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Sample records for hot rolled stainless

  1. Microstructure and properties of hot roll bonding layer of dissimilar metals. 2. Bonding interface microstructure of Zr/stainless steel by hot roll bonding and its controlling

    International Nuclear Information System (INIS)

    Yasuyama, Masanori; Ogawa, Kazuhiro; Taka, Takao; Nakasuji, Kazuyuki; Nakao, Yoshikuni; Nishimoto, Kazutoshi.

    1996-01-01

    The hot roll bonding of zirconium and stainless steel inserted with tantalium was investigated using the newly developed rolling mill. The effect of hot rolling temperatures of zirconium/stainless steel joints on bonding interface structure was evaluated. Intermetallic compound layer containing cracks was observed at the bonding interface between stainless steel and tantalium when the rolling temperature was above 1373K. The hardness of the bonding layer of zirconium and tantalium bonded above 1273K was higher than tantalium or zirconium base metal in spite of absence of intermetallic compound. The growth of reaction layer at the stainless steel and tantalium interface and at the tantalium and zirconium interface was conforming a parabolic low when that was isothermally heated after hot roll bonding, and the growth rate was almost same as that of static diffusion bonding without using hot roll bonding process. It is estimated that the strain caused by hot roll bonding gives no effect on the growth of reaction layer. It was confirmed that the dissimilar joint of zirconium and stainless steel with insert of tantalium having the sound bonding interface were obtained at the suitable bonding temperature of 1173K by the usage of the newly developed hot roll bonding process. (author)

  2. Effect of Hot Rolling on the Microstructure and Mechanical Properties of Nitrogen Alloyed Austenitic Stainless Steel

    Science.gov (United States)

    Chenna Krishna, S.; Karthick, N. K.; Jha, Abhay K.; Pant, Bhanu; Cherian, Roy M.

    2018-05-01

    In the present investigation, the effect of multi-pass hot rolling in the temperature range of 700-1000 °C on the microstructure and mechanical properties of nitrogen alloyed austenitic stainless steel was studied with the aid of optical microscopy, tensile testing and x-ray diffraction measurements. The microstructural changes that occurred in the hot rolled specimens were elongation of grains in rolling direction, nucleation of new grains at the grain boundaries of elongated grains and growth of nucleated grains to form fully recrystallized grains. Elongated grains formed at lower rolling temperature (700-800 °C) due to inadequate strain/temperature for the initiation of dynamic recrystallization. At higher rolling temperature (900-1000 °C), fine grains formed due to dynamic recrystallization. Tensile properties showed strong dependency on the rolling temperature. Tensile strength increased with the decrease in the rolling temperature at the cost of ductility. Maximum strength was observed in samples hot rolled at 700 °C with yield strength of 917 MPa and ductility of 25%. This variation in the tensile properties with the rolling temperature is attributed to changes in the dislocation density and grain structure. The estimated yield strength from the dislocation density, solid solution and grain boundary strengthening closely matched with experimentally determined yield strength confirming the role of dislocation density and grain size in the strengthening.

  3. Effects of alloying elements on sticking occurring during hot rolling of ferritic stainless steels

    International Nuclear Information System (INIS)

    Ha, Dae Jin; Kim, Yong Jin; Lee, Yong Deuk; Lee, Sung Hak; Lee, Jong Seog

    2008-01-01

    In this study, effects of alloying elements on the sticking occurring during hot rolling of five kinds of ferritic STS430J1L stainless steels were investigated by analyzing high-temperature hardness and oxidation behavior of the rolled steels. Hot-rolling simulation tests were conducted by a high-temperature wear tester which could simulate actual hot rolling. The simulation test results revealed that the sticking process proceeded with three stages, i.e., nucleation, growth, and saturation. Since the hardness continuously decreased as the test temperature increased, whereas the formation of Fe-Cr oxides in the rolled steel surface region increased, the sticking of five stainless steels was evaluated by considering both the high-temperature hardness and oxidation effects. The addition of Zr, Cu, or Si had a beneficial effect on the sticking resistance, while the Ni addition did not show any difference in the sticking. Particularly in the case of the Si addition, Si oxides formed first in the initial stage of high-temperature oxidation, worked as initiation sites for Fe-Cr oxides, accelerated the formation of Fe-Cr oxides, and thus raised the sticking resistance by about 10 times in comparison with the steel without Si content

  4. Hot rolling of chromium - nickel - manganese stainless steel containing nitrogen and boron

    International Nuclear Information System (INIS)

    Khorosh, V.A.; Bulat, S.I.; Mukhina, M.A.; Sorokina, N.A.; Yushchenko, K.A.; Tsentral'nyj Nauchno-Issledovatel'skij Inst. Chernoj Metallurgii, Moscow; AN Ukrainskoj SSR, Kiev. Inst. Ehlektrosvarki)

    1976-01-01

    The strength of stainless steel of the 03Kh2ON16AG6 type increases perceptibly with an increase in the nitrogen content from 0.11 to 0.37%. At the same time, however, its ductility in the region of hot deformation temperatures (red brittleness range of 800 to 1,000 deg C) decreases. Microalloying with boron (0.002 to 0.005% by calculation) permits enhancing the hot ductility to an acceptable level without adversely affecting the working properties. The mechaniusm of boron effect is analyzed. The temperature at which ingots are heated prior to rolling to achieve the desired effect must be sufficiently low. Optimum condition for two stage heating of 6.2-ton ingots are recommeded

  5. Phenomenological Model Describing the Formation of Peeling Defects on Hot-Rolled Duplex Stainless Steel 2205

    Science.gov (United States)

    Yong-jun, Zhang; Hui, Zhang; Jing-tao, Han

    2017-05-01

    The chemical composition, morphology, and microstructure of peeling defects formed on the surface of sheets from steel 2205 under hot rolling are studied. The microstructure of the surface is analyzed using scanning electron and light microscopy. The zones affected are shown to contain nonmetallic inclusions of types Al2O3 and CaO - SiO2 - Al2O3 - MgO in the form of streak precipitates and to have an unfavorable content of austenite, which causes decrease in the ductility of the area. The results obtained are used to derive a five-stage phenomenological model of formation of such defects.

  6. Effect of carbon content on microstructure and mechanical properties of hot-rolled low carbon 12Cr-Ni stainless steel

    International Nuclear Information System (INIS)

    Zheng, H.; Ye, X.N.; Li, J.D.; Jiang, L.Z.; Liu, Z.Y.; Wang, G.D.; Wang, B.S.

    2010-01-01

    Research highlights: → Hot-rolled ultra low carbon martensite is characterized by dislocation cells substructure. → The formation of dislocation cells is attributed to high Ms and low interstitial atoms content. → Hot-rolled ultra low carbon 12Cr-Ni stainless steel has excellent impact toughness. → Delta ferrite deteriorates the impact toughness of hot-rolled 12Cr-Ni stainless steel. - Abstract: 12Cr-Ni stainless steels containing different carbon contents from 0.004 wt.% to 0.034 wt.% were hot-rolled and air-cooled. Their corresponding microstructures were observed with optical microscope and transmission electron microscope, and the Vickers hardness, tensile and impact tests were also carried out. It was found that the martensitic morphology was significantly influenced by carbon content. The as-received ultra low carbon martensite in the steel containing 0.004 wt.% C is characterized by dislocation cells substructure. The formation of dislocation cells is attributed to high martensite finishing point (above 400 deg. C) and low interstitial atoms content. On the other hand, the martensite in the steel containing 0.034 wt.% C consists mainly of typical martensite laths because of low martensite finishing point and high interstitial atoms content which hinder dislocation motion. Furthermore, carbon content has an evident effect on the mechanical properties of 12Cr-Ni steels. The hardness and strength of the as-received steels increase with an increase in carbon content, but their elongation and impact toughness decrease with the carbon content. The steel containing 0.004 wt.% C has excellent impact toughness due to the ultra low carbon content in the martensite composed of dislocation cells.

  7. The effect of heat treatment on recrystallized microstructure, precipitation and ductility of hot-rolled Fe–Cr–Al–REM ferritic stainless steel sheets

    International Nuclear Information System (INIS)

    Qu, H.P.; Lang, Y.P.; Yao, C.F.; Chen, H.T.; Yang, C.Q.

    2013-01-01

    This study presents research works about the effects of heat treatment on recrystallized equiaxed grain size, precipitation, room temperature (RT) toughness and ductile to brittle transition temperature (DBTT) of Fe–Cr–Al–REM ferritic stainless steel (FSS) hot-rolled sheet. Results showed that the recrystallization of hot-rolled Fe–Cr–Al–REM FSS sheet could be completed after annealing treatment at 750 °C for 15 min with the equiaxed grain diameter of approximately 50 μm. Inappropriate annealing treatment would inevitably leads to the unexpected grain coarsening. On the other hand, a great deal of needle-like or spot-like fine aluminum–lanthanum compound Al 11 La 3 precipitates were observed in the ferrite matrix after 1 h aging treatment at 750 °C. The microstructure observation results associated with the impact test definitely illustrated that the Al 11 La 3 precipitates was the reason for the brittle crack in the as-casted ingot and as-forged slab. The real DBTT of the annealed Fe–Cr–Al–REM FSS sheet with average grain size of about 50 μm was −4 °C. Meanwhile, the DBTT of the hot-rolled Fe–Cr–Al–REM stainless steel sheet was evidently increased as the recrystallized grain size increased.

  8. The effect of heat treatment on recrystallized microstructure, precipitation and ductility of hot-rolled Fe-Cr-Al-REM ferritic stainless steel sheets

    Energy Technology Data Exchange (ETDEWEB)

    Qu, H.P., E-mail: quhuapeng0926@163.com [Institute for Special Steels (Formerly Institute for Structural Materials), Central Iron and Steel Research Institute (CISRI), 76 HaiDianNan Road, Beijing 100081 (China); Lang, Y.P. [Institute for Special Steels (Formerly Institute for Structural Materials), Central Iron and Steel Research Institute (CISRI), 76 HaiDianNan Road, Beijing 100081 (China); Yao, C.F. [Institute for Special Steels (Formerly Institute for Structural Materials), Central Iron and Steel Research Institute (CISRI), 76 HaiDianNan Road, Beijing 100081 (China); Zhuozhou Works, Central Iron and Steel Research Institute (CISRI), 2 HuoJuNan Road, Zhuozhou 072750, Hebei (China); Chen, H.T.; Yang, C.Q. [Institute for Special Steels (Formerly Institute for Structural Materials), Central Iron and Steel Research Institute (CISRI), 76 HaiDianNan Road, Beijing 100081 (China)

    2013-02-01

    This study presents research works about the effects of heat treatment on recrystallized equiaxed grain size, precipitation, room temperature (RT) toughness and ductile to brittle transition temperature (DBTT) of Fe-Cr-Al-REM ferritic stainless steel (FSS) hot-rolled sheet. Results showed that the recrystallization of hot-rolled Fe-Cr-Al-REM FSS sheet could be completed after annealing treatment at 750 Degree-Sign C for 15 min with the equiaxed grain diameter of approximately 50 {mu}m. Inappropriate annealing treatment would inevitably leads to the unexpected grain coarsening. On the other hand, a great deal of needle-like or spot-like fine aluminum-lanthanum compound Al{sub 11}La{sub 3} precipitates were observed in the ferrite matrix after 1 h aging treatment at 750 Degree-Sign C. The microstructure observation results associated with the impact test definitely illustrated that the Al{sub 11}La{sub 3} precipitates was the reason for the brittle crack in the as-casted ingot and as-forged slab. The real DBTT of the annealed Fe-Cr-Al-REM FSS sheet with average grain size of about 50 {mu}m was -4 Degree-Sign C. Meanwhile, the DBTT of the hot-rolled Fe-Cr-Al-REM stainless steel sheet was evidently increased as the recrystallized grain size increased.

  9. Development of dissimilar metal transition joint by hot bond rolling

    International Nuclear Information System (INIS)

    Kurokawa, Hiroyuki; Nakasuji, Kazuyuki; Kajimura, Haruhiko; Nagai, Takayuki; Takeda, Seiichiro.

    1997-01-01

    Metallurgically bonded transition joints which enable to connect reprocessing equipments made of superior corrosion resistant valve metals (Ti-5Ta, Zr or Ti) to stainless steel piping are required for nuclear fuel reprocessing plants. The authors have developed dissimilar transition joints made of stainless steel and Ti-5Ta, Zr or Ti with an insert metal of Ta by the hot bond rolling process of clad bars and clad pipes, using a newly developed mill called 'rotary reduction mill'. This report presents the manufacturing process of dissimilar transition joints produced from the clad pipe with three layers by the hot bond rolling. First, the method of hot bond rolling of clad pipe is proposed. Then, the mechanical and corrosion properties of the dissimilar transition joints are evaluated in detail by carrying out various tests. Finally, the rolling properties in the clad pipe method are discussed. (author)

  10. Microstructure and Mechanical Properties of Fe-18Mn-18Cr-0.5N Austenitic Nonmagnetic Stainless Steel in Asymmetric Hot Rolling

    Science.gov (United States)

    Song, Y. L.; Li, C. S.; Ma, B.; Han, Y. H.

    2017-05-01

    Asymmetric hot rolling (ASHR) with a mismatch speed ratio of 1.15 in a single pass was applied to Fe-18Mn-18Cr-0.5N steel and was compared with symmetric hot rolling (SHR). The results indicated that a through-thickness microstructure gradient was formed in the plate due to the shear strain (0.36) introduced by ASHR. A fine-grained layer with the average size of 3 μm was achieved at the top surface of ASHR plate, while numerous elongated grains with a few recrystallized grains were presented at the center layer. The texture was distributed randomly at the top surface of ASHR plate, and a weaker intensity of typical hot-rolled texture in austenitic steel was obtained at the center layer of ASHR plate compared to SHR plate. An excellent combination of microhardness, strength and ductility was obtained in the ASHR plate, which was attributed to gradient microstructure induced by ASHR.

  11. 75 FR 19369 - Certain Hot-Rolled Flat-Rolled Carbon Quality Steel Products from Brazil: Preliminary Results of...

    Science.gov (United States)

    2010-04-14

    .... Hot-rolled dual phase steel, phase-hardened, primarily with a ferritic-martensitic microstructure.... See Preliminary Results of Antidumping Duty Administrative Review: Stainless Steel Sheet and Strip in... Antidumping Duty Administrative Review: Stainless Steel Sheet and Strip in Coils From France, 68 FR 69379...

  12. Hot rolling of thick uranium molybdenum alloys

    Science.gov (United States)

    DeMint, Amy L.; Gooch, Jack G.

    2015-11-17

    Disclosed herein are processes for hot rolling billets of uranium that have been alloyed with about ten weight percent molybdenum to produce cold-rollable sheets that are about one hundred mils thick. In certain embodiments, the billets have a thickness of about 7/8 inch or greater. Disclosed processes typically involve a rolling schedule that includes a light rolling pass and at least one medium rolling pass. Processes may also include reheating the rolling stock and using one or more heavy rolling passes, and may include an annealing step.

  13. Hot rolled composite billet for nuclear control rods

    International Nuclear Information System (INIS)

    Miller, G.E.

    1976-01-01

    This invention relates to a composite plate shaped billet, useful in the fabrication of nuclear control rods, which comprises a core of stainless steel containing about 2 percent boron 10, a thin coating of zirconia on the surfaces of said core, and said zirconia coating being completely encased in a jacket of mild steel, said composite having been hot rolled between about 1075 0 and about 1165 0 C. 1 claim, 8 figures

  14. METHOD OF HOT ROLLING URANIUM METAL

    Science.gov (United States)

    Kaufmann, A.R.

    1959-03-10

    A method is given for quickly and efficiently hot rolling uranium metal in the upper part of the alpha phase temperature region to obtain sound bars and sheets possessing a good surface finish. The uranium metal billet is heated to a temperature in the range of 1000 deg F to 1220 deg F by immersion iii a molten lead bath. The heated billet is then passed through the rolls. The temperature is restored to the desired range between successive passes through the rolls, and the rolls are turned down approximately 0.050 inch between successive passes.

  15. Microstructural characterization of Zr1Nb alloy after hot rolling

    Energy Technology Data Exchange (ETDEWEB)

    Souza, A.C. [Universidade Estadual do Mato Grosso do Sul (UEMS), MS (Brazil); Rossi, J.L.; Martinez, L.G.; Mucsi, C.S. [Instituto de Pesquisas Energéticas e Nucleares (IPEN/CNEN-SP), São Paulo, SP (Brazil); Tsakiropoulos, P. [University of Sheffield (United Kingdom); Ceoni, F.C.; Grandini, C.R. [Universidade Estadual Paulista Julio de Mesquita Filho (UNESP), SP (Brazil)

    2016-07-01

    Full text: The different research lines within the scope in engineering and materials science have developed new materials that can be used in different industrial sectors, such as, energy, health and transportation. For the nuclear industry, for example, the Zr alloys, are of great interest due to its good mechanical properties, excellent corrosion resistance and above all, the high permeability to thermal neutrons. In the health sector, the zirconium poses one of the lowest Young's modulus when compared to other metallic biomaterials, e.g., pure Zr is 68 GPa, bone mineral hydroxyapatite is 80 GPa, for Ti alloys is 90 GPa and above, for Nb is 105 GPa and stainless steels above 189 GPa. This is particularly important for implants in bones, whose elasticity modulus can reach 30 GPa and it is desirable an as close match as possible. However, the zirconium alloys, have great chemical affinity with oxygen and nitrogen. Moreover, oxides and nitrides may form during the melting process, heat treatment and hot rolling, changing the physic-chemical properties of the alloy. This experimental work shows the results of the evolution of the microstructure after hot rolling of the Zr1Nb alloy. It was possible to confirm the absence of formation of oxides and nitrides, thus confirming the of the experimental method of melting and hot rolling of the Zr1Nb alloy. (author)

  16. Properties of hot rolled steels for enamelling

    International Nuclear Information System (INIS)

    Gavrilovski, Dragica; Gavrilovski, Milorad

    2003-01-01

    The results of an investigation of the structure and properties of experimental produced hot rolled steels suitable for enamelling are presented in the paper. Hot rolled steels for enamelling represent a special group of the steels for conventional enamelling. Their quality has to be adapted to the method and conditions of enamelling. Therefore, these steels should meet some specific requirements. In addition to usual investigation of the chemical composition and mechanical properties, microstructure and quality of the steel surface also were investigated. The basic aim was to examine steels capability for enamelling, i. e. steels resistance to the fish scales phenomena, by trial enamelling, as well as quality of the steel - enamel contact surface, to evaluate the binding. Also, the changes of the mechanical properties, especially the yield point, during thermal treatment, as a very specific requirement, were investigated, by simplified method. Good results were obtained confirming the steels capability for enamelling. (Original)

  17. Rietveld and impedance analysis of cold and hot rolled duplex and lean duplex steels for application in paper and pulp industry

    Energy Technology Data Exchange (ETDEWEB)

    Esteves, Luiza; Lins, Vanessa de Freitas Cunha, E-mail: luizaeq@yahoo.com.br [Universidade Federal de Minas Gerais (UFMG), Belo Horizonte, MG (Brazil). Departamento de Engenharia Quimica; Paiva, Paulo Renato Perdigao [Centro Federal de Educacao Tecnologica de Minas Gerais (CEFET), Belo Horizonte, MG (Brazil); Viana, Adolfo Kalergis do Nascimento [APERAM South America, Timoteo, MG (Brazil)

    2017-01-15

    In this study, X-Ray Diffraction (XRD) and Rietveld Refinement were performed to identify and quantify the ferrite and austenite phase of cold and hot rolled duplex stainless steels (UNS S31803) and lean duplex stainless steels (UNS S32304). Electrochemical impedance spectroscopy (EIS) was applied to evaluate the chemical behavior of duplex and lean duplex stainless steels in white, green, and black liquors of paper and pulp industry. Rietveld analysis results showed a higher austenite content than the standard limit for duplex steels in the hot rolled condition. The hot rolling condition plays a major role in improving corrosion resistance in white liquor mainly for the lean duplex steel. (author)

  18. Rietveld and impedance analysis of cold and hot rolled duplex and lean duplex steels for application in paper and pulp industry

    International Nuclear Information System (INIS)

    Esteves, Luiza; Lins, Vanessa de Freitas Cunha; Viana, Adolfo Kalergis do Nascimento

    2017-01-01

    In this study, X-Ray Diffraction (XRD) and Rietveld Refinement were performed to identify and quantify the ferrite and austenite phase of cold and hot rolled duplex stainless steels (UNS S31803) and lean duplex stainless steels (UNS S32304). Electrochemical impedance spectroscopy (EIS) was applied to evaluate the chemical behavior of duplex and lean duplex stainless steels in white, green, and black liquors of paper and pulp industry. Rietveld analysis results showed a higher austenite content than the standard limit for duplex steels in the hot rolled condition. The hot rolling condition plays a major role in improving corrosion resistance in white liquor mainly for the lean duplex steel. (author)

  19. Investigation of Hot Rolling Influence on the Explosive-Welded Clad Plate

    Directory of Open Access Journals (Sweden)

    Guanghui ZHAO

    2016-11-01

    Full Text Available The microstructure, the shear strength and tensile strength of stainless steel explosive-welded clad plate at different rolling reduction were studied. The mechanical properties of the explosive-welded and explosive-rolled clad plates were experimentally measured. Simultaneously, the microstructures of the clad plate were investigated by the Ultra deep microscope and the tensile fracture surface were observed by the scan electron microscope (SEM. It was observed that the tensile strength has been increased considerably, whereas the elongation percentage has been reduced with the increase of hot rolling reduction. In the tensile shear test, the bond strength is higher than the strength of the ferritic stainless steel layer and meets the relevant known standard criterion. Microstructural evaluations showed that the grain of the stainless steel and steel refined with the increase of thickness reduction. Examination of the tensile fracture surfaces reveal that, after hot rolling, the fracture in the low alloy steel and ferritic stainless steel clad plates is of the ductile type.DOI: http://dx.doi.org/10.5755/j01.ms.22.4.12409

  20. Metallurgical analysis of spalled work roll of hot strip mill

    International Nuclear Information System (INIS)

    Khan, M.M.; Khan, M.A.

    1993-01-01

    In this study failure analysis of four work roll of the Hot Strip Mill is carried out. The microstructure is correlated with the chemical composition of shell and roll-life. It was concluded that for the longer service of the roll, cementite, graphite and martensite should be balanced (as per working requirement of the mill). (author)

  1. Hot-rolling metals in vacuum. Information circular

    International Nuclear Information System (INIS)

    Beall, R.A.; Worthington, R.B.; Blickensderfer, R.

    1979-01-01

    The process of hot-rolling metals, alloys, and composites in vacuum is studied. First, a comprehensive review of the literature is presented, including the advantages and disadvantages of using vacuum. Next, details of hot-rolling titanium, chromium, and molybdenum-iron bimetal are given. Finally, the design of new equipment is described

  2. A simulation study on the multi-pass rolling bond of 316L/Q345R stainless clad plate

    Directory of Open Access Journals (Sweden)

    Qin Qin

    2015-07-01

    Full Text Available This article describes an investigation into interface bonding research of 316L/Q345R stainless clad plate. A three-dimensional thermal–elastic–plastic model has been established using finite element analysis to model the multi-pass hot rolling process. Results of the model have been compared with those obtained from a rolling experiment of stainless clad plate. The comparisons of temperature and profile of the rolled stainless clad plate have indicated a satisfactory accuracy of finite element analysis simulation. Effects on interface bonding by different parameters including pre-heating temperature, multi-pass thickness reduction rules, rolling speed, covering rate, and different assemble patterns were analyzed systematically. The results show that higher temperature and larger thickness reduction are beneficial to achieve the bonding in vacuum hot rolling process. The critical reduction in the bond at the temperature of 1200 °C is 28%, and the critical thickness reduction reduces by about 2% when the temperature increases by 50 °C during the range from 1000 °C to 1250 °C. And the relationship between the minimum pass number and thickness reduction has been suggested. The results also indicate that large covering rate in the assemble pattern of outer soft and inner hard is beneficial to achieve the bond of stainless clad plate.

  3. 75 FR 42782 - Hot-Rolled Flat-Rolled Carbon-Quality Steel Products From Brazil, Japan, and Russia

    Science.gov (United States)

    2010-07-22

    ...)] Hot-Rolled Flat-Rolled Carbon-Quality Steel Products From Brazil, Japan, and Russia AGENCY: United... Brazil and Japan, and the suspended investigation on hot-rolled steel from Russia. SUMMARY: The... Japan, and the suspended investigation on hot-rolled steel from Russia would be likely to lead to...

  4. 75 FR 62566 - Hot-Rolled Flat-Rolled Carbon-Quality Steel Products From Brazil, Japan, and Russia

    Science.gov (United States)

    2010-10-12

    ...)] Hot-Rolled Flat-Rolled Carbon-Quality Steel Products From Brazil, Japan, and Russia AGENCY: United... antidumping duty investigation on hot-rolled steel from Russia. SUMMARY: The Commission hereby gives notice of... suspended investigation on hot-rolled steel from Russia would be likely to lead to continuation or...

  5. Development of dissimilar metal transition joint by hot roll bonding technique

    International Nuclear Information System (INIS)

    Nagai, Takayuki; Takeda, Seiichiro; Tanaka, Yasumasa; Ogawa, Kazuhiro; Nakasuji, Kazuyuki; Ikenaga, Yoshiaki.

    1994-01-01

    Metallurgically bonded transition joints which enable to connect reprocessing equipments made of superior corrosion resistant valve metals (Ti-5Ta, Zr or Ti) with stainless steel piping is needed for nuclear fuel reprocessing plants. The authors have developed dissimilar metal transition joints between stainless steel and Ti-5Ta, Zr or Ti with an insert metal of Ta by the hot roll bonding process, using the newly developed mill called 'rotary reduction mill'. In the R and D program, appropriate bonding conditions in the manufacturing process of the joints were established. This report presents the structure of transition joints and the manufacturing process by the hot roll bonding technique. Then, the evaluation of mechanical and corrosion properties and the results of demonstration test of joints for practical use are described. (author)

  6. Development of dissimilar metal transition joint by hot roll bonding technique

    International Nuclear Information System (INIS)

    Nagai, Takayuki; Takeuchi, Masayuki; Takeda, Seiichiro; Shikakura, Sakae; Ogawa, Kazuhiro; Nakasuji, Kazuyuki; Kajimura, Haruhiko.

    1995-01-01

    Metallurgically bonded transition joints which enable to connect reprocessing equipments made of superior corrosion resistant valve metals (Ti-5Ta, Zr or Ti) with stainless steel piping is needed for nuclear fuel reprocessing plants. The authors have developed dissimilar metal transition joints between stainless steel and Ti-5Ta, Zr or Ti with an insert metal of Ta by the hot roll bonding process, using the newly developed mill called 'rotary reduction mill'. In the R and D program, appropriate bonding conditions in the manufacturing process of the joints were established. This report presents the structure of transition joints and the manufacturing process by hot roll bonding technique. Then, the evaluation of mechanical and corrosion properties and the results of demonstration test of joints for practical use are described. (author)

  7. Engineering study for a melting, casting, rolling and fabrication facility for recycled contaminated stainless steel

    International Nuclear Information System (INIS)

    1994-01-01

    This Preliminary Report is prepared to study the facilities required for recycling contaminated stainless steel scrap into plate which will be fabricated into boxes suitable for the storage of contaminated wastes and rubble. The study is based upon the underlying premise that the most cost effective way to produce stainless steel is to use the same processes employed by companies now in production of high quality stainless steel. Therefore, the method selected for this study for the production of stainless steel plate from scrap is conventional process using an Electric Arc Furnace for meltdown to hot metal, a Continuous Caster for production of cast slabs, and a Reversing Hot Mill for rolling the slabs into plate. The fabrication of boxes from the plate utilizes standard Shears, Punch Presses and welding equipment with Robotic Manipulators. This Study presumes that all process fumes, building dusts and vapors will be cycled through a baghouse and a nuclear grade HEPA filter facility prior to discharge. Also, all process waste water will be evaporated into the hot flue gas stream from the furnace utilizing a quench tank; so there will be no liquid discharges from the facility and all vapors will be processed through a HEPA filter. Even though HEPA filters are used today in controlling radioactive contamination from nuclear facilities there is a sparsity of data concerning radioactivity levels and composition of waste that may be collected from contaminated scrap steel processing. This report suggests some solutions to these problems but it is recommended that additional study must be given to these environmental problems

  8. Effect of Rolling and Subsequent Annealing on Microstructure, Microtexture, and Properties of an Experimental Duplex Stainless Steel

    Science.gov (United States)

    Mandal, Arka; Patra, Sudipta; Chakrabarti, Debalay; Singh, Shiv Brat

    2017-12-01

    A lean duplex stainless steel (LDSS) has been prepared with low-N content and processed by different thermo-mechanical schedules, similar to the industrial processing that comprised hot-rolling, cold-rolling, and annealing treatments. The microstructure developed in the present study on low-N LDSS has been compared to that of high-N LDSS as reported in the literature. As N is an austenite stabilizer, lower-N content reduced the stability of austenite and the austenite content in low-N LDSS with respect to the conventional LDSS. Due to low stability of austenite in low-N LDSS, cold rolling resulted in strain-induced martensitic transformation and the reversion of martensite to austenite during subsequent annealing contributed to significant grain refinement within the austenite regions. δ-ferrite grains in low-N LDSS, on the other hand, are refined by extended recovery mechanism. Initial solidification texture (mainly cube texture) within the δ-ferrite region finally converted into gamma-fiber texture after cold rolling and annealing. Although MS-brass component dominated the austenite texture in low-N LDSS after hot rolling and cold rolling, that even transformed into alpha-fiber texture after the final annealing. Due to the significant grain refinement and formation of beneficial texture within both austenite and ferrite, good combination of strength and ductility has been achieved in cold-rolled and annealed sample of low-N LDSS steel.

  9. Image recognition of shape defects in hot steel rolling

    NARCIS (Netherlands)

    Balmashnova, E.; Bruurmijn, L.C.M.; Dissanayake, R.; Duits, R.; Kampmeijer, L.; Noorden, van T.L.; Boon, M.A.A.

    2013-01-01

    A frequently occurring issue in hot rolling of steel is so-called tail pinching. Prominent features of a pinched tail are ripple-like defects and a pointed tail. In this report two algorithms are presented to detect those features accurately in 2D gray scale images of steel strips. The two ripple

  10. Simulation of Bimetallic Bush Hot Rolling Bonding Process

    Directory of Open Access Journals (Sweden)

    Yaqin Tian

    2015-01-01

    Full Text Available Three-dimensional model of bimetallic bush was established including the drive roller and the core roller. The model adopted the appropriate interface assumptions. Based on the bonding properties of bimetallic bush the hot rolling process was analyzed. The optimum reduction ratio of 28% is obtained by using the finite element simulation software MARC on the assumption of the bonding conditions. The stress-strain distribution of three dimensions was research assumptions to interface deformation of rolling. At the same time, based on the numerical simulation, the minimum reduction ratio 20% is obtained by using a double metal composite bush rolling new technology from the experiment research. The simulation error is not more than 8%.

  11. Development of TRIP-Aided Lean Duplex Stainless Steel by Twin-Roll Strip Casting and Its Deformation Mechanism

    Science.gov (United States)

    Zhao, Yan; Zhang, Weina; Liu, Xin; Liu, Zhenyu; Wang, Guodong

    2016-12-01

    In the present work, twin-roll strip casting was carried out to fabricate thin strip of a Mn-N alloyed lean duplex stainless steel with the composition of Fe-19Cr-6Mn-0.4N, in which internal pore defects had been effectively avoided as compared to conventional cast ingots. The solidification structure observed by optical microscope indicated that fine Widmannstatten structure and coarse-equiaxed crystals had been formed in the surface and center, respectively, with no columnar crystal structures through the surface to center of the cast strip. By applying hot rolling and cold rolling, thin sheets with the thickness of 0.5 mm were fabricated from the cast strips, and no edge cracks were formed during the rolling processes. With an annealing treatment at 1323 K (1050 °C) for 5 minutes after cold rolling, the volume fractions of ferrite and austenite were measured to be approximately equal, and the distribution of alloying elements in the strip was further homogenized. The cold-rolled and annealed sheet exhibited an excellent combination of strength and ductility, with the ultimate tensile strength and elongation having been measured to be 1000 MPa and 65 pct, respectively. The microstructural evolution during deformation was investigated by XRD, EBSD, and TEM, indicating that ferrite and austenite had different deformation mechanisms. The deformation of ferrite phase was dominated by dislocation slipping, and the deformation of austenite phase was mainly controlled by martensitic transformation in the sequence of γ→ ɛ-martensite→ α'-martensite, leading to the improvement of strength and plasticity by the so-called transformation-induced plasticity (TRIP) effect. By contrast, lean duplex stainless steels of Fe-21Cr-6Mn-0.5N and Fe-23Cr-7Mn-0.6N fabricated by twin-roll strip casting did not show TRIP effects and exhibited lower strength and elongation as compared to Fe-19Cr-6Mn-0.4N.

  12. 75 FR 64246 - Certain Hot-Rolled Flat-Rolled Carbon-Quality Steel Products From Brazil: Correction to Notice of...

    Science.gov (United States)

    2010-10-19

    ...-Rolled Carbon-Quality Steel Products From Brazil: Correction to Notice of Antidumping Duty Order AGENCY... certain hot-rolled flat-rolled carbon-quality steel products from Brazil. See Antidumping Duty Order: Certain Hot-Rolled Flat-Rolled Carbon-Quality Steel Products From Brazil, 67 FR 11093 (March 12, 2002...

  13. Boron effect on stainless steel plasticity under hot deformation

    International Nuclear Information System (INIS)

    Bulat, S.I.; Kardonov, B.A.; Sorokina, N.A.

    1978-01-01

    The effect of boron on plasticity of stainless steels at temperatures of hot deformation has been studied at three levels of alloying, i.e. 0-0.01% (micro-alloying or modifying), 0.01-0.02% (low alloying) and 0.02-2.0% (high alloying). Introduction of 0.001-0.005% of boron increases hot plasticity of both low and high carbon stainless steels due to decrease in grain size and strengthening of grain boundaries. Microalloying by boron has a positive effect at temperatures below 1200-1220 deg C. At higher temperatures, particularly when its content exceeds 0.008%, boron deteriorates plasticity by increasing the size of grains and weakening their boundaries. 0.1-2% boron strengthen the stainless steel and dectease its plasticity

  14. A review of hot cracking in austenitic stainless steel weldments

    International Nuclear Information System (INIS)

    Shankar, V.; Gill, T.P.S.; Mannan, S.L.; Rodriguez, P.

    1991-01-01

    The occurrence of hot cracking in austenitic stainless steel weldments is discussed with respect to its origin and metallurgical contributory factors. Of the three types of hot cracking, namely solidification cracking, liquation and ductility dip cracking, solidification cracking occurs in the interdendritic regions in weld metal while liquation and ductility dip cracking occur intergranularly in the heat-affected zone (HAZ). Segregation of impurity and minor elements such as sulphur, phosphorous, silicon, niobium, boron etc to form low melting eutectic phases has been found to be the major cause of hot cracking. Control of HAZ cracking requires minimisation of impurity elements in the base metal. In stabilized stainless steels containing niobium, higher amounts of delta-ferrite have been found necessary to prevent cracking than in unstabilized compositions. Titanium compounds have been found to cause liquation cracking in maraging steels and titanium containing stainless steels and superalloys. In nitrogen added stainless steels, cracking resistance decreases when the solidification mode changes to primary austenitic due to nitrogen addition. A review of the test methods to evaluate hot cracking behaviour showed that several external restraint and semi-self-restraint tests are available. The finger Test, WRC Fissure Bend Test, the PVR test and the Varestraint Test are described along with typical test results. Hot ductility testing to reveal HAZ cracking tendency during welding is described, which is of particular importance to stabilized stainless steels. Based on the literature, recommendations are made for welding stabilized and nitrogen added steels, indicating areas of further work. (author). 81 refs., 30 figs., 1 tab

  15. Flow behavior of polymers during the roll-to-roll hot embossing process

    International Nuclear Information System (INIS)

    Deng, Yujun; Yi, Peiyun; Peng, Linfa; Lai, Xinmin; Lin, Zhongqin

    2015-01-01

    The roll-to-roll (R2R) hot embossing process is a recent advancement in the micro hot embossing process and is capable of continuously fabricating micro/nano-structures on polymers, with a high efficiency and a high throughput. However, the fast forming of the R2R hot embossing process limits the time for material flow and results in complicated flow behavior in the polymers. This study presents a fundamental investigation into the flow behavior of polymers and aims towards the comprehensive understanding of the R2R hot embossing process. A three-dimensional (3D) finite element (FE) model based on the viscoelastic model of polymers is established and validated for the fabrication of micro-pyramids using the R2R hot embossing process. The deformation and recovery of micro-pyramids on poly(vinyl chloride) (PVC) film are analyzed in the filling stage and the demolding stage, respectively. Firstly, in the analysis of the filling stage, the temperature distribution on the PVC film is discussed. A large temperature gradient is observed along the thickness direction of the PVC film and the temperature of the top surface is found to be higher than that of the bottom surface, due to the poor thermal conductivity of PVC. In addition, creep strains are demonstrated to depend highly on the temperature and are also observed to concentrate on the top layer of the PVC film because of high local temperature. In the demolding stage, the recovery of the embossed micro-pyramids is obvious. The cooling process is shown to be efficient for the reduction of recovery, especially when the mold temperature is high. In conclusion, this research advances the understanding of the flow behavior of polymers in the R2R hot embossing process and might help in the development of the highly accurate and highly efficient fabrication of microstructures on polymers. (paper)

  16. Characterizing the stretch-flangeability of hot rolled multiphase steels

    International Nuclear Information System (INIS)

    Pathak, N.; Butcher, C.; Worswick, M.; Gao, J.

    2013-01-01

    Hole expansion tests are commonly used to characterize the edge stretching limit of a material. Traditionally, a conical punch is used to expand a punched hole until a through-thickness crack appears. However, many automotive stretch flanging operations involve in-plane edge stretching that is best captured with a flat punch. In this paper, hole expansion tests were carried out on two different hot-rolled multiphase steels using both flat and conical punches. The fracture mechanisms for both punch types were investigated using scanning electron microscopy (SEM)

  17. Numerical cooling strategy design for hot rolled dual phase steel

    Energy Technology Data Exchange (ETDEWEB)

    Suwanpinij, Piyada; Prahl, Ulrich; Bleck, Wolfgang [RWTH Aachen (DE). Dept. of Ferrous Metallurgy (IEHK); Togobytska, Nataliya; Weiss, Wolf; Hoemberg, Dietmar [Weierstrass-Institut fuer Angewandte Analysis und Stochastik (WIAS) im Forschungsverbund Berlin e.V. (Germany)

    2010-10-21

    In this article, the Mo-Mn dual phase steel and its process parameters in hot rolling are discussed. The process window was derived by combining the experimental work in a hot deformation dilatometer and numerical calculation of process parameters using rate law models for ferrite and martensite transformation. The ferrite formation model is based on the Leblond and Devaux approach while martensite formation is based on the Koistinen- Marburger (K-M) formula. The carbon enrichment during ferrite formation is taken into account for the following martensite formation. After the completion of the parameter identification for the rate law model, the evolution of phases in multiphase steel can be addressed. Particularly, the simulations allow for predicting the preferable degree of retained strain and holding temperature on the run out table (ROT) for the required ferrite fraction. (orig.)

  18. Hot-rolled Process of Multilayered Composite Metal Plate

    Directory of Open Access Journals (Sweden)

    YU Wei

    2017-02-01

    Full Text Available For multi-layer plate, it is a difficult problem to increase product yield rate and improve bonding interface quality. A high yield hot-rolled method of multilayered plate was proposed. The raw strips and plate were fixed by argon arc welding. The combined billet was put into a metal box and vacuum pumped, and then heated and rolled by multi passes at the temperature of 1000-1200℃. The 67 layered plate with the thickness of 2.5mm was successfully produced. The interfacial microstructures and diffusion behavior were investigated and analyzed by optical microscopy and scan electronic microscopy. The tensile and shear strength were tested,and the shear fractures were analyzed. The results show that the multilayered plate yield rate is more than 90% by two steps billet combination method and rolling process optimization. The good bonding interface quality is obtained, the shear strength of multilayered plate reaches 241 MPa. Nickel interlayer between 9Cr18 and 1Cr17 can not only prevent the diffusion of carbon, but also improve the microstructure characteristics.

  19. 76 FR 34101 - Hot-Rolled Flat-Rolled Carbon-Quality Steel Products From Brazil, Japan, and Russia

    Science.gov (United States)

    2011-06-10

    ...] Hot-Rolled Flat-Rolled Carbon-Quality Steel Products From Brazil, Japan, and Russia Determinations On...-quality steel products from Russia would be likely to lead to continuation or recurrence of material injury to an industry in the United States within a reasonably foreseeable time. The Commission further...

  20. Mechanical Behaviour of 304 Austenitic Stainless Steel Processed by Room Temperature Rolling

    Science.gov (United States)

    Singh, Rahul; Goel, Sunkulp; Verma, Raviraj; Jayaganthan, R.; Kumar, Abhishek

    2018-03-01

    To study the effect of room temperature rolling on mechanical properties of 304 Austenitic Stainless Steel, the as received 304 ASS was rolled at room temperature for different percentage of plastic deformation (i.e. 30, 50, 70 and 90 %). Microstructural study, tensile and hardness tests were performed in accordance with ASTM standards to study the effect of rolling. The ultimate tensile strength (UTS) and hardness of a rolled specimen have enhanced with rolling. The UTS has increased from 693 MPa (as received) to 1700 MPa (after 90% deformation). The improvement in UTS of processed samples is due to combined effect of grain refinement and stress induced martensitic phase transformation. The hardness values also increases from 206 VHN (as received) to 499 VHN (after 90% deformation). Magnetic measurements were also conducted to confirm the formation of martensitic phase.

  1. Patterned immobilization of antibodies within roll-to-roll hot embossed polymeric microfluidic channels.

    Directory of Open Access Journals (Sweden)

    Belachew Feyssa

    Full Text Available This paper describes a method for the patterned immobilization of capture antibodies into a microfluidic platform fabricated by roll-to-roll (R2R hot embossing on poly (methyl methacrylate (PMMA. Covalent attachment of antibodies was achieved by two sequential inkjet printing steps. First, a polyethyleneimine (PEI layer was deposited onto oxygen plasma activated PMMA foil and further cross-linked with glutaraldehyde (GA to provide an amine-reactive aldehyde surface (PEI-GA. This step was followed by a second deposition of antibody by overprinting on the PEI-GA patterned PMMA foil. The PEI polymer ink was first formulated to ensure stable drop formation in inkjet printing and the printed films were characterized using atomic force microscopy (AFM and X-ray photoelectron spectroscopy (XPS. Anti-CRP antibody was patterned on PMMA foil by the developed method and bonded permanently with R2R hot embossed PMMA microchannels by solvent bonding lamination. The functionality of the immobilized antibody inside the microfluidic channel was evaluated by fluorescence-based sandwich immunoassay for detection of C-reactive protein (CRP. The antibody-antigen assay exhibited a good level of linearity over the range of 10 ng/ml to 500 ng/ml (R(2 = 0.991 with a calculated detection limit of 5.2 ng/ml. The developed patterning method is straightforward, rapid and provides a versatile approach for creating multiple protein patterns in a single microfluidic channel for multiplexed immunoassays.

  2. Effects of microalloying on hot-rolled and cold-rolled Q&P steels

    Science.gov (United States)

    Azevedo de Araujo, Ana Luiza

    Third generation advanced high strength steels (AHSS) have been a major focus in steel development over the last decade. The premise of these types of steel is based on the potential to obtain excellent combinations of strength and ductility with low-alloy compositions by forming mixed microstructures containing retained austenite (RA). The development of heat treatments able to achieve the desired structures and properties, such as quenching and partitioning (Q&P) steels, is driven by new requirements to increase vehicle fuel economy by reducing overall weight while maintaining safety and crashworthiness. Microalloying additions of niobium (Nb) and vanadium (V) in sheet products are known to provide strengthening via grain refinement and precipitation hardening and may influence RA volume fraction and transformation behavior. Additions of microalloying elements in Q&P steels have not been extensively studied to date, however. The objective of the present study was to begin to understand the potential roles of Nb and V in hot-rolled and cold-rolled Q&P steel. For that, a common Q&P steel composition was selected as a Base alloy with 0.2C-1.5Si-2.0Mn (wt. %). Two alloys with an addition of Nb (0.02 and 0.04 wt. %) and one with an addition of V (0.06 wt. %) to the Base alloy were investigated. Both hot-rolled and cold-rolled/annealed Q&P simulations were conducted. In the hot-rolled Q&P study, thermomechanical processing was simulated via hot torsion testing in a GleebleRTM 3500, and four coiling temperatures (CT) were chosen. Microstructural evaluation (including RA measurements via electron backscattered diffraction - EBSD) and hardness measurements were performed for all alloys and coiling conditions. The analysis showed that Nb additions led to overall refinement of the prior microstructure. Maximum RA fractions were measured at the 375 °C CT, and microalloying was associated with increased RA in this condition when compared to the Base alloy. A change in

  3. Hot Ductility of the 17-4 PH Stainless Steels

    Science.gov (United States)

    Herrera Lara, V.; Guerra Fuentes, L.; Covarrubias Alvarado, O.; Salinas Rodriguez, A.; Garcia Sanchez, E.

    2016-03-01

    The mechanisms of loss of hot ductility and the mechanical behavior of 17-4 PH alloys were investigated using hot tensile testing at temperatures between 700 and 1100 °C and strain rates of 10-4, 10-2, and 10-1 s-1. Scanning electron microscopy was used in conjunction with the results of the tensile tests to find the temperature region of loss of ductility and correlate it with cracking observed during processing by hot upsetting prior to ring rolling. It is reported that 17-4 PH alloys lose ductility in a temperature range around 900 °C near to the duplex austenite + ferrite phase field. Furthermore, it is found that niobium carbides precipitated at austenite/ferrite interfaces and grain boundaries have a pronounced effect on the mechanical behavior of the alloy during high-temperature deformation.

  4. Enhancement of strength properties of hot rolled 10KHSND steel

    International Nuclear Information System (INIS)

    Nasibov, A.G.; Popova, L.V.; Pikulin, S.A.; Globa, N.I.

    1989-01-01

    To find out the reasons of low hot rolling yield for 10KhSND steel sheets in mechanical properties, titanium effect in the range of 0.008-0.03% concentrations is studied. It is established that the titanium content in a solid solution is conserved within 0.003-0.005%, the rest of titanium is bound to carbonitrides Ti(C, N). It is shown that alloys with 0.025-0.03% titanium content possess the increased values of ultimate and yield strength the necessary level of impact strength and good wealdability. The good steel yield, when the titanium content is sustained at the given level, increases from 40 to 85%

  5. Mechanical Properties of a Bainitic Steel Producible by Hot Rolling

    Directory of Open Access Journals (Sweden)

    Rana R.

    2017-12-01

    Full Text Available A carbide-free bainitic microstructure is suitable for achieving a combination of ultra high strength and high ductility. In this work, a steel containing nominally 0.34C-2Mn-1.5Si-1Cr (wt.% was produced via industrial hot rolling and laboratory heat treatments. The austenitization (900°C, 30 min. and austempering (300-400°C, 3 h treatments were done in salt bath furnaces. The austempering treatments were designed to approximately simulate the coiling step, following hot rolling and run-out-table cooling, when the bainitic transformation would take place and certain amount of austenite would be stabilized due to suppression of carbide precipitation. The microstructures and various mechanical properties (tensile properties, bendability, flangeability, and room and subzero temperature impact toughness relevant for applications were characterized. It was found that the mechanical properties were highly dependent on the stability of the retained austenite, presence of martensite in the microstructure and the size of the microstructural constituents. The highest amount of retained austenite (~ 27 wt.% was obtained in the sample austempered at 375°C but due to lower austenite stability and coarser overall microstructure, the sample exhibited lower tensile ductility, bendability, flangeability and impact toughness. The sample austempered at 400°C also showed poor properties due to the presence of initial martensite and coarse microstructure. The best combination of mechanical properties was achieved for the samples austempered at 325-350°C with a lower amount of retained austenite but with the highest mechanical stability.

  6. Dynamic Recrystallization and Hot Workability of 316LN Stainless Steel

    Directory of Open Access Journals (Sweden)

    Chaoyang Sun

    2016-07-01

    Full Text Available To identify the optimal deformation parameters for 316LN austenitic stainless steel, it is necessary to study the macroscopic deformation and the microstructural evolution behavior simultaneously in order to ascertain the relationship between the two. Isothermal uniaxial compression tests of 316LN were conducted over the temperature range of 950–1150 °C and for the strain rate range of 0.001–10 s−1 using a Gleeble-1500 thermal-mechanical simulator. The microstructural evolution during deformation processes was investigated by studying the constitutive law and dynamic recrystallization behaviors. Dynamic recrystallization volume fraction was introduced to reveal the power dissipation during the microstructural evolution. Processing maps were developed based on the effects of various temperatures, strain rates, and strains, which suggests that power dissipation efficiency increases gradually with increasing temperature and decreasing stain rate. Optimum regimes for the hot deformation of 316LN stainless steel were revealed on conventional hot processing maps and verified effectively through the examination of the microstructure. In addition, the regimes for defects of the product were also interpreted on the conventional hot processing maps. The developed power dissipation efficiency maps allow optimized processing routes to be selected, thus enabling industry producers to effectively control forming variables to enhance practical production process efficiency.

  7. Cold-rolled sheets production of stainless martensite-ageing steel smelted by vacuum arc and electroslag techniques

    Energy Technology Data Exchange (ETDEWEB)

    Rivkin, A A; Grishkov, A I; Suslin, A P; Nesterenko, A A; Lola, V N [Tsentral' nyj Nauchno-Issledovatel' skij Inst. Chernoj Metallurgii, Moscow (USSR)

    1975-05-01

    In cooperation with a number of metallurgical works the production of a high strength sheet stainless maraging steel EHP678 (000KH11N10M2T) has been tested by rolling cylindrical ingots of vacuum arc smelting at the blooming (the mass of rough ingots was 5.1 to 6.0 t, that of cleaned ingots - 3.8 to 5.1 t) or rectangular ingots of electroslag smelting (13 t) at the slabbing. The recommended regimes of heating and deformation are much similar to those used for the steel-KH18N10T. The output of valid cold-rolled sheets proved to be rather low (0.24 t/t for the vacuum arc smelting and 0.30 t/t for the electroslag smelting) mainly due to the losses on cleaning and a considerable portion of wrong-size slabs. The data are presented on the steel-EHP678 properties after various heat treatments. For the production of wide cold-rolled sheets of the steel EHP678 it is recommended to use steelmaking procedure with electroslag smelting including open-hearth melting in arc furnaces, rolling of ingots at the slabbing with heating up to 1260-1280 deg C (hold-up of 4.5 to 5 hrs); electroslag smelting for rectangular section slabs, rolling of ingots of electroslag smelting at the slabbing with their heating up to 1250 deg C (hold-up of 5.5 to 6 hrs), rolling at the 1680-type mill with heating up to 1250-1260 deg C (hold-up of 4 to 4.5 hrs ensuring the rolling temperature after a rough group not below 1100 deg C), quenching of hot-rolled sheets heating up to 920-940 deg C (hold-up of 3 to 3.5 min/mm), shot peening of sheets for descaling (provided the respective equipment is available) with a subsequent short-time pickling in an acid solution and cold rolling with a summary deformation of 35 to 45 %. The steelmaking with the electroslag smelting is much more profitable as regards to the fine technology of number of the main procedures, convenient cooperation of the works and a considerably greater output of the final products out of one ton of the steel produced.

  8. Analysis of hot rolling and hot forging effects on mechanical properties and microstructure of ZrNbMoGe alloy

    International Nuclear Information System (INIS)

    AH Ismoyo; Parikin; Bandriyana

    2014-01-01

    Research on formation technique by a combined method of rolling and forging has been carried out in order to improve the mechanical properties of ZrNbMoGe alloy to be used as fuel cladding in NPP (Nuclear Power Plant) application. The effects of rolling and forging were analyzed several tests. The tests were conducted for zirconium alloy specimen with a composition of (in % wt.) 97% Zr, 0,5% Mo, 2% Nb and 0,5% Ge, where the specimen was melted with an arc-furnace. The hot rolling and forging were conducted at 900 °C and 950 °C respectively. Hardness test was carried out by using a microhardness testing machine, while microstructure examination and crystal structure analysis were conducted with an optical microscope and an X-ray diffractometer. The results show that the hardness of the alloy increase from 141.21 HV (starting material) to 210.47 HV (hot rolled material) and 365.75 HV (hot forged material). Texturing phenomenon is clearly figured on the microstructure due to hot rolling and forging process. Analysis by diffractogram also indicates that the hot rolling and forging process has influence on the crystal orientation of dominant preferred direction in the reflection plane of (10ī1), recorded from the rise of intensity counting from about 2500 to 3000. In summary, hot forging and rolling process can change the mechanical properties (hardness and texture) and microstructure of materials. (author)

  9. Strain hardening of cold-rolled lean-alloyed metastable ferritic-austenitic stainless steels

    Energy Technology Data Exchange (ETDEWEB)

    Papula, Suvi [Aalto University School of Engineering, Department of Mechanical Engineering, P.O. Box 14200, FI-00076 Aalto (Finland); Anttila, Severi [Centre for Advanced Steels Research, University of Oulu, P.O. Box 4200, 90014 Oulu (Finland); Talonen, Juho [Outokumpu Oyj, P.O. Box 245, FI-00181 Helsinki (Finland); Sarikka, Teemu; Virkkunen, Iikka; Hänninen, Hannu [Aalto University School of Engineering, Department of Mechanical Engineering, P.O. Box 14200, FI-00076 Aalto (Finland)

    2016-11-20

    Mechanical properties and strain hardening of two pilot-scale lean-alloyed ferritic-austenitic stainless steels having metastable austenite phase, present at 0.50 and 0.30 volume fractions, have been studied by means of tensile testing and nanoindentation. These ferritic-austenitic stainless steels have high strain-hardening capacity, due to the metastable austenite phase, which leads to an improved uniform elongation and higher tensile strength in comparison with most commercial lean duplex stainless steels. According to the results, even as low as 0.30 volume fraction of austenite seems efficient for achieving nearly 40% elongation. The austenite phase is initially the harder phase, and exhibits more strain hardening than the ferrite phase. The rate of strain hardening and the evolution of the martensite phase were found to depend on the loading direction: both are higher when strained in the rolling direction as compared to the transverse direction. Based on the mechanical testing, characterization of the microstructure by optical/electron microscopy, magnetic balance measurements and EBSD texture analysis, this anisotropy in mechanical properties of the cold-rolled metastable ferritic-austenitic stainless steels can be explained by the elongated dual-phase microstructure, fiber reinforcement effect of the harder austenite phase and the presence and interplay of rolling textures in the two phases.

  10. Tribological study in roll forming of lean duplex stainless steel sheets

    DEFF Research Database (Denmark)

    Nielsen, Peter Søe; Nielsen, Morten Strogaard; Bay, Niels

    2012-01-01

    . Production tests show that galling can be a problem but pick-up formation on the tools seems to reach a consistent level. Improvements to tool surfaces and lubricant quality are proposed with a view to optimizing the tribo-system in order to increase the produced length before galling initiates and tool...... are relatively low and surface expansion is more or less non-existent, long roll forming production runs imply large sliding/contact lengths due to relative movement between steel strip and rolls. This requires an efficient tribological system to prevent pick-up formation on the forming tools. The present work...... focus on tribological issues are galling and pick-up formation as well as tool life in roll forming of stainless duplex steel sheets. The roll forming process is exemplified by production of an s-shaped profile used in interlock carcass production for flexible pipes used in off-shore oil extraction...

  11. 75 FR 32160 - Certain Hot-Rolled Flat-Rolled Carbon-Quality Steel Products from Brazil: Extension of Time Limit...

    Science.gov (United States)

    2010-06-07

    ...-Rolled Carbon-Quality Steel Products from Brazil: Extension of Time Limit for Preliminary Results of...-quality steel products from Brazil. See Agreement Suspending the Countervailing Duty Investigation on Hot... duty order on certain hot-rolled flat-rolled carbon-quality steel products from Brazil. See Initiation...

  12. Effect of cold-rolling on pitting corrosion of 304 austenitic stainless steel

    International Nuclear Information System (INIS)

    Peguet, L.; Malki, B.; Baroux, B.

    2004-01-01

    Full text of publication follows: This paper deals with a not very often investigated topic on relation between cold-working and stainless steels localized corrosion resistance. It is devoted to the study of the cold-rolling effects on the pitting corrosion behavior of a 304 stainless steel grade in chloride containing aqueous electrolytes. It focus particularly on the analysis of metastable pitting transients observed at Open Circuit Potential using an experimental protocol including two identical working electrodes connected through a zero-impedance. As received the used specimens were heat-treated at 1100 C for 30 s and cold-rolled at 10%, 20%, 30% up to a final reduction pass of 70% inducing a large amount of α'-martensite. Then, current-potential fluctuations measurements were performed at OCP in NaCl 0.1 M + FeCl 3 2.10 -4 M containing aqueous solution during 24 h from the immersion time. As expected, a detrimental effect on corrosion behavior induced by cold rolling has been confirmed. Surprisingly, this is a nonlinear effect as a function of cold-rolling rate which controverts the hypothesis that strain induced martensite is the principal factor to explain this kind of sensibilizing. In particular, the results show a maximum of the metastable pits initiation frequency at 20% of cold-rolling rate. Moreover, the passive film/electrochemical double layer resistance and capacity deduced from the transients study show an analog nonlinear behavior. So, the transfer resistance show a minimum around 10-20% of cold-rolling rate where one can assume an increase of the electrons transfer kinetics through the interface. Conversely, the interfacial capacity is the highest at 20% of cold-rolling rate. Finally, It is expected a combined effect of the cold-rolled induced martensite and the dislocations arrangement via the mechano-chemical theory discussed by Gutman. (authors)

  13. 75 FR 77828 - Certain Hot-Rolled Flat-Rolled Carbon-Quality Steel Products From Brazil: Extension of Time Limit...

    Science.gov (United States)

    2010-12-14

    ...-Rolled Carbon-Quality Steel Products From Brazil: Extension of Time Limit for Final Results of...-Rolled Carbon Quality Steel Products From Brazil: Preliminary Results of Countervailing Duty... administrative review of the countervailing duty order on certain hot-rolled flat-rolled carbon- quality steel...

  14. The Corrosion Behavior of Cold-Rolled 304 Stainless Steel In Salt Spray Environments

    International Nuclear Information System (INIS)

    Chiang, M.F.; Young, M.C.; Huang, J.Y.

    2011-01-01

    Saline corrosion is one of the major degradation mechanisms for stainless steel type 304 (SS304) dry storage cask during the spent fuel interim storage period. Slow strain rate test (SSRT) and neutral salt spray test (NSS) were performed at 85 degrees Celsius and 200 degrees Celsius with 0.5 wt% sodium chloride mist sprayed on the cold-rolled SS304 specimens of different degrees of reduction in this study. The weight changes of the NSS specimens tested at 85 degrees Celsius for 2000 hours differed greatly from those at 200 degrees Celsius. The weight loss of NSS specimens was not significant at 85 degrees Celsius but the weight gain decreased gradually with increasing the cold-rolled reduction. The yield strength (YS) and ultimate tensile stress (UTS) values obtained from the SSRT tests for lightly cold-rolled specimens in the salt spray environment at 85 degrees Celsius and 200 degrees Celsius are slightly lower than in air. But for those with 20% reductions, the specimen strengths were no longer changed by the saline corrosion. The preliminary results demonstrated that the quality and performance of cold-rolled SS304 is acceptable for fabrication of dry storage casks. However, more work on the corrosion behavior of cold-rolled stainless steel in the saline atmosphere is needed to better understand its long-term performance.

  15. 78 FR 11901 - Hot-Rolled Steel Products From China, India, Indonesia, Taiwan, Thailand, and Ukraine; Notice of...

    Science.gov (United States)

    2013-02-20

    ... 906-908 (Second Review)] Hot-Rolled Steel Products From China, India, Indonesia, Taiwan, Thailand, and... determine whether revocation of the countervailing duty orders on hot-rolled steel products from India, Indonesia, and Thailand and the revocation of the antidumping duty orders on hot-rolled steel products from...

  16. Hot compression deformation behavior of AISI 321 austenitic stainless steel

    Science.gov (United States)

    Haj, Mehdi; Mansouri, Hojjatollah; Vafaei, Reza; Ebrahimi, Golam Reza; Kanani, Ali

    2013-06-01

    The hot compression behavior of AISI 321 austenitic stainless steel was studied at the temperatures of 950-1100°C and the strain rates of 0.01-1 s-1 using a Baehr DIL-805 deformation dilatometer. The hot deformation equations and the relationship between hot deformation parameters were obtained. It is found that strain rate and deformation temperature significantly influence the flow stress behavior of the steel. The work hardening rate and the peak value of flow stress increase with the decrease of deformation temperature and the increase of strain rate. In addition, the activation energy of deformation ( Q) is calculated as 433.343 kJ/mol. The microstructural evolution during deformation indicates that, at the temperature of 950°C and the strain rate of 0.01 s-1, small circle-like precipitates form along grain boundaries; but at the temperatures above 950°C, the dissolution of such precipitates occurs. Energy-dispersive X-ray analyses indicate that the precipitates are complex carbides of Cr, Fe, Mn, Ni, and Ti.

  17. Influence of ring growth rate on damage development in hot ring rolling

    NARCIS (Netherlands)

    Wang, C.; Geijselaers, H. J.M.; Omerspahic, E.; Recina, V.; van den Boogaard, A. H.

    2015-01-01

    As an incremental forming process of bulk metal, ring rolling provides a cost effective process route to manufacture seamless rings. In the production of hot rolled rings, defects such as porosity can sometimes be found in high alloyed steel, manufactured from ingots having macro-segregation. For

  18. Hot forging of roll-cast high aluminum content magnesium alloys

    Science.gov (United States)

    Kishi, Tomohiro; Watari, Hisaki; Suzuki, Mayumi; Haga, Toshio

    2017-10-01

    This paper reports on hot forging of high aluminum content magnesium alloy sheets manufactured using horizontal twin-roll casting. AZ111 and AZ131 were applied for twin-roll casting, and a hot-forging test was performed to manufacture high-strength magnesium alloy components economically. For twin-roll casting, the casting conditions of a thick sheet for hot forging were investigated. It was found that twin-roll casting of a 10mm-thick magnesium alloy sheet was possible at a roll speed of 2.5m/min. The grain size of the cast strip was 50 to 70µm. In the hot-forging test, blank material was obtained from as-cast strip. A servo press machine with a servo die cushion was used to investigate appropriate forging conditions (e.g., temperature, forging load, and back pressure) for twin-roll casts (TRCs) AZ111 and AZ131. It was determined that high aluminum content magnesium alloy sheets manufactured using twin-roll casting could be forged with a forging load of 150t and a back pressure of 3t at 420 to 430°C. Applying back pressure during hot forging effectively forged a pin-shaped product.

  19. Improvement of impact toughness by modified hot working and heat treatment in 13%Cr martensitic stainless steel

    Energy Technology Data Exchange (ETDEWEB)

    Srivatsa, Kulkarni, E-mail: srivatsa.kulkarni@kcssl.com; Srinivas, Perla; Balachandran, G.; Balasubramanian, V.

    2016-11-20

    Improvement of the general mechanical properties and in particular sub-zero impact toughness in a 0.2%C-13%Cr martensitic stainless steel has been explored by varying the hot deformation and heat treatment conditions. The deformation conditions include hot rolling an ingot in one case and cogging the ingot to a semis followed by hot rolling in another case. The bars made from both routes were subjected to a single hardening heat treatment at 980 °C and 1040 °C oil quenched and a double hardening heat treatment at 1040 °C followed by 980 °C oil quenched. The hardened steels were subjected to a standard two stage tempering at 710 °C followed by 680 °C. The impact toughness was found to be doubled in the cogged and rolled steel in double hardened condition. Other processing conditions show varying impact toughness levels. The toughness observed was correlated to the grain size and the carbide distribution in the matrix and the fractography features.

  20. The Influence of Hot-Rolled Temperature on Plasma Nitriding Behavior of Iron-Based Alloys

    Science.gov (United States)

    El-Hossary, F. M.; Khalil, S. M.; Lotfy, Kh.; Kassem, M. A.

    2009-07-01

    Experiments were performed with an aim of studying the effect of hot-rolled temperature (600 and 900°C) on radio frequency (rf) plasma nitriding of Fe93Ni4Zr3 alloy. Nitriding was carried out for 10 min in a nitrogen atmosphere at a base pressure of 10-2 mbarr. Different continuous plasma processing powers of 300-550 W in steps 50 W or less were applied. Nitrided hot-rolled specimens were characterized by optical microscopy (OM), X-ray diffraction (XRD) and microhardness measurements. The results reveal that the surface of hot-rolled rf plasma nitrided specimens at 600°C is characterized with a fine microstructure as a result of the high nitrogen solubility and diffusivity. Moreover, the hot-rolled treated samples at 600°C exhibit higher microhardness value than the associated values of hot-rolled treated samples at 900°C. The enhancement of microhardness is due to precipitation and predominance of new phases ( γ and ɛ phases). Mainly, this conclusion has been attributed to the high defect densities and small grain sizes of the samples hot-rolled at 600°C. Generally, the refinement of grain size plays a dramatic role in improvement of mechanical properties of tested samples.

  1. Static recrystallisation and precipitation after hot deformation of austenitic stainless steels containing molybdenum and niobium

    International Nuclear Information System (INIS)

    Lombry, R.; Rossard, C.; Thomas, B.J.

    1981-01-01

    In general the hot workability of austenite depends on the work hardening during deformation and the kinetics of the dynamic and static restoration processes. Static recrystallisation is a very important factor in the case of hot rolling. The present work was undertaken to determine the effect of additions of molybdenum or niobium on the kinetics of static recrystallisation. The results show that the rate of static recrystallisation of type 304, 316 and 347 stainless steels decreases in this order for a given amount of prior deformation (epsilon=0,44). The differences in the rates of recrystallisation increases as the temperature is lowered towards 900 deg C. The effect of molybdenum appears to be attribuable to a solute drag effect on the mobility of dislocations, subgrain boundaries or grain boundaries whereas niobium additions lead to the formation of NbC precipitates on the dislocation cell walls and sub boundaries. It is also shown that in the case of type 316 and type 347 steels the dynamic recrystallisation process (observed in type 304 steels at all temperatures above 900 deg C) is replaced by dynamic recovery at temperatures egal to or below about 1000 deg C [fr

  2. Closure behavior of spherical void in slab during hot rolling process

    Science.gov (United States)

    Cheng, Rong; Zhang, Jiongming; Wang, Bo

    2018-04-01

    The mechanical properties of steels are heavily deteriorated by voids. The influence of voids on the product quality should be eliminated through rolling processes. The study on the void closure during hot rolling processes is necessary. In present work, the closure behavior of voids at the center of a slab at 800 °C during hot rolling processes has been simulated with a 3D finite element model. The shape of the void and the plastic strain distribution of the slab are obtained by this model. The void decreases along the slab thickness direction and spreads along the rolling direction but hardly changes along the strip width direction. The relationship between closure behavior of voids and the plastic strain at the center of the slab is analyzed. The effects of rolling reduction, slab thickness and roller diameter on the closure behavior of voids are discussed. The larger reduction, thinner slab and larger roller diameter all improve the closure of voids during hot rolling processes. Experimental results of the closure behavior of a void in the slab during hot rolling process mostly agree with the simulation results..

  3. Evolution of microstructure, macrotexture and microtexture during hot rolling of Ti-6Al-4V

    International Nuclear Information System (INIS)

    Ari-Gur, P.; Semiatin, S.L.

    1998-01-01

    The evolution of microstructure, macrotexture and microtexture during subtransus hot working of Ti-6Al-4V with two different types of transformed β starting microstructures (lamellar colony, acicular martensitic α) was investigated. Globularization of the transformed microstructures required heavy rolling reductions or moderate reductions coupled with near transus post-rolling heat treatment. Despite the sluggish dynamic globularization kinetics, noticeable macrotexture changes were noted after low reductions, an effect ascribed to the rotations associated with kinking and bending of the lamellar acicular plates. Noticeable microtextures, noted in samples with an initial lamellar colony microstructure, persisted through hot rolling suggesting that dynamic globularization does not involve recrystallization. In contrast, hot rolled material with a starting acicular α microstructure exhibited weak microtextures and strong macrotextures. The absence of microtexture in these latter cases was explained on the basis of multiple transformation variants within each colony/prior β grain following the β-annealing-and-water-quenching process used to obtain the microstructure. (orig.)

  4. Application of powder metallurgy and hot rolling processes for manufacturing aluminum/alumina composite strips

    Energy Technology Data Exchange (ETDEWEB)

    Zabihi, Majed, E-mail: m.zabihi@ma.iut.ac.ir [Department of Materials Engineering, Isfahan University of Technology, Isfahan 84156-83111 (Iran, Islamic Republic of); Toroghinejad, Mohammad Reza, E-mail: toroghi@cc.iut.ac.ir [Department of Materials Engineering, Isfahan University of Technology, Isfahan 84156-83111 (Iran, Islamic Republic of); Shafyei, Ali, E-mail: shafyei@cc.iut.ac.ir [Department of Materials Engineering, Isfahan University of Technology, Isfahan 84156-83111 (Iran, Islamic Republic of)

    2013-01-10

    In this study, aluminum matrix composites (AMC) with 2, 4, 6 and 10 wt% alumina were produced using powder metallurgy (PM), mechanical milling (MM) and vacuum hot pressing (VHP) techniques; then, this was followed by the hot-rolling process. During hot rolling, AMCs with 6 and 10 wt% Al{sub 2}O{sub 3} were fractured whereas strip composites with 2 and 4 wt% Al{sub 2}O{sub 3} were produced successfully. Microstructure and mechanical properties of the samples were investigated by optical and scanning electron microscopes and tensile and hardness tests, respectively. Microscopic evaluations of the hot-rolled composites showed a uniform distribution of alumina particles in the aluminum matrix. It was found that with increasing alumina content in the matrix, tensile strength (TS) and hardness increased and the percentage of elongation also decreased. Scanning electron microscope (SEM) was used to investigate aluminum/alumina interfaces and fracture surfaces of the hot rolled specimens after tensile test. SEM observations demonstrated that the failure mode in the hot-rolled Al-2 wt% Al{sub 2}O{sub 3} composite strips is a typical ductile fracture, while the failure mode was shear ductile fracture with more flat surfaces in Al-4 wt% Al{sub 2}O{sub 3} strips.

  5. Investigation of the effect of heat treatment on the structure of the cold-rolled ferrite stainless steels

    Directory of Open Access Journals (Sweden)

    В. Л. Грешта

    2015-03-01

    Full Text Available The work presents the estimation of a factor, namely, the solid solution super saturation by carbon and nitrogen on crystalline nature of high-chromium ferrite (HCF in defining the inhibition mechanism of recrystallization processes in ferritic stainless steel. The essence of the study was to conduct an additional heat treatment of hot (h/r tackle for the following modes: annealing 800 ° C - 4 hours, tempering with temperatures of 900, 1000, 1100 ° C after exposure to 1 min/mm. It is established that the determining factor that influences the amount of the carbide phase in c/r sheet is prior treatment of h/r tackle. A definite connection between the volume fraction of the secondary phase and the degree of cold deformation was observed. In the structure of cold-rolled sheet the same pattern with respect to the degree of implementation processes allocation of excess phases is maintained as in hot-rolled, after appropriate heat treatment. The smallest amount of the secondary phase structure was observed in the letter after hardening from 1100 °C - 1 min/mm. The reason is the thermodynamic state of HCF, to which at 1100 °C all the excess carbon and nitrogen must exist in solid solution. Thus, it is found that according to the present analysis of structural changes it should be noted that the best option of thermal prior treatment of h/r tackle is the annealing at 800 °C – 4 hours

  6. Cold rolling texture development of α/γ duplex stainless steels

    International Nuclear Information System (INIS)

    Akdut, N.; Foct, J.; Gottstein, G.

    1996-01-01

    The cold rolling texture development of two α/γ duplex stainless steels (DSS) with similar volume fractions of both phases but with totally different microstructures were investigated. Due to the limited number of available pole figures using X-rays, for the calculation of the ODFs both a direct method and a recent iterative series expansion method were used. The results were checked by neutron diffraction measurements. The austenitic phases of both DSS behave similarly to single phase materials with a low stacking fault energy which develop a brass-type rolling texture. In contrast, the texture development of the ferritic phases strongly differs from those of single phase ferrites. Instead of a fibre type texture the α-phase in both DSS exhibits a peak dominated texture regardless of whether it is the matrix phase or not. These differences, as well as the sharpness of both phases, are explained by the presence of the second phase. (orig.)

  7. Welding hot cracking in an austenitic stainless steel

    International Nuclear Information System (INIS)

    Kerrouault, N.

    2001-01-01

    The occurrence of hot cracking is linked to several conditions, in particular, the composition of the material and the local strains due to clambering. The aim of this study is to better analyse the implied mechanisms and to lead to a local thermomechanical criterion for hot cracking. The example studied is an AISI 321-type stainless steel (X10CrNiTi18-12) strongly prone to cracking. Two weldability tests are studied: - the first one consists in carrying out a fusion line by the TIG process on a thin sheet. In the case of the defect occurrence, the crack is longitudinal and follows the back of the molten bath. The influence of the operating conditions welding (speed, welding heat input, width test sample) is studied. - the second one is the Varestraint test. It is widely used to evaluate the sensitivity of a material to hot cracking. It consists in loading the material by bending during a fusion line by the TIG process and in characterising the defects quantity (length, number). Various thermal and mechanical instrumentation methods were used. The possibilities of a local instrumentation instrumentation being limited because of the melting, the experimental results were complemented by a numerical modelling whose aim is to simulate the thermomechanical evolution of the loading thanks to the finite element analysis code ABAQUS. First, the heat input for thermal simulation is set by the use of an inverse method in order to optimise the energy deposit mode during welding in the calculation. Then, the mechanical simulation needs the input of a constitutive law that fits the mechanical behaviour over a wide temperature range from ambient to melting temperature. Thus, a mechanical characterization is performed by selecting strain values and strain rates representative of what the material undergoes during the tests. The results come from tensile and compressive tests and allow to settle an elasto-visco-plastic constitutive law over temperatures up to liquidus. Once

  8. Rolling process simulation of a pair-crossed hot strip mill

    International Nuclear Information System (INIS)

    Chen Shaojie; Xu Jianzhong; Liu Xianghua; Wang Guodong

    2000-01-01

    Process simulation can help optimize the operating parameters aiming to improve the quality of rolled products. In this paper, software in Visual Basic language is developed to simulate the hot rolling process of a pair-crossed mill. The strip temperature is calculated by considering air cooling, water cooling, heat generation and conduction.The production parameters including rolling speeds, resistance to deformation, rolling forces, drive torques and powers are evaluated by mathematical models and their parameter identification support tools. The deformation of roll stack is calculated by influential function method. The roll temperature and expansion are calculated by finite differential method, and the roll wear is described by empirical formula. Based on these calculations as well as the effect of heredity is taken into account, the strip crown and flatness then can be obtained. The results show that the simulation software has friendly user interface, high accuracy and practicability. It can be served as a basis for the mill design and optimization of process parameters to acquire high quality of hot rolled strip. (author)

  9. Hot Roll Bonding of Aluminum to Twin-Roll Cast (TRC) Magnesium and Its Subsequent Deformation Behavior

    Science.gov (United States)

    Saleh, H.; Schmidtchen, M.; Kawalla, R.

    2018-02-01

    In an experiment in which twin-roll cast AZ31 magnesium alloy and commercial purity aluminum (AA 1050) sheets were bonded by hot rolling as Al/Mg/Al laminate composites, it was found that increasing the preheating temperatures up to 400 °C enhances the bonding strength of composites. Further increases in the preheating temperatures accelerate the magnesium oxide growth and thus reduce the bonding strength. The influence of the reduction ratio on the bonding properties was also studied, whereby it was observed that increasing the rolling reduction led to an increase in the bonding strength. The experimental results show that the optimum bonding strength can be obtained at rolling temperatures of 375-400 °C with a 50-60% reduction in thickness. On the other hand, the subsequent deformation behavior of composite was assessed using plane strain compression and deep drawing tests. We demonstrate that the composites produced using the optimum roll bonding conditions exhibited sufficient bonding during subsequent deformation and did not reveal any debonding at the bonding interface.

  10. 76 FR 31938 - Certain Hot-Rolled Carbon Steel Flat Products From India: Notice of Preliminary Results of 2009...

    Science.gov (United States)

    2011-06-02

    ... the File from Christopher Hargett, International Trade Compliance Analyst, through Melissa Skinner... Skinner, Office Director, concerning ``Certain Hot-Rolled Carbon Steel Flat Products from India: Customs...

  11. Cold rolled texture and microstructure in types 304 and 316L austenitic stainless steels

    International Nuclear Information System (INIS)

    Wasnik, D.N.; Samajdar, I.; Gopalakrishnan, I.K.; Yakhmi, J.V.; Kain, V.

    2003-01-01

    Two grades of austenitic stainless steel (ASS), types 304 (UNS S 30400) and 316L (UNS S 31603), were cold rolled to different reductions by unidirectional and by cross-rolling. The steels had reasonable difference in stacking fault energy (estimated respectively as 15 and 61 mJ/m 2 in types 304 and 316L) and also in starting (or pre-deformation) crystallographic texture-being relatively weak and reasonably strong in types 304 and 316L respectively. The cold rolling increased texturing in type 304, but not in type 316L ASS. The more significant effect of cold rolled texture development was in the relative increase of Brass ({011} ) against Copper ({112} ) and S ({231} ) orientations. In type 304 the increase in Brass was significant, while in type 316L the increase in Copper and S was stronger. This effect could be captured by Taylor type deformation texture simulations considering stronger twinning contributions in type 304 - for example the respective 'best-fits' (in terms of matching the changes in the volume fractions of Brass against Copper and S) were obtained by full constraint Taylor model with 1:100 and 1:10 slip:twin activities in types 304 and 316L ASS respectively. Microstructural developments during cold rolling were generalized as strain induced martensite formation and developments of dislocation substructure. The former, as estimated by vibrating sample magnetometer (VSM), increased with cold reduction, being significantly more in type 304 and was also noticeably stronger in both grades under cross-rolling. The most significant aspect of substructural developments was the formation of strain localizations. These were observed as dense dislocation walls (DDWs), micro-bands (MBs) and twin lamellar structures (TLS). The TLS contribution gained significance at higher reductions and during cross-rolling, especially in type 304. Large misorientation development and the accompanying grain splittings were always associated with such strain localizations

  12. Characterization of a hot-rolled Cu--Al--Ni--Ti shape memory alloy

    International Nuclear Information System (INIS)

    Segui, C.; Pons, J.; Cesari, E.

    1999-01-01

    The changes in the martensitic transformation of a Cu-Al-Ni-Ti alloy hot-rolled at different temperatures have been studied in detail, covering different aspects such as ageing in the parent phase at temperatures ranging between 250 and 350 o C, stabilisation of the martensite and betatization of the previously hot-rolled specimens. Besides the evolution of transformation temperatures upon different thermal treatments, special attention has been paid to the changes in mechanical properties of the alloy, such as elastic modulus and internal friction. These results are analysed in relation to the microstructural changes as observed by transmission electron microscopy. (orig.)

  13. Properties of Galvanized and Galvannealed Advanced High Strength Hot Rolled Steels

    Energy Technology Data Exchange (ETDEWEB)

    V.Y. Guertsman; E. Essadiqi; S. Dionne; O. Dremmailova; R. Bouchard; B. Voyzelle; J. McDermid; R. Fourmentin

    2008-04-01

    The objectives of the project were (i) to develop the coating process information to achieve good quality coatings on 3 advanced high strength hot rolled steels while retaining target mechanical properties, (ii) to obtain precise knowledge of the behavior of these steels in the various forming operations and (iii) to establish accurate user property data in the coated conditions. Three steel substrates (HSLA, DP, TRIP) with compositions providing yield strengths in the range of 400-620 MPa were selected. Only HSLA steel was found to be suitable for galnaizing and galvannealing in the hot rolled condition.

  14. Effects of hot rolled microstructure after twin-roll casting on microstructure, texture and magnetic properties of low silicon non-oriented electrical steel

    International Nuclear Information System (INIS)

    Liu, Hai-Tao; Wang, Yin-Ping; An, Ling-Zi; Wang, Zhao-Jie; Hou, Dao-Yuan; Chen, Jun-Mou; Wang, Guo-Dong

    2016-01-01

    In this work, a 0.71 wt%Si+0.44 wt%Al as-cast strip was produced by novel twin-roll casting. Some as-cast samples were respectively reheated and hot rolled at different temperatures in order to obtain different microstructure prior to cold rolling and annealing. The effects of the hot rolled microstructure on microstructure, texture evolution and magnetic properties were investigated in detail. A coarse deformed microstructure with λ-fiber texture was formed after hot rolling at 850–1050 °C, finally leading to an inhomogeneous recrystallization microstructure with strong λ-fiber, Goss and extremely weak γ-fiber texture. By contrast, a fine transformed microstructure was formed after hot rolling at 1150–1250 °C, finally leading to a fine and homogeneous recrystallization microstructure with stronger α-fiber, γ-fiber and much weaker λ-fiber texture. It should be noted that both the magnetic induction and core loss non-monotonically decreased or increased according to the hot rolling temperature. The unfavorable α-fiber and γ-fiber textures in the annealed sheets were much weaker than those of the conventional products regardless of the hot rolling temperature, thus contributing to a much higher magnetic induction. However, the average grain size in the annealed sheets was much lower than those of the conventional products regardless of the hot rolling temperature, thus leading to a higher core loss except the case of 1050 °C. Hence, it is underscored that better integrated magnetic properties than those of the conventional products can be obtained by optimizing the hot rolled microstructure to produce final desirable recrystallization microstructure and texture. - Highlights: • Non-oriented silicon steel was fabricated using twin-roll casting route. • Microstructure and texture evolution were clarified. • Effects of the hot rolled microstructure were investigated in detail. • Formation mechanism of the recrystallization texture was explored.

  15. Effects of hot rolled microstructure after twin-roll casting on microstructure, texture and magnetic properties of low silicon non-oriented electrical steel

    Energy Technology Data Exchange (ETDEWEB)

    Liu, Hai-Tao, E-mail: liuht@ral.neu.edu.cn; Wang, Yin-Ping; An, Ling-Zi; Wang, Zhao-Jie; Hou, Dao-Yuan; Chen, Jun-Mou; Wang, Guo-Dong

    2016-12-15

    In this work, a 0.71 wt%Si+0.44 wt%Al as-cast strip was produced by novel twin-roll casting. Some as-cast samples were respectively reheated and hot rolled at different temperatures in order to obtain different microstructure prior to cold rolling and annealing. The effects of the hot rolled microstructure on microstructure, texture evolution and magnetic properties were investigated in detail. A coarse deformed microstructure with λ-fiber texture was formed after hot rolling at 850–1050 °C, finally leading to an inhomogeneous recrystallization microstructure with strong λ-fiber, Goss and extremely weak γ-fiber texture. By contrast, a fine transformed microstructure was formed after hot rolling at 1150–1250 °C, finally leading to a fine and homogeneous recrystallization microstructure with stronger α-fiber, γ-fiber and much weaker λ-fiber texture. It should be noted that both the magnetic induction and core loss non-monotonically decreased or increased according to the hot rolling temperature. The unfavorable α-fiber and γ-fiber textures in the annealed sheets were much weaker than those of the conventional products regardless of the hot rolling temperature, thus contributing to a much higher magnetic induction. However, the average grain size in the annealed sheets was much lower than those of the conventional products regardless of the hot rolling temperature, thus leading to a higher core loss except the case of 1050 °C. Hence, it is underscored that better integrated magnetic properties than those of the conventional products can be obtained by optimizing the hot rolled microstructure to produce final desirable recrystallization microstructure and texture. - Highlights: • Non-oriented silicon steel was fabricated using twin-roll casting route. • Microstructure and texture evolution were clarified. • Effects of the hot rolled microstructure were investigated in detail. • Formation mechanism of the recrystallization texture was explored.

  16. Independency of Elasticity on Residual Stress of Room Temperature Rolled Stainless Steel 304 Plates for Structure Materials

    Directory of Open Access Journals (Sweden)

    Parikin Parikin

    2015-12-01

    Full Text Available Mechanical strengths of materials are widely expected in general constructions of any building. These properties depend on its formation (cold/hot forming during fabrication. This research was carried out on cold-rolled stainless steel (SS 304 plates, which were deformed to 0, 34, 84, and 152% reduction in thickness. The tests were conducted using Vickers method. Ultra micro indentation system (UMIS 2000 was used to determine the mechanical properties of the material, i.e.: hardness, modulus elasticity, and residual stresses. The microstructures showed lengthening outcropping due to stress corrosion cracking for all specimens. It was found that the tensile residual stress in a specimen was maximum, reaching 442 MPa, for a sample reducing 34% in thickness and minimum; and about 10 MPa for a 196% sample. The quantities showed that the biggest residual stress caused lowering of the proportional limit of material in stress-strain curves. The proportional modulus elasticity varied between 187 GPa and of about 215 GPa and was free from residual stresses.

  17. Influence of severe plastic deformation obtained by warm rolling on microstructure and mechanical properties of the ferritic stainless steel

    Energy Technology Data Exchange (ETDEWEB)

    Barbosa, Luana Alves; Campos, Wagner Reis Costa; Vilela, Jefferson José, E-mail: luana_alves_barbosa@hotmail.com, E-mail: wrrc@cdtn.br, E-mail: jjv@cdtn.br [Centro de Desenvolvimento da Tecnologia Nuclear (CDTN/CNEN-MG), Belo Horizonte, MG (Brazil); Miqueletti, Estevesson Ferreira; Mazzer, Eric Marchezini; Santos, Dagoberto B., E-mail: estevess@demet.ufmg.br, E-mail: marchezini@demet.ufmg.br, E-mail: dsantos@demet.ufmg.br [Universidade Federal de Minas Gerais (UFMG), Belo Horizonte, MG (Brazil)

    2017-07-01

    Generation IV reactors require research on new materials. For example, materials that will be used in the reactor vessel must be resistant to creep and have high toughness. Grain refining is a technique used to improve toughness. This grain refinement can be achieved by severe plastic deformation. In this work, the stainless steel 409 was used to simulate the EUROFER one type of ODS steel. The rolling process was applied to make the severe plastic deformation. The rolling was performed at 600°C which corresponds to the warm working condition in the absence of dynamic recrystallization. The rolling schedule studied allowed a logarithmic strain accumulation of 3.16. The rolled sheet had a yield stress of 822 MPa and a hardness of 302 HV. The grains became quite elongated characteristic of a severe plastic deformation. The recrystallization temperature of the rolled sheet was approximately 500°C. It was obtained by heat treatment and hardness measurement. (author)

  18. Influence of severe plastic deformation obtained by warm rolling on microstructure and mechanical properties of the ferritic stainless steel

    International Nuclear Information System (INIS)

    Barbosa, Luana Alves; Campos, Wagner Reis Costa; Vilela, Jefferson José; Miqueletti, Estevesson Ferreira; Mazzer, Eric Marchezini; Santos, Dagoberto B.

    2017-01-01

    Generation IV reactors require research on new materials. For example, materials that will be used in the reactor vessel must be resistant to creep and have high toughness. Grain refining is a technique used to improve toughness. This grain refinement can be achieved by severe plastic deformation. In this work, the stainless steel 409 was used to simulate the EUROFER one type of ODS steel. The rolling process was applied to make the severe plastic deformation. The rolling was performed at 600°C which corresponds to the warm working condition in the absence of dynamic recrystallization. The rolling schedule studied allowed a logarithmic strain accumulation of 3.16. The rolled sheet had a yield stress of 822 MPa and a hardness of 302 HV. The grains became quite elongated characteristic of a severe plastic deformation. The recrystallization temperature of the rolled sheet was approximately 500°C. It was obtained by heat treatment and hardness measurement. (author)

  19. Roll-to-roll hot embossing system with shape preserving mechanism for the large-area fabrication of microstructures

    Science.gov (United States)

    Peng, Linfa; Wu, Hao; Shu, Yunyi; Yi, Peiyun; Deng, Yujun; Lai, Xinmin

    2016-10-01

    Roll-to-roll (R2R) hot embossing is a promising approach to fulfilling the demands of high throughput fabrication of large-area polymeric components with micro-structure arrays which have been widely employed in the domains of optics, optoelectronics, biology, chemistry, etc. Nevertheless, the characteristic of continuous and fast forming for the R2R hot embossing process limits material flow during filling stage and results in significant springback during demolding stage. As a result, forming defects usually appear and the process window is very narrow which hinders the industrialization of this technology. This study developed a R2R hot embossing machine and proposed a shape preserving mechanism to extend the material filling time and realized the cooling effect during the demolding process. Comparative experiments were conducted on the R2R hot embossing process for micro-pyramid arrays to understand the effect of shape preserving mechanism. The influence of tension force and encapsulation angle to the forming quality was systematically analyzed. Furthermore, the influence of processing parameters has been investigated by using the one-variable-at-a-time method. Afterwards, a series of experiments based on the central composite design approach have been conducted for the analysis of variance and the establishment of empirical models of the R2R hot embossing process. As a result, the process window was extended by the shape preserving mechanism. More importantly, the feeding speed was improved from 0.5 m min-1 to 2.5 m min-1 for the large-area fabrication of micro-pyramid arrays, which is very attractive to the industrialization of this technology.

  20. Mechanical properties of CO2/MIG welded structural rolled steel and stainless steel

    International Nuclear Information System (INIS)

    Lim, Jong Young; Yoon, Myong Jin; Kim, Sang Youn; Kim, Tae Gyu; Shin, Hyeon Seung

    2015-01-01

    To accomplish long-term use of specific parts of steel, welding technology is widely applied. In this study, to compare the efficiency in improving mechanical properties, rolled steel (SS400) was welded with stainless steel (STS304) by both CO 2 welding method and MIG (metal inert gas) welding method, respectively. Multi-tests were conducted on the welded specimen, such as X-ray irradiation, Vickers' Hardness, tensile test, fatigue test and fatigue crack growth test. Based on the fatigue crack growth test performed by two different methods, the relationship of da/dN was analyzed. Although the hardness by the two methods was similar, tensile test and fatigue properties of MIG welded specimen are superior to CO 2 welded one.

  1. Structure and hot-rolled reinforcement rods properties evolution in the process of long service life

    International Nuclear Information System (INIS)

    Mikryukov, V.R.; Syomin, A.P.; Konovalov, S.V.; Ivanov, Yu.F.; Gromov, V.E.

    2006-01-01

    The physical nature of mechanical properties of hot-rolled reinforcement rods degradation during long-life operation is established by methods of transmission diffraction electron microscopy. It is shown that strength and plasticity properties decrease is due to cementite plates cutting and dissolution, microcracks formation process as a result of interstitial phase inclusions creation in the near-surface layer of material

  2. Structure and hot-rolled reinforcement rods properties evolution in the process of long service life

    Energy Technology Data Exchange (ETDEWEB)

    Mikryukov, V R [Siberian State Industrial University, Kirov str., 42. 654007, Novokuznetsk (Russian Federation); Syomin, A P [Siberian State Industrial University, Kirov str., 42. 654007, Novokuznetsk (Russian Federation); Konovalov, S V [Siberian State Industrial University, Kirov str., 42. 654007, Novokuznetsk (Russian Federation); Ivanov, Yu F [Siberian State Industrial University, Kirov str., 42. 654007, Novokuznetsk (Russian Federation); Gromov, V E [Siberian State Industrial University, Kirov str., 42. 654007, Novokuznetsk (Russian Federation)

    2006-08-25

    The physical nature of mechanical properties of hot-rolled reinforcement rods degradation during long-life operation is established by methods of transmission diffraction electron microscopy. It is shown that strength and plasticity properties decrease is due to cementite plates cutting and dissolution, microcracks formation process as a result of interstitial phase inclusions creation in the near-surface layer of material.

  3. 78 FR 24435 - Hot-Rolled Steel Products From China, India, Indonesia, Taiwan, Thailand, and Ukraine

    Science.gov (United States)

    2013-04-25

    ... Ukraine Scheduling of full five-year reviews concerning the countervailing duty orders on hot-rolled steel... China, India, Indonesia, Taiwan, Thailand, and Ukraine. AGENCY: United States International Trade..., India, Indonesia, Taiwan, Thailand, and Ukraine would be likely to lead to continuation or recurrence of...

  4. PERSPECTIVES OF MODERNIZATION OF WIRE MILL OF HOT ROLLING 150 AT RUP “BMZ”

    Directory of Open Access Journals (Sweden)

    A. V. Gontarj

    2004-01-01

    Full Text Available The offered modernization of the mill presumes the increase of capacity of the small-sort wire mill of hot milling 150 approximately till 40% at reduction of cost of the produced on it rolled wire by 15%, that will allow in future as well to grow the volumes of hardware production.

  5. Texture evolution of experimental silicon steel grades. Part I: Hot rolling

    Energy Technology Data Exchange (ETDEWEB)

    Sandoval Robles, J.A., E-mail: jsandoval.uanl@yahoo.com [Universidad Autónoma de Nuevo León, Facultad de Ingeniería Mecánica y Eléctrica, Ave. Universidad S/N, Cd. Universitaria, San Nicolás de los Garza, Nuevo León C.P. 66450 (Mexico); Salas Zamarripa, A.; Guerrero Mata, M.P. [Universidad Autónoma de Nuevo León, Facultad de Ingeniería Mecánica y Eléctrica, Ave. Universidad S/N, Cd. Universitaria, San Nicolás de los Garza, Nuevo León C.P. 66450 (Mexico); Cabrera, J. [Universitat Politècnica de Catalunya, Departament de Ciència dels Materials I Enginyeria Metal-lúrgica, Av. Diagonal 647, Barcelona 08028 (Spain)

    2017-05-01

    The metallurgical understanding of the deformation processes during the fabrication of non-oriented electrical steels plays a key role in improving their final properties. Texture control and optimization is critical in these steels for the enhancement of their magnetic properties. The aim of the present work is to study the texture evolution of six non-oriented experimental silicon steel grades during hot rolling. These steels were low carbon steel with a silicon content from 0.5 to 3.0 wt%. The first rolling schedule was performed in the austenitic (γ-Fe) region for the steel with a 0.5 wt% of silicon content, while the 1.0 wt% silicon steel was rolled in the two-phase (α+γ) region. Steels with higher silicon content were rolled in the ferritic (α-Fe) region. The second rolling schedule was performed in the α-Fe region. Samples of each stage were analyzed by means of Electron Backscatter Diffraction (EBSD). Findings showed that the texture was random and heterogeneous in all samples after 60% of rolling reduction, which is due to the low deformation applied during rolling. After the second rolling program, localized deformation and substructured grains near to surface were observed in all samples. The Goss {110}<001>texture-component was found in the 0.5 and 1.0 wt.-%silicon steels. This is due to the thermomechanical conditions and the corresponding hot band microstructure obtained after the first program. Moreover, the α<110>//RD and the γ <111>//ND fiber components of the texture presented a considerable increment as the silicon content increases. Future research to be published soon will be related to the texture evolution during the cold-work rolling process. - Highlights: • We analyze six silicon steel experimental grades alloys trough the rolling process. • Material was subjected to a hot deformation process in the α-γ region. • No recrystalization was observed during-after the rolling schedules. • Rise of the magnetic texture components

  6. Effect of asymmetric hot rolling on texture, microstructure and magnetic properties in a non-grain oriented electrical steel

    Energy Technology Data Exchange (ETDEWEB)

    Chen, S., E-mail: Shangping.chen@tatasteel.com [Tata Steel, 1970 CA IJmuiden (Netherlands); Butler, J. [Tata Steel, S60 3AR South Yorkshire (United Kingdom); Melzer, S. [Tata Steel, 1970 CA IJmuiden (Netherlands)

    2014-11-15

    In this study, both asymmetric hot rolling (AHR) and conventional hot rolling (CHR) were carried out to study the effect of the hot rolling conditions on the evolution of the texture and microstructure in a non-grain oriented (NGO) steel. The microstructure and texture in the subsequent processing stages were characterised and related to the final magnetic properties. The results show that AHR, compared with CHR, tends to homogenise texture through thickness of the hot band strips. AHR results in a higher fraction of the θ-fibre ({0 0 1}) and a lower fraction of the γ-fibre ({1 1 1}) in the hot band strips, which are favourable features in relation to the magnetic properties of the strip. However, the favourable features observed in hot rolled AHR strips are eliminated after cold rolling and annealing. Contrarily, the required θ-fibre is decreased and the unwanted γ-fibre is intensified in the AHR sheet after cold rolling and their strength is maintained in the subsequent process steps. On the other hand, AHR does not produce a discernible change in the grain size in the hot band annealed strip and in the final annealed sheet, except that the magnetic anisotropy in the AHR is improved after skin pass and extra annealing as the result of the redistribution of the texture components within the θ-fibre, no significant improvement of the magnetic properties as a direct consequence of the application of asymmetric hot rolling has been observed under the current AHR experimental conditions. - Highlights: • Asymmetrical hot rolling (AHR) produces more uniform distribution of texture through the thickness of the hot rolled strips and of the hot band annealed strips when compared with conventional hot rolling (CHR). • AHR results in a higher fraction of the θ-fibre ({0 0 1}) and a lower fraction of the γ-fibre ({1 1 1}) in the hot band strips. The θ-fibre is decreased but the γ-fibre is intensified in the AHR sheet after cold rolling

  7. Effect of asymmetric hot rolling on texture, microstructure and magnetic properties in a non-grain oriented electrical steel

    International Nuclear Information System (INIS)

    Chen, S.; Butler, J.; Melzer, S.

    2014-01-01

    In this study, both asymmetric hot rolling (AHR) and conventional hot rolling (CHR) were carried out to study the effect of the hot rolling conditions on the evolution of the texture and microstructure in a non-grain oriented (NGO) steel. The microstructure and texture in the subsequent processing stages were characterised and related to the final magnetic properties. The results show that AHR, compared with CHR, tends to homogenise texture through thickness of the hot band strips. AHR results in a higher fraction of the θ-fibre ({0 0 1}) and a lower fraction of the γ-fibre ({1 1 1}) in the hot band strips, which are favourable features in relation to the magnetic properties of the strip. However, the favourable features observed in hot rolled AHR strips are eliminated after cold rolling and annealing. Contrarily, the required θ-fibre is decreased and the unwanted γ-fibre is intensified in the AHR sheet after cold rolling and their strength is maintained in the subsequent process steps. On the other hand, AHR does not produce a discernible change in the grain size in the hot band annealed strip and in the final annealed sheet, except that the magnetic anisotropy in the AHR is improved after skin pass and extra annealing as the result of the redistribution of the texture components within the θ-fibre, no significant improvement of the magnetic properties as a direct consequence of the application of asymmetric hot rolling has been observed under the current AHR experimental conditions. - Highlights: • Asymmetrical hot rolling (AHR) produces more uniform distribution of texture through the thickness of the hot rolled strips and of the hot band annealed strips when compared with conventional hot rolling (CHR). • AHR results in a higher fraction of the θ-fibre ({0 0 1}) and a lower fraction of the γ-fibre ({1 1 1}) in the hot band strips. The θ-fibre is decreased but the γ-fibre is intensified in the AHR sheet after cold rolling

  8. Hot embossing holographic images in BOPP shrink films through large-area roll-to-roll nanoimprint lithography

    Energy Technology Data Exchange (ETDEWEB)

    Jiang, Menglin; Lin, Shiwei, E-mail: linsw@hainu.edu.cn; Jiang, Wenkai; Pan, Nengqian

    2014-08-30

    Highlights: • High-quality holographic images were replicated in large-area shrink film. • Surface morphology evolution was analyzed in films embossed at different temperatures. • Optical, mechanical, and thermal characteristics were systematically analyzed. - Abstract: Diffraction grating-based holographic images have been successfully replicated in biaxially oriented polypropylene (BOPP) shrink films through large-area roll-to-roll nanoimprint technique. Such hot embossing of holographic images on BOPP films represents a promising means of creating novel security features in packaging applications. The major limitation of the high-quality replication is the relatively large thermal shrinkage of BOPP shrink film. However, although an appropriate shrinkage is demanded after embossing, over-shrinking not only causes distortion in embossed images, but also reduces the various properties of BOPP shrink films mainly due to the disappearance of orientation. The effects of embossing temperature on the mechanical, thermal and optical properties as well as polymer surface morphologies were systematically analyzed. The results show that the optimal process parameters are listed as follows: the embossing temperature at 104–110 °C, embossing force 6 kg/cm{sup 2} and film speed 32 m/min. The variation in flow behavior of polymer surface during hot embossing process is highly dependent on the temperature. In addition, the adhesion from the direct contact between the rubber press roller and polymer surfaces is suggested to cause the serious optical properties failure.

  9. A model for prediction of profile and flatness of hot and cold rolled flat products in four-high mills

    Science.gov (United States)

    Overhagen, Christian; Mauk, Paul Josef

    2018-05-01

    For flat rolled products, the thickness profile in the transversal direction is one of the most important product properties. For further processing, a defined crown of the product is necessary. In the rolling process, several mechanical and thermal influences interact with each other to form the strip shape at the roll gap exit. In the present analysis, a process model for rolling of strip and sheet is presented. The core feature of the process model is a two-dimensional stress distribution model based on von Karman's differential equation. Sub models for the mechanical influences of work roll flattening as well as work and backup roll deflection and the thermal influence of work roll expansion have been developed or extended. The two-dimensional stress distribution serves as an input parameter for the roll deformation models. For work roll flattening, a three-dimensional model based on the Boussinesq problem is adopted, while the work and backup roll deflection, including contact flattening is calculated by means of finite beam elements. The thermal work roll crown is calculated with help of an axisymmetric numerical solution of the heat equation for the work roll, considering azimuthal averaging for the boundary conditions at the work roll surface. Results are presented for hot rolling of a strip in a seven-stand finishing train of a hot strip mill, showing the calculated evolution of the strip profile. A variation of the strip profile from the first to the 20th rolled strip is shown. This variation is addressed to the progressive increase of work roll temperature during the first 20 strips. It is shown that a CVC® system can lead to improvements in strip profile and therefore flatness.

  10. Correlation between Fatigue Crack Growth Behavior and Fracture Surface Roughness on Cold-Rolled Austenitic Stainless Steels in Gaseous Hydrogen

    Directory of Open Access Journals (Sweden)

    Tai-Cheng Chen

    2018-03-01

    Full Text Available Austenitic stainless steels are often considered candidate materials for use in hydrogen-containing environments because of their low hydrogen embrittlement susceptibility. In this study, the fatigue crack growth behavior of the solution-annealed and cold-rolled 301, 304L, and 310S austenitic stainless steels was characterized in 0.2 MPa gaseous hydrogen to evaluate the hydrogen-assisted fatigue crack growth and correlate the fatigue crack growth rates with the fracture feature or fracture surface roughness. Regardless of the testing conditions, higher fracture surface roughness could be obtained in a higher stress intensity factor (∆K range and for the counterpart cold-rolled specimen in hydrogen. The accelerated fatigue crack growth of 301 and 304L in hydrogen was accompanied by high fracture surface roughness and was associated with strain-induced martensitic transformation in the plastic zone ahead of the fatigue crack tip.

  11. Study of the structure of intermetalics from Fe - Al system after the hot rolling

    Directory of Open Access Journals (Sweden)

    M. Jabłońska

    2015-10-01

    Full Text Available This paper presents the results of structure analysis of Fe - Al alloys after hot rolling deformation. Microstructure analysis were performed before and after deformation using a scanning transmission electron microscopy (STEM technique. The detailed quantities research of the structures was conducted using scanning electron microscopy (SEM equipped with the gun with cold field emission and the detector of electron back scattering diffraction (EBSD.

  12. Numerical simulation of springback of medium-thick plates in local hot rolling

    Directory of Open Access Journals (Sweden)

    XIE Dong

    2017-10-01

    Full Text Available [Objectives] In order to understand the factors of springback in the local hot rolling of medium-thick steel plates,[Methods] a 3D thermal-elastic-plastic analysis is conducted to investigate the factors affecting the amount of springback. Through a series of numerical analyses,the influence of deformation temperature,temperature field distribution,plate size and local loading are examined. [Results] The results show that when the deformation temperature exceeds a certain level at which material yield stress begins to decrease significantly,the springback will reduce markedly with the increase in temperature. Due to the distribution characteristics of the deformation area,the influence of temperature distribution on springback where the local deformation scale is larger is dominated by the three dimensions of temperature field distribution. Changes in the length and width of the plate have a certain influence on the springback,in which changes to the length of a plate where the local deformation scale is larger have a more obvious influence on springback. The springback of the plate decreases with the increase of local loading. [Conclusions] The results of this study can assist in the optimization of parameters in the automatic hot rolling of thick plates,while also having a basic guiding effect on the further study of springback in the local hot rolling of thick plates.

  13. Evolution of the texture, mechanical properties, and microstructure of Cu-2.7Be alloys during hot cross-rolling

    Energy Technology Data Exchange (ETDEWEB)

    Zhu, Daibo; Liu, Chuming; Liu, Yadi; Gao, Yonghao; Jiang, Shunong [Central South University, School of Materials Science and Engineering, Changsha (China); Han, Tan [Suzhou Kinkou Copper Industry Limited Liability Company, Taicang (China)

    2015-09-15

    The evolution of the microstructure and texture of Cu-2.7Be alloys during hot rolling was investigated and related to the mechanical properties of the resulting sheets. Hot cross-rolling is shown to be an effective way to refine the hard and brittle secondary-phase particles in Cu-2.7Be alloys. The Cu- and brass-type textures increase and decrease in prevalence, respectively, during the rolling process. The yield strengths along the first and second rolling directions, and 45 to the former, are all enhanced because the corresponding Schmid factors decrease as the sheets are rolled thinner. The ductility anisotropy of the as-rolled sheets is related to the distribution and shape of the secondary-phase particles therein. (orig.)

  14. 76 FR 48143 - Certain Hot-Rolled Carbon Steel Flat Products From the People's Republic of China: Preliminary...

    Science.gov (United States)

    2011-08-08

    ..., 75 FR 81565 (December 28, 2010). \\3\\ Certain Oil Country Tubular Goods from the People's Republic of..., from Steven Hampton, International Trade Analyst, ``Certain Hot-Rolled Carbon Steel Flat Products from...

  15. Characterization of a cold-rolled 2101 lean duplex stainless steel.

    Science.gov (United States)

    Bassani, Paola; Breda, Marco; Brunelli, Katya; Mészáros, Istvan; Passaretti, Francesca; Zanellato, Michela; Calliari, Irene

    2013-08-01

    Duplex stainless steels (DSS) may be defined as a category of steels with a two-phase ferritic-austenitic microstructure, which combines good mechanical and corrosion properties. However, these steels can undergo significant microstructural modification as a consequence of either thermo-mechanical treatments (ferrite decomposition, which causes σ- and χ-phase formation and nitride precipitation) or plastic deformation at room temperature [austenite transformation into strain-induced martensite (SIM)]. These secondary phases noticeably affect the properties of DSS, and therefore are of huge industrial interest. In the present work, SIM formation was investigated in a 2101 lean DSS. The material was subjected to cold rolling at various degrees of deformation (from 10 to 80% thickness reduction) and the microstructure developed after plastic deformation was investigated by electron backscattered diffraction, X-ray diffraction measurements, and hardness and magnetic tests. It was observed that SIM formed as a consequence of deformations higher than ~20% and residual austenite was still observed at 80% of thickness reduction. Furthermore, a direct relationship was found between microstructure and magnetic properties.

  16. Effects of interface roughness on the annealing behaviour of laminated Ti-Al composite deformed by hot rolling

    DEFF Research Database (Denmark)

    Du, Y.; Fan, G.H.; Yu, Tianbo

    2015-01-01

    A laminated Ti-Al composite has been fabricated by hot compaction and hot rolling of alternate layers of commercial purity Ti and Al sheets with a thickness of 200 μm. The hot compaction temperature was 500˚C and in a following step the composite has been reduced 50% in thickness by hot rolling....... The fully consolidated composite has been annealed at 300˚C and 500˚C for different length of time. As a result of the differences in crystal structure and mechanical properties between Ti and Al protrusions and retrusions formed at the interface. A heterogeneous interface has thereby been created...

  17. High thermal shock resistance of the hot rolled and swaged bulk W–ZrC alloys

    Energy Technology Data Exchange (ETDEWEB)

    Xie, Z.M.; Liu, R.; Miao, S.; Yang, X.D. [Key Laboratory of Materials Physics, Institute of Solid State Physics, Hefei Science Center, Chinese Academy of Sciences, Hefei 230031 (China); University of Science and Technology of China, Hefei 230026 (China); Zhang, T., E-mail: zhangtao@issp.ac.cn [Key Laboratory of Materials Physics, Institute of Solid State Physics, Hefei Science Center, Chinese Academy of Sciences, Hefei 230031 (China); University of Science and Technology of China, Hefei 230026 (China); Fang, Q.F.; Wang, X.P. [Key Laboratory of Materials Physics, Institute of Solid State Physics, Hefei Science Center, Chinese Academy of Sciences, Hefei 230031 (China); University of Science and Technology of China, Hefei 230026 (China); Liu, C.S., E-mail: csliu@issp.ac.cn [Key Laboratory of Materials Physics, Institute of Solid State Physics, Hefei Science Center, Chinese Academy of Sciences, Hefei 230031 (China); University of Science and Technology of China, Hefei 230026 (China); Lian, Y.Y. [Southwestern Institute of Physics, Chengdu (China); Liu, X., E-mail: xliu@swip.ac.cn [Southwestern Institute of Physics, Chengdu (China); Luo, G.N. [Institute of Plasma Physics, Chinese Academy of Sciences, Hefei 230031 (China)

    2016-02-15

    The thermal shock (single shot) resistance and mechanical properties of the W–0.5wt% ZrC (WZC) alloys manufactured by ordinary sintering followed by swaging or rolling process were investigated. No cracks or surface melting were detected on the surface of the rolled WZC alloy plates after thermal shock at a power density of 0.66 GW/m{sup 2} for 5 ms, while primary intergranular cracks appear on the surface of the swaged WZC samples after thermal shock at a power density of 0.44 GW/m{sup 2} for 5 ms. Three point bending tests indicate that the rolled WZC alloy has a flexural strength of ∼2.4 GPa and a total strain of 1.8% at room temperature, which are 100% and 260% higher than those of the swaged WZC, respectively. The fracture energy density of the rolled WZC alloy is 3.23 × 10{sup 7} J/m{sup 3}, about 10 times higher than that of the swaged WZC (2.9 × 10{sup 6} J/m{sup 3}). The high thermal shock resistance of the rolled WZC alloys can be ascribed to their extraordinary ductility and plasticity. - Graphical abstract: (Left panel) surface morphology observed by optical microscope after a single pulse for 5 ms with various absorbed power densities at RT on the rolled WZC. (Right panel) curves of flexural stress versus strain at RT (a) and the calculated fracture energy (b) for the swaged WZC and rolled WZC alloys. - Highlights: • No cracks or surface melting were detected on the rolled WZC alloy samples after thermal shock at 0.66 GW/m{sup 2} for 5 ms. • Hot rolled WZC alloy plates exhibit a flexural strength of 2.4 GPa and a strain of 1.8% at RT. • The fracture energy of the rolled WZC alloy is 3.23 × 10{sup 7} J/m{sup 3} at RT, about 10 times higher than that of the swaged WZC. • A detailed analysis of the relationships between the mechanical properties and the thermal shock resistance is given.

  18. The influence of delta ferrite in the AISI 416 stainless steel hot workability

    International Nuclear Information System (INIS)

    Cardoso, P.H.S.; Kwietniewski, C.; Porto, J.P.; Reguly, A.; Strohaecker, T.R.

    2003-01-01

    Delta ferrite in martensitic stainless steels may have an adverse effect on the mechanical properties of these materials at high temperature. The occurrence of such phase is determined by the material chemical composition (mainly Cr and C), as-received microstructure condition and hot working temperature. The aim of this investigation is to assess the influence of delta ferrite on the hot workability of the martensitic AISI 416 stainless steel. Hence, different heats of this material (differing in chemical composition and as-received microstructure) were submitted to heating tests in order to observe the microstructural transformations that take place at high temperature and then examine the influence of these transformations on the mechanical behaviour. Phase characterisation and quantification were carried out using scanning electron microscopy/energy-dispersive X-ray microanalysis and image analysis. The heating tests were performed in the temperature range of 1100-1350 deg. C and hot workability in two heats with different delta ferrite content was assessed by hot torsion tests in the temperature range of 1000-1250 deg. C. The results have indicated that chemical composition and as-received microstructure strongly affect delta ferrite formation, which in turn deteriorates hot workability of the martensitic AISI 416 stainless steel

  19. Experimental and numerical approaches to studying hot cracking in stainless steel welds

    International Nuclear Information System (INIS)

    Le, Minh

    2014-01-01

    This work concerns experimental and numerical approaches to studying hot cracking in welds in stainless steel. Metallurgical weldability of two filler products used for the welding of an AISI-316L(N) austenitic stainless steel grade is evaluated. These filler metals are distinguished by their solidification microstructures: austeno-ferritic for the 19Cr-12Ni-2Mo grade and austenitic for the 19-15H Thermanit grade. The study of weldability concerns the assessment of the susceptibility to hot cracking of these three alloys, the proposition of a hot cracking criterion, and the evaluation of its transferability to structure-scale tests. Hot cracks are material separations occurring at high temperatures along the grain boundaries (dendrite boundaries), when the level of strain and the strain rate exceed a certain level. The hot cracks studied are formed during solidification from the liquid phase of weld metals. The bibliography study brings to the fore the complexity of initiation and propagation mechanisms of these material separations. Three types of tests are studied in this work: hot cracking tests, such as trapezoidal and Varestraint tests, allowing to initiate the phenomenon in controlled experimental conditions, and tests on the Gleeble thermomechanical simulator for thermomechanical (materials behavior laws, fracture properties) and metallurgical (brittle temperature range (BTR), evolution of delta ferrite) characterizations of the alloys. All these tests on the three materials were analyzed via numerical modeling and simulations implemented in the Cast3M finite element code in order to bring out a thermomechanical hot cracking criterion. (author) [fr

  20. Hot Corrosion Behavior of Stainless Steel with Al-Si/Al-Si-Cr Coating

    Science.gov (United States)

    Fu, Guangyan; Wu, Yongzhao; Liu, Qun; Li, Rongguang; Su, Yong

    2017-03-01

    The 1Cr18Ni9Ti stainless steel with Al-Si/Al-Si-Cr coatings is prepared by slurry process and vacuum diffusion, and the hot corrosion behavior of the stainless steel with/without the coatings is studied under the condition of Na2SO4 film at 950 °C in air. Results show that the corrosion kinetics of stainless steel, the stainless steel with Al-Si coating and the stainless steel with Al-Si-Cr coating follow parabolic laws in several segments. After 24 h corrosion, the sequence of the mass gain for the three alloys is the stainless steel with Al-Si-Cr coating coating coating. The corrosion products of the three alloys are layered. Thereinto, the corrosion products of stainless steel without coating are divided into two layers, where the outside layer contains a composite of Fe2O3 and FeO, and the inner layer is Cr2O3. The corrosion products of the stainless steel with Al-Si coating are also divided into two layers, of which the outside layer mainly consists of Cr2O3, and the inner layer is mainly SiO2. The corrosion film of the stainless steel with Al-Si-Cr coating is thin and dense, which combines well with substrate. Thereinto, the outside layer is mainly Cr2O3, and the inside layer is Al2O3. In the matrix of all of the three alloys, there exist small amount of sulfides. Continuous and protective films of Cr2O3, SiO2 and Al2O3 form on the surface of the stainless steel with Al-Si and Al-Si-Cr coatings, which prevent further oxidation or sulfide corrosion of matrix metals, and this is the main reason for the much smaller mass gain of the two alloys than that of the stainless steel without any coatings in the 24 h hot corrosion process.

  1. Effects of Changing Hot Rolling Direction on Microstructure, Texture and Mechanical Properties of Cu-2.7Be Sheets

    Science.gov (United States)

    Zhu, Daibo; Liu, Chuming; Yu, Haijun; Han, Tan

    2018-03-01

    A hot rolling scheme (cross-rolling and unidirectional rolling) was adopted to process Cu-2.7Be sheets used as multiplier dynodes in photomultiplier. The effects of changing rolling direction on microstructure, texture and mechanical properties were studied by a combination of XRD, EBSD and TEM. It was found that higher copper-type texture and lower brass texture intensity were obtained in the ultimately cross-rolling (CR) sheet compared with the unidirectional rolling (UR) sheet.The EBSD results indicated that the grain orientation from mainly for UR sample turns to random for CR sample. Great enhancements in YS and UTS after unidirectional rolling were attributed to the massive and polygonal γ precipitates. The CR sample exhibited lower anisotropy, because of the increase of S and γ precipitates with spherical and tiny shape.

  2. Evolution of Oxide Inclusions in Si-Mn Killed Steels During Hot-Rolling Process

    Science.gov (United States)

    Yang, Wen; Guo, Changbo; Zhang, Lifeng; Ling, Haitao; Li, Chao

    2017-10-01

    The evolution of oxide inclusions in Si-Mn killed steels refined by slags of different basicity during a four-pass industrial hot-rolling process was investigated using an automated microscopy system. High-basicity refining slag induced the formation of CaO- and Al2O3-containing inclusions, while refining slag with 0.8 basicity induced dominant inclusions of SiO2 and MnO-SiO2. CaO-SiO2-Al2O3 inclusions mainly formed endogenously during solidification and cooling of Ca-containing steels, where Ca originated from slag-steel reactions. However, the larger-sized higher-CaO inclusions originated from slag entrainment. Different inclusions presented different hot-rolling behaviors. The inclusion composition changed by deformation and new phase formation. The dominant oxide types were unchanged under refinement by low-basicity slag; however, they changed under refinement with high-basicity slag. The deformation index of inclusions decreased with increasing accumulated reduction (AR) of the steel. The difference in deformation index between different inclusion types was the largest in the first rolling stage and decreased in subsequent stages. SiO2-CaO and SiO2-MnO-CaO inclusions had larger deformation indices during hot rolling but smaller indices in the last two stages. High-basicity slag increased inclusion complexity; from the perspective of cold-drawing performance, low-basicity refining slag is better for the industrial production of tire-cord steels.

  3. Simulation of accelerated strip cooling on the hot rolling mill run-out roller table

    International Nuclear Information System (INIS)

    Muhin, U.; Belskij, S.; Makarov, E.; Koinov, T.

    2013-01-01

    Full text: A mathematical model of the thermal state of the metal on the run-out roller table of a continuous wide hot-strip mill is presented. The mathematical model takes into account the heat generation during the polymorphic γ → α transformation of super cooled austenite phase and the influence of chemical composition on the physical properties of the steel. The model allows the calculation of modes of accelerated cooling of strips on the run-out roller table of a continuous wide hot strip mill. Winding temperature calculation error does not exceed 20 °C for 98.5 % of the strips from low-carbon and low-alloyed steels. key words: hot rolled, wide-strip, accelerated cooling, run-out roller table, polymorphic transformation, mathematical modeling

  4. Effect of Temperature on the Fracture Toughness of Hot Isostatically Pressed 304L Stainless Steel

    Science.gov (United States)

    Cooper, A. J.; Brayshaw, W. J.; Sherry, A. H.

    2018-03-01

    Herein, we have performed J- Resistance multi-specimen fracture toughness testing of hot isostatically pressed (HIP'd) and forged 304L austenitic stainless steel, tested at elevated (300 °C) and cryogenic (- 140 °C) temperatures. The work highlights that although both materials fail in a pure ductile fashion, stainless steel manufactured by HIP displays a marked reduction in fracture toughness, defined using J 0.2BL, when compared to equivalently graded forged 304L, which is relatively constant across the tested temperature range.

  5. Effect of Temperature on the Fracture Toughness of Hot Isostatically Pressed 304L Stainless Steel

    OpenAIRE

    Cooper, Adam J.; Sherry, Andrew

    2018-01-01

    Herein, we have performed J-Resistance multi-specimen fracture toughness testing of hot isostatically pressed (HIP’d) and forged 304L austenitic stainless steel, tested at elevated (300 °C) and cryogenic (− 140 °C) temperatures. The work highlights that although both materials fail in a pure ductile fashion, stainless steel manufactured by HIP displays a marked reduction in fracture toughness, defined using J0.2BL, when compared to equivalently graded forged 304L, which is relatively constant...

  6. Studies of Hot Crack Properties of Laser Welded Stainless Steel

    DEFF Research Database (Denmark)

    Juhl, Thomas Winther

    During the present work crack testing concerning small and fast solidifying laser welds in austenitic stainless steel has been studied. A set of methods has been applied to investigate alloy properties, including ·Application of known information to predict solidification phases from the alloy...... composition. ·Weld metal solidification rate measurements for prediction of phases. ·Various crack tests to assess the crack susceptibility of alloys. ·A combination of the above for selection of suitable, weldable alloys. The possibility of using such specific methods for alloys and applications has been...... to the crack behaviour, but do not show an expected correlation between the crack resistance and the solidification rate. The employment of pulsed seams is therefore assessed not to be usable in the present selection methods. From evaluation of several crack tests, the Weeter spot weld test has been chosen...

  7. Assessment of Hot Crack Properties of Laser Welded Stainless Steel

    DEFF Research Database (Denmark)

    Juhl, Thomas Winther; Olsen, Flemming Ove

    2003-01-01

    Crack testing concerning small and fast solidifying laser welds in austenitic stainless steel has been studied. A set of methods has been applied to investigate alloy properties, including (1) Application of known information to predict solidification phases, (2) Weld metal solidification rate...... crack tests, the Weeter spot weld test has been chosen to form a basis for the development of a practicable method to select specific alloys for welding applications. A new test, the Groove weld test was developed, which has reduced the time consumption and lightened the analysis effort considerably...... measurements for prediction of phases, (3) Various crack tests to assess the crack susceptibility of alloys and (4) A combination of the above for selection of suitable, weldable alloys. The possibility of using such specific methods for alloys and applications has been investigated and recommendations...

  8. Development and industrial mastering hot rolling procedure for low-ductile steels and alloys

    International Nuclear Information System (INIS)

    Degterenko, V.K.; Sokolov, V.A.

    1980-01-01

    The technique for the development of the sheet hot rolling procedure for low-ductile steels and alloys (0Kh17N14M2, 12Kh21N5T, 20Kh25N20C2,40Kh13, 36NKhTYu etc.) is proposed, using plastometer which permits to obtain the data on the deformation resistance in the wide range of temperatures (800-1300 deg C), of deformation degrees (0.1-0.3) and deformation rates (0.001-300 c -1 ). With the help of the plastometric data processed on the computer the calculation of the rolling regimes for the sheet with improved surface quality is carried out at the more uniform loading on the mill stands

  9. 75 FR 47541 - Hot-Rolled Flat-Rolled Carbon-Quality Steel Products from Brazil and Japan: Final Results of...

    Science.gov (United States)

    2010-08-06

    ... DEPARTMENT OF COMMERCE International Trade Administration [A-351-828, A-588-846] Hot-Rolled Flat..., Department of Commerce. SUMMARY: On April 1, 2010, the Department of Commerce (the Department) initiated... Department has conducted expedited (120-day) sunset reviews for both orders pursuant to 19 CFR 351.218(e)(1...

  10. THE METHOD OF ROLL SURFACE QUALITY MEASUREMENT FOR CONTINUOUS HOT DIP ZINC COATED STEEL SHEET PRODUCTION LINE

    Directory of Open Access Journals (Sweden)

    Ki Yong Choi

    2015-01-01

    Full Text Available The present paper describes a developed analyzing system of roll surface during the process of continuous hot dip zinc coated steel sheet production line, in particular, adhering problem by transferred inclusions from roll to steel sheet surface during annealing process so called the pickup. The simulated test machine for coated roll surface in processing line has been designed and performed. The system makes it possible to analyze roll surface condition according to pickup phenomena from various roll coatings concerning operating conditions of hearth rolls in annealing furnace. The algorithm of fast pickup detection on surface is developed on the base of processing of several optical images of surface. The parameters for quality estimation of surface with pickups were developed. The optical system for images registration and image processing electronics may be used in real time and embed in processing line.

  11. Evaluation of factors affecting the edge formability of two hot rolled multiphase steels

    Science.gov (United States)

    Mukherjee, Monideepa; Tiwari, Sumit; Bhattacharya, Basudev

    2018-02-01

    In this study, the effect of various factors on the hole expansion ratio and hence on the edge formability of two hot rolled multiphase steels, one with a ferrite-martensite microstructure and the other with a ferrite-bainite microstructure, was investigated through systematic microstructural and mechanical characterization. The study revealed that the microstructure of the steels, which determines their strain hardening capacity and fracture resistance, is the principal factor controlling edge formability. The influence of other factors such as tensile strength, ductility, anisotropy, and thickness, though present, are secondary. A critical evaluation of the available empirical models for hole expansion ratio prediction is also presented.

  12. Effect of hot rolling on the microstructure and mechanical properties of Ti3Al based dual phase alloys

    International Nuclear Information System (INIS)

    Wu, J.; Zhang, L.; Hua, W.; Qiu, G.

    1999-01-01

    Development of α 2 -Ti 3 Al based dual phase alloys have shown some promising potentials in property improvement by introducing Ti 5 Si 3 silicide phase into the matrix via Si alloying. However, the presence of coarse network of Ti 5 Si 3 phase formed by eutectic reaction in the as-cast state also embrittles the alloy. Both hot rolling and powder metallurgy are considered to be the possible ways to refine the Ti 5 Si 3 phase in the matrix. Two Ti-Al-Si-Nb alloys whose Si contents are 2 and 5 at.% respectively were arc melted into ingots and then hot rolled to sheets in this investigation. Optical metallographic examination correlates the microstructures of the as-cast and as-rolled alloys with the different rolling amounts, showing that the coarse silicide network is broken into small particles after hot rolling. Mechanical property testing from room temperature to 800 C indicates that the strength and plastic elongation of the hot-rolled alloys are much higher than those of the as-cast ones. The data obtained in this investigation are comparable with those obtained in the P/M processed specimens. Fracture surfaces of the alloys are also examined

  13. ABOUT RATIONING MAXIMUM ALLOWABLE DEFECT DEPTH ON THE SURFACE OF STEEL BILLETS IN PRODUCTION OF HOT-ROLLED STEEL

    Directory of Open Access Journals (Sweden)

    PARUSOV E. V.

    2017-01-01

    Full Text Available Formulation of the problem. Significant influence on the quality of rolled steel have various defects on its surface, which in its turn inherited from surface defects of billet and possible damage to the surface of rolled steel in the rolling mill line. One of the criteria for assessing the quality indicators of rolled steel is rationing of surface defects [1; 2; 3; 6; 7]. Current status of the issue. Analyzing the different requirements of regulations to the surface quality of the rolled high-carbon steels, we can conclude that the maximum allowable depth of defects on the surface of billet should be in the range of 2.0...5.0 mm (depending on the section of the billet, method of its production and further the destination Purpose. Develop a methodology for calculating the maximum allowable depth of defects on the steel billet surface depending on the requirements placed on the surface quality of hot-rolled steel. Results. A simplified method of calculation, allowing at the rated depth of defects on the surface of the hot-rolled steel to make operatively calculation of the maximum allowable depth of surface defects of steel billets before heating the metal in the heat deformation was developed. The findings shows that the maximum allowable depth of surface defects is reduced with increasing diameter rolled steel, reducing the initial section steel billet and degrees of oxidation of the metal in the heating furnace.

  14. Annealing effects on the microstructure and mechanical properties of hot-rolled 14Cr-ODS steel

    International Nuclear Information System (INIS)

    Gao, R.; Zhang, T.; Ding, H.L.; Jiang, Y.; Wang, X.P.; Fang, Q.F.; Liu, C.S.

    2015-01-01

    The oxide dispersion strengthened ferritic steels with nominal composition (weight percent) of Fe–14Cr–2W-0.5Ti-0.06Si-0.2V-0.1Mn-0.05Ta-0.03C-0.3Y_2O_3 were fabricated by sol–gel method, mechanical alloying, and hot isostatic pressing techniques. The evolution of microstructure and mechanical properties of the hot-rolled specimens with heat treatment was investigated. Tensile strength and hardness of hot-rolled ODS steel are significantly enhanced due to the formation of mechanical twins and high density dislocations. Uniformly dispersed oxide particles (10–40 nm) and fine-grained structure (200–400 nm) are responsible for the superior mechanical properties of the hot-rolled specimen annealed between 650 °C and 850 °C. With further increasing annealing temperature, the grain size of the hot-rolled specimens increases while the size of oxide particles decreases, which leads to lower strength and hardness but better ductility. The tensile strength and total elongation of samples in the rolling direction are higher than those in the transverse direction after the same treatments owing to the grain anisotropy induced by the large mechanical deformation.

  15. Annealing effects on the microstructure and mechanical properties of hot-rolled 14Cr-ODS steel

    Science.gov (United States)

    Gao, R.; Zhang, T.; Ding, H. L.; Jiang, Y.; Wang, X. P.; Fang, Q. F.; Liu, C. S.

    2015-10-01

    The oxide dispersion strengthened ferritic steels with nominal composition (weight percent) of Fe-14Cr-2W-0.5Ti-0.06Si-0.2V-0.1Mn-0.05Ta-0.03C-0.3Y2O3 were fabricated by sol-gel method, mechanical alloying, and hot isostatic pressing techniques. The evolution of microstructure and mechanical properties of the hot-rolled specimens with heat treatment was investigated. Tensile strength and hardness of hot-rolled ODS steel are significantly enhanced due to the formation of mechanical twins and high density dislocations. Uniformly dispersed oxide particles (10-40 nm) and fine-grained structure (200-400 nm) are responsible for the superior mechanical properties of the hot-rolled specimen annealed between 650 °C and 850 °C. With further increasing annealing temperature, the grain size of the hot-rolled specimens increases while the size of oxide particles decreases, which leads to lower strength and hardness but better ductility. The tensile strength and total elongation of samples in the rolling direction are higher than those in the transverse direction after the same treatments owing to the grain anisotropy induced by the large mechanical deformation.

  16. Development of high strength hot rolled low carbon copper-bearing steel containing nanometer sized carbides

    Energy Technology Data Exchange (ETDEWEB)

    Phaniraj, M.P. [High Temperature Energy Materials Research Center, Korea Institute of Science and Technology, Seoul 136-791 (Korea, Republic of); Shin, Young-Min [High Temperature Energy Materials Research Center, Korea Institute of Science and Technology, Seoul 136-791 (Korea, Republic of); Department of Materials Science and Engineering, Korea University, Seoul 136-701 (Korea, Republic of); Lee, Joonho [Department of Materials Science and Engineering, Korea University, Seoul 136-701 (Korea, Republic of); Goo, Nam Hoon [Sheet Product Design Group, Hyundai Steel Co., North Industrial Street 1400, 343-823, DangJin 343-823 (Korea, Republic of); Kim, Dong-Ik; Suh, Jin-Yoo; Jung, Woo-Sang [High Temperature Energy Materials Research Center, Korea Institute of Science and Technology, Seoul 136-791 (Korea, Republic of); Shim, Jae-Hyeok, E-mail: jhshim@kist.re.kr [High Temperature Energy Materials Research Center, Korea Institute of Science and Technology, Seoul 136-791 (Korea, Republic of); Choi, In-Suk, E-mail: insukchoi@kist.re.kr [High Temperature Energy Materials Research Center, Korea Institute of Science and Technology, Seoul 136-791 (Korea, Republic of)

    2015-05-01

    A low carbon ferritic steel was alloyed with Ti, Mo and Cu with the intention of achieving greater increment in strength by multiple precipitate strengthening. The steel is hot rolled and subjected to interrupted cooling to enable precipitation of Ti–Mo carbides and copper. Thermodynamic calculations were carried out to determine equilibrium phase fractions at different temperatures. Microstructure characterization using transmission electron microscopy and composition analysis revealed that the steel contains ~5 nm size precipitates of (Ti,Mo)C. Precipitation kinetics calculations using MatCalc software showed that mainly body centered cubic copper precipitates of size < 5nm form under the cooling conditions in the present study. The steel has the high tensile strength of 853 MPa and good ductility. The yield strength increases by 420 MPa, which is more than that achieved in hot rolled low carbon ferritic steels with only copper precipitates or only carbide precipitates. The precipitation and strengthening contribution of copper and (Ti,Mo)C precipitates and their effect on the work hardening behavior is discussed.

  17. Simulation-based prediction of hot-rolled coil forced cooling

    Energy Technology Data Exchange (ETDEWEB)

    Saboonchi, Ahmad [Department of Mechanical Engineering, Isfahan University of Technology, Isfahan 84154 (Iran); Hassanpour, Saeid [Rayan Tahlil Sepahan Co., Isfahan Science and Technology Town, Isfahan 84155 (Iran)

    2008-09-15

    Hot-rolled coils take a long time to cool under normal storehouse conditions due to their high mass. Hotter seasons will lead to even longer storage times and, thus, to shortage of space. Forced cooling methods such as water-immersion and water-spray can be employed to reduce hot-rolled coil cooling time. In this paper, a mathematical model of the thermal behavior of coils is developed to predict and to evaluate the results expected from employing these methods before any real changes can be made on the ground. The results obtained from the model were compared with those from various experiments to verify the model's accuracy. The cooling time was then computed based on changes effected in the boundary conditions appropriate to each of the forced cooling methods employed. Moreover, the savings in storage times were compared to identify the best cooling method. Predictions showed that water immersion at the beginning of cooling cycle was more effective and that the cycle should not exceed 1 h for cost efficiency considerations. When using nozzles to spray it was found that spraying water on end surfaces of coils would be the optimum option resulting in savings in time, water and energy, and with restricted temperature gradient. (author)

  18. Effect of roll hot press temperature on crystallite size of PVDF film

    Energy Technology Data Exchange (ETDEWEB)

    Hartono, Ambran, E-mail: ambranhartono@yahoo.com; Sanjaya, Edi [Departement of Physics Faculty of Science and Technology, Islamic State University Syarif Hidayatullah , Jl. Juanda 95 Ciputat Jakarta (Indonesia); Djamal, Mitra; Satira, Suparno; Bahar, Herman [Theoretical High Energy Physics and Instrumentation Group Research, Faculty Mathematics and Natural Sciences, Institut Teknologi Bandung, Jl. Ganesa 10 Bandung (Indonesia); Ramli [Departement of Physics, Faculty of Mathematics and Natural Sciences, Universitas Negeri Padang, Jl.Prof. Hamka, Padang 25131 (Indonesia)

    2014-03-24

    Fabrication PVDF films have been made using Hot Roll Press. Preparation of samples carried out for nine different temperatures. This condition is carried out to see the effect of Roll Hot Press temperature on the size of the crystallite of PVDF films. To obtain the diffraction pattern of sample characterization is performed using X-Ray Diffraction. Furthermore, from the diffraction pattern is obtained, the calculation to determine the crystallite size of the sample by using the Scherrer equation. From the experimental results and the calculation of crystallite sizes obtained for the samples with temperature 130 °C up to 170 °C respectively increased from 7.2 nm up to 20.54 nm. These results show that increasing temperatures will also increase the size of the crystallite of the sample. This happens because with the increasing temperature causes the higher the degree of crystallization of PVDF film sample is formed, so that the crystallite size also increases. This condition indicates that the specific volume or size of the crystals depends on the magnitude of the temperature as it has been studied by Nakagawa.

  19. Study of Microstructure of the Al-Fe Alloys After Hot Rolling Deformation

    Science.gov (United States)

    Jabłońska, Magdalena Barbara; Rodak, Kinga; Bednarczyk, Iwona

    The aim of the paper is a microstructure analysis of alloys from the Al-Fe system after hot rolling tests, conducted by using a scanning transmission electron microscopy STEM and scanning electron microscope equipped with EBSD detector. Hot rolling was carried out at Technical University of Ostrava, Faculty of Metallurgy and Material Engineering, Institute of Modelling and Control of Forming Processes. The samples were heated to a temperature of 1200°C. The EBSD and STEM techniques have been applied in order to determine the influence of chemical composition and deformation parameters on structural changes. The microstructure analysis has included parameters such us: grain/sub-grain size, area fraction of grains/subgrains, misorientation angles, grains/subgrains shape aspect ratio and dislocations structure. The research structure techniques in scanning-transmission electron microscopy revealed numerous FeAl28 alloy phase separations of secondary nucleating sites favoured energetically, which are the boundary of grains/subgrains and dislocations. These changes in the structure of the test results have been confirmed by EBSD, which revealed the presence of grains/subgrains misorientation angle boundaries above 15°.

  20. Precipitation Strengthening by Induction Treatment in High Strength Low Carbon Microalloyed Hot-Rolled Plates

    Science.gov (United States)

    Larzabal, G.; Isasti, N.; Rodriguez-Ibabe, J. M.; Uranga, P.

    2018-03-01

    The use of microalloyed steels in the production of thick plates is expanding due to the possibility of achieving attractive combinations of strength and toughness. As market requirements for high strength plates are increasing and new applications require reduced weight and innovative designs, novel approaches to attaining cost-effective grades are being developed. The mechanism of precipitation strengthening has been widely used in thin strip products, since the optimization of the coiling strategy offers interesting combinations in terms of final properties and microalloying additions. Precipitation strengthening in thick plates, however, is less widespread due to the limitation of interphase precipitation during continuous cooling after hot rolling. With the main objective of exploring the limits of this strengthening mechanism, laboratory thermomechanical simulations that reproduced plate hot rolling mill conditions were performed using low carbon steels microalloyed with Nb, NbMo, and TiMo additions. After continuous cooling to room temperature, a set of heat treatments using fast heating rates were applied simulating the conditions of induction heat treatments. An important increase of both yield and tensile strengths was measured after induction treatment without any important impairment in toughness properties. A significant precipitation hardening is observed in Mo-containing grades under specific heat treatment parameters.

  1. Study of the influence between the strength of antibending of working rolls on the widening during hot rolling of thin sheet metal

    Directory of Open Access Journals (Sweden)

    U. Muhin

    2016-07-01

    Full Text Available Based on the variation principle of Jourdan was developed a mathematical model of the process of widening freely in hot rolling of thin sheet metal. The principle applies to rigid-plastic materials and for the cinematically admissible area of speeds. The developed model allows to study the distribution of the widening on the length of the deformation zone depending on the parameters of the rolling process and sheet metal. Results are obtained, characterizing the size of the widening and effectiveness of the process control on tension at the entrance and exit from the stand. The widening is dependent on the strength of anti bending.

  2. Structure changes of Co-Ni-Al ferromagnetic shape memory alloys after vacuum annealing and hot rolling

    International Nuclear Information System (INIS)

    Maziarz, Wojciech

    2008-01-01

    The structure changes of vacuum annealed and hot rolled Co 35+x -Ni 40-x -Al 25 (x = 0, 2.5, 5.0) ferromagnetic shape memory alloys were examined by optical microscopy and X-ray diffraction measurements. Almost the same content of γ phase was observed in alloys after vacuum annealing. The change of grains morphology from dendrite in to equiaxed ones appeared after vacuum annealing. The hot rolling process was applied after annealing at 900 deg. C with thickness reduction up to about 90%. The structure of hot rolled samples revealed elongated grains of different phases. The hardness changes after heat treatment and plastic deformation processes have reflected the solution hardening and work hardening, respectively

  3. Effects of hot rolling and titanium content on the microstructure and mechanical properties of high boron Fe–B alloys

    International Nuclear Information System (INIS)

    He, Lin; Liu, Ying; Li, Jun; Li, Binghong

    2012-01-01

    Highlights: ► The content of B is 1.8 wt.% in the high boron Fe–B alloys. ► Hot-rolling improves the mechanical properties, especially the elongation. ► The Ti content affects the microstructure and mechanical properties. ► Eutectic boride can be eliminated when the atomic ratio of Ti/B is no less than 0.5. ► Alloy exhibits balanced mechanical properties when the atomic ratio of Ti/B is 0.5. -- Abstract: High boron Fe–B alloys (1.8 wt.% B) with different titanium contents are fabricated by Vacuum Induction Melting (VIM) technique. The integrated mechanical properties of the as-cast alloys are poor, especially the ductility. In this investigation, hot-rolling technology is used to improve the microstructure and mechanical properties. The microstructure analysis shows that hot rolling can reduce the size and improve the distribution of the reinforcements. The mechanical properties testing indicates that the yield strength is unchanged basically, but the tensile strength and elongation are improved greatly by hot rolling, especially the elongation. The content of titanium also has great effects on the microstructures and mechanical properties of the hot-rolled alloys. For the hot-rolled alloys, with the titanium content increasing, the ultimate tensile strength and yield strength first decrease slightly and then increase. The elongation and impact toughness are improved significantly. In particular, when the atomic ratio of Ti to B is 0.5, the reinforcements are almost entirely TiB 2 and uniformly distributed in the Fe-matrix. The ternary Fe–B–Ti alloy exhibits balanced mechanical properties: yield strength, ultimate tensile strength, elongation and impact toughness are 334 MPa, 602 MPa, 16.2% and 213 kJ/m 2 , respectively.

  4. A Study on Compressive Anisotropy and Nonassociated Flow Plasticity of the AZ31 Magnesium Alloy in Hot Rolling

    Directory of Open Access Journals (Sweden)

    Guoqiang Wang

    2014-01-01

    Full Text Available Effect of anisotropy in compression is studied on hot rolling of AZ31 magnesium alloy with a three-dimensional constitutive model based on the quadratic Hill48 yield criterion and nonassociated flow rule (non-AFR. The constitutive model is characterized by compressive tests of AZ31 billets since plastic deformations of materials are mostly caused by compression during rolling processes. The characterized plasticity model is implemented into ABAQUS/Explicit as a user-defined material subroutine (VUMAT based on semi-implicit backward Euler's method. The subroutine is employed to simulate square-bar rolling processes. The simulation results are compared with rolled specimens and those predicted by the von Mises and the Hill48 yield function under AFR. Moreover, strip rolling is also simulated for AZ31 with the Hill48 yield function under non-AFR. The strip rolling simulation demonstrates that the lateral spread generated by the non-AFR model is in good agreement with experimental data. These comparisons between simulation and experiments validate that the proposed Hill48 yield function under non-AFR provides satisfactory description of plastic deformation behavior in hot rolling for AZ31 alloys in case that the anisotropic parameters in the Hill48 yield function and the non-associated flow rule are calibrated by the compressive experimental results.

  5. A constitutive equation for hot deformation range of 304 stainless steel considering grain sizes

    International Nuclear Information System (INIS)

    Parsa, M.H.; Ohadi, D.

    2013-01-01

    Highlights: • A hot deformation constitutive equation based on invariant theory is proposed. • Deformation variables are evaluated based on objectivity, entropy principle, etc. • Using hot compression tests, coefficients of equation have been found. • The ability of equation to show the variation of stress with strain is examined. - Abstract: A general constitutive equation based on the framework of invariant theory by consideration of hot deformation key variables and also the properties of the material such as initial grain size is presented in the current work. Soundness of the considered parameters to be used in the developed formula was initially verified based on the important axioms such as objectivity, entropy principle, and thermodynamics stability. To access the prediction ability of the method, the formula was simplified for the simple hot compression test. To evaluate the simplified formula, single-hit hot compression tests were carried out at the temperature range of 900–1100 °C under true strain rate of 0.01–1 s −1 on a AISI 304 stainless steel. The capability of proposed formula for reproducing the variation of flow stress with strain and the strain hardening rate with stress for the resultant flow stress data was examined. The good agreement between model predictions and actual results signified the applicability of this method as a general constitutive equation in hot deformation studies

  6. Interface characteristic during bonding of Be and HR-1 stainless steel by hot pressing

    International Nuclear Information System (INIS)

    Li Hui; Kang Renmu; Zhou Shangqi; Kong Jilan; Zhang Pengcheng

    2010-01-01

    Be and HR-I stainless steel was diffusion bonded by hot pressing. The microstructure,composition and phase distribution and mechanical properties of the joints were analyzed using the optical microscopy, scanning electron microscopy(SEM), scanning auger microspectroscopy(SAM) and x-ray diffraction(XRD), and the effect of different interlayer materials Cu and Al and Ag-Cu alloy was also discussed. The results show that it is not easy to joint Be and HR-1 stainless when Al was used as the interlayer material, but good joints can be obtained using Cu and Ag and Cu alloy as the interlayer materials, because the formation of Be-Fe brittle intermetallic compounds was prevented. Ag-Cu alloy is the best interlayer materials among them, as it can reduce the mutual diffusion between Be and Fe. (authors)

  7. Deformation Characteristic and Constitutive Modeling of 2707 Hyper Duplex Stainless Steel under Hot Compression

    Directory of Open Access Journals (Sweden)

    Huabing Li

    2016-09-01

    Full Text Available Hot deformation behavior and microstructure evolution of 2707 hyper duplex stainless steel (HDSS were investigated through hot compression tests in the temperature range of 900–1250 °C and strain rate range of 0.01–10 s−1. The results showed that the flow behavior strongly depended on strain rate and temperature, and flow stress increased with increasing strain rate and decreasing temperature. At lower temperatures, many precipitates appeared in ferrite and distributed along the deformation direction, which could restrain processing of discontinuous dynamic recrystallization (DRX because of pinning grain boundaries. When the temperature increased to 1150 °C, the leading softening behaviors were dynamic recovery (DRV in ferrite and discontinuous DRX in austenite. When the temperature reached 1250 °C, softening behavior was mainly DRV in ferrite. The increase of strain rate was conducive to the occurrence of discontinuous DRX in austenite. A constitutive equation at peak strain was established and the results indicated that 2707 HDSS had a higher Q value (569.279 kJ·mol−1 than other traditional duplex stainless steels due to higher content of Cr, Mo, Ni, and N. Constitutive modeling considering strain was developed to model the hot deformation behavior of 2707 HDSS more accurately, and the correlation coefficient and average absolute relative error were 0.992 and 5.22%, respectively.

  8. Microstructure and microtexture evolutions of deformed oxide layers on a hot-rolled microalloyed steel

    International Nuclear Information System (INIS)

    Yu, Xianglong; Jiang, Zhengyi; Zhao, Jingwei; Wei, Dongbin; Zhou, Cunlong; Huang, Qingxue

    2015-01-01

    Highlights: • Microtexture development of deformed oxide layers is investigated. • Magnetite shares the {0 0 1} fibre texture with wustite. • Hematite develops the {0 0 0 1} basal fibre parallel to the oxide growth. • Stress relief and ion vacancy diffusion mechanism for magnetite seam. - Abstract: Electron backscatter diffraction (EBSD) analysis has been presented to investigate the microstructure and microtexture evolutions of deformed oxide scale formed on a microalloyed steel during hot rolling and accelerated cooling. Magnetite and wustite in oxide layers share a strong {0 0 1} and a weak {1 1 0} fibres texture parallel to the oxide growth. Trigonal hematite develops the {0 0 0 1} basal fibre parallel to the crystallographic plane {1 1 1} in magnetite. Taylor factor estimates have been conducted to elucidate the microtexture evolution. The fine-grained magnetite seam adjacent to the substrate is governed by stress relief and ions vacancy diffusion mechanism

  9. Tribology and Tool Wear of Hot Dip Galvanized Zinc Magnesium Alloys on Cold Rolled Steel Sheets

    Science.gov (United States)

    Raab, A. E.; Berger, E.; Freudenthaler, J.; Leomann, F.; Walch, C.

    2011-05-01

    Recently zinc based coatings on cold rolled steel with improved functionality in terms of forming and/or corrosion behaviour have been intensively investigated in the steel industry1,2,3. One of the most promising products are zinc magnesium alloys produced in hot dip galvanizing process. These coatings were already introduced in construction industry a few years ago1. With some modifications the improved properties of the coating are also interesting for automotive industry. In the present work the tribological potential of hot dip galvanized zinc magnesium coatings (HDG/ZM) produced at an industrial line under regular production, was studied in terms of sliding properties, adhesive and abrasive tool wear. First a short introduction into surface morphology of HDG/ZM will be given. For the tribological characterization of the material, which is the main topic of the contribution, different tests were performed on hot dip galvanised zinc magnesium material and results were compared with classic hot dip galvanized zinc coating (HDG/Z). The investigations are mainly based on the strip draw test which allows the determination of the friction coefficient directly by using a constant contact pressure. Deep drawing property was tested by forming model cups. The abrasive tool wear was tested using a standard test for material used in automotive industry. The adhesive tool wear was investigated by characterizing the coating material transferred to the tool in the strip draw test. All performed tests show an improved drawability of HDG/ZM compared to classical HDG/Z reference material. However the most promising difference between HDG/ZM and HDG/Z is that galling was found to be less for HDG/ZM than for HDG/Z. Therefore HDG/ZM is an interesting system not only with respect to corrosion protection but also in terms of tribology and provides clear advantages in formability.

  10. Tribology and Tool Wear of Hot Dip Galvanized Zinc Magnesium Alloys on Cold Rolled Steel Sheets

    International Nuclear Information System (INIS)

    Raab, A. E.; Berger, E.; Freudenthaler, J.; Leomann, F.; Walch, C.

    2011-01-01

    Recently zinc based coatings on cold rolled steel with improved functionality in terms of forming and/or corrosion behaviour have been intensively investigated in the steel industry. One of the most promising products are zinc magnesium alloys produced in hot dip galvanizing process. These coatings were already introduced in construction industry a few years ago. With some modifications the improved properties of the coating are also interesting for automotive industry. In the present work the tribological potential of hot dip galvanized zinc magnesium coatings (HDG/ZM) produced at an industrial line under regular production, was studied in terms of sliding properties, adhesive and abrasive tool wear.First a short introduction into surface morphology of HDG/ZM will be given. For the tribological characterization of the material, which is the main topic of the contribution, different tests were performed on hot dip galvanised zinc magnesium material and results were compared with classic hot dip galvanized zinc coating (HDG/Z). The investigations are mainly based on the strip draw test which allows the determination of the friction coefficient directly by using a constant contact pressure. Deep drawing property was tested by forming model cups. The abrasive tool wear was tested using a standard test for material used in automotive industry. The adhesive tool wear was investigated by characterizing the coating material transferred to the tool in the strip draw test.All performed tests show an improved drawability of HDG/ZM compared to classical HDG/Z reference material. However the most promising difference between HDG/ZM and HDG/Z is that galling was found to be less for HDG/ZM than for HDG/Z. Therefore HDG/ZM is an interesting system not only with respect to corrosion protection but also in terms of tribology and provides clear advantages in formability.

  11. Microstructural characterization and formation mechanism of abnormal segregation band of hot rolled ferrite/pearlite steel

    Energy Technology Data Exchange (ETDEWEB)

    Feng, Rui [School of Materials Science and Engineering, Shandong University, Jinan 250061 (China); Engineering Research Center of Large Size Alloy Structural Steel Bars of Shandong Province, Jinan 250061 (China); School of Materials Science and Engineering, Shandong University of Technology, Zibo 255049 (China); Li, Shengli, E-mail: lishengli@sdu.edu.cn [School of Materials Science and Engineering, Shandong University, Jinan 250061 (China); Engineering Research Center of Large Size Alloy Structural Steel Bars of Shandong Province, Jinan 250061 (China); Zhu, Xinde [School of Materials Science and Engineering, Shandong University, Jinan 250061 (China); Ao, Qing [School of Materials Science and Engineering, Shandong University, Jinan 250061 (China); Engineering Research Center of Large Size Alloy Structural Steel Bars of Shandong Province, Jinan 250061 (China)

    2015-10-15

    In order to further reveal the microstructural characterization and formation mechanism of abnormal segregation band of hot rolled ferrite/pearlite steel, the microstructure of this type steel was intensively studied with Scanning Auger Microprobe (SAM), etc. The results show that severe C–Mn segregation exists in the abnormal segregation band region at the center of hot rolled ferrite/pearlite steel, which results from the Mn segregation during solidification process of the continuous casting slab. The C–Mn segregation causes relative displacement of pearlite transformation curve and bainite transformation curve of C curve in the corresponding region, leading to bay-like shaped C curve. The bay-like shaped C curve creates conditions for the transformation from supercooling austenite to bainite at relatively lower cooling rate in this region. The Fe–Mn–C Atomic Segregation Zone (FASZ) caused by C–Mn segregation can powerfully retard the atomic motion, and increase the lattice reconstruction resistance of austenite transformation. These two factors provide thermodynamic and kinetic conditions for the bainite transformation, and result in the emergence of granular bainitic abnormal segregation band at the center of steel plate, which leads to lower plasticity and toughness of this region, and induces the layered fracture. - Highlights: • Scanning Auger Microprobe (SAM) is applied in the fracture analysis. • The abnormal segregation band region appears obvious C–Mn segregation. • The C–Mn segregation leads to bay-like shaped C curve. • The C–Mn segregation leads to Fe–Mn–C Atomic Segregation Zone.

  12. 76 FR 42679 - Certain Hot-Rolled Carbon Steel Flat Products From India: Final Results of Antidumping Duty...

    Science.gov (United States)

    2011-07-19

    .... Steel''), Nucor Corporation (``Nucor''), and ArcelorMittal USA Inc. DATES: Effective Date: July 19, 2011..., 2011. We received briefs from U.S. Steel and Nucor and a rebuttal brief from Tata.\\5\\ On May 17, the... India, dated April 14, 2011; Letter from Nucor to the Department, regarding Certain Hot-Rolled Carbon...

  13. 78 FR 64008 - Hot-Rolled Steel Products From China, India, Indonesia, Taiwan, Thailand, and Ukraine; Revised...

    Science.gov (United States)

    2013-10-25

    ... INTERNATIONAL TRADE COMMISSION [Investigation Nos. 701-TA-405, 406, and 408 and 731-TA-899-901 and 906-908 (Second Review)] Hot-Rolled Steel Products From China, India, Indonesia, Taiwan, Thailand, and Ukraine; Revised Schedule for the Subject Five Year Reviews AGENCY: United States International Trade...

  14. 78 FR 16252 - Certain Hot-Rolled Carbon Steel Flat Products From India, Indonesia, and Thailand: Final Results...

    Science.gov (United States)

    2013-03-14

    ... Indonesia P.T. Krakatau Steel 10.21 All Others 10.21 Thailand Sahaviriya Steel Industries Public Company...] Certain Hot-Rolled Carbon Steel Flat Products From India, Indonesia, and Thailand: Final Results of... products (``HR steel'') from India, Indonesia, and Thailand pursuant to section 751(c) of the Tariff Act of...

  15. 78 FR 25701 - Certain Hot-Rolled Carbon Steel Flat Products From India: Notice of Second Amended Final Results...

    Science.gov (United States)

    2013-05-02

    ... Essar I, the CIT remanded Commerce's AFA determination that Essar benefited from the CIP.\\10\\ The CIT... DEPARTMENT OF COMMERCE International Trade Administration [C-533-821] Certain Hot-Rolled Carbon... Commerce. SUMMARY: On April 9, 2013, the United States Court of International Trade (CIT) sustained the...

  16. Layer texture of hot-rolled BCC metals and its significance for stress-corrosion cracking of main gas pipelines

    Science.gov (United States)

    Perlovich, Yu. A.; Isaenkova, M. G.; Krymskaya, O. A.; Morozov, N. S.

    2016-10-01

    Based on data of X-ray texture analysis of hot-rolled BCC materials it was shown that the layerwise texture inhomogeneity of products is formed during their manufacturing. The effect can be explained by saturation with interstitial impurities of the surface layer, resulting in dynamical deformation aging (DDA). DDA prevents the dislocation slip under rolling and leads to an increase of lattice parameters in the external layer. The degree of arising inhomogeneity correlates with the tendency of hot-rolled sheets and obtained therefrom tubes to stress-corrosion cracking under exploitation, since internal layers have a compressive effect on external layers, and prevents opening of corrosion cracks at the tube surface.

  17. Tensile Fracture Behavior of 316L Austenitic Stainless Steel Manufactured by Hot Isostatic Pressing

    Science.gov (United States)

    Cooper, A. J.; Brayshaw, W. J.; Sherry, A. H.

    2018-02-01

    Herein we investigate how the oxygen content in hot isostatically pressed (HIP'd) 316L stainless steel affects the mechanical properties and tensile fracture behavior. This work follows on from previous studies, which aimed to understand the effect of oxygen content on the Charpy impact toughness of HIP'd steel. We expand on the work by performing room-temperature tensile testing on different heats of 316L stainless steel, which contain different levels of interstitial elements (carbon and nitrogen) as well as oxygen in the bulk material. Throughout the work we repeat the experiments on conventionally forged 316L steel as a reference material. The analysis of the work indicates that oxygen does not contribute to a measureable solution strengthening mechanism, as is the case with carbon and nitrogen in austenitic stainless steels (Werner in Mater Sci Eng A 101:93-98, 1988). Neither does oxygen, in the form of oxide inclusions, contribute to precipitation hardening due to the size and spacing of particles. However, the oxide particles do influence fracture behavior; fractography of the failed tension test specimens indicates that the average ductile dimple size is related to the oxygen content in the bulk material, the results of which support an on-going hypothesis relating oxygen content in HIP'd steels to their fracture mechanisms by providing additional sites for the initiation of ductile damage in the form of voids.

  18. Formation of microstructural features in hot-dip aluminized AISI 321 stainless steel

    Science.gov (United States)

    Huilgol, Prashant; Rajendra Udupa, K.; Udaya Bhat, K.

    2018-02-01

    Hot-dip aluminizing (HDA) is a proven surface coating technique for improving the oxidation and corrosion resistance of ferrous substrates. Although extensive studies on the HDA of plain carbon steels have been reported, studies on the HDA of stainless steels are limited. Because of the technological importance of stainless steels in high-temperature applications, studies of their microstructural development during HDA are needed. In the present investigation, the HDA of AISI 321 stainless steel was carried out in a pure Al bath. The microstructural features of the coating were studied using scanning electron microscopy and transmission electron microscopy. These studies revealed that the coating consists of two regions: an Al top coat and an aluminide layer at the interface between the steel and Al. The Al top coat was found to consist of intermetallic phases such as Al7Cr and Al3Fe dispersed in an Al matrix. Twinning was observed in both the Al7Cr and the Al3Fe phases. Furthermore, the aluminide layer comprised a mixture of nanocrystalline Fe2Al5, Al7Cr, and Al. Details of the microstructural features are presented, and their formation mechanisms are discussed.

  19. Novel process chain for hot metal gas forming of ferritic stainless steel 1.4509

    Science.gov (United States)

    Mosel, André; Lambarri, Jon; Degenkolb, Lars; Reuther, Franz; Hinojo, José Luis; Rößiger, Jörg; Eurich, Egbert; Albert, André; Landgrebe, Dirk; Wenzel, Holger

    2018-05-01

    Exhaust gas components of automobiles are often produced in ferritic stainless steel 1.4509 due to the low thermal expansion coefficient and the low material price. Until now, components of the stainless steel with complex geometries have been produced in series by means of multi-stage hydroforming at room temperature with intermediate annealing operations. The application of a single-stage hot-forming process, also referred to as hot metal gas forming (HMGF), offers great potential to significantly reduce the production costs of such components. The article describes a novel process chain for the HMGF process. Therefore the tube is heated in two steps. After pre-heating of the semi-finished product outside the press, the tube is heated up to forming start temperature by means of a tool-integrated conductive heating before forming. For the tube of a demonstrator geometry, a simulation model for the conduction heating was set up. In addition to the tool development for this process, experimental results are also described for the production of the demonstrator geometry.

  20. Analysis of the influence of the anisotropy induced by cold rolling on duplex and super-austenitic stainless steels

    Directory of Open Access Journals (Sweden)

    Martino Labanti

    2010-07-01

    Full Text Available This report contains the results obtained from the mechanical characterization tests carried out on two different stainless steel (duplex 6%Ni, 22%Cr and super-austenitic 31%Ni, 28%Cr used for the manufacturing of pipes which are employed in the oil production. The activity has been performed in order to evaluate the effects of anisotropy, induced by cold rolling, on the mechanical characteristics of the investigated steels, measured in the three main directions. Considering the small size of the component, the method and the specimens used for the tests were not the standard one. The procedure carried out provided the strain measurement of the specimen during testing by means of resistive strain gages, bonded on the specimens.

  1. Evaluation of the mechanical properties after thermal treatment of a structural hot rolled multiphase steel

    Directory of Open Access Journals (Sweden)

    Asensio-Lozano, J.

    2007-12-01

    Full Text Available The present paper corresponds to the experimental study conducted on a hot rolled (HR multiphase (MP steel, in which hardness, tensile and toughness properties were measured after the application of a series of subcritical and intercritical heat treatments (HT to the hot rolled stock. The aforementioned values were compared to the corresponding ones in the as-rolled state and after normalizing. The microstructure in the longitudinal plane of the strip was analyzed by light optical microscopy in the as-rolled state and in the HT samples. Longitudinal (L and transverse (T tensile and toughness specimens were cut to characterize every condition studied. Toughness properties were evaluated by means of Charpy V-notch tests conducted at 20 °C, 0 °C, –20 °C, –40 °C, –60 °C and –80 °C . It was observed that the yield stress increased with the increase in the heat treatment temperature in the subcritical range, while the tensile strength decreased slightly over the same range of temperatures. Uniform and total elongation only showed a slight improvement when the treatment was conducted at 620 °C and 700 °C, while the best toughness response corresponded to the sample treated at 500 °C for operating temperatures comprised between –40 °C and room temperature (RT.

    El presente estudio corresponde al trabajo experimental desarrollado en un acero multifase laminado en caliente, en el que se evaluaron las propiedades de dureza, tracción y tenacidad a impacto, tras realizar tratamientos térmicos subcríticos e intercríticos al material laminado en caliente. Los valores precedentes se comparan con el material de partida laminado en caliente y tras tratamiento de normalizado. Se analiza la microestructura en microscopía óptica de reflexión, en el plano longitudinal tanto en el estado laminado como en las muestras tratadas térmicamente. Se estudiaron los comportamientos longitudinales y transversales en tracción y frente a impacto

  2. The effect of additional elements on the magnetic properties of hot-rolled Nd-Fe-B alloys

    International Nuclear Information System (INIS)

    Chang, W.C.; Nakamura, H.; Paik, C.R.; Sugimoto, S.; Okada, M.; Homma, M.

    1992-01-01

    The magnetic properties of hot-rolled Nd 16 Fe bal. B 6 M 1.5 (M = Cu, Ga and Al) and Nd 16 Fe 76 B 5.5 Ga 1.5 Al 1 alloys were investigated, in order to study the role of additive elements in improving the magnetic properties in the Nd-Fe-B system. It is found that the original grain size of Cu, Ga or Ga-Al added alloys is much finer than that of the ternary and Al added alloys. But the grain size is almost identical for all the alloys after hot-rolling at 1000degC with 90% reduction in thickness. The coercivity of hot-rolled alloys with Cu, Ga or Ga-Al addition is not improved as was expected, because Nd-rich liquid phase in these alloys is very easily squeezed out during high-reduction-ratio rolling. Less quantity and nonuniform distribution of Nd-rich phase between distributed grains are believed to be the main reasons to depress the effect on the grain boundary smoothing. This effect is not the same as those observed in the Pr-Fe-B system. The highest magnetic properties achieved in this study are B r = 10 kG, i H c = 8.2 kOe, (BH) max = 18.5 MGOe for the Nd 16 Fe 76.5 B 6 Al 1.5 alloy. (orig.)

  3. 75 FR 64254 - Certain Hot-Rolled Flat-Rolled Carbon Quality Steel Products From Brazil; Final Results of...

    Science.gov (United States)

    2010-10-19

    ...-Rolled Carbon Quality Steel Products From Brazil; Final Results of Antidumping Duty Administrative Review... for the Final Results, 75 FR 19369 (April 14, 2010) (Preliminary Results). This review covers sales of... Products from Brazil,'' dated June 22, 2010 (USIMINAS Sales Verification Report). Following the release of...

  4. Cladding of aluminum on AISI 304L stainless steel by cold roll bonding: Mechanism, microstructure, and mechanical properties

    Energy Technology Data Exchange (ETDEWEB)

    Akramifard, H.R., E-mail: akrami.1367@ut.ac.ir [School of Metallurgy and Materials Engineering, College of Engineering, University of Tehran, P.O. Box 11155-4563, Tehran (Iran, Islamic Republic of); Mirzadeh, H., E-mail: hmirzadeh@ut.ac.ir [School of Metallurgy and Materials Engineering, College of Engineering, University of Tehran, P.O. Box 11155-4563, Tehran (Iran, Islamic Republic of); Advanced Metalforming and Thermomechanical Processing Laboratory, School of Metallurgy and Materials Engineering, University of Tehran, Tehran (Iran, Islamic Republic of); Parsa, M.H., E-mail: mhparsa@ut.ac.ir [School of Metallurgy and Materials Engineering, College of Engineering, University of Tehran, P.O. Box 11155-4563, Tehran (Iran, Islamic Republic of); Center of Excellence for High Performance Materials, School of Metallurgy and Materials Engineering, University of Tehran, Tehran (Iran, Islamic Republic of); Advanced Metalforming and Thermomechanical Processing Laboratory, School of Metallurgy and Materials Engineering, University of Tehran, Tehran (Iran, Islamic Republic of)

    2014-09-08

    The AA1050 aluminum alloy and AISI 304L stainless steel sheets were stacked together to fabricate Al/304L/Al clad sheet composites by the cold roll bonding process, which was performed at temperatures of ∼100 and 23 °C to produce austenitic and austenitic–martensitic microstructures in the AISI 304L counterpart, respectively. The peel test results showed that the threshold reduction required to make a suitable bond at room temperature is below 10%, which is significantly lower than the required reduction for cold roll bonding of Al sheets. The tearing of the Al sheet during the peel test signified that the bond strength of the roll bonded sheets by only 38% reduction has reached the strength of Al, which is a key advantage of the developed sheets. The extrusion of Al through the surface cracks and settling inside the 304L surface valleys due to strong affinity between Al and Fe was found to be the bonding mechanism. Subsequently, the interface and tensile behaviors of three-layered clad sheets after soaking at 200–600 °C for 1 h were investigated to characterize the effect of annealing treatment on the formation and thickening of intermetallic compound layer and the resultant mechanical properties. Field emission scanning electron microscopy, X-ray diffraction, and optical microscopy techniques revealed that an intermediate layer composed mainly of Al{sub 13}Fe{sub 4}, FeC and Al{sub 8}SiC{sub 7} forms during annealing at 500–600 °C. A significant drop in tensile stress–strain curves after the maximum point (UTS) was correlated to the interface debonding. It was found that the formation of intermediate layer by post heat treatment deteriorates the bond quality and encourages the debonding process. Moreover, the existence of strain-induced martensite in clad sheets was found to play a key role in the enhancement of tensile strength.

  5. Microstructural Evolutions During Reversion Annealing of Cold-Rolled AISI 316 Austenitic Stainless Steel

    Science.gov (United States)

    Naghizadeh, Meysam; Mirzadeh, Hamed

    2018-06-01

    Microstructural evolutions during reversion annealing of a plastically deformed AISI 316 stainless steel were investigated and three distinct stages were identified: the reversion of strain-induced martensite to austenite, the primary recrystallization of the retained austenite, and the grain growth process. It was found that the slow kinetics of recrystallization at lower annealing temperatures inhibit the formation of an equiaxed microstructure and might effectively impair the usefulness of this thermomechanical treatment for the objective of grain refinement. By comparing the behavior of AISI 316 and 304 alloys, it was found that the mentioned slow kinetics is related to the retardation effect of solute Mo in the former alloy. At high reversion annealing temperature, however, an equiaxed austenitic microstructure was achieved quickly in AISI 316 stainless steel due to the temperature dependency of retardation effect of molybdenum, which allowed the process of recrystallization to happen easily. Conclusively, this work can shed some light on the issues of this efficient grain refining approach for microstructural control of austenitic stainless steels.

  6. Passivity and passivity breakdown of 304L stainless steel in hot and concentrated nitric acid

    International Nuclear Information System (INIS)

    Gillard-Tcharkhtchi, Elsa

    2014-01-01

    The objective of this study is to characterize the oxidation behavior of 304L stainless steel (SS) in representative conditions of spent nuclear fuel reprocessing, i.e. in hot and concentrated nitric acid. In these conditions the SS electrochemical potential is in the passive domain and its corrosion rate is low. However when the media becomes more aggressive, the potential may be shifted towards the trans-passive domain characterized with a high corrosion rate. Passivity and passivity breakdown in the trans-passive domain are of a major interest for the industry. So as to characterize these phenomenons, this work was undertaken with the following representative conditions: a 304L SS from an industrial sheet was studied, the media was hot and concentrated HNO 3 , long term tests were performed. First, the surface of an immersed 304L SS was characterized with several complementary techniques from the micro to the nanometer scale. Then oxidation kinetics was studied in the passive and in the trans-passive domain. The oxidation behavior was studied thanks to weight loss determination and surface analysis. Finally, oxidation evolution as a function of the potential was studied from the passive to the trans-passive domain. In particular, this allowed us to obtain the anodic curve of 304L SS in hot and concentrated and to define precisely the 304L SS limits of in such conditions. (author) [fr

  7. Interdiffusion studies on hot rolled U-10Mo/AA1050

    Energy Technology Data Exchange (ETDEWEB)

    Saliba-Silva, A.M.; Martins, I.C.; Carvalho, E.U.; Durazzo, M.; Riella, H.G. [Instituto de Pesquisas Energeticas e Nucleares (CCN/IPEN/CNEN-SP), Sao Paulo, SP (Brazil). Centro de Combustivel Nuclear], e-mail: saliba@ipen.br

    2010-07-01

    The U-Mo alloys are investigated with the goal of becoming nuclear material to fabricate high-density fuel elements for high performance research reactors. This enrichment level suggests that the U-Mo alloys should be between 6 to 10wt%, which can give up to 9gU/cm{sup 3} as fuel density. Nevertheless, the U-Mo alloys are very reactive with Al. Interdiffusion reaction products are formed since nuclear fission promotes chemical interaction layer during operation, leading to potential structural failure. Present studies were made with treated hot rolled diffusion couples of U-10Mo inserted in Al (AA1050). The U-10Mo/AA1050 pairs were treated in two temperature (150 degree C and 550 degree C) with three soaking times (5h, 40h and 80h). From microstructure analyses, rapid diffusion of Al happened inside U-10Mo in the first heating at 540 degree C during 15 min, reaching 8 at%Al in a range of 200 {mu}m towards U-10Mo. Longer time (5, 40, 80h) at 550 degree C maintain this level of Al-content up to 1000 {mu}m inside U-10Mo. A minor depth ({approx}1 {mu}m) near the interdiffusion contact had higher Al-content, but not sufficient to form identifiable (U,Mo)Al{sub x} structures. Probably, residual elements reduced drastically the interdiffusion phenomena between U-10Mo and AA1050, maybe due to silicon presence. (author)

  8. Studies of the AA2519 Alloy Hot Rolling Process and Cladding with EN AW-1050A Alloy

    Directory of Open Access Journals (Sweden)

    Płonka B.

    2016-03-01

    Full Text Available The objective of the study was to determine the feasibility of plastic forming by hot rolling of the AA2519 aluminium alloy sheets and cladding these sheets with a layer of the EN AW-1050A alloy. Numerous hot-rolling tests were carried out on the slab ingots to define the parameters of the AA2519 alloy rolling process. It has been established that rolling of the AA2519 alloy should be carried out in the temperature range of 400-440°C. Depending on the required final thickness of the sheet metal, appropriate thickness of the EN AW-1050A alloy sheet, used as a cladding layer, was selected. As a next step, structure and mechanical properties of the resulting AA2519 alloy sheets clad with EN AW-1050A alloy was examined. The thickness of the coating layer was established at 0,3÷0,5mm. Studies covered alloy grain size and the core alloy-cladding material bond strength.

  9. 75 FR 65453 - Certain Hot-Rolled Flat-Rolled Carbon Quality Steel Flat Products From Brazil: Notice of...

    Science.gov (United States)

    2010-10-25

    ... Nucor Corporation (Nucor) and United States Steel Corporation (U.S. Steel), domestic producers of hot..., the Department received requests from Nucor and U.S. Steel (collectively, domestic producers), that... July 6, 2010 (CBP Memo). On July 22, 2010, and July 23, 2010, respectively, Nucor and U.S. Steel timely...

  10. Microstructure characteristics of high borated stainless steel fabricated by hot-pressing sintering

    Energy Technology Data Exchange (ETDEWEB)

    Zhou, Xuan; Wang, Mingjia, E-mail: mingjiawangysu@126.com; Zhao, Hongchang

    2016-04-25

    The present study investigated the microstructure of powder metallurgy (P/M) high borated stainless steel through hot-pressing sintering in a temperature range of 1000–1150 °C within 30 min under 30 MPa. Microstructure and phase examinations were carried out by applying scanning electron microscope, electron backscatter diffraction and X-ray diffraction analysis. The results of as-atomized powders demonstrated that many powders kept egg-type structure with an austenite outer layer and the eutectic borides were much finer than those in traditional cast products. Microstructure studies revealed that borides suffered Ostwald ripening and were significantly influenced by the sintering temperature. Orientation maps indicated that the inter-particle contact areas consisted of equiaxed grains and the regions consisting of large elongated grains partly inherited the microstructure characteristics of as-atomized powder particles. Furthermore, the mechanisms governing the morphological changes in microstructure were discussed. - Highlights: • Near-complete densification could be obtained through hot-pressing sintering. • There was no phase transformation and present phases were M{sub 2}B and austenite. • Borides suffered Ostwald ripening and were significantly influenced by temperature. • Inter-particle contact areas consisted of equiaxed grains for recrystallization. • Deformation-free zones exhibited elongated grains for dendritic arms coarsening.

  11. Hot Ductility Characterization of Sanicro-28 Super-Austenitic Stainless Steel

    Science.gov (United States)

    Mirzaei, A.; Zarei-Hanzaki, A.; Abedi, H. R.

    2016-05-01

    The hot ductility behavior of a super-austenitic stainless steel has been studied using tensile testing method in the temperature range from 1073 K to 1373 K (800 °C to 1100 °C) under the strain rates of 0.1, 0.01, and 0.001 s-1. The hot compression tests were also performed at the same deformation condition to identify the activated restoration mechanisms. At lower temperatures [ i.e., 1073 K and 1173 K (800 °C and 900 °C)], the serration of initial grain boundaries confirms the occurrence of dynamic recovery as the predominant restoration process. However, in the course of applied deformation, the initial microstructure is recrystallized at higher temperatures [ i.e., 1273 K and 1373 K (1000 °C and 1100 °C)]. In this respect, annealing the twin boundaries could well stimulate the recrystallization kinetic through initiation new annealing twins on prior annealing twin boundaries. The hot tensile results show that there is a general trend of increasing ductility by temperature. However, two regions of ductility drop are recognized at 1273 K and 1373 K (1000°C)/0.1s-1 and (1100°C)/0.01s-1. The ductility variations at different conditions of temperature and strain rate are discussed in terms of simultaneous activation of grain boundary sliding and restoration processes. The observed ductility troughs are attributed to the occurrence of grain boundary sliding and the resulting R-type and W-type cracks. The occurrence of dynamic recrystallization is also considered as the main factor increasing the ductility at higher temperatures. The enhanced ductility is primarily originated from the post-uniform elongation behavior, which is directly associated with the strain rate sensitivity of the experimental material.

  12. Measurements of Residual Stresses In Cold-Rolled 304 Stainless Steel Plates Using X-Ray Diffraction with Rietveld Refinement Method

    International Nuclear Information System (INIS)

    Parikin; Killen, P; Rafterry, A.

    2009-01-01

    The determination of the residual stresses using X-ray powder diffraction in a series of cold-rolled 304 stainless steel plates, deforming 0, 34, 84, 152, 158, 175 and 196 % reduction in thickness has been carried out. The diffraction data were analyzed using the Rietveld structure refinement method. The analysis shows that for all specimens, the martensite particles are closely in compression and the austenite matrix is in tension. Both the martensite and austenite, for a sample reducing 34% in thickness (containing of about 1% martensite phase) the average lattice strains are anisotropic and decrease approximately exponential with an increase in the corresponding percent reduction (essentially phase content). It is shown that this feature can be qualitatively understood by taking into consideration the thermal expansion mismatch between the martensite and austenite grains. Also, for all cold-rolled stainless steel specimens, the diffraction peaks are broader than the unrolled one (instrumental resolution), indicating that the strains in these specimens are inhomogeneous. From an analysis of the refined peak shape parameters, the average root-mean square strain, which describes the distribution of the inhomogeneous strain field, was predicted. The average residual stresses in cold-rolled 304 stainless steel plates showed a combination effect of hydrostatic stresses of the martensite particles and the austenite matrix. (author)

  13. Effect of electropulsing on surface mechanical properties and microstructure of AISI 304 stainless steel during ultrasonic surface rolling process

    Energy Technology Data Exchange (ETDEWEB)

    Wang, Haibo [Advanced Materials Institute, Graduate School at Shenzhen, Tsinghua University, Shenzhen 518055 (China); Key Laboratory of Advanced Materials, Tsinghua University, Beijing 100084 (China); Song, Guolin [Advanced Materials Institute, Graduate School at Shenzhen, Tsinghua University, Shenzhen 518055 (China); Tang, Guoyi, E-mail: tanggy@mail.tsinghua.edu.cn [Advanced Materials Institute, Graduate School at Shenzhen, Tsinghua University, Shenzhen 518055 (China); Key Laboratory of Advanced Materials, Tsinghua University, Beijing 100084 (China)

    2016-04-26

    The present work integrates 3D digital optical microscopy (OM), nano-indentation, X-ray diffraction (XRD), scanning electron microscopy (SEM) with electron backscatter diffraction (EBSD) and transmission electron microscopy (TEM) to systematically investigate the effect of electropulsing on the surface mechanical properties and microstructure of AISI 304 stainless steel during the ultrasonic surface rolling process (USRP). Compared with the original USRP, the introduction of electropulsing with optimal parameters can effectively facilitate surface crack healing and improve surface hardness and wear resistance dramatically, and the residual compressive stress is further enhanced. Meanwhile, more martensite phase and fewer deformation twins can be found in the strengthened layer. Rapid improvement of the surface mechanical properties should be attributed to the ultra-refined grains, accelerated martensitic phase transformation and suppressed deformation twining induced by the coupling effect of USRP and electropulsing. The high strain rate given by USRP, increased stacking fault energy and accelerated dislocation mobility caused by electropulsing are likely the primary intrinsic reasons for the observed phenomena.

  14. Austenitic Reversion of Cryo-rolled Ti-Stabilized Austenitic Stainless Steel: High-Resolution EBSD Investigation

    Science.gov (United States)

    Tiamiyu, A. A.; Odeshi, A. G.; Szpunar, J. A.

    2018-02-01

    In this study, AISI 321 austenitic stainless steel (ASS) was cryo-rolled and subsequently annealed at 650 and 800 °C to reverse BCC α'-martensite to FCC γ-austenite. The texture evolution associated with the reversion at the selected temperatures was investigated using high-resolution EBSD. After the reversion, TiC precipitates were observed to be more stable in 650 °C-annealed specimens than those reversed at 800 °C. {110} texture was mainly developed in specimens subjected to both annealing temperatures. However, specimens reversed at 650 °C have stronger texture than those annealed at 800 °C, even at the higher annealing time. The strong intensity of {110} texture component is attributed to the ability of AISI 321 ASS to memorize the crystallographic orientation of the deformed austenite, a phenomenon termed texture memory. The development of weaker texture in 800 °C-annealed specimens is attributed to the residual strain relief in grains, dissolution of grain boundary precipitates, and an increase in atomic migration along the grain boundaries. Based on the observed features of the reversed austenite grains and estimation from an existing model, it is suspected that the austenite reversion at 650 and 800 °C undergone diffusional and martensitic shear reversion, respectively.

  15. Evaluation of rolling contact fatigue of induction heated 13Cr-2Ni-2Mo Stainless steel bar with Si3N4-ball

    Science.gov (United States)

    Yadoiwa, Ariyasu; Mizobe, Koshiro; Kida, Katsuyuki

    2018-03-01

    13Cr % martensitic stainless steels were used in various industry, because they have excellent corrosion resistance and high hardness among other stainless steels. They are also expected as a bearing material, however, the research on rolling contact fatigue (RCF) is not enough. In this study, 13Cr-2Ni-2Mo stainless steels were quenched by induction heating and their RCF lives were evaluated. A Si3N4-ball was used in order to apply higher stress (Pmax = 5.6 GPa) than our previous tests (Pmax=5.3 GPa), in a single-ball RCF testing machine. It was found that the basic life (L10) was 2.20×106 cycles and Median life (L50) was 6.04×106 cycles. In addition, Weibull modulus became higher than the previous tests.

  16. Influence of feed rate on damage development in hot ring rolling

    NARCIS (Netherlands)

    Wang, Chao; van den Boogaard, Antonius H.; Omerspahic, E.; Recina, V.; Geijselaers, Hubertus J.M.; Ishikawa, T.; Mori, K.-I.

    2014-01-01

    As an incremental forming process of bulk metal, ring rolling provides a cost effective process route to manufacture seamless rings. Applications of ring rolling cover a wide range of products in aerospace, automotive and civil engineering industries. Under some process conditions, defects such as

  17. Microstructure analysis of AISI 304 stainless steel produced by twin-roll thin strip casting process

    Institute of Scientific and Technical Information of China (English)

    2007-01-01

    The microstructure of AISI 304 austenite stainless steel fabricated by the thin strip casting process were investigated using optical microscope, scanning electron microscope (SEM), transmission electron microscope (TEM), and X-ray diffraction (XRD).The microstructures of the casting strips show a duplex structure consisting of delta ferrite and austenite. The volume fraction of the delta ferrite is about 9.74vol% at the center and 6.77vol% at the surface of the casting thin strip, in vermicular and band shapes. On account of rapid cooling and solidification in the continuous casting process, many kinds of inclusions and precipitates have been found. Most of the inclusions and precipitates are spherical complex compounds consisting of oxides, such as, SiO2, MnO, Al2O3,Cr2O3,and FeO or their multiplicity oxides of MnO·Al2O3,2FeO·SiO2, and 2MnO·SiO2. Many defects including dislocations and stacking faults have also formed during the rapid cooling and solidification process, which is helpful to improve the mechanical properties of the casting strips.

  18. The Role of Nano-TiO2 Lubricating Fluid on the Hot Rolled Surface and Metallographic Structure of SS41 Steel

    Directory of Open Access Journals (Sweden)

    Yanan Meng

    2018-02-01

    Full Text Available In this paper, nano-TiO2lubricating fluid was chosen as an advanced rolling lubricant to investigate its effect on the hot rolled surface and metallographic structure of SS41 steel strips. The tribological performances of nano-TiO2 lubricating fluid were measured by a four-ball tribotester. The hot rolling experiments under different lubrication conditions were carried out by a four-high rolling mill. The surface morphology, oxide scales and metallographic structure after hot rolling were observed using a confocal laser scanning microscope and scanning electron microscope (SEM, respectively. The composition of surface attachments was analyzed with X-ray photoelectron spectroscopy (XPS. The results indicate that the nano-TiO2 lubricating fluid has a better tribological performance. The surface defects on the hot rolled surface could be decreased. The phase composition of the surface still appears as a mixture of ferrite and pearlite. The surface of steel strips is not micro-alloyed with titanium as predicted. Additionally, the grain size of rolled steel strips which were lubricated with the nano-TiO2lubricating fluid decreased by nearly 50%, compared with traditional lubricating fluid. Furthermore, it was found that the thickness of the oxide layers on the surface reduced, whilst the Rockwell hardness of the oxide layers was enhanced as nano-TiO2 lubricating fluid was applied.

  19. Mechanical properties and hot-rolled microstructures of a low carbon bainitic steel with Cu-P alloying

    International Nuclear Information System (INIS)

    Cui, W.F.; Zhang, S.X.; Jiang, Y.; Dong, J.; Liu, C.M.

    2011-01-01

    Highlights: → Mechanical properties and microstructures of low carbon bainite steel are examined. → Cu-P alloying promotes strengthening and uniform plastic deformation. → Cu-P alloying delays recovery process during rolling interval. → Lowering rolling temperature is favorable to increasing toughness. - Abstract: A low carbon bainitic steel with Cu-P alloying was developed. The new steel aims to meet the demand of high strength, high toughness and resistance to chloride ion corrosion for the components used in the environment of sea water and oceanic atmosphere. Mechanical properties of the steel were tested and strengthening and toughening mechanisms were analyzed by comparing hot-rolled microstructures of the low carbon bainitic steels with and without Cu-P alloying. The results show that Cu-P alloying provided strong solution strengthening with weak effect on ductility. The toughness loss caused by Cu-P alloying could be balanced by increasing the amount of martensite/remained austenite (M/A island) at lower finishing temperature. The static recovery process during rolling interval was delayed by the interaction of phosphorous, copper atoms with dislocations, which was favorable to the formation of bainitic plates. Super-fine Nb(C, N) particles precipitated on dislocations had coherency with bainite ferrite at 830 deg. C finishing temperature. Raising finishing temperature to 880 deg. C, Nb(C, N) particles were prone to coarsening and losing coherency. It was also found that no accurate lattice match relationship among retained austenite, martensite and bainite in granular bainitic microstructure.

  20. Mechanical properties and hot-rolled microstructures of a low carbon bainitic steel with Cu-P alloying

    Energy Technology Data Exchange (ETDEWEB)

    Cui, W.F., E-mail: wenfangcui@yahoo.com.cn [Key Laboratory for Anisotropy and Texture of Materials (Ministry of Education), Northeastern University, Shenyang 110004 (China); Zhang, S.X. [Key Laboratory for Anisotropy and Texture of Materials (Ministry of Education), Northeastern University, Shenyang 110004 (China); Technology Center of Laiwu Iron and Steel (Group) Co. Ltd., Laiwu 271104 (China); Jiang, Y. [School of Chemical Engineering, University of Queensland, Brisbane 4072 (Australia); Dong, J. [Technology Center of Laiwu Iron and Steel (Group) Co. Ltd., Laiwu 271104 (China); Liu, C.M. [Key Laboratory for Anisotropy and Texture of Materials (Ministry of Education), Northeastern University, Shenyang 110004 (China)

    2011-08-15

    Highlights: {yields} Mechanical properties and microstructures of low carbon bainite steel are examined. {yields} Cu-P alloying promotes strengthening and uniform plastic deformation. {yields} Cu-P alloying delays recovery process during rolling interval. {yields} Lowering rolling temperature is favorable to increasing toughness. - Abstract: A low carbon bainitic steel with Cu-P alloying was developed. The new steel aims to meet the demand of high strength, high toughness and resistance to chloride ion corrosion for the components used in the environment of sea water and oceanic atmosphere. Mechanical properties of the steel were tested and strengthening and toughening mechanisms were analyzed by comparing hot-rolled microstructures of the low carbon bainitic steels with and without Cu-P alloying. The results show that Cu-P alloying provided strong solution strengthening with weak effect on ductility. The toughness loss caused by Cu-P alloying could be balanced by increasing the amount of martensite/remained austenite (M/A island) at lower finishing temperature. The static recovery process during rolling interval was delayed by the interaction of phosphorous, copper atoms with dislocations, which was favorable to the formation of bainitic plates. Super-fine Nb(C, N) particles precipitated on dislocations had coherency with bainite ferrite at 830 deg. C finishing temperature. Raising finishing temperature to 880 deg. C, Nb(C, N) particles were prone to coarsening and losing coherency. It was also found that no accurate lattice match relationship among retained austenite, martensite and bainite in granular bainitic microstructure.

  1. AISI/DOE Advanced Process Control Program Vol. 3 of 6: MICROSTRUCTURAL ENGINEERING IN HOT-STRIP MILLS Part 2 of 2: Constitutive Behavior Modeling of Steels Under Hot-Rolling Conditions; FINAL

    International Nuclear Information System (INIS)

    Yi-Wen Cheng; Patrick Purtscher

    1999-01-01

    This report describes the development of models for predicting (1) constitutive behaviors and (2) mechanical properties of hot-rolled steels as functions of chemical composition, microstructural features, and processing variables. The study includes the following eight steels: A36, DQSK, HSLA-V, HSLA-Nb, HSLA-50/Ti-Nb, and two interstitial-free (IF) grades. These developed models have been integrated into the Hot-Strip Mill Model (HSMM), which simulates the hot strip rolling mills and predicts the mechanical properties of hot-rolled products. The HSMM model has been developed by the University of British Columbia-Canada as a part of project on the microstructural engineering in hot-strip mills

  2. The Effect of Hot Working on Structure and Strength of a Precipitation Strengthened Austenitic Stainless Steel

    Science.gov (United States)

    Mataya, M. C.; Carr, M. J.; Krauss, G.

    1984-02-01

    The development of microstructure and strength during forging in a γ' strengthened austenitic stainless steel, JBK-75, was investigated by means of forward extrusion of cylindrical specimens. The specimens were deformed in a strain range of 0.16 to 1.0, from 800°C to 1080°C, and at approximate strain rates of 2 (press forging) and 2 × 103 s-1 (high energy rate forging), and structures examined by light and transmission microscopy. Mechanical properties were determined by tensile testing as-forged and forged and aged specimens. The alloy exhibited an extremely wide variety of structures and properties within the range of forging pzrameters studied. Deformation at the higher strain rate via high energy rate forging resulted in unrecovered substructures and high strengths at low forging temperatures, and static recrystallization and low strengths at high temperatures. In contrast, however, deformation at the lower strain rate via press forging resulted in retention of the well developed subgrain structure and associated high strength produced at high forging temperatures and strains. At lower temperatures and strains during press forging a subgrain structure formed preferentially at high angle grain boundaries, apparently by a creep-type deformation mechanism. Dynamic recrystallization was not an important restoration mechanism for any of the forging conditions. The results are interpreted on the basis of stacking fault energy and the accumulation of strain energy during hot working. The significance of observed microstructural differences for equivalent deformation conditions (iso-Z, where Z is the Zener-Holloman parameter) is discussed in relation to the utilization of Z for predicting hot work structures and strengths. Aging showed that the γ' precipitation process is not affected by substructure and that the strengthening contributions, from substructure and precipitation, were independent and additive. Applications for these findings are discussed in terms

  3. The effect of hot working on structure and strength of a precipitation strengthened austenitic stainless steel

    International Nuclear Information System (INIS)

    Mataya, M.C.; Carr, M.J.; Krauss, G.

    1984-01-01

    The development of microstructure and strength during forging a γ' strengthened austenitic stainless steel, JBK-75, was investigated. The specimens were deformed in a strain range of 0.16 to 1.0, from 800 0 C to 1080 0 C at approximate strain rates of 2 (press forging) and 2 X 10 3 S -1 (high energy rate forging). Mechanical properties were determined by tensile testing as-forged and forged and aged specimens. The alloy exhibited a wide variety of structures and properties within the range of forging parameters studied. Deformation at the higher strain rate via high energy rate forging resulted in unrecovered substructures and high strengths at low forging temperatures, and static recrystallization and low strengths at high temperatures. In contrast, however, deformation at the lower strain rate via press forging resulted in retention of the well developed subgrain structure and associated high strength produced at high forging temperatures and strains. At lower temperatures and strains during press forging a subgrain structure formed preferentially at high angle grain boundaries, apparently by a creep-type deformation mechanism. Dynamic recrystallization was not an important restoration mechanism for any of the forging conditions. The results are interpreted on the basis of stacking fault energy and the accumulation of strain energy during hot working. The significance of microstructural differences for equivalent deformation conditions (iso-Z, where Z is the Zener-Holloman parameter) is discussed in relation to the utilization of Z for predicting hot work structures and strengths. Aging showed that γ' precipitation is not affected by substructure and that the strengthening contributions were independent and additive. Applications for these findings are discussed in terms of process design criteria

  4. An Assessment of the Ductile Fracture Behaviour of Hot Isostatically Pressed and Forged 304L Stainless Steel

    OpenAIRE

    Cooper, Adam; Smith, R. J.; Sherry, Andrew

    2017-01-01

    Type 300 austenitic stainless steel manufactured by hot isostatic pressing (HIP) has recently been shown to exhibit subtly different fracture behavior from that of equivalent graded forged steel, whereby the oxygen remaining in the component after HIP manifests itself in the austenite matrix as nonmetallic oxide inclusions. These inclusions facilitate fracture by acting as nucleation sites for the initiation, growth, and coalescence of microvoids in the plastically deforming austenite matrix....

  5. EBSD study of purity effects during hot working in austenitic stainless steels

    International Nuclear Information System (INIS)

    El Wahabi, M.; Gavard, L.; Cabrera, J.M.; Prado, J.M.; Montheillet, F.

    2005-01-01

    The technique of electron back scattering diffraction (EBSD) is considered as a powerful instrument for the study of the microstructural changes during hot forming processes and gives the possibility to present the information in different ways (OIM, misorientation diagram and pole figures). The present work is focused on the observation by EBSD of the microstructure evolution during deformation at high temperature of three austenitic stainless steels: AISI-304H, AISI-304L and a high purity steel HP. The difference between the three steels is the content carbon and the presence of residual elements. To this aim compression tests were carried out at a constant strain rate of 0.001 s -1 and different temperatures. The study showed an increase of twin boundary fractions and a diminution of substructure (low angle densities boundaries) at increasing temperatures. On the other hand, increasing carbon content promotes lower twin boundary fractions and larger amounts of low angle boundaries. This effect can be explained by the reduction of grain boundary mobility caused by increasing carbon contents, which in turn reduces the migration rate and consequently the probability of twin boundary generation. Moreover, the increment of low angle boundaries with carbon content accelerates the twin character loss. It was also found that the dynamically recrystallized grain size decreased at increasing carbon content due to a typical drag effect. No important features on textures were found during DDRX

  6. Dynamic Recrystallization Behavior of AISI 422 Stainless Steel During Hot Deformation Processes

    Science.gov (United States)

    Ahmadabadi, R. Mohammadi; Naderi, M.; Mohandesi, J. Aghazadeh; Cabrera, Jose Maria

    2018-02-01

    In this work, hot compression tests were performed to investigate the dynamic recrystallization (DRX) process of a martensitic stainless steel (AISI 422) at temperatures of 950, 1000, 1050, 1100 and 1150 °C and strain rates of 0.01, 0.1 and 1 s-1. The dependency of strain-hardening rate on flow stress was used to estimate the critical stress for the onset of DRX. Accordingly, the critical stress to peak stress ratio was calculated as 0.84. Moreover, the effect of true strain was examined by fitting stress values to an Arrhenius type constitutive equation, and then considering material constants as a function of strain by using a third-order polynomial equation. Finally, two constitutive models were used to investigate the competency of the strain-dependent constitutive equations to predict the flow stress curves of the studied steel. It was concluded that one model offers better precision on the flow stress values after the peak stress, while the other model gives more accurate results before the peak stress.

  7. Effects of Al content on structure and mechanical properties of hot-rolled ZrTiAlV alloys

    International Nuclear Information System (INIS)

    Liang, S.X.; Yin, L.X.; Che, H.W.; Jing, R.; Zhou, Y.K.; Ma, M.Z.; Liu, R.P.

    2013-01-01

    Highlights: • Phase structure is greatly dependent on the Al content. • Intermetallic compound will precipitates while Al content is over 6.9 wt%. • Equiaxed α-phase grains present in the hot-rolled alloy with 6.9 wt% Al. • Alloys with Al content from 3.3 wt% to 5.6 wt% have good mechanical properties. - Abstract: Zirconium alloys show attractive properties for astronautic applications where the most important factors are anti-irradiation, corrosion resistance, anti-oxidant, very good strength-to-weight ratio. The effects of Al content (2.2–6.9 wt%) on structure and mechanical properties of the hot-rolled ZrTiAlV alloy samples were investigated in this study. Each sample of the hot-rolled ZrTiAlV alloys with Al contents from 2.2 wt% to 5.6 wt% is composed of the α phase and β phase, meanwhile, the relative content of the α phase increased with the Al content. However, the (ZrTi) 3 Al intermetallic compound was observed as the Al content increased to 6.9 wt%. Changes of phase compositions and structure with Al content distinctly affected mechanical properties of ZrTiAlV alloys. Yield strength of the alloy with 2.2 wt% Al is below 200 MPa. As Al content increased to 5.6 wt%, the yield strength, tensile strength and elongation of the examined alloy are 1088 MPa, 1256 MPa and 8%, respectively. As Al content further increased to 6.9 wt%, a rapid decrease in ductility was observed as soon as the (ZrTi) 3 Al intermetallic compound precipitated. Results show that the ZrTiAlV alloys with Al contents between 3.3 wt% and 5.6 wt% have excellent mechanical properties

  8. Service behaviour of high speed steel rolling rolls used in hot strip mills; Comportamiento en servicio de los aceros rapidos utilizados en la fabricacion de los cilindros de trabajo de los trenes de bandas en caliente

    Energy Technology Data Exchange (ETDEWEB)

    Ziadi, A.; Belzunce, F. J.; Rodriguez, C.; Fernandez, I.

    2005-07-01

    Work rolls used in hot strip mills may be able to carry out severe actions: very high thermal stresses and wear, along with mechanical stresses due to normal rolling loads, which develop in the presence of cracks, produced by the former actions. The microstructure and the mechanical behaviour (strength and toughness) of high speed steels, which recently have been introduced in this applications, were studied in this work in comparison with high chromium cast irons. (Author) 7 refs.

  9. Hot Ductility Behaviors in the Weld Heat-Affected Zone of Nitrogen-Alloyed Fe-18Cr-10Mn Austenitic Stainless Steels

    Science.gov (United States)

    Moon, Joonoh; Lee, Tae-Ho; Hong, Hyun-Uk

    2015-04-01

    Hot ductility behaviors in the weld heat-affected zone (HAZ) of nitrogen-alloyed Fe-18Cr-10Mn austenitic stainless steels with different nitrogen contents were evaluated through hot tension tests using Gleeble simulator. The results of Gleeble simulations indicated that hot ductility in the HAZs deteriorated due to the formation of δ-ferrite and intergranular Cr2N particles. In addition, the amount of hot ductility degradation was strongly affected by the fraction of δ-ferrite.

  10. Effect of rolling deformation and solution treatment on microstructure ...

    Indian Academy of Sciences (India)

    Department of Metallurgy and Materials Engineering, Bengal Engineering and Science ... lume percent of elongated band of δ-ferrite (∼40%) and austenite phase which ... Duplex stainless steel; hot rolling; cold deformation; microstructure; tensile properties. 1. ... ssure vessels, storage tanks, rotors, impellers and shafts,.

  11. Analysis of the strengthening mechanisms in pipeline steels as a function of the hot rolling parameters

    International Nuclear Information System (INIS)

    Carretero Olalla, V.; Bliznuk, V.; Sanchez, N.; Thibaux, P.; Kestens, L.A.I.; Petrov, R.H.

    2014-01-01

    The yield strength of different pipeline steel grades, rolled under four different conditions, was correlated with calculated strengthening contributions. Slabs with the same composition were rolled under identical roughing conditions but varied finish rolling temperature (FRT). Two cooling routes, consisting of accelerated water cooling condition (ACC) followed by slow cooling in an oven to simulate coiling and air cooling were applied after the last rolling pass. The microstructures obtained after each thermo mechanical controlled process (TMCP) schedule, were characterized using Transmission Electron Microscopy (TEM), Inductively Coupled Plasma Mass Spectrometry (ICP-MS) and Electron backscatter diffraction (EBSD). The mechanical properties of the plates were determined by means of tensile tests and Charpy V-notch impact test. It was confirmed that a combination of fast cooling rate and low finish rolling temperature produces higher strength than the slow cooling rate and high finish rolling temperature. Contributions to the strengthening arising from the various microstructural features like solid solution strengthening, grain size, dislocation density and precipitation hardening, were analyzed using Taylor, Hall–Petch and Ashby–Orowan approaches. The root of the sum of the squares method was applied to link the experimental with the model-predicted strength. It is believed that this approach provides a better understanding of the effect of TMCP parameters on the microstructure and strengthening mechanisms in pipeline steels

  12. Electron backscatter diffraction study of dislocation content of a macrozone in hot-rolled Ti-6Al-4V alloy

    International Nuclear Information System (INIS)

    Britton, T. Ben; Birosca, Soran; Preuss, Michael; Wilkinson, Angus J.

    2010-01-01

    We compare the dislocation substructure within macrozone and non-macrozone regions of hot-rolled Ti-6Al-4 V. Hough-based and cross-correlation-based analysis of electron backscatter diffraction (EBSD) patterns are used to establish the grain orientations and intra-granular misorientations, respectively. The set of geometrically necessary dislocations (GNDs) that support measured lattice curvatures and minimize the total GND line energy are calculated. The GND content in the macrozone is approximately twice that in the non-macrozone region, and GNDs are present at densities ∼10 times higher than GNDs.

  13. Investigation of the structure dependence of diffusivity, solubility and permeability of hydrogen in hot-rolled low-carbon steels

    Energy Technology Data Exchange (ETDEWEB)

    Forcey, K S; Ross, D K [Birmingham Univ. (UK). Dept. of Physics; Iordanova, I A [Sofia Univ. (Bulgaria). Dept. of Solid State Physics

    1989-01-01

    A time-lag method for estimating the diffusivity, permeability and solubility of hydrogen in low-carbon hot-rolled steels has been applied. Oriani's model has been used to investigate and explain the effects of microstructure on the trapping of hydrogen. The results show that the initial microstructure of steel significantly affects the behaviour of hydrogen atoms. Of the three sites, namely: Dislocations, interstitial atoms and particles, the most effective traps seem to be interfaces between coarse particles and the matrix. (orig.).

  14. Investigation of the structure dependence of diffusivity, solubility and permeability of hydrogen in hot-rolled low-carbon steels

    International Nuclear Information System (INIS)

    Forcey, K.S.; Ross, D.K.; Iordanova, I.A.

    1989-01-01

    A time-lag method for estimating the diffusivity, permeability and solubility of hydrogen in low-carbon hot-rolled steels has been applied. Oriani's model has been used to investigate and explain the effects of microstructure on the trapping of hydrogen. The results show that the initial microstructure of steel significantly affects the behaviour of hydrogen atoms. Of the three sites, namely: Dislocations, interstitial atoms and particles, the most effective traps seem to be interfaces between coarse particles and the matrix. (orig.)

  15. Mechanisms of ultrafine-grained austenite formation under different isochronal conditions in a cold-rolled metastable stainless steel

    Energy Technology Data Exchange (ETDEWEB)

    Celada-Casero, C., E-mail: c.celada@cenim.csic.es [MATERALIA group, Dpt. of Physical Metallurgy, Centro Nacional de Investigaciones Metalúrgicas (CENIM-CSIC), Av. Gregorio del Amo 8, 28040 Madrid (Spain); Huang, B.M. [National Taiwan University, Dpt. of Materials Science and Engineering, 1 Roosvelt Road, Section 4, 10617 Taipei, Taiwan, ROC (China); Aranda, M.M. [MATERALIA group, Dpt. of Physical Metallurgy, Centro Nacional de Investigaciones Metalúrgicas (CENIM-CSIC), Av. Gregorio del Amo 8, 28040 Madrid (Spain); Yang, J.-R. [National Taiwan University, Dpt. of Materials Science and Engineering, 1 Roosvelt Road, Section 4, 10617 Taipei, Taiwan, ROC (China); Martin, D. San [MATERALIA group, Dpt. of Physical Metallurgy, Centro Nacional de Investigaciones Metalúrgicas (CENIM-CSIC), Av. Gregorio del Amo 8, 28040 Madrid (Spain)

    2016-08-15

    The primary objective of this work is to obtain fundamental insights on phase transformations, with focus on the reaustenitization process (α′→γ transformation), of a cold-rolled (CR) semi-austenitic metastable stainless steel upon different isochronal conditions (0.1, 1, 10 and 100 °C/s). For this purpose, an exhaustive microstructural characterization has been performed by using complementary experimental such as scanning and transmission electron microscopy (SEM and TEM), electron backscattered diffraction (EBSD), electron probe microanalysis (EPMA), micro-hardness Vickers and magnetization measurements. It has been detected that all microstructural changes shift to higher temperatures as the heating rate increases. The reaustenitization occurs in two-steps for all heating rates, which is attributed to the chemical banding present in the CR state. The α′→γ transformation is controlled by the migration of substitutional alloying elements across the austenite/martensite (γ/α′) interface, which finally leads to ultrafine-grained reaustenitized microstructures (440–280 nm). The morphology of the martensite phase in the CR state has been found to be the responsible for such a grain refinement, along with the presence of χ-phase and nanometric Ni{sub 3}(Ti,Al) precipitates that pin the austenite grain growth, especially upon slowly heating at 0.1 °C/s. - Highlights: •Ultrafine-grained austenite structures are obtained isochronally at 0.1–100 °C/s •The α′→γ transformation occurs in two steps due to the initial chemical banding •A diffusional mechanism governs the α′→γ transformation for all heating rates •The dislocation-cell-type of martensite promotes a diffusional mechanism •Precipitates located at α′/γ interfaces hinder the austenite growth.

  16. Design of Experiment as a powerful tool when applying Finite Element Method: a case study on prediction of hot rolling process parameters

    Directory of Open Access Journals (Sweden)

    Giancarlo G. Bordonaro

    2018-04-01

    Full Text Available The ultimate goal in hot roll pass design is to manufacture a rolled product with the required dimensional accuracy, defect free surface, and mechanical properties. The proper selection of process parameters is crucial to meet increasing requirements for desired quality and geometrical properties of rolled products. Due to the complex behavior of the metal flow at high temperatures and the severe plastic deformations in shape rolling, most efforts that have been made so far only rely upon the practical experience gained by operators. The large number of variables involved and the difficulty in investigating the process characteristics, make the use of finite element (FE tools an effective and attractive opportunity towards a thorough understanding of the rolling process. In this work, Design of Experiment (DOE is proposed as a powerful and viable method for the prediction of rolling process parameters while reducing the computational effort. Nonlinear 3D FE models of the hot rolling process are developed for a large set of complex cross-section shapes and validated against experimental evidences provided by real plant products at each stage of the deformation sequence. Based on the accuracy of the validated FE models, DOE is applied to investigate the flat rolling process under a series of many parameters and scenarios. Effects of main roll forming variables are analyzed on material flow behavior and geometrical features of a rolled product. The selected DOE factors are the workpiece temperature, diameter size, diameter reduction (draught, and rolls angular velocity. The selected DOE responses are workpiece spread, effective stresses, contact stresses, and rolls reaction loads. Eventually, the application of Pareto optimality (a Multi-Criteria Decision Making method allows to detect an optimal combination of design factors which respect desired target requirements for the responses.

  17. A Feeding Strategy in Inner L-Shape Ring Hot Rolling Process

    Directory of Open Access Journals (Sweden)

    Wen Meng

    2017-01-01

    Full Text Available In order to make the inner L-shape ring polling process with a closed die structure (ILRRCDS on the top and bottom of the driven roll stable, at first, this paper established the mathematical model for ILRRCDS. Then, the plastic penetration and biting-in conditions for ILRRCDS were deduced based on plain ring rolling theory. Moreover, a feeding strategy that can realize a constant growth of the ring’s outer radius was proposed and the reasonable value ranges of the feed rate of the mandrel were determined. The numerical simulation model for ILRRCDS is established based on ABAQUS software. Finally, the equivalent plastic strain (PEEQ and temperature distributions of rolled ring were obtained. The results indicated that the proposed feeding strategy can realize a stable ILRRCDS. At the end of ILRRCDS, the PEEQ at the inner radius surface of the ring is maximum, the PEEQ at the outer radius surface of the ring takes the second place, and the PEEQ at the middle part of ring is minimum. With the increase of rolling time, the higher temperature zone of the rolled ring gradually moves from the center part of the ring to the “inner corner zone” of the ring.

  18. Application of MMC model on simulation of shearing process of thick hot-rolled high strength steel plate

    Energy Technology Data Exchange (ETDEWEB)

    Dong, Liang; Li, Shuhui [Shanghai Key Laboratory of Digital Manufacture for Thin-walled Structures, Shanghai Jiao Tong University, Shanghai 200240 (China); Yang, Bing; Gao, Yongsheng [Automotive Steel Research Institute, R and D Center, BaoShan Iron and Steel Co.,Ltd, Shanghai 201900 (China)

    2013-12-16

    Shear operation is widely used as the first step in sheet metal forming to cut the sheet or plate into the required size. The shear of thick hot-rolled High Strength Steel (HSS) requires large shearing force and the sheared edge quality is relatively poor because of the large thickness and high strength compared with the traditional low carbon steel. Bad sheared edge quality will easily lead to edge cracking during the post-forming process. This study investigates the shearing process of thick hot-rolled HSS plate metal, which is generally exploited as the beam of heavy trucks. The Modified Mohr-Coulomb fracture criterion (MMC) is employed in numerical simulation to calculate the initiation and propagation of cracks during the process evolution. Tensile specimens are designed to obtain various stress states in tension. Equivalent fracture strains are measured with Digital Image Correlation (DIC) equipment to constitute the fracture locus. Simulation of the tension test is carried out to check the fracture model. Then the MMC model is applied to the simulation of the shearing process, and the simulation results show that the MMC model predicts the ductile fracture successfully.

  19. Use of Hot Rolling for Generating Low Deviation Twins and a Disconnected Random Boundary Network in Inconel 600 Alloy

    Science.gov (United States)

    Sahu, Sandeep; Yadav, Prabhat Chand; Shekhar, Shashank

    2018-02-01

    In this investigation, Inconel 600 alloy was thermomechanically processed to different strains via hot rolling followed by a short-time annealing treatment to determine an appropriate thermomechanical process to achieve a high fraction of low-Σ CSL boundaries. Experimental results demonstrate that a certain level of deformation is necessary to obtain effective "grain boundary engineering"; i.e., the deformation must be sufficiently high to provide the required driving force for postdeformation static recrystallization, yet it should be low enough to retain a large fraction of original twin boundaries. Samples processed in such a fashion exhibited 77 pct length fraction of low-Σ CSL boundaries, a dominant fraction of which was from Σ3 ( 64 pct), the latter with very low deviation from its theoretical misorientation. The application of hot rolling also resulted in a very low fraction of Σ1 ( 1 pct) boundaries, as desired. The process also leads to so-called "triple junction engineering" with the generation of special triple junctions, which are very effective in disrupting the connectivity of the random grain boundary network.

  20. Application of MMC model on simulation of shearing process of thick hot-rolled high strength steel plate

    International Nuclear Information System (INIS)

    Dong, Liang; Li, Shuhui; Yang, Bing; Gao, Yongsheng

    2013-01-01

    Shear operation is widely used as the first step in sheet metal forming to cut the sheet or plate into the required size. The shear of thick hot-rolled High Strength Steel (HSS) requires large shearing force and the sheared edge quality is relatively poor because of the large thickness and high strength compared with the traditional low carbon steel. Bad sheared edge quality will easily lead to edge cracking during the post-forming process. This study investigates the shearing process of thick hot-rolled HSS plate metal, which is generally exploited as the beam of heavy trucks. The Modified Mohr-Coulomb fracture criterion (MMC) is employed in numerical simulation to calculate the initiation and propagation of cracks during the process evolution. Tensile specimens are designed to obtain various stress states in tension. Equivalent fracture strains are measured with Digital Image Correlation (DIC) equipment to constitute the fracture locus. Simulation of the tension test is carried out to check the fracture model. Then the MMC model is applied to the simulation of the shearing process, and the simulation results show that the MMC model predicts the ductile fracture successfully

  1. Effect of both sulphur content and deoxidation degree on the hot ductility of resulphurized austenitic stainless steels in the solidified state

    International Nuclear Information System (INIS)

    Botella, J.; Sanchez, R.

    1998-01-01

    The manufacture of free machining austenitic stainless steels features a specific drawback derived from their high sulphur content, which is needed for generating, into the austenitic matrix inclusions to optimize the different machining operations. However, sulphur has ahamfull effect on hot workability. This paper deals with assessing the effect of sulphur content and deoxidation level on the hot ductility of resulphurized austenitic stainless steels in as cast condition. Hot tensile tests were conducted on a Gleeble machine, at temperatures between 1,150 and 1,250 degree celsius, studying a suctility factor as a function of sulphur content, deoxidation degree, as well as type, size and distribution of sulfides. Results point out the harmful effect of increasing sulphur and oxygen contents on the hot workability of resulphurized austenitic stainless steels, and the need to control carefully the level of oxides of these steels. (Author) 5 refs

  2. On the Effects of Hot Forging and Hot Rolling on the Microstructural Development and Mechanical Response of a Biocompatible Ti Alloy

    Science.gov (United States)

    Okazaki, Yoshimitsu

    2012-01-01

    Zr, Nb, and Ta as alloying elements for Ti alloys are important for attaining superior corrosion resistance and biocompatibility in the long term. However, note that the addition of excess Nb and Ta to Ti alloys leads to higher manufacturing cost. To develop low-cost manufacturing processes, the effects of hot-forging and continuous-hot-rolling conditions on the microstructure, mechanical properties, hot forgeability, and fatigue strength of Ti-15Zr-4Nb-4Ta alloy were investigated. The temperature dependences with a temperature difference (ΔT) from β-transus temperature (Tβ) for the volume fraction of the α- and β-phases were almost the same for both Ti-15Zr-4Nb-4Ta and Ti-6Al-4V alloys. In the α-β-forged Ti-15Zr-4Nb-4Ta alloy, a fine granular α-phase structure containing a fine granular β-phase at grain boundaries of an equiaxed α-phase was observed. The Ti-15Zr-4Nb-4Ta alloy billet forged at Tβ-(30 to 50) °C exhibited high strength and excellent ductility. The effects of forging ratio on mechanical strength and ductility were small at a forging ratio of more than 3. The maximum strength (σmax) markedly increased with decreasing testing temperature below Tβ. The reduction in area (R.A.) value slowly decreased with decreasing testing temperature below Tβ. The temperature dependences of σmax for the Ti-15Zr-4Nb-4Ta and Ti-6Al-4V alloys show the same tendency and might be caused by the temperature difference (ΔT) from Tβ. It was clarified that Ti-15Zr-4Nb-4Ta alloy could be manufactured using the same manufacturing process as for previously approved Ti-6Al-4V alloy, taking into account the difference (ΔT) between Tβ and heat treatment temperature. Also, the manufacturing equivalency of Ti-15Zr-4Nb-4Ta alloy to obtain marketing approval of implants was established. Thus, it was concluded that continuous hot rolling is useful for manufacturing α-β-type Ti alloy.

  3. Effects of Loading Frequency on Fatigue Behavior, Residual Stress, and Microstructure of Deep-Rolled Stainless Steel AISI 304 at Elevated Temperatures

    Science.gov (United States)

    Nikitin, I.; Juijerm, P.

    2018-02-01

    The effects of loading frequency on the fatigue behavior of non-deep-rolled (NDR) and deep-rolled (DR) austenitic stainless steel AISI 304 were systematically clarified at elevated temperatures, especially at temperatures exhibiting the dynamic strain aging (DSA) phenomena. Tension-compression fatigue tests were performed isothermally at temperatures of 573 K and 773 K (300 °C and 500 °C) with different loading frequencies of 5, 0.5, 0.05, and 0.005 Hz. For the DR condition, the residual stresses and work-hardening states will be presented. It was found that DSA would be detected at appropriate temperatures and deformation rates. The cyclic deformation curves and the fatigue lives of the investigated austenitic stainless steel AISI 304 are considerably affected by the DSA, especially on the DR condition having high dislocation densities at the surface and in near-surface regions. In the temperature range of the DSA, residual stresses and work-hardening states of the DR condition seem to be stabilized. The microstructural alterations were investigated by transmission electron microscopy (TEM). At an appropriate temperature with low loading frequency, the plastic deformation mechanism shifted from a wavy slip manner to a planar slip manner in the DSA regimes, whereas the dislocation movements were obstructed.

  4. Processing of fine grained AISI 304L austenitic stainless steel by cold rolling and high-temperature short-term annealing

    Science.gov (United States)

    Naghizadeh, Meysam; Mirzadeh, Hamed

    2018-05-01

    An advanced thermomechanical process based on the formation and reversion of deformation-induced martensite was used to refine the grain size and enhance the hardness of an AISI 304L austenitic stainless steel. Both low and high reversion annealing temperatures and also the repetition of the whole thermomechanical cycle were considered. While a microstructure with average austenite grain size of a few micrometers was achieved based on cold rolling and high-temperature short-term annealing, an extreme grain refinement up to submicrometer regime was obtained by cold rolling followed by low-temperature long-term annealing. However, the required annealing time was found to be much longer, which negates its appropriateness for industrial production. While a magnificent grain refinement was achieved by one pass of the high-temperature thermomechanical process, the reduction in grain size was negligible by the repetition of the whole cycle. It was found that the hardness of the thermomechanically processed material is much higher than that of the as-received material. The results of the present work were shown to be compatible with the general trend of grain size dependence of hardness for AISI 304L stainless steel based on the Hall-Petch relationship. The results were also discussed based on the X-ray evaluation of dislocation density by modified Williamson-Hall plots.

  5. In-Situ Characterization of Deformation and Fracture Behavior of Hot-Rolled Medium Manganese Lightweight Steel

    Science.gov (United States)

    Zhao, Zheng-zhi; Cao, Rong-hua; Liang, Ju-hua; Li, Feng; Li, Cheng; Yang, Shu-feng

    2018-02-01

    The deformation and fracture behavior of hot-rolled medium manganese lightweight (0.32C-3.85Mn-4.18Al-1.53Si) steel was revealed by an in situ tensile test. Deformed δ-ferrite with plenty of cross-parallel deformation bands during in situ tensile tests provides δ-ferrite of good plasticity and ductility, although it is finally featured by the cleavage fracture. The soft and ductile δ-ferrite and high-volume fraction of austenite contribute to the superior mechanical properties of medium manganese lightweight steel heated at 800°C, with a tensile strength of 924 MPa, total elongation of 35.2% and product of the strength and elongation of 32.5 GPa %.

  6. Influence of hot rolling and high speed hydrostatic extrusion on the microstructure and mechanical properties of RAF ODS steel

    International Nuclear Information System (INIS)

    Oksiuta, Z.; Kurzydlowski, K.J.; Baluc, N.

    2009-01-01

    Argon gas atomized, pre-alloyed Fe-14Cr-2W-0.3Ti oxide dispersion strengthened (ODS) ferritic steel powder was mechanically alloyed with 0.3Y2O3 (wt.%) nano-particles in attritor ball mill and consolidated by hot isostatic pressing (HIP) at 1150 deg. C under pressure of 200 MPa for 3 hrs. To improve mechanical properties of as HIPped ODS ingots the material was undergone further thermo-mechanical treatment (TMT), namely: hot rolling (HR) at 850 deg. C or high speed hot extrusion (HSHE) at 850 deg. C. After TMT both materials were annealed at 1050 deg. C for 1 h in vacuum. Transmission electron microscopy (TEM) observations of the ODS alloys after TMT and heat treatment exhibited elongated in a longitudinal direction grains with an average size of 75 μm. However, an equiaxed, smaller than 500 nm grains were also found in the microstructure of both materials. Different size and morphology of oxides particles were also observed. Bigger, about 150 nm Ti-Al-O particles were usually located at grain boundaries whereas Y-Ti-O nanoclusters of about 5 nm were uniformly distributed in ODS steel matrix. The Charpy impact tests revealed significantly better about 90% (5.8 J) upper shelf energy (USE) of material after HSHE but ductile to brittle transition temperature (DBTT) of both alloys was unsatisfactory. As-HR ODS steel has shown DBTT of about 55 deg. C whereas HSHE ODS steel has about 75 deg. C. This relatively high values of transition temperature were probably caused by oxides particles present at grain boundaries of the ODS alloys which decreased fracture properties of the ODS steels. High temperature tensile properties of both ODS alloys are found to be satisfactory in full range of the testing temperature from 23 up to 750 deg. C. However, about 15% better UTS and YS0.2 (1350 MPa and 1285 MPa, respectively) as well as ductility were measured in the case of the as-HSHE ODS steel. These results indicates that HSHE process of the ODS steel can be considered as more

  7. Examining the microtexture evolution in a hole-edge punched into 780 MPa grade hot-rolled steel

    Energy Technology Data Exchange (ETDEWEB)

    Shin, J.H.; Kim, M.S. [Department of Printed Electronics Engineering, Sunchon National University, 315 Maegok, Sunchon, Jeonnam 540-950 (Korea, Republic of); Kim, S.I.; Seo, S.J. [POSCO Technical Research Laboratories, Gwangyang 545-090 (Korea, Republic of); Choi, S.-H., E-mail: shihoon@sunchon.ac.kr [Department of Printed Electronics Engineering, Sunchon National University, 315 Maegok, Sunchon, Jeonnam 540-950 (Korea, Republic of)

    2016-08-15

    The deformation behavior in the hole-edge of 780 MPa grade hot-rolled steel during the punching process was investigated via microstructure characterization and computational simulation. Microstructure characterization was conducted to observe the edges of punched holes through the thickness direction, and electron back-scattered diffraction (EBSD) was used to analyze the heterogeneity of the deformation. Finite element analysis (FEA) that could account for a ductile fracture criterion was conducted to simulate the deformation and fracture behaviors of 780 MPa grade hot-rolled steel during the punching process. Calculation of rotation rate fields at the edges of the punched holes during the punching process revealed that metastable orientations in Euler space were confined to specific orientation groups. Rotation-rate fields effectively explained the stability of the initial texture components in the hole-edge region during the punching process. A visco-plastic self-consistent (VPSC) polycrystal model was used to calculate the microtexture evolution in the hole-edge region during the punching process. FEA revealed that the heterogeneous effective strain was closely related to the heterogeneity of the Kernel average misorientation (KAM) distribution in the hole-edge region. A simulation of the deformation microtexture evolution in the hole-edge region using a VPSC model was in good agreement with the experimental results. - Highlights: •We analyzed the microstructure in a hole-edge punched in HR 780HB steel. •Rotation rate fields revealed the stability of the initial texture components. •Heterogeneous effective stain was closely related to the KAM distribution. •VPSC model successfully simulated the deformation microtexture evolution.

  8. Simulation of accelerated strip cooling on the hot rolling mill run-out roller table

    Directory of Open Access Journals (Sweden)

    E.Makarov

    2016-07-01

    Full Text Available A mathematical model of the thermal state of the metal in the run-out roller table continuous wide hot strip mill. The mathematical model takes into account heat generation due to the polymorphic γ → α transformation of supercooled austenite phase state and the influence of the chemical composition of the steel on the physical properties of the metal. The model allows calculation of modes of accelerated cooling strips on run-out roller table continuous wide hot strip mill. Winding temperature calculation error does not exceed 20°C for 98.5 % of strips of low-carbon and low-alloy steels

  9. FATIGUE BEHAVIOR OF HOT-ROLLED STEEL INTENDED FOR COLD FORMING

    Directory of Open Access Journals (Sweden)

    Gejza Rosenberg

    2011-07-01

    Full Text Available In the work, there are presented measured tension and fatigue properties of eight low-carbon steels moulded in form of 20 kg ingots that were processed by controlled regime of rolling /cooling and then exposed to simulated effect of two coiling temperatures. The experimental results presented in the work show, that steels with ferrite-martensite or ferrite-bainitic microstructure have in comparison to ferrite-pearlitic or ferrite-carbidic microstructure better strength-plastic properties, but worse resistance to cyclic loading.

  10. Hot rolling effect on the characters of Zr-0.6Nb-0.5Fe-0.5Cr alloy

    International Nuclear Information System (INIS)

    Sungkono; Siti Aidah

    2015-01-01

    Characters of Zr-0.6Nb-0.5Fe-0.5Cr alloy after hot rolling have been studied. The objective of this research was to obtain of hot rolling effect on the characteristics of microstructures, hardness and phases formed in Zr-0.6Nb-0.5Fe-0.5Cr alloy. The hot rolling process of alloy carried out at temperature of 800 °C with retention time of 1.5 and 2 hours and a thickness reduction between 5 to 25 %. The results of this experiment showed that the Zr-0.6Nb-0.5Fe-0.5Cr alloy has Widmanstaetten structure with microstructure evolving into deformed columnar grains and deformed elongated grains with increasing thickness reduction. Besides, the longer the retention time at temperature of 800 °C is the larger are the grain structures and formation of α-Zr and Zr_3Fe phase. The hardness of Zr-0.6Nb-0.5Fe-0.5Cr alloy has same trends i.e the larger thickness reduction gives higher hardness. The Zr-0.6Nb-0.5Fe-0.5Cr alloy can under go hot rolling deformation at a thickness reduction of 25 % and the formation of α-Zr and Zr_3Fe can increased of hardness and strength of Zr-0.6 Nb-0.5 Fe-0.5 Cr alloy. (author)

  11. Evaluation and Control of Mechanical Degradation of Austenitic Stainless 310S Steel Substrate During Coated Superconductor Processing

    Science.gov (United States)

    Kim, Seung-Gyu; Kim, Najung; Shim, Hyung-Seok; Kwon, Oh Min; Kwon, Dongil

    2018-05-01

    The superconductor industry considers cold-rolled austenitic stainless 310S steel a less expensive substitute for Hastelloy X as a substrate for coated superconductor. However, the mechanical properties of cold-rolled 310S substrate degrade significantly in the superconductor deposition process. To overcome this, we applied hot rolling at 900 °C (or 1000 °C) to the 310S substrate. To check the property changes, a simulated annealing condition equivalent to that used in manufacturing was determined and applied. The effects of the hot rolling on the substrate were evaluated by analyzing its physical properties and texture.

  12. Refinement of ferrite grain size during hot direct rolling of hsla steel

    International Nuclear Information System (INIS)

    Ajmal, M.

    2001-01-01

    Steel ingots containing 0.04 wt % Nb and varying contents of carbon were made in laboratory, that simulated thin slab casting. Mn and Si content were kept constant at 1.35 % and 0.25 % respectively. After each casting the mould assembly was transferred to the rolling mill and the temperature of the ingot was monitored. Each ingot was rolled to 4mm thickness in three passes. The first pass of 43% reduction for all the ingots were given at 1140 degree C. The second pass (reduction, 35 %) for all the ingots were given at 1040 degree C. However the temperature for third pass (reduction, 30 %) was varied to retain more strain in the austenite prior to transformation. It was shown that third pass at lower temperature i.e. 810 degree C in the austenite range yields a ferrite grains size of 2-3 micrometer. A yield strength of 465 Mpa and tensile strength of 530 Mpa can also be achieved in these plates. (author)

  13. Finite-element model to predict roll-separation force and defects during rolling of U-10Mo alloys

    Science.gov (United States)

    Soulami, Ayoub; Burkes, Douglas E.; Joshi, Vineet V.; Lavender, Curt A.; Paxton, Dean

    2017-10-01

    A major goal of the Convert Program of the U.S. Department of Energy's National Nuclear Security Administration (DOE/NNSA) is to enable high-performance research reactors to operate with low-enriched uranium rather than the high-enriched uranium currently used. To this end, uranium alloyed with 10 wt% molybdenum (U-10Mo) represents an ideal candidate because of its stable gamma phase, low neutron caption cross section, acceptable swelling response, and predictable irradiation behavior. However, because of the complexities of the fuel design and the need for rolled monolithic U-10Mo foils, new developments in processing and fabrication are necessary. This study used a finite-element code, LS-DYNA, as a predictive tool to optimize the rolling process. Simulations of the hot rolling of U-10Mo coupons encapsulated in low-carbon steel were conducted following two different schedules. Model predictions of the roll-separation force and roll pack thicknesses at different stages of the rolling process were compared with experimental measurements. The study reported here discussed various attributes of the rolled coupons revealed by the model (e.g., waviness and thickness non-uniformity like dog-boning). To investigate the influence of the cladding material on these rolling defects, other cases were simulated: hot rolling with alternative can materials, namely, 304 stainless steel and Zircaloy-2, and bare-rolling. Simulation results demonstrated that reducing the mismatch in strength between the coupon and can material improves the quality of the rolled sheet. Bare-rolling simulation results showed a defect-free rolled coupon. The finite-element model developed and presented in this study can be used to conduct parametric studies of several process parameters (e.g., rolling speed, roll diameter, can material, and reduction).

  14. An Assessment of the Ductile Fracture Behavior of Hot Isostatically Pressed and Forged 304L Stainless Steel

    Science.gov (United States)

    Cooper, A. J.; Smith, R. J.; Sherry, A. H.

    2017-05-01

    Type 300 austenitic stainless steel manufactured by hot isostatic pressing (HIP) has recently been shown to exhibit subtly different fracture behavior from that of equivalent graded forged steel, whereby the oxygen remaining in the component after HIP manifests itself in the austenite matrix as nonmetallic oxide inclusions. These inclusions facilitate fracture by acting as nucleation sites for the initiation, growth, and coalescence of microvoids in the plastically deforming austenite matrix. Here, we perform analyses based on the Rice-Tracey (RT) void growth model, supported by instrumented Charpy and J-integral fracture toughness testing at ambient temperature, to characterize the degree of void growth ahead of both a V-notch and crack in 304L stainless steel. We show that the hot isostatically pressed (HIP'd) 304L steel exhibits a lower critical void growth at the onset of fracture than that observed in forged 304L steel, which ultimately results in HIP'd steel exhibiting lower fracture toughness at initiation and impact toughness. Although the reduction in toughness of HIP'd steel is not detrimental to its use, due to the steel's sufficiently high toughness, the study does indicate that HIP'd and forged 304L steel behave as subtly different materials at a microstructural level with respect to their fracture behavior.

  15. Interfacial layers evolution during annealing in Ti-Al multi-laminated composite processed using hot press and roll bonding

    Science.gov (United States)

    Assari, A. H.; Eghbali, B.

    2016-09-01

    Ti-Al multi-laminated composites have great potential in high strength and low weight structures. In the present study, tri-layer Ti-Al composite was synthesized by hot press bonding under 40 MPa at 570 °C for 1 h and subsequent hot roll bonding at about 450 °C. This process was conducted in two accumulative passes to 30% and to 67% thickness reduction in initial and final passes, respectively. Then, the final annealing treatments were done at 550, 600, 650, 700 and 750 °C for 2, 4 and 6 h. Investigations on microstructural evolution and thickening of interfacial layers were performed by scanning electron microscopes, energy dispersive spectrometer, X-ray diffraction and micro-hardness tests. The results showed that the thickening of diffusion layers corresponds to amount of deformation. In addition to thickening of the diffusion layers, the thickness of aluminum layers decreased and after annealing treatment at 750 °C for 6 h the aluminum layers were consumed entirely, which occurred because of the enhanced interdiffusion of Ti and Al elements. Scanning electron microscope equipped with energy dispersive spectrometer showed that the sequence of interfacial layers as Ti3Al-TiAl-TiAl2-TiAl3 which are believed to be the result of thermodynamic and kinetic of phase formation. Micro-hardness results presented the variation profile in accordance with the sequence of intermetallic phases and their different structures.

  16. The feasibility of bonding aluminum alloy 6061 via hot isostatic pressing (HIP)/rolling

    International Nuclear Information System (INIS)

    Fenolietto, R.A.

    1991-01-01

    The advantage of developing a HIP bonding process for dispersion fuel plates is that applying a thin cladding in a more uniform manner could allow the upper limit for LEU U 3 Si-Al dispersion fuel plate densities to be overcome. Since much less mechanical deformation would be required, the existing process limitations on the density could be removed, theoretically allowing more fuel to be added. These increases are, of course, subject to irradiation behavior of the higher loadings which is not addressed in this paper. Initial results indicate that aluminum Alloy 6061 can be successfully bonded by seal welding via electron beam (EB), HIPping, and finishing with a limited amount of rolling. (orig.)

  17. Effect of borides on hot deformation behavior and microstructure evolution of powder metallurgy high borated stainless steel

    Energy Technology Data Exchange (ETDEWEB)

    Zhou, Xuan [State Key Laboratory of Metastable Materials Science and Technology, College of Materials Science and Engineering, Yanshan University, Qinhuangdao 066004 (China); Wang, Mingjia, E-mail: mingjiawangysu@126.com [State Key Laboratory of Metastable Materials Science and Technology, College of Materials Science and Engineering, Yanshan University, Qinhuangdao 066004 (China); Fu, Yifeng [State Key Laboratory of Metastable Materials Science and Technology, College of Materials Science and Engineering, Yanshan University, Qinhuangdao 066004 (China); Wang, Zixi; Li, Yanmei [Yanming Alloy Roll Co. Ltd, Qinhuangdao 066004 (China); Yang, Shunkai; Zhao, Hongchang; Li, Hangbo [State Key Laboratory of Metastable Materials Science and Technology, College of Materials Science and Engineering, Yanshan University, Qinhuangdao 066004 (China)

    2017-02-15

    To investigate borides effect on the hot deformation behavior and microstructure evolution of powder metallurgy high borated stainless steel, hot compression tests at the temperatures of 950– 1150 °C and the strain rates of 0.01– 10 s{sup −1} were performed. Flow stress curves indicated that borides increased the material's stress level at low temperature but the strength was sacrificed at temperatures above 1100 °C. A hyperbolic-sine equation was used to characterize the dependence of the flow stress on the deformation temperature and strain rate. The hot deformation activation energy and stress exponent were determined to be 355 kJ/mol and 3.2, respectively. The main factors leading to activation energy and stress exponent of studied steel lower than those of commercial 304 stainless steel were discussed. Processing maps at the strains of 0.1, 0.3, 0.5, and 0.7 showed that flow instability mainly concentrated at 950– 1150 °C and strain rate higher than 0.6 s{sup −1}. Results of microstructure illustrated that dynamic recrystallization was fully completed at both high temperature-low strain rate and low temperature-high strain rate. In the instability region cracks were generated in addition to cavities. Interestingly, borides maintained a preferential orientation resulting from particle rotation during compression. - Highlights: •The decrement of activation energy was affected by boride and boron solution. •The decrease of stress exponent was influenced by composition and Cottrell atmosphere. •Boride represented a preferential orientation caused by particle rotation.

  18. Effects by the microstructure after hot and cold rolling on the texture and grain size after final annealing of ferritic non-oriented FeSi electrical steel

    Science.gov (United States)

    Schneider, J.; Stöcker, A.; Franke, A.; Kawalla, R.

    2018-04-01

    The magnetic properties of fully processed non-oriented FeSi electrical steel are characterized by their magnetization behavior and specific magnetic losses. The magnetic properties are determined by the texture and microstructure. Less gamma fiber intensity and a high intensity of preferable texture components, especially cube fiber texture, are desirable to obtain an excellent magnetizing behavior. Furthermore, large grain sizes are necessary to reach low values of the specific magnetic losses. The fabrication route of the fully processed non-oriented electrical steels comprises a heavy cold rolling of the hot rolled material before final annealing. To fulfill the requirements on large grain size for low loss materials, grain growth, which appears after complete recrystallization, plays an important role. In this paper we will analyze the influence of different microstructures of the hot strip and the resulting microstructure after cold rolling on the appearance of recrystallization and grain growth after final annealing. The evolution of texture reflects the present ongoing softening processes: recovery, recrystallization and finally grain growth at the given annealing conditions. It will be shown that the image of texture at recrystallization is remarkable different from the texture at grain growth. Substantially grain growth is obtained at lower annealing temperatures for an optimum microstructure of the hot rolled material.

  19. Effects by the microstructure after hot and cold rolling on the texture and grain size after final annealing of ferritic non-oriented FeSi electrical steel

    Directory of Open Access Journals (Sweden)

    J. Schneider

    2018-04-01

    Full Text Available The magnetic properties of fully processed non-oriented FeSi electrical steel are characterized by their magnetization behavior and specific magnetic losses. The magnetic properties are determined by the texture and microstructure. Less gamma fiber intensity and a high intensity of preferable texture components, especially cube fiber texture, are desirable to obtain an excellent magnetizing behavior. Furthermore, large grain sizes are necessary to reach low values of the specific magnetic losses. The fabrication route of the fully processed non-oriented electrical steels comprises a heavy cold rolling of the hot rolled material before final annealing. To fulfill the requirements on large grain size for low loss materials, grain growth, which appears after complete recrystallization, plays an important role. In this paper we will analyze the influence of different microstructures of the hot strip and the resulting microstructure after cold rolling on the appearance of recrystallization and grain growth after final annealing. The evolution of texture reflects the present ongoing softening processes: recovery, recrystallization and finally grain growth at the given annealing conditions. It will be shown that the image of texture at recrystallization is remarkable different from the texture at grain growth. Substantially grain growth is obtained at lower annealing temperatures for an optimum microstructure of the hot rolled material.

  20. Finite-element model to predict roll-separation force and defects during rolling of U-10Mo alloys

    Energy Technology Data Exchange (ETDEWEB)

    Soulami, Ayoub; Burkes, Douglas E.; Joshi, Vineet V.; Lavender, Curt A.; Paxton, Dean

    2017-10-01

    This study used a finite element code, LSDYNA, as a predictive tool to optimize the rolling process. Simulations of the hot rolling of U-10Mo coupons encapsulated in low-carbon steel were conducted following two different schedules. Model predictions of the roll-separation force and roll pack thicknesses at different stages of the rolling process were compared with experimental measurements. The study reported here discussed various attributes of the rolled coupons revealed by the model (e.g., waviness and thickness non-uniformity like dog boning). To investigate the influence of the cladding material on these rolling defects, other cases were simulated:  hot rolling with alternative can materials, namely, 304 stainless steel and Zircaloy-2, and bare-rolling.

  1. Study of the microstructure evolution of ferritic stainless ODS steels during hot working

    International Nuclear Information System (INIS)

    Karch, Abdellatif

    2014-01-01

    The production of ODS steels involves a powder consolidation step usually using the hot extrusion (HE) process. The anisotropic properties of extruded materials, especially in the ODS ferritic grades (≥wt%12Cr), need a better understanding of the metallurgical phenomena which may occur during HE and lead to the observed microstructure. The hot working behavior of these materials is of particular interest. The methodology of this work includes the microstructure analysis after interrupted hot extrusion, hot torsion and hot compression (1000-1200 C) tests of ferritic steels with 14%Cr and different amounts in Ti and Y 2 O 3 . The microstructure evolution during hot extrusion process is associated with continuous dynamic recrystallization (CDRX). It leads to the creation of new grains by the formation of low angle boundaries, and then the increase of their misorientation under plastic deformation. The investigations highlight also the role of precipitation on the kinetics of this mechanism; it remains incomplete in the presence of fine and dense nano-precipitates. After hot deformation in torsion and compression, it is noticed that both precipitates and temperature deformation have a significant impact on the deformation mechanisms and microstructure evolution. Indeed, the CDRX is dominant when temperature and amount of reinforcement are limited. However, when they are increased, limited microstructure evolution is observed. In this case, the results are interpreted through a mechanism of strain accommodation at grain boundaries, with low dislocation activity in the bulk of the grains. (author) [fr

  2. The effects of cold rolling orientation and water chemistry on stress corrosion cracking behavior of 316L stainless steel in simulated PWR water environments

    Energy Technology Data Exchange (ETDEWEB)

    Chen, Junjie [Institute of Materials Science, School of Materials Science and Engineering, Shanghai University, Mailbox 269, 149 Yanchang Road, Shanghai, 200072 (China); Lu, Zhanpeng, E-mail: zplu@t.shu.edu.cn [Institute of Materials Science, School of Materials Science and Engineering, Shanghai University, Mailbox 269, 149 Yanchang Road, Shanghai, 200072 (China); State Key Laboratory of Advanced Special Steels, Shanghai University, 149 Yanchang Road, Shanghai, 200072 (China); Xiao, Qian; Ru, Xiangkun; Han, Guangdong; Chen, Zhen [Institute of Materials Science, School of Materials Science and Engineering, Shanghai University, Mailbox 269, 149 Yanchang Road, Shanghai, 200072 (China); Zhou, Bangxin [Institute of Materials Science, School of Materials Science and Engineering, Shanghai University, Mailbox 269, 149 Yanchang Road, Shanghai, 200072 (China); State Key Laboratory of Advanced Special Steels, Shanghai University, 149 Yanchang Road, Shanghai, 200072 (China); Shoji, Tetsuo [New Industry Creation Hatchery Center, Tohoku University, Sendai 980-8579 (Japan)

    2016-04-15

    Stress corrosion cracking behaviors of one-directionally cold rolled 316L stainless steel specimens in T–L and L–T orientations were investigated in hydrogenated and deaerated PWR primary water environments at 310 °C. Transgranular cracking was observed during the in situ pre-cracking procedure and the crack growth rate was almost not affected by the specimen orientation. Locally intergranular stress corrosion cracks were found on the fracture surfaces of specimens in the hydrogenated PWR water. Extensive intergranular stress corrosion cracks were found on the fracture surfaces of specimens in deaerated PWR water. More extensive cracks were found in specimen T–L orientation with a higher crack growth rate than that in the specimen L–T orientation with a lower crack growth rate. Crack branching phenomenon found in specimen L–T orientation in deaerated PWR water was synergistically affected by the applied stress direction as well as the preferential oxidation path along the elongated grain boundaries, and the latter was dominant. - Highlights: • Transgranular fatigue crack growth rate was not affected by the cold rolling orientation. • Locally intergranular SCC was found in the hydrogenated PWR water. • Extensive intergranular SCC cracks were found in deaerated PWR water. • T–L specimen showed more extensive SCC cracks and a higher crack growth rate. • Crack branching related to the applied stress and the preferential oxidation path.

  3. Influence of hot rolling and high speed hydrostatic extrusion on the microstructure and mechanical properties of an ODS RAF steel

    Energy Technology Data Exchange (ETDEWEB)

    Oksiuta, Z., E-mail: oksiuta@pb.edu.pl [Bialystok Technical University, Faculty of Mechanical Engineering, Wiejska 45c, 15-352 Bialystok (Poland); Lewandowska, M.; Kurzydlowski, K.J. [Warsaw University of Technology, Faculty of Materials Science and Engineering, Woloska 141, 02-504 Warsaw (Poland); Baluc, N. [Ecole Polytechnique Federale de Lausanne (EPFL), Centre de Recherches en Physique des Plasmas, Association Euratom-Confederation Suisse, 5232 Villigen PSI (Switzerland)

    2011-02-15

    An argon gas atomized, pre-alloyed Fe-14Cr-2W-0.3Ti (wt.%) reduced activation ferritic (RAF) steel powder was mechanically alloyed with 0.3wt.% Y{sub 2}O{sub 3} nano-particles in an attritor ball mill and consolidated by hot isostatic pressing at 1150 {sup o}C under a pressure of 200 MPa for 3 h. In the aim to improve its mechanical properties the ODS steel was then submitted to a thermo-mechanical treatment (TMT): hot rolling (HR) at 850 deg. C or high speed hydrostatic extrusion (HSHE) at 900 deg. C, followed by heat treatment (HT). Transmission electron microscopy (TEM) observations of the ODS alloys after TMT and heat treatment revealed the presence of elongated grains in the longitudinal direction, with an average width of 8 {mu}m and an average length of 75 {mu}m, and equiaxed grains, a few microns in diameter, in the transverse direction. Two populations of oxide particles were observed by TEM: large Ti-Al-O particles, up to 250 nm in diameter, usually located at the grain boundaries and small Y-Ti-O nanoclusters, about 2.5 nm in diameter, uniformly distributed in the matrix. Charpy impact tests revealed that the HSHE material exhibits a larger upper shelf energy (5.8 J) than the HR material (2.9 J). The ductile-to-brittle transition temperature of both alloys is relatively high, in the range of 55-72 deg. C. Tensile mechanical properties of both ODS alloys were found satisfactory over the full range of investigated temperatures (23-750 deg. C). The HSHE material exhibits better tensile strength and ductility than the HR material. These results indicate that HSHE can be considered as a promising TMT method for improving the mechanical properties of ODS RAF steels.

  4. Experimental and Simulation Analysis of Hot Isostatic Pressing of Gas Atomized Stainless Steel 316L Powder Compacts

    International Nuclear Information System (INIS)

    Lin, Dongguo; Park, Seong Jin; Ha, Sangyul; Shin, Youngho; Park, Dong Yong; Chung, Sung Taek; Bollina, Ravi; See, Seongkyu

    2016-01-01

    In this work, both experimental and numerical studies were conducted to investigate the densification behavior of stainless steel 316L (STS 316L) powders during hot isostatic pressing (HIP), and to characterize the mechanical properties of HIPed specimens. The HIP experiments were conducted with gas atomized STS 316L powders with spherical particle shapes under controlled pressure and temperature conditions. The mechanical properties of HIPed samples were determined based on a series of tensile tests, and the results were compared to a reference STS 316L sample prepared by the conventional process, i.e., extrusion and annealing process. Corresponding microstructures before and after tensile tests were observed using scanning electron microscopy and their relationships to the mechanical properties were addressed. Furthermore, a finite element simulation based on the power-law creep model was carried out to predict the density distribution and overall shape change of the STS316L powder compact during HIP process, which agreed well with the experimental results.

  5. Experimental and Simulation Analysis of Hot Isostatic Pressing of Gas Atomized Stainless Steel 316L Powder Compacts

    Energy Technology Data Exchange (ETDEWEB)

    Lin, Dongguo; Park, Seong Jin [Pohang University of Science and Technology, Pohang (Korea, Republic of); Ha, Sangyul [Samsung Electro-Mechanics, Suwon (Korea, Republic of); Shin, Youngho [Doosan Heavy Industries and Construction Co., Ltd., Changwon (Korea, Republic of); Park, Dong Yong [Korea Institute of Energy Research, Daejeon (Korea, Republic of); Chung, Sung Taek [CetaTech Inc., Sacheon (Korea, Republic of); Bollina, Ravi [Bahadurpally Jeedimetla, Hyderabad (India); See, Seongkyu [POSCO, Pohang (Korea, Republic of)

    2016-10-15

    In this work, both experimental and numerical studies were conducted to investigate the densification behavior of stainless steel 316L (STS 316L) powders during hot isostatic pressing (HIP), and to characterize the mechanical properties of HIPed specimens. The HIP experiments were conducted with gas atomized STS 316L powders with spherical particle shapes under controlled pressure and temperature conditions. The mechanical properties of HIPed samples were determined based on a series of tensile tests, and the results were compared to a reference STS 316L sample prepared by the conventional process, i.e., extrusion and annealing process. Corresponding microstructures before and after tensile tests were observed using scanning electron microscopy and their relationships to the mechanical properties were addressed. Furthermore, a finite element simulation based on the power-law creep model was carried out to predict the density distribution and overall shape change of the STS316L powder compact during HIP process, which agreed well with the experimental results.

  6. Quantitative influence of minor and impurity elements on hot cracking susceptibility of extra high-purity type 310 stainless steel

    International Nuclear Information System (INIS)

    Saida, Kazuyoshi; Matsushita, Hideki; Nishimoto, Kazutoshi; Kiuchi, Kiyoshi; Nakayama, Junpei

    2013-01-01

    To evaluate the influence of minor and impurity elements such as C, Mn, P and S on the solidification and ductility-dip cracking susceptibilities of extra high-purity type 310 stainless steels, the transverse-Varestraint test was conducted by using several type 310 stainless steels with different amounts of C, Mn, P and S. Two types of hot cracks occurred in these steels by Varestraint test; solidification and ductility-dip cracks. The solidification cracking susceptibility was significantly reduced as the amounts of C, P and S decreased. The ductility-dip cracking susceptibility also reduced with a decrease in P and S contents. It adversely, however, increased as the C content of the steels was reduced. Mn didn't greatly affect the hot cracking susceptibility of the extra high-purity steels. The characteristic influence on solidification cracking was the ratio of P:S:C=1:1.3:0.56, while Mn negligibly ameliorated solidification cracking in the extra low S (and P) steels. The numerical analysis on the solidification brittle temperature range (BTR) revealed that the reduced solidification cracking susceptibility with decreasing the amounts of C, P and S in steel could be attributed to the reduced BTR due to the suppression of solidification segregation of minor and impurity elements in the finally solidified liquid film between dendrites. On the other hand, a molecular orbital analysis to estimate the binding strength of the grain boundary suggested that the increased ductility-dip cracking susceptibility in extra high-purity steels was caused by grain boundary embrittlement due to the refining of beneficial elements for grain boundary strengthening such as C. (author)

  7. A Study on the Low Temperature Brittleness by Cyclic Cooling-Heating of Low Carbon Hot Rolled Steel Plate

    International Nuclear Information System (INIS)

    Lee, Hyo Bok

    1979-01-01

    The ductile-brittle transition phenomenon of low carbon steel has been investigated using the standard Charpy V-notch specimen. Dry ice and acetone were used as refrigerants. Notched specimens were cut from the hot rolled plate produced at POSCO for the Olsen impact test. The effect of cyclic cooling and heating of 0.14% carbon steel on the embrittlement was extensively examined. The ductile-brittle transition temperature was found to be approximately-30 .deg. C. The transition temperature was gradually increased as the number of cooling-heating cycles increased. On a typical V-notch fracture surface it was found that the ductile fracture surface showed a thick and fibrous structure, while the brittle fracture surface a small and light grain with irregular disposition. As expected, the transition temperature was also increased as the carbon content of steel increased. Compared with the case of 0.14% carbon steel, the transition temperature of 0.17% carbon steel was found to be increased about 12 .deg. C

  8. Effect of decreased hot-rolling reduction treatment on fracture toughness of low-alloy structural steels

    Science.gov (United States)

    Tomita, Yoshiyuki

    1990-09-01

    Commercial low-alloy structural steels, 0.45 pct C (AISI 1045 grade), 0.40 pct C-Cr-Mo (AISI 4140 grade), and 0.40 pct C-Ni-Cr-Mo (AISI 4340 grade), have been studied to determine the effect of the decreased hot-rolling reduction treatment (DHRRT) from 98 to 80 pct on fracture toughness of quenched and highly tempered low-alloy structural steels. The significant conclusions are as follows: (1) the sulfide inclusions were modified through the DHRRT from a stringer (mean aspect ratio: 16.5 to 17.6) to an ellipse (mean aspect ratio: 3.8 to 4.5), independent of the steels studied; (2) the DHRRT significantly improved J Ic in the long-transverse and shorttransverse orientations, independent of the steels studied; and (3) the shelf energy in the Charpy V-notch impact test is also greatly improved by the DHRRT, independent of testing orientation and steels studied; however, (4) the ductile-to-brittle transition temperature was only slightly affected by the DHRRT. The beneficial effect on the J Ic is briefly discussed in terms of a crack extension model involving the formation of voids at the inclusion sites and their growth and eventual linking up through the rupture of the intervening ligaments by local shear.

  9. Effect of microstructural anisotropy on fracture toughness of hot rolled 13Cr ODS steel - The role of primary and secondary cracking

    Science.gov (United States)

    Das, A.; Viehrig, H. W.; Bergner, F.; Heintze, C.; Altstadt, E.; Hoffmann, J.

    2017-08-01

    ODS steels have been known to exhibit anisotropic fracture behaviour and form secondary cracks. In this work, the factors responsible for the anisotropic fracture behaviour have been investigated using scanning electron microscopy and electron backscatter microscopy. Fracture toughness of hot rolled 13Cr ODS steel was determined using unloading compliance method for L-T and T-L orientations at various temperatures. L-T orientation had higher fracture toughness than T-L orientation and also contained more pronounced secondary cracking. Secondary cracks appeared at lower loads than primary cracks in both orientations. Primary crack propagation was found to be preferentially through fine grains in a bimodal microstructure. Grains were aligned and elongated the most towards rolling direction followed by T and S directions resulting in fracture anisotropy. Crystallographic texture and preferential alignment of Ti enriched particles parallel to rolling direction also contributed towards fracture anisotropy.

  10. Nickel alloys and high-alloyed special stainless steels. Properties, manufacturing, applications. 4. compl. rev. ed.

    International Nuclear Information System (INIS)

    Heubner, Ulrich; Kloewer, Jutta; Alves, Helena; Behrens, Rainer; Schindler, Claudius; Wahl, Volker; Wolf, Martin

    2012-01-01

    This book contains the following eight topics: 1. Nickel alloys and high-alloy special stainless steels - Material overview and metallurgical principles (U. Heubner); 2. Corrosion resistance of nickel alloys and high-alloy special stainless steels (U. Heubner); 3. Welding of nickel alloys and high-alloy special stainless steels (T. Hoffmann, M. Wolf); 4. High-temperature materials for industrial plant construction (J. Kloewer); 5. Nickel alloys and high-alloy special stainless steels as hot roll clad composites-a cost-effective alternative (C. Schindler); 6. Selected examples of the use of nickel alloys and high-alloy special stainless steels in chemical plants (H. Alves); 7. The use of nickel alloys and stainless steels in environmental engineering (V. Wahl); 8: Nickel alloys and high-alloy special stainless steels for the oil and gas industry (R. Behrens).

  11. Hot rolling and annealing effects on the microstructure and mechanical properties of ODS austenitic steel fabricated by electron beam selective melting

    Science.gov (United States)

    Gao, Rui; Ge, Wen-jun; Miao, Shu; Zhang, Tao; Wang, Xian-ping; Fang, Qian-feng

    2016-03-01

    The grain morphology, nano-oxide particles and mechanical properties of oxide dispersion strengthened (ODS)-316L austenitic steel synthesized by electron beam selective melting (EBSM) technique with different post-working processes, were explored in this study. The ODS-316L austenitic steel with superfine nano-sized oxide particles of 30-40 nm exhibits good tensile strength (412 MPa) and large total elongation (about 51%) due to the pinning effect of uniform distributed oxide particles on dislocations. After hot rolling, the specimen exhibits a higher tensile strength of 482 MPa, but the elongation decreases to 31.8% owing to the introduction of high-density dislocations. The subsequent heat treatment eliminates the grain defects induced by hot rolling and increases the randomly orientated grains, which further improves the strength and ductility of EBSM ODS-316L steel.

  12. The influence of the hardening coolant agent on the properties of hot rolled bars of the steel 42CrMo4

    Directory of Open Access Journals (Sweden)

    M. Stańczyk

    2014-10-01

    Full Text Available In the work the influence results of two different hardening coolant agents on the basic mechanical proprieties and microstructure of the round hot rolled bars were presented. The bars of 42CrMo4 steel were exposed to analysis, and for those bars in the hardening process, water and modern pro-ecological polymer cooling agents Aqua Quench MK were used.

  13. A study on the mechanism of stress corrosion cracking of duplex stainless steels in hot alkaline-sulfide solution

    Science.gov (United States)

    Chasse, Kevin Robert

    Duplex stainless steels (DSS) generally have superior strength and corrosion resistance as compared to most standard austenitic and ferritic stainless grades owing to a balanced microstructure of austenite and ferrite. As a result of having favorable properties, DSS have been selected for the construction of equipment in pulp and paper, chemical processing, nuclear, oil and gas as well as other industries. The use of DSS has been restricted in some cases because of stress corrosion cracking (SCC), which can initiate and grow in either the ferrite or austenite phase depending on the environment. Thorough understanding of SCC mechanisms of DSS in chloride- and hydrogen sulfide-containing solutions has been useful for material selection in many environments. However, understanding of SCC mechanisms of DSS in sulfide-containing caustic solutions is limited, which has restricted the capacity to optimize process and equipment design in pulp and paper environments. Process environments may contain different concentrations of hydroxide, sulfide, and chloride, altering corrosion and SCC susceptibility of each phase. Crack initiation and growth behavior will also change depending on the relative phase distribution and properties of austenite and ferrite. The role of microstructure and environment on the SCC of standard grade UNS S32205 and lean grade UNS S32101 in hot alkaline-sulfide solution were evaluated in this work using electrochemical, film characterization, mechanical testing, X-ray diffraction, and microscopy techniques. Microstructural aspects, which included residual stress state, phase distribution, phase ratio, and microhardness, were related to the propensity for SCC crack initiation in different simulated alkaline pulping liquors at 170 °C. Other grades of DSS and reference austenitic and superferritic grades of stainless steel were studied using exposure coupons for comparison to understand compositional effects and individual phase susceptibility

  14. Investigation of the influence of the chemical composition of HSLA steel grades on the microstructure homogeneity during hot rolling in continuous rolling mills using a fast layer model

    International Nuclear Information System (INIS)

    Schmidtchen, M; Kawalla, R; Rimnac, A; Bragin, S; Linzer, B; Warczok, P; Kozeschnik, E; Bernhard, C

    2016-01-01

    The newly developed LaySiMS simulation tool provides new insight for inhomogeneous material flow and microstructure evolution in an endless strip production (ESP) plant. A deepened understanding of the influence of inhomogeneities in initial material state, temperature profile and material flow and their impact on the finished product can be reached e.g. by allowing for variable layer thickness distributions in the roll gap. Coupling temperature, deformation work and work hardening/recrystallization phenomena accounts for covering important effects in the roll gap. The underlying concept of the LaySiMS approach will be outlined and new insight gained regarding microstructural evolution, shear and inhomogeneous stress and strain states in the roll gap as well as local residual stresses will be presented. For the case of thin slab casting and direct rolling (TSDR) the interrelation of inhomogeneous initial state, micro structure evolution and dissolution state of micro alloying elements within the roughing section of an ESP line will be discussed. Special emphasis is put on the influence of the local chemical composition arising from direct charging on throughthickness homogeneity of the final product. It is concluded that, due to the specific combination of large reductions in the high reduction mills (HRM) and the highly inhomogeneous inverse temperature profile, the ESP-concept provides great opportunities for homogenizing the microstructure across the strip thickness. (paper)

  15. UTILIZATION OF TORAY FLY ASH AS FILLER SUBSTITUTION IN THE HOT ROLLED SHEET-WEARING COURSE (HRS-WC MIXTURE

    Directory of Open Access Journals (Sweden)

    F. Candra

    2012-02-01

    Full Text Available In road construction materials, the utilization of fly ash as additive materials is limited and also small in quantity, while the disposal of fly ash is quite high. An abundance of fly ash can be found at PT Toray Company in Jakarta and Surabaya. Toray fly ash is disposed coal ash resulting from coal-fired electricity generating power plants. Toray fly ash in this research is used as substitute mineral filler in asphalt paving mixtures. Research on utilization of Toray fly ash as filler is conducted in the Hot Rolled Sheet – Wearing Course Mixture.  Filler content in the HRS –WC mixture is 9%. Variations of Toray fly ash in the mixture tested are 0%, 25%, 50%, 75%, 100% and the variations of asphalt content are 6%, 6.5%, 7%, 7.5%, 8%. Marshall test is  performed to determine the Optimum Asphalt Content  and Marshall Stability, Indirect Tensile Strength (ITS test and Tensile Strength Ratio (TSR to select the optimum Toray fly ash utilization in the mixture based on the moisture susceptibility of specimens. The research results show that in variations of 0%, 25%, 50%, 75% and 100% Toray fly ash in the HRS-WC Mixture, the Optimum Asphalt Contents are at 6.8%, 7.0%, 7.0%, 7.1% and 7.6%  and Marshall Stability values of the variations are 1649 kg, 1541 kg, 1568 kg, 1678 kg, 1718 kg respectively. TSR values in variations of Toray fly ash are 98.32%, 90.28%, 89.38%, 87.62%, 64.71% respectively, with Minimum TSR value required is 80%. Based on the overall parameters, the optimum Toray fly ash utilization in the HRS-WC Mixture recommended is 75% of Toray fly ash at 7.1% Optimum Asphalt Content.

  16. Microstructure and partitioning behavior characteristics in low carbon steels treated by hot-rolling direct quenching and dynamical partitioning processes

    International Nuclear Information System (INIS)

    Li, Yun-jie; Li, Xiao-lei; Yuan, Guo; Kang, Jian; Chen, Dong; Wang, Guo-dong

    2016-01-01

    In this work, a new process and composition design are proposed for “quenching and partitioning” or Q&P treatment. Three low carbon steels were treated by hot-rolling direct quenching and dynamical partitioning processes (DQ&P). The effects of proeutectoid ferrite and carbon concentration on microstructure evolution and mechanical properties were investigated. The present work obtained DQ&P prototype steels with good mechanical properties and established a new notion on compositions for Q&P processing. Microstructures were characterized by means of electro probe microanalyzer (EPMA), scanning electron microscopy (SEM), electron backscatter diffraction (EBSD), transmission electron microscopy (TEM) and X-ray diffraction (XRD), especially the morphology and size of retained austenite. Mechanical properties were measured by uniaxial tensile tests. The results indicated that introducing proeutectoid ferrite can increase the volume fraction of retained austenite and thus improve mechanical properties. TEM observation showed that retained austenite included the film-like inter-lath austenite and blocky austenite located in martensite/ferrite interfaces or surrounded by ferrites. It was interesting that when the carbon concentration is as low as ~ 0.078%, the film-like inter-lath untransformed austenite cannot be stabilized to room temperature and almost all of them transformed into twin martensite. The blocky retained austenite strengthened the interfaces and transformed into twin martensite during the tensile deformation process. The PSEs of specimens all exceeded 20 GPa.%. - Highlights: •This study focused on a new process: Q&P process applying dynamical partitioning. •Ferrite can increase the volume fraction of retained austenite. •The film-like austenite and the blocky austenite were observed. •The low carbon steels treated by new process reached PSEs higher than 20 GPa.%.

  17. Effects of external stresses on hot corrosion behavior of stainless steel TP347HFG

    International Nuclear Information System (INIS)

    Fu, Jiapeng; Zhou, Qulan; Li, Na; Liu, Zhuhan; Liu, Taisheng

    2016-01-01

    Highlights: • Hot corrosion tests of TP347HFG under different stresses were conducted. • The corrosion resistance was strengthened by the exertion of tensile stresses. • External stresses promoted faster formation of the protective Cr_2O_3 layer. • Specimens under critical stress 40 MPa condition present the best resistance. - Abstract: Hot corrosion experiments of alloy TP347HFG under different stresses were conducted. Corroded specimens were examined by means of corrosion products, morphology and compositional changes in corrosion scales. The corrosion behavior was strongly associated with the formation of oxides layers. The corrosion resistance was strengthened by the external stress. It seemed that the exertion of stresses caused many micro cracks and defects, which acted as faster and easier diffusion paths for Cr atoms to diffuse to the surface, and thus, promote faster formation of the protective Cr_2O_3 oxide layer. Critical stress 40 MPa was found, specimens under which present the best resistance.

  18. Welding hot cracking in an austenitic stainless steel; Fissuration a chaud en soudage d'un acier inoxydable austenitique

    Energy Technology Data Exchange (ETDEWEB)

    Kerrouault, N

    2001-07-01

    The occurrence of hot cracking is linked to several conditions, in particular, the composition of the material and the local strains due to clambering. The aim of this study is to better analyse the implied mechanisms and to lead to a local thermomechanical criterion for hot cracking. The example studied is an AISI 321-type stainless steel (X10CrNiTi18-12) strongly prone to cracking. Two weldability tests are studied: - the first one consists in carrying out a fusion line by the TIG process on a thin sheet. In the case of the defect occurrence, the crack is longitudinal and follows the back of the molten bath. The influence of the operating conditions welding (speed, welding heat input, width test sample) is studied. - the second one is the Varestraint test. It is widely used to evaluate the sensitivity of a material to hot cracking. It consists in loading the material by bending during a fusion line by the TIG process and in characterising the defects quantity (length, number). Various thermal and mechanical instrumentation methods were used. The possibilities of a local instrumentation instrumentation being limited because of the melting, the experimental results were complemented by a numerical modelling whose aim is to simulate the thermomechanical evolution of the loading thanks to the finite element analysis code ABAQUS. First, the heat input for thermal simulation is set by the use of an inverse method in order to optimise the energy deposit mode during welding in the calculation. Then, the mechanical simulation needs the input of a constitutive law that fits the mechanical behaviour over a wide temperature range from ambient to melting temperature. Thus, a mechanical characterization is performed by selecting strain values and strain rates representative of what the material undergoes during the tests. The results come from tensile and compressive tests and allow to settle an elasto-visco-plastic constitutive law over temperatures up to liquidus. Once

  19. Development of Duplex Stainless Steels by Field-Assisted Hot Pressing: Influence of the Particle Size and Morphology of the Powders on the Final Mechanical Properties

    Science.gov (United States)

    García-Junceda, A.; Rincón, M.; Torralba, J. M.

    2018-01-01

    The feasibility of processing duplex stainless steels with promising properties using a powder metallurgical route, including the consolidation by field-assisted hot pressing, is assessed in this investigation. The influence of the particle size and morphology of the raw austenitic and ferritic powders on the final microstructure and properties is also evaluated for an austenitic content of 60 wt pct. In addition, the properties of a new microconstituent generated between the initial constituents are analyzed. The maximum sintered density (98.9 pct) and the best mechanical behavior, in terms of elastic modulus, nanohardness, yield strength, ultimate tensile strength, and ductility, are reached by the duplex stainless steel processed with austenitic and ferritic gas atomized stainless steel powders.

  20. Hot Deformation Behavior of 1Cr12Ni3Mo2VN Martensitic Stainless Steel

    Science.gov (United States)

    He, Xiaomao; Jiang, Peng; Zhou, Leyu; Chen, Chao; Deng, Xiaochun

    2017-08-01

    1Cr12Ni3Mo2VN is a new type of martensitic stainless steel for the last-stage blades of large-capacity nuclear and thermal power turbines. The deformation behavior of this steel was studied by thermal compression experiments that performed on a Gleeble-3500 thermal simulator at a temperature range of 850°C to 1200°C and a strain rate of 0.01s-1 to 20s-1. When the deformation was performed at high temperature and low strain rate, a necklace type of microstructures was observed, the plastic deformation mechanism is grain boundary slip and migration, when at low temperature and lower strain rate, the slip bands were observed, the mechanism is intracrystalline slips, and when at strain rate of 20s-1, twins were observed, the mechanism are slips and twins. The Arrhenius equation was applied to describe the constitutive equation of the flow stress. The accuracy of the equation was verified by using the experimental data and the correlation coefficient R2 = 0.9786, and the equation can provide reasonable data for the design and numerical simulation of the forging process.

  1. Softening mechanisms of the AISI 410 martensitic stainless steel under hot torsion simulation

    Energy Technology Data Exchange (ETDEWEB)

    Oliveira, Thiago Santana de; Silva, Eden Santos; Rodrigues, Samuel Filgueiras; Nascimento, Carmem Celia Francisco; Leal, Valdemar Silva; Reis, Gedeon Silva, E-mail: samuel.filgueiras@ifma.edu.br [Instituto Federal do Maranhao (PPGEM/IFMA), Sao Luis, MA (Brazil)

    2017-03-15

    This study investigated the softening mechanisms of the AISI 410 martensitic stainless steel during torsion simulation under isothermal continuous in the temperature range of 900 to 1150 °C and strain rates of 0.1 to 5.0s{sup -1}. In the first part of the curves, before the peak, the results show that the critical (ε-c) and peak (ε-p) strains are elevated for higher strain rate and lower temperatures contributing for higher strain hardening rate (h). Moreover, this indicated that dynamic recrystallization (DRX) and dynamic recovery (DRV) are not effective in this region. After the peak, the reductions in stresses are associated to the different DRX/DRV competitions. For lower temperatures and higher strain rates there is a delay in the DRX while the DRV is acting predominantly (with low Avrami exponent (n) and high t{sub 0.5}). The steady state was reached after large strains showing DRX grains, formation of retained austenite and the presence of chromium carbide (Cr{sub 23}C{sub 6}) and ferrite δ at the martensitic grain boundaries. These contribute for impairing the toughness and ductility on the material. The constitutive equations at the peak strain indicated changes in the deformation mechanism, with variable strain rate sensitivity (m), which affected the final microstructure. (author)

  2. Microstructure and mechanical properties of hot wire laser clad layers for repairing precipitation hardening martensitic stainless steel

    Science.gov (United States)

    Wen, Peng; Cai, Zhipeng; Feng, Zhenhua; Wang, Gang

    2015-12-01

    Precipitation hardening martensitic stainless steel (PH-MSS) is widely used as load-bearing parts because of its excellent overall properties. It is economical and flexible to repair the failure parts instead of changing new ones. However, it is difficult to keep properties of repaired part as good as those of the substrate. With preheating wire by resistance heat, hot wire laser cladding owns both merits of low heat input and high deposition efficiency, thus is regarded as an advantaged repairing technology for damaged parts of high value. Multi-pass layers were cladded on the surface of FV520B by hot wire laser cladding. The microstructure and mechanical properties were compared and analyzed for the substrate and the clad layer. For the as-cladded layer, microstructure was found non-uniform and divided into quenched and tempered regions. Tensile strength was almost equivalent to that of the substrate, while ductility and impact toughness deteriorated much. With using laser scanning layer by layer during laser cladding, microstructure of the clad layers was tempered to fine martensite uniformly. The ductility and toughness of the clad layer were improved to be equivalent to those of the substrate, while the tensile strength was a little lower than that of the substrate. By adding TiC nanoparticles as well as laser scanning, the precipitation strengthening effect was improved and the structure was refined in the clad layer. The strength, ductility and toughness were all improved further. Finally, high quality clad layers were obtained with equivalent or even superior mechanical properties to the substrate, offering a valuable technique to repair PH-MSS.

  3. Effect of copper, tin, phosphorous and arsenic on the surface cracking of a 18-8 stainless steel during hot compression tests

    International Nuclear Information System (INIS)

    Botella, J.; Fernandez, M.T.; Fernandez de Castillo, I.

    1998-01-01

    The effect of certain different concentrations of Cu, Sn, P and As on the surface cracking of 18-8 austenitic stainless steel hot compressed specimens has been studied, at 1,123 and 1,273 K, in an oxidizing atmosphere (air). A procedure for determining surface cracking has been established, and the cracking factor obtained in this ways is correlated with the chemical composition of the materials at both temperatures. The cracking factors obtained at 1,273 K have been compared with the reduction of area drops obtained by hot tension tests at the same temperature. (Author) 5 refs

  4. Physical Simulation of a Duplex Stainless Steel Friction Stir Welding by the Numerical and Experimental Analysis of Hot Torsion Tests

    Science.gov (United States)

    da Fonseca, Eduardo Bertoni; Santos, Tiago Felipe Abreu; Button, Sergio Tonini; Ramirez, Antonio Jose

    2016-09-01

    Physical simulation of friction stir welding (FSW) by means of hot torsion tests was performed on UNS S32205 duplex stainless steel. A thermomechanical simulator Gleeble 3800® with a custom-built liquid nitrogen cooling system was employed to reproduce the thermal cycle measured during FSW and carry out the torsion tests. Microstructures were compared by means of light optical microscopy and electron backscatter diffraction. True strain and strain rate were calculated by numerical simulation of the torsion tests. Thermomechanically affected zone (TMAZ) was reproduced at peak temperature of 1303 K (1030 °C), rotational speeds of 52.4 rad s-1 (500 rpm) and 74.5 rad s-1 (750 rpm), and 0.5 to 0.75 revolutions, which represent strain rate between 10 and 16 s-1 and true strain between 0.5 and 0.8. Strong grain refinement, similar to the one observed in the stir zone (SZ), was attained at peak temperature of 1403 K (1130 °C), rotational speed of 74.5 rad s-1 (750 rpm), and 1.2 revolution, which represent strain rate of 19 s-1 and true strain of 1.3. Continuous dynamic recrystallization in ferrite and dynamic recrystallization in austenite were observed in the TMAZ simulation. At higher temperature, dynamic recovery of austenite was also observed.

  5. Influence o the microstructure of duplex stainless steels on their failure characteristics during hot deformation

    Directory of Open Access Journals (Sweden)

    Reis G.S.

    2000-01-01

    Full Text Available Two types of duplex stainless steels were deformed by torsion at a temperature range of 900 to 1200 °C and strain rate of 1.0 s-1 and their final microstructures were observed. The austenite volume fraction of steel A (26.5Cr - 4.9Ni - 1.6Mo is approximately 25% at room temperature, after conventional annealing, while that of steel B (24Cr - 7.5Ni - 2.3Mo is around 55%. Experimental data show that steel A is ductile at high temperatures and displays low ductility at low temperatures, while steel B has low ductility in the entire range of temperatures studied. At high temperatures, steel A is essentially ferritic and shows dynamic recrystallized grains after deformation. When steel A is strained at low temperatures and displays low austenite volume fraction, microstructural observations indicate that failure is triggered by grain boundary sliding due to the formation of an austenite net structure at the ferrite grain boundaries. At intermediate volume fraction, when austenite forms a dispersed second-phase in steels A and B, failure begins at the ferrite/ferrite boundaries since some of the new ferrite grains may become immobilized by the austenite particles. When steel B is strained at volume fraction of around 50% of austenite and both phases percolate the microstructure, failure occurs after low straining as a consequence of the different plastic behaviors of each of the phases. The failure characteristics of both steels are correlated not only with the volume fraction of austenite but also with its distribution within the ferrite matrix, which limits attainable strain without failure.

  6. Effect of intercritical deformation on microstructure and mechanical properties of a low-silicon aluminum-added hot-rolled directly quenched and partitioned steel

    Energy Technology Data Exchange (ETDEWEB)

    Tan, Xiao-Dong, E-mail: tan.x@mpie.de [State Key Laboratory of Rolling and Automation, Northeastern University, Shenyang 110819 (China); Max-Planck-Institut für Eisenforschung GmbH, Max-Planck-Str. 1, 40237 Düsseldorf (Germany); Xu, Yun-Bo, E-mail: yunbo_xu@126.com [State Key Laboratory of Rolling and Automation, Northeastern University, Shenyang 110819 (China); Ponge, Dirk [Max-Planck-Institut für Eisenforschung GmbH, Max-Planck-Str. 1, 40237 Düsseldorf (Germany); Yang, Xiao-Long; Hu, Zhi-Ping; Peng, Fei [State Key Laboratory of Rolling and Automation, Northeastern University, Shenyang 110819 (China); Ju, Xiao-Wei [CERI LONG PRODUCT CO., LTD., Beijing 100176 (China); Wu, Di [State Key Laboratory of Rolling and Automation, Northeastern University, Shenyang 110819 (China); Raabe, Dierk [Max-Planck-Institut für Eisenforschung GmbH, Max-Planck-Str. 1, 40237 Düsseldorf (Germany)

    2016-02-22

    Here, we applied hot-rolling in conjunction with direct quenching and partitioning (HDQ&P) processes with different rolling schedules to a low-C low-Si Al-added steel. Ferrite was introduced into the steel by intercritical rolling and air cooling after hot-rolling. The effect of intercritcal deformation on the microstructure evolution and mechanical properties was investigated. The promotion of austenite stabilization and the optimization of the TRIP effect due to a moderate degree of intercritical deformation were systematically explored. The results show that the addition of 1.46 wt% of Al can effectively promote ferrite formation. An intercritical deformation above 800 °C can result in a pronounced bimodal grain size distribution of ferrite and some elongated ferrite grains containing sub-grains. The residual strain states of both austenite and ferrite and the occurrence of bainite transformation jointly increase the retained austenite fraction due to its mechanical stabilization and the enhanced carbon partitioning into austenite from its surrounding phases. An intercritical deformation below 800 °C can profoundly increase the ferrite fraction and promote the recrystallization of deformed ferrite. The formation of this large fraction of ferrite enhances the carbon enrichment in the untransformed austenite and retards the bainite transformation during the partitioning process and finally enhances martensite transformation and decreases the retained austenite fraction. The efficient TRIP effect of retained austenite and the possible strain partitioning of bainite jointly improve the work hardening and formability of the steel and lead to the excellent mechanical properties with relatively high tensile strength (905 MPa), low yield ratio (0.60) and high total elongation (25.2%).

  7. Application of the Finite Element Method to Reveal the Causes of Loss of Planeness of Hot-Rolled Steel Sheets during Laser Cutting

    Science.gov (United States)

    Garber, E. A.; Bolobanova, N. L.; Trusov, K. A.

    2018-01-01

    A finite element technique is developed to simulate the stresses and the strains during strip flattening to reveal the causes of the cutting-assisted loss of planeness of hot-rolled steel sheets processed in roller levelers. The loss of planeness is found to be caused by a nonuniform distribution of the flattening-induced longitudinal tensile stresses over the strip thickness and width. The application of tensile forces to a strip in a roller leveler decreases this nonuniformity and prevents loss of planeness in cutting.

  8. Effect of Strength Coefficient of Bainite on Micromechanical Deformation and Failure Behaviors of Hot-Rolled 590FB Steel during Uniaxial Tension

    Energy Technology Data Exchange (ETDEWEB)

    Kim, Eun-Young; Choi, Shi-Hoon [Sunchon National University, Suncheon (Korea, Republic of); Kim, Sung Il [POSCO Technical Research Laboratories, Gwangyang (Korea, Republic of)

    2016-11-15

    The effect of the strength coefficient (K{sub B}) of bainite on micromechanical deformation and failure behaviors of a hot-rolled 590MPa steel (590FB) during uniaxial tension was simulated using the elasto-plastic finite element method (FEM). The spatial distribution of the constituent phases was obtained using a phase identification technique based on optical microstructure. Empirical equations which depend on chemical composition were used to determine the stress-strain relationship of the constituent phases of the 590FB steel. The stress-strain partitioning and failure behavior were analyzed by increasing the K{sub B} of bainite. The elasto-plastic FEM results revealed that effective strain in the ferrite-bainite boundaries, and maximum principal stress in fibrous bainite, were enhanced as the K{sub B} increased. The elasto-plastic FEM results also demonstrated that the K{sub B} significantly affects the micromechanical deformation and failure behaviors of the hot-rolled 590FB steel during uniaxial tension.

  9. 77 FR 70142 - Initialed Draft Revision to the Agreement Suspending the Antidumping Investigation on Certain Hot...

    Science.gov (United States)

    2012-11-23

    ... the Agreement Suspending the Antidumping Investigation on Certain Hot-Rolled Flat-Rolled Carbon... revision to the Agreement Suspending the Antidumping Investigation on Certain Hot-Rolled Flat-Rolled Carbon...'') investigation on hot-rolled flat-rolled carbon-quality steel products (``hot-rolled steel'') from the Russian...

  10. Refinement of the microstructure of steel by cross rolling

    International Nuclear Information System (INIS)

    Tsay, Kira; Arbuz, Alexandr; Gusseynov, Nazim; Nemkaeva, Renata; Ospanov, Nurlan; Krupen'kin, Ivan

    2016-01-01

    One of the most effective ways for refinement of metal microstructure is a severe plastic deformation. The cross rolling is the one of most perspective methods of severe plastic deformation, because it allows to get the long billets, unlike equal angular pressing and other popular methods. This fact provides some industrial expectation for this method. However, deformation and motion path of the metal is very heterogeneous across the section of the rolled piece. This paper presents the finite element modeling of hot cross rolling of steel in the software package DEFORM-3D features implemented and studied the stress-strain state. An experimental study of the effect of the cross rolling on a three-roll mill on the microstructure of structural alloy steel and stainless steel AISI321 in different zones of the bar. Analysis of microsections made after rolling with high total stretch and the final pass temperature 700°C, shows the formation of equiaxial ultrafinegrain structure on the periphery of an elongated rod and “rolling” texture in the central zone. The resulting microstructure corresponds to that obtained in models of stress-strain state. Keywords: cross rolling, ultra-fine grain structure, steel.

  11. Effect of Cooling Rate on the Microstructure and Mechanical Properties of C-Mn-Al-Si-Nb Hot-Rolled TRIP Steels

    Science.gov (United States)

    Fu, B.; Y Lu, M.; Y Yang, W.; Li, L. F.; Y Zhao, Z.

    2017-12-01

    A novel thermomechanical process to manufacture hot-rolled TRIP steels has been proposed based on dynamic transformation of undercooled austenite (DTUA). The cooling rate between DTUA and isothermal bainitic treatment in the novel process is important. In the present study, effect of this cooling rate on the final microstructures and mechanical properties of a C-Mn-Al-Si-Nb TRIP steel was investigated. The results showed that the volume fractions of acicular ferrite and retained austenite were increased with the increment of cooling rate. As a consequence, higher yield strength and larger total elongation were obtained for the investigated steel with higher cooling rate. In addition, a value of 30.24 GPa% for the product of tensile strength and total elongation was acquired when the cooling rate was 25 K/s. This value has met the standard of the “Third Generation” of advanced high strength sheet steels.

  12. Research on the Microstructures and Mechanical Properties of Ti Micro-Alloyed Cold Rolled Hot-Dip Galvanizing DP980 Steel

    Science.gov (United States)

    Han, Yun; Kuang, Shuang; Qi, Xiumei; Xie, Chunqian; Liu, Guanghui

    Effects of galvanizing simulation parameters on microstructures and mechanical properties of Ti-microalloyed cold rolled hot-dip galvanizing DP980 steel were investigated in this study by optical microscopy (OM), transmission electron microscopy (TEM), energy dispersive spectroscopy (EDS) and tensile test. Moreover, the precipitation behavior of Ti in the experimental steel was also studied. The results show that, as the heating temperature increases, the tensile strength of experimental galvanizing DP980 steel decreases while the yield ratio and elongation of the steel are enhanced. The microstructures of experimental steels exhibit typical dual phase steel character and the volume fractions of MA islands are almost 30%. In addition, lots of nano-sized TiC precipitates can be found in the ferrite grains.

  13. Influence of Al content on the corrosion resistance of micro-alloyed hot rolled steel as a function of grain size

    Science.gov (United States)

    Qaban, Abdullah; Naher, Sumsun

    2018-05-01

    High-strength low-alloy steel (HSLA) has been widely used in many applications involving automobiles, aerospace, construction, and oil and gas pipelines due to their enhanced mechanical and chemical properties. One of the most critical elements used to improve these properties is Aluminium. This work will explore the effect of Al content on the corrosion behaviour of hot rolled high-strength low-alloy steel as a function of grain size. The method of investigation employed was weight loss technique. It was obvious that the increase in Al content enhanced corrosion resistance through refinement of grain size obtained through AlN precipitation by pinning grain boundaries and hindering their growth during solidification which was found to be beneficial in reducing corrosion rate.

  14. Effect of two-step intercritical annealing on microstructure and mechanical properties of hot-rolled medium manganese TRIP steel containing δ-ferrite

    International Nuclear Information System (INIS)

    Xu, Yun-bo; Hu, Zhi-ping; Zou, Ying; Tan, Xiao-dong; Han, Ding-ting; Chen, Shu-qing; Ma, De-gang; Misra, R.D.K.

    2017-01-01

    The microstructure-properties relationship, work-hardening behavior and retained austenite stability have been systematically investigated in a hot-rolled medium manganese transformation-induced-plasticity (TRIP) steel containing δ-ferrite subjected to one-step and two-step intercritical annealing. The steel exhibited tensile strength of 752 MPa and total elongation of 52.7% for one-step intercritical annealing at 740 °C, tensile strength of 954 MPa and total elongation of 39.2% in the case of intercritical quenching at 800 °C and annealing at 740 °C. The austenite obtained by two-step annealing mostly consists of refined lath structures and increased fraction of block-type particles existing at various kinds of sites, which is highly distinguished from those characterized by long lath morphology and small amounts of granular shape in one-step annealed samples. In spite of a higher C and Mn content in austenite and finer austenite laths, two-step annealing can lead to an active and continuous TRIP effect provided by a mixed blocky and lath-type austenitic structure with lower stability, contributing to a higher UTS. In contrast, one-step annealing gave rise to a less active but sustained TRIP effect given by the dominant lath-like austenite having higher stability, leading to a very high elongation. The further precipitation of vanadium carbides and the presence of both dislocation substructure and fine equiaxed grain in ferrite matrix facilitate the increase of yield strength after double annealing. - Highlights: • A novel two-step process was applied to a hot-rolled Fe-0.2C-6.5Mn-3Al steel. • The interplay between different microstructures and mechanical properties was studied. • Two-step annealing led to an active and continuous TRIP. • An outstanding combination of strength of 954 MPa and elongation of 39.2% was obtained.

  15. Effect of two-step intercritical annealing on microstructure and mechanical properties of hot-rolled medium manganese TRIP steel containing δ-ferrite

    Energy Technology Data Exchange (ETDEWEB)

    Xu, Yun-bo [State Key Laboratory of Rolling and Automation, Northeastern University, Shenyang 110819, People' s Republic China (China); Hu, Zhi-ping, E-mail: huzhiping900401@126.com [State Key Laboratory of Rolling and Automation, Northeastern University, Shenyang 110819, People' s Republic China (China); Zou, Ying; Tan, Xiao-dong; Han, Ding-ting; Chen, Shu-qing [State Key Laboratory of Rolling and Automation, Northeastern University, Shenyang 110819, People' s Republic China (China); Ma, De-gang [Tangshan Iron and Steel Company, Tangshan 063000, People' s Republic China (China); Misra, R.D.K. [Laboratory for Excellence in Advanced Steel Research, Department of Metallurgical, Materials and Biomedical Engineering, University of Texas at El Paso, TX 79968 (United States)

    2017-03-14

    The microstructure-properties relationship, work-hardening behavior and retained austenite stability have been systematically investigated in a hot-rolled medium manganese transformation-induced-plasticity (TRIP) steel containing δ-ferrite subjected to one-step and two-step intercritical annealing. The steel exhibited tensile strength of 752 MPa and total elongation of 52.7% for one-step intercritical annealing at 740 °C, tensile strength of 954 MPa and total elongation of 39.2% in the case of intercritical quenching at 800 °C and annealing at 740 °C. The austenite obtained by two-step annealing mostly consists of refined lath structures and increased fraction of block-type particles existing at various kinds of sites, which is highly distinguished from those characterized by long lath morphology and small amounts of granular shape in one-step annealed samples. In spite of a higher C and Mn content in austenite and finer austenite laths, two-step annealing can lead to an active and continuous TRIP effect provided by a mixed blocky and lath-type austenitic structure with lower stability, contributing to a higher UTS. In contrast, one-step annealing gave rise to a less active but sustained TRIP effect given by the dominant lath-like austenite having higher stability, leading to a very high elongation. The further precipitation of vanadium carbides and the presence of both dislocation substructure and fine equiaxed grain in ferrite matrix facilitate the increase of yield strength after double annealing. - Highlights: • A novel two-step process was applied to a hot-rolled Fe-0.2C-6.5Mn-3Al steel. • The interplay between different microstructures and mechanical properties was studied. • Two-step annealing led to an active and continuous TRIP. • An outstanding combination of strength of 954 MPa and elongation of 39.2% was obtained.

  16. Roll force prediction of high strength steel using foil rolling theory in cold skin pass rolling

    International Nuclear Information System (INIS)

    Song, Gil Ho; Jung, Jae Chook

    2013-01-01

    Skin pass rolling is a very important process for applying a certain elongation to a strip in the cold rolling and annealing processes, which play an important role in preventing the stretching of the yield point when the material is processed. The exact prediction of the rolling force is essential for obtaining a given elongation with the steel grade and strip size. Unlike hot rolling and cold rolling, skin pass rolling is used to apply an elongation of within 2% to the strip. Under a small reduction, it is difficult to predict the rolling force because the elastic deformation behavior of the rolls is complicated and a model for predicting the rolling force has not yet been established. Nevertheless, the exact prediction of the rolling force in skin pass rolling has gained increasing importance in recent times with the rapid development of high strength steels for use in automobiles. In this study, the possibility of predicting the rolling force in skin pass rolling for producing various steel grades was examined using foil rolling theory, which is known to have similar elastic deformation behavior of rolls in the roll bite. It was found that a noncircular arc model is more accurate than a circular model in predicting the roll force of high strength steel below TS 980 MPa in skin pass rolling

  17. Hot-Dip Aluminizing on AISI F55–UNS S32760 Super Duplex Stainless Steel Properties: Effect of Thermal Treatments

    Directory of Open Access Journals (Sweden)

    Andrea Francesco Ciuffini

    2017-11-01

    Full Text Available The behavior of super duplex stainless steels AISI F55-UNS S32760 in hot-dip aluminizing process has been studied, investigating the influence of cold working and of different initial microstructures obtained through a preliminary thermal treatment. The microstructural features examined are the secondary austenite precipitation, the static recovery of ferrite and the thermal dissolution of austenite within ferritic matrix. The hot-dip aluminizing temperature has been optimized through sessile drop tests. The treatment has been performed at 1100 °C for 300 s, 900 s and 2700 s. A strong chemical interaction occurs, generating intermetallic compounds at the interface. Molten aluminum interacts exclusively with the ferritic phase due to its much higher diffusivity in this phase coupled with its marked ferrite-stabilizer behavior. Thus, the influence of cold working is not remarkable, since the strains are mainly allocated by austenitic phase. The diffusivity of aluminum increases due to lattice defects thermally generated and, mainly, to influence given by grain boundaries, multiplied by secondary austenite precipitation, which act as short-circuit diffusion paths. Ni and Cr contents in the ferritic matrix have an influence but not highly relevant. Then, the best starting condition of the super duplex stainless steel substrates, to obtain a thick interfacial layer, are the thermal annealing at 1080 °C for 360 s/mm after a solution thermal treatment at 1300 °C for 60 s/mm.

  18. 76 FR 7546 - Certain Hot-Rolled Carbon Steel Flat Products From Brazil: Rescission of Countervailing Duty...

    Science.gov (United States)

    2011-02-10

    ..., through December 31, 2009. Since Nucor Corporation (Nucor) was the only party that requested a review of... administrative review. This rescission is based on Nucor's timely withdrawal of its request for review. DATES... 19 CFR 351.213(b), the Department received a timely request from Nucor, a domestic producer of hot...

  19. Low cycle fatigue behavior of hot-bent 347 stainless steel in a simulated PWR water environment

    Energy Technology Data Exchange (ETDEWEB)

    Lee, Jun Ho; Seo, Myung Gyu; Jang, Chang Heui [Dept. of Nuclear and Quantum Engineering, Korea Advanced Institute of Science and Technology, Daejeon (Korea, Republic of); Hong, Jong Tae [Korea Atomic Energy Research Institute, Daejeon (Korea, Republic of); Kim, Tae Soon [Central Research InstituteKorea Hydro and Nuclear Power Co., Ltd., Daejeon (Korea, Republic of)

    2016-11-15

    The effect of hot bending on the Low cycle fatigue (LCF) behavior of 347 SS was evaluated in Room temperature (RT) air and simulated Pressurized water reactor (PWR) water environments. The LCF life of 347 SS in PWR water was shorter than that in RT air for the as-received and hot-bent conditions. The LCF life of hot-bent 347 SS was relatively longer than that of the as-received condition in both RT air and PWR water. Microstructure analysis indicated development of dislocation structure near niobium carbide particles and increase in dislocation density for the hot-bent 347 SS. Such microstructure acted as barriers to dislocation movement during the LCF test, resulting in minimal hardening for the hot-bent 347 SS in RT air.

  20. NUMERICAL EVALUATION OF TEMPERATURE DISTRIBUTION IN THE ROLLING MILL ROLLS

    Directory of Open Access Journals (Sweden)

    José Claudino de Lira Júnior

    2013-06-01

    Full Text Available In hot rolling processes occur changes in the profile of the rolling mill rolls (expansion and contraction and constant wear due to mechanical stress and continuous thermal cycles of heating/cooling caused by contact rolled material- working roll and the cooling system by water jets in their surface, decreasing their lifetime. This paper presents a computational model to simulate the thermal performance of rolling mill rolls. The model was developed using the finite volume method for a transient two-dimensional system and allows calculating the temperature distribution of the rolling mill rolls under various conditions of service. Here it is investigated the influence of flow rate and temperature of the cooling water on the temperature distribution. The results show that the water temperature has greater influence than the water flow to control the surface temperature of the cylinders.

  1. The effect of microstructure on the sheared edge quality and hole expansion ratio of hot-rolled 700 MPa steel

    Science.gov (United States)

    Kaijalainen, A.; Kesti, V.; Vierelä, R.; Ylitolva, M.; Porter, D.; Kömi, J.

    2017-09-01

    The effects of microstructure on the cutting and hole expansion properties of three thermomechanically rolled steels have been investigated. The yield strength of the studied 3 mm thick strip steels was approximately 700 MPa. Detailed microstructural studies using laser scanning confocal microscopy (LCSM), FESEM and FESEM-EBSD revealed that the three investigated materials consist of 1) single-phase polygonal ferrite, 2) polygonal ferrite with precipitates and 3) granular bainite. The quality of mechanically sheared edges were evaluated using visual inspection and LSCM, while hole expansion properties were characterised according to the methods described in ISO 16630. Roughness values (Ra and Rz) of the sheet edge with different cutting clearances varied between 12 µm to 21 µm and 133 µm to 225 µm, respectively. Mean hole expansion ratios varied from 28.4% to 40.5%. It was shown that granular bainite produced the finest cutting edge, but the hole expansion ratio remained at the same level as in the steel comprising single-phase ferrite. This indicates that a single-phase ferritic matrix enhances hole expansion properties even with low quality edges. A brief discussion of the microstructural features controlling the cutting quality and hole expansion properties is given.

  2. Investigation of the fabrication process of hot-worked stainless-steel and Mo sheathed PbMo6 S8 wires

    International Nuclear Information System (INIS)

    Yamasaki, H.; Kimura, Y.

    1988-01-01

    Stainless-steel and Mo sheathed PbMo 6 S 8 wires have been fabricated by hot working from modified PbS, Mo, and MoS 2 mixed powders which were prepared by reacting Pb, Mo, and S at 530 0 C. Critical current densities were investigated for different preparation conditions, and it is revealed that obtaining continuous current path between PbMo 6 S 8 grains is the most important factor to achieve high critical current density. The J/sub c/ value of 2.8 x 10 4 Acm 2 (8 T), 7.8 x 10 3 Acm 2 (15 T), and 1.3 x 10 3 Acm 2 (23 T) was observed for the PbMo 6 S/sub 7.0/ wire heat treated at 700 0 C.copic

  3. Hot-rolled and cold-finished zirconium and zirconium alloy bars, rod, and wire for nuclear application

    International Nuclear Information System (INIS)

    Anon.

    1981-01-01

    The specification covers hot- and cold-finished zirconium alloy bars, rod, and wire, other than those required for reforging, including rounds, squares, and shapes. One unalloyed grade and three alloy grades for use in nuclear applications are described. The products covered include the following sections and sizes: bars, rounds in coils for subsequent reworking (6.4 to 19 mm) and flats (6.4 to 250 mm); rods, rounds in coils for subsequent reworking (6.4 to 19 mm); wire (9.5 mm). The specification covers ordering information, manufacture, condition, chemical requirements, mechanical properties, corrosion properties, permissible variations in dimensions, significance of numerical limits, lot size, special tests, workmanship, finish, inspection, certification, packaging and marking

  4. Dominant root locus in state estimator design for material flow processes: A case study of hot strip rolling.

    Science.gov (United States)

    Fišer, Jaromír; Zítek, Pavel; Skopec, Pavel; Knobloch, Jan; Vyhlídal, Tomáš

    2017-05-01

    The purpose of the paper is to achieve a constrained estimation of process state variables using the anisochronic state observer tuned by the dominant root locus technique. The anisochronic state observer is based on the state-space time delay model of the process. Moreover the process model is identified not only as delayed but also as non-linear. This model is developed to describe a material flow process. The root locus technique combined with the magnitude optimum method is utilized to investigate the estimation process. Resulting dominant roots location serves as a measure of estimation process performance. The higher the dominant (natural) frequency in the leftmost position of the complex plane the more enhanced performance with good robustness is achieved. Also the model based observer control methodology for material flow processes is provided by means of the separation principle. For demonstration purposes, the computer-based anisochronic state observer is applied to the strip temperatures estimation in the hot strip finishing mill composed of seven stands. This application was the original motivation to the presented research. Copyright © 2017 ISA. Published by Elsevier Ltd. All rights reserved.

  5. Structural and spectroscopic characterisations of the surface oxide scales and inclusions present on edge-burst hot-rolled steel coils

    International Nuclear Information System (INIS)

    Chowdhury, Anirban; Iyyappan, Ramasamy; Majumdar, Dipanwita; Singha, Achintya

    2014-01-01

    Detailed structural and spectroscopic characterisations have been carried out on the inclusions and the surface oxides present on edge-burst hot-rolled steel coils. Surface scales were characterised through X-ray diffraction (XRD), scanning electron microscopy (SEM) and Raman spectroscopy. Evidence of different types of regular and non-stoichiometric Fe-oxides was found on the cracked surface of the steel wire. Along with the surface scales inclusions with calcium aluminate and spinel was characterized using Raman spectroscopy. The usefulness of Raman spectroscopy has been explored in detail for the characterisation of these inclusions; especially when XRD information ceases to be a limiting tool. The samples collected from the clogged nozzle area were found to be of grossite (CaO·2Al 2 O 3 ) phase and this was also observed in the inclusions in the finished coils. It was found that this particular calcium aluminate phase has a detrimental effect on casting and final finished steel products. - Highlights: • First investigation and surface study report on edge-bursting issue of steel coils. • Detailed characterisations of the inclusions and surface oxide scales in steel. • Influence of a particular type of calcium aluminate phase on process chemistry

  6. Fatigue crack growth behaviors in hot-rolled low carbon steels: A comparison between ferrite–pearlite and ferrite–bainite microstructures

    International Nuclear Information System (INIS)

    Guan, Mingfei; Yu, Hao

    2013-01-01

    The roles of microstructure types in fatigue crack growth behaviors in ferrite–pearlite steel and ferrite–bainite steel were investigated. The ferrite–bainite dual-phase microstructure was obtained by intermediate heat treatment, conducted on ferrite–pearlite hot-rolled low carbon steel. This paper presents the results from investigation using constant stress-controlled fatigue tests with in-situ scanning electron microscopy (SEM), fatigue crack growth (FCG) rate tests, and fatigue fractography analysis. Microscopy images arrested by in-situ SEM showed that the fatigue crack propagation in F–P steel could become unstable more ealier compared with that in F–B steel. The fatigue cracks in ferrite–pearlite were more tortuous and could propagate more freely than that in ferrite–bainite microstructures. However, frequent crack branching were observed in ferrite–bainite steel and it indicated that the second hard bainite phase effectively retarded the crack propagation. The variation of FCG rate (da/dN) with stress intensity factor range (ΔK) for F–P and F–B steels was discussed within the Paris region. It was shown that FCG rate of F–P steel was higher than that of F–B steel. Moreover, the fatigue fracture surface analysis proved that grain boundaries could also play a role in the resistance of crack propagation.

  7. Tensile property improvement of TWIP-cored three-layer steel sheets fabricated by hot-roll-bonding with low-carbon steel or interstitial-free steel

    Science.gov (United States)

    Park, Jaeyeong; Kim, Jung-Su; Kang, Minju; Sohn, Seok Su; Cho, Won Tae; Kim, Hyoung Seop; Lee, Sunghak

    2017-01-01

    TWIP-cored three-layer steel sheets were newly fabricated by hot rolling of TWIP steel sheet surrounded by low-carbon (LC) or interstitial-free (IF) steel sheets. TWIP/LC or TWIP/IF interfaces were well bonded without pores or voids, while a few pearlites were thinly formed along the interfaces. The strengths and elongation of the TWIP-cored sheets increased as the volume fraction of TWIP-cored region increased, and were also well matched with the ones calculated by a rule of mixtures based on volume fraction or force fraction. According to digital image correlation and electron back-scatter diffraction analyses, very high strain hardening effect in the initial deformation stage and active twin formation in the interfacial region beneficially affected the overall homogeneous deformation in the TWIP-cored sheets without any yield point phenomenon occurring in the LC sheet and serrations occurring in the TWIP sheet, respectively. These TWIP-cored sheets can cover a wide range of yield strength, tensile strength, and ductility levels, e.g., 320~498 MPa, 545~878 MPa, and 48~54%, respectively, by controlling the volume fraction of TWIP-cored region, and thus present new applications to multi-functional automotive steel sheets requiring excellent properties.

  8. Texture evolution in Nd:YAG-laser welds of AZ31 magnesium alloy hot rolled sheets and its influence on mechanical properties

    International Nuclear Information System (INIS)

    Commin, Lorelei; Dumont, Myriam; Rotinat, Rene; Pierron, Fabrice; Masse, Jean-Eric; Barrallier, Laurent

    2011-01-01

    Research highlights: → AZ31 LBW fusion zone results in Mg 17 (Al-Zn) 12 precipitation, twins formation and {0 0 2} texture modification. → The mechanical properties were reduced after LBW but the fracture occurred in the base metal. → The mechanical properties were reduced after LBW but the fracture occurred in the base metal. → A recovery of elongation and UTS can be achieved by a 300 deg. C/1 h heat treatment. The texture evolution is mainly responsible for the yield strength reduction in the fusion zone. - Abstract: AZ31 hot rolled magnesium alloy presents a strong basal texture. Using laser beam welding (LBW) as a joining process induces high temperature gradients leading to major texture changes. Electron back scattered diffraction (EBSD) was used to study the texture evolution, and tensile tests coupled with speckle interferometry were performed to understand its influence on mechanical properties. The random texture obtained in the LBW fusion zone is mainly responsible for the yield strength reduction.

  9. Fabrication of Hadfield-Cored Multi-layer Steel Sheet by Roll-Bonding with 1.8-GPa-Strength-Grade Hot-Press-Forming Steel

    Science.gov (United States)

    Chin, Kwang-Geun; Kang, Chung-Yun; Park, Jaeyeong; Lee, Sunghak

    2018-05-01

    An austenitic Hadfield steel was roll-bonded with a 1.8-GPa-strength-grade martensitic hot-press-forming (HPF) steel to fabricate a multi-layer steel (MLS) sheet. Near the Hadfield/HPF interface, the carburized and decarburized layers were formed by the carbon diffusion from the Hadfield (1.2%C) to HPF (0.35%C) layers, and could be regarded as kinds of very thin multi-layers of 35 μm in thickness. The tensile test and fractographic data indicated that the MLS sheet was fractured abruptly within the elastic range by the intergranular fracture occurred in the carburized layer. This was because C was mainly segregated at prior austenite grain boundaries in the carburized layer, which weakened grain boundaries to induce the intergranular fracture. In order to solve the intergranular facture problem, the MLS sheet was tempered at 200 °C. The stress-strain curve of the tempered MLS sheet lay between those of the HPF and Hadfield sheets, and a rule of mixtures was roughly satisfied. Tensile properties of the MLS sheet were dramatically improved after the tempering, and the intergranular fracture was erased completely. In particular, the yield strength up to 1073 MPa along with the high strain hardening and excellent ductility of 32.4% were outstanding because the yield strength over 1 GPa was hardly achieved in conventional austenitic steels.

  10. Deformation mechanism study of a hot rolled Zr-2.5Nb alloy by transmission electron microscopy. I. Dislocation microstructures in as-received state and at different plastic strains

    Energy Technology Data Exchange (ETDEWEB)

    Long, Fei; Daymond, Mark R., E-mail: mark.daymond@queensu.ca; Yao, Zhongwen [Department of Mechanical and Materials Engineering, Queen' s University Kingston, Ontario K7L 3N6 (Canada)

    2015-03-07

    Thin foil dog bone samples prepared from a hot rolled Zr-2.5Nb alloy have been deformed by tensile deformation to different plastic strains. The development of slip traces during loading was observed in situ through SEM, revealing that deformation starts preferentially in certain sets of grains during the elastic-plastic transition region. TEM characterization showed that sub-grain boundaries formed during hot rolling consisted of screw 〈a〉 dislocations or screw 〈c〉 and 〈a〉 dislocations. Prismatic 〈a〉 dislocations with large screw or edge components have been identified from the sample with 0.5% plastic strain. Basal 〈a〉 and pyramidal 〈c + a〉 dislocations were found in the sample that had been deformed with 1.5% plastic strain, implying that these dislocations require larger stresses to be activated.

  11. Mechanical behaviour of austenitic stainless steels in inert environment and in hot chloride environment: influence of molybdenum addition

    International Nuclear Information System (INIS)

    Daret, Jacques

    1978-01-01

    This research thesis reports the study of the influence of molybdenum addition. It is based on an experimental method which brings to the fore correlations between mechanical and electrochemical parameters of the phenomenon of stress corrosion cracking of austenitic stainless steels. After having recalled some characteristics of dry corrosion and electrochemical corrosion, presented austenitic stainless steels (mechanical properties such as elastic modulus, yield strength, tensile strength, ultimate elongation, creep behaviour, inter-crystalline and pitting corrosion, stress corrosion cracking behaviour), the author addresses the stress corrosion cracking behaviour of these steels in chloride environment (general characteristics, parameters, proposes theories to explain stress corrosion cracking), reports the study of the influence of molybdenum in these steels, notably on corrosion resistance and on stress corrosion cracking. Experimental method and results are described and discussed: tensile tests and creep tests in inert environment, stress corrosion cracking test in chloride environment with analysis based either on corrosion potential evolution or on sample elongation evolution. Results are notably discussed in terms of crack situation within metal lattice, crack growth rate, and scanning electronic microscopy observations [fr

  12. Application of a non-dynamometric method to the measurement of the coefficient of static friction in cold and hot water between stainless steel and two alloys of zirconium

    International Nuclear Information System (INIS)

    D'Agraives, B.C.; Toornvliet, J.

    1977-01-01

    A method is proposed to perform comparative measurements of the coefficient of friction, either in cold water (25 0 C) or in hot pressurized water (240 0 C). For the purpose, a pin-on-disc tribometer, working with no force transducer, in which the coefficient of friction μ is measured through an angle 0, and given by μ=K sin 0 is used. The method is presently applied to the determination of the incipient friction along a distance of few millimetres. At low speed (1 mm/s) and with light contacts loads (from 50 to 150 g), two different friction mechanisms are observed for the following couples of materials; Zircalloy 2/304L stainless steel, Zirconium Niobium 2.5/304L stainless steel, 304L stainless steel/304L stainless steel. The first mechanism, which is observed essentially in cold conditions, is characterized by a regular sliding since friction starts, whereas the second appears mostly in hot conditions and shows peaks of friction with irregular and scattered values of μ. These two mechanisms seem to be related to intermetallic affinity of the mating materials, and also to the existence of preoxydized surface layers, and, to a large extent, to the change in the water viscosity. In such conditions, it appears that it is not possible to replace friction experiments in hot water by easier experiments in cold water

  13. Preparation and characterization of 304 stainless steel/Q235 carbon steel composite material

    Science.gov (United States)

    Shen, Wenning; Feng, Lajun; Feng, Hui; Cao, Ying; Liu, Lei; Cao, Mo; Ge, Yanfeng

    The composite material of 304 stainless steel reinforced Q235 carbon steel has been prepared by modified hot-rolling process. The resulted material was characterized by scanning electron microscope, three-electrode method, fault current impact method, electrochemical potentiodynamic polarization curve measurement and electrochemical impedance spectroscopy. The results showed that metallurgical bond between the stainless steel layer and carbon steel substrate has been formed. The composite material exhibited good electrical conductivity and thermal stability. The average grounding resistance of the composite material was about 13/20 of dip galvanized steel. There has no surface crack and bubbling formed after fault current impact. The composite material led to a significant decrease in the corrosion current density in soil solution, compared with that of hot dip galvanized steel and bare carbon steel. On the basis polarization curve and EIS analyses, it can be concluded that the composite material showed improved anti-corrosion property than hot-dip galvanized steel.

  14. Promoting Ti{sub 4}C{sub 2}S{sub 2} strain induced precipitation during asymmetrical hot rolling to improve r value and advantaged texture in Ti stabilized IF steel

    Energy Technology Data Exchange (ETDEWEB)

    Dong, Futao, E-mail: dongft@sina.com [College of Metallurgy and Energy, Hebei United University, Tangshan 063000 (China); Xue, Fei [College of Electrical Engineering, Hebei United University, Tangshan 063000 (China); Du, Linxiu; Liu, Xianghua [The State Key Laboratory of Rolling and Automation, Northeastern University, Shenyang 110819 (China)

    2015-01-25

    Highlights: • We study Ti{sub 4}C{sub 2}S{sub 2} strain induced precipitation in Ti stabilized IF steel. • The PTT diagram is obtained by plotting 1/A{sub r}–time curves. • Hot rolling at the nose of P{sub s} line effectively promotes Ti{sub 4}C{sub 2}S{sub 2} precipitation. • Annealed sheet with promoted Ti{sub 4}C{sub 2}S{sub 2} exhibits higher r value and stronger γ fiber texture. • Adverse impact of tiny TiC has been significantly mitigated. - Abstract: The kinetic of Ti{sub 4}C{sub 2}S{sub 2} strain induced precipitation in a Ti stabilized IF steel was investigated using two stage interrupted compression test with high true strain (0.5). The PTT (precipitation–time–temperature) diagram was obtained by plotting 1/A{sub r}–time curves. TEM (transmission electron microscopy) observation confirmed that the evolution of Ti{sub 4}C{sub 2}S{sub 2} precipitate in the quenched samples of thermal simulation is in good agreement with the PTT diagram. Hot strips were produced at three different rolling temperatures with high strain and slight shear deformation. It was found that hot rolling at the nose temperature of the P{sub s} line of the PTT diagram can effectively promote the precipitation of Ti{sub 4}C{sub 2}S{sub 2} and retard the precipitation of TiC. Cold rolled and annealed sheets from hot strip containing higher volume fraction of Ti{sub 4}C{sub 2}S{sub 2} exhibited higher r value and stronger γ fiber texture with equal {1 1 1}〈1 1 2〉 and {1 1 1}〈1 1 0〉 components. By contrast, cold rolled and annealed sheets from hot strips containing lower volume fraction of Ti{sub 4}C{sub 2}S{sub 2} represented lower r values and weaker γ fiber texture with significant drops from {1 1 1}〈1 1 2〉 to {1 1 1}〈1 1 0〉 component.

  15. Influence of precipitation behavior on mechanical properties and hydrogen induced cracking during tempering of hot-rolled API steel for tubing

    Energy Technology Data Exchange (ETDEWEB)

    Moon, Joonoh, E-mail: mjo99@kims.re.kr [Ferrous Alloy Department, Advanced Metallic Materials Division, Korea Institute of Materials Science, 797 Changwondae-ro, Seongsan-gu, Changwon, Gyeongnam 642-831 (Korea, Republic of); Choi, Jongmin; Han, Seong-Kyung; Huh, Sungyul; Kim, Seong-Ju [Sheet Products Design Team, Technical Research Center, Hyundai Steel Company, 1480 Bukbusaneop-ro, Dangjin, Chungnam 343-823 (Korea, Republic of); Lee, Chang-Hoon; Lee, Tae-Ho [Ferrous Alloy Department, Advanced Metallic Materials Division, Korea Institute of Materials Science, 797 Changwondae-ro, Seongsan-gu, Changwon, Gyeongnam 642-831 (Korea, Republic of)

    2016-01-15

    Precipitation behavior and its effect on hydrogen embrittlement during tempering process of hot-rolled API steel designed with 0.4 wt% Cr and 0.25 wt% Mo were investigated. The base steel was normalized and then tempered at 650 °C for up to 60 min. The precipitation behavior of the examined steel was explored using transmission electron microscopy (TEM) analysis, and it was found that the precipitation sequence during tempering at 650 °C were as follows: MX+M{sub 3}C→MX→MX+M{sub 7}C{sub 3}+M{sub 23}C{sub 6}. The change of particle fraction was measured by electrolytic extraction technique. At the early stage of tempering, the particle fraction greatly decreased due to dissolution of M{sub 3}C particle, and increased after 10 min by the precipitation of M{sub 7}C{sub 3} and M{sub 23}C{sub 6} particles. The particle fraction showed a peak at 30 min tempering and decreased again due to the dissolution of M{sub 7}C{sub 3} particle. Vickers hardness tests of base steel and tempered samples were carried out, and then the hardness was changed by accompanying with the change of particle fraction. The sensitivity of hydrogen embrittlement was evaluated through hydrogen induced cracking (HIC) tests, and the results clearly proved that HIC resistance of tempered samples was better than that of base steel due to the formation of tempered martensite, and then the HIC resistance changed depending on the precipitation behavior during tempering, i.e., the precipitation of coarse M{sub 23}C{sub 6} and M{sub 7}C{sub 3} particles deteriorated the HIC resistance.

  16. Influence of precipitation behavior on mechanical properties and hydrogen induced cracking during tempering of hot-rolled API steel for tubing

    International Nuclear Information System (INIS)

    Moon, Joonoh; Choi, Jongmin; Han, Seong-Kyung; Huh, Sungyul; Kim, Seong-Ju; Lee, Chang-Hoon; Lee, Tae-Ho

    2016-01-01

    Precipitation behavior and its effect on hydrogen embrittlement during tempering process of hot-rolled API steel designed with 0.4 wt% Cr and 0.25 wt% Mo were investigated. The base steel was normalized and then tempered at 650 °C for up to 60 min. The precipitation behavior of the examined steel was explored using transmission electron microscopy (TEM) analysis, and it was found that the precipitation sequence during tempering at 650 °C were as follows: MX+M_3C→MX→MX+M_7C_3+M_2_3C_6. The change of particle fraction was measured by electrolytic extraction technique. At the early stage of tempering, the particle fraction greatly decreased due to dissolution of M_3C particle, and increased after 10 min by the precipitation of M_7C_3 and M_2_3C_6 particles. The particle fraction showed a peak at 30 min tempering and decreased again due to the dissolution of M_7C_3 particle. Vickers hardness tests of base steel and tempered samples were carried out, and then the hardness was changed by accompanying with the change of particle fraction. The sensitivity of hydrogen embrittlement was evaluated through hydrogen induced cracking (HIC) tests, and the results clearly proved that HIC resistance of tempered samples was better than that of base steel due to the formation of tempered martensite, and then the HIC resistance changed depending on the precipitation behavior during tempering, i.e., the precipitation of coarse M_2_3C_6 and M_7C_3 particles deteriorated the HIC resistance.

  17. Initiation of Stress Corrosion Cracking of 26Cr-1Mo Ferritic Stainless Steels in Hot Chloride Solution

    International Nuclear Information System (INIS)

    Kwon, H. S.; Hehemann, R. F.

    1987-01-01

    Elongation measurements of 26Cr-1Mo ferritic stainless steels undergoing stress corrosion in boiling LiCl solution allow the induction period to be distinguished from the propagation period of cracks by the deviation of elongation from the logarithmic creep law. Localised corrosion cells are activated exclusively at slip steps by loading and developed into corrosion trenches. No cracks have developed from the corrosion trenches until the induction period is exceeded. The induction period is regarded as a time for localised corrosion cells to achieve a critical degree of occlusion for crack initiation. The repassivation rate of exposed metal by creep or emergence of slip steps decreases as the load increases and is very sensitive to the microstructural changes that affect slip tep height. The greater susceptibility to stress corrosion cracking of either prestrained or grain coarsened 26Cr-1Mo alloy compared with that of mill annealed material results from a significant reduction of repassivation rate associated with the increased slip step height. The angular titanium carbonitrides particles dispersed in Ti-stabilized 26Cr-1Mo alloy have a detrimental effect on the resistance to stress corrosion cracking

  18. Constitutive Relationship Modeling and Characterization of Flow Behavior under Hot Working for Fe–Cr–Ni–W–Cu–Co Super-Austenitic Stainless Steel

    Directory of Open Access Journals (Sweden)

    Li-Chih Yang

    2015-09-01

    Full Text Available The hot deformation behavior of a Fe–22Cr–25Ni–3.5W–3Cu–1.5Co super-austenitic stainless steel was investigated using isothermal compression tests with a wide range of temperatures (1173–1373 K and strain rates (0.1–10 s−1. The results showed that all the flow curves gradually turned to balanced stress state without notable peak stress characteristics during the entire deformation, which indicated that the dynamic recovery behavior played a main restoration mechanism in the steel. Modeling constitutive equations relating to the temperature, strain rate and flow stress were proposed to determine the materials constants and activation energy necessary for deformation. In order to give the precise predicted values of the flow behavior, the influence of strain was identified using polynomial functions. The relationship of flow stress, temperature and strain rate was represented by the Zener-Hollomon parameter including the Arrhenius term. The predicted results validated that the developed constitutive equations can describe high temperature flow behavior well. Furthermore, a modified Zener-Hollomon parameter map of the studied steel was developed to clarify the restoration mechanism based on the constitutive modeling data and microstructural observation.

  19. Effect of hot rolling on the structure and the mechanical properties of nitrogen-bearing austenitic-martensitic 14Kh15AN4M steel

    Science.gov (United States)

    Bannykh, O. A.; Betsofen, S. Ya.; Lukin, E. I.; Blinov, V. M.; Voznesenskaya, N. M.; Tonysheva, O. A.; Blinov, E. V.

    2016-04-01

    The effect of the rolling temperature and strain on the structure and the properties of corrosionresistant austenitic-martensitic 14Kh15AN4M steel is studied. The steel is shown to exhibit high ductility: upon rolling in the temperature range 700-1100°C at a reduction per pass up to 80%, wedge steel specimens are uniformly deformed along and across the rolling direction without cracking and other surface defects. Subsequent cold treatment and low-temperature tempering ensure a high hardness of the steel (50-56 HRC). Austenite mainly contributes to the hardening upon rolling in the temperature range 700-800°C at a reduction of 50-70%, and martensite makes the main contribution at higher temperatures and lower strains. Texture does not form under the chosen deformation conditions, which indicates dynamic recrystallization with the nucleation and growth of grains having no preferential orientation.

  20. Study of the mechanical properties of stainless steel 316LN prepared by hot isostatic compression. Influence of preparation parameters

    International Nuclear Information System (INIS)

    Couturier, Raphael

    1999-01-01

    This research thesis has been performed within an R and D programme which aimed at optimising and certifying the HIP process (hot isostatic pressing) from a technological as well as metallurgical point of view. The objective has been to improve dimensional reproducibility of fabricated parts, and metallurgical properties of the dense material. Reference parts are those belonging to PWR primary circuit, and are made in cast austenitic-ferritic steel. Thus, the objective has been to show that these parts can be beneficially fabricated by powder metallurgy in austenitic grade. A mock part (a primary circuit pump wheel at the 1/2 scale) has first been fabricated by HIP, and a more complex shape generator has been designed. The author reports the determination of microstructure and mechanical characteristics of the austenitic 316LN steel produced by HIP and used to fabricate mock parts and demonstrator parts, the study of the relationship between dense material properties and fabrication parameters (temperature, pressure, consolidation time), and the analysis of the consequences of an elaboration by HIP on the 316LN steel with comparison with forged parts. After a presentation of the Powder Metallurgy elaboration technique, the author reports a bibliographical study on the precipitation at Prior Particle Boundaries (PPB), reports the study of microstructure and mechanical properties of the HIPed 316LN, and discusses the possibility of a decrease of precipitation at PPBs by adjusting powder degassing or a granulometric sorting. The last part reports the extension of the study of steel coherence to a temperature range which encompasses the primary circuit operation temperature (350 C). Resilience tests are performed as well as mechanical tests on notched axisymmetric samples. A finite element calculation of these samples allows the validation of the use of a Thomson-type model to describe the emergence of defects which are typical of a steel elaborated by powder

  1. Hot corrosion of the ceramic composite coating Ni{sub 3}Al-Al{sub 2}O{sub 3}-Al{sub 2}O{sub 3}/MgO plasma sprayed on 316L stainless steel

    Energy Technology Data Exchange (ETDEWEB)

    Shirazi, Amir Khodaparast; Kiahosseini, Seyed Rahim [Islamic Azad Univ., Damghan (Iran, Islamic Republic of). Dept. of Engineering

    2017-08-15

    Ni{sub 3}Al-Al{sub 2}O{sub 3}-Al{sub 2}O{sub 3}/MgO three-layered coatings with thicknesses of 50, 100, and 150 μm for Al{sub 2}O{sub 3}/MgO and 100 μm for the other layers were deposited on 316L stainless steel using plasma spraying. X-ray diffraction, atomic force microscopy, furnace hot corrosion testing in the presence of a mixture of Na{sub 2}SO{sub 4} and V{sub 2}O{sub 5} corrosive salts and scanning electron microscopy were used to determine the structural, morphological and hot corrosion resistance of samples. Results revealed that the crystalline grains of MgO and Al{sub 2}O{sub 3} coating were very small. Weight loss due to hot corrosion decreased from approximately 4.267 g for 316L stainless steel without coating to 2.058 g. The samples with 150 μm outer coating showed improved resistance with the increase in outer layer thickness. Scanning electron microscopy of the coated surface revealed that the coating's resistance to hot corrosion is related to the thickness and the grain size of Al{sub 2}O{sub 3}/MgO coatings.

  2. Spray rolling aluminum alloy strip

    Energy Technology Data Exchange (ETDEWEB)

    McHugh, Kevin M.; Delplanque, J.-P.; Johnson, S.B.; Lavernia, E.J.; Zhou, Y.; Lin, Y

    2004-10-10

    Spray rolling combines spray forming with twin-roll casting to process metal flat products. It consists of atomizing molten metal with a high velocity inert gas, cooling the resultant droplets in flight and directing the spray between mill rolls. In-flight convection heat transfer from atomized droplets teams with conductive cooling at the rolls to rapidly remove the alloy's latent heat. Hot deformation of the semi-solid material in the rolls results in fully consolidated, rapidly solidified product. While similar in some ways to twin-roll casting, spray rolling has the advantage of being able to process alloys with broad freezing ranges at high production rates. This paper describes the process and summarizes microstructure and tensile properties of spray-rolled 2124 and 7050 aluminum alloy strips. A Lagrangian/Eulerian poly-dispersed spray flight and deposition model is described that provides some insight into the development of the spray rolling process. This spray model follows droplets during flight toward the rolls, through impact and spreading, and includes oxide film formation and breakup when relevant.

  3. Structure and microstructure evolution of a ternary Fe–Cr–Ni alloy akin to super martensitic stainless steel

    International Nuclear Information System (INIS)

    Ravi Kumar, B.; Sharma, Sailaja; Munda, Parikshit; Minz, R.K.

    2013-01-01

    Highlights: • Reaustenisation by recrystallisation rather by a diffusion controlled process. • Ultrafine grained austenite formation in martensite matrix by recrystallisation. • In situ high temperature austenite transformation studies by X-ray diffraction. • Microstructure tailoring to achieve tensile strength (∼1 GPa) with good ductility. - Abstract: A ternary Fe–Cr–Ni alloy, akin to super martensitic stainless steels was prepared in vacuum induction furnace. The as cast ingot was solution treated at 1200 °C for 25 h and then hot forged and rolled to reduce into plate form. The hot rolled plate of martensitic microstructure was then cold rolled to 80% of thickness reduction. The phase transformation studies by X-ray diffraction analysis of hot and cold rolled specimens showed presence of retained austenite in air cooled as well as in water quenched state after annealing/austenising temperature of 1060 °C. The reaustenisation behaviour of the cold rolled alloy in water quenched state was studied by high temperature X-ray diffraction analysis. It showed very stable martensitic phase and the completion of reaustenisation process were observed to occur at about 950 °C. The recrystallisation behaviour of cold rolled material under isothermal and repeated annealing treatment was studied in detail by electron microscope. The tensile properties of the material were evaluated after various annealing treatments. The study revealed that by a suitable sequence of repetitive annealing process microstructure could be tailored to achieve tensile strength above 1 GPa with good ductility in a super martensitic stainless steel

  4. Manufacture of thin-walled clad tubes by pressure welding of roll bonded sheets

    Science.gov (United States)

    Schmidt, Hans Christian; Grydin, Olexandr; Stolbchenko, Mykhailo; Homberg, Werner; Schaper, Mirko

    2017-10-01

    Clad tubes are commonly manufactured by fusion welding of roll bonded metal sheets or, mechanically, by hydroforming. In this work, a new approach towards the manufacture of thin-walled tubes with an outer diameter to wall thickness ratio of about 12 is investigated, involving the pressure welding of hot roll bonded aluminium-steel strips. By preparing non-welded edges during the roll bonding process, the strips can be zip-folded and (cold) pressure welded together. This process routine could be used to manufacture clad tubes in a continuous process. In order to investigate the process, sample tube sections with a wall thickness of 2.1 mm were manufactured by U-and O-bending from hot roll bonded aluminium-stainless steel strips. The forming and welding were carried out in a temperature range between RT and 400°C. It was found that, with the given geometry, a pressure weld is established at temperatures starting above 100°C. The tensile tests yield a maximum bond strength at 340°C. Micrograph images show a consistent weld of the aluminium layer over the whole tube section.

  5. Influence of stainless steel Internals on Corrosion of tower wall materials

    Science.gov (United States)

    Chen, Bing; Ren, Ke

    2017-12-01

    In view of the galvanic corrosion of the tower wall material in the tower of a refinery atmospheric vacuum distillation unit, the electrochemical behavior of Q345R steel, stainless steel (201, 304 cold-rolled plate, 304 hot rolled plate and 316L) in 3.5%NaCl solution was studied by electrochemical method. The results show that the corrosion potential of Q345R is much lower than that of stainless steel, and the corrosion rate of Q345R is higher than that of stainless steel. As the anode is etched as the anode corrosion, the anode polarizability of stainless steel shows strong polarization ability, which is anodic polarization control, and Q345R is anode Active polarization control; Q345R / 201 galvanic pair may be the most serious corrosion, and Q345R/316L galvanic couple may be relatively slight. Therefore, in the actual production of tower equipment, material design or tower to upgrade the replacement, it are recommended to use the preferred anode and cathode potential difference with the use of materials.

  6. Improvements to the corrosion resistance of stainless steels for fuel cell applications : supplementary report for phase 2

    Energy Technology Data Exchange (ETDEWEB)

    Kuyucak, S.; Li, J.; Liu, P.; Shehata, M.; Kruszewski, J.; Lo, J.; Guertsman, V.Y.; Gu, G.P. [Natural Resources Canada, Ottawa, ON (Canada). CANMET Materials Technology Laboratory

    2007-07-15

    This paper reported on a newly developed method of making bipolar electrodes from type 304 stainless steel. Two stainless steels were cast, hot-rolled and heat treated. The microstructures were then examined to determine the chromium carbide formation. Plain and mechanically polished samples were sent to General Motors for conductivity measurements to investigate the thermo-mechanical treatment as a means of improving the contact resistance of stainless steel bipolar plates subject to the operating conditions in a proton-exchange membrane (PEM) fuel cell. The treatment induces precipitation of conducive particles. The surface of the stainless steel is etched so that particles protrude from the surface. When the bipolar plates are stacked with sufficient load, the protruding surface precipitates indent into adjacent graphite electrodes, making direct electrical contact. The most common precipitate is M{sub 23}C{sub 6} carbide. This paper described the carbide precipitation required for electrical conductivity and presented a model for electrical conductance across a bipolar plate. It included a description of inter-particle distance and carbide size; carbide formation in type 304 stainless steels; heat-treatment processing of 304 steel for electrical conductance and desensitization; and the effect of steel composition on carbide growth. The experimental work was outlined in terms of casting, hot rolling, cold rolling, heat treatment, aging treatment for carbide growth, and desensitization treatment. Both alloys that were subjected to the thermo-mechanical treatment in this study showed a uniform distribution of carbide precipitates. Their size varied from very small to about 0.8{mu}m. Scanning electron microscopy (SEM) analysis did not detect a change in particle size and population density of these particles with prolonged annealing at 800 degrees C. 4 refs., 6 tabs., 14 figs.

  7. Fabrication of cold-rolled bands of the alloy-ehi 702 in rolls

    International Nuclear Information System (INIS)

    Zhuchin, V.N.; Gindin, A.Sh.; Shaburov, V.E.; Vladimirov, S.M.; Sokolov, V.A.; Shavkun, V.V.; Perepelitsa, I.V.; Markov, V.V.; Naymov, E.P.; Evstaf'ev, P.P.

    1977-01-01

    The questions are discussed, connected with the manufacture of cold-rolled strip of alloy EI702 in reels from strip blanks. It has been established that in the manufacture of hot-rolled stock from EI702 slabs it is necessary to use powerful rolling equipment because of high resistance to deformation. The reel method for manufacturing EI702 alloy improves the rolled stock and increases percentage of serviceable stock, as well as the output

  8. Rolling force prediction for strip casting using theoretical model and artificial intelligence

    Institute of Scientific and Technical Information of China (English)

    CAO Guang-ming; LI Cheng-gang; ZHOU Guo-ping; LIU Zhen-yu; WU Di; WANG Guo-dong; LIU Xiang-hua

    2010-01-01

    Rolling force for strip casting of 1Cr17 ferritic stainless steel was predicted using theoretical model and artificial intelligence.Solution zone was classified into two parts by kiss point position during casting strip.Navier-Stokes equation in fluid mechanics and stream function were introduced to analyze the rheological property of liquid zone and mushy zone,and deduce the analytic equation of unit compression stress distribution.The traditional hot rolling model was still used in the solid zone.Neural networks based on feedforward training algorithm in Bayesian regularization were introduced to build model for kiss point position.The results show that calculation accuracy for verification data of 94.67% is in the range of+7.0%,which indicates that the predicting accuracy of this model is very high.

  9. Aluminum and stainless steel tubes joined by simple ring and welding process

    Science.gov (United States)

    Townhill, A.

    1967-01-01

    Duranel ring is used to join aluminum and stainless steel tubing. Duranel is a bimetal made up of roll-bonded aluminum and stainless steel. This method of joining the tubing requires only two welding operations.

  10. ROLLING PROCESS WITH OHSAS AND TEXTURE FORMATION– A REVIEW

    Directory of Open Access Journals (Sweden)

    P. CHANDRAMOHAN

    2009-03-01

    Full Text Available Rolling is a mechanical treatment, which plays an important part in the processing of ferrous and nonferrous alloys. Texturing is an important phenomenon that occurs after rolling process. Preferred orientation increases the strength of the material enormously. Hence the research is focused on the rolling studies and the texture formation, which occurs after rolling process. This review mainly focuses on rolling process carried out in different alloys. It also highlights the analysis made on various rolling parameters for improving the mechanical properties. Texture studies carried on various ferrous and non-ferrous alloys; particularly in nitrogen alloyed duplex stainless steel is discussed. Finally the need for implementation of occupational health and safety during a thermomechanical treatment is also discussed. The state of art in this field is encouraging and showing positive signs of commercializing rolled nitrogen alloyed duplex stainless steel after proper texture control.

  11. PROTECCIÓN CONTRA LA CORROSIÓN EN SALES FUNDIDAS DE UN ACERO HOT ROLLED, EN EL RANGO DE TEMPERATURAS DE 400 ºC-600 ºC, RECUBIERTO POR ROCIADO TÉRMICO CON ACERO INOXIDABLE 312

    Directory of Open Access Journals (Sweden)

    JOSE LUDDEY MARULANDA

    2009-01-01

    Full Text Available Se evaluó la corrosión por sales fundidas mediante la técnica gravimétrica en un acero de bajo carbono tipo hot rolled, rociado térmicamente con una aleación de acero inoxidable tipo 312, con el equipo Rototec, en una mezcla de sal 20% Na2SO4 - 80% V2O5, entre 400ºC - 600ºC, durante tiempos de 1-7-22 horas. Los resultados mostraron una moderada protección de la capa rociada térmicamente y se presentó alta degradación en el recubrimiento a 600ºC. Se concluyó que la velocidad de corrosión aumenta con la temperatura y disminuye con el tiempo de exposición.

  12. Preparation and characterization of 304 stainless steel/Q235 carbon steel composite material

    Directory of Open Access Journals (Sweden)

    Wenning Shen

    Full Text Available The composite material of 304 stainless steel reinforced Q235 carbon steel has been prepared by modified hot-rolling process. The resulted material was characterized by scanning electron microscope, three-electrode method, fault current impact method, electrochemical potentiodynamic polarization curve measurement and electrochemical impedance spectroscopy. The results showed that metallurgical bond between the stainless steel layer and carbon steel substrate has been formed. The composite material exhibited good electrical conductivity and thermal stability. The average grounding resistance of the composite material was about 13/20 of dip galvanized steel. There has no surface crack and bubbling formed after fault current impact. The composite material led to a significant decrease in the corrosion current density in soil solution, compared with that of hot dip galvanized steel and bare carbon steel. On the basis polarization curve and EIS analyses, it can be concluded that the composite material showed improved anti-corrosion property than hot-dip galvanized steel. Keywords: Stainless steel, Carbon steel, Anti-corrosion, Conductivity, Electrochemical, EIS

  13. Surface conditioning of a cold-rolled dual-phase steel by annealing in nitriding atmospheres prior to hot-dip galvanizing

    Energy Technology Data Exchange (ETDEWEB)

    Luther, F.; Beste, D.; Bleck, W. [Institute for Ferrous Metallurgy (IEHK), RWTH Aachen (Germany); Dimyati, A.; Mayer, J. [Central Facility for Electron Microscopy (GFE), RWTH Aachen (Germany)

    2007-04-15

    The development of steel grades for automotive applications in the recent years has been driven on by two trends: lightweight and improved crash safety. By using steels like DP (dual phase) the goals of passenger safety, fuel efficiency and environmental friendliness can be met at reasonable price. The favorite corrosion protection method for sheet steels in the car industry is the hot-dip galvanizing process. Here, an approach was made to reduce the surface enrichment of critical alloying elements of a dual phase steel grade by reactive annealing in ammonia containing atmospheres. The effects of this treatment on mechanical properties and hot-dip coating behavior are reported. (Abstract Copyright [2007], Wiley Periodicals, Inc.)

  14. Kulturens rolle

    DEFF Research Database (Denmark)

    Hasse, Cathrine

    2007-01-01

    Kulturens rolle. Herunder kulturens betydning for psykologisk teori og forskning set i lyset af den stigende globalisering og væksten i kulturmøder. Der gives eksempler fra hverdagssituationer, den pædagogiske praksis, fra indvandrerforskning, turister men også fra avisernes referater af kulturmø......Kulturens rolle. Herunder kulturens betydning for psykologisk teori og forskning set i lyset af den stigende globalisering og væksten i kulturmøder. Der gives eksempler fra hverdagssituationer, den pædagogiske praksis, fra indvandrerforskning, turister men også fra avisernes referater af...

  15. Rolling Process Modeling Report: Finite-Element Prediction of Roll Separating Force and Rolling Defects

    Energy Technology Data Exchange (ETDEWEB)

    Soulami, Ayoub [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Lavender, Curt A. [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Paxton, Dean M. [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Burkes, Douglas [Pacific Northwest National Lab. (PNNL), Richland, WA (United States)

    2014-04-23

    Pacific Northwest National Laboratory (PNNL) has been investigating manufacturing processes for the uranium-10% molybdenum (U-10Mo) alloy plate-type fuel for the U.S. high-performance research reactors. This work supports the Convert Program of the U.S. Department of Energy’s National Nuclear Security Administration (DOE/NNSA) Global Threat Reduction Initiative. This report documents modeling results of PNNL’s efforts to perform finite-element simulations to predict roll separating forces and rolling defects. Simulations were performed using a finite-element model developed using the commercial code LS-Dyna. Simulations of the hot rolling of U-10Mo coupons encapsulated in low-carbon steel have been conducted following two different schedules. Model predictions of the roll-separation force and roll-pack thicknesses at different stages of the rolling process were compared with experimental measurements. This report discusses various attributes of the rolled coupons revealed by the model (e.g., dog-boning and thickness non-uniformity).

  16. Effects of Ultra-Fast Cooling After Hot Rolling and Intercritical Treatment on Microstructure and Cryogenic Toughness of 3.5%Ni Steel

    Science.gov (United States)

    Wang, Meng; Liu, Zhenyu

    2017-07-01

    A novel process comprised of ultra-fast cooling after control rolling, intercritical quenching and tempering (UFC-LT) was applied to 3.5%Ni steel. In addition, quenching and tempering (QT) treatment was conducted in comparison. The present study focuses on the relationship between the microstructure and cryogenic toughness of 3.5%Ni steel. Results show that the microstructure of steel treated by UFC-LT consisted of tempered martensite, intercritical ferrite and two types of reversed austenite (RA) (needle shape and blocky). Compared to the QT sample, the UFC-LT sample's ultimate tensile strength decreased slightly, while its elongation increased from 32.3 to 35.7%, and its Charpy absorption energy at -135 °C increased from 112 to 237 J. The ductile-brittle transition temperature of UFC-LT sample was lower than that of the QT sample by 18 °C. The superior cryogenic toughness after UFC-LT compared to QT treatment can be attributed to the dissolution of cementite, approximately 3.0% increase in RA and the decrease in effective grain size.

  17. Phase transformation kinetics in rolled U-10 wt. % Mo foil: Effect of post-rolling heat treatment and prior γ-UMo grain size

    Energy Technology Data Exchange (ETDEWEB)

    Jana, Saumyadeep; Overman, Nicole; Varga, Tamas; Lavender, Curt; Joshi, Vineet V.

    2017-12-01

    The effect of sub-eutectoid heat treatment on the phase transformation behavior in rolled U-10 wt.percent Mo (U10Mo) foils was systematically investigated. The as-cast 5 mm thick foils were initially homogenized at 900 degrees C for 48 hours and were hot rolled to 2 mm and later cold rolled down to 0.2 mm. Three starting microstructures were evaluated: (i) hot- + cold-rolled to 0.2 mm (as-rolled condition), (ii) hot- + cold-rolled to 0.2 mm + annealed at 700 deg. C for 1 hour, and (iii) hot- + cold-rolled to 0.2 mm + annealed at 1000 deg. C for 60 hours. U10Mo rolled foils went through various degrees of decomposition when subjected to the sub-eutectoid heat-treatment step and formed a lamellar microstructure through a cellular reaction mostly along the previous γ-UMo grain boundaries.

  18. Characterization of thermal aging of duplex stainless steel by SQUID

    International Nuclear Information System (INIS)

    Isobe, Y.; Kamimura, A.; Aoki, K.; Nakayasu, F.

    1995-01-01

    Thermal aging is a growing concern for long-term-aged duplex stainless steel piping in nuclear power plants. Superconducting QUantum Interference Device (SQUID) was used for the detection of thermal aging of SUS329 rolled duplex stainless steel and SCS16 cast duplex stainless steel. It was found that the SQUID output signal pattern in the presence of AC magnetic field applied to the specimen was sensitive to the changes in electromagnetic properties due to thermal aging

  19. Solidification cracking in austenitic stainless steel welds

    Indian Academy of Sciences (India)

    M. Senthilkumar (Newgen Imaging) 1461 1996 Oct 15 13:05:22

    Hot cracking in stainless steel welds is caused by low-melting eutectics containing impurities such as S, ... Total crack length (TCL), used extensively in hot cracking assessment, exhibits greater variability due to ... behaviour appear to be complex and the mechanisms thereof are not completely under- stood. Development of ...

  20. 77 FR 49477 - WTO Dispute Settlement Proceeding Regarding United States-Countervailing Measures on Certain Hot...

    Science.gov (United States)

    2012-08-16

    ... Proceeding Regarding United States-- Countervailing Measures on Certain Hot-Rolled Carbon Steel Flat Products... certain hot-rolled carbon steel flat products from India. That request may be found at www.wto.org... countervailing measures regarding certain hot-rolled carbon steel flat products from India (Investigation C-533...

  1. 77 FR 26600 - WTO Dispute Settlement Proceeding Regarding United States-Countervailing Measures on Certain Hot...

    Science.gov (United States)

    2012-05-04

    ... Proceeding Regarding United States-- Countervailing Measures on Certain Hot-Rolled Carbon Steel Flat Products... certain hot-rolled carbon steel flat products from India. That request may be found at www.wto.org... requested consultations concerning countervailing measures regarding certain hot-rolled carbon steel flat...

  2. Manufacture and qualification of hot roll-clad composites with nickel base cladding material for use in flue gas desulphurization plants. Final report; Herstellung und Qualifizierung warmwalzplattierter Verbundwerkstoffe mit Nickelbasisauflagen fuer den Einsatz in Rauchgasentschwefelungsanlagen. Schlussbericht

    Energy Technology Data Exchange (ETDEWEB)

    Kirchheiner, R.; Stenner, F.

    1992-03-16

    Flue gas desulphurization plants (FGD), which have been required by law since 1983, mainly apply wet scrubbing techniques. The chemical reactions taking place in those plants lead to extremely corrosive situations. Unprotected carbon steel surfaces or organic based anticorrosive systems are extremely affected after being in operation for only a few years. NiCrM alloys applied by the chemical industry in comparable situations have proved their efficiency for decades. When such massive components are newly built in FDGs, economic aspects require the use of those NiCrMo alloys in clad form. Within the frame of this project tests included the manufacture of hot roll-clad composites comprising cladding materials of the type NiMo16Cr15W (2.4819) and NiCr21Mo14W (2.4602) on the base steel RST 37-2. Large-sized sheets (10000 x 2000 x 10+2 mm) were made by means of an optimized cladding technique. The behaviour of the cladding material in case of uniform and local corrosion exposure was examined in standard laboratory tests. An increased susceptibility to intercrystalline corrosion was not detected, according to the excellent microstructure. Further laboratory tests under simulated FGD conditions and exposure tests in FGDs in operation permitted the transfer of those positive test results to practical work. The same applies without limitation to the joint-welded state with similar filler material of clad a comparable chemical composition. With respect to their technological behaviour the new hot roll-clad composites correspond to that of solid sheets of NiCrMo alloys; therefore they are qualified for use in flue gas desulphurization plants. (orig./BBR) With 32 refs., 13 tabs., 29 figs. [Deutsch] In den seit 1983 gesetzlich vorgeschriebenen Anlagen zur Rauchgasentschwefelung (REA) werden ueberwiegend nasse Waschverfahren eingesetzt. Die in diesen Anlagen ablaufenden chemischen Reaktionen fuehren zu extrem korrosiven Bedingungen. Ungeschuetzte C-Stahl-Oberflaechen bzw

  3. A morphological evaluation of a duplex stainless steel processed by high energy Ball Mill

    International Nuclear Information System (INIS)

    Yonekubo, Ariane Emi; Cintho, Osvaldo Mitsuyuki; Aguiar, Denilson Jose Marcolino de; Capocchi, Jose Deodoro Trani

    2009-01-01

    The duplex stainless steels are formed by a ferrite and austenite mixture, giving them a combination of properties. Commercially, these steels are hot rolled, developing an anisotropic, alternated ferrite and austenite elongated lamellae microstructure. In this work, a duplex stainless steel was produced by the mixture of elementary powders with the composition Fe-19.5Cr-5Ni processed in an ATTRITOR ball mill during periods up to 15 hours. The powders obtained were compressed in specimens and were heat treated in the temperatures of 900, 1050 and 1200 °C during 1 hour and analysed by x ray diffraction, optic microscopy, scanning electron microscopy and energy dispersion spectroscopy. An optimized microstructure with ultrafine, equiaxial and regular duplex microstructure was obtained in the 15 hour milling and 1200 °C heat treatment. Afterwards, a commercially super duplex stainless steel UNS S32520 was aged at 800 °C aiming the precipitation of σ phase in order to reduce its toughness and then, milled in SPEX mill. The resulting microstructure was a very fine duplex type with irregular grain boundary morphology duo to the grain growth barrier promoted by the renascent σ phase particles during sintering process. (author)

  4. Tritiated Water Interaction with Stainless Steel

    International Nuclear Information System (INIS)

    Glen R. Longhurst

    2007-01-01

    Experiments conducted to study tritium permeation of stainless steel at ambient and elevated temperatures revealed that HT converts relatively quickly to HTO. Further, the HTO partial pressure contributes essentially equally with elemental tritium gas in driving permeation through the stainless steel. Such permeation appears to be due to dissociation of the water molecule on the hot stainless steel surface. There is an equilibrium concentration of HTO vapor above adsorbed gas on the walls of the experimental apparatus evident from freezing transients. The uptake process of tritium from the carrier gas involves both surface adsorption and isotopic exchange with surface bound water

  5. Rolling induced size effects in elastic–viscoplastic sheet metals

    DEFF Research Database (Denmark)

    Nielsen, Kim Lau

    2015-01-01

    sheet rolling, where a non-homogeneous material deformation takes place between the rollers. Large strain gradients develop where the rollers first come in contact with the sheet, and a higher order plasticity model is employed to illustrate their influence at small scales. The study reveals...... presented revolves around the rolling induced effect of visco-plasticity (ranging hot and cold rolling) in combination with strain gradient hardening – including both dissipative and energetic contributions. To bring out first order effects on rolling at small scale, the modeling efforts are limited to flat...

  6. Review of the continuous casting of steel by strip casting technology. Twin roll method system

    International Nuclear Information System (INIS)

    Ibarrondo, I.

    2008-01-01

    In order to compete in the future steel market and to maintain market share, the steel makers will need to use new efficient technologies capable of supplying steel strip products of high quality at low cost. In this way, the strip casting technology by twin rol method is one of the most important research are in the iron and steel industry today. This review makes a general description of the strip casting technology as well as its different steps, such us; metal delivery and casting, solidification process, hot rolling reduction step, etc. Through mathematical and physical models, the influence on microstructure texture surface quality and mechanical properties of the materials obtained by this method are described as a function of processing parameters, specially the roughness of the rolls. the manufacturing of carbon, stainless and electrical steels involves smaller capital and operating cost, lower gas emissions, and an opportunity to create new grades due to a faster solidification rate that leads to a different solidification structures. In sight of all this it is likely that Strip Casting technology will make a profound impact on the manufacturing landscape of the 21 s t century. (Author) 177 refs

  7. Industrialization of hot wire chemical vapor deposition for thin film applications

    NARCIS (Netherlands)

    Schropp, Ruud

    2015-01-01

    The consequences of implementing a Hot Wire Chemical Vapor Deposition (HWCVD) chamber into an existing in-line or roll-to-roll reactor are described. The hardware and operation of the HWCVD production reactor is compared to that of existing roll-to-roll reactors based on Plasma Enhanced Chemical

  8. Stainless steel recycle FY94 progress report

    International Nuclear Information System (INIS)

    Imrich, K.J.

    1994-01-01

    The Materials Technology Section (MTS) of the Savannah River Technology Center (SRTC) was asked to demonstrate the practicality of recycling previously contaminated stainless steel components such as reactor heat exchanger heads, process water piping and slug buckets into 208 liters (55 gallon) drums and 2.8 cubic meter (100 ft 3 ) storage boxes. Radioactively contaminated stainless steel scrap will be sent to several industrial partners where it will be melted, decontaminated/cast into ingots, and rolled into plate and sheet and fabricated into the drums and boxes. As part of this recycle initiative, MTS was requested to demonstrate that radioactively contaminated Type 304L stainless steel could be remelted and cast to meet the applicable ASTM specification for fabrication of drums and boxes. In addition, MTS was requested to develop the technical basis of melt decontamination and establish practicality of using this approach for value added products. The findings presented in this investigation lead to the following conclusions: recycle of 18 wt% Cr-8 wt% Ni alloy can be achieved by melting Type 304 stainless steel in a air vacuum induction furnace; limited melt decontamination of the contaminated stainless steel was achieved, surface contamination was removed by standard decontamination techniques; carbon uptake in the as-cast ingots resulted from the graphite susceptor used in this experiment and is unavoidable with this furnace configuration. A new furnace optimized for melting stainless steel has been installed and is currently being tested for use in this program

  9. Effect of Solution Annealing on Susceptibility to Intercrystalline Corrosion of Stainless Steel with 20% Cr and 8% Ni

    Science.gov (United States)

    Taiwade, R. V.; Patil, A. P.; Patre, S. J.; Dayal, R. K.

    2013-06-01

    In general, as-received (AR) austenitic stainless steels (ASSs) contain complex carbide precipitates due to manufacturing operations, subsequent annealing treatment, or due to the fabrication processes such as welding. The presence of pre-existing carbides leads to cumulative sensitization and make the steel susceptible to intercrystalline corrosion (ICC)/intergranular corrosion (IGC) which causes premature failure during service. Solution annealing (SA) is one of the ways to deal with such situations. In this present investigation, the AR (hot rolled and mill annealed) chromium-nickel (Cr-Ni) ASS is compared with SA Cr-Ni ASS. The extent of ICC/IGC was evaluated qualitatively and quantitatively by various electrochemical tests including ASTM standard A-262 Practice A and Practice E, double loop electrochemical potentiokinetic reactivation and electrochemical impedance spectroscopy. The degree of sensitization for hot rolled mill annealed AR condition is found to be substantially higher (51.55%) than that of SA condition (26.9%) for thermally aged samples (at 700 °C). The chemical composition across the grain boundary was measured using electron probe micro-analyzer for both (AR and SA) conditions and confirms that the pre-sensitization effect was completely removed after SA treatment.

  10. Effect of Starting As-cast Structure on the Microstructure-Texture Evolution During Subsequent Processing and Finally Ridging Behavior of Ferritic Stainless Steel

    Science.gov (United States)

    Modak, Pranabananda; Patra, Sudipta; Mitra, Rahul; Chakrabarti, Debalay

    2018-06-01

    Effect of the initial as-cast structure on the microstructure-texture evolution during thermomechanical processing of 409L grade ferritic stainless steel was studied. Samples from the regions of cast slab having `columnar,' `equiaxed,' and a mixture of `columnar' and `equiaxed' grains were subjected to two different processing schedules: one with intermediate hot-band annealing before cold-rolling followed by final annealing, and another without any hot-band annealing. EBSD study reveals that large columnar crystals with cube orientation are very difficult to deform and recrystallize uniformly. Resultant variations in ferrite grain structure and retention of cube-textured band in cold-rolled and annealed sheet contribute to ridging behavior during stretch forming. Initial equiaxed grain structure is certainly beneficial to reduce or even eliminate ridging defect by producing uniform ferrite grain structure, free from any texture banding. Application of hot-band annealing treatment is also advantageous as it can maximize the evolution of beneficial gamma-fiber texture and eliminate the ridging defect in case of completely `equiaxed' starting structure. Such treatment reduces the severity of ridging even if the initial structure contains typically mixed `columnar-equiaxed' grains.

  11. Rolling Shutter Motion Deblurring

    KAUST Repository

    Su, Shuochen

    2015-06-07

    Although motion blur and rolling shutter deformations are closely coupled artifacts in images taken with CMOS image sensors, the two phenomena have so far mostly been treated separately, with deblurring algorithms being unable to handle rolling shutter wobble, and rolling shutter algorithms being incapable of dealing with motion blur. We propose an approach that delivers sharp and undis torted output given a single rolling shutter motion blurred image. The key to achieving this is a global modeling of the camera motion trajectory, which enables each scanline of the image to be deblurred with the corresponding motion segment. We show the results of the proposed framework through experiments on synthetic and real data.

  12. Ring rolling process simulation for geometry optimization

    Science.gov (United States)

    Franchi, Rodolfo; Del Prete, Antonio; Donatiello, Iolanda; Calabrese, Maurizio

    2017-10-01

    Ring Rolling is a complex hot forming process where different rolls are involved in the production of seamless rings. Since each roll must be independently controlled, different speed laws must be set; usually, in the industrial environment, a milling curve is introduced to monitor the shape of the workpiece during the deformation in order to ensure the correct ring production. In the present paper a ring rolling process has been studied and optimized in order to obtain anular components to be used in aerospace applications. In particular, the influence of process input parameters (feed rate of the mandrel and angular speed of main roll) on geometrical features of the final ring has been evaluated. For this purpose, a three-dimensional finite element model for HRR (Hot Ring Rolling) has been implemented in SFTC DEFORM V11. The FEM model has been used to formulate a proper optimization problem. The optimization procedure has been implemented in the commercial software DS ISight in order to find the combination of process parameters which allows to minimize the percentage error of each obtained dimension with respect to its nominal value. The software allows to find the relationship between input and output parameters applying Response Surface Methodology (RSM), by using the exact values of output parameters in the control points of the design space explored through FEM simulation. Once this relationship is known, the values of the output parameters can be calculated for each combination of the input parameters. After the calculation of the response surfaces for the selected output parameters, an optimization procedure based on Genetic Algorithms has been applied. At the end, the error between each obtained dimension and its nominal value has been minimized. The constraints imposed were the maximum values of standard deviations of the dimensions obtained for the final ring.

  13. Control of surface thermal scratch of strip in tandem cold rolling

    Science.gov (United States)

    Chen, Jinshan; Li, Changsheng

    2014-07-01

    The thermal scratch seriously affects the surface quality of the cold rolled stainless steel strip. Some researchers have carried out qualitative and theoretical studies in this field. However, there is currently a lack of research on effective forecast and control of thermal scratch defects in practical production, especially in tandem cold rolling. In order to establish precise mathematical model of oil film thickness in deformation zone, the lubrication in cold rolling process of SUS410L stainless steel strip is studied, and major factors affecting oil film thickness are also analyzed. According to the principle of statistics, mathematical model of critical oil film thickness in deformation zone for thermal scratch is built, with fitting and regression analytical method, and then based on temperature comparison method, the criterion for deciding thermal scratch defects is put forward. Storing and calling data through SQL Server 2010, a software on thermal scratch defects control is developed through Microsoft Visual Studio 2008 by MFC technique for stainless steel in tandem cold rolling, and then it is put into practical production. Statistics indicate that the hit rate of thermal scratch is as high as 92.38%, and the occurrence rate of thermal scratch is decreased by 89.13%. Owing to the application of the software, the rolling speed is increased by approximately 9.3%. The software developed provides an effective solution to the problem of thermal scratch defects in tandem cold rolling, and helps to promote products surface quality of stainless steel strips in practical production.

  14. Effect of cold working and aging on high temperature deformation of high Mn stainless steel

    International Nuclear Information System (INIS)

    Yoshikawa, M.; Habara, Y.; Matsuki, R.; Aoyama, H.

    1999-01-01

    By the addition of N, the strength of high Mn stainless steel can be increased. Cold rolling and aging are effective to increase its strength further, and with those treatments this grade is often used for high temperature applications. In this study, creep deformation behavior and high temperature strength of the high Mn stainless steel in cold rolled and aged conditions are discussed as compared to Type 304 stainless steel. It has been revealed that as-rolled specimens show instant elongation at the beginning of creep tests and its amount is larger in the high Mn grade than in Type 304. Also, the creep rate of the high Mn stainless steel is smaller than that of Type 304. These facts may be related to the change in microstructure. (orig.)

  15. Development of Rolling Schedules for AZ31 Magnesium Alloy Sheets

    Science.gov (United States)

    2015-06-01

    Materials 2 2.2 Hot Rolling 3 2.2 Sample Characterization: Microstructure and Tensile Properties 3 3. Rolling Experiments 5 3.1 High-Temperature...material systems for protective and structural applications, especially in ground vehicles. Magnesium (Mg), due to its low density (~25% that of steel ...applications, wrought Mg is difficult to produce in thin sheets because of its inherently low ductility . As a result, Mg sheet is often produced at

  16. An advanced dissymmetric rolling model for online regulation

    Science.gov (United States)

    Cao, Trong-Son

    2017-10-01

    Roll-bite model is employed to predict the rolling force, torque as well as to estimate the forward slip for preset or online regulation at industrial rolling mills. The rolling process is often dissymmetric in terms of work-rolls rotation speeds and diameters as well as the friction conditions at upper and lower contact surfaces between work-rolls and the strip. The roll-bite model thus must be able to account for these dissymmetries and in the same time has to be accurate and fast enough for online applications. In the present study, a new method, namely Adapted Discretization Slab Method (ADSM) is proposed to obtain a robust roll-bite model, which can take into account the aforementioned dissymmetries and has a very short response time, lower than one millisecond. This model is based on the slab method, with an adaptive discretization and a global Newton-Raphson procedure to improve the convergence speed. The model was validated by comparing with other dissymmetric models proposed in the literature, as well as Finite Element simulations and industrial pilot trials. Furthermore, back-calculation tool was also constructed for friction management for both offline and online applications. With very short CPU time, the ADSM-based model is thus attractive for all online applications, both for cold and hot rolling.

  17. Ship Roll Damping Control

    DEFF Research Database (Denmark)

    Perez, Tristan; Blanke, Mogens

    2012-01-01

    limitations and large variations of the spectral characteristics of wave-induced roll motion. This tutorial paper presents an account of the development of various ship roll motion control systems together with the challenges associated with their design. It discusses the assessment of performance...

  18. Cosmology with rolling tachyon

    Indian Academy of Sciences (India)

    Email: sami@iucaa.ernet.in. Abstract. We examine the possibility of rolling tachyon to play the dual role of inflaton at early epochs and dark matter at late times. We argue that enough inflation can be generated with the rolling tachyon either by invoking the large number of branes or brane world assisted inflation. However ...

  19. Origins of Rolling Friction

    Science.gov (United States)

    Cross, Rod

    2017-01-01

    When a hard object rolls on a soft surface, or vice versa, rolling friction arises from deformation of the soft object or the soft surface. The friction force can be described in terms of an offset in the normal reaction force or in terms of energy loss arising from the deformation. The origin of the friction force itself is not entirely clear. It…

  20. Evolution of microstructure at hot band annealing of ferritic FeSi steels

    Energy Technology Data Exchange (ETDEWEB)

    Schneider, Jürgen, E-mail: juergen.schneider@t-online.de [Institute of Metal Forming, Technische Universität Bergakademie Freiberg, Bernhard-von Cotta-Str. 4, D-09596 Freiberg (Germany); Stahlzentrum Freiberg e.V., Leipziger Straße 34, D-09599 Freiberg (Germany); Li, Guangqiang [State Key Lab. of Refractories and Metallurgy, Wuhan University of Science and Technology, No. 947 Heping Avenue, Qingshan District, Wuhan 430081 (China); Franke, Armin [Stahlzentrum Freiberg e.V., Leipziger Straße 34, D-09599 Freiberg (Germany); Zhou, Bowen [State Key Lab. of Refractories and Metallurgy, Wuhan University of Science and Technology, No. 947 Heping Avenue, Qingshan District, Wuhan 430081 (China)

    2017-02-15

    The magnetic properties of the finally fabricated nonoriented FeSi steels critically depend on the microstructure and on the occurring crystallographic texture. The fabrication route comprises hot rolling, coiling and cooling, hot band annealing before cold rolling (optional), cold rolling and the final thermal treatment. As well known there is an interplay between the microstructure and texture during the various processing steps. For that reason, it is of interest to know more on the evolution of the microstructure at hot band annealing of hot band prepared in different ways. In this paper we will summarize our recent results on the evolution of microstructure during thermal annealing of hot band: thermal treatment following immediately the last pass of hot rolling or a hot band annealing as a separate processing step before cold rolling.

  1. Fatigue Crack Growth Behavior of Gas Metal Arc Welded AISI 409 Grade Ferritic Stainless Steel Joints

    Science.gov (United States)

    Lakshminarayanan, A. K.; Shanmugam, K.; Balasubramanian, V.

    2009-10-01

    The effect of filler metals such as austenitic stainless steel, ferritic stainless steel, and duplex stainless steel on fatigue crack growth behavior of the gas metal arc welded ferritic stainless steel joints was investigated. Rolled plates of 4 mm thickness were used as the base material for preparing single ‘V’ butt welded joints. Center cracked tensile specimens were prepared to evaluate fatigue crack growth behavior. Servo hydraulic controlled fatigue testing machine with a capacity of 100 kN was used to evaluate the fatigue crack growth behavior of the welded joints. From this investigation, it was found that the joints fabricated by duplex stainless steel filler metal showed superior fatigue crack growth resistance compared to the joints fabricated by austenitic and ferritic stainless steel filler metals. Higher yield strength and relatively higher toughness may be the reasons for superior fatigue performance of the joints fabricated by duplex stainless steel filler metal.

  2. Deformation mechanisms of pure Mg materials fabricated by using pre-rolled powders

    Energy Technology Data Exchange (ETDEWEB)

    Shen, J., E-mail: shen-j@jwri.osaka-u.ac.jp [Joining and Welding Research Institute, Osaka University (Japan); Imai, H. [Joining and Welding Research Institute, Osaka University (Japan); Chen, B. [Graduate School of Engineering, Osaka University (Japan); Ye, X.; Umeda, J.; Kondoh, K. [Joining and Welding Research Institute, Osaka University (Japan)

    2016-03-21

    In the present work, a powder rolling process was utilized in the fabrication of fine grained pure Mg via powder metallurgy. Mg flakes were obtained after each rolling process, and broken into pieces for further rolling or sintering. Mg samples of experiencing 0, 5 and 10 rolling passes were obtained following spark plasma sintering (SPS) and hot extrusion. Microstructural results from electron backscatter diffraction (EBSD) revealed that, without experiencing powder rolling, the specimen contained a great number of residual tensile twins; in contrast, after powder rolling the specimen showed uniform and equiaxed grain structures. In addition, the average grain size was measured to be around 9.2, 2.9 and 2.1 µm for the samples subjected to 0, 5 and 10 rolling passes. The powder rolled specimens were found superior in mechanical properties. Post-loading microstructure examinations were also performed for the samples and a discussion regarding the relationship between their mechanical behavior and microstructures was provided.

  3. Deformation mechanisms of pure Mg materials fabricated by using pre-rolled powders

    International Nuclear Information System (INIS)

    Shen, J.; Imai, H.; Chen, B.; Ye, X.; Umeda, J.; Kondoh, K.

    2016-01-01

    In the present work, a powder rolling process was utilized in the fabrication of fine grained pure Mg via powder metallurgy. Mg flakes were obtained after each rolling process, and broken into pieces for further rolling or sintering. Mg samples of experiencing 0, 5 and 10 rolling passes were obtained following spark plasma sintering (SPS) and hot extrusion. Microstructural results from electron backscatter diffraction (EBSD) revealed that, without experiencing powder rolling, the specimen contained a great number of residual tensile twins; in contrast, after powder rolling the specimen showed uniform and equiaxed grain structures. In addition, the average grain size was measured to be around 9.2, 2.9 and 2.1 µm for the samples subjected to 0, 5 and 10 rolling passes. The powder rolled specimens were found superior in mechanical properties. Post-loading microstructure examinations were also performed for the samples and a discussion regarding the relationship between their mechanical behavior and microstructures was provided.

  4. Hot Flashes

    Science.gov (United States)

    Hot flashes Overview Hot flashes are sudden feelings of warmth, which are usually most intense over the face, neck and chest. Your skin might redden, as if you're blushing. Hot flashes can also cause sweating, and if you ...

  5. HOT 2015

    DEFF Research Database (Denmark)

    Hannibal, Sara Stefansen

    2016-01-01

    HOT samler og formidler 21 literacykyndiges bud på, hvad der er hot, og hvad der bør være hot inden for literacy – og deres begrundelser for disse bud.......HOT samler og formidler 21 literacykyndiges bud på, hvad der er hot, og hvad der bør være hot inden for literacy – og deres begrundelser for disse bud....

  6. Precision ring rolling technique and application in high-performance bearing manufacturing

    Directory of Open Access Journals (Sweden)

    Hua Lin

    2015-01-01

    Full Text Available High-performance bearing has significant application in many important industry fields, like automobile, precision machine tool, wind power, etc. Precision ring rolling is an advanced rotary forming technique to manufacture high-performance seamless bearing ring thus can improve the working life of bearing. In this paper, three kinds of precision ring rolling techniques adapt to different dimensional ranges of bearings are introduced, which are cold ring rolling for small-scale bearing, hot radial ring rolling for medium-scale bearing and hot radial-axial ring rolling for large-scale bearing. The forming principles, technological features and forming equipments for three kinds of precision ring rolling techniques are summarized, the technological development and industrial application in China are introduced, and the main technological development trend is described.

  7. Standard practice for evaluation of disbonding of bimetallic stainless alloy/steel plate for use in high-pressure, high-temperature refinery hydrogen service

    CERN Document Server

    American Society for Testing and Materials. Philadelphia

    2001-01-01

    1.1 This practice covers a procedure for the evaluation of disbonding of bimetallic stainless alloy/steel plate for use in refinery high-pressure/high-temperature (HP/HT) gaseous hydrogen service. It includes procedures to (1) produce suitable laboratory test specimens, (2) obtain hydrogen charging conditions in the laboratory that are similar to those found in refinery HP/HT hydrogen gas service for evaluation of bimetallic specimens exposed to these environments, and (3) perform analysis of the test data. The purpose of this practice is to allow for comparison of data among test laboratories on the resistance of bimetallic stainless alloy/steels to hydrogen-induced disbonding (HID). 1.2 This practice applies primarily to bimetallic products fabricated by weld overlay of stainless alloy onto a steel substrate. Most of the information developed using this practice has been obtained for such materials. The procedures described herein, may also be appropriate for evaluation of hot roll bonded, explosive bonded...

  8. Aluminide Coating on Stainless Steel for Nuclear Reactor Application: A Preliminary Study

    International Nuclear Information System (INIS)

    Hishamuddin Husain; Zaifol Samsu; Yusof Abdullah; Muhamad Daud

    2015-01-01

    Stainless steels have been used as structural materials in the nuclear reactor since its first generation. Stainless steels type 304 and 316 are commonly used in structural components. Since the first generation materials, improvements were made on Stainless steels. This includes addition of stabilizing elements and by modification of metallurgical structure. This study investigates the formation of aluminide coating on Stainless steels by diffusion to help improve corrosion resistance. Stainless steels type 304 and 316 substrates were immersed in molten aluminium at 750 degree Celsius for 5 minutes. Interaction between molten aluminium and solid to form the outer aluminide coating by hot dipped aluminizing is studied. (Author)

  9. Phosphate coating on stainless steel 304 sensitized

    International Nuclear Information System (INIS)

    Cruz V, J. P.; Vite T, J.; Castillo S, M.; Vite T, M.

    2009-01-01

    The stainless steel 304 can be sensitized when welding processes are applied, that causes the precipitation of chromium carbide in the grain limits, being promoted in this way the formation of galvanic cells and consequently the corrosion process. Using a phosphate coating is possible to retard the physiochemical damages that can to happen in the corrosion process. The stainless steel 304 substrate sensitized it is phosphate to base of Zn-Mn, in a immersion cell very hot. During the process was considered optimization values, for the characterization equipment of X-rays diffraction and scanning electron microscopy was used. The XRD technique confirmed the presence of the phases of manganese phosphate, zinc phosphate, as well as the phase of the stainless steel 304. When increasing the temperature from 60 to 90 C in the immersion process a homogeneous coating is obtained. (Author)

  10. Weldability of Stainless Steels

    International Nuclear Information System (INIS)

    Saida, Kazuyoshi

    2010-01-01

    It gives an outline of metallographic properties of welding zone of stainless steels, generation and mechanisms of welding crack and decreasing of corrosion resistance of welding zone. It consists of seven chapters such as introduction, some kinds of stainless steels and properties, metallographic properties of welding zone, weld crack, toughness of welding zone, corrosion resistance and summary. The solidification modes of stainless steels, each solidification mode on the cross section of Fe-Cr-Ni alloy phase diagram, each solidification mode of weld stainless steels metal by electron beam welding, segregation state of alloy elements at each solidification mode, Schaeffler diagram, Delong diagram, effects of (P + S) mass content in % and Cr/Ni equivalent on solidification cracking of weld stainless steels metal, solidification crack susceptibility of weld high purity stainless steels metal, effects of trace impurity elements on solidification crack susceptibility of weld high purity stainless steels metal, ductile fracture susceptibility of weld austenitic stainless steels metal, effects of H2 and ferrite content on generation of crack of weld 25Cr-5N duplex stainless steels, effects of O and N content on toughness of weld SUS 447J1 metals, effect of ferrite content on aging toughness of weld austenitic stainless steel metal, corrosion morphology of welding zone of stainless steels, generation mechanism of knife line attack phenomenon, and corrosion potential of some kinds of metals in seawater at room temperature are illustrated. (S.Y.)

  11. Investigation of hot cracking in deep penetration electron beam welds

    Energy Technology Data Exchange (ETDEWEB)

    Thorvaldson, W.G.

    1978-06-10

    A defect in a deep penetration electron beam weld of 304L stainless steel to 21-6-9 stainless steel has been identified as a centerline hot crack. The study discussed in this report was made to define and to eliminate the cause of cracking.

  12. Crystal plasticity modeling of through-thickness texture heterogeneity in heavily rolled aluminum

    DEFF Research Database (Denmark)

    Delannay, Laurent; Mishin, Oleg V.

    2013-01-01

    from hot rolling producing shear near the surface and conditions approaching plane strain compression in the center layer. Model predictions confirm experimental observations that such a gradient strengthens significantly during further heavy cold rolling. Copyright © 2013 Trans Tech Publications Ltd....

  13. Diffusionless bonding of aluminum to type 304 stainless steel

    Energy Technology Data Exchange (ETDEWEB)

    Watson, R D

    1963-03-15

    High strength diffusionless bonds can be produced between 1S aluminum and oxidized 304 stainless steel by hot pressing and extrusion bonding. Both the hot pressing and extrusion bonding techniques have been developed to a point where consistently good bonds can be obtained. Although the bonding is performed at elevated temperatures (about 510{sup o}C) a protective atmosphere is not required to produce strong bonds. The aluminum-stainless steel bonded specimens can be used to join aluminum and stainless steel by conventional welding. Welding close to the bond zone does not appear to affect the integrity of the bond. The extrusion bonding technique is covered by Canadian patent 702,438 January 26, 1965 and the hot press bonding technique by Canadian patent application 904,548 June 6, 1964. (author)

  14. Diffusionless bonding of aluminum to type 304 stainless steel

    International Nuclear Information System (INIS)

    Watson, R.D.

    1963-03-01

    High strength diffusionless bonds can be produced between 1S aluminum and oxidized 304 stainless steel by hot pressing and extrusion bonding. Both the hot pressing and extrusion bonding techniques have been developed to a point where consistently good bonds can be obtained. Although the bonding is performed at elevated temperatures (about 510 o C) a protective atmosphere is not required to produce strong bonds. The aluminum-stainless steel bonded specimens can be used to join aluminum and stainless steel by conventional welding. Welding close to the bond zone does not appear to affect the integrity of the bond. The extrusion bonding technique is covered by Canadian patent 702,438 January 26, 1965 and the hot press bonding technique by Canadian patent application 904,548 June 6, 1964. (author)

  15. Advanced cold rolled steels for automotive applications

    Energy Technology Data Exchange (ETDEWEB)

    Hofmann, Harald; Mattissen, Dorothea; Schaumann, Thomas Wilhelm [ThyssenKrupp Steel AG, Center of Materials Excellence, Dortmund (Germany)

    2009-01-15

    Advanced high-strength steels offer a great potential for the further development of automobile bodies-in-white due to their combined mechanical properties of high formability and strength. They represent the first choice in material selection for strength and crash-relevant parts with challenging geometries. The intensive development of multiphase steels by ThyssenKrupp Steel has led to hot dip galvanizing concepts with an outstanding forming potential. Hot rolled, hot dip galvanized complex-phase steels are currently produced in addition to cold rolled dual phase (DP) and retained austenite (RA) or transformation induced plasticity (TRIP) steels. New continuously annealed grades of steel are being developed with tensile strength levels of up to 1000 MPa in combination with sufficient ductility for the high demands of structural automobile components. These steels make use of the classic advantages of microalloying as well as the principles of DP steels and RA / TRIP steels. Further improvement of properties will be reached by the new class of high manganese alloyed steels. (orig.)

  16. Mechanical shielded hot cell

    International Nuclear Information System (INIS)

    Higgy, H.R.; Abdel-Rassoul, A.A.

    1983-01-01

    A plan to erect a mechanical shielded hot cell in the process hall of the Radiochemical Laboratory at Inchas is described. The hot cell is designed for safe handling of spent fuel bundles, from the Inchas reactor, and for dismantling and cutting the fuel rods in preparation for subsequent treatment. The biological shielding allows for the safe handling of a total radioactivity level up to 10,000 MeV-Ci. The hot cell consists of an α-tight stainless-steel box, connected to a γ-shielded SAS, through an air-lock containing a movable carriage. The α-box is tightly connected with six dry-storage cavities for adequate storage of the spent fuel bundles. Both the α-box, with the dry-storage cavities, and the SAS are surrounded by 200-mm thick biological lead shielding. The α-box is equipped with two master-slave manipulators, a lead-glass window, a monorail crane and Padirac and Minirag systems. The SAS is equipped with a lead-glass window, tong manipulator, a shielded pit and a mechanism for the entry of the spent fuel bundle. The hot cell is served by adequate ventilation and monitoring systems. (author)

  17. Rolling at small scales

    DEFF Research Database (Denmark)

    Nielsen, Kim L.; Niordson, Christian F.; Hutchinson, John W.

    2016-01-01

    The rolling process is widely used in the metal forming industry and has been so for many years. However, the process has attracted renewed interest as it recently has been adapted to very small scales where conventional plasticity theory cannot accurately predict the material response. It is well....... Metals are known to be stronger when large strain gradients appear over a few microns; hence, the forces involved in the rolling process are expected to increase relatively at these smaller scales. In the present numerical analysis, a steady-state modeling technique that enables convergence without...

  18. METHOD OF ROLLING URANIUM

    Science.gov (United States)

    Smith, C.S.

    1959-08-01

    A method is described for rolling uranium metal at relatively low temperatures and under non-oxidizing conditions. The method involves the steps of heating the uranium to 200 deg C in an oil bath, withdrawing the uranium and permitting the oil to drain so that only a thin protective coating remains and rolling the oil coated uranium at a temperature of 200 deg C to give about a 15% reduction in thickness at each pass. The operation may be repeated to accomplish about a 90% reduction without edge cracking, checking or any appreciable increase in brittleness.

  19. Effect of skin pass rolling reduction rate on the texture evolution of a non-oriented electrical steel after inclined cold rolling

    Energy Technology Data Exchange (ETDEWEB)

    Mehdi, Mehdi [CanmetMATERIALS, Natural Resources Canada, Hamilton, ON L8P 0A5 (Canada); Department of Mechanical, Automotive, and Materials Engineering, University of Windsor, Windsor, ON N9B 3P4 (Canada); He, Youliang, E-mail: youliang.he@canada.ca [CanmetMATERIALS, Natural Resources Canada, Hamilton, ON L8P 0A5 (Canada); Hilinski, Erik J. [Tempel Steel Co., Chicago, IL 60640-1020 (United States); Edrisy, Afsaneh [Department of Mechanical, Automotive, and Materials Engineering, University of Windsor, Windsor, ON N9B 3P4 (Canada)

    2017-05-01

    In order to promote the magnetically favourable <001>//ND texture (θ-fibre) and minimize the unfavourable <111>//ND fibre (γ-fibre) in non-oriented electrical steel, an unconventional cold rolling scheme was employed in this study, in which the cold rolling was carried out at an angle (i.e. 30°, 45°, 60°, and 90°) to the hot rolling direction (HRD). After annealing, two steel sheets (i.e. those after cold rolling at 60° and 45° to the HRD) were found to have considerably different textures from other sheets, i.e. showing the strongest and the weakest θ-fibre textures, respectively. These two sheets were then subjected to skin pass rolling to various reduction rates from 5–20% to investigate the effect of rolling reduction on the evolution of texture. It was found that during skin pass rolling, the cube texture ({001}<100>) was gradually weakened and the rotated cube orientation ({001}<110>) was strengthened. With the increase of the reduction rate, the {112}<110> orientation on the α-fibre became a major component. Upon final annealing, the cube texture was slightly restored, but the volume fraction was considerably lower than that before skin pass rolling. - Highlights: • Inclined cold rolling optimizes the textures of non-oriented electrical steels. • A 60° angle to the hot rolling direction results in the largest improvement of the favorable texture. • Skin pass rolling weakens the cube texture and promotes the {112}<110> texture. • Final annealing restores some of the cube texture and strengthens the rotated cube texture. • Low Taylor factor of the cube orientation leads to its easy deformation in skin pass rolling.

  20. Influence of structure and properties of tubular billets of the 12 Kh 18N10T steel on deformability of tubes at cold-rolling mills

    International Nuclear Information System (INIS)

    Vil'yams, O.S.; Bol'shova, N.M.; Olejnik, O.V.; Velikotnaya, E.S.

    1979-01-01

    Metallographic analysis of the defects of the ''oblique cracks'' type on the surface of hot-rolled tubes of the 12Kh18N10T steel has been carried out. Recommended is the complex of mechanical properties and the structure factors (grain size) of conversion hot-rolled tubes, providing the combination of ductility and high rapture strength during rolling at pilger mills. At a grain size not coarser than number 5, a billet must have σsub(T) 5 >=40 %. Hot-rolled coarse-grained billet is not recommended for warm rolng because of high strain hardening

  1. To study the mechanical properties of unidirectionally and cross rolled Ni-Cu alloy produced in VIM

    International Nuclear Information System (INIS)

    Afzal, M.; Ajmal, M.; Butt, Z.T.

    2009-01-01

    Ni-Cu alloy was developed by melting in a vacuum induction furnace using pure elements i.e., Ni, Cu, Fe, Si, Mn and Cr. Four heats of approximately 4 kg each were prepared. All the heats have been casted in an ingot of 10 cm long and 5 cm in diameter in vacuum. These ingots were hot forged at a temperature of 900 deg. C to break down the cast dendritic structure. All forged plates were cut into two halve. One half was rolled in unidirectional while other was rolled in multiple directions (cross rolling). During rolling after every 25 % reduction, the cold rolled samples were annealed at a temperature of 900 deg. C for one hour. Each plate was cold rolled to a final thickness of 0.345 mm. Half of these rolled plate produced either by cross rolling or unidirectional rolling were annealed at 900 deg. C for 20 minutes. The mechanical properties of each rolled plate in cold reduction and in annealed were also measured. Unidirectional rolling and cross rolling has almost similar mechanical properties. The annealing of cross rolled and unidirectional rolling drastically reduced the yield strength. It was observed that the Ni-Cu alloy produced has slightly lower yield and ultimate tensile strength compared to the values reported in standards of Monel-400. However, it is within the acceptable range to be used for the various applications. (author)

  2. Comparative Study of Hardening Mechanisms During Aging of a 304 Stainless Steel Containing α'-Martensite

    Science.gov (United States)

    Jeong, S. W.; Kang, U. G.; Choi, J. Y.; Nam, W. J.

    2012-09-01

    Strain aging and hardening behaviors of a 304 stainless steel containing deformation-induced martensite were investigated by examining mechanical properties and microstructural evolution for different aging temperature and time. Introduced age hardening mechanisms of a cold rolled 304 stainless steel were the additional formation of α'-martensite, hardening of α'-martensite, and hardening of deformed austenite. The increased amount of α'-martensite at an aging temperature of 450 °C confirmed the additional formation of α'-martensite as a hardening mechanism in a cold rolled 304 stainless steel. Additionally, the increased hardness in both α'-martensite and austenite phases with aging temperature proved that hardening of both α'-martensite and austenite phases would be effective as hardening mechanisms in cold rolled and aged 304 stainless steels. The results suggested that among hardening mechanisms, hardening of an α'-martensite phase, including the diffusion of interstitial solute carbon atoms to dislocations and the precipitation of fine carbide particles would become a major hardening mechanism during aging of cold rolled 304 stainless steels.

  3. Stress corrosion inhibitors for type 18-10 stainless steels with low carbon content in hot and concentrated solutions of MgCl2. Study of some inorganic iodides

    International Nuclear Information System (INIS)

    Pinard, J.-L.

    1974-01-01

    Stress corrosion inhibitors for type Z2CN18-10 austenitic stainless steels with low carbon content in a solution of Cl 2 Mg at 105 deg C were investigated. It was established that iodides are the most adequate corrosion inhibitors because they react simultaneously upon the three main components of the alloy (Fe, Ni, Cr). A difference of behavior between I 2 Mg and the other iodides was observed (in electrochemistry and in simple stress corrosion experiments) and the influence of the metallic cation associated to I - was studied. The formation of the superficial film and the phenomena liable to occur at the interface film-corrosive solution were examined: film growth in MgCl 2 ; influence of certain substances added to the solution. A mechanism of inhibition by I - is suggested. It is similar to the mechanism proposed by BERGEN for the stress corrosion cracking by Cl - [fr

  4. Person og Rolle

    DEFF Research Database (Denmark)

    Szatkowski, Janek

    2011-01-01

    Distinktionen mellem person og rolle forslås som grundlag for et præcist og anlytisk anvendeligt begreb om performativitet. Begrebet tager sigte på at beskrive enkeltindividers og gruppers kommunikation med henblik på hvordan kommunikation etableres. Performativitet gør det muligt at iagttage den...

  5. Ship Roll Motion Control

    DEFF Research Database (Denmark)

    Perez, Tristan; Blanke, Mogens

    2010-01-01

    . This tutorial paper presents an account of the development of various ship roll motion control systems and the challenges associated with their design. The paper discusses how to assess performance, the applicability of dierent models, and control methods that have been applied in the past....

  6. Rolling Cylinder Phase 1

    DEFF Research Database (Denmark)

    Margheritini, Lucia; Taraborrelli, Valeria Taraborrelli

    Margheritini and Valeria Taraborrelli(valeria.taraborrelli@hotmail.it) with a total of 3 day visit from the developers. Laboratory tests in irregular waves will be performed by Lucia Margheritini. The report is aimed at the first stage testing of the Rolling Cylinder wave energy device. This phase includes...

  7. IMPROVEMENT PROCESS FOR ROLLING MILL THROUGH THE DMAIC SIX SIGMA APPROACH

    Directory of Open Access Journals (Sweden)

    Kunal Ganguly

    2012-09-01

    Full Text Available This project aims to address the problems that are facing a large aluminum company in a Developing Hot Rolling Mill Capabilities for Wider Widths Hard Alloys Rolling and b Eliminate down time due to strip /coil slippage during hard alloys 5xxx rolling at Hot Mill. The challenge for the company was to cater the fast changing export demand for Flat Rolled products with its existing resources. By applying Six Sigma principles, the team identified the current situation that the rolling mills operations were in. Si x Sigma DMAIC methodologies were use d in the project to determine the project's CTQ characteristics, defining the possible causes, Identifying the variation sources, establishing variable relationships and Implementing Control Plans. The project can be useful for any company that needs to fi nd the most cost efficient way to improve and utilize its resources.

  8. Effect of Reduction in Thickness and Rolling Conditions on Mechanical Properties and Microstructure of Rolled Mg-8Al-1Zn-1Ca Alloy

    Directory of Open Access Journals (Sweden)

    Yuta Fukuda

    2017-01-01

    Full Text Available A cast Mg-8Al-1Zn-1Ca magnesium alloy was multipass hot rolled at different sample and roll temperatures. The effect of the rolling conditions and reduction in thickness on the microstructure and mechanical properties was investigated. The optimal combination of the ultimate tensile strength, 351 MPa, yield strength, 304 MPa, and ductility, 12.2%, was obtained with the 3 mm thick Mg-8Al-1Zn-1Ca rolled sheet, which was produced with a roll temperature of 80°C and sample temperature of 430°C. This rolling process resulted in the formation of a bimodal structure in the α-Mg matrix, which consequently led to good ductility and high strength, exclusively by the hot rolling process. The 3 mm thick rolled sheet exhibited fine (mean grain size of 2.7 μm and coarse grain regions (mean grain size of 13.6 μm with area fractions of 29% and 71%, respectively. In summary, the balance between the strength and ductility was enhanced by the grain refinement of the α-Mg matrix and by controlling the frequency and orientation of the grains.

  9. Experimental determination of heat transfer coefficients in roll bite and air cooling for computer simulations of 1100 MPa carbon steel rolling

    Science.gov (United States)

    Leinonen, Olli; Ilmola, Joonas; Seppälä, Oskari; Pohjonen, Aarne; Paavola, Jussi; Koskenniska, Sami; Larkiola, Jari

    2018-05-01

    In modeling of hot rolling pass schedules the heat transfer phenomena have to be known. Radiation to ambient, between rolls and a steel slab as well as heat transfer in contacts must be considered to achieve accurate temperature distribution and thereby accurate material behavior in simulations. Additional heat is generated by friction between the slab and the work roll and by plastic deformation. These phenomena must be taken into account when the effective heat transfer coefficient is determined from experimental data. In this paper we determine the effective heat transfer coefficient at the contact interface and emissivity factor of slab surface for 1100MPa strength carbon steel for hot rolling simulations. Experimental pilot rolling test were carried out and slab temperatures gathered right below the interface and at the mid thickness of the slab. Emissivity factor tests were carried out in the same manner but without rolling. Experimental data is utilized to derive contact heat transfer coefficient at the interface and emissivity factor of slab surface. Pilot rolling test is reproduced in FE-analysis to further refine the heat transfer coefficient and emissivity factor. Material mechanical properties at rolling temperatures were determined by Gleeble™ thermo-mechanical simulator and IDS thermodynamic-kinetic-empirical software.

  10. Hot ductility of continuously cast structural steels

    International Nuclear Information System (INIS)

    Pytel, S.M.

    1995-01-01

    The objective of this investigation was to explain the hot ductility of the structural steels characterized by different amount of carbon and morphology of sulfides. Two different rolling processes were simulated under computer controlled, high temperature deformation MTS system. Results of this study show that morphology of sulfides as well as temperature and amount of deformation are responsible for level of hot ductility of the steel tested. (author)

  11. Ductility of high chromium stainless steels

    International Nuclear Information System (INIS)

    Peretyat'ko, V.N.; Kazantsev, A.A.

    1997-01-01

    Aimed to optimize the hot working conditions for high chromium stainless steels the experiments were carried in the temperature range of 800-1300 deg C using hot torsion tests and cylindrical specimens of ferritic and ferritic-martensitic steels 08Kh13, 12Kh13, 20Kh13, 30Kh13 and 40Kh13. Testing results showed that steel plasticity varies in a wide range depending on carbon content. Steels of lesser carbon concentration (08Kh13 and 12Kh13) exhibit a sharp increase in plasticity with a temperature rise, especially in the interval of 1200-1250 deg C. Steels 20Kh13 and 30Kh13 display insignificant plasticity increasing, whereas plastic properties of steel 40Kh13 increase noticeably in the range of 1000-1300 deg C. It is shown that optimal hot working conditions for specific steel must be selected with account of steel phase composition at high temperatures

  12. Damage on 316LN stainless steel transformed by powder metallurgy

    International Nuclear Information System (INIS)

    Couturier, R.; Burlet, H.

    1998-01-01

    This study deals with the 316 LN stainless steel elaboration by powder metallurgy. This method allows the realization of structures in austenitic steel less affected by the thermal aging than the cast austenitic-ferritic components. The components are performed by the method of HIP (Hot Isostatic Pressing). Mechanical tests are provided to control mechanical properties

  13. Effect of initial longitudinal stresses on the linearity of the shape rolled products after accelerated cooling

    International Nuclear Information System (INIS)

    Shetulov, D.I.

    1991-01-01

    Consideration is given to results of investigation into effect of initial longitudinal stresses on the linearity of the shaped rolled products after accelerated cooling. Particular attention is placed on the influence of an initial stresses state of material on qualiti of heat-treated rolled products. Effect of stresses state of worked material residual bending is studed by the use of computerized simulation.Theoretical analysis of stress-strain state of shape hot-rolled products during accelerated cooling after finishing stand of rolls is developed. A residual stress-strain state of material does not affected by rolling stresses when using a rautine cooling device with rigid centering of the product under rolling. It is expected that the effect of initial stresses could be significant in the absence of a limitator for bending deformation of shaped product longitudinal axis

  14. HOT 2012

    DEFF Research Database (Denmark)

    Lund, Henriette Romme

    Undersøgelse af, hvad der er hot - og hvad der burde være hot på læseområdet med 21 læsekyndige. Undersøgelsen er gennemført siden 2010. HOT-undersøgelsen er foretaget af Nationalt Videncenter for Læsning - Professionshøjskolerne i samarb. med Dansklærerforeningen......Undersøgelse af, hvad der er hot - og hvad der burde være hot på læseområdet med 21 læsekyndige. Undersøgelsen er gennemført siden 2010. HOT-undersøgelsen er foretaget af Nationalt Videncenter for Læsning - Professionshøjskolerne i samarb. med Dansklærerforeningen...

  15. The influence of cold work on the oxidation behaviour of stainless steel

    International Nuclear Information System (INIS)

    Langevoort, J.C.

    1985-01-01

    In this thesis the study of the interaction of oxygen gas with stainless steel surfaces is described. Thermogravimetry, microscopy and ellipsometry have been used to follow the oxidation in situ, while EDX, AES and XPS have been used to determine the oxide compositions. The aim of this thesis is to reveal the influence on the oxidation behaviour of stainless steel of i) cold work (rolling, drawing, milling, polishing and Ar ion bombardment) ii) the initially formed oxide and iii) the experimental conditions. Two types of stainless steels have been used (AISI 304 (a 18/8 Cr/Ni steel) and Incoloy 800 H (a 20/30 Cr/Ni steel)). (Auth.)

  16. Development of oxide dispersion strengthened 2205 duplex stainless steel composite

    Directory of Open Access Journals (Sweden)

    Oladayo OLANIRAN

    2015-05-01

    Full Text Available Composites of duplex stainless steel were produced by oxide dispersion strengthening with comparatively improved mechanical properties by hot press sintering of partially stabilized Zirconia (PSZ, 3% yttria, mole fraction dispersion in 2205 duplex stainless steels. Ceramic oxide was added as reinforcement, while chromium (Cr and Nickel (Ni were incorporated to maintain the austenitic/ferritic phase balance of the duplex stainless steel. The powders and sintered were characterized in detail using scanning electron microscopy (SEM and X-ray diffraction (XRD. The microstructural evolution and phase formation during oxide dispersion strengthening of duplex stainless steel composites were investigated. The influence of composition variation of the reinforcements on the microstructural and corrosion behaviour in simulated mine water of the composites were investigated. In this manuscript, it was established that composition has great influence on the structure/properties relationship of the composites developed.

  17. HOT 2014

    DEFF Research Database (Denmark)

    Lund, Henriette

    Undersøgelse af, hvad der er hot - og hvad der burde være hot på læseområdet med 21 læsekyndige. Undersøgelsen er gennemført siden 2010. HOT-undersøgelsen er foretaget af Nationalt Videncenter for Læsning - Professionshøjskolerne i samarb. med Dansklærerforeningen...

  18. NDE of explosion welded copper stainless steel first wall mock-up

    International Nuclear Information System (INIS)

    Taehtinen, S.; Kauppinen, P.; Jeskanen, H.; Lahdenperae, K.; Ehrnsten, U.

    1997-04-01

    The study showed that reflection type C-mode scanning acoustic microscope (C-SAM) and internal ultrasonic inspection (IRIS) equipment can be applied for ultrasonic examination of copper stainless steel compound structures of ITER first wall mock-ups. Explosive welding can be applied to manufacture fully bonded copper stainless steel compound plates. However, explosives can be applied only for mechanical tightening of stainless steel cooling tubes within copper plate. If metallurgical bonding between stainless steel tubes and copper plate is required Hot Isostatic Pressing (HIP) method can be applied. (orig.)

  19. HIP bonding for the different material between Niobium and Stainless steel

    International Nuclear Information System (INIS)

    Inoue, H.; Saito, K.; Abe, K.; Fujino, T.; Hitomi, N.; Kobayashi, Y.

    2000-01-01

    In the future advanced cryomodule for superconducting RF cavities, a helium vessel made from titanium or stainless steel has to be welded directly to the niobium cavity wall in order to be simple structure. For that, we need a transformer from niobium to titanium or stainless steel. Stainless steel will have many benefits if the reliable bonding to the niobium is developed. We have tested the niobium/stainless steel bonding by HIP (Hot Isostatic Pressing) with the heat shock between 1023K and 2K. The bonding interface was also observed by SEM. These test results will be presented. (author)

  20. Rolling bearing analysis

    CERN Document Server

    Harris, Tedric A

    2001-01-01

    One of the most well-known experts in the field brings cutting-edge research to practitioners in the new edition of this important reference. Covers the improved mathematical calculations for rolling bearing endurance developed by the American Society of Mechanical Engineers and the Society of Lubrication and Tribology Engineers. Updated with new material on Condition-Based Maintenance, new testing methods, and new bearing materials.

  1. Roll of honour

    Energy Technology Data Exchange (ETDEWEB)

    Moxon, Suzanne

    1999-07-01

    This article gives details of the design and construction of dams selected by members of the dam construction industry for praise as feats of construction. The dams covered in the roll of honour include the dam at the Guri hydroelectric power station in Venezuela on the Caroni river, the Contra dam on the Verzrasca river in Switzerland, and the double curvature arc Ertan dam on the Yalong river in China. (UK)

  2. Shear Roll Mill Reactivation

    Science.gov (United States)

    2012-09-13

    pneumatically operated paste dumper and belt conveyor system, the loss in weight feeder system, the hydraulically operated shear roll mill, the pellet...out feed belt conveyor , and the pack out system comprised of the metal detector, scale, and pack out empty and full drum roller conveyors . Page | 4...feed hopper and conveyor supplying the loss in weight feeder were turned on, and it was verified that these items functioned as designed . The

  3. HOT 2011

    DEFF Research Database (Denmark)

    Lund, Henriette Romme

    En undersøgelse af, hvad der er hot - og burde være hot på læseområdet. I undersøgelsen deltager 21 læsekyndige fra praksisfeltet, professionshøjskolerne og forskningsområdet.......En undersøgelse af, hvad der er hot - og burde være hot på læseområdet. I undersøgelsen deltager 21 læsekyndige fra praksisfeltet, professionshøjskolerne og forskningsområdet....

  4. Transformation kinetics of microalloyed steels after hot controlled ...

    African Journals Online (AJOL)

    Transformation kinetics of austenite into ferrite after controlled hot rolling has been investigated in three microalloyed steels (Nb, Nb-Ti and C-Mn-V) using hot interrupted compression tests on the Gleeble 1500 within the testing temperature range of 875°C-1100°C. Holding times were varied between 0.5 and 30s, strain ...

  5. Effect of rare earth element yttrium addition on microstructures and properties of a 21Cr-11Ni austenitic heat-resistant stainless steel

    International Nuclear Information System (INIS)

    Chen, Lei; Ma, Xiaocong; Wang, Longmei; Ye, Xiaoning

    2011-01-01

    Research highlights: → Applications of Y in 21Cr-11Ni austenitic heat-resistant stainless steel. → Sensible characteristics of microstructure and properties have been observed. → Y has been found be effective in improving hot ductility of 21Cr-11Ni steel. → Inhibitory effect of Y on S segregation to the grain boundary has been observed. -- Abstract: In this comparative study, the microstructure and the mechanical properties of a 21Cr-11Ni austenitic heat-resistant stainless steel with and without addition of rare earth (RE) element yttrium have been investigated. The results show that a number of fine spherical yttrium-rich oxide particles are not uniformly distributed in the matrix of steel with yttrium; instead, they are aligned along the rolling direction. The grains surrounding the alignment are nearly one order of magnitude smaller than those farther away from the alignment. The approximate calculation results indirectly show that the grain refinement may be mainly attributed to the stimulation for nucleation of recrystallization rather than to pinning by particles. Furthermore, the alignment has resulted in significant loss in transverse impact toughness and tensile elongation at room temperature. There is a trough in the hot ductility-temperature curve, which is located between 973 and 1173 K. The ductility trough of steel with yttrium becomes shallow within a certain temperature range, especially around 1073 K, indicating that improvement on hot ductility is achieved by yttrium addition. The results may be attributed to the increase of grain boundary cohesion indicated by the effective improvement on intergranular failure tendency, and the inhibitory effect of yttrium on sulfur segregation to grain boundaries is believed to be an important cause.

  6. Annealing of a ferritic stainless steel 409 stabilized with titanium and zirconium additions

    Directory of Open Access Journals (Sweden)

    Zambrano, P.

    2011-02-01

    Full Text Available A ferritic stainless steel 409 stabilized with titanium and zirconium was subject to thermomechanical processing. It was heated at 1210 °C for one hour, followed by a 75 % hot reduction in three passes, this rolling schedule ended at 980 °C. Samples were cooled to 600 °C by water spraying followed by air-cooling. The alloy was pickled, and was reduced 80 % by cold rolling. The alloy was annealed at different temperatures for 105 s. Additional annealing treatments were carried out at temperatures of 800, 850 and 900 °C for different times. Mechanical testing and texture were made to corroborate the degree of annealing and formability. Mechanical properties and Texture analyses showed that the alloy annealed at 850 °C for 14 min was both completely recrystallized and a very good formability.

    Un acero inoxidable ferrítico 409 estabilizado con titanio y zirconio fue sujeto a procesos termomecánicos. El acero fue calentado a 1210 ºC durante una hora, seguido por un laminado en caliente del 75 % en tres pases, el proceso terminó a los 980 ºC. Las muestras fueron enfriadas hasta 600 ºC por agua atomizada seguido de enfriamiento al aire. La aleación fue decapada y laminada en frío un 80 %. Posteriormente de desarrollaron tratamientos térmicos de recocido a diferentes temperaturas por un tiempo de 105 s. Adicionalmente se desarrollaron tratamientos de recocido a temperaturas de 800, 850 y 900 ºC a diferentes tiempos. Pruebas mecánicas y textura fueron realizadas para corroborar el grado de recocido y su formalidad. El análisis de las propiedades mecánicas y la Textura mostraron que la aleación recocida a 850 ºC por 14 min (840 s fue completamente recristalizada obteniendo la mejor formabilidad.

  7. Cause of Damage. Hot cracking; Schadensursache Heissrissigkeit

    Energy Technology Data Exchange (ETDEWEB)

    Wader, Therese [BENTELER Steel/Tube GmbH, Paderborn (Germany). Vorentwicklung Werkstoffe

    2016-10-15

    Under certain conditions, Nb-containing stainless steels are susceptible to hot cracking. Such conditions include low melting phases on the grain boundaries, a coarse-grained microstructure such as cast structures, microstructure orientations towards the main tensile direction and high processing temperatures. The case of damage was characterized using metallographic and microanalytical methods. In the laboratory, the critical temperature range for the formation of hot cracks could furthermore specifically be localized under mechanical stresses by means of a dilatometer aiming at clearly verifying the cause of the damage, namely ''hot cracks''.

  8. Effect of Low-Temperature Sensitization on Hydrogen Embrittlement of 301 Stainless Steel

    OpenAIRE

    Chieh Yu; Ren-Kae Shiue; Chun Chen; Leu-Wen Tsay

    2017-01-01

    The effect of metastable austenite on the hydrogen embrittlement (HE) of cold-rolled (30% reduction in thickness) 301 stainless steel (SS) was investigated. Cold-rolled (CR) specimens were hydrogen-charged in an autoclave at 300 or 450 °C under a pressure of 10 MPa for 160 h before tensile tests. Both ordinary and notched tensile tests were performed in air to measure the tensile properties of the non-charged and charged specimens. The results indicated that cold rolling caused the transforma...

  9. Effect of ultrafine grain on tensile behaviour and corrosion resistance of the duplex stainless steel.

    Science.gov (United States)

    Jinlong, Lv; Tongxiang, Liang; Chen, Wang; Limin, Dong

    2016-05-01

    The ultrafine grained 2205 duplex stainless steel was obtained by cold rolling and annealing. The tensile properties were investigated at room temperature. Comparing with coarse grained stainless steel, ultrafine grained sample showed higher strength and plasticity. In addition, grain size changed deformation orientation. The strain induced α'-martensite was observed in coarse grained 2205 duplex stainless steel with large strain. However, the grain refinement inhibited the transformation of α'-martensite;nevertheless, more deformation twins improved the strength and plasticity of ultrafine grained 2205 duplex stainless steel. In addition, the grain refinement improved corrosion resistance of the 2205 duplex stainless steel in sodium chloride solution. Copyright © 2016 Elsevier B.V. All rights reserved.

  10. Roll-to-Roll production of carbon nanotubes based supercapacitors

    Science.gov (United States)

    Zhu, Jingyi; Childress, Anthony; Karakaya, Mehmet; Roberts, Mark; Arcilla-Velez, Margarita; Podila, Ramakrishna; Rao, Apparao

    2014-03-01

    Carbon nanomaterials provide an excellent platform for electrochemical double layer capacitors (EDLCs). However, current industrial methods for producing carbon nanotubes are expensive and thereby increase the costs of energy storage to more than 10 Wh/kg. In this regard, we developed a facile roll-to-roll production technology for scalable manufacturing of multi-walled carbon nanotubes (MWNTs) with variable density on run-of-the-mill kitchen Al foils. Our method produces MWNTs with diameter (heights) between 50-100 nm (10-100 μm), and a specific capacitance as high as ~ 100 F/g in non-aqueous electrolytes. In this talk, the fundamental challenges involved in EDLC-suitable MWNT growth, roll-to-roll production, and device manufacturing will be discussed along with electrochemical characteristics of roll-to-roll MWNTs. Research supported by NSF CMMI Grant1246800.

  11. Effect of microstructure on the localized corrosion of Fe-Cr-Mn-N stainless steels

    International Nuclear Information System (INIS)

    Kim, Jae Young; Park, Yong Soo; Kim, Young Sik

    1998-01-01

    This paper dealt with the effect of microstructure on the localized corrosion of Fe-Cr-Mn-N stainless steels. The experimental alloys were made by vacuum induction melting and then hot rolled. The alloys were designed by controlling Cr eq /Ni eq ratio. Two alloys had austenitic phase and one alloy showed (austenite+ferrite) du-plex phase. High nitrogen addition in austenitic alloys stabilized the austenitic structure and then suppressed the formations of ferrite and α martensite, but martensite was formed in the case of large Cr eq /Ni eq ratio and low nitrogen addition. Pitting initiation site was grain boundary in austenitic alloys and was ferrite/austenite phase boundary in duplex alloy in the HCl solution. In sulfuric acids, austenitic alloys showed uniform corrosion, but ferrite phase was preferentially corroded in duplex alloy. The preferential dissolution seems to be related with the distribution of alloying elements between ferrite and austenite. Intergranular corrosion test showed that corrosion rate by immersion Huey test had a linear relation with degree of sensitization by EPR test

  12. Microstructure evolution during spray rolling and heat treatment of 2124 Al

    Energy Technology Data Exchange (ETDEWEB)

    McHugh, K.M. [Industrial Technology Department, Idaho National Laboratory, Idaho Falls, ID 83415-2050 (United States)], E-mail: kevin.mchugh@inl.gov; Lin, Y.; Zhou, Y.; Johnson, S.B.; Delplanque, J.-P.; Lavernia, E.J. [Department of Chemical Engineering and Materials Science, University of California, Davis, CA 95616 (United States)

    2008-03-25

    Spray rolling is a strip-casting technology that combines elements of spray forming and twin-roll casting. It consists of atomizing molten metal with a high velocity inert gas, quenching the resultant droplets in flight, and directing the spray between mill rolls. In-flight convection heat transfer from atomized droplets and conduction heat transfer at the rolls rapidly remove the metal's latent heat. Hot deformation of the semi-solid material in the rolls results in fully consolidated, rapidly-solidified strip. Spray rolling operates at a higher solidification rate than conventional twin-roll casting and is able to process a broader range of alloys at high production rates. A laboratory-scale strip caster was constructed and used to evaluate the interplay of processing parameters and strip quality for strips up to 200 mm wide and 1.6-6.4 mm thick. This paper examines microstructure evolution during spray rolling and explores how gas-to-metal mass flow ratio influences the microstructure and mechanical properties of spray-rolled 2124 Al. The influences of solution heat treatment and cold rolling on grain structure and constituent particle spheroidization are also examined.

  13. Advanced cold rolled steels for automotive applications

    Energy Technology Data Exchange (ETDEWEB)

    Hofmann, H. [ThyssenKrupp Steel AG, Eberhardstrasse 12, 44145 Dortmund (Germany); Mattissen, D.; Schaumann, T.W. [ThyssenKrupp Steel AG, Duisburg (Germany)

    2006-09-15

    Advanced multiphase steels offer a great potential for bodies-in-white through their combination of formability and achievable component strength levels. They are first choice for strength and crash-relevant parts of challenging geometry. The intensive development of high-strength multiphase steels by ThyssenKrupp has led to hot dip galvanizing concepts with an outstanding forming potential. Hot rolled, hot dip galvanized complex phase steels are currently produced in addition to cold rolled DP and RA steels. New continuously annealed grades with tensile strength levels of up to 1000 MPa in combination with sufficient ductility for applications mainly in the field of structural automobile elements make use of the classic advantages of microalloying as well as the principles of DP and TRIP steels. Further improvement of properties will be reached by the new class of high manganese alloyed steels. (Abstract Copyright [2006], Wiley Periodicals, Inc.) [German] Fortschrittliche Multiphasen-Staehle eroeffnen wegen der inzwischen erreichbaren Kombination aus Umformbarkeit und Bauteilfestigkeit ein enormes Potenzial fuer Rohkarosserien. Sie stellen eine erste Wahl dar, wenn es um Festigkeit und um Crashsicherheit geht und besondere Anforderungen an die Bauteilgeometrien gestellt werden. Bei ThyssenKrupp hat die Entwicklung hochfester Multiphasen-Staehle in Verbindung mit dem Feuerverzinken zur Realisierung von Blechhalbzeugen gefuehrt, die hervorragend formbar sind. Es werden heute feuerverzinkte Komplexphasenstaehle neben den bewaehrten kaltgewalzten Dualphasen(DP) - und Retained Austenit(RA)-Staehlen produziert. Die neuen kontinuierlich gegluehten Stahlvarianten mit Festigkeiten bis zu 1000 MPa in Kombination mit der bei Strukturbauteilen im Automobilbau geforderten Duktilitaet nutzen sowohl die klassischen Vorteile des Mikrolegierens aus und dazu die Prinzipien, die man bei DP- und TRIP-Staehlen anwendet. Eine weitere Verbesserung des Eigenschaftsprofils wird mit dem

  14. Strain direction dependency of martensitic transformation in austenitic stainless steels: The effect of gamma-texture

    NARCIS (Netherlands)

    Hilkhuijsen, P.; Geijselaers, Hubertus J.M.; Bor, Teunis Cornelis; Perdahcioglu, Emin Semih; van den Boogaard, Antonius H.; Akkerman, Remko

    2013-01-01

    Uniaxial tensile tests on both a non-textured and a highly textured, fully austenitic stainless steel were performed in both the rolling and the transverse directions. Both materials show mechanically induced phase transformation from the austenitic FCC to the martensitic BCC phase. Differences in

  15. Microscopic analysis of the influence of ratcheting on the evolution of dislocation structures observed in AISI 316L stainless steel during low cycle fatigue

    Energy Technology Data Exchange (ETDEWEB)

    Facheris, G., E-mail: giacomo.facheris@psi.ch [Laboratory for Nuclear Materials, Nuclear Energy and Safety Research Department, Paul Scherrer Institute, Villigen PSI (Switzerland); Pham, M.-S. [Department of Materials Science and Engineering, Carnegie Mellon University, 5000 Forbes Avenue, Pittsburgh, PA 15213 (United States); High Temperature Integrity Group, Mechanics for Modelling and Simulation, Swiss Federal Laboratories for Materials Science and Technology, EMPA, Dübendorf (Switzerland); Janssens, K.G.F., E-mail: koen.janssens@psi.ch [Laboratory for Nuclear Materials, Nuclear Energy and Safety Research Department, Paul Scherrer Institute, Villigen PSI (Switzerland); Holdsworth, S.R. [High Temperature Integrity Group, Mechanics for Modelling and Simulation, Swiss Federal Laboratories for Materials Science and Technology, EMPA, Dübendorf (Switzerland)

    2013-12-10

    When subjected to controlled cyclic deformation, the response of austenitic stainless steel typically involves primary hardening followed by softening, and eventually cyclic stabilization with or without secondary hardening. If a continuously drifting mean strain is superposed to an alternating strain path (i.e. strain controlled ratcheting), the response in terms of mean stress and strain amplitude is significantly different. A series of low cycle fatigue and ratcheting experiments are performed at room temperature on round specimens extracted from a batch of AISI 316L hot rolled plate. The experiments are interrupted at cycle numbers selected to correspond with the different strain controlled cycle response stages. The as-received material and the fatigued specimens are analyzed by means of transmission electron microscopy to characterize the microstructure and its evolution with cyclic loading. The low cycle fatigue experiments, performed to establish a reference point for the zero mean strain loading condition, are in line with observations reported for AISI 316L stainless steel by other authors. The continuously increasing mean strain is found to induce higher dislocation densities in the channels of the evolving microstructure, being responsible for the macroscopically observed additional hardening. The observed polarized dislocation walls at least partially accommodate the continuously drifting mean strain and play a role in the non-zero mean stress response.

  16. Rolls-Royce digital Rod Control System

    International Nuclear Information System (INIS)

    Pouillot, M.

    2010-01-01

    Full text of publication follows: Rolls-Royce has developed a new generation of Rod Control System, based on 40 years of experience. The fifth-generation Rod Control System (RCS) from Rolls-Royce offers a reliable, modular design with adaptability to your preferred platform, for modernization projects or new reactors. Flexible implementation provides the option for you to keep existing cabinets, which permits you to optimize installation approach. Main features for the power part: - Control Rod Drive Mechanism (CRDM) type: 3-coil. - Independent control of each sub-bank. - Each sub-bank is controlled by a cycler unit and 3 identical power racks, each including 4 identical power modules and a common power-supply module. - Coil-per-coil digital control: each power module embeds power-conversion, current-control, and current-monitoring functions for one coil. Control and monitoring are carried out by separate electronics in the module. Current is digitized and fully monitored by means of min-max templates. - A double-hold function is included: a power module assigned to a gripper will activate its coil if a fault risking to cause a reactor trip occurs. - Power modules are standardized, hot-pluggable and self-configured: a power module includes a set of parameters for each type of coil SG, MG, LC. The module recognizes the rack it is plugged in, and chooses automatically parameters to be used. Main benefits: - Reduced operational, maintenance, training, and inventory costs: standardization of power modules and integration of control and monitoring on the same PC-card lead to a drastic reduction of spare part types, and simplification of the system. - Easy maintenance: - Replacement of a power module solves nearly all failures due to current control or monitoring for a coil. It is done instantly thanks to hot-plug capability. - On the front plate of power-modules, LEDs provide useful information for diagnostic: current setpoint from cycler, output current bar

  17. The Effect of Rolling As-Cast and Homogenized U-10Mo Samples on the Microstructure Development and Recovery Curves

    Energy Technology Data Exchange (ETDEWEB)

    Joshi, Vineet V. [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Paxton, Dean M. [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Lavender, Curt A. [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Burkes, Douglas [Pacific Northwest National Lab. (PNNL), Richland, WA (United States)

    2016-07-30

    Over the past several years Pacific Northwest National Laboratory (PNNL) has been actively involved in supporting the U.S. Department of Energy National Nuclear Security Administration Office of Material Management and Minimization (formerly Global Threat Reduction Initiative). The U.S. High- Power Research Reactor (USHPRR) project is developing alternatives to existing highly enriched uranium alloy fuel to reduce the proliferation threat. One option for a high-density metal fuel is uranium alloyed with 10 wt% molybdenum (U-10Mo). Forming the U-10Mo fuel plates/foils via rolling is an effective technique and is actively being pursued as part of the baseline manufacturing process. The processing of these fuel plates requires systematic investigation/understanding of the pre- and post-rolling microstructure, end-state mechanical properties, residual stresses, and defects, their effect on the mill during processing, and eventually, their in-reactor performance. In the work documented herein, studies were conducted to determine the effect of cold and hot rolling the as-cast and homogenized U-10Mo on its microstructure and hardness. The samples were homogenized at 900°C for 48 h, then later annealed for several durations and temperatures to investigate the effect on the material’s microstructure and hardness. The rolling of the as-cast plate, both hot and cold, was observed to form a molybdenum-rich and -lean banded structure. The cold rolling was ineffective, and in some cases exacerbated the as-cast defects. The grains elongated along the rolling direction and formed a pancake shape, while the carbides fractured perpendicularly to the rolling direction and left porosity between fractured particles of UC. The subsequent annealing of these samples at sub-eutectoid temperatures led to rapid precipitation of the ' lamellar phase, mainly in the molybdenum-lean regions. Annealing the samples above the eutectoid temperature did not refine the grain size or the banded

  18. Diamond deposition on siliconized stainless steel

    International Nuclear Information System (INIS)

    Alvarez, F.; Reinoso, M.; Huck, H.; Rosenbusch, M.

    2010-01-01

    Silicon diffusion layers in AISI 304 and AISI 316 type stainless steels were investigated as an alternative to surface barrier coatings for diamond film growth. Uniform 2 μm thick silicon rich interlayers were obtained by coating the surface of the steels with silicon and performing diffusion treatments at 800 deg. C. Adherent diamond films with low sp 2 carbon content were deposited on the diffused silicon layers by a modified hot filament assisted chemical vapor deposition (HFCVD) method. Characterization of as-siliconized layers and diamond coatings was performed by energy dispersive X-ray analysis, scanning electron microscopy, X-ray diffraction and Raman spectroscopy.

  19. Roll back malaria update.

    Science.gov (United States)

    1999-10-01

    This article presents the activities under WHO's Roll Back Malaria (RBM) program in Asia, particularly in Nepal, Indonesia, India, Bangladesh, Sri Lanka and the Philippines. In India, the RBM program will start in 5 districts with a major malaria problem. A national committee has been formed by researchers, which will be able to provide operational and strategic support and research expertise in relation to malaria. In Bangladesh, the RBM program was initiated in the sparsely populated hill tract areas of Banderban and Chittagong where access to health care is very poor. At the district level, effective partnerships with private practitioners, politicians, community leaders, school teachers, the press and district Ministry of Health officials are operating to plan for rolling back malaria. In Myanmar, Cambodia, Lao People's Democratic Republic, Yunnan province of China, Vietnam, and Thailand, the focus of the RBM program was to move health care closer to the malaria-infected communities. WHO¿s Global Health Leadership Fellowship Programme, supported by the UN Foundation and Rockefeller Foundation, enables potential leaders to experience the work of UN agencies and contribute to the work of the organization for 2 years. Three out of four persons appointed to the RBM program received prestigious awards: Dr. Paola Marchesini of Brazil; Dr. Tieman Diarra of Mali; and Dr. Bob Taylor of the UK.

  20. Thickness profile measuring device for rolling metal bands or sheets

    International Nuclear Information System (INIS)

    Campas, J.J.; Terreaux, S.

    1995-01-01

    Previous radiometric thickness gages were affected by insufficient water proofing and limited cooling performances for the detection subsystem (in general specially designed photodiodes). This resulted in poor reliability and life expectancy, in particular when heavy humidity and constant radiative heat are present as for hot rolling in the metal industry. This new gage design brings enhanced performances for these two factors. (D.L.). 4 refs., 3 figs

  1. Roll-to-roll manufacturing of amorphous silicon alloy solar cells with in situ cell performance diagnostics

    International Nuclear Information System (INIS)

    Izu, M.; Ellison, T.

    2003-01-01

    In order to meet the price target necessary for widespread use of solar cell products, Energy Conversion Devices, Inc., ECD, has developed and commercialized a continuous roll-to-roll manufacturing technology for the production of a-Si alloy solar cells. Since the early 1980s, we have advanced this technology from a small-scale pilot machine to a large-scale production machine. In 2002, ECD commissioned a 30 MW per year machine for United Solar Systems Corp. in Auburn Hills, Michigan. The RF PECVD a-Si alloy solar cell processor, designed and built by ECD, deposits triple-junction solar cell materials consisting of nine layers of a-Si alloys in a continuous roll-to-roll operation simultaneously on six coils of 130 μm thick, 0.36 m wide, 2.6 km long stainless-steel substrate at 1 cm/s. In order to minimize production losses due to undetected deviations of production conditions and carry on a continuous program of device optimization, we have developed and are incorporating in situ cell performance diagnostic systems. (author)

  2. Roll-to-roll UV imprint lithography for flexible electronics

    NARCIS (Netherlands)

    Maury, P.; Turkenburg, D.H.; Stroeks, N.; Giesen, P.; Barbu, I.; Meinders, E.R.; Bremen, A. van; Iosad, N.; Werf, R. van der; Onvlee, H.

    2011-01-01

    We propose a roll-to-roll UV imprint lithography tool as a way to pattern flexible PET foil with µm-resolution. As a way to overcome dimensional instability of the foil and its effect on overlay, a self-align approach was investigated, that permits to make several layers in a single lithography

  3. RELATIONSHIP BETWEEN ROLLING AND SLIP RESISTANCE IN ROLLING BEARINGS

    Directory of Open Access Journals (Sweden)

    L. M. Bondarenko

    2016-06-01

    Full Text Available Purpose. About one of the causes of slip rolling is known from the second half of the 19th century, it was believed that the slip resistance appears at the place of contact due to different speeds on the arc of contact. Only in the mid-20th century it was proved that this resistance is negligible in rolling resistance. However (for some unknown reason it is ignored the fact that in practice in rolling bearings may rotate both the inner ring with a stationary outer one, and vice versa almost in equal relations. It is not taken into account the fact that the ball or roller in the rolling bearings runs the different distance along the roller path of the outer and inner bearing cages in one revolution. This fact is not taken into account in determining the calculated values for the friction coefficient of a rolling bearing reduced to the shaft. Therefore, the aim of this work is to determine the influence of path length on the track riding the outer and inner race of the bearing on the determination of the calculated value of the coefficient of friction of rolling bearings is given to the shaft. Methodology. The solution technique is based on the theory of plane motion of a rigid body, the theory of Hertzian contact deformation and the analytical dependencies for determination of coefficient of rolling friction. Findings. The obtained dependences on determination of rolling resistance of the balls or rollers along the bearing tracks of inner and outer bearing cages as well as path difference metering of the rolling on them allows to analytically obtain the rolling resistance and slipping for any size of bearings and different devices of bearing units. It is also possible at the design stage of rolling nodes to handle not only the design but also the content of the node. Originality. Using the analytical dependences for determination of the rolling resistance of bodies at point and line contacts, and also account for the difference in the path of the

  4. HOT 2010

    DEFF Research Database (Denmark)

    Lund, Henriette Romme

    En undersøgelse af, hvad der er hot - og burde være hot på læseområdet. I undersøgelsen deltager en række læsekyndige fra praksisfeltet, professionshøjskolerne og forskningsområdet. Undersøgelsen er gentaget hvert år siden 2010.......En undersøgelse af, hvad der er hot - og burde være hot på læseområdet. I undersøgelsen deltager en række læsekyndige fra praksisfeltet, professionshøjskolerne og forskningsområdet. Undersøgelsen er gentaget hvert år siden 2010....

  5. HOT 2013

    DEFF Research Database (Denmark)

    Lund, Henriette Romme

    En undersøgelse af, hvad der er hot - og burde være hot på læseområdet. I undersøgelsen deltager en række læsekyndige fra praksisfeltet, professionshøjskolerne og forskningsområdet. Undersøgelsen er gentaget hvert år siden 2010.......En undersøgelse af, hvad der er hot - og burde være hot på læseområdet. I undersøgelsen deltager en række læsekyndige fra praksisfeltet, professionshøjskolerne og forskningsområdet. Undersøgelsen er gentaget hvert år siden 2010....

  6. Effect of weld metal properties on fatigue crack growth behaviour of gas tungsten arc welded AISI 409M grade ferritic stainless steel joints

    International Nuclear Information System (INIS)

    Shanmugam, K.; Lakshminarayanan, A.K.; Balasubramanian, V.

    2009-01-01

    The effect of filler metals such as austenitic stainless steel, ferritic stainless steel and duplex stainless steel on fatigue crack growth behaviour of the gas tungsten arc welded ferritic stainless steel joints was investigated. Rolled plates of 4 mm thickness were used as the base material for preparing single 'V' butt welded joints. Centre cracked tensile (CCT) specimens were prepared to evaluate fatigue crack growth behaviour. Servo hydraulic controlled fatigue testing machine was used to evaluate the fatigue crack growth behaviour of the welded joints. From this investigation, it was found that the joints fabricated by duplex stainless steel filler metal showed superior fatigue crack growth resistance compared to the joints fabricated by austenitic and ferritic stainless steel filler metals. Higher yield strength, hardness and relatively higher toughness may be the reasons for superior fatigue performance of the joints fabricated by duplex stainless steel filler metal.

  7. Characterization of beryllium foil produced by hot rolling

    International Nuclear Information System (INIS)

    Wittenauer, J.; Nieh, T.G.; Waychunas, G.

    1992-01-01

    Beryllium foil is important for a number of aerospace applications including honeycomb structures and metal-matrix composites. In this study, a method of producing beryllium foil directly from powder or flake is demonstrated. A variety of foils were produced in the thickness range 90-300 μm, free from defects such as pinholes and excessive surface roughness, and exhibiting sufficient formability for honeycomb manufacture. Foil produced directly from powder or flake exhibits crystallographic texture, microstructure, and formability equivalent to foil produced from more massive precursors. (Author)

  8. Controlled rolling process for dual phase steels and application to rod, wire, sheet and other shapes

    Science.gov (United States)

    Thomas, Gareth; Ahn, Jae-Hwan; Kim, Nack-Joon

    1986-01-01

    An improved, energy efficient, hot rolling method for direct production of cold formable dual-phase steel is provided. The steel is heated to completely austenitize it and then continuously hot rolled and cooled down into the ferrite-austenite two phase region to a temperature which is just below the effective Ar.sub.3 temperature. The hot rolled steel is then rapidly quenched to provide an alloy containing strong, tough lath martensite (fibers) in a ductile soft ferrite matrix. The method is particularly useful for providing rods in which form the alloy is capable of being drawn into high strength wire or the like in a cold drawing operation without any intermediate annealing or patenting, and has excellent strength, ductility and fatigue characteristics.

  9. LEDs are on a roll

    NARCIS (Netherlands)

    Blom, P.W.M.; Mol, A.M.B. van

    2011-01-01

    Light-emitting diodes are more efficient than conventional lighting, but high production costs limit their uptake. Organic versions that can be produced using a cheap newspaper-style 'roll-to-roll' printing process are likely to revolutionize our lighting and signage, say Paul Blom and Ton van Mol.

  10. Anisotropic constant-roll inflation

    Energy Technology Data Exchange (ETDEWEB)

    Ito, Asuka; Soda, Jiro [Kobe University, Department of Physics, Kobe (Japan)

    2018-01-15

    We study constant-roll inflation in the presence of a gauge field coupled to an inflaton. By imposing the constant anisotropy condition, we find new exact anisotropic constant-roll inflationary solutions which include anisotropic power-law inflation as a special case. We also numerically show that the new anisotropic solutions are attractors in the phase space. (orig.)

  11. Rolling up a Graphene Sheet

    NARCIS (Netherlands)

    Calvaresi, Matteo; Quintana, Mildred; Rudolf, Petra; Zerbetto, Francesco; Prato, Maurizio

    2013-01-01

    Carbon Nanotubes, CNTs, have been described as rolled-up graphene layers. Matching this concept to experiments has been a great experimental challenge for it requires a method to exfoliate graphite, generate ordered and stable dangling carbon bonds, and roll up the layer without affecting the

  12. Rudder roll stabilization for ships

    NARCIS (Netherlands)

    van Amerongen, J.; van der Klugt, P.G.M.; van Nauta lemke, H.R.

    1990-01-01

    This paper describes the design of an autopilot for rudder roll stabilization for ships. This autopilot uses the rudder not only for course keeping but also for reduction of the roll. The system has a series of properties which make the controller design far from straightforward: the process has

  13. Computational design of rolling bearings

    CERN Document Server

    Nguyen-Schäfer, Hung

    2016-01-01

    This book comprehensively presents the computational design of rolling bearings dealing with many interdisciplinary difficult working fields. They encompass elastohydrodynamics (EHD), Hertzian contact theory, oil-film thickness in elastohydrodynamic lubrication (EHL), bearing dynamics, tribology of surface textures, fatigue failure mechanisms, fatigue lifetimes of rolling bearings and lubricating greases, Weibull distribution, rotor balancing, and airborne noises (NVH) in the rolling bearings. Furthermore, the readers are provided with hands-on essential formulas based on the up-to-date DIN ISO norms and helpful examples for computational design of rolling bearings. The topics are intended for undergraduate and graduate students in mechanical and material engineering, research scientists, and practicing engineers who want to understand the interactions between these working fields and to know how to design the rolling bearings for automotive industry and many other industries.

  14. Chromium-Makes stainless steel stainless

    Science.gov (United States)

    Kropschot, S.J.; Doebrich, Jeff

    2010-01-01

    Chromium, a steely-gray, lustrous, hard metal that takes a high polish and has a high melting point, is a silvery white, hard, and bright metal plating on steel and other material. Commonly known as chrome, it is one of the most important and indispensable industrial metals because of its hardness and resistance to corrosion. But it is used for more than the production of stainless steel and nonferrous alloys; it is also used to create pigments and chemicals used to process leather.

  15. Microstructure based procedure for process parameter control in rolling of aluminum thin foils

    Science.gov (United States)

    Johannes, Kronsteiner; Kabliman, Evgeniya; Klimek, Philipp-Christoph

    2018-05-01

    In present work, a microstructure based procedure is used for a numerical prediction of strength properties for Al-Mg-Sc thin foils during a hot rolling process. For this purpose, the following techniques were developed and implemented. At first, a toolkit for a numerical analysis of experimental stress-strain curves obtained during a hot compression testing by a deformation dilatometer was developed. The implemented techniques allow for the correction of a temperature increase in samples due to adiabatic heating and for the determination of a yield strength needed for the separation of the elastic and plastic deformation regimes during numerical simulation of multi-pass hot rolling. At the next step, an asymmetric Hot Rolling Simulator (adjustable table inlet/outlet height as well as separate roll infeed) was developed in order to match the exact processing conditions of a semi-industrial rolling procedure. At each element of a finite element mesh the total strength is calculated by in-house Flow Stress Model based on evolution of mean dislocation density. The strength values obtained by numerical modelling were found in a reasonable agreement with results of tensile tests for thin Al-Mg-Sc foils. Thus, the proposed simulation procedure might allow to optimize the processing parameters with respect to the microstructure development.

  16. Effect of rolling temperature on 12Kh18N10T steel tube hardening

    International Nuclear Information System (INIS)

    Yushkevich, P.M.; Stepanovich, V.E.; Manankova, L.V.; Usenko, V.N.; Semenov, I.A.

    1984-01-01

    Mechanical properties and substructure of tubes at the constant reduction degree k(the ratio of deformation over wall thickness to deformation over diameter), depending on strain degree during cold and hot tube rolling, have been studied. The investigations are carried out using hot-rolled tubes with the dimensions 88x8 mm of 12Kh1hN10T steel. With the decrease of strain over the wall of the tube, produced of 12Kh18N10T steel as to strain over diameter the values of yield strength and ultimate strength increase with simultaneous decrease in ductility during warm rolling and yield strength and ultimate strength decrease with the increase in ductility-during cold rolling. During warm rolling of the tubes at 250 deg C the hardening of 12Kh18N10T steel is higher, than at the rolling temperature 150 deg C. The optimum temperature range of warm rolling is 120-150 deg C. Grain orientation in the metal of the tubes and degree of texture perfection increase with the temperature increase of the tube warm drolling as compared with col rolli

  17. Deformation in Micro Roll Forming of Bipolar Plate

    Science.gov (United States)

    Zhang, P.; Pereira, M.; Rolfe, B.; Daniel, W.; Weiss, M.

    2017-09-01

    Micro roll forming is a new processing technology to produce bipolar plates for Proton Exchange Membrane Fuel Cells (PEMFC) from thin stainless steel foil. To gain a better understanding of the deformation of the material in this process, numerical studies are necessary before experimental implementation. In general, solid elements with several layers through the material thickness are required to analyse material thinning in processes where the deformation mode is that of bending combined with tension, but this results in high computational costs. This pure solid element approach is especially time-consuming when analysing roll forming processes which generally involves feeding a long strip through a number of successive roll stands. In an attempt to develop a more efficient modelling approach without sacrificing accuracy, two solutions are numerically analysed with ABAQUS/Explicit in this paper. In the first, a small patch of solid elements over the strip width and in the centre of the “pre-cut” sheet is coupled with shell elements while in the second approach pure shell elements are used to discretize the full sheet. In the first approach, the shell element enables accounting for the effect of material being held in the roll stands on material flow while solid elements can be applied to analyse material thinning in a small discrete area of the sheet. Experimental micro roll forming trials are performed to prove that the coupling of solid and shell elements can give acceptable model accuracy while using shell elements alone is shown to result in major deviations between numerical and experimental results.

  18. Plasticity of low carbon stainless steels

    International Nuclear Information System (INIS)

    Bulat, S.I.; Fel'dgandler, Eh.G.; Kareva, E.N.

    1975-01-01

    In the temperature range 800-1200 0 C and with strain rates of from 10 -3 to 3 s -1 , austenitic (000Kh18N12) and austenitic-ferrite (000Kh26N6) very low carbon stainless steels containing 0.02-0.03% C exhibit no higher resilience than corresponding ordinary steels containing 0.10-0.12% C. However, the plasticity of such steels (particularly two-phase steels) at 900-1100 0 C is appreciably inferior owing to the development of intergranular brittle fracture. Pressure treatment preceded by partial cooling of the surface to 850 0 C yields rolled and forged products with acceptable indices but is inconvenient technically. At the Zlatoustovsk and Ashin metallurgical plants successful tests have been performed involving the forging and rolling of such steels heated to 1280-1300 0 C without partial cooling; it was necessary to improve the killing conditions, correct the chemical composition (increasing the proportion of ferrite) and take measures against heat loss. (author)

  19. Effect of nitrogen and boron on weldability of austenitic stainless steels

    International Nuclear Information System (INIS)

    Bhaduri, A.K.; Albert, S.K.; Srinivasan, G.; Divya, M.; Das, C.R.

    2012-01-01

    Hot cracking is a major problem in the welding of austenitic stainless steels, particularly the fully austenitic grades. A group of alloys of enhanced-nitrogen 316LN austenitic stainless steel is being developed for structural components of the Indian Fast Reactor programme. Studying the hot cracking behaviour of this nitrogen-enhanced austenitic stainless steel is an important consideration during welding, as this material solidifies without any residual delta ferrite in the primary austenitic mode. Nitrogen has potent effects on the solidification microstructure, and hence has a strong influence on the hot cracking behaviour. Different heats of this material were investigated, which included fully austenitic stainless steels containing 0.070.22 wt% nitrogen. Also, borated austenitic stainless steels, such as type 304B4, have been widely used in the nuclear applications primarily due to its higher neutron absorption efficiency. Weldability is a major concern for this alloy due to the formation of low melting eutectic phase that is enriched with iron, chromium, molybdenum and boron. Fully austenitic stainless steels are prone to hot cracking during welding in the absence of a small amount of delta ferrite, especially for compositions rich in elements like boron that increases the tendency to form low melting eutectics. Detailed weldability investigations were carried out on a grade 304B4 stainless steel containing 1.3 wt% boron. Among the many approaches that have been used to determine the hot cracking susceptibility of different alloys, Variable-Restraint (Varestraint) weld test and Hot Ductility (Gleeble) tests are commonly used to evaluate the weldability of austenitic alloys. Hence, investigations on these materials consisted of detailed metallurgical characterization and weldability studies that included studying both the fusion zone and liquation cracking susceptibility, using Varestraint tests at 0.254.0%, strain levels and Gleeble (thermo

  20. Stress and accidental defect detection on rolling mill rolls

    International Nuclear Information System (INIS)

    Auzas, J.-D.

    1999-01-01

    During the rolling mill process, rolls are submitted to high pressures that can lead to local decohesion or metallurgical changes. Both these cracks or softened areas must be detected as soon as they appear because of the risk of spalling, marks on the product, and mill wreck. These defects can be detected using the eddy current method, and particularly sensors specially developed for micro-defects detection. These sensors must be adapted to the environment of a roll grinding machine on which they must be installed. Users' schedule of conditions also require them to be attached to a wide range of eddy current generator and automatic computerized interpretation. Mill requirements for new high tech roll grades and quality lead to continuous development and improvement of the tools that will provide immediate 'go - no go' information. This paper is an update of these developments. (author)

  1. Roll bonding of strained aluminium

    DEFF Research Database (Denmark)

    Staun, Jakob M.

    2003-01-01

    This report investigates roll bonding of pre-strained (å ~ 4) aluminium sheets to produce high strain material from high purity aluminium (99.996%) and commercial pure aluminium (99.6%). The degree of bonding is investigated by optical microscopy and ultrasonic scanning. Under the right...... of the cross rolled volume fraction is found. To further asses this effect, and the anisotropy, it is necessary to acquire knowledge about both texture and microstructure, e.g. by TEM. Roll bonding of pre-strained aluminium is found to be a possible alternative to ARB in the quest for ultra-fine grained...

  2. Effect of reversion annealing on the formation of nano/ultrafine grained structure in 201 austenitic stainless steel

    Energy Technology Data Exchange (ETDEWEB)

    Moallemi, Mohammad; Najafizadeh, Abbas; Kermanpur, Ahmad [Department of Materials Engineering, Isfahan University of Technology, Isfahan 84156-83111 (Iran, Islamic Republic of); Rezaee, Ahad, E-mail: a.rezaee@ma.iut.ac.ir [Department of Materials Engineering, Isfahan University of Technology, Isfahan 84156-83111 (Iran, Islamic Republic of)

    2011-12-15

    Highlights: Black-Right-Pointing-Pointer The secondary increase in the martensite content after reversion annealing. Black-Right-Pointing-Pointer Formation of thermally induced martensite due to carbide precipitation. Black-Right-Pointing-Pointer The smallest average grain size of 70 nm is achieved by annealing at 850 Degree-Sign C for 15 s. Black-Right-Pointing-Pointer A fully austenitic structure with grain size of 100 nm and 1370 MPa yield strength. - Abstract: The formation of nano/ultrafine grain structure in a 201 austenitic stainless steel was investigated by the martensite thermomechanical treatment. Cast ingots were first homogenized, then hot-forged and solution-annealed to reduce the initial grain size. Cold rolling was then conducted down to 90% reduction in thickness, followed by reversion annealing at a temperature in the range of 1023-1173 K for 15-1800 s. The effect of reversion parameters on grain refinement was investigated. The resulting microstructures were characterized by a scanning electron microscopy equipped with X-ray energy-dispersive spectrometer, an X-ray diffractometer and a Feritscope. The hardness was measured by the Vickers method. The results show that a nano/ultrafine-grained structure formed in the initial stages of the reversion, but significant grain growth took place during the entire course of reversion. Initially lowered, the volume fraction of martensite increased again during the reversion treatment due to carbide precipitation. A fully austenitic nano grained 201 stainless steel with the average grain size of 100 nm was produced, possessing a yield strength of about 1370 MPa.

  3. Manufacturing Demonstration Facility: Roll-to-Roll Processing

    Energy Technology Data Exchange (ETDEWEB)

    Datskos, Panos G [ORNL; Joshi, Pooran C [ORNL; List III, Frederick Alyious [ORNL; Duty, Chad E [ORNL; Armstrong, Beth L [ORNL; Ivanov, Ilia N [ORNL; Jacobs, Christopher B [ORNL; Graham, David E [ORNL; Moon, Ji Won [ORNL

    2015-08-01

    This Manufacturing Demonstration Facility (MDF)e roll-to-roll processing effort described in this report provided an excellent opportunity to investigate a number of advanced manufacturing approaches to achieve a path for low cost devices and sensors. Critical to this effort is the ability to deposit thin films at low temperatures using nanomaterials derived from nanofermentation. The overarching goal of this project was to develop roll-to-roll manufacturing processes of thin film deposition on low-cost flexible substrates for electronics and sensor applications. This project utilized ORNL s unique Pulse Thermal Processing (PTP) technologies coupled with non-vacuum low temperature deposition techniques, ORNL s clean room facility, slot dye coating, drop casting, spin coating, screen printing and several other equipment including a Dimatix ink jet printer and a large-scale Kyocera ink jet printer. The roll-to-roll processing project had three main tasks: 1) develop and demonstrate zinc-Zn based opto-electronic sensors using low cost nanoparticulate structures manufactured in a related MDF Project using nanofermentation techniques, 2) evaluate the use of silver based conductive inks developed by project partner NovaCentrix for electronic device fabrication, and 3) demonstrate a suite of low cost printed sensors developed using non-vacuum deposition techniques which involved the integration of metal and semiconductor layers to establish a diverse sensor platform technology.

  4. Systematics of constant roll inflation

    Science.gov (United States)

    Anguelova, Lilia; Suranyi, Peter; Wijewardhana, L. C. R.

    2018-02-01

    We study constant roll inflation systematically. This is a regime, in which the slow roll approximation can be violated. It has long been thought that this approximation is necessary for agreement with observations. However, recently it was understood that there can be inflationary models with a constant, and not necessarily small, rate of roll that are both stable and compatible with the observational constraint ns ≈ 1. We investigate systematically the condition for such a constant-roll regime. In the process, we find a whole new class of inflationary models, in addition to the known solutions. We show that the new models are stable under scalar perturbations. Finally, we find a part of their parameter space, in which they produce a nearly scale-invariant scalar power spectrum, as needed for observational viability.

  5. Finite element modelling of process-integrated powder coating by radial axial rolling of rings

    International Nuclear Information System (INIS)

    Frischkorn, J.; Kebriaei, R.; Reese, S.; Moll, H.; Theisen, W.; Husmann, T.; Meier, H.

    2011-01-01

    The process-integrated powder coating by radial axial rolling of rings represents a new hybrid production technique applied in the manufacturing of large ring-shaped work pieces with functional layers. It is thought to break some limitations that come along with the hot isostatic pressing (HIP) which is used nowadays to apply the powdery layer material onto the rolled substrate ring. Within the new process the compaction of the layer material is integrated into the ring rolling and HIP becomes dispensable. Following this approach the rolling of such compound rings brings up some new challenges. The volume of a solid ring stays nearly constant during the rolling. This behaviour can be exploited to determine the infeed of the rollers needed to reach the desired ring shape. Since volume consistency cannot be guaranteed for the rolling of a compound ring the choice of appropriate infeed of the rollers is still an open question. This paper deals with the finite element (FE) simulation of this new process. First, the material model that is used to describe the compaction of the layer material is shortly reviewed. The main focus of the paper is then put on a parameterized FE ring rolling model that incorporates a control system in order to stabilize the process. Also the differences in the behaviour during the rolling stage between a compound and a solid ring will be discussed by means of simulation results.

  6. Grease lubrication in rolling bearings

    CERN Document Server

    Lugt, Piet M

    2012-01-01

    The definitive book on the science of grease lubrication for roller and needle bearings in industrial and vehicle engineering. Grease Lubrication in Rolling Bearings provides an overview of the existing knowledge on the various aspects of grease lubrication (including lubrication systems) and the state of the art models that exist today. The book reviews the physical and chemical aspects of grease lubrication, primarily directed towards lubrication of rolling bearings. The first part of the book covers grease composition, properties and rheology, including thermal

  7. Rolling Resistance Measurement and Model Development

    DEFF Research Database (Denmark)

    Andersen, Lasse Grinderslev; Larsen, Jesper; Fraser, Elsje Sophia

    2015-01-01

    There is an increased focus worldwide on understanding and modeling rolling resistance because reducing the rolling resistance by just a few percent will lead to substantial energy savings. This paper reviews the state of the art of rolling resistance research, focusing on measuring techniques, s......, surface and texture modeling, contact models, tire models, and macro-modeling of rolling resistance...

  8. Development of CSS-42L{trademark}, a high performance carburizing stainless steel for high temperature aerospace applications

    Energy Technology Data Exchange (ETDEWEB)

    Burrier, H.I.; Milam, L. [Timken Co., Canton, OH (United States); Tomasello, C.M.; Balliett, S.A.; Maloney, J.L. [Latrobe Steel Co., Latrobe, PA (United States); Ogden, W.P. [MPB Corp., Lebanon, NH (United States)

    1998-12-31

    Today`s aerospace engineering challenges demand materials which can operate under conditions of temperature extremes, high loads and harsh, corrosive environments. This paper presents a technical overview of the on-going development of CSS-42L (US Patent No. 5,424,028). This alloy is a case-carburizable, stainless steel alloy suitable for use in applications up to 427 C, particularly suited to high performance rolling element bearings, gears, shafts and fasteners. The nominal chemistry of CSS-42L includes: (by weight) 0.12% carbon, 14.0% chromium, 0.60% vanadium, 2.0% nickel, 4.75% molybdenum and 12.5% cobalt. Careful balancing of these components combined with VIM-VAR melting produces an alloy that can be carburized and heat treated to achieve a high surface hardness (>58 HRC at 1mm (0.040 in) depth) with excellent corrosion resistance. The hot hardness of the carburized case is equal to or better than all competitive grades, exceeding 60 HRC at 427 C. The fracture toughness and impact resistance of the heat treated core material have likewise been evaluated in detail and found to be better than M50-NiL steel. The corrosion resistance has been shown to be equivalent to that of 440C steel in tests performed to date.

  9. First results of laser welding of neutron irradiated stainless steel

    International Nuclear Information System (INIS)

    Osch, E.V. van; Hulst, D.S. d'; Laan, J.G. van der.

    1994-10-01

    First results of experimental investigations on the laser reweldability of neutron irradiated material are reported. These experiments include the manufacture of 'heterogeneous' joints, which means joining of irradiated stainless steel of type AISI 316L-SPH to 'fresh' unirradiated material. The newly developed laser welding facility in the ECN Hot Cell Laboratory and experimental procedures are described. Visual inspections of welded joints are reported as well as results of electron microscopy and preliminary metallographic examinations. (orig.)

  10. The role of martensitic transformation on bimodal grain structure in ultrafine grained AISI 304L stainless steel

    International Nuclear Information System (INIS)

    Sabooni, S.; Karimzadeh, F.; Enayati, M.H.; Ngan, A.H.W.

    2015-01-01

    In the present study, metastable AISI 304L austenitic stainless steel samples were subjected to different cold rolling reductions from 70% to 93%, followed by annealing at 700 °C for 300 min to form ultrafine grained (UFG) austenite with different grain structures. Transmission electron microscopy (TEM) and nanoindentation were used to characterize the martensitic transformation, in order to relate it to the bimodal distribution of the austenite grain size after subsequent annealing. The results showed that the martensite morphology changed from lath type in the 60% rolled sample to a mixture of lath and dislocation-cell types in the higher rolling reductions. Calculation of the Gibbs free energy change during the reversion treatment showed that the reversion mechanism is shear controlled at the annealing temperature and so the morphology of the reverted austenite is completely dependent on the morphology of the deformation induced martensite. It was found that the austenite had a bimodal grain size distribution in the 80% rolled and annealed state and this is related to the existence of different types of martensite. Increasing the rolling reduction to 93% followed by annealing caused changing of the grain structure to a monomodal like structure, which was mostly covered with small grains of around 300 nm. The existence of bimodal austenite grain size in the 80% rolled and annealed 304L stainless steel led to the improvement of ductility while maintaining a high tensile strength in comparison with the 93% rolled and annealed sample

  11. Void swelling behaviour of austenitic stainless steel during electron irradiation

    International Nuclear Information System (INIS)

    Sheng Zhongqi; Xiao Hong; Peng Feng; Ti Zhongxin

    1994-04-01

    The irradiation swelling behaviour of 00Cr17Ni14Mo2 austenitic stainless steel (AISI 316L) was investigated by means of high voltage electron microscope. Results showed that in solution annealed condition almost no swelling incubation period existed, and the swelling shifted from the transition period to the steady-state one when the displacement damage was around 40 dpa. In cold rolled condition there was evidently incubation period, and when the displacement damage was up to 84 dpa the swelling still remained in the transition period. The average size and density of voids in both conditions were measured, and the factors, which influenced the void swelling, were discussed. (3 figs.)

  12. Apparatus and process for ultrasonic seam welding stainless steel foils

    Science.gov (United States)

    Leigh, Richard W.

    1992-01-01

    An ultrasonic seam welding apparatus having a head which is rotated to form contact, preferably rolling contact, between a metallurgically inert coated surface of the head and an outside foil of a plurality of layered foils or work materials. The head is vibrated at an ultrasonic frequency, preferably along a longitudinal axis of the head. The head is constructed to transmit vibration through a contacting surface of the head into each of the layered foils. The contacting surface of the head is preferably coated with aluminum oxide to prevent the head from becoming welded to layered stainless steel foils.

  13. Numerical and Experimental Approach to Investigate Plane-view Shape and Crop Loss in Multistage Plate Rolling

    International Nuclear Information System (INIS)

    Byon, Sang Min

    2013-01-01

    A finite element based approach that can be used to investigate the plane-view shape and crop loss of a material during plate rolling is presented. We employed a three-dimensional finite element model to continuously simulate the shape change of the head and tail of a plate as the number of rolling passes increases. The main feature of the proposed model lies in the fact that the multistage rolling can be simulated without a break because the rolling direction of the material is reversibly controlled as the roll gap sequentially decreases. The material constants required in the finite element analysis were experimentally obtained by hot tensile tests. We also performed a pilot hot plate rolling test to verify the usefulness of the proposed finite element model. Results reveal that the computed plane-view shapes as well as crop losses by the proposed finite element model were in good agreement with the measured ones. The crop losses predicted by the proposed model were within 5% of those measured from the pilot hot plate rolling test

  14. HOT 2017

    DEFF Research Database (Denmark)

    Hannibal, Sara Stefansen

    HOT er en kvalitativ undersøgelse, der hvert år diskuterer og undersøger en lille udvalgt skare af danskkyndige fagpersoners bud på, hvad de er optagede af på literacyområdet her og nu – altså hvilke emner, de vil vurdere som aktuelle at forholde sig til i deres nuværende praksis.......HOT er en kvalitativ undersøgelse, der hvert år diskuterer og undersøger en lille udvalgt skare af danskkyndige fagpersoners bud på, hvad de er optagede af på literacyområdet her og nu – altså hvilke emner, de vil vurdere som aktuelle at forholde sig til i deres nuværende praksis....

  15. Experimental analysis of two-layered dissimilar metals by roll bonding

    Science.gov (United States)

    Zhao, Guanghui; Li, Yugui; Li, Juan; Huang, Qingxue; Ma, Lifeng

    2018-02-01

    Rolling reduction and base layers thickness have important implications for rolling compounding. A two-layered 304 stainless steel/Q345R low alloyed steel was roll bonded. The roll bonding was performed at the three thickness reductions of 25%, 40% and 55% with base layers of various thicknesses (Q345R). The microstructures of the composite were investigated by the ultra-deep microscope (OM) and scanning electron microscope (SEM) and Transmission electron microscope (TEM). Simultaneously, the mechanical properties of the composite were experimentally measured and the tensile fracture surfaces were observed by SEM. The interfaces were successfully bonded without any cracking or voids, which indicated a good fabrication of the 304/Q345R composite. The rolling reduction rate and thinning increase of the substrate contributed to the bonding effects appearance of the roll bonded sheet. The Cr and Ni enriched diffusion layer was formed by the interface elements diffusion. The Cr and Ni diffusion led to the formation of ˜10 μm wide Cr and Ni layers on the carbon steel side.

  16. Effects of cold working on the pitting corrosion behavior s of AISI 304 stainless steels

    Energy Technology Data Exchange (ETDEWEB)

    Jung, Kee Min; Kim, Jong Soo; Kim, Young Jun; Kwon, Houk Sang [KAIST, Daejon (Korea, Republic of)

    2015-12-15

    These microstructural changes by cold working can lead improvement of mechanical properties, however from a corrosion resistant point of view, the effects of cold working on the corrosion resistance of stainless steel have been argued. Several studies has been focused on the influence of cold working on the localized corrosion resistance of stainless steels. However, the opinions about the role of cold working on the localized corrosion resistance are highly in consistence. Some studies report that the pitting potential of austenitic stainless steels decreased with cold working level, on the other hands, other studies claimed that the pitting resistance was increased by cold working. Therefore it is necessary to verify how cold working affects pitting corrosion behavior of austenitic stainless steels. In the present work, the influence of cold working on the localized corrosion of AISI 304stainless steel in the neutral chloride solution was studied based on point defect model (PDM). The fraction of deformation-induced martensite was linearly increased with cold rolling level. Through cold rolling, the pitting potential was decreased, the metastable pitting event density was significantly increased and the repassivation potential was decreased. The overall localized corrosion resistance was decreased with cold working, however cold working level increased from 30 % to 50 %, localized corrosion resistance was recovered. The accumulated cation vacancy generates a void at metal/film interface, therefore film breakdown accelerates for cold worked alloys.

  17. Effects of cold working on the pitting corrosion behavior s of AISI 304 stainless steels

    International Nuclear Information System (INIS)

    Jung, Kee Min; Kim, Jong Soo; Kim, Young Jun; Kwon, Houk Sang

    2015-01-01

    These microstructural changes by cold working can lead improvement of mechanical properties, however from a corrosion resistant point of view, the effects of cold working on the corrosion resistance of stainless steel have been argued. Several studies has been focused on the influence of cold working on the localized corrosion resistance of stainless steels. However, the opinions about the role of cold working on the localized corrosion resistance are highly in consistence. Some studies report that the pitting potential of austenitic stainless steels decreased with cold working level, on the other hands, other studies claimed that the pitting resistance was increased by cold working. Therefore it is necessary to verify how cold working affects pitting corrosion behavior of austenitic stainless steels. In the present work, the influence of cold working on the localized corrosion of AISI 304stainless steel in the neutral chloride solution was studied based on point defect model (PDM). The fraction of deformation-induced martensite was linearly increased with cold rolling level. Through cold rolling, the pitting potential was decreased, the metastable pitting event density was significantly increased and the repassivation potential was decreased. The overall localized corrosion resistance was decreased with cold working, however cold working level increased from 30 % to 50 %, localized corrosion resistance was recovered. The accumulated cation vacancy generates a void at metal/film interface, therefore film breakdown accelerates for cold worked alloys

  18. Advances in stainless steels

    International Nuclear Information System (INIS)

    Baldev Raj; Jayakumar, T.; Saibaba, Saroja; Sivaprasad, P.V.; Shankar, P.

    2010-01-01

    This book covers a broad spectrum of topics spanning the entire life cycle of stainless steel-from alloy design and characterization to engineering design, fabrication, mechanical properties, corrosion, quality assurance of components, in-service performance assessment, life prediction and finally failure analysis of materials and components. The contents provide useful feedback for further developments aimed at effective utilization of this class of materials. The book comprises articles that bring out contemporary developments in stainless steels and is thematically classified into the following sections. 1. Component design, modelling and structural integrity, 2. Manufacturing technology, 3. Property evaluation, 4. Alloy development and applications, 5. NDE methods, 6. Corrosion and surface modification. The book commences with articles on component design and structural integrity, thus opening up the areas of challenge for researchers and academia. The articles in the book relevant to INIS are indexed separately

  19. Hot particles

    International Nuclear Information System (INIS)

    Merwin, S.E.; Moeller, M.P.

    1989-01-01

    Nuclear Regulatory Commission (NRC) licensees are required to assess the dose to skin from a hot particle contamination event at a depth of skin of7mg/cm 2 over an area of 1 cm 2 and compare the value to the current dose limit for the skin. Although the resulting number is interesting from a comparative standpoint and can be used to predict local skin reactions, comparison of the number to existing limits based on uniform exposures is inappropriate. Most incidents that can be classified as overexposures based on this interpretation of dose actually have no effect on the health of the worker. As a result, resources are expended to reduce the likelihood that an overexposure event will occur when they could be directed toward eliminating the cause of the problem or enhancing existing programs such as contamination control. Furthermore, from a risk standpoint, this practice is not ALARA because some workers receive whole body doses in order to minimize the occurrence of hot particle skin contaminations. In this paper the authors suggest an alternative approach to controlling hot particle exposures

  20. Multilayer Steel Materials Deformation Resistance and Roll Force Measurement

    Directory of Open Access Journals (Sweden)

    A. G. Kolesnikov

    2014-01-01

    Full Text Available To create new types of cars, raise their reliability, gain operational life, and decrease in metal consumption of products it is necessary to improve mechanical, physical, and also special properties of the constructional materials applied in mechanical engineering. Presently, there are intensive researches and developments under way to create materials with ultrafine-grained structure (the sizes of grains in their crystal lattice make less than 1 micron in one of the measurements.BMSTU developed a manufacturing technology of multilayer steel sheets with steady ultrafine-grained structure based on the multiple hot rolling of billet as a composition consisting of the alternating metal sheets. A principled condition for implementation of such technology is existence of different crystallographic modifications in the adjoining sheets of the composition at specified temperature of rolling.Power parameters of rolling are important technical characteristics of the process. Usually, to determine a deformation resistance value when rolling the diverse multilayer materials, is used the actual resistance value averaging in relation to the components of the composition. The aim of this work is a comparative analysis of known calculated dependences with experimental data when rolling the 100-layer samples. Objects of research were the 100-layer compositions based on the alternating layers of steel 08H18N10 and U8.Experimental samples represented the vacuumized capsules with height, width, and length of 53 mm x 53 mm x 200 mm, respectively, in which there were the 100-layer packs from sheets, each of 0.5 mm, based on the composition of steels (U8+08H18N10. Rolling was made on the double-high mill with rolls of 160 mm in diameter during 19 passes to the thickness of 7 mm with the speed of 0,1 m/s. Relative sinking in each pass was accepted to be equal 10±2,5%. Rolling forces were measured by the strain-gauging method using the measuring cells, located under

  1. Hydrogen effects in stainless steel

    International Nuclear Information System (INIS)

    Caskey, G.R. Jr.

    1983-01-01

    The effects of hydrogen on stainless steels have been reviewed and are summarized in this paper. Discussion covers hydrogen solution and transport in stainless steels as well as the effects of hydrogen on deformation and fracture under various loading conditions. Damage is caused also by helium that arises from decay of the hydrogen isotope tritium. Austenitic, ferritic, martensite, and precipitation-hardenable stainless steels are included in the discussion. 200 references

  2. The effect of roll gap geometry on microstructure in cold-rolled aluminum

    DEFF Research Database (Denmark)

    Mishin, Oleg; Bay, B.; Winther, G.

    2004-01-01

    Microstructure and texture are analyzed through the thickness of two aluminum plates cold-rolled 40% with different roll gap geometries. It is found that both texture and microstructure are strongly affected by the rolling geometry. After rolling with intermediate-size draughts a rolling-type tex......Microstructure and texture are analyzed through the thickness of two aluminum plates cold-rolled 40% with different roll gap geometries. It is found that both texture and microstructure are strongly affected by the rolling geometry. After rolling with intermediate-size draughts a rolling...... layers. In these layers, extended planar dislocation boundaries are frequently found to be inclined closely to the rolling direction. The subsurface and central layers of this plate exhibit microstructures similar to those in the plate rolled with intermediate draughts. It is suggested...

  3. Combined process "helical rolling-pressing" and its effect on the microstructure of ferrous and non-ferrous materials

    Science.gov (United States)

    Naizabekov, Abdrakhman; Lezhnev, Sergey; Arbuz, Alexandr; Panin, Evgeniy

    2018-02-01

    Ultrafine-grained materials are one of the most promising structural and functional materials. However, the known methods of obtaining them are not enough powerful and technologically advanced for profitable industrial applications. Development of the combined process "helical rolling-pressing" is an attempt to bring technology to produce ultrafine-grained materials to the industry. The combination of intense processing of the surface by helical rolling and the entire cross section of workpiece in equal channel angular matrix, with intense deformation by torsion between rolls and matrix will increase the degree of deformation per pass and allows to mutually compensate disadvantages of these methods in the case of their separate use. This paper describes the development of a laboratory stand and study of influence of combined process "helical rolling-pressing"on the microstructure of tool steel, technical copper and high alloy stainless high-temperature steel.

  4. Semi-solid twin-roll casting process of magnesium alloy sheets

    International Nuclear Information System (INIS)

    Watari, H.; Davey, K.; Rasgado, M.T. Alonso; Haga, T.; Koga, N.

    2004-01-01

    An experimental approach has been performed to ascertain the effectiveness of semi-solid strip casting using a horizontal twin roll caster. The demand for light-weight products with high strength has grown recently due to the rapid development of automobile and aircraft technology. One key to such development has been utilization of magnesium alloys, which can potentially reduce the total product weight. However, the problems of utilizing magnesium alloys are still mainly related to high manufacturing cost. One of the solutions to this problem is to develop magnesium casting-rolling technology in order to produce magnesium sheet products at competitive cost for commercial applications. In this experiment, magnesium alloy AZ31B was used to ascertain the effectiveness of semi-solid roll strip casting for producing magnesium alloy sheets. The temperature of the molten magnesium, and the roll speeds of the upper and lower rolls, (which could be changed independently), were varied to find an appropriate manufacturing condition. Rolling and heat treatment conditions were changed to examine which condition would be appropriate for producing wrought magnesium alloys with good formability. Microscopic observation of the crystals of the manufactured wrought magnesium alloys was performed. It has been found that a limiting drawing ratio of 2.7 was possible in a warm deep drawing test of the cast magnesium alloy sheets after being hot rolled

  5. Robust Rudder Roll Damping Control

    DEFF Research Database (Denmark)

    Yang, C.

    The results of a systematic research to solve a specific ship motion control problem, simultaneous roll damping and course keeping using the rudder are presented in this thesis. The fundamental knowledge a priori is that rudder roll damping is highly sensitive to the model uncertainty, therefore H-infinity...... theory is used to deal with the problem. The necessary mathematical tools and the H-Infinity theory as the basis of controller design are presented in Chapter 2 and 3. The mu synthesis and the D-K iteration are introduced in Chapter 3. The ship dynamics and modeling technology are discussed in Chapter 4...

  6. Development of austenitic stainless steel PC wire and strand

    International Nuclear Information System (INIS)

    Tsubono, Hideyoshi; Kawabata, Yoshinori; Yamaoka, Yukio

    1986-01-01

    The effects of aging and stress-aging (called hot stretching) at the temperatures from 120 deg C to 700 deg C on the mechanical properties, relaxation values, Charpy impact values and SCC behavior of hard drawn SUS 304, SUS 316 stainless steel wires have been studied. The main results obtained are as follows: (1) Yield and tensile strength of the wires increased by aging at 230 deg C and 530 deg C as well as by hot stretching. The strengthening after 230 deg C treatment may be due to the strain aging by C and the increase of strength after 530 deg C treatment results from precipitation of Cr 23 C 6 on dislocations. (2) Stress relaxation values up to 250 deg C are low due to precipitation of Cr 23 C 6 . Almost no difference can be observed between aging and hot stretching. (3) Impact value at -196 deg C of SUS 304 stainless steel wire which was measured with 1 mm V-notched specimen was found to be about the same as that of 9 % Ni steel. (4) It is considered that in comparison with high carbon PC wire SUS 304 stainless steel showing high tensile strength is insensitive to SCC in NH 4 SCN and NH 4 NO 3 solutions. (5) In practice, tension member of the austenitic stainless steel wire and strand which were produced by aging at 500 deg C may be useful in special industrial field, for example, (a) SUS 304, in cryogenic field use (b) SUS 316, in intensive magnetic field use as a nonmagnetic material. (author)

  7. Stainless steels low temperature nitriding

    International Nuclear Information System (INIS)

    Roux, T.; Darbeida, A.; Von Stebut, J.; Michel, H.; Lebrun, J.P.; Hertz, D.

    1995-01-01

    Nitrogen ions implantation of 316L stainless steel leads to monophasic diffusion layers, which are constituted of a solid solution (γ N ) fcc, metastable, nitrogen sur-saturated, and without order. This article shows that for 316L stainless steels,these layers improve the tribological properties without degradation of the corrosion resistance. (A.B.). 13 refs. 6 figs

  8. The effect of roll with passive segment on the planetary rolling process

    Directory of Open Access Journals (Sweden)

    Qing-Ling Zeng

    2015-03-01

    Full Text Available In three-roll planetary rolling process, there is secondary torsion phenomenon that may lead to rolling instability. This article proposed a new idea to alleviate the secondary torsion phenomenon by dividing the secondary torsion segment out of the roll as an independent and passive one. To study the performance of the roll with passive segment, the three-dimensional finite element models of planetary rolling process using actual roll or new roll with passive segment involving elastic–plastic and thermal–mechanical coupling were established by the software ABAQUS/Explicit, and a series of analysis had been done successfully. The rolling temperature and rolling force of planetary mill were in good agreement with the measured results, which indicated that the finite element method would supply important reference merit for three-dimensional thermo-mechanical simulation of the three-roll planetary rolling process. Comparing the simulation results of the two models, the results indicated that the change in the roll structure had just a little influence on the metal deformation, temperature, and rolling force, but it lessened the secondary torsion deformation effectively and improved the outside roundness of the rolled tube slightly. The research provided a new idea for the roll design of three-roll planetary mill (PSW.

  9. Influence of Atomic Oxygen Exposure on Friction Behavior of 321 Stainless Steel

    Science.gov (United States)

    Liu, Y.; Yang, J.; Ye, Z.; Dong, S.; Zhang, L.; Zhang, Z.

    Atomic oxygen (AO) exposure testing has been conducted on a 321 stainless steel rolled 1 mm thick sheet to simulate the effect of AO environment on steel in low Earth orbit (LEO). An atomic oxygen exposure facility was employed to carry out AO experiments with the fluence up to ~1021 atom/cm2. The AO exposed specimens were evaluated in air at room temperature using a nanoindenter and a tribological system. The exposed surfaces were analyzed usign XPS technique.

  10. Strength of interface in stainless clad steels

    International Nuclear Information System (INIS)

    Ohji, Kiyotsugu; Nakai, Yoshikazu; Hashimoto, Shinji

    1990-01-01

    Mechanical tests were conducted on four kinds of stainless clad steels to establish test methods for determining crack growth resistance of bimaterial interface. In tension tests, smooth specimens and shallow notched specimens were employed. In these tests, all of the smooth specimens were broken in carbon steel, not along the bimaterial interface. On the other hand, most of the shallow notched specimens were broken along the interface, when the notch root was located at the interface. Therefore, the shallow notched specimens were suitable for estimating the strength of the interface in tension tests. For fracture toughness tests, chevron notched specimens are recommended, since pre-fatigue cracks were susceptible to initiate and grow in carbon steel for conventional straight notched specimens. In fatigue crack growth tests, side-grooved and non-side-grooved specimens were employed. Although the side-grooves were machined so that the minimum cross-sectional plane of the specimens coincided with the plane of the bimaterial interface, cracks did not always propagate along the interface. Therefore, the side-grooves were judged not to be effective for cracks to propagate along the bimaterial interface. Both in fracture toughness tests and fatigue tests, the crack growth resistance along bimaterial interface was much lower than the resistance of matrix steels. In all of the mechanical tests conducted, the crack growth resistance along the interface was higher for the normalized material than that for the as-rolled material. The nickel foil inserted between carbon steel and stainless steel improved the growth resistance of interfacial cracks. (author)

  11. The Influence of Vanadium Microalloying on the Production of Thin Slab Casting and Direct Rolled Steel Strip

    Science.gov (United States)

    Li, Yu; Milbourn, David

    Vanadium microalloying is highly effective in high strength strip steels produced by thin slab casting and direct rolled process. Because of the high solubility of V(C,N) in austenite, vanadium is likely to remain in solution during casting, equalisation and rolling. Vanadium microalloyed steels have better hot ductility and are less prone to transverse cracking than niobium containing steels. Despite a coarse as-cast austenite grain size before rolling, significant grain refinement can be achieved in vanadium microalloyed steels by repeated recrystallization during rolling, resulting in a fine uniform ferrite microstructure in final strip. Almost all vanadium present in microalloyed steels is available to precipitate in ferrite as very fine particles, contributing to precipitation strengthening. Vanadium microalloyed steels show less sensitivity to rolling process variables and exhibit excellent combination of strength and toughness.

  12. Microstructural characterization of Cu82.3Al8.3Mn9.4 shape memory alloy after rolling

    Directory of Open Access Journals (Sweden)

    Mirko Gojić

    2017-09-01

    Full Text Available In this paper, the microstructure of Cu82.3Al8.3Mn9.4 (in wt. % shape memory alloy after hot and cold rolling was investigated. The Cu82.3Al8.3Mn9.4 alloy was produced by a vertical continuous casting method in the form a cylinder rod of 8 mm in diameter. After the casting, hot and cold rolling was performed. By hot rolling a strip with a thickness of 1.75 mm was obtained, while by cold rolling a strip with a thickness of 1.02 mm was produced. After the rolling process, heat treatment was performed. Heat treatment was carried out by solution annealing at 900 °C held for 30 minutes and water quenched immediately after heating. The microstructure characterization of the investigated alloy was carried out by optical microscopy (OM, scanning electron microscopy (SEM equipped with a device for energy dispersive spectroscopy (EDS. Phase transformation temperatures and fusion enthalpies were determined by differential scanning calorimetry (DSC method. The homogenous martensite microstructure was confirmed by OM and SEM micrographs after casting. During rolling the two-phase microstructure occurred. Results of DSC analysis showed martensite start (Ms, martensite finish (Mf, austenite start (As and austenite finish (Af temperatures.

  13. Rolling motion in moving droplets

    Indian Academy of Sciences (India)

    motions. The two limits of a thin sheet-like drop in sliding motion on a surface, and a spherical drop in roll, have been extensively .... rigid body rotation. The solid body rotation makes sense in the context of small Reynolds. (Re) number flows ...

  14. Micro-Abrasion Wear Resistance of Borided 316L Stainless Steel and AISI 1018 Steel

    Science.gov (United States)

    Reséndiz-Calderon, C. D.; Rodríguez-Castro, G. A.; Meneses-Amador, A.; Campos-Silva, I. E.; Andraca-Adame, J.; Palomar-Pardavé, M. E.; Gallardo-Hernández, E. A.

    2017-11-01

    The 316L stainless steel has high corrosion resistance but low tribological performance. In different industrial sectors (biomedical, chemical, petrochemical, and nuclear engineering), improvement upon wear resistance of 316L stainless steel components using accessible and inexpensive methods is critical. The AISI 1018 steel is widely used in industry, but its tribological performance is not the best among steels. Therefore, in this study the behavior of the borided 316L stainless steel and 1018 steel is evaluated under micro-abrasion wear. The boriding was carried out at 1223 K over 6 h of exposure time, resulting in a biphase layer composed of FeB/Fe2B phases. In order to evaluate Fe2B phase with no influence from FeB phase, AISI 1018 steel samples were borided at 1273 K for over 20 min and then diffusion annealed at 1273 K over 2 h to obtain a Fe2B mono-phase layer. Micro-abrasion wear resistance was evaluated by a commercial micro-abrasion testing rig using a mix of F-1200 SiC particles with deionized water as abrasive slurry. The obtained wear rates for FeB and Fe2B phases and for the 316L stainless steel were compared. Wear resistance of 316L stainless steel increases after boriding. The wear mechanisms for both phases and for the stainless steel were identified. Also, transient conditions for rolling and grooving abrasion were determined for the FeB and Fe2B phases.

  15. Texture and magnetic properties of non-oriented electrical steels processed by an unconventional cold rolling scheme

    Energy Technology Data Exchange (ETDEWEB)

    He, Youliang, E-mail: youliang.he@canada.ca [CanmetMATERIALS, Natural Resources Canada, Hamilton, ON (Canada); Hilinski, Erik J. [Formerly Research and Technology Centre, United States Steel Corporation, Munhall, PA (United States); Now Tempel Steel Co., Chicago, IL (United States)

    2016-05-01

    Two non-oriented electrical steels containing 0.9 wt% and 2.8 wt% of silicon were processed using an unconventional cold rolling scheme, i.e. the cold rolling direction (CRD) was intentionally inclined at an angle to the hot rolling direction (HRD) so that the initial texture before cold rolling and the rotation paths of crystals during cold deformation were both altered as compared to conventional cold rolling along the original HRD. The cold-rolled steel strips were then annealed, skin-pass rolled and final annealed. The texture and microstructure of the materials were characterized by X-ray diffraction (XRD), electron backscatter diffraction (EBSD) and optical microscopy, and considerable differences in average grain size and texture were observed at different inclination angles. The magnetic properties of the steel strips were measured at 400 Hz and 1.0 T/1.5 T using a specially designed Epstein frame, and apparent differences were also noticed at various angles. The magnetic quality of texture was evaluated using different texture factors/parameters and compared to the measured magnetic properties. Although apparent improvement on the magnetic quality of texture can be noted by inclining the CRD to HRD, the trend does not match the measured magnetic properties at 400 Hz, which may have been affected by other parameters in addition to crystallographic texture. - Highlights: • The cold rolling direction is inclined an angle to the hot rolling direction. • The deformation and annealing textures are both changed by the inclined rolling. • Magnetic quality of texture is improved at specific inclination angles. • Low silicon steel is more sensitive in texture change than high silicon steel. • High frequency core loss does not follow the computed magnetic quality of texture.

  16. Maintenance Appointments in Railway Rolling Stock Rescheduling

    NARCIS (Netherlands)

    J.C. Wagenaar (Joris); L.G. Kroon (Leo); M.E. Schmidt (Marie)

    2016-01-01

    textabstractThis paper addresses the Rolling Stock Rescheduling Problem (RSRP), while taking maintenance appointments into account. After a disruption, the rolling stock of the disrupted passenger trains has to be rescheduled in order to restore a feasible rolling stock circulation. Usually, a

  17. Rolling block mazes are PSPACE-complete

    NARCIS (Netherlands)

    Buchin, K.; Buchin, M.

    2012-01-01

    In a rolling block maze, one or more blocks lie on a rectangular board with square cells. In most mazes, the blocks have size k × m × n where k, m, n are integers that determine the size of the block in terms of units of the size of the board cells. The task of a rolling block maze is to roll a

  18. Efficient Circulation of Railway Rolling Stock

    NARCIS (Netherlands)

    Alfieri, A.; Groot, R.; Kroon, L.G.; Schrijver, A.

    2006-01-01

    Railway rolling stock (locomotives, carriages, and train units) is one of the most significant cost sources for operatorsof passenger trains, both public and private. Rolling stock costsare due to material acquisition, power supply, and material maintenance. The efficient circulation of rolling

  19. Prediction of δ-ferrite distribution in continuously cast type 304 stainless steel slabs by diffusion transformation analysis

    International Nuclear Information System (INIS)

    Kim, J. Joon; Kim, Sun K.; Kim, Jong W.

    1998-01-01

    Retained δ-ferrite in 304 stainless steel is known to prevent hot cracking during continuous casting. Excess content of retained δ-ferrite lowers the hot workability. So it is necessary to control the amount of retained δ-ferrite in stainless steel. A numerical model based on coupled analysis of macro heat transfer and micro diffusion transformation has been developed in order to predict retained δ-ferrite in continuously cast 304 stainless steel slab. The finite difference technique for moving boundary problem has been formulated utilizing 'murray-landis variable-grid method'. The reliability of numerical model is compared with the other results. The prediction of δ-ferrite content in CC type 304 stainless steel slabs shows good agreement between measured and predicted results. Effect of secondary cooling condition on the δ-ferrite has been also investigated

  20. Hot working alkali halides for laser window applications

    International Nuclear Information System (INIS)

    Koepke, B.G.; Anderson, R.H.; Stokes, R.J.

    1975-01-01

    The techniques used to hot work alkali halide crystals into laser window blanks are reviewed. From the point of view of high power laser window applications one of the materials with a high figure of merit is KCl. Thus the materials examined are KCl and alloys of KCl-KBr containing 5 mole percent KBr. The fabrication techniques include conventional and constrained press forging, isostatic press forging and hot rolling. Optical properties are paramount to the ultimate usefulness of these materials. Results on the optical properties of the hot worked material are included together with mechanical properties and microstructural data

  1. The Work Softening by Deformation-Induced Disordering and Cold Rolling of 6.5 wt pct Si Steel Thin Sheets

    Science.gov (United States)

    Wang, Xianglong; Li, Haoze; Zhang, Weina; Liu, Zhenyu; Wang, Guodong; Luo, Zhonghan; Zhang, Fengquan

    2016-09-01

    As-cast strip of 6.5 wt pct Si steel was fabricated by twin-roll strip casting. After hot rolling at 1323 K (1050 °C), thin sheets with the thickness of 0.35 mm were produced by warm rolling at 373 K (100 °C) with rolling reductions of 15, 25, 35, 45, 55, and 65 pct. Influence of warm rolling reduction on ductility was investigated by room temperature bending test. The measurement of macro-hardness showed that "work softening" could begin when the warm rolling reduction exceeded 35 pct. The room temperature ductility of the thin sheets gradually increased with the increase of warm rolling reductions, and the plastic deformation during bending began to form when the warm rolling reduction was greater than 45 pct, the 65 pct rolled thin sheet exhibited the maximum plastic deformation of about 0.6 pct during bending at room temperature, with a few small dimples having been observed on the fracture surfaces. B2-ordered domains were formed in the 15, 25, 35, 45, and 55 pct rolled specimens, and their average size decreased with the increase of warm rolling reductions. By contrast, no B2-ordered domain could be found in the 65 pct rolled specimen. It had been observed that large-ordered domains could be split into several small parts by the slip of partial super-dislocations during warm rolling, which led to significant decrease of the order degree to cause the phenomenon of deformation-induced disordering. On the basis of these results, cold rolling schedule was developed to successfully fabricate 0.25-mm-thick sheets with good surface qualities and magnetic properties from warm rolled sheets.

  2. Multivariable control of a rolling spider drone

    Science.gov (United States)

    Lyu, Haifeng

    The research and application of Unmanned Aerial Vehicles (UAVs) has been a hot topic recently. A UAV is dened as an aircraft which is designed not to carry a human pilot or operated with remote electronic input by the flight controller. In this thesis, the design of a control system for a quadcopter named Rolling Spider Drone is conducted. The thesis work presents the design of two kinds of controllers that can control the Drone to keep it balanced and track different kinds of input trajectories. The nonlinear mathematical model for the Drone is derived by the Newton-Euler method. The rotational subsystem and translational system are derived to describe the attitude and position motion of Drone. Techniques from linear control theory are employed to linearize the highly coupled and nonlinear quadcopter plant around equilibrium points and apply the linear feedback controller to stabilize the system. The controller is a digital tracking system that deploys LQR for system stability design. Fixed gain and adaptive gain scheduled controllers are developed and compared with different LQR weights. Step references and reference trajectories involving signicant variation for the yaw angle in the xy-plane and three-dimensional spaces are tracked in the simulation. The physical implementation and an output feedback controller are considered for future work.

  3. Annealing of (DU-10Mo)-Zr Co-Rolled Foils

    International Nuclear Information System (INIS)

    Pacheco, Robin Montoya; Alexander, David John; Mccabe, Rodney James; Clarke, Kester Diederik; Scott, Jeffrey E.; Montalvo, Joel Dwayne; Papin, Pallas; Ansell, George S.

    2017-01-01

    Producing uranium-10wt% molybdenum (DU-10Mo) foils to clad with Al first requires initial bonding of the DU-10Mo foil to zirconium (Zr) by hot rolling, followed by cold rolling to final thickness. Rolling often produces wavy (DU-10Mo)-Zr foils that should be flattened before further processing, as any distortions could affect the final alignment and bonding of the Al cladding to the Zr co-rolled surface layer; this bonding is achieved by a hot isostatic pressing (HIP) process. Distortions in the (DU-10Mo)-Zr foil may cause the fuel foil to press against the Al cladding and thus create thinner or thicker areas in the Al cladding layer during the HIP cycle. Post machining is difficult and risky at this stage in the process since there is a chance of hitting the DU-10Mo. Therefore, it is very important to establish a process to flatten and remove any waviness. This study was conducted to determine if a simple annealing treatment could flatten wavy foils. Using the same starting material (i.e. DU-10Mo coupons of the same thickness), five different levels of hot rolling and cold rolling, combined with five different annealing treatments, were performed to determine the effect of these processing variables on flatness, bonding of layers, annealing response, microstructure, and hardness. The same final thickness was reached in all cases. Micrographs, textures, and hardness measurements were obtained for the various processing combinations. Based on these results, it was concluded that annealing at 650°C or higher is an effective treatment to appreciably reduce foil waviness.

  4. Annealing of (DU-10Mo)-Zr Co-Rolled Foils

    Energy Technology Data Exchange (ETDEWEB)

    Pacheco, Robin Montoya [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Alexander, David John [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Mccabe, Rodney James [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Clarke, Kester Diederik [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Scott, Jeffrey E. [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Montalvo, Joel Dwayne [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Papin, Pallas [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Ansell, George S. [Colorado School of Mines, Golden, CO (United States)

    2017-01-20

    Producing uranium-10wt% molybdenum (DU-10Mo) foils to clad with Al first requires initial bonding of the DU-10Mo foil to zirconium (Zr) by hot rolling, followed by cold rolling to final thickness. Rolling often produces wavy (DU-10Mo)-Zr foils that should be flattened before further processing, as any distortions could affect the final alignment and bonding of the Al cladding to the Zr co-rolled surface layer; this bonding is achieved by a hot isostatic pressing (HIP) process. Distortions in the (DU-10Mo)-Zr foil may cause the fuel foil to press against the Al cladding and thus create thinner or thicker areas in the Al cladding layer during the HIP cycle. Post machining is difficult and risky at this stage in the process since there is a chance of hitting the DU-10Mo. Therefore, it is very important to establish a process to flatten and remove any waviness. This study was conducted to determine if a simple annealing treatment could flatten wavy foils. Using the same starting material (i.e. DU-10Mo coupons of the same thickness), five different levels of hot rolling and cold rolling, combined with five different annealing treatments, were performed to determine the effect of these processing variables on flatness, bonding of layers, annealing response, microstructure, and hardness. The same final thickness was reached in all cases. Micrographs, textures, and hardness measurements were obtained for the various processing combinations. Based on these results, it was concluded that annealing at 650°C or higher is an effective treatment to appreciably reduce foil waviness.

  5. Towards roll-to-roll manufacturing of polymer photonic devices

    Science.gov (United States)

    Subbaraman, Harish; Lin, Xiaohui; Ling, Tao; Guo, L. Jay; Chen, Ray T.

    2014-03-01

    Traditionally, polymer photonic devices are fabricated using clean-room processes such as photolithography, e-beam lithography, reactive ion etching (RIE) and lift-off methods etc, which leads to long fabrication time, low throughput and high cost. We have utilized a novel process for fabricating polymer photonic devices using a combination of imprinting and ink jet printing methods, which provides high throughput on a variety of rigid and flexible substrates with low cost. We discuss the manufacturing challenges that need to be overcome in order to realize true implementation of roll-to-roll manufacturing of flexible polymer photonic systems. Several metrology and instrumentation challenges involved such as availability of particulate-free high quality substrate, development and implementation of high-speed in-line and off-line inspection and diagnostic tools with adaptive control for patterned and unpatterned material films, development of reliable hardware, etc need to be addressed and overcome in order to realize a successful manufacturing process. Due to extreme resolution requirements compared to print media, the burden of software and hardware tools on the throughput also needs to be carefully determined. Moreover, the effect of web wander and variations in web speed need to accurately be determined in the design of the system hardware and software. In this paper, we show the realization of solutions for few challenges, and utilizing these solutions for developing a high-rate R2R dual stage ink-jet printer that can provide alignment accuracy of web speed of 5m/min. The development of a roll-to-roll manufacturing system for polymer photonic systems opens limitless possibilities for the deployment of high performance components in a variety of applications including communication, sensing, medicine, agriculture, energy, lighting etc.

  6. Design of a Small Scale Roll to Roll Device

    OpenAIRE

    Pereira, Amon A; White, Edward; Kramer, Rebecca Krone

    2014-01-01

    In the soft robotics field, hyperelastic polymer films are used in conjunction with eutectic gallium indium to create flexible strain gages. However, rapid large scale manufacturing methods of such sensors have yet to be developed. Developing new manufacturing methods will allow for researchers to build and test new soft sensor concepts faster but also pave the way for future mass-production of these sensors for consumer or industrial consumption. One of those methods would be a Roll to...

  7. Perovskite solar cells for roll-to-roll fabrication

    Directory of Open Access Journals (Sweden)

    Uddin Ashraf

    2017-01-01

    Full Text Available Perovskite solar cell (PSCs is considered as the game changer in emerging photovoltaics technology. The highest certified efficiency is 22% with high temperature processed (∼500 °C TiO2 based electron transport layer (ETL. High temperature process is a rudimentary hindrance towards roll-to-roll processing of PSCs on flexible substrates. Low temperature solution process (<150 °C ZnO based ETL is one of the most promising candidate for large scale roll-to-roll fabrication of cells as it has nearly identical electron affinity (4.2 eV of TiO2. The mixed organic perovskite (MA0.6FA0.4PbI3 devices with Al doped ZnO (AZO ETL demonstrate average cell efficiency over 16%, which is the highest ever reported efficiency for this device configuration. The energy level alignment and related interfacial charge transport dynamics at the interface of ZnO and perovskite films and the adjacent charge transport layers are investigated. Significantly improved device stability, hysteresis free device photocurrent have been observed in MA0.6FA0.4PbI3 cells. A systematic electrochemical impedance spectroscopy, frequency dependent capacitance spectra, surface morphology and topography characterization have been conducted to understand the role of interfacial electronic properties between perovskite and neighbouring layers in perovskite device. A standardized degradation study, interfacial electronic property and capacitive spectra analysis of aged device, have been measured to understand the enhanced device stability in mixed MA0.6FA0.4PbI3 cells. Slow perovskite material decomposition rate and augmented device lifetime with AZO based devices have been found to be correlated with the more hydrophobic and acidic nature of AZO surface compared to pristine ZnO film.

  8. Stainless steel decontamination manipulators

    International Nuclear Information System (INIS)

    Sullivan, R.J.

    1986-01-01

    Three, large-volume coverage manipulator systems were designed and built for the Defense Water Processing Facility at the Savannah River Laboratory. These stainless steel systems will be used for high-pressure spray decontamination of waste containers and large process equipment modules. Each system has a manipulator arm, folding boom, and vertical drive and guide structure. Handling capacity is 45 kg, horizontal reach is 4.6 m with a 180-deg swing motion, and the vertical travel is 6 m. The system is remotely removable and replaceable in modules using an overhead crane and an impact wrench. The manipulator arm has seven motions: Shoulder rotation and pivot, elbow pivot, wrist pivot and rotation, and grip open-close. All motions are variable speed and are slip-clutch protected to prevent overloading from external forces (collisions)

  9. On the constant-roll inflation

    Science.gov (United States)

    Yi, Zhu; Gong, Yungui

    2018-03-01

    The primordial power spectra of scalar and tensor perturbations during slow-roll inflation are usually calculated with the method of Bessel function approximation. For constant-roll or ultra slow-roll inflation, the method of Bessel function approximation may be invalid. We compare the numerical results with the analytical results derived from the Bessel function approximation, and we find that they differ significantly on super-horizon scales if the constant slow-roll parameter ηH is not small. More accurate method is needed for calculating the primordial power spectrum for constant-roll inflation.

  10. Hot-working behavior of cast Pr-Fe-B magnets

    International Nuclear Information System (INIS)

    Shimoda, T.; Akioka, K.; Kobayashi, O.; Yamagami, T.; Ohki, T.; Miyagawa, M.; Yuri, T.

    1989-01-01

    The hot-working behavior of cast Pr-Fe-B magnets is investigated. The hot-working is done both at a low strain rate (hot-pressing) and a high strain rate (hot-rolling). Magnetic alignment induced by the hot-working is found to be closely related to the macrostructure of the cast ingots and the direction of principal stress. The appropriate structure is a columnar structure. The c-axis of the Pr2Fe14B phase is lying in the plane perpendicular to the growth direction of the dendrites. The principal stress during working should be given perpendicular to the growth direction

  11. Introduction of hot cell facility in research center Rez - Poster

    International Nuclear Information System (INIS)

    Petrickova, A.; Srba, O.; Miklos, M.; Svoboda, P.

    2015-01-01

    This poster presents the hot cell facility which is being constructed as part of the SUSEN project at the Rez research center (Czech Republic). Within this project a new complex of 10 hot cells and one semi-hot cell will be built. There will be 8 gamma hot cells and 2 alpha hot cells. In each hot cell a hermetic, removable box made of stainless steel will home different type of devices. The hot cells and semi hot cell will be equipped with devices for processing samples (cutting, welding, drilling, machining) as well as equipment for testing (sample preparation area, stress testing machine, fatigue machine, electromechanical creep machine, high frequency resonance pulsator...) and equipment for studying material microstructure (nano-indenter with nano-scratch tester and scanning electron microscope). An autoclave with water loop, installed in a cell will allow mechanical testing in control environment of water, pressure and temperature. A scheme shows the equipment of each cell. This hot laboratory will be able to cover all the process to study radioactive materials: receiving the material, the preparation of the samples, mechanical testing and microstructure observation. Our hot cells will be close to the research nuclear reactor LVR-15 and new irradiation facility (high irradiation by cobalt source) is planned to be built within the SUSEN project

  12. Influence of the Radiation Shield on the Temperature of Rails Rolled in the Reversing Mill

    Directory of Open Access Journals (Sweden)

    Gołdasz A.

    2015-04-01

    Full Text Available The paper presents a mathematical model of heat transfer during cooling of hot-rolled rails in the reversing mill. The influence of the radiation shield on the temperature of rolled rails has been analyzed. The heat transfer model for cooling a strip covered by the thermal shield has been presented. The two types of shields build of steel and aluminum sheets separated with insulating layer have been studded. Calculations have been performed with self developed software which utilizes the finite element method.

  13. Aging in PWR conditions of martensitic stainless steels

    International Nuclear Information System (INIS)

    Boursier, J.M.; Buisine, D.; Fronteau, M.; Michel, D.; Rouillon, Y.; Yrieix, B.; Meyzaud, Y.

    1998-01-01

    Martensitic stainless steels are largely used in Nuclear Power Plant (pump impeller, valve stem...) because of their high mechanical characteristics and their good resistance to corrosion. Nevertheless some of those components could operate at temperature higher than 250 deg.C, which could embrittle the material by the precipitation of a chromium-rich phase during aging. In collaboration with Framatome, Electricite de France has undertaken numerous studies in order to understand this process of embrittlement. This paper presents a review of the metallurgical investigations on martensitic stainless steels components which were performed in the EDF hot laboratory. In peculiar, it should be noted the good correlation between inservice experience and the modelling developed by EDF R and D division. Finally and in association with safety analysis, these results will allow to establish the maintenance strategy of the French Nuclear Power Plants. (authors)

  14. Tensile properties of the modified 13Cr martensitic stainless steels

    Energy Technology Data Exchange (ETDEWEB)

    Mabruri, Efendi, E-mail: effe004@lipi.go.id; Anwar, Moch Syaiful, E-mail: moch.syaiful.anwar@lipi.go.id; Prifiharni, Siska, E-mail: siska.prifiharni@lipi.go.id; Romijarso, Toni B.; Adjiantoro, Bintang [Research Center for Metallurgy and Materials, Indonesian Institute of Sciences (LIPI) Kawasan Puspiptek Gd. 470 Serpong, Tangerang Selatan 15314 (Indonesia)

    2016-04-19

    This paper reports the influence of Mo and Ni on the tensile properties of the modified 13Cr martensitic stainless steels in tempered condition. Four steels with different content of Mo and Ni were prepared by induction melting followed by hot forging, quenching and tempering. The experimental results showed that the addition of about 1% and 3% Mo has a beneficial effect to increase both the tensile strength and the elongation of the steels. On the contrary, the addition of about 3% Ni into the martensitic stainless steel results in decreasing of both the tensile strength and the elongation. Among the alloys investigated the 13Cr3Mo type steel exhibited largest tensile strength of 1348 MPa and largest elongation of 12%. The observation on the tensile fractured surfaces by using scanning electron microscope supported these findings.

  15. Tensile properties of the modified 13Cr martensitic stainless steels

    International Nuclear Information System (INIS)

    Mabruri, Efendi; Anwar, Moch Syaiful; Prifiharni, Siska; Romijarso, Toni B.; Adjiantoro, Bintang

    2016-01-01

    This paper reports the influence of Mo and Ni on the tensile properties of the modified 13Cr martensitic stainless steels in tempered condition. Four steels with different content of Mo and Ni were prepared by induction melting followed by hot forging, quenching and tempering. The experimental results showed that the addition of about 1% and 3% Mo has a beneficial effect to increase both the tensile strength and the elongation of the steels. On the contrary, the addition of about 3% Ni into the martensitic stainless steel results in decreasing of both the tensile strength and the elongation. Among the alloys investigated the 13Cr3Mo type steel exhibited largest tensile strength of 1348 MPa and largest elongation of 12%. The observation on the tensile fractured surfaces by using scanning electron microscope supported these findings.

  16. Improved Dutch Roll Approximation for Hypersonic Vehicle

    Directory of Open Access Journals (Sweden)

    Liang-Liang Yin

    2014-06-01

    Full Text Available An improved dutch roll approximation for hypersonic vehicle is presented. From the new approximations, the dutch roll frequency is shown to be a function of the stability axis yaw stability and the dutch roll damping is mainly effected by the roll damping ratio. In additional, an important parameter called roll-to-yaw ratio is obtained to describe the dutch roll mode. Solution shows that large-roll-to-yaw ratio is the generate character of hypersonic vehicle, which results the large error for the practical approximation. Predictions from the literal approximations derived in this paper are compared with actual numerical values for s example hypersonic vehicle, results show the approximations work well and the error is below 10 %.

  17. Variability in creep and rupture test results in a single heat of type 304 stainless steel. R and D report LR:75:4213-01:3

    International Nuclear Information System (INIS)

    Leyda, W.E.; Schultz, C.C.

    1975-09-01

    Results of uniaxial creep and rupture tests, from a single heat of type 304 stainless steel, are examined to determine the reasons for their greater-than-expected variability. The test results were obtained as part of a program to develop and verify high temperature structural design methods for liquid metal fast breeder reactor system components. A single heat of material (heat 9T2796) is being used throughout the program, by all investigators and in several product forms, to minimize the problem of heat-to-heat variations in elevated temperature behavior. The same laboratory reanneal was specified for each product form to reduce differences in behavior among the several being used. The data discussed was obtained from the 5/8-inch diameter, hot-rolled bar product form. The laboratory reanneal was performed after finish machining to minimize specimen-to-specimen differences. In spite of these efforts to reduce data variability, significant scatter was observed in both short-time and long-time deformation response, and also in time-to-rupture results

  18. Roll type conducting polymer legs for rigid-flexible thermoelectric generator

    Directory of Open Access Journals (Sweden)

    Teahoon Park

    2017-07-01

    Full Text Available A roll-type conducting polymer film was explored as a flexible organic p-type thermoelectric leg using poly(3,4-ethylenedioxythiophene (PEDOT doped with tosylate. The PEDOT films were prepared through solution casting polymerization and rolled up for a roll-type leg. Due to the high flexibility, the roll-type PEDOT leg enabled easy contact to both top and bottom electrodes. Simulation on the dynamic heat transfer and convective cooling for a vertically roosted rod- and roll-type PEDOT leg showed that the temperature difference (ΔT between the hot and cold sides of the leg was much higher in the roll than that of the rod. The PEDOT legs were integrated with n-type Bi2Te3 blocks, to give a 36-couple rigid-flexible thermoelectric generator (RF-TEG. The maximum output voltage from the 36-couple RF-TEG under a ΔT of 7.9 K was determined as 36.7 mV along with a high output power of 115 nW. A wearable RF-TEG was prepared upon the combination of the 36-couple RF-TEG with an arm warmer, to afford an output voltage of 10.6 mV, which was generated constantly and steadily from human wrist heat.

  19. Tachyon constant-roll inflation

    Science.gov (United States)

    Mohammadi, A.; Saaidi, Kh.; Golanbari, T.

    2018-04-01

    The constant-roll inflation is studied where the inflaton is taken as a tachyon field. Based on this approach, the second slow-roll parameter is taken as a constant which leads to a differential equation for the Hubble parameter. Finding an exact solution for the Hubble parameter is difficult and leads us to a numerical solution for the Hubble parameter. On the other hand, since in this formalism the slow-roll parameter η is constant and could not be assumed to be necessarily small, the perturbation parameters should be reconsidered again which, in turn, results in new terms appearing in the amplitude of scalar perturbations and the scalar spectral index. Utilizing the numerical solution for the Hubble parameter, we estimate the perturbation parameter at the horizon exit time and compare it with observational data. The results show that, for specific values of the constant parameter η , we could have an almost scale-invariant amplitude of scalar perturbations. Finally, the attractor behavior for the solution of the model is presented, and we determine that the feature could be properly satisfied.

  20. Development of microstructure and texture in Fe–26Mn–3Si–3Al alloy during cold-rolling and annealing

    International Nuclear Information System (INIS)

    Kowalska, Joanna; Ratuszek, Wiktoria; Witkowska, Małgorzata; Zielińska-Lipiec, Anna

    2014-01-01

    Highlights: • We report evolution of microstructure and texture in the Fe–26Mn–3Si–3Al alloy during cold-rolling and annealing. • Mechanical twinning and martensitic transformation (γ → ε and γ → ε → α′) had occurred during cold-rolling. • The crystallographic relations between austenite γ and martensite ε have been ascertained. • During annealing the reverse martensite to austenite transformation occurred. - Abstract: Fe–26 wt.% Mn–3 wt.% Si–3 wt.% Al alloy was cast, forged, hot-rolled at temperatures between 1200 °C and 900 °C and cold-rolled with 5–66% reductions in thickness. The specimens which were cold-rolled 57% were annealed in the temperature range 500–750 °C. Microstructure and texture of this alloy, which has a low stacking fault energy, were evaluated after cold-rolling and after subsequent annealing, X-ray diffraction and transmission electron microscopy showed that mechanical twinning and martensitic transformations (γ → ε and γ → ε → α′) took place during cold-rolling. The crystallographic Burgers relations {0 0 0 1}ε || {1 1 1}γ and 〈1 1 2 0〉ε || 〈1 1 0〉γ between martensite (ε) and austenite (γ), were found in the cold-rolled material. During annealing the reverse martensite to austenite transformation occurred

  1. Effect of cold rolling on microstructure and mechanical property of extruded Mg–4Sm alloy during aging

    Energy Technology Data Exchange (ETDEWEB)

    Li, Rongguang, E-mail: lirongguang1980@126.com [School of Mechanical Engineering, Shenyang University of Chemical Technology, Shenyang 110142 (China); Xin, Renlong; Chapuis, Adrien; Liu, Qing [School of Materials Science and Engineering, Chongqing University, Chongqing 400045 (China); Fu, Guangyan; Zong, Lin; Yu, Yongmei; Guo, Beitao; Guo, Shuguo [School of Mechanical Engineering, Shenyang University of Chemical Technology, Shenyang 110142 (China)

    2016-02-15

    Microstructure and mechanical properties of the Mg–4Sm (wt.%) alloy, prepared via combined processes of extrusion, cold rolling and aging, have been investigated. The hot extruded alloy exhibits a weak rare earth magnesium alloy texture with < 11 − 21 >//ED, while the cold-rolled alloy shows a stronger basal texture with < 0001 >//ND. Many tensile twins and double twins are observed in grains after rolling. The cold-rolled alloy shows a weak age-hardening response compared with the extruded alloy, which is the result of more precipitation in the twin boundary during aging. The rolled alloy exhibits almost no precipitate free zone during aging compared with the extruded alloy. The higher proof stress of the rolled alloy in peak-aged condition is attributed to the presence of twin boundaries, stronger basal texture, higher dislocation density, and the suppression of precipitate free zone compared with the extruded alloy. - Highlights: • No precipitate free zone appears in cold-rolled alloy after aging. • Segregation and precipitates are observed in twin boundaries and grain boundaries. • Cold-rolled alloy shows a weak age-hardening response.

  2. Austenitic stainless steel weld inspection

    International Nuclear Information System (INIS)

    Mech, S.J.; Emmons, J.S.; Michaels, T.E.

    1978-01-01

    Analytical techniques applied to ultrasonic waveforms obtained from inspection of austenitic stainless steel welds are described. Experimental results obtained from a variety of geometric and defect reflectors are presented. Specifically, frequency analyses parameters, such as simple moments of the power spectrum, cross-correlation techniques, and adaptive learning network analysis, all represent improvements over conventional time domain analysis of ultrasonic waveforms. Results for each of these methods are presented, and the overall inspection difficulties of austenitic stainless steel welds are discussed

  3. Effects of S and Mn on the hot workability of STS 316L and 309S steels

    International Nuclear Information System (INIS)

    Lee, Soo Chan; Kim, Young Hwan; Lee, Yun Yong

    1998-01-01

    Effects of sulfur and manganese on the hot workability of STS 316L and 309S steels have been investigated. From the results of hot workability test, the hot ductility was decreased with increasing sulfur content and reheating temperature. This is considered to be caused by sulfur segregations and sulfide precipitates at grain boundaries. Sulfur would be dissolved under the reheating conditions and reprecipitated with decreasing temperatures during hot rolling. The content of reprecipitated sulfur is decreased with increasing manganese content and decreasing reheating temperature. Therefore, the hot ductility is increased with increasing manganese content. It was also found that the hot ductility is increased with decreasing reheating temperature

  4. Prediction of microstructure and ductile damage of a high-speed railway axle steel during cross wedge rolling

    OpenAIRE

    Huo, Y; Lin, J; Bai, Q; Wang, B; Tang, X; Ji, H

    2016-01-01

    Microstructure and ductile damage have a significant influence on the deformation behavior of high-speed railway axles during hot cross wedge rolling (CWR) and its final performance. In this study, based on the continuum damage mechanics, a multiaxial constitutive model coupling microstructure and ductile damage was established to predict the evolution of microstructure and ductile damage of 25CrMo4 during hot CWR processes. Material constants within the multiaxial constitutive model were det...

  5. Weldability and microstructural analysis of nuclear-grade austenitic stainless steels

    International Nuclear Information System (INIS)

    Lee, C.H.

    1988-01-01

    This study evaluated the hot-ductility response, and hot-cracking susceptibility (fusion-zone solidification cracking and HAZ liquation cracking) of modified nuclear-grade and standard austenitic stainless steels. Extensive microstructural characterization using state-of-the-art analytical electron microscopy (TEM and STEM) as well as SEM (EDAX) and OLM was performed to correlate the material behavior with metallurgical characteristics. In addition, studies of the effect of Si, N, and rare earth elements on hot-cracking susceptibility, significance of the ductility dip phenomena and backfilled solidification cracks were also performed. Furthermore, based on the metallurgical evaluation, the possible mechanisms involved in solidification cracking and HAZ liquation cracking of the modified alloys are proposed. Finally, the optimized chemical specifications and requirements for nuclear-grade stainless steels are also suggested

  6. Residual stresses and fatigue in a duplex stainless steel

    International Nuclear Information System (INIS)

    Johansson, Johan

    1999-01-01

    Duplex stainless steels, consisting of approximately equal amounts of austenite and ferrite, often combine the best features of austenitic and ferritic stainless steels. They generally have good mechanical properties, including high strength and ductility, and the corrosion resistance is often better than conventional austenitic grades. This has lead to a growing use of duplex stainless steels as a material in mechanically loaded constructions. However, detailed knowledge regarding its mechanical properties and deformation mechanisms are still lacking. In this thesis special emphasis has been placed on the residual stresses and their influence on mechanical behaviour of duplex stainless steels. Due to the difference in coefficient of thermal expansion between the two phases, tensile microstresses are found in the austenitic phase and balancing compressive microstresses in the ferritic phase. The first part of this thesis is a literature survey, which will give an introduction to duplex stainless steels and review the fatigue properties of duplex stainless steels and the influence of residual stresses in two-phase material. The second part concerns the evolution of the residual stress state during uniaxial loading. Initial residual stresses were found to be almost two times higher in the transverse direction compared to the rolling direction. During loading the absolute value of the microstresses increased in the macroscopic elastic regime but started to decrease with increasing load in the macroscopic plastic regime. A significant increase of the microstresses was also found to occur during unloading. Finite element simulations also show stress variation within one phase and a strong influence of both the elastic and plastic anisotropy of the individual phases on the simulated stress state. In the third part, the load sharing between the phases during cyclic loading is studied. X-ray diffraction stress analysis and transmission electron microscopy show that even if

  7. Residual stresses and fatigue in a duplex stainless steel

    Energy Technology Data Exchange (ETDEWEB)

    Johansson, Johan

    1999-05-01

    Duplex stainless steels, consisting of approximately equal amounts of austenite and ferrite, often combine the best features of austenitic and ferritic stainless steels. They generally have good mechanical properties, including high strength and ductility, and the corrosion resistance is often better than conventional austenitic grades. This has lead to a growing use of duplex stainless steels as a material in mechanically loaded constructions. However, detailed knowledge regarding its mechanical properties and deformation mechanisms are still lacking. In this thesis special emphasis has been placed on the residual stresses and their influence on mechanical behaviour of duplex stainless steels. Due to the difference in coefficient of thermal expansion between the two phases, tensile microstresses are found in the austenitic phase and balancing compressive microstresses in the ferritic phase. The first part of this thesis is a literature survey, which will give an introduction to duplex stainless steels and review the fatigue properties of duplex stainless steels and the influence of residual stresses in two-phase material. The second part concerns the evolution of the residual stress state during uniaxial loading. Initial residual stresses were found to be almost two times higher in the transverse direction compared to the rolling direction. During loading the absolute value of the microstresses increased in the macroscopic elastic regime but started to decrease with increasing load in the macroscopic plastic regime. A significant increase of the microstresses was also found to occur during unloading. Finite element simulations also show stress variation within one phase and a strong influence of both the elastic and plastic anisotropy of the individual phases on the simulated stress state. In the third part, the load sharing between the phases during cyclic loading is studied. X-ray diffraction stress analysis and transmission electron microscopy show that even if

  8. Investigation of austenitic alloys for advanced heat recovery and hot-gas cleanup systems

    Energy Technology Data Exchange (ETDEWEB)

    Swindeman, R.W. [Oak Ridge National Lab., TN (United States)

    1997-12-01

    Materials properties were collected for the design and construction of structural components for use in advanced heat recovery and hot gas cleanup systems. Alloys systems included 9Cr-1Mo-V steel, modified 316 stainless steel, modified type 310 stainless steel, modified 20Cr-25Ni-Nb stainless steel, and modified alloy 800. Experimental work was undertaken to expand the databases for potentially useful alloys. Types of testing included creep, stress-rupture, creep-crack growth, fatigue, and post-exposure short-time tensile tests. Because of the interest in relatively inexpensive alloys for service at 700 C and higher, research emphasis was placed on a modified type 310 stainless steel and a modified 20Cr-25Ni-Nb stainless steel. Both steels were found to have useful strength to 925 C with good weldability and ductility.

  9. Size effects in winding roll formed profiles: A study of carcass production for flexible pipes in offshore industry

    DEFF Research Database (Denmark)

    Nielsen, Peter Søe; Nielsen, Morten Storgaard; Bay, Niels

    2013-01-01

    neutral plane. Other parameters such as profile entry angle on the mandrel and spiral pitch are likely to have significant importance. Proper dividing point position is shown to be obtainable by adjusting the profile in the roll forming stage. The profile rolling is successfully modeled by Finite Element......Carcass production of flexible offshore oil and gas pipes implies winding and interlocking of a roll formed stainless steel profile around a mandrel in a spiral shape. The location of the dividing point between the left and right half of the s-shaped profile in the finished carcass is very...... Analysis (FEA), whereas a simplified FE-model of the subsequent winding operation shows that full interlock modeling is required for proper prediction of profile deformation. © (2013) Trans Tech Publications....

  10. Characterization of microstructure, texture and magnetic properties in twin-roll casting high silicon non-oriented electrical steel

    Energy Technology Data Exchange (ETDEWEB)

    Li, Hao-Ze; Liu, Hai-Tao, E-mail: liuht@ral.neu.edu.cn; Liu, Zhen-Yu, E-mail: zyliu@mail.neu.edu.cn; Lu, Hui-Hu; Song, Hong-Yu; Wang, Guo-Dong

    2014-02-15

    An Fe-6.5 wt.% Si-0.3 wt.% Al as-cast sheet was produced by twin-roll strip casting process, then treated with hot rolling, warm rolling and annealing. A detailed study of the microstructure and texture evolution at different processing stages was carried out by optical microscopy, X-ray diffraction and electron backscattered diffraction analysis. The initial as-cast strip showed strong columnar grains and pronounced < 001 >//ND texture. The hot rolled and warm rolled sheets were characterized by large amounts of shear bands distributed through the thickness together with strong < 110 >//RD texture and weak < 111 >//ND texture. After annealing, detrimental < 111 >//ND texture almost disappeared while beneficial (001)<210 >, (001)<010 >, (115)<5 − 10 1 > and (410) < 001 > recrystallization textures were formed, thus the magnetic induction of the annealed sheet was significantly improved. The recrystallization texture in the present study could be explained by preferred nucleation and grain growth mechanism. - Highlights: • A high silicon as-cast strip with columnar structure was produced. • A thin warm rolled sheet without large edge cracks was obtained. • Microstructure and texture evolution at each stage were investigated. • Beneficial (001)<210 >, (001)<010 >, (410)<001 > recrystallization textures were formed. • The magnetic induction of annealed sheet was significantly improved.

  11. Fluid management in roll-to-roll nanoimprint lithography

    Science.gov (United States)

    Jain, A.; Bonnecaze, R. T.

    2013-06-01

    The key process parameters of UV roll-to-roll nanoimprint lithography are identified from an analysis of the fluid, curing, and peeling dynamics. The process includes merging of droplets of imprint material, curing of the imprint material from a viscous liquid to elastic solid resist, and pattern replication and detachment of the resist from template. The time and distances on the web or rigid substrate over which these processes occur are determined as function of the physical properties of the uncured liquid, the cured solid, and the roller configuration. The upper convected Maxwell equation is used to model the viscoelastic liquid and to calculate the force on the substrate and the torque on the roller. The available exposure time is found to be the rate limiting parameter and it is O(√Rho /uo), where R is the radius of the roller, ho is minimum gap between the roller and web, and uo is the velocity of the web. The residual layer thickness of the resist should be larger than the gap between the roller and the substrate to ensure complete feature filling and optimal pattern replication. For lower residual layer thickness, the droplets may not merge to form a continuous film for pattern transfer.

  12. Solar 'hot spots' are still hot

    Science.gov (United States)

    Bai, Taeil

    1990-01-01

    Longitude distributions of solar flares are not random but show evidence for active zones (or hot spots) where flares are concentrated. According to a previous study, two hot spots in the northern hemisphere, which rotate with a synodic period of about 26.72 days, produced the majority of major flares, during solar cycles 20 and 21. The more prominent of these two hot spots is found to be still active during the rising part of cycle 22, producing the majority of northern hemisphere major flares. The synodic rotation period of this hot spot is 26.727 + or - 0.007 days. There is also evidence for hot spots in the southern hemisphere. Two hot spots separated by 180 deg are found to rotate with a period of 29.407 days, with one of them having persisted in the same locations during cycles 19-22 and the other, during cycles 20-22.

  13. Solar hot spots are still hot

    International Nuclear Information System (INIS)

    Bai, T.

    1990-01-01

    Longitude distributions of solar flares are not random but show evidence for active zones (or hot spots) where flares are concentrated. According to a previous study, two hot spots in the northern hemisphere, which rotate with a synodic period of about 26.72 days, produced the majority of major flares, during solar cycles 20 and 21. The more prominent of these two hot spots is found to be still active during the rising part of cycle 22, producing the majority of northern hemisphere major flares. The synodic rotation period of this hot spot is 26.727 + or - 0.007 days. There is also evidence for hot spots in the southern hemisphere. Two hot spots separated by 180 deg are found to rotate with a period of 29.407 days, with one of them having persisted in the same locations during cycles 19-22 and the other, during cycles 20-22. 14 refs

  14. The real time rolling shutter

    OpenAIRE

    Monaghan, David; O'Connor, Noel E.; Cleary, Anne; Connolly, Denis

    2015-01-01

    From an early age children are often told either, you are creative you should do art but stay away from science and maths. Or that you are mathematical you should do science but you're not that creative. Compounding this there also exist some traditional barriers of artistic rhetoric that say, "don't touch, don't think and don't be creative, we've already done that for you, you can just look...". The Real Time Rolling Shutter is part of a collaborative Art/Science partnership whose core tenet...

  15. Grooved tube plug rolls in

    International Nuclear Information System (INIS)

    Krausser, P.

    1991-01-01

    The removable plugs used to date by the Power Generation Group (KWU) of Siemens to seal defective steam generator tubes have a good track record. Their sealing principle is based on the elastic tensioning of three seal disks against the inside wall of the tube. Now a further removable plug is available -a roll-in plug with a metal-coated surface. It is particularly suitable for use in the roller-expanded zone of the tubes at the tube sheet. The plugs can be used in both Siemens-KWU steam generators and in steam generators manufactured in compliance with the guidelines of the ASME Code. (author)

  16. ROLL OUT THE TALENT : Final project report

    OpenAIRE

    Eerola, Tuomas; Tuominen, Pirjo; Hakkarainen, Riitta-Liisa; Laurikainen, Marja; Mero, Niina

    2014-01-01

    The ROLL OUT THE TALENT project was born out of the desire to recognise and support the strengths of vocational students and to develop new and innovative operating models. ROLL OUT THE TALENT promoted regional cooperation between institutes and companies. The project produced operating and study path models that take into consideration the individual strengths of vocational students and the principles of lifelong learning. This is the final report of the ROLL OUT THE TALENT project, and ...

  17. Interlayer adhesion in roll-to-roll processed flexible inverted polymer solar cells

    KAUST Repository

    Dupont, Stephanie R.; Oliver, Mark; Krebs, Frederik C.; Dauskardt, Reinhold H.

    2012-01-01

    The interlayer adhesion of roll-to-roll processed flexible inverted P3HT:PCBM bulk heterojunction (BHJ) polymer solar cells is reported. Poor adhesion between adjacent layers may result in loss of device performance from delamination driven

  18. Hot embossing and mechanical punching of biodegradable microcontainers for oral drug delivery

    DEFF Research Database (Denmark)

    Petersen, Ritika Singh; Mahshid, Rasoul; Andersen, Nis Korsgaard

    2015-01-01

    A process has been developed to fabricate discrete three-dimensional microcontainers for oral drug delivery application in Poly-L-Lactic Acid (PLLA) polymer. The method combines hot embossing for the definition of holes in a PLLA film and mechanical punching to penetrate the polymer layer around...... and shapes of microcontainers. Finally, the process is compatible with roll-to-roll processing that could lead to low cost high volume production. © 2014 Elsevier B.V. All rights reserved....

  19. Radiometric study of creep in ingot rolling

    International Nuclear Information System (INIS)

    Kubicek, P.; Zamyslovsky, Z.; Uherek, J.

    The radiometric study of creep during ingot rolling performed in the rolling mill of the Vitkovice Iron and Steel Works and the first results are described. Selected sites in 3 to 8 ton ingots were labelled with 2 to 3.7x10 5 Bq of 60 Co and after rolling into blocks, the transposition of the labelled sites of the ingots was investigated. The results indicate creep during rolling, local extension in certain sites under study and help to determine the inevitable bottom crop incurred in the forming. Finally, the requirements put on the radiometric apparatus for the next stages of technological research are presented. (author)

  20. COMPETITION BEETWEN DYNAMIC RECUPERATION AND RECRYSTALLIZATION OF ASTM F 138 AUSTENITIC STAINLESS STEEL UTILIZED IN MEDICAL DEVICES

    Directory of Open Access Journals (Sweden)

    Fabio Henrique Casarini Geronimo

    2013-06-01

    Full Text Available ASTM F 138 austenitic stainless steel has being used in the manufacture of orthopedical devices by hot forging. In this work, the flow stress curves are determined by hot torsion tests in a wide range of temperatures and strain rates. With the observed microestrutural evolution by optical microscopy in different hot forming conditions in addiction with EBSD (Electron Backscatter Diffraction techniques it is possible to obtained the recrystallized volume fraction and the misorientation angles of the samples. Due to the intermediate level of stacking fault energy of this material, during the dynamic softening occurs a competition between recrystallization and recovery. The aim of this work is to identify the softening mechanisms in this stainless steel, as well as in which hot work conditions they become more active.

  1. Effect of Low-Temperature Sensitization on Hydrogen Embrittlement of 301 Stainless Steel

    Directory of Open Access Journals (Sweden)

    Chieh Yu

    2017-02-01

    Full Text Available The effect of metastable austenite on the hydrogen embrittlement (HE of cold-rolled (30% reduction in thickness 301 stainless steel (SS was investigated. Cold-rolled (CR specimens were hydrogen-charged in an autoclave at 300 or 450 °C under a pressure of 10 MPa for 160 h before tensile tests. Both ordinary and notched tensile tests were performed in air to measure the tensile properties of the non-charged and charged specimens. The results indicated that cold rolling caused the transformation of austenite into α′ and ε-martensite in the 301 SS. Aging at 450 °C enhanced the precipitation of M23C6 carbides, G, and σ phases in the cold-rolled specimen. In addition, the formation of α′ martensite and M23C6 carbides along the grain boundaries increased the HE susceptibility and low-temperature sensitization of the 450 °C-aged 301 SS. In contrast, the grain boundary α′-martensite and M23C6 carbides were not observed in the as-rolled and 300 °C-aged specimens.

  2. Quality Parameters Defined by Chebyshev Polynomials in Cold Rolling Process Chain

    International Nuclear Information System (INIS)

    Judin, Mika; Nylander, Jari; Larkiola, Jari; Verho, Martti

    2011-01-01

    The thickness profile of hot strip is of importance to profile, flatness and shape of the final cold rolled product. In this work, strip thickness and flatness profiles are decomposed into independent components by solving Chebyshev polynomials coefficients using matrix calculation. Four terms are used to characterize most common shapes of thickness and flatness profile. The calculated Chebyshev coefficients from different line measurements are combined together and analysed using neural network tools. The most common types of shapes are classified.

  3. Rolling into spatial disorientation: Simulator demonstration of the post-roll (Gillingham) illusion

    NARCIS (Netherlands)

    Nooij, S.A.E.; Groen, E.L.

    2011-01-01

    Introduction: Spatial disorientation (SD) is still a contributing factor in many aviation accidents, stressing the need for adequate SD training scenarios. In this article we focused on the post-roll effect (the sensation of rolling back after a roll maneuver, such as an entry of a coordinated turn)

  4. Hot roller embossing system equipped with a temperature margin-based controller

    Energy Technology Data Exchange (ETDEWEB)

    Kim, Seyoung, E-mail: seyoungkim@kimm.re.kr; Son, Youngsu; Lee, Sunghee; Ham, Sangyong; Kim, Byungin [Department of Robotics and Mechatronics, Korea Institute of Machinery and Materials (KIMM), Daejeon (Korea, Republic of)

    2014-08-15

    A temperature control system was proposed for hot roller embossing. The roll surface was heated using induction coils and cooled with a circulating chilled water system. The temperature of the roll surface was precisely controlled by a temperature margin-based control algorithm that we developed. Implementation of the control system reduced deviations in the roll surface temperature to less than ±2 °C. The tight temperature control and the ability to rapidly increase and decrease the roll temperature will allow optimum operating parameters to be developed quickly. The temperature margin-based controller could also be used to optimize the time course of electrical power and shorten the cooling time by choosing an appropriate temperature margin, possibly for limited power consumption. The chiller-equipped heating roll with the proposed control algorithm is expected to decrease the time needed to determine the optimal embossing process.

  5. Hot roller embossing system equipped with a temperature margin-based controller

    International Nuclear Information System (INIS)

    Kim, Seyoung; Son, Youngsu; Lee, Sunghee; Ham, Sangyong; Kim, Byungin

    2014-01-01

    A temperature control system was proposed for hot roller embossing. The roll surface was heated using induction coils and cooled with a circulating chilled water system. The temperature of the roll surface was precisely controlled by a temperature margin-based control algorithm that we developed. Implementation of the control system reduced deviations in the roll surface temperature to less than ±2 °C. The tight temperature control and the ability to rapidly increase and decrease the roll temperature will allow optimum operating parameters to be developed quickly. The temperature margin-based controller could also be used to optimize the time course of electrical power and shorten the cooling time by choosing an appropriate temperature margin, possibly for limited power consumption. The chiller-equipped heating roll with the proposed control algorithm is expected to decrease the time needed to determine the optimal embossing process

  6. The fabrication of ZnO nanowire field-effect transistors combining dielectrophoresis and hot-pressing

    International Nuclear Information System (INIS)

    Chang, Y-K; Chau-N H, Franklin

    2009-01-01

    Zinc oxide nanowire field-effect transistors (NW-FETs) were fabricated combining the dielectrophoresis (DEP) and the hot-pressing methods. DEP was used to position both ends of the nanowires on top of the source and the drain electrodes, respectively. Hot-pressing of nanowires on the electrodes was then employed to ensure good contacts between the nanowires and the electrodes. The good device performance achieved with our method of fabrication indicates that DEP combined with hot-pressing has the potential to be applied to the fabrication of flexible electronics on a roll-to-roll basis.

  7. Chemical decontamination of stainless steel

    International Nuclear Information System (INIS)

    Onuma, Tsutomu; Akimoto, Hidetoshi

    1991-01-01

    The present invention concerns a method for chemical decontamination of radioactive metal waste materials contaminated with radioactive materials on the surface, generated in radioactive materials-handling facilities. The invention is comprised of a method of chemical decontamination of stainless steel, characterized by comprising a first process of immersing a stainless steel-based metal waste material contaminated by radioactive materials on the surface in a sulfuric acid solution and second process of immersing in an aqueous solution of sulfuric acid and oxidizing metal salt, in which a portion of the surface of the stainless steel to be decontaminated is polished mechanically to expose a portion of the base material before the above first and second processes. 1 figs., 2 tabs

  8. Effects of Niobium Microalloying on Microstructure and Properties of Hot-Dip Galvanized Sheet

    Energy Technology Data Exchange (ETDEWEB)

    Mohrbacher, Hardy [NiobelCon bvba, Brussels (Belgium)

    2010-04-15

    Niobium microalloying is effective in hot-rolled and cold-rolled steels by providing a fine-grained microstructure resulting in increased strength. To optimize the strengthening effect, alloy design and hot-rolling conditions have to be adapted. As a key issue the dissolution and precipitation characteristics of Nb are discussed in particular with regard to the run-out table conditions. It is then considered how the hot-rolled microstructure and the solute state of Nb interact with the hot-dip galvanizing cycle. The adjusted conditions allow controlling the morphology and distribution of phases in the cold-rolled annealed material. Additional precipitation hardening can be achieved as well. The derived options can be readily applied to produce conventional HSLA and IF high strength steels as well as to modem multiphase steels. It will be explained how important application properties such as strength, elongation, bendability, weldability and delayed cracking resistance can be influenced in a controlled and favorable way. Examples of practical relevance and experience are given.

  9. Development of nuclear grade stainless steels at KCSSL

    International Nuclear Information System (INIS)

    Balachandran, G.; Dhere, M.; Mahadik, A.; Hinge, N.M.; Balasubramanian, V.

    2011-01-01

    Kalyani Carpenter Special Steels Ltd is an alloy steel plant, where a variety of alloy steel grades are produced for automotive, defence, nuclear and aerospace applications. The plant has developed expertise in processing of several alloy steel grades of superior quality that meets stringent specifications. Primary steel is processed through a combination of electric arc furnace, ladle furnace and vacuum degassing where stringent control over dephosphorisation, desulphurization, deoxidation is effected to get a refined high quality steel. The molten steel is cast through continuous casting of slabs or ingot casting. In grades specific to nuclear application, the primary cast products are further subjected to electroslag remelting to achieve further freedom from inclusions and to achieve a favourable solidification grain structure, which ultimately improve the hot workability of the alloy steel. Appropriate choice of slag and operating parameters are needed for realising the required ingot quality. The present study would examine the processing and quality aspects of some important grades of steels used in nuclear industry namely ferritic 9Cr-1Mo steel, martensitic stainless steels 403, 410, precipitation hardenable 17-4 PH stainless steel and austenitic 321, 316LN stainless steel, which were made and supplied for applications to Indian nuclear industry. The expertise developed in processing the steels in terms of melting, heat treatment and their relationship to structural features and mechanical properties would be highlighted. (author)

  10. In-service thermal ageing of martensitic stainless steels

    International Nuclear Information System (INIS)

    Tampigny, R.; Molinie, E.; Foct, F.; Dignocourt, P.

    2011-01-01

    Martensitic stainless steels are largely used in Nuclear Power Plants (NPPs) mainly as valve stems, bolts or nuts due to their high mechanical properties and their good resistance to corrosion in primary water. At the end of the eighties, research studies have demonstrated a thermal ageing irreversible embrittlement due to the precipitation of a chromium-rich phase for X6 CrNiCu 17-04, X6 CrNiMo 16.04 and X12 Cr 13 martensitic stainless steels and a semi-empirical modeling has been proposed. Numerous metallurgical examinations have been performed in hot laboratories to consolidate the good correlation between in-service experience and the modeling developed by EDF RD. According to the feedback analysis, thermal ageing embrittlement can appear at different in-service temperatures or do not appear in relation with chemical composition of martensitic stainless steels and end of manufacturing heat treatments associated. A new campaign of metallurgical examinations has been proposed to consolidate previous studies and to contribute to maintenance policy for the next ten years after the third decennial outages for 900 MWe NPP. Influence of real in-service temperatures and end of manufacturing heat treatments have been examined to understand reasons why in some cases thermal ageing embrittlement does not occur or occur with a lowest intensity. These new results have contributed to reinforce EDF RD modeling validity and technical specifications defined in RCC-M for new valve stems, bolts or nuts. (authors)

  11. Plating on stainless steel alloys

    International Nuclear Information System (INIS)

    Dini, J.W.; Johnson, H.R.

    1981-01-01

    Quantitative adhesion data are presented for a variety of electroplated stainless steel type alloys. Results show that excellent adhesion can be obtained by using a Wood's nickel strike or a sulfamate nickel strike prior to final plating. Specimens plated after Wood's nickel striking failed in the deposit rather than at the interface between the substrate and the coating. Flyer plate quantitative tests showed that use of anodic treatment in sulfuric acid prior to Wood's nickel striking even further improved adhesion. In contrast activation of stainless steels by immersion or cathodic treatment in hydrochloric acid resulted in very reduced bond strengths with failure always occurring at the interface between the coating and substrate

  12. INFLUENCE OF MICRO-SEGREGATION IN PB-S-ALLOYED FREE MACHINING STEELS ON THE SURFACE QUALITY OF THE ROLLED WIRE-ROD

    OpenAIRE

    Leuschke, U.; Rajesh Puvvada, N.; Puvvada, Rajesh

    2008-01-01

    Free machining steel billets were manufactured at the continuous casting machine. The manufactured billets did not exhibit any kind of surface defects but surface cracks and slivers appeared when the billets were rolled into wires and rods at the wire-rod mill. The defects on rolled wire-rod have been detected by a hot eddy current system. Further investigations in these defects with the help of microprobe analysis system and scanning electron microscope equipped with image analysis system re...

  13. Microstructure control during twin roll casting of an AZ31 magnesium alloy

    International Nuclear Information System (INIS)

    Huang, Y; Bayandorian, I; Fan, Z

    2012-01-01

    The existing twin roll casting technique for magnesium alloys suffers heterogeneity in both microstructure and chemistry and downstream processing is required to improve the strip quality, resulting in cost rise. In the present work, twin roll casting was carried out using an AZ31 magnesium alloy, with the application of intensive shearing melt conditioning prior to casting. The effect of process parameters such as pouring temperature and casting speed on microstructure control during casting and subsequent downstream processing was studied. Experimental results showed that the melt conditioning treatment allowed the production of AZ31 strips with uniform and refined microstructure free of centreline segregations. It was also shown that an optimized combination of pouring temperature and casting speed, in conjunction with a strip thickness control operation, resulted in uniformly distributed stored energies due to enhanced plastic deformation, which promoted recrystallization during casting and subsequent heat treatment. Strips prepared by twin roll casting and homogenization developed similar microstructural features to those prepared by twin roll casting followed by lengthy downstream processing by homogenization, hot rolling and annealing and displayed a weaker basal texture, exhibiting a potentially better formability.

  14. Secondary recrystallization behavior in a twin-roll cast grain-oriented electrical steel

    Energy Technology Data Exchange (ETDEWEB)

    Song, Hong-Yu; Liu, Hai-Tao, E-mail: liuht@ral.neu.edu.cn; Wang, Yin-Ping; Wang, Guo-Dong

    2017-04-15

    The microstructure and texture evolution along the processing was investigated with a particular focus on the secondary recrystallization behavior in a 0.23 mm-thick twin-roll cast grain-oriented electrical steel. A striking feature is that Goss orientation originated during twin-roll casting as a result of shear deformation and it was further enhanced during hot rolling and normalizing. After primary recrystallization annealing, a homogeneous microstructure associated with a sharp γ-fiber texture was produced. During secondary recrystallization annealing, the γ-fiber texture was first strengthened and weakened with increasing temperature prior to the onset of secondary recrystallization. Goss grains always exhibited more 20–45° misoriented boundaries than the matrix. The matrix was quite stable during secondary recrystallization with the aid of dense inhibitors. Finally, a complete secondary recrystallization microstructure consisting of large Goss grains was produced. The grain boundary characteristics distribution indicated that the high energy model was responsible for the abnormal growth of Goss grains under the present conditions. - Highlights: • A 0.23 mm twin-roll cast grain-oriented silicon steel sheet was produced. • Goss orientation originated during twin-roll casting. • Secondary recrystallization behavior was briefly investigated. • γ-fiber texture was enhanced prior to the onset of secondary recrystallization. • A complete secondary recrystallization microstructure was produced.

  15. Roll forming of eco-friendly stud

    Science.gov (United States)

    Keum, Y. T.; Lee, S. Y.; Lee, T. H.; Sim, J. K.

    2013-12-01

    In order to manufacture an eco-friendly stud, the sheared pattern is designed by the Taguchi method and expanded by the side rolls. The seven geometrical shape of sheared pattern are considered in the structural and thermal analyses to select the best functional one in terms of the durability and fire resistance of dry wall. For optimizing the size of the sheared pattern chosen, the L9 orthogonal array and smaller-the-better characteristics of the Taguchi method are used. As the roll gap causes forming defects when the upper-and-lower roll type is adopted for expanding the sheared pattern, the side roll type is introduced. The stress and strain distributions obtained by the FEM simulation of roll-forming processes are utilized for the design of expanding process. The expanding process by side rolls shortens the length of expanding process and minimizes the cost of dies. Furthermore, the stud manufactured by expanding the sheared pattern of the web is an eco-friend because of the scrapless roll-forming process. In addition, compared to the conventionally roll-formed stud, the material cost is lessened about 13.6% and the weight is lightened about 15.5%.

  16. Pipe Rolling from Continuous Cast Metal

    International Nuclear Information System (INIS)

    Zhordania, I.; Chkhartishvili, I.; Lordkipanidze, J.; Melashvili, Z.; Papava, K.; Khundadze, K.

    2007-01-01

    The approach to manufacturing of high quality pipes as a result of solid and hollow billet rolling from continuous cast metal is shown. Optimal parameters of piercing, temperature of piercing and piercing rolling mill rollers speed have been experimentally established. (author)

  17. Numerical analysis of Swiss roll metamaterials

    International Nuclear Information System (INIS)

    Demetriadou, A; Pendry, J B

    2009-01-01

    A Swiss roll metamaterial is a resonant magnetic medium, with a negative magnetic permeability for a range of frequencies, due to its self-inductance and self-capacitance components. In this paper, we discuss the band structure, S-parameters and effective electromagnetic parameters of Swiss roll metamaterials, with both analytical and numerical results, which show an exceptional convergence.

  18. Efficient Circulation of Railway Rolling Stock

    NARCIS (Netherlands)

    A. Alfieri (Arianna); R. Groot (Rutger); L.G. Kroon (Leo); A. Schrijver (Lex)

    2002-01-01

    textabstractRailway rolling stock (locomotives, carriages, and train units) is one of the most significant cost sources for operatorsof passenger trains, both public and private. Rolling stock costsare due to material acquisition, power supply, and material maintenance. The efficient circulation of

  19. Hot tub folliculitis

    Science.gov (United States)

    ... survives in hot tubs, especially tubs made of wood. Symptoms The first symptom of hot tub folliculitis ... may help prevent the problem. Images Hair follicle anatomy References D'Agata E. Pseudomonas aeruginosa and other ...

  20. Dynamical recrystallization of high purity austenitic stainless steels

    International Nuclear Information System (INIS)

    Gavard, L.

    2001-01-01

    The aim of this work is to optimize the performance of structural materials. The elementary mechanisms (strain hardening and dynamical regeneration, germination and growth of new grains) occurring during the hot working of metals and low pile defect energy alloys have been studied for austenitic stainless steels. In particular, the influence of the main experimental parameters (temperature, deformation velocity, initial grain size, impurities amount, deformation way) on the process of discontinuous dynamical recrystallization has been studied. Alloys with composition equal to those of the industrial stainless steel-304L have been fabricated from ultra-pure iron, chromium and nickel. Tests carried out in hot compression and torsion in order to cover a wide range of deformations, deformation velocities and temperatures for two very different deformation ways have allowed to determine the rheological characteristics (sensitivity to the deformation velocity, apparent activation energy) of materials as well as to characterize their microstructural deformations by optical metallography and electron back-scattered diffraction. The influence of the initial grain size and the influence of the purity of the material on the dynamical recrystallization kinetics have been determined. An analytical model for the determination of the apparent mobility of grain boundaries, a semi-analytical model for the dynamical recrystallization and at last an analytical model for the stationary state of dynamical recrystallization are proposed as well as a new criteria for the transition between the refinement state and the state of grain growth. (O.M.)

  1. Superplastic Forming of Duplex Stainless Steel for Aerospace Part

    Science.gov (United States)

    Lee, Ho-Sung; Yoon, Jong-Hoon; Yoo, Joon-Tae; Yi, Young-Moo

    2011-08-01

    In this study, the high temperature forming behavior of duplex stainless steel has been characterized and the outer shell of a combustion chamber was fabricated with pressure difference of hot gas. It consists of two parts which are the outer skin made of stainless steel to sustain the internal pressure and the inner shell made of copper alloy for regenerative cooling channels. Two outer skins partitioned to half with respect to the symmetric axis was prepared by hot gas forming process with a maximum pressure of 7 MPa following to FEM analysis. For inner layer, copper alloy was machined for cooling channels and then placed in the gas pressure welding fixture. It is shown that the optimum condition of gas pressure welding is 7 MPa at 890 °C, for one hour. EDX analysis and scanning electron microscope micrograph confirm the atomic diffusion process is observed at the interface and copper atoms diffuse into steel, while iron and chrome atoms diffuse into copper. The result shows that the manufacturing method with superplastic forming and gas pressure welding of steel and copper alloy has been successful for near net shape manufacturing of scaled combustion chamber of launch vehicle.

  2. Rolling-element fatigue life of silicon nitride balls. [as compared to that of steel, ceramic, and cermet materials

    Science.gov (United States)

    Parker, R. J.; Zaretsky, E. V.

    1974-01-01

    The five-ball fatigue tester was used to evaluate silicon nitride as a rolling-element bearing material. Results indicate that hot-pressed silicon nitride running against steel may be expected to yield fatigue lives comparable to or greater than those of bearing quality steel running against steel at stress levels typical rolling-element bearing application. The fatigue life of hot-pressed silicon nitride is considerably greater than that of any ceramic or cermet tested. Computer analysis indicates that there is no improvement in the lives of 120-mm-bore angular--contact ball bearings of the same geometry operating at DN values from 2 to 4 million where hot-pressed silicon nitride balls are used in place of steel balls.

  3. Constant-roll (quasi-)linear inflation

    Science.gov (United States)

    Karam, A.; Marzola, L.; Pappas, T.; Racioppi, A.; Tamvakis, K.

    2018-05-01

    In constant-roll inflation, the scalar field that drives the accelerated expansion of the Universe is rolling down its potential at a constant rate. Within this framework, we highlight the relations between the Hubble slow-roll parameters and the potential ones, studying in detail the case of a single-field Coleman-Weinberg model characterised by a non-minimal coupling of the inflaton to gravity. With respect to the exact constant-roll predictions, we find that assuming an approximate slow-roll behaviour yields a difference of Δ r = 0.001 in the tensor-to-scalar ratio prediction. Such a discrepancy is in principle testable by future satellite missions. As for the scalar spectral index ns, we find that the existing 2-σ bound constrains the value of the non-minimal coupling to ξphi ~ 0.29–0.31 in the model under consideration.

  4. Analytical method for establishing indentation rolling resistance

    Directory of Open Access Journals (Sweden)

    Gładysiewicz Lech

    2018-01-01

    Full Text Available Belt conveyors are highly reliable machines able to work in special operating conditions. Harsh environment, long distance of transporting and great mass of transported martials are cause of high energy usage. That is why research in the field of belt conveyor transportation nowadays focuses on reducing the power consumption without lowering their efficiency. In this paper, previous methods for testing rolling resistance are described, and new method designed by authors was presented. New method of testing rolling resistance is quite simple and inexpensive. Moreover it allows to conduct the experimental tests of the impact of different parameters on the value of indentation rolling resistance such as core design, cover thickness, ambient temperature, idler travel frequency, or load value as well. Finally results of tests of relationship between rolling resistance and idler travel frequency and between rolling resistance and idler travel speed was presented.

  5. Analytical method for establishing indentation rolling resistance

    Science.gov (United States)

    Gładysiewicz, Lech; Konieczna, Martyna

    2018-01-01

    Belt conveyors are highly reliable machines able to work in special operating conditions. Harsh environment, long distance of transporting and great mass of transported martials are cause of high energy usage. That is why research in the field of belt conveyor transportation nowadays focuses on reducing the power consumption without lowering their efficiency. In this paper, previous methods for testing rolling resistance are described, and new method designed by authors was presented. New method of testing rolling resistance is quite simple and inexpensive. Moreover it allows to conduct the experimental tests of the impact of different parameters on the value of indentation rolling resistance such as core design, cover thickness, ambient temperature, idler travel frequency, or load value as well. Finally results of tests of relationship between rolling resistance and idler travel frequency and between rolling resistance and idler travel speed was presented.

  6. New perspectives on constant-roll inflation

    Science.gov (United States)

    Cicciarella, Francesco; Mabillard, Joel; Pieroni, Mauro

    2018-01-01

    We study constant-roll inflation using the β-function formalism. We show that the constant rate of the inflaton roll is translated into a first order differential equation for the β-function which can be solved easily. The solutions to this equation correspond to the usual constant-roll models. We then construct, by perturbing these exact solutions, more general classes of models that satisfy the constant-roll equation asymptotically. In the case of an asymptotic power law solution, these corrections naturally provide an end to the inflationary phase. Interestingly, while from a theoretical point of view (in particular in terms of the holographic interpretation) these models are intrinsically different from standard slow-roll inflation, they may have phenomenological predictions in good agreement with present cosmological data.

  7. Sensitization of Laser-beam Welded Martensitic Stainless Steels

    Science.gov (United States)

    Dahmen, Martin; Rajendran, Kousika Dhasanur; Lindner, Stefan

    Ferritic and martensitic stainless steels are an attractive alternative in vehicle production due to their inherent corrosion resistance. By the opportunity of press hardening, their strength can be increased to up to 2000 MPa, making them competitors for unalloyed ultra-high strength steels. Welding, nevertheless, requires special care, especially when it comes to joining of high strength heat treated materials. With an adopted in-line heat treatment of the welds in as-rolled as well as press hardened condition, materials with sufficient fatigue strength and acceptable structural behavior can be produced. Because of microstructural transformations in the base material such as grain coarsening and forced carbide precipitation, the corrosion resistance of the weld zone may be locally impaired. Typically the material in the heat-affected zone becomes sensitive to intergranular cracking in the form of knife-edge corrosion besides the fusion line. The current study comprises of two text scenarios. By an alternating climate test, general response in a corroding environment is screened. In order to understand the corrosion mechanisms and to localize the sensitive zones, sensitisation tests were undertaken. Furthermore, the applicability of a standard test according to ASTM 763-83 was examined. It was found that the alternative climate test does not reveal any corrosion effects. Testing by the oxalic acid test revealed clearly the effect of welding, weld heat treatment and state of thermal processing. Also application of the standard which originally suited for testing ferritic stainless steels could have been justified.

  8. Microstructure Evolution During Creep of Cold Worked Austenitic Stainless Steel

    Science.gov (United States)

    Krishan Yadav, Hari; Ballal, A. R.; Thawre, M. M.; Vijayanand, V. D.

    2018-04-01

    The 14Cr–15Ni austenitic stainless steel (SS) with additions of Ti, Si, and P has been developed for their superior creep strength and better resistance to void swelling during service as nuclear fuel clad and wrapper material. Cold working induces defects such as dislocations that interact with point defects generated by neutron irradiation and facilitates recombination to make the material more resistant to void swelling. In present investigation, creep properties of the SS in mill annealed condition (CW0) and 40 % cold worked (CW4) condition were studied. D9I stainless steel was solution treated at 1333 K for 30 minutes followed by cold rolling. Uniaxial creep tests were performed at 973 K for various stress levels ranging from 175-225 MPa. CW4 samples exhibited better creep resistance as compared to CW0 samples. During creep exposure, cold worked material exhibited phenomena of recovery and recrystallization wherein new strain free grains were observed with lesser dislocation network. In contrast CW0 samples showed no signs of recovery and recrystallization after creep exposure. Partial recrystallization on creep exposure led to higher drop in hardness in cold worked sample as compared to that in mill annealed sample. Accelerated precipitation of carbides at the grain boundaries was observed during creep exposure and this phenomenon was more pronounced in cold worked sample.

  9. Upscaling of polymer solar cell fabrication using full roll-to-roll processing

    DEFF Research Database (Denmark)

    Krebs, Frederik C; Tromholt, Thomas; Jørgensen, Mikkel

    2010-01-01

    factors (excluding bus bars) of 50, 67 and 75% respectively. In addition modules with lengths of 6, 10, 20, 22.5 and 25 cm were explored. The devices were prepared by full roll-to-roll solution processing in a web width of 305 mm and roll lengths of up to 200 m. The devices were encapsulated...... with a barrier material in a full roll-to-roll process using standard adhesives giving the devices excellent stability during storage and operation. The total area of processed polymer solar cell was around 60 m2 per run. The solar cells were characterised using a roll-to-roll system comprising a solar simulator...... to the cost for electricity using existing technologies the levelized cost of electricity (LCOE) is expected to be significantly higher than the existing technologies due to the inferior operational lifetime. The presented devices are thus competitive for consumer electronics but ill-suited for on...

  10. Plasticity of low carbon steel in a hot state

    Energy Technology Data Exchange (ETDEWEB)

    Konovalov, V P; Rizol' , A I; Shram, N N [Ural' skij Nauchno-Issledovatel' skij Inst. Chernykh Metallov, Sverdlovsk (USSR)

    1977-07-01

    The hot ductility (in tapered-specimen piersing test and the in wedge-shaped specimen rolling test) is studied of the Armeo-type low carbon steel produced by vacuum induction and open hearth techniques. The variations of the chemical composition within specified ranges, particularly as regards sulphur, oxygen and the Mn/S ratio, have a marked effect on the processing ductility. The temperature range of brittle fracture and acceptable hot working reductions as functions of the chemical composition have been revealed.

  11. Plasticity of low carbon steel in a hot state

    International Nuclear Information System (INIS)

    Konovalov, V.P.; Rizol', A.I.; Shram, N.N.

    1977-01-01

    The hot ductility (in tapered-specimen piersing test and the in wedge-shaped specimen rolling test) is studied of the Armeo-type low carbon steel produced by vacuum induction and open hearth techniques. The variations of the chemical composition within specified ranges, particularly as regards sulphur, oxygen and the Mn/S ratio, have a marked effect on the processing ductility. The temperature range of brittle fracture and acceptable hot working reductions as functions of the chemical composition have been revealed

  12. Modelling Hot Air Balloons.

    Science.gov (United States)

    Brimicombe, M. W.

    1991-01-01

    A macroscopic way of modeling hot air balloons using a Newtonian approach is presented. Misleading examples using a car tire and the concept of hot air rising are discussed. Pressure gradient changes in the atmosphere are used to explain how hot air balloons work. (KR)

  13. Effect of shot peening on metastable austenitic stainless steels

    Energy Technology Data Exchange (ETDEWEB)

    Fargas, G., E-mail: gemma.fargas@upc.edu [CIEFMA - Departament de Ciència dels Materials i Enginyeria Metallúrgica, Universitat Politècnica de Catalunya, 08028 Barcelona (Spain); CRnE, Centre de Recerca en Nanoenginyeria, Universitat Politècnica de Catalunya, 08028 Barcelona (Spain); Roa, J.J.; Mateo, A. [CIEFMA - Departament de Ciència dels Materials i Enginyeria Metallúrgica, Universitat Politècnica de Catalunya, 08028 Barcelona (Spain); CRnE, Centre de Recerca en Nanoenginyeria, Universitat Politècnica de Catalunya, 08028 Barcelona (Spain)

    2015-08-12

    In this work, shot peening was performed in a metastable austenitic stainless steel EN 1.4318 (AISI 301LN) in order to evaluate its effect on austenite to martensite phase transformation and also the influence on the fatigue limit. Two different steel conditions were considered: annealed, i.e., with a fully austenitic microstructure, and cold rolled, consisting of a mixture of austenite and martensite. X-ray diffraction, electron back-scattered diffraction and focus ion beam, as well as nanoindentation techniques, were used to elucidate deformation mechanisms activated during shot peening and correlate with fatigue response. Results pointed out that extensive plastic deformation and phase transformation developed in annealed specimens as a consequence of shot peening. However, the increase of roughness and the generation of microcracks led to a limited fatigue limit improvement. In contrast, shot peened cold rolled specimens exhibited enhanced fatigue limit. In the latter case, the main factor that determined the influence on the fatigue response was the distance from the injector, followed successively by the exit speed of the shots and the coverage factor.

  14. Corrosion of austenitic stainless steel

    Energy Technology Data Exchange (ETDEWEB)

    Silva, M C.M. [Instituto Nacional de Tecnologia, Rio de Janeiro (Brazil)

    1977-01-01

    Types of corrosion observed in a heat exchanger pipe and on a support of still of molasses fermented wort, both in austenitic stainless steel, are focused. Not only are the causes which might have had any kind of influence on them examined, but also the measures adopted in order to avoid and lessen its occurence.

  15. Phosphate coating on stainless steel 304 sensitized;Recubrimiento fosfatado sobre acero inoxidable 304 sensibilizado

    Energy Technology Data Exchange (ETDEWEB)

    Cruz V, J. P. [IPN, Centro de Investigacion en Ciencia Aplicada y Tecnologia Avanzada, Unidad Altamira, Km. 14.5 Carretera Tampico-Puerto Industrial Altamira, 89600 Altamira, Tamaulipas (Mexico); Vite T, J. [ININ, Carretera Mexico-Toluca s/n, Ocoyoacac 52750, Estado de Mexico (Mexico); Castillo S, M.; Vite T, M., E-mail: jpcruz@ipn.m [IPN, Escuela Superior de Ingenieria Mecanica y Electrica, Seccion de Estudios de Posgrado e Investigacion, Unidad Profesional -Adolfo Lopez Mateos-, Zacatenco, 07738 Mexico, D. F. (Mexico)

    2009-07-01

    The stainless steel 304 can be sensitized when welding processes are applied, that causes the precipitation of chromium carbide in the grain limits, being promoted in this way the formation of galvanic cells and consequently the corrosion process. Using a phosphate coating is possible to retard the physiochemical damages that can to happen in the corrosion process. The stainless steel 304 substrate sensitized it is phosphate to base of Zn-Mn, in a immersion cell very hot. During the process was considered optimization values, for the characterization equipment of X-rays diffraction and scanning electron microscopy was used. The XRD technique confirmed the presence of the phases of manganese phosphate, zinc phosphate, as well as the phase of the stainless steel 304. When increasing the temperature from 60 to 90 C in the immersion process a homogeneous coating is obtained. (Author)

  16. Corrosion behavior of 2205 duplex stainless steel.

    Science.gov (United States)

    Platt, J A; Guzman, A; Zuccari, A; Thornburg, D W; Rhodes, B F; Oshida, Y; Moore, B K

    1997-07-01

    The corrosion of 2205 duplex stainless steel was compared with that of AISI type 316L stainless steel. The 2205 stainless steel is a potential orthodontic bracket material with low nickel content (4 to 6 wt%), whereas the 316L stainless steel (nickel content: 10 to 14 wt%) is a currently used bracket material. Both stainless steels were subjected to electrochemical and immersion (crevice) corrosion tests in 37 degrees C, 0.9 wt% sodium chloride solution. Electrochemical testing indicates that 2205 has a longer passivation range than 316L. The corrosion rate of 2205 was 0.416 MPY (milli-inch per year), whereas 316L exhibited 0.647 MPY. When 2205 was coupled to 316L with equal surface area ratio, the corrosion rate of 2205 reduced to 0.260 MPY, indicating that 316L stainless steel behaved like a sacrificial anode. When 316L is coupled with NiTi, TMA, or stainless steel arch wire and was subjected to the immersion corrosion test, it was found that 316L suffered from crevice corrosion. On the other hand, 2205 stainless steel did not show any localized crevice corrosion, although the surface of 2205 was covered with corrosion products, formed when coupled to NiTi and stainless steel wires. This study indicates that considering corrosion resistance, 2205 duplex stainless steel is an improved alternative to 316L for orthodontic bracket fabrication when used in conjunction with titanium, its alloys, or stainless steel arch wires.

  17. Inflation with a constant rate of roll

    International Nuclear Information System (INIS)

    Motohashi, Hayato; Starobinsky, Alexei A.; Yokoyama, Jun'ichi

    2015-01-01

    We consider an inflationary scenario where the rate of inflaton roll defined by ·· φ/H φ-dot remains constant. The rate of roll is small for slow-roll inflation, while a generic rate of roll leads to the interesting case of 'constant-roll' inflation. We find a general exact solution for the inflaton potential required for such inflaton behaviour. In this model, due to non-slow evolution of background, the would-be decaying mode of linear scalar (curvature) perturbations may not be neglected. It can even grow for some values of the model parameter, while the other mode always remains constant. However, this always occurs for unstable solutions which are not attractors for the given potential. The most interesting particular cases of constant-roll inflation remaining viable with the most recent observational data are quadratic hilltop inflation (with cutoff) and natural inflation (with an additional negative cosmological constant). In these cases even-order slow-roll parameters approach non-negligible constants while the odd ones are asymptotically vanishing in the quasi-de Sitter regime

  18. Design and analysis of roll cage

    Science.gov (United States)

    Angadi, Gurusangappa; Chetan, S.

    2018-04-01

    Wildlife fire fighting vehicles are used to extinguish fires in forests, in this process vehicles face falling objects like rocks, tree branches and other objects. Also due to uneven conditions of the terrain like cliff edges, uneven surfaces etc. makes the vehicle to roll over and these can cause injuries to both the driver and the operator. Roll over of a vehicle is a common incident which makes fatal injuries to the operator and also stands next to the crash accidents. In order to reduce the injury level and continuous roll over of the vehicle it is necessary to equip suitable roll cage according to standards of vehicle. In this present work roll cage for pump operator in wildfire fighting vehicle is designed and analysis is carried out in computer simulated environment when seating position of operator seated outside of the cabin. According to NFPA 1906 standards wildlife fire apparatus, Design and Test procedures that are carried out in Hyperworks maintaining SAE J1194.1983 standards. G load case, roof crush analysis and pendulum impact analysis tests are carried out on roll cage to ensure the saftey of design. These load cases are considerd to satisfy the situation faced in forest terrain. In these test procedures roll cage is analysed for stresses and deformation in various load cases. After recording results these are compared with standards mentioned in SAE J1194.1983.

  19. Cause-specific mortality in Finnish ferrochromium and stainless steel production workers.

    Science.gov (United States)

    Huvinen, M; Pukkala, E

    2016-04-01

    Although stainless steel has been produced for more than a hundred years, exposure-related mortality data for production workers are limited. To describe cause-specific mortality in Finnish ferrochromium and stainless steel workers. We studied Finnish stainless steel production chain workers employed between 1967 and 2004, from chromite mining to cold rolling of stainless steel, divided into sub-cohorts by production units with specific exposure patterns. We obtained causes of death for the years 1971-2012 from Statistics Finland. We calculated standardized mortality ratios (SMRs) as ratios of observed and expected numbers of deaths based on population mortality rates of the same region. Among 8088 workers studied, overall mortality was significantly decreased (SMR 0.77; 95% confidence interval [CI] 0.70-0.84), largely due to low mortality from diseases of the circulatory system (SMR 0.71; 95% CI 0.61-0.81). In chromite mine, stainless steel melting shop and metallurgical laboratory workers, the SMR for circulatory disease was below 0.4 (SMR 0.33; 95% CI 0.07-0.95, SMR 0.22; 95% CI 0.05-0.65 and SMR 0.16; 95% CI 0.00-0.90, respectively). Mortality from accidents (SMR 0.84; 95% CI 0.67-1.04) and suicides (SMR 0.72; 95% CI 0.56-0.91) was also lower than in the reference population. Working in the Finnish ferrochromium and stainless steel industry appears not to be associated with increased mortality. © The Author 2015. Published by Oxford University Press on behalf of the Society of Occupational Medicine.

  20. Inflationary dynamics with a smooth slow-roll to constant-roll era transition

    Energy Technology Data Exchange (ETDEWEB)

    Odintsov, S.D. [ICREA, Passeig Luis Companys, 23, 08010 Barcelona (Spain); Oikonomou, V.K., E-mail: odintsov@ieec.uab.es, E-mail: v.k.oikonomou1979@gmail.com [Laboratory for Theoretical Cosmology, Tomsk State University of Control Systems and Radioelectronics (TUSUR), Lenin Avenue 40, 634050 Tomsk (Russian Federation)

    2017-04-01

    In this paper we investigate the implications of having a varying second slow-roll index on the canonical scalar field inflationary dynamics. We shall be interested in cases that the second slow-roll can take small values and correspondingly large values, for limiting cases of the function that quantifies the variation of the second slow-roll index. As we demonstrate, this can naturally introduce a smooth transition between slow-roll and constant-roll eras. We discuss the theoretical implications of the mechanism we introduce and we use various illustrative examples in order to better understand the new features that the varying second slow-roll index introduces. In the examples we will present, the second slow-roll index has exponential dependence on the scalar field, and in one of these cases, the slow-roll era corresponds to a type of α-attractor inflation. Finally, we briefly discuss how the combination of slow-roll and constant-roll may lead to non-Gaussianities in the primordial perturbations.