Annealing effects on the microstructure and mechanical properties of hot-rolled 14Cr-ODS steel

Science.gov (United States)

Gao, R.; Zhang, T.; Ding, H. L.; Jiang, Y.; Wang, X. P.; Fang, Q. F.; Liu, C. S.

2015-10-01

The oxide dispersion strengthened ferritic steels with nominal composition (weight percent) of Fe-14Cr-2W-0.5Ti-0.06Si-0.2V-0.1Mn-0.05Ta-0.03C-0.3Y2O3 were fabricated by sol-gel method, mechanical alloying, and hot isostatic pressing techniques. The evolution of microstructure and mechanical properties of the hot-rolled specimens with heat treatment was investigated. Tensile strength and hardness of hot-rolled ODS steel are significantly enhanced due to the formation of mechanical twins and high density dislocations. Uniformly dispersed oxide particles (10-40 nm) and fine-grained structure (200-400 nm) are responsible for the superior mechanical properties of the hot-rolled specimen annealed between 650 °C and 850 °C. With further increasing annealing temperature, the grain size of the hot-rolled specimens increases while the size of oxide particles decreases, which leads to lower strength and hardness but better ductility. The tensile strength and total elongation of samples in the rolling direction are higher than those in the transverse direction after the same treatments owing to the grain anisotropy induced by the large mechanical deformation.

Forming of High-strength Steels Using a Hot-melt Dry Lubricant

DEFF Research Database (Denmark)

Hörnström, Sven-Erik; Karlsson, Erik; Olsson, Mikael

2008-01-01

during forming resulting in seizure of the tool/steel sheet contact and extensive scratching of the steel sheet surface. As a result, a number of concepts have been developed in order to reduce the tendency to galling in metal forming, including the development of new dry lubricants, new forming tool...... steel grades and improved surface engineering treatments such as the deposition of low friction CVD and PVD coatings. In the present study the performance of a hot-melt dry lubricant in the forming of hot and cold rolled and hot-dip galvanized high strength steel has been evaluated and compared...... with a conventional rust protection oil using four different tests methods, i.e. a strip reduction test, a bending under tension test, a stretch-forming test and a pin-on disc test. In the tests, two different cold work tool steels, a conventional steel grade and a nitrogen alloyed PM steel grade were evaluated...

Rietveld and impedance analysis of cold and hot rolled duplex and lean duplex steels for application in paper and pulp industry

Energy Technology Data Exchange (ETDEWEB)

Esteves, Luiza; Lins, Vanessa de Freitas Cunha, E-mail: luizaeq@yahoo.com.br [Universidade Federal de Minas Gerais (UFMG), Belo Horizonte, MG (Brazil). Departamento de Engenharia Quimica; Paiva, Paulo Renato Perdigao [Centro Federal de Educacao Tecnologica de Minas Gerais (CEFET), Belo Horizonte, MG (Brazil); Viana, Adolfo Kalergis do Nascimento [APERAM South America, Timoteo, MG (Brazil)

2017-01-15

In this study, X-Ray Diffraction (XRD) and Rietveld Refinement were performed to identify and quantify the ferrite and austenite phase of cold and hot rolled duplex stainless steels (UNS S31803) and lean duplex stainless steels (UNS S32304). Electrochemical impedance spectroscopy (EIS) was applied to evaluate the chemical behavior of duplex and lean duplex stainless steels in white, green, and black liquors of paper and pulp industry. Rietveld analysis results showed a higher austenite content than the standard limit for duplex steels in the hot rolled condition. The hot rolling condition plays a major role in improving corrosion resistance in white liquor mainly for the lean duplex steel. (author)

Rietveld and impedance analysis of cold and hot rolled duplex and lean duplex steels for application in paper and pulp industry

International Nuclear Information System (INIS)

Esteves, Luiza; Lins, Vanessa de Freitas Cunha; Viana, Adolfo Kalergis do Nascimento

2017-01-01

In this study, X-Ray Diffraction (XRD) and Rietveld Refinement were performed to identify and quantify the ferrite and austenite phase of cold and hot rolled duplex stainless steels (UNS S31803) and lean duplex stainless steels (UNS S32304). Electrochemical impedance spectroscopy (EIS) was applied to evaluate the chemical behavior of duplex and lean duplex stainless steels in white, green, and black liquors of paper and pulp industry. Rietveld analysis results showed a higher austenite content than the standard limit for duplex steels in the hot rolled condition. The hot rolling condition plays a major role in improving corrosion resistance in white liquor mainly for the lean duplex steel. (author)

Effects of Changing Hot Rolling Direction on Microstructure, Texture and Mechanical Properties of Cu-2.7Be Sheets

Science.gov (United States)

Zhu, Daibo; Liu, Chuming; Yu, Haijun; Han, Tan

2018-03-01

A hot rolling scheme (cross-rolling and unidirectional rolling) was adopted to process Cu-2.7Be sheets used as multiplier dynodes in photomultiplier. The effects of changing rolling direction on microstructure, texture and mechanical properties were studied by a combination of XRD, EBSD and TEM. It was found that higher copper-type texture and lower brass texture intensity were obtained in the ultimately cross-rolling (CR) sheet compared with the unidirectional rolling (UR) sheet.The EBSD results indicated that the grain orientation from mainly for UR sample turns to random for CR sample. Great enhancements in YS and UTS after unidirectional rolling were attributed to the massive and polygonal γ precipitates. The CR sample exhibited lower anisotropy, because of the increase of S and γ precipitates with spherical and tiny shape.

Microstructure and texture evolution of ultra-thin grain-oriented silicon steel sheet fabricated using strip casting and three-stage cold rolling method

Energy Technology Data Exchange (ETDEWEB)

Song, Hong-Yu; Liu, Hai-Tao, E-mail: liuht@ral.neu.edu.cn; Wang, Yin-Ping; Wang, Guo-Dong

2017-03-15

A 0.1 mm-thick grain-oriented silicon steel sheet was successfully produced using strip casting and three-stage cold rolling method. The microstructure, texture and inhibitor evolution during the processing was briefly analyzed. It was found that Goss texture was absent in the hot rolled sheet because of the lack of shear deformation. After normalizing, a large number of dispersed MnS precipitates with the size range of 15–90 nm were produced. During first cold rolling, dense shear bands were generated in the deformed ferrite grains, resulting in the intense Goss texture after first intermediate annealing. The microstructure was further refined and homogenized during the subsequent cold rolling and annealing processes. After primary recrystallization annealing, a homogeneous microstructure consisting of fine and equiaxed grains was produced while the associated texture was characterized by a strong γ-fiber texture. Finally, a complete secondary recrystallization microstructure consisting of entirely large Goss grains was produced. The magnetic induction B{sub 8} and iron loss P{sub 10/400} was 1.79 T and 6.9 W/kg, respectively. - Highlights: • Ultra-thin grain-oriented silicon steel was produced by strip casting process. • Microstructure, texture and inhibitor evolution was briefly investigated. • Goss texture was absent in primary recrystallization annealed sheet. • MnS precipitates with a size range of 15–90 nm formed after normalizing. • A complete secondary recrystallization microstructure was produced.

Annealing effects on the microstructure and mechanical properties of hot-rolled 14Cr-ODS steel

International Nuclear Information System (INIS)

Gao, R.; Zhang, T.; Ding, H.L.; Jiang, Y.; Wang, X.P.; Fang, Q.F.; Liu, C.S.

2015-01-01

The oxide dispersion strengthened ferritic steels with nominal composition (weight percent) of Fe–14Cr–2W-0.5Ti-0.06Si-0.2V-0.1Mn-0.05Ta-0.03C-0.3Y_2O_3 were fabricated by sol–gel method, mechanical alloying, and hot isostatic pressing techniques. The evolution of microstructure and mechanical properties of the hot-rolled specimens with heat treatment was investigated. Tensile strength and hardness of hot-rolled ODS steel are significantly enhanced due to the formation of mechanical twins and high density dislocations. Uniformly dispersed oxide particles (10–40 nm) and fine-grained structure (200–400 nm) are responsible for the superior mechanical properties of the hot-rolled specimen annealed between 650 °C and 850 °C. With further increasing annealing temperature, the grain size of the hot-rolled specimens increases while the size of oxide particles decreases, which leads to lower strength and hardness but better ductility. The tensile strength and total elongation of samples in the rolling direction are higher than those in the transverse direction after the same treatments owing to the grain anisotropy induced by the large mechanical deformation.

Hot forging of roll-cast high aluminum content magnesium alloys

Science.gov (United States)

Kishi, Tomohiro; Watari, Hisaki; Suzuki, Mayumi; Haga, Toshio

2017-10-01

This paper reports on hot forging of high aluminum content magnesium alloy sheets manufactured using horizontal twin-roll casting. AZ111 and AZ131 were applied for twin-roll casting, and a hot-forging test was performed to manufacture high-strength magnesium alloy components economically. For twin-roll casting, the casting conditions of a thick sheet for hot forging were investigated. It was found that twin-roll casting of a 10mm-thick magnesium alloy sheet was possible at a roll speed of 2.5m/min. The grain size of the cast strip was 50 to 70µm. In the hot-forging test, blank material was obtained from as-cast strip. A servo press machine with a servo die cushion was used to investigate appropriate forging conditions (e.g., temperature, forging load, and back pressure) for twin-roll casts (TRCs) AZ111 and AZ131. It was determined that high aluminum content magnesium alloy sheets manufactured using twin-roll casting could be forged with a forging load of 150t and a back pressure of 3t at 420 to 430°C. Applying back pressure during hot forging effectively forged a pin-shaped product.

Numerical cooling strategy design for hot rolled dual phase steel

Energy Technology Data Exchange (ETDEWEB)

Suwanpinij, Piyada; Prahl, Ulrich; Bleck, Wolfgang [RWTH Aachen (DE). Dept. of Ferrous Metallurgy (IEHK); Togobytska, Nataliya; Weiss, Wolf; Hoemberg, Dietmar [Weierstrass-Institut fuer Angewandte Analysis und Stochastik (WIAS) im Forschungsverbund Berlin e.V. (Germany)

2010-10-21

In this article, the Mo-Mn dual phase steel and its process parameters in hot rolling are discussed. The process window was derived by combining the experimental work in a hot deformation dilatometer and numerical calculation of process parameters using rate law models for ferrite and martensite transformation. The ferrite formation model is based on the Leblond and Devaux approach while martensite formation is based on the Koistinen- Marburger (K-M) formula. The carbon enrichment during ferrite formation is taken into account for the following martensite formation. After the completion of the parameter identification for the rate law model, the evolution of phases in multiphase steel can be addressed. Particularly, the simulations allow for predicting the preferable degree of retained strain and holding temperature on the run out table (ROT) for the required ferrite fraction. (orig.)

Tribology and Tool Wear of Hot Dip Galvanized Zinc Magnesium Alloys on Cold Rolled Steel Sheets

International Nuclear Information System (INIS)

Raab, A. E.; Berger, E.; Freudenthaler, J.; Leomann, F.; Walch, C.

2011-01-01

Recently zinc based coatings on cold rolled steel with improved functionality in terms of forming and/or corrosion behaviour have been intensively investigated in the steel industry. One of the most promising products are zinc magnesium alloys produced in hot dip galvanizing process. These coatings were already introduced in construction industry a few years ago. With some modifications the improved properties of the coating are also interesting for automotive industry. In the present work the tribological potential of hot dip galvanized zinc magnesium coatings (HDG/ZM) produced at an industrial line under regular production, was studied in terms of sliding properties, adhesive and abrasive tool wear.First a short introduction into surface morphology of HDG/ZM will be given. For the tribological characterization of the material, which is the main topic of the contribution, different tests were performed on hot dip galvanised zinc magnesium material and results were compared with classic hot dip galvanized zinc coating (HDG/Z). The investigations are mainly based on the strip draw test which allows the determination of the friction coefficient directly by using a constant contact pressure. Deep drawing property was tested by forming model cups. The abrasive tool wear was tested using a standard test for material used in automotive industry. The adhesive tool wear was investigated by characterizing the coating material transferred to the tool in the strip draw test.All performed tests show an improved drawability of HDG/ZM compared to classical HDG/Z reference material. However the most promising difference between HDG/ZM and HDG/Z is that galling was found to be less for HDG/ZM than for HDG/Z. Therefore HDG/ZM is an interesting system not only with respect to corrosion protection but also in terms of tribology and provides clear advantages in formability.

Tribology and Tool Wear of Hot Dip Galvanized Zinc Magnesium Alloys on Cold Rolled Steel Sheets

Science.gov (United States)

Raab, A. E.; Berger, E.; Freudenthaler, J.; Leomann, F.; Walch, C.

2011-05-01

Recently zinc based coatings on cold rolled steel with improved functionality in terms of forming and/or corrosion behaviour have been intensively investigated in the steel industry1,2,3. One of the most promising products are zinc magnesium alloys produced in hot dip galvanizing process. These coatings were already introduced in construction industry a few years ago1. With some modifications the improved properties of the coating are also interesting for automotive industry. In the present work the tribological potential of hot dip galvanized zinc magnesium coatings (HDG/ZM) produced at an industrial line under regular production, was studied in terms of sliding properties, adhesive and abrasive tool wear. First a short introduction into surface morphology of HDG/ZM will be given. For the tribological characterization of the material, which is the main topic of the contribution, different tests were performed on hot dip galvanised zinc magnesium material and results were compared with classic hot dip galvanized zinc coating (HDG/Z). The investigations are mainly based on the strip draw test which allows the determination of the friction coefficient directly by using a constant contact pressure. Deep drawing property was tested by forming model cups. The abrasive tool wear was tested using a standard test for material used in automotive industry. The adhesive tool wear was investigated by characterizing the coating material transferred to the tool in the strip draw test. All performed tests show an improved drawability of HDG/ZM compared to classical HDG/Z reference material. However the most promising difference between HDG/ZM and HDG/Z is that galling was found to be less for HDG/ZM than for HDG/Z. Therefore HDG/ZM is an interesting system not only with respect to corrosion protection but also in terms of tribology and provides clear advantages in formability.

Characterizing the stretch-flangeability of hot rolled multiphase steels

International Nuclear Information System (INIS)

Pathak, N.; Butcher, C.; Worswick, M.; Gao, J.

2013-01-01

Hole expansion tests are commonly used to characterize the edge stretching limit of a material. Traditionally, a conical punch is used to expand a punched hole until a through-thickness crack appears. However, many automotive stretch flanging operations involve in-plane edge stretching that is best captured with a flat punch. In this paper, hole expansion tests were carried out on two different hot-rolled multiphase steels using both flat and conical punches. The fracture mechanisms for both punch types were investigated using scanning electron microscopy (SEM)

Multilayer Steel Materials Deformation Resistance and Roll Force Measurement

Directory of Open Access Journals (Sweden)

A. G. Kolesnikov

2014-01-01

Full Text Available To create new types of cars, raise their reliability, gain operational life, and decrease in metal consumption of products it is necessary to improve mechanical, physical, and also special properties of the constructional materials applied in mechanical engineering. Presently, there are intensive researches and developments under way to create materials with ultrafine-grained structure (the sizes of grains in their crystal lattice make less than 1 micron in one of the measurements.BMSTU developed a manufacturing technology of multilayer steel sheets with steady ultrafine-grained structure based on the multiple hot rolling of billet as a composition consisting of the alternating metal sheets. A principled condition for implementation of such technology is existence of different crystallographic modifications in the adjoining sheets of the composition at specified temperature of rolling.Power parameters of rolling are important technical characteristics of the process. Usually, to determine a deformation resistance value when rolling the diverse multilayer materials, is used the actual resistance value averaging in relation to the components of the composition. The aim of this work is a comparative analysis of known calculated dependences with experimental data when rolling the 100-layer samples. Objects of research were the 100-layer compositions based on the alternating layers of steel 08H18N10 and U8.Experimental samples represented the vacuumized capsules with height, width, and length of 53 mm x 53 mm x 200 mm, respectively, in which there were the 100-layer packs from sheets, each of 0.5 mm, based on the composition of steels (U8+08H18N10. Rolling was made on the double-high mill with rolls of 160 mm in diameter during 19 passes to the thickness of 7 mm with the speed of 0,1 m/s. Relative sinking in each pass was accepted to be equal 10±2,5%. Rolling forces were measured by the strain-gauging method using the measuring cells, located under

Development of high strength hot rolled low carbon copper-bearing steel containing nanometer sized carbides

Energy Technology Data Exchange (ETDEWEB)

Phaniraj, M.P. [High Temperature Energy Materials Research Center, Korea Institute of Science and Technology, Seoul 136-791 (Korea, Republic of); Shin, Young-Min [High Temperature Energy Materials Research Center, Korea Institute of Science and Technology, Seoul 136-791 (Korea, Republic of); Department of Materials Science and Engineering, Korea University, Seoul 136-701 (Korea, Republic of); Lee, Joonho [Department of Materials Science and Engineering, Korea University, Seoul 136-701 (Korea, Republic of); Goo, Nam Hoon [Sheet Product Design Group, Hyundai Steel Co., North Industrial Street 1400, 343-823, DangJin 343-823 (Korea, Republic of); Kim, Dong-Ik; Suh, Jin-Yoo; Jung, Woo-Sang [High Temperature Energy Materials Research Center, Korea Institute of Science and Technology, Seoul 136-791 (Korea, Republic of); Shim, Jae-Hyeok, E-mail: jhshim@kist.re.kr [High Temperature Energy Materials Research Center, Korea Institute of Science and Technology, Seoul 136-791 (Korea, Republic of); Choi, In-Suk, E-mail: insukchoi@kist.re.kr [High Temperature Energy Materials Research Center, Korea Institute of Science and Technology, Seoul 136-791 (Korea, Republic of)

2015-05-01

A low carbon ferritic steel was alloyed with Ti, Mo and Cu with the intention of achieving greater increment in strength by multiple precipitate strengthening. The steel is hot rolled and subjected to interrupted cooling to enable precipitation of Ti–Mo carbides and copper. Thermodynamic calculations were carried out to determine equilibrium phase fractions at different temperatures. Microstructure characterization using transmission electron microscopy and composition analysis revealed that the steel contains ~5 nm size precipitates of (Ti,Mo)C. Precipitation kinetics calculations using MatCalc software showed that mainly body centered cubic copper precipitates of size < 5nm form under the cooling conditions in the present study. The steel has the high tensile strength of 853 MPa and good ductility. The yield strength increases by 420 MPa, which is more than that achieved in hot rolled low carbon ferritic steels with only copper precipitates or only carbide precipitates. The precipitation and strengthening contribution of copper and (Ti,Mo)C precipitates and their effect on the work hardening behavior is discussed.

Effect of carbon content on microstructure and mechanical properties of hot-rolled low carbon 12Cr-Ni stainless steel

International Nuclear Information System (INIS)

Zheng, H.; Ye, X.N.; Li, J.D.; Jiang, L.Z.; Liu, Z.Y.; Wang, G.D.; Wang, B.S.

2010-01-01

Research highlights: → Hot-rolled ultra low carbon martensite is characterized by dislocation cells substructure. → The formation of dislocation cells is attributed to high Ms and low interstitial atoms content. → Hot-rolled ultra low carbon 12Cr-Ni stainless steel has excellent impact toughness. → Delta ferrite deteriorates the impact toughness of hot-rolled 12Cr-Ni stainless steel. - Abstract: 12Cr-Ni stainless steels containing different carbon contents from 0.004 wt.% to 0.034 wt.% were hot-rolled and air-cooled. Their corresponding microstructures were observed with optical microscope and transmission electron microscope, and the Vickers hardness, tensile and impact tests were also carried out. It was found that the martensitic morphology was significantly influenced by carbon content. The as-received ultra low carbon martensite in the steel containing 0.004 wt.% C is characterized by dislocation cells substructure. The formation of dislocation cells is attributed to high martensite finishing point (above 400 deg. C) and low interstitial atoms content. On the other hand, the martensite in the steel containing 0.034 wt.% C consists mainly of typical martensite laths because of low martensite finishing point and high interstitial atoms content which hinder dislocation motion. Furthermore, carbon content has an evident effect on the mechanical properties of 12Cr-Ni steels. The hardness and strength of the as-received steels increase with an increase in carbon content, but their elongation and impact toughness decrease with the carbon content. The steel containing 0.004 wt.% C has excellent impact toughness due to the ultra low carbon content in the martensite composed of dislocation cells.

78 FR 16252 - Certain Hot-Rolled Carbon Steel Flat Products From India, Indonesia, and Thailand: Final Results...

Science.gov (United States)

2013-03-14

... Indonesia P.T. Krakatau Steel 10.21 All Others 10.21 Thailand Sahaviriya Steel Industries Public Company...] Certain Hot-Rolled Carbon Steel Flat Products From India, Indonesia, and Thailand: Final Results of... products (``HR steel'') from India, Indonesia, and Thailand pursuant to section 751(c) of the Tariff Act of...

CO2 Laser Cutting of Hot Stamping Boron Steel Sheets

OpenAIRE

Pasquale Russo Spena

2017-01-01

This study investigates the quality of CO2 laser cutting of hot stamping boron steel sheets that are employed in the fabrication of automotive body-in-white. For this purpose, experimental laser cutting tests were conducted on 1.2 mm sheets at varying levels of laser power, cutting speed, and oxygen pressure. The resulting quality of cut edges was evaluated in terms of perpendicularity tolerance, surface irregularity, kerf width, heat affected zone, and dross extension. Experimental tests wer...

Manufacture of thin-walled clad tubes by pressure welding of roll bonded sheets

Science.gov (United States)

Schmidt, Hans Christian; Grydin, Olexandr; Stolbchenko, Mykhailo; Homberg, Werner; Schaper, Mirko

2017-10-01

Clad tubes are commonly manufactured by fusion welding of roll bonded metal sheets or, mechanically, by hydroforming. In this work, a new approach towards the manufacture of thin-walled tubes with an outer diameter to wall thickness ratio of about 12 is investigated, involving the pressure welding of hot roll bonded aluminium-steel strips. By preparing non-welded edges during the roll bonding process, the strips can be zip-folded and (cold) pressure welded together. This process routine could be used to manufacture clad tubes in a continuous process. In order to investigate the process, sample tube sections with a wall thickness of 2.1 mm were manufactured by U-and O-bending from hot roll bonded aluminium-stainless steel strips. The forming and welding were carried out in a temperature range between RT and 400°C. It was found that, with the given geometry, a pressure weld is established at temperatures starting above 100°C. The tensile tests yield a maximum bond strength at 340°C. Micrograph images show a consistent weld of the aluminium layer over the whole tube section.

Advanced cold rolled steels for automotive applications

Energy Technology Data Exchange (ETDEWEB)

Hofmann, Harald; Mattissen, Dorothea; Schaumann, Thomas Wilhelm [ThyssenKrupp Steel AG, Center of Materials Excellence, Dortmund (Germany)

2009-01-15

Advanced high-strength steels offer a great potential for the further development of automobile bodies-in-white due to their combined mechanical properties of high formability and strength. They represent the first choice in material selection for strength and crash-relevant parts with challenging geometries. The intensive development of multiphase steels by ThyssenKrupp Steel has led to hot dip galvanizing concepts with an outstanding forming potential. Hot rolled, hot dip galvanized complex-phase steels are currently produced in addition to cold rolled dual phase (DP) and retained austenite (RA) or transformation induced plasticity (TRIP) steels. New continuously annealed grades of steel are being developed with tensile strength levels of up to 1000 MPa in combination with sufficient ductility for the high demands of structural automobile components. These steels make use of the classic advantages of microalloying as well as the principles of DP steels and RA / TRIP steels. Further improvement of properties will be reached by the new class of high manganese alloyed steels. (orig.)

AISI/DOE Advanced Process Control Program Vol. 3 of 6: MICROSTRUCTURAL ENGINEERING IN HOT-STRIP MILLS Part 2 of 2: Constitutive Behavior Modeling of Steels Under Hot-Rolling Conditions; FINAL

International Nuclear Information System (INIS)

Yi-Wen Cheng; Patrick Purtscher

1999-01-01

This report describes the development of models for predicting (1) constitutive behaviors and (2) mechanical properties of hot-rolled steels as functions of chemical composition, microstructural features, and processing variables. The study includes the following eight steels: A36, DQSK, HSLA-V, HSLA-Nb, HSLA-50/Ti-Nb, and two interstitial-free (IF) grades. These developed models have been integrated into the Hot-Strip Mill Model (HSMM), which simulates the hot strip rolling mills and predicts the mechanical properties of hot-rolled products. The HSMM model has been developed by the University of British Columbia-Canada as a part of project on the microstructural engineering in hot-strip mills

Effect of Cooling Rate on the Microstructure and Mechanical Properties of C-Mn-Al-Si-Nb Hot-Rolled TRIP Steels

Science.gov (United States)

Fu, B.; Y Lu, M.; Y Yang, W.; Li, L. F.; Y Zhao, Z.

2017-12-01

A novel thermomechanical process to manufacture hot-rolled TRIP steels has been proposed based on dynamic transformation of undercooled austenite (DTUA). The cooling rate between DTUA and isothermal bainitic treatment in the novel process is important. In the present study, effect of this cooling rate on the final microstructures and mechanical properties of a C-Mn-Al-Si-Nb TRIP steel was investigated. The results showed that the volume fractions of acicular ferrite and retained austenite were increased with the increment of cooling rate. As a consequence, higher yield strength and larger total elongation were obtained for the investigated steel with higher cooling rate. In addition, a value of 30.24 GPa% for the product of tensile strength and total elongation was acquired when the cooling rate was 25 K/s. This value has met the standard of the “Third Generation” of advanced high strength sheet steels.

Promoting Ti{sub 4}C{sub 2}S{sub 2} strain induced precipitation during asymmetrical hot rolling to improve r value and advantaged texture in Ti stabilized IF steel

Energy Technology Data Exchange (ETDEWEB)

Dong, Futao, E-mail: dongft@sina.com [College of Metallurgy and Energy, Hebei United University, Tangshan 063000 (China); Xue, Fei [College of Electrical Engineering, Hebei United University, Tangshan 063000 (China); Du, Linxiu; Liu, Xianghua [The State Key Laboratory of Rolling and Automation, Northeastern University, Shenyang 110819 (China)

2015-01-25

Highlights: • We study Ti{sub 4}C{sub 2}S{sub 2} strain induced precipitation in Ti stabilized IF steel. • The PTT diagram is obtained by plotting 1/A{sub r}–time curves. • Hot rolling at the nose of P{sub s} line effectively promotes Ti{sub 4}C{sub 2}S{sub 2} precipitation. • Annealed sheet with promoted Ti{sub 4}C{sub 2}S{sub 2} exhibits higher r value and stronger γ fiber texture. • Adverse impact of tiny TiC has been significantly mitigated. - Abstract: The kinetic of Ti{sub 4}C{sub 2}S{sub 2} strain induced precipitation in a Ti stabilized IF steel was investigated using two stage interrupted compression test with high true strain (0.5). The PTT (precipitation–time–temperature) diagram was obtained by plotting 1/A{sub r}–time curves. TEM (transmission electron microscopy) observation confirmed that the evolution of Ti{sub 4}C{sub 2}S{sub 2} precipitate in the quenched samples of thermal simulation is in good agreement with the PTT diagram. Hot strips were produced at three different rolling temperatures with high strain and slight shear deformation. It was found that hot rolling at the nose temperature of the P{sub s} line of the PTT diagram can effectively promote the precipitation of Ti{sub 4}C{sub 2}S{sub 2} and retard the precipitation of TiC. Cold rolled and annealed sheets from hot strip containing higher volume fraction of Ti{sub 4}C{sub 2}S{sub 2} exhibited higher r value and stronger γ fiber texture with equal {1 1 1}〈1 1 2〉 and {1 1 1}〈1 1 0〉 components. By contrast, cold rolled and annealed sheets from hot strips containing lower volume fraction of Ti{sub 4}C{sub 2}S{sub 2} represented lower r values and weaker γ fiber texture with significant drops from {1 1 1}〈1 1 2〉 to {1 1 1}〈1 1 0〉 component.

Study of the influence between the strength of antibending of working rolls on the widening during hot rolling of thin sheet metal

Directory of Open Access Journals (Sweden)

U. Muhin

2016-07-01

Full Text Available Based on the variation principle of Jourdan was developed a mathematical model of the process of widening freely in hot rolling of thin sheet metal. The principle applies to rigid-plastic materials and for the cinematically admissible area of speeds. The developed model allows to study the distribution of the widening on the length of the deformation zone depending on the parameters of the rolling process and sheet metal. Results are obtained, characterizing the size of the widening and effectiveness of the process control on tension at the entrance and exit from the stand. The widening is dependent on the strength of anti bending.

The Role of Nano-TiO2 Lubricating Fluid on the Hot Rolled Surface and Metallographic Structure of SS41 Steel

Directory of Open Access Journals (Sweden)

Yanan Meng

2018-02-01

Full Text Available In this paper, nano-TiO2lubricating fluid was chosen as an advanced rolling lubricant to investigate its effect on the hot rolled surface and metallographic structure of SS41 steel strips. The tribological performances of nano-TiO2 lubricating fluid were measured by a four-ball tribotester. The hot rolling experiments under different lubrication conditions were carried out by a four-high rolling mill. The surface morphology, oxide scales and metallographic structure after hot rolling were observed using a confocal laser scanning microscope and scanning electron microscope (SEM, respectively. The composition of surface attachments was analyzed with X-ray photoelectron spectroscopy (XPS. The results indicate that the nano-TiO2 lubricating fluid has a better tribological performance. The surface defects on the hot rolled surface could be decreased. The phase composition of the surface still appears as a mixture of ferrite and pearlite. The surface of steel strips is not micro-alloyed with titanium as predicted. Additionally, the grain size of rolled steel strips which were lubricated with the nano-TiO2lubricating fluid decreased by nearly 50%, compared with traditional lubricating fluid. Furthermore, it was found that the thickness of the oxide layers on the surface reduced, whilst the Rockwell hardness of the oxide layers was enhanced as nano-TiO2 lubricating fluid was applied.

CO2 Laser Cutting of Hot Stamping Boron Steel Sheets

Directory of Open Access Journals (Sweden)

Pasquale Russo Spena

2017-10-01

Full Text Available This study investigates the quality of CO2 laser cutting of hot stamping boron steel sheets that are employed in the fabrication of automotive body-in-white. For this purpose, experimental laser cutting tests were conducted on 1.2 mm sheets at varying levels of laser power, cutting speed, and oxygen pressure. The resulting quality of cut edges was evaluated in terms of perpendicularity tolerance, surface irregularity, kerf width, heat affected zone, and dross extension. Experimental tests were based on a L9(34 orthogonal array design, with the effects of the process parameters on the quality responses being determined by means of a statistical analysis of variance (ANOVA. Quadratic mathematical models were developed to determine the relationships between the cutting parameters and the quality responses. Finally, a routine based on an optimization criterion was employed to predict the optimal setting of cutting factors and its effect on the quality responses. A confirmation experiment was conducted to verify the appropriateness of the optimization routine. The results show that all of the examined process parameters have a key role in determining the cut quality of hot stamping boron steel sheets, with cutting speed and their interactions having the most influencing effects. Particularly, interactions can have an opposite behavior for different levels of the process parameters.

Rolling induced size effects in elastic–viscoplastic sheet metals

DEFF Research Database (Denmark)

Nielsen, Kim Lau

2015-01-01

sheet rolling, where a non-homogeneous material deformation takes place between the rollers. Large strain gradients develop where the rollers first come in contact with the sheet, and a higher order plasticity model is employed to illustrate their influence at small scales. The study reveals...... presented revolves around the rolling induced effect of visco-plasticity (ranging hot and cold rolling) in combination with strain gradient hardening – including both dissipative and energetic contributions. To bring out first order effects on rolling at small scale, the modeling efforts are limited to flat...

78 FR 24435 - Hot-Rolled Steel Products From China, India, Indonesia, Taiwan, Thailand, and Ukraine

Science.gov (United States)

2013-04-25

... Ukraine Scheduling of full five-year reviews concerning the countervailing duty orders on hot-rolled steel... China, India, Indonesia, Taiwan, Thailand, and Ukraine. AGENCY: United States International Trade..., India, Indonesia, Taiwan, Thailand, and Ukraine would be likely to lead to continuation or recurrence of...

A Study of the Batch Annealing of Cold-Rolled HSLA Steels Containing Niobium or Titanium

Science.gov (United States)

Fang, Chao; Garcia, C. Isaac; Choi, Shi-Hoon; DeArdo, Anthony J.

2015-08-01

The batch annealing behavior of two cold-rolled, microalloyed HSLA steels has been studied in this program. One steel was microalloyed with niobium while the other with titanium. A successfully batch annealed steel will exhibit minimum variation in properties along the length of the coil, even though the inner and outer wraps experience faster heating and cooling rates and lower soaking temperatures, i.e., the so-called "cold spot" areas, than the mid-length portion of the coil, i.e., the so-called "hot spot" areas. The variation in strength and ductility is caused by differences in the extent of annealing in the different areas. It has been known for 30 years that titanium-bearing HSLA steels show more variability after batch annealing than do the niobium-bearing steels. One of the goals of this study was to try to explain this observation. In this study, the annealing kinetics of the surface and center layers of the cold-rolled sheet were compared. The surface and center layers of the niobium steel and the surface layer of the titanium steel all showed similar annealing kinetics, while the center layer of the titanium steel exhibited much slower kinetics. Metallographic results indicate that the stored energy of the cold-rolled condition, as revealed by grain center sub-grain boundary density, appeared to strongly influence the annealing kinetics. The kinetics were followed by the Kernel Average Misorientation reconstruction of the microstructure at different stages on annealing. Possible pinning effects caused by microalloy precipitates were also considered. Methods of improving uniformity and increasing kinetics, involving optimizing both hot-rolled and cold-rolled microstructure, are suggested.

76 FR 48143 - Certain Hot-Rolled Carbon Steel Flat Products From the People's Republic of China: Preliminary...

Science.gov (United States)

2011-08-08

..., 75 FR 81565 (December 28, 2010). \\3\\ Certain Oil Country Tubular Goods from the People's Republic of..., from Steven Hampton, International Trade Analyst, ``Certain Hot-Rolled Carbon Steel Flat Products from...

Medium carbon steel deep drawing: A study on the evolution of mechanical properties, texture and simulations, from cold rolling to the end product

Energy Technology Data Exchange (ETDEWEB)

Plaut, Ronald L. [University of Sao Paulo, Sao Paulo (Brazil)], E-mail: rlplaut@usp.br; Padilha, Angelo F. [University of Sao Paulo, Sao Paulo (Brazil); Lima, N.B. [IPEN-CNEN/SP, Sao Paulo (Brazil); Herrera, Clara [Max-Planck-Institut fuer Eisenforschung (Germany); Filho, Antenor Ferreira [Industrial Director, Brasmetal Waelzholz S/A, Diadema (Brazil); Yoshimura, Leandro H. [CCS Consulting, Sao Paulo (Brazil)

2009-01-15

Medium carbon steels are mostly used for simple applications; nevertheless new applications have been developed for which good sheet formability is required. This class of steels has an inherent low formability. A medium carbon hot rolled SAE 1050 steel has been selected for this study. It has been cold rolled with reductions in the 7-80% range. Samples have been used to assess the cold work hardening curve. For samples with a 50 and 80% thickness reduction, an annealing heat treatment has been performed to obtain recrystallization. The material has been characterized in the 'as received', cold rolled and annealed conditions, using several methods: optical microscopy, X-ray diffraction (texture), Vickers hardness and tensile testing. The 50% cold rolled and recrystallized material has been further studied in terms of sheet metal formability and texture evolution during the actual stamping of a steel toecap that has been used to validate the finite element simulations.

76 FR 31938 - Certain Hot-Rolled Carbon Steel Flat Products From India: Notice of Preliminary Results of 2009...

Science.gov (United States)

2011-06-02

... the File from Christopher Hargett, International Trade Compliance Analyst, through Melissa Skinner... Skinner, Office Director, concerning ``Certain Hot-Rolled Carbon Steel Flat Products from India: Customs...

76 FR 42679 - Certain Hot-Rolled Carbon Steel Flat Products From India: Final Results of Antidumping Duty...

Science.gov (United States)

2011-07-19

.... Steel''), Nucor Corporation (``Nucor''), and ArcelorMittal USA Inc. DATES: Effective Date: July 19, 2011..., 2011. We received briefs from U.S. Steel and Nucor and a rebuttal brief from Tata.\\5\\ On May 17, the... India, dated April 14, 2011; Letter from Nucor to the Department, regarding Certain Hot-Rolled Carbon...

Effect of Hot Rolling on the Microstructure and Mechanical Properties of Nitrogen Alloyed Austenitic Stainless Steel

Science.gov (United States)

Chenna Krishna, S.; Karthick, N. K.; Jha, Abhay K.; Pant, Bhanu; Cherian, Roy M.

2018-05-01

In the present investigation, the effect of multi-pass hot rolling in the temperature range of 700-1000 °C on the microstructure and mechanical properties of nitrogen alloyed austenitic stainless steel was studied with the aid of optical microscopy, tensile testing and x-ray diffraction measurements. The microstructural changes that occurred in the hot rolled specimens were elongation of grains in rolling direction, nucleation of new grains at the grain boundaries of elongated grains and growth of nucleated grains to form fully recrystallized grains. Elongated grains formed at lower rolling temperature (700-800 °C) due to inadequate strain/temperature for the initiation of dynamic recrystallization. At higher rolling temperature (900-1000 °C), fine grains formed due to dynamic recrystallization. Tensile properties showed strong dependency on the rolling temperature. Tensile strength increased with the decrease in the rolling temperature at the cost of ductility. Maximum strength was observed in samples hot rolled at 700 °C with yield strength of 917 MPa and ductility of 25%. This variation in the tensile properties with the rolling temperature is attributed to changes in the dislocation density and grain structure. The estimated yield strength from the dislocation density, solid solution and grain boundary strengthening closely matched with experimentally determined yield strength confirming the role of dislocation density and grain size in the strengthening.

Hot rolling of thick uranium molybdenum alloys

Science.gov (United States)

DeMint, Amy L.; Gooch, Jack G.

2015-11-17

Disclosed herein are processes for hot rolling billets of uranium that have been alloyed with about ten weight percent molybdenum to produce cold-rollable sheets that are about one hundred mils thick. In certain embodiments, the billets have a thickness of about 7/8 inch or greater. Disclosed processes typically involve a rolling schedule that includes a light rolling pass and at least one medium rolling pass. Processes may also include reheating the rolling stock and using one or more heavy rolling passes, and may include an annealing step.

Roll force prediction of high strength steel using foil rolling theory in cold skin pass rolling

International Nuclear Information System (INIS)

Song, Gil Ho; Jung, Jae Chook

2013-01-01

Skin pass rolling is a very important process for applying a certain elongation to a strip in the cold rolling and annealing processes, which play an important role in preventing the stretching of the yield point when the material is processed. The exact prediction of the rolling force is essential for obtaining a given elongation with the steel grade and strip size. Unlike hot rolling and cold rolling, skin pass rolling is used to apply an elongation of within 2% to the strip. Under a small reduction, it is difficult to predict the rolling force because the elastic deformation behavior of the rolls is complicated and a model for predicting the rolling force has not yet been established. Nevertheless, the exact prediction of the rolling force in skin pass rolling has gained increasing importance in recent times with the rapid development of high strength steels for use in automobiles. In this study, the possibility of predicting the rolling force in skin pass rolling for producing various steel grades was examined using foil rolling theory, which is known to have similar elastic deformation behavior of rolls in the roll bite. It was found that a noncircular arc model is more accurate than a circular model in predicting the roll force of high strength steel below TS 980 MPa in skin pass rolling

Effect of Annealing on Mechanical Properties and Formability of Cold Rolled Thin Sheets of Fe-P P/M Alloys

Science.gov (United States)

Trivedi, Shefali; Ravi Kumar, D.; Aravindan, S.

2016-10-01

Phosphorus in steel is known to increase strength and hardness and decrease ductility. Higher phosphorus content (more than 0.05%), however, promotes brittle behavior due to segregation of Fe3P along the grain boundaries which makes further mechanical working of these alloys difficult. In this work, thin sheets of Fe-P alloys (with phosphorus in range of 0.1-0.35%) have been developed through processing by powder metallurgy followed by hot rolling and cold rolling. The effect of phosphorus content and annealing parameters (temperature and time) on microstructure, mechanical properties, formability in biaxial stretching and fracture behavior of the cold rolled and annealed sheets has been studied. A comparison has also been made between the properties of the sheets made through P/M route and the conventional cast route with similar phosphorus content. It has been shown that thin sheets of Fe-P alloys with phosphorous up to 0.35% possessing a good combination of strength and formability can be produced through rolling of billets of these alloys made through powder metallurgy technique without the problem of segregation.

Hot rolling of chromium - nickel - manganese stainless steel containing nitrogen and boron

International Nuclear Information System (INIS)

Khorosh, V.A.; Bulat, S.I.; Mukhina, M.A.; Sorokina, N.A.; Yushchenko, K.A.; Tsentral'nyj Nauchno-Issledovatel'skij Inst. Chernoj Metallurgii, Moscow; AN Ukrainskoj SSR, Kiev. Inst. Ehlektrosvarki)

1976-01-01

The strength of stainless steel of the 03Kh2ON16AG6 type increases perceptibly with an increase in the nitrogen content from 0.11 to 0.37%. At the same time, however, its ductility in the region of hot deformation temperatures (red brittleness range of 800 to 1,000 deg C) decreases. Microalloying with boron (0.002 to 0.005% by calculation) permits enhancing the hot ductility to an acceptable level without adversely affecting the working properties. The mechaniusm of boron effect is analyzed. The temperature at which ingots are heated prior to rolling to achieve the desired effect must be sufficiently low. Optimum condition for two stage heating of 6.2-ton ingots are recommeded

78 FR 64008 - Hot-Rolled Steel Products From China, India, Indonesia, Taiwan, Thailand, and Ukraine; Revised...

Science.gov (United States)

2013-10-25

... INTERNATIONAL TRADE COMMISSION [Investigation Nos. 701-TA-405, 406, and 408 and 731-TA-899-901 and 906-908 (Second Review)] Hot-Rolled Steel Products From China, India, Indonesia, Taiwan, Thailand, and Ukraine; Revised Schedule for the Subject Five Year Reviews AGENCY: United States International Trade...

METHOD OF HOT ROLLING URANIUM METAL

Science.gov (United States)

Kaufmann, A.R.

1959-03-10

A method is given for quickly and efficiently hot rolling uranium metal in the upper part of the alpha phase temperature region to obtain sound bars and sheets possessing a good surface finish. The uranium metal billet is heated to a temperature in the range of 1000 deg F to 1220 deg F by immersion iii a molten lead bath. The heated billet is then passed through the rolls. The temperature is restored to the desired range between successive passes through the rolls, and the rolls are turned down approximately 0.050 inch between successive passes.

Investigation of Hot Rolling Influence on the Explosive-Welded Clad Plate

Directory of Open Access Journals (Sweden)

Guanghui ZHAO

2016-11-01

Full Text Available The microstructure, the shear strength and tensile strength of stainless steel explosive-welded clad plate at different rolling reduction were studied. The mechanical properties of the explosive-welded and explosive-rolled clad plates were experimentally measured. Simultaneously, the microstructures of the clad plate were investigated by the Ultra deep microscope and the tensile fracture surface were observed by the scan electron microscope (SEM. It was observed that the tensile strength has been increased considerably, whereas the elongation percentage has been reduced with the increase of hot rolling reduction. In the tensile shear test, the bond strength is higher than the strength of the ferritic stainless steel layer and meets the relevant known standard criterion. Microstructural evaluations showed that the grain of the stainless steel and steel refined with the increase of thickness reduction. Examination of the tensile fracture surfaces reveal that, after hot rolling, the fracture in the low alloy steel and ferritic stainless steel clad plates is of the ductile type.DOI: http://dx.doi.org/10.5755/j01.ms.22.4.12409

Development of dissimilar metal transition joint by hot bond rolling

International Nuclear Information System (INIS)

Kurokawa, Hiroyuki; Nakasuji, Kazuyuki; Kajimura, Haruhiko; Nagai, Takayuki; Takeda, Seiichiro.

1997-01-01

Metallurgically bonded transition joints which enable to connect reprocessing equipments made of superior corrosion resistant valve metals (Ti-5Ta, Zr or Ti) to stainless steel piping are required for nuclear fuel reprocessing plants. The authors have developed dissimilar transition joints made of stainless steel and Ti-5Ta, Zr or Ti with an insert metal of Ta by the hot bond rolling process of clad bars and clad pipes, using a newly developed mill called 'rotary reduction mill'. This report presents the manufacturing process of dissimilar transition joints produced from the clad pipe with three layers by the hot bond rolling. First, the method of hot bond rolling of clad pipe is proposed. Then, the mechanical and corrosion properties of the dissimilar transition joints are evaluated in detail by carrying out various tests. Finally, the rolling properties in the clad pipe method are discussed. (author)

Evaluation of factors affecting the edge formability of two hot rolled multiphase steels

Science.gov (United States)

Mukherjee, Monideepa; Tiwari, Sumit; Bhattacharya, Basudev

2018-02-01

In this study, the effect of various factors on the hole expansion ratio and hence on the edge formability of two hot rolled multiphase steels, one with a ferrite-martensite microstructure and the other with a ferrite-bainite microstructure, was investigated through systematic microstructural and mechanical characterization. The study revealed that the microstructure of the steels, which determines their strain hardening capacity and fracture resistance, is the principal factor controlling edge formability. The influence of other factors such as tensile strength, ductility, anisotropy, and thickness, though present, are secondary. A critical evaluation of the available empirical models for hole expansion ratio prediction is also presented.

Microstructure and Mechanical Properties of Fe-18Mn-18Cr-0.5N Austenitic Nonmagnetic Stainless Steel in Asymmetric Hot Rolling

Science.gov (United States)

Song, Y. L.; Li, C. S.; Ma, B.; Han, Y. H.

2017-05-01

Asymmetric hot rolling (ASHR) with a mismatch speed ratio of 1.15 in a single pass was applied to Fe-18Mn-18Cr-0.5N steel and was compared with symmetric hot rolling (SHR). The results indicated that a through-thickness microstructure gradient was formed in the plate due to the shear strain (0.36) introduced by ASHR. A fine-grained layer with the average size of 3 μm was achieved at the top surface of ASHR plate, while numerous elongated grains with a few recrystallized grains were presented at the center layer. The texture was distributed randomly at the top surface of ASHR plate, and a weaker intensity of typical hot-rolled texture in austenitic steel was obtained at the center layer of ASHR plate compared to SHR plate. An excellent combination of microhardness, strength and ductility was obtained in the ASHR plate, which was attributed to gradient microstructure induced by ASHR.

Mechanical properties and hot-rolled microstructures of a low carbon bainitic steel with Cu-P alloying

International Nuclear Information System (INIS)

Cui, W.F.; Zhang, S.X.; Jiang, Y.; Dong, J.; Liu, C.M.

2011-01-01

Highlights: → Mechanical properties and microstructures of low carbon bainite steel are examined. → Cu-P alloying promotes strengthening and uniform plastic deformation. → Cu-P alloying delays recovery process during rolling interval. → Lowering rolling temperature is favorable to increasing toughness. - Abstract: A low carbon bainitic steel with Cu-P alloying was developed. The new steel aims to meet the demand of high strength, high toughness and resistance to chloride ion corrosion for the components used in the environment of sea water and oceanic atmosphere. Mechanical properties of the steel were tested and strengthening and toughening mechanisms were analyzed by comparing hot-rolled microstructures of the low carbon bainitic steels with and without Cu-P alloying. The results show that Cu-P alloying provided strong solution strengthening with weak effect on ductility. The toughness loss caused by Cu-P alloying could be balanced by increasing the amount of martensite/remained austenite (M/A island) at lower finishing temperature. The static recovery process during rolling interval was delayed by the interaction of phosphorous, copper atoms with dislocations, which was favorable to the formation of bainitic plates. Super-fine Nb(C, N) particles precipitated on dislocations had coherency with bainite ferrite at 830 deg. C finishing temperature. Raising finishing temperature to 880 deg. C, Nb(C, N) particles were prone to coarsening and losing coherency. It was also found that no accurate lattice match relationship among retained austenite, martensite and bainite in granular bainitic microstructure.

Mechanical properties and hot-rolled microstructures of a low carbon bainitic steel with Cu-P alloying

Energy Technology Data Exchange (ETDEWEB)

Cui, W.F., E-mail: wenfangcui@yahoo.com.cn [Key Laboratory for Anisotropy and Texture of Materials (Ministry of Education), Northeastern University, Shenyang 110004 (China); Zhang, S.X. [Key Laboratory for Anisotropy and Texture of Materials (Ministry of Education), Northeastern University, Shenyang 110004 (China); Technology Center of Laiwu Iron and Steel (Group) Co. Ltd., Laiwu 271104 (China); Jiang, Y. [School of Chemical Engineering, University of Queensland, Brisbane 4072 (Australia); Dong, J. [Technology Center of Laiwu Iron and Steel (Group) Co. Ltd., Laiwu 271104 (China); Liu, C.M. [Key Laboratory for Anisotropy and Texture of Materials (Ministry of Education), Northeastern University, Shenyang 110004 (China)

2011-08-15

Highlights: {yields} Mechanical properties and microstructures of low carbon bainite steel are examined. {yields} Cu-P alloying promotes strengthening and uniform plastic deformation. {yields} Cu-P alloying delays recovery process during rolling interval. {yields} Lowering rolling temperature is favorable to increasing toughness. - Abstract: A low carbon bainitic steel with Cu-P alloying was developed. The new steel aims to meet the demand of high strength, high toughness and resistance to chloride ion corrosion for the components used in the environment of sea water and oceanic atmosphere. Mechanical properties of the steel were tested and strengthening and toughening mechanisms were analyzed by comparing hot-rolled microstructures of the low carbon bainitic steels with and without Cu-P alloying. The results show that Cu-P alloying provided strong solution strengthening with weak effect on ductility. The toughness loss caused by Cu-P alloying could be balanced by increasing the amount of martensite/remained austenite (M/A island) at lower finishing temperature. The static recovery process during rolling interval was delayed by the interaction of phosphorous, copper atoms with dislocations, which was favorable to the formation of bainitic plates. Super-fine Nb(C, N) particles precipitated on dislocations had coherency with bainite ferrite at 830 deg. C finishing temperature. Raising finishing temperature to 880 deg. C, Nb(C, N) particles were prone to coarsening and losing coherency. It was also found that no accurate lattice match relationship among retained austenite, martensite and bainite in granular bainitic microstructure.

Microstructural characterization and formation mechanism of abnormal segregation band of hot rolled ferrite/pearlite steel

Energy Technology Data Exchange (ETDEWEB)

Feng, Rui [School of Materials Science and Engineering, Shandong University, Jinan 250061 (China); Engineering Research Center of Large Size Alloy Structural Steel Bars of Shandong Province, Jinan 250061 (China); School of Materials Science and Engineering, Shandong University of Technology, Zibo 255049 (China); Li, Shengli, E-mail: lishengli@sdu.edu.cn [School of Materials Science and Engineering, Shandong University, Jinan 250061 (China); Engineering Research Center of Large Size Alloy Structural Steel Bars of Shandong Province, Jinan 250061 (China); Zhu, Xinde [School of Materials Science and Engineering, Shandong University, Jinan 250061 (China); Ao, Qing [School of Materials Science and Engineering, Shandong University, Jinan 250061 (China); Engineering Research Center of Large Size Alloy Structural Steel Bars of Shandong Province, Jinan 250061 (China)

2015-10-15

In order to further reveal the microstructural characterization and formation mechanism of abnormal segregation band of hot rolled ferrite/pearlite steel, the microstructure of this type steel was intensively studied with Scanning Auger Microprobe (SAM), etc. The results show that severe C–Mn segregation exists in the abnormal segregation band region at the center of hot rolled ferrite/pearlite steel, which results from the Mn segregation during solidification process of the continuous casting slab. The C–Mn segregation causes relative displacement of pearlite transformation curve and bainite transformation curve of C curve in the corresponding region, leading to bay-like shaped C curve. The bay-like shaped C curve creates conditions for the transformation from supercooling austenite to bainite at relatively lower cooling rate in this region. The Fe–Mn–C Atomic Segregation Zone (FASZ) caused by C–Mn segregation can powerfully retard the atomic motion, and increase the lattice reconstruction resistance of austenite transformation. These two factors provide thermodynamic and kinetic conditions for the bainite transformation, and result in the emergence of granular bainitic abnormal segregation band at the center of steel plate, which leads to lower plasticity and toughness of this region, and induces the layered fracture. - Highlights: • Scanning Auger Microprobe (SAM) is applied in the fracture analysis. • The abnormal segregation band region appears obvious C–Mn segregation. • The C–Mn segregation leads to bay-like shaped C curve. • The C–Mn segregation leads to Fe–Mn–C Atomic Segregation Zone.

Hot rolling and annealing effects on the microstructure and mechanical properties of ODS austenitic steel fabricated by electron beam selective melting

Science.gov (United States)

Gao, Rui; Ge, Wen-jun; Miao, Shu; Zhang, Tao; Wang, Xian-ping; Fang, Qian-feng

2016-03-01

The grain morphology, nano-oxide particles and mechanical properties of oxide dispersion strengthened (ODS)-316L austenitic steel synthesized by electron beam selective melting (EBSM) technique with different post-working processes, were explored in this study. The ODS-316L austenitic steel with superfine nano-sized oxide particles of 30-40 nm exhibits good tensile strength (412 MPa) and large total elongation (about 51%) due to the pinning effect of uniform distributed oxide particles on dislocations. After hot rolling, the specimen exhibits a higher tensile strength of 482 MPa, but the elongation decreases to 31.8% owing to the introduction of high-density dislocations. The subsequent heat treatment eliminates the grain defects induced by hot rolling and increases the randomly orientated grains, which further improves the strength and ductility of EBSM ODS-316L steel.

Effects of Niobium Microalloying on Microstructure and Properties of Hot-Dip Galvanized Sheet

Energy Technology Data Exchange (ETDEWEB)

Mohrbacher, Hardy [NiobelCon bvba, Brussels (Belgium)

2010-04-15

Niobium microalloying is effective in hot-rolled and cold-rolled steels by providing a fine-grained microstructure resulting in increased strength. To optimize the strengthening effect, alloy design and hot-rolling conditions have to be adapted. As a key issue the dissolution and precipitation characteristics of Nb are discussed in particular with regard to the run-out table conditions. It is then considered how the hot-rolled microstructure and the solute state of Nb interact with the hot-dip galvanizing cycle. The adjusted conditions allow controlling the morphology and distribution of phases in the cold-rolled annealed material. Additional precipitation hardening can be achieved as well. The derived options can be readily applied to produce conventional HSLA and IF high strength steels as well as to modem multiphase steels. It will be explained how important application properties such as strength, elongation, bendability, weldability and delayed cracking resistance can be influenced in a controlled and favorable way. Examples of practical relevance and experience are given.

Fabrication and properties of strip casting 4.5 wt% Si steel thin sheet

Energy Technology Data Exchange (ETDEWEB)

Zu, Guoqing, E-mail: gz854@uowmail.edu.au [State Key Laboratory of Rolling and Automation, Northeastern University, Shenyang 110819 (China); School of Mechanical, Materials and Mechatronic Engineering, University of Wollongong, NSW 2522 (Australia); Zhang, Xiaoming [State Key Laboratory of Rolling and Automation, Northeastern University, Shenyang 110819 (China); Zhao, Jingwei [School of Mechanical, Materials and Mechatronic Engineering, University of Wollongong, NSW 2522 (Australia); Wang, Yuqian [State Key Laboratory of Rolling and Automation, Northeastern University, Shenyang 110819 (China); Yan, Yi [School of Mechanical, Materials and Mechatronic Engineering, University of Wollongong, NSW 2522 (Australia); Li, Chengang; Cao, Guangming [State Key Laboratory of Rolling and Automation, Northeastern University, Shenyang 110819 (China); Jiang, Zhengyi [School of Mechanical, Materials and Mechatronic Engineering, University of Wollongong, NSW 2522 (Australia)

2017-02-15

Three 4.5 wt% Si steel thin sheets with different thicknesses were efficiently fabricated by twin-roll strip casting, warm rolling and cold rolling followed by final annealing. A comprehensive investigation from the workability of the as-cast strip to the magnetic property of the produces was performed to illustrate the superiority of the new materials. The results show that the as-cast strip, which has a much lower Vickers hardness than that of the 6.5 wt% Si steel, is suitable for rolling processing. The X-ray diffraction (XRD) and transmission electron microscopy (TEM) studies confirm that no ordering phase exists in the as-cast strip. The cold-rolled thin sheets exhibit good surface quality without edge cracks. Furthermore, all the three 4.5 wt% Si steel thin sheets possess relative strong <100>//ND texture and present high magnetic inductions and low iron losses after finial annealing. - Highlights: • 4.5 wt% Si as-cast sheet with excellent workability was produced by strip casting. • Three 4.5 wt% Si thin sheets were effectively fabricated by warm and cold rolling. • The microstructure and macro-texture of the thin sheets were elucidated. • High magnetic inductions and low iron losses were achieved simultaneously.

A novel ultra-low carbon grain oriented silicon steel produced by twin-roll strip casting

Energy Technology Data Exchange (ETDEWEB)

Wang, Yang, E-mail: wy069024019@163.com [State Key Laboratory of Rolling and Automation, Northeastern University, Shenyang 110819 (China); Zhang, Yuan-Xiang; Lu, Xiang; Fang, Feng; Xu, Yun-Bo; Cao, Guang-Ming; Li, Cheng-Gang [State Key Laboratory of Rolling and Automation, Northeastern University, Shenyang 110819 (China); Misra, R.D.K. [Laboratory for Excellence in Advanced Steel Research, Department of Metallurgical, Materials and Biomedical Engineering, University of Texas at El Paso, TX 79968 (United States); Wang, Guo-Dong [State Key Laboratory of Rolling and Automation, Northeastern University, Shenyang 110819 (China)

2016-12-01

A novel ultra-low carbon grain oriented silicon steel was successfully produced by strip casting and two-stage cold rolling method. The microstructure, texture and precipitate evolution under different first cold rolling reduction were investigated. It was shown that the as-cast strip was mainly composed of equiaxed grains and characterized by very weak Goss texture ({110}<001>) and λ-fiber (<001>//ND). The coarse sulfides of size ~100 nm were precipitated at grain boundaries during strip casting, while nitrides remained in solution in the as-cast strip and the fine AlN particles of size ~20–50 nm, which were used as grain growth inhibitors, were formed in intermediate annealed sheet after first cold rolling. In addition, the suitable Goss nuclei for secondary recrystallization were also formed during intermediate annealing, which is totally different from the conventional process that the Goss nuclei originated in the subsurface layer of the hot rolled sheet. Furthermore, the number of AlN inhibitors and the intensity of desirable Goss texture increased with increasing first cold rolling reduction. After secondary recrystallization annealing, very large grains of size ~10–40 mm were formed and the final magnetic induction, B{sub 8}, was as high as 1.9 T. - Highlights: • A novel chemical composition base on strip casting silicon steel was proposed. • The ultra-low carbon design could shorten the processing routes. • The novel composition and processes were beneficial to obtain more inhibitors. • The magnetic induction of grain oriented silicon steel was significantly improved.

IMPACT OF STRAIN RATE ON MICROALLOYED STEEL SHEET BREAKING

Directory of Open Access Journals (Sweden)

Mária Mihaliková

2014-08-01

Full Text Available Strain rate is a significant external factor and its influence on material behavior in forming process is a function of its internal structure. The contribution is analysis of the impact of loading rate from 1.6 x 10-4 ms-1 to 24 ms-1 to changes in the fracture of steel sheet used for bodywork components in cars. Experiments were performed on samples taken from HC420LA grade strips produced by cold rolling and hot dip galvanizing. Material strength properties were compared based on measured values, and changes to fracture surface character were observed.

Recent trend of titanium-clad steel plate/sheet (NKK)

International Nuclear Information System (INIS)

Kimura, Hideto

1997-01-01

The roll-bonding process for titanium-clad steel production enabled the on-line manufacturing and quality control of the products which are usually applied for the production of steel plate and sheet by the steel producers. The recent trend of roll-bonded titanium-clad steel which has an excellent corrosion resistance together with the advantage in cost-saving are mainly described in this article as to the demand, production technique and new application aspects. Though the predominant usage of titanium-clad steel plate has been in power-generating plants, enlargeing utilization in the chemical plants such as terephthalic acid production plants is leading the growth in the market of titanium-clad steel plate. Also, the application of titanium-clad steel plates and sheets for the lining the marine structures is expected as one of the best solution to long-term surface protection for their outstanding corrosion resistance against sea water. (author)

Magnetic properties and recrystallization texture of phosphorus-added non-oriented electrical steel sheets

International Nuclear Information System (INIS)

Tanaka, I.; Yashiki, H.

2006-01-01

The effect of phosphorus on magnetic properties and recrystallization texture has been investigated in non-oriented electrical steel sheets to develop low core loss and high permeability core materials. Specimens with different phosphorus contents were cold-rolled to various thicknesses, i.e. with various cold-rolling reductions, and annealed for recrystallization and grain growth. Although magnetic induction of the steel with low phosphorus content dramatically dropped with reducing thickness, i.e. with increasing in cold-rolling reduction, that of the steel with high phosphorus content only slightly decreased. The most effective way to reduce core loss was to reduce thickness of electrical steel sheets. Therefore, phosphorus-added thin gauge non-oriented electrical steel sheets have achieved low core loss and high permeability. The typical magnetic properties of phosphorus-added non-oriented electrical steel sheets 0.27mm in sheet thickness were 16.6W/kg in W 10/400 and 1.73T in B 50 . These excellent magnetic properties were due to the recrystallization texture control. {111} component in recrystallization texture was suppressed by the phosphorus segregation at initial grain boundaries. Accordingly, phosphorus would greatly contribute to the improvement of magnetic properties

Investigation of shinning Spot Defect on Hot-Dip Galvanized Steel Sheets

International Nuclear Information System (INIS)

Yonggang, Liu; Lei, Cui

2014-01-01

Shinning spot defects on galvanized steel sheets were studied by optical microscope, scanning electron microscope(SEM), Energy Dispersive Spectrometer (EDS) and Laser-Induced Breakdown Spectroscopy Original Position Statistic Distribution Analysis (LIBSOPA) in this study. The research shows that the coating thickness of shinning spot defects which caused by the substrate defect is much lower than normal area, and when skin passed, the shinning spot defect area can not touch with skin pass roll which result in the surface of shinning spot is flat while normal area is rough. The different coating morphologies have different effects on the reflection of light, which cause the shinning spot defects more brighter than normal area

Mechanical Properties of a Bainitic Steel Producible by Hot Rolling

Directory of Open Access Journals (Sweden)

Rana R.

2017-12-01

Full Text Available A carbide-free bainitic microstructure is suitable for achieving a combination of ultra high strength and high ductility. In this work, a steel containing nominally 0.34C-2Mn-1.5Si-1Cr (wt.% was produced via industrial hot rolling and laboratory heat treatments. The austenitization (900°C, 30 min. and austempering (300-400°C, 3 h treatments were done in salt bath furnaces. The austempering treatments were designed to approximately simulate the coiling step, following hot rolling and run-out-table cooling, when the bainitic transformation would take place and certain amount of austenite would be stabilized due to suppression of carbide precipitation. The microstructures and various mechanical properties (tensile properties, bendability, flangeability, and room and subzero temperature impact toughness relevant for applications were characterized. It was found that the mechanical properties were highly dependent on the stability of the retained austenite, presence of martensite in the microstructure and the size of the microstructural constituents. The highest amount of retained austenite (~ 27 wt.% was obtained in the sample austempered at 375°C but due to lower austenite stability and coarser overall microstructure, the sample exhibited lower tensile ductility, bendability, flangeability and impact toughness. The sample austempered at 400°C also showed poor properties due to the presence of initial martensite and coarse microstructure. The best combination of mechanical properties was achieved for the samples austempered at 325-350°C with a lower amount of retained austenite but with the highest mechanical stability.

Secondary recrystallization behavior in a twin-roll cast grain-oriented electrical steel

Energy Technology Data Exchange (ETDEWEB)

Song, Hong-Yu; Liu, Hai-Tao, E-mail: liuht@ral.neu.edu.cn; Wang, Yin-Ping; Wang, Guo-Dong

2017-04-15

The microstructure and texture evolution along the processing was investigated with a particular focus on the secondary recrystallization behavior in a 0.23 mm-thick twin-roll cast grain-oriented electrical steel. A striking feature is that Goss orientation originated during twin-roll casting as a result of shear deformation and it was further enhanced during hot rolling and normalizing. After primary recrystallization annealing, a homogeneous microstructure associated with a sharp γ-fiber texture was produced. During secondary recrystallization annealing, the γ-fiber texture was first strengthened and weakened with increasing temperature prior to the onset of secondary recrystallization. Goss grains always exhibited more 20–45° misoriented boundaries than the matrix. The matrix was quite stable during secondary recrystallization with the aid of dense inhibitors. Finally, a complete secondary recrystallization microstructure consisting of large Goss grains was produced. The grain boundary characteristics distribution indicated that the high energy model was responsible for the abnormal growth of Goss grains under the present conditions. - Highlights: • A 0.23 mm twin-roll cast grain-oriented silicon steel sheet was produced. • Goss orientation originated during twin-roll casting. • Secondary recrystallization behavior was briefly investigated. • γ-fiber texture was enhanced prior to the onset of secondary recrystallization. • A complete secondary recrystallization microstructure was produced.

Effect of Strength Coefficient of Bainite on Micromechanical Deformation and Failure Behaviors of Hot-Rolled 590FB Steel during Uniaxial Tension

Energy Technology Data Exchange (ETDEWEB)

Kim, Eun-Young; Choi, Shi-Hoon [Sunchon National University, Suncheon (Korea, Republic of); Kim, Sung Il [POSCO Technical Research Laboratories, Gwangyang (Korea, Republic of)

2016-11-15

The effect of the strength coefficient (K{sub B}) of bainite on micromechanical deformation and failure behaviors of a hot-rolled 590MPa steel (590FB) during uniaxial tension was simulated using the elasto-plastic finite element method (FEM). The spatial distribution of the constituent phases was obtained using a phase identification technique based on optical microstructure. Empirical equations which depend on chemical composition were used to determine the stress-strain relationship of the constituent phases of the 590FB steel. The stress-strain partitioning and failure behavior were analyzed by increasing the K{sub B} of bainite. The elasto-plastic FEM results revealed that effective strain in the ferrite-bainite boundaries, and maximum principal stress in fibrous bainite, were enhanced as the K{sub B} increased. The elasto-plastic FEM results also demonstrated that the K{sub B} significantly affects the micromechanical deformation and failure behaviors of the hot-rolled 590FB steel during uniaxial tension.

Surface conditioning of a cold-rolled dual-phase steel by annealing in nitriding atmospheres prior to hot-dip galvanizing

Energy Technology Data Exchange (ETDEWEB)

Luther, F.; Beste, D.; Bleck, W. [Institute for Ferrous Metallurgy (IEHK), RWTH Aachen (Germany); Dimyati, A.; Mayer, J. [Central Facility for Electron Microscopy (GFE), RWTH Aachen (Germany)

2007-04-15

The development of steel grades for automotive applications in the recent years has been driven on by two trends: lightweight and improved crash safety. By using steels like DP (dual phase) the goals of passenger safety, fuel efficiency and environmental friendliness can be met at reasonable price. The favorite corrosion protection method for sheet steels in the car industry is the hot-dip galvanizing process. Here, an approach was made to reduce the surface enrichment of critical alloying elements of a dual phase steel grade by reactive annealing in ammonia containing atmospheres. The effects of this treatment on mechanical properties and hot-dip coating behavior are reported. (Abstract Copyright [2007], Wiley Periodicals, Inc.)

Refinement of the microstructure of steel by cross rolling

International Nuclear Information System (INIS)

Tsay, Kira; Arbuz, Alexandr; Gusseynov, Nazim; Nemkaeva, Renata; Ospanov, Nurlan; Krupen'kin, Ivan

2016-01-01

One of the most effective ways for refinement of metal microstructure is a severe plastic deformation. The cross rolling is the one of most perspective methods of severe plastic deformation, because it allows to get the long billets, unlike equal angular pressing and other popular methods. This fact provides some industrial expectation for this method. However, deformation and motion path of the metal is very heterogeneous across the section of the rolled piece. This paper presents the finite element modeling of hot cross rolling of steel in the software package DEFORM-3D features implemented and studied the stress-strain state. An experimental study of the effect of the cross rolling on a three-roll mill on the microstructure of structural alloy steel and stainless steel AISI321 in different zones of the bar. Analysis of microsections made after rolling with high total stretch and the final pass temperature 700°C, shows the formation of equiaxial ultrafinegrain structure on the periphery of an elongated rod and “rolling” texture in the central zone. The resulting microstructure corresponds to that obtained in models of stress-strain state. Keywords: cross rolling, ultra-fine grain structure, steel.

Influence of cold rolling direction on texture, inhibitor and magnetic properties in strip-cast grain-oriented 3% silicon steel

Energy Technology Data Exchange (ETDEWEB)

Fang, F., E-mail: fangfengdbdx@163.com [State Key Laboratory of Rolling Technology and Automation, Northeastern University, Shenyang 110819 (China); Lu, X.; Zhang, Y.X.; Wang, Y.; Jiao, H.T.; Cao, G.M.; Yuan, G.; Xu, Y.B. [State Key Laboratory of Rolling Technology and Automation, Northeastern University, Shenyang 110819 (China); Misra, R.D.K. [Laboratory for Excellence in Advanced Steel Research, Department of Metallurgical, Materials and Biomedical Engineering, University of Texas at El Paso, EL Paso, TX 79968 (United States); Wang, G.D. [State Key Laboratory of Rolling Technology and Automation, Northeastern University, Shenyang 110819 (China)

2017-02-15

An unconventional cold rolling scheme (inclined rolling at 0°, 30°, 45°, 90° during second-stage cold rolling process) was adopted to process grain-oriented silicon steel based on strip casting process. The influences of inclination angles on microstructure, texture, inhibitor and magnetic properties were studied by a combination of EBSD, XRD and TEM. It was found that the α-fiber texture was weakened and γ-fiber was strengthened in cold rolled sheet with increase in inclination angle. The primary recrystallization sheet exhibited more homogeneous microstructure with relatively strong γ-fiber, medium α-fiber texture, weak λ-fiber texture and Goss component at high inclination angles. Fine and homogeneous inhibitors were obtained after primary annealing with increase in inclination angle from 0° to 90° because of more uniform deformation after inclined rolling. The grain-oriented silicon steel experienced completely secondary recrystallization at various inclination angles after final annealing process, with superior magnetic properties at 0° and 90°. Furthermore, Goss nuclei capable of final secondary recrystallization in strip casting process newly formed both in-grain shear bands and grain boundaries region during second-stage cold rolling and subsequent annealing process, which is different from the well-accepted results that Goss texture originated from the subsurface layer of the hot rolled sheet or during intermediate annealing process. In addition, the Goss texture that nucleated in-grain shear bands was weaker but more accurate as compared to that in grain boundaries region. - Highlights: • Inclined cold rolling was adopted to process strip-cast grain-oriented silicon steel. • Influence of inclination angles on texture, inhibitor and magnetic properties was studied. • The initial texture was changed with respect to the inclination angle. • Homogeneous inhibitors were obtained after primary annealing at various inclination angles. �

Evolution of the texture, mechanical properties, and microstructure of Cu-2.7Be alloys during hot cross-rolling

Energy Technology Data Exchange (ETDEWEB)

Zhu, Daibo; Liu, Chuming; Liu, Yadi; Gao, Yonghao; Jiang, Shunong [Central South University, School of Materials Science and Engineering, Changsha (China); Han, Tan [Suzhou Kinkou Copper Industry Limited Liability Company, Taicang (China)

2015-09-15

The evolution of the microstructure and texture of Cu-2.7Be alloys during hot rolling was investigated and related to the mechanical properties of the resulting sheets. Hot cross-rolling is shown to be an effective way to refine the hard and brittle secondary-phase particles in Cu-2.7Be alloys. The Cu- and brass-type textures increase and decrease in prevalence, respectively, during the rolling process. The yield strengths along the first and second rolling directions, and 45 to the former, are all enhanced because the corresponding Schmid factors decrease as the sheets are rolled thinner. The ductility anisotropy of the as-rolled sheets is related to the distribution and shape of the secondary-phase particles therein. (orig.)

Investigation of the structure dependence of diffusivity, solubility and permeability of hydrogen in hot-rolled low-carbon steels

Energy Technology Data Exchange (ETDEWEB)

Forcey, K S; Ross, D K [Birmingham Univ. (UK). Dept. of Physics; Iordanova, I A [Sofia Univ. (Bulgaria). Dept. of Solid State Physics

1989-01-01

A time-lag method for estimating the diffusivity, permeability and solubility of hydrogen in low-carbon hot-rolled steels has been applied. Oriani's model has been used to investigate and explain the effects of microstructure on the trapping of hydrogen. The results show that the initial microstructure of steel significantly affects the behaviour of hydrogen atoms. Of the three sites, namely: Dislocations, interstitial atoms and particles, the most effective traps seem to be interfaces between coarse particles and the matrix. (orig.).

Investigation of the structure dependence of diffusivity, solubility and permeability of hydrogen in hot-rolled low-carbon steels

International Nuclear Information System (INIS)

Forcey, K.S.; Ross, D.K.; Iordanova, I.A.

1989-01-01

A time-lag method for estimating the diffusivity, permeability and solubility of hydrogen in low-carbon hot-rolled steels has been applied. Oriani's model has been used to investigate and explain the effects of microstructure on the trapping of hydrogen. The results show that the initial microstructure of steel significantly affects the behaviour of hydrogen atoms. Of the three sites, namely: Dislocations, interstitial atoms and particles, the most effective traps seem to be interfaces between coarse particles and the matrix. (orig.)

Hot ductility of continuously cast structural steels

International Nuclear Information System (INIS)

Pytel, S.M.

1995-01-01

The objective of this investigation was to explain the hot ductility of the structural steels characterized by different amount of carbon and morphology of sulfides. Two different rolling processes were simulated under computer controlled, high temperature deformation MTS system. Results of this study show that morphology of sulfides as well as temperature and amount of deformation are responsible for level of hot ductility of the steel tested. (author)

In-Situ Characterization of Deformation and Fracture Behavior of Hot-Rolled Medium Manganese Lightweight Steel

Science.gov (United States)

Zhao, Zheng-zhi; Cao, Rong-hua; Liang, Ju-hua; Li, Feng; Li, Cheng; Yang, Shu-feng

2018-02-01

The deformation and fracture behavior of hot-rolled medium manganese lightweight (0.32C-3.85Mn-4.18Al-1.53Si) steel was revealed by an in situ tensile test. Deformed δ-ferrite with plenty of cross-parallel deformation bands during in situ tensile tests provides δ-ferrite of good plasticity and ductility, although it is finally featured by the cleavage fracture. The soft and ductile δ-ferrite and high-volume fraction of austenite contribute to the superior mechanical properties of medium manganese lightweight steel heated at 800°C, with a tensile strength of 924 MPa, total elongation of 35.2% and product of the strength and elongation of 32.5 GPa %.

Studies of the AA2519 Alloy Hot Rolling Process and Cladding with EN AW-1050A Alloy

Directory of Open Access Journals (Sweden)

Płonka B.

2016-03-01

Full Text Available The objective of the study was to determine the feasibility of plastic forming by hot rolling of the AA2519 aluminium alloy sheets and cladding these sheets with a layer of the EN AW-1050A alloy. Numerous hot-rolling tests were carried out on the slab ingots to define the parameters of the AA2519 alloy rolling process. It has been established that rolling of the AA2519 alloy should be carried out in the temperature range of 400-440°C. Depending on the required final thickness of the sheet metal, appropriate thickness of the EN AW-1050A alloy sheet, used as a cladding layer, was selected. As a next step, structure and mechanical properties of the resulting AA2519 alloy sheets clad with EN AW-1050A alloy was examined. The thickness of the coating layer was established at 0,3÷0,5mm. Studies covered alloy grain size and the core alloy-cladding material bond strength.

Closure behavior of spherical void in slab during hot rolling process

Science.gov (United States)

Cheng, Rong; Zhang, Jiongming; Wang, Bo

2018-04-01

The mechanical properties of steels are heavily deteriorated by voids. The influence of voids on the product quality should be eliminated through rolling processes. The study on the void closure during hot rolling processes is necessary. In present work, the closure behavior of voids at the center of a slab at 800 °C during hot rolling processes has been simulated with a 3D finite element model. The shape of the void and the plastic strain distribution of the slab are obtained by this model. The void decreases along the slab thickness direction and spreads along the rolling direction but hardly changes along the strip width direction. The relationship between closure behavior of voids and the plastic strain at the center of the slab is analyzed. The effects of rolling reduction, slab thickness and roller diameter on the closure behavior of voids are discussed. The larger reduction, thinner slab and larger roller diameter all improve the closure of voids during hot rolling processes. Experimental results of the closure behavior of a void in the slab during hot rolling process mostly agree with the simulation results..

Influence of hot rolling and high speed hydrostatic extrusion on the microstructure and mechanical properties of RAF ODS steel

International Nuclear Information System (INIS)

Oksiuta, Z.; Kurzydlowski, K.J.; Baluc, N.

2009-01-01

Argon gas atomized, pre-alloyed Fe-14Cr-2W-0.3Ti oxide dispersion strengthened (ODS) ferritic steel powder was mechanically alloyed with 0.3Y2O3 (wt.%) nano-particles in attritor ball mill and consolidated by hot isostatic pressing (HIP) at 1150 deg. C under pressure of 200 MPa for 3 hrs. To improve mechanical properties of as HIPped ODS ingots the material was undergone further thermo-mechanical treatment (TMT), namely: hot rolling (HR) at 850 deg. C or high speed hot extrusion (HSHE) at 850 deg. C. After TMT both materials were annealed at 1050 deg. C for 1 h in vacuum. Transmission electron microscopy (TEM) observations of the ODS alloys after TMT and heat treatment exhibited elongated in a longitudinal direction grains with an average size of 75 μm. However, an equiaxed, smaller than 500 nm grains were also found in the microstructure of both materials. Different size and morphology of oxides particles were also observed. Bigger, about 150 nm Ti-Al-O particles were usually located at grain boundaries whereas Y-Ti-O nanoclusters of about 5 nm were uniformly distributed in ODS steel matrix. The Charpy impact tests revealed significantly better about 90% (5.8 J) upper shelf energy (USE) of material after HSHE but ductile to brittle transition temperature (DBTT) of both alloys was unsatisfactory. As-HR ODS steel has shown DBTT of about 55 deg. C whereas HSHE ODS steel has about 75 deg. C. This relatively high values of transition temperature were probably caused by oxides particles present at grain boundaries of the ODS alloys which decreased fracture properties of the ODS steels. High temperature tensile properties of both ODS alloys are found to be satisfactory in full range of the testing temperature from 23 up to 750 deg. C. However, about 15% better UTS and YS0.2 (1350 MPa and 1285 MPa, respectively) as well as ductility were measured in the case of the as-HSHE ODS steel. These results indicates that HSHE process of the ODS steel can be considered as more

Examining the microtexture evolution in a hole-edge punched into 780 MPa grade hot-rolled steel

Energy Technology Data Exchange (ETDEWEB)

Shin, J.H.; Kim, M.S. [Department of Printed Electronics Engineering, Sunchon National University, 315 Maegok, Sunchon, Jeonnam 540-950 (Korea, Republic of); Kim, S.I.; Seo, S.J. [POSCO Technical Research Laboratories, Gwangyang 545-090 (Korea, Republic of); Choi, S.-H., E-mail: shihoon@sunchon.ac.kr [Department of Printed Electronics Engineering, Sunchon National University, 315 Maegok, Sunchon, Jeonnam 540-950 (Korea, Republic of)

2016-08-15

The deformation behavior in the hole-edge of 780 MPa grade hot-rolled steel during the punching process was investigated via microstructure characterization and computational simulation. Microstructure characterization was conducted to observe the edges of punched holes through the thickness direction, and electron back-scattered diffraction (EBSD) was used to analyze the heterogeneity of the deformation. Finite element analysis (FEA) that could account for a ductile fracture criterion was conducted to simulate the deformation and fracture behaviors of 780 MPa grade hot-rolled steel during the punching process. Calculation of rotation rate fields at the edges of the punched holes during the punching process revealed that metastable orientations in Euler space were confined to specific orientation groups. Rotation-rate fields effectively explained the stability of the initial texture components in the hole-edge region during the punching process. A visco-plastic self-consistent (VPSC) polycrystal model was used to calculate the microtexture evolution in the hole-edge region during the punching process. FEA revealed that the heterogeneous effective strain was closely related to the heterogeneity of the Kernel average misorientation (KAM) distribution in the hole-edge region. A simulation of the deformation microtexture evolution in the hole-edge region using a VPSC model was in good agreement with the experimental results. - Highlights: •We analyzed the microstructure in a hole-edge punched in HR 780HB steel. •Rotation rate fields revealed the stability of the initial texture components. •Heterogeneous effective stain was closely related to the KAM distribution. •VPSC model successfully simulated the deformation microtexture evolution.

Hot rolled composite billet for nuclear control rods

International Nuclear Information System (INIS)

Miller, G.E.

1976-01-01

This invention relates to a composite plate shaped billet, useful in the fabrication of nuclear control rods, which comprises a core of stainless steel containing about 2 percent boron 10, a thin coating of zirconia on the surfaces of said core, and said zirconia coating being completely encased in a jacket of mild steel, said composite having been hot rolled between about 1075 0 and about 1165 0 C. 1 claim, 8 figures

Research on the Microstructures and Mechanical Properties of Ti Micro-Alloyed Cold Rolled Hot-Dip Galvanizing DP980 Steel

Science.gov (United States)

Han, Yun; Kuang, Shuang; Qi, Xiumei; Xie, Chunqian; Liu, Guanghui

Effects of galvanizing simulation parameters on microstructures and mechanical properties of Ti-microalloyed cold rolled hot-dip galvanizing DP980 steel were investigated in this study by optical microscopy (OM), transmission electron microscopy (TEM), energy dispersive spectroscopy (EDS) and tensile test. Moreover, the precipitation behavior of Ti in the experimental steel was also studied. The results show that, as the heating temperature increases, the tensile strength of experimental galvanizing DP980 steel decreases while the yield ratio and elongation of the steel are enhanced. The microstructures of experimental steels exhibit typical dual phase steel character and the volume fractions of MA islands are almost 30%. In addition, lots of nano-sized TiC precipitates can be found in the ferrite grains.

Semi-solid twin-roll casting process of magnesium alloy sheets

International Nuclear Information System (INIS)

Watari, H.; Davey, K.; Rasgado, M.T. Alonso; Haga, T.; Koga, N.

2004-01-01

An experimental approach has been performed to ascertain the effectiveness of semi-solid strip casting using a horizontal twin roll caster. The demand for light-weight products with high strength has grown recently due to the rapid development of automobile and aircraft technology. One key to such development has been utilization of magnesium alloys, which can potentially reduce the total product weight. However, the problems of utilizing magnesium alloys are still mainly related to high manufacturing cost. One of the solutions to this problem is to develop magnesium casting-rolling technology in order to produce magnesium sheet products at competitive cost for commercial applications. In this experiment, magnesium alloy AZ31B was used to ascertain the effectiveness of semi-solid roll strip casting for producing magnesium alloy sheets. The temperature of the molten magnesium, and the roll speeds of the upper and lower rolls, (which could be changed independently), were varied to find an appropriate manufacturing condition. Rolling and heat treatment conditions were changed to examine which condition would be appropriate for producing wrought magnesium alloys with good formability. Microscopic observation of the crystals of the manufactured wrought magnesium alloys was performed. It has been found that a limiting drawing ratio of 2.7 was possible in a warm deep drawing test of the cast magnesium alloy sheets after being hot rolled

Influence of ring growth rate on damage development in hot ring rolling

NARCIS (Netherlands)

Wang, C.; Geijselaers, H. J.M.; Omerspahic, E.; Recina, V.; van den Boogaard, A. H.

2015-01-01

As an incremental forming process of bulk metal, ring rolling provides a cost effective process route to manufacture seamless rings. In the production of hot rolled rings, defects such as porosity can sometimes be found in high alloyed steel, manufactured from ingots having macro-segregation. For

Advanced cold rolled steels for automotive applications

Energy Technology Data Exchange (ETDEWEB)

Hofmann, H. [ThyssenKrupp Steel AG, Eberhardstrasse 12, 44145 Dortmund (Germany); Mattissen, D.; Schaumann, T.W. [ThyssenKrupp Steel AG, Duisburg (Germany)

2006-09-15

Advanced multiphase steels offer a great potential for bodies-in-white through their combination of formability and achievable component strength levels. They are first choice for strength and crash-relevant parts of challenging geometry. The intensive development of high-strength multiphase steels by ThyssenKrupp has led to hot dip galvanizing concepts with an outstanding forming potential. Hot rolled, hot dip galvanized complex phase steels are currently produced in addition to cold rolled DP and RA steels. New continuously annealed grades with tensile strength levels of up to 1000 MPa in combination with sufficient ductility for applications mainly in the field of structural automobile elements make use of the classic advantages of microalloying as well as the principles of DP and TRIP steels. Further improvement of properties will be reached by the new class of high manganese alloyed steels. (Abstract Copyright [2006], Wiley Periodicals, Inc.) [German] Fortschrittliche Multiphasen-Staehle eroeffnen wegen der inzwischen erreichbaren Kombination aus Umformbarkeit und Bauteilfestigkeit ein enormes Potenzial fuer Rohkarosserien. Sie stellen eine erste Wahl dar, wenn es um Festigkeit und um Crashsicherheit geht und besondere Anforderungen an die Bauteilgeometrien gestellt werden. Bei ThyssenKrupp hat die Entwicklung hochfester Multiphasen-Staehle in Verbindung mit dem Feuerverzinken zur Realisierung von Blechhalbzeugen gefuehrt, die hervorragend formbar sind. Es werden heute feuerverzinkte Komplexphasenstaehle neben den bewaehrten kaltgewalzten Dualphasen(DP) - und Retained Austenit(RA)-Staehlen produziert. Die neuen kontinuierlich gegluehten Stahlvarianten mit Festigkeiten bis zu 1000 MPa in Kombination mit der bei Strukturbauteilen im Automobilbau geforderten Duktilitaet nutzen sowohl die klassischen Vorteile des Mikrolegierens aus und dazu die Prinzipien, die man bei DP- und TRIP-Staehlen anwendet. Eine weitere Verbesserung des Eigenschaftsprofils wird mit dem

Method of Maintaining the Required Values of Surface Roughness and Prediction of Technological Conditions for Cold Sheet Rolling

Directory of Open Access Journals (Sweden)

Valíček J.

2014-06-01

Full Text Available The paper is based on results obtained from topography of surfaces of sheets rolled from deep-drawing steel of the type KOHAL grade 697, non-alloy low-carbon structural steel EN 10263-2:2004 and aluminium. The presented results document correctness of the assumption that the rolling force Froll increases with the increasing reduction Δh and the quality of the rolled surface is improved at the simultaneous increasing of strength of rolled sheets and the decreasing of size of structural grains. The experiment was performed on the two-high rolling stand DUO 210 SVa, which enables only non-continuous technology in contrast to the rolling mill with continuous reduction on one sheet in several degrees on rolling trains, in consequence of which the obtained height parameters of the section are in close correlation with the predicted dependence. Contribution of the work consists in the creation of a mathematical model (algorithm for predicting technological parameters of the two-high rolling stand DUO 210 SVa at change of the absolute reduction Δh, for example for a deep-drawing steel of the type KOHAL grade 697 and non-alloy lowcarbon structural steel PN EN 10263-2:2004 and aluminium, and also in the development of a method of calculation applicable to any material being rolled in general, because the authors have found that various materials can be differentiated by a derived analytical criterion IKP. This criterion is a function of ratio between the modulus of elasticity of reference material and that of actually rolled material. The reference material is here deep-drawing steel of the type KOHAL grade 697. Verification was carried out by measuring changes of final surface roughness profile and final strength of rolled sheets of the stated materials in relation to reductions and those were compared with theoretically predicted values. It is possible to identify and predict on the basis of this algorithm an instant state of surface topography in

Experiment and simulation analysis of roll-bonded Q235 steel plate

International Nuclear Information System (INIS)

Zhao, G.; Huang, Q.; Zhou, C.; Zhang, Z.; Ma, L.; Wang, X.

2016-01-01

Heavy-gauge Q235 steel plate was roll bonded, and the process was simulated using MARC software. Ultrasonic testing results revealed the presence of cracks and lamination defects in an 80-mm clad steel sheet, especially at the head and tail of the steel plate. There were non-uniform ferrite + pearlite microstructures and unbound areas at a bond interface. Through scanning electron microscopy analysis, long cracks and additional inclusions in the cracks were observed at the interface. A fracture analysis revealed non-uniform inclusions that pervaded the interface. Moreover, MARC simulations demonstrated that there was little equivalent strain at the centre of the slab during the first rolling pass. The equivalent centre increased to 0.5 by the fourth rolling pass. Prior to the final pass, the equivalent strain was not consistent across the thickness direction, preventing bonding interfaces from forming consistent deformation and decreasing the residual stress. The initial rolling reduction rate should not be very small (e.g. 5%) as it is averse to the coordination of rolling deformation. Such rolling processes are averse to the rolling bond. (Author)

Evolution of microstructure at hot band annealing of ferritic FeSi steels

Energy Technology Data Exchange (ETDEWEB)

Schneider, Jürgen, E-mail: juergen.schneider@t-online.de [Institute of Metal Forming, Technische Universität Bergakademie Freiberg, Bernhard-von Cotta-Str. 4, D-09596 Freiberg (Germany); Stahlzentrum Freiberg e.V., Leipziger Straße 34, D-09599 Freiberg (Germany); Li, Guangqiang [State Key Lab. of Refractories and Metallurgy, Wuhan University of Science and Technology, No. 947 Heping Avenue, Qingshan District, Wuhan 430081 (China); Franke, Armin [Stahlzentrum Freiberg e.V., Leipziger Straße 34, D-09599 Freiberg (Germany); Zhou, Bowen [State Key Lab. of Refractories and Metallurgy, Wuhan University of Science and Technology, No. 947 Heping Avenue, Qingshan District, Wuhan 430081 (China)

2017-02-15

The magnetic properties of the finally fabricated nonoriented FeSi steels critically depend on the microstructure and on the occurring crystallographic texture. The fabrication route comprises hot rolling, coiling and cooling, hot band annealing before cold rolling (optional), cold rolling and the final thermal treatment. As well known there is an interplay between the microstructure and texture during the various processing steps. For that reason, it is of interest to know more on the evolution of the microstructure at hot band annealing of hot band prepared in different ways. In this paper we will summarize our recent results on the evolution of microstructure during thermal annealing of hot band: thermal treatment following immediately the last pass of hot rolling or a hot band annealing as a separate processing step before cold rolling.

Effect of rolling temperature on 12Kh18N10T steel tube hardening

International Nuclear Information System (INIS)

Yushkevich, P.M.; Stepanovich, V.E.; Manankova, L.V.; Usenko, V.N.; Semenov, I.A.

1984-01-01

Mechanical properties and substructure of tubes at the constant reduction degree k(the ratio of deformation over wall thickness to deformation over diameter), depending on strain degree during cold and hot tube rolling, have been studied. The investigations are carried out using hot-rolled tubes with the dimensions 88x8 mm of 12Kh1hN10T steel. With the decrease of strain over the wall of the tube, produced of 12Kh18N10T steel as to strain over diameter the values of yield strength and ultimate strength increase with simultaneous decrease in ductility during warm rolling and yield strength and ultimate strength decrease with the increase in ductility-during cold rolling. During warm rolling of the tubes at 250 deg C the hardening of 12Kh18N10T steel is higher, than at the rolling temperature 150 deg C. The optimum temperature range of warm rolling is 120-150 deg C. Grain orientation in the metal of the tubes and degree of texture perfection increase with the temperature increase of the tube warm drolling as compared with col rolli

Development of dissimilar metal transition joint by hot roll bonding technique

International Nuclear Information System (INIS)

Nagai, Takayuki; Takeda, Seiichiro; Tanaka, Yasumasa; Ogawa, Kazuhiro; Nakasuji, Kazuyuki; Ikenaga, Yoshiaki.

1994-01-01

Metallurgically bonded transition joints which enable to connect reprocessing equipments made of superior corrosion resistant valve metals (Ti-5Ta, Zr or Ti) with stainless steel piping is needed for nuclear fuel reprocessing plants. The authors have developed dissimilar metal transition joints between stainless steel and Ti-5Ta, Zr or Ti with an insert metal of Ta by the hot roll bonding process, using the newly developed mill called 'rotary reduction mill'. In the R and D program, appropriate bonding conditions in the manufacturing process of the joints were established. This report presents the structure of transition joints and the manufacturing process by the hot roll bonding technique. Then, the evaluation of mechanical and corrosion properties and the results of demonstration test of joints for practical use are described. (author)

Development of dissimilar metal transition joint by hot roll bonding technique

International Nuclear Information System (INIS)

Nagai, Takayuki; Takeuchi, Masayuki; Takeda, Seiichiro; Shikakura, Sakae; Ogawa, Kazuhiro; Nakasuji, Kazuyuki; Kajimura, Haruhiko.

1995-01-01

Metallurgically bonded transition joints which enable to connect reprocessing equipments made of superior corrosion resistant valve metals (Ti-5Ta, Zr or Ti) with stainless steel piping is needed for nuclear fuel reprocessing plants. The authors have developed dissimilar metal transition joints between stainless steel and Ti-5Ta, Zr or Ti with an insert metal of Ta by the hot roll bonding process, using the newly developed mill called 'rotary reduction mill'. In the R and D program, appropriate bonding conditions in the manufacturing process of the joints were established. This report presents the structure of transition joints and the manufacturing process by hot roll bonding technique. Then, the evaluation of mechanical and corrosion properties and the results of demonstration test of joints for practical use are described. (author)

Effect of microstructural anisotropy on fracture toughness of hot rolled 13Cr ODS steel - The role of primary and secondary cracking

Science.gov (United States)

Das, A.; Viehrig, H. W.; Bergner, F.; Heintze, C.; Altstadt, E.; Hoffmann, J.

2017-08-01

ODS steels have been known to exhibit anisotropic fracture behaviour and form secondary cracks. In this work, the factors responsible for the anisotropic fracture behaviour have been investigated using scanning electron microscopy and electron backscatter microscopy. Fracture toughness of hot rolled 13Cr ODS steel was determined using unloading compliance method for L-T and T-L orientations at various temperatures. L-T orientation had higher fracture toughness than T-L orientation and also contained more pronounced secondary cracking. Secondary cracks appeared at lower loads than primary cracks in both orientations. Primary crack propagation was found to be preferentially through fine grains in a bimodal microstructure. Grains were aligned and elongated the most towards rolling direction followed by T and S directions resulting in fracture anisotropy. Crystallographic texture and preferential alignment of Ti enriched particles parallel to rolling direction also contributed towards fracture anisotropy.

Effects by the microstructure after hot and cold rolling on the texture and grain size after final annealing of ferritic non-oriented FeSi electrical steel

Science.gov (United States)

Schneider, J.; Stöcker, A.; Franke, A.; Kawalla, R.

2018-04-01

The magnetic properties of fully processed non-oriented FeSi electrical steel are characterized by their magnetization behavior and specific magnetic losses. The magnetic properties are determined by the texture and microstructure. Less gamma fiber intensity and a high intensity of preferable texture components, especially cube fiber texture, are desirable to obtain an excellent magnetizing behavior. Furthermore, large grain sizes are necessary to reach low values of the specific magnetic losses. The fabrication route of the fully processed non-oriented electrical steels comprises a heavy cold rolling of the hot rolled material before final annealing. To fulfill the requirements on large grain size for low loss materials, grain growth, which appears after complete recrystallization, plays an important role. In this paper we will analyze the influence of different microstructures of the hot strip and the resulting microstructure after cold rolling on the appearance of recrystallization and grain growth after final annealing. The evolution of texture reflects the present ongoing softening processes: recovery, recrystallization and finally grain growth at the given annealing conditions. It will be shown that the image of texture at recrystallization is remarkable different from the texture at grain growth. Substantially grain growth is obtained at lower annealing temperatures for an optimum microstructure of the hot rolled material.

Effects by the microstructure after hot and cold rolling on the texture and grain size after final annealing of ferritic non-oriented FeSi electrical steel

Directory of Open Access Journals (Sweden)

J. Schneider

2018-04-01

Full Text Available The magnetic properties of fully processed non-oriented FeSi electrical steel are characterized by their magnetization behavior and specific magnetic losses. The magnetic properties are determined by the texture and microstructure. Less gamma fiber intensity and a high intensity of preferable texture components, especially cube fiber texture, are desirable to obtain an excellent magnetizing behavior. Furthermore, large grain sizes are necessary to reach low values of the specific magnetic losses. The fabrication route of the fully processed non-oriented electrical steels comprises a heavy cold rolling of the hot rolled material before final annealing. To fulfill the requirements on large grain size for low loss materials, grain growth, which appears after complete recrystallization, plays an important role. In this paper we will analyze the influence of different microstructures of the hot strip and the resulting microstructure after cold rolling on the appearance of recrystallization and grain growth after final annealing. The evolution of texture reflects the present ongoing softening processes: recovery, recrystallization and finally grain growth at the given annealing conditions. It will be shown that the image of texture at recrystallization is remarkable different from the texture at grain growth. Substantially grain growth is obtained at lower annealing temperatures for an optimum microstructure of the hot rolled material.

Designing the Color of Hot-Dip Galvanized Steel Sheet Through Destructive Light Interference Using a Zn-Ti Liquid Metallic Bath

Science.gov (United States)

Levai, Gabor; Godzsák, Melinda; Török, Tamas I.; Hakl, Jozsef; Takáts, Viktor; Csik, Attila; Vad, Kalman; Kaptay, George

2016-07-01

The color of hot-dip galvanized steel sheet was adjusted in a reproducible way using a liquid Zn-Ti metallic bath, air atmosphere, and controlling the bath temperature as the only experimental parameter. Coloring was found only for samples cooled in air and dipped into Ti-containing liquid Zn. For samples dipped into a 0.15 wt pct Ti-containing Zn bath, the color remained metallic (gray) below a 792 K (519 °C) bath temperature; it was yellow at 814 K ± 22 K (541 °C ± 22 °C), violet at 847 K ± 10 K (574 °C ± 10 °C), and blue at 873 K ± 15 K (600 °C ± 15 °C). With the increasing bath temperature, the thickness of the adhered Zn-Ti layer gradually decreased from 52 to 32 micrometers, while the thickness of the outer TiO2 layer gradually increased from 24 to 69 nm. Due to small Al contamination of the Zn bath, a thin (around 2 nm) alumina-rich layer is found between the outer TiO2 layer and the inner macroscopic Zn layer. It is proven that the color change was governed by the formation of thin outer TiO2 layer; different colors appear depending on the thickness of this layer, mostly due to the destructive interference of visible light on this transparent nano-layer. A complex model was built to explain the results using known relationships of chemical thermodynamics, adhesion, heat flow, kinetics of chemical reactions, diffusion, and optics. The complex model was able to reproduce the observations and allowed making predictions on the color of the hot-dip galvanized steel sample, as a function of the following experimental parameters: temperature and Ti content of the Zn bath, oxygen content, pressure, temperature and flow rate of the cooling gas, dimensions of the steel sheet, velocity of dipping the steel sheet into the Zn-Ti bath, residence time of the steel sheet within the bath, and the velocity of its removal from the bath. These relationships will be valuable for planning further experiments and technologies on color hot-dip galvanization of steel

Characterization of microstructure, texture and magnetic properties in twin-roll casting high silicon non-oriented electrical steel

Energy Technology Data Exchange (ETDEWEB)

Li, Hao-Ze; Liu, Hai-Tao, E-mail: liuht@ral.neu.edu.cn; Liu, Zhen-Yu, E-mail: zyliu@mail.neu.edu.cn; Lu, Hui-Hu; Song, Hong-Yu; Wang, Guo-Dong

2014-02-15

An Fe-6.5 wt.% Si-0.3 wt.% Al as-cast sheet was produced by twin-roll strip casting process, then treated with hot rolling, warm rolling and annealing. A detailed study of the microstructure and texture evolution at different processing stages was carried out by optical microscopy, X-ray diffraction and electron backscattered diffraction analysis. The initial as-cast strip showed strong columnar grains and pronounced < 001 >//ND texture. The hot rolled and warm rolled sheets were characterized by large amounts of shear bands distributed through the thickness together with strong < 110 >//RD texture and weak < 111 >//ND texture. After annealing, detrimental < 111 >//ND texture almost disappeared while beneficial (001)<210 >, (001)<010 >, (115)<5 − 10 1 > and (410) < 001 > recrystallization textures were formed, thus the magnetic induction of the annealed sheet was significantly improved. The recrystallization texture in the present study could be explained by preferred nucleation and grain growth mechanism. - Highlights: • A high silicon as-cast strip with columnar structure was produced. • A thin warm rolled sheet without large edge cracks was obtained. • Microstructure and texture evolution at each stage were investigated. • Beneficial (001)<210 >, (001)<010 >, (410)<001 > recrystallization textures were formed. • The magnetic induction of annealed sheet was significantly improved.

Investigation into springback characteristics of two HSS sheets during cold v-bending

Energy Technology Data Exchange (ETDEWEB)

Fang, Gang; Gao, Wei-Ran [Department of Mechanical Engineering, Tsinghua University, Beijing 100084 (China)

2013-12-16

Considering the safety and the light-weight structure, there is an increasing requirement of high strength steel (HSS) sheets in the automotive industry. The high-precise prediction of the springback depends on constitutive equations and their corresponding material parameters. In order to investigate the springback of HSS sheets, DP590 and B280VK, their constitutive behaviors were analyzed based on the sheet tension tests. With respect to the constitutive equation, the Voce model is more proper to two hot-rolled steels, DP590 and B280VK, than the Swift model. Two steels are all saturated hardening, and the degree of hardening decreases with the strain. The cold v-banding tests of two HSS sheets were carried out for evaluation of springback characteristics. Results of v-bending experiments showed that the springback angle increases with the bending along 45°, 90° and 0° to the rolling direction of steel in turn.

Investigation into springback characteristics of two HSS sheets during cold v-bending

International Nuclear Information System (INIS)

Fang, Gang; Gao, Wei-Ran

2013-01-01

Considering the safety and the light-weight structure, there is an increasing requirement of high strength steel (HSS) sheets in the automotive industry. The high-precise prediction of the springback depends on constitutive equations and their corresponding material parameters. In order to investigate the springback of HSS sheets, DP590 and B280VK, their constitutive behaviors were analyzed based on the sheet tension tests. With respect to the constitutive equation, the Voce model is more proper to two hot-rolled steels, DP590 and B280VK, than the Swift model. Two steels are all saturated hardening, and the degree of hardening decreases with the strain. The cold v-banding tests of two HSS sheets were carried out for evaluation of springback characteristics. Results of v-bending experiments showed that the springback angle increases with the bending along 45°, 90° and 0° to the rolling direction of steel in turn

Transformation kinetics of microalloyed steels after hot controlled ...

African Journals Online (AJOL)

Transformation kinetics of austenite into ferrite after controlled hot rolling has been investigated in three microalloyed steels (Nb, Nb-Ti and C-Mn-V) using hot interrupted compression tests on the Gleeble 1500 within the testing temperature range of 875°C-1100°C. Holding times were varied between 0.5 and 30s, strain ...

Effect of intercritical deformation on microstructure and mechanical properties of a low-silicon aluminum-added hot-rolled directly quenched and partitioned steel

Energy Technology Data Exchange (ETDEWEB)

Tan, Xiao-Dong, E-mail: tan.x@mpie.de [State Key Laboratory of Rolling and Automation, Northeastern University, Shenyang 110819 (China); Max-Planck-Institut für Eisenforschung GmbH, Max-Planck-Str. 1, 40237 Düsseldorf (Germany); Xu, Yun-Bo, E-mail: yunbo_xu@126.com [State Key Laboratory of Rolling and Automation, Northeastern University, Shenyang 110819 (China); Ponge, Dirk [Max-Planck-Institut für Eisenforschung GmbH, Max-Planck-Str. 1, 40237 Düsseldorf (Germany); Yang, Xiao-Long; Hu, Zhi-Ping; Peng, Fei [State Key Laboratory of Rolling and Automation, Northeastern University, Shenyang 110819 (China); Ju, Xiao-Wei [CERI LONG PRODUCT CO., LTD., Beijing 100176 (China); Wu, Di [State Key Laboratory of Rolling and Automation, Northeastern University, Shenyang 110819 (China); Raabe, Dierk [Max-Planck-Institut für Eisenforschung GmbH, Max-Planck-Str. 1, 40237 Düsseldorf (Germany)

2016-02-22

Here, we applied hot-rolling in conjunction with direct quenching and partitioning (HDQ&P) processes with different rolling schedules to a low-C low-Si Al-added steel. Ferrite was introduced into the steel by intercritical rolling and air cooling after hot-rolling. The effect of intercritcal deformation on the microstructure evolution and mechanical properties was investigated. The promotion of austenite stabilization and the optimization of the TRIP effect due to a moderate degree of intercritical deformation were systematically explored. The results show that the addition of 1.46 wt% of Al can effectively promote ferrite formation. An intercritical deformation above 800 °C can result in a pronounced bimodal grain size distribution of ferrite and some elongated ferrite grains containing sub-grains. The residual strain states of both austenite and ferrite and the occurrence of bainite transformation jointly increase the retained austenite fraction due to its mechanical stabilization and the enhanced carbon partitioning into austenite from its surrounding phases. An intercritical deformation below 800 °C can profoundly increase the ferrite fraction and promote the recrystallization of deformed ferrite. The formation of this large fraction of ferrite enhances the carbon enrichment in the untransformed austenite and retards the bainite transformation during the partitioning process and finally enhances martensite transformation and decreases the retained austenite fraction. The efficient TRIP effect of retained austenite and the possible strain partitioning of bainite jointly improve the work hardening and formability of the steel and lead to the excellent mechanical properties with relatively high tensile strength (905 MPa), low yield ratio (0.60) and high total elongation (25.2%).

Rolling-element fatigue life of silicon nitride balls. [as compared to that of steel, ceramic, and cermet materials

Science.gov (United States)

Parker, R. J.; Zaretsky, E. V.

1974-01-01

The five-ball fatigue tester was used to evaluate silicon nitride as a rolling-element bearing material. Results indicate that hot-pressed silicon nitride running against steel may be expected to yield fatigue lives comparable to or greater than those of bearing quality steel running against steel at stress levels typical rolling-element bearing application. The fatigue life of hot-pressed silicon nitride is considerably greater than that of any ceramic or cermet tested. Computer analysis indicates that there is no improvement in the lives of 120-mm-bore angular--contact ball bearings of the same geometry operating at DN values from 2 to 4 million where hot-pressed silicon nitride balls are used in place of steel balls.

FATIGUE BEHAVIOR OF HOT-ROLLED STEEL INTENDED FOR COLD FORMING

Directory of Open Access Journals (Sweden)

Gejza Rosenberg

2011-07-01

Full Text Available In the work, there are presented measured tension and fatigue properties of eight low-carbon steels moulded in form of 20 kg ingots that were processed by controlled regime of rolling /cooling and then exposed to simulated effect of two coiling temperatures. The experimental results presented in the work show, that steels with ferrite-martensite or ferrite-bainitic microstructure have in comparison to ferrite-pearlitic or ferrite-carbidic microstructure better strength-plastic properties, but worse resistance to cyclic loading.

A Study on the Low Temperature Brittleness by Cyclic Cooling-Heating of Low Carbon Hot Rolled Steel Plate

International Nuclear Information System (INIS)

Lee, Hyo Bok

1979-01-01

The ductile-brittle transition phenomenon of low carbon steel has been investigated using the standard Charpy V-notch specimen. Dry ice and acetone were used as refrigerants. Notched specimens were cut from the hot rolled plate produced at POSCO for the Olsen impact test. The effect of cyclic cooling and heating of 0.14% carbon steel on the embrittlement was extensively examined. The ductile-brittle transition temperature was found to be approximately-30 .deg. C. The transition temperature was gradually increased as the number of cooling-heating cycles increased. On a typical V-notch fracture surface it was found that the ductile fracture surface showed a thick and fibrous structure, while the brittle fracture surface a small and light grain with irregular disposition. As expected, the transition temperature was also increased as the carbon content of steel increased. Compared with the case of 0.14% carbon steel, the transition temperature of 0.17% carbon steel was found to be increased about 12 .deg. C

Effect of decreased hot-rolling reduction treatment on fracture toughness of low-alloy structural steels

Science.gov (United States)

Tomita, Yoshiyuki

1990-09-01

Commercial low-alloy structural steels, 0.45 pct C (AISI 1045 grade), 0.40 pct C-Cr-Mo (AISI 4140 grade), and 0.40 pct C-Ni-Cr-Mo (AISI 4340 grade), have been studied to determine the effect of the decreased hot-rolling reduction treatment (DHRRT) from 98 to 80 pct on fracture toughness of quenched and highly tempered low-alloy structural steels. The significant conclusions are as follows: (1) the sulfide inclusions were modified through the DHRRT from a stringer (mean aspect ratio: 16.5 to 17.6) to an ellipse (mean aspect ratio: 3.8 to 4.5), independent of the steels studied; (2) the DHRRT significantly improved J Ic in the long-transverse and shorttransverse orientations, independent of the steels studied; and (3) the shelf energy in the Charpy V-notch impact test is also greatly improved by the DHRRT, independent of testing orientation and steels studied; however, (4) the ductile-to-brittle transition temperature was only slightly affected by the DHRRT. The beneficial effect on the J Ic is briefly discussed in terms of a crack extension model involving the formation of voids at the inclusion sites and their growth and eventual linking up through the rupture of the intervening ligaments by local shear.

The Influence of Vanadium Microalloying on the Production of Thin Slab Casting and Direct Rolled Steel Strip

Science.gov (United States)

Li, Yu; Milbourn, David

Vanadium microalloying is highly effective in high strength strip steels produced by thin slab casting and direct rolled process. Because of the high solubility of V(C,N) in austenite, vanadium is likely to remain in solution during casting, equalisation and rolling. Vanadium microalloyed steels have better hot ductility and are less prone to transverse cracking than niobium containing steels. Despite a coarse as-cast austenite grain size before rolling, significant grain refinement can be achieved in vanadium microalloyed steels by repeated recrystallization during rolling, resulting in a fine uniform ferrite microstructure in final strip. Almost all vanadium present in microalloyed steels is available to precipitate in ferrite as very fine particles, contributing to precipitation strengthening. Vanadium microalloyed steels show less sensitivity to rolling process variables and exhibit excellent combination of strength and toughness.

The influence of the hardening coolant agent on the properties of hot rolled bars of the steel 42CrMo4

Directory of Open Access Journals (Sweden)

M. Stańczyk

2014-10-01

Full Text Available In the work the influence results of two different hardening coolant agents on the basic mechanical proprieties and microstructure of the round hot rolled bars were presented. The bars of 42CrMo4 steel were exposed to analysis, and for those bars in the hardening process, water and modern pro-ecological polymer cooling agents Aqua Quench MK were used.

Theories, Methods and Numerical Technology of Sheet Metal Cold and Hot Forming Analysis, Simulation and Engineering Applications

CERN Document Server

Hu, Ping; Liu, Li-zhong; Zhu, Yi-guo

2013-01-01

Over the last 15 years, the application of innovative steel concepts in the automotive industry has increased steadily. Numerical simulation technology of hot forming of high-strength steel allows engineers to modify the formability of hot forming steel metals and to optimize die design schemes. Theories, Methods and Numerical Technology of Sheet Metal Cold and Hot Forming focuses on hot and cold forming theories, numerical methods, relative simulation and experiment techniques for high-strength steel forming and die design in the automobile industry. Theories, Methods and Numerical Technology of Sheet Metal Cold and Hot Forming introduces the general theories of cold forming, then expands upon advanced hot forming theories and simulation methods, including: • the forming process, • constitutive equations, • hot boundary constraint treatment, and • hot forming equipment and experiments. Various calculation methods of cold and hot forming, based on the authors’ experience in commercial CAE software f...

Experimental determination of heat transfer coefficients in roll bite and air cooling for computer simulations of 1100 MPa carbon steel rolling

Science.gov (United States)

Leinonen, Olli; Ilmola, Joonas; Seppälä, Oskari; Pohjonen, Aarne; Paavola, Jussi; Koskenniska, Sami; Larkiola, Jari

2018-05-01

In modeling of hot rolling pass schedules the heat transfer phenomena have to be known. Radiation to ambient, between rolls and a steel slab as well as heat transfer in contacts must be considered to achieve accurate temperature distribution and thereby accurate material behavior in simulations. Additional heat is generated by friction between the slab and the work roll and by plastic deformation. These phenomena must be taken into account when the effective heat transfer coefficient is determined from experimental data. In this paper we determine the effective heat transfer coefficient at the contact interface and emissivity factor of slab surface for 1100MPa strength carbon steel for hot rolling simulations. Experimental pilot rolling test were carried out and slab temperatures gathered right below the interface and at the mid thickness of the slab. Emissivity factor tests were carried out in the same manner but without rolling. Experimental data is utilized to derive contact heat transfer coefficient at the interface and emissivity factor of slab surface. Pilot rolling test is reproduced in FE-analysis to further refine the heat transfer coefficient and emissivity factor. Material mechanical properties at rolling temperatures were determined by Gleeble™ thermo-mechanical simulator and IDS thermodynamic-kinetic-empirical software.

Determination of Proper Austenitization Temperatures for Hot Stamping of AISI 4140 Steel

Science.gov (United States)

Samadian, Pedram; Parsa, Mohammad Habibi; Shakeri, Amid

2014-04-01

High strength steels are desirable materials for use in automobile bodies in order to reduce vehicle weight and increase the safety of car passengers, but steel grades with high strength commonly show poor formability. Recently, steels with controlled microstructures and compositions are used to gain adequate strength after hot stamping while maintaining good formability during processing. In this study, microstructure evolutions and changes in mechanical properties of AISI 4140 steel sheets resulting from the hot stamping process at different austenitization temperatures were investigated. To determine the proper austenitization temperatures, the results were compared with those of the cold-worked and cold-worked plus quench-tempered specimens. Comparisons showed that the austenitization temperatures of 1000 and 1100 °C are proper for hot stamping of 3-mm-thick AISI 4140 steel sheets due to the resultant martensitic microstructure which led to the yield and ultimate tensile strength of 1.3 and 2.1 GPa, respectively. Such conditions resulted in more favorable simultaneous strength and elongation than those of hot-stamped conventional boron steels.

Development of TRIP-Aided Lean Duplex Stainless Steel by Twin-Roll Strip Casting and Its Deformation Mechanism

Science.gov (United States)

Zhao, Yan; Zhang, Weina; Liu, Xin; Liu, Zhenyu; Wang, Guodong

2016-12-01

In the present work, twin-roll strip casting was carried out to fabricate thin strip of a Mn-N alloyed lean duplex stainless steel with the composition of Fe-19Cr-6Mn-0.4N, in which internal pore defects had been effectively avoided as compared to conventional cast ingots. The solidification structure observed by optical microscope indicated that fine Widmannstatten structure and coarse-equiaxed crystals had been formed in the surface and center, respectively, with no columnar crystal structures through the surface to center of the cast strip. By applying hot rolling and cold rolling, thin sheets with the thickness of 0.5 mm were fabricated from the cast strips, and no edge cracks were formed during the rolling processes. With an annealing treatment at 1323 K (1050 °C) for 5 minutes after cold rolling, the volume fractions of ferrite and austenite were measured to be approximately equal, and the distribution of alloying elements in the strip was further homogenized. The cold-rolled and annealed sheet exhibited an excellent combination of strength and ductility, with the ultimate tensile strength and elongation having been measured to be 1000 MPa and 65 pct, respectively. The microstructural evolution during deformation was investigated by XRD, EBSD, and TEM, indicating that ferrite and austenite had different deformation mechanisms. The deformation of ferrite phase was dominated by dislocation slipping, and the deformation of austenite phase was mainly controlled by martensitic transformation in the sequence of γ→ ɛ-martensite→ α'-martensite, leading to the improvement of strength and plasticity by the so-called transformation-induced plasticity (TRIP) effect. By contrast, lean duplex stainless steels of Fe-21Cr-6Mn-0.5N and Fe-23Cr-7Mn-0.6N fabricated by twin-roll strip casting did not show TRIP effects and exhibited lower strength and elongation as compared to Fe-19Cr-6Mn-0.4N.

Non-Metallic Inclusions and Hot-Working Behaviour of Advanced High-Strength Medium-Mn Steels

Directory of Open Access Journals (Sweden)

Grajcar A.

2016-06-01

Full Text Available The work addresses the production of medium-Mn steels with an increased Al content. The special attention is focused on the identification of non-metallic inclusions and their modification using rare earth elements. The conditions of the thermomechanical treatment using the metallurgical Gleeble simulator and the semi-industrial hot rolling line were designed for steels containing 3 and 5% Mn. Hot-working conditions and controlled cooling strategies with the isothermal holding of steel at 400°C were selected. The effect of Mn content on the hot-working behaviour and microstructure of steel was addressed. The force-energetic parameters of hot rolling were determined. The identification of structural constituents was performed using light microscopy and scanning electron microscopy methods. The addition of rare earth elements led to the total modification of non-metallic inclusions, i.e., they replaced Mn and Al forming complex oxysulphides. The Mn content in a range between 3 and 5% does not affect the inclusion type and the hot-working behaviour. In contrast, it was found that Mn has a significant effect on a microstructure.

75 FR 65453 - Certain Hot-Rolled Flat-Rolled Carbon Quality Steel Flat Products From Brazil: Notice of...

Science.gov (United States)

2010-10-25

... Nucor Corporation (Nucor) and United States Steel Corporation (U.S. Steel), domestic producers of hot..., the Department received requests from Nucor and U.S. Steel (collectively, domestic producers), that... July 6, 2010 (CBP Memo). On July 22, 2010, and July 23, 2010, respectively, Nucor and U.S. Steel timely...

Texture and magnetic properties of non-oriented electrical steels processed by an unconventional cold rolling scheme

Energy Technology Data Exchange (ETDEWEB)

He, Youliang, E-mail: youliang.he@canada.ca [CanmetMATERIALS, Natural Resources Canada, Hamilton, ON (Canada); Hilinski, Erik J. [Formerly Research and Technology Centre, United States Steel Corporation, Munhall, PA (United States); Now Tempel Steel Co., Chicago, IL (United States)

2016-05-01

Two non-oriented electrical steels containing 0.9 wt% and 2.8 wt% of silicon were processed using an unconventional cold rolling scheme, i.e. the cold rolling direction (CRD) was intentionally inclined at an angle to the hot rolling direction (HRD) so that the initial texture before cold rolling and the rotation paths of crystals during cold deformation were both altered as compared to conventional cold rolling along the original HRD. The cold-rolled steel strips were then annealed, skin-pass rolled and final annealed. The texture and microstructure of the materials were characterized by X-ray diffraction (XRD), electron backscatter diffraction (EBSD) and optical microscopy, and considerable differences in average grain size and texture were observed at different inclination angles. The magnetic properties of the steel strips were measured at 400 Hz and 1.0 T/1.5 T using a specially designed Epstein frame, and apparent differences were also noticed at various angles. The magnetic quality of texture was evaluated using different texture factors/parameters and compared to the measured magnetic properties. Although apparent improvement on the magnetic quality of texture can be noted by inclining the CRD to HRD, the trend does not match the measured magnetic properties at 400 Hz, which may have been affected by other parameters in addition to crystallographic texture. - Highlights: • The cold rolling direction is inclined an angle to the hot rolling direction. • The deformation and annealing textures are both changed by the inclined rolling. • Magnetic quality of texture is improved at specific inclination angles. • Low silicon steel is more sensitive in texture change than high silicon steel. • High frequency core loss does not follow the computed magnetic quality of texture.

Hot drawn Fe–6.5 wt.%Si wires with good ductility

International Nuclear Information System (INIS)

Yang, W.; Li, H.; Yang, K.; Liang, Y.F.; Yang, J.; Ye, F.

2014-01-01

Highlights: • Fe–6.5wt%Si steel wire with diameter of 1.6 mm can be successfully obtained by hot drawing process. • The ductility of Fe–6.5wt%Si alloy can be improved significantly when it is fabricated in the form of wire. • The Dc magnetic property of Fe–6.5wt%Si steel wire 1.6 mm in diameter is excellent, which is close to that of 0.3 mm thick cold-rolling sheet. - Abstract: Fe–6.5 wt.%Si high silicon steel wires with a diameter of 1.6 mm are fabricated successfully by hot drawing. The high silicon steel wires show much better ductility than sheets. The tensile strength and elongation of the wires at the room temperature can reach 1.31 GPa and 1.4%, respectively. The tensile strength and elongation of the rolling sheet at the room temperature are 0.8 GPa and 0, respectively. The microstructure analyses show that the elongated grains after drawing and reduced ordering phases by deformation in the wires might contribute to its good ductility. Bs value of 1.437 T and Hc value of 16.96 A/m are obtained for the wire after proper heat treatment for the wires

Surface investigation and tribological mechanism of a sulfate-based lubricant deposited on zinc-coated steel sheets

Energy Technology Data Exchange (ETDEWEB)

Timma, Christian, E-mail: christian.timma@thyssenkrupp.com [ThyssenKrupp Steel Europe AG, Technology & Innovation, Kaiser-Wilhelm Str. 100, 47166 Duisburg (Germany); University of Duisburg-Essen, Faculty of Chemistry, CENIDE, Universitätsstraße 7, 45141 Essen (Germany); Lostak, Thomas; Janssen, Stella; Flock, Jörg [ThyssenKrupp Steel Europe AG, Technology & Innovation, Kaiser-Wilhelm Str. 100, 47166 Duisburg (Germany); Mayer, Christian [University of Duisburg-Essen, Faculty of Chemistry, CENIDE, Universitätsstraße 7, 45141 Essen (Germany)

2016-12-30

Highlights: • Skin-passed hot-dip galvanized (HDG-) steel sheets were coated with (NH{sub 4}){sub 2}SO{sub 4} in a common roll-coating method. • A formation of (NH{sub 4}){sub 2}Zn(SO{sub 4}) * xH{sub 2}O was observed and the reaction mainly occurred in the skin-passed areas of the surface. • Sulfate coated samples reveal a superior friction behaviour in oil-like conditions compared non-sulfated specimen. - Abstract: Phosphatation is a well-known technique to improve friction and wear behaviour of zinc coated steel, but has a variety of economic and ecologic limitations. In this study an alternative coating based on ammonium sulfate ((NH{sub 4}){sub 2}SO{sub 4}) is applied on skin-passed hot-dip galvanized steel sheets in order to investigate its surface chemical and tribological behaviour in a Pin-on-Disk Tribometer. Raman- and X-ray photoelectron spectroscopic results revealed a formation of ammonium zinc sulfate ((NH{sub 4}){sub 2}Zn(SO{sub 4}){sub 2} * xH{sub 2}O) on the surface, which is primarily located in the skin-passed areas of the steel material. Sulfate coated samples exhibited a superior friction behaviour in Pin-on-Disk Tests using squalane as a model substance for oil-like lubricated conditions and a formation of a thin lubrication film is obtained in the wear track. Squalane acts as a carrier substance for ammonium zinc sulfate, leading to an effective lubrication film in the wear track.

Investigation of the Formability of TRIP780 Steel Sheets

Science.gov (United States)

Song, Yang

The formability of a metal sheet is dependent on its work hardening behaviour and its forming limits; and both aspects must be carefully determined in order to accurately simulate a particular forming process. This research aims to characterize the formability of a TRIP780 sheet steel using advanced experimental testing and analysis techniques. A series of flat rolling and tensile tests, as well as shear tests were conducted to determine the large deformation work hardening behaviour of this TRIP780 steel. Nakazima tests were carried out up to fracture to determine the forming limits of this sheet material. A highly-automated method for generating a robust FLC for sheet materials from DIC strain measurements was created with the help of finite element simulations, and evaluated against the conventional method. A correction algorithm that aims to compensate for the process dependent effects in the Nakazima test was implemented and tested with some success.

Service behaviour of high speed steel rolling rolls used in hot strip mills; Comportamiento en servicio de los aceros rapidos utilizados en la fabricacion de los cilindros de trabajo de los trenes de bandas en caliente

Energy Technology Data Exchange (ETDEWEB)

Ziadi, A.; Belzunce, F. J.; Rodriguez, C.; Fernandez, I.

2005-07-01

Work rolls used in hot strip mills may be able to carry out severe actions: very high thermal stresses and wear, along with mechanical stresses due to normal rolling loads, which develop in the presence of cracks, produced by the former actions. The microstructure and the mechanical behaviour (strength and toughness) of high speed steels, which recently have been introduced in this applications, were studied in this work in comparison with high chromium cast irons. (Author) 7 refs.

Model for prediction of strip temperature in hot strip steel mill

International Nuclear Information System (INIS)

Panjkovic, Vladimir

2007-01-01

Proper functioning of set-up models in a hot strip steel mill requires reliable prediction of strip temperature. Temperature prediction is particularly important for accurate calculation of rolling force because of strong dependence of yield stress and strip microstructure on temperature. A comprehensive model was developed to replace an obsolete model in the Western Port hot strip mill of BlueScope Steel. The new model predicts the strip temperature evolution from the roughing mill exit to the finishing mill exit. It takes into account the radiative and convective heat losses, forced flow boiling and film boiling of water at strip surface, deformation heat in the roll gap, frictional sliding heat, heat of scale formation and the heat transfer between strip and work rolls through an oxide layer. The significance of phase transformation was also investigated. Model was tested with plant measurements and benchmarked against other models in the literature, and its performance was very good

Model for prediction of strip temperature in hot strip steel mill

Energy Technology Data Exchange (ETDEWEB)

Panjkovic, Vladimir [BlueScope Steel, TEOB, 1 Bayview Road, Hastings Vic. 3915 (Australia)]. E-mail: Vladimir.Panjkovic@BlueScopeSteel.com

2007-10-15

Proper functioning of set-up models in a hot strip steel mill requires reliable prediction of strip temperature. Temperature prediction is particularly important for accurate calculation of rolling force because of strong dependence of yield stress and strip microstructure on temperature. A comprehensive model was developed to replace an obsolete model in the Western Port hot strip mill of BlueScope Steel. The new model predicts the strip temperature evolution from the roughing mill exit to the finishing mill exit. It takes into account the radiative and convective heat losses, forced flow boiling and film boiling of water at strip surface, deformation heat in the roll gap, frictional sliding heat, heat of scale formation and the heat transfer between strip and work rolls through an oxide layer. The significance of phase transformation was also investigated. Model was tested with plant measurements and benchmarked against other models in the literature, and its performance was very good.

Fatigue crack growth behaviors in hot-rolled low carbon steels: A comparison between ferrite–pearlite and ferrite–bainite microstructures

International Nuclear Information System (INIS)

Guan, Mingfei; Yu, Hao

2013-01-01

The roles of microstructure types in fatigue crack growth behaviors in ferrite–pearlite steel and ferrite–bainite steel were investigated. The ferrite–bainite dual-phase microstructure was obtained by intermediate heat treatment, conducted on ferrite–pearlite hot-rolled low carbon steel. This paper presents the results from investigation using constant stress-controlled fatigue tests with in-situ scanning electron microscopy (SEM), fatigue crack growth (FCG) rate tests, and fatigue fractography analysis. Microscopy images arrested by in-situ SEM showed that the fatigue crack propagation in F–P steel could become unstable more ealier compared with that in F–B steel. The fatigue cracks in ferrite–pearlite were more tortuous and could propagate more freely than that in ferrite–bainite microstructures. However, frequent crack branching were observed in ferrite–bainite steel and it indicated that the second hard bainite phase effectively retarded the crack propagation. The variation of FCG rate (da/dN) with stress intensity factor range (ΔK) for F–P and F–B steels was discussed within the Paris region. It was shown that FCG rate of F–P steel was higher than that of F–B steel. Moreover, the fatigue fracture surface analysis proved that grain boundaries could also play a role in the resistance of crack propagation.

Finite-element model to predict roll-separation force and defects during rolling of U-10Mo alloys

Science.gov (United States)

Soulami, Ayoub; Burkes, Douglas E.; Joshi, Vineet V.; Lavender, Curt A.; Paxton, Dean

2017-10-01

A major goal of the Convert Program of the U.S. Department of Energy's National Nuclear Security Administration (DOE/NNSA) is to enable high-performance research reactors to operate with low-enriched uranium rather than the high-enriched uranium currently used. To this end, uranium alloyed with 10 wt% molybdenum (U-10Mo) represents an ideal candidate because of its stable gamma phase, low neutron caption cross section, acceptable swelling response, and predictable irradiation behavior. However, because of the complexities of the fuel design and the need for rolled monolithic U-10Mo foils, new developments in processing and fabrication are necessary. This study used a finite-element code, LS-DYNA, as a predictive tool to optimize the rolling process. Simulations of the hot rolling of U-10Mo coupons encapsulated in low-carbon steel were conducted following two different schedules. Model predictions of the roll-separation force and roll pack thicknesses at different stages of the rolling process were compared with experimental measurements. The study reported here discussed various attributes of the rolled coupons revealed by the model (e.g., waviness and thickness non-uniformity like dog-boning). To investigate the influence of the cladding material on these rolling defects, other cases were simulated: hot rolling with alternative can materials, namely, 304 stainless steel and Zircaloy-2, and bare-rolling. Simulation results demonstrated that reducing the mismatch in strength between the coupon and can material improves the quality of the rolled sheet. Bare-rolling simulation results showed a defect-free rolled coupon. The finite-element model developed and presented in this study can be used to conduct parametric studies of several process parameters (e.g., rolling speed, roll diameter, can material, and reduction).

Effects of interface roughness on the annealing behaviour of laminated Ti-Al composite deformed by hot rolling

DEFF Research Database (Denmark)

Du, Y.; Fan, G.H.; Yu, Tianbo

2015-01-01

A laminated Ti-Al composite has been fabricated by hot compaction and hot rolling of alternate layers of commercial purity Ti and Al sheets with a thickness of 200 μm. The hot compaction temperature was 500˚C and in a following step the composite has been reduced 50% in thickness by hot rolling....... The fully consolidated composite has been annealed at 300˚C and 500˚C for different length of time. As a result of the differences in crystal structure and mechanical properties between Ti and Al protrusions and retrusions formed at the interface. A heterogeneous interface has thereby been created...

Influence of severe plastic deformation obtained by warm rolling on microstructure and mechanical properties of the ferritic stainless steel

Energy Technology Data Exchange (ETDEWEB)

Barbosa, Luana Alves; Campos, Wagner Reis Costa; Vilela, Jefferson José, E-mail: luana_alves_barbosa@hotmail.com, E-mail: wrrc@cdtn.br, E-mail: jjv@cdtn.br [Centro de Desenvolvimento da Tecnologia Nuclear (CDTN/CNEN-MG), Belo Horizonte, MG (Brazil); Miqueletti, Estevesson Ferreira; Mazzer, Eric Marchezini; Santos, Dagoberto B., E-mail: estevess@demet.ufmg.br, E-mail: marchezini@demet.ufmg.br, E-mail: dsantos@demet.ufmg.br [Universidade Federal de Minas Gerais (UFMG), Belo Horizonte, MG (Brazil)

2017-07-01

Generation IV reactors require research on new materials. For example, materials that will be used in the reactor vessel must be resistant to creep and have high toughness. Grain refining is a technique used to improve toughness. This grain refinement can be achieved by severe plastic deformation. In this work, the stainless steel 409 was used to simulate the EUROFER one type of ODS steel. The rolling process was applied to make the severe plastic deformation. The rolling was performed at 600°C which corresponds to the warm working condition in the absence of dynamic recrystallization. The rolling schedule studied allowed a logarithmic strain accumulation of 3.16. The rolled sheet had a yield stress of 822 MPa and a hardness of 302 HV. The grains became quite elongated characteristic of a severe plastic deformation. The recrystallization temperature of the rolled sheet was approximately 500°C. It was obtained by heat treatment and hardness measurement. (author)

Influence of severe plastic deformation obtained by warm rolling on microstructure and mechanical properties of the ferritic stainless steel

International Nuclear Information System (INIS)

Barbosa, Luana Alves; Campos, Wagner Reis Costa; Vilela, Jefferson José; Miqueletti, Estevesson Ferreira; Mazzer, Eric Marchezini; Santos, Dagoberto B.

2017-01-01

Generation IV reactors require research on new materials. For example, materials that will be used in the reactor vessel must be resistant to creep and have high toughness. Grain refining is a technique used to improve toughness. This grain refinement can be achieved by severe plastic deformation. In this work, the stainless steel 409 was used to simulate the EUROFER one type of ODS steel. The rolling process was applied to make the severe plastic deformation. The rolling was performed at 600°C which corresponds to the warm working condition in the absence of dynamic recrystallization. The rolling schedule studied allowed a logarithmic strain accumulation of 3.16. The rolled sheet had a yield stress of 822 MPa and a hardness of 302 HV. The grains became quite elongated characteristic of a severe plastic deformation. The recrystallization temperature of the rolled sheet was approximately 500°C. It was obtained by heat treatment and hardness measurement. (author)

Investigation of the effect of heat treatment on the structure of the cold-rolled ferrite stainless steels

Directory of Open Access Journals (Sweden)

В. Л. Грешта

2015-03-01

Full Text Available The work presents the estimation of a factor, namely, the solid solution super saturation by carbon and nitrogen on crystalline nature of high-chromium ferrite (HCF in defining the inhibition mechanism of recrystallization processes in ferritic stainless steel. The essence of the study was to conduct an additional heat treatment of hot (h/r tackle for the following modes: annealing 800 ° C - 4 hours, tempering with temperatures of 900, 1000, 1100 ° C after exposure to 1 min/mm. It is established that the determining factor that influences the amount of the carbide phase in c/r sheet is prior treatment of h/r tackle. A definite connection between the volume fraction of the secondary phase and the degree of cold deformation was observed. In the structure of cold-rolled sheet the same pattern with respect to the degree of implementation processes allocation of excess phases is maintained as in hot-rolled, after appropriate heat treatment. The smallest amount of the secondary phase structure was observed in the letter after hardening from 1100 °C - 1 min/mm. The reason is the thermodynamic state of HCF, to which at 1100 °C all the excess carbon and nitrogen must exist in solid solution. Thus, it is found that according to the present analysis of structural changes it should be noted that the best option of thermal prior treatment of h/r tackle is the annealing at 800 °C – 4 hours

Influence of Al content on the corrosion resistance of micro-alloyed hot rolled steel as a function of grain size

Science.gov (United States)

Qaban, Abdullah; Naher, Sumsun

2018-05-01

High-strength low-alloy steel (HSLA) has been widely used in many applications involving automobiles, aerospace, construction, and oil and gas pipelines due to their enhanced mechanical and chemical properties. One of the most critical elements used to improve these properties is Aluminium. This work will explore the effect of Al content on the corrosion behaviour of hot rolled high-strength low-alloy steel as a function of grain size. The method of investigation employed was weight loss technique. It was obvious that the increase in Al content enhanced corrosion resistance through refinement of grain size obtained through AlN precipitation by pinning grain boundaries and hindering their growth during solidification which was found to be beneficial in reducing corrosion rate.

Improvement of impact toughness by modified hot working and heat treatment in 13%Cr martensitic stainless steel

Energy Technology Data Exchange (ETDEWEB)

Srivatsa, Kulkarni, E-mail: srivatsa.kulkarni@kcssl.com; Srinivas, Perla; Balachandran, G.; Balasubramanian, V.

2016-11-20

Improvement of the general mechanical properties and in particular sub-zero impact toughness in a 0.2%C-13%Cr martensitic stainless steel has been explored by varying the hot deformation and heat treatment conditions. The deformation conditions include hot rolling an ingot in one case and cogging the ingot to a semis followed by hot rolling in another case. The bars made from both routes were subjected to a single hardening heat treatment at 980 °C and 1040 °C oil quenched and a double hardening heat treatment at 1040 °C followed by 980 °C oil quenched. The hardened steels were subjected to a standard two stage tempering at 710 °C followed by 680 °C. The impact toughness was found to be doubled in the cogged and rolled steel in double hardened condition. Other processing conditions show varying impact toughness levels. The toughness observed was correlated to the grain size and the carbide distribution in the matrix and the fractography features.

Hot Roll Bonding of Aluminum to Twin-Roll Cast (TRC) Magnesium and Its Subsequent Deformation Behavior

Science.gov (United States)

Saleh, H.; Schmidtchen, M.; Kawalla, R.

2018-02-01

In an experiment in which twin-roll cast AZ31 magnesium alloy and commercial purity aluminum (AA 1050) sheets were bonded by hot rolling as Al/Mg/Al laminate composites, it was found that increasing the preheating temperatures up to 400 °C enhances the bonding strength of composites. Further increases in the preheating temperatures accelerate the magnesium oxide growth and thus reduce the bonding strength. The influence of the reduction ratio on the bonding properties was also studied, whereby it was observed that increasing the rolling reduction led to an increase in the bonding strength. The experimental results show that the optimum bonding strength can be obtained at rolling temperatures of 375-400 °C with a 50-60% reduction in thickness. On the other hand, the subsequent deformation behavior of composite was assessed using plane strain compression and deep drawing tests. We demonstrate that the composites produced using the optimum roll bonding conditions exhibited sufficient bonding during subsequent deformation and did not reveal any debonding at the bonding interface.

Advanced automobile steels subjected to plate rolling at 773 K or 1373 K

Science.gov (United States)

Torganchuk, Vladimir; Belyakov, Andrey; Kaibyshev, Rustam

2017-12-01

The high manganese steels exhibiting the effects of twinning-induced plasticity (TWIP) and transformation-induced plasticity (TRIP) demonstrate an excellent combination of enhanced formability, strength and ductility. Such unique mechanical properties make high-manganese steel the most attractive material for various applications, including the segment of advanced automobile steels. The strain hardening in such steels can be achieved through martensitic transformation, when the stacking fault energy (SFE) is about 10 mJ m-2, and/or twinning, when SFE is about 20 to 50 mJ m-2. The actual mechanical properties of high-Mn steels could vary, depending on the conditions of thermo-mechanical processing. In the present study, the effect of rolling temperature on the microstructure and mechanical properties of 18% Mn steels was clarified. The steels hot rolled at 1373 K were characterized by uniform almost equiaxed grains with near random crystallographic orientations that resulted in relatively low yield strengths of 300-360 MPa, followed by pronounced strain hardening that led to the total elongation above 60%. In contrast, the steels warm rolled at 773 K were characterized by flattened grains with a strong rolling texture and high yield strengths of 850-950 MPa combined with a total elongation of about 30%.

75 FR 64254 - Certain Hot-Rolled Flat-Rolled Carbon Quality Steel Products From Brazil; Final Results of...

Science.gov (United States)

2010-10-19

...-Rolled Carbon Quality Steel Products From Brazil; Final Results of Antidumping Duty Administrative Review... for the Final Results, 75 FR 19369 (April 14, 2010) (Preliminary Results). This review covers sales of... Products from Brazil,'' dated June 22, 2010 (USIMINAS Sales Verification Report). Following the release of...

Structural and spectroscopic characterisations of the surface oxide scales and inclusions present on edge-burst hot-rolled steel coils

International Nuclear Information System (INIS)

Chowdhury, Anirban; Iyyappan, Ramasamy; Majumdar, Dipanwita; Singha, Achintya

2014-01-01

Detailed structural and spectroscopic characterisations have been carried out on the inclusions and the surface oxides present on edge-burst hot-rolled steel coils. Surface scales were characterised through X-ray diffraction (XRD), scanning electron microscopy (SEM) and Raman spectroscopy. Evidence of different types of regular and non-stoichiometric Fe-oxides was found on the cracked surface of the steel wire. Along with the surface scales inclusions with calcium aluminate and spinel was characterized using Raman spectroscopy. The usefulness of Raman spectroscopy has been explored in detail for the characterisation of these inclusions; especially when XRD information ceases to be a limiting tool. The samples collected from the clogged nozzle area were found to be of grossite (CaO·2Al 2 O 3 ) phase and this was also observed in the inclusions in the finished coils. It was found that this particular calcium aluminate phase has a detrimental effect on casting and final finished steel products. - Highlights: • First investigation and surface study report on edge-bursting issue of steel coils. • Detailed characterisations of the inclusions and surface oxide scales in steel. • Influence of a particular type of calcium aluminate phase on process chemistry

Effects of rolling temperature on microstructure, texture, formability and magnetic properties in strip casting Fe-6.5 wt% Si non-oriented electrical steel

International Nuclear Information System (INIS)

Liu, Hai-Tao; Li, Hao-Ze; Li, Hua-Long; Gao, Fei; Liu, Guo-Huai; Luo, Zhong-Han; Zhang, Feng-Quan; Chen, Sheng-Lin; Cao, Guang-Ming; Liu, Zhen-Yu; Wang, Guo-Dong

2015-01-01

Fe-6.5 wt% Si non-oriented electrical steel sheets with a thickness of 0.50 mm were produced by using a new processing route: strip casting followed by hot rolling, intermediate temperature (150–850 °C) rolling and final annealing. The present study focused on exploring the effects of rolling temperature varying from 150 to 850 °C on the microstructure and texture evolution, the formability and final magnetic properties. The microstructure and texture evolution at the various processing steps were investigated in detail by using OM, XRD, EBSD and TEM. It was found that the formability during rolling, the microstructure and texture before and after annealing and final magnetic properties highly depended on rolling temperature. The formability during rolling was gradually improved with increasing rolling temperature due to the slipping of dislocation. In particular, the rolling temperature dominated the formation of in-grain shear bands in the rolled microstructure, which played an important role in the development of final recrystallization microstructure and texture. In the case of lower temperature (150–450 °C) rolling, an inhomogeneous microstructure with a large amount of in-grain shear bands was formed in the rolled sheets, which finally resulted in a fine and inhomogeneous annealing microstructure dominated by mild λ-fiber texture composed of cube and {001}〈210〉 components and α*-fiber texture concentrated on {115}〈5–10 1〉 component. By contrast, in the case of higher temperature (650–850 °C) rolling, a relatively homogeneous microstructure without in-grain shear bands was formed instead in the rolled sheets, which finally led to a coarse and relatively homogeneous annealing microstructure characterized by strong α-fiber and γ-fiber texture. Accordingly, on the whole, both the magnetic induction (B 8 and B 50 ) and iron loss (P 15/50 and P 10/400 ) decreased with raising rolling temperature. - Highlights: • Fe−6.5 wt% Si sheet was

Effects of rolling temperature on microstructure, texture, formability and magnetic properties in strip casting Fe-6.5 wt% Si non-oriented electrical steel

Energy Technology Data Exchange (ETDEWEB)

Liu, Hai-Tao, E-mail: liuht@ral.neu.edu.cn [State Key Laboratory of Rolling and Automation, Northeastern University, P.O. Box 105, Shenyang 110819 (China); Institute of Research of Iron and Steel, Shasteel, Zhangjiagang 215625, Jiangsu (China); Li, Hao-Ze [State Key Laboratory of Rolling and Automation, Northeastern University, P.O. Box 105, Shenyang 110819 (China); Li, Hua-Long [Institute of Research of Iron and Steel, Shasteel, Zhangjiagang 215625, Jiangsu (China); Gao, Fei; Liu, Guo-Huai [State Key Laboratory of Rolling and Automation, Northeastern University, P.O. Box 105, Shenyang 110819 (China); Luo, Zhong-Han; Zhang, Feng-Quan; Chen, Sheng-Lin [National Engineering Research Center for Silicon Steel, Wuhan Iron & Steel (Group) Corp, Wuhan 430083 (China); Cao, Guang-Ming; Liu, Zhen-Yu; Wang, Guo-Dong [State Key Laboratory of Rolling and Automation, Northeastern University, P.O. Box 105, Shenyang 110819 (China)

2015-10-01

Fe-6.5 wt% Si non-oriented electrical steel sheets with a thickness of 0.50 mm were produced by using a new processing route: strip casting followed by hot rolling, intermediate temperature (150–850 °C) rolling and final annealing. The present study focused on exploring the effects of rolling temperature varying from 150 to 850 °C on the microstructure and texture evolution, the formability and final magnetic properties. The microstructure and texture evolution at the various processing steps were investigated in detail by using OM, XRD, EBSD and TEM. It was found that the formability during rolling, the microstructure and texture before and after annealing and final magnetic properties highly depended on rolling temperature. The formability during rolling was gradually improved with increasing rolling temperature due to the slipping of dislocation. In particular, the rolling temperature dominated the formation of in-grain shear bands in the rolled microstructure, which played an important role in the development of final recrystallization microstructure and texture. In the case of lower temperature (150–450 °C) rolling, an inhomogeneous microstructure with a large amount of in-grain shear bands was formed in the rolled sheets, which finally resulted in a fine and inhomogeneous annealing microstructure dominated by mild λ-fiber texture composed of cube and {001}〈210〉 components and α*-fiber texture concentrated on {115}〈5–10 1〉 component. By contrast, in the case of higher temperature (650–850 °C) rolling, a relatively homogeneous microstructure without in-grain shear bands was formed instead in the rolled sheets, which finally led to a coarse and relatively homogeneous annealing microstructure characterized by strong α-fiber and γ-fiber texture. Accordingly, on the whole, both the magnetic induction (B{sub 8} and B{sub 50}) and iron loss (P{sub 15/50} and P{sub 10/400}) decreased with raising rolling temperature. - Highlights: • Fe−6

Microstructure and microtexture evolutions of deformed oxide layers on a hot-rolled microalloyed steel

International Nuclear Information System (INIS)

Yu, Xianglong; Jiang, Zhengyi; Zhao, Jingwei; Wei, Dongbin; Zhou, Cunlong; Huang, Qingxue

2015-01-01

Highlights: • Microtexture development of deformed oxide layers is investigated. • Magnetite shares the {0 0 1} fibre texture with wustite. • Hematite develops the {0 0 0 1} basal fibre parallel to the oxide growth. • Stress relief and ion vacancy diffusion mechanism for magnetite seam. - Abstract: Electron backscatter diffraction (EBSD) analysis has been presented to investigate the microstructure and microtexture evolutions of deformed oxide scale formed on a microalloyed steel during hot rolling and accelerated cooling. Magnetite and wustite in oxide layers share a strong {0 0 1} and a weak {1 1 0} fibres texture parallel to the oxide growth. Trigonal hematite develops the {0 0 0 1} basal fibre parallel to the crystallographic plane {1 1 1} in magnetite. Taylor factor estimates have been conducted to elucidate the microtexture evolution. The fine-grained magnetite seam adjacent to the substrate is governed by stress relief and ions vacancy diffusion mechanism

Behaviors of Deformation, Recrystallization and Textures Evolution of Columnar Grains in 3%Si Electrical Steel Slabs

Directory of Open Access Journals (Sweden)

SHAO Yuan-yuan

2017-11-01

Full Text Available The behaviors of deformation and recrystallization and textures evolution of 3% (mass fraction Si columnar-grained electrical steel slabs were investigated by electron backscatter diffractometer technique and X-ray diffraction. The results indicate that the three columnar-grained samples have different initial textures with the long axes arranged along rolling, transverse and normal directions. Three shear orientations can be obtained in surface layer after hot rolling, of which Goss orientation is formed easily. The α and γ fibre rolling orientations are obtained in RD sample, while strong γ fibre orientations in TD sample and sharp {100} orientations in ND sample are developed respectively. In addition, cube orientation can be found in all the three samples. The characteristics of hot rolled orientations in center region reveal distinct dependence on initial columnar-grained orientations. Strong {111}〈112〉 orientation in RD and TD samples separately comes from Goss orientation of hot rolled sheets, and sharp rotated cube orientation in ND sample originates from the initial {100} orientation of hot rolled sheets after cold rolling. Influenced by initial deviated orientations and coarse grain size, large orientation gradient of rotated cube oriented grain can be observed in ND sample. The coarse {100} orientated grains of center region in the annealed sheets show the heredity of the initial columnar-grained orientations.

Powdering of Hot-dip Galvannealed steel using Finite Element Analysis

International Nuclear Information System (INIS)

Kim, D. W.; Jang, Y. C.; Lee, Y. S.; Kim, S. I.

2007-01-01

Demand for hot-dip galvannealed steel has been increased due to it high corrosion resistance, paintability, and formability in automotive industry. Coating of Hot-dip galvannealed steel consists of various Fe-Zn intermetallic compounds. Since the coating is hard and therefore it is very brittle, the surface of steel sheet is easy to be ruptured during second manufacturing processing. This is called as powdering. Hence, various research have been carried out to prohibit powdering for improving the quality of GA steel during second manufacturing processing. This paper performed finite element analysis to evaluate local powdering and compared FEA results with V-bending test. The effects of punch radius and coating strength on the powdering was examined

Adhesiveness of cold rolled steels for car body parts

Directory of Open Access Journals (Sweden)

Kleiner Marques Marra

2007-09-01

Full Text Available The aim of this work was to evaluate the adhesiveness of uncoated and zinc-electrogalvanized steel sheets used in the automotive industry. Three types of adhesives, one acrylic and two epoxy resins, were employed to join low carbon cold rolled steels, one uncoated and another electrogalvanized, both previously degreased or chemically pickled. Mechanical strength of the joints was evaluated by the T-peel and tensile strength tests. Steel grade, surface condition and heating below the cure temperatures did not influence the joints' mechanical strength. However, their shear strength decreased drastically as the test temperature increased. The exposure of the joints to an atmosphere with 90% relative humidity at 40 °C caused reduction of their shear strength. Epoxy adhesives showed higher mechanical strength, but exhibited higher degradation by humidity.

Microstructural characterization of Zr1Nb alloy after hot rolling

Energy Technology Data Exchange (ETDEWEB)

Souza, A.C. [Universidade Estadual do Mato Grosso do Sul (UEMS), MS (Brazil); Rossi, J.L.; Martinez, L.G.; Mucsi, C.S. [Instituto de Pesquisas Energéticas e Nucleares (IPEN/CNEN-SP), São Paulo, SP (Brazil); Tsakiropoulos, P. [University of Sheffield (United Kingdom); Ceoni, F.C.; Grandini, C.R. [Universidade Estadual Paulista Julio de Mesquita Filho (UNESP), SP (Brazil)

2016-07-01

Full text: The different research lines within the scope in engineering and materials science have developed new materials that can be used in different industrial sectors, such as, energy, health and transportation. For the nuclear industry, for example, the Zr alloys, are of great interest due to its good mechanical properties, excellent corrosion resistance and above all, the high permeability to thermal neutrons. In the health sector, the zirconium poses one of the lowest Young's modulus when compared to other metallic biomaterials, e.g., pure Zr is 68 GPa, bone mineral hydroxyapatite is 80 GPa, for Ti alloys is 90 GPa and above, for Nb is 105 GPa and stainless steels above 189 GPa. This is particularly important for implants in bones, whose elasticity modulus can reach 30 GPa and it is desirable an as close match as possible. However, the zirconium alloys, have great chemical affinity with oxygen and nitrogen. Moreover, oxides and nitrides may form during the melting process, heat treatment and hot rolling, changing the physic-chemical properties of the alloy. This experimental work shows the results of the evolution of the microstructure after hot rolling of the Zr1Nb alloy. It was possible to confirm the absence of formation of oxides and nitrides, thus confirming the of the experimental method of melting and hot rolling of the Zr1Nb alloy. (author)

Simulation of accelerated strip cooling on the hot rolling mill run-out roller table

International Nuclear Information System (INIS)

Muhin, U.; Belskij, S.; Makarov, E.; Koinov, T.

2013-01-01

Full text: A mathematical model of the thermal state of the metal on the run-out roller table of a continuous wide hot-strip mill is presented. The mathematical model takes into account the heat generation during the polymorphic γ → α transformation of super cooled austenite phase and the influence of chemical composition on the physical properties of the steel. The model allows the calculation of modes of accelerated cooling of strips on the run-out roller table of a continuous wide hot strip mill. Winding temperature calculation error does not exceed 20 °C for 98.5 % of the strips from low-carbon and low-alloyed steels. key words: hot rolled, wide-strip, accelerated cooling, run-out roller table, polymorphic transformation, mathematical modeling

Layer texture of hot-rolled BCC metals and its significance for stress-corrosion cracking of main gas pipelines

Science.gov (United States)

Perlovich, Yu. A.; Isaenkova, M. G.; Krymskaya, O. A.; Morozov, N. S.

2016-10-01

Based on data of X-ray texture analysis of hot-rolled BCC materials it was shown that the layerwise texture inhomogeneity of products is formed during their manufacturing. The effect can be explained by saturation with interstitial impurities of the surface layer, resulting in dynamical deformation aging (DDA). DDA prevents the dislocation slip under rolling and leads to an increase of lattice parameters in the external layer. The degree of arising inhomogeneity correlates with the tendency of hot-rolled sheets and obtained therefrom tubes to stress-corrosion cracking under exploitation, since internal layers have a compressive effect on external layers, and prevents opening of corrosion cracks at the tube surface.

Plasticity of low carbon steel in a hot state

Energy Technology Data Exchange (ETDEWEB)

Konovalov, V P; Rizol' , A I; Shram, N N [Ural' skij Nauchno-Issledovatel' skij Inst. Chernykh Metallov, Sverdlovsk (USSR)

1977-07-01

The hot ductility (in tapered-specimen piersing test and the in wedge-shaped specimen rolling test) is studied of the Armeo-type low carbon steel produced by vacuum induction and open hearth techniques. The variations of the chemical composition within specified ranges, particularly as regards sulphur, oxygen and the Mn/S ratio, have a marked effect on the processing ductility. The temperature range of brittle fracture and acceptable hot working reductions as functions of the chemical composition have been revealed.

Plasticity of low carbon steel in a hot state

International Nuclear Information System (INIS)

Konovalov, V.P.; Rizol', A.I.; Shram, N.N.

1977-01-01

The hot ductility (in tapered-specimen piersing test and the in wedge-shaped specimen rolling test) is studied of the Armeo-type low carbon steel produced by vacuum induction and open hearth techniques. The variations of the chemical composition within specified ranges, particularly as regards sulphur, oxygen and the Mn/S ratio, have a marked effect on the processing ductility. The temperature range of brittle fracture and acceptable hot working reductions as functions of the chemical composition have been revealed

Deformation and damage mechanisms of zinc coatings on hot-dip galvanized steel sheets: Part II. Damage modes

Science.gov (United States)

Parisot, Rodolphe; Forest, Samuel; Pineau, André; Grillon, François; Demonet, Xavier; Mataigne, Jean-Michel

2004-03-01

Zinc-based coatings are widely used for protection against corrosion of steel-sheet products in the automotive industry. The objective of the present article is to investigate the damage modes at work in three different microstructures of a zinc coating on an interstitial-free steel substrate under tension, planestrain tension, and expansion loading. Plastic-deformation mechanisms are addressed in the companion article. Two main fracture mechanisms, namely, intergranular cracking and transgranular cleavage fracture, were identified in an untempered cold-rolled coating, a tempered cold-rolled coating, and a recrystallized coating. No fracture at the interface between the steel and zinc coating was observed that could lead to spalling, in the studied zinc alloy. A complex network of cleavage cracks and their interaction with deformation twinning is shown to develop in the material. An extensive quantitative analysis based on systematic image analysis provides the number and cumulative length of cleavage cracks at different strain levels for the three investigated microstructures and three loading conditions. Grain refinement by recrystallization is shown to lead to an improved cracking resistance of the coating. A model for crystallographic cleavage combining the stress component normal to the basal plane and the amount of plastic slip on the basal slip systems is proposed and identified from equibiaxial tension tests and electron backscattered diffraction (EBSD) analysis of the cracked grains. This analysis requires the computation of the nonlinear stress-strain response of each grain using a crystal-plasticity constitutive model. The model is then applied successfully to other loading conditions and is shown to account for the preferred orientations of damaged grains observed in the case of plane-strain tension.

Microstructural Evolution During Cold Rolling and Subsequent Annealing in Low-Carbon Steel with Different Initial Microstructures

Science.gov (United States)

Ogawa, Toshio; Dannoshita, Hiroyuki; Maruoka, Kuniaki; Ushioda, Kohsaku

2017-08-01

Microstructural evolution during cold rolling and subsequent annealing of low-carbon steel with different initial microstructures was investigated from the perspective of the competitive phenomenon between recrystallization of ferrite and reverse phase transformation from ferrite to austenite. Three kinds of hot-rolled sheet specimens were prepared. Specimen P consisted of ferrite and pearlite, specimen B consisted of bainite, and specimen M consisted of martensite. The progress of recovery and recrystallization of ferrite during annealing was more rapid in specimen M than that in specimens P and B. In particular, the recrystallized ferrite grains in specimen M were fine and equiaxed. The progress of ferrite-to-austenite phase transformation during intercritical annealing was more rapid in specimen M than in specimens P and B. In all specimens, the austenite nucleation sites were mainly at high-angle grain boundaries, such as those between recrystallized ferrite grains. The austenite distribution was the most uniform in specimen M. Thus, we concluded that fine equiaxed recrystallized ferrite grains were formed in specimen M, leading to a uniform distribution of austenite.

Effect of two-step intercritical annealing on microstructure and mechanical properties of hot-rolled medium manganese TRIP steel containing δ-ferrite

International Nuclear Information System (INIS)

Xu, Yun-bo; Hu, Zhi-ping; Zou, Ying; Tan, Xiao-dong; Han, Ding-ting; Chen, Shu-qing; Ma, De-gang; Misra, R.D.K.

2017-01-01

The microstructure-properties relationship, work-hardening behavior and retained austenite stability have been systematically investigated in a hot-rolled medium manganese transformation-induced-plasticity (TRIP) steel containing δ-ferrite subjected to one-step and two-step intercritical annealing. The steel exhibited tensile strength of 752 MPa and total elongation of 52.7% for one-step intercritical annealing at 740 °C, tensile strength of 954 MPa and total elongation of 39.2% in the case of intercritical quenching at 800 °C and annealing at 740 °C. The austenite obtained by two-step annealing mostly consists of refined lath structures and increased fraction of block-type particles existing at various kinds of sites, which is highly distinguished from those characterized by long lath morphology and small amounts of granular shape in one-step annealed samples. In spite of a higher C and Mn content in austenite and finer austenite laths, two-step annealing can lead to an active and continuous TRIP effect provided by a mixed blocky and lath-type austenitic structure with lower stability, contributing to a higher UTS. In contrast, one-step annealing gave rise to a less active but sustained TRIP effect given by the dominant lath-like austenite having higher stability, leading to a very high elongation. The further precipitation of vanadium carbides and the presence of both dislocation substructure and fine equiaxed grain in ferrite matrix facilitate the increase of yield strength after double annealing. - Highlights: • A novel two-step process was applied to a hot-rolled Fe-0.2C-6.5Mn-3Al steel. • The interplay between different microstructures and mechanical properties was studied. • Two-step annealing led to an active and continuous TRIP. • An outstanding combination of strength of 954 MPa and elongation of 39.2% was obtained.

Effect of two-step intercritical annealing on microstructure and mechanical properties of hot-rolled medium manganese TRIP steel containing δ-ferrite

Energy Technology Data Exchange (ETDEWEB)

Xu, Yun-bo [State Key Laboratory of Rolling and Automation, Northeastern University, Shenyang 110819, People' s Republic China (China); Hu, Zhi-ping, E-mail: huzhiping900401@126.com [State Key Laboratory of Rolling and Automation, Northeastern University, Shenyang 110819, People' s Republic China (China); Zou, Ying; Tan, Xiao-dong; Han, Ding-ting; Chen, Shu-qing [State Key Laboratory of Rolling and Automation, Northeastern University, Shenyang 110819, People' s Republic China (China); Ma, De-gang [Tangshan Iron and Steel Company, Tangshan 063000, People' s Republic China (China); Misra, R.D.K. [Laboratory for Excellence in Advanced Steel Research, Department of Metallurgical, Materials and Biomedical Engineering, University of Texas at El Paso, TX 79968 (United States)

2017-03-14

The microstructure-properties relationship, work-hardening behavior and retained austenite stability have been systematically investigated in a hot-rolled medium manganese transformation-induced-plasticity (TRIP) steel containing δ-ferrite subjected to one-step and two-step intercritical annealing. The steel exhibited tensile strength of 752 MPa and total elongation of 52.7% for one-step intercritical annealing at 740 °C, tensile strength of 954 MPa and total elongation of 39.2% in the case of intercritical quenching at 800 °C and annealing at 740 °C. The austenite obtained by two-step annealing mostly consists of refined lath structures and increased fraction of block-type particles existing at various kinds of sites, which is highly distinguished from those characterized by long lath morphology and small amounts of granular shape in one-step annealed samples. In spite of a higher C and Mn content in austenite and finer austenite laths, two-step annealing can lead to an active and continuous TRIP effect provided by a mixed blocky and lath-type austenitic structure with lower stability, contributing to a higher UTS. In contrast, one-step annealing gave rise to a less active but sustained TRIP effect given by the dominant lath-like austenite having higher stability, leading to a very high elongation. The further precipitation of vanadium carbides and the presence of both dislocation substructure and fine equiaxed grain in ferrite matrix facilitate the increase of yield strength after double annealing. - Highlights: • A novel two-step process was applied to a hot-rolled Fe-0.2C-6.5Mn-3Al steel. • The interplay between different microstructures and mechanical properties was studied. • Two-step annealing led to an active and continuous TRIP. • An outstanding combination of strength of 954 MPa and elongation of 39.2% was obtained.

Effects of homogenization treatment on recrystallization behavior of 7150 aluminum sheet during post-rolling annealing

International Nuclear Information System (INIS)

Guo, Zhanying; Zhao, Gang; Chen, X.-Grant

2016-01-01

The effects of two homogenization treatments applied to the direct chill (DC) cast billet on the recrystallization behavior in 7150 aluminum alloy during post-rolling annealing have been investigated using the electron backscatter diffraction (EBSD) technique. Following hot and cold rolling to the sheet, measured orientation maps, the recrystallization fraction and grain size, the misorientation angle and the subgrain size were used to characterize the recovery and recrystallization processes at different annealing temperatures. The results were compared between the conventional one-step homogenization and the new two-step homogenization, with the first step being pretreated at 250 °C. Al_3Zr dispersoids with higher densities and smaller sizes were obtained after the two-step homogenization, which strongly retarded subgrain/grain boundary mobility and inhibited recrystallization. Compared with the conventional one-step homogenized samples, a significantly lower recrystallized fraction and a smaller recrystallized grain size were obtained under all annealing conditions after cold rolling in the two-step homogenized samples. - Highlights: • Effects of two homogenization treatments on recrystallization in 7150 Al sheets • Quantitative study on the recrystallization evolution during post-rolling annealing • Al_3Zr dispersoids with higher densities and smaller sizes after two-step treatment • Higher recrystallization resistance of 7150 sheets with two-step homogenization

77 FR 70142 - Initialed Draft Revision to the Agreement Suspending the Antidumping Investigation on Certain Hot...

Science.gov (United States)

2012-11-23

... the Agreement Suspending the Antidumping Investigation on Certain Hot-Rolled Flat-Rolled Carbon... revision to the Agreement Suspending the Antidumping Investigation on Certain Hot-Rolled Flat-Rolled Carbon...'') investigation on hot-rolled flat-rolled carbon-quality steel products (``hot-rolled steel'') from the Russian...

Investigation of the hot ductility of a high-strength boron steel

International Nuclear Information System (INIS)

Güler, Hande; Ertan, Rukiye; Özcan, Reşat

2014-01-01

In this study, the high-temperature ductility behaviour of an Al–Si-coated 22MnB5 sheet was investigated. The mechanical properties of Al–Si-coated 22MnB5 boron steel were examined via hot tensile tests performed at temperatures ranging from 400 to 900 °C at a strain rate of 0.083 s −1 . The deformation and fracture mechanisms under hot tensile testing were considered in relation to the testing data and to the fracture-surface observations performed via SEM. The hot ductility of the tested boron steel was observed as a function of increasing temperature and the Al–Si-coated 22MnB5 boron steel exhibited a ductility loss at 700 °C

The effect of microstructure on the sheared edge quality and hole expansion ratio of hot-rolled 700 MPa steel

Science.gov (United States)

Kaijalainen, A.; Kesti, V.; Vierelä, R.; Ylitolva, M.; Porter, D.; Kömi, J.

2017-09-01

The effects of microstructure on the cutting and hole expansion properties of three thermomechanically rolled steels have been investigated. The yield strength of the studied 3 mm thick strip steels was approximately 700 MPa. Detailed microstructural studies using laser scanning confocal microscopy (LCSM), FESEM and FESEM-EBSD revealed that the three investigated materials consist of 1) single-phase polygonal ferrite, 2) polygonal ferrite with precipitates and 3) granular bainite. The quality of mechanically sheared edges were evaluated using visual inspection and LSCM, while hole expansion properties were characterised according to the methods described in ISO 16630. Roughness values (Ra and Rz) of the sheet edge with different cutting clearances varied between 12 µm to 21 µm and 133 µm to 225 µm, respectively. Mean hole expansion ratios varied from 28.4% to 40.5%. It was shown that granular bainite produced the finest cutting edge, but the hole expansion ratio remained at the same level as in the steel comprising single-phase ferrite. This indicates that a single-phase ferritic matrix enhances hole expansion properties even with low quality edges. A brief discussion of the microstructural features controlling the cutting quality and hole expansion properties is given.

Effect of hot rolling on the microstructure and mechanical properties of Ti3Al based dual phase alloys

International Nuclear Information System (INIS)

Wu, J.; Zhang, L.; Hua, W.; Qiu, G.

1999-01-01

Development of α 2 -Ti 3 Al based dual phase alloys have shown some promising potentials in property improvement by introducing Ti 5 Si 3 silicide phase into the matrix via Si alloying. However, the presence of coarse network of Ti 5 Si 3 phase formed by eutectic reaction in the as-cast state also embrittles the alloy. Both hot rolling and powder metallurgy are considered to be the possible ways to refine the Ti 5 Si 3 phase in the matrix. Two Ti-Al-Si-Nb alloys whose Si contents are 2 and 5 at.% respectively were arc melted into ingots and then hot rolled to sheets in this investigation. Optical metallographic examination correlates the microstructures of the as-cast and as-rolled alloys with the different rolling amounts, showing that the coarse silicide network is broken into small particles after hot rolling. Mechanical property testing from room temperature to 800 C indicates that the strength and plastic elongation of the hot-rolled alloys are much higher than those of the as-cast ones. The data obtained in this investigation are comparable with those obtained in the P/M processed specimens. Fracture surfaces of the alloys are also examined

Hot-rolling metals in vacuum. Information circular

International Nuclear Information System (INIS)

Beall, R.A.; Worthington, R.B.; Blickensderfer, R.

1979-01-01

The process of hot-rolling metals, alloys, and composites in vacuum is studied. First, a comprehensive review of the literature is presented, including the advantages and disadvantages of using vacuum. Next, details of hot-rolling titanium, chromium, and molybdenum-iron bimetal are given. Finally, the design of new equipment is described

75 FR 47541 - Hot-Rolled Flat-Rolled Carbon-Quality Steel Products from Brazil and Japan: Final Results of...

Science.gov (United States)

2010-08-06

... DEPARTMENT OF COMMERCE International Trade Administration [A-351-828, A-588-846] Hot-Rolled Flat..., Department of Commerce. SUMMARY: On April 1, 2010, the Department of Commerce (the Department) initiated... Department has conducted expedited (120-day) sunset reviews for both orders pursuant to 19 CFR 351.218(e)(1...

Possible influences on textures in unalloyed steels and their effects on steel properties

International Nuclear Information System (INIS)

Grossterlinden, R.; Imlau, K.P.; Kawalla, R.; Lotter, U.; Reip, C.-P.

1996-01-01

Textures in steels play an essential role for applications where anisotropic properties are favourable. For the example of deep-drawing steel sheet the correlation between parameters characterising the behaviour in the deep-drawing process, as Lankford r-value and planar anisotropy Δr, and the crystallographic texture is considered. Furthermore, the development of texture in the course of manufacturing cold strip is followed for unalloyed and microalloyed deep-drawing grades. For representation of typical features of textures the method of orientation distribution functions (ODF) together with the description of texture by characteristic fibres is used. In detail, the parameters influencing textures, such as chemical composition, finishing temperature in the hot-rolling mill (in relation to the austenite or ferrite region), transformation behaviour, cold-rolling reduction and the course of temperature during recrystallizing annealing, are discussed. From the given survey it may be concluded, that in the manufacturing process there are many possibilities to control the texture of the finished product. Finally, it is shown that the impact of textures on the r-value can be calculated with high precision. On the other hand, the formation of texture itself, particularly during hot-rolling, transformation and recrystallization after cold-rolling, at present can be calculated and modelled only in simple cases. (orig.)

Effect of Rolling and Subsequent Annealing on Microstructure, Microtexture, and Properties of an Experimental Duplex Stainless Steel

Science.gov (United States)

Mandal, Arka; Patra, Sudipta; Chakrabarti, Debalay; Singh, Shiv Brat

2017-12-01

A lean duplex stainless steel (LDSS) has been prepared with low-N content and processed by different thermo-mechanical schedules, similar to the industrial processing that comprised hot-rolling, cold-rolling, and annealing treatments. The microstructure developed in the present study on low-N LDSS has been compared to that of high-N LDSS as reported in the literature. As N is an austenite stabilizer, lower-N content reduced the stability of austenite and the austenite content in low-N LDSS with respect to the conventional LDSS. Due to low stability of austenite in low-N LDSS, cold rolling resulted in strain-induced martensitic transformation and the reversion of martensite to austenite during subsequent annealing contributed to significant grain refinement within the austenite regions. δ-ferrite grains in low-N LDSS, on the other hand, are refined by extended recovery mechanism. Initial solidification texture (mainly cube texture) within the δ-ferrite region finally converted into gamma-fiber texture after cold rolling and annealing. Although MS-brass component dominated the austenite texture in low-N LDSS after hot rolling and cold rolling, that even transformed into alpha-fiber texture after the final annealing. Due to the significant grain refinement and formation of beneficial texture within both austenite and ferrite, good combination of strength and ductility has been achieved in cold-rolled and annealed sample of low-N LDSS steel.

Analysis of the strengthening mechanisms in pipeline steels as a function of the hot rolling parameters

International Nuclear Information System (INIS)

Carretero Olalla, V.; Bliznuk, V.; Sanchez, N.; Thibaux, P.; Kestens, L.A.I.; Petrov, R.H.

2014-01-01

The yield strength of different pipeline steel grades, rolled under four different conditions, was correlated with calculated strengthening contributions. Slabs with the same composition were rolled under identical roughing conditions but varied finish rolling temperature (FRT). Two cooling routes, consisting of accelerated water cooling condition (ACC) followed by slow cooling in an oven to simulate coiling and air cooling were applied after the last rolling pass. The microstructures obtained after each thermo mechanical controlled process (TMCP) schedule, were characterized using Transmission Electron Microscopy (TEM), Inductively Coupled Plasma Mass Spectrometry (ICP-MS) and Electron backscatter diffraction (EBSD). The mechanical properties of the plates were determined by means of tensile tests and Charpy V-notch impact test. It was confirmed that a combination of fast cooling rate and low finish rolling temperature produces higher strength than the slow cooling rate and high finish rolling temperature. Contributions to the strengthening arising from the various microstructural features like solid solution strengthening, grain size, dislocation density and precipitation hardening, were analyzed using Taylor, Hall–Petch and Ashby–Orowan approaches. The root of the sum of the squares method was applied to link the experimental with the model-predicted strength. It is believed that this approach provides a better understanding of the effect of TMCP parameters on the microstructure and strengthening mechanisms in pipeline steels

Influence of the Radiation Shield on the Temperature of Rails Rolled in the Reversing Mill

Directory of Open Access Journals (Sweden)

Gołdasz A.

2015-04-01

Full Text Available The paper presents a mathematical model of heat transfer during cooling of hot-rolled rails in the reversing mill. The influence of the radiation shield on the temperature of rolled rails has been analyzed. The heat transfer model for cooling a strip covered by the thermal shield has been presented. The two types of shields build of steel and aluminum sheets separated with insulating layer have been studded. Calculations have been performed with self developed software which utilizes the finite element method.

Plastic anisotropy of straight and cross rolled molybdenum sheets

International Nuclear Information System (INIS)

Oertel, C.-G.; Huensche, I.; Skrotzki, W.; Knabl, W.; Lorich, A.; Resch, J.

2008-01-01

The microstructure, texture and mechanical properties of molybdenum sheets produced by different rolling processes were investigated by orientation imaging in the scanning electron microscope, X-ray diffraction and tensile tests, respectively. For comparable recrystallization degree of the sheets investigated, straight rolling with low reduction ratio produces α-fiber textures with a maximum at {100} . At higher rolling degrees the maximum shifts to {112} . Cross rolling increases the rotated cube component {100} . The strong differences in the texture measured are reflected in the plastic anisotropy characterized by differences in the yield stress and Lankford parameter which were measured along directions in the rolling plane at angles of 0 deg., 45 deg. and 90 deg. with the rolling direction. The Taylor-Bishop-Hill theory is used successfully to qualitatively explain the plastic anisotropy

Travel to Steel Warehouse Inc., Southbend, Indiana. Trip report, May 4, 1995

International Nuclear Information System (INIS)

Hill, N.F.

1995-01-01

On May 4, 1995 the author visited a steel plate and coil, cold reduction facility at Steel Warehouse Inc. located in South Bend, Indiana about 150 miles from Argonne. Some very interesting facts were learned about cold reduction of hot rolled steel during this visit. The company selected is only a cold reduction mill and buys steel from a number of steel producers. The author spent a total of about three hours with these people, and this included a tour of their pickling line, the small cold reduction mill which at present is limited to 15.5 in width maximum, and their large cold reduction mill which produces sheet and coil up to 72 in. wide. Some of the things that were learned, that will have an impact on the production of the Atlas steel plates are given here. (1) Hot rolled coils have some inherent, interesting, characteristics that must be taken into consideration when being cold reduced. (2) The monitoring of the coil thickness is only done along the center line of the coil, this has a serious impact on QC of plates cut from this coil for a number of reasons. (3) Hot rolled coils of steel in this particular instance may come from a number of different sources. This could cause problems if magnetic permeability is a serious issue. It was the author's impression that this facility is fairly typical of what one might expect from any similar facility

77 FR 26600 - WTO Dispute Settlement Proceeding Regarding United States-Countervailing Measures on Certain Hot...

Science.gov (United States)

2012-05-04

... Proceeding Regarding United States-- Countervailing Measures on Certain Hot-Rolled Carbon Steel Flat Products... certain hot-rolled carbon steel flat products from India. That request may be found at www.wto.org... requested consultations concerning countervailing measures regarding certain hot-rolled carbon steel flat...

77 FR 49477 - WTO Dispute Settlement Proceeding Regarding United States-Countervailing Measures on Certain Hot...

Science.gov (United States)

2012-08-16

... Proceeding Regarding United States-- Countervailing Measures on Certain Hot-Rolled Carbon Steel Flat Products... certain hot-rolled carbon steel flat products from India. That request may be found at www.wto.org... countervailing measures regarding certain hot-rolled carbon steel flat products from India (Investigation C-533...

Influence of structure and properties of tubular billets of the 12 Kh 18N10T steel on deformability of tubes at cold-rolling mills

International Nuclear Information System (INIS)

Vil'yams, O.S.; Bol'shova, N.M.; Olejnik, O.V.; Velikotnaya, E.S.

1979-01-01

Metallographic analysis of the defects of the ''oblique cracks'' type on the surface of hot-rolled tubes of the 12Kh18N10T steel has been carried out. Recommended is the complex of mechanical properties and the structure factors (grain size) of conversion hot-rolled tubes, providing the combination of ductility and high rapture strength during rolling at pilger mills. At a grain size not coarser than number 5, a billet must have σsub(T) 5 >=40 %. Hot-rolled coarse-grained billet is not recommended for warm rolng because of high strain hardening

Numerical simulation of springback of medium-thick plates in local hot rolling

Directory of Open Access Journals (Sweden)

XIE Dong

2017-10-01

Full Text Available [Objectives] In order to understand the factors of springback in the local hot rolling of medium-thick steel plates,[Methods] a 3D thermal-elastic-plastic analysis is conducted to investigate the factors affecting the amount of springback. Through a series of numerical analyses,the influence of deformation temperature,temperature field distribution,plate size and local loading are examined. [Results] The results show that when the deformation temperature exceeds a certain level at which material yield stress begins to decrease significantly,the springback will reduce markedly with the increase in temperature. Due to the distribution characteristics of the deformation area,the influence of temperature distribution on springback where the local deformation scale is larger is dominated by the three dimensions of temperature field distribution. Changes in the length and width of the plate have a certain influence on the springback,in which changes to the length of a plate where the local deformation scale is larger have a more obvious influence on springback. The springback of the plate decreases with the increase of local loading. [Conclusions] The results of this study can assist in the optimization of parameters in the automatic hot rolling of thick plates,while also having a basic guiding effect on the further study of springback in the local hot rolling of thick plates.

Effects of Cold Rolling Reduction and Initial Goss Grains Orientation on Texture Evolution and Magnetic Performance of Ultra-thin Grain-oriented Silicon Steel

Directory of Open Access Journals (Sweden)

LIANG Rui-yang

2017-06-01

Full Text Available The ultra-thin grain-oriented silicon steel strips with a thickness of 0.06-0.12mm were produced by one-step-rolling methods with different Goss-orientation of grain-oriented silicon steel sheets. The effect of cold rolling reduction and initial Goss-orientation of samples on texture evolution and magnetic performance of ultra-thin grain-oriented silicon steel strips was studied by EBSD. The result shows that with the increase of cold rolling reduction and decrease of strips thickness, the recrystallization texture is enhanced after annealing.When the cold rolling reduction is 70%,RD//〈001〉 recrystallization texture is the sharpest, and the magnetic performance is the best. The higher degree of Goss orientation in initial sample is, the better magnetic performance of ultra-thin grain-oriented silicon steel.Therefore, for producing an ultra-thin grain-oriented silicon steel with high performance, a material with a concentrated orientation of Goss grains can be used.

The evolution of texture in aluminum alloy sheet during asymmetric rolling

International Nuclear Information System (INIS)

Kim, K-H.; Lee, D.N.

2000-01-01

Asymmetric rolling, in which the upper and lower roll radii are different, imposes shear deformation on sheets through the thickness, which in turn gives rise to shear deformation textures in the sheets through the thickness. A component of ND// in the shear deformation textures can improve the plastic strain ratios of aluminum sheets. In order to understand the evolution of ND// , the strain histories and distributions in the sheets during the asymmetric rolling are calculated by the finite element method. The strain history and distribution are used to calculate crystallographic orientations and stable orientations based on the Taylor-Bishop-Hill theory and the Renouward-Wintenberger theory. The shear deformation texture can vary with the ratio of shear to normal strain increments. As the ratio increases from zero to infinity, the texture moves from the plane strain compression texture (β fiber) to the ideal shear deformation texture consisting of {001} , {111} , and {111} . The ratio increases with rolling reduction per pass in asymmetric rolling. However, it is practically difficult to the rolling reduction per pass high enough to obtain the ideal shear deformation texture. Imposing the positive and negative shear deformations on the sheet by reversing the shearing direction can give rise to the ideal shear deformation texture. This has been discussed. (author)

Development of manufacturing process for production of 500 MWe calandria sheets

International Nuclear Information System (INIS)

Hariharan, R.; Ramesh, P.; Lakshminarayana, B.; Bhaskara Rao, C.V.; Pande, P.; Agarwala, G.C.

1992-01-01

Calandria tubes made of zircaloy-2 are being used as structural components in pressurised heavy water power reactors. The sheets required for producing calandria tube for 235 MWe reactors are being manufactured at Zircaloy Fabrication Plant (ZFP), NFC utilizing a 2 Hi/4 Hi rolling mill procured for the purpose, by carrying out cold rolling process to achieve the required size after hot rolling suitable extruded slabs. Due to limitation of width of the sheet that can be rolled with the mill as well as the size of the slab that can be extruded with the existing press, difficulties arose in producing acceptable full length sheets of size 6600 mm long x 435 mm wide x 1.6 mm thick for manufacturing 500 MWe calandria tube. This paper deals with the details of the process problem resolved. They are: (a)designing of suitable hot and cold rolling pass schedules, (b)selection and standardization of process parameters such as beta quenching, hot rolling and cold rolling, and (c)details of the overall manufacturing process. Due to implementation of above, sheets required for manufacturing 500 MWe calandria tube sheets were successfully rolled. About 40 nos. of acceptable full length sheets have already been manufactured. (author). 1 fig., 3 tabs

Microstructural changes after control rolling and interrupted accelerated cooling simulations in pipeline steel

Energy Technology Data Exchange (ETDEWEB)

Sanchez-Mourino, Nuria; Petrov, Roumen [Department of Materials Science and Engineering, Ghent University, Technologiepark Zwijnaarde 903, B-9052 Ghent (Belgium); Bae, Jin-Ho; Kim, Kisoo [Sheet Products and Process Research Group, POSCO, Jeonnam, 545-090 (Korea, Republic of); Kestens, Leo A.I. [Department of Materials Science and Engineering, Ghent University, Technologiepark Zwijnaarde 903, B-9052 Ghent (Belgium); Department of Materials Science and Engineering, Delft University of Technology, Mekelweg 2, 2628 CD, Delft (Netherlands)

2011-04-15

The {gamma}-{alpha} transformation and final microstructure in pipeline steel was studied by carrying out a number of physical simulations of industrial hot rolling schedules. Particularly, the effect of the reheating temperature, deformation and cooling parameters on the transformation temperatures and final grain size were considered with a goal to obtain an appropriate thermo-mechanical processing route which will generate appropriate microstructures for pipeline applications. The CCT diagram of the steel was derived experimentally by means of dilatometric tests. Hot torsion experiments were applied in a multi-deformation cycle at various temperatures in the austenite region to simulate industrial rolling schedules. By variation of the reheating temperature, equivalent strain, and accelerated cooling, different types of microstructures were obtained. It was found that the deformation increases the transformation temperatures whereas the higher cooling rates after deformation decrease them. Post-deformation microstructure consists of fine bainitic-ferrite grains with dispersed carbides and small amount of dispersed martensite/austenite islands which can be controlled by varying the reheating temperature, deformation and post-deformation cooling. The detailed microstructure characteristics obtained from the present work could be used to optimize the mechanical properties, strength and toughness of pipeline steel grades by an appropriate control of the thermo-mechanical processing. (Copyright copyright 2011 WILEY-VCH Verlag GmbH and Co. KGaA, Weinheim)

Effect of the Die Temperature and Blank Thickness on the Formability of a Laser-Welded Blank of a Boron Steel Sheet with Removing Al-Si Coating Layer

Directory of Open Access Journals (Sweden)

M. S. Lee

2014-05-01

Full Text Available Reducing carbon emissions has been a major focus in the automobile industry to address various environmental issues. In particular, studies on parts comprised of high strength sheets and light car bodies are ongoing. Accordingly, this study examined the use of boron steel, which is commonly used in high strength sheets. Boron steel is a type of sheet used for hot stamping parts. Although it has high strength, the elongation is inferior, which reduces its crash energy absorption capacity. To solve this problem, two sheets of different thickness were welded so the thin sheet would absorb crash energy and the thick sheet would work as a support. Boron steel, however, may show weakening at the welding spot due to the Al-Si coating layer used to prevent oxidation from occurring during the welding process. Therefore, a certain part of the coating layer of a double-thickness boron steel sheet that is welded in the hot stamping process is removed through laser ablation, and the formability of the hot-work was examined.

Hot-Dip Coating of Lead-free Aluminum on Steel Substrates with Ultrasonic Vibration

Institute of Scientific and Technical Information of China (English)

无

2008-01-01

Hot-dip coating has been practically employed in manufacturing zinc alloy coated steel sheets. However, it is difficult to coat aluminum alloy on a bulky steel substrate without sufficient preheating, because a rapidly solidified layer containing gas babbles is formed on a substrate surface. A variety of iron-aluminides are also formed at the interface of a steel and aluminum hot-dip coating system, which is the main difficulty in joining of steel with aluminum. Ultrasonic vibration was applied to a steel substrate during hot-dip coating of aluminum alloy to control a rapidly solidified layer and a brittle reaction layer. Hot dipping of columnar steel substrates into molten aluminum alloy (Al-2.7 mass fraction Si-4.6 mass fraction Sn) was carried out through the use of a Langevin oscillator with resonant frequency of 19.5 kHz. The application of ultrasonic vibration is quite effective to control a rapidly solidified layer and a surface oxide layer from a substrate surface by the sonocapillary effect based on a cavitation phenomenon, so that the intimate contact is achieved at the beginning of hot-dip coating. The application of ultrasonic vibration to hot-dipping is effective to control a reaction layer with less than 5μm in thickness. An impact test exhibits that the good adhesive strength is approved in hot-dipped aluminum coatings with a thin reaction layer of approximately 5μm.

Refinement of ferrite grain size during hot direct rolling of hsla steel

International Nuclear Information System (INIS)

Ajmal, M.

2001-01-01

Steel ingots containing 0.04 wt % Nb and varying contents of carbon were made in laboratory, that simulated thin slab casting. Mn and Si content were kept constant at 1.35 % and 0.25 % respectively. After each casting the mould assembly was transferred to the rolling mill and the temperature of the ingot was monitored. Each ingot was rolled to 4mm thickness in three passes. The first pass of 43% reduction for all the ingots were given at 1140 degree C. The second pass (reduction, 35 %) for all the ingots were given at 1040 degree C. However the temperature for third pass (reduction, 30 %) was varied to retain more strain in the austenite prior to transformation. It was shown that third pass at lower temperature i.e. 810 degree C in the austenite range yields a ferrite grains size of 2-3 micrometer. A yield strength of 465 Mpa and tensile strength of 530 Mpa can also be achieved in these plates. (author)

[Factors influencing electrocardiogram results in workers exposed to noise in steel-making and steel-rolling workshops of an iron and steel plant].

Science.gov (United States)

Li, Y H; Yu, S F; Gu, G Z; Chen, G S; Zhou, W H; Wu, H; Jiao, J

2016-02-20

To investigate the factors influencing the electrocardiogram results in the workers exposed to noise in steel-making and steel rolling workshops of an iron and steel plant. From September to December, 2013, cluster sampling was used to select 3 150 workers exposed to noise in the steel-making and steel-rolling workshops of an iron and steel plant, and a questionnaire survey and physical examinations were performed. The number of valid workers was 2 915, consisting of 1 606 workers in the steel-rolling workshop and 1 309 in the steel-making workshop. The electrocardiogram results of the workers in steel-making and steel-rolling workshops were analyzed. The overall abnormal rate of electrocardiogram was 26.35%, and the workers in the steel-making workshop had a significantly higher abnormal rate of electrocardiogram than those in the steel-rolling workshop(32.24% vs 21.54%, Pelectrocardiogram than female workers(27.59% vs 18.61%, Pelectrocardiogram than those who did not drink(28.17% vs 23.75%, Pelectrocardiogram than those who were not exposed to high temperature(29.43% vs 20.14%, Pelectrocardiogram in the workers with cumulative noise exposure levels of electrocardiogram results. High cumulative noise exposure, alcohol consumption, and high temperature may affect the abnormal rate of electrocardiogram in the workers exposed to noise in steel-making and steel-rolling workshops.

Strong tough low-carbon bainite structural steels exposed to heat treatment and mechanical working

International Nuclear Information System (INIS)

Lauprecht, W.; Imgrund, H.; Coldren, P.

1975-01-01

A review of results of studying the mechanical properties and structure of extremely strong construction low-pearlite and pearlite-free steels subjected to thermomechanical processing (TMP) is presented. The development of TMP of low-pearlite and pearlite-free steels has led to creation of steel of the following composition: 0.06% of C; 1.8% of Mn; 0.3% of Mo; 0.05-0.09% of Nb. Depending on the kind of TMP the most important parameters of which are the temperature of the termination of rolling and the total deformation below 900 deg C, transformation in these steels occurs partially or completely in the intermediate domain. The increased density of dislocations of beinite structure affects substantially the increase in the yield limit. High degrees of squeezing at temperatures below 870 deg C promote formation of ferrite nuclei. The laboratory rolling demonstrates that by selecting the conditions of TMP one can control the mechanical properties of a steel. The sheets of 13 mm thick allow to obtain the guaranteed values of the yield limit of 70 kgf/mm 2 the transition temperature T 50 = -25 deg C, whereas after rolling under different conditions the low-temperature limit of cold shortness is - 125 deg C, and the yield limit - 45 kgf/mm 2 . As followed from the estimate of numerous industrial experiments, with sheets 20 mm thick in hot-rolled state one can obtain the yield limit no less than 50 kgf/mm 2 . On rolling mills that make possible to produce large deformation at low temperature these values can be increased. For instance, with sheets 30 mm thick one can obtain the yield limit of 56 kgf/mm 2 and the transition temperature of - 60 deg C. The dependence of the yield limit on the holding time in steel tempering is given. The steel possesses a considerable reserve of the increase of strength due to dispersion hardening, which after tempering at 600-625 deg C constitutes 8-12 kgf/mm 2 . Because of low carbon content, this steel is characterized by good

Processing and properties of solid state nitrided stainless steels

International Nuclear Information System (INIS)

Rennhard, C.A.P.

1993-02-01

The properties of austenitic steels and duplex-steels are significantly improved by nitrogen (N) addition. In the present investigation, new alloys were produced and characterized using the high solid N-solubility and diffusion alloying from the gas phase. Most suitable base materials are powder, wire or sheet because of the short diffusion distance. PM-materials were in-can nitrided or treated in a fluidized bed and compacted by Hot Isostatic Pressing (HIP) or hot extrusion. The impact toughness level of PM alloys at room temperature is about 120 to 200 J, compared to 250 to 300 J for steels with equal strength that are produced by ingot metallurgy (IM). The toughness can be improved by high temperature deformation such as forging, hot rolling or hot extrusion or by removing the oxide layer on the particle surface by hydrogen gas reduction. A duplex steel with 22 Cr, 5.6 Ni and 2.7 Mo was transformed to a fully austenitic steel with over 500 MPa yield strength by increasing the N content from 0.2 to 0.65 weight-percent. The expensive Ni can successfully be replaced by N. Nitrided wire material is the base material for cold deformed high-strength wire. The improved strain hardening rate of nitrogen alloyed steels helps to achieve ductile and corrosion resistant materials with strength up to 2200 MPa. Sheet materials were diffusion bonded in the HIP or compacted in a 5000 kN press immediately after in-can nitriding to form solid blocks. Nitrided powder, wire and sheet materials lead to near net shape products that cannot be produced by conventional ingot metallurgy or would require the expensive high-pressure metallurgy. (author) 67 figs., tabs., 70 refs

Effect of hot rolling on the structure and the mechanical properties of nitrogen-bearing austenitic-martensitic 14Kh15AN4M steel

Science.gov (United States)

Bannykh, O. A.; Betsofen, S. Ya.; Lukin, E. I.; Blinov, V. M.; Voznesenskaya, N. M.; Tonysheva, O. A.; Blinov, E. V.

2016-04-01

The effect of the rolling temperature and strain on the structure and the properties of corrosionresistant austenitic-martensitic 14Kh15AN4M steel is studied. The steel is shown to exhibit high ductility: upon rolling in the temperature range 700-1100°C at a reduction per pass up to 80%, wedge steel specimens are uniformly deformed along and across the rolling direction without cracking and other surface defects. Subsequent cold treatment and low-temperature tempering ensure a high hardness of the steel (50-56 HRC). Austenite mainly contributes to the hardening upon rolling in the temperature range 700-800°C at a reduction of 50-70%, and martensite makes the main contribution at higher temperatures and lower strains. Texture does not form under the chosen deformation conditions, which indicates dynamic recrystallization with the nucleation and growth of grains having no preferential orientation.

Microstructure and texture evolution of different high manganese cast steels during hot deformation and subsequent treatment

Energy Technology Data Exchange (ETDEWEB)

Lima, M.N.S.; Andrade, C.D.; Abreu, H.F.G. de; Klug, J.; Masoumi, M., E-mail: mohammad@alu.ufc.br [Universidade Federal do Ceara (UFC), Fortaleza, CE (Brazil). Depto. de Engenharia Metalurgica e de Materiais; Ferreira, W.M. [Universidade Federal do Piaui (UFPI), Teresina, PI (Brazil). Curso de Engenharia Mecanica

2016-07-01

Microstructure and texture evolution were studied in two different austenitic high manganese cast steels in each processing condition. Special attention was paid to the effects of hot deformation and subsequent treatment on grain orientation behavior. The roles of Mn and C elements as well as heat treatment processes were investigated by Thermo-Calc. The texture evolutions in the as-cast, solution heat treatment, as-rolled and subsequent treatment were explored via orientation distribution function. The results showed that face-centred cube austenite was developed in steels. Strong {110}<115> texture component was characterized in as-cast in both alloys. Then, the inhomogeneity microstructure and the pronounced microsegregations were removed by annealing and Brass {110}<112>, {110}<111> and {221}<102> components were formed. Finally, cube {001}<100> component was developed during hot rolling in samples. (author)

Microstructure and texture evolution of different high manganese cast steels during hot deformation and subsequent treatment

International Nuclear Information System (INIS)

Lima, M.N.S.; Andrade, C.D.; Abreu, H.F.G. de; Klug, J.; Masoumi, M.; Ferreira, W.M.

2016-01-01

Microstructure and texture evolution were studied in two different austenitic high manganese cast steels in each processing condition. Special attention was paid to the effects of hot deformation and subsequent treatment on grain orientation behavior. The roles of Mn and C elements as well as heat treatment processes were investigated by Thermo-Calc. The texture evolutions in the as-cast, solution heat treatment, as-rolled and subsequent treatment were explored via orientation distribution function. The results showed that face-centred cube austenite was developed in steels. Strong {110}<115> texture component was characterized in as-cast in both alloys. Then, the inhomogeneity microstructure and the pronounced microsegregations were removed by annealing and Brass {110}<112>, {110}<111> and {221}<102> components were formed. Finally, cube {001}<100> component was developed during hot rolling in samples. (author)

Precipitation Strengthening by Induction Treatment in High Strength Low Carbon Microalloyed Hot-Rolled Plates

Science.gov (United States)

Larzabal, G.; Isasti, N.; Rodriguez-Ibabe, J. M.; Uranga, P.

2018-03-01

The use of microalloyed steels in the production of thick plates is expanding due to the possibility of achieving attractive combinations of strength and toughness. As market requirements for high strength plates are increasing and new applications require reduced weight and innovative designs, novel approaches to attaining cost-effective grades are being developed. The mechanism of precipitation strengthening has been widely used in thin strip products, since the optimization of the coiling strategy offers interesting combinations in terms of final properties and microalloying additions. Precipitation strengthening in thick plates, however, is less widespread due to the limitation of interphase precipitation during continuous cooling after hot rolling. With the main objective of exploring the limits of this strengthening mechanism, laboratory thermomechanical simulations that reproduced plate hot rolling mill conditions were performed using low carbon steels microalloyed with Nb, NbMo, and TiMo additions. After continuous cooling to room temperature, a set of heat treatments using fast heating rates were applied simulating the conditions of induction heat treatments. An important increase of both yield and tensile strengths was measured after induction treatment without any important impairment in toughness properties. A significant precipitation hardening is observed in Mo-containing grades under specific heat treatment parameters.

Influence of magnetostriction on hysteresis loss of electrical steel sheet

Energy Technology Data Exchange (ETDEWEB)

Tada, Hirotoshi, E-mail: tada.547.hirotoshi@jp.nssmc.com [Steel Research Laboratories, Nippon Steel and Sumitomo Metal Corporation, 1-8 Fuso-cho, Amagasaki, Hyogo 660-0891 (Japan); Fujimura, Hiroshi; Yashiki, Hiroyoshi [Steel Research Laboratories, Nippon Steel and Sumitomo Metal Corporation, 1-8 Fuso-cho, Amagasaki, Hyogo 660-0891 (Japan)

2013-01-15

To reveal influence of magnetostriction on hysteresis loss of electrical steel sheet, hysteresis loss and magnetostriction of non-oriented electrical steel sheets (NOs) with various Si and Al content and grain size and grain oriented electrical steel sheet (GO) were measured under compressive or tensile stress. Here, Si and Al content and stress were focused on as the way to change magnetostriction. Stress direction and magnetizing direction were parallel to the rolling direction. Following three main results were obtained. The first is hysteresis loss of NO with same grain size which increased with magnetostriction independently of Si and Al content and stress. The second is hysteresis loss of NO was larger than that of GO under same magnetostriction. The third is hysteresis loss of NO at magnetostriction of zero was inversely proportional to grain size. Even if the grain size of NO increased to be similar size of GO without changing texture, the hysteresis loss of NO at magnetostriction of zero would be larger than that of GO because of the difference in texture. - Highlights: Black-Right-Pointing-Pointer Hysteresis loss and magnetostriction of NO and GO were measured under stress. Black-Right-Pointing-Pointer Hysteresis loss of NO was proportional to magnetostriction. Black-Right-Pointing-Pointer Hysteresis loss of GO was proportional to magnetostriction. Black-Right-Pointing-Pointer Hysteresis loss of NO was larger than that of GO under samemagnetostriction. Black-Right-Pointing-Pointer Hysteresis loss was separated into 4 components.

Evaluation of the mechanical properties after thermal treatment of a structural hot rolled multiphase steel

Directory of Open Access Journals (Sweden)

Asensio-Lozano, J.

2007-12-01

Full Text Available The present paper corresponds to the experimental study conducted on a hot rolled (HR multiphase (MP steel, in which hardness, tensile and toughness properties were measured after the application of a series of subcritical and intercritical heat treatments (HT to the hot rolled stock. The aforementioned values were compared to the corresponding ones in the as-rolled state and after normalizing. The microstructure in the longitudinal plane of the strip was analyzed by light optical microscopy in the as-rolled state and in the HT samples. Longitudinal (L and transverse (T tensile and toughness specimens were cut to characterize every condition studied. Toughness properties were evaluated by means of Charpy V-notch tests conducted at 20 °C, 0 °C, –20 °C, –40 °C, –60 °C and –80 °C . It was observed that the yield stress increased with the increase in the heat treatment temperature in the subcritical range, while the tensile strength decreased slightly over the same range of temperatures. Uniform and total elongation only showed a slight improvement when the treatment was conducted at 620 °C and 700 °C, while the best toughness response corresponded to the sample treated at 500 °C for operating temperatures comprised between –40 °C and room temperature (RT.

El presente estudio corresponde al trabajo experimental desarrollado en un acero multifase laminado en caliente, en el que se evaluaron las propiedades de dureza, tracción y tenacidad a impacto, tras realizar tratamientos térmicos subcríticos e intercríticos al material laminado en caliente. Los valores precedentes se comparan con el material de partida laminado en caliente y tras tratamiento de normalizado. Se analiza la microestructura en microscopía óptica de reflexión, en el plano longitudinal tanto en el estado laminado como en las muestras tratadas térmicamente. Se estudiaron los comportamientos longitudinales y transversales en tracción y frente a impacto

Heat transfer modeling in asymmetrical sheet rolling of aluminium alloys with ultra high shear strain

Directory of Open Access Journals (Sweden)

Pesin Alexander

2016-01-01

Full Text Available Asymmetrical sheet rolling is a method of severe plastic deformation (SPD for production of aluminium alloys with UFG structure. Prediction of sheet temperature during SPD is important. The temperature of sheet is changed due to the conversion of mechanical work into heat through sliding on contact surfaces and high shear strain. Paper presents the results of FEM simulation of the effect of contact friction, rolling speed and rolls speed ratio on the heating of aluminium sheets during asymmetrical rolling.

Review of the continuous casting of steel by strip casting technology. Twin roll method system

International Nuclear Information System (INIS)

Ibarrondo, I.

2008-01-01

In order to compete in the future steel market and to maintain market share, the steel makers will need to use new efficient technologies capable of supplying steel strip products of high quality at low cost. In this way, the strip casting technology by twin rol method is one of the most important research are in the iron and steel industry today. This review makes a general description of the strip casting technology as well as its different steps, such us; metal delivery and casting, solidification process, hot rolling reduction step, etc. Through mathematical and physical models, the influence on microstructure texture surface quality and mechanical properties of the materials obtained by this method are described as a function of processing parameters, specially the roughness of the rolls. the manufacturing of carbon, stainless and electrical steels involves smaller capital and operating cost, lower gas emissions, and an opportunity to create new grades due to a faster solidification rate that leads to a different solidification structures. In sight of all this it is likely that Strip Casting technology will make a profound impact on the manufacturing landscape of the 21 s t century. (Author) 177 refs

The Study on Weldability of Boron Steel and Hot-Stamped Steel by Using Laser Heat Source (Ⅲ) - Comparison on Laser Weldability of Boron Steel and Hot -Stamped Steel-

Energy Technology Data Exchange (ETDEWEB)

Choi, So Young; Kim, Jong Do [Korea Maritime and Ocean University, Busan (Korea, Republic of); Kim, Jong Su [Korea Institute of Machinery and Materials, Daejeon (Korea, Republic of)

2015-01-15

This study was conducted to compare the laser weldability of boron steel and hot-stamped steel. In general, boron steel is used in the hot-stamping process. Hot-stamping is a method for simultaneously forming and cooling boron steel in a press die after heating it to the austenitizing temperature. Hot-stamped steel has a strength of 1500 MPa or more. Thus, in this study, the laser weldability of boron steel and that of hot-stamped steel were investigated and compared. A continuous wave disk laser was used to produce butt and lap joints. In the butt welding, the critical cooling speed at which full penetration was obtained in the hot-stamped steel was lower than that of boron steel. In the lap welding, the joint widths were similar regardless of the welding speed when full penetration was obtained.

The Study on Weldability of Boron Steel and Hot-Stamped Steel by Using Laser Heat Source (Ⅲ) - Comparison on Laser Weldability of Boron Steel and Hot -Stamped Steel-

International Nuclear Information System (INIS)

Choi, So Young; Kim, Jong Do; Kim, Jong Su

2015-01-01

This study was conducted to compare the laser weldability of boron steel and hot-stamped steel. In general, boron steel is used in the hot-stamping process. Hot-stamping is a method for simultaneously forming and cooling boron steel in a press die after heating it to the austenitizing temperature. Hot-stamped steel has a strength of 1500 MPa or more. Thus, in this study, the laser weldability of boron steel and that of hot-stamped steel were investigated and compared. A continuous wave disk laser was used to produce butt and lap joints. In the butt welding, the critical cooling speed at which full penetration was obtained in the hot-stamped steel was lower than that of boron steel. In the lap welding, the joint widths were similar regardless of the welding speed when full penetration was obtained

Influence of hot rolling and high speed hydrostatic extrusion on the microstructure and mechanical properties of an ODS RAF steel

Energy Technology Data Exchange (ETDEWEB)

Oksiuta, Z., E-mail: oksiuta@pb.edu.pl [Bialystok Technical University, Faculty of Mechanical Engineering, Wiejska 45c, 15-352 Bialystok (Poland); Lewandowska, M.; Kurzydlowski, K.J. [Warsaw University of Technology, Faculty of Materials Science and Engineering, Woloska 141, 02-504 Warsaw (Poland); Baluc, N. [Ecole Polytechnique Federale de Lausanne (EPFL), Centre de Recherches en Physique des Plasmas, Association Euratom-Confederation Suisse, 5232 Villigen PSI (Switzerland)

2011-02-15

An argon gas atomized, pre-alloyed Fe-14Cr-2W-0.3Ti (wt.%) reduced activation ferritic (RAF) steel powder was mechanically alloyed with 0.3wt.% Y{sub 2}O{sub 3} nano-particles in an attritor ball mill and consolidated by hot isostatic pressing at 1150 {sup o}C under a pressure of 200 MPa for 3 h. In the aim to improve its mechanical properties the ODS steel was then submitted to a thermo-mechanical treatment (TMT): hot rolling (HR) at 850 deg. C or high speed hydrostatic extrusion (HSHE) at 900 deg. C, followed by heat treatment (HT). Transmission electron microscopy (TEM) observations of the ODS alloys after TMT and heat treatment revealed the presence of elongated grains in the longitudinal direction, with an average width of 8 {mu}m and an average length of 75 {mu}m, and equiaxed grains, a few microns in diameter, in the transverse direction. Two populations of oxide particles were observed by TEM: large Ti-Al-O particles, up to 250 nm in diameter, usually located at the grain boundaries and small Y-Ti-O nanoclusters, about 2.5 nm in diameter, uniformly distributed in the matrix. Charpy impact tests revealed that the HSHE material exhibits a larger upper shelf energy (5.8 J) than the HR material (2.9 J). The ductile-to-brittle transition temperature of both alloys is relatively high, in the range of 55-72 deg. C. Tensile mechanical properties of both ODS alloys were found satisfactory over the full range of investigated temperatures (23-750 deg. C). The HSHE material exhibits better tensile strength and ductility than the HR material. These results indicate that HSHE can be considered as a promising TMT method for improving the mechanical properties of ODS RAF steels.

Imposition of Antidumping Duty (BAMD Towards China’s Cold Rolled Coil/Sheet (CRC/S Products

Directory of Open Access Journals (Sweden)

Lila Pratiwi

2013-05-01

Full Text Available Steel industry is a strategic sector in the economy of a country. Steel industry in Indonesia has not been able to fulfill their domestic demand that is still necessary to import steel product. However, many of these imported products are sold at dumping prices, especially those from china giving rise to unfair trade. One of trade remedy measures as a result of unfair trade remedies can recover trough the imposition of antidumping duty. In 2013, Indonesia imposes antidumping duty for Cold Rolled Coil/Sheet (CRC/S from China and other countries. Imposition of antidumping duty will be analyzed descriptively with the antidumping agreement conformity. While, it cannot be denied that political factors also determine imposition of antidumping duty. It is need to use analytical theory of justice in order to enforce fair-trade

On rolling of alloyed steels on the continuous light-section mill 250

International Nuclear Information System (INIS)

Grigor'ev, V.K.; Antipov, V.F.; Zamotin, V.M.; Kuznetsov, Yu.M.

1976-01-01

Using the method of computed ratios, the expected loads (torques) have been calculated in the rolling of alloyed steels on the light-section mill 250 of the Chelyabinsk metallurgical works. The deviation of the computed torques from those measured for steels 35GS and St5ps does not exceed -6%. Data are given on changes in torques during the rolling of alloyed steels in the different stands as compared with the actual data for the rolling of ordinary steel. Calculations show, and experimental data confirm, that, according to the torque value, it is possible to roll alloyed steels of sufficiently wide assortment on mill 250

Microstructure and mechanical properties of Mg-Al-Mn-Ca alloy sheet produced by twin roll casting and sequential warm rolling

International Nuclear Information System (INIS)

Wang Yinong; Kang, Suk Bong; Cho, Jaehyung

2011-01-01

Research highlights: → This work, taking AM30 + 0.2Ca alloy as experimental material, will provide some new information as follows: one is microstructural difference between twin roll cast and ingot cast AM31-0.2Ca alloy. The other is the comparison of tensile properties after warm rolling and annealing. Suggesting the possibility of the development of wrought magnesium alloy sheets by strip casting. - Abstract: Microstructural evolution and mechanical properties of twin roll cast (TRC) Mg-3.3 wt.%Al-0.8 wt.%Mn-0.2 wt.%Ca (AM31 + 0.2Ca) alloy strip during warm rolling and subsequent annealing were investigated in this paper. The as-TRC alloy strip shows columnar dendrites in surface and equiaxed dendrites in center regions, as well as finely dispersed primary Al 8 Mn 5 particles on interdendritic boundaries which result in the beneficial effect on microstructural refinement of strip casting. The warm rolled sheets show intensively deformed band or shear band structures, as well as finely and homogeneously dispersed Al-Mn particles. No evident dynamic recrystallization (DRX) takes place during warm rolling process, which is more likely attributed to the finely dispersed particle and high solid solution of Al and Mn atoms in α-Mg matrix. After annealing at 350 deg. C for 1 h, the warm rolled TRC sheets show fine equiaxed grains around 7.8 μm in average size. It has been shown that the present TRC alloy sheet has superior tensile strength and comparative elongation compared to commercial ingot cast (IC) one, suggesting the possibility of the development of wrought magnesium alloy sheets by twin roll strip casting processing. The microstructural evolution during warm rolling and subsequent annealing as well as the resulting tensile properties were analyzed and discussed.

Hot coiled steel strip with elevated niobium content for pipelines and its weldability

International Nuclear Information System (INIS)

Brozda, J.; Zeman, M.

2010-01-01

Examinations and tests have been performed on thermomechanically rolled and hot coiled 14 mm thick steel strips with a low carbon and elevated niobium content, assigned for the production of pipelines. There were examined basic mechanical properties of the steels, brittle fracture resistance of the parent material and simulated HAZ's, susceptibility to cold cracking as well as properties of MMA and GMA welded joints. It was found that the tested steels are characterized by a good weldability, are not prone to cold cracking, have a low brittle fracture transition temperature and the HAZ of welded joints shows a sufficient high brittle fracture resistance. (authors)

Heterogeneous multi-layered IF steel with simultaneous high strength and good ductility

Science.gov (United States)

Zhang, Ling; Jiang, Xiaojuan; Wang, Yuhui; Chen, Qiang; Chen, Zhen; Zhang, Yonghong; Huang, Tianlin; Wu, Guilin

2017-07-01

Multi-layered IF steel samples were designed and fabricated by hot compression followed by cold forging of an alternating stack of cold-rolled and annealed IF steel sheets, with an aim to improve the strength of the material without losing much ductility. A very good combination of strength and ductility was achieved by proper annealing after deformation. Microstructural analysis by electron back-scatter diffraction revealed that the good combination of strength and ductility is related to a characteristic hierarchical structure that is characterized by layered and lamella structures with different length scales.

Fatigue characteristics of dual-phase steel sheets

Energy Technology Data Exchange (ETDEWEB)

Onn, Irwan Herman; Ahmad, Norhayati; Tamin, Mohd Nasir [Universiti Teknologi Malaysia, Skudai (Malaysia)

2015-01-15

Fatigue characteristics of dual-phase steel sheets, commonly used in automobile body construction were established. For this purpose, a series of fatigue tests, each at constant stress amplitude were conducted on 1.2 mm-thick, dual-phase DP600 steel sheet specimens with two different load ratios of minimum-to-maximum stress, R = 0.1 and -1. The resulting fatigue behavior is expressed in terms of fatigue strength-life (S-N) curves. Fatigue behavior of the steel sheets in the high-cycle fatigue region can be represented by Basquin's equation with coefficient and exponent value of 921.2 and 0.093, respectively. An endurance limit of 255 MPa is observed. In addition, fatigue strengths of the dual-phase steel sheets display lower magnitude than their bulk counterparts. Effect of mean stress on fatigue behavior of the steel sheets is well predicted by Walker's model. Exponential calibration factor is introduced to the models by SWT, Goodman and Morrow with comparable prediction to the Walker's model.

Influence of precipitation behavior on mechanical properties and hydrogen induced cracking during tempering of hot-rolled API steel for tubing

Energy Technology Data Exchange (ETDEWEB)

Moon, Joonoh, E-mail: mjo99@kims.re.kr [Ferrous Alloy Department, Advanced Metallic Materials Division, Korea Institute of Materials Science, 797 Changwondae-ro, Seongsan-gu, Changwon, Gyeongnam 642-831 (Korea, Republic of); Choi, Jongmin; Han, Seong-Kyung; Huh, Sungyul; Kim, Seong-Ju [Sheet Products Design Team, Technical Research Center, Hyundai Steel Company, 1480 Bukbusaneop-ro, Dangjin, Chungnam 343-823 (Korea, Republic of); Lee, Chang-Hoon; Lee, Tae-Ho [Ferrous Alloy Department, Advanced Metallic Materials Division, Korea Institute of Materials Science, 797 Changwondae-ro, Seongsan-gu, Changwon, Gyeongnam 642-831 (Korea, Republic of)

2016-01-15

Precipitation behavior and its effect on hydrogen embrittlement during tempering process of hot-rolled API steel designed with 0.4 wt% Cr and 0.25 wt% Mo were investigated. The base steel was normalized and then tempered at 650 °C for up to 60 min. The precipitation behavior of the examined steel was explored using transmission electron microscopy (TEM) analysis, and it was found that the precipitation sequence during tempering at 650 °C were as follows: MX+M{sub 3}C→MX→MX+M{sub 7}C{sub 3}+M{sub 23}C{sub 6}. The change of particle fraction was measured by electrolytic extraction technique. At the early stage of tempering, the particle fraction greatly decreased due to dissolution of M{sub 3}C particle, and increased after 10 min by the precipitation of M{sub 7}C{sub 3} and M{sub 23}C{sub 6} particles. The particle fraction showed a peak at 30 min tempering and decreased again due to the dissolution of M{sub 7}C{sub 3} particle. Vickers hardness tests of base steel and tempered samples were carried out, and then the hardness was changed by accompanying with the change of particle fraction. The sensitivity of hydrogen embrittlement was evaluated through hydrogen induced cracking (HIC) tests, and the results clearly proved that HIC resistance of tempered samples was better than that of base steel due to the formation of tempered martensite, and then the HIC resistance changed depending on the precipitation behavior during tempering, i.e., the precipitation of coarse M{sub 23}C{sub 6} and M{sub 7}C{sub 3} particles deteriorated the HIC resistance.

Influence of precipitation behavior on mechanical properties and hydrogen induced cracking during tempering of hot-rolled API steel for tubing

International Nuclear Information System (INIS)

Moon, Joonoh; Choi, Jongmin; Han, Seong-Kyung; Huh, Sungyul; Kim, Seong-Ju; Lee, Chang-Hoon; Lee, Tae-Ho

2016-01-01

Precipitation behavior and its effect on hydrogen embrittlement during tempering process of hot-rolled API steel designed with 0.4 wt% Cr and 0.25 wt% Mo were investigated. The base steel was normalized and then tempered at 650 °C for up to 60 min. The precipitation behavior of the examined steel was explored using transmission electron microscopy (TEM) analysis, and it was found that the precipitation sequence during tempering at 650 °C were as follows: MX+M_3C→MX→MX+M_7C_3+M_2_3C_6. The change of particle fraction was measured by electrolytic extraction technique. At the early stage of tempering, the particle fraction greatly decreased due to dissolution of M_3C particle, and increased after 10 min by the precipitation of M_7C_3 and M_2_3C_6 particles. The particle fraction showed a peak at 30 min tempering and decreased again due to the dissolution of M_7C_3 particle. Vickers hardness tests of base steel and tempered samples were carried out, and then the hardness was changed by accompanying with the change of particle fraction. The sensitivity of hydrogen embrittlement was evaluated through hydrogen induced cracking (HIC) tests, and the results clearly proved that HIC resistance of tempered samples was better than that of base steel due to the formation of tempered martensite, and then the HIC resistance changed depending on the precipitation behavior during tempering, i.e., the precipitation of coarse M_2_3C_6 and M_7C_3 particles deteriorated the HIC resistance.

Interlocking multi-material components made of structured steel sheets and high-pressure die cast aluminium

Science.gov (United States)

Senge, S.; Brachmann, J.; Hirt, G.; Bührig-Polaczek, A.

2017-10-01

Lightweight design is a major driving force of innovation, especially in the automotive industry. Using hybrid components made of two or more different materials is one approach to reduce the vehicles weight and decrease fuel consumption. As a possible way to increase the stiffness of multi-material components, this paper presents a process chain to produce such components made of steel sheets and high-pressure die cast aluminium. Prior to the casting sequence the steel sheets are structured in a modified rolling process which enables continuous interlocking with the aluminium. Two structures manufactured by this rolling process are tested. The first one is a channel like structure and the second one is a channel like structure with undercuts. These undercuts enable the formation of small anchors when the molten aluminium fills them. The correlation between thickness reduction during rolling and the shape of the resulting structure was evaluated for both structures. It can be stated that channels with a depth of up to 0.5 mm and a width of 1 mm could be created. Undercuts with different size depending on the thickness reduction could be realised. Subsequent aluminium high-pressure die casting experiments were performed to determine if the surface structure can be filled gap-free with molten aluminium during the casting sequence and if a gap-free connection can be achieved after contraction of the aluminium. The casting experiments showed that both structures could be filled during the high-pressure die casting. The channel like structure results in a gap between steel and aluminium after contraction of the cast metal whereas the structure with undercuts leads to a good interlocking resulting in a gap-free connection.

Effect of Coating-thickness on the formability of hot dip aluminized steel

International Nuclear Information System (INIS)

Awan, G.H.; Ahmed, F.; Hasan, F.

2008-01-01

The influence of coating thickness on the formability and ductility of hot-dip-aluminized steel has been determined using a 3-point bend test and optical metallography. The ductility / formability was estimated from the 3-point bend test wherein the angle of bend at which the cracks start to appear on the surface of the aluminized sheet during bending, was taken as an index of the formability / ductility. It was observed that as the amount of silicon in the aluminising melt was gradually increased the measured ductility of the sheet sample also increased. Metallographic examination has shown that as the amount of silicon in the aluminising melt was increased the thickness of the intermediate compound layer, between the outer aluminum coat and the substrate steel, decreased. It was thus indicated from these experiments that the formability / ductility of the sheet was inversely related to the thickness of the interlayer. (author)

Model of mechanical properties change of steel during rolling with use of hightemperature thermomechanical treatment

International Nuclear Information System (INIS)

Zhadan, V.T.; Gubenko, V.T.; Bernshtejn, M.L.; Binarskij, M.S.

1975-01-01

A mathematical model is proposed of changes in the mechanical properties of the steel-50KHGA in the process of rolling with application of a high-temperature thermomechanical treatment (HTTMT). The model accounts for all the main particularities of the structure formation processes during a high temperature deformation of metals and alloys. The nonmonotonic dependence of the steel mechanical properties on the deformation velocity can be presented as a result of a summary effect of three parallel processes on the formation of these properties: hot working, softening and substructural hardening. The mathematical model has been constructed by the iteration method

A Novel Method of Modeling the Deformation Resistance for Clad Sheet

International Nuclear Information System (INIS)

Hu Jianliang; Yi Youping; Xie Mantang

2011-01-01

Because of the excellent thermal conductivity, the clad sheet (3003/4004/3003) of aluminum alloy is extensively used in various heat exchangers, such as radiator, motorcar air conditioning, evaporator, and so on. The deformation resistance model plays an important role in designing the process parameters of hot continuous rolling. However, the complex behaviors of the plastic deformation of the clad sheet make the modeling very difficult. In this work, a novel method for modeling the deformation resistance of clad sheet was proposed by combining the finite element analysis with experiments. The deformation resistance model of aluminum 3003 and 4004 was proposed through hot compression test on the Gleeble-1500 thermo-simulation machine. And the deformation resistance model of clad sheet was proposed through finite element analysis using DEFORM-2D software. The relationship between cladding ratio and the deformation resistance was discussed in detail. The results of hot compression simulation demonstrate that the cladding ratio has great effects on the resistance of the clad sheet. Taking the cladding ratio into consideration, the mathematical model of the deformation resistance for clad sheet has been proved to have perfect forecasting precision of different cladding ratio. Therefore, the presented model can be used to predict the rolling force of clad sheet during the hot continuous rolling process.

Hot ductility of a microalloyed steel in the intermediate temperature range

International Nuclear Information System (INIS)

Darsouni, A.; Bouzabata, B.; Montheillet, F.

1995-01-01

In this study hot ductility has been determined from tensile tests for two states of a microalloyed steel: after casting and after rolling processes. Hot deformations were carried out at speeds varying from 10 -4 s -1 to 10 -2 s -1 and temperatures from 750 C to 1100 C. Two heat treatments were chosen before hot deformation. A ferrite precipitation is observed at austenitic grain boundaries in the intercritical temperature range, causing intergranular embrittlement. Ductility trough is deeper in the as-cast samples due to the growth of large grain size. Also, precipitation makes the hot ductility curve wider and deeper around 900 C. The results show a decrease in hot ductility. Minimum values of hot ductility are determined for (ITC) treatment at 900 C and for (DTC) treatment at 800 C. For this second treatment another decrease in hot ductility was observed at 900 C. We can explain hot ductility losses by the presence of precipitates in the austenitic region and the presence of the two-phase structure in the intercritical region. (orig.)

Laser Beam Welding of Ultra-high Strength Chromium Steel with Martensitic Microstructure

Science.gov (United States)

Dahmen, Martin; Janzen, Vitalij; Lindner, Stefan; Wagener, Rainer

A new class of steels is going to be introduced into sheet manufacturing. Stainless ferritic and martensitic steels open up opportunities for sheet metal fabrication including hot stamping. Strengths of up to 2 GPa at fracture elongations of 15% can be attained through this. Welding of these materials, as a result, became a challenge. Energy-reduced welding methods with in-situ heat treatment are required in order to ensure the delicate and complex heat control. Laser beam welding is the joining technique of choice to supply minimum heat input to the fusion process and to apply efficient heat control. For two application cases, tailored blank production in as-rolled condition and welding during assembly in hot stamped condition, welding processes have been developed. The welding suitability is shown through metallurgical investigations of the welds. Crash tests based on the KS-II concept as well as fatigue tests prove the applicability of the joining method.

Rolling process simulation of a pair-crossed hot strip mill

International Nuclear Information System (INIS)

Chen Shaojie; Xu Jianzhong; Liu Xianghua; Wang Guodong

2000-01-01

Process simulation can help optimize the operating parameters aiming to improve the quality of rolled products. In this paper, software in Visual Basic language is developed to simulate the hot rolling process of a pair-crossed mill. The strip temperature is calculated by considering air cooling, water cooling, heat generation and conduction.The production parameters including rolling speeds, resistance to deformation, rolling forces, drive torques and powers are evaluated by mathematical models and their parameter identification support tools. The deformation of roll stack is calculated by influential function method. The roll temperature and expansion are calculated by finite differential method, and the roll wear is described by empirical formula. Based on these calculations as well as the effect of heredity is taken into account, the strip crown and flatness then can be obtained. The results show that the simulation software has friendly user interface, high accuracy and practicability. It can be served as a basis for the mill design and optimization of process parameters to acquire high quality of hot rolled strip. (author)

INFLUENCE OF MICRO-SEGREGATION IN PB-S-ALLOYED FREE MACHINING STEELS ON THE SURFACE QUALITY OF THE ROLLED WIRE-ROD

OpenAIRE

Leuschke, U.; Rajesh Puvvada, N.; Puvvada, Rajesh

2008-01-01

Free machining steel billets were manufactured at the continuous casting machine. The manufactured billets did not exhibit any kind of surface defects but surface cracks and slivers appeared when the billets were rolled into wires and rods at the wire-rod mill. The defects on rolled wire-rod have been detected by a hot eddy current system. Further investigations in these defects with the help of microprobe analysis system and scanning electron microscope equipped with image analysis system re...

Analysis of hot rolling and hot forging effects on mechanical properties and microstructure of ZrNbMoGe alloy

International Nuclear Information System (INIS)

AH Ismoyo; Parikin; Bandriyana

2014-01-01

Research on formation technique by a combined method of rolling and forging has been carried out in order to improve the mechanical properties of ZrNbMoGe alloy to be used as fuel cladding in NPP (Nuclear Power Plant) application. The effects of rolling and forging were analyzed several tests. The tests were conducted for zirconium alloy specimen with a composition of (in % wt.) 97% Zr, 0,5% Mo, 2% Nb and 0,5% Ge, where the specimen was melted with an arc-furnace. The hot rolling and forging were conducted at 900 °C and 950 °C respectively. Hardness test was carried out by using a microhardness testing machine, while microstructure examination and crystal structure analysis were conducted with an optical microscope and an X-ray diffractometer. The results show that the hardness of the alloy increase from 141.21 HV (starting material) to 210.47 HV (hot rolled material) and 365.75 HV (hot forged material). Texturing phenomenon is clearly figured on the microstructure due to hot rolling and forging process. Analysis by diffractogram also indicates that the hot rolling and forging process has influence on the crystal orientation of dominant preferred direction in the reflection plane of (10ī1), recorded from the rise of intensity counting from about 2500 to 3000. In summary, hot forging and rolling process can change the mechanical properties (hardness and texture) and microstructure of materials. (author)

Corrosion resistance and protection mechanism of hot-dip Zn-Al-Mg alloy coated steel sheet under accelerated corrosion environment; Yoyu Zn-Al-Mg kei gokin mekki koban no sokushin fushoku kankyoka ni okeru taishokusei toi boshoku kiko

Energy Technology Data Exchange (ETDEWEB)

Komatsu, A.; Izutani, H.; Tsujimura, T.; Ando, A.; Kittaka, T. [NKK Corp., Tokyo (Japan)

2000-08-01

Corrosion behavior of hot-dip Zn-6%Al 0-3%Mg alloy coated steel sheets in cyclic corrosion test (CCT) has been investigated. The corrosion resistance was improved with increasing Mg content in the coating layer, and the highest corrosion resistance was observed at 3% Mg. In Zn-6%Al-3%Mg alloy coated steel sheet, the formations of zinc carbonate hydroxide and zinc oxide were suppressed for longer duration compared with Zn-0.2%Al and Zn-4.5%Al-0.l%Mg alloy coated steel sheets. As a result, zinc chloride hydroxide existed stable on the surface of the coating layer. From the polarization behaviors in 5% NaCl aqueous solution after CCT, it was found that the corrosion current density of Zn-6%At-3%Mg alloy coated steel sheet was much smaller than those of Zn-0.2%Al and Zn-4.5%Al-0.1%Mg alloy coated steel sheets. As zinc carbonate hydroxide and zinc oxide had poor adhesion to the coating layer and had porous structures, these corrosion products were considered to have little protective action for the coating layer. Therefore, it was concluded that Mg suppressed the formation of such nonprotective corrosion products. resulting in the remarkable improvement of corrosion resistance. (author)

Effects of S and Mn on the hot workability of STS 316L and 309S steels

International Nuclear Information System (INIS)

Lee, Soo Chan; Kim, Young Hwan; Lee, Yun Yong

1998-01-01

Effects of sulfur and manganese on the hot workability of STS 316L and 309S steels have been investigated. From the results of hot workability test, the hot ductility was decreased with increasing sulfur content and reheating temperature. This is considered to be caused by sulfur segregations and sulfide precipitates at grain boundaries. Sulfur would be dissolved under the reheating conditions and reprecipitated with decreasing temperatures during hot rolling. The content of reprecipitated sulfur is decreased with increasing manganese content and decreasing reheating temperature. Therefore, the hot ductility is increased with increasing manganese content. It was also found that the hot ductility is increased with decreasing reheating temperature

A model for prediction of profile and flatness of hot and cold rolled flat products in four-high mills

Science.gov (United States)

Overhagen, Christian; Mauk, Paul Josef

2018-05-01

For flat rolled products, the thickness profile in the transversal direction is one of the most important product properties. For further processing, a defined crown of the product is necessary. In the rolling process, several mechanical and thermal influences interact with each other to form the strip shape at the roll gap exit. In the present analysis, a process model for rolling of strip and sheet is presented. The core feature of the process model is a two-dimensional stress distribution model based on von Karman's differential equation. Sub models for the mechanical influences of work roll flattening as well as work and backup roll deflection and the thermal influence of work roll expansion have been developed or extended. The two-dimensional stress distribution serves as an input parameter for the roll deformation models. For work roll flattening, a three-dimensional model based on the Boussinesq problem is adopted, while the work and backup roll deflection, including contact flattening is calculated by means of finite beam elements. The thermal work roll crown is calculated with help of an axisymmetric numerical solution of the heat equation for the work roll, considering azimuthal averaging for the boundary conditions at the work roll surface. Results are presented for hot rolling of a strip in a seven-stand finishing train of a hot strip mill, showing the calculated evolution of the strip profile. A variation of the strip profile from the first to the 20th rolled strip is shown. This variation is addressed to the progressive increase of work roll temperature during the first 20 strips. It is shown that a CVC® system can lead to improvements in strip profile and therefore flatness.

Engineering of rolled constructional microalloyed steel products

International Nuclear Information System (INIS)

Adamczyk, J.

2003-01-01

Flexibility of the microalloyed steels on manufacturing of products with high mechanical and technological properties at not exaggerated production costs, it caused of their application for different constructions and machines in many branches of economy. It is a reason of the big interest of this steel group and the improvement of metallurgical and technological processing. In the work the examples of applications of C-Mn microalloyed steels with V and N microadditions for production of long shape products of R p0.2 > 650 MPa and KCU2 > 57 Jcm -2 are presented. They are manufactured in the controlled rolling process. Moreover this work presents liquid metal treatment in ladlemann process and influence of ingots solidification conditions, controlled rolling of weldable plates with Nb, Ti, V and B microadditions which after quenching and tempering have R p0.2 > 870 MPa, KV -50 o C > 27 J and plastic strain ratio equals 1.2. This work also presents the energy saving rolling technology with controlled recrystallization (method of thermomechanical treatment) of improved Weldox 960 steel plates with Mb, Ti, V and B microadditions which have after high-temperature tempering R p0.2 > 100 MPa, KV -50 o C >90 J and plastic strain ratio is less than 1.2. The introduction of microalloyed constructional steels and the appropriate technology in the domestic industry will contribute to high-processed products with properties competitive to products manufactured in high-industrialized countries. Thanks to that it will be possible to increase the technical level as well as to reduce production costs and import. (author)

Formation of Outburst Structure in Hot Dip Galvannealed Coatings on IF Steels

Directory of Open Access Journals (Sweden)

Kollárová, M.

2007-01-01

Full Text Available Outburst structure in two industrially produced hot dip galvanized interstitial free steel sheets for automotive industry after additional annealing has been examined. Ti IF steel was found to form weak outburst structure in the early stage of annealing, followed by frontal growth of Fe-Zn phases during further heating. The high reactivity of this steel was confirmed by rapid G-phase formation. Under the same conditions, Ti-Nb-P IF steel exhibited frontal growth of Fe-Zn compounds without G-phase formation due to relatively high phosphorous content, which is known as inhibitor of Fe-Zn reaction, but simultaneously significant occurrence of undesired outburst structures was recorded. It was assumed that the phosphorous content was insufficient and/or ferrite grain was very fine.

Fracture Mechanics Approach to X-Ray Diffraction Method for Spot Welded Lap Joint Structure of Rolled Steel Considered Residual Stress

International Nuclear Information System (INIS)

Baek, Seung Yeb; Bae, Dong Ho

2011-01-01

Cold and hot-rolled carbon steel sheets are commonly used in railroad cars or commercial vehicles such as the automobile. The sheets used in these applications are mainly fabricated by spot welding, which is a type of electric resistance welding. However, the fatigue strength of a spot-welded joint is lower than that of the base metal because of high stress concentration at the nugget edge of the spot-welded part. In particular, the fatigue strength of the joint is influenced by not only geometrical and mechanical factors but also the welding conditions for the spot-welded joint. Therefore, there is a need for establishing a reasonable criterion for a long-life design for spot-welded structures. In this thesis, ΔP-N f relation curves have been used to determine a long-life fatigue-design criterion for thin-sheet structures. However, as these curves vary under the influence of welding conditions, mechanical conditions, geometrical factors, etc. It is very difficult to systematically determine a fatigue-design criterion on the basis of these curves. Therefore, in order to eliminate such problems, the welding residual stresses generated during welding and the stress distributions around the weld generated by external forces were numerically and experimentally analyzed on the basis of the results, reassessed fatigue strength of gas welded joints

Finite-element model to predict roll-separation force and defects during rolling of U-10Mo alloys

Energy Technology Data Exchange (ETDEWEB)

Soulami, Ayoub; Burkes, Douglas E.; Joshi, Vineet V.; Lavender, Curt A.; Paxton, Dean

2017-10-01

This study used a finite element code, LSDYNA, as a predictive tool to optimize the rolling process. Simulations of the hot rolling of U-10Mo coupons encapsulated in low-carbon steel were conducted following two different schedules. Model predictions of the roll-separation force and roll pack thicknesses at different stages of the rolling process were compared with experimental measurements. The study reported here discussed various attributes of the rolled coupons revealed by the model (e.g., waviness and thickness non-uniformity like dog boning). To investigate the influence of the cladding material on these rolling defects, other cases were simulated:  hot rolling with alternative can materials, namely, 304 stainless steel and Zircaloy-2, and bare-rolling.

Zinc coated sheet steel for press hardening

Science.gov (United States)

Ghanbari, Zahra N.

Galvanized steels are of interest to enhance corrosion resistance of press-hardened steels, but concerns related to liquid metal embrittlement have been raised. The objective of this study was to assess the soak time and temperature conditions relevant to the hot-stamping process during which Zn penetration did or did not occur in galvanized 22MnB5 press-hardening steel. A GleebleRTM 3500 was used to heat treat samples using hold times and temperatures similar to those used in industrial hot-stamping. Deformation at both elevated temperature and room temperature were conducted to assess the coating and substrate behavior related to forming (at high temperature) and service (at room temperature). The extent of alloying between the coating and substrate was assessed on undeformed samples heat treated under similar conditions to the deformed samples. The coating transitioned from an α + Gamma1 composition to an α (bcc Fe-Zn) phase with increased soak time. This transition likely corresponded to a decrease in availability of Zn-rich liquid in the coating during elevated temperature deformation. Penetration of Zn into the substrate sheet in the undeformed condition was not observed for any of the processing conditions examined. The number and depth of cracks in the coating and substrate steel was also measured in the hot-ductility samples. The number of cracks appeared to increase, while the depth of cracks appeared to decrease, with increasing soak time and increasing soak temperature. The crack depth appeared to be minimized in the sample soaked at the highest soak temperature (900 °C) for intermediate and extended soak times (300 s or 600 s). Zn penetration into the substrate steel was observed in the hot-ductility samples soaked at each hold temperature for the shortest soak time (10 s) before being deformed at elevated temperature. Reduction of area and elongation measurements showed that the coated sample soaked at the highest temperature and longest soak time

Effect of Reduction in Thickness and Rolling Conditions on Mechanical Properties and Microstructure of Rolled Mg-8Al-1Zn-1Ca Alloy

Directory of Open Access Journals (Sweden)

Yuta Fukuda

2017-01-01

Full Text Available A cast Mg-8Al-1Zn-1Ca magnesium alloy was multipass hot rolled at different sample and roll temperatures. The effect of the rolling conditions and reduction in thickness on the microstructure and mechanical properties was investigated. The optimal combination of the ultimate tensile strength, 351 MPa, yield strength, 304 MPa, and ductility, 12.2%, was obtained with the 3 mm thick Mg-8Al-1Zn-1Ca rolled sheet, which was produced with a roll temperature of 80°C and sample temperature of 430°C. This rolling process resulted in the formation of a bimodal structure in the α-Mg matrix, which consequently led to good ductility and high strength, exclusively by the hot rolling process. The 3 mm thick rolled sheet exhibited fine (mean grain size of 2.7 μm and coarse grain regions (mean grain size of 13.6 μm with area fractions of 29% and 71%, respectively. In summary, the balance between the strength and ductility was enhanced by the grain refinement of the α-Mg matrix and by controlling the frequency and orientation of the grains.

Engineering study for a melting, casting, rolling and fabrication facility for recycled contaminated stainless steel

International Nuclear Information System (INIS)

1994-01-01

This Preliminary Report is prepared to study the facilities required for recycling contaminated stainless steel scrap into plate which will be fabricated into boxes suitable for the storage of contaminated wastes and rubble. The study is based upon the underlying premise that the most cost effective way to produce stainless steel is to use the same processes employed by companies now in production of high quality stainless steel. Therefore, the method selected for this study for the production of stainless steel plate from scrap is conventional process using an Electric Arc Furnace for meltdown to hot metal, a Continuous Caster for production of cast slabs, and a Reversing Hot Mill for rolling the slabs into plate. The fabrication of boxes from the plate utilizes standard Shears, Punch Presses and welding equipment with Robotic Manipulators. This Study presumes that all process fumes, building dusts and vapors will be cycled through a baghouse and a nuclear grade HEPA filter facility prior to discharge. Also, all process waste water will be evaporated into the hot flue gas stream from the furnace utilizing a quench tank; so there will be no liquid discharges from the facility and all vapors will be processed through a HEPA filter. Even though HEPA filters are used today in controlling radioactive contamination from nuclear facilities there is a sparsity of data concerning radioactivity levels and composition of waste that may be collected from contaminated scrap steel processing. This report suggests some solutions to these problems but it is recommended that additional study must be given to these environmental problems

Microstructure and partitioning behavior characteristics in low carbon steels treated by hot-rolling direct quenching and dynamical partitioning processes

International Nuclear Information System (INIS)

Li, Yun-jie; Li, Xiao-lei; Yuan, Guo; Kang, Jian; Chen, Dong; Wang, Guo-dong

2016-01-01

In this work, a new process and composition design are proposed for “quenching and partitioning” or Q&P treatment. Three low carbon steels were treated by hot-rolling direct quenching and dynamical partitioning processes (DQ&P). The effects of proeutectoid ferrite and carbon concentration on microstructure evolution and mechanical properties were investigated. The present work obtained DQ&P prototype steels with good mechanical properties and established a new notion on compositions for Q&P processing. Microstructures were characterized by means of electro probe microanalyzer (EPMA), scanning electron microscopy (SEM), electron backscatter diffraction (EBSD), transmission electron microscopy (TEM) and X-ray diffraction (XRD), especially the morphology and size of retained austenite. Mechanical properties were measured by uniaxial tensile tests. The results indicated that introducing proeutectoid ferrite can increase the volume fraction of retained austenite and thus improve mechanical properties. TEM observation showed that retained austenite included the film-like inter-lath austenite and blocky austenite located in martensite/ferrite interfaces or surrounded by ferrites. It was interesting that when the carbon concentration is as low as ~ 0.078%, the film-like inter-lath untransformed austenite cannot be stabilized to room temperature and almost all of them transformed into twin martensite. The blocky retained austenite strengthened the interfaces and transformed into twin martensite during the tensile deformation process. The PSEs of specimens all exceeded 20 GPa.%. - Highlights: •This study focused on a new process: Q&P process applying dynamical partitioning. •Ferrite can increase the volume fraction of retained austenite. •The film-like austenite and the blocky austenite were observed. •The low carbon steels treated by new process reached PSEs higher than 20 GPa.%.

Rolling Process Modeling Report: Finite-Element Prediction of Roll Separating Force and Rolling Defects

Energy Technology Data Exchange (ETDEWEB)

Soulami, Ayoub [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Lavender, Curt A. [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Paxton, Dean M. [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Burkes, Douglas [Pacific Northwest National Lab. (PNNL), Richland, WA (United States)

2014-04-23

Pacific Northwest National Laboratory (PNNL) has been investigating manufacturing processes for the uranium-10% molybdenum (U-10Mo) alloy plate-type fuel for the U.S. high-performance research reactors. This work supports the Convert Program of the U.S. Department of Energy’s National Nuclear Security Administration (DOE/NNSA) Global Threat Reduction Initiative. This report documents modeling results of PNNL’s efforts to perform finite-element simulations to predict roll separating forces and rolling defects. Simulations were performed using a finite-element model developed using the commercial code LS-Dyna. Simulations of the hot rolling of U-10Mo coupons encapsulated in low-carbon steel have been conducted following two different schedules. Model predictions of the roll-separation force and roll-pack thicknesses at different stages of the rolling process were compared with experimental measurements. This report discusses various attributes of the rolled coupons revealed by the model (e.g., dog-boning and thickness non-uniformity).

Metallurgical analysis of spalled work roll of hot strip mill

International Nuclear Information System (INIS)

Khan, M.M.; Khan, M.A.

1993-01-01

In this study failure analysis of four work roll of the Hot Strip Mill is carried out. The microstructure is correlated with the chemical composition of shell and roll-life. It was concluded that for the longer service of the roll, cementite, graphite and martensite should be balanced (as per working requirement of the mill). (author)

Study of aluminum nitride precipitation in Fe- 3%Si steel

Directory of Open Access Journals (Sweden)

F.L. Alcântara

2013-01-01

Full Text Available For good performance of electrical steels it is necessary a high magnetic induction and a low power loss when submitted to cyclic magnetization. A fine dispersion of precipitates is a key requirement in the manufacturing process of Fe- 3%Si grain oriented electrical steel. In the production of high permeability grain oriented steel precipitate particles of copper and manganese sulphides and aluminium nitride delay normal grain growth during primary recrystallization, causing preferential growth of grains with Goss orientation during secondary recrystallization. The sulphides precipitate during the hot rolling process. The aluminium nitride particles are formed during hot rolling and the hot band annealing process. In this work AlN precipitation during hot deformation of a high permeability grain oriented 3%Si steel is examined. In the study, transfer bar samples were submitted to controlled heating, compression and cooling treatments in order to simulate a reversible hot rolling finishing. The samples were analyzed using the transmission electron microscope (TEM in order to identify the precipitates and characterize size distribution. Precipitate extraction by dissolution method and analyses by inductively coupled plasma optical emission spectrometry (ICP-OES were used to quantify the precipitation. The results allowed to describe the precipitation kinetics by a precipitation-time-temperature (PTT diagram for AlN formation during hot rolling.

Microstructure, texture evolution and magnetic properties of strip-casting non-oriented 6.5 wt.% Si electrical steel doped with cerium

Energy Technology Data Exchange (ETDEWEB)

Li, Hao-Ze, E-mail: lhzqq83@163.com; Liu, Hai-Tao; Liu, Zhen-Yu, E-mail: zyliu@mail.neu.edu.cn; Wang, Guo-Dong

2015-05-15

A 0.3 mm thick non-oriented 6.5 wt.% Si electrical steel sheet doped with cerium is produced by twin-roll strip casting, hot rolling, warm rolling and annealing. A detailed study of the cerium precipitates in the as-cast strip, microstructure and texture evolution at different processing stages is carried out by electron probe micro-analysis, optical microscopy, X-ray diffraction and electron backscattered diffraction analysis. Grain interior distributing precipitates identified as Ce-oxides, Ce-oxysulfides and Ce-phosphides, and boundary distributing Ce-oxides and Ce-phosphides are observed in the as-cast strip. The initial as-cast strip is characterized by a much finer solidification microstructure and dominated by obvious < 001 >//ND texture through the strip thickness. After hot and warm rolling, inhomogeneous microstructure containing large amounts of in-grain shear bands is characterized by mixed < 110 >//RD and < 111 >//ND textures. The texture of the annealed sheet with a relatively large average grain size is far more optimized by the domination of the beneficial cube, rotated cube, (001)< 120 > to (001)< 130 > and Goss texture components, and the elimination of the detrimental γ-fiber texture, leading to a superior magnetic induction and improved iron loss. - Highlights: • An Fe–6.5 wt.% Si as-cast strip doped with cerium was produced. • A thin warm rolled sheet with limited edge cracks was obtained. • Microstructure and texture evolution at each stage were investigated. • Strong λ-fiber and Goss recrystallization textures were formed. • The magnetic properties of the annealed sheet were significantly improved.

Novel twin-roll-cast Ti/Al clad sheets with excellent tensile properties.

Science.gov (United States)

Kim, Dae Woong; Lee, Dong Ho; Kim, Jung-Su; Sohn, Seok Su; Kim, Hyoung Seop; Lee, Sunghak

2017-08-14

Pure Ti or Ti alloys are recently spot-lighted in construction industries because they have excellent resistance to corrosions, chemicals, and climates as well as various coloring characteristics, but their wide applications are postponed by their expensiveness and poor formability. We present a new fabrication process of Ti/Al clad sheets by bonding a thin Ti sheet on to a 5052 Al alloy melt during vertical-twin-roll casting. This process has merits of reduced production costs as well as improved tensile properties. In the as-twin-roll-cast clad sheet, the homogeneously cast microstructure existed in the Al alloy substrate side, while the Ti/Al interface did not contain any reaction products, pores, cracks, or lateral delamination, which indicated the successful twin-roll casting. When this sheet was annealed at 350 °C~600 °C, the metallurgical bonding was expanded by interfacial diffusion, thereby leading to improvement in tensile properties over those calculated by a rule of mixtures. The ductility was also improved over that of 5052-O Al alloy (25%) or pure Ti (25%) by synergic effect of homogeneous deformation due to excellent Ti/Al bonding. This work provides new applications of Ti/Al clad sheets to lightweight-alloy clad sheets requiring excellent formability and corrosion resistance as well as alloy cost saving.

The Influence of Hot-Rolled Temperature on Plasma Nitriding Behavior of Iron-Based Alloys

Science.gov (United States)

El-Hossary, F. M.; Khalil, S. M.; Lotfy, Kh.; Kassem, M. A.

2009-07-01

Experiments were performed with an aim of studying the effect of hot-rolled temperature (600 and 900°C) on radio frequency (rf) plasma nitriding of Fe93Ni4Zr3 alloy. Nitriding was carried out for 10 min in a nitrogen atmosphere at a base pressure of 10-2 mbarr. Different continuous plasma processing powers of 300-550 W in steps 50 W or less were applied. Nitrided hot-rolled specimens were characterized by optical microscopy (OM), X-ray diffraction (XRD) and microhardness measurements. The results reveal that the surface of hot-rolled rf plasma nitrided specimens at 600°C is characterized with a fine microstructure as a result of the high nitrogen solubility and diffusivity. Moreover, the hot-rolled treated samples at 600°C exhibit higher microhardness value than the associated values of hot-rolled treated samples at 900°C. The enhancement of microhardness is due to precipitation and predominance of new phases ( γ and ɛ phases). Mainly, this conclusion has been attributed to the high defect densities and small grain sizes of the samples hot-rolled at 600°C. Generally, the refinement of grain size plays a dramatic role in improvement of mechanical properties of tested samples.

78 FR 25701 - Certain Hot-Rolled Carbon Steel Flat Products From India: Notice of Second Amended Final Results...

Science.gov (United States)

2013-05-02

... Essar I, the CIT remanded Commerce's AFA determination that Essar benefited from the CIP.\\10\\ The CIT... DEPARTMENT OF COMMERCE International Trade Administration [C-533-821] Certain Hot-Rolled Carbon... Commerce. SUMMARY: On April 9, 2013, the United States Court of International Trade (CIT) sustained the...

Chromate-free Hybrid Coating for Corrosion Protection of Electrogalvanized Steel Sheets

International Nuclear Information System (INIS)

Jo, Duhwan; Kwon, Moonjae; Kim, Jongsang

2012-01-01

Both electrogalvanized and hot-dip galvanized steel sheets have been finally produced via organic-inorganic surface coating process on the zinc surface to enhance corrosion resistance and afford additional functional properties. Recently, POSCO has been developed a variety of chromate-free coated steels that are widely used in household, construction and automotive applications. New organic-inorganic hybrid coating solutions as chromate alternatives are comprised of surface modified silicate with silane coupling agent and inorganic corrosion inhibitors as an aqueous formulation. In this paper we have prepared new type of hybrid coatings and evaluated quality performances such as corrosion resistance, spot weldability, thermal tolerance, and paint adhesion property etc. The electrogalvanized steels with these coating solutions exhibit good anti-corrosion property compared to those of chromate coated steels. Detailed components composition of coating solutions and experimental results suggest that strong binding between organic-inorganic hybrid coating layer and zinc surface plays a key role in the advanced quality performances

Up-scaling perovskite solar cell manufacturing from sheet-to-sheet to roll-to-roll: challenges and solutions

Science.gov (United States)

Di Giacomo, Francesco; Galagan, Yulia; Shanmugam, Santhosh; Gorter, Harrie; van den Bruele, Fieke; Kirchner, Gerwin; de Vries, Ike; Fledderus, Henri; Lifka, Herbert; Veenstra, Sjoerd; Aernouts, Tom; Groen, Pim; Andrissen, Ronn

2017-08-01

Organometallic halide perovskite solar cells (PSCs) are extremely promising novel materials for thin-film photovoltaics, exhibiting efficiencies over 22% on glass and over 17% on foil 1, 2 . First, a sheet-to-sheet (S2S) production of PSCs and modules on 152x152 mm2 substrates was established, using a combination of sputtering, e-beam evaporation, slot die coating and thermal evaporation (average PCE of 14.6 +/- 1.3 % over 64 devices, more than 10% initial PCE on modules). Later the steps towards a roll-to-roll production will be investigated, starting from the optimization of the stack to make it compatible with a faster production at low temperature. A water based SnOx nanoparticles dispersion was used as solution processable ETL, and the deposition process was scaled-up from spin coating to R2R slot die coating on a 300 mm wide roll of PET/ITO. R2R production is often carried out in ambient atmosphere and involve the use of large volumes of materials, thus a first point is the development of a green solvent and precursor system for the perovskite layer to prevent the emission of toxic compound in the environment. The first results on device fabrication are encouraging, which allow partial R2R manufacturing of flexible PSC (R2R coating of SnOx and perovskite, S2S for Spiro-OMeTAD and gold) with stabilized PCE of 12.6%, a remarkable value for these novel devices. This result can be considered an important milestone towards the production of efficient, low cost, lightweight, flexible PSC on large area.

Properties of Rolled AZ31 Magnesium Alloy Sheet Fabricated by Continuous Variable Cross-Section Direct Extrusion

Science.gov (United States)

Liu, Yang; Li, Feng; Li, Xue Wen; Shi, Wen Yong

2018-03-01

Rolling is currently a widely used method for manufacturing and processing high-performance magnesium alloy sheets and has received widespread attention in recent years. Here, we combined continuous variable cross-section direct extrusion (CVCDE) and rolling processes. The microstructure and mechanical properties of the resulting sheets rolled at different temperatures from CVCDE extrudate were investigated by optical microscopy, scanning electron microscope, transmission electron microscopy and electron backscatter diffraction. The results showed that a fine-grained microstructure was present with an average grain size of 3.62 μm in sheets rolled from CVCDE extrudate at 623 K. Dynamic recrystallization and a large strain were induced by the multi-pass rolling, which resulted in grain refinement. In the 573-673 K range, the yield strength, tensile strength and elongation initially increased and then declined as the CVCDE temperature increased. The above results provide an important scientific basis of processing, manufacturing and the active control on microstructure and property for high-performance magnesium alloy sheet.

Texture and mechanical properties of Al-0.5Mg-1.0Si-0.5Cu alloy sheets manufactured via a cross rolling method

Science.gov (United States)

Jeon, Jae-Yeol; Son, Hyeon-Taek; Woo, Kee-Do; Lee, Kwang-Jin

2012-04-01

The relationship between the texture and mechanical properties of 6xxx aluminum alloy sheets processed via cross rolling was investigated. The microstructures of the conventional rolled and cross rolled sheets after annealing were analyzed using optical micrographs (OM). The texture distribution across the thickness in the Al-Mg-Si-Cu alloy, conventional rolled sheets, and cross rolled sheets both before and after annealing was investigated via X-ray texture measurements. The texture was analyzed in three layers from the surface to the center of the sheet. The β-fiber texture of the conventional rolled sheet was typical of the texture obtained using aluminumoll ring. After annealing, the typical β-fiber orientations were changed to recrystallization textures: cube{001} and normal direction (ND)-rotated cubes. However, the texture of the cross rolled sheet was composed of an asymmetrical, rolling direction (RD)-rotated cubes. After annealing, the asymmetrical orientations in the cross rolled sheet were changed to a randomized texture. The average R-value of the annealed cross rolled sheets was higher than that of the conventional rolled sheets. The limit dome height (LDH) test results demonstrated that cross rolling is effective in improving the formability of the Al-Mg-Si-Cu alloy sheets.

A computer system to aid in the planning of steel rolls cuts

Directory of Open Access Journals (Sweden)

Nelson Maculan

2007-03-01

Full Text Available The planning of cuts in steel rolls is a combinatory optimization problem. Some companies of the metallurgical industry use the steel cold lamination process so that it acquires the necessary physical properties. In this case, the cutting patterns should consist of compartments of items compatible with the lamination process, hindering the task of cuts planning. A compartment represents an intermediate roll to be laminated, so that it is possible to combine intermediate rolls with different lamination needs in the same roll of the stock. In this work the prototype of the RollCut System will be presented to aid with the cuts planning.

State parameter-based modelling of microstructure evolution in micro-alloyed steel during hot forming

International Nuclear Information System (INIS)

Buken, H; Kozeschnik, E

2016-01-01

In steel production, thermo-mechanical treatment at elevated temperatures is an inevitable step for controlling the microstructure and, thus, the mechanical-technological properties of the final product. One of the main goals in modelling microstructure evolution is the prediction of progress and interaction of hardening and softening mechanism at temperatures, where reheating, hot rolling, finish rolling and coiling are typically carried out. The main mechanisms that need to be accounted for are precipitation, grain growth, solute drag, recovery, recrystallization and phase transformation, which are to be described as functions of temperature, external loading and chemical composition of the material. In the present work, we present a new approach for dealing with these problems and apply it to the thermal and mechanical loading of microalloyed steel. Within this model, we quantitatively predict, for instance, the phenomenon of recrystallization stop in the presence of precipitation. The computational treatment is verified against experimental data from literature, where good agreement is achieved. (paper)

High-Strength Low-Alloy Steel Strengthened by Multiply Nanoscale Microstructures

Science.gov (United States)

Shen, Y. F.; Zuo, L.

Recently, we have being focused on improving the strength without sacrificing ductility of High-strength low-alloy (HSLA) steels by designing nanostructures. Several developments have been obtained, summarized as the following three parts: (a) Depressively nanoscale precipitates: A ferritic steel with finely dispersed precipitates reveals a yield strength of 760 MPa, approximately three times higher than that of conventional Ti-bearing high strength hot-rolled sheet steels, and its ultimate tensile strength reaches 850 MPa with an elongation-to-failure value of 18%. The finely dispersed TiC precipitates in the matrix provide matrix strengthening. The estimated magnitude of precipitation strengthening is around 458 MPa. The effects of the particle size, particle distribution and intrinsic particle strength have been investigated through dislocation dynamics (DD) simulations. The DD results show that strengthening is not only a function of the density of the nano-scale precipitates but also of their size. (b) Ultrafinely ferritic plate: An interstitial-free (IF) steel sheet with a cold-rolling reduction of 75% shows a high tensile strength (710MPa) while preserving a considerable plastic strain (13%). The ductility recovery with increasing the rolling reduction up to 75% is related with the decreasing both in lamellar spacings and cell blocks sizes. (c) Parallel nano-laminated austenite: A composite microstructure consisting of ferrite, bainitic ferrite (BF) laths and retained austenite (RA) platelets has been found for the steel with a chemical composition of 0.19C-0.30Si-1.76Mn-1.52Al (in mass fraction), processed with annealing and bainitic holding. The sample annealed at 820oC (for 120s) and partitioned at 400oC (for 300s) has the best combination of ultimate tensile strength (UTS, 682 MPa) and elongation to failure ( 70%) with about 26% of BF plates 16% RA in its microstructure.

Three-Sheet Spot Welding of Advanced High-Strength Steels

DEFF Research Database (Denmark)

Nielsen, Chris Valentin; Friis, Kasper Storgaard; Zhang, W.

2011-01-01

The automotive industry has introduced the three-layer weld configuration, which represents new challenges compared to normal two-sheet lap welds. The process is further complicated by introducing high-strength steels in the joint. The present article investigates the weldability of thin, low....... The weld mechanisms are analyzed numerically and compared with metallographic analyses showing how the primary bonding mechanism between the thin, low-carbon steel sheet and the thicker sheet of high-strength steel is solid-state bonding, whereas the two high-strength steels are joined by melting, forming...... a weld nugget at their mutual interface. Despite the absence of the typical fusion nugget through the interface between the low-carbon steel and high-strength steel, the weld strengths obtained are acceptable. The failure mechanism in destructive testing is ductile fracture with plug failure....

Mechanical Properties of Laser Beam Welded Ultra-high Strength Chromium Steel with Martensitic Microstructure

Science.gov (United States)

Dahmen, Martin; Janzen, Vitalij; Lindner, Stefan; Wagener, Rainer

A new class of steels is going to be introduced into sheet manufacturing. Stainless ferritic and martensitic steels open up opportunities for sheet metal fabrication including hot stamping. A strength of up to 2 GPa at a fracture strain of 15% can be attained. Welding of these materials became apparently a challenge. Energy-reduced welding methods with in-situ heat treatment are required in order to ensure the delicate and complex heat control. Laser beam welding is the joining technique of choice to supply minimum heat input to the fusion process and to apply an efficient heat control. For two application cases, production of tailored blanks in as-rolled condition and welding in assembly in hot stamped conditions, welding processes have been developed. The welding suitability is shown in metallurgical investigations of the welds. Crash tests based on the KSII concept as well as fatigue tests prove the applicability of the joining method. For the case of assembly also joining with deep drawing and manganese boron steel was taken into consideration. The strength of the joint is determined by the weaker partner but can benefit from its ductility.

New developments in tribomechanical modeling of automotive sheet steel forming

Science.gov (United States)

Khandeparkar, Tushar; Chezan, Toni; van Beeck, Jeroen

2018-05-01

Forming of automotive sheet metal body panels is a complex process influenced by both the material properties and contact conditions in the forming tooling. Material properties are described by the material constitutive behavior and the material flow into the forming die can be described by the tribological system. This paper investigates the prediction accuracy of the forming process using the Tata Steel state of the art description of the material constitutive behavior in combination with different friction models. A cross-die experiment is used to investigate the accuracy of local deformation modes typically seen in automotive sheet metal forming operations. Results of advanced friction models as well as the classical Coulomb friction description are compared to the experimentally measured strain distribution and material draw-in. Two hot-dip galvanized coated steel forming grades were used for the investigations. The results show that the accuracy of the simulation is not guaranteed by the advanced friction models for the entire investigated blank holder force range, both globally and locally. A measurable difference between the calculated and measured local strains is seen for both studied models even in the case where the global indicator, i.e. the draw-in, is well predicted.

Cladding of aluminum on AISI 304L stainless steel by cold roll bonding: Mechanism, microstructure, and mechanical properties

Energy Technology Data Exchange (ETDEWEB)

Akramifard, H.R., E-mail: akrami.1367@ut.ac.ir [School of Metallurgy and Materials Engineering, College of Engineering, University of Tehran, P.O. Box 11155-4563, Tehran (Iran, Islamic Republic of); Mirzadeh, H., E-mail: hmirzadeh@ut.ac.ir [School of Metallurgy and Materials Engineering, College of Engineering, University of Tehran, P.O. Box 11155-4563, Tehran (Iran, Islamic Republic of); Advanced Metalforming and Thermomechanical Processing Laboratory, School of Metallurgy and Materials Engineering, University of Tehran, Tehran (Iran, Islamic Republic of); Parsa, M.H., E-mail: mhparsa@ut.ac.ir [School of Metallurgy and Materials Engineering, College of Engineering, University of Tehran, P.O. Box 11155-4563, Tehran (Iran, Islamic Republic of); Center of Excellence for High Performance Materials, School of Metallurgy and Materials Engineering, University of Tehran, Tehran (Iran, Islamic Republic of); Advanced Metalforming and Thermomechanical Processing Laboratory, School of Metallurgy and Materials Engineering, University of Tehran, Tehran (Iran, Islamic Republic of)

2014-09-08

The AA1050 aluminum alloy and AISI 304L stainless steel sheets were stacked together to fabricate Al/304L/Al clad sheet composites by the cold roll bonding process, which was performed at temperatures of ∼100 and 23 °C to produce austenitic and austenitic–martensitic microstructures in the AISI 304L counterpart, respectively. The peel test results showed that the threshold reduction required to make a suitable bond at room temperature is below 10%, which is significantly lower than the required reduction for cold roll bonding of Al sheets. The tearing of the Al sheet during the peel test signified that the bond strength of the roll bonded sheets by only 38% reduction has reached the strength of Al, which is a key advantage of the developed sheets. The extrusion of Al through the surface cracks and settling inside the 304L surface valleys due to strong affinity between Al and Fe was found to be the bonding mechanism. Subsequently, the interface and tensile behaviors of three-layered clad sheets after soaking at 200–600 °C for 1 h were investigated to characterize the effect of annealing treatment on the formation and thickening of intermetallic compound layer and the resultant mechanical properties. Field emission scanning electron microscopy, X-ray diffraction, and optical microscopy techniques revealed that an intermediate layer composed mainly of Al{sub 13}Fe{sub 4}, FeC and Al{sub 8}SiC{sub 7} forms during annealing at 500–600 °C. A significant drop in tensile stress–strain curves after the maximum point (UTS) was correlated to the interface debonding. It was found that the formation of intermediate layer by post heat treatment deteriorates the bond quality and encourages the debonding process. Moreover, the existence of strain-induced martensite in clad sheets was found to play a key role in the enhancement of tensile strength.

Investigation of bending fatigue-life of aluminum sheets based on rolling direction

Directory of Open Access Journals (Sweden)

Raif Sakin

2018-03-01

Full Text Available High-cycle fatigue (HCF and low-cycle fatigue (LCF fatigue lives of rolled AA1100 and AA1050 aluminum sheets along different directions were evaluated at room temperature. Four types of samples denoted as longitudinal (L and transverse (T to the rolling direction were compared because the samples along the two typical directions show an obvious anisotropy. A cantilever plane-bending and multi-type fatigue testing machine was specially designed for this purpose. Deflection-controlled fatigue tests were conducted under fully reversed loading. The longest fatigue lives in the LCF region were obtained for AA1050 (L while AA1100 (L samples had the longest fatigue lives in the HCF region. Keywords: AA1100, AA1050, Aluminum sheet, Bending fatigue life, Rolling direction

Rolling contact fatigue of low hardness steel for slewing ring application

Science.gov (United States)

Knuth, Jason A.

This thesis discusses the rolling contact fatigue of steel utilized in anti-friction bearings, also referred to as slewing bearings. These slewing bearings are utilized in cranes, excavators, wind turbines and other similar applications. Five materials composed of two different material types were tested. The two material types were high carbon steel and medium carbon alloy steel. The test specimens were processed from forged rolled rings. Two machines were evaluated a ZF-RCF and 3-Ball test machine. The evaluation was to determine which machine can best simulate the application in which the slewing bearing is utilized. Initially, each specimen will be pretested to determine the appropriate testing direction from within the forged rolled rings. Pretesting is needed in order to establish consistent failure modes between samples. The primary goal of the test is to understand the life differences and failure modes between high carbon steel and medium carbon alloy steel. The high carbon steel ring was cut into two sections, one of which was stress relieved and the other was quenched and tempered. The medium carbon alloy steel was cut into three sections, all of which were quenched and tempered to different hardness levels. The test program was dynamically adjusted based upon the previous sample's life and load. An S-N curve was then established from the 5 materials tested at two target loads. The samples were run until the first sign of a crack was detected by an eddy current. At the completion of the rolling contact test, select sample's microstructure was evaluated for crack initiation location. The selected samples were divided into four groups which represent different maximum shear stress levels. These samples displayed indications of material deformation in which the high carbon steel experienced an increased amount of cold work when compared to medium carbon alloy steel. The life of the high carbon steel was nearly equivalent to the expected life of the medium

Effect of rolling on the residual stresses and magnetic properties of a 0.5% Si electrical steel

International Nuclear Information System (INIS)

Campos, M.F. de; Sablik, M.J.; Landgraf, F.J.G.; Hirsch, T.K.; Machado, R.; Magnabosco, R.; Gutierrez, C.J.; Bandyopadhyay, A.

2008-01-01

Cold-rolled (0-19% of reduction) 0.5% Si electrical steel sheets were studied in detail, including macro and micro residual stress measurements, crystallographic texture, dc-hysteresis curves and iron losses. Even for the smallest deformation, losses increase significantly, with large increase of the hysteresis losses, whereas the anomalous losses reduce slightly. The residual microstresses are ∼150-350 MPa, whereas residual macrostresses are compressive, ∼50 MPa. The large increase of the hysteresis losses is attributed to the residual microstresses. The dislocation density estimated by X-ray diffraction is in reasonable agreement with that predicted from the Sablik et al. model for effect of plastic deformation on hysteresis. The intensity of the texture fibers {1 1 1} and //RD (RD=rolling direction) increases with the reduction

Application of powder metallurgy and hot rolling processes for manufacturing aluminum/alumina composite strips

Energy Technology Data Exchange (ETDEWEB)

Zabihi, Majed, E-mail: m.zabihi@ma.iut.ac.ir [Department of Materials Engineering, Isfahan University of Technology, Isfahan 84156-83111 (Iran, Islamic Republic of); Toroghinejad, Mohammad Reza, E-mail: toroghi@cc.iut.ac.ir [Department of Materials Engineering, Isfahan University of Technology, Isfahan 84156-83111 (Iran, Islamic Republic of); Shafyei, Ali, E-mail: shafyei@cc.iut.ac.ir [Department of Materials Engineering, Isfahan University of Technology, Isfahan 84156-83111 (Iran, Islamic Republic of)

2013-01-10

In this study, aluminum matrix composites (AMC) with 2, 4, 6 and 10 wt% alumina were produced using powder metallurgy (PM), mechanical milling (MM) and vacuum hot pressing (VHP) techniques; then, this was followed by the hot-rolling process. During hot rolling, AMCs with 6 and 10 wt% Al{sub 2}O{sub 3} were fractured whereas strip composites with 2 and 4 wt% Al{sub 2}O{sub 3} were produced successfully. Microstructure and mechanical properties of the samples were investigated by optical and scanning electron microscopes and tensile and hardness tests, respectively. Microscopic evaluations of the hot-rolled composites showed a uniform distribution of alumina particles in the aluminum matrix. It was found that with increasing alumina content in the matrix, tensile strength (TS) and hardness increased and the percentage of elongation also decreased. Scanning electron microscope (SEM) was used to investigate aluminum/alumina interfaces and fracture surfaces of the hot rolled specimens after tensile test. SEM observations demonstrated that the failure mode in the hot-rolled Al-2 wt% Al{sub 2}O{sub 3} composite strips is a typical ductile fracture, while the failure mode was shear ductile fracture with more flat surfaces in Al-4 wt% Al{sub 2}O{sub 3} strips.

Milled Die Steel Surface Roughness Correlation with Steel Sheet Friction

DEFF Research Database (Denmark)

Berglund, J.; Brown, C.A.; Rosén, B.-G.

2010-01-01

This work investigates correlations between the surface topography ofmilled steel dies and friction with steel sheet. Several die surfaces were prepared by milling. Friction was measured in bending under tension testing. Linear regression coefficients (R2) between the friction and texture...

Nanograined Ti–Nb microalloy steel achieved by Accumulative Roll Bonding (ARB) process

International Nuclear Information System (INIS)

Tohidi, A.A.; Ketabchi, M.; Hasannia, A.

2013-01-01

Over the last decade, nanocrystalline and ultra-fine grained (UFG) materials with grain size less than 1 μm have aroused considerable interest due to their superior mechanical properties compared to conventionally grained materials. In this work Ti–Nb microalloy steel was processed by the severe plastic deformation (SPD) technique called Accumulative Roll Bonding (ARB) in order to produce an ultra-fine grained microstructure and improve the mechanical properties. After initial preparation to achieve good sheet bonding, 8 cycles of ARB at 550 °C were successfully performed. Observation of optical microstructure, scanning electron microscopy (SEM) micrographs, and X-Ray Diffraction (XRD) peak broadening analysis were used for the characterization of grain structure of the ARB processed sample. The mechanical attributes after rolling and cooling were examined. It was calculated that metal's yield and tensile strength increased by 334% and 215% respectively, while the ductility dropped from as-received value of 34% to 2.9%. Microhardness of the material was studied at room temperature. There was a continuous enhancement of hardness by increasing the pass number of the ARB process. At the 8th pass, the hardness values increased by 230%. The rolling process was stopped at 8th cycle when cracking of the edge became pronounced

Formability of aluminium sheets manufactured by solid state recycling

Science.gov (United States)

Kore, A. S.; Nayak, K. C.; Date, P. P.

2017-09-01

Conventional recycling practices for non-ferrous metallic scrap involves melting followed by purification. This practice is suitable for recycling when the large volume of scrap is available. Though such recycling reduces consumption of diminishing metallic resources, high energy requirement and material loss during melting and purification limit its applicability. In the present work, manufacturing of solid state recycled aluminium sheet by hot rolling is explored and its formability characterized. Aluminium chips were divided into smaller particles (1~2mm) by crushing. After stress relief annealing, chips were cold compacted into square slabs (75*75mm section) of different thicknesses. Another similar set of slabs was made by hot compaction. The compacted slabs were hot rolled over a number of passes at 400°C. Each slab was reduced to approximately 90% thickness to get the sheet thickness in the range of 0.6 to 1.5 mm. Microstructure revealed good interface bonding between the chip particles. Mechanical properties of the sheet from room temperature up to 200°C and at different strain rates were characterized by a number of tensile tests. Circular blanks from sheet were drawn into cylindrical cups and strain distribution was observed along different directions of rolling using circle grid analysis.

Local laser-strengthening: Customizing the forming behavior of car body steel sheets

Science.gov (United States)

Wagner, M.; Jahn, A.; Beyer, E.; Balzani, D.

2018-05-01

Future trends in designing lightweight components especially for automotive applications increasingly require complex and delicate structures with highest possible level of capacity [1]. The manufacturing of metallic car body components is primarily realized by deep or stretch drawing. The forming process of especially cold rolled and large-sized components is typically characterized by inhomogeneous stress and strain distributions. As a result, the avoidance of undesirable deep drawing effects like earing and local necking is among the greatest challenges in forming complex car body structures [2]. Hence, a novel local laser-treatment approach with the objective of customizing the forming behavior of car body steel sheets is currently explored.

Ni-Flash-Coated Galvannealed Steel Sheet with Improved Properties

Science.gov (United States)

Pradhan, D.; Dutta, M.; Venugopalan, T.

2016-11-01

In the last several years, automobile industries have increasingly focused on galvannealed (GA) steel sheet due to their superior properties such as weldability, paintability and corrosion protection. To improve the properties further, different coatings on GA have been reported. In this context, an electroplating process (flash coating) of bright and adherent Ni plating was developed on GA steel sheet for covering the GA defects and enhancing the performances such as weldability, frictional behavior, corrosion resistance and phosphatability. For better illustration, a comparative study with bare GA steel sheet has also been carried out. The maximum electroplating current density of 700 A/m2 yielded higher cathode current efficiency of 95-98%. The performances showed that Ni-coated (coating time 5-7 s) GA steel sheet has better spot weldability, lower dynamic coefficient of friction (0.07 in lubrication) and three times more corrosion resistance compared to bare GA steel sheet. Plate-like crystal of phosphate coating with size of 10-25 µm was obtained on the Ni-coated GA. The main phase in the phosphate compound was identified as hopeite (63.4 wt.%) along with other phases such as spencerite (28.3 wt.%) and phosphophyllite (8.3 wt.%).

Recent development of non-oriented electrical steel sheet for automobile electrical devices

International Nuclear Information System (INIS)

Oda, Yoshihiko; Kohno, Masaaki; Honda, Atsuhito

2008-01-01

This paper describes non-oriented electrical steel sheet for automobile motors and reactors. Electrical steel sheets for energy efficient motors show high magnetic flux density and low iron loss. They are suitable for HEV traction motors and EPS motors. A thin-gauge electrical steel sheet and a gradient Si steel sheet show low iron loss in the high-frequency range. Therefore, the efficiency of high-frequency devices can be greatly improved. Since a 6.5% Si steel sheet possesses low iron loss and zero magnetostriction, it contributes to reduce the core loss and audible noise of high-frequency reactors

77 FR 32998 - Tin- and Chromium-Coated Steel Sheet From Japan

Science.gov (United States)

2012-06-04

...-Coated Steel Sheet From Japan Determination On the basis of the record \\1\\ developed in the subject five... order on tin- and chromium-coated steel sheet from Japan would be likely to lead to continuation or... USITC Publication 4325 (May 2012), entitled Tin- and Chromium-Coated Steel Sheet from Japan...

Flow behavior of polymers during the roll-to-roll hot embossing process

International Nuclear Information System (INIS)

Deng, Yujun; Yi, Peiyun; Peng, Linfa; Lai, Xinmin; Lin, Zhongqin

2015-01-01

The roll-to-roll (R2R) hot embossing process is a recent advancement in the micro hot embossing process and is capable of continuously fabricating micro/nano-structures on polymers, with a high efficiency and a high throughput. However, the fast forming of the R2R hot embossing process limits the time for material flow and results in complicated flow behavior in the polymers. This study presents a fundamental investigation into the flow behavior of polymers and aims towards the comprehensive understanding of the R2R hot embossing process. A three-dimensional (3D) finite element (FE) model based on the viscoelastic model of polymers is established and validated for the fabrication of micro-pyramids using the R2R hot embossing process. The deformation and recovery of micro-pyramids on poly(vinyl chloride) (PVC) film are analyzed in the filling stage and the demolding stage, respectively. Firstly, in the analysis of the filling stage, the temperature distribution on the PVC film is discussed. A large temperature gradient is observed along the thickness direction of the PVC film and the temperature of the top surface is found to be higher than that of the bottom surface, due to the poor thermal conductivity of PVC. In addition, creep strains are demonstrated to depend highly on the temperature and are also observed to concentrate on the top layer of the PVC film because of high local temperature. In the demolding stage, the recovery of the embossed micro-pyramids is obvious. The cooling process is shown to be efficient for the reduction of recovery, especially when the mold temperature is high. In conclusion, this research advances the understanding of the flow behavior of polymers in the R2R hot embossing process and might help in the development of the highly accurate and highly efficient fabrication of microstructures on polymers. (paper)

A quality approach to maintain the properties of S235 JR structural carbon steel in Lebanon

International Nuclear Information System (INIS)

Sidawi, J.A.; Al Khatib, H.

2004-01-01

Full text.S235JR carbon steel is one of the most popular steels used in Lebanon. It is imported by steel dealers and is widely used by all fabricators and manufacturers of steels for many structural purposes and applications. This kind of steel has good ductile properties as well as excellent weldability. It is still known by its previous designation St 37-2 or E 24-2. S235JR is produced in many shapes and thicknesses such as steel plates, sheets, angles and different other geometric shapes. Standard chemical and mechanical tests were conducted and reported on S235JR hot-rolled structural low-carbon mild steel specimens collected from Lebanese steel market. The main objective of this work is to assure the compliance of these properties with those set by the steel manufacturer. The above mentioned tests were performed at the laboratories of the Industrial Research Institute (IR) in Lebanon to assure the quality and credibility of the results. related European and American standards were presented as references and compared with the achieved results. Discussion was presented to show the similarities and differences between S235JR steel samples and standard requirements. Some of the reasons for such differences were discussed. Sufficient data was furnished through this work for the public and mainly for the Lebanese Standard Organization LIBNOR to easily adopt and implement the EN 10025:1993 European standard that can be applied in Lebanon concerning the most commonly used hot rolled low carbon structural steel. A follow up concerning adopting and implementing EN 10025:1993 will be briefed

CO2 laser welding of galvanized steel sheets using vent holes

International Nuclear Information System (INIS)

Chen Weichiat; Ackerson, Paul; Molian, Pal

2009-01-01

Joining of galvanized steels is a challenging issue in the automotive industry because of the vaporization of zinc at 906 deg. C during fusion welding of steel (>1530 deg. C). In this work, hot-dip galvanized steel sheets of 0.68 mm thick (24-gage) were pre-drilled using a pulsed Nd:YAG laser to form vent holes along the weld line and then seam welded in the lap-joint configuration using a continuous wave CO 2 laser. The welds were evaluated through optical and scanning electron microscopy and tensile/hardness tests. The vent holes allowed zinc vapors to escape through the weld zone without causing expulsion of molten metal, thereby eliminating the defects such as porosity, spatter, and loss of penetration. In addition, riveting of welds occurred so long as the weld width was greater than the hole diameter that in turn provided much higher strength over the traditional 'joint gap' method

Simulation of Bimetallic Bush Hot Rolling Bonding Process

Directory of Open Access Journals (Sweden)

Yaqin Tian

2015-01-01

Full Text Available Three-dimensional model of bimetallic bush was established including the drive roller and the core roller. The model adopted the appropriate interface assumptions. Based on the bonding properties of bimetallic bush the hot rolling process was analyzed. The optimum reduction ratio of 28% is obtained by using the finite element simulation software MARC on the assumption of the bonding conditions. The stress-strain distribution of three dimensions was research assumptions to interface deformation of rolling. At the same time, based on the numerical simulation, the minimum reduction ratio 20% is obtained by using a double metal composite bush rolling new technology from the experiment research. The simulation error is not more than 8%.

Additional grain refinement in recrystallization controlled rolling of Ti-microalloyed steels processed by near-net-shape casting technology

International Nuclear Information System (INIS)

Arribas, M.; Lopez, B.; Rodriguez-Ibabe, J.M.

2008-01-01

This paper analyzes the recrystallization kinetics in Ti-microalloyed steels processed using 'beam blank' casting technology. The faster solidification rates associated with this technology brings a finer precipitation of TiN particles which are very effective in controlling austenite grain growth during hot working. Furthermore, these small precipitates have been shown to delay static and dynamic recrystallization. The finer the precipitates the higher the delay in recrystallization. Nevertheless, beyond particle size and distribution, the level of delay is very dependent on microstructure (above all austenite grain size) and deformation conditions (strain and temperature). This paper studies the effects of this recrystallization delay on the microstructure evolution during hot rolling. Special attention was paid to the study of the occurrence of partial recrystallization during the final stages of rolling, which could lead to the presence of mixed microstructures before transformation. The possibility of achieving an additional austenite grain size refinement prior to transformation was evaluated

Experimental analysis of two-layered dissimilar metals by roll bonding

Science.gov (United States)

Zhao, Guanghui; Li, Yugui; Li, Juan; Huang, Qingxue; Ma, Lifeng

2018-02-01

Rolling reduction and base layers thickness have important implications for rolling compounding. A two-layered 304 stainless steel/Q345R low alloyed steel was roll bonded. The roll bonding was performed at the three thickness reductions of 25%, 40% and 55% with base layers of various thicknesses (Q345R). The microstructures of the composite were investigated by the ultra-deep microscope (OM) and scanning electron microscope (SEM) and Transmission electron microscope (TEM). Simultaneously, the mechanical properties of the composite were experimentally measured and the tensile fracture surfaces were observed by SEM. The interfaces were successfully bonded without any cracking or voids, which indicated a good fabrication of the 304/Q345R composite. The rolling reduction rate and thinning increase of the substrate contributed to the bonding effects appearance of the roll bonded sheet. The Cr and Ni enriched diffusion layer was formed by the interface elements diffusion. The Cr and Ni diffusion led to the formation of ˜10 μm wide Cr and Ni layers on the carbon steel side.

Research on Forming Mechanisms and Controlling Measurements for Surface Light Spot Defects of Galvanizing Steel Coils for Automobile Use

Science.gov (United States)

Guangmin, Wei; Haiyan, Sun; Jianqiang, Shi; Lianxuan, Wang; Haihong, Wu

When producing high surface quality galvanizing steel coils for automobile use, there are always many light spots on the surface since Hansteel CGL No.1 has been put into operation. The defect samples were analyzed by SEM and EDS. The result shows that cause for light spot is not only one. There are more Mn and P in high strength auto sheet, which can result in difficulty to be cleaned off the oxide on the hot rolled coils, so the defects coming. This is why the defects come with high strength auto sheet. When coils galvanized, the defects can't be covered up. To the contrary, the defects will be more obvious when zinc growing on the surface. And sometimes zinc or residue can adhere to work rolls when strips passing through SPM. The deposits then press normal coating. So the light spots come more. When the defect comes from pressing, there is no defect on steel base. The causation is found and measures were taken including high pressure cleaning equipments adopted. Result shows that the defects disappeared.

Identification of a process window for tailored carburization of sheet metals in hot stamping

Science.gov (United States)

Horn, Alexander; Merklein, Marion

2018-05-01

Due to governmental regulations concerning the reduction of CO2 emissions and increasing safety standards, hot stamping of high strength boron manganese steel sheets has evolved into a state of the art process for manufacturing structural car body parts. The combined forming and in-die quenching process enables the formation of a fully martensitic microstructure. Therefore, press hardened steels offer high strength, but low ductility. In order to further improve passenger safety, a tailored configuration of mechanical properties is desired. Besides state of the art methods, like the application of locally different heat treatment temperatures or varying quenching rates, the adjustment of mechanical properties of sheet metals by a tailored carburization is a novel approach. For the carburization process, the specimens are first coated with graphite and subsequently heat treated. Within this contribution, different coating strategies as well as heat treatment temperatures and dwell times are investigated. For the determination of a process window, mechanical properties such as tensile strength and microhardness will be analyzed and correlated with the resulting microstructure.

Surface finishing and levelling of thermomechanically hardened rolled steel

International Nuclear Information System (INIS)

Grosval'd, V.G.; Bashchenko, A.P.; Grishkov, A.I.; Gutnik, M.V.; Kanevskij, B.L.; Nikozov, A.I.; Sedov, N.D.; Prosin, K.A.; Safonov, L.I.

1975-01-01

The finishing of high-strength merchant shapes from alloy steel was tried out under industrial conditions with the equipment of metallurgical plants. After thermomechanical hardening in the production line of the rolling mill, 30KhGSN2A and 40Kh1NVA steel rounds 32 and 31 mm in diameter were straightened on a two-roller straightening machine designed by the All-Union Scientific Research Institute for Metallurgical Machinery (VNII Metmash). This made possible subsequent turning and grinding of the rods. The conditions of straightening, turning and grinding have been worked so as to obtain thermomechanically strengthened and ground rolled products approximating the gauged and ground metal in shape geometry and surface finish. It is shown that the labour-consuming operation of turning can be eliminated by reducing the machining pass of the rolled product, and this lowers the labour required for the finishing operations by 75%. After grinding with 40- and 25-grain abrasive wheels, high strength rolled shapes were obtained with a diameter of 30-0.20 mm and a surface finish of class 6-5 satisfying the technical specifications. (author)

Continuum Mechanical Modelling of Skin-pass Rolling

DEFF Research Database (Denmark)

Kijima, Hideo; Bay, Niels

2007-01-01

The special contact conditions in skin-pass rolling of steel strip is analyzed by studying plane strain upsetting of thin sheet with low reduction applying long narrow tools and dry friction conditions. An extended sticking region is estimated by an elasto-plastic FEM analysis of the plane strain...

Through-process characterization of local anisotropy of Non-oriented electrical steel using magnetic Barkhausen noise

Science.gov (United States)

He, Youliang; Mehdi, Mehdi; Hilinski, Erik J.; Edrisy, Afsaneh

2018-05-01

Magnetic Barkhausen noise (MBN) signals were measured on a non-oriented electrical steel through all the thermomechanical processing stages, i.e. hot rolling, hot band annealing, cold rolling and final annealing. The temperature of the final annealing was varied from 600 °C to 750 °C so that the steel consisted of partially or completely recrystallized microstructures and different levels of residual stresses. The angular MBNrms (root mean square) values were compared to the texture factors in the same directions, the latter being calculated from the crystallographic texture measured by electron backscatter diffraction (EBSD). It was found that, in the cold-rolled, hot-rolled and completely recrystallized steels, the angular MBNrms followed a cosine function with respect to the angle of magnetization, while in partially recrystallized state such a relation does not exist. After cold rolling, the maximum MBNrms was observed in the rolling direction (RD) and the minimum MBNrms was in the transverse direction (TD), which was inconsistent with the magnetocrystalline anisotropy as indicated by the texture factor. After hot rolling, the maximum and minimum MBNrms values were observed in the TD and RD, respectively, exactly opposite to the cold-rolled state. If the steel was completely recrystallized, the maximum MBNrms was normally observed at a direction that was 15-30° from the minimum texture factor. If the steel was partially recrystallized, both the magnetocrystalline anisotropy of the material and the residual stress contributed to the angular MBNrms, which resulted in the deviation of the relationship from a cosine function. The relative strength of the two factors determined which factor would dominate the overall magnetic anisotropy.

Evolution of microstructure, texture and inhibitor along the processing route for grain-oriented electrical steels using strip casting

Energy Technology Data Exchange (ETDEWEB)

Liu, Hai-Tao, E-mail: liuht@ral.neu.edu.cn [State Key Laboratory of Rolling and Automation, Northeastern University, P.O. Box 105, Shenyang 110819 (China); Institute of Research of Iron and Steel, Shasteel, Zhangjiagang 215625, Jiangsu (China); Yao, Sheng-Jie [School of Materials Science and Engineering, Harbin Institute of Technology at Weihai, 264209 (China); Sun, Yu; Gao, Fei; Song, Hong-Yu; Liu, Guo-Huai [State Key Laboratory of Rolling and Automation, Northeastern University, P.O. Box 105, Shenyang 110819 (China); Li, Lei; Geng, Dian-Qiao [Key Laboratory of Electromagnetic Processing of Materials, Ministry of Education, Northeastern University, Shenyang 110819 (China); Liu, Zhen-Yu; Wang, Guo-Dong [State Key Laboratory of Rolling and Automation, Northeastern University, P.O. Box 105, Shenyang 110819 (China)

2015-08-15

In the present work, a regular grade GO sheet was produced successively by strip casting, hot rolling, normalizing annealing, two-stage cold rolling with intermediate annealing, primary recrystallization annealing, secondary recrystallization annealing and purification. The aim of this paper was to characterize the evolution of microstructure, texture and inhibitor along the new processing route by comprehensive utilization of optical microscopy, X-ray diffraction and transmission electron microscopy. It was found that a fine microstructure with the ferrite grain size range of 7–12 μm could be obtained in the primary recrystallization annealed sheet though a very coarse microstructure was produced in the initial as-cast strip. The main finding was that the “texture memory” effect on Goss texture started on the through-thickness intermediate annealed strip after first cold rolling, which was not similar to the “texture memory” effect on Goss texture starting on the surface layers of the hot rolled strip in the conventional production route. As a result, the origin of Goss nuclei capable of secondary recrystallization lied in the grains already presented in Goss orientation in the intermediate annealed strip after first cold rolling. Another finding was that fine and dispersive inhibitors (mainly AlN) were easy to be produced in the primary recrystallization microstructure due to the initial rapid solidification during strip casting and the subsequent rapid cooling, and the very high temperature reheating usually used before hot rolling in the conventional production route could be avoided. - Highlights: • A regular grade grain-oriented electrical steel was produced. • Evolution of microstructure, texture and inhibitor was characterized. • Origin of Goss nuclei lied in the intermediate annealed strip. • A fine primary recrystallization microstructure could be produced. • Effective inhibitors were easy to be obtained in the new processing route.

Static recrystallisation and precipitation after hot deformation of austenitic stainless steels containing molybdenum and niobium

International Nuclear Information System (INIS)

Lombry, R.; Rossard, C.; Thomas, B.J.

1981-01-01

In general the hot workability of austenite depends on the work hardening during deformation and the kinetics of the dynamic and static restoration processes. Static recrystallisation is a very important factor in the case of hot rolling. The present work was undertaken to determine the effect of additions of molybdenum or niobium on the kinetics of static recrystallisation. The results show that the rate of static recrystallisation of type 304, 316 and 347 stainless steels decreases in this order for a given amount of prior deformation (epsilon=0,44). The differences in the rates of recrystallisation increases as the temperature is lowered towards 900 deg C. The effect of molybdenum appears to be attribuable to a solute drag effect on the mobility of dislocations, subgrain boundaries or grain boundaries whereas niobium additions lead to the formation of NbC precipitates on the dislocation cell walls and sub boundaries. It is also shown that in the case of type 316 and type 347 steels the dynamic recrystallisation process (observed in type 304 steels at all temperatures above 900 deg C) is replaced by dynamic recovery at temperatures egal to or below about 1000 deg C [fr

ADVANTAGES OF RAPID METHOD FOR DETERMINING SCALE MASS AND DECARBURIZED LAYER OF ROLLED COIL STEEL

Directory of Open Access Journals (Sweden)

E. V. Parusov

2016-08-01

Full Text Available Purpose. To determine the universal empirical relationships that allow for operational calculation of scale mass and decarbonized layer depth based on the parameters of the technological process for rolled coil steel production. Methodology. The research is carried out on the industrial batches of the rolled steel of SAE 1006 and SAE 1065 grades. Scale removability was determined in accordance with the procedure of «Bekaert» company by the specifi-cations: GA-03-16, GA-03-18, GS-03-02, GS-06-01. The depth of decarbonized layer was identified in accordance with GOST 1763-68 (M method. Findings. Analysis of experimental data allowed us to determine the rational temperature of coil formation of the investigated steel grades, which provide the best possible removal of scale from the metal surface, a minimal amount of scale, as well as compliance of the metal surface color with the require-ments of European consumers. Originality. The work allowed establishing correlation of the basic quality indicators of the rolled coil high carbon steel (scale mass, depth of decarbonized layer and inter-laminar distance in pearlite with one of the main parameters (coil formation temperature of the deformation and heat treatment mode. The re-sulting regression equations, without metallographic analysis, can be used to determine, with a minimum error, the quantitative values of the total scale mass, depth of decarbonized layer and the average inter-lamellar distance in pearlite of the rolled coil high carbon steel. Practical value. Based on the specifications of «Bekaert» company (GA-03-16, GA-03-18, GS-03-02 and GS-06-01 the method of testing descaling by mechanical means from the surface of the rolled coil steel of low- and high-carbon steel grades was developed and approved in the environment of PJSC «ArcelorMittal Kryvyi Rih». The work resulted in development of the rapid method for determination of total and remaining scale mass on the rolled coil steel

Influence of surface defects on the fatigue crack initiation in pearlitic steel

Directory of Open Access Journals (Sweden)

Toribio Jesús

2014-06-01

Full Text Available Tensile fatigue tests were performed under load control, with constant stress range Δσ on pearlitic steel wires, from the hot rolled bar to the commercial prestressing steel wire (which has undergone seven cold drawing steps. Results show that fatigue cracks in pearlitic steels initiate at the wire surface starting from small defects, whose size decreases with the drawing process. Fatigue cracks created from defects (initiation phase exhibit a fractographic appearance consisting of ductile microtearing events which can be classified as tearing topography surface or TTS, and exhibit a remarkably lower spacing in the prestressing steel wire than in the hot rolled bar. In addition, some S-N tests were performed in both material forms under a stress range of about half the yield strength. In these tests, the main part of the fatigue life corresponds to the propagation stage in the hot rolled bar whereas such a main part of the life is associated with the initiation stage in the case of the prestressing steel wire.

High-strength high-conductivity Cu-Nb microcomposite sheet fabricated via multiple roll bonding

International Nuclear Information System (INIS)

Jha, S.C.; Delagi, R.G.; Forster, J.A.; Krotz, P.D.

1993-01-01

Copper-niobium microcomposites are a new class of high-strength high-conductivity materials that have attractive properties for room- and elevated-temperature applications. Since Nb has little solid solubility in Cu, addition of Nb to Cu does not affect its conductivity. Copper-niobium microcomposites are melted and cast so that the microstructure of cast Cu-Nb ingots consists of 1- to 10 μm Nb dendrites uniformly distributed within the copper matrix. Extensive wire drawing with a true processing strain (η> 12) of Cu-Nb alloy leads to refinement and elongation of Nb dendrites into 1- to 10 nm-thick filaments. The presence of such fine Nb filaments causes a significant increase in the strength of Cu-Nb wires. The tensile strength of heavily drawn Cu-Nb wires was determined to be significantly higher than the values predicted by the rule of mixtures. This article reports the fabrication of high-strength Cu-Nb microcomposite sheet by multiple roll bonding. It is difficult and impractical to attain high processing strains (η>3) by simple cold rolling. In most practical cold-rolling operation, the thickness reduction does not exceed 90 pct (η ≅2). Therefore, innovative processing is required to generate high strength in Cu-Nb microcomposite sheet. Multiple roll bonding of Cu-Nb has been utilized to store high processing strain ( η>10) in the material and refine the Nb particle size within the copper matrix. This article describes the microstructure, mechanical properties, and thermal stability of roll-bonded Cu-Nb microcomposite sheet

Research on Al-alloy sheet forming formability during warm/hot sheet hydroforming based on elliptical warm bulging test

Science.gov (United States)

Cai, Gaoshen; Wu, Chuanyu; Gao, Zepu; Lang, Lihui; Alexandrov, Sergei

2018-05-01

An elliptical warm/hot sheet bulging test under different temperatures and pressure rates was carried out to predict Al-alloy sheet forming limit during warm/hot sheet hydroforming. Using relevant formulas of ultimate strain to calculate and dispose experimental data, forming limit curves (FLCS) in tension-tension state of strain (TTSS) area are obtained. Combining with the basic experimental data obtained by uniaxial tensile test under the equivalent condition with bulging test, complete forming limit diagrams (FLDS) of Al-alloy are established. Using a quadratic polynomial curve fitting method, material constants of fitting function are calculated and a prediction model equation for sheet metal forming limit is established, by which the corresponding forming limit curves in TTSS area can be obtained. The bulging test and fitting results indicated that the sheet metal FLCS obtained were very accurate. Also, the model equation can be used to instruct warm/hot sheet bulging test.

Mathematical Modelling of Carbonitride Precipitation during Hot Working in Nb Microalloyed Steels

Institute of Scientific and Technical Information of China (English)

无

2006-01-01

Based on thermodynamics and kinetics, precipitation behavior of microalloyed steels was analyzed. Deformation greatly promotes isothermal carbonitride precipitation and makes C-curve shift leftwards. The position and shape of C-curve also depend on the content of Nb and N. C-curve shifts leftwards a little when N content increases and the nose temperature is raised with increasing Nb content. Deformation shortened precipitation start time during continuous cooling, raised precipitation start temperature, accelerated precipitation kinetics of carbonitrides. With decreasing the finishing temperature and coiling temperature, the precipitates volume fraction increases and strength increment is raised during hot rolling. The simulated results are in agreementwith experiment results.

Influence of grain size and texture prior to warm rolling on microstructure, texture and magnetic properties of Fe-6.5 wt% Si steel

Science.gov (United States)

Xu, H. J.; Xu, Y. B.; Jiao, H. T.; Cheng, S. F.; Misra, R. D. K.; Li, J. P.

2018-05-01

Fe-6.5 wt% Si steel hot bands with different initial grain size and texture were obtained through different annealing treatment. These bands were then warm rolled and annealed. An analysis on the evolution of microstructure and texture, particularly the formation of recrystallization texture was studied. The results indicated that initial grain size and texture had a significant effect on texture evolution and magnetic properties. Large initial grains led to coarse deformed grains with dense and long shear bands after warm rolling. Such long shear bands resulted in growth advantage for {1 1 3} 〈3 6 1〉 oriented grains during recrystallization. On the other hand, sharp {11 h} 〈1, 2, 1/h〉 (α∗-fiber) texture in the coarse-grained sample led to dominant {1 1 2} 〈1 1 0〉 texture after warm rolling. Such {1 1 2} 〈1 1 0〉 deformed grains provided massive nucleation sites for {1 1 3} 〈3 6 1〉 oriented grains during subsequent recrystallization. These {1 1 3} 〈3 6 1〉 grains were confirmed to exhibit an advantage on grain growth compared to γ-fiber grains. As a result, significant {1 1 3} 〈3 6 1〉 texture was developed and unfavorable γ-fiber texture was inhibited in the final annealed sheet. Both these aspects led to superior magnetic properties in the sample with largest initial grain size. The magnetic induction B8 was 1.36 T and the high frequency core loss P10/400 was 17.07 W/kg.

46 CFR 105.20-3 - Cargo tanks.

Science.gov (United States)

2010-10-01

...) Construction and Materials. (1) The cargo tanks must be constructed of iron, steel, copper, nickel alloy... inches and gage number 2,3 Nickel copper B127, hot rolled sheet or plate 0.107 (USSG 12). Copper nickel 1... sheet and plate iron and steel. The letters “AWG” stand for “American Wire Gage” (or Brown and Sharpe...

Preparation and characterization of 304 stainless steel/Q235 carbon steel composite material

Science.gov (United States)

Shen, Wenning; Feng, Lajun; Feng, Hui; Cao, Ying; Liu, Lei; Cao, Mo; Ge, Yanfeng

The composite material of 304 stainless steel reinforced Q235 carbon steel has been prepared by modified hot-rolling process. The resulted material was characterized by scanning electron microscope, three-electrode method, fault current impact method, electrochemical potentiodynamic polarization curve measurement and electrochemical impedance spectroscopy. The results showed that metallurgical bond between the stainless steel layer and carbon steel substrate has been formed. The composite material exhibited good electrical conductivity and thermal stability. The average grounding resistance of the composite material was about 13/20 of dip galvanized steel. There has no surface crack and bubbling formed after fault current impact. The composite material led to a significant decrease in the corrosion current density in soil solution, compared with that of hot dip galvanized steel and bare carbon steel. On the basis polarization curve and EIS analyses, it can be concluded that the composite material showed improved anti-corrosion property than hot-dip galvanized steel.

Electrochemical Corrosion Behavior of Carbon Steel and Hot Dip Galvanized Steel in Simulated Concrete Solution with Different pH Values

Directory of Open Access Journals (Sweden)

Wanchen XIE

2017-08-01

Full Text Available Hot dip galvanizing technology is now widely used as a method of protection for steel rebars. The corrosion behaviors of Q235 carbon steel and hot galvanized steel in a Ca(OH2 solution with a pH from 10 to 13 was investigated by electrode potential and polarization curves testing. The results indicated that carbon steel and hot galvanized steel were all passivated in a strong alkaline solution. The electrode potential of hot dip galvanized steel was lower than that of carbon steel; thus, hot dip galvanized steel can provide very good anodic protection for carbon steel. However, when the pH value reached 12.5, a polarity reversal occurred under the condition of a certain potential. Hot dip galvanized coating became a cathode, and the corrosion of carbon steel accelerated. The electrochemical behaviors and passivation abilities of hot dip galvanized steel and carbon steel were affected by pH. The higher the pH value was, the more easily they were passivated.DOI: http://dx.doi.org/10.5755/j01.ms.23.3.16675

Investigation of Forming Performance of Laminated Steel Sheets Using Finite Element Analyses

International Nuclear Information System (INIS)

Liu Wenning; Sun Xin; Ruokolainen, Robert; Gayden Xiaohong

2007-01-01

Laminated steel sheets have been used in automotive structures for reducing in-cabin noise. However, due to the marked difference in material properties of the different laminated layers, integrating laminated steel parts into the manufacturing processes can be challenging. Especially, the behavior of laminated sheets during forming processes is very different from that of monolithic steel sheets. During the deep-draw forming process, large shear deformation and corresponding high interfacial stress may initiate and propagate interfacial cracks between the core polymer and the metal skin, hence degrading the performance of the laminated sheets. In this paper, the formability of the laminated steel sheets is investigated by means of numerical analysis. The goal of this work is to gain insight into the relationship between the individual properties of the laminated sheet layers and the corresponding formability of the laminated sheet as a whole, eventually leading to reliable design and successful forming process development of such materials. Finite element analyses of laminate sheet forming are presented. Effects of polymer core thickness and viscoelastic properties of the polymer core, as well as punching velocity, are also investigated

About the influence of the topography of the steel surface on faults during hot galvanizing of part loads; Zum Einfluss der Topographie der Stahloberflaeche auf Fehler beim Stueckgut-Feuerverzinken

Energy Technology Data Exchange (ETDEWEB)

Schulz, W.D. [Institut fuer Korrosionsschutz GmbH, Dresden (Germany); Schubert, P.

2002-03-01

The topography of the steel surface can influence the formation of layers during hot galvanizing in many ways. Information is given on galvanizing faults caused by impressions in the steel surface (rolling and drawing ridges). Flux remainders accumulated in these impressions can be encapsulated in the zinc coating during hot galvanizing. This leads to cavities and pores in the coating or to sponge-like zinc raisings at its surface. The flux remainders from the zinc coating can boil during powder coating and lead to blisters and pimple-like rises in the coating. Therefore, steel surfaces designed for galvanizing should be even or only have flat impressions. (orig.)

Preparation and characterization of 304 stainless steel/Q235 carbon steel composite material

Directory of Open Access Journals (Sweden)

Wenning Shen

Full Text Available The composite material of 304 stainless steel reinforced Q235 carbon steel has been prepared by modified hot-rolling process. The resulted material was characterized by scanning electron microscope, three-electrode method, fault current impact method, electrochemical potentiodynamic polarization curve measurement and electrochemical impedance spectroscopy. The results showed that metallurgical bond between the stainless steel layer and carbon steel substrate has been formed. The composite material exhibited good electrical conductivity and thermal stability. The average grounding resistance of the composite material was about 13/20 of dip galvanized steel. There has no surface crack and bubbling formed after fault current impact. The composite material led to a significant decrease in the corrosion current density in soil solution, compared with that of hot dip galvanized steel and bare carbon steel. On the basis polarization curve and EIS analyses, it can be concluded that the composite material showed improved anti-corrosion property than hot-dip galvanized steel. Keywords: Stainless steel, Carbon steel, Anti-corrosion, Conductivity, Electrochemical, EIS

Effects of initial microstructure and texture on microstructure, texture evolution and magnetic properties of non-oriented electrical steel

Energy Technology Data Exchange (ETDEWEB)

Liu, Hai-Tao, E-mail: liuht@ral.neu.edu.cn [State Key Laboratory of Rolling and Automation, Northeastern University, P.O. Box 105, Shenyang 110819 (China); Institute of Research of Iron and Steel, Shasteel, Zhangjiagang 215625, Jiangsu (China); Li, Hua-Long [Institute of Research of Iron and Steel, Shasteel, Zhangjiagang 215625, Jiangsu (China); Wang, Hui [Science and Technology on Surface Physics and Chemistry Laboratory, P.O. Box No. 9-35, Huafengxincun, Jiangyou City, Sichuan Province 621908 (China); National Key Laboratory for Nuclear Fuel and Materials, Nuclear Power Institute of China, Chengdu 610041 (China); Liu, Yi; Gao, Fei; An, Ling-Zi; Zhao, Shi-Qi; Liu, Zhen-Yu; Wang, Guo-Dong [State Key Laboratory of Rolling and Automation, Northeastern University, P.O. Box 105, Shenyang 110819 (China)

2016-05-15

An equiaxed grained as-cast strip and a columnar grained as-cast strip was produced by using twin-roll strip casting, respectively. Both as-cast strips mainly containing 0.71 wt%Si and 0.44 wt%Al were cold rolled and annealed with or without the hot rolling prior to cold rolling. Microstructure, texture evolution along the whole processing routes and the magnetic properties were investigated in detail. It was found that the equiaxed grained strip was characterized by almost random texture while the columnar grained strip was dominated by strong λ-fiber (<001>‖ND) texture. After cold rolling and annealing, all the final sheets of both the as-cast strips showed extremely weak γ-fiber (<111>‖ND) recrystallization texture. In addition, the finally annealed sheets of the equiaxed grained strip were dominated by relatively weak λ-fiber and strong Goss ({110}<001>) recrystallization texture while those of the columnar grained strip were dominated by much stronger λ-fiber and much weaker Goss recrystallization texture regardless of whether the hot rolling was adopted before cold rolling, thus the former showed much lower magnetic induction than the latter. On the other hand, even though the finally annealed sheets of the equiaxed grained strip showed a little more homogeneous recrystallization microstructure with a little bigger grain size than those of the columnar grained strip in the case of no hot rolling, a much higher iron loss was displayed. By contrast, in the case of hot rolling, the former exhibited a little lower iron loss than the latter as a result of the more significant increase in grain size and λ-fiber recrystallization texture. The introduction of the hot rolling could increase the grain size, strengthen λ-fiber texture and weaken Goss texture of the finally annealed sheets of both the as-cast strips, leading to a much improvement in both the magnetic induction and iron loss. - Highlights: • Equiaxed and columnar grained as-cast strips were

Hot ductility behavior of boron microalloyed steels

International Nuclear Information System (INIS)

Lopez-Chipres, E.; Mejia, I.; Maldonado, C.; Bedolla-Jacuinde, A.; Cabrera, J.M.

2007-01-01

The current study analyses the influence of boron contents (between 29 and 105 ppm) on the hot ductility of boron microalloyed steels. For this purpose, hot tensile tests were carried out at different temperatures (700, 800, 900 and 1000 deg. C) at a constant true strain rate of 0.001 s -1 . In general, results revealed an improvement of the hot ductility of steels at increasing boron content. At 700, 900 and 1000 deg. C the ductility is higher than at 800 deg. C, where boron microalloyed steels exhibit a region of ductility loss (trough region). Likewise, dynamic recrystallization only occurred at 900 and 1000 deg. C. The fracture surfaces of the tested steels at temperatures giving the high temperature ductility regime show that the fracture mode is a result of ductile failure, whereas it is ductile-brittle failure in the trough region. Results are discussed in terms of dynamic recrystallization and boron segregation towards austenite grain boundaries, which may retard the formation of pro-eutectoid ferrite and increase grain boundary cohesion

Characterization of a hot-rolled Cu--Al--Ni--Ti shape memory alloy

International Nuclear Information System (INIS)

Segui, C.; Pons, J.; Cesari, E.

1999-01-01

The changes in the martensitic transformation of a Cu-Al-Ni-Ti alloy hot-rolled at different temperatures have been studied in detail, covering different aspects such as ageing in the parent phase at temperatures ranging between 250 and 350 o C, stabilisation of the martensite and betatization of the previously hot-rolled specimens. Besides the evolution of transformation temperatures upon different thermal treatments, special attention has been paid to the changes in mechanical properties of the alloy, such as elastic modulus and internal friction. These results are analysed in relation to the microstructural changes as observed by transmission electron microscopy. (orig.)

The Effects of Finish Rolling Temperature and Niobium Microalloying on the Microstructure and Properties of a Direct Quenched High-Strength Steel

Directory of Open Access Journals (Sweden)

Kaijalainen A.

2017-06-01

Full Text Available This paper comprehends the effects of finish rolling temperature (FRT and Nb-microalloying on the microstructural evolution and resultant properties of a low carbon direct quenched steel in the yield strength category of ≥900 MPa. Results indicate that a decrease in FRT close to Ar3 temperature significantly influenced the microstructure following phase transformation, especially at the subsurface (~50-400 μm of the rolled strip. On decreasing the FRT, the subsurface microstructure revealed a fine mixture of ferrite and bainite obviously as a result of strain-induced transformation, whereas the structure at the centreline remained essentially martensitic. Further, Nb-microalloying promoted the formation of ferrite and bainite even at higher FRTs, thus influencing the mechanical properties. The microstructures of the hot-rolled strips were further corroborated with the aid of CCT diagrams.

Splitting in Dual-Phase 590 high strength steel plates

International Nuclear Information System (INIS)

Yang Min; Chao, Yuh J.; Li Xiaodong; Tan Jinzhu

2008-01-01

Charpy V-notch impact tests on 5.5 mm thick, hot-rolled Dual-Phase 590 (DP590) steel plate were evaluated at temperatures ranging from 90 deg. C to -120 deg. C. Similar tests on 2.0 mm thick DP590 HDGI steel plate were also conducted at room temperature. Splitting or secondary cracks was observed on the fractured surfaces. The mechanisms of the splitting were then investigated. Fracture surfaces were analyzed by optical microscope (OM) and scanning electron microscope (SEM). Composition of the steel plates was determined by electron probe microanalysis (EPMA). Micro Vickers hardness of the steel plates was also surveyed. Results show that splitting occurred on the main fractured surfaces of hot-rolled steel specimens at various testing temperatures. At temperatures above the ductile-brittle-transition-temperature (DBTT), -95 deg. C, where the fracture is predominantly ductile, the length and amount of splitting decreased with increasing temperature. At temperatures lower than the DBTT, where the fracture is predominantly brittle, both the length and width of the splitting are insignificant. Splitting in HDGI steel plates only appeared in specimens of T-L direction. The analysis revealed that splitting in hot-rolled plate is caused by silicate and carbide inclusions while splitting in HDGI plate results from strip microstructure due to its high content of manganese and low content of silicon. The micro Vickers hardness of either the inclusions or the strip microstructures is higher than that of the respective base steel

Texture and magnetic properties improvement of a 3% Si non-oriented electrical steel by Sb addition

Energy Technology Data Exchange (ETDEWEB)

Rodrigues, Marcio Ferreira, E-mail: marciof.rodrigues@aperam.com [Aperam South America, Timóteo, MG (Brazil); Cunha, Marco Antonio da; Costa Paolinelli, Sebastião da [Aperam South America, Timóteo, MG (Brazil); Cota, André Barros [Physics Department—Universidade Federal de Ouro Preto, Redemat, Ouro Preto, MG (Brazil)

2013-04-15

The influence of small antimony addition and thermomechanical processing on the magnetic properties of a 3% Si steel was investigated. The samples were processed in the laboratory with 930 °C hot rolling finishing temperature, three different hot band thicknesses, hot band annealing at 1030 °C, cold rolling with three different reductions to 0.35 mm thickness and final annealing at 1030 °C. The results have shown that the best combination of core loss and magnetic induction can be obtained by Sb content of 0.045% and 76% cold rolling reduction, and that Eta/Gamma ratio is higher and grain size larger at this Sb content. -- Highlights: ► The Sb addition on the magnetic properties of a 3% Si steel was investigated. ► The 0.045% Sb and cold rolling reduction of 76% results in the best magnetic properties. ► Sb and cold rolling reduction results in a optimum final grain size and texture. ► The work was performed in a 3% Si non-oriented electrical steel.

Evolution of microstructure, macrotexture and microtexture during hot rolling of Ti-6Al-4V

International Nuclear Information System (INIS)

Ari-Gur, P.; Semiatin, S.L.

1998-01-01

The evolution of microstructure, macrotexture and microtexture during subtransus hot working of Ti-6Al-4V with two different types of transformed β starting microstructures (lamellar colony, acicular martensitic α) was investigated. Globularization of the transformed microstructures required heavy rolling reductions or moderate reductions coupled with near transus post-rolling heat treatment. Despite the sluggish dynamic globularization kinetics, noticeable macrotexture changes were noted after low reductions, an effect ascribed to the rotations associated with kinking and bending of the lamellar acicular plates. Noticeable microtextures, noted in samples with an initial lamellar colony microstructure, persisted through hot rolling suggesting that dynamic globularization does not involve recrystallization. In contrast, hot rolled material with a starting acicular α microstructure exhibited weak microtextures and strong macrotextures. The absence of microtexture in these latter cases was explained on the basis of multiple transformation variants within each colony/prior β grain following the β-annealing-and-water-quenching process used to obtain the microstructure. (orig.)

Rolling Contact Fatigue Performances of Carburized and High-C Nanostructured Bainitic Steels

OpenAIRE

Wang, Yanhui; Zhang, Fucheng; Yang, Zhinan; Lv, Bo; Zheng, Chunlei

2016-01-01

In the present work, the nanostructured bainitic microstructures were obtained at the surfaces of a carburized steel and a high-C steel. The rolling contact fatigue (RCF) performances of the two alloy steels with the same volume fraction of undissolved carbide were studied under lubrication. Results show that the RCF life of the carburized nanostructured bainitic steel is superior to that of the high-C nanostructured bainitic steel in spite of the chemical composition, phase constituent, plat...

UTILIZATION OF TORAY FLY ASH AS FILLER SUBSTITUTION IN THE HOT ROLLED SHEET-WEARING COURSE (HRS-WC MIXTURE

Directory of Open Access Journals (Sweden)

F. Candra

2012-02-01

Full Text Available In road construction materials, the utilization of fly ash as additive materials is limited and also small in quantity, while the disposal of fly ash is quite high. An abundance of fly ash can be found at PT Toray Company in Jakarta and Surabaya. Toray fly ash is disposed coal ash resulting from coal-fired electricity generating power plants. Toray fly ash in this research is used as substitute mineral filler in asphalt paving mixtures. Research on utilization of Toray fly ash as filler is conducted in the Hot Rolled Sheet – Wearing Course Mixture.  Filler content in the HRS –WC mixture is 9%. Variations of Toray fly ash in the mixture tested are 0%, 25%, 50%, 75%, 100% and the variations of asphalt content are 6%, 6.5%, 7%, 7.5%, 8%. Marshall test is  performed to determine the Optimum Asphalt Content  and Marshall Stability, Indirect Tensile Strength (ITS test and Tensile Strength Ratio (TSR to select the optimum Toray fly ash utilization in the mixture based on the moisture susceptibility of specimens. The research results show that in variations of 0%, 25%, 50%, 75% and 100% Toray fly ash in the HRS-WC Mixture, the Optimum Asphalt Contents are at 6.8%, 7.0%, 7.0%, 7.1% and 7.6%  and Marshall Stability values of the variations are 1649 kg, 1541 kg, 1568 kg, 1678 kg, 1718 kg respectively. TSR values in variations of Toray fly ash are 98.32%, 90.28%, 89.38%, 87.62%, 64.71% respectively, with Minimum TSR value required is 80%. Based on the overall parameters, the optimum Toray fly ash utilization in the HRS-WC Mixture recommended is 75% of Toray fly ash at 7.1% Optimum Asphalt Content.

Effect of rolling deformation and solution treatment on microstructure ...

Indian Academy of Sciences (India)

Department of Metallurgy and Materials Engineering, Bengal Engineering and Science ... lume percent of elongated band of δ-ferrite (∼40%) and austenite phase which ... Duplex stainless steel; hot rolling; cold deformation; microstructure; tensile properties. 1. ... ssure vessels, storage tanks, rotors, impellers and shafts,.

Microstructural and magnetic properties study of Fe–P rolled sheet alloys

International Nuclear Information System (INIS)

Jafari, S.; Beitollahi, A.; EftekhariYekta, B.; Kanada, Keiu; Ohkubo, T.; Gopalan, R.; Herzer, Giselher; Hono, K.

2014-01-01

In the work presented here, the soft magnetic properties of Fe 1−x P x (x=0.36, 0.7, 1.1 at%) rolled sheet alloys were investigated. In this respect, the as-rolled sheets were subjected to a two steps annealing processes; the first one between 800 and 1000 °C for 1 h referred as first stage annealing and the second one at lower temperatures (500 and 600 °C) for 30 min, referred as second step annealing. BH tracer measurements at 50 Hz showed that for all of the phosphorous containing alloys, in general, the magnitude of coercivity decreased by applying these two annealing steps compared to those of as-rolled samples. For all of the studied samples, the B 50 values measured at 50 Hz were in the range of 1.6–1.7 tesla (T). Samples having highest amount of phosphorous (1.1 at%) exhibited lower eddy current loss compared to the rest of the specimens due to the increased electrical resistivity. Besides, microstructural studies revealed that the prepared samples were free from Fe 3 P phase precipitation and the average grain size increased (∼three times) with increasing the phosphorous content giving rise to the decrease of hysteresis losses. Further, amongst the whole prepared samples, the alloy containing 1.1 at% P showed the lowest hysteresis loss (6.99 W/kg), eddy current loss (9.25 W/kg) as well as the highest magnetic induction (1.7 T) at 5000 A/M (B 50 ). - Highlights: • We have studied magnetic properties and microstructure of Fe 1−x P x rolled sheet alloys. • Increasing phosphorous content increases the B 50 from 1.65 to 1.70 T. • Increasing phosphorous content causes the decline of the eddy current loss. • The grain size increases about 3 times with increasing phosphorous concentration. • The hysteresis loss decreases with increasing the phosphorous content (88%)

Microstructural and magnetic properties study of Fe–P rolled sheet alloys

Energy Technology Data Exchange (ETDEWEB)

Jafari, S. [Center of Excellence for Ceramics in Energy and Environment, School of Metallurgy and Materials Engineering, Iran University of Science and Technology (IUST), Narmak, Tehran 16846-13114 (Iran, Islamic Republic of); Beitollahi, A., E-mail: beitolla@iust.ac.ir [Center of Excellence for Ceramics in Energy and Environment, School of Metallurgy and Materials Engineering, Iran University of Science and Technology (IUST), Narmak, Tehran 16846-13114 (Iran, Islamic Republic of); EftekhariYekta, B. [Center of Excellence for Ceramics in Energy and Environment, School of Metallurgy and Materials Engineering, Iran University of Science and Technology (IUST), Narmak, Tehran 16846-13114 (Iran, Islamic Republic of); Kanada, Keiu [Toyota Motor Corporation, Aichi Prefecture, Toyota (Japan); Ohkubo, T.; Gopalan, R. [Magnetic Materials Unit, National Institute for Materials Science, 1-2-1 Sengen, Tsukuba 305-0047 (Japan); Herzer, Giselher [Vacuumschmelze GmBH, D-63450 Hanau (Germany); Hono, K. [Magnetic Materials Unit, National Institute for Materials Science, 1-2-1 Sengen, Tsukuba 305-0047 (Japan)

2014-05-01

In the work presented here, the soft magnetic properties of Fe{sub 1−x}P{sub x} (x=0.36, 0.7, 1.1 at%) rolled sheet alloys were investigated. In this respect, the as-rolled sheets were subjected to a two steps annealing processes; the first one between 800 and 1000 °C for 1 h referred as first stage annealing and the second one at lower temperatures (500 and 600 °C) for 30 min, referred as second step annealing. BH tracer measurements at 50 Hz showed that for all of the phosphorous containing alloys, in general, the magnitude of coercivity decreased by applying these two annealing steps compared to those of as-rolled samples. For all of the studied samples, the B{sub 50} values measured at 50 Hz were in the range of 1.6–1.7 tesla (T). Samples having highest amount of phosphorous (1.1 at%) exhibited lower eddy current loss compared to the rest of the specimens due to the increased electrical resistivity. Besides, microstructural studies revealed that the prepared samples were free from Fe{sub 3}P phase precipitation and the average grain size increased (∼three times) with increasing the phosphorous content giving rise to the decrease of hysteresis losses. Further, amongst the whole prepared samples, the alloy containing 1.1 at% P showed the lowest hysteresis loss (6.99 W/kg), eddy current loss (9.25 W/kg) as well as the highest magnetic induction (1.7 T) at 5000 A/M (B{sub 50}). - Highlights: • We have studied magnetic properties and microstructure of Fe{sub 1−x}P{sub x} rolled sheet alloys. • Increasing phosphorous content increases the B{sub 50} from 1.65 to 1.70 T. • Increasing phosphorous content causes the decline of the eddy current loss. • The grain size increases about 3 times with increasing phosphorous concentration. • The hysteresis loss decreases with increasing the phosphorous content (88%)

A study of roll-bonding MS90 alloy to steel utilizing chromized interlayer

International Nuclear Information System (INIS)

Tolaminejad, B.; Arabi, H.

2008-01-01

This article describes a study of the application of a roll bonding technique to MS90(CuZn10) alloy strips and steel sheets using a chromized interlayer. It was found that the overall bond between these two metals resulted from two different types of bonds: a block bond, linking the MS90 alloy strips and chromium topcoat layer, and a blank bond, linking the MS90 alloy strips and bare steel surface in the area where the chromium coating has been fragmented. This study investigated the effects of plating time on the thickness of the coating layers and of the area fraction of the blank bond on the bond strength. The overall bond strength depends mainly on the strength and the area fraction of the blank bond. A linear relationship model exists between the overall bond strength and the area fraction of the blank bond. The bond strength of the blank bond was eight times greater than that of the block bond. The area fraction of the blank bond increased with increasing the coating thickness up to 55 μm, but thereafter decreased due to the rotation of the chromium blocks

Strain hardening of cold-rolled lean-alloyed metastable ferritic-austenitic stainless steels

Energy Technology Data Exchange (ETDEWEB)

Papula, Suvi [Aalto University School of Engineering, Department of Mechanical Engineering, P.O. Box 14200, FI-00076 Aalto (Finland); Anttila, Severi [Centre for Advanced Steels Research, University of Oulu, P.O. Box 4200, 90014 Oulu (Finland); Talonen, Juho [Outokumpu Oyj, P.O. Box 245, FI-00181 Helsinki (Finland); Sarikka, Teemu; Virkkunen, Iikka; Hänninen, Hannu [Aalto University School of Engineering, Department of Mechanical Engineering, P.O. Box 14200, FI-00076 Aalto (Finland)

2016-11-20

Mechanical properties and strain hardening of two pilot-scale lean-alloyed ferritic-austenitic stainless steels having metastable austenite phase, present at 0.50 and 0.30 volume fractions, have been studied by means of tensile testing and nanoindentation. These ferritic-austenitic stainless steels have high strain-hardening capacity, due to the metastable austenite phase, which leads to an improved uniform elongation and higher tensile strength in comparison with most commercial lean duplex stainless steels. According to the results, even as low as 0.30 volume fraction of austenite seems efficient for achieving nearly 40% elongation. The austenite phase is initially the harder phase, and exhibits more strain hardening than the ferrite phase. The rate of strain hardening and the evolution of the martensite phase were found to depend on the loading direction: both are higher when strained in the rolling direction as compared to the transverse direction. Based on the mechanical testing, characterization of the microstructure by optical/electron microscopy, magnetic balance measurements and EBSD texture analysis, this anisotropy in mechanical properties of the cold-rolled metastable ferritic-austenitic stainless steels can be explained by the elongated dual-phase microstructure, fiber reinforcement effect of the harder austenite phase and the presence and interplay of rolling textures in the two phases.

Investigation of hot ductility in Al-killed boron steels

International Nuclear Information System (INIS)

Chown, L.H.; Cornish, L.A.

2008-01-01

The influence of boron to nitrogen ratio, strain rate and cooling rate on hot ductility of aluminium-killed, low carbon, boron microalloyed steel was investigated. Hot tensile testing was performed on steel samples reheated in argon to 1300 deg. C, cooled at rates of 0.3, 1.2 and 3.0 deg. C s -1 to temperatures in the range 750-1050 deg. C, and then strained to failure at initial strain rates of 1 x 10 -4 or 1 x 10 -3 s -1 . It was found that the steel with a B:N ratio of 0.19 showed deep hot ductility troughs for all tested conditions; the steel with a B:N ratio of 0.47 showed a deep ductility trough for a high cooling rate of 3.0 deg. C s -1 and the steel with a near-stoichiometric B:N ratio of 0.75 showed no ductility troughs for the tested conditions. The ductility troughs extended from ∼900 deg. C (near the Ae 3 temperature) to ∼1000 or 1050 deg. C in the single-phase austenite region. The proposed mechanism of hot ductility improvement with increase in B:N ratio in these steels is that the B removes N from solution, thus reducing the strain-induced precipitation of AlN. Additionally, BN co-precipitates with sulphides, preventing precipitation of fine MnS, CuS and FeS, and forming large, complex precipitates that have no effect on hot ductility

Structure changes of Co-Ni-Al ferromagnetic shape memory alloys after vacuum annealing and hot rolling

International Nuclear Information System (INIS)

Maziarz, Wojciech

2008-01-01

The structure changes of vacuum annealed and hot rolled Co 35+x -Ni 40-x -Al 25 (x = 0, 2.5, 5.0) ferromagnetic shape memory alloys were examined by optical microscopy and X-ray diffraction measurements. Almost the same content of γ phase was observed in alloys after vacuum annealing. The change of grains morphology from dendrite in to equiaxed ones appeared after vacuum annealing. The hot rolling process was applied after annealing at 900 deg. C with thickness reduction up to about 90%. The structure of hot rolled samples revealed elongated grains of different phases. The hardness changes after heat treatment and plastic deformation processes have reflected the solution hardening and work hardening, respectively

Using CCT Diagrams to Optimize the Composition of an As-Rolled Dual-Phase Steel

Science.gov (United States)

Coldren, A. Phillip; Eldis, George T.

1980-03-01

A continuous-cooling transformation (CCT) diagram study was conducted for the purpose of optimizing the composition of a Mn-Si-Cr-Mo as-rolled dual-phase (ARDP) steel. The individual effects of chromium, molybdenum, and silicon on the allowable cooling rates were determined. On the basis of the CCT diagram study and other available information, an optimum composition was selected. Data from recent mill trials at three steel companies, involving steels with compositions in or near the newly recommended range, are presented and compared with earlier mill trial data. The comparison shows that the optimized composition is highly effective in making the steel's properties more uniform and reproducible in the as-rolled condition.

Improvement of formability of high strength steel sheets in shrink flanging

International Nuclear Information System (INIS)

Hamedon, Z; Abe, Y; Mori, K

2016-01-01

In the shrinkage flanging, the wrinkling tends to occur due to compressive stress. The wrinkling will cause a difficulty in assembling parts, and severe wrinkling may leads to rupture of parts. The shrinkage flange of the ultra-high strength steel sheets not only defects the product by the occurrence of the wrinkling but also causes seizure and wear of the dies and shortens the life of dies. In the present study, a shape of a punch having gradual contact was optimized in order to prevent the wrinkling in shrinkage flanging of ultra-high strength steel sheets. The sheet was gradually bent from the corner of the sheet to reduce the compressive stress. The wrinkling in the shrink flanging of the ultra-high strength steel sheets was prevented by the punch having gradual contact. It was found that the punch having gradual contact is effective in preventing the occurrence of wrinkling in the shrinkage flanging. (paper)

Solutions for Safe Hot Coil Evacuation and Coil Handling in Case of Thick and High Strength Steel

Directory of Open Access Journals (Sweden)

Sieberer Stefan

2016-01-01

Full Text Available Currently hot rolling plants are entering the market segment for thick gauges and high strength steel grades where the elastic bending property of the strip leads to internal forces in the coil during coiling operation. The strip tends to open. Primetals is investigating several possibilities to facilitate safe coil evacuation and coil handling under spring-back conditions. The contribution includes finite element models of such mechanical solutions. Results of parameter variation and stability limits of case studies are presented in the paper.

Presentation of the 'Atlas hot workability in steels'

International Nuclear Information System (INIS)

Merlone, G.F.; Nunez Pettinari, S.I.; Ruzzante, J.E.

1993-01-01

The Atlas summarizes the experience of almost two decades of applied research in the siderurgical industry (IAS-CNEA joint agreements), by means of hot torsion test to evaluate the hot workability in steels through ductility properties and the formation strength. It has a technical prologue, from the abundant specific bibliography, and diagrams of about 40 steels of domestic manufacturing. The information is of industrial application as well as metallurgical research. (Author)

The development of PVC-laminated steel sheet by an electron beam curing method

International Nuclear Information System (INIS)

Masuhara, Ken-ichi; Koshiishi, Kenji; Tomosue, Takao; Mori, Koji; Honma, Nobuyuki

1988-01-01

Polyvinyl chloride (PVC) film-laminated steel sheets are used for household electric appliances and building materials. Those are produced usually by pressing a PVC film onto a steel sheet imediately after a themosetting adhesive has been applied to the sheet and curing. However, a major problem of this method is that the appearance of the PVC films such as gloss and embossment changes during pressing due to the heat that is required for causing bonding, therefore, the development of an adhesive which can be cured at lower temperature is necessary. Nisshin Steel Co., Ltd. has developed PVC film-laminated steel sheets for which electron beam (EB) curable adhesives are used to overcome this problem. The advantage of these adhesives is that they can be quickly cured at room temperature. The production procedure of PVC-laminated steel sheets by EB curing is outlined. But this method has encountered two problems: poor adhesion between substrates and adhesive due to the residual stress, and the deterioration of the PVC films due to EB irradiation. EB curable adhesives are mainly composed of acrylic ester oligomers and monomers, and thier adhesion was improved by organic pretreatment. On the other hand, EB-proof PVC films were developed. The general properties of PVC-laminated steel sheets produced by EB curing are reported. (K.I.)

Mechanical properties of CO2/MIG welded structural rolled steel and stainless steel

International Nuclear Information System (INIS)

Lim, Jong Young; Yoon, Myong Jin; Kim, Sang Youn; Kim, Tae Gyu; Shin, Hyeon Seung

2015-01-01

To accomplish long-term use of specific parts of steel, welding technology is widely applied. In this study, to compare the efficiency in improving mechanical properties, rolled steel (SS400) was welded with stainless steel (STS304) by both CO 2 welding method and MIG (metal inert gas) welding method, respectively. Multi-tests were conducted on the welded specimen, such as X-ray irradiation, Vickers' Hardness, tensile test, fatigue test and fatigue crack growth test. Based on the fatigue crack growth test performed by two different methods, the relationship of da/dN was analyzed. Although the hardness by the two methods was similar, tensile test and fatigue properties of MIG welded specimen are superior to CO 2 welded one.

Predicting Hot Deformation of AA5182 Sheet

Science.gov (United States)

Lee, John T.; Carpenter, Alexander J.; Jodlowski, Jakub P.; Taleff, Eric M.

Aluminum 5000-series alloy sheet materials exhibit substantial ductilities at hot and warm temperatures, even when grain size is not particularly fine. The relatively high strain-rate sensitivity exhibited by these non-superplastic materials, when deforming under solute-drag creep, is a primary contributor to large tensile ductilities. This active deformation mechanism influences both plastic flow and microstructure evolution across conditions of interest for hot- and warm-forming. Data are presented from uniaxial tensile and biaxial bulge tests of AA5182 sheet material at elevated temperatures. These data are used to construct a material constitutive model for plastic flow, which is applied in finite-element-method (FEM) simulations of plastic deformation under multiaxial stress states. Simulation results are directly compared against experimental data to explore the usefulness of this constitutive model. The effects of temperature and stress state on plastic response and microstructure evolution are discussed.

Tribological evaluation of surface modified H13 tool steel in warm forming of Ti–6Al–4V titanium alloy sheet

OpenAIRE

Wang, Dan; Li, Heng; Yang, He; Ma, Jun; Li, Guangjun

2014-01-01

The H13 hot-working tool steel is widely used as die material in the warm forming of Ti–6Al–4V titanium alloy sheet. However, under the heating condition, severe friction and lubricating conditions between the H13 tools and Ti–6Al–4V titanium alloy sheet would cause difficulty in guaranteeing forming quality. Surface modification may be used to control the level of friction force, reduce the friction wear and extend the service life of dies. In this paper, four surface modification methods (c...

Hot-rolled Process of Multilayered Composite Metal Plate

Directory of Open Access Journals (Sweden)

YU Wei

2017-02-01

Full Text Available For multi-layer plate, it is a difficult problem to increase product yield rate and improve bonding interface quality. A high yield hot-rolled method of multilayered plate was proposed. The raw strips and plate were fixed by argon arc welding. The combined billet was put into a metal box and vacuum pumped, and then heated and rolled by multi passes at the temperature of 1000-1200℃. The 67 layered plate with the thickness of 2.5mm was successfully produced. The interfacial microstructures and diffusion behavior were investigated and analyzed by optical microscopy and scan electronic microscopy. The tensile and shear strength were tested,and the shear fractures were analyzed. The results show that the multilayered plate yield rate is more than 90% by two steps billet combination method and rolling process optimization. The good bonding interface quality is obtained, the shear strength of multilayered plate reaches 241 MPa. Nickel interlayer between 9Cr18 and 1Cr17 can not only prevent the diffusion of carbon, but also improve the microstructure characteristics.

Design of Helical Self-Piercing Rivet for Joining Aluminum Alloy and High-Strength Steel Sheets

International Nuclear Information System (INIS)

Kim, W. Y.; Kim, D. B.; Park, J. G; Kim, D. H.; Kim, K. H.; Lee, I. H.; Cho, H. Y.

2014-01-01

A self-piercing rivet (SPR) is a mechanical component for joining dissimilar material sheets such as those of aluminum alloy and steel. Unlike conventional rivets, the SPR directly pierces sheets without the need for drilling them beforehand. However, the regular SPR can undergo buckling when it pierces a high-strength steel sheet, warranting the design of a helical SPR. In this study, the joining and forging processes using the helical SPR were simulated using the commercial FEM code, DEFORM-3D. High-tensile-strength steel sheets of different strengths were joined with aluminum alloy sheets using the designed helical SPR. The simulation results were found to agree with the experimental results, validating the optimal design of a helical SPR that can pierce high-strength steel sheets

Design of Helical Self-Piercing Rivet for Joining Aluminum Alloy and High-Strength Steel Sheets

Energy Technology Data Exchange (ETDEWEB)

Kim, W. Y.; Kim, D. B.; Park, J. G; Kim, D. H.; Kim, K. H.; Lee, I. H.; Cho, H. Y. [Chungbuk National University, Cheongju (Korea, Republic of)

2014-07-15

A self-piercing rivet (SPR) is a mechanical component for joining dissimilar material sheets such as those of aluminum alloy and steel. Unlike conventional rivets, the SPR directly pierces sheets without the need for drilling them beforehand. However, the regular SPR can undergo buckling when it pierces a high-strength steel sheet, warranting the design of a helical SPR. In this study, the joining and forging processes using the helical SPR were simulated using the commercial FEM code, DEFORM-3D. High-tensile-strength steel sheets of different strengths were joined with aluminum alloy sheets using the designed helical SPR. The simulation results were found to agree with the experimental results, validating the optimal design of a helical SPR that can pierce high-strength steel sheets.

Influence of different kinds of rolling on the crystallographic texture and magnetic induction of a NOG 3 wt% Si steel

Energy Technology Data Exchange (ETDEWEB)

Silva, J.M.; Baêta Júnior, E.S.; Moraes, N.R.D.C.; Botelho, R.A. [Department of Mechanical and Materials Engineering, Military Institute of Engineering (IME), Praça General Tibúrcio, 80,Urca, Rio de Janeiro/RJ (Brazil); Felix, R.A.C. [Scientific Instrumentation and Mechanical Technology Laboratory, Brazilian Center for Physics Research (CBPF), Rua Dr. Xavier Sigaud, 150-Urca, Rio de Janeiro-RJ (Brazil); Brandao, L., E-mail: brandao@ime.eb.br [Department of Mechanical and Materials Engineering, Military Institute of Engineering (IME), Praça General Tibúrcio, 80,Urca, Rio de Janeiro/RJ (Brazil)

2017-01-01

The purpose of this work was to study the influence of different kinds of rolling on the magnetic properties of NOG steel, an electric steel widely used in electrical motors. These properties are highly correlated with the crystallographic texture of the material, which can be changed by rolling. Three kinds of rolling were examined: conventional rolling, cross-rolling and asymmetrical rolling. The crystallographic texture was determined by X-ray diffraction and the magnetic properties were calculated from a theoretical model that related the magnetic induction to crystallographic texture through the anisotropy energy. The results show that cross-rolling yields higher values of magnetic induction than the other processes. - Highlights: • The B{sub 50} of NOG steels was evaluated via texture for different rolling processes. • On comparison to all processes used, the cross-rolling led to highest average B{sub 50}. • Cross-rolling enhances Goss and γ-fiber after annealing. • The better B{sub 50} values were obtained for symmetrical and cross-rolling processes. • For asymmetric rolling process, cylinder diameter ratio changed slightly the texture.

Investigation of the Phase Formation of AlSi-Coatings for Hot Stamping of Boron Alloyed Steel

International Nuclear Information System (INIS)

Veit, R.; Kolleck, R.; Hofmann, H.; Sikora, S.

2011-01-01

Hot stamping of boron alloyed steel is gaining more and more importance for the production of high strength automotive body parts. Within hot stamping of quenchenable steels the blank is heated up to austenitization temperature, transferred to the tool, formed rapidly and quenched in the cooled tool. To avoid scale formation during the heating process of the blank, the sheet metal can be coated with an aluminium-silicum alloy. The meltimg temperature of this coating is below the austenitization temperature of the base material. This means, that a diffusion process between base material and coating has to take place during heating, leading to a higher melting temperature of the coating.In conventional heating devices, like roller hearth furnaces, the diffusion process is reached by relatively low heating rates. New technologies, like induction heating, reach very high heating rates and offer great potentials for the application in hot stamping. Till now it is not proofed, that this technology can be used with aluminum-silicon coated materials. This paper will present the results of comparative heating tests with a conventional furnace and an induction heating device. For different time/temperature-conditions the phase formation within the coating will be described.

Numerical simulation of the roll levelling of third generation fortiform 1050 steel using a nonlinear combined hardening material model

Science.gov (United States)

Galdos, L.; Saenz de Argandoña, E.; Mendiguren, J.; Silvestre, E.

2017-09-01

The roll levelling is a flattening process used to remove the residual stresses and imperfections of metal strips by means of plastic deformations. During the process, the metal sheet is subjected to cyclic tension-compression deformations leading to a flat product. The process is especially important to avoid final geometrical errors when coils are cold formed or when thick plates are cut by laser. In the last years, and due to the appearance of high strength materials such as Ultra High Strength Steels, machine design engineers are demanding reliable tools for the dimensioning of the levelling facilities. Like in other metal forming fields, finite element analysis seems to be the most widely used solution to understand the occurring phenomena and to calculate the processing loads. In this paper, the roll levelling process of the third generation Fortiform 1050 steel is numerically analysed. The process has been studied using the MSC MARC software and two different material laws. A pure isotropic hardening law has been used and set as the baseline study. In the second part, tension-compression tests have been carried out to analyse the cyclic behaviour of the steel. With the obtained data, a new material model using a combined isotropic-kinematic hardening formulation has been fitted. Finally, the influence of the material model in the numerical results has been analysed by comparing a pure isotropic model and the later combined mixed hardening model.

Model for texture evolution in cold rolling of 2.4 wt.-% Si non-oriented electrical steel

Science.gov (United States)

Wei, X.; Hojda, S.; Dierdorf, J.; Lohmar, J.; Hirt, G.

2017-10-01

Iron loss and limited magnetic flux density are constraints for NGO electrical steel used in highly efficient electrical machinery cores. The most important factors that affect these properties are the final microstructure and the texture of the NGO steel. Reviewing the whole process chain, cold rolling plays an important role because the recrystallization and grain growth during the final heat treatment can be strongly affected by the stored energy and microstructure of cold rolling, and some texture characteristics can be inherited as well. Therefore, texture evolution during cold rolling of NGO steel is worth a detailed investigation. In this paper, texture evolution in cold rolling of non-oriented (NGO) electrical steel is simulated with a crystal plasticity finite element method (CPFEM) model. In previous work, a CPFEM model has been implemented for simulating the texture evolution with periodic boundary conditions and a phenomenological constitutive law. In a first step the microstructure in the core of the workpiece was investigated and mapped to a representative volume element to predict the texture evolution. In this work an improved version of the CPFEM model is described that better reflects the texture evolution in cold rolling of NGO electrical steel containing 2.4 wt.-% Si. This is achieved by applying the deformation gradient and calibrating the flow curve within the CPFEM model. Moreover, the evolution of dislocation density is calculated and visualized in this model. An in depth comparison of the numerical and experimental results reveals, that the improved CPFEM model is able to represent the important characteristics of texture evolution in the core of the workpiece during cold rolling with high precision.

A review of hot cracking in austenitic stainless steel weldments

International Nuclear Information System (INIS)

Shankar, V.; Gill, T.P.S.; Mannan, S.L.; Rodriguez, P.

1991-01-01

The occurrence of hot cracking in austenitic stainless steel weldments is discussed with respect to its origin and metallurgical contributory factors. Of the three types of hot cracking, namely solidification cracking, liquation and ductility dip cracking, solidification cracking occurs in the interdendritic regions in weld metal while liquation and ductility dip cracking occur intergranularly in the heat-affected zone (HAZ). Segregation of impurity and minor elements such as sulphur, phosphorous, silicon, niobium, boron etc to form low melting eutectic phases has been found to be the major cause of hot cracking. Control of HAZ cracking requires minimisation of impurity elements in the base metal. In stabilized stainless steels containing niobium, higher amounts of delta-ferrite have been found necessary to prevent cracking than in unstabilized compositions. Titanium compounds have been found to cause liquation cracking in maraging steels and titanium containing stainless steels and superalloys. In nitrogen added stainless steels, cracking resistance decreases when the solidification mode changes to primary austenitic due to nitrogen addition. A review of the test methods to evaluate hot cracking behaviour showed that several external restraint and semi-self-restraint tests are available. The finger Test, WRC Fissure Bend Test, the PVR test and the Varestraint Test are described along with typical test results. Hot ductility testing to reveal HAZ cracking tendency during welding is described, which is of particular importance to stabilized stainless steels. Based on the literature, recommendations are made for welding stabilized and nitrogen added steels, indicating areas of further work. (author). 81 refs., 30 figs., 1 tab

Low carbon manganese-nickel-niobium steel

International Nuclear Information System (INIS)

Heisterkamp, F.; Hulka, K.

1983-11-01

Experimental heats of a low carbon-manganese-0.5% nickel-0.15% niobium steel have been rolled to plates between 13.5 and 50 mm thickness and to a 16 mm hot strip. Various combinations of soaking temperatures form 1100 0 C to 1300 0 C and of finish rolling temperatures between 710 0 C and 930 0 C have been investigated. From mechanical properties obtained, one can conclude that the investigated steel composition provides very good properties e.g. for pipe steels X65 to X75. In particular, the toughness at low temperature is outstanding despite relaxed rolling conditions. Metalographic and special investigations such as electron microscopy, texture evaluation and chemical extraction, correlated with applied rolling schedules and the mechanical properties obtained resulted in a comprehensive understanding about the benefits of high niobium metallurgy combined with nickel addition. All practically applied welding processes generated mechanical properties, in particular toughness of the weldment, that meet arctic specifications.(Author) [pt

Processing hot-dip galvanized AHSS grades: a challenging task

Energy Technology Data Exchange (ETDEWEB)

Pichler, A.; Hebesberger, T.; Tragl, E.; Traint, S.; Faderl, J.; Angeli, G.; Koesters, K. [voestalpine Stahl GmbH, Linz (Austria)

2005-07-01

High-strength thin sheet steel grades have gained a considerable market share. At present a very strong demand has been observed for DP (dual-phase), CP (complex phase) and TRIP grades, which are often summarized as advanced high-strength steel grades (AHSS). The potential benefits of applying AHSS grades were impressively demonstrated in the ULSAC-AVC project, in which a remarkable reduction in mass and an increase in stiffness and crash safety were achieved by using a very high share of AHSS steel grades. The present contribution concentrates on hot-dip galvanized AHSS thin sheet grades. The hot-dip galvanizeability of such grades is critically discussed after an overview is provided of the metallurgy of AHSS grades, including microstructure, mechanical properties, phase transformations and required alloy design. Based on these fundamentals, the processing of AHSS grades in the hot-dip galvanizing line is discussed and the resulting properties presented. (orig.)

Effect of zinc crystals size on galvanized steel deformation and electrochemical behavior

Directory of Open Access Journals (Sweden)

José Daniel Culcasi

2009-09-01

Full Text Available Hot-dip galvanized steel sheets with different spangle sizes were deformed by means of rolling and tension. The change of preferential crystallographic orientation and of superficial characteristics due to the deformation was analyzed by means of both X-rays diffraction and optical and scanning electronic microscopy. A correlation between such changes and the involving deformation modes was intended to be done and the spangle size influence on these modes was studied. Coating reactivity change due to the deformation was investigated by means of quasi-steady DC electrochemical tests. The results allow to infer that, in great spangle samples, the main deformation mechanism is twinning whereas in small spangle ones, pyramidal slip systems happen as well. The increase of the reactivity with the deformation is greater in tension than in rolling and it is more important in small than in great spangle samples.

75 FR 59744 - Stainless Steel Sheet and Strip From Germany, Italy, Japan, Korea, Mexico, and Taiwan

Science.gov (United States)

2010-09-28

...)] Stainless Steel Sheet and Strip From Germany, Italy, Japan, Korea, Mexico, and Taiwan AGENCY: United States... duty orders on stainless steel sheet and strip from Germany, Italy, Japan, Korea, Mexico, and Taiwan... stainless steel sheet and strip from Germany, Italy, Japan, Korea, Mexico, and Taiwan would be likely to...

Influence of deformation process on the improvement of non-oriented electrical steel

International Nuclear Information System (INIS)

Fischer, O.; Schneider, J.

2003-01-01

World-wide there is a trend to develop higher permeability grades of non-oriented electrical steels. The paper discusses the practical relevance of these developments and describes the progress in higher permeability materials utilizing optimized hot rolling and cold rolling processes

Ductile failure analysis of high strength steel in hot forming based on micromechanical damage model

Directory of Open Access Journals (Sweden)

Ying Liang

2016-01-01

Full Text Available The damage evolution of high strength steel at elevated temperature is investigated by using the Gurson-Tvergaard-Needleman (GTN model. A hybrid method integrated thermal tensile test and numerical technique is employed to identify the damage parameters. The analysis results show that the damage parameters are different at different temperature as the variation of tested material microstructure. Furthermore, the calibrated damage parameters are implemented to simulate a bugling forming at elevated temperature. The experimental results show the availability of GTN damage model in analyzing sheet formability in hot forming.

Effect of nanoprecipitates and grain size on the mechanical properties of advanced structural steels

International Nuclear Information System (INIS)

Suarez, M.A.; Alvarez-Perez, M.A.; Alvarez-Fregoso, O.; Juarez-Islas, J.A.

2011-01-01

Highlights: → The composition of the steel responded positively to the thermomechanical processing. → Yield strength was increased due to micrometric grain size of 2.2 μm. → Mechanical properties were improved due to nanometric precipitates of 5 nm. → Yield strength values of the API steel were improved up to 877.9 MPa. - Abstract: The microstructure and nanometric precipitates present in advanced structured steel have been studied by high resolution transmission electron microscopy equipped with energy dispersion X-ray microanalysis, in order to relate the nanometric precipitates and grain size with the improvement of the yield strength value of the API steel. The microstructure and nanometric precipitates of the advanced steel were obtained by a combination of thermo-mechanical controlled hot rolling and accelerated cooling procedures. The API steel composition consisted of hot rolled Nb-Ti microalloyed with: 0.07C, 1.40Mn, 0.24Si, 0.020Al, 0.009P, 0.001S, 0.05Mo, 0.5Cr, 0.05Nb, 0.25Ni, 0.10Cu, 0.012Ti, 0.05N in wt%. As a result, this hot rolled steel tested at a strain rate of 5 x 10 -3 s -1 showed an improved yield strength from 798 MPa to 878 MPa due to the micrometric grain size of 2.2 μm and to the nanometric precipitates with a size of around 5 nm in the microstructure of the steel studied.

design chart procedures for polygonal concrete-filled steel columns

African Journals Online (AJOL)

ADMIN

hexagonal and octagonal steel-concrete composite columns subjected to ... This paper also outlines procedures that will enable preparation of ... buildings and in a variety of large-span building ... Likewise, hot-rolled steel tubes are used while ... small moderate large. Fig. 2. Possible arrangement of composite polygonal ...

Hydro-mechanical deep drawing of rolled magnesium sheets

Energy Technology Data Exchange (ETDEWEB)

Bach, F.W.; Rodman, M.; Rossberg, A. [Hannover Univ., Garbsen (Germany). Inst. of Materials Science; Behrens, B.A.; Vogt, O. [Hannover Univ., Garbsen (DE). Inst. of Metal Forming and Metal Forming Machine Tools (IFUM)

2005-12-01

Magnesium sheets offer high specific properties which make them very attractive in modern light weight constructions. The main obstacles for a wider usage are their high production costs, the poor corrosion properties and the limited ductility. Until today, forming processes have to be conducted at temperatures well above T=220 C. In the first place, this is a cost factor. Moreover, technical aspects, such as grain growth or the limited use of lubrication speak against high temperatures. The first aim of the presented research work is to increase the ductility at lower temperatures by alloy modification and by an adapted rolling technology. The key factor to reach isotropic mechanical properties and increased limit drawing ratios in deep drawing tools, is to achieve fine, homogeneous microstructures. This can be done by cross rolling at moderate temperatures. The heat treatment has to be adapted accordingly. In a second stage, hydro-mechanical deep drawing experiments were carried out at elevated temperature. The results show that the forming behaviour of the tested Mg-alloys is considerably improved compared to conventional deep drawing. (orig.)

Electron backscatter diffraction study of deformation and recrystallization textures of individual phases in a cross-rolled duplex steel

Energy Technology Data Exchange (ETDEWEB)

Zaid, Md; Bhattacharjee, P.P., E-mail: pinakib@iith.ac.in

2014-10-15

The evolution of microstructure and texture during cross-rolling and annealing was investigated by electron backscatter diffraction in a ferritic–austenitic duplex stainless steel. For this purpose an alloy with nearly equal volume fraction of the two phases was deformed by multi-pass cross-rolling process up to 90% reduction in thickness. The rolling and transverse directions were mutually interchanged in each pass by rotating the sample by 90° around the normal direction. In order to avoid deformation induced phase transformation and dynamic strain aging, the rolling was carried out at an optimized temperature of 898 K (625 °C) at the warm-deformation range. The microstructure after cross warm-rolling revealed a lamellar structure with alternate arrangement of the bands of two phases. Strong brass and rotated brass components were observed in austenite in the steel after processing by cross warm-rolling. The ferrite in the cross warm-rolling processed steel showed remarkably strong RD-fiber (RD//< 011 >) component (001)< 011 >. The development of texture in the two phases after processing by cross warm-rolling could be explained by the stability of the texture components. During isothermal annealing of the 90% cross warm-rolling processed material the lamellar morphology was retained before collapse of the lamellar structure to the mutual interpenetration of the phase bands. Ferrite showed recovery resulting in annealing texture similar to the deformation texture. In contrast, the austenite showed primary recrystallization without preferential orientation selection leading to the retention of deformation texture. The evolution of deformation and annealing texture in the two phases of the steel was independent of one another. - Highlights: • Effect of cross warm-rolling on texture formation is studied in duplex steel. • Brass texture in austenite and (001)<110 > in ferrite are developed. • Ferrite shows recovery during annealing retaining the (001

Soil Contamination with Heavy Metals around Jinja Steel Rolling Mills in Jinja Municipality, Uganda

Directory of Open Access Journals (Sweden)

Noel Namuhani

2015-01-01

Conclusions. The concentration levels of heavy metals around the steel rolling mills did not appear to be of serious concern, except for copper and cadmium, which showed moderate pollution and moderate to strong pollution, respectively. All heavy metals were within the limits of the United States Environmental Protection Agency (USEPA residential soil standards and the Dutch intervention soil standards. Overall, soils around the Jinja steel rolling mills were slightly polluted with heavy metals, and measures therefore need to be taken to prevent further soil contamination with heavy metals.

Effect of niobium and titanium addition on the hot ductility of boron containing steel

International Nuclear Information System (INIS)

Cho, Kyung Chul; Mun, Dong Jun; Koo, Yang Mo; Lee, Jae Sang

2011-01-01

Research highlights: → Addition of only Nb without Ti has little influence in the hot ductility of B steel. → Hot ductility loss of B-Nb steel is due to grain boundary precipitation of BN. → Adding a small amount of Ti improve the hot ductility of B-Nb steel. → In B-Nb-Ti steel, hot ductility improvement is related to presence of TiN particle. → Presence of TiN particles makes the BN precipitates' distribution more homogeneous. - Abstract: Hot ductility of boron containing steel (B steel) with adding Nb (0.03 wt.%) (B-Nb steel) and B-Nb steel with adding Ti (0.0079 wt.%) (B-Nb-Ti steel) was quantified using hot tensile tests. The specimens were solution-treated at 1350 deg. C and cooled at 20 deg. C s -1 to tensile test temperature (T) in the range of 750 ≤ T ≤ 1050 deg. C. After that, they were strained to failure at a strain rate of 2.5 x 10 -3 s -1 . For the B-Nb steel, severe hot ductility loss was observed at 850 ≤ T ≤ 950 deg. C, which covered the low temperature in which austenite (γ) single-phase exists, and the high temperature at which γ and ferrite (α) coexist. Ductility loss in the B-Nb steel was caused by the presence of a network of BN precipitates, rather than by Nb(C, N) precipitates at the γ grain boundaries. In contrast, hot ductility of the B-Nb-Ti steel was remarkably improved at 850 ≤ T ≤ 950 deg. C. In the B-Nb-Ti steel, BN precipitates preferentially on TiN particles, resulting in increased BN precipitation in the γ grain interior and a decrease in the network of BN precipitates at the γ grain boundaries. These changes reduce strain localization at the γ grain boundaries and therefore increase the hot ductility of the steel.

Effect of cold-rolling on pitting corrosion of 304 austenitic stainless steel

International Nuclear Information System (INIS)

Peguet, L.; Malki, B.; Baroux, B.

2004-01-01

Full text of publication follows: This paper deals with a not very often investigated topic on relation between cold-working and stainless steels localized corrosion resistance. It is devoted to the study of the cold-rolling effects on the pitting corrosion behavior of a 304 stainless steel grade in chloride containing aqueous electrolytes. It focus particularly on the analysis of metastable pitting transients observed at Open Circuit Potential using an experimental protocol including two identical working electrodes connected through a zero-impedance. As received the used specimens were heat-treated at 1100 C for 30 s and cold-rolled at 10%, 20%, 30% up to a final reduction pass of 70% inducing a large amount of α'-martensite. Then, current-potential fluctuations measurements were performed at OCP in NaCl 0.1 M + FeCl 3 2.10 -4 M containing aqueous solution during 24 h from the immersion time. As expected, a detrimental effect on corrosion behavior induced by cold rolling has been confirmed. Surprisingly, this is a nonlinear effect as a function of cold-rolling rate which controverts the hypothesis that strain induced martensite is the principal factor to explain this kind of sensibilizing. In particular, the results show a maximum of the metastable pits initiation frequency at 20% of cold-rolling rate. Moreover, the passive film/electrochemical double layer resistance and capacity deduced from the transients study show an analog nonlinear behavior. So, the transfer resistance show a minimum around 10-20% of cold-rolling rate where one can assume an increase of the electrons transfer kinetics through the interface. Conversely, the interfacial capacity is the highest at 20% of cold-rolling rate. Finally, It is expected a combined effect of the cold-rolled induced martensite and the dislocations arrangement via the mechano-chemical theory discussed by Gutman. (authors)

Phase analysis of fume during arc weld brazing of steel sheets with protective coatings

Directory of Open Access Journals (Sweden)

J. Matusiak

2016-04-01

Full Text Available The article presents the results of research of the phase identification and of the quantitative phase analysis of fume generated during Cold Metal Transfer (CMT, ColdArc and Metal Inert Gas / Metal Active Gas (MIG / MAG weld brazing. Investigations were conducted for hot - dip coated steel sheets with zinc (Zn and zinc-iron (Zn - Fe alloy coatings. Arc shielding gases applied during the research-related tests were Ar + O2, Ar + CO2, Ar + H2 and Ar + CO2 + H2 gas mixtures. The analysis of the results covers the influence of the chemical composition of shielding gas on the chemical composition of welding fume.

Roll-to-roll hot embossing system with shape preserving mechanism for the large-area fabrication of microstructures

Science.gov (United States)

Peng, Linfa; Wu, Hao; Shu, Yunyi; Yi, Peiyun; Deng, Yujun; Lai, Xinmin

2016-10-01

Roll-to-roll (R2R) hot embossing is a promising approach to fulfilling the demands of high throughput fabrication of large-area polymeric components with micro-structure arrays which have been widely employed in the domains of optics, optoelectronics, biology, chemistry, etc. Nevertheless, the characteristic of continuous and fast forming for the R2R hot embossing process limits material flow during filling stage and results in significant springback during demolding stage. As a result, forming defects usually appear and the process window is very narrow which hinders the industrialization of this technology. This study developed a R2R hot embossing machine and proposed a shape preserving mechanism to extend the material filling time and realized the cooling effect during the demolding process. Comparative experiments were conducted on the R2R hot embossing process for micro-pyramid arrays to understand the effect of shape preserving mechanism. The influence of tension force and encapsulation angle to the forming quality was systematically analyzed. Furthermore, the influence of processing parameters has been investigated by using the one-variable-at-a-time method. Afterwards, a series of experiments based on the central composite design approach have been conducted for the analysis of variance and the establishment of empirical models of the R2R hot embossing process. As a result, the process window was extended by the shape preserving mechanism. More importantly, the feeding speed was improved from 0.5 m min-1 to 2.5 m min-1 for the large-area fabrication of micro-pyramid arrays, which is very attractive to the industrialization of this technology.

Patterned immobilization of antibodies within roll-to-roll hot embossed polymeric microfluidic channels.

Directory of Open Access Journals (Sweden)

Belachew Feyssa

Full Text Available This paper describes a method for the patterned immobilization of capture antibodies into a microfluidic platform fabricated by roll-to-roll (R2R hot embossing on poly (methyl methacrylate (PMMA. Covalent attachment of antibodies was achieved by two sequential inkjet printing steps. First, a polyethyleneimine (PEI layer was deposited onto oxygen plasma activated PMMA foil and further cross-linked with glutaraldehyde (GA to provide an amine-reactive aldehyde surface (PEI-GA. This step was followed by a second deposition of antibody by overprinting on the PEI-GA patterned PMMA foil. The PEI polymer ink was first formulated to ensure stable drop formation in inkjet printing and the printed films were characterized using atomic force microscopy (AFM and X-ray photoelectron spectroscopy (XPS. Anti-CRP antibody was patterned on PMMA foil by the developed method and bonded permanently with R2R hot embossed PMMA microchannels by solvent bonding lamination. The functionality of the immobilized antibody inside the microfluidic channel was evaluated by fluorescence-based sandwich immunoassay for detection of C-reactive protein (CRP. The antibody-antigen assay exhibited a good level of linearity over the range of 10 ng/ml to 500 ng/ml (R(2 = 0.991 with a calculated detection limit of 5.2 ng/ml. The developed patterning method is straightforward, rapid and provides a versatile approach for creating multiple protein patterns in a single microfluidic channel for multiplexed immunoassays.

Phase evolution and mechanical behavior of 0.36 wt% C high strength TRIP-assisted steel

Energy Technology Data Exchange (ETDEWEB)

Ghosh, Swarup Kumar; Chattopadhyay, Partha Protim [Department of Metallurgy and Materials Engineering, Bengal Engineering and Science University, Shibpur, Howrah 711 103 (India)

2012-12-15

Phase evolution in a 0.36 wt% C steel has been studied by thermodynamic calculation and dilatometric analysis with an aim to achieve high strength TRIP-assisted steel with bainitic microstructure. The equilibrium phase fraction calculated as the function of temperature indicated the formation of {delta}-ferrite ({approx}98%) at 1417 C. In contrast, similar calculation under para-equilibrium condition exhibited transformation of {delta}-ferrite to austenite at the temperature below 1300 C. During further cooling two-phase ({alpha}+{gamma}) microstructure has been found to be stable at the intercritical temperature range. The experimentally determined CCT diagram has revealed that adequate hardenability is achievable in the steel under continuous cooling condition at cooling rate >5 C s{sup -1}. In view of the aforesaid results, the steel has been hot rolled and subjected to different process schedule conducive to the evolution of bainitic microstructure. The hot rolled steel has exhibited reasonably good tensile properties. However, cold deformation of the hot rolled sample followed by intercritical annealing and subsequent isothermal bainitic transformation has resulted in high strength (>1000 MPa) with attractive elongation due to the favorable work hardening condition during plastic deformation offered by the multiphase microstructure. (Copyright copyright 2012 WILEY-VCH Verlag GmbH and Co. KGaA, Weinheim)

Influence of different kinds of rolling on the crystallographic texture and magnetic induction of a NOG 3 wt% Si steel

Science.gov (United States)

Silva, J. M.; Baêta Júnior, E. S.; Moraes, N. R. D. C.; Botelho, R. A.; Felix, R. A. C.; Brandao, L.

2017-01-01

The purpose of this work was to study the influence of different kinds of rolling on the magnetic properties of NOG steel, an electric steel widely used in electrical motors. These properties are highly correlated with the crystallographic texture of the material, which can be changed by rolling. Three kinds of rolling were examined: conventional rolling, cross-rolling and asymmetrical rolling. The crystallographic texture was determined by X-ray diffraction and the magnetic properties were calculated from a theoretical model that related the magnetic induction to crystallographic texture through the anisotropy energy. The results show that cross-rolling yields higher values of magnetic induction than the other processes.

Thickness profile measuring device for rolling metal bands or sheets

International Nuclear Information System (INIS)

Campas, J.J.; Terreaux, S.

1995-01-01

Previous radiometric thickness gages were affected by insufficient water proofing and limited cooling performances for the detection subsystem (in general specially designed photodiodes). This resulted in poor reliability and life expectancy, in particular when heavy humidity and constant radiative heat are present as for hot rolling in the metal industry. This new gage design brings enhanced performances for these two factors. (D.L.). 4 refs., 3 figs

Strategic surface topographies for enhanced lubrication in sheet forming of stainless steel

DEFF Research Database (Denmark)

Nilsson, Morten Sixten; Olsson, David Dam; Petrushina, Irina

2010-01-01

Strategic stainless steel surfaces have been developed for which the tribological properties are significantly improved for sheet-metal forming compared with the as-received surfaces. The improvements have been achieved by modification of the surface to promote Micro-Plasto Hydrodynamic Lubrication....... The technique, which has been developed, is based on an electrochemical treatment changing the topography of the stainless steel surface. Comparative testing of the new surface topographies in ironing and deep drawing of stainless steel sheet shows significant improvements and possibilities of replacing...

Deformability of Oxide Inclusions in Tire Cord Steels

Science.gov (United States)

Zhang, Lifeng; Guo, Changbo; Yang, Wen; Ren, Ying; Ling, Haitao

2018-04-01

The deformation of oxide inclusions in tire cord steels during hot rolling was analyzed, and the factors influencing their deformability at high and low temperatures were evaluated and discussed. The aspect ratio of oxide inclusions decreased with the increasing reduction ratio of the steel during hot rolling owing to the fracture of the inclusions. The aspect ratio obtained after the first hot-rolling process was used to characterize the high-temperature deformability of the inclusions. The deformation first increased and then decreased with the increasing (MgO + Al2O3)/(SiO2 + MnO) ratio of the inclusions. It also increased with the decreasing melting temperatures of the inclusions. Young's modulus was used to evaluate the low-temperature deformability of the inclusions. An empirical formula was fitted to calculate the Young's moduli of the oxides using the mean atomic volume. The moduli values of the inclusions causing wire fracture were significantly greater than the average. To reduce fracture in tire cord steel wires during cold drawing, it is proposed that inclusions be controlled to those with high SiO2 content and extremely low Al2O3 content. This proposal is based on the hypothesis that the deformabilities of oxides during cold drawing are inversely proportional to their Young's moduli. The future study thus proposed includes an experimental confirmation for the abovementioned predictions.

Deformation in Micro Roll Forming of Bipolar Plate

Science.gov (United States)

Zhang, P.; Pereira, M.; Rolfe, B.; Daniel, W.; Weiss, M.

2017-09-01

Micro roll forming is a new processing technology to produce bipolar plates for Proton Exchange Membrane Fuel Cells (PEMFC) from thin stainless steel foil. To gain a better understanding of the deformation of the material in this process, numerical studies are necessary before experimental implementation. In general, solid elements with several layers through the material thickness are required to analyse material thinning in processes where the deformation mode is that of bending combined with tension, but this results in high computational costs. This pure solid element approach is especially time-consuming when analysing roll forming processes which generally involves feeding a long strip through a number of successive roll stands. In an attempt to develop a more efficient modelling approach without sacrificing accuracy, two solutions are numerically analysed with ABAQUS/Explicit in this paper. In the first, a small patch of solid elements over the strip width and in the centre of the “pre-cut” sheet is coupled with shell elements while in the second approach pure shell elements are used to discretize the full sheet. In the first approach, the shell element enables accounting for the effect of material being held in the roll stands on material flow while solid elements can be applied to analyse material thinning in a small discrete area of the sheet. Experimental micro roll forming trials are performed to prove that the coupling of solid and shell elements can give acceptable model accuracy while using shell elements alone is shown to result in major deviations between numerical and experimental results.

Direct Laser Writing of Single-Material Sheets with Programmable Self-Rolling Capability

Science.gov (United States)

Bauhofer, Anton; KröDel, Sebastian; Bilal, Osama; Daraio, Chiara; Constantinescu, Andrei

Direct laser writing, a sub-class of two-photon polymerization, facilitates 3D-printing of single-material microstructures with inherent residual stresses. Here we show that controlled distribution of these stresses allows for fast and cost-effective fabrication of structures with programmable self-rolling capability. We investigate 2D sheets that evolve into versatile 3D structures. Precise control over the shape morphing potential is acquired through variations in geometry and writing parameters. Effects of capillary action and gravity were shown to be relevant for very thin sheets (thickness 1.5um) are dominated by residual stresses and adhesion forces. The presented structures create local tensions up to 180MPa, causing rolling curvatures of 25E3m-1. A comprehensive analytical model that captures the relevant influence factors was developed based on laminate plate theory. The predicted curvature and directionality correspond well with the experimentally obtained data. Potential applications are found in drug encapsulation and particle traps for emulsions with differing surface energies. This work was supported by the Swiss National Science Foundation.

Microstructural analysis of hot press formed 22MnB5 steel

Science.gov (United States)

Aziz, Nuraini; Aqida, Syarifah Nur; Ismail, Izwan

2017-10-01

This paper presents a microstructural study on hot press formed 22MnB5 steel for enhanced mechanical properties. Hot press forming process consists of simultaneous forming and quenching of heated blank. The 22MnB5 steel was processed at three different parameter settings: quenching time, water temperature and water flow rate. 22MnB5 was processed using 33 full factorial design of experiment (DOE). The full factorial DOE was designed using three factors of quenching time, water temperature and water flow rate at three levels. The factors level were quenching time range of 5 - 11 s, water temperature; 5 - 27°C and water flow rate; 20 - 40 L/min. The as-received and hot press forming processed steel was characterised for metallographic study and martensitic structure area percentage using JEOL Field Emission Scanning Electron Microscopic (FESEM). From the experimental finding, the hot press formed 22MnB5 steel consisted of 50 to 84% martensitic structure area. The minimum quenching time of 8 seconds was required to obtain formed sample with high percentage of martensite. These findings contribute to initial design of processing parameters in hot press forming of 22MnB5 steel blanks for automotive component.

Simulation-based prediction of hot-rolled coil forced cooling

Energy Technology Data Exchange (ETDEWEB)

Saboonchi, Ahmad [Department of Mechanical Engineering, Isfahan University of Technology, Isfahan 84154 (Iran); Hassanpour, Saeid [Rayan Tahlil Sepahan Co., Isfahan Science and Technology Town, Isfahan 84155 (Iran)

2008-09-15

Hot-rolled coils take a long time to cool under normal storehouse conditions due to their high mass. Hotter seasons will lead to even longer storage times and, thus, to shortage of space. Forced cooling methods such as water-immersion and water-spray can be employed to reduce hot-rolled coil cooling time. In this paper, a mathematical model of the thermal behavior of coils is developed to predict and to evaluate the results expected from employing these methods before any real changes can be made on the ground. The results obtained from the model were compared with those from various experiments to verify the model's accuracy. The cooling time was then computed based on changes effected in the boundary conditions appropriate to each of the forced cooling methods employed. Moreover, the savings in storage times were compared to identify the best cooling method. Predictions showed that water immersion at the beginning of cooling cycle was more effective and that the cycle should not exceed 1 h for cost efficiency considerations. When using nozzles to spray it was found that spraying water on end surfaces of coils would be the optimum option resulting in savings in time, water and energy, and with restricted temperature gradient. (author)

Mechanical Behaviour of 304 Austenitic Stainless Steel Processed by Room Temperature Rolling

Science.gov (United States)

Singh, Rahul; Goel, Sunkulp; Verma, Raviraj; Jayaganthan, R.; Kumar, Abhishek

2018-03-01

To study the effect of room temperature rolling on mechanical properties of 304 Austenitic Stainless Steel, the as received 304 ASS was rolled at room temperature for different percentage of plastic deformation (i.e. 30, 50, 70 and 90 %). Microstructural study, tensile and hardness tests were performed in accordance with ASTM standards to study the effect of rolling. The ultimate tensile strength (UTS) and hardness of a rolled specimen have enhanced with rolling. The UTS has increased from 693 MPa (as received) to 1700 MPa (after 90% deformation). The improvement in UTS of processed samples is due to combined effect of grain refinement and stress induced martensitic phase transformation. The hardness values also increases from 206 VHN (as received) to 499 VHN (after 90% deformation). Magnetic measurements were also conducted to confirm the formation of martensitic phase.

Testing new tribo-systems for sheet metal forming of advanced high strength steels and stainless steels

DEFF Research Database (Denmark)

Bay, Niels; Ceron, Ermanno

2014-01-01

of a methodology for off-line testing of new tribo-systems for advanced high strength steels and stainless steels. The methodology is presented and applied to an industrial case, where different tribo-systems are tested. A universal sheet tribotester has been developed, which can run automatically repetitive......Testing of new tribo-systems in sheet metal forming has become an important issue due to new legislation, which forces industry to replace current, hazardous lubricants. The present paper summarizes the work done in a recent PhD project at the Technical University of Denmark on the development...

Hot flow behavior of boron microalloyed steels

International Nuclear Information System (INIS)

Lopez-Chipres, E.; Mejia, I.; Maldonado, C.; Bedolla-Jacuinde, A.; El-Wahabi, M.; Cabrera, J.M.

2008-01-01

This research work studies the effect of boron contents on the hot flow behavior of boron microalloyed steels. For this purpose, uniaxial hot-compression tests were carried out in a low carbon steel microalloyed with four different amounts of boron over a wide range of temperatures (950, 1000, 1050 and 1100 deg. C) and constant true strain rates (10 -3 , 10 -2 and 10 -1 s -1 ). Experimental results revealed that both peak stress and peak strain tend to decrease as boron content increases, which indicates that boron additions have a solid solution softening effect. Likewise, the flow curves show a delaying effect on the kinetics of dynamic recrystallization (DRX) when increasing boron content. Deformed microstructures show a finer austenitic grain size in the steel with higher boron content (grain refinement effect). Results are discussed in terms of boron segregation towards austenitic grain boundaries during plastic deformation, which increases the movement of dislocations, enhances the grain boundary cohesion and modificates the grain boundary structure

Review on Cold-Formed Steel Connections

Science.gov (United States)

Tan, Cher Siang; Mohammad, Shahrin; Md Tahir, Mahmood; Shek, Poi Ngian

2014-01-01

The concept of cold-formed light steel framing construction has been widespread after understanding its structural characteristics with massive research works over the years. Connection serves as one of the important elements for light steel framing in order to achieve its structural stability. Compared to hot-rolled steel sections, cold-formed steel connections perform dissimilarity due to the thin-walled behaviour. This paper aims to review current researches on cold-formed steel connections, particularly for screw connections, storage rack connections, welded connections, and bolted connections. The performance of these connections in the design of cold-formed steel structures is discussed. PMID:24688448

The crack growth resistance of thin steel sheets under eccentric ...

Indian Academy of Sciences (India)

Ľ AMBRIŠKO

2018-03-10

Mar 10, 2018 ... of zinc-coated automotive steel sheets (IF – deep drawing interstitial free steel ..... to determine; therefore, the Ji was determined for observ- able crack initiation .... M R S, da Silva L F M and de Castro P M S T 2011. Analysis of ...

Effects of Ultra-Fast Cooling After Hot Rolling and Intercritical Treatment on Microstructure and Cryogenic Toughness of 3.5%Ni Steel

Science.gov (United States)

Wang, Meng; Liu, Zhenyu

2017-07-01

A novel process comprised of ultra-fast cooling after control rolling, intercritical quenching and tempering (UFC-LT) was applied to 3.5%Ni steel. In addition, quenching and tempering (QT) treatment was conducted in comparison. The present study focuses on the relationship between the microstructure and cryogenic toughness of 3.5%Ni steel. Results show that the microstructure of steel treated by UFC-LT consisted of tempered martensite, intercritical ferrite and two types of reversed austenite (RA) (needle shape and blocky). Compared to the QT sample, the UFC-LT sample's ultimate tensile strength decreased slightly, while its elongation increased from 32.3 to 35.7%, and its Charpy absorption energy at -135 °C increased from 112 to 237 J. The ductile-brittle transition temperature of UFC-LT sample was lower than that of the QT sample by 18 °C. The superior cryogenic toughness after UFC-LT compared to QT treatment can be attributed to the dissolution of cementite, approximately 3.0% increase in RA and the decrease in effective grain size.

Effects of hot rolling and titanium content on the microstructure and mechanical properties of high boron Fe–B alloys

International Nuclear Information System (INIS)

He, Lin; Liu, Ying; Li, Jun; Li, Binghong

2012-01-01

Highlights: ► The content of B is 1.8 wt.% in the high boron Fe–B alloys. ► Hot-rolling improves the mechanical properties, especially the elongation. ► The Ti content affects the microstructure and mechanical properties. ► Eutectic boride can be eliminated when the atomic ratio of Ti/B is no less than 0.5. ► Alloy exhibits balanced mechanical properties when the atomic ratio of Ti/B is 0.5. -- Abstract: High boron Fe–B alloys (1.8 wt.% B) with different titanium contents are fabricated by Vacuum Induction Melting (VIM) technique. The integrated mechanical properties of the as-cast alloys are poor, especially the ductility. In this investigation, hot-rolling technology is used to improve the microstructure and mechanical properties. The microstructure analysis shows that hot rolling can reduce the size and improve the distribution of the reinforcements. The mechanical properties testing indicates that the yield strength is unchanged basically, but the tensile strength and elongation are improved greatly by hot rolling, especially the elongation. The content of titanium also has great effects on the microstructures and mechanical properties of the hot-rolled alloys. For the hot-rolled alloys, with the titanium content increasing, the ultimate tensile strength and yield strength first decrease slightly and then increase. The elongation and impact toughness are improved significantly. In particular, when the atomic ratio of Ti to B is 0.5, the reinforcements are almost entirely TiB 2 and uniformly distributed in the Fe-matrix. The ternary Fe–B–Ti alloy exhibits balanced mechanical properties: yield strength, ultimate tensile strength, elongation and impact toughness are 334 MPa, 602 MPa, 16.2% and 213 kJ/m 2 , respectively.

Evaluation of interlocking bond strength between structured 1.0338 steel sheets and high pressure die cast AlMg5Si2

Science.gov (United States)

Senge, S.; Brachmann, J.; Hirt, G.; Bührig-Polaczek, A.

2018-05-01

Multi-material components open up new possibilities for functional design. Such components combine beneficial physical properties of different materials in a single component as for instance chemical resistance, high strength or low density. The challenge is a reliable bond between both materials to enable a long term usage. This paper deals with a form closure connection to ensure a solid connection between steel strips and high pressure die cast aluminium. Two different sizes of channel structures with width ratios of 1.0 and 1.35 are produced on a steel sheet. An ensuing flat rolling pass is performed to create undercuts with a width of up to 50 µm, enabling an interlocking of the molten aluminium in the concluding casting process. For both rolling processes the resulting geometry is analysed depending on the thickness reduction. In a subsequent high pressure die casting process, aluminium is applied resulting in a complete form filling for the coarser structure. Comparing structures with and without undercuts, only structures suited with undercuts remain gap-free after solidification contraction. The finer structure could not be filled completely; nevertheless these structures result in shear strength of up to 45 MPa transversal to the channel-direction.

Effect of thermo-mechanical treatments on the microstructure and mechanical properties of an ODS ferritic steel

International Nuclear Information System (INIS)

Oksiuta, Z.; Mueller, P.; Spaetig, P.; Baluc, N.

2011-01-01

The Fe-14Cr-2W-0.3Ti-0.3Y 2 O 3 oxide dispersion strengthened (ODS) reduced activation ferritic (RAF) steel was fabricated by mechanical alloying of a pre-alloyed, gas atomised powder with yttria nano-particles, followed by hot isostatic pressing and thermo-mechanical treatments (TMTs). Two kinds of TMT were applied: (i) hot pressing, or (ii) hot rolling, both followed by annealing in vacuum at 850 deg. C. The use of a thermo-mechanical treatment was found to yield strong improvement in the microstructure and mechanical properties of the ODS RAF steel. In particular, hot pressing leads to microstructure refinement, equiaxed grains without texture, and an improvement in Charpy impact properties, especially in terms of the upper shelf energy (about 4.5 J). Hot rolling leads to elongated grains in the rolling direction, with a grain size ratio of 6:1, higher tensile strength and reasonable ductility up to 750 deg. C, and better Charpy impact properties, especially in terms of the ductile-to-brittle transition temperature (about 55 deg. C).

Effect of thermo-mechanical treatments on the microstructure and mechanical properties of an ODS ferritic steel

Energy Technology Data Exchange (ETDEWEB)

Oksiuta, Z., E-mail: oksiuta@pb.edu.pl [Bialystok Technical University, Mechanical Department, Wiejska 45c, 15-351 Bialystok (Poland); Mueller, P.; Spaetig, P.; Baluc, N. [Ecole Polytechnique Federale de Lausanne (EPFL), Centre de Recherches en Physique des Plasmas, Association Euratom-Confederation Suisse, 5232 Villigen PSI (Switzerland)

2011-05-15

The Fe-14Cr-2W-0.3Ti-0.3Y{sub 2}O{sub 3} oxide dispersion strengthened (ODS) reduced activation ferritic (RAF) steel was fabricated by mechanical alloying of a pre-alloyed, gas atomised powder with yttria nano-particles, followed by hot isostatic pressing and thermo-mechanical treatments (TMTs). Two kinds of TMT were applied: (i) hot pressing, or (ii) hot rolling, both followed by annealing in vacuum at 850 deg. C. The use of a thermo-mechanical treatment was found to yield strong improvement in the microstructure and mechanical properties of the ODS RAF steel. In particular, hot pressing leads to microstructure refinement, equiaxed grains without texture, and an improvement in Charpy impact properties, especially in terms of the upper shelf energy (about 4.5 J). Hot rolling leads to elongated grains in the rolling direction, with a grain size ratio of 6:1, higher tensile strength and reasonable ductility up to 750 deg. C, and better Charpy impact properties, especially in terms of the ductile-to-brittle transition temperature (about 55 deg. C).

Preliminary Feasibility Study on the Construction of Steel Hot Cell Facility for Precise Manipulated Examinations

International Nuclear Information System (INIS)

Ahn, Sangbok; Kwon, Hyungmun; Kim, Heemoon; Kim, Dosik; Min, Duckkee; Hong, Kwonpyo

2006-01-01

Hot laboratory is essential facility to research and develop in the nuclear industries to examine radioactive materials. The post irradiation examinations for irradiated fuels and materials should be mainly conducted in the hot cell facility to protect radiations to operators. Hot cells are divided into a concrete hot cell and a steel hot cell according to the wall materials. Usually a concrete hot cell is applied to test for high level radioactive materials like as a fuel assembly, rods, and large structure specimens, and a steel hot cell for comparatively lower level activity materials in fuel fragments, and small structural materials. A steel hot cell has many benefits in a specimen manipulation, construction and maintenance costs. In recent the test for the irradiated materials is more frequently required a small and precise manipulating examination for higher degree tests of research and developments. Unfortunately hot laboratory facilities in domestics have mainly constituted of concrete hot cells, and not ready for techniques in steel hot cells. In this paper the construction feasibility of steel hot cell facility is preliminary reviewed in the points of the status of domestic facilities, the test demand prospect and detailed plans

The evolution with strain of the stored energy in different texture components of cold-rolled IF steel revealed by high resolution X-ray diffraction

Energy Technology Data Exchange (ETDEWEB)

Wauthier-Monnin, A. [LSPM–CNRS, Université Paris 13, 99, Av. J.B. Clément, 93430 Villetaneuse (France); ArcelorMittal Research Voie Romaine BP 30320, 57 283 Maizières-les Metz (France); Chauveau, T.; Castelnau, O. [LSPM–CNRS, Université Paris 13, 99, Av. J.B. Clément, 93430 Villetaneuse (France); Réglé, H. [ArcelorMittal Research Voie Romaine BP 30320, 57 283 Maizières-les Metz (France); Bacroix, B., E-mail: brigitte.bacroix@univ-paris13.fr [LSPM–CNRS, Université Paris 13, 99, Av. J.B. Clément, 93430 Villetaneuse (France)

2015-06-15

During the deformation of low carbon steel by cold-rolling, dislocations are created and stored in grains depending on local crystallographic orientation, deformation, and deformation gradient. Orientation dependent dislocation densities have been estimated from the broadening of X-ray diffraction lines measured on a synchrotron beamline. Different cold-rolling levels (from 30% to 95% thickness reduction) have been considered. It is shown that the present measurements are consistent with the hypothesis of the sole consideration of screw dislocations for the analysis of the data. The presented evolutions show that the dislocation density first increases within the α fiber (=(hkl)<110>) and then within the γ fiber (=(111)). A comparison with EBSD measurements is done and confirms that the storage of dislocations during the deformation process is orientation dependent and that this dependence is correlated to the cold-rolling level. If we assume that this dislocation density acts as a driving force during recrystallization, these observations can explain the fact that the recrystallization mechanisms are generally different after moderate or large strains. - Highlights: • Dislocation densities are assessed by XRD in main texture components of a steel sheet. • Dislocation densities vary with both strain and texture components. • The analysis relies on the sole presence of screw dislocations. • The measured dislocation densities include the contribution of both SSD and GND.

The hot working characteristics of a boron bearing and a conventional low carbon steel

International Nuclear Information System (INIS)

Stumpf, Waldo; Banks, Kevin

2006-01-01

Constitutive hot working constants were determined for an 11 ppm boron low carbon strip steel and compared from 875 to 1140 deg. C and strain rates of 0.001-2.5 s -1 to a high nitrogen low carbon strip steel. The boron steel showed a different hot working behaviour than the conventional steel with the steady state flow stress about 50-60% higher, the peak strain more than 50% higher and the eventual ferrite grain size about 40% smaller, if compared at the same temperature compensated strain rates or Z values. This difference persisted where the soaking temperature before compression was varied between 1140 and 1250 deg. C, proving that undissolved AlN in the boron-bearing steel was not responsible. With systematically varied linear cooling rates after hot working, the final ferrite grain size in the boron steel is finer and is independent of the two Z values applied during hot working. Retarded softening by dynamic recrystallisation during hot working in the boron containing steel is probably caused by boron solute drag of moving grain boundaries

The Corrosion Behavior of Cold-Rolled 304 Stainless Steel In Salt Spray Environments