accelerator complex. Water is by far the most common medium for carrying excess heat away from components, primarily electromagnets, in this facility. The largest of the water systems found in Pbar is the 95 degree Fahrenheit Low Conductivity Water (LCW) system. LCW is water which has had free ions removed, increasing its resistance to electrical current. This water circuit is used to cool magnets, power supplies, and stochastic cooling components and typically has a resistivity of 11--18 megaohms-cm. For more than ten years the Antiproton rings were plagued with overheating magnets due to plugged water-cooling channels. Various repairs have been tried over the years with no permanent success. Throughout all of this time, water samples have indicated copper oxide, CuO, as the source of the contamination. Matters came to a head in early 1997 following a major underground LCW leak between the Central Utilities Building and the Antiproton Rings enclosures. Over a span of several weeks following system turn-on, some twenty magnets overheated leading to unreliable Pbar source operation. Although it was known that oxygen in the system reacts with the copper tubing to form CuO, work to remedy this problem was not undertaken until this time period. Leaks, large quantities of make-up water, infrequent filter replacement, and thermal cycling also result in an increase in the corrosion product release rate. A three-pronged approach has been implemented to minimize the amount of copper oxide available to plug the magnets: (1) installation of an oxygen removal system capable of achieving dissolved oxygen concentrations in the parts per billion (ppb) range; (2) regular closed-loop filter/flushing of the copper headers and magnets and stainless

  10. Comparision of ICP-OES and MP-AES in determing soil nutrients by Mechlich3 method

    Science.gov (United States)

    Tonutare, Tonu; Penu, Priit; Krebstein, Kadri; Rodima, Ako; Kolli, Raimo; Shanskiy, Merrit

    2014-05-01

    flammable (C2H2) gases, cylinder handling and the running costs of equipment are low. Detection limits of elements for MP-AES lays between the AAS and ICP ones. The objective of this study was to compare the results of soil analysis using two multielemental analytical methods - ICP-OES and MP-AES. In the experiment, different soil types with various texture, content of organic matter and pH were used. For the study soil samples of Albeluvisols, Leptosols, Cambisols, Regosols and Histosols were used . The plant available nutrients were estimated by Mehlich 3 extraction. The ICP-OES analysis were provided in the Estonian Agricultural Research Centre and MP-AES analysis in department of Soil Science and Agrochemistry at Estonian University of Life Sciences. The detection limits and limits of quantification of Ca, K, Mg and P in extracts are calculated and reported.

  11. MRMer, an interactive open source and cross-platform system for data extraction and visualization of multiple reaction monitoring experiments.

    Science.gov (United States)

    Martin, Daniel B; Holzman, Ted; May, Damon; Peterson, Amelia; Eastham, Ashley; Eng, Jimmy; McIntosh, Martin

    2008-11-01

    Multiple reaction monitoring (MRM) mass spectrometry identifies and quantifies specific peptides in a complex mixture with very high sensitivity and speed and thus has promise for the high throughput screening of clinical samples for candidate biomarkers. We have developed an interactive software platform, called MRMer, for managing highly complex MRM-MS experiments, including quantitative analyses using heavy/light isotopic peptide pairs. MRMer parses and extracts information from MS files encoded in the platform-independent mzXML data format. It extracts and infers precursor-product ion transition pairings, computes integrated ion intensities, and permits rapid visual curation for analyses exceeding 1000 precursor-product pairs. Results can be easily output for quantitative comparison of consecutive runs. Additionally MRMer incorporates features that permit the quantitative analysis experiments including heavy and light isotopic peptide pairs. MRMer is open source and provided under the Apache 2.0 license.

  12. PyGaze: an open-source, cross-platform toolbox for minimal-effort programming of eyetracking experiments.

    Science.gov (United States)

    Dalmaijer, Edwin S; Mathôt, Sebastiaan; Van der Stigchel, Stefan

    2014-12-01

    The PyGaze toolbox is an open-source software package for Python, a high-level programming language. It is designed for creating eyetracking experiments in Python syntax with the least possible effort, and it offers programming ease and script readability without constraining functionality and flexibility. PyGaze can be used for visual and auditory stimulus presentation; for response collection via keyboard, mouse, joystick, and other external hardware; and for the online detection of eye movements using a custom algorithm. A wide range of eyetrackers of different brands (EyeLink, SMI, and Tobii systems) are supported. The novelty of PyGaze lies in providing an easy-to-use layer on top of the many different software libraries that are required for implementing eyetracking experiments. Essentially, PyGaze is a software bridge for eyetracking research.

  13. An open source digital servo for atomic, molecular, and optical physics experiments

    Energy Technology Data Exchange (ETDEWEB)

    Leibrandt, D. R., E-mail: david.leibrandt@nist.gov; Heidecker, J. [National Institute of Standards and Technology, Boulder, Colorado 80305 (United States)

    2015-12-15

    We describe a general purpose digital servo optimized for feedback control of lasers in atomic, molecular, and optical physics experiments. The servo is capable of feedback bandwidths up to roughly 1 MHz (limited by the 320 ns total latency); loop filter shapes up to fifth order; multiple-input, multiple-output control; and automatic lock acquisition. The configuration of the servo is controlled via a graphical user interface, which also provides a rudimentary software oscilloscope and tools for measurement of system transfer functions. We illustrate the functionality of the digital servo by describing its use in two example scenarios: frequency control of the laser used to probe the narrow clock transition of {sup 27}Al{sup +} in an optical atomic clock, and length control of a cavity used for resonant frequency doubling of a laser.

  14. An open source digital servo for atomic, molecular, and optical physics experiments

    Science.gov (United States)

    Leibrandt, D. R.; Heidecker, J.

    2015-12-01

    We describe a general purpose digital servo optimized for feedback control of lasers in atomic, molecular, and optical physics experiments. The servo is capable of feedback bandwidths up to roughly 1 MHz (limited by the 320 ns total latency); loop filter shapes up to fifth order; multiple-input, multiple-output control; and automatic lock acquisition. The configuration of the servo is controlled via a graphical user interface, which also provides a rudimentary software oscilloscope and tools for measurement of system transfer functions. We illustrate the functionality of the digital servo by describing its use in two example scenarios: frequency control of the laser used to probe the narrow clock transition of 27Al+ in an optical atomic clock, and length control of a cavity used for resonant frequency doubling of a laser.

  15. An open source digital servo for atomic, molecular, and optical physics experiments

    International Nuclear Information System (INIS)

    Leibrandt, D. R.; Heidecker, J.

    2015-01-01

    We describe a general purpose digital servo optimized for feedback control of lasers in atomic, molecular, and optical physics experiments. The servo is capable of feedback bandwidths up to roughly 1 MHz (limited by the 320 ns total latency); loop filter shapes up to fifth order; multiple-input, multiple-output control; and automatic lock acquisition. The configuration of the servo is controlled via a graphical user interface, which also provides a rudimentary software oscilloscope and tools for measurement of system transfer functions. We illustrate the functionality of the digital servo by describing its use in two example scenarios: frequency control of the laser used to probe the narrow clock transition of 27 Al + in an optical atomic clock, and length control of a cavity used for resonant frequency doubling of a laser

  16. Heat Transfer by Thermo-Capillary Convection. Sounding Rocket COMPERE Experiment SOURCE

    Science.gov (United States)

    Fuhrmann, Eckart; Dreyer, Michael

    2009-08-01

    This paper describes the results of a sounding rocket experiment which was partly dedicated to study the heat transfer from a hot wall to a cold liquid with a free surface. Natural or buoyancy-driven convection does not occur in the compensated gravity environment of a ballistic phase. Thermo-capillary convection driven by a temperature gradient along the free surface always occurs if a non-condensable gas is present. This convection increases the heat transfer compared to a pure conductive case. Heat transfer correlations are needed to predict temperature distributions in the tanks of cryogenic upper stages. Future upper stages of the European Ariane V rocket have mission scenarios with multiple ballistic phases. The aims of this paper and of the COMPERE group (French-German research group on propellant behavior in rocket tanks) in general are to provide basic knowledge, correlations and computer models to predict the thermo-fluid behavior of cryogenic propellants for future mission scenarios. Temperature and surface location data from the flight have been compared with numerical calculations to get the heat flux from the wall to the liquid. Since the heat flux measurements along the walls of the transparent test cell were not possible, the analysis of the heat transfer coefficient relies therefore on the numerical modeling which was validated with the flight data. The coincidence between experiment and simulation is fairly good and allows presenting the data in form of a Nusselt number which depends on a characteristic Reynolds number and the Prandtl number. The results are useful for further benchmarking of Computational Fluid Dynamics (CFD) codes such as FLOW-3D and FLUENT, and for the design of future upper stage propellant tanks.

  17. Analysis of the Source Physics Experiment SPE4 Prime Using State-Of Parallel Numerical Tools.

    Science.gov (United States)

    Vorobiev, O.; Ezzedine, S. M.; Antoun, T.; Glenn, L.

    2015-12-01

    This work describes a methodology used for large scale modeling of wave propagation from underground chemical explosions conducted at the Nevada National Security Site (NNSS) fractured granitic rock. We show that the discrete natures of rock masses as well as the spatial variability of the fabric of rock properties are very important to understand ground motions induced by underground explosions. In order to build a credible conceptual model of the subsurface we integrated the geological, geomechanical and geophysical characterizations conducted during recent test at the NNSS as well as historical data from the characterization during the underground nuclear test conducted at the NNSS. Because detailed site characterization is limited, expensive and, in some instances, impossible we have numerically investigated the effects of the characterization gaps on the overall response of the system. We performed several computational studies to identify the key important geologic features specific to fractured media mainly the joints characterized at the NNSS. We have also explored common key features to both geological environments such as saturation and topography and assess which characteristics affect the most the ground motion in the near-field and in the far-field. Stochastic representation of these features based on the field characterizations has been implemented into LLNL's Geodyn-L hydrocode. Simulations were used to guide site characterization efforts in order to provide the essential data to the modeling community. We validate our computational results by comparing the measured and computed ground motion at various ranges for the recently executed SPE4 prime experiment. We have also conducted a comparative study between SPE4 prime and previous experiments SPE1 and SPE3 to assess similarities and differences and draw conclusions on designing SPE5.

  18. Effect of postural changes on ICP in healthy and ill subjects

    DEFF Research Database (Denmark)

    Petersen, Lonnie G; Juhler, Marianne

    2015-01-01

    to distinguish normal human physiology from disease entities such as idiopathic intracranial hypertension and normal pressure hydrocephalus, we investigated ICP in different body postures in both normal and ill subjects. METHODS: Thirty-one patients were included: four normal patients following complete removal......: upright standing, sitting in a chair, supine and right lateral lumbar puncture position. RESULTS: Linear regression of median ICP based on patient posture, group, and purpose of monitoring presented a significant model (p ... of differences in median ICP between body postures and supine ICP as the baseline, presented a highly significant model (p posture (p postures enabled...

  19. Hybrid Ground-Source Heat Pump Installations: Experiences, Improvements, and Tools

    Energy Technology Data Exchange (ETDEWEB)

    Scott Hackel; Amanda Pertzborn

    2011-06-30

    One innovation to ground-source heat pump (GSHP, or GHP) systems is the hybrid GSHP (HyGSHP) system, which can dramatically decrease the first cost of GSHP systems by using conventional technology (such as a cooling tower or a boiler) to meet a portion of the peak heating or cooling load. This work uses three case studies (two cooling-dominated, one heating-dominated) to demonstrate the performance of the hybrid approach. Three buildings were studied for a year; the measured data was used to validate models of each system. The models were used to analyze further improvements to the hybrid approach, and establish that this approach has positive impacts, both economically and environmentally. Lessons learned by those who design and operate the systems are also documented, including discussions of equipment sizing, pump operation, and cooling tower control. Finally, the measured data sets and models that were created during this work are described; these materials have been made freely available for further study of hybrid systems.

  20. Pilot plant experience on anaerobic codigestion of source selected OFMSW and sewage sludge.

    Science.gov (United States)

    Cabbai, Valentina; De Bortoli, Nicola; Goi, Daniele

    2016-03-01

    Anaerobic codigestion of source selected organic fraction of municipal solid waste (SS-OFMSW) and sewage sludge may be one of the most viable solutions to optimize oversized digesters efficiency in wastewater treatment plants. Based on results of BMP tests obtained for sewage sludge and SS-OFMSW, pilot plant tests were carried out by 3.4 m(3) CSTR reactor at mesophilic temperature. A mix of fruit and vegetable waste from wholesale market and canteen waste was used as SS-OFMSW substrate. Tests were conducted applying an OLR (organic loading rate) ramp with 6 different phases until a value of 3.2 kgVS/m(3) d. Feedstock and digestate characteristics, efficiency and process parameters were monitored. The anaerobic codigestion development was stable in each phase: early indicators like VFA (volatile fatty acids) and FOS/TAC ratio were always below instability threshold values. The maximum OLR tested determined a GPR (gas production rate) of 0.95 N m(3)/m(3) d and SGP (specific gas production) of 0.49 N m(3)/kgVS with a VS abatement of 67.3%. Copyright © 2015 Elsevier Ltd. All rights reserved.

  1. Determination of trace Np and Pu by ICP-MS with extraction chromatography in emergency situations

    International Nuclear Information System (INIS)

    Yanqin, Ji; Qing, Tian; Baoming, Shen; Xianzhang, Shao

    2008-01-01

    Full text: An accurate determination of radioculides from various sources in the environmental samples is essential for assessment of the potential hazards and suitable countermeasures both in case of accidents, authorised release and routine surveillance. However, the concentrationof neptunium and plutonium is extremely low in environmental samples, and such samples have a complex matrix composition, which is to be taken into account for a proper analysis. Conventional radiochemical methods such as alpha spectrometry, neutron activation analysis, liquid, liquid scintillation system, fission track and gamma spectrometry for the quantitative determination of neptunium and plutonium often require complicated and time-consuming sample preparation and separation procedures. Due to the large amount of the complex and often unknown matrix, the analysis may also be covered by naturally occurring radionuclides. With the development of new analysis techniques, non-radioactive methods are increasingly used for the determination of trace or ultra-trace radionuclides in environmental samples. Inductively coupled plasma mass spectrometry (ICP-MS) is one of the most suitable analysis techniques for the measurement of the long-lived radionuclides with its high sensitivity, low detection limits, short analysis time, less chemical interferences and multi-elemental capability. The throughput is therefore very high (approx.100 samples a day). The main objective of the present study was to set up of a simple, fast separation procedure to measure Np and Pu in the environmental samples ICP-MS. An unique extraction chromatographic column (TOA: tri-n-octylamine on Teflon powder) with a two-stage sample loading was prepared to separate Np and Pu from the environmental matrix. Np and Pu were efficiently retained in 4 M HNO 3 medium on the column and easiy eluted with 0.02 M oxalic acid 0.16 M HNO 3 at 95 C degree. The separated solutions were free from most of the matrix elements and were

  2. Diffusion from a Ground Level Point Source Experiment with Thermoluminescence Dosimeters and Kr 85 as Tracer Substance

    Energy Technology Data Exchange (ETDEWEB)

    Gyllander, Ch; Hollman, S; Widemo, U

    1969-04-15

    Within the framework of the IRIS-project (Iodine Research in Safety Project) an experiment to study diffusion at near-ground level was carried out on 19 December 1967 using {sup 85}Kr as the tracer element. The object of the experiment was a) to test the method using |3-sensitive thermoluminescence dosimeters under actual field conditions. b) to study the initial dilution from a ground level point source. The test area chosen was the Tranvik valley just south of Trobbofjaerden, an inland bay of the Baltic. Dose distributions have been studied at two sections, 50 and 200 m respectively, from the release point. At each level various dispersion parameters have been experimentally determined and their conformity to normal distribution have been calculated. Dilution factors valid for the centre of the plume are related to the values reported in the literature. The experiment was made under ideal weather conditions above snow-free ground. Results of the next experiment, a point release at ground level from a building at Studsvik, are expected to yield valuable information concerning the effect of buildings on the diffusion pattern.

  3. Integrated Verification Experiment data collected as part of the Los Alamos National Laboratory's Source Region Program

    Energy Technology Data Exchange (ETDEWEB)

    Whitaker, R.W.; Noel, S.D.

    1992-12-01

    The summary report by Tom Weaver gives the overall background for the series of IVE (Integrated Verification Experiment) experiments including information on the full set of measurements made. This appendix presents details of the infrasound data for the and discusses certain aspects of a few special experiments. Prior to FY90, the emphasis of the Infrasound Program was on underground nuclear test (UGT) detection and yield estimation. During this time the Infrasound Program was a separate program at Los Alamos, and it was suggested to DOE/OAC that a regional infrasound network be established around NTS. The IVE experiments took place in a time frame that allowed simultaneous testing of possible network sites and examination of propagation in different directions. Whenever possible, infrasound stations were combined with seismic stations so that a large number could be efficiently fielded. The regional infrasound network was not pursued by DOE, as world events began to change the direction of verification toward non-proliferation. Starting in FY90 the infrasound activity became part of the Source Region Program which has a goal of understanding how energy is transported from the UGT to a variety of measurement locations.

  4. Diffusion from a Ground Level Point Source Experiment with Thermoluminescence Dosimeters and Kr 85 as Tracer Substance

    International Nuclear Information System (INIS)

    Gyllander, Ch.; Hollman, S.; Widemo, U.

    1969-04-01

    Within the framework of the IRIS-project (Iodine Research in Safety Project) an experiment to study diffusion at near-ground level was carried out on 19 December 1967 using 85 Kr as the tracer element. The object of the experiment was a) to test the method using |3-sensitive thermoluminescence dosimeters under actual field conditions. b) to study the initial dilution from a ground level point source. The test area chosen was the Tranvik valley just south of Trobbofjaerden, an inland bay of the Baltic. Dose distributions have been studied at two sections, 50 and 200 m respectively, from the release point. At each level various dispersion parameters have been experimentally determined and their conformity to normal distribution have been calculated. Dilution factors valid for the centre of the plume are related to the values reported in the literature. The experiment was made under ideal weather conditions above snow-free ground. Results of the next experiment, a point release at ground level from a building at Studsvik, are expected to yield valuable information concerning the effect of buildings on the diffusion pattern

  5. Lead isotope measurements on aerosol samples with ICP-MS

    International Nuclear Information System (INIS)

    Widmer, C.R.; Kraehenbuehl, U.; Kramers, J.; Tobler, L.

    2000-01-01

    Size fractionated aerosols were collected with low pressure Berner impactors on a radio/TV tower 110 m above ground on a hill 10 km east of Bern at a total elevation of 1060 m asl. Two different wind sectors were chosen with the goal of assessing any differences in lead concentration and the 3 radiogenic lead isotopes (206,207,208) for east and west wind, respectively. A leaching technique was used to extract the lead quantitatively from the surface of the impaction foils. This method has been proven to be better suited for airborne particles than complete microwave digestion because it is less time consuming and contamination risk is smaller. Blank considerations played a major role in choosing all the chemicals, tubes, beakers and selecting the analytical method. Lead concentrations were determined with GF-AAS and lead isotopes with two different ICP-MS systems, one being a multicollector system. Precision of the simultaneous multicollector system was found to be at least a factor of 3 better than that of the sequentially operating ICP-MS. The small variations in isotope ratios from the two wind sectors can be distinctly seen with this enhanced precision. The observed relative difference in isotope ratios between east- and westwind was ∝0.6% for 207 Pb/ 206 Pb and ∝0.5% for 208 Pb/ 206 Pb. (orig.)

  6. Indigenous development of a glove box for ICP-OES

    International Nuclear Information System (INIS)

    Khan, A.M.; Anwar, M.K.; Bangash, M.A.

    2011-01-01

    Chemical analysis involving nuclear materials are bound to be carried out in safety enclosures like glove box, fume hood etc. whereas chemical analysis which produce mist or vapors of these materials like Atomic absorption Spectrometry, Flame photometry and ICP-AE spectrometry etc. must be performed in a glove box with HEPA filters on exhaust. These instruments with glove box adaptation are rare and impossible to import for our country. An ICP-OES, model Integra-XL of GBC-Australia was purchased in 2008 for chemical analysis of similar materials. As usual it was manufactured to operate in open atmosphere. The required analytical work could not be done in open atmosphere due to active nature of the samples. Therefore modification and glove box (GB) adaptation was required. Although large in size yet difficult to adapt for GB, the instrument had to be modified to a large extent as only sample handling part of the instrument had to placed inside GB, leaving rest of the instrument available for later repair/maintenance work. Different options were considered for modification keeping in mind the isolation and negative pressure inside the GB and maintaining the integrity of the instrument. One of such option was finalized which involved shifting the optic tank etc. A no of isolation gadgets were designed and fabricated locally. This indigenization has saved some handsome amount of foreign exchange. (Author)

  7. Glass particles produced by laser ablation for ICP-MSmeasurements

    Energy Technology Data Exchange (ETDEWEB)

    Gonzalez, J.; Liu, C.; Wen, S.; Mao, X.; Russo, R.E.

    2007-06-01

    Pulsed laser ablation (266nm) was used to generate glass particles from two sets of standard reference materials using femtosecond (150fs) and nanosecond (4ns) laser pulses with identical fluences of 50 J cm{sup -2}. Scanning electron microscopy (SEM) images of the collected particles revealed that there are more and larger agglomerations of particles produced by nanosecond laser ablation. In contrast to the earlier findings for metal alloy samples, no correlation between the concentration of major elements and the median particle size was found. When the current data on glass were compared with the metal alloy data, there were clear differences in terms of particle size, crater depth, heat affected zone, and ICP-MS response. For example, glass particles were larger than metal alloy particles, the craters in glass were less deep than craters in metal alloys, and damage to the sample was less pronounced in glass compared to metal alloys samples. The femtosecond laser generated more intense ICP-MS signals compared to nanosecond laser ablation for both types of samples, although glass sample behavior was more similar between ns and fs-laser ablation than for metals alloys.

  8. Dual-source CT coronary angiography in patients with premature heart-beats: initial experience

    International Nuclear Information System (INIS)

    Wang Yining; Zhang Zhuhua; Kong Lingyan; Song Lan; Mu Wenbin; Wang Yun; Jin Zhengyu

    2008-01-01

    Objective: To evaluate the feasibility of dual-source computed tomography (DSCT) coronary angiography in a population with premature heart-beats. Methods: Seventy patients with suspected coronary artery disease and premature heart-beats were routinely imaged on a DSCT scanner (Somatom Definition, Siemens AG, Germany). The images were reconstmcted before and after ECG editing. Two readers independently assessed image quality of all coronary segments using a four-point grading scale from excellent (1) to non-assessable (4). The results of the two groups were compared with a paired t-test, and a P value of less than 0.05 was considered significant. Results: The mean heart rate during examination ranged from 49 to 111 bpm[ mean(70.7±12.4) bpm]. Twenty-eight of 70 patients with relatively small variability of the heart rate [(41.0±18.4) bpm] got diagnostic image quality without ECG editing. In other 42 patients with larger variability of the heart rate [(71.4±28.7) bpm], the mean image quality scores were 2.09±1.27 and 1.50±0.79 before and after ECG editing, there was a significant difference (t= 13.764, P 2 =121.846, P<0.01). Finally, the diagnostic image accounted 98.0% (1014/1035) in all segments of 70 patients. Conclusion: DSCT can provide diagnostic images for patients with premature heart-beats. The image quality in patients with larger variability of the heart rate can be significantly improved through ECG editing. (authors)

  9. Preshot predictions for the near-source region in the non-proliferation experiment

    Energy Technology Data Exchange (ETDEWEB)

    Patch, D.F.; Welch, J.E.; Zerkle, J. [SAIC/Simulation Technology Operation, San Diego, CA (United States)

    1994-12-31

    This paper summarizes a number of one and two-dimensional, ground motion calculations made in support of the Non-Proliferation Experiment (NPE), a 1KT high explosive shot fired on 22 September 1993 at the Nevada Test Site. These calculations were sponsored by the Defense Nuclear Agency`s late-time containment program, and were completed well before the test was executed. They addressed a variety of test design, analysis and construction issues, and sought to identify any potential safety concerns. The test site model used in these calculations was based in large part on earlier work performed at SAIC and by other Defense Nuclear Agency (DNA) contractors for the nearby underground nuclear test, code named MISTY ECHO. In particular, to obtain physical property and quasi-static material response data for the site, a number of core samples recovered near the MISTY ECHO working point (WP) were tested by TerraTek. We then used these data to develop a numerical response model for the site.

  10. Maternal experiences with and sources of information on galactagogues to support lactation: a cross-sectional study.

    Science.gov (United States)

    Bazzano, Alessandra N; Cenac, Lauren; Brandt, Amelia J; Barnett, Josephine; Thibeau, Shelley; Theall, Katherine P

    2017-01-01

    An increase in the marketing and use of herbal galactagogues among breastfeeding mothers in the US has raised the issue of how best to provide support and information on the use of these products, particularly in light of limited availability of certified lactation counselors and continued suboptimal rates of breastfeeding globally. Currently, no cross-sectional data are available on the experiences and attitudes of mothers regarding the use of herbal and pharmaceutical galactagogues for lactation in the US. The findings of an online survey of 188 breastfeeding mothers on experiences with and sources of information on galactagogues are presented. Most mothers (76%) reported that while breastfeeding, they felt as though they were not making enough milk to meet the needs of their child, and yet 54% also indicated that they had not supplemented with formula. A large proportion of respondents reported utilizing galactagogues to increase lactation and finding them useful. The results indicated that most women learned about galactagogues from the Internet or by word of mouth through friends. Lactation consultants were the third-most reported sources of information on these products. While many respondents reported perceiving galactagogues as innocuous, more evidence on safety and efficacy is needed to support women properly who seek out and use them. Large-scale studies of the prevalence of galactagogue use in the US and rigorous evaluation of use globally are needed to ensure that mothers who choose to breastfeed may safely avail themselves of all options when counseling support is insufficient.

  11. The Internet as a source of health information: experiences of cancer survivors and caregivers with healthcare providers.

    Science.gov (United States)

    Dolce, Maria C

    2011-05-01

    To describe the experiences of cancer survivors and caregivers with healthcare providers in the context of the Internet as a source of health information. Qualitative description. Online cancer communities hosted by the Association of Cancer Online Resources. Purposive sample of 488 cancer survivors, with varying cancer types and survivorship stages, and caregivers. Secondary data analysis using Krippendorff's thematic clustering technique of qualitative content analysis. Survivorship, healthcare relationships, and the Internet. Disenchantment with healthcare relationships was associated with failed expectations related to evidence-based practice, clinical expertise, informational support, and therapeutic interpersonal communication. Survivors and caregivers exercised power in healthcare relationships through collaboration, direct confrontation, becoming expert, and endorsement to influence and control care decisions. Disenchantment propelled cancer survivors and caregivers to search the Internet for health information and resources. Conversely, Internet information-seeking precipitated the experience of disenchantment. Through online health information and resources, concealed failures in healthcare relationships were revealed and cancer survivors and caregivers were empowered to influence and control care decisions. The findings highlight failures in cancer survivorship care and underscore the importance of novel interdisciplinary programs and models of care that support evidence-informed decision making, self-management, and improved quality of life. Healthcare professionals need to receive education on survivors' use of the Internet as a source of health information and its impact on healthcare relationships. Future research should include studies examining the relationship between disenchantment and survivorship outcomes.

  12. First experiments with a liquid-lithium based high-intensity 25-keV neutron source

    International Nuclear Information System (INIS)

    Paul, M.

    2014-01-01

    A high-intensity neutron source based on a Liquid-Lithium Target (LiLiT) and the 7 Li(p,n) reaction was developed at SARAF (Soreq Applied Research Accelerator Facility, Israel) and is used for nuclear astrophysics experiments. The setup was commissioned with a 1.3 mA proton beam at 1.91 MeV, producing a neutron yield of ~ 2 ×10 10 n/s, more than one order of magnitude larger than conventional 7 Li(p,n)-based neutron sources and peaked at ~25 keV. The LiLiT device consists of a high-velocity (> 4 m/s) vertical jet of liquid lithium (~200 °C) whose free surface is bombarded by the proton beam. The lithium jet acts both as the neutron-producing target and as a power beam dump. The target dissipates a peak power areal density of 2.5 kW/cm 2 and peak volume density of 0.5 MW/cm 3 with no change of temperature or vacuum regime in the vacuum chamber. Preliminary results of Maxwellian-averaged cross section measurements for stable isotopes of Zr and Ce, performed by activation in the neutron flux of LiLiT, and nuclear-astrophysics experiments in planning will be described. (author)

  13. Aerosol composition, chemistry, and source characterization during the 2008 VOCALS Experiment

    Energy Technology Data Exchange (ETDEWEB)

    Lee, Y.; Springston, S.; Jayne, J.; Wang, J.; Senum, G.; Hubbe, J.; Alexander, L.; Brioude, J.; Spak, S.; Mena-Carrasco, M.; Kleinman, L.; Daum, P.

    2010-03-15

    Chemical composition of fine aerosol particles over the northern Chilean coastal waters was determined onboard the U.S. DOE G-1 aircraft during the VOCALS (VAMOS Ocean-Cloud-Atmosphere-Land Study) field campaign between October 16 and November 15, 2008. SO42-, NO3-, NH4+, and total organics (Org) were determined using an Aerodyne Aerosol Mass Spectrometer, and SO42-, NO3-, NH4+, Na+, Cl-, CH3SO3-, Mg2+, Ca2+, and K+ were determined using a particle-into-liquid sampler-ion chromatography technique. The results show the marine boundary layer (MBL) aerosol mass was dominated by non- sea-salt SO42- followed by Na+, Cl-, Org, NO3-, and NH4+, in decreasing importance; CH3SO3-, Ca2+, and K+ rarely exceeded their respective limits of detection. The SO42- aerosols were strongly acidic as the equivalent NH4+ to SO42- ratio was only {approx}0.25 on average. NaCl particles, presumably of sea-salt origin, showed chloride deficits but retained Cl- typically more than half the equivalency of Na+, and are externally mixed with the acidic sulfate aerosols. Nitrate was observed only on sea-salt particles, consistent with adsorption of HNO3 on sea-salt aerosols, responsible for the Cl- deficit. Dust particles appeared to play a minor role, judging from the small volume differences between that derived from the observed mass concentrations and that calculated based on particle size distributions. Because SO42- concentrations were substantial ({approx}0.5 - {approx}3 {micro}g/m3) with a strong gradient (highest near the shore), and the ocean-emitted dimethylsulfide and its unique oxidation product, CH3SO3-, were very low (i.e., {le} 40 parts per trillion and <0.05 {micro}g/m3, respectively), the observed SO42- aerosols are believed to be primarily of terrestrial origin. Back trajectory calculations indicate sulfur emissions from smelters and power plants along coastal regions of Peru and Chile are the main sources of these SO4- aerosols. However, compared to observations, model

  14. Ultrasonic power transfer from a spherical acoustic wave source to a free-free piezoelectric receiver: Modeling and experiment

    Energy Technology Data Exchange (ETDEWEB)

    Shahab, S.; Gray, M.; Erturk, A., E-mail: alper.erturk@me.gatech.edu [G. W. Woodruff School of Mechanical Engineering, Georgia Institute of Technology, Atlanta, Georgia 30332 (United States)

    2015-03-14

    Contactless powering of small electronic components has lately received growing attention for wireless applications in which battery replacement or tethered charging is undesired or simply impossible, and ambient energy harvesting is not a viable solution. As an alternative to well-studied methods of contactless energy transfer, such as the inductive coupling method, the use of ultrasonic waves transmitted and received by piezoelectric devices enables larger power transmission distances, which is critical especially for deep-implanted electronic devices. Moreover, energy transfer by means of acoustic waves is well suited in situations where no electromagnetic fields are allowed. The limited literature of ultrasonic acoustic energy transfer is mainly centered on proof-of-concept experiments demonstrating the feasibility of this method, lacking experimentally validated modeling efforts for the resulting multiphysics problem that couples the source and receiver dynamics with domain acoustics. In this work, we present fully coupled analytical, numerical, and experimental multiphysics investigations for ultrasonic acoustic energy transfer from a spherical wave source to a piezoelectric receiver bar that operates in the 33-mode of piezoelectricity. The fluid-loaded piezoelectric receiver under free-free mechanical boundary conditions is shunted to an electrical load for quantifying the electrical power output for a given acoustic source strength of the transmitter. The analytical acoustic-piezoelectric structure interaction modeling framework is validated experimentally, and the effects of system parameters are reported along with optimal electrical loading and frequency conditions of the receiver.

  15. Ultrasonic power transfer from a spherical acoustic wave source to a free-free piezoelectric receiver: Modeling and experiment

    International Nuclear Information System (INIS)

    Shahab, S.; Gray, M.; Erturk, A.

    2015-01-01

    Contactless powering of small electronic components has lately received growing attention for wireless applications in which battery replacement or tethered charging is undesired or simply impossible, and ambient energy harvesting is not a viable solution. As an alternative to well-studied methods of contactless energy transfer, such as the inductive coupling method, the use of ultrasonic waves transmitted and received by piezoelectric devices enables larger power transmission distances, which is critical especially for deep-implanted electronic devices. Moreover, energy transfer by means of acoustic waves is well suited in situations where no electromagnetic fields are allowed. The limited literature of ultrasonic acoustic energy transfer is mainly centered on proof-of-concept experiments demonstrating the feasibility of this method, lacking experimentally validated modeling efforts for the resulting multiphysics problem that couples the source and receiver dynamics with domain acoustics. In this work, we present fully coupled analytical, numerical, and experimental multiphysics investigations for ultrasonic acoustic energy transfer from a spherical wave source to a piezoelectric receiver bar that operates in the 33-mode of piezoelectricity. The fluid-loaded piezoelectric receiver under free-free mechanical boundary conditions is shunted to an electrical load for quantifying the electrical power output for a given acoustic source strength of the transmitter. The analytical acoustic-piezoelectric structure interaction modeling framework is validated experimentally, and the effects of system parameters are reported along with optimal electrical loading and frequency conditions of the receiver

  16. Determination of stable isotope ratio of lead in airborne particulate matter by ICP-MS

    International Nuclear Information System (INIS)

    Mukai, Hitoshi; Ambe, Yoshinari

    1990-01-01

    ICP-MS was applied to the measurement of stable isotope ratios of lead, which are used as an indicator of the source of lead in airborne particulate matter. For the measurement of lead isotopes ratios, the influences of machine conditions, lead concentration and matrix elements to the precision and accuracy of the measurements were studied. At a scanning mode, dwell time of 40∼160 μs gave the best precision to the isotope ratio measurements; about 0.3 % of R.S.D. for 206 Pb/ 207 Pb and 206 Pb/ 208 Pb, 0.6 % for 206 Pb/ 204 Pb. Precision of the measurement was better at a high concentration of lead in sample solution. The observed value of 206 Pb/ 207 Pb ratio was not affected by the lead concentration, but in the cases of 206 Pb/ 204 Pb and 206 Pb/ 208 Pb, about 1 % of the value changed in the observed ratios with the lead concentration of 100∼500 μg/l. Six matrix elements (Na, K, Ca, Mg, Al, Fe) did not affect the observed isotope ratios up to 200 mg/l. The lead isotope ratios of reference materials {Urban Particulates (NIST) and Vehicle Exhausted Particulates (NIES)} were measured by using two kinds of sample; crude sample and lead-isolated sample from matrix elements by anodic deposition. Both cases gave the same isotope ratio values, therefore, lead isotope ratios in airborne particulate samples can be measured by ICP-MS without any separation of lead from matrix elements. (author)

  17. Identification of TRIM27 as a novel degradation target of herpes simplex virus 1 ICP0.

    Science.gov (United States)

    Conwell, Sara E; White, Anne E; Harper, J Wade; Knipe, David M

    2015-01-01

    The herpes simplex virus 1 (HSV-1) immediate early protein ICP0 performs many functions during infection, including transactivation of viral gene expression, suppression of innate immune responses, and modification and eviction of histones from viral chromatin. Although these functions of ICP0 have been characterized, the detailed mechanisms underlying ICP0's complex role during infection warrant further investigation. We thus undertook an unbiased proteomic approach to identifying viral and cellular proteins that interact with ICP0 in the infected cell. Cellular candidates resulting from our analysis included the ubiquitin-specific protease USP7, the transcriptional repressor TRIM27, DNA repair proteins NBN and MRE11A, regulators of apoptosis, including BIRC6, and the proteasome. We also identified two HSV-1 early proteins involved in nucleotide metabolism, UL39 and UL50, as novel candidate interactors of ICP0. Because TRIM27 was the most statistically significant cellular candidate, we investigated the relationship between TRIM27 and ICP0. We observed rapid, ICP0-dependent loss of TRIM27 during HSV-1 infection. TRIM27 protein levels were restored by disrupting the RING domain of ICP0 or by inhibiting the proteasome, arguing that TRIM27 is a novel degradation target of ICP0. A mutant ICP0 lacking E3 ligase activity interacted with endogenous TRIM27 during infection as demonstrated by reciprocal coimmunoprecipitation and supported by immunofluorescence data. Surprisingly, ICP0-null mutant virus yields decreased upon TRIM27 depletion, arguing that TRIM27 has a positive effect on infection despite being targeted for degradation. These results illustrate a complex interaction between TRIM27 and viral infection with potential positive or negative effects of TRIM27 on HSV under different infection conditions. During productive infection, a virus must simultaneously redirect multiple cellular pathways to replicate itself while evading detection by the host's defenses. To

  18. The baseline pressure of intracranial pressure (ICP) sensors can be altered by electrostatic discharges.

    Science.gov (United States)

    Eide, Per K; Bakken, André

    2011-08-22

    The monitoring of intracranial pressure (ICP) has a crucial role in the surveillance of patients with brain injury. During long-term monitoring of ICP, we have seen spontaneous shifts in baseline pressure (ICP sensor zero point), which are of technical and not physiological origin. The aim of the present study was to explore whether or not baseline pressures of ICP sensors can be affected by electrostatics discharges (ESD's), when ESD's are delivered at clinically relevant magnitudes. We performed bench-testing of a set of commercial ICP sensors. In our experimental setup, the ICP sensor was placed in a container with 0.9% NaCl solution. A test person was charged 0.5-10 kV, and then delivered ESD's to the sensor by touching a metal rod that was located in the container. The continuous pressure signals were recorded continuously before/after the ESD's, and the pressure readings were stored digitally using a computerized system A total of 57 sensors were tested, including 25 Codman ICP sensors and 32 Raumedic sensors. When charging the test person in the range 0.5-10 kV, typically ESD's in the range 0.5-5 kV peak pulse were delivered to the ICP sensor. Alterations in baseline pressure ≥ 2 mmHg was seen in 24 of 25 (96%) Codman sensors and in 17 of 32 (53%) Raumedic sensors. Lasting changes in baseline pressure > 10 mmHg that in the clinical setting would affect patient management, were seen frequently for both sensor types. The changes in baseline pressure were either characterized by sudden shifts or gradual drifts in baseline pressure. The baseline pressures of commercial solid ICP sensors can be altered by ESD's at discharge magnitudes that are clinically relevant. Shifts in baseline pressure change the ICP levels visualised to the physician on the monitor screen, and thereby reveal wrong ICP values, which likely represent a severe risk to the patient.

  19. The PROTEUS Experiment: Active Source Seismic Imaging of the Crustal Magma Plumbing Structure of the Santorini Arc Volcano

    Science.gov (United States)

    Hooft, E. E. E.; Morgan, J. V.; Nomikou, P.; Toomey, D. R.; Papazachos, C. V.; Warner, M.; Heath, B.; Christopoulou, M. E.; Lampridou, D.; Kementzetzidou, D.

    2016-12-01

    The goal of the PROTEUS seismic experiment (Plumbing Reservoirs Of The Earth Under Santorini) is to examine the entire crustal magma plumbing system beneath a continental arc volcano and determine the magma geometry and connections throughout the crust. These physical parameters control magma migration, storage, and eruption and inform the question of how physical and chemical processing of magma at arc volcanoes forms the andesitic rock compositions that dominate the lower continental crust. These physical parameters are also important to understand volcanic-tectonic interactions and geohazards. Santorini is ideal for these goals because the continental crust has been thinned by extension and so the deep magmatic system is more accessible, also it is geologically well studied. Since the volcano is a semi-submerged, it was possible to collect a unique 3D marine-land active source seismic dataset. During the PROTEUS experiment in November-December of 2015, we recorded 14,300 marine sound sources from the US R/V Langseth on 89 OBSIP short period ocean bottom seismometers and 60 German and 5 Greek land seismometers. The experiment was designed for high-density spatial sampling of the seismic wavefield to allow us to apply two state-of-the-art 3D inversion methods: travel time tomography and full waveform inversion. A preliminary travel time tomography model of the upper crustal seismic velocity structure of the volcano and surrounding region is presented in an accompanying poster. We also made marine geophysical maps of the seafloor using multi-beam bathymetry and of the gravity and magnetic fields. The new seafloor map reveals the detailed structure of the major fault system between Santorini and Amorgos, of associated landslides, and of newly discovered volcanic features. The PROTEUS project will provide new insights into the structure of the whole crustal magmatic system of a continental arc volcano and its evolution within the surrounding tectonic setting.

  20. Study of Long-Lived Radionuclides in Environmental Samples by ICP-MS; Estudio de Radionucleidos de Vida Larga en Muestras Medioambientales por ICP-MS

    Energy Technology Data Exchange (ETDEWEB)

    Conde, E.; Navarro, N.; Fernández, M.

    2015-07-01

    Thorium is considered as one of the highly radiotoxic elements, because following its decay a number of other α, β and/or γ emitting daughters are produced. Uranium mining and processing, as well as remediation of impacted soils, are one of the principal anthropogenic sources of thorium release to the air, soil and water. Measurement of Th isotopes requires the use of analytical techniques capable of reliably measure the content of Th isotopes at trace levels. 230Th determination has generally been performed by α-spectrometry. However, this method needs sample preparation of 3-4 days and counting times from days to up to two weeks. A way to face this difficulty is the use of inductively coupled plasma mass spectrometry (ICP-MS). This technique is adequate for the determination of 232Th and 238U, long-lived radionuclides, and it can be applied, successfully, in the determination of 230Th, particularly if it is associated with a pre-concentration stage. This work presents the development of a rapid and simple analytical procedure based on mass spectrometry for the determination of 230Th and the results obtained in the analysis of environmental filters.

  1. Direct determination of uranium in human urine by Icp-SFMS; Determinacion directa de uranio en orina humana por ICP-SFMS

    Energy Technology Data Exchange (ETDEWEB)

    Hernandez M, H. [ININ, Departamento de Quimica, Carretera Mexico-Toluca s/n, 52750 Ocoyoacac, Estado de Mexico (Mexico); Yllera de Ll, A., E-mail: hector.hernandez520@gmail.com [Centro de Investigaciones Energeticas, Medioambientales y Tecnologicas, Departamento de Medio Ambiente, Av. Complutense 22, 28040 Madrid (Spain)

    2013-10-15

    The success of the measurement and the evaluation of the internal exposure are highly dependent of the effective capacities for the radiation measurement in biological samples (mainly urine and the feces). Usually, during the samples bioassay of human urine, a pre-concentration and purification of the radionuclides is carried out previously to the quantitative analysis. These stages, as the analysis time are the main source of uncertainty in the measurement process. In the uranium case, this is not necessary when are used mass spectrometry techniques, in particular, Mass Spectrometry of Magnetic Sector with Inductively Coupled Plasma (Icp-SFMS). This work presents the results obtained for the uranium analysis in samples of human urine during the participation in the inter-comparison exercises of the Association pour la Promotion de Controle de Qualite des Analyses de Biologie Medicale en Radiotoxicologie (PROCORAD) in the period 2010 and 2011. The analyses were realized directly in the diluted urine samples (dilution factor 1:20) in 5% of HNO{sub 3}. The obtained results, were normalized to the total urine sample (V = 0.5 L), these values coincide with the waited reference values of uranium in the urine sample. Additionally, were calculated the detection limits of {sup 235}U= 0.049 x 10{sup -3} μg L{sup -1} and {sup 238}U= 7.37 x 10{sup -3} μg L{sup -1}. (author)

  2. Ion chromatography separation of lanthanides at trace concentrations from Gd Matrix and quantification by ICP-MS

    International Nuclear Information System (INIS)

    Raut, V.V.; Jeyakumar, S.; Nagar, B.K.; Deb, S.B.; Saxena, M.K.; Tomar, B.S.

    2014-01-01

    Gadolinium compounds are mainly used as burnable poison. The presence of certain impurities is undesirable in the nuclear grade Gd compounds. Gd 2 O 3 , a most common raw material used for the preparation of nuclear grade Gd compounds. Analysis of rare earth impurities in Gd-matrices is one of the important exercises carried out to ensure the purity of Gd 2 O 3 . Determination of lanthanides at trace concentrations in lanthanide (Gd) matrix is complicated and difficult to realize. This is because the selective separation of REE's in one of the lanthanide elements is a challenging task. The present study was carried out to explore the feasibility of separating trace level lanthanides from Gd matrix by ion interaction chromatography (IIC) and to develop an analytical methodology for the determination of lanthanides by inductively coupled plasma mass spectrometry (ICP-MS). In the present investigation, the reversed phase column was dynamically modified into sulphonic acid functionalized surface by using 0.025 M n-Octane sulphonic acid (OSA). With α-HIBA eluent system, the elution order follows as Lu to La. The separations are employed with gradient elution mode. Since the sample has large excess of Gd, elution profiles with concentration gradient of HIBA were attempted. Separated fractions of Light lanthanides (LLn) and Heavy lanthanides (HLn) were collected and analyzed by ICP-MS. During MS analysis, it was observed that due to high concentration of salt (Na salt of OSA) present in the collected fractions caused difficulty in ICP-MS . Hence the experiments were carried out using another ion interacting reagent viz. 0.03 M camphor-10-sulphonic acid (CSA). Initial concentration of HIBA was kept at 0.025 M up to 15 min for the elution of HLns i.e. from Lu to Tb and it was then increased to 0.05 M to 0.3 M in 30 min. After elution of Tb, outlet of the column was switched to drain for 7 min to separate bulk Gd fraction. From 22 to 35 min effluent fraction containing Eu

  3. Sample introduction systems for the analysis of liquid microsamples by ICP-AES and ICP-MS

    Energy Technology Data Exchange (ETDEWEB)

    Todoli, Jose L. [Departamento de Quimica Analitica, Nutricion y Bromatologia, Universidad de Alicante, 03080 Alicante (Spain)]. E-mail: jose.todoli@ua.es; Mermet, Jean M. [Spectroscopy Forever, 01390 Tramoyes (France)

    2006-03-15

    There are many fields in which the available sample volume is the limiting factor for an elemental analysis. Over the last ten years, sample introduction systems used in plasma spectrometry (i.e., Inductively Coupled Plasma Atomic Emission Spectrometry, ICP-AES, and Mass Spectrometry, ICP-MS) have evolved in order to expand the field of applicability of these techniques to the analysis of micro- and nanosamples. A full understanding of the basic processes occurring throughout the sample introduction system is absolutely necessary to improve analytical performance. The first part of the present review deals with fundamental studies concerning the different phenomena taking place from aerosol production to analyte excitation/ionization when the liquid consumption rate does not exceed 100 {mu}l/min. Existing sample introduction systems are currently far from the ideal and a significant effort has been made to develop new and efficient devices. Different approaches for continuously introducing small sample volumes (i.e., microsamples) have been reviewed and compared in the present work. Finally, applications as well as basic guidelines to select the best sample introduction system according to the sample particularities are given at the end of this review.

  4. Sample introduction systems for the analysis of liquid microsamples by ICP-AES and ICP-MS

    International Nuclear Information System (INIS)

    Todoli, Jose L.; Mermet, Jean M.

    2006-01-01

    There are many fields in which the available sample volume is the limiting factor for an elemental analysis. Over the last ten years, sample introduction systems used in plasma spectrometry (i.e., Inductively Coupled Plasma Atomic Emission Spectrometry, ICP-AES, and Mass Spectrometry, ICP-MS) have evolved in order to expand the field of applicability of these techniques to the analysis of micro- and nanosamples. A full understanding of the basic processes occurring throughout the sample introduction system is absolutely necessary to improve analytical performance. The first part of the present review deals with fundamental studies concerning the different phenomena taking place from aerosol production to analyte excitation/ionization when the liquid consumption rate does not exceed 100 μl/min. Existing sample introduction systems are currently far from the ideal and a significant effort has been made to develop new and efficient devices. Different approaches for continuously introducing small sample volumes (i.e., microsamples) have been reviewed and compared in the present work. Finally, applications as well as basic guidelines to select the best sample introduction system according to the sample particularities are given at the end of this review

  5. The effect of dielectric top lids on materials processing in a low frequency inductively coupled plasma (LF-ICP) reactor

    International Nuclear Information System (INIS)

    Lim, J.W.M.; Chan, C.S.; Xu, L.; Xu, S.

    2014-01-01

    The advent of the plasma revolution began in the 1970's with the exploitation of plasma sources for anisotropic etching and processing of materials. In recent years, plasma processing has gained popularity, with research institutions adopting projects in the field and industries implementing dry processing in their production lines. The advantages of utilizing plasma sources would be uniform processing over a large exposed surface area, and the reduction of toxic emissions. This leads to reduced costs borne by manufacturers which could be passed down as consumer savings, and a reduction in negative environmental impacts. Yet, one constraint that plagues the industry would be the control of contaminants in a plasma reactor which becomes evident when reactions are conducted in a clean vacuum environment. In this work, amorphous silicon (a-Si) thin films were grown on glass substrates in a low frequency inductively coupled plasma (LF-ICP) reactor with a top lid made of quartz. Even though the chamber was kept at high vacuum (~10 −4 Pa), it was evident through secondary ion mass spectroscopy (SIMS) and Fourier-transform infra-red spectroscopy (FTIR) that oxygen contaminants were present. With the aid of optical emission spectroscopy (OES) the contaminant species were identified. The design of the LF-ICP reactor was then modified to incorporate an Alumina (Al 2 O 3 ) lid. Results indicate that there were reduced amounts of contaminants present in the reactor, and that an added benefit of increased power transfer to the plasma, improving deposition rate of thin films was realized. The results of this study is conclusive in showing that Al 2 O 3 is a good alternative as a top-lid of an LF-ICP reactor, and offers industries a solution in improving quality and rate of growth of thin films. (author)

  6. The use of ICP-MS and LA-ICP-MS techniques for uranium analysis in real-life swipe samples for safeguards purposes

    International Nuclear Information System (INIS)

    Pestana, Rafael C.B.; Sarkis, Jorge E.S.; Carvalho, Elita F.U.; Abreu Junior, Cassio H.

    2013-01-01

    Environmental swipe sampling for safeguards purposes is a powerful tool to detect undeclared materials and activities, and has been used by the International Atomic Energy Agency since 1997. This work describes the utilization of the inductively coupled plasma mass spectrometry (ICP-MS) and laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS) for determining uranium isotopic ratios in a real-life swipe samples collected in a conversion plant at IPEN/CNEN, Brazil. Uncertainties were estimated by following the International Organization for Standardization - Guide to the Expression of Uncertainties in Measurement (ISO GUM), with a confidence level of 95%. The major uncertainties percentage for n( 235 U)/n( 238 U) ratio for ICP-MS was 3% and for LA-ICP-MS was 30% The values of uranium isotopic ratios obtained for each technique demonstrate the viability of these analytical techniques as an alternative tool for uranium analysis in swipe samples for safeguards purposes. (author)

  7. Redox speciation of final repository relevant elements using separation methods in combination with ICP mass spectrometry

    International Nuclear Information System (INIS)

    Graser, Carl-Heinrich

    2015-01-01

    ) and Fe (III) was investigated using different organic complexing ligands, EDTA and o-phenanthroline. For the Fe redox system, a limit of detection of 10 -8 mol.L -1 was calculated. An improvement for the recovery values of the analytes was achieved by lowering the surface tension of the make up electrolyte. To determine the performance of the method a comparison of the speciation results with other methods like UV/vis, solvent extraction and thermodynamical calculations was done. The reproducibility of the method was examined and the linearity of the calibration in trace concentration levels was determined. To identify the redox species in different samples the electrophoretic mobilities of the analytes were calculated. Additional experiments to determine the redox species distribution of uranium and iron were done by hyphenating an ion chromatography column to a quadrupol inductively coupled plasma mass spectrometer (Q - ICP - MS). This method was applied to determine the redox species distribution of dissolved uranium in a fertilizer solution. With the data derived from iron experiments with CE - ICP - MS and IC - ICP - MS the characteristic values of both methods like separation times and detection limits were compared. The comparison of the performance of both methods was done by contrasting the linearity of calibration, analytical precision and recoveries.

  8. Operating experience in processing of differently sourced deeply depleted uranium oxide and production of deeply depleted uranium metal ingots

    International Nuclear Information System (INIS)

    Manna, S.; Ladola, Y.S.; Sharma, S.; Chowdhury, S.; Satpati, S.K.; Roy, S.B.

    2009-01-01

    Uranium Metal Plant (UMP) of BARC had first time experience on production of three Depleted Uranium Metal (DUM) ingots of 76kg, 152kg and 163kg during March 1991. These ingots were produced by processing depleted uranyl nitrate solution produced at Plutonium Plant (PP), Trombay. In recent past Uranium Metal Plant (UMP), Uranium Extraction Division (UED), has been assigned to produce tonnage quantity of Deeply DUM (DDUM) from its oxide obtained from PP, PREFRE and RMP, BARC. This is required for shielding the high radioactive source of BHABHATRON Tele-cobalt machine, which is used for cancer therapy. The experience obtained in processing of various DDU oxides is being utilized for design of large scale DDU-metal plant under XIth plan project. The physico- chemical characteristics like morphology, density, flowability, reactivity, particle size distribution, which are having direct effect on reactivity of the powders of the DDU oxide powder, were studied and the shop-floor operational experience in processing of different oxide powder were obtained and recorded. During campaign trials utmost care was taken to standardized all operating conditions using the same equipment which are in use for natural uranium materials processing including safety aspects both with respect to radiological safety and industrial safety. Necessary attention and close monitoring were specially arranged and maintained for the safety aspects during the trial period. In-house developed pneumatic transport system was used for powder transfer and suitable dust arresting system was used for reduction of powder carry over

  9. Comparison of Time-of-flight and Multicollector ICP Mass Spectrometers for Measuring Actinides in Small Samples using single shot Laser Ablation

    International Nuclear Information System (INIS)

    R.S. Houk; D.B. Aeschliman; S.J. Bajic; D. Baldwin

    2005-01-01

    The objective of these experiments is to evaluate the performance of two types of ICP-MS device for measurement of actinide isotopes by laser ablation (LA) ICP-MS. The key advantage of ICP-MS compared to monitoring of radioactive decay is that the element need not decay during the measurement time. Hence ICP-MS is much faster for long-lived radionuclides. The LA process yields a transient signal. When spatially resolved analysis is required for small samples, the laser ablation sample pulse lasts only ∼10 seconds. It is difficult to measure signals at several isotopes with analyzers that are scanned for such a short sample transient. In this work, a time-of-flight (TOF) ICP-MS device, the GBC Optimass 8000 (Figure 1) is one instrument used. Strictly speaking, ions at different m/z values are not measured simultaneously in TOF. However, they are measured in very rapid sequence with little or no compromise between the number of m/z values monitored and the performance. Ions can be measured throughout the m/z range in single sample transients by TOF. The other ICP-MS instrument used is a magnetic sector multicollector MS, the NU Plasma 1700 (Figure 2). Up to 8 adjacent m/z values can be monitored at one setting of the magnetic field and accelerating voltage. Three of these m/z values can be measured with an electron multiplier. This device is usually used for high precision isotope ratio measurements with the Faraday cup detectors. The electron multipliers have much higher sensitivity. In our experience with the scanning magnetic sector instrument in Ames, these devices have the highest sensitivity and lowest background of any ICP-MS device. The ability to monitor several ions simultaneously, or nearly so, should make these devices valuable for the intended application: measurement of actinide isotopes at low concentrations in very small samples for nonproliferation purposes. The primary sample analyzed was an urban dust pellet reference material, NIST 1648. The

  10. A Space Experiment to Measure the Atomic Oxygen Erosion of Polymers and Demonstrate a Technique to Identify Sources of Silicone Contamination

    Science.gov (United States)

    Banks, Bruce A.; deGroh, Kim K.; Baney-Barton, Elyse; Sechkar, Edward A.; Hunt, Patricia K.; Willoughby, Alan; Bemer, Meagan; Hope, Stephanie; Koo, Julie; Kaminski, Carolyn; hide

    1999-01-01

    A low Earth orbital space experiment entitled, "Polymers Erosion And Contamination Experiment", (PEACE) has been designed as a Get-Away Special (GAS Can) experiment to be accommodated as a Shuttle in-bay environmental exposure experiment. The first objective is to measure the atomic oxygen erosion yields of approximately 40 different polymeric materials by mass loss and erosion measurements using atomic force microscopy. The second objective is to evaluate the capability of identifying sources of silicone contamination through the use of a pin-hole contamination camera which utilizes environmental atomic oxygen to produce a contaminant source image on an optical substrate.

  11. Utilization of ICP/OES for the determination of trace metal binding to different humic fractions.

    Science.gov (United States)

    de la Rosa, G; Peralta-Videa, J R; Gardea-Torresdey, J L

    2003-02-28

    In this study, the use of inductively coupled plasma/optical emission spectrometry (ICP/OES) to determine multi-metal binding to three biomasses, Sphagnum peat moss, humin and humic acids is reported. All the investigations were performed under part per billion (ppb) concentrations. Batch pH profile experiments were performed using multi-metal solutions of Cd(II), Cu(II), Pb(II), Ni(II), Cr(III) and Cr(VI). The results showed that at pH 2 and 3, the metal affinity of the three biomasses exposed to the multi-metal solution that included Cr(III) presented the following order: Cu(II), Pb(II)>Ni(II)>Cr(III)>Cd(II). On the other hand, when Cr(VI) was in the heavy metal mixture, Sphagnum peat moss and humin showed the following affinity: Cu(II), Pb(II)>Ni(II)>Cr(VI)>Cd(II); however, the affinity of the humic acids was: Cu(II)>Pb(II), Cr(VI)>Ni(II)>Cd(II). The results demonstrated that pH values of 4 and 5 were the most favorable for the heavy metal binding process. At pH 5, all the metals, except for Cr(VI), were bound between 90 and 100% to the three biomasses. However, the binding capacity of humic acids decreased at pH 6 in the presence of Cr(VI). The results showed that the ICP/OES permits the determination of heavy metal binding to organic matter at ppb concentration. These results will be very useful in understanding the role of humic substances in the fate and transport of heavy metals, and thus could provide information to develop new methodologies for the removal of low concentrations of toxic heavy metals from contaminated waters.

  12. New approach of a transient ICP-MS measurement method for samples with high salinity.

    Science.gov (United States)

    Hein, Christina; Sander, Jonas Michael; Kautenburger, Ralf

    2017-03-01

    In the near future it is necessary to establish a disposal for high level nuclear waste (HLW) in deep and stable geological formations. In Germany typical host rocks are salt or claystone. Suitable clay formations exist in the south and in the north of Germany. The geochemical conditions of these clay formations show a strong difference. In the northern ionic strengths of the pore water up to 5M are observed. The determination of parameters like K d values during sorption experiments of metal ions like uranium or europium as homologues for trivalent actinides onto clay stones are very important for long term safety analysis. The measurement of the low concentrated, not sorbed analytes commonly takes place by inductively coupled plasma mass spectrometry (ICP-MS). A direct measurement of high saline samples like seawater with more than 1% total dissolved salt content is not possible. Alternatives like sample clean up, preconcentration or strong dilution have more disadvantages than advantages for example more preparation steps or additional and expensive components. With a small modification of the ICP-MS sample introduction system and a home-made reprogramming of the autosampler a transient analysing method was developed which is suitable for measuring metal ions like europium and uranium in high saline sample matrices up to 5M (NaCl). Comparisons at low ionic strength between the default and the transient measurement show the latter performs similarly well to the default measurement. Additionally no time consuming sample clean-up or expensive online dilution or matrix removal systems are necessary and the analysation shows a high sensitivity due to the data processing based on the peak area. Copyright © 2016 Elsevier B.V. All rights reserved.

  13. Surface modification of ceramic materials induced by irradiation of high power pulsed ICP

    International Nuclear Information System (INIS)

    Ishigaki, Takamasa; Okada, Nobuhiro; Ohashi, Naoki; Haneda, Hajime

    2003-01-01

    Newly developed pulse-modulated high-power inductively coupled plasma [ICP] is expected to offer the unique physico-chemical condition, such as the increased concentration of chemically reactive species, as well as the appropriate heat flux for materials processing. Two kinds of oxide materials, titanium and zinc oxide, were placed at the downstream of Ar-H 2 ICP and irradiated in the plasma of continuous [CN] and pulse-modulated [PM] modes. The CN-ICP irradiation at the position close to the plasma tail gave rise to the thermal reduction of oxides. In the PM-ICP irradiation, the degree of thermal reduction depended on the lower power level during pulse-off time, as well as the total electric power. Irradiation in PM-ICP led to the increased formation of oxygen vacancies in titanium dioxide. In the case of zinc oxide, the UV emission efficiency was improved by PM-ICP irradiation, while the green emission became predominant by CN-ICP irradiation at the appropriate position. Induced effects in the two oxides by PM-ICP would be related to the high concentration of hydrogen radicals in the plasma. (author)

  14. Early Implementation of THAM for ICP Control: Therapeutic Hypothermia Avoidance and Reduction in Hypertonics/Hyperosmotics

    Directory of Open Access Journals (Sweden)

    F. A. Zeiler

    2014-01-01

    Full Text Available Background. Tromethamine (THAM has been demonstrated to reduce intracranial pressure (ICP. Early consideration for THAM may reduce the need for other measures for ICP control. Objective. To describe 4 cases of early THAM therapy for ICP control and highlight the potential to avoid TH and paralytics and achieve reduction in sedation and hypertonic/hyperosmotic agent requirements. Methods. We reviewed the charts of 4 patients treated with early THAM for ICP control. Results. We identified 2 patients with aneurysmal subarachnoid hemorrhage (SAH and 2 with traumatic brain injury (TBI receiving early THAM for ICP control. The mean time to initiation of THAM therapy was 1.8 days, with a mean duration of 5.3 days. In all patients, after 6 to 12 hours of THAM administration, ICP stability was achieved, with reduction in requirements for hypertonic saline and hyperosmotic agents. There was a relative reduction in mean hourly hypertonic saline requirements of 89.1%, 96.1%, 82.4%, and 97.0% for cases 1, 2, 3, and 4, respectively, comparing pre- to post-THAM administration. Mannitol, therapeutic hypothermia, and paralytics were avoided in all patients. Conclusions. Early administration of THAM for ICP control could potentially lead to the avoidance of other ICP directed therapies. Prospective studies of early THAM administration are warranted.

  15. Theoretical Investigation of Spectral-Interferences of Cadmium Isotopes in ICP-MS

    International Nuclear Information System (INIS)

    Rashad, A.M.; Rashad, A.M.

    2015-01-01

    Thermal properties of polyatomic ions which can interfere with cadmium during the analysis process using the inductively coupled plasma mass spectrometer ICP-MS are studied. Ionization energies and heats of formation, of the selected species at 0 K and 298 K of the expected reactions to occur under the effect of plasma conditions in ICP-MS, are calculated using Gaussian 03

  16. Elemental mapping of structural materials for a nuclear reactor by means of LA-ICP-MS

    Czech Academy of Sciences Publication Activity Database

    Vaculovič, T.; Warchilová, T.; Šimo, T.; Matal, O.; Otruba, V.; Mikuška, Pavel; Kanický, V.

    2012-01-01

    Roč. 27, č. 8 (2012), s. 1321-1326 ISSN 0267-9477 Institutional research plan: CEZ:AV0Z40310501 Keywords : LA- ICP -MS * ICP -OES * LiF–NaF salts Subject RIV: CB - Analytical Chemistry, Separation Impact factor: 3.155, year: 2012

  17. Salpeterzuurdestructie en ICP-MS analyse van biotisch materiaal en voeding

    NARCIS (Netherlands)

    Velde-Koerts T van der; LAC

    2000-01-01

    Voor de bepaling van elementen in voeding en biotisch materiaal werd een analytische methode ontwikkeld, bestaande uit een salpeterzuurdestructie en een ICP-MS-analyse. De destructie werd geoptimaliseerd op basis van de salpeterzuurconcentratie en de destructietijd. De ICP-MS-analyse werd

  18. Multielement determination and speciation of major-to-ultratrace elements in green tea leaves by ICP-AES and ICP-MS

    International Nuclear Information System (INIS)

    Matsuura, Hirotaka; Hokura, Akiko; Haraguchi, Hiroki

    2000-01-01

    In order to investigate the multi-elemental composition of green tea leaves as well as chemical species in tea infusions, inductively coupled plasma atomic emission spectrometry (ICP-AES) and inductively coupled plasma mass spectrometry (ICP-MS) were used for elemental analysis and elemental speciation with the aid of size exclusion chromatography (SEC). As a result, the multielement determination of major-to-ultratrace elements in green tea leaves and green tea infusions was carried out by ICP-AES and ICP-MS. About 40 elements in these tea samples could be determined in a wide concentration range of over 8 orders of magnitude. The extraction efficiency of each element was estimated as the ratio of its concentration in tea infusion to that in tea leaves. It was found from the experimental results that the elements in tea leaves could be classified into three characteristic groups, depending on their extraction efficiencies. Furthermore, tea infusions were analyzed by a combined system of SEC, UV absorption detector, and ICP-AES (or ICP-MS) for the speciation of major-to-ultratrace elements. Most of the elements in tea infusions were found to be present as associated complexes with large organic molecules. (author)

  19. Determination of hafnium with the inductively coupled plasma (ICP)

    International Nuclear Information System (INIS)

    Wuensch, G.; Pose, K.

    1985-01-01

    The relative intensities of 198 hafnium lines in the Ar-ICP are listed. Spectral interference tables are given for the 9 analytically best lines, covering the range of +-60 pm around the Hf-lines. They include measured (not calculated) data of the interferent equivalent concentrations (IEC) and the critical concentration ratios (CCR) for 115 lines of all 34 possibly interfering elements. In many cases, these IEC- or CCR-data differ by 1 or 2 orders of magnitude from those calculated from intensities observed in the NBS-copper arc. Since no intense Hf-line is free from spectral interferences, examples are given for the calculation of the most suitable line for a known matrix. (orig.) [de

  20. Current role of ICP-MS in clinical toxicology and forensic toxicology: a metallic profile.

    Science.gov (United States)

    Goullé, Jean-Pierre; Saussereau, Elodie; Mahieu, Loïc; Guerbet, Michel

    2014-08-01

    As metal/metalloid exposure is inevitable owing to its omnipresence, it may exert toxicity in humans. Recent advances in metal/metalloid analysis have been made moving from flame atomic absorption spectrometry and electrothermal atomic absorption spectrometry to the multi-elemental inductively coupled plasma (ICP) techniques as ICP atomic emission spectrometry and ICP-MS. ICP-MS has now emerged as a major technique in inorganic analytical chemistry owing to its flexibility, high sensitivity and good reproducibility. This in depth review explores the ICP-MS metallic profile in human toxicology. It is now routinely used and of great importance, in clinical toxicology and forensic toxicology to explore biological matrices, specifically whole blood, plasma, urine, hair, nail, biopsy samples and tissues.

  1. Operational Experience with Radioactive Source Calibration of the CMS Hadron Endcap Calorimeter Wedges with Phase I Upgrade Electronics

    CERN Document Server

    Bilki, Burak

    2017-01-01

    The Phase I Upgrade of the CMS Hadron Endcap Calorimeters consist of new photodetectors (Silicon Photomultipliers in place of Hybrid Photo-Diodes) and front-end electronics (QIE11). The upgrade will allow the elimination of the high amplitude noise and drifting response of the Hybrid Photo-Diodes, at the same time enabling the mitigation of the radiation damage of the scintillators and the wavelength shifting fibers with a larger spectral acceptance of the Silicon Photomultipliers. The upgrade will also allow to increase the longitudinal segmentation of the readout to be beneficial for pile-up mitigation and recalibration due to depth-dependent radiation damage.As a realistic operational exercise, the responses of the Hadron Endcap Calorimeter wedges are being calibrated with a $^{60}$Co radioactive source both with current and upgrade electronics. The exercise will provide a manifestation of the benefits of the upgrade. Here we describe the instrumentation details and the operational experiences related to t...

  2. Analysis of source term aspects in the experiment Phebus FPT1 with the MELCOR and CFX codes

    Energy Technology Data Exchange (ETDEWEB)

    Martin-Fuertes, F. [Universidad Politecnica de Madrid, UPM, Nuclear Engineering Department, Jose Gutierrez Abascal 2, 28006 Madrid (Spain)]. E-mail: francisco.martinfuertes@upm.es; Barbero, R. [Universidad Politecnica de Madrid, UPM, Nuclear Engineering Department, Jose Gutierrez Abascal 2, 28006 Madrid (Spain); Martin-Valdepenas, J.M. [Universidad Politecnica de Madrid, UPM, Nuclear Engineering Department, Jose Gutierrez Abascal 2, 28006 Madrid (Spain); Jimenez, M.A. [Universidad Politecnica de Madrid, UPM, Nuclear Engineering Department, Jose Gutierrez Abascal 2, 28006 Madrid (Spain)

    2007-03-15

    Several aspects related to the source term in the Phebus FPT1 experiment have been analyzed with the help of MELCOR 1.8.5 and CFX 5.7 codes. Integral aspects covering circuit thermalhydraulics, fission product and structural material release, vapours and aerosol retention in the circuit and containment were studied with MELCOR, and the strong and weak points after comparison to experimental results are stated. Then, sensitivity calculations dealing with chemical speciation upon release, vertical line aerosol deposition and steam generator aerosol deposition were performed. Finally, detailed calculations concerning aerosol deposition in the steam generator tube are presented. They were obtained by means of an in-house code application, named COCOA, as well as with CFX computational fluid dynamics code, in which several models for aerosol deposition were implemented and tested, while the models themselves are discussed.

  3. A new atomic beam polarized ion source for the Triangle Universities Nuclear Laboratory: overview, operating experience, and performance

    International Nuclear Information System (INIS)

    Clegg, T.B.; Karwowski, H.J.; Lemieux, S.K.; Sayer, R.W.; Crosson, E.R.; Hooke, W.M.; Howell, C.R.; Lewis, H.W.; Lovette, A.W.; Pfutzner, H.J.; Sweeton, K.A.; Wilburn, W.S.

    1995-01-01

    A newly constructed source of polarized H ± and D ± ions is described. Atomic H or D beams from a dissociator with a cooled nozzle enter a system of two sextupole magnets and several radio-frequency transitions where they are focused and polarized. They enter a downstream electron-cyclotron-resonance-heated plasma ionizer from which positive ions are extracted. When negative ions are desired, they may be produced from the positive beam by charge-exchange in cesium vapor. Emerging beams are intense, have good polarization, low energy spread, and good optical quality. Descriptions are included for all major systems and for diagnostic procedures used to optimize both the intensity and the polarization of the output H ± or D ± beams obtained. Typical operating experience, performance figures, and a description of routine maintenance procedures are given. ((orig.))

  4. Adubação da batatinha experiências com leucita, sulfato e cloreto de potássio Fertilizer experiments with potatoes sources of potassium

    Directory of Open Access Journals (Sweden)

    O. J. Boock

    1960-01-01

    Full Text Available Neste trabalho são relatados os resultados obtidos em sete experiências de adubação da batatinha (Solanum tuberosum L., conduzidas em 1952-53 e 1953-54 em várias localidades do Estado de São Paulo, e nas quais foram comparadas três formas de potássio na presença de nitrogênio e fósforo. O efeito da adubação potássica foi praticamente nulo em três experiências. Em média das outras quatro a produção com NP foi de 6,66 t/ha e os aumentos provocados pela adição de 30, 60 e 90 kg/ha de K(20 foram respectivamente de 20, 23 e 27% com sulfato e cloreto de potássio aumentaram um pouco o tamanho dos tubérculos, ao passo que leucíta o diminuiu consideravelmente. A incidência de manchas internas ("chocolate" nos tubérculos não foi modificada pela adubação potássica.This paper presents the results obtained in seven experiments conducted in 1952-53 and 1953-54 at various localities of the State of São Paulo, in which three sources of potassium were tested in the presence of nitrogen and phosphorus. No response to potassium was observed in three of the experiments. Based on the average results from the other four trials the yield with NP was 6.66 tons per hectare and the increases due to additions of 30, 60 and 90 kilograms of K(20 per hectare were respectively of 20, 23 and 27% with sulphate of potassium and 12, 17 and 17% with potassium chloride; equal K(20 applications in the form of leucite did not modify the yields. While potassium sulphate and chloride incfeased a little the size of the tubers, leucite decreased it considerably. Potassium applications did not modify the incidence of internal brown spots.

  5. Maternal experiences with and sources of information on galactagogues to support lactation: a cross-sectional study

    Directory of Open Access Journals (Sweden)

    Bazzano AN

    2017-02-01

    Full Text Available Alessandra N Bazzano,1 Lauren Cenac,1 Amelia J Brandt,1 Josephine Barnett,2 Shelley Thibeau,3 Katherine P Theall1 1Department of Global Community Health and Behavioral Sciences, Tulane University School of Public Health and Tropical Medicine, New Orleans, LA, 2City University of New York, CUNY Graduate Center, New York, NY, 3Ochsner Clinic Foundation, New Orleans, LA, USA Abstract: An increase in the marketing and use of herbal galactagogues among breastfeeding mothers in the US has raised the issue of how best to provide support and information on the use of these products, particularly in light of limited availability of certified lactation counselors and continued suboptimal rates of breastfeeding globally. Currently, no cross-sectional data are available on the experiences and attitudes of mothers regarding the use of herbal and pharmaceutical galactagogues for lactation in the US. The findings of an online survey of 188 breastfeeding mothers on experiences with and sources of information on galactagogues are presented. Most mothers (76% reported that while breastfeeding, they felt as though they were not making enough milk to meet the needs of their child, and yet 54% also indicated that they had not supplemented with formula. A large proportion of respondents reported utilizing galactagogues to increase lactation and finding them useful. The results indicated that most women learned about galactagogues from the Internet or by word of mouth through friends. Lactation consultants were the third-most reported sources of information on these products. While many respondents reported perceiving galactagogues as innocuous, more evidence on safety and efficacy is needed to support women properly who seek out and use them. Large-scale studies of the prevalence of galactagogue use in the US and rigorous evaluation of use globally are needed to ensure that mothers who choose to breastfeed may safely avail themselves of all options when counseling

  6. Realization of radiobiological in vitro cell experiments at conventional X-ray tubes and unconventional radiation sources

    International Nuclear Information System (INIS)

    Beyreuther, Elke

    2010-01-01

    More than hundred years after the discovery of X-rays different kinds of ionizing radiation are ubiquitous in medicine, applied to clinical diagnostics and cancer treatment as well. Irrespective of their nature, the widespread application of radiation implies its precise dosimetric characterization and detailed knowledge of the radiobiological effects induced in cancerous and normal tissue. Starting with in vitro cell irradiation experiments, which define basic parameters for the subsequent tissue and animal studies, the whole multi-stage process is completed by clinical trials that translate the results of fundamental research into clinical application. In this context, the present dissertation focuses on the establishment of radiobiological in vitro cell experiments at unconventional, but clinical relevant radiation qualities. In the first part of the present work the energy dependent biological effectiveness of photons was studied examining low-energy X-rays (≤ 50 keV), as used for mammography, and high-energy photons (≥ 20 MeV) as proposed for future radiotherapy. Cell irradiation experiments have been performed at conventional X-ray tubes providing low-energy photons and 200 kV reference radiation as well. In parallel, unconventional quasi-monochromatic channeling X-rays and high-energy bremsstrahlung available at the radiation source ELBE of the Forschungszentrum Dresden-Rossendorf were considered for radiobiological experimentation. For their precise dosimetric characterization dosimeters based on the thermally stimulated emission of exoelectrons and on radiochromic films were evaluated, whereas just the latter was found to be suitable for the determination of absolute doses and spatial dose distributions at cell position. Standard ionization chambers were deployed for the online control of cell irradiation experiments. Radiobiological effects were analyzed in human mammary epithelial cells on different subcellular levels revealing an increasing amount

  7. Realization of radiobiological in vitro cell experiments at conventional X-ray tubes and unconventional radiation sources

    Energy Technology Data Exchange (ETDEWEB)

    Beyreuther, Elke

    2010-09-10

    More than hundred years after the discovery of X-rays different kinds of ionizing radiation are ubiquitous in medicine, applied to clinical diagnostics and cancer treatment as well. Irrespective of their nature, the widespread application of radiation implies its precise dosimetric characterization and detailed knowledge of the radiobiological effects induced in cancerous and normal tissue. Starting with in vitro cell irradiation experiments, which define basic parameters for the subsequent tissue and animal studies, the whole multi-stage process is completed by clinical trials that translate the results of fundamental research into clinical application. In this context, the present dissertation focuses on the establishment of radiobiological in vitro cell experiments at unconventional, but clinical relevant radiation qualities. In the first part of the present work the energy dependent biological effectiveness of photons was studied examining low-energy X-rays (≤ 50 keV), as used for mammography, and high-energy photons (≥ 20 MeV) as proposed for future radiotherapy. Cell irradiation experiments have been performed at conventional X-ray tubes providing low-energy photons and 200 kV reference radiation as well. In parallel, unconventional quasi-monochromatic channeling X-rays and high-energy bremsstrahlung available at the radiation source ELBE of the Forschungszentrum Dresden-Rossendorf were considered for radiobiological experimentation. For their precise dosimetric characterization dosimeters based on the thermally stimulated emission of exoelectrons and on radiochromic films were evaluated, whereas just the latter was found to be suitable for the determination of absolute doses and spatial dose distributions at cell position. Standard ionization chambers were deployed for the online control of cell irradiation experiments. Radiobiological effects were analyzed in human mammary epithelial cells on different subcellular levels revealing an increasing amount

  8. Very high-energy {gamma}-ray observations of the Crab nebula and other potential sources with the GRAAL experiment

    Energy Technology Data Exchange (ETDEWEB)

    Arqueros, F.A.; Ballestrin, J.; Berenguel, M.; Borque, D.M.; Camacho, E.F.; Diaz, M.; Enriquez, R.; Gebauer, H.J.; Plaga, R.

    2001-07-01

    The Gamma Ray Astronomy at Almeria (GRAAL) experiment uses 63 heliostat-mirrors with a total mirror area of {approx}2500 m''2 from the CESA-1 field to collect Cherenkov light from air showers. The detector is located in a central solar tower and detects photon-induced showers with an energy threshold of 250{+-}110 GeV and an asymptotic effective detection area of about 15000 m''2. Data sets taken in the period September 1999-September 2000 in the direction of the Crab pulsar and the active galaxy 3C 454.3 were analysed for high energy {gamma}-ray emission. Evidence for {gamma}-ray flux from the Crab pulsar with an integral flux of 2.2{+-}0.4 (stat) ''1.9{sub 1}.5 (syst x 10''-9 cm''-2 s''-1) above threshold and a significance of 4.5 {sigma} in a total (usable) observing time of 7 hours and 10 minutes on source was found. No evidence for emission from the other sources was seen. The effect of the field-of-view restricted to the central part of a detected air shower on the lateral distribution and iming properties of Cherenkov light and their effect on an efficient {gamma}-hadron separation are discussed. (Author) 6 refs.

  9. Design, manufacture and factory testing of the Ion Source and Extraction Power Supplies for the SPIDER experiment

    International Nuclear Information System (INIS)

    Bigi, Marco; Rinaldi, Luigi; Simon, Muriel; Sita, Luca; Taddia, Giuseppe; Carrozza, Saverino; Decamps, Hans; Luchetta, Adriano; Meddour, Abdelraouf; Moressa, Modesto; Morri, Cristiano; Musile Tanzi, Antonio; Recchia, Mauro; Wagner, Uwe; Zamengo, Andrea; Toigo, Vanni

    2015-01-01

    Highlights: • 5 MVA ion source power supplies effectively integrated in 150 m"2 Faraday cage. • Load protection and performance requirements met of custom design high voltage power supplies. • 200 kW tetrode oscillator with 200 kHz frequency range successfully tested. - Abstract: The SPIDER experiment, currently under construction at the Neutral Beam Test Facility in Padua, Italy, is a full-size prototype of the ion source for the ITER Neutral Beam Injectors. The Ion Source and Extraction Power Supplies (ISEPS) for SPIDER are supplied by OCEM Energy Technology s.r.l. (OCEM) under a procurement contract with Fusion for Energy (F4E) covering also the units required for MITICA and ITER injectors. The detailed design of SPIDER ISEPS was finalized in 2011 and manufacture of most components completed by end 2013. The Factory Acceptance Tests took place early 2014. ISEPS, with an overall power rating of 5 MVA, form a heterogeneous set of items including solid state power converters and 1 MHz radiofrequency generators of 200 kW output power. The paper presents the main features of the detailed design developed by OCEM, focusing in particular on the high output voltage pulse step modulators, the high output current resonant converters, the radiofrequency generators by HIMMELWERK GmbH and the architecture and implementation of the complex control system. Details are given on non-standard factory tests verifying the insulation requirements specific to this application. Performance of ISEPS during the factory acceptance tests is described, with emphasis on demonstration of the load protection requirements, a crucial point for all neutral beam power supplies. Finally, key dates of SPIDER ISEPS installation and site testing schedule are provided.

  10. Premarital sexual experience and preferred sources of reproductive health information among young men in Kumbotso, northern Nigeria.

    Science.gov (United States)

    Iliyasu, Z; Zubairu, I; Abubakar, I S; Isa, S A; Galadanci, H S; Hadiza, S G; Babam Maryam, A; Babam-Maryam, A; Aliyu, M H; Muktar, H A

    2012-01-01

    Despite well known risks associated with unprotected premarital sex, this phenomenon has not been well explored among young men in rural northern Nigeria. We studied the predictors of premarital sex and preferred sources of sexual and reproductive health information among young unmarried men in Kumbotso, northern Nigeria. A cross section of 400 young men were interviewed using structured questionnaires with mostly closed ended questions. Of the 385 respondents, 39 (10.1%) were sexually experienced. Less than half of respondents (48.7%) used a condom at sexual debut, and an equal proportion reported having multiple sex partners. Only 41.0% of sexually experienced respondents reported subsequent consistent condom use Age (adjusted odds ratio [AOR] = 4.12; 95% confidence interval (CI): 2.24-5.20 and educational attainment [AOR = 3.57; 95% CI (1.49-9.10)] were significant predictors of sexual experience. The current versus preferred sources of sexual and reproductive health information included friends (51.3% vs. 93.3%), Islamic school teachers (41.0% vs. 72.7%) and school teachers (8.8% vs. 15.1%). Although the prevalence of premarital sex among young men in this community in northern Nigeria as low, those that did engage in such activity were likely to not use condoms and to have multiple partners. Preferred and trusted sources of information included peers and religious leaders. The findings in this study could be used to develop innovative strategies for reaching young men with accurate sexual and reproductive health information.

  11. Design, manufacture and factory testing of the Ion Source and Extraction Power Supplies for the SPIDER experiment

    Energy Technology Data Exchange (ETDEWEB)

    Bigi, Marco, E-mail: marco.bigi@igi.cnr.it [Consorzio RFX (CNR, ENEA, INFN, Università di Padova, Acciaierie Venete SpA), Corso Stati Uniti 4, 35127 Padova (Italy); Rinaldi, Luigi [OCEM Energy Technology, Via della Solidarietà 2/1, 40056 Valsamoggia (località Crespellano), Bologna (Italy); Simon, Muriel [Fusion for Energy, Josep Pla 2, 08019 Barcelona (Spain); Sita, Luca; Taddia, Giuseppe; Carrozza, Saverino [OCEM Energy Technology, Via della Solidarietà 2/1, 40056 Valsamoggia (località Crespellano), Bologna (Italy); Decamps, Hans [ITER Organization, Route de Vinon sur Verdon, 13115 Saint Paul lez Durance (France); Luchetta, Adriano [Consorzio RFX (CNR, ENEA, INFN, Università di Padova, Acciaierie Venete SpA), Corso Stati Uniti 4, 35127 Padova (Italy); Meddour, Abdelraouf [HIMMELWERK Hoch- und Mittelfrequenzanlagen GmbH, Jopestr. 10, 72072 Tübingen (Germany); Moressa, Modesto [Consorzio RFX (CNR, ENEA, INFN, Università di Padova, Acciaierie Venete SpA), Corso Stati Uniti 4, 35127 Padova (Italy); Morri, Cristiano; Musile Tanzi, Antonio [OCEM Energy Technology, Via della Solidarietà 2/1, 40056 Valsamoggia (località Crespellano), Bologna (Italy); Recchia, Mauro [Consorzio RFX (CNR, ENEA, INFN, Università di Padova, Acciaierie Venete SpA), Corso Stati Uniti 4, 35127 Padova (Italy); Wagner, Uwe [HIMMELWERK Hoch- und Mittelfrequenzanlagen GmbH, Jopestr. 10, 72072 Tübingen (Germany); Zamengo, Andrea; Toigo, Vanni [Consorzio RFX (CNR, ENEA, INFN, Università di Padova, Acciaierie Venete SpA), Corso Stati Uniti 4, 35127 Padova (Italy)

    2015-10-15

    Highlights: • 5 MVA ion source power supplies effectively integrated in 150 m{sup 2} Faraday cage. • Load protection and performance requirements met of custom design high voltage power supplies. • 200 kW tetrode oscillator with 200 kHz frequency range successfully tested. - Abstract: The SPIDER experiment, currently under construction at the Neutral Beam Test Facility in Padua, Italy, is a full-size prototype of the ion source for the ITER Neutral Beam Injectors. The Ion Source and Extraction Power Supplies (ISEPS) for SPIDER are supplied by OCEM Energy Technology s.r.l. (OCEM) under a procurement contract with Fusion for Energy (F4E) covering also the units required for MITICA and ITER injectors. The detailed design of SPIDER ISEPS was finalized in 2011 and manufacture of most components completed by end 2013. The Factory Acceptance Tests took place early 2014. ISEPS, with an overall power rating of 5 MVA, form a heterogeneous set of items including solid state power converters and 1 MHz radiofrequency generators of 200 kW output power. The paper presents the main features of the detailed design developed by OCEM, focusing in particular on the high output voltage pulse step modulators, the high output current resonant converters, the radiofrequency generators by HIMMELWERK GmbH and the architecture and implementation of the complex control system. Details are given on non-standard factory tests verifying the insulation requirements specific to this application. Performance of ISEPS during the factory acceptance tests is described, with emphasis on demonstration of the load protection requirements, a crucial point for all neutral beam power supplies. Finally, key dates of SPIDER ISEPS installation and site testing schedule are provided.

  12. The electron cyclotron resonance coupled to laser ion source for charge state enhancement experiment: production of high inensity ion beams by means of hybrid ion source

    Czech Academy of Sciences Publication Activity Database

    Gammino, S.; Torrisi, L.; Ciavola, G.; Andó, L.; Celona, L.; Manciagli, S.; Krása, Josef; Láska, Leoš; Pfeifer, Miroslav; Rohlena, Karel; Mazzasalma, A. M.; Gentile, C.; Picciotto, A.; Wolowski, J.; Woryna, E.; Badziak, J.; Parys, P.; Hitz, D.; Shirkov, G. D.

    2004-01-01

    Roč. 96, č. 5 (2004), s. 2961-2967 ISSN 0021-8979 Institutional research plan: CEZ:AV0Z1010921 Keywords : laser ion sources * ECR ion sources Subject RIV: BH - Optics, Masers, Lasers Impact factor: 2.255, year: 2004

  13. A comparison of food safety knowledge among restaurant managers, by source of training and experience, in Oklahoma County, Oklahoma.

    Science.gov (United States)

    Lynch, Robert A; Elledge, Brenda L; Griffith, Charles C; Boatright, Daniel T

    2003-09-01

    The annual incidence of illness related to food consumption continues to present a challenge to environmental health management. A significant fraction of cases have been attributed to consumption of food in restaurants, and as the number of meals eaten away from the home continues to rise, the potential for large-scale foodborne-disease outbreaks will continue to increase. Food handlers in retail establishments contribute to the incidence of foodborne disease; therefore, it is essential that workers and management staff have a thorough understanding of safe food practices. Since the training, certification, and experience of food service managers vary greatly, it is also likely that managers' knowledge base may differ. In the study reported here, restaurant managers were administered a survey designed to measure their understanding of basic food safety principles. The sources of training, certification, and experience were found to significantly affect the level of food safety knowledge; however, increased hours of training did not increase knowledge. In addition, the time lapsed since training did not significantly affect the level of knowledge.

  14. Inductively coupled plasma and ion sources: History and state-of-the-art

    International Nuclear Information System (INIS)

    Hopwood, J.

    1994-01-01

    Over 100 years ago Hittorf first generated an electrodeless ''ring'' discharge by electromagnetic induction and began a 40 year controversy as to the true physical origin of such a discharge. Even Tesla advocated that these plasmas were merely the result of large electrostatic potential differences rather than electric fields induced by high frequency currents. Through clever experiments using crude spark gaps and leyden jars, the inductive nature of the discharge was confirmed in the late 1920's by MacKinnon, thus supporting the theories and experiments of Sir J.J. Thomson, perhaps the most staunch advocate of the induction mechanism. Today the authors routinely exploit the intense plasmas which are generated by induction. In this talk, the characteristics of inductively coupled plasma (ICP) and ion sources will be reviewed and future applications of intense plasma sources will be discussed. The inductively coupled plasma is Joule heated at moderate gas pressures, but the electromagnetic field penetration of these dense plasmas is limited by the plasma skin depth, typically a few millimeters to a few centimeters. The induction plasma is thus edge heated, a fact that constrains uniformity over large areas if helical induction coils are used. Flat, spiral coils may be used to improve uniformity by driving the plasma using a planar geometry. Issues of dimensional and frequency scaling will be discussed as they apply to large diameter sources. Ion beams extracted from ICPs are used for many applications including space propulsion, high power neutral beams, and materials processing. Broad ion beam (∼10 cm) current densities in excess of 100 mA-cm 2 at 100 keV are obtained in pulsed mode operation. Recently, however, more consumer-oriented applications of less intense ICPs are emerging

  15. ICP-MS as advantageous analytical technique for the determination of long-lived /sup 99/Tc in the environment

    International Nuclear Information System (INIS)

    Ihsanullah

    1992-05-01

    Technetium (Tc) was the first artificially created by man and has no stable isotope. The most crucial technetium isotope environmentally /sup 99/Tc is a pure beta emitter with a half-life of 2.1 X 105 years. The main source of /sup 99/Tc to the environment is the disposal of liquid wastes from nuclear installations or during separation and recovery of spent nuclear fuels. Because of its long half life, high fission yield, mobility and current interest in the collective long term doses, it is necessary to establish a knowledge of the behavior of /sup 99/Tc in the environment for complete assessment of the impact of nuclear industry. Due to various analytical difficulties however, data on the behavior of Tc in the environment are limited. In the literature, many techniques are reported for the analysis of Tc. A very sensitive, precise and powerful technique is required which can be applied to environmental samples in order to gain information by obtaining more precise data to assess the impact of Tc releases on man. Attention has been focussed for this purpose on a new powerful technique i.e. inductively coupled plasma mass spectrometry (ICP-MS). This report has been directed towards the development of ICP-MS. The technique gives a very high sensitivity enabling long lived radionuclides including /sup 99/Tc to be measured directly down to pg ml-1 levels in solution. Because of its versatility ICP-MS is finding applications for trace multielement analysis and low detection limits in almost all fields. (author)

  16. Precise determination of Pb isotope ratios by simple double spike MC-ICP-MS technique without Tl addition

    Digital Repository Service at National Institute of Oceanography (India)

    Makishima, A.; Nath, B.N.; Nakamura, E.

    A double-spike multicollector ICP-MS (DS-MC-ICP-MS) technique for Pb isotope analysis without Tl addition is established and its analytical performance is examined in detail. This simple DS-MC-ICP-MS technique using 20 ng ml sup(-1) gave averages...

  17. Relative impact of key sources of systematic noise in Affymetrix and Illumina gene-expression microarray experiments

    Directory of Open Access Journals (Sweden)

    Kitchen Robert R

    2011-12-01

    Full Text Available Abstract Background Systematic processing noise, which includes batch effects, is very common in microarray experiments but is often ignored despite its potential to confound or compromise experimental results. Compromised results are most likely when re-analysing or integrating datasets from public repositories due to the different conditions under which each dataset is generated. To better understand the relative noise-contributions of various factors in experimental-design, we assessed several Illumina and Affymetrix datasets for technical variation between replicate hybridisations of Universal Human Reference (UHRR and individual or pooled breast-tumour RNA. Results A varying degree of systematic noise was observed in each of the datasets, however in all cases the relative amount of variation between standard control RNA replicates was found to be greatest at earlier points in the sample-preparation workflow. For example, 40.6% of the total variation in reported expressions were attributed to replicate extractions, compared to 13.9% due to amplification/labelling and 10.8% between replicate hybridisations. Deliberate probe-wise batch-correction methods were effective in reducing the magnitude of this variation, although the level of improvement was dependent on the sources of noise included in the model. Systematic noise introduced at the chip, run, and experiment levels of a combined Illumina dataset were found to be highly dependant upon the experimental design. Both UHRR and pools of RNA, which were derived from the samples of interest, modelled technical variation well although the pools were significantly better correlated (4% average improvement and better emulated the effects of systematic noise, over all probes, than the UHRRs. The effect of this noise was not uniform over all probes, with low GC-content probes found to be more vulnerable to batch variation than probes with a higher GC-content. Conclusions The magnitude of systematic

  18. Relative impact of key sources of systematic noise in Affymetrix and Illumina gene-expression microarray experiments.

    Science.gov (United States)

    Kitchen, Robert R; Sabine, Vicky S; Simen, Arthur A; Dixon, J Michael; Bartlett, John M S; Sims, Andrew H

    2011-12-01

    Systematic processing noise, which includes batch effects, is very common in microarray experiments but is often ignored despite its potential to confound or compromise experimental results. Compromised results are most likely when re-analysing or integrating datasets from public repositories due to the different conditions under which each dataset is generated. To better understand the relative noise-contributions of various factors in experimental-design, we assessed several Illumina and Affymetrix datasets for technical variation between replicate hybridisations of Universal Human Reference (UHRR) and individual or pooled breast-tumour RNA. A varying degree of systematic noise was observed in each of the datasets, however in all cases the relative amount of variation between standard control RNA replicates was found to be greatest at earlier points in the sample-preparation workflow. For example, 40.6% of the total variation in reported expressions were attributed to replicate extractions, compared to 13.9% due to amplification/labelling and 10.8% between replicate hybridisations. Deliberate probe-wise batch-correction methods were effective in reducing the magnitude of this variation, although the level of improvement was dependent on the sources of noise included in the model. Systematic noise introduced at the chip, run, and experiment levels of a combined Illumina dataset were found to be highly dependent upon the experimental design. Both UHRR and pools of RNA, which were derived from the samples of interest, modelled technical variation well although the pools were significantly better correlated (4% average improvement) and better emulated the effects of systematic noise, over all probes, than the UHRRs. The effect of this noise was not uniform over all probes, with low GC-content probes found to be more vulnerable to batch variation than probes with a higher GC-content. The magnitude of systematic processing noise in a microarray experiment is variable

  19. Intertidal Sandbar Welding as a Primary Source of Sediment for Dune Growth: Evidence from a Large Scale Field Experiment

    Science.gov (United States)

    Cohn, N.; Ruggiero, P.; de Vries, S.

    2016-12-01

    Dunes provide the first line of defense from elevated water levels in low-lying coastal systems, limiting potentially major flooding, economic damages, and loss of livelihood. Despite the well documented importance of healthy dunes, our predictive ability of dune growth, particularly following erosive storm events, remains poor - resulting in part from traditionally studying the wet and dry beach as separate entities. In fact, however, dune recovery and growth is closely tied to the subtidal morphology and the nearshore hydrodynamic conditions, necessitating treating the entire coastal zone from the shoreface to the backshore as an integrated system. In this context, to further improve our understanding of the physical processes allowing for beach and dune growth during fair weather conditions, a large field experiment, the Sandbar-aEolian Dune EXchange EXperiment, was performed in summer 2016 in southwestern Washington, USA. Measurements of nearshore and atmospheric hydrodynamics, in-situ sediment transport, and morphology change provide insight into the time and space scales of nearshore-beach-dune exchanges along a rapidly prograding stretch of coast over a 6 week period. As part of this experiment, the hypothesis that dune growth is limited by the welding of intertidal sandbars to the shoreline (Houser, 2009) was tested. Using laser particle counters, bed elevation sensors (sonar altimeters and Microsoft Kinect), continuously logging sediment traps, RGB and IR cameras, and repeat morphology surveys (terrestrial lidar, kite based structure from motion, and RTK GPS), spatial and temporal trends in aeolian sediment transport were assessed in relation to the synoptic onshore migration and welding of intertidal sandbars. Observations from this experiment demonstrate that (1) the intertidal zone is the primary source of sediment to the dunes during non-storm conditions, (2) rates of saltation increase during later stages of bar welding but equivalent wind conditions

  20. Comparison of GC-ICP-MS and HPLC-ICP-MS for species-specific isotope dilution analysis of tributyltin in sediment after accelerated solvent extraction

    International Nuclear Information System (INIS)

    Wahlen, Raimund; Wolff-Briche, Celine

    2003-01-01

    This study describes a direct comparison of GC and HPLC hyphenated to ICP-MS determination of tributyltin (TBT) in sediment by species-specific isotope dilution analysis (SS-IDMS). The certified reference sediment PACS-2 (NRC, Canada) and a candidate reference sediment (P-18/HIPA-1) were extracted using an accelerated solvent extraction (ASE) procedure. For comparison of GC and LC methods an older bottle of PACS-2 was used, whilst a fresh bottle was taken for demonstration of the accuracy of the methods. The data obtained show good agreement between both methods for both the PACS-2 sediment (LC-ICP-IDMS 828±87 ng g -1 TBT as Sn, GC-ICP-IDMS 848±39 ng g -1 TBT as Sn) and the P-18/ HIPA-1 sediment (LC-ICP-IDMS 78.0±9.7 ng g -1 TBT as Sn, GC-ICP-IDMS 79.2±3.8 ng g -1 TBT as Sn). The analysis by GC-ICP-IDMS offers a greater signal-to-noise ratio and hence a superior detection limit of 0.03 pg TBT as Sn, in the sediment extracts compared to HPLC-ICP-IDMS (3 pg TBT as Sn). A comparison of the uncertainties associated with both methods indicates superior precision of the GC approach. This is related to the better reproducibility of the peak integration, which affects the isotope ratio measurements used for IDMS. The accuracy of the ASE method combined with HPLC-ICP-IDMS was demonstrated during the international interlaboratory comparison P-18 organised by the Comite Consultatif pour la Quantite de Matiere (CCQM). The results obtained by GC-ICP-IDMS for a newly opened bottle of PACS-2 were 1087±77 ng g -1 Sn for DBT and 876±51 ng g -1 Sn for TBT (expanded uncertainties with a coverage factor of 2), which are in good agreement with the certified values of 1090±150 ng g -1 Sn and 980±130 ng g -1 Sn, respectively. (orig.)

  1. Sustaining an Online, Shared Community Resource for Models, Robust Open source Software Tools and Data for Volcanology - the Vhub Experience

    Science.gov (United States)

    Patra, A. K.; Valentine, G. A.; Bursik, M. I.; Connor, C.; Connor, L.; Jones, M.; Simakov, N.; Aghakhani, H.; Jones-Ivey, R.; Kosar, T.; Zhang, B.

    2015-12-01

    Over the last 5 years we have created a community collaboratory Vhub.org [Palma et al, J. App. Volc. 3:2 doi:10.1186/2191-5040-3-2] as a place to find volcanology-related resources, and a venue for users to disseminate tools, teaching resources, data, and an online platform to support collaborative efforts. As the community (current active users > 6000 from an estimated community of comparable size) embeds the tools in the collaboratory into educational and research workflows it became imperative to: a) redesign tools into robust, open source reusable software for online and offline usage/enhancement; b) share large datasets with remote collaborators and other users seamlessly with security; c) support complex workflows for uncertainty analysis, validation and verification and data assimilation with large data. The focus on tool development/redevelopment has been twofold - firstly to use best practices in software engineering and new hardware like multi-core and graphic processing units. Secondly we wish to enhance capabilities to support inverse modeling, uncertainty quantification using large ensembles and design of experiments, calibration, validation. Among software engineering practices we practice are open source facilitating community contributions, modularity and reusability. Our initial targets are four popular tools on Vhub - TITAN2D, TEPHRA2, PUFF and LAVA. Use of tools like these requires many observation driven data sets e.g. digital elevation models of topography, satellite imagery, field observations on deposits etc. These data are often maintained in private repositories that are privately shared by "sneaker-net". As a partial solution to this we tested mechanisms using irods software for online sharing of private data with public metadata and access limits. Finally, we adapted use of workflow engines (e.g. Pegasus) to support the complex data and computing workflows needed for usage like uncertainty quantification for hazard analysis using physical

  2. Results on the role of metastable Ar atoms in a 9-MHz high-power atmospheric ICP by using emission/absorption spectrometry

    International Nuclear Information System (INIS)

    Gunter, W.; Zeeman, P.B.; Visser, K.

    1984-01-01

    An investigation into the role of overpopulations of metastable argon levels as agents for causing non-local thermal equilibrium (LTE) in an inductively coupled plasma source (ICP), was carried out. Four argon transitions in the near infrared region were monitored through absorption measurements at two different observation heights in a 9-MHz high-power ICP. The lower states of the four transitions consist of two metastable (11.55 and 11.72 eV) and two radiating (11.62 and 11.83 eV) levels. Comparison of measured metastable level to radiating level absorbance ratios with calculated population ratios gave an indication whether overpopulations of certain levels existed. Results indicate no overpopulation of metastable states with respect to radiating states, arguing against their role as non-LTE mechanism agents. This conclusion is, however, preliminary, since the calculation of absolute population densities from absorbance measurements must still be carried out

  3. Determination of chemical form of iodine with IC-ICP-MS system and its application to the environmental samples

    International Nuclear Information System (INIS)

    Yoshida, S.; Katou, S.; Sekimoto, H.; Muramatsu, Y.

    2005-01-01

    Iodine-129 is one of the important radionuclides possibly released into the environment from nuclear weapons testing and from the nuclear facilities such as nuclear fuel reprocessing plants. Because of its long half-life (1.57 x 10 7 y), knowing its long-term behavior in the environment is a major concern. As I-129 is expected to act together with stable iodine (I-127) in the environment after long time, the biogeochemical cycling of stable iodine in the environment can be used for the reliable safety assessment of I-129. Chemical form is the one of the important factors controlling the 'iodine behavior in the environment. Iodide (I - ) and iodate (IO 3 - ) are known to be the major chemical form in the aqueous solution. However, the information on the chemical form of iodine in the environmental sample is limited because of lack of reliable analytical technique for trace level of iodine in the environment. In this study, the analytical system by using ion chromatograph (IC) followed by inductively coupled plasma mass spectrometry (ICP-MS) was developed for the separate determination of I - and IO 3 - in the aqueous solution. The IC with anion exchange column (EXCELPAK ICS-A23) was used for the separation of I - and IO 3 - with 30 mM (NH 4 ) 2 CO 3 as eluent. Separated iodine was determined with ICP-MS on line. with the detection limit 0.1 - 1 μg/L. The total iodine concentration was also measured by the direct determination with ICP-MS. The iodine in the several environmental samples such as irrigation water in paddy field was successfully determined with information of chemical form. In incubation experiment with flooded soil, the change of the chemical form of iodine in the soil solution with change of Eh was observed. Detailed data will be discussed in the presentation.

  4. Multielement determination of major-to-ultratrace elements in deep-seawater salts by ICP-AES and ICP-MS

    International Nuclear Information System (INIS)

    Sakai, Takeshi; Nakagawa, Koji; Nakajima, Hiroshi; Itoh, Akihide; Ji, Shan; Haraguchi, Hiroki

    2002-01-01

    Major-to-ultratrace elements in deep-seawater salts were determined by ICP-AES and ICP-MS, after they were separated into the water-soluble, acid-soluble, and insoluble particle components. Deep-seawater salts were prepared from seawater collected at 344 m deep near the off-shore of Cape Muroto in Kochi Prefecture. The major and minor elements in salts were determined by ICP-AES after appropriate dilution with pure water. Trace and ultratrace elements in the water-soluble and acid-soluble components were preconcentrated by a chelating resin preconcentration method. In addition, the major to-ultratrace elements in the insoluble particle component were determined by ICP-AES and ICP-MS, after acid-digestion using HNO 3 /HF/HClO 4 . As a result, 21-35 elements in deep-seawater salts could be determined over the wide concentration range. It was found that the elements, such as Al, V, Fe, Mn, Co, Cu, Zn, and rare earth elements, were more abundant in the acid-soluble component of deep-seawater salts, which may play some essential roles in physiological effectiveness for intake of salt. (author)

  5. Ultratrace analysis of {sup 129}I in sediments by ICP-MS with collision cell

    Energy Technology Data Exchange (ETDEWEB)

    Izmer, A.V.; Becker, J.S. [Research Center Juelich (Germany). Central Div. of Analytical Chemistry; Boulyga, S.F. [Mainz Univ. (Germany). Inst. for Inorganic Chemistry and Analytical Chemistry; Zoriy, M.V. [Research Center Juelich (Germany). Central Div. of Analytical Chemistry]|[Research Center Juelich (Germany). Dept. for Safety and Radiation Protection

    2004-07-01

    The aim of the work was the development of a rapid and high-sensitive analytical method using ICP-MS with hexapole collision cell (ICP-CC-MS) for the determination of low 129I+/127I+ isotope ratios in synthetic lab standards and environmental samples. A special direct sample introduction device for iodine extraction via the gas phase from solid environmental material coupled on-line to ICP-CC-QMS was developed. The detection limit for 129I+ determination in aqueous solution and soil samples via gas-phase extraction was determined to be of 0.8 pg/g and 30 pg/g, respectively. (orig.)

  6. Metal ion transport quantified by ICP-MS in intact cells

    Science.gov (United States)

    Figueroa, Julio A. Landero; Stiner, Cory A.; Radzyukevich, Tatiana L.; Heiny, Judith A.

    2016-01-01

    The use of ICP-MS to measure metal ion content in biological tissues offers a highly sensitive means to study metal-dependent physiological processes. Here we describe the application of ICP-MS to measure membrane transport of Rb and K ions by the Na,K-ATPase in mouse skeletal muscles and human red blood cells. The ICP-MS method provides greater precision and statistical power than possible with conventional tracer flux methods. The method is widely applicable to studies of other metal ion transporters and metal-dependent processes in a range of cell types and conditions. PMID:26838181

  7. Quality assurance of Vari-source high dose rate (HDR) brachytherapy- remote after loader and cost effectiveness of Vari-source HDR- brachytherapy: NORI, Islamabad experience

    International Nuclear Information System (INIS)

    Ahmad, N.; Mahmood, H.; Jafri, S.R.A.

    2004-01-01

    A quality control of Vari-Source high dose rate (HDR) remote after loading brachytherapy machine was carried out and the cost effectiveness of HDR brachytherapy machine was also evaluated considering the cost of ten Iridium-192 wire sources at Nuclear Medicine, Oncology and Radiotherapy Institute (NORI), Islamabad, Pakistan. A total number of 253 intracavitary insertions were done in 98 patients from October 1996 to May 2001. The results of the quality control tests performed during 1996 to 2001 were within the acceptable limits. The cost effectiveness of Vari-Source HDR brachytherapy machine was also evaluated. The average cost per patient was calculated as US$ 491. Small number of patients was treated as the machine was used for gynecologic malignancies only. The objective was to assess the quality control status of HDR brachytherapy machine on patient treatment day, source exchange day and periodic day (monthly basis). It was found that the cost per patient can be minimized if other type of cancer patients are also treated on Vari-Source HDR machine. (author)

  8. Validation of multigroup neutron cross sections and calculational methods for the advanced neutron source against the FOEHN critical experiments measurements

    International Nuclear Information System (INIS)

    Smith, L.A.; Gallmeier, F.X.; Gehin, J.C.

    1995-05-01

    The FOEHN critical experiment was analyzed to validate the use of multigroup cross sections and Oak Ridge National Laboratory neutronics computer codes in the design of the Advanced Neutron Source. The ANSL-V 99-group master cross section library was used for all the calculations. Three different critical configurations were evaluated using the multigroup KENO Monte Carlo transport code, the multigroup DORT discrete ordinates transport code, and the multigroup diffusion theory code VENTURE. The simple configuration consists of only the fuel and control elements with the heavy water reflector. The intermediate configuration includes boron endplates at the upper and lower edges of the fuel element. The complex configuration includes both the boron endplates and components in the reflector. Cross sections were processed using modules from the AMPX system. Both 99-group and 20-group cross sections were created and used in two-dimensional models of the FOEHN experiment. KENO calculations were performed using both 99-group and 20-group cross sections. The DORT and VENTURE calculations were performed using 20-group cross sections. Because the simple and intermediate configurations are azimuthally symmetric, these configurations can be explicitly modeled in R-Z geometry. Since the reflector components cannot be modeled explicitly using the current versions of these codes, three reflector component homogenization schemes were developed and evaluated for the complex configuration. Power density distributions were calculated with KENO using 99-group cross sections and with DORT and VENTURE using 20-group cross sections. The average differences between the measured values and the values calculated with the different computer codes range from 2.45 to 5.74%. The maximum differences between the measured and calculated thermal flux values for the simple and intermediate configurations are ∼ 13%, while the average differences are < 8%

  9. Environmental radioactivity research on the Fukushima Dai-ichi Nuclear Power Plant accident by ICP-MS

    International Nuclear Information System (INIS)

    Ohno, Takeshi; Muramatsu, Yasuyuki

    2015-01-01

    Inductively coupled plasma (ICP) is characterized by high ionization efficiency for almost all elements. Recently, a triple quadrupole ICP-MS (ICP-MS/MS) has been applied to the measurements of isotope ratios for ultra-low level radioisotopes. The ICP-MS/MS features an additional quadrupole mass filter situated in front of the octopole reaction cell and quadrupole mass filter, which allows only the analyte ion to enter the cell by rejecting all the other ions. In this manuscript, we review recent studies on environmental radioactivity in Fukushima achieved by ICP-MS/MS techniques. (author)

  10. Characterization of Elements Regulating the Nuclear-to-Cytoplasmic Translocation of ICP0 in Late Herpes Simplex Virus 1 Infection.

    Science.gov (United States)

    Samrat, Subodh Kumar; Ha, Binh L; Zheng, Yi; Gu, Haidong

    2018-01-15

    Infected cell protein 0 (ICP0) of herpes simplex virus 1 (HSV-1) is an immediate early protein containing a RING-type E3 ubiquitin ligase. It targets several host factors for proteasomal degradation and subsequently activates viral expression. ICP0 has a nuclear localization sequence and functions in the nucleus early during infection. However, later in infection, ICP0 is found solely in the cytoplasm. The molecular mechanism and biological function of the ICP0 nuclear-to-cytoplasmic translocation are not well understood. In this study, we sought to characterize elements important for this translocation. We found that (i) in human embryonic lung fibroblast (HEL) cells, ICP0 C-terminal residues 741 to 775 were necessary but not sufficient for the nuclear-to-cytoplasmic translocation; (ii) the loss of ICP0 E3 ubiquitin ligase activity, which led to defective viral replication in nonpermissive cells, also caused mutant ICP0 to be retained in the nucleus of HEL cells; (iii) in permissive U2OS cells, however, ICP0 lacking E3 ligase activity was translocated to the cytoplasm at a pace faster than that of wild-type ICP0, suggesting that nuclear retention of ICP0 occurs in an ICP0 E3 ligase-dependent manner; and (iv) the ICP0 C terminus and late viral proteins cooperate in order to overcome nuclear retention and stimulate ICP0 cytoplasmic translocation. Taken together, less ICP0 nuclear retention may contribute to the permissiveness of U2OS cells to HSV-1 in the absence of functional ICP0. IMPORTANCE A distinct characteristic for eukaryotes is the compartmentalization of cell metabolic pathways, which allows greater efficiency and specificity of cellular functions. ICP0 of HSV-1 is a multifunctional viral protein that travels through different compartments as infection progresses. Its main regulatory functions are carried out in the nucleus, but it is translocated to the cytoplasm late during HSV-1 infection. To understand the biological significance of cytoplasmic ICP0 in

  11. The application of LA-ICP-MS in the examination of the thin plating layers found in late Roman coins

    Energy Technology Data Exchange (ETDEWEB)

    Vlachou-Mogire, C. [Numismatic Museum, 12 El. Venizelou Avenue, 106 71 Athens (Greece)], E-mail: vlachou_mogire@yahoo.co.uk; Stern, B.; McDonnell, J.G. [Department of Archaeological Sciences, University of Bradford, Bradford BD7 1RD (United Kingdom)

    2007-12-15

    During the late Roman period the production of complex copper alloy (Cu-Sn-Pb-Ag) coins with a silvered surface, became common practice. Previous analyses of these coins did not solve key technological issues and in particular, the silvering process. Two methods have been suggested for the production of the thin plating layers in late Roman coins the dipping in molten silver chloride and the use of silvering pastes. However, there are questions about their use. More recent research showed that hot-dipping methods, such as the dipping in molten silver chloride, were not really suitable for mass production. Also, the earliest references to the use of silvering pastes dated to 17th century AD. A review of ancient sources and historic literature indicated silver amalgam plating as the possible method for the production of the plating in late Roman coins. Results derived from non-destructive LA-ICP-MS analysis have demonstrated, for the first time, the presence of Hg in the surface layers of these coins. The optimization of the method and the factors influenced the analyses results, are discussed. The examination of the coins by means of EPMA confirmed the ICP-MS results. The introduction of a new technique for the examination of plating layers, helped in the identification of amalgam silvering as the method used in the production of the coins.

  12. Detection of lead nanoparticles in game meat by single particle ICP-MS following use of lead-containing bullets.

    Science.gov (United States)

    Kollander, Barbro; Widemo, Fredrik; Ågren, Erik; Larsen, Erik H; Loeschner, Katrin

    2017-03-01

    This study investigated whether game meat may contain nanoparticles of lead from ammunition. Lead nanoparticles in the range 40 to 750 nm were detected by ICP-MS in single particle mode in game shot with lead-containing bullets. The median diameter of the detected nanoparticles was around 60 nm. The particle mass concentration ranged from 290 to 340 ng/g meat and the particle number concentrations from 27 to 50 million particles/g meat. The size limit of detection strongly depended on the level of dissolved lead and was in the range of 40 to 80 nm. In game meat sampled more than 10 cm away from the wound channel, no lead particles with a diameter larger than 40 nm were detected. In addition to dissolved lead in meat that originated from particulates, the presence of lead nano particles in game meat represents a hitherto unattended source of lead with a largely unknown toxicological impact to humans. Graphical Abstract Detection of lead nanoparticles in game meat by single particle ICP-MS following use of leadcontaining bullets.

  13. THE INTERPLANETARY NETWORK SUPPLEMENT TO THE BURST AND TRANSIENT SOURCE EXPERIMENT 5B CATALOG OF COSMIC GAMMA-RAY BURSTS

    International Nuclear Information System (INIS)

    Hurley, K.; Briggs, M. S.; Kippen, R. M.; Kouveliotou, C.; Fishman, G.; Meegan, C.; Cline, T.; Trombka, J.; McClanahan, T.; Boynton, W.; Starr, R.; McNutt, R.; Boer, M.

    2011-01-01

    We present Interplanetary Network localization information for 343 gamma-ray bursts observed by the Burst and Transient Source Experiment (BATSE) between the end of the 4th BATSE catalog and the end of the Compton Gamma-Ray Observatory (CGRO) mission, obtained by analyzing the arrival times of these bursts at the Ulysses, Near Earth Asteroid Rendezvous (NEAR), and CGRO spacecraft. For any given burst observed by CGRO and one other spacecraft, arrival time analysis (or t riangulation ) results in an annulus of possible arrival directions whose half-width varies between 11 arcsec and 21 0 , depending on the intensity, time history, and arrival direction of the burst, as well as the distance between the spacecraft. This annulus generally intersects the BATSE error circle, resulting in an average reduction of the area of a factor of 20. When all three spacecraft observe a burst, the result is an error box whose area varies between 1 and 48,000 arcmin 2 , resulting in an average reduction of the BATSE error circle area of a factor of 87.

  14. SLAC's Polarized Electron Source LaserSystem and Minimization of Helicity Correlations for the E-158 Parity Violation Experiment

    CERN Document Server

    Humensky, T

    2002-01-01

    SLAC E-158 is an experiment designed to make the first measurement of parity violation in Moeller scattering. E-158 will measure the right-left cross-section asymmetry, A sub L sub R sup M sup o sup e sup l sup l sup e sup r , in the elastic scattering of a 45-GeV polarized electron beam off unpolarized electrons in a liquid hydrogen target. E-158 plans to measure the expected Standard Model asymmetry of approx 10 sup - sup 7 to an accuracy of better than 10 sup - sup 8. To make this measurement, the polarized electron source requires for operation an intense circularly polarized laser beam and the ability to quickly switch between right- and left-helicity polarization states with minimal right-left helicity-correlated asymmetries in the resulting beam parameters (intensity, position, angle, spot size, and energy), sup b sup e sup a sup m A sub L sub R 's. This laser beam is produced by a unique SLAC-designed flashlamp-pumped Ti:Sapphire laser and is propagated through a carefully designed set of polarization...

  15. Potentials and Problems of Internet as a Source of Purchasing Information – Experiences and Attitudes of University Students in Croatia

    Directory of Open Access Journals (Sweden)

    Blaženka Knežević

    2014-06-01

    Full Text Available Gathering information online prior to offline purchase became the com - mon way of using Internet within student population. On the other hand, there are more and more Internet users and online shoppers at all Central European Countries. In the CEE region companies are searching the way how to approach students as a target group via their web sites. The purpose of this research was to explain (1 how student population in Croatia use Internet as a tool for gathering information on products and services and (2 to assess perceived problems and potential of Internet as a retail information source. The paper is based on a primary research – a survey on attitudes of Croatian students towards Internet and online shopping. Results are analyzed by using descriptive and inferential statistical method. Discussion of the results brings us to conclusions that there are statistically different attitudes among groups according to gender and according previous experience with the on-line shopping. For illustration: (a males and females differ in assortment that they are choosing and buying online, (b male students have a more positive attitude towards online shopping benefits than female students, and (c online shoppers have more positive attitudes towards security issues than non-online shoppers.

  16. OASYS (OrAnge SYnchrotron Suite): an open-source graphical environment for x-ray virtual experiments

    Science.gov (United States)

    Rebuffi, Luca; Sanchez del Rio, Manuel

    2017-08-01

    The evolution of the hardware platforms, the modernization of the software tools, the access to the codes of a large number of young people and the popularization of the open source software for scientific applications drove us to design OASYS (ORange SYnchrotron Suite), a completely new graphical environment for modelling X-ray experiments. The implemented software architecture allows to obtain not only an intuitive and very-easy-to-use graphical interface, but also provides high flexibility and rapidity for interactive simulations, making configuration changes to quickly compare multiple beamline configurations. Its purpose is to integrate in a synergetic way the most powerful calculation engines available. OASYS integrates different simulation strategies via the implementation of adequate simulation tools for X-ray Optics (e.g. ray tracing and wave optics packages). It provides a language to make them to communicate by sending and receiving encapsulated data. Python has been chosen as main programming language, because of its universality and popularity in scientific computing. The software Orange, developed at the University of Ljubljana (SLO), is the high level workflow engine that provides the interaction with the user and communication mechanisms.

  17. Synchronous Databus Network in ITER: Open source real-time network for the next nuclear fusion experiment

    International Nuclear Information System (INIS)

    Boncagni, L.; Centioli, C.; Iannone, F.; Neri, C.; Panella, M.; Pangione, L.; Riva, M.; Scappaticci, M.; Vitale, V.; Zaccarian, L.

    2008-01-01

    The next nuclear fusion experiment, ITER, is