WorldWideScience

Sample records for high resolution spectrometers

  1. High-Resolution Mass Spectrometers

    Science.gov (United States)

    Marshall, Alan G.; Hendrickson, Christopher L.

    2008-07-01

    Over the past decade, mass spectrometry has been revolutionized by access to instruments of increasingly high mass-resolving power. For small molecules up to ˜400 Da (e.g., drugs, metabolites, and various natural organic mixtures ranging from foods to petroleum), it is possible to determine elemental compositions (CcHhNnOoSsPp…) of thousands of chemical components simultaneously from accurate mass measurements (the same can be done up to 1000 Da if additional information is included). At higher mass, it becomes possible to identify proteins (including posttranslational modifications) from proteolytic peptides, as well as lipids, glycoconjugates, and other biological components. At even higher mass (˜100,000 Da or higher), it is possible to characterize posttranslational modifications of intact proteins and to map the binding surfaces of large biomolecule complexes. Here we review the principles and techniques of the highest-resolution analytical mass spectrometers (time-of-flight and Fourier transform ion cyclotron resonance and orbitrap mass analyzers) and describe some representative high-resolution applications.

  2. Superconducting High Resolution Fast-Neutron Spectrometers

    Energy Technology Data Exchange (ETDEWEB)

    Hau, Ionel Dragos [Univ. of California, Berkeley, CA (United States)

    2006-01-01

    Superconducting high resolution fast-neutron calorimetric spectrometers based on 6LiF and TiB{sub 2} absorbers have been developed. These novel cryogenic spectrometers measure the temperature rise produced in exothermal (n, α) reactions with fast neutrons in 6Li and 10B-loaded materials with heat capacity C operating at temperatures T close to 0.1 K. Temperature variations on the order of 0.5 mK are measured with a Mo/Cu thin film multilayer operated in the transition region between its superconducting and its normal state. The advantage of calorimetry for high resolution spectroscopy is due to the small phonon excitation energies kBT on the order of μeV that serve as signal carriers, resulting in an energy resolution ΔE ~ (kBT2C)1/2, which can be well below 10 keV. An energy resolution of 5.5 keV has been obtained with a Mo/Cu superconducting sensor and a TiB2 absorber using thermal neutrons from a 252Cf neutron source. This resolution is sufficient to observe the effect of recoil nuclei broadening in neutron spectra, which has been related to the lifetime of the first excited state in 7Li. Fast-neutron spectra obtained with a 6Li-enriched LiF absorber show an energy resolution of 16 keV FWHM, and a response in agreement with the 6Li(n, α)3H reaction cross section and Monte Carlo simulations for energies up to several MeV. The energy resolution of order of a few keV makes this novel instrument applicable to fast-neutron transmission spectroscopy based on the unique elemental signature provided by the neutron absorption and scattering resonances. The optimization of the energy resolution based on analytical and numerical models of the detector response is discussed in the context of these applications.

  3. High resolution solar soft X-ray spectrometer

    Institute of Scientific and Technical Information of China (English)

    ZHANG Fei; WANG Huan-Yu; PENG Wen-Xi; LIANG Xiao-Hua; ZHANG Chun-Lei; CAO Xue-Lei; JIANG Wei-Chun; ZHANG Jia-Yu; CUI Xing-Zhu

    2012-01-01

    A high resolution solar soft X-ray spectrometer (SOX) payload onboard a satellite is developed.A silicon drift detector (SDD) is adopted as the detector of the SOX spectrometer.The spectrometer consists of the detectors and their readout electronics,a data acquisition unit and a payload data handling unit.A ground test system is also developed to test SOX.The test results show that the design goals of the spectrometer system have been achieved.

  4. Workshop on high-resolution, large-acceptance spectrometers

    Energy Technology Data Exchange (ETDEWEB)

    Zeidman, B. (ed.)

    1981-01-01

    The purpose of the Workshop on High-Resolution, Large-Acceptance Spectrometers was to provide a means for exchange of information among those actively engaged in the design and construction of these new spectrometers. Thirty-seven papers were prepared for the data base.

  5. CHIRON – A new high resolution spectrometer for CTIO

    Directory of Open Access Journals (Sweden)

    Marcy G.W.

    2011-07-01

    Full Text Available Small telescopes can play an important role in the search for exoplanets because they offer an opportunity for high cadence observations that are not possible with large aperture telescopes. However, there is a shortage of high resolution spectrometers for precision Doppler planet searches. We report on an innovative design for CHIRON, an inexpensive spectrometer that we are building for the 1.5-m telescope at CTIO in Chile. The resolution will be R >80.000, the spectral format spanning 410 to 880 nm. The total throughput of the telescope and spectrometer will be better than 12%, comparable with the efficiency of state-of-the-art spectrometers. The design is driven by the requirements for precision Doppler searches for exoplanets using an iodine cell. The optical layout is a classical echelle with 140 mm beam size. The bench-mounted spectrometer will be fibre-fed followed by an image slicer. An apochromatic refractor is used as the camera. Image quality and throughput of the design are excellent over the full spectral range. Extensive use of commercially available components and avoidance of complicated custom optics are key for quick and resource-efficient implementation.

  6. High resolution ultraviolet imaging spectrometer for latent image analysis.

    Science.gov (United States)

    Lyu, Hang; Liao, Ningfang; Li, Hongsong; Wu, Wenmin

    2016-03-21

    In this work, we present a close-range ultraviolet imaging spectrometer with high spatial resolution, and reasonably high spectral resolution. As the transmissive optical components cause chromatic aberration in the ultraviolet (UV) spectral range, an all-reflective imaging scheme is introduced to promote the image quality. The proposed instrument consists of an oscillating mirror, a Cassegrain objective, a Michelson structure, an Offner relay, and a UV enhanced CCD. The finished spectrometer has a spatial resolution of 29.30μm on the target plane; the spectral scope covers both near and middle UV band; and can obtain approximately 100 wavelength samples over the range of 240~370nm. The control computer coordinates all the components of the instrument and enables capturing a series of images, which can be reconstructed into an interferogram datacube. The datacube can be converted into a spectrum datacube, which contains spectral information of each pixel with many wavelength samples. A spectral calibration is carried out by using a high pressure mercury discharge lamp. A test run demonstrated that this interferometric configuration can obtain high resolution spectrum datacube. The pattern recognition algorithm is introduced to analyze the datacube and distinguish the latent traces from the base materials. This design is particularly good at identifying the latent traces in the application field of forensic imaging.

  7. A high resolution, low background fast neutron spectrometer

    CERN Document Server

    Abdurashitov, J N; Kalikhov, A V; Matushko, V L; Shikhin, A A; Yants, V E; Zaborskaia, O S; Adams, J M; Nico, J S; Thompson, A K

    2002-01-01

    We discuss the possibility to create a spectrometer of full absorption based on liquid scintillator doped with enriched sup 6 Li. Of specific interest, the spectrometer will have energy resolution estimated to lie in the range 5-10% for 14 MeV neutrons. It will be sensitive to fluxes from 10 sup - sup 4 to 10 sup 6 cm sup - sup 2 s sup - sup 1 above a threshold of 1 MeV in a gamma-background of up to 10 sup 4 s sup - sup 1. The detector's efficiency will be determined by the volume of the scintillator only (approx 3 l) and is estimated to be 0.2-10%. The main reason for the poor resolution of an organic scintillator based spectrometer of full absorption is a non-linear light-yield of the scintillator for recoil protons. The neutron energy is occasionally distributed among recoil protons, and due to non-linear light-yield the total amount of light from all recoil protons ambiguously determines the initial neutron energy. The high-energy resolution will be achieved by compensation of the non-linear light-yield ...

  8. High-resolution wide-band Fast Fourier Transform spectrometers

    CERN Document Server

    Klein, Bernd; Krämer, Ingo; Bell, Andreas; Meyer, Klaus; Güsten, Rolf

    2012-01-01

    We describe the performance of our latest generations of sensitive wide-band high-resolution digital Fast Fourier Transform Spectrometer (FFTS). Their design, optimized for a wide range of radio astronomical applications, is presented. Developed for operation with the GREAT far infrared heterodyne spectrometer on-board SOFIA, the eXtended bandwidth FFTS (XFFTS) offers a high instantaneous bandwidth of 2.5 GHz with 88.5 kHz spectral resolution and has been in routine operation during SOFIA's Basic Science since July 2011. We discuss the advanced field programmable gate array (FPGA) signal processing pipeline, with an optimized multi-tap polyphase filter bank algorithm that provides a nearly loss-less time-to-frequency data conversion with significantly reduced frequency scallop and fast sidelobe fall-off. Our digital spectrometers have been proven to be extremely reliable and robust, even under the harsh environmental conditions of an airborne observatory, with Allan-variance stability times of several 1000 se...

  9. Development and Characterization of a High Resolution Portable Gamma Spectrometer

    Science.gov (United States)

    Ali, Muhammad

    The recent disaster of Fukushima in Japan combined with the high demand to enhance nuclear safety and to minimize personal exposure to radioactive materials has a significant impact on research and development of radiation detection instrumentation. Currently, there is ample effort worldwide in the pursuit of radiation detection to maximize the accuracy and meet international standards in terms of size and specifications to enable radiation protection decision making. Among the requirements is the development of a portable, light-weight gamma-ray isotope identifier to be used by first responders in nuclear accidents as well as for radiation security and identification of illicit material isotopes. From nuclear security perspective, research into advanced screening technologies has become a high priority in all aspects, while for occupational safety, and environmental radiation protection, the regulatory authorities are requiring specific performance of radiation detection and measuring devices. At the applied radiation laboratory of the University of Ontario Institute of Technology, UOIT, the development of a high resolution spectrometer for medium and high energy gamma ray has been conducted. The spectrometer used a newly developed scintillator based on a LaBr3(Ce) crystal. The detector has been modeled using advanced Monte Carlo code (MCNP/X code) for the response function simulation and parameter characterization. The simulation results have been validated by experimental investigations using a wide range of gamma radiation energies. The developed spectrometer has been characterized in terms of resolution and response in different fields. It has also been compared with other crystals such as NaI(TI) and LiI(Eu).

  10. A high-resolution Fourier Transform Spectrometer for planetary spectroscopy

    Science.gov (United States)

    Cruikshank, D. P.; Sinton, W. M.

    1973-01-01

    The employment of a high-resolution Fourier Transform Spectrometer (FTS) is described for planetary and other astronomical spectroscopy in conjunction with the 88-inch telescope at Mauna Kea Observatory. The FTS system is designed for a broad range of uses, including double-beam laboratory spectroscopy, infrared gas chromatography, and nuclear magnetic resonance spectroscopy. The data system is well-suited to astronomical applications because of its great speed in acquiring and transforming data, and because of the enormous storage capability of the magnetic tape unit supplied with the system. The basic instrument is outlined 2nd some of the initial results from the first attempted use on the Mauna Kea 88-inch telescope are reported.

  11. Progress Toward A Very High Angular Resolution Imaging Spectrometer (VERIS)

    Science.gov (United States)

    Korendyke, Clarence M.; Vourlidas, A.; Landi, E.; Seely, J.; Klimchuck, J.

    2007-07-01

    Recent imaging at arcsecond (TRACE) and sub-arcsecond (VAULT) spatial resolution clearly show that structures with fine spatial scales play a key role in the physics of the upper solar atmosphere. Both theoretical and observational considerations point to the importance of small spatial scales, impulsive energy release, strong dynamics, and extreme plasma nonuniformity. Fundamental questions regarding the nature, structure, properties and dynamics of loops and filamentary structures in the upper atmosphere have been raised. To address these questions, we are developing a next generation, VEry high angular Resolution Imaging Spectrometer (VERIS) as a sounding rocket instrument. VERIS will obtain the necessary high spatial resolution, high fidelity measurements of plasma temperatures, densities and velocities. With broad simultaneous temperature coverage, the VERIS observations will directly address unresolved issues relating to interconnections of various temperature solar plasmas. VERIS will provide the first ever subarcsecond spectra of transition region and coronal structures. It will do so with a sufficient spectral resolution of to allow centroided Doppler velocity determinations to better than 3 km/s. VERIS uses a novel two element, normal incidence optical design with highly reflective EUV coatings to access a spectral range with broad temperature coverage (0.03-15 MK) and density-sensitive line ratios. Finally, in addition to the spectra, VERIS will simultaneously obtain spectrally pure slot images (10x150 arcsec) in the +/-1 grating orders, which can be combined to make instantaneous line-of-sight velocity maps with 8km/s accuracy over an unprecedented field of view. The VERIS program is beginning the second year of its three year development cycle. All design activities and reviews are complete. Fabrication of all major components has begun. Brassboard electronics cards have been fabricated, assembled and tested. The paper presents the essential scientific

  12. Soft x-ray spectrometer (SXS): the high-resolution cryogenic spectrometer onboard ASTRO-H

    Science.gov (United States)

    Mitsuda, Kazuhisa; Kelley, Richard L.; Akamatsu, Hiroki; Bialas, Thomas; Boyce, Kevin R.; Brown, Gregory V.; Canavan, Edgar; Chiao, Meng; Costantini, Elisa; den Herder, Jan-Willem; de Vries, Cor; DiPirro, Michael J.; Eckart, Megan E.; Ezoe, Yuichiro; Fujimoto, Ryuichi; Haas, Daniel; Hoshino, Akio; Ishikawa, Kumi; Ishisaki, Yoshitaka; Iyomoto, Naoko; Kilbourne, Caroline A.; Kimball, Mark; Kitamoto, Shunji; Konami, Saori; Leutenegger, Maurice A.; McCammon, Dan; Miko, Joseph; Mitsuishi, Ikuyuki; Murakami, Hiroshi; Murakami, Masahide; Noda, Hirofumi; Ogawa, Mina; Ohashi, Takaya; Okamoto, Atsushi; Ota, Naomi; Paltani, Stéphane; Porter, F. Scott; Sato, Kosuke; Sato, Yoichi; Sawada, Makoto; Seta, Hiromi; Shinozaki, Keisuke; Shirron, Peter J.; Sneiderman, Gary A.; Sugita, Hiroyuki; Szymkowiak, Andrew; Takei, Yoh; Tamagawa, Toru; Tashiro, Makoto S.; Terada, Yukikatsu; Tsujimoto, Masahiro; Yamada, Shinya; Yamasaki, Noriko Y.

    2014-07-01

    We present the development status of the Soft X-ray Spectrometer (SXS) onboard the ASTRO-H mission. The SXS provides the capability of high energy-resolution X-ray spectroscopy of a FWHM energy resolution of operated at 50 mK. The SXS microcalorimeter subsystem is being developed in an EM-FM approach. The EM SXS cryostat was developed and fully tested and, although the design was generally confirmed, several anomalies and problems were found. Among them is the interference of the detector with the micro-vibrations from the mechanical coolers, which is the most difficult one to solve. We have pursued three different countermeasures and two of them seem to be effective. So far we have obtained energy resolutions satisfying the requirement with the FM cryostat.

  13. The spectrometer of the High-Resolution Multi position Thomson Scattering Diagnostic for TJ-II

    Energy Technology Data Exchange (ETDEWEB)

    Herranz, J.; Barth, C.J.; Castejon, F.; Lopez-Sanchez, A.; Mirones, E.; Pastor, I.; Perez, D.; Rodriguez, C.

    2001-07-01

    Since 1998, a high-resolution multiposition thompson scattering system is in operation at the stellarator TJ-II, combining high accuracy and excellent spatial resolution. A description of the diagnostic spectrometer is presented. The main characteristics of the spectrometer that allow YJ-II Thomson scattering diagnostic to have high spatial and spectral resolution are described in this paper. (Author)

  14. A high-resolution Fourier-transform infrared spectrometer.

    Science.gov (United States)

    Johnson, H. L.; Forbes, F. F.; Thompson, R. I.; Steinmetz , D. L.; Harris, O.

    1973-01-01

    We have developed a Fourier-transform infrared spectrometer having a resolution of 0.5/cm over the range of wavelength from 1 to 5.5 microns. It has been used to observe the sun over this wavelength range from a Lear Jet flying at an altitude of 14 km, and to observe a number of stars from the ground, using the 229-cm telescope of the Steward Observatory and the 152-cm aluminum-mirror telescope at the Observatorio Astronomico Nacional in the Sierra de San Pedro Martir, Baja California, Mexico. The solar spectrum is given here, while the ground-based spectra are being published separately.

  15. Superconducting High Energy Resolution Gamma-ray Spectrometers

    Energy Technology Data Exchange (ETDEWEB)

    Chow, D T

    2002-02-22

    We have demonstrated that a bulk absorber coupled to a TES can serve as a good gamma-ray spectrometer. Our measured energy resolution of 70 eV at 60 keV is among the best measurements in this field. We have also shown excellent agreement between the noise predictions and measured noise. Despite this good result, we noted that our detector design has shortcomings with a low count rate and vulnerabilities with the linearity of energy response. We addressed these issues by implementation of an active negative feedback bias. We demonstrated the effects of active bias such as additional pulse shortening, reduction of TES change in temperature during a pulse, and linearization of energy response at low energy. Linearization at higher energy is possible with optimized heat capacities and thermal conductivities of the microcalorimeter. However, the current fabrication process has low control and repeatability over the thermal properties. Thus, optimization of the detector performance is difficult until the fabrication process is improved. Currently, several efforts are underway to better control the fabrication of our gamma-ray spectrometers. We are developing a full-wafer process to produce TES films. We are investigating the thermal conductivity and surface roughness of thicker SiN membranes. We are exploring alternative methods to couple the absorber to the TES film for reproducibility. We are also optimizing the thermal conductivities within the detector to minimize two-element phonon noise. We are experimenting with different absorber materials to optimize absorption efficiency and heat capacity. We are also working on minimizing Johnson noise from the E S shunt and SQUID amplifier noise. We have shown that our performance, noise, and active bias models agree very well with measured data from several microcalorimeters. Once the fabrication improvements have been implemented, we have no doubt that our gamma-ray spectrometer will achieve even more spectacular results.

  16. An Overview of High-Resolution, Non-Dispersive, Imaging Spectrometers for High-Energy Photons

    Science.gov (United States)

    Kilbourne, Caroline

    2010-01-01

    High-resolution x-ray spectroscopy has become a powerful tool for studying the evolving universe. The grating spectrometers on the XMM and Chandra satellites initiated a new era in x-ray astronomy. Despite their successes, there is still need for instrumentation that can provide higher spectral resolution with high throughput in the Fe-K band and for extended sources. What is needed is a non-dispersive imaging spectrometer - essentially a 14-bit x-ray color camera. And a requirement for a nondispersive spectrometer designed to provide eV-scale spectral resolution is a temperature below 0.1 K. The required spectral resolution and the constraints of thermodynamics and engineering dictate the temperature regime nearly independently of the details of the sensor or the read-out technology. Low-temperature spectrometers can be divided into two classes - - equilibrium and non-equilibrium. In the equilibrium devices, or calorimeters, the energy is deposited in an isolated thermal mass and the resulting increase in temperature is measured. In the non-equilibrium devices, the absorbed energy produces quantized excitations that are counted to determine the energy. The two approaches have different strong points, and within each class a variety of optimizations have been pursued. I will present the basic fundamentals of operation and the details of the most successful device designs to date. I will also discuss how the measurement priorities (resolution, energy band, count rate) influence the optimal choice of detector technology.

  17. A High Resolution Fourier-Transform Spectrometer for the Measurement of Atmospheric Column Abundances

    Science.gov (United States)

    Cageao, R.; Sander, S.; Blavier, J.; Jiang, Y.; Nemtchinov, V.

    2000-01-01

    A compact, high resolution Fourier-transform spectrometer for atmospheric near ultraviolet spectroscopy has been installed at the Jet Propulsion Laboratory's Table Mountain Facility (34.4N, 117.7 W, elevation 2290m).

  18. High Resolution Stellar Spectroscopy with VBT Echelle Spectrometer

    Indian Academy of Sciences (India)

    N. Kameswara Rao; S. Sriram; K. Jayakumar; F. Gabriel

    2005-06-01

    The optical design and performance of the recently commissioned fiber fed echelle spectrometer of 2.34 meter Vainu Bappu Telescope are described. The use of it for stellar spectroscopic studies is discussed.

  19. Optical alignment of high resolution Fourier transform spectrometers

    Science.gov (United States)

    Breckinridge, J. B.; Ocallaghan, F. G.; Cassie, A. G.

    1980-01-01

    Remote sensing, high resolution FTS instruments often contain three primary optical subsystems: Fore-Optics, Interferometer Optics, and Post, or Detector Optics. We discuss the alignment of a double-pass FTS containing a cat's-eye retro-reflector. Also, the alignment of fore-optics containing confocal paraboloids with a reflecting field stop which relays a field image onto a camera is discussed.

  20. Compact high-resolution micro-spectrometer on chip: spectral calibration and first spectrum

    Science.gov (United States)

    Diard, Thomas; de la Barrière, Florence; Ferrec, Yann; Guérineau, Nicolas; Rommeluère, Sylvain; Le Coarer, Etienne; Martin, Guillermo

    2016-05-01

    Compact and hand-held spectrometers may be very interesting for the measurement of spectral signatures of chemicals or objects. To achieve this goal, ONERA and IPAG have developed a new on chip Fourier Transform Spectrometer operating in the visible spectral range with a high spectral resolution (near 2 cm-1), named visible HR SPOC (visible High Resolution Spectrometer On Chip). It is directly inspired from the MICROSPOC infrared spectrometer, studied at ONERA in the past years. This spectrometer is made of a stair-step two-wave interferometer directly glued on a CMOS detector making it a very compact prototype. After calibrating the optical path difference, measurements of experimental spectra are presented.

  1. A magnetic-free high-resolution parabolic mirror time-of-flight electron energy spectrometer

    Institute of Scientific and Technical Information of China (English)

    张戈; 沈鸿元; 曾瑞荣; 黄呈辉; 林文雄; 黄见洪

    2001-01-01

    The principle and structure of a magnetic-free high-resolution high-efficiency parabolic mirror time-offligght electron energy spectrometer are presented. The electron energy spectrum of Nz in a flight tube is measured using a 105 fs Ti:sappbire laser under different gas pressures.

  2. R×B drift momentum spectrometer with high resolution and large phase space acceptance.

    Science.gov (United States)

    Wang, X; Konrad, G; Abele, H

    2013-02-11

    We propose a new type of momentum spectrometer, which uses the R×B drift effect to disperse the charged particles in a uniformly curved magnetic field, and measures the particles with large phase space acceptance and high resolution. This kind of R×B spectrometer is designed for the momentum analyses of the decay electrons and protons in the PERC (Proton and Electron Radiation Channel) beam station, which provides a strong magnetic field to guide the charged particles in the instrument. Instead of eliminating the guiding field, the R×B spectrometer evolves the field gradually to the analysing field, and the charged particles can be adiabatically transported during the dispersion and detection. The drifts of the particles have similar properties as their dispersion in the normal magnetic spectrometer. Besides, the R×B spectrometer is especially ideal for the measurements of particles with low momenta and large incident angles. We present a design of the R×B spectrometer, which can be used in PERC. For the particles with solid angle smaller than 88 msr, the maximum aberration is below 10(-4). The resolution of the momentum spectra can reach 14.4 keV/c, if the particle position measurements have a resolution of 1 mm.

  3. The Joint Astrophysical Plasmadynamic Experiment (J-PEX): a high-resolution rocket spectrometer

    Science.gov (United States)

    Barstow, Martin A.; Bannister, Nigel P.; Cruddace, Raymond G.; Kowalski, Michael P.; Wood, Kent S.; Yentis, Daryl J.; Gursky, Herbert; Barbee, Troy W., Jr.; Goldstein, William H.; Kordas, Joseph F.; Fritz, Gilbert G.; Culhane, J. Leonard; Lapington, Jonathan S.

    2003-02-01

    We report on the successful sounding rocket flight of the high resolution (R=3000-4000) J-PEX EUV spectrometer. J-PEX is a novel normal incidence instrument, which combines the focusing and dispersive elements of the spectrometer into a single optical element, a multilayer-coated grating. The high spectral resolution achieved has had to be matched by unprecedented high spatial resolution in the imaging microchannel plate detector used to record the data. We illustrate the performance of the complete instrument through an analysis of the 220-245Å spectrum of the white dwarf G191-B2B obtained with a 300 second exposure. The high resolution allows us to detect a low-density ionized helium component along the line of sight to the star and individual absorption lines from heavier elements in the photosphere.

  4. The Joint astrophysical Plasmadynamic EXperiment (J-PEX) A high-resolution rocket spectrometer

    CERN Document Server

    Barstow, M A; Cruddace, R G; Kowalski, M; Wood, K S; Yentis, D J; Gursky, H; Barbee, T W; Goldstein, W H; Kordas, J F; Fritz, G G; Culhane, J L; Lapingtone, J S

    2002-01-01

    We report on the successful sounding rocket flight of the high resolution (R=3000-4000) J-PEX EUV spectrometer. J-PEX is a novel normal incidence instrument, which combines the focusing and dispersive elements of the spectrometer into a single optical element, a multilayer-coated grating. The high spectral resolution achieved has had to be matched by unprecedented high spatial resolution in the imaging microchannel plate detector used to record the data. We illustrate the performance of the complete instrument through an analysis of the 220-245A spectrum of the white dwarf G191-B2B obtained with a 300 second exposure. The high resolution allows us to detect a low-density ionized helium component along the line of sight to the star and individual absorption lines from heavier elements in the photosphere.

  5. Design and performance of AERHA, a high acceptance high resolution soft x-ray spectrometer

    Energy Technology Data Exchange (ETDEWEB)

    Chiuzbăian, Sorin G., E-mail: gheorghe.chiuzbaian@upmc.fr; Hague, Coryn F.; Brignolo, Stefania; Baumier, Cédric; Lüning, Jan [Sorbonne Universités, UPMC Univ Paris 06, UMR 7614, Laboratoire de Chimie Physique-Matière et Rayonnement, 11 rue Pierre et Marie Curie, F-75005 Paris (France); CNRS, UMR 7614, Laboratoire de Chimie Physique-Matière et Rayonnement, 11 rue Pierre et Marie Curie, F-75005 Paris (France); Synchrotron SOLEIL, L’Orme des Merisiers, Saint-Aubin, B.P. 48, F-91192 Gif-sur-Yvette (France); Avila, Antoine; Delaunay, Renaud; Mariot, Jean-Michel [Sorbonne Universités, UPMC Univ Paris 06, UMR 7614, Laboratoire de Chimie Physique-Matière et Rayonnement, 11 rue Pierre et Marie Curie, F-75005 Paris (France); CNRS, UMR 7614, Laboratoire de Chimie Physique-Matière et Rayonnement, 11 rue Pierre et Marie Curie, F-75005 Paris (France); Jaouen, Nicolas; Polack, François; Thomasset, Muriel; Lagarde, Bruno; Nicolaou, Alessandro [Synchrotron SOLEIL, L’Orme des Merisiers, Saint-Aubin, B.P. 48, F-91192 Gif-sur-Yvette (France); Sacchi, Maurizio [Synchrotron SOLEIL, L’Orme des Merisiers, Saint-Aubin, B.P. 48, F-91192 Gif-sur-Yvette (France); Sorbonne Universités, UPMC Univ Paris 06, UMR 7588, Institut des NanoSciences de Paris, 4 place Jussieu, F-75252 Paris Cedex 05 (France); CNRS, UMR 7588, Institut des NanoSciences de Paris, 4 place Jussieu, F-75252 Paris Cedex 05 (France)

    2014-04-15

    A soft x-ray spectrometer based on the use of an elliptical focusing mirror and a plane varied line spacing grating is described. It achieves both high resolution and high overall efficiency while remaining relatively compact. The instrument is dedicated to resonant inelastic x-ray scattering studies. We set out how this optical arrangement was judged best able to guarantee performance for the 50 − 1000 eV range within achievable fabrication targets. The AERHA (adjustable energy resolution high acceptance) spectrometer operates with an effective angular acceptance between 100 and 250 μsr (energy dependent) and a resolving power well in excess of 5000 according to the Rayleigh criterion. The high angular acceptance is obtained by means of a collecting pre-mirror. Three scattering geometries are available to enable momentum dependent measurements with 135°, 90°, and 50° scattering angles. The instrument operates on the Synchrotron SOLEIL SEXTANTS beamline which serves as a high photon flux 2 × 200 μm{sup 2} focal spot source with full polarization control.

  6. The High Time Resolution Spectrometer (HTRS) aboard the International X-ray Observatory (IXO)

    NARCIS (Netherlands)

    Barret, Didier; Ravera, Laurent; Bodin, Pierre; Amoros, Carine; Boutelier, Martin; Glorian, Jean-Michel; Godet, Olivier; Orttner, Guillaume; Lacombe, Karine; Pons, Roger; Rambaud, Damien; Ramon, Pascale; Ramchoun, Souad; Biffi, Jean-Marc; Belasic, Marielle; Clédassou, Rodolphe; Faye, Delphine; Pouilloux, Benjamin; Motch, Christian; Michel, Laurent; Lechner, Peter H.; Niculae, Adrian; Strueder, Lothar W.; Distratis, Giuseppe; Kendziorra, Eckhard; Santangelo, Andréa; Tenzer, Christoph; Wende, Henning; Wilms, Joern; Kreykenbohm, Ingo; Schmid, Christian; Paltani, Stéphane; Cadoux, Franck; Fiorini, Carlo; Bombelli, Luca; Méndez, Mariano; Mereghetti, Sandro

    2010-01-01

    The High Time Resolution Spectrometer (HTRS) is one of the five focal plane instruments of the International X-ray Observatory (IXO). The HTRS is the only instrument matching the top level mission requirement of handling a one Crab X-ray source with an efficiency greater than 10%. It will provide IX

  7. Study of high resolution x-ray spectrometer concepts for NIF experiments

    Science.gov (United States)

    Hill, K. W.; Bitter, M.; Delgado-Aparicio, L.; Efthimion, P.; Gao, L.; Maddox, J.; Pablant, N. A.; Beiersdorfer, P.; Chen, H.; Coppari, F.; Ma, T.; Nora, R.; Scott, H.; Schneider, M.; Mancini, R.

    2015-11-01

    Options have been investigated for DIM-insertable (Diagnostic Instrument Manipulator) high resolution (E/ ΔE ~ 3000 - 5000) Bragg crystal x-ray spectrometers for experiments on the NIF. Of interest are time integrated Cu K- and Ta L-edge absorption spectra and time resolved Kr He- β emission from compressed symcaps for inference of electron temperature from dielectronic satellites and electron density from Stark broadening. Cylindrical and conical von Hamos, Johann, and advanced high throughput designs have been studied. Predicted x-ray intensities, spectrometer throughputs, spectral resolution, and spatial focusing properties, as well as lab evaluations of some spectrometer candidates will be presented. Performed under the auspices of the US DOE by PPPL under contract DE-AC02-09CH11466 and by LLNL under contract DE-AC52-07NA27344.

  8. High-resolution Laue-type DuMond curved crystal spectrometer.

    Science.gov (United States)

    Szlachetko, M; Berset, M; Dousse, J-Cl; Hoszowska, J; Szlachetko, J

    2013-09-01

    We report on a high-resolution transmission-type curved crystal spectrometer based on the modified DuMond slit geometry. The spectrometer was developed at the University of Fribourg for the study of photoinduced X-ray spectra. K and L X-ray transitions with energies above about 10 keV can be measured with an instrumental resolution comparable to their natural linewidths. Construction details and operational characteristics of the spectrometer are presented. The variation of the energy resolution as a function of the focal distance and diffraction order is discussed. The high sensitivity of the spectrometer is demonstrated via the 2s-1s dipole-forbidden X-ray transition of Gd which could be observed despite its extremely low intensity. The precision of the instrument is illustrated by comparing the sum of the energies of the Au K-L2 and L2-M3 cascading transitions with the energy of the crossover K-M3 transition as well as by considering the energy differences of the Gd Kα1 X-ray line measured at five different diffraction orders. Finally, to demonstrate the versatility of the spectrometer, it is shown that the latter can also be used for in-house extended X-ray absorption fine structure measurements.

  9. High energy resolution characteristics on 14MeV neutron spectrometer for fusion experimental reactor

    Energy Technology Data Exchange (ETDEWEB)

    Iguchi, Tetsuo [Tokyo Univ., Tokai, Ibaraki (Japan). Nuclear Engineering Research Lab.; Takada, Eiji; Nakazawa, Masaharu

    1996-10-01

    A 14MeV neutron spectrometer suitable for an ITER-like fusion experimental reactor is now under development on the basis of a recoil proton counter telescope principle in oblique scattering geometry. To verify its high energy resolution characteristics, preliminary experiments are made for a prototypical detector system. The comparison results show reasonably good agreement and demonstrate the possibility of energy resolution of 2.5% in full width at half maximum for 14MeV neutron spectrometry. (author)

  10. Lineshape spectroscopy with a very high resolution, very high signal-to-noise crystal spectrometer

    Energy Technology Data Exchange (ETDEWEB)

    Beiersdorfer, P.; Magee, E. W.; Brown, G. V.; Chen, H.; Emig, J. [Lawrence Livermore National Laboratory, Livermore, California 94550 (United States); Hell, N. [Lawrence Livermore National Laboratory, Livermore, California 94550 (United States); Dr. Remeis-Sternwarte & ECAP, Universität Erlangen-Nürnberg, 96049 Bamberg (Germany); Bitter, M.; Hill, K. W. [Princeton Plasma Physics Laboratory, Princeton, New Jersey 08543 (United States); Allan, P.; Brown, C. R. D.; Hill, M. P.; Hoarty, D. J.; Hobbs, L. M. R.; James, S. F. [Directorate of Research and Applied Science, AWE plc, Reading RG7 4PR (United Kingdom)

    2016-06-15

    We have developed a high-resolution x-ray spectrometer for measuring the shapes of spectral lines produced from laser-irradiated targets on the Orion laser facility. The instrument utilizes a spherically bent crystal geometry to spatially focus and spectrally analyze photons from foil or microdot targets. The high photon collection efficiency resulting from its imaging properties allows the instrument to be mounted outside the Orion chamber, where it is far less sensitive to particles, hard x-rays, or electromagnetic pulses than instruments housed close to the target chamber center in ten-inch manipulators. Moreover, Bragg angles above 50° are possible, which provide greatly improved spectral resolution compared to radially viewing, near grazing-incidence crystal spectrometers. These properties make the new instrument an ideal lineshape diagnostic for determining plasma temperature and density. We describe its calibration on the Livermore electron beam ion trap facility and present spectral data of the K-shell emission from highly charged sulfur produced by long-pulse as well as short-pulse beams on the Orion laser in the United Kingdom.

  11. SHARAQ spectrometer for high-resolution studies for RI-induced reactions

    Energy Technology Data Exchange (ETDEWEB)

    Michimasa, S., E-mail: mitimasa@cns.s.u-tokyo.ac.jp [Center for Nuclear Study, University of Tokyo, RIKEN Campus, Wako, Saitama 351-0198 (Japan); Takaki, M.; Sasamoto, Y. [Center for Nuclear Study, University of Tokyo, RIKEN Campus, Wako, Saitama 351-0198 (Japan); Dozono, M. [RIKEN Nishina Center, Wako, Saitama 351-0198 (Japan); Nishi, T. [Department of Physics, University of Tokyo, Bunkyo, Tokyo 113-0033 (Japan); Kawabata, T. [Department of Physics, Kyoto University, Kyoto, Kyoto 606-8502 (Japan); Ota, S. [Center for Nuclear Study, University of Tokyo, RIKEN Campus, Wako, Saitama 351-0198 (Japan); Baba, H. [RIKEN Nishina Center, Wako, Saitama 351-0198 (Japan); Baba, T. [Department of Physics, Kyoto University, Kyoto, Kyoto 606-8502 (Japan); Fujii, T.; Go, S.; Kawase, S.; Kikuchi, Y.; Kisamori, K.; Kobayashi, M.; Kubota, Y.; Lee, C.S. [Center for Nuclear Study, University of Tokyo, RIKEN Campus, Wako, Saitama 351-0198 (Japan); Matsubara, H. [RIKEN Nishina Center, Wako, Saitama 351-0198 (Japan); Miki, K. [RCNP, Osaka University, Ibaraki, Osaka 567-0047 (Japan); Miya, H. [Center for Nuclear Study, University of Tokyo, RIKEN Campus, Wako, Saitama 351-0198 (Japan); and others

    2013-12-15

    Highlights: • Report on recent achievement of the SHARAQ spectrometer. • Demonstration of two ion optics modes for high-resolution spectroscopy. • Discussion on measured transport matrix elements by comparison with designed values. • Demonstration of event-by-event momentum tagging by the achromatic transport. • Achievement of momentum resolution of 1/8100 by the dispersion-matching transport. -- Abstract: The SHARAQ spectrometer and High-Resolution Beamline, which began operation in March 2009, have been put into use for six experiments using charge exchange reactions with radioactive isotope beams. For experiments at SHARAQ, detector developments and ion optics studies continue to improve performance in high-resolution nuclear spectroscopy. We have introduced improved timing resolution with CVD diamond detectors, high count-rate beamline tracking detectors and development of multi-particle detection by cathode-readout drift chambers. Ion-optics studies for the high-resolution achromatic (HA) and dispersion-matching (DM) transport modes are also reported here. Momentum tagging in the HA mode demonstrated an improvement in spectroscopic resolution with respect to the momentum spread of the radioactive beam. For the DM transportation mode, a momentum resolution of 1/8100 (FWHM) was achieved by taking into account the positions and angles of the beam at the third focal plane of BigRIPS.

  12. Monte-Carlo simulation of a high-resolution inverse geometry spectrometer on the SNS. Long Wavelength Target Station

    Energy Technology Data Exchange (ETDEWEB)

    Bordallo, H.N. [Intense Pulsed Neutron Source, Argonne National Laboratory, Argonne, IL (United States); Herwig, K.W. [Spallation Neutron Source, Oak Ridge National Laboratory, Oak Ridge, TN (United States)

    2001-03-01

    Using the Monte-Carlo simulation program McStas, we present the design principles of the proposed high-resolution inverse geometry spectrometer on the SNS-Long Wavelength Target Station (LWTS). The LWTS will provide the high flux of long wavelength neutrons at the requisite pulse rate required by the spectrometer design. The resolution of this spectrometer lies between that routinely achieved by spin echo techniques and the design goal of the high power target station backscattering spectrometer. Covering this niche in energy resolution will allow systematic studies over the large dynamic range required by many disciplines, such as protein dynamics. (author)

  13. High resolution Si(Li) X-ray spectrometer with high throughput rate

    Energy Technology Data Exchange (ETDEWEB)

    Bacso, J.; Kalinka, G.; Kertesz, Zs.; Kovacs, P.; Lakatos, T. (Magyar Tudomanyos Akademia Atommag Kutato Intezete, Debrecen)

    1982-06-01

    The paper presents the description of a modern Si(Li) X-ray spectrometer developed in ATOMKI. The Si(Li) detectors are single-grooved with an active area of 20-50 mm/sup 2/. The Be window is coated with a special protective layer against corrosion. A small getter-ion pump maintains the high vacuum in the cryostat chamber. The preamplifier employs pulsed drain feedback; in its first stage selected, teflon-encapsulated field effect transistors are used. The analogue signal processor is direct coupled and employs time variant pulse shaping. This construction provides high resolution (150-170 eV), high throughput rate, excellent stability, effective pile-up elimination, accurate live-time correction and simplicity in the applications. The live-time correction is performed by a random pulse generator, its average frequency is stabilized and the corresponding peak appears at zero energy in the spectra.

  14. Using a multimode fiber as a high resolution, low loss spectrometer

    CERN Document Server

    Redding, Brandon

    2015-01-01

    We propose and demonstrate that a conventional multimode fiber can function as a high resolution, low loss spectrometer. The proposed spectrometer consists only of the fiber and a camera that images the speckle pattern generated by interference among the fiber modes. While this speckle pattern is detrimental to many applications, it encodes information about the spectral content of the input signal which can be recovered using calibration data. We achieve a spectral resolution of 0.15 nm over 25 nm bandwidth using 1 meter long fiber, and 0.03 nm resolution over 5 nm bandwidth with a 5 meter fiber. The insertion loss is less than 10%, and the signal to noise ratio in the reconstructed spectra is over 1000.

  15. High-resolution XES and RIXS studies with a von Hamos Bragg crystal spectrometer

    CERN Document Server

    Hoszowska, J; 10.1016/j.elspec.2004.02.005

    2004-01-01

    The high-resolution von Hamos Bragg crystal spectrometer was constructed for the study of K X-ray emission from low-Z elements and L and M X-ray spectra of medium to high Z elements. Recently, this instrument was applied to high-resolution XES and RIXS studies using X-ray synchrotron radiation at the ID21 and BM5 beamlines at the ESRF. An outline of the spectrometer design and performance characteristics will be given. The studies deal with the energy dependent KL double photoexcitation of argon, the L3 and M1 atomic- level widths of elements 54

  16. High-resolution VUV spectrometer/detector investigations of rare-earth pulsed plasma source (abstract)

    Science.gov (United States)

    Roberts, J. R.; Cromer, C. L.; Bridges, J. M.; Lucatorto, T. B.

    1985-05-01

    A 1.5-m grazing incidence spectrometer with a channel electron multiplier (CEMA) and electronic readout detector has been incorporated with a rare-earth target, pulsed plasma, continuum source. The spectrometer is compact and portable while maintaining high resolution. The CEMA detector consists of a single multichannel plate (MCP) with coned-shaped input pores which are cut at a 15-degree bias to improve efficiency at grazing angles. The source is a rare-earth plasma generated by a 10-J ruby laser producing intense continuum emission for wavelengths from 170 to 5 nm. This system will be used for both stationary and transient high-resolution atomic photoabsorption spectroscopy. The pulsed plasma source itself will be investigated for suitability as a radiometric transfer standard source. Preliminary results obtained with this integrated system will be discussed.

  17. A pulse-front-tilt–compensated streaked optical spectrometer with high throughput and picosecond time resolution

    Energy Technology Data Exchange (ETDEWEB)

    Katz, J., E-mail: jkat@lle.rochester.edu; Boni, R.; Rivlis, R. [Laboratory for Laser Energetics, University of Rochester, Rochester, New York 14623-1299 (United States); Muir, C. [Department of Mechanical Engineering, University of Rochester, Rochester, New York 14623-1299 (United States); Froula, D. H. [Laboratory for Laser Energetics, University of Rochester, Rochester, New York 14623-1299 (United States); Department of Physics, University of Rochester, Rochester, New York 14623-1299 (United States)

    2016-11-15

    A high-throughput, broadband optical spectrometer coupled to the Rochester optical streak system equipped with a Photonis P820 streak tube was designed to record time-resolved spectra with 1-ps time resolution. Spectral resolution of 0.8 nm is achieved over a wavelength coverage range of 480 to 580 nm, using a 300-groove/mm diffraction grating in conjunction with a pair of 225-mm-focal-length doublets operating at an f/2.9 aperture. Overall pulse-front tilt across the beam diameter generated by the diffraction grating is reduced by preferentially delaying discrete segments of the collimated input beam using a 34-element reflective echelon optic. The introduced delay temporally aligns the beam segments and the net pulse-front tilt is limited to the accumulation across an individual sub-element. The resulting spectrometer design balances resolving power and pulse-front tilt while maintaining high throughput.

  18. A pulse-front-tilt-compensated streaked optical spectrometer with high throughput and picosecond time resolution

    Science.gov (United States)

    Katz, J.; Boni, R.; Rivlis, R.; Muir, C.; Froula, D. H.

    2016-11-01

    A high-throughput, broadband optical spectrometer coupled to the Rochester optical streak system equipped with a Photonis P820 streak tube was designed to record time-resolved spectra with 1-ps time resolution. Spectral resolution of 0.8 nm is achieved over a wavelength coverage range of 480 to 580 nm, using a 300-groove/mm diffraction grating in conjunction with a pair of 225-mm-focal-length doublets operating at an f/2.9 aperture. Overall pulse-front tilt across the beam diameter generated by the diffraction grating is reduced by preferentially delaying discrete segments of the collimated input beam using a 34-element reflective echelon optic. The introduced delay temporally aligns the beam segments and the net pulse-front tilt is limited to the accumulation across an individual sub-element. The resulting spectrometer design balances resolving power and pulse-front tilt while maintaining high throughput.

  19. A High-Resolution Time-of-Flight Mass Spectrometer for Experiments with Ultracold Gases

    CERN Document Server

    Kraft, S D; Staanum, P; Fioretti, A; Lange, J; Wester, R; Weidemüller, M; Kraft, Stephan D.; Mikosch, Jochen; Staanum, Peter; Fioretti, Andrea; Lange, Joerg; Wester, Roland; Weidemueller, Matthias

    2005-01-01

    We have realized a high-resolution time-of-flight mass spectrometer combined with a magneto-optical trap. The spectrometer enables excellent optical access to the trapped atomic cloud using properly devised acceleration and deflection electrodes. The ions are extracted along a laser axis and deflected onto an off axis detector. The setup is applied to detect atoms and molecules photoassociated from ultracold atoms. The detection is based on resonance-enhanced multi-photon ionization. The versatile setup can easily be implemented in more complex experiments with ultracold atomic and molecular gases. Mass resolution up to $m/\\Delta m_{rms} = 1000$ at the mass of $^{133}$Cs is achieved.

  20. High resolution infrared spectroscopy of planetary molecules using diode lasers and Fourier transform spectrometers

    Science.gov (United States)

    Jennings, Donald E.

    1990-01-01

    Modern observations of infrared molecular lines in planets are performed at spectral resolutions which are as high as those available in the laboratory. Analysis of such data requires laboratory measurements at the highest possible resolution, which also yield accurate line positions and intensities. For planetary purposes the spectrometer must be coupled to sample cells which can be reduced in temperature and varied in pressure. An approach which produces the full range of required molecular line parameters uses a combination of tunable diode lasers and Fourier transform spectrometers (FTS). The FTS provides board spectral coverage and good calibration accuracy, while the diode laser can be used to study those regions which are not resolved by the FTS.

  1. Analysis of High-Resolution Spectra From a Hybrid Interferometric/Dispersive Spectrometer

    CERN Document Server

    Ko, P; Jovanovic, I

    2015-01-01

    To more fully take advantage of a low-cost, small footprint hybrid interferometric/dispersive spectrometer, a mathematical reconstruction technique was developed to accurately capture the high-resolution and relative peak intensities from complex spectral patterns. A Fabry-Perot etalon was coupled to a Czerny-Turner spectrometer, leading to increased spectral resolution by more than an order of magnitude without the commensurate increase in spectrometer size. Measurement of the industry standard Hg 313.1555/313.1844 nm doublet yielded a ratio of 0.682, which agreed well with an independent measurement and literature values. The doublet separation (29 pm) is similar to the U isotope shift (25 pm) at 424.437 nm that is of interest to monitoring nuclear nonproliferation activities. Additionally, the technique was applied to LIBS measurement of the mineral cinnabar (HgS) and resulted in a ratio of 0.682. This reconstruction method could enable significantly smaller, portable high-resolution instruments with isoto...

  2. Design of a Multi-Channel Ultra-High Resolution Superconducting Gamma-Ray Spectrometer

    Energy Technology Data Exchange (ETDEWEB)

    Friedrich, S; Terracol, S F; Miyazaki, T; Drury, O B; Ali, Z A; Cunningham, M F; Niedermayr, T R; Barbee Jr., T W; Batteux, J D; Labov, S E

    2004-11-29

    Superconducting Gamma-ray microcalorimeters operated at temperatures around {approx}0.1 K offer an order of magnitude improvement in energy resolution over conventional high-purity Germanium spectrometers. The calorimeters consist of a {approx}1 mm{sup 3} superconducting or insulating absorber and a sensitive thermistor, which are weakly coupled to a cold bath. Gamma-ray capture increases the absorber temperature in proportion to the Gamma-ray energy, this is measured by the thermistor, and both subsequently cool back down to the base temperature through the weak link. We are developing ultra-high-resolution Gamma-ray spectrometers based on Sn absorbers and superconducting Mo/Cu multilayer thermistors for nuclear non-proliferation applications. They have achieved an energy resolution between 60 and 90 eV for Gamma-rays up to 100 keV. We also build two-stage adiabatic demagnetization refrigerators for user-friendly detector operation at 0.1 K. We present recent results on the performance of single pixel Gamma-ray spectrometers, and discuss the design of a large detector array for increased sensitivity.

  3. Development of a high resolution alpha spectrometer using a magnetic calorimeter

    Energy Technology Data Exchange (ETDEWEB)

    Yoon, W.S. [Center for Underground Physics, Institute for Basic Science (IBS), Daejeon 305-811 (Korea, Republic of); Korea Research Institute of Standards and Science (KRISS), Daejeon 305-340 (Korea, Republic of); Korea University of Science and Technology (UST), Daejeon 305-350 (Korea, Republic of); Kang, C.S. [Center for Underground Physics, Institute for Basic Science (IBS), Daejeon 305-811 (Korea, Republic of); Korea Research Institute of Standards and Science (KRISS), Daejeon 305-340 (Korea, Republic of); Kim, S.R., E-mail: yhkim@kriss.re.kr [Center for Underground Physics, Institute for Basic Science (IBS), Daejeon 305-811 (Korea, Republic of); Korea Research Institute of Standards and Science (KRISS), Daejeon 305-340 (Korea, Republic of); Kim, G.B. [Center for Underground Physics, Institute for Basic Science (IBS), Daejeon 305-811 (Korea, Republic of); Lee, H.J. [Center for Underground Physics, Institute for Basic Science (IBS), Daejeon 305-811 (Korea, Republic of); Korea Research Institute of Standards and Science (KRISS), Daejeon 305-340 (Korea, Republic of); Lee, M.K.; Lee, J.H. [Korea Research Institute of Standards and Science (KRISS), Daejeon 305-340 (Korea, Republic of); So, J.H. [Center for Underground Physics, Institute for Basic Science (IBS), Daejeon 305-811 (Korea, Republic of); Korea Research Institute of Standards and Science (KRISS), Daejeon 305-340 (Korea, Republic of); Kim, Y.H. [Center for Underground Physics, Institute for Basic Science (IBS), Daejeon 305-811 (Korea, Republic of); Korea Research Institute of Standards and Science (KRISS), Daejeon 305-340 (Korea, Republic of); Korea University of Science and Technology (UST), Daejeon 305-350 (Korea, Republic of)

    2015-06-01

    We have developed a high resolution alpha spectrometer with a magnetic calorimeter. The operating principle of the detector is the calorimetric measurement of the temperature increase from particle absorption in a gold foil absorber at milli-Kelvin temperatures. A magnetic calorimeter made of gold doped with erbium on a superconducting meander pickup coil was used to accurately measure the temperature change, thereby acting as an ultra-sensitive thermometer. The detector demonstrated 1.2 keV FWHM equivalent resolution in alpha particle detection with an {sup 241}Am source. Many peaks were observed in the low-energy region from the absorption of low-energy X-rays, gamma rays, and conversion electrons. An energy resolution of 400 eV FWHM was achieved for 60 keV gamma rays that were measured with the alpha particles. Possible applications of such high resolution detectors are discussed.

  4. A high-resolution x-ray spectrometer for a kaon mass measurement

    Science.gov (United States)

    Phelan, Kevin; Suzuki, Ken; Zmeskal, Johann; Tortorella, Daniele; Bühler, Matthias; Hertrich, Theo

    2017-02-01

    The ASPECT consortium (Adaptable Spectrometer Enabled by Cryogenic Technology) is currently constructing a generalised cryogenic platform for cryogenic detector work which will be able to accommodate a wide range of sensors. The cryogenics system is based on a small mechanical cooler with a further adiabatic demagnetisation stage and will work with cryogenic detectors at sub-Kelvin temperatures. The commercial aim of the consortium is to produce a compact, user-friendly device with an emphasis on reliability and portability which can easily be transported for specialised on-site work, such as beam-lines or telescope facilities. The cryogenic detector platform will accommodate a specially developed cryogenic sensor, either a metallic magnetic calorimeter or a magnetic penetration-depth thermometer. The detectors will be designed to work in various temperatures regions with an emphasis on optimising the various detector resolutions for specific temperatures. One resolution target is of about 10 eV at the energies range typically created in kaonic atoms experiments (soft x-ray energies). A following step will see the introduction of continuous, high-power, sub-Kelvin cooling which will bring the cryogenic basis for a high resolution spectrometer system to the market. The scientific goal of the project will produce an experimental set-up optimised for kaon-mass measurements performing high-resolution x-ray spectroscopy on a beam-line provided foreseeably by the J-PARC (Tokai, Japan) or DAΦNE (Frascati, Italy) facilities.

  5. A multiplexed high-resolution imaging spectrometer for resonant inelastic soft X-ray scattering spectroscopy.

    Science.gov (United States)

    Warwick, Tony; Chuang, Yi De; Voronov, Dmitriy L; Padmore, Howard A

    2014-07-01

    The optical design of a two-dimensional imaging soft X-ray spectrometer is described. A monochromator will produce a dispersed spectrum in a narrow vertical illuminated stripe (∼2 µm wide by ∼2 mm tall) on a sample. The spectrometer will use inelastically scattered X-rays to image the extended field on the sample in the incident photon energy direction (vertical), resolving the incident photon energy. At the same time it will image and disperse the scattered photons in the orthogonal (horizontal) direction, resolving the scattered photon energy. The principal challenge is to design a system that images from the flat-field illumination of the sample to the flat field of the detector and to achieve sufficiently high spectral resolution. This spectrometer provides a completely parallel resonant inelastic X-ray scattering measurement at high spectral resolution (∼30,000) over the energy bandwidth (∼5 eV) of a soft X-ray absorption resonance.

  6. Development of high resolution x-ray spectrometers for the investigation of bioinorganic chemistry in metalloproteins

    Science.gov (United States)

    Drury, Owen Byron

    We have built an X-ray spectrometer for synchrotron-based high-resolution soft X-ray spectroscopy. The spectrometer uses four 9-pixel arrays of superconducting tunnel junctions (STJs) as sensors. They infer the energy of an absorbed X-ray from a temporary increase in tunneling current. The STJs are operated in a two-stage adiabatic demagnetization refrigerator (ADR) that uses liquid nitrogen and helium for precooling to 77 K and 4.2 K, and gallium gadolinium garnet and iron ammonium sulfate to attain a base temperature below 0.1 K. The sensors are held at the end of a 40-cm-long cold finger within ˜1 cm of a sample located inside the vacuum chamber of a synchrotron beam line end station. The spectrometer has an energy resolution between 10 eV and 20 eV FWHM below 1 keV, can be operated at rates up to ˜106 counts/s. STJ spectrometers are suited for chemical analysis of dilute samples by fluorescence-detected X-ray absorption spectroscopy (XAS) in cases where conventional germanium detectors do not have enough energy resolution. We have used this STJ spectrometer at the Advanced Light Source synchrotron for spectroscopy on the lower energy X-ray absorption edges of the elements Mo, S, Fe and N. These elements play an important role in biological nitrogen fixation at the metalloprotein nitrogenase, and we have examined if STJ spectrometers can be used to provide new insights into some of the open questions regarding the reaction mechanism of this protein. We have taken X-ray absorption near-edge spectra (XANES) and extended fine structure spectra (EXAFS) of an Fe 6N(CO)15-compound containing a single N atom inside a cluster of six Fe atoms, as postulated to exist inside the Fe-S cluster of the FeMo-cofactor (FeMo-co) in nitrogenase. The STJ detector has enabled the first-ever extended range EXAFS scans on nitrogen through the oxygen K-edge, enabling a comparison with N EXAFS on FeMo-co. We have taken iron L23-edge spectra of the Fe-S cluster in FeMo-co, which can be

  7. A High Resolution Orbitrap Mass Spectrometer for In-Situ Analysis in Planetary Science

    Science.gov (United States)

    Briois, C.; Thirkell, L.; Boukrara, A.; Lebreton, J. P.; Thissen, R.; Puget, P.; Cottin, H.; Grand, N.; Pennanech, C.; Zapf, P.; Szopa, C.; Carrasco, N.; Chapuis, C.; Bouabdellah, A.; Berthelier, J. J.; Engrand, C.; Makarov, A.

    2012-04-01

    Solar System exploration is dealing more and more with chemically complex matter, potentially associated with astrobiology or prebiotic questions, requiring optimized methods of analysis. Due to its ability to reveal quantitatively almost any chemical element, mass spectrometry has served as an invaluable scientific analytical instruments. Nevertheless the best mass resolution (M/deltaM) currently achieved by mass spectrometers in space is about 3000 at mass 28 (ROSINA's DFMS on board ESA's comet chaser Rosetta). This resolution allows separation of peaks for only a limited number of isobaric species (e.g. N2 / CO at 28 Da). Yet, purely electrostatic orbital traps in laboratory are showing mass resolution above 100 000 for m/z <= 400 [1, 2], that provides separation for each detected isobaric species. Therefore it opens new opportunity for molecular characterization, isotopic abundance evaluation, and more generally environmental characterization. Our French consortium of laboratories, in collaboration with ThermoFischer Scientific, is currently working on the adaptation of this type of mass spectrometer for space instrumentation. We present here this innovative concept of mass analyzer for space that is lightweight, uses DC voltages, and provides ultra high resolving power capabilities. A mass resolution of 140,000 at mass 56 has been recently achieved with our prototype.

  8. High resolution X-ray spherically bent crystal spectrometer for laser-produced plasma diagnostics

    Institute of Scientific and Technical Information of China (English)

    Shali Xiao; Hongjian Wang; Jun Shi; Changhuan Tang; Shenye Liu

    2009-01-01

    A new high spectral resolution crystal spectrometer is designed to measure very low emissive X-ray spectra of laser-produced plasma in 0.5 - 0.9 nm range. A large open aperture (30 x 20 (mm)) mica (002) spherically bent crystal with curvature radius R = 380 mm is used as dispersive and focusing element. The imaging plate is employed to obtain high spectral resolution with effective area of 30 x 80 (mm). The long designed path of the X-ray spectrometer beam is 980 mm from the source to the detector via the crystal. Experiment is carried out at a 20-J laser facility. X-ray spectra in an absolute intensity scale is obtained from Al laser produced plasmas created by laser energy of 6.78 J. Samples of spectra obtained with spectral resolution of up to E/鈻矱 ~ 1500 are presented. The results clearly show that the device is good to diagnose laser high-density plasmas.

  9. Quantitative proteomics using the high resolution accurate mass capabilities of the quadrupole-orbitrap mass spectrometer.

    Science.gov (United States)

    Gallien, Sebastien; Domon, Bruno

    2014-08-01

    High resolution/accurate mass hybrid mass spectrometers have considerably advanced shotgun proteomics and the recent introduction of fast sequencing capabilities has expanded its use for targeted approaches. More specifically, the quadrupole-orbitrap instrument has a unique configuration and its new features enable a wide range of experiments. An overview of the analytical capabilities of this instrument is presented, with a focus on its application to quantitative analyses. The high resolution, the trapping capability and the versatility of the instrument have allowed quantitative proteomic workflows to be redefined and new data acquisition schemes to be developed. The initial proteomic applications have shown an improvement of the analytical performance. However, as quantification relies on ion trapping, instead of ion beam, further refinement of the technique can be expected.

  10. Characterization of spatially resolved high resolution x-ray spectrometers for high energy density physics and light source experiments.

    Science.gov (United States)

    Hill, K W; Bitter, M; Delgado-Aparacio, L; Efthimion, P; Pablant, N A; Lu, J; Beiersdorfer, P; Chen, H; Magee, E

    2014-11-01

    A high resolution 1D imaging x-ray spectrometer concept comprising a spherically bent crystal and a 2D pixelated detector is being optimized for diagnostics of small sources such as high energy density physics (HEDP) and synchrotron radiation or x-ray free electron laser experiments. This instrument is used on tokamak experiments for Doppler measurements of ion temperature and plasma flow velocity profiles. Laboratory measurements demonstrate a resolving power, E/ΔE of order 10,000 and spatial resolution better than 10 μm. Initial tests of the high resolution instrument on HEDP plasmas are being performed.

  11. A compact high-resolution X-ray ion mobility spectrometer

    Energy Technology Data Exchange (ETDEWEB)

    Reinecke, T.; Kirk, A. T.; Heptner, A.; Niebuhr, D.; Böttger, S.; Zimmermann, S. [Department of Sensors and Measurement Technology, Institute of Electrical Engineering and Measurement Technology, Leibniz Universität Hannover, Appelstr. 9A, 30167 Hannover (Germany)

    2016-05-15

    For the ionization of gaseous samples, most ion mobility spectrometers employ radioactive ionization sources, e.g., containing {sup 63}Ni or {sup 3}H. Besides legal restrictions, radioactive materials have the disadvantage of a constant radiation with predetermined intensity. In this work, we replaced the {sup 3}H source of our previously described high-resolution ion mobility spectrometer with 75 mm drift tube length with a commercially available X-ray source. It is shown that the current configuration maintains the resolving power of R = 100 which was reported for the original setup containing a {sup 3}H source. The main advantage of an X-ray source is that the intensity of the radiation can be adjusted by varying its operating parameters, i.e., filament current and acceleration voltage. At the expense of reduced resolving power, the sensitivity of the setup can be increased by increasing the activity of the source. Therefore, the performance of the setup can be adjusted to the specific requirements of any application. To investigate the relation between operating parameters of the X-Ray source and the performance of the ion mobility spectrometer, parametric studies of filament current and acceleration voltage are performed and the influence on resolving power, peak height, and noise is analyzed.

  12. The High Resolution Microcalorimeter Soft X-ray Spectrometer for the Astro-H Mission

    Science.gov (United States)

    Kelley, Richard L.; Mitsuda, K.; International SXS Team

    2013-04-01

    We are developing the Soft X-Ray Spectrometer (SXS) for the JAXA Astro-H mission. The instrument is based on a 36-pixel array of semiconductor micro calorimeters that provides high spectral resolution over the 0.3-12 keV energy band at the focus of a high throughput, grazing-incidence x-ray mirror, giving a 3 x 3 arcmin field of view and more than 200 cm2 of collecting area at 6 keV. The instrument is a collaboration between the JAXA Institute of Space and Astronautical Science and their partners in Japan, the NASA/Goddard Space Flight Center, the University of Wisconsin, the Space Research Organization of the Netherlands, and Geneva University. The principal components of the spectrometer are the microcalorimeter detector system, low-temperature anticoincidence detector, 3-stage ADR and dewar. The dewar is a long-life, hybrid design with a superfluid helium cryostat, Joule-Thomson cooler, and Stirling coolers. The instrument is capable of achieving 4-5 eV resolution across the array and is designed to operate for at least three years in orbit, and can operate either without liquid helium or the cooling power of the Joule-Thomson cooler. In this presentation we describe the design and status of the Astro-H/SXS instrument.

  13. Development of a high resolution x-ray spectrometer for the National Ignition Facility (NIF).

    Science.gov (United States)

    Hill, K W; Bitter, M; Delgado-Aparicio, L; Efthimion, P C; Ellis, R; Gao, L; Maddox, J; Pablant, N A; Schneider, M B; Chen, H; Ayers, S; Kauffman, R L; MacPhee, A G; Beiersdorfer, P; Bettencourt, R; Ma, T; Nora, R C; Scott, H A; Thorn, D B; Kilkenny, J D; Nelson, D; Shoup, M; Maron, Y

    2016-11-01

    A high resolution (E/ΔE = 1200-1800) Bragg crystal x-ray spectrometer is being developed to measure plasma parameters in National Ignition Facility experiments. The instrument will be a diagnostic instrument manipulator positioned cassette designed mainly to infer electron density in compressed capsules from Stark broadening of the helium-β (1s(2)-1s3p) lines of krypton and electron temperature from the relative intensities of dielectronic satellites. Two conically shaped crystals will diffract and focus (1) the Kr Heβ complex and (2) the Heα (1s(2)-1s2p) and Lyα (1s-2p) complexes onto a streak camera photocathode for time resolved measurement, and a third cylindrical or conical crystal will focus the full Heα to Heβ spectral range onto an image plate to provide a time integrated calibration spectrum. Calculations of source x-ray intensity, spectrometer throughput, and spectral resolution are presented. Details of the conical-crystal focusing properties as well as the status of the instrumental design are also presented.

  14. [Design and study of a high resolution vacuum ultraviolet imaging spectrometer carried by satellite].

    Science.gov (United States)

    Yu, Lei; Lin, Guan-yu; Qu, Yi; Wang, Shu-rong; Wang, Long-qi

    2011-12-01

    A high resolution vacuum ultraviolet imaging spectrometer prototype carried by satellite applied to the atmosphere detection of particles distribution in 115-300 nm was developed for remote sensing. First, based on the analysis of advanced loads, the optical system including an off-axis parabolic mirror as the telescope and Czerny-Turner structure as the imaging spectrometer was chosen Secondly, the 2-D photon counting detector with MCP was adopted for the characteristic that the radiation is weak in vacuum ultraviolet waveband. Then the geometric method and 1st order differential calculation were introduced to improve the disadvantages that aberrations in the traditional structure can not be corrected homogeneously to achieve perfect broadband imaging based on the aberration theory. At last, an advanced example was designed. The simulation and calculation of results demonstrate that the modulation transfer function (MTF) of total field of view is more than 0.6 in the broadband, and the spectral resolution is 1.23 nm. The structure is convenient and predominant. It proves that the design is feasible.

  15. Development of a high resolution x-ray spectrometer for the National Ignition Facility (NIF)

    Science.gov (United States)

    Hill, K. W.; Bitter, M.; Delgado-Aparicio, L.; Efthimion, P. C.; Ellis, R.; Gao, L.; Maddox, J.; Pablant, N. A.; Schneider, M. B.; Chen, H.; Ayers, S.; Kauffman, R. L.; MacPhee, A. G.; Beiersdorfer, P.; Bettencourt, R.; Ma, T.; Nora, R. C.; Scott, H. A.; Thorn, D. B.; Kilkenny, J. D.; Nelson, D.; Shoup, M.; Maron, Y.

    2016-11-01

    A high resolution (E/ΔE = 1200-1800) Bragg crystal x-ray spectrometer is being developed to measure plasma parameters in National Ignition Facility experiments. The instrument will be a diagnostic instrument manipulator positioned cassette designed mainly to infer electron density in compressed capsules from Stark broadening of the helium-β (1s2-1s3p) lines of krypton and electron temperature from the relative intensities of dielectronic satellites. Two conically shaped crystals will diffract and focus (1) the Kr Heβ complex and (2) the Heα (1s2-1s2p) and Lyα (1s-2p) complexes onto a streak camera photocathode for time resolved measurement, and a third cylindrical or conical crystal will focus the full Heα to Heβ spectral range onto an image plate to provide a time integrated calibration spectrum. Calculations of source x-ray intensity, spectrometer throughput, and spectral resolution are presented. Details of the conical-crystal focusing properties as well as the status of the instrumental design are also presented.

  16. High-resolution x-ray spectroscopy with the EBIT Calorimeter Spectrometer

    Energy Technology Data Exchange (ETDEWEB)

    Porter, F S; Adams, J S; Beiersdorfer, P; Brown, G V; Clementson, J; Frankel, M; Kahn, S M; Kelley, R L; Kilbourne, C A

    2009-10-01

    The EBIT Calorimeter Spectrometer (ECS) is a production-class 36 pixel x-ray calorimeter spectrometer that has been continuously operating at the Electron Beam Ion Trap (EBIT) facility at Lawrence Livermore National Laboratory for almost 2 years. The ECS was designed to be a long-lifetime, turn-key spectrometer that couples high performance with ease of operation and minimal operator intervention. To this end, a variant of the Suzaku/XRS spaceflight detector system has been coupled to a low-maintenance cryogenic system consisting of a long-lifetime liquid He cryostat, and a closed cycle, {sup 3}He pre-cooled adiabatic demagnetization refrigerator. The ECS operates for almost 3 weeks between cryogenic servicing and the ADR operates at 0.05 K for more than 60 hours between automatic recycles under software control. Half of the ECS semiconductor detector array is populated with mid-band pixels that have a resolution of 4.5 eV FWHM, a bandpass from 0.05-12 keV, and a quantum efficiency of 95% at 6 keV. The other half of the array has thick HgTe absorbers that have a bandpass from 0.3 to over 100 keV, an energy resolution of 33 eV FWHM, and a quantum efficiency of 32% at 60 keV. In addition, the ECS uses a real-time, autonomous, data collection and analysis system developed for the Suzaku/XRS instrument and implemented in off-the-shelf hardware for the ECS. Here we will discuss the performance of the ECS instrument and its implementation as a turnkey cryogenic detector system.

  17. Performance of the High Resolution, Multi-collector Helix MC Plus Noble Gas Mass Spectrometer at the Australian National University

    Science.gov (United States)

    Zhang, Xiaodong; Honda, Masahiko; Hamilton, Doug

    2016-12-01

    Performance of the Helix MC Plus noble gas mass spectrometer installed at the Australian National University (ANU) is reported. Results for sensitivity, mass discrimination and their linearity against partial pressure of noble gases, and mass resolution of the mass spectrometer are presented, and the results are compared with those of conventional noble gas mass spectrometers. The application of the five detectors on the Helix MC Plus in measuring various noble gas isotopes in multi-collector modes and the integration of the software drivers of peripheral hardware devices into the controlling program Qtegra of the mass spectrometer are discussed. High mass resolution (>1800) and mass resolving power (>8000) make this mass spectrometer unique in noble gas cosmo-geochemistry. It provides the capability to measure isobaric interference-free noble gas isotopes in multi-collector mode, significantly improves the accuracy to determine isotopic ratios, and greatly increases the efficiency of data acquisition.

  18. Performance of the High Resolution, Multi-collector Helix MC Plus Noble Gas Mass Spectrometer at the Australian National University

    Science.gov (United States)

    Zhang, Xiaodong; Honda, Masahiko; Hamilton, Doug

    2016-09-01

    Performance of the Helix MC Plus noble gas mass spectrometer installed at the Australian National University (ANU) is reported. Results for sensitivity, mass discrimination and their linearity against partial pressure of noble gases, and mass resolution of the mass spectrometer are presented, and the results are compared with those of conventional noble gas mass spectrometers. The application of the five detectors on the Helix MC Plus in measuring various noble gas isotopes in multi-collector modes and the integration of the software drivers of peripheral hardware devices into the controlling program Qtegra of the mass spectrometer are discussed. High mass resolution (>1800) and mass resolving power (>8000) make this mass spectrometer unique in noble gas cosmo-geochemistry. It provides the capability to measure isobaric interference-free noble gas isotopes in multi-collector mode, significantly improves the accuracy to determine isotopic ratios, and greatly increases the efficiency of data acquisition.

  19. High-resolution proton energy-loss spectrometer for surface analysis

    Energy Technology Data Exchange (ETDEWEB)

    Itoh, Noriaki; Kanasaki, Junichi; Matsunami, Noriaki; Matsuda, Kouji; Aoki, Masahiko.

    1988-11-01

    We describe a new ion-beam surface analyzer, proton energy loss spectrometer. It analyzes ions incident at 100 keV and scattered by 180degC at solid surfaces with a resolution of 5eV. The results of computer simulation of the energy spectra of scattered ions and the informations on surface electronic and atomic structures possibly derived by the analysis are described. Application of the spectrometer in several areas of science and technology is briefly discussed.

  20. SIEMENS ADVANCED QUANTRA FTICR MASS SPECTROMETER FOR ULTRA HIGH RESOLUTION AT LOW MASS

    Energy Technology Data Exchange (ETDEWEB)

    Spencer, W; Laura Tovo, L

    2008-07-08

    The Siemens Advanced Quantra Fourier Transform Ion Cyclotron Resonance (FTICR) mass spectrometer was evaluated as an alternative instrument to large double focusing mass spectrometers for gas analysis. High resolution mass spectrometers capable of resolving the common mass isomers of the hydrogen isotopes are used to provide data for accurate loading of reservoirs and to monitor separation of tritium, deuterium, and helium. Conventional double focusing magnetic sector instruments have a resolution that is limited to about 5000. The Siemens FTICR instrument achieves resolution beyond 400,000 and could possibly resolve the tritium ion from the helium-3 ion, which differ by the weight of an electron, 0.00549 amu. Working with Y-12 and LANL, SRNL requested Siemens to modify their commercial Quantra system for low mass analysis. To achieve the required performance, Siemens had to increase the available waveform operating frequency from 5 MHz to 40 MHz and completely redesign the control electronics and software. However, they were able to use the previous ion trap, magnet, passive pump, and piezo-electric pulsed inlet valve design. NNSA invested $1M in this project and acquired four systems, two for Y-12 and one each for SRNL and LANL. Siemens claimed a $10M investment in the Quantra systems. The new Siemens Advanced Quantra demonstrated phenomenal resolution in the low mass range. Resolution greater than 400,000 was achieved for mass 2. The new spectrometer had a useful working mass range to 500 Daltons. However, experiments found that a continuous single scan from low mass to high was not possible. Two useful working ranges were established covering masses 1 to 6 and masses 12 to 500 for our studies. A compromise performance condition enabled masses 1 to 45 to be surveyed. The instrument was found to have a dynamic range of about three orders of magnitude and quantitative analysis is expected to be limited to around 5 percent without using complex fitting algorithms

  1. High-energy resolution μ-XRF analysis by position sensitive spectrometer

    Institute of Scientific and Technical Information of China (English)

    2000-01-01

    With a high-energy resolution micro-X-ray fluorescence (μ-XRF) analysis setup, which basically consists of an X-ray microbeam formed by an X-ray focusing lens combined with an X-ray apparatus and a wavelength dispersive position sensitive spectrometer with a flat crystal (PSS), preliminary results have been obtained. The counting rate of the analyzed element linearly increased with the power of X-ray apparatus, and the energy resolution, full width of half maximum (FWHM) of Ka lines of Ti and Cr reached 16.6 and 23.6 eV, respectively. The Cr Kb and Mn Ka lines in a sample of stainless steel could clearly be resolved. The above-mentioned results are also compared with those obtained by synchrotron radiation light microbeam combined with the PSS. The facts show that the high-energy resolution element analysis is feasible by using the setup. Moreover, problems for the setup and the ways to resolve them are discussed as well.

  2. High resolution NO2 remote sensing from the Airborne Prism EXperiment (APEX imaging spectrometer

    Directory of Open Access Journals (Sweden)

    B. Buchmann

    2012-03-01

    Full Text Available We present and evaluate the retrieval of high spatial resolution maps of NO2 vertical column densities (VCD from the Airborne Prism EXperiment (APEX imaging spectrometer. APEX is a novel instrument providing airborne measurements of unique spectral and spatial resolution and coverage as well as high signal stability. In this study, we use spectrometer data acquired over Zurich, Switzerland, in the morning and late afternoon during a flight campaign on a cloud-free summer day in June 2010. NO2 VCD are derived with a two-step approach usually applied to satellite NO2 retrievals, i.e. a DOAS analysis followed by air mass factor calculations based on radiative transfer computations. Our analysis demonstrates that APEX is clearly sensitive to NO2 VCD above typical European tropospheric background abundances (>1 × 1015 molec cm−2. The two-dimensional maps of NO2 VCD reveal a very plausible spatial distribution with strong gradients around major NOx sources (e.g. Zurich airport, waste incinerator, motorways and low NO2 in remote areas. The morning overflights resulted in generally higher NO2 VCD and a more distinct pattern than the afternoon overflights which can be attributed to the meteorological conditions prevailing during that day (development of the boundary layer and increased wind speed in the afternoon as well as to photochemical loss of NO2. The remotely sensed NO2 VCD are also highly correlated with ground-based in-situ measurements from local and national air quality networks (R=0.73. Airborne NO2 remote sensing using APEX will be valuable to detect NO2 emission sources, to provide input for NO2 emission modeling, and to establish links between in-situ measurements, air quality models, and satellite NO2 products.

  3. Radiological Shielding Design for the Neutron High-Resolution Backscattering Spectrometer EMU at the OPAL Reactor

    Science.gov (United States)

    Ersez, Tunay; Esposto, Fernando; Souza, Nicolas R. de

    2017-09-01

    The shielding for the neutron high-resolution backscattering spectrometer (EMU) located at the OPAL reactor (ANSTO) was designed using the Monte Carlo code MCNP 5-1.60. The proposed shielding design has produced compact shielding assemblies, such as the neutron pre-monochromator bunker with sliding cylindrical block shields to accommodate a range of neutron take-off angles, and in the experimental area - shielding of neutron focusing guides, choppers, flight tube, backscattering monochromator, and additional shielding elements inside the Scattering Tank. These shielding assemblies meet safety and engineering requirements and cost constraints. The neutron dose rates around the EMU instrument were reduced to < 0.5 µSv/h and the gamma dose rates to a safe working level of ≤ 3 µSv/h.

  4. High-resolution NO2 remote sensing from the Airborne Prism EXperiment (APEX imaging spectrometer

    Directory of Open Access Journals (Sweden)

    B. Buchmann

    2012-09-01

    Full Text Available We present and evaluate the retrieval of high spatial resolution maps of NO2 vertical column densities (VCD from the Airborne Prism EXperiment (APEX imaging spectrometer. APEX is a novel instrument providing airborne measurements of unique spectral and spatial resolution and coverage as well as high signal stability. In this study, we use spectrometer data acquired over Zurich, Switzerland, in the morning and late afternoon during a flight campaign on a cloud-free summer day in June 2010. NO2 VCD are derived with a two-step approach usually applied to satellite NO2 retrievals, i.e. a DOAS analysis followed by air mass factor calculations based on radiative transfer computations. Our analysis demonstrates that APEX is clearly sensitive to NO2 VCD above typical European tropospheric background abundances (>1 × 1015 molec cm−2. The two-dimensional maps of NO2 VCD reveal a very convincing spatial distribution with strong gradients around major NOx sources (e.g. Zurich airport, waste incinerator, motorways and low NO2 in remote areas. The morning overflights resulted in generally higher NO2 VCD and a more distinct pattern than the afternoon overflights which can be attributed to the meteorological conditions prevailing during that day with stronger winds and hence larger dilution in the afternoon. The remotely sensed NO2 VCD are also in reasonably good agreement with ground-based in-situ measurements from air quality networks considering the limitations of comparing column integrals with point measurements. Airborne NO2 remote sensing using APEX will be valuable to detect NO2 emission sources, to provide input for NO2 emission modelling, and to establish links between in-situ measurements, air quality models, and satellite NO2 products.

  5. The Astro-H high resolution soft x-ray spectrometer

    Science.gov (United States)

    Kelley, Richard L.; Akamatsu, Hiroki; Azzarello, Phillipp; Bialas, Tom; Boyce, Kevin R.; Brown, Gregory V.; Canavan, Edgar; Chiao, Meng P.; Costantini, Elisa; DiPirro, Michael J.; Eckart, Megan E.; Ezoe, Yuichiro; Fujimoto, Ryuichi; Haas, Daniel; den Herder, Jan-Willem; Hoshino, Akio; Ishikawa, Kumi; Ishisaki, Yoshitaka; Iyomoto, Naoko; Kilbourne, Caroline A.; Kimball, Mark O.; Kitamoto, Shunji; Konami, Saori; Koyama, Shu; Leutenegger, Maurice A.; McCammon, Dan; Mitsuda, Kazuhisa; Mitsuishi, Ikuyuki; Moseley, Harvey; Murakami, Hiroshi; Murakami, Masahide; Noda, Hirofumi; Ogawa, Mina; Ohashi, Takaya; Okamoto, Atsushi; Ota, Naomi; Paltani, Stéphane; Porter, F. S.; Sakai, Kazuhiro; Sato, Kosuke; Sato, Yohichi; Sawada, Makoto; Seta, Hiromi; Shinozaki, Keisuke; Shirron, Peter J.; Sneiderman, Gary A.; Sugita, Hiroyuki; Szymkowiak, Andrew E.; Takei, Yoh; Tamagawa, Toru; Tashiro, Makoto; Terada, Yukikatsu; Tsujimoto, Masahiro; de Vries, Cor P.; Yamada, Shinya; Yamasaki, Noriko Y.; Yatsu, Yoichi

    2016-07-01

    We present the overall design and performance of the Astro-H (Hitomi) Soft X-Ray Spectrometer (SXS). The instrument uses a 36-pixel array of x-ray microcalorimeters at the focus of a grazing-incidence x-ray mirror Soft X-Ray Telescope (SXT) for high-resolution spectroscopy of celestial x-ray sources. The instrument was designed to achieve an energy resolution better than 7 eV over the 0.3-12 keV energy range and operate for more than 3 years in orbit. The actual energy resolution of the instrument is 4-5 eV as demonstrated during extensive ground testing prior to launch and in orbit. The measured mass flow rate of the liquid helium cryogen and initial fill level at launch predict a lifetime of more than 4 years assuming steady mechanical cooler performance. Cryogen-free operation was successfully demonstrated prior to launch. The successful operation of the SXS in orbit, including the first observations of the velocity structure of the Perseus cluster of galaxies, demonstrates the viability and power of this technology as a tool for astrophysics.

  6. The construction of a high resolution crystal backscattering spectrometer HERMES I

    Energy Technology Data Exchange (ETDEWEB)

    Larese, J.Z.

    1998-11-01

    There is a need in the United States for a state-of-the-art, cold-neutron, crystal backscattering spectrometer (CBS) designed to investigate the structure and dynamics of condensed matter systems by the simultaneous utilization of long wavelength elastic diffraction and high-energy-resolution inelastic scattering. Cold neutron spectroscopy with CBS-type instruments has already made many important contributions to the study of atomic and molecular diffusion in biomaterials, polymers, semiconductors, liquid crystals, superionic conductors and the like. Such instruments have also been invaluable for ultra high resolution investigations of the low-lying quantum tunneling processes that provide direct insight into the dynamical response of solids at the lowest energies. Until relatively recently, however, all such instruments were located at steady-state reactors. This proposal describes HERMES I (High Energy Resolution Machines I) a CBS intended for installation at the LANSCE pulsed neutron facility of Los Alamos National Laboratory. As explained in detail in the main text, the authors propose to construct an updated, high-performance CBS which incorporates neutron techniques developed during the decade since IRIS was built, i.e., improved supermirror technology, a larger area crystal analyzer and high efficiency wire gas detectors. The instrument is designed in such a way as to be readily adaptable to future upgrades. HERMES I, they believe, will substantially expand the range and flexibility of neutron investigations in the United States and open new and potentially fruitful directions for condensed matter exploration. This document describes a implementation plan with a direct cost range between $4.5 to 5.6 M and scheduled duration of 39--45 months for identified alternatives.

  7. FRONT-END ASIC FOR HIGH RESOLUTION X-RAY SPECTROMETERS.

    Energy Technology Data Exchange (ETDEWEB)

    DE GERONIMO,G.; CHEN, W.; FRIED, J.; LI, Z.; PINELLI, D.A.; REHAK, P.; VERNON, E.; GASKIN, J.A.; RAMSEY, B.D.; ANELLI, G.

    2007-10-27

    We present an application specific integrated circuit (ASIC) for high-resolution x-ray spectrometers. The ASIC is designed to read out signals from a pixelated silicon drift detector (SDD). Each hexagonal pixel has an area of 15 mmz and an anode capacitance of less than 100 fF. There is no integrated Field Effect transistor (FET) in the pixel, rather, the readout is done by wirebonding the anodes to the inputs of the ASIC. The ASIC provides 14 channels of low-noise charge amplification, high-order shaping with baseline stabilization, and peak detection with analog memory. The readout is sparse and based on low voltage differential signaling. An interposer provides all the interconnections required to bias and operate the system. The channel dissipates 1.6 mW. The complete 14-pixel unit covers an area of 210 mm{sup 2}, dissipates 12 mW cm{sup -2}, and can be tiled to cover an arbitrarily large detection area. We measured a preliminary resolution of 172 eV at -35 C on the 6 keV peak of a {sup 55}Fe source.

  8. Development of Compton X-ray spectrometer for high energy resolution single-shot high-flux hard X-ray spectroscopy.

    Science.gov (United States)

    Kojima, Sadaoki; Ikenouchi, Takahito; Arikawa, Yasunobu; Sakata, Shohei; Zhang, Zhe; Abe, Yuki; Nakai, Mitsuo; Nishimura, Hiroaki; Shiraga, Hiroyuki; Ozaki, Tetsuo; Miyamoto, Shuji; Yamaguchi, Masashi; Takemoto, Akinori; Fujioka, Shinsuke; Azechi, Hiroshi

    2016-04-01

    Hard X-ray spectroscopy is an essential diagnostics used to understand physical processes that take place in high energy density plasmas produced by intense laser-plasma interactions. A bundle of hard X-ray detectors, of which the responses have different energy thresholds, is used as a conventional single-shot spectrometer for high-flux (>10(13) photons/shot) hard X-rays. However, high energy resolution (Δhv/hv spectrometer because its energy resolution is limited by energy differences between the response thresholds. Experimental demonstration of a Compton X-ray spectrometer has already been performed for obtaining higher energy resolution than that of DET spectrometers. In this paper, we describe design details of the Compton X-ray spectrometer, especially dependence of energy resolution and absolute response on photon-electron converter design and its background reduction scheme, and also its application to the laser-plasma interaction experiment. The developed spectrometer was used for spectroscopy of bremsstrahlung X-rays generated by intense laser-plasma interactions using a 200 μm thickness SiO2 converter. The X-ray spectrum obtained with the Compton X-ray spectrometer is consistent with that obtained with a DET X-ray spectrometer, furthermore higher certainly of a spectral intensity is obtained with the Compton X-ray spectrometer than that with the DET X-ray spectrometer in the photon energy range above 5 MeV.

  9. Objectives and Layout of a High-Resolution X-ray Imaging Crystal Spectrometer for the Large Helical Device (LHD)

    Energy Technology Data Exchange (ETDEWEB)

    Bitter, M; Gates, D; Monticello, D; Neilson, H; Reiman, A; Roquemore, A L; Morita, S; Goto, M; Yamada, H

    2010-07-29

    A high-resolution X-ray imaging crystal spectrometer, whose concept was tested on NSTX and Alcator C-Mod, is being designed for LHD. This instrument will record spatially resolved spectra of helium-like Ar16+ and provide ion temperature profiles with spatial and temporal resolutions of < 2 cm and ≥ 10 ms. The stellarator equilibrium reconstruction codes, STELLOPT and PIES, will be used for the tomographic inversion of the spectral data. The spectrometer layout and instrumental features are largely determined by the magnetic field structure of LHD.

  10. Monte-Carlo simulations of a high-resolution backscattering spectrometer on the SNS - Long Wavelength Target Station

    Science.gov (United States)

    Bordallo, H. N.; Herwig, K. W.

    2001-03-01

    It is proposed to build an inverse geometry spectrometer to provide extremely high energy resolution (0.2 μeV FWHM, elastic) at the Long Wavelength Target Station (LWTS) at SNS. The design employs mica analyzers in close to backscattering geometry (final neutron wavelength of 20 ÅAnalytical calculations and Monte Carlo simulations (using the McStas package) have been used to optimize the layout of individual components and to estimate the instrument performance. This design requires a long initial guide section of 63 m from moderator to sample in order to achieve the timing resolution necessary for the desired δω. The LWTS will provide the high flux of long wavelength neutrons at the requisite pulse rate required by the spectrometer design. The resolution of this spectrometer lies between that routinely achieved by spin echo techniques and the design goal of the high power target station backscattering spectrometer. Covering this niche in energy resolution will allow systematic studies over the large dynamic range required by many disciplines. Molecular biology, for example, often requires systematic studies of many similar molecules under slightly different conditions, requiring a large range of energy/timing resolutions for optimum study.

  11. Design and Performance of A High Resolution Micro-Spec: An Integrated Sub-Millimeter Spectrometer

    Science.gov (United States)

    Barrentine, Emily M.; Cataldo, Giuseppe; Brown, Ari D.; Ehsan, Negar; Noroozian, Omid; Stevenson, Thomas R.; U-Yen, Kongpop; Wollack, Edward J.; Moseley, S. Harvey

    2016-01-01

    Micro-Spec is a compact sub-millimeter (approximately 100 GHz--1:1 THz) spectrometer which uses low loss superconducting microstrip transmission lines and a single-crystal silicon dielectric to integrate all of the components of a diffraction grating spectrometer onto a single chip. We have already successfully evaluated the performance of a prototype Micro-Spec, with spectral resolving power, R=64. Here we present our progress towards developing a higher resolution Micro-Spec, which would enable the first science returns in a balloon flight version of this instrument. We describe modifications to the design in scaling from a R=64 to a R=256 instrument, as well as the ultimate performance limits and design concerns when scaling this instrument to higher resolutions.

  12. High mass resolution time of flight mass spectrometer for measuring products in heterogeneous catalysis in highly sensitive microreactors

    DEFF Research Database (Denmark)

    Andersen, Thomas; Jensen, Robert; Christensen, M. K.

    2012-01-01

    response. Gas analysis is performed with a time of flight mass spectrometer with a modified nude Bayard-Alpert ionization gauge as gas ionization source. The mass resolution of the time of flight mass spectrometer using the ion gauge as ionization source is estimated to m∕Δm > 2500. The system design...

  13. Fragmentation reactions of labeled and untabeled Rhodamine B in a high-resolution Fourier transform ion cyclotron resonance mass spectrometer.

    Science.gov (United States)

    Clemen, Martin; Gernert, Claus; Peters, Jonathan; Grotemeyer, Jürgen

    2013-01-01

    The fragmentation reactions of Rhodamine B have been investigated by the use of electrospray ionization mass spectra in a high mass resolving ion cyclotron resonance mass spectrometer. Using high resolution, it could be shown that the loss of 44 mass units from the molecular ion is due to propane; the measured masses were inconsistent with loss of carbon dioxide. These conclusions are supported using deuterium-labeled Rhodamine B. This sample again only shows the loss of fully-deuterated propane verifying the high-resolution data. These findings illustrate very clearly that the conclusions based solely on low resolution spectra were false. The general implication on fragmentations of aromatic acids is discussed.

  14. Study of $\\overline{p}$-Nucleus Interaction with a High Resolution Magnetic Spectrometer

    CERN Multimedia

    2002-01-01

    This experiment uses the high resolution, large solid angle and large momentum acceptance magnetic spectrometer SPES~II to study the interaction between @* and complex nuclei in the following experiments: \\\\ \\\\ \\item 1)~~~~A(@*, @*)A. Angular distribution of @* elastically scattered from |1|2C, |4|0Ca and |2|0|8Pb. \\item 2)~~~~A(@*, @*')A*. Excitation energy spectra and some angular distributions of @* inelastically scattered from |1|2C, |4|0Ca and |2|0|8Pb up to an excitation energy of &prop.~100~MeV. \\item 3)~~~~A(@*, p)A^z^-^1 (@*). Excitation energy spectra for knock out reaction on |6Li, |1|2C, |6|3Cu and |2|0|9Bi at several angles. \\end{enumerate}\\\\ \\\\ Any beam momentum between 300 MeV/c and 800 MeV/c will be suitable for this experiment. In order to vary the effect of strong absorption of @* by nuclei, elastic and inelastic scattering will be performed at two or three different @* momenta (depending on the way LEAR will be operated) down to 300~MeV/c.

  15. Extended-range grazing-incidence spectrometer for high-resolution extreme ultraviolet measurements on an electron beam ion trap

    Energy Technology Data Exchange (ETDEWEB)

    Beiersdorfer, P.; Magee, E. W.; Brown, G. V.; Träbert, E.; Widmann, K. [Lawrence Livermore National Laboratory, Livermore, California 94550 (United States); Hell, N. [Lawrence Livermore National Laboratory, Livermore, California 94550 (United States); Dr. Remeis-Sternwarte and ECAP, Universität Erlangen-Nürnberg, 96049 Bamberg (Germany)

    2014-11-15

    A high-resolution grazing-incidence grating spectrometer has been implemented on the Livermore electron beam ion traps for performing very high-resolution measurements in the soft x-ray and extreme ultraviolet region spanning from below 10 Å to above 300 Å. The instrument operates without an entrance slit and focuses the light emitted by highly charged ions located in the roughly 50 μm wide electron beam onto a cryogenically cooled back-illuminated charge-coupled device detector. The measured line widths are below 0.025 Å above 100 Å, and the resolving power appears to be limited by the source size and Doppler broadening of the trapped ions. Comparisons with spectra obtained with existing grating spectrometers show an order of magnitude improvement in spectral resolution.

  16. High resolution Thomson Parabola Spectrometer for full spectral capture of multi-species ion beams

    Energy Technology Data Exchange (ETDEWEB)

    Alejo, A.; Kar, S., E-mail: s.kar@qub.ac.uk; Ahmed, H.; Doria, D.; Borghesi, M. [Centre for Plasma Physics, School of Mathematics and Physics, Queen’s University Belfast, Belfast BT7 1NN (United Kingdom); Tebartz, A.; Ding, J.; Neumann, N. [Institut für Kernphysik, Technische Universität Darmstadt, Schloßgartenstrasse 9, D-64289 Darmstadt (Germany); Astbury, S.; Carroll, D. C.; Scott, G. G. [Central Laser Facility, Rutherford Appleton Laboratory, Didcot, Oxfordshire OX11 0QX (United Kingdom); Higginson, A.; McKenna, P. [Department of Physics, SUPA, University of Strathclyde, Glasgow G4 0NG (United Kingdom); Wagner, F. [GSI Helmholtzzentrum für Schwerionenforschung GmbH, Planckstraße 1, 64291 Darmstadt (Germany); Roth, M. [Institut für Kernphysik, Technische Universität Darmstadt, Schloßgartenstraße 9, D-64289 Darmstadt (Germany)

    2016-08-15

    We report on the experimental characterisation of laser-driven ion beams using a Thomson Parabola Spectrometer (TPS) equipped with trapezoidally shaped electric plates, proposed by Gwynne et al. [Rev. Sci. Instrum. 85, 033304 (2014)]. While a pair of extended (30 cm long) electric plates was able to produce a significant increase in the separation between neighbouring ion species at high energies, deploying a trapezoidal design circumvented the spectral clipping at the low energy end of the ion spectra. The shape of the electric plate was chosen carefully considering, for the given spectrometer configuration, the range of detectable ion energies and species. Analytical tracing of the ion parabolas matches closely with the experimental data, which suggests a minimal effect of fringe fields on the escaping ions close to the wedged edge of the electrode. The analytical formulae were derived considering the relativistic correction required for the high energy ions to be characterised using such spectrometer.

  17. High resolution Thomson Parabola Spectrometer for full spectral capture of multi-species ion beams.

    Science.gov (United States)

    Alejo, A; Kar, S; Tebartz, A; Ahmed, H; Astbury, S; Carroll, D C; Ding, J; Doria, D; Higginson, A; McKenna, P; Neumann, N; Scott, G G; Wagner, F; Roth, M; Borghesi, M

    2016-08-01

    We report on the experimental characterisation of laser-driven ion beams using a Thomson Parabola Spectrometer (TPS) equipped with trapezoidally shaped electric plates, proposed by Gwynne et al. [Rev. Sci. Instrum. 85, 033304 (2014)]. While a pair of extended (30 cm long) electric plates was able to produce a significant increase in the separation between neighbouring ion species at high energies, deploying a trapezoidal design circumvented the spectral clipping at the low energy end of the ion spectra. The shape of the electric plate was chosen carefully considering, for the given spectrometer configuration, the range of detectable ion energies and species. Analytical tracing of the ion parabolas matches closely with the experimental data, which suggests a minimal effect of fringe fields on the escaping ions close to the wedged edge of the electrode. The analytical formulae were derived considering the relativistic correction required for the high energy ions to be characterised using such spectrometer.

  18. First high-statistics and high-resolution recoil-ion data from the WITCH retardation spectrometer

    Energy Technology Data Exchange (ETDEWEB)

    Finlay, P.; Breitenfeldt, M.; Porobic, T.; Wursten, E.; Couratin, C.; Soti, G.; Severijns, N. [KU Leuven University, Instituut voor Kern-en Stralingsfysica, Leuven (Belgium); Ban, G.; Fabian, X.; Flechard, X.; Lienard, E. [Normandie Univ., ENSICAEN, UNICAEN, CNRS/IN2P3, LPC Caen, Caen (France); Beck, M.; Friedag, P.; Weinheimer, C. [Universitaet Muenster, Institut fuer Kernphysik, Muenster (Germany); Glueck, F.; Kozlov, V.Y. [Karlsruhe Institute of Technology, Institut fuer Kernphysik, Karlsruhe (Germany); Herlert, A. [FAIR, Darmstadt (Germany); Knecht, A. [KU Leuven University, Instituut voor Kern-en Stralingsfysica, Leuven (Belgium); CERN, PH Department, Geneva (Switzerland); Tandecki, M. [TRIUMF, Vancouver BC (Canada); Traykov, E. [CEA/DSM-CNRS/IN2P3, GANIL, Caen (France); Van Gorp, S. [RIKEN, Atomic Physics Laboratory, Saitama (Japan); Zakoucky, D. [ASCR, Nuclear Physics Institute, Rez (Czech Republic)

    2016-07-15

    The first high-statistics and high-resolution data set for the integrated recoil-ion energy spectrum following the β{sup +} decay of {sup 35}Ar has been collected with the WITCH retardation spectrometer located at CERN-ISOLDE. Over 25 million recoil-ion events were recorded on a large-area multichannel plate (MCP) detector with a time-stamp precision of 2 ns and position resolution of 0.1 mm due to the newly upgraded data acquisition based on the LPC Caen FASTER protocol. The number of recoil ions was measured for more than 15 different settings of the retardation potential, complemented by dedicated background and half-life measurements. Previously unidentified systematic effects, including an energy-dependent efficiency of the main MCP and a radiation-induced time-dependent background, have been identified and incorporated into the analysis. However, further understanding and treatment of the radiation-induced background requires additional dedicated measurements and remains the current limiting factor in extracting a beta-neutrino angular correlation coefficient for {sup 35}Ar decay using the WITCH spectrometer. (orig.)

  19. A high-resolution mass spectrometer to measure atmospheric ion composition

    Directory of Open Access Journals (Sweden)

    H. Junninen

    2010-02-01

    Full Text Available In this paper we present recent achievements on developing and testing a tool to detect the composition of ambient ions in the mass/charge range up to 2000 Th. The instrument is an Atmospheric Pressure Interface Time-of-Flight Mass Spectrometer (APi-TOF, Tofwerk AG. Its mass accuracy is better than 0.002%, and the mass resolving power is 3000 Th/Th. In the data analysis, a new efficient Matlab based set of programs (tofTools were developed, tested and used. The APi-TOF was tested both in laboratory conditions and applied to outdoor air sampling in Helsinki at the SMEAR III station. Transmission efficiency calibrations showed a throughput of 0.1–0.5% in the range 100–1300 Th for positive ions, and linearity over 3 orders of magnitude in concentration was determined. In the laboratory tests the APi-TOF detected sulphuric acid-ammonia clusters in high concentration from a nebulised sample illustrating the potential of the instrument in revealing the role of sulphuric acid clusters in atmospheric new particle formation. The APi-TOF features a high enough accuracy, resolution and sensitivity for the determination of the composition of atmospheric small ions although the total concentration of those ions is typically only 400–2000 cm-3. The atmospheric ions were identified based on their exact masses, utilizing Kendrick analysis and correlograms as well as narrowing down the potential candidates based on their proton affinities as well isotopic patterns. In Helsinki during day-time the main negative ambient small ions were inorganic acids and their clusters. The positive ions were more complex, the main compounds were (polyalkyl pyridines and – amines. The APi-TOF provides a near universal interface for atmospheric pressure sampling, and this key feature will be utilized in future laboratory and field studies.

  20. In situ measurement of ions parameters of laser produced ion source using high resolution Thomson Parabola Spectrometer

    Science.gov (United States)

    Chaurasia, S.; Kaur, C.; Rastogi, V.; Poswal, A. K.; Munda, D. S.; Bhatia, R. K.; Nataraju, V.

    2016-08-01

    The laser produced plasma based heavy ion source has become an outstanding front end for heavy ion accelerators. Before being implemented in the heavy ion accelerators its detailed characterization is required. For this purpose, a high resolution and high dispersion Thomson parabola spectrometer comprising of Time-of-Flight diagnostics has been developed for the characterization of ions with energy in the range from 1 keV to 1 MeV/nucleon and incorporated in the Laser plasma experimental chamber. The ion spectrometer is optimized with graphite target. The carbon ions of charge states C1+ to C6+ are observed in the energy range from 3 keV to 300 keV, which has also been verified by Time-of-Flight measurement. Experimental results were matched with simulation done by SIMION 7.0 code which is used for the design of the spectrometer. We also developed data analysis software using Python language to measure in situ ion's parameters and the results are in better agreement to the experimental results than the commercially available software SIMION 7.0. The resolution of the spectrometer is ΔE/E = 0.026 @ 31 keV for charge state (C4+) of carbon.

  1. Ambient Aerosol in Southeast Asia: High Resolution Aerosol Mass Spectrometer Measurements Over Oil Palm (Elaeis guineensis)

    Science.gov (United States)

    Phillips, G.; Dimarco, C.; Misztal, P.; Nemitz, E.; Farmer, D.; Kimmel, J.; Jimenez, J.

    2008-12-01

    The emission of organic compounds in the troposphere is important factor in the formation of secondary organic aerosol (SOA). A very large proportion of organic material emitted globally is estimated to arise from biogenic sources, with almost half coming from tropical and sub-tropical forests. Preliminary analyses of leave cuvette emission studies suggest that oil palm (Elaeis guineensis) is a significantly larger source of isoprene than tropical forest. Much larger sources of isoprene over oil palm allied with a larger anthropogenic component of local emissions contrast greatly with the remote tropical forest environment and therefore the character of SOA formed may differ significantly. These issues, allied with the high price of palm oil on international markets leading to increased use of land for oil palm production, could give rise to rapidly changing chemical and aerosol regimes in the tropics. It is therefore important to understand the current emissions and composition of organic aerosol over all important land-uses in the tropical environment. This in turn will lead to a greater understanding of the present, and to an improvement in predictive capacity for the future system. To help address these issues, a high resolution time of flight aerosol mass spectrometer (HR-ToF-AMS) was deployed in the Sabahmas (PPB OIL) oil palm plantation near Lahad Datu, in Eastern Sabah, as part of the field component of the Aerosol Coupling in the Earth System (ACES) project, part of the UK NERC APPRAISE program. This project was allied closely with measurements made of similar chemical species and aerosol components at a forest site in the Danum Valley as part of the UK Oxidant and Particle Photochemical Processes above a Southeast Asian tropical rainforest (OP3) project. Measurements of submicron non- refractory aerosol composition are presented along with some preliminary analysis of chemically resolved aerosol fluxes made with a new eddy covariance system, based on the

  2. Analytical calculations and Monte-Carlo simulations of a high-resolution backscattering spectrometer for the long wavelength target station at the Spallation neutron source

    Energy Technology Data Exchange (ETDEWEB)

    Bordallo, H.N. E-mail: bordallo@hmi.de; Herwig, K.W.; Zsigmond, G

    2002-09-21

    Using the Monte-Carlo simulation programs McStas and VITESS, we present the design principles of the proposed high-resolution inverse geometry spectrometer on the Spallation neutron source (SNS) - long wavelength target station (LWTS). LWTS will enable the combination of large energy and momentum transfer ranges with energy resolution. Indeed the resolution of this spectrometer lie between that routinely achieved by spin echo techniques and the design goal of the high-power target station (HPTS) backscattering spectrometer. This niche of energy resolution is interesting for the study of slow motions of large objects and we are led to the domain of large molecules - polymers and biological molecules.

  3. Analytical calculations and Monte-Carlo simulations of a high-resolution backscattering spectrometer for the long wavelength target station at the Spallation neutron source

    CERN Document Server

    Bordallo, H N; Zsigmond, G

    2002-01-01

    Using the Monte-Carlo simulation programs McStas and VITESS, we present the design principles of the proposed high-resolution inverse geometry spectrometer on the Spallation neutron source (SNS) - long wavelength target station (LWTS). LWTS will enable the combination of large energy and momentum transfer ranges with energy resolution. Indeed the resolution of this spectrometer lie between that routinely achieved by spin echo techniques and the design goal of the high-power target station (HPTS) backscattering spectrometer. This niche of energy resolution is interesting for the study of slow motions of large objects and we are led to the domain of large molecules - polymers and biological molecules.

  4. Arcus: an ISS-attached high-resolution x-ray grating spectrometer

    Science.gov (United States)

    Smith, R. K.; Ackermann, M.; Allured, R.; Bautz, M. W.; Bregman, J.; Bookbinder, J.; Burrows, D.; Brenneman, L.; Brickhouse, N.; Cheimets, P.; Carrier, A.; Freeman, M.; Kaastra, J.; McEntaffer, R.; Miller, J.; Ptak, A.; Petre, R.; Vacanti, G.

    2014-07-01

    We present the design and scientific motivation for Arcus, an X-ray grating spectrometer mission to be deployed on the International Space Station. This mission will observe structure formation at and beyond the edges of clusters and galaxies, feedback from supermassive black holes, the structure of the interstellar medium and the formation and evolution of stars. The mission requirements will be R>2500 and >600 cm2 of effective area at the crucial O VII and O VIII lines, values similar to the goals of the IXO X-ray Grating Spectrometer. The full bandpass will range from 8-52Å (0.25-1.5 keV), with an overall minimum resolution of 1300 and effective area >150 cm2. We will use the silicon pore optics developed at cosine Research and proposed for ESA's Athena mission, paired with off-plane gratings being developed at the University of Iowa and combined with MIT/Lincoln Labs CCDs. This mission achieves key science goals of the New Worlds, New Horizons Decadal survey while making effective use of the International Space Station (ISS).

  5. High-resolution Fourier-transform spectrometer chip with microphotonic silicon spiral waveguides.

    Science.gov (United States)

    Velasco, Aitor V; Cheben, Pavel; Bock, Przemek J; Delâge, André; Schmid, Jens H; Lapointe, Jean; Janz, Siegfried; Calvo, María L; Xu, Dan-Xia; Florjańczyk, Mirosław; Vachon, Martin

    2013-03-01

    We report a stationary Fourier-transform spectrometer chip implemented in silicon microphotonic waveguides. The device comprises an array of 32 Mach-Zehnder interferometers (MZIs) with linearly increasing optical path delays between the MZI arms across the array. The optical delays are achieved by using Si-wire waveguides arranged in tightly coiled spirals with a compact device footprint of 12 mm2. Spectral retrieval is demonstrated in a single measurement of the stationary spatial interferogram formed at the output waveguides of the array, with a wavelength resolution of 40 pm within a free spectral range of 0.75 nm. The phase and amplitude errors arising from fabrication imperfections are compensated using a transformation matrix spectral retrieval algorithm.

  6. a Decade-Spanning High-Resolution Asynchronous Optical Sampling Based Terahertz Time-Domain Spectrometer

    Science.gov (United States)

    Good, Jacob T.; Holland, Daniel; Finneran, Ian A.; Carroll, Brandon; Allodi, Marco A.; Blake, Geoffrey

    2015-06-01

    High-resolution ASynchronous OPtical Sampling (ASOPS) is a technique that substantially improves the combined frequency resolution and bandwidth of ASOPS based TeraHertz Time-Domain Spectroscopy (THz-TDS) systems. We employ two mode-locked femtosecond Ti:Sapphire oscillators with repetition frequencies of 80 MHz operating at a fixed repetition frequency offset of 100 Hz. This offset lock is maintained by a Phase-Locked Loop (PLL) operating at the 60th harmonic of the repetition rate of the Ti:Sapphire oscillators. Their respective time delay is scanned across 12.5 ns requiring a scan time of 10 ms, supporting a time delay resolution of up to 15.6 fs. ASOPS-THz-TDS enables high-resolution spectroscopy that is impossible for a THz-TDS system employing a mechanical delay stage. We measure a timing jitter of 1.36 fs for the system using an air-gap etalon and an optical cross-correlator. We report a Root-Mean-Square deviation of 20.7 MHz and a mean deviation of 14.4 MHz for water absorption lines from 0.5 to 2.7. High-resolution ASOPS-THz-TDS enables high resolution spectroscopy of both gas-phase and condensed-phase samples across a decade of THz bandwidth.

  7. Fiber-coupled high resolution infrared array spectrometer for the Kuiper Airborne Observatory

    Science.gov (United States)

    Glenar, D. A.; Reuter, D.; Mumma, M. J.; Chin, G.; Wiedemann, G.; Jennings, D.

    1990-01-01

    A novel cryogenic grating spectrometer (FCAS) is being designed for observations of volatiles in cometary and planetary atmospheres, and in newly forming planetary systems. The instrument features two-dimensional detector arrays coupled to a high-dispersion echelle by infrared fibers, and will achieve a spectral resolving power of about 40,000. The primary observational platform for this instrument will be the Kuiper Airborne Observatory, but it will also be configured for use at ground-based observatories. Initially, the spectrometer will use a 58 x 62, 1- to 5-micron InSb array. Larger-format IR arrays and arrays of different composition, will later be incorporated as they become available. The instrument will be used in two modes. The first uses a large format IR array in the spectral image plane for the customary one-dimensional spectral-one-dimensional spatial coverage. In the second mode, a massive, coherent bundle of infrared transmitting ZrF4 fibers will be installed after the dispersive element, to reformat the two-dimensional array into an elongated one-dimensional array for wide spectral coverage, allowing multiple lines to be measured in a single integration with high sensitivity. The overall instrument design is discussed, and the system sensitivity is estimated.

  8. A diamond 14 MeV neutron energy spectrometer with high energy resolution

    Energy Technology Data Exchange (ETDEWEB)

    Shimaoka, Takehiro, E-mail: t.shimaoka@eng.hokudai.ac.jp; Kaneko, Junichi H.; Tsubota, Masakatsu; Shimmyo, Hiroaki [Graduate School of Engineering, Hokkaido University, Kita 13, Nishi 8, Kita-ku, Sapporo, Hokkaido 060-8628 (Japan); Ochiai, Kentaro [Fusion Research and Development Directorate, Japan Atomic Energy Agency, Tokai-mura, Naka-gun, Ibaraki 319-1195 (Japan); Chayahara, Akiyoshi; Umezawa, Hitoshi; Shikata, Shin-ichi [National Institute of Advanced Industrial Science and Technology (AIST), 1-8-31 Midorigaoka, Ikeda, Osaka 563-8577 (Japan); Watanabe, Hideyuki [National Institute of Advanced Industrial Science and Technology, 1-1-1 Higashi, Tsukuba, Ibaraki 305-8565 (Japan); Isobe, Mitsutaka; Osakabe, Masaki [National Institute for Fusion Science, 322-6, Oroshi-cho, Toki-City, Gifu 509-5292 (Japan)

    2016-02-15

    A self-standing single-crystal chemical vapor deposited diamond was obtained using lift-off method. It was fabricated into a radiation detector and response function measurements for 14 MeV neutrons were taken at the fusion neutronics source. 1.5% of high energy resolution was obtained by using the {sup 12}C(n, α){sup 9}Be reaction at an angle of 100° with the deuteron beam line. The intrinsic energy resolution, excluding energy spreading caused by neutron scattering, slowing in the target and circuit noises was 0.79%, which was also the best resolution of the diamond detector ever reported.

  9. Matrix-assisted ionization vacuum for high-resolution Fourier transform ion cyclotron resonance mass spectrometers.

    Science.gov (United States)

    Wang, Beixi; Tisdale, Evgenia; Trimpin, Sarah; Wilkins, Charles L

    2014-07-15

    Matrix-assisted ionization vacuum (MAIV) produces charge states similar to electrospray ionization (ESI) from the solid state without requiring high voltage or added heat. MAIV differs from matrix-assisted laser desorption/ionization (MALDI) in that no laser is needed and abundant multiply charged ions are produced from molecules having multiple basic sites such as proteins. Here we introduce simple modifications to the commercial vacuum MALDI and ESI sources of a 9.4 T Fourier transform-ion cyclotron resonance (FT-ICR) mass spectrometer to perform MAIV from both intermediate and atmospheric pressure. The multiply charged ions are shown for the proteins bovine insulin, ubiquitin, and lysozyme using 3-nitrobenzonitrile as matrix. These are the first examples of MAIV operating at pressures as low as 10(-6) mbar in an FT-ICR mass spectrometer source, and the expected mass resolving power of 100000 to 400000 is achieved. Identical protein charge states are observed with and without laser ablation indicating minimal, if any, role of photochemical ionization for the compounds studied.

  10. Influence of the thorium decay series on the background of high-resolution gamma-ray spectrometers.

    Science.gov (United States)

    Bučar, K; Korun, M; Vodenik, B

    2012-06-01

    The background induced by the members of the thorium decay sequence in six high-resolution, gamma-ray spectrometers was analyzed. For the analysis, the count rates in the peaks of the background spectra, normalized to the unit of emission probability and detection probability, were used. The energy dependence of these normalized count rates carries information about the location of the sources of contamination. The contributions of the detector contamination, the contamination of the shielding material and the radiation penetrating the shield were calculated. The comparison of these contributions among the spectrometers pointed to the weaknesses of some shields, making such a comparison a useful tool for assessing the effectiveness of the shields.

  11. High resolution {gamma}-spectroscopy at the big-bite spectrometer

    Energy Technology Data Exchange (ETDEWEB)

    Savran, D.; Ramspeck, K.; Zilges, A. [Technische Univ. Darmstadt (Germany). Inst. fuer Kernphysik; Berg, A.M. van den; Harakeh, M.N.; Woertche, H.J. [Kernfysisch Versneller Inst. (KVI), Groningen (Netherlands)

    2006-04-05

    An array of HPGe detectors has been set up at the Big-Bite Spectrometer at AGOR cyclotron of KVI Groningen to allow coincident measurements of the {gamma}-decay of nuclei excited in inelastic hadron scattering at 100-400 MeV incident energies. Compared to previous experiments, where NaI detectors have been used, the energy resolution of the {gamma}-detection could be improved by more than one order of magnitude to about {delta}E{sub {gamma}}/E{sub {gamma}}=0.2 % in the energy region of interest. The coincident measurement of the {gamma}-decay in inelastic hadron scattering experiments is very useful for the separation of nearby excitations, the assignment of multipolarities, the determination of branching ratios and to study the isospin character of bound excitations. The experimental setup and the results of a first ({alpha},{alpha}'{gamma}) test experiment at E{sub {alpha}}=136 MeV on {sup 58}Ni are presented. (orig.)

  12. The High-Resolution X-Ray Microcalorimeter Spectrometer, SXS, on Astro-H

    Science.gov (United States)

    Mitsuda, Kazuhisa; Kelley, Richard L.; Boyce, Kevin R.; Brown, Gregory V.; Costantini, Elisa; DiPirro, Michael J.; Ezoe, Yuichiro; Fujimoto, Ryuichi; Gendreau, Keith C.; denHerder, Jan-Willem; Hoshino, Akio; Ishisaki, Yoshitaka; Kilbourne, Caroline A.; Kitamoto, Shunji; McCammon, Dan; Murakami, Masahide; Murakami, Hiroshi; Ogawa, Mina; Ohashi, Takaya; Okamoto, Atsushi; Paltani, Stephane; Pohl, Martin; Porter, F. Scott; Sato, Yoichi; Shinozaki, Keisuke

    2012-01-01

    The science and an overview of the Soft X-ray Spectrometer onboard the STRO-H mission are presented. The SXS consists of X-ray focusing mirrors and a microcalorimeter array and is developed by international collaboration lead by JAXA and NASA with European participation. The detector is a 6 x 6 format microcalorimeter array operated at a cryogenic temperature of 50 mK and covers a 3' x 3' field of view of the X-ray telescope of 5.6 m focal length. We expect an energy resolution better than 7 eV (FWHM, requirement) with a goal of 4 eV. The effective area of the instrument will be 225 square centimeters at 7 keV; by a factor of about two larger than that of the X-ray microcalorimeter on board Suzaku. One of the main scientific objectives of the SXS is to investigate turbulent and/or macroscopic motions of hot gas in clusters of galaxies.

  13. A high-resolution time-of-flight spectrometer for fission fragments and ion beams

    Energy Technology Data Exchange (ETDEWEB)

    Kosev, Krasimir Milchev

    2007-07-01

    For the purpose of fission-fragment detection a double time-of-flight (TOF) spectrometer has been developed. The key component of the TOF spectrometer is a TOF detector consisting of multichannel-plate (MCP) detectors with a position-sensitive readout, a foil for secondary electron (SE) production and an electrostatic mirror. The fission fragments are detected by measuring the SEs impinging on the position-sensitive anode after emission from the foil, acceleration and deflection by the electrostatic mirror. The functionality of the different detector components is proven in detail. Optimised schemes for the high-voltage supplies of the MCP detectors have been implemented successfully. In order to process the multichannel-plate detector signals optimally, a new state-of-the-art constant-fraction discriminator based on the amplitude and rise time compensated technique with very low threshold capabilities and optimised walk properties has been developed and incorporated into the setup. In a setup consisting of two mirror MCP detectors, we could successfully observe the TOF spectrum of a mixed ({sup 226}Ra,{sup 222}Rn,{sup 210}Po,{sup 218}Po,{sup 214}Po) {alpha}-source. Testing photo-fission experiments were performed at the bremsstrahlung facility at the ELBE accelerator. The setup consisted of two mirror detectors (first arm) and a 80 mm diameter MCP detector (second arm) with a {sup 238}U target positioned in between. TOF measurements with two bremsstrahlung end-point energies of 12.9 and 16.0 MeV were carried out. A clear cut separation of the TOF peaks for the medium-mass and heavy fission fragments was observed. (orig.)

  14. [Study and design on Dyson imaging spectrometer in spectral broadband with high resolution].

    Science.gov (United States)

    Yan, Ling-Wei

    2014-04-01

    The paper designs and improves a telecentric imaging spectrometer, the Dyson imaging spectrometer. The optical structure of the imaging spectrometer is simple and compact, which is only composed of a hemispherical lens and a concave grating. Based on the Rowland circle and refraction theory, the broadband anastigmatic imaging condition of Dyson imaging spectrometer which is the ratio of the grating radius and hemispherical lens radius has been analyzed. By imposing this condition for two different wavelengths, the parameters of the optical system presenting low aberrations and excellent imaging quality are obtained. To make the design spectrometer more suitable for the engineering application, the paper studies the method making the detector not to attach the surface of the hemispherical lens. A design example using optimal conditions was designed to prove our theory. The Dyson imaging spectrometer of which the imaging RMS radii are less than 2.5 microm and the advanced spectrometer of which the imaging RMS radii are less than 8 microm, with NA 0.33, waveband 0.38-1.7 microm and the slit length 15 mm, have been obtained. The design method and results are more feasible and predominant, and can be applied in the areas of the industry and remote sensing.

  15. High spatial resolution imaging of methane and other trace gases with the airborne Hyperspectral Thermal Emission Spectrometer (HyTES)

    Science.gov (United States)

    Hulley, Glynn C.; Duren, Riley M.; Hopkins, Francesca M.; Hook, Simon J.; Vance, Nick; Guillevic, Pierre; Johnson, William R.; Eng, Bjorn T.; Mihaly, Jonathan M.; Jovanovic, Veljko M.; Chazanoff, Seth L.; Staniszewski, Zak K.; Kuai, Le; Worden, John; Frankenberg, Christian; Rivera, Gerardo; Aubrey, Andrew D.; Miller, Charles E.; Malakar, Nabin K.; Sánchez Tomás, Juan M.; Holmes, Kendall T.

    2016-06-01

    Currently large uncertainties exist associated with the attribution and quantification of fugitive emissions of criteria pollutants and greenhouse gases such as methane across large regions and key economic sectors. In this study, data from the airborne Hyperspectral Thermal Emission Spectrometer (HyTES) have been used to develop robust and reliable techniques for the detection and wide-area mapping of emission plumes of methane and other atmospheric trace gas species over challenging and diverse environmental conditions with high spatial resolution that permits direct attribution to sources. HyTES is a pushbroom imaging spectrometer with high spectral resolution (256 bands from 7.5 to 12 µm), wide swath (1-2 km), and high spatial resolution (˜ 2 m at 1 km altitude) that incorporates new thermal infrared (TIR) remote sensing technologies. In this study we introduce a hybrid clutter matched filter (CMF) and plume dilation algorithm applied to HyTES observations to efficiently detect and characterize the spatial structures of individual plumes of CH4, H2S, NH3, NO2, and SO2 emitters. The sensitivity and field of regard of HyTES allows rapid and frequent airborne surveys of large areas including facilities not readily accessible from the surface. The HyTES CMF algorithm produces plume intensity images of methane and other gases from strong emission sources. The combination of high spatial resolution and multi-species imaging capability provides source attribution in complex environments. The CMF-based detection of strong emission sources over large areas is a fast and powerful tool needed to focus on more computationally intensive retrieval algorithms to quantify emissions with error estimates, and is useful for expediting mitigation efforts and addressing critical science questions.

  16. Development of high resolution arrayed waveguide grating spectrometers for astronomical applications: first results

    CERN Document Server

    Gatkine, Pradip; Hu, Yiwen; Zhu, Tiecheng; Meng, Yang; Bland-Hawthorn, Joss; Dagenais, Mario

    2016-01-01

    Astrophotonics is the next-generation approach that provides the means to miniaturize near-infrared (NIR) spectrometers for upcoming large telescopes and make them more robust and inexpensive. The target requirements for our spectrograph are: a resolving power of about 3000, wide spectral range (J and H bands), free spectral range of about 30 nm, high on-chip throughput of about 80% (-1dB) and low crosstalk (high contrast ratio) between adjacent on-chip wavelength channels of less than 1% (-20dB). A promising photonic technology to achieve these requirements is Arrayed Waveguide Gratings (AWGs). We have developed our first generation of AWG devices using a silica-on-silicon substrate with a very thin layer of silicon-nitride in the core of our waveguides. The waveguide bending losses are minimized by optimizing the geometry of the waveguides. Our first generation of AWG devices are designed for H band and have a resolving power of around 1500 and free spectral range of about 10 nm around a central wavelength ...

  17. Compact High-Resolution Broad-Band Terahertz Fabry-Perot Spectrometer Project

    Data.gov (United States)

    National Aeronautics and Space Administration — Our objective is to develop a compact scanning Fabry-Perot spectrometer, for satellite far-infrared astronomy and Earth remote sensing, that operates at wavelengths...

  18. Calibration of the OHREX high-resolution imaging crystal spectrometer at the Livermore electron beam ion traps

    Science.gov (United States)

    Hell, N.; Beiersdorfer, P.; Magee, E. W.; Brown, G. V.

    2016-11-01

    We report the calibration of the Orion High-Resolution X-ray (OHREX) imaging crystal spectrometer at the EBIT-I electron beam ion trap at Livermore. Two such instruments, dubbed OHREX-1 and OHREX-2, are fielded for plasma diagnostics at the Orion laser facility in the United Kingdom. The OHREX spectrometer can simultaneously house two spherically bent crystals with a radius of curvature of r = 67.2 cm. The focusing properties of the spectrometer allow both for larger distance to the source due to the increase in collected light and for observation of extended sources. OHREX is designed to cover a 2.5°-3° spectral range at Bragg angles around 51.3°. The typically high resolving powers at these large Bragg angles are ideally suited for line shape diagnostics. For instance, the nominal resolving power of the instrument (>10 000) is much higher than the effective resolving power associated with the Doppler broadening due to the temperature of the trapped ions in EBIT-I. The effective resolving power is only around 3000 at typical EBIT-I conditions, which nevertheless is sufficient to set up and test the instrument's spectral characteristics. We have calibrated the spectral range for a number of crystals using well known reference lines in the first and second order and derived the ion temperatures from these lines. We have also made use of the 50 μm size of the EBIT-I source width to characterize the spatial focusing of the spectrometer.

  19. Calibration of the OHREX high-resolution imaging crystal spectrometer at the Livermore electron beam ion traps

    Energy Technology Data Exchange (ETDEWEB)

    Hell, N. [Lawrence Livermore National Laboratory, Livermore, California 94550 (United States); Dr. Remeis-Sternwarte and ECAP, Universität Erlangen-Nürnberg, Bamberg 96049 (Germany); Beiersdorfer, P.; Magee, E. W.; Brown, G. V. [Lawrence Livermore National Laboratory, Livermore, California 94550 (United States)

    2016-11-15

    We report the calibration of the Orion High-Resolution X-ray (OHREX) imaging crystal spectrometer at the EBIT-I electron beam ion trap at Livermore. Two such instruments, dubbed OHREX-1 and OHREX-2, are fielded for plasma diagnostics at the Orion laser facility in the United Kingdom. The OHREX spectrometer can simultaneously house two spherically bent crystals with a radius of curvature of r = 67.2 cm. The focusing properties of the spectrometer allow both for larger distance to the source due to the increase in collected light and for observation of extended sources. OHREX is designed to cover a 2.5°–3° spectral range at Bragg angles around 51.3°. The typically high resolving powers at these large Bragg angles are ideally suited for line shape diagnostics. For instance, the nominal resolving power of the instrument (>10 000) is much higher than the effective resolving power associated with the Doppler broadening due to the temperature of the trapped ions in EBIT-I. The effective resolving power is only around 3000 at typical EBIT-I conditions, which nevertheless is sufficient to set up and test the instrument’s spectral characteristics. We have calibrated the spectral range for a number of crystals using well known reference lines in the first and second order and derived the ion temperatures from these lines. We have also made use of the 50 μm size of the EBIT-I source width to characterize the spatial focusing of the spectrometer.

  20. High-resolution, high-transmission soft x-ray spectrometer for the study of biological samples

    Energy Technology Data Exchange (ETDEWEB)

    Fuchs, Oliver; Weinhardt, L.; Blum, M.; Welgand, M.; Umbach, E.; Bar, M.; Heske, C.; Denlinger, J.; Chuang, Y.-D.; McKinney, W.; Hussain, Z.; Gullikson, E.; Jones, M.; Batson, P.; Nelles, B.; Follath, R.

    2009-06-11

    We present a variable line-space grating spectrometer for soft s-rays that coverst the photon energy range between 130 and 650 eV. The optical design is based on the Hettrick-Underwood principle and tailored to synchrotron-based studies of radiation-sensitive biological samples. The spectrometer is able to record the entire spectral range in one shot, i.e., without any mechanical motion, at a resolving power of 1200 or better. Despite is slitless design, such a resolving power can be achieved for a source spot as large as (30 x 3000) micrometers squared, which is important for keeping beam damage effects in radiation-sensitive samples low. The high spectrometer efficiency allows recording of comprehensive two-dimensional resonant inelastic soft x-ray scatters (RIXS) maps with good statistics within several minutes. This is exemplarily demonstrated for a RIXS map of highly oriented pyrolytic graphite, which was taken with 10 min.

  1. High-resolution, high-transmission soft x-ray spectrometer for the study of biological samples

    Energy Technology Data Exchange (ETDEWEB)

    Fuchs, Oliver; Weinhardt, L.; Blum, M.; Weigand, M.; Umbach, E.; Bar, M.; Heske, Clemens; Denlinger, Jonathan; Chuang, Y.-D.; McKinney, Wayne; Hussain, Zahid; Gullikson, Eric; Jones, M.; Batson, Phil; Nelles, B.; Follath, R.

    2009-03-09

    We present a variable line-space grating spectrometer for soft x-rays that covers the photon energy range between 130 and 650 eV. The optical design is based on the Hettrick-Underwood principle and tailored to synchrotron-based studies of radiation-sensitive biological samples. The spectrometer is able to record the entire spectral range in one shot, i.e., without any mechanical motion, at a resolving power of 1200 or better. Despite its slitless design, such a resolving power can be achieved for a source spot as large as 30x3000 mu m2, which is important for keeping beam damage effects in radiation-sensitive samples low. The high spectrometer efficiency allows recording of comprehensive two-dimensional resonant inelastic soft x-ray scattering (RIXS) maps with good statistics within several minutes. This is exemplarily demonstrated for a RIXS map of highly oriented pyrolytic graphite, which was taken within 10 min.

  2. High-resolution mid-IR spectrometer based on frequency upconversion

    DEFF Research Database (Denmark)

    Hu, Qi; Dam, Jeppe Seidelin; Pedersen, Christian

    2012-01-01

    allowing for direct detection with a silicon-based CCD camera. This approach allows for low noise detection even without cooling of the detector. A setup is realized for the 3xA0;x3BC;m regime with a spectral resolution of 0.2xA0;nm using lithium niobate as the nonlinear material and mixing with a single......We demonstrate a novel approach for high-resolution spectroscopy based on frequency upconversion and postfiltering by means of a scanning Fabryx2013;Perot interferometer. The system is based on sum-frequency mixing, shifting the spectral content from the mid-infrared to the near-visible region...

  3. [The rapid analysis of polychlorinated quaterphenyls in blood using different diameter capillary column with the high-resolution gas chromatograph high-resolution mass spectrometer].

    Science.gov (United States)

    Yasutake, Daisuke; Ashizuka, Yuki; Hori, Tsuguhide; Kurokawa, Youichi; Kajiwara, Jumboku; Hirata, Teruaki; Ishiguro, Yasuhisa; Iida, Takao; Uchi, Hiroshi; Furue, Masutaka

    2011-04-01

    The polychlorinated quaterphenyl (PCQ) concentrations in blood are important discriminative parameters in yusho patient. In this study, a rapid analytical method for PCQ using different diameter capillary column (rapid-Rtx65TG) with high-resolution gas chromatograph high-resolution mass spectrometer (HRGC/HRMS) instead of the gas chromatograph electron capture detector (ECD/GC) was developed. Using different diameter capillary columns, the analysis time of the HRGC/HRMS was drastically shortened, and the detection sensitivity was improved. In the rapid-Rtx65TG column, a small-bore capillary column (length 1m, I.D. 0.1mm) was connected with the inlet side of the GC, and behind that column, a large-bore capillary column (length 15mm, I.D. 0.53mm) for octadecachloroquaterphenyl (ODCQ) analysis was connected. In the HRGC/HRMS measurement of ODCQ by the rapid-Rtx65TG column, the minimum limit of detection for the apparatus was 0.4 pg, and the minimum limit of determination for the blood was 0.008 ppb. On ECD/GC in the conventional method and HRGC/HRMS in this study, the PCQ concentration in blood including yusho patients and yusho suspected persons was almost equivalent.

  4. Experiments with the High Resolution Kaon Spectrometer at Jlab Hall C and the New Spectroscopy of ^12_Lambda B Hypernuclei

    Energy Technology Data Exchange (ETDEWEB)

    Tang, Liguang; Chen, Chunhua; Gogami, Toshiyuki; Kawama, Daisuke; Han, Yuncheng; Yuan, Lulin; Matsumura, Akihiko; Okayasu, Yuichi; Seva, Tomislav; Rodriguez, Victor; Baturin, Pavlo; Acha Quimper, Armando; Achenbach, Carsten; Ahmidouch, Abdellah; Albayrak, Ibrahim; Androic, Darko; Asaturyan, Arshak; Asaturyan, Razmik; Ates, Ozgur; Badui, Rafael; Baker, Oliver; Benmokhtar, Fatiha; Boeglin, Werner; Bono, Jason; Bosted, Peter; Brash, Edward; Carter, Philip; Carlini, Roger; Chiba, Atsushi; Christy, Michael; Cole, Leon; Dalton, Mark; Danagoulian, Samuel; Daniel, Aji; De Leo, Raffaele; Dharmawardane, Kahanawita; Doi, Daisuke; Egiyan, Kim; Elaasar, Mostafa; Ent, Rolf; Fenker, Howard; Fujii, Yu; Furic, Miroslav; Gabrielyan, Marianna; Gan, Liping; Garibaldi, Franco; Gaskell, David; Gasparian, Ashot; Gibson, Edward; Gueye, Paul; Hashimoto, Osamu; Honda, D; Horn, Tanja; Hu, Bitao; Hungerford, Ed; Jayalath, Chandana; Jones, Mark; Johnston, Kathleen; Kalantarians, Narbe; Kanda, Hiroki; Kaneta, M; Kato, F; Kato, Seigo; Kawai, Masaharu; Keppel, Cynthia; Khanal, Hari; Kohl, M; Kramer, Laird; Lan, Kejian; Li, Ya; Habarakada Liyanage, Anusha; Luo, Wei; Mack, David; Maeda, Kazushige; Malace, Simona; Margaryan, Amur; Marikyan, Gagik; Markowitz, Pete; Maruta, Tomofumi; Maruyama, Nayuta; Maxwell, Victor; Millener, David; Miyoshi, Toshinobu; Mkrtchyan, Arthur; Mkrtchyan, Hamlet; Motoba, Toshio; Nagao, Sho; Nakamura, Satoshi; Narayan, Amrendra; Neville, Casey; Niculescu, Gabriel; Niculescu, Maria; Nunez, Angel; Nuruzzaman, nfn; Nomura, Hiroshi; Nonaka, Kenichi; Ohtani, Atsushi; Oyamada, Masamichi; Perez, Naipy; Petkovic, Tomislav; Pochodzalla, J; Qiu, Xiyu; Randeniya, Kapugodage; Raue, Brian; Reinhold, Joerg; Rivera, R; Roche, Julie; Samanta, Chhanda; Sato, Yoshinori; Sawatzky, Bradley; Segbefia, Edwin; Schott, Diane; Shichijo, Ayako; Simicevic, Neven; Smith, Gregory; Song, Yushou; Sumihama, Mizuki; Tadevosyan, Vardan; Takahashi, Toshiyuki; Taniya, Naotaka; Tsukada, Kyo; Tvaskis, Vladas; Veilleux, Micah; Vulcan, William; Wells, Steven; Wesselmann, Frank; Wood, Stephen; Yamamoto, Taku; Yan, Chen; Ye, Z; Yokota, Kosuke; Zhamkochyan, Simon; Zhu, Lingyan

    2014-09-01

    Since the pioneering experiment, E89-009 studying hypernuclear spectroscopy using the $(e,e^{\\prime}K^+)$ reaction was completed, two additional experiments, E01-011 and E05-115, were performed at Jefferson Lab. These later experiments used a modified experimental design, the "Tilt Method", to dramatically suppress the large electromagnetic background, and allowed for a substantial increase in luminosity. Additionally, a new kaon spectrometer, HKS (E01-011), a new electron spectrometer, HES, and a new splitting magnet were added to produce precision, high-resolution hypernuclear spectroscopy. These two experiments, E01-011 and E05-115, resulted in two new data sets, producing sub-MeV energy resolution in the spectra of ${}^{7}_{\\Lambda}\\text{He}$, ${}^{12}_{\\Lambda}\\text{B}$ and ${}^{28}_{\\Lambda} \\text{Al}$ and ${}^{7}_{\\Lambda}\\text{He}$, ${}^{10}_{\\Lambda}\\text{Be}$, ${}^{12}_{\\Lambda}\\text{B}$ and ${}^{52}_{\\Lambda}\\text{V}$. All three experiments obtained a ${}^{12}_{\\Lambda}\\text{B}$, spectrum, which is the most characteristic $p$-shell hypernucleus and is commonly used for calibration. Independent analyses of these different experiments demonstrate excellent consistency and provide the clearest level structure to date of this hypernucleus as produced by the $(e,e^{\\prime}K^+)$ reaction. This paper presents details of these experiments, and the extraction and analysis of the observed ${}^{12}_{\\Lambda}\\text{B}$ spectrum.

  5. Progress, Performance, and Prospects of Ultra-High Resolution Microcalorimeter Spectrometers

    Energy Technology Data Exchange (ETDEWEB)

    Hoover, Andrew Scott [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Bennett, D. A. [National Inst. of Standards and Technology (NIST), Boulder, CO (United States); Croce, Mark Philip [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Rabin, Michael W. [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Ullom, J. N. [National Inst. of Standards and Technology (NIST), Boulder, CO (United States); Univ. of Colorado, Boulder, CO (United States)

    2017-01-23

    In 2005 the LANL/NIST team used a single high-resolution microcalorimeter detector to measure the gamma-ray spectrum of a plutonium sample. After more than a decade of research and development on this topic, both the technology and our general understanding of its capabilities have advanced greatly, such that a progress review is now timely. We examine the scenario of a large-scale reprocessing plant and conclude that current non-destructive analysis (NDA) methods are inadequate to safeguard such a facility to the desired levels, leading to undesirable dependence on massspectrometry (MS) destructive analysis (DA). The development of microcalorimeter detectors is intended to close the performance gap between NDA and DA methods to address the needs of nuclear facilities.

  6. Conception of broadband stigmatic high-resolution spectrometers for the soft X-ray range

    Energy Technology Data Exchange (ETDEWEB)

    Vishnyakov, E A; Shatokhin, A N; Ragozin, E N [P N Lebedev Physics Institute, Russian Academy of Sciences, Moscow (Russian Federation)

    2015-04-30

    We formulate an approach to the development of stigmatic high-resolution spectral instruments for the soft X-ray range (λ ≤ 300 Å), which is based on the combined operation of normalincidence multilayer mirrors (including broadband aperiodic ones) and grazing-incidence reflection gratings with nonequidistant grooves (so-called VLS gratings). A concave multilayer mirror serves to produce a slightly astigmatic image of the radiation source (for instance, an entrance slit), and the diffraction grating produces a set of its dispersed stigmatic spectral images. The width of the operating spectral region is determined by the aperiodic structure of the multilayer mirror and may range up to an octave in wavelength. (laser applications and other topics in quantum electronics)

  7. SONGS - A high resolution imaging gamma-ray spectrometer for the Space Station

    Science.gov (United States)

    Nakano, G. H.; Chase, L. F.; Kilner, J. R.; Sandie, W. G.; Fishman, G. J.; Paciesas, W. S.

    1989-11-01

    The overall design and the instrumental features of the Space-Station Observer for Nuclear Gamma-ray Spectroscopy (SONGS) instrument are described. SONGS comprises an array of 19 two-segment n-type Ge detectors, which have the capability of determining the interaction site in either the upper or the lower segment or in both segments. The detectors provide high energy resolution of 1 keV at 100 keV and of 2 keV at 1 MeV. The close-packed Ge sensor array provides a natural sensitivity for the measurement of gamma ray polarization in the 100 keV to 1 MeV energy range, making it possible to obtain information on the structure of the magnetosphere of neutron stars and of the accretion disk of black holes.

  8. Mobile high-resolution time-of-flight mass spectrometer for in-situ analytics

    Energy Technology Data Exchange (ETDEWEB)

    Lang, Johannes; Ebert, Jens [II. Physikalisches Institut, JLU, Giessen (Germany); Dickel, Timo; Geissel, Hans; Plass, Wolfgang; Scheidenberger, Christoph [II. Physikalisches Institut, JLU, Giessen (Germany); GSI, Darmstadt (Germany)

    2011-07-01

    A compact multiple-reflection time-of-flight mass spectrometer (MR-TOF-MS) has been developed. For the first time it allows for mass measurements with a resolving power exceeding 100000 and sub ppm accuracy in a mobile device. Thus it allows to resolve isobars and enables to accurately determine the composition and structure of biomolecules. The MR-TOF-MS consists of an atmospheric pressure interface for DESI and REIMS, ion cooler, ion trap, time-of-flight analyzer, MCP detector and DAQ. Vacuum system components, power supplies as well as electronics are mounted together with the ion optical spectrometer parts on a single frame with a total volume of 0.8 m{sup 3}. Applications of the device within the AmbiProbe research program include in-situ mass spectrometry such as real-time tissue recognition in electrosurgery, identification of mycotoxins and analysis of soil samples for environmental studies.

  9. High-energy resolution Thomson Parabola spectrometer for laser plasma diagnostics

    Energy Technology Data Exchange (ETDEWEB)

    Cirrone, G. A. P.; Schillaci, F. [Istituto Nazionale di Fisica Nucleare, Laboratori Nazionali del Sud, Via Santa Sofia 62, Catania, Italy and Institute of Physics of the ASCR, ELI-Beamlines project, Na Slovance 2, Prague (Czech Republic); Carpinelli, M. [INFN Sezione di Cagliari, c/o Dipartimento di Fisica, Università di Cagliari, Cagliari (Italy); Cuttone, G.; Romano, F. [Istituto Nazionale di Fisica Nucleare, Laboratori Nazionali del Sud, Via Santa Sofia 62, Catania (Italy); Maggiore, M. [Institute of Physics of the ASCR, ELI-Beamlines project, Na Slovance 2, Prague, Czech Republic and Laboratori Nazionali di Legnaro, INFN, Via Università 2, Legnaro (PD) (Italy); Ter-Avetisyan, S. [Laboratori Nazionali di Legnaro, INFN, Via Università 2, Legnaro (PD) (Italy); Tramontana, A. [Istituto Nazionale di Fisica Nucleare, Laboratori Nazionali del Sud, Via Santa Sofia 62, Catania, Italy and School of Mathematics and Physics, The Queen' s University Belfast, BT7 1NN (United Kingdom); Velyhan, A. [Institute of Physics of the ASCR, ELI-Beamlines project, Na Slovance 2, Prague (Czech Republic)

    2013-07-26

    Thomson Parabola (TP) spectrometers are widely used devices for laser-driven beam diagnostics as they provide a complete set of information on the accelerated particles. A novel TP has been developed at LNS with a design able to detect protons up to 20 MeV. The layout design and some results obtained during the experimental campaign at PALS laboratory will be reported in the following.

  10. Guide design study for the high-resolution backscattering spectrometer FIRES

    Energy Technology Data Exchange (ETDEWEB)

    Pelley, C; Kargl, F; Sakai, V Garcia; Telling, M T F; Fernandez-Alonso, F; Demmel, F, E-mail: franz.demmel@stfc.ac.uk

    2010-11-01

    Different options are considered to transport cold neutrons along 90 m for the proposed new spectrometer FIRES at the ISIS facility. Monte Carlo simulations using the McStas programme package are used to assess the performance of various guide designs from the biological shield to the sample position. By employing a curved geometry, to avoid the direct line of sight, a hybrid design which combines a curved ballistic guide and an elliptic focusing section appears to be the best solution.

  11. Analytical calculations and Monte-Carlo simulations of a high-resolution backscattering spectrometer for the long wavelength target station at the Spallation neutron source

    Science.gov (United States)

    Bordallo, H. N.; Herwig, K. W.; Zsigmond, G.

    2002-09-01

    Using the Monte-Carlo simulation programs McStas and VITESS, we present the design principles of the proposed high-resolution inverse geometry spectrometer on the Spallation neutron source (SNS)—long wavelength target station (LWTS). LWTS will enable the combination of large energy and momentum transfer ranges with energy resolution. Indeed the resolution of this spectrometer lie between that routinely achieved by spin echo techniques and the design goal of the high-power target station (HPTS) backscattering spectrometer. This niche of energy resolution is interesting for the study of slow motions of large objects and we are led to the domain of large molecules—polymers and biological molecules.

  12. Ultra high energy resolution focusing monochromator for inelastic X-ray scattering spectrometer

    CERN Document Server

    Suvorov, A; Chubar, O; Cai, Y Q

    2015-01-01

    A further development of a focusing monochromator concept for X-ray energy resolution of 0.1 meV and below is presented. Theoretical analysis of several optical layouts based on this concept was supported by numerical simulations performed in the "Synchrotron Radiation Workshop" software package using the physical-optics approach and careful modeling of partially-coherent synchrotron (undulator) radiation. Along with the energy resolution, the spectral shape of the energy resolution function was investigated. It was shown that under certain conditions the decay of the resolution function tails can be faster than that of the Gaussian function.

  13. Recent Developments of an Opto-Electronic THz Spectrometer for High-Resolution Spectroscopy

    Directory of Open Access Journals (Sweden)

    Guillaume Ducournau

    2009-11-01

    Full Text Available A review is provided of sources and detectors that can be employed in the THz range before the description of an opto-electronic source of monochromatic THz radiation. The realized spectrometer has been applied to gas phase spectroscopy. Air-broadening coefficients of HCN are determined and the insensitivity of this technique to aerosols is demonstrated by the analysis of cigarette smoke. A multiple pass sample cell has been used to obtain a sensitivity improvement allowing transitions of the volatile organic compounds to be observed. A solution to the frequency metrology is presented and promises to yield accurate molecular line center measurements.

  14. High-Resolution X-ray Spectroscopy with a Grating Spectrometer Explorer on the ISS

    Science.gov (United States)

    Smith, Randall

    We present the design and scientific motivation for a X-ray grating spectrometer mission to be deployed on the International Space Station. This mission would observe the Warm-Hot Intergalactic Medium, feedback from supermassive black holes, and the structure of the interstellar medium and halo of the Milky Way, amongst other goals. The mission requirements are similar to those of the IXO X-ray Grating Spectrometer of R=3000 and 1000 cm(2) \\ of effective area at 0.5 keV, with a full bandpass covering at least between 0.3-1 keV. Our initial design baselines the silicon pore optics proposed for ESA's Athena mission with a 4.3 m focal length, paired with off-plane gratings being developed at the University of Iowa combined with MIT/Lincoln Labs CCDs. This mission would achieve core science described in the 2010 New Worlds, New Horizons Decadal survey performed by the US National Research Council while effectively using the ISS and at low cost and low risk.

  15. High resolution imaging Fourier transform spectrometer with no moving components for the measurement of atmospheric trace gases

    Science.gov (United States)

    Mortimer, H.

    2014-12-01

    A high resolution Static Imaging Fourier Transform Spectrometer, SIFTS, with no moving parts has been developed for the detection of atmospheric gases. The instrument has been shown to have high spectral resolution (4 cm-1) and temporal resolution (10kHz) resolution in both the mid and near infrared and moderate spectral resolution (14cm-1) in the visible. This instrument has been developed for the remote sensing and in-situ measurements of atmospheric gases. It has been identified that due to the low mass and compact size of the instrument system, that the SIFTS could be deployed as a remote sensing instrument onboard a Earth Observation satellite or Unmanned Aerial Vehicle (UAV), or conversely as a radiosonde instrument for in-situ measurements of atmospheric gases. The technique is based on a static optical configuration whereby light is split into two paths and made to recombine along a focal plane producing an interference pattern. The spectral information is returned using a detector array to digitally capture the interferogram which can then be processed into a spectrum by applying a Fourier transform. As there are no moving components, the speed of measurement is determined by the frame rate of the detector array. Thus, this instrument has a temporal advantage over common Michelson FTIR instruments. Using a high speed Toshiba CCD line array, sensitive over the spectral region of 400 - 1100nm, spectra have been recorded at a rate of one every 100 microseconds. Using an uncooled microbolometer infrared detector array, sensitive over the spectral region of 2 to 15μm, the gases NH3, O3 and CH4 have been used to demonstrate the sensitivity of the SIFTS instrument. It has been shown that the Signal to Noise of the SIFTSMIR is >1200 using an integration time of 77msec. The novel optical design has reduced the optics to only 3 optical components, and the detector array, to generate and measure the interferogram. The experimental performance of the SIFTS instrument

  16. Resolution of a triple axis spectrometer

    DEFF Research Database (Denmark)

    Nielsen, Mourits; Bjerrum Møller, Hans

    1969-01-01

    A new method for obtaining the resolution function for a triple-axis neutron spectrometer is described, involving a combination of direct measurement and analytical calculation. All factors which contribute to the finite resolution of the instrument may be taken into account, and Gaussian...

  17. Mineralogical determination in situ of a highly heterogeneous material using a miniaturized laser ablation mass spectrometer with high spatial resolution

    Science.gov (United States)

    Neubeck, Anna; Tulej, Marek; Ivarsson, Magnus; Broman, Curt; Riedo, Andreas; McMahon, Sean; Wurz, Peter; Bengtson, Stefan

    2016-04-01

    Techniques enabling in situ elemental and mineralogical analysis on extraterrestrial planets are strongly required for upcoming missions and are being continuously developed. There is ample need for quantitative and high-sensitivity analysis of elemental as well as isotopic composition of heterogeneous materials. Here we present in situ spatial and depth elemental profiles of a heterogeneous rock sample on a depth-scale of nanometres using a miniaturized laser ablation mass spectrometer (LMS) designed for planetary space missions. We show that the LMS spectra alone could provide highly detailed compositional, three-dimensional information and oxidation properties of a natural, heterogeneous rock sample. We also show that a combination of the LMS and Raman spectroscopy provide comprehensive mineralogical details of the investigated sample. These findings are of great importance for future space missions where quick, in situ determination of the mineralogy could play a role in the process of selecting a suitable spot for drilling.

  18. A high resolution X-ray crystal spectrometer to study electron and heavy-ion impact atomic collisions

    Indian Academy of Sciences (India)

    Ajay Kumar; D Misra; A H Kelkar; U R Kadhane; K V Thulasiram; Lokesh C Tribedi

    2007-06-01

    We have studied fast ion–atom and electron–atom collision processes using a reconditioned high resolution X-ray spectrometer. The X-rays, generated by the collisions, are dispersed by a curved ADP crystal (Johansson geometry) and detected by a gas proportional counter. A self-written LabVIEW based program has been used to give precise and controlled movement to the crystal and for data acquisition. The performance was tested by detecting the K diagram and satellite lines of several elements. The K satellite lines of Al have been studied in collision with 3–12 keV electrons and 40 MeV C4+ ions. In ion collisions as large as four L-vacancies are created simultaneously with the K-vacancy, compared to two satellites in case of the e-impact. In addition, we have measured the X-rays from H-, He- and Li-like Si ions which arise due to the electron loss/capture process in highly charged 80 MeV Si7+ ions in collision with thin carbon foil. Approximate charge state distribution has been obtained using this new technique.

  19. Radiometric calibration of IR Fourier transform spectrometers - Solution to a problem with the High-Resolution Interferometer Sounder

    Science.gov (United States)

    Revercomb, Henry E.; Smith, William L.; Buijs, H.; Howell, Hugh B.; Laporte, D. D.

    1988-01-01

    A calibrated Fourier transform spectrometer, known as the High-Resolution Interferometer Sounder (HIS), has been flown on the NASA U-2 research aircraft to measure the infrared emission spectrum of the earth. The primary use - atmospheric temperature and humidity sounding - requires high radiometric precision and accuracy (of the order of 0.1 and 1 C, respectively). To meet these requirements, the HIS instruments, the HIS instrument performs inflight radiometric calibration, using observations of hot and cold blackbody reference sources as the basis for two-point calibrations at each wavenumber. Initially, laboratory tests revealed a calibration problem with brightness temperature errors as large as 15 C between 600 and 900/cm. The symptom of the problem, which occurred in one of the three spectral bands of HIS, was a source-dependent phase response. Minor changes to the calibration equations completely eliminated the anomalous errors. The new analysis properly accounts for the situation in which the phase response for radiance from the instrument itself differs from that for radiance from an external source. The mechanism responsible for the dual phase response of the HIS instrument is identified as emission from the interferometer beam splitter.

  20. High Resolution Soft X-ray Spectroscopy of M87 with the Reflection Grating Spectrometers on XMM-Newton

    CERN Document Server

    Sakelliou, I; Tamura, T; Paerels, F B S; Kaastra, J S; Belsole, E; Böhringer, H; Branduardi-Raymont, G; Ferrigno, C; Den Herder, J W A; Kennea, J; Mushotzky, R F; Vestrand, W T; Worrall, D M

    2002-01-01

    We present high-resolution X-ray spectroscopic observations of M87 with the Reflection Grating Spectrometers on XMM-Newton. We detect strong K-shell line emission from N, O, Ne, Mg, some emission from He-like Si, a fully resolved set of Fe L-shell emission spectra, and some emission from C. The angular intensity distributions of the strong emission lines are detectably resolved on scales (15-160) arcsec. The gas in the inner arcmin of M87 has a multi-phase structure, as indicated by the similarity of the emission line profiles of Fe L shell ions with widely separated ionization potentials. The global Fe L spectrum is approximately consistent with an isothermal plasma at kT_e ~ 1.8 keV, in addition to a component with a temperature distribution appropriate to an isobaric cooling flow, but with a minimum temperature cutoff of kT_min ~ 600 eV. The behaviour of this cooling-flow component is qualitatively similar to what is seen in other cooling flow clusters. Finally, we do not find any strong evidence for a spa...

  1. The upGREAT 1.9 THz multi-pixel high resolution spectrometer for the SOFIA Observatory

    CERN Document Server

    Risacher, C; Stutzki, J; Huebers, H -W; Bell, A; Buchbender, C; Buechel, D; Csengeri, T; Graf, U U; Heyminck, S; Higgins, R D; Honingh, C E; Jacobs, K; Klein, B; Okada, Y; Parikka, A; Puetz, P; Reyes, N; Ricken, O; Riquelme, D; Simon, R; Wiesemeyer, H

    2016-01-01

    We present a new multi-pixel high resolution (R >10^7) spectrometer for the Stratospheric Observatory for Far-Infrared Astronomy (SOFIA). The receiver uses 2 x 7-pixel subarrays in orthogonal polarization, each in an hexagonal array around a central pixel. We present the first results for this new instrument after commissioning campaigns in May and December 2015 and after science observations performed in May 2016 . The receiver is designed to ultimately cover the full 1.8-2.5 THz frequency range but in its first implementation, the observing range was limited to observations of the [CII] line at 1.9 THz in 2015 and extended to 1.83-2.07 THz in 2016. The instrument sensitivities are state-of-the-art and the first scientific observations performed shortly after the commissioning confirm that the time efficiency for large scale imaging is improved by more than an order of magnitude as compared to single pixel receivers. An example of large scale mapping around the Horsehead Nebula is presented here illustrating...

  2. The upGREAT 1.9 THz multi-pixel high resolution spectrometer for the SOFIA Observatory

    Science.gov (United States)

    Risacher, C.; Güsten, R.; Stutzki, J.; Hübers, H.-W.; Bell, A.; Buchbender, C.; Büchel, D.; Csengeri, T.; Graf, U. U.; Heyminck, S.; Higgins, R. D.; Honingh, C. E.; Jacobs, K.; Klein, B.; Okada, Y.; Parikka, A.; Pütz, P.; Reyes, N.; Ricken, O.; Riquelme, D.; Simon, R.; Wiesemeyer, H.

    2016-10-01

    We present a new multi-pixel high resolution (R ≳ 107) spectrometer for the Stratospheric Observatory for Far-Infrared Astronomy (SOFIA). The receiver uses 2 × 7-pixel subarrays in orthogonal polarization, each in an hexagonal array around a central pixel. We present the first results for this new instrument after commissioning campaigns in May and December 2015 and after science observations performed in May 2016. The receiver is designed to ultimately cover the full 1.8-2.5 THz frequency range but in its first implementation, the observing range was limited to observations of the [CII] line at 1.9 THz in 2015 and extended to 1.83-2.07 THz in 2016. The instrument sensitivities are state-of-the-art and the first scientific observations performed shortly after the commissioning confirm that the time efficiency for large scale imaging is improved by more than an order of magnitude as compared to single pixel receivers. An example of large scale mapping around the Horsehead Nebula is presented here illustrating this improvement. The array has been added to SOFIA's instrument suite already for ongoing observing cycle 4. The datacube of the Horsehead observations is only available at the CDS via anonymous ftp to http://cdsarc.u-strasbg.fr (http://130.79.128.5) or via http://cdsarc.u-strasbg.fr/viz-bin/qcat?J/A+A/595/A34

  3. Copper L X-ray spectra measured by a high resolution ion-induced X-ray spectrometer

    Energy Technology Data Exchange (ETDEWEB)

    Takahashi, Ryohei; Hamaguchi, Dai; Kageyama, Hiroyoshi [Kyoto Inst. of Tech. (Japan)] [and others

    1997-03-01

    High resolution L X-ray emission spectra of Cu have been measured by 0.75 MeV/u H, He, and F, 0.73 MeV/u Ar, 0.64 MeV/u Si, and 0.073 MeV/u Si ion impacts with a crystal spectrometer. The X-ray transition energies in the Cu target for L{iota}, L{eta}, L{alpha}{sub 1,2}, L{beta}{sub 1}, and L{beta}{sub 3,4} diagram lines induced by light ion impacts are determined, which are in good agreement with those given in the reference. The difference in L X-ray emission spectra produced by H, He, F, Si, and Ar ions are considered and the L{alpha}{sub 1,2} and L{beta}{sub 1} emission spectra are compared with the calculated ones based on the multiconfiguration Dirac-Fock method. (author)

  4. Development of High Resolution X-Ray spectrometers for the Investigation of Bioinorganic Chemistry in Metalloproteins

    Energy Technology Data Exchange (ETDEWEB)

    Drury, Owen Byron [Univ. of California, Davis, CA (United States)

    2007-01-01

    Metals play as varied a role in biology as the proteins they are part of. They are involved in structure formation, they help transfer material and information, and they catalyze chemical reactions. Other proteins transport material or information, such as hemoglobin that distributes O2 and takes up CO2, or insulin that signals cells to increase glucose uptake in response to high blood glucose levels. Again other proteins promote chemical reactions, such as photosystem II responsible for photosynthetic oxygen evolution or nitrogenase which catalyzes the reduction of N2 to NH3. All of these proteins require the presence of a metal ion for their activity.

  5. Development of a high resolution laser based angle-resolving time-of-flight photoelectron spectrometer

    CERN Document Server

    Berntsen, M H; Tjernberg, O

    2011-01-01

    We present the design and performance of a novel Laser-based Angle-Resolving Time-of-Flight (LARTOF) system for photoemission from solids in the vacuum ultraviolet (VUV) energy range. A pulsed laser provides photons which through a third harmonic generation (THG) process performed in a xenon filled gas cell generates VUV photons of energy 10.5 eV. The time-of-flight analyzer is able to collect all electrons that are emitted from the sample within a circular cone of up to +/-15 degrees. By simultaneously measuring the energy and emission angle along two spatial directions for the electrons the analyzer provides three-dimensional detection capability. Data from a test measurement performed on the Au(111) surface state is presented along with some more advanced measurements of the Fermi surface of the high-temperature superconductor Bi2212.

  6. Advanced Materials and Processes for High Energy Resolution Room Temperature Gamma Ray Spectrometers

    Energy Technology Data Exchange (ETDEWEB)

    Douglas S. McGregor

    2007-12-12

    A significant amount of progress has been achieved in the development of the novel vacuum distillation method described in the proposal. The process for the purification of Te was fully developed and characterized in a series of trials. The purification effect was confirmed with GDMS sample analysis and indicates the process yields very high purity Te metal. Results of this initial process study have been submitted for publication in the Proceedings of the SPIE and will be presented on August 28, 2007 at the SPIE Optics and Photonics 2007 conference in San Diego, CA. Concurrent to the development of the Te process, processes for the purification of Cd, Zn, and Mn have also progressed. The development of the processes for Cd and Zn are nearly complete, while the development of the process for Mn is still in its infancy. It is expected that a full characterization of the Cd process will be completed within the next quarter, followed by Zn. Parallel to those characterization studies, efforts will be made to further develop the Mn purification process. Zone melting work for Te and Cd has also been efforted as per the project work schedule. Initial trials have been completed and the processes developed. Characterization of the results will be completed within the first fiscal year. Finally, an apparatus for the zone refinement of Cd, Zn, and Mn has been constructed and initial trials are set to begin shortly.

  7. Momentum and energy dependent resolution function of the ARCS neutron chopper spectrometer at high momentum transfer: Comparing simulation and experiment

    Science.gov (United States)

    Diallo, S. O.; Lin, J. Y. Y.; Abernathy, D. L.; Azuah, R. T.

    2016-11-01

    Inelastic neutron scattering at high momentum transfers (i.e. Q ≥ 20 A ˚), commonly known as deep inelastic neutron scattering (DINS), provides direct observation of the momentum distribution of light atoms, making it a powerful probe for studying single-particle motions in liquids and solids. The quantitative analysis of DINS data requires an accurate knowledge of the instrument resolution function Ri(Q , E) at each momentum Q and energy transfer E, where the label i indicates whether the resolution was experimentally observed i = obs or simulated i=sim. Here, we describe two independent methods for determining the total resolution function Ri(Q , E) of the ARCS neutron instrument at the Spallation Neutron Source, Oak Ridge National Laboratory. The first method uses experimental data from an archetypical system (liquid 4He) studied with DINS, which are then numerically deconvoluted using its previously determined intrinsic scattering function to yield Robs(Q , E). The second approach uses accurate Monte Carlo simulations of the ARCS spectrometer, which account for all instrument contributions, coupled to a representative scattering kernel to reproduce the experimentally observed response S(Q , E). Using a delta function as scattering kernel, the simulation yields a resolution function Rsim(Q , E) with comparable lineshape and features as Robs(Q , E), but somewhat narrower due to the ideal nature of the model. Using each of these two Ri(Q , E) separately, we extract characteristic parameters of liquid 4He such as the intrinsic linewidth α2 (which sets the atomic kinetic energy ∼α2) in the normal liquid and the Bose-Einstein condensate parameter n0 in the superfluid phase. The extracted α2 values agree well with previous measurements at saturated vapor pressure (SVP) as well as at elevated pressure (24 bars) within experimental precision, independent of which Ri(Q , y) is used to analyze the data. The actual observed n0 values at each Q vary little with the

  8. A Prototype Experiment to Study Charmed Particle Production and Decay using a Holographic High Resolution Hydrogen Chamber (HOLEBC) and the European Hybrid Spectrometer

    CERN Multimedia

    2002-01-01

    The high resolution Hydrogen bubble chamber LEBC has already been used in experiments at the SPS to detect particles with lifetime @$>$ 5.10|-|1|3s (NA13 & NA16). For this experiment, a new version of LEBC called HOLEBC, has been constructed. This chamber and the NA26 version of the spectrometer have been used with classical optics in the NA27 experiment. A significant improvement in resolution was achieved (@= 20 microns compared with @= 40@mm in LEBC) and hence a good sensitivity all (known) charmed particle decays. The development of holographic recording techniques with HOLEBC is in progress. The prototype NA26 experiment is designed to evaluate the feasibility of the high sensitivity, high resolution holographic hydrogen bubble chamber technique and evaluate various possible charm selective triggers using the information from the spectrometer.

  9. DOTS: A High Resolution Orbitrap Mass Spectrometer for In Situ Analysis of the surface samples of Airless Planetary Bodies

    Science.gov (United States)

    Briois, Christelle; Thissen, Roland; Engrand, Cécile; Altwegg, Kathrin; Bouabdellah, Abdel; Boukrara, Amirouche; Carrasco, Nathalie; Chapuis, Claude; Cottin, Hervé; Grün, Eberhard; Grand, Noel; Henkel, Hartmut; Kempf, Sascha; Lebreton, Jean-Pierre; Makarov, Alexander A.; Postber, Frank; Srama, Ralf; Schmidt, Jürgen; Szopa, Cyril; Thirkell, Laurent; Tobie, Gabriel; Wurz, Peter; Zolotov, Mikhail Yu

    2013-04-01

    The dust detectors on board the Ulysses and Galileo spacecraft have shown that the Galilean satellites are surrounded by clouds of sub-micrometer size grains generated by impacts of interplanetary (micro-) meteoroids [1, 2]. In situ chemical analysis from orbit of these ballistic grains ejected from the surface of airless bodies provides a unique opportunity to remotely access the chemical composition of the Jovian moons' surface and subsurface. For Saturn, in situ identification by the Cassini Dust Analyzer (CDA) of sodium in icy grains in the E-Ring and in Enceladus plumes have proven a subsurface liquid water reservoir inside Enceladus [3, 4]. Noticeably, this was not accessible to other in situ or traditional remote sensing techniques. In situ measurements, either during a flyby or from orbit, of grains ejected from the surface, or emerging from the subsurface, of an airless body is a powerful tool to remotely study its surface composition and the nature of its geological activity. Crucial constraints on habitability can thus be determined. Our consortium of laboratories, in collaboration with Thermo Fischer Scientific [5, 6], is currently developing a high mass resolution Fourier Transform (FT) Orbitrap-based mass spectrometer optimized for in situ analysis of dust and icy grains in the environment of Solar System airless bodies. This new generation of dust mass spectrometer was studied in the framework of the Europa Jupiter System Mission (EJSM) instrument study in 2010-2012 and proposed in response to ESA's AO for the JUpiter ICy moons Explorer (JUICE) mission [7]. This mass analyser can provide very high mass resolution analysis (M/ΔM reaching 50 000 at m/z 50 Da). DOTS would allow identification of elemental and molecular species with excellent accuracy, in the 20-1000 Da mass range. In the context of the JUICE mission, DOTS would provide decisive information on the surface composition and on the putative liquid oceans in the subsurface of Ganymede

  10. OZSPEC-2: an improved broadband high-resolution elliptical crystal x-ray spectrometer for high-energy density physics experiments (invited).

    Science.gov (United States)

    Heeter, R F; Anderson, S G; Booth, R; Brown, G V; Emig, J; Fulkerson, S; McCarville, T; Norman, D; Schneider, M B; Young, B K F

    2008-10-01

    A novel time, space, and energy-resolved x-ray spectrometer has been developed which produces, in a single snapshot, a broadband and relatively calibrated spectrum of the x-ray emission from a high-energy density laboratory plasma. The opacity zipper spectrometer (OZSPEC-1) records a nearly continuous spectrum for x-ray energies from 240 to 5800 eV in a single shot. The second-generation OZSPEC-2, detailed in this work, records fully continuous spectra on a single shot from any two of these three bands: 270-650, 660-1580, and 1960-4720 eV. These instruments thus record thermal and line radiation from a wide range of plasmas. These instruments' single-shot bandwidth is unmatched in a time-gated spectrometer; conversely, other broadband instruments are either time-integrated (using crystals or gratings), lack spectral resolution (diode arrays), or cover a lower energy band (gratings). The OZSPECs are based on the zipper detector, a large-format (100x35 mm) gated microchannel plate detector, with spectra dispersed along the 100 mm dimension. OZSPEC-1 and -2 both use elliptically bent crystals of OHM, RAP, and/or PET. Individual spectra are gated in 100 ps. OZSPEC-2 provides one-dimensional spatial imaging with 30-50 microm resolution over a 1500 microm field of view at the source. The elliptical crystal design yields broad spectral coverage with resolution E/DeltaE>500, strong rejection of hard x-ray backgrounds, and negligible source broadening for extended sources. Near-term applications include plasma opacity measurements, detailed spectra of inertial fusion Hohlraums, and laboratory astrophysics experiments.

  11. Lifetime effects for high-resolution gamma-ray spectroscopy at relativistic energies and their implications for the RISING spectrometer

    Energy Technology Data Exchange (ETDEWEB)

    Doornenbal, P., E-mail: pieter@ribf.riken.j [Institut fuer Kernphysik, Universitaet zu Koeln, 50937 Koeln (Germany); GSI Helmholtzzentrum fuer Schwerionenforschung GmbH, 64291 Darmstadt (Germany); Reiter, P. [Institut fuer Kernphysik, Universitaet zu Koeln, 50937 Koeln (Germany); Grawe, H.; Saito, T. [GSI Helmholtzzentrum fuer Schwerionenforschung GmbH, 64291 Darmstadt (Germany); Al-Khatib, A. [Helmholtz-Institut fuer Strahlen- und Kernphysik, Universitaet Bonn, 53115 Bonn (Germany); Banu, A.; Beck, T.; Becker, F. [GSI Helmholtzzentrum fuer Schwerionenforschung GmbH, 64291 Darmstadt (Germany); Bednarczyk, P. [GSI Helmholtzzentrum fuer Schwerionenforschung GmbH, 64291 Darmstadt (Germany); The Niewodniczanski Institute of Nuclear Physics, Polish Academy of Sciences, 31-342 Krakow (Poland); Benzoni, G. [INFN Sezione di Milano, 20133 Milano (Italy); Bracco, A. [INFN Sezione di Milano, 20133 Milano (Italy); Dipartimento di Fisica, Universita di Milano, 20133 Milano (Italy); Buerger, A. [Helmholtz-Institut fuer Strahlen- und Kernphysik, Universitaet Bonn, 53115 Bonn (Germany); Caceres, L. [GSI Helmholtzzentrum fuer Schwerionenforschung GmbH, 64291 Darmstadt (Germany); Departamento de Fisica Teorica, Universidad Autonoma de Madrid, 28049 Madrid (Spain); Camera, F. [INFN Sezione di Milano, 20133 Milano (Italy); Dipartimento di Fisica, Universita di Milano, 20133 Milano (Italy); Chmel, S. [Helmholtz-Institut fuer Strahlen- und Kernphysik, Universitaet Bonn, 53115 Bonn (Germany); Crespi, F.C.L. [INFN Sezione di Milano, 20133 Milano (Italy); Dipartimento di Fisica, Universita di Milano, 20133 Milano (Italy); Geissel, H.; Gerl, J.; Gorska, M. [GSI Helmholtzzentrum fuer Schwerionenforschung GmbH, 64291 Darmstadt (Germany); Grebosz, J. [GSI Helmholtzzentrum fuer Schwerionenforschung GmbH, 64291 Darmstadt (Germany); Niewodniczanski Institute of Nuclear Physics, Polish Academy of Sciences, 31-342 Krakow (Poland)

    2010-02-01

    The lineshapes and peak position of Doppler corrected gamma-ray spectra from in-beam experiments at relativistic energies are investigated with respect to the intrinsic energy resolution of the employed detectors, the particles' velocities, and the photons' emission angle uncertainties at the moment of gamma-ray emission. The uncertainties in velocity and photon emission angle are dependent on the lifetime of the excited state. The impact of these two observables on the lineshape and energy resolution are studied for the RISING gamma-spectrometer by means of simulations and experimental results from a two-step fragmentation experiment at approx200MeV/u. Potential use of the distinct lineshape for lifetime determination is demonstrated for measured gamma-ray transitions.

  12. Design Parameters and Objectives of a High-­Resolution X-­ray Imaging Crystal Spectrometer for the Large Helical Device (LHD)

    Energy Technology Data Exchange (ETDEWEB)

    Bitter, M; Gates, D; Neilson, H; Reiman, A; Roquemore, A L; Morita, S; Goto, M; Yamada, H

    2010-05-19

    A high-resolution X-ray imaging crystal spectrometer, whose instrumental concept was thoroughly tested on NSTX and Alcator C-Mod, is presently being designed for LHD. The instrument will record spatially resolved spectra of helium-like Ar16+ and provide ion temperature profiles with spatial and temporal resolutions of 1 cm and > 10 ms which are obtained by a tomographic inversion of the spectral data, using the stellarator equilibrium reconstruction codes, STELLOPT and PIES. Since the spectrometer will be equipped with radiation hardened, high count rate, PILATUS detectors,, it is expected to be operational for all experimental conditions on LHD, which include plasmas of high density and plasmas with auxiliary RF and neutral beam heating. The special design features required by the magnetic field structure at LHD will be described.

  13. Fast Airborne Aerosol Size and Chemistry Measurements with the High Resolution Aerosol Mass Spectrometer during the MILAGRO Campaign

    Science.gov (United States)

    DeCarlo, P. F.; Dunlea, E. J.; Kimmel, J. R.; Aiken, A. C.; Sueper, D.; Crounse, J.; Wennberg, P. O.; Emmons, L.; Shinozuka, Y.; Clarke, A.; Zhou, J.; Tomlinson, J.; Collins,D. R.; Knapp, D.; Weinheimer, A. J.; Montzka,D. D.; Campos,T.; Jimenez, J. L.

    2007-01-01

    The concentration, size, and composition of non-refractory submicron aerosol (NR-PM(sub l)) was measured over Mexico City and central Mexico with a High-Resolution Time-of-Flight Aerosol Mass Spectrometer (HR-ToF-AMS) onboard the NSF/NCAR C-130 aircraft as part of the MILAGRO field campaign. This was the first aircraft deployment of the HR-ToF-AMS. During the campaign the instrument performed very well, and provided 12 s data. The aerosol mass from the AMS correlates strongly with other aerosol measurements on board the aircraft. Organic aerosol (OA) species dominate the NR-PM(sub l) mass. OA correlates strongly with CO and HCN indicating that pollution (mostly secondary OA, SOA) and biomass burning (BB) are the main OA sources. The OA to CO ratio indicates a typical value for aged air of around 80 microg/cubic m (STP) ppm(exp -1). This is within the range observed in outflow from the Northeastern US, which could be due to a compensating effect between higher BB but lower biogenic VOC emissions during this study. The O/C atomic ratio for OA is calculated from the HR mass spectra and shows a clear increase with photochemical age, as SOA forms rapidly and quickly overwhelms primary urban OA, consistent with Volkamer et al. (2006) and Kleinman et al. (2008). The stability of the OA/CO while O/C increases with photochemical age implies a net loss of carbon from the OA. BB OA is marked by signals at m/z 60 and 73, and also by a signal enhancement at large m/z indicative of larger molecules or more resistance to fragmentation. The main inorganic components show different spatial patterns and size distributions. Sulfate is regional in nature with clear volcanic and petrochemical/power plant sources, while the urban area is not a major regional source for this species. Nitrate is enhanced significantly in the urban area and immediate outflow, and is strongly correlated with CO indicating a strong urban source. The importance of nitrate decreases with distance from the city

  14. Fast airborne aerosol size and chemistry measurements with the high resolution aerosol mass spectrometer during the MILAGRO Campaign

    Science.gov (United States)

    Decarlo, P. F.; Dunlea, E. J.; Kimmel, J. R.; Aiken, A. C.; Sueper, D.; Crounse, J.; Wennberg, P. O.; Emmons, L.; Shinozuka, Y.; Clarke, A.; Zhou, J.; Tomlinson, J.; Collins, D. R.; Knapp, D.; Weinheimer, A. J.; Montzka, D. D.; Campos, T.; Jimenez, J. L.

    2007-12-01

    The concentration, size, and composition of non-refractory submicron aerosol (NR-PM1) was measured over Mexico City and central Mexico with a High-Resolution Time-of-Flight Aerosol Mass Spectrometer (HR-ToF-AMS) onboard the NSF/NCAR C-130 aircraft as part of the MILAGRO field campaign. This was the first aircraft deployment of the HR-ToF-AMS, in which the instrument performed very well, and provided 12 s data. The aerosol mass from the AMS correlates strongly with other aerosol measurements on board the aircraft. Organic aerosol (OA) species dominate the NR-PM1 mass. OA correlates strongly with CO and HCN indicating that pollution (mostly secondary OA, SOA) and biomass burning (BB) are the main OA sources. The OA to CO ratio indicates a typical value for aged air of around 80 μg m-3 (STP) ppm-1. This is within the range observed in outflow from the Northeastern US, which could be due to a compensating effect between higher BB but lower biogenic VOC emissions during this study. The O/C atomic ratio for OA is calculated from the HR mass spectra and shows a clear increase with photochemical age, as SOA forms rapidly and quickly overwhelms primary urban OA, consistent with Volkamer et al. (2006) and Kleinman et al. (2007b). BB OA is marked by signals at m/z 60 and 73, and also by a signal enhancement at large m/z indicative of larger molecules or more resistance to fragmentation. The main inorganic components show different spatial patterns and size distributions. Sulfate is regional in nature with clear volcanic and petrochemical/power plant sources, while the urban area is not a major source for this species. Nitrate is enhanced significantly in the urban area and immediate outflow, and is strongly correlated with CO indicating a strong urban source. The importance of nitrate decreases with distance from the city likely due to evaporation. BB does not appear to be a strong source of nitrate despite its high emissions of nitrogen oxides, presumably due to low ammonia

  15. Fast airborne aerosol size and chemistry measurements with the high resolution aerosol mass spectrometer during the MILAGRO Campaign

    Directory of Open Access Journals (Sweden)

    P. F. DeCarlo

    2007-12-01

    Full Text Available The concentration, size, and composition of non-refractory submicron aerosol (NR-PM1 was measured over Mexico City and central Mexico with a High-Resolution Time-of-Flight Aerosol Mass Spectrometer (HR-ToF-AMS onboard the NSF/NCAR C-130 aircraft as part of the MILAGRO field campaign. This was the first aircraft deployment of the HR-ToF-AMS, in which the instrument performed very well, and provided 12 s data. The aerosol mass from the AMS correlates strongly with other aerosol measurements on board the aircraft. Organic aerosol (OA species dominate the NR-PM1 mass. OA correlates strongly with CO and HCN indicating that pollution (mostly secondary OA, SOA and biomass burning (BB are the main OA sources. The OA to CO ratio indicates a typical value for aged air of around 80 μg m−3 (STP ppm−1. This is within the range observed in outflow from the Northeastern US, which could be due to a compensating effect between higher BB but lower biogenic VOC emissions during this study. The O/C atomic ratio for OA is calculated from the HR mass spectra and shows a clear increase with photochemical age, as SOA forms rapidly and quickly overwhelms primary urban OA, consistent with Volkamer et al. (2006 and Kleinman et al. (2007b. BB OA is marked by signals at m/z 60 and 73, and also by a signal enhancement at large m/z indicative of larger molecules or more resistance to fragmentation. The main inorganic components show different spatial patterns and size distributions. Sulfate is regional in nature with clear volcanic and petrochemical/power plant sources, while the urban area is not a major source for this species. Nitrate is enhanced significantly in the urban area and immediate outflow, and is strongly correlated with CO indicating a strong urban source. The importance of nitrate decreases with distance from the city likely due to evaporation. BB does not appear to be a strong source of nitrate

  16. Technical note: Sensitivity of instrumental line shape monitoring for the ground-based high-resolution FTIR spectrometer with respect to different optical attenuators

    Science.gov (United States)

    Sun, Youwen; Palm, Mathias; Weinzierl, Christine; Petri, Christof; Notholt, Justus; Wang, Yuting; Liu, Cheng

    2017-03-01

    The TCCON (Total Carbon Column Observing Network) and most NDACC (Network for Detection of Atmospheric Composition Change) sites assume an ideal ILS (instrumental line shape) for analysis of the spectra. In order to adapt the radiant energy received by the detector, an attenuator or different sizes of field stop can be inserted in the light path. These processes may alter the alignment of a high-resolution FTIR (Fourier transform infrared) spectrometer, and may result in bias due to ILS drift. In this paper, we first investigated the sensitivity of the ILS monitoring with respect to application of different kinds of attenuators for ground-based high-resolution FTIR spectrometers within the TCCON and NDACC networks. Both lamp and sun cell measurements were conducted after the insertion of five different attenuators in front of and behind the interferometer. The ILS characteristics derived from lamp and sun spectra are in good agreement. ILSs deduced from all lamp cell measurements were compared. As a result, the disturbances to the ILS of a high-resolution FTIR spectrometer with respect to the insertion of different attenuators at different positions were quantified. A potential strategy to adapt the incident intensity of a detector was finally deduced.

  17. High-resolution miniature FTIR spectrometer enabled by a large linear travel MEMS pop-up mirror

    Science.gov (United States)

    Deutsch, Erik R.; Reyes, David; Schildkraut, Elliot R.; Kim, Jinhong

    2009-05-01

    This paper reports the design, fabrication, and characterization of a millimeter diameter, surface micromachined Micro-Electro-Mechanical-Systems (MEMS) mirror, which is assembled perpendicular to the substrate and can be linearly and repeatedly traversed through 600 μm. The moving mirror, when combined with a fixed mirror and beamsplitter, make up a monolithic MEMS Michelson interferometer; all are made on the same substrate and in the same surface micromachined fabrication process. The beamsplitter has been specifically designed such that the motion of the mirror enables modulation of light over the 2-14 μm spectral region. The rapid scan MEMS Michelson interferometer is the engine behind a miniaturized, Fourier transform infrared (FTIR) absorption spectrometer. The FTIR measures the absorption of infrared (IR) radiation by a target material, which can be used for the detection and identification of gases, liquids, or solids. The fabrication of the mirror with the ability to displace 600 μm along the optical axis enables the miniaturized system to have species identification resolution, while leveraging wafer scale batch fabrication to enable extremely low system cost. The successful fabrication of the millimeter diameter mirrors and beamsplitter with interferometric alignment over the range of travel of the moving mirror promises unprecedented sensitivity relative to the size of the FTIR spectrometer system.

  18. Factor analysis of combined organic and inorganic aerosol mass spectra from high resolution aerosol mass spectrometer measurements

    Directory of Open Access Journals (Sweden)

    Y. L. Sun

    2012-05-01

    Full Text Available The high resolution mass spectra of organic and inorganic aerosols from aerosol mass spectrometer (AMS measurements were first combined into positive matrix factorization (PMF analysis to investigate the sources and evolution processes of atmospheric aerosols. The new approach is able to study the mixing of organic aerosols (OA and inorganic species, the acidity of OA factors, and the fragment ion patterns related to photochemical processing. In this study, PMF analysis of the unified AMS spectral matrices resolved 8 factors for the submicron aerosols measured at Queens College in New York City in summer 2009. The hydrocarbon-like OA (HOA and cooking OA (COA contain very minor inorganic species, indicating the different sources and mixing characteristics between primary OA and secondary species. The two factors that are primarily ammonium sulfate (SO4-OA and ammonium nitrate (NO3-OA, respectively, are overall neutralized, of which the OA in SO4-OA shows the highest oxidation state (O/C = 0.69 among OA factors. The semi-volatile oxygenated OA comprises two components, i.e., a less oxidized (LO-OOA and a more oxidized (MO-OOA. The MO-OOA represents a local photochemical product with the diurnal profile exhibiting a pronounced noon peak, consistent with those of formaldehyde (HCHO and Ox (= O3+NO2. The much higher NO+/NO2+ fragment ion ratio in MO-OOA than that from ammonium nitrate alone provides evidence for the formation of organic nitrates. The amine-related nitrogen-enriched OA (NOA contains ~25% of acidic inorganic salts, elucidating the formation of secondary OA from amines in acidic environments. The size distributions derived from 3-dimensional size-resolved mass spectra show distinct diurnal evolving behaviors for different OA factors, but overall a progressing evolution from smaller to larger particle mode as a function of oxidation states

  19. The Compact High Resolution Imaging Spectrometer (CHRIS): the future of hyperspectral satellite sensors. Imagery of Oostende coastal and inland waters

    OpenAIRE

    B. De Mol; Ruddick, K

    2004-01-01

    The gap between airborne imaging spectroscopy and traditional multi spectral satellite sensors is decreasing thanks to a new generation of satellite sensors of which CHRIS mounted on the small and low-cost PROBA satellite is the prototype. Although image acquisition and analysis are still in a test phase, the high spatial and spectral resolution and pointability have proved their potential. Because of the high resolution small features, which were before only visible on airborne images, becom...

  20. The MIRI Medium Resolution Spectrometer calibration pipeline

    CERN Document Server

    Labiano, A; Bailey, J I; Beard, S; Dicken, D; García-Marín, M; Geers, V; Glasse, A; Glauser, A; Gordon, K; Justtanont, K; Klaassen, P; Lahuis, F; Law, D; Morrison, J; Müller, M; Rieke, G; Vandenbussche, B; Wright, G

    2016-01-01

    The Mid-Infrared Instrument (MIRI) Medium Resolution Spectrometer (MRS) is the only mid-IR Integral Field Spectrometer on board James Webb Space Telescope. The complexity of the MRS requires a very specialized pipeline, with some specific steps not present in other pipelines of JWST instruments, such as fringe corrections and wavelength offsets, with different algorithms for point source or extended source data. The MRS pipeline has also two different variants: the baseline pipeline, optimized for most foreseen science cases, and the optimal pipeline, where extra steps will be needed for specific science cases. This paper provides a comprehensive description of the MRS Calibration Pipeline from uncalibrated slope images to final scientific products, with brief descriptions of its algorithms, input and output data, and the accessory data and calibration data products necessary to run the pipeline.

  1. Rapid Detection of Gas Hazards and Leaks with an Atmospheric Sampling, High Resolution, Mass Spectrometer with Low Pumping Requirements Project

    Data.gov (United States)

    National Aeronautics and Space Administration — Miniaturization of mass spectrometers is restricted almost exclusively by the ability of small vacuum pumps to remove gas loads during operation of the instrument....

  2. Momentum and Energy Dependent Resolution Function of the ARCS Neutron Chopper Spectrometer at High Momentum Transfer: Comparing Simulation and Experimen

    CERN Document Server

    Diallo, S O; Abernathy, D L; Azuah, R T

    2016-01-01

    Inelastic neutron scattering at high momentum transfers (i.e. $Q\\ge20$ {\\AA}) or DINS provides direct observation of the momentum distribution of light atoms, making it a powerful probe for studying single-particle motions in liquids and solids. The quantitative analysis of DINS data requires an accurate knowledge of the instrument resolution function $R_{i}({Q},E)$ at each $Q$ and energy transfer $E$, where the label $i$ indicates whether the resolution was experimentally observed $i={obs}$ or simulated $i=sim$. Here, we describe two independent methods for determining the total resolution function $R_{i}({Q},E)$ of the ARCS neutron instrument at the Spallation Neutron Source, Oak Ridge National Laboratory. The first method uses experimental data from an archetypical system (liquid $^4$He) studied with DINS, which are then numerically deconvoluted using its previously determined intrinsic scattering function to yield $R_{obs}({Q},E)$. The second approach uses accurate Monte Carlo simulations of the ARCS spec...

  3. Ozone-induced dissociation on a traveling wave high-resolution mass spectrometer for determination of double-bond position in lipids.

    Science.gov (United States)

    Vu, Ngoc; Brown, Jeffery; Giles, Kevin; Zhang, Qibin

    2017-09-15

    The position of C=C within fatty acyl chains affects the biological function of lipids. Ozone-induced dissociation mass spectrometry (OzID-MS) has great potential in determination of lipid double-bond position, but has generally been implemented on low-resolution ion trap mass spectrometers. In addition, most of the OzID-MS experiments carried out so far were focused on the sodiated adducts of lipids; fragmentation of the most commonly observed protonated ions generated in LC/MS-based lipidomics workflow has been less explored. Ozone generated in line from an ozone generator was connected to the trap and transfer gas supply line of a Synapt G2 high-resolution mass spectrometer. Protonated ions of different phosphatidylcholines (PC) were generated by electrospray ionization through direct infusion. Different parameters, including traveling wave height and velocity, trap entrance and DC potential, were adjusted to maximize the OzID efficiency. sn-positional isomers and cis/trans isomers of lipids were compared for their reactivity with ozone. Traveling wave height and velocity were tuned to prolong the encounter time between lipid ions and ozone, and resulted in improved OzID efficiency, as did increasing trapping region DC and entrance potential. Under optimized settings, at least 1000 times enhancement in OzID efficiency was achieved compared to that under default settings for monounsaturated PC standards. Monounsaturated C=C in the sn-2 PC isomer reacted faster with ozone than the sn-1 isomer. Similarly, the C=C in trans PC reacted faster than in cis PC. This is the first implementation of OzID in the trap and transfer region of a traveling wave enabled high-resolution mass spectrometer. The OzID reaction efficiency is significantly improved by slowing down ions in the trap region for their prolonged interaction with ozone. This will facilitate application of high-resolution OzID-MS in lipidomics. Copyright © 2017 John Wiley & Sons, Ltd.

  4. An iodide-adduct high-resolution time-of-flight chemical-ionization mass spectrometer: application to atmospheric inorganic and organic compounds.

    Science.gov (United States)

    Lee, Ben H; Lopez-Hilfiker, Felipe D; Mohr, Claudia; Kurtén, Theo; Worsnop, Douglas R; Thornton, Joel A

    2014-06-03

    A high-resolution time-of-flight chemical-ionization mass spectrometer (HR-ToF-CIMS) using Iodide-adducts has been characterized and deployed in several laboratory and field studies to measure a suite of organic and inorganic atmospheric species. The large negative mass defect of Iodide, combined with soft ionization and the high mass-accuracy (5500) of the time-of-flight mass spectrometer, provides an additional degree of separation and allows for the determination of elemental compositions for the vast majority of detected ions. Laboratory characterization reveals Iodide-adduct ionization generally exhibits increasing sensitivity toward more polar or acidic volatile organic compounds. Simultaneous retrieval of a wide range of mass-to-charge ratios (m/Q from 25 to 625 Th) at a high frequency (>1 Hz) provides a comprehensive view of atmospheric oxidative chemistry, particularly when sampling rapidly evolving plumes from fast moving platforms like an aircraft. We present the sampling protocol, detection limits and observations from the first aircraft deployment for an instrument of this type, which took place aboard the NOAA WP-3D aircraft during the Southeast Nexus (SENEX) 2013 field campaign.

  5. A stretch/compress scheme for a high temporal resolution detector for the magnetic recoil spectrometer time (MRSt)

    Science.gov (United States)

    Hilsabeck, T. J.; Frenje, J. A.; Hares, J. D.; Wink, C. W.

    2016-11-01

    A time-resolved detector concept for the magnetic recoil spectrometer for time-resolved measurements of the NIF neutron spectrum is presented. The measurement is challenging due to the time spreading of the recoil protons (or deuterons) as they transit an energy dispersing magnet system. Ions arrive at the focal plane of the magnetic spectrometer over an interval of tens of nanoseconds. We seek to measure the time-resolved neutron spectrum with 20 ps precision by manipulating an electron signal derived from the ions. A stretch-compress scheme is employed to remove transit time skewing while simultaneously reducing the bandwidth requirements for signal recording. Simulation results are presented along with design concepts for structures capable of establishing the required electromagnetic fields.

  6. Highly time-resolved chemical characterization of atmospheric submicron particles during 2008 Beijing Olympic Games using an Aerodyne High-Resolution Aerosol Mass Spectrometer

    Directory of Open Access Journals (Sweden)

    X.-F. Huang

    2010-05-01

    Full Text Available As part of Campaigns of Air Quality Research in Beijing and Surrounding Region–2008 (CAREBeijing-2008, an Aerodyne High-Resolution Time-of-Flight Aerosol Mass Spectrometer (HR-ToF-AMS was deployed in urban Beijing to characterize submicron aerosol particles during the time of 2008 Beijing Olympic Games and Paralytic Games (24 July to 20 September 2008. The campaign mean PM1 mass concentration was 63.1±39.8 μg m−3; the mean composition consisted of organics (37.9%, sulfate (26.7%, ammonium (15.9%, nitrate (15.8%, black carbon (3.1%, and chloride (0.87%. The average size distributions of the species (except BC were all dominated by an accumulation mode peaking at about 600 nm in vacuum aerodynamic diameter, and organics was characterized by an additional smaller mode extending below 100 nm. Positive Matrix Factorization (PMF analysis of the high resolution organic mass spectral dataset differentiated the organic aerosol into four components, i.e., hydrocarbon-like (HOA, cooking-related (COA, and two oxygenated organic aerosols (OOA-1 and OOA-2, which on average accounted for 18.1, 24.4, 33.7 and 23.7% of the total organic mass, respectively. The HOA was identified to be closely associated with primary combustion sources, while the COA mass spectrum showed high similarity to that measured from cooking aerosol emissions. The OOA components correspond to aged secondary organic aerosol. Although the two OOA components have similar elemental (O/C, H/C compositions, they display differences in mass spectra and time series which appear to correlate with the different source regions sampled during the campaign. Back trajectory clustering analysis indicated that the southerly air flows were associated with the highest PM1 pollution during the campaign. This result is similar to observations made in the summer of 2006, although the average PM1 concentration level for the southerly air flows is 31% lower than

  7. A decade-spanning high-resolution asynchronous optical sampling terahertz time-domain and frequency comb spectrometer

    Science.gov (United States)

    Good, Jacob T.; Holland, Daniel B.; Finneran, Ian A.; Carroll, P. Brandon; Kelley, Matthew J.; Blake, Geoffrey A.

    2015-10-01

    We present the design and capabilities of a high-resolution, decade-spanning ASynchronous OPtical Sampling (ASOPS)-based TeraHertz Time-Domain Spectroscopy (THz-TDS) instrument. Our system employs dual mode-locked femtosecond Ti:Sapphire oscillators with repetition rates offset locked at 100 Hz via a Phase-Locked Loop (PLL) operating at the 60th harmonic of the ˜80 MHz oscillator repetition rates. The respective time delays of the individual laser pulses are scanned across a 12.5 ns window in a laboratory scan time of 10 ms, supporting a time delay resolution as fine as 15.6 fs. The repetition rate of the pump oscillator is synchronized to a Rb frequency standard via a PLL operating at the 12th harmonic of the oscillator repetition rate, achieving milliHertz (mHz) stability. We characterize the timing jitter of the system using an air-spaced etalon, an optical cross correlator, and the phase noise spectrum of the PLL. Spectroscopic applications of ASOPS-THz-TDS are demonstrated by measuring water vapor absorption lines from 0.55 to 3.35 THz and acetonitrile absorption lines from 0.13 to 1.39 THz in a short pathlength gas cell. With 70 min of data acquisition, a 50 dB signal-to-noise ratio is achieved. The achieved root-mean-square deviation is 14.6 MHz, with a mean deviation of 11.6 MHz, for the measured water line center frequencies as compared to the JPL molecular spectroscopy database. Further, with the same instrument and data acquisition hardware, we use the ability to control the repetition rate of the pump oscillator to enable THz frequency comb spectroscopy (THz-FCS). Here, a frequency comb with a tooth width of 5 MHz is generated and used to fully resolve the pure rotational spectrum of acetonitrile with Doppler-limited precision. The oscillator repetition rate stability achieved by our PLL lock circuits enables sub-MHz tooth width generation, if desired. This instrument provides unprecedented decade-spanning, tunable resolution, from 80 MHz down to sub

  8. Highly time-resolved chemical characterization of atmospheric submicron particles during 2008 Beijing Olympic Games using an Aerodyne High-Resolution Aerosol Mass Spectrometer

    Directory of Open Access Journals (Sweden)

    X.-F. Huang

    2010-09-01

    Full Text Available As part of Campaigns of Air Quality Research in Beijing and Surrounding Region-2008 (CAREBeijing-2008, an Aerodyne High-Resolution Time-of-Flight Aerosol Mass Spectrometer (HR-ToF-AMS was deployed in urban Beijing to characterize submicron aerosol particles during the time of 2008 Beijing Olympic Games and Paralympic Games (24 July to 20 September 2008. The campaign mean PM1 mass concentration was 63.1 ± 39.8 μg m−3; the mean composition consisted of organics (37.9%, sulfate (26.7%, ammonium (15.9%, nitrate (15.8%, black carbon (3.1%, and chloride (0.87%. The average size distributions of the species (except BC were all dominated by an accumulation mode peaking at about 600 nm in vacuum aerodynamic diameter, and organics was characterized by an additional smaller mode extending below 100 nm. Positive Matrix Factorization (PMF analysis of the high resolution organic mass spectral dataset differentiated the organic aerosol into four components, i.e., hydrocarbon-like (HOA, cooking-related (COA, and two oxygenated organic aerosols (OOA-1 and OOA-2, which on average accounted for 18.1, 24.4, 33.7 and 23.7% of the total organic mass, respectively. The HOA was identified to be closely associated with primary combustion sources, while the COA mass spectrum and diurnal pattern showed similar characteristics to that measured for cooking emissions. The OOA components correspond to aged secondary organic aerosol. Although the two OOA components have similar elemental (O/C, H/C compositions, they display differences in mass spectra and time series which appear to correlate with the different source regions sampled during the campaign. Back trajectory clustering analysis indicated that the southerly air flows were associated with the highest PM1 pollution during the campaign. Aerosol particles in southern airmasses were especially rich in inorganic and oxidized organic species. Aerosol particles in northern airmasses

  9. The chemical composition and mineralogy of meteorites measured with very high spatial resolution by a laser mass spectrometer for in situ planetary research

    Science.gov (United States)

    Brigitte Neuland, Maike; Mezger, Klaus; Tulej, Marek; Frey, Samira; Riedo, Andreas; Wurz, Peter; Wiesendanger, Reto

    2017-04-01

    The knowledge of the chemical composition of moons, comets, asteroids or other planetary bodies is of particular importance for the investigation of the origin and evolution of the Solar System. High resolution in situ studies on planetary surfaces can yield important information on surface heterogeneity, basic grain mineralogy and chemical composition of surface and subsurface. In turn, these data are the basis for our understanding of the physical and chemical processes which led to the formation and alteration of planetary material [1]. We investigated samples of Allende and Sayh al Uhaymir with a highly miniaturised laser mass spectrometer (LMS), which has been designed and built for in situ space research [2,3]. Both meteorite samples were investigated with a spatial resolution of about 10μm in lateral direction. The high sensitivity and high dynamic range of the LMS allow for quantitative measurements of the abundances of the rock-forming and minor and trace elements with high accuracy [4]. From the data, the modal mineralogy of micrometre-sized chondrules can be inferred [5], conclusions about the condensation sequence of the material are possible and the sensitivity for radiogenic elements allows for dating analyses of the investigated material. We measured the composition of various chondrules in Allende, offering valuable clues about the condensation sequence of the different components of the meteorite. We explicitly investigated the chemical composition and heterogeneity of the Allende matrix with an accuracy that cannot be reached by the mechanical analysis methods that were and are widely used in meteoritic research. We demonstrate the capabilities for dating analyses with the LMS. By applying the U-Th-dating method, the age of the SaU169 sample could be determined. Our analyses show that the LMS would be a suitable instrument for high-quality quantitative chemical composition measurements on the surface of a celestial body like a planet, moon or

  10. Observation of the fully reconstructed $D^{0}\\overline{D}$$^{0}$ pair with long lifetimes in a high resolution hydrogen bubble chamber and the European Hybrid Spectrometer

    CERN Document Server

    AUTHOR|(CDS)2067425; Allison, W W M; Bagnaia, P; Touboul, M C; Baldo, B; Barone, L; Bartl, Walter; Bergier, A; Bettini, A; Bizzarri, R; Boratav, M; Borreani, G; Brooks, B; Bruyant, F; Castelli, Edoardo; Centro, Sandro; Checchia, P; Chliapnikov, P V; Ciapetti, G; Bertrand-Coremans, G H; Crennell, D J; Cresti, M; Crijns, F; De Giorgi, M; Dibon, Heinz; Di Capua, E; Dionisi, C; Dolbeau, J; Duboc, J; Dumarchez, J; Dykes, M; Etienne, F; Ferrando, A; Fisher, Colin M; Fisyak, Yu; Frühwirth, R; Gatignon, L; Gentile, S; Grard, F; Güsewell, D; Hartjes, F G; Hernández, J; Herquet, P; Hervé, A; Holmgren, S O; Hrubec, Josef; Hughes, P; Jacobs, D; Johansson, E K; Kesteman, J; Kistenev, E P; Kitamura, S; Kittel, E W; Kuhn, D; Kurtz, N; Ladrón de Guevara, P; Lecoq, P; Lemonne, J; Lesceux, J M; Leutz, H; Lipari, P; Loverre, P F; Lyons, L; Marchetto, F; Marin, J C; Markytan, Manfred; Marzano, F; Mazzucato, M; Menichetti, E; Michalon-Mentzer, M E; Michalon, A; Moa, T; Montanet, Lucien; Mulvey, J; Neuhofer, Günther; Nguyen, H; Nilsson, S; Paler, Kenneth; Pascoli, D; Peruzzo, L; Pilette, P; Piredda, G; Poljakov, B F; Poppleton, Alan; Rinaudo, G; Poropat, P; Porth, Paul; Powell, B; Regler, Meinhard; Reucroft, S; Robb, L; Rossi, P; Rubio, J; Sartori, G; Sessa, M I; Settles, Ronald; Stergiou, Athanase; Stopchenko, V A; Subramanian, A; Tavernier, Stefaan; Chikilev, O G; Toet, D Z; Touchard, A M; Troncon, C; Van Immerseel, M; Van de Walle, R T; Ventura, L; Voltolini, C; Wenninger, Horst; Wickens, J H; Willmott, C; Yiou, T P; Zanello, D; Zanello, L; Zholobov, G V; Zotto, P L; Zemerle, G

    1981-01-01

    In an experiment with a 360 GeV/c $\\pi^{-}$ beam at the CERN SPS using the high resolution hydrogen bubble chamber LEBC and the European Hybrid Spectrometer, an event has been observed of the type $\\pi^{-}p$ to $D^{0}D^{0}+8$ prongs. The fully reconstructed decay modes are $D^{0} \\rightarrow K^{-}\\pi^{+}\\pi^{0}\\pi^{0}$ and $D^{0} \\rightarrow K^{+}\\pi^{+}\\pi^{-}\\pi^{-}$, with all six charged tracks being detected in the spectrometer and all four photons from the $\\pi^{0}$ decays detected in the lead glass gamma detection system. The $D^{0}$ has momentum $119.0 \\pm 0.6$ GeV/c, $x_{F}=0.31$, length $4.1 \\pm 0.1$ mm and proper lifetime $(2.1 \\pm 0.1)\\times10^{-13}$s. The $D^{0}$ has momentum $78.5 \\pm 0.3$ GeV/c, $x_{F}=0.19$, length $7.5 \\pm 0.1$ mm and proper lifetime $(5.9 \\pm 0.1)\\times 10^{-13}$s.

  11. Imaging crystal spectrometer for high-resolution x-ray measurements on electron beam ion traps and tokamaks

    Science.gov (United States)

    Beiersdorfer, P.; Magee, E. W.; Hell, N.; Brown, G. V.

    2016-11-01

    We describe a crystal spectrometer implemented on the Livermore electron beam ion traps that employ two spherically bent quartz crystals and a cryogenically cooled back-illuminated charge-coupled device detector to measure x rays with a nominal resolving power of λ/Δλ ≥ 10 000. Its focusing properties allow us to record x rays either with the plane of dispersion perpendicular or parallel to the electron beam and, thus, to preferentially select one of the two linear x-ray polarization components. Moreover, by choice of dispersion plane and focussing conditions, we use the instrument either to image the distribution of the ions within the 2 cm long trap region, or to concentrate x rays of a given energy to a point on the detector, which optimizes the signal-to-noise ratio. We demonstrate the operation and utility of the new instrument by presenting spectra of Mo34+, which prepares the instrument for use as a core impurity diagnostic on the NSTX-U spherical torus and other magnetic fusion devices that employ molybdenum as plasma facing components.

  12. a 530-590 GHZ Schottky Heterodyne Receiver for High-Resolution Molecular Spectroscopy with Lille's Fast-Scan Fully Solid-State DDS Spectrometer

    Science.gov (United States)

    Pienkina, A.; Margulès, L.; Motiyenko, R. A.; Wiedner, Martina C.; Maestrini, Alain; Defrance, Fabien

    2017-06-01

    Laboratory spectroscopy, especially at THz and mm-wave ranges require the advances in instrumentation techniques to provide high resolution of the recorded spectra with precise frequency measurement that facilitates the mathematical treatment. We report the first implementation of a Schottky heterodyne receiver, operating at room temperature and covering the range between 530 and 590 GHz, for molecular laboratory spectroscopy. A 530-590 GHz non-cryogenic Schottky solid-state receiver was designed at LERMA, Observatoire de Paris and fabricated in partnership with LPN- CNRS (Laboratoire de Photonique et de Nanostructures), and was initially developed for ESA Jupiter Icy Moons Explorer (JUICE), intended to observe Jupiter and its icy moon atmospheres. It is based on a sub-harmonic Schottky diode mixer, designed and fabricated at LERMA-LPN, pumped by a Local Oscillator (LO), consisting of a frequency Amplifier/Multiplier chains (AMCs) from RPG (Radiometer Physics GmBh). The performance of the receiver was demonstrated by absorption spectroscopy of CH_3CH_2CN with Lille's fast-scan DDS spectrometer. A series of test measurements showed the receiver's good sensitivity, stability and frequency accuracy comparable to those of 4K QMC bolometers, thus making room-temperature Schottky receiver a competitive alternative to 4K QMC bolometers to laboratory spectroscopy applications. We will present the first results with such a combination of a compact room temperature Schottky heterodyne receiver and a fast-scan DDS spectrometer. J. Treuttel, L. Gatilova, A. Maestrini et al., 2016, IEEE Trans. Terahertz Science and Tech., 6, 148-155. This work was funded by the French ANR under the Contract No. ANR-13-BS05-0008-02 IMOLABS.

  13. High resolution spectrometer for extended x-ray absorption fine structure measurements in the 6 keV to 15 keV energy range

    Science.gov (United States)

    Seely, J. F.; Hudson, L. T.; Henins, Albert; Feldman, U.

    2016-11-01

    A Cauchois transmission-crystal spectrometer has been developed with high crystal resolving power in the 6 keV-15 keV energy range and sufficient sensitivity to record single-shot spectra from the Lawrence Livermore National Laboratory (LLNL) Titan laser and other comparable or more energetic lasers. The spectrometer capabilities were tested by recording the W L transitions from a laboratory source and the extended x-ray absorption fine structure (EXAFS) spectrum through a Cu foil.

  14. Analysis of the chemical composition of organic aerosol at the Mt. Sonnblick observatory using a novel high mass resolution thermal-desorption proton-transfer-reaction mass-spectrometer (hr-TD-PTR-MS)

    NARCIS (Netherlands)

    Holzinger, R.|info:eu-repo/dai/nl/337989338; Kasper-Giebl, A.; Staudinger, M.; Schauer, G.; Roeckmann, T.|info:eu-repo/dai/nl/304838233

    2010-01-01

    For the first time a high mass resolution thermal desorption proton transfer reaction mass spectrometer (hr-TD-PTR-MS) was deployed in the field to analyze the composition of the organic fraction of aerosols. We report on measurements from the remote Mt. Sonnblick observatory in the Austrian alps

  15. Conformational ordering of biomolecules in the gas phase: nitrogen collision cross sections measured on a prototype high resolution drift tube ion mobility-mass spectrometer.

    Science.gov (United States)

    May, Jody C; Goodwin, Cody R; Lareau, Nichole M; Leaptrot, Katrina L; Morris, Caleb B; Kurulugama, Ruwan T; Mordehai, Alex; Klein, Christian; Barry, William; Darland, Ed; Overney, Gregor; Imatani, Kenneth; Stafford, George C; Fjeldsted, John C; McLean, John A

    2014-02-18

    Ion mobility-mass spectrometry measurements which describe the gas-phase scaling of molecular size and mass are of both fundamental and pragmatic utility. Fundamentally, such measurements expand our understanding of intrinsic intramolecular folding forces in the absence of solvent. Practically, reproducible transport properties, such as gas-phase collision cross-section (CCS), are analytically useful metrics for identification and characterization purposes. Here, we report 594 CCS values obtained in nitrogen drift gas on an electrostatic drift tube ion mobility-mass spectrometry (IM-MS) instrument. The instrument platform is a newly developed prototype incorporating a uniform-field drift tube bracketed by electrodynamic ion funnels and coupled to a high resolution quadrupole time-of-flight mass spectrometer. The CCS values reported here are of high experimental precision (±0.5% or better) and represent four chemically distinct classes of molecules (quaternary ammonium salts, lipids, peptides, and carbohydrates), which enables structural comparisons to be made between molecules of different chemical compositions for the rapid "omni-omic" characterization of complex biological samples. Comparisons made between helium and nitrogen-derived CCS measurements demonstrate that nitrogen CCS values are systematically larger than helium values; however, general separation trends between chemical classes are retained regardless of the drift gas. These results underscore that, for the highest CCS accuracy, care must be exercised when utilizing helium-derived CCS values to calibrate measurements obtained in nitrogen, as is the common practice in the field.

  16. Compact high performance spectrometers using computational imaging

    Science.gov (United States)

    Morton, Kenneth; Weisberg, Arel

    2016-05-01

    Compressive sensing technology can theoretically be used to develop low cost compact spectrometers with the performance of larger and more expensive systems. Indeed, compressive sensing for spectroscopic systems has been previously demonstrated using coded aperture techniques, wherein a mask is placed between the grating and a charge coupled device (CCD) and multiple measurements are collected with different masks. Although proven effective for some spectroscopic sensing paradigms (e.g. Raman), this approach requires that the signal being measured is static between shots (low noise and minimal signal fluctuation). Many spectroscopic techniques applicable to remote sensing are inherently noisy and thus coded aperture compressed sensing will likely not be effective. This work explores an alternative approach to compressed sensing that allows for reconstruction of a high resolution spectrum in sensing paradigms featuring significant signal fluctuations between measurements. This is accomplished through relatively minor changes to the spectrometer hardware together with custom super-resolution algorithms. Current results indicate that a potential overall reduction in CCD size of up to a factor of 4 can be attained without a loss of resolution. This reduction can result in significant improvements in cost, size, and weight of spectrometers incorporating the technology.

  17. Characterization of submicron aerosols at a rural site in Pearl River Delta of China using an Aerodyne High-Resolution Aerosol Mass Spectrometer

    Directory of Open Access Journals (Sweden)

    X.-F. Huang

    2010-11-01

    Full Text Available The Pearl River Delta (PRD region in South China is one of the most economically developed regions in China, but it is also noted for its severe air pollution due to industrial/metropolitan emissions. In order to continuously improve the understanding and quantification of air pollution in this region, an intensive campaign was executed in PRD during October–November 2008. Here, we report and analyze Aerodyne High-Resolution Aerosol Mass Spectrometer measurements at Kaiping, a rural site downwind of the highly-polluted central PRD area, to characterize the general features of submicron particulate pollution in the regional air. The mean measured PM1 mass concentration was 33.1 ± 18.1 μg m−3 during the campaign and composed of organic matter (33.8%, sulfate (33.7%, ammonium (14.0%, nitrate (10.7%, black carbon (6.7%, and chloride (1.1%, which is characterized by high fractions of inorganic ions due to huge emissions of SO2 and NOx in PRD. The average size distributions of the species (except BC were all dominated by an accumulation mode peaking at ~450 nm in vacuum aerodynamic diameter. Calculations based on high-resolution organic mass spectra indicate that C, H, O, and N on average contributed 56.6, 7.0, 35.1, and 1.3% to the total organic mass, respectively, corresponding to an organic matter mass to organic carbon mass ratio (OM/OC of 1.77 ± 0.08. Based on the high-resolution organic mass spectral dataset observed, Positive Matrix Factorization (PMF analysis differentiated the organic aerosol into three components, i.e., biomass burning (BBOA and two oxygenated (LV-OOA and SV-OOA organic aerosols, which on average accounted for 24.5, 39.6 and 35.8% of the total organic mass, respectively. The BBOA showed strong features of biomass burning emissions and has been mainly attributed to field rice straw burning after harvest. The LV-OOA and SV-OOA were found to correspond to more aged (and thus

  18. [A novel spatial modulation Fourier transform spectrometer with adjustable spectral resolution].

    Science.gov (United States)

    Lian, Yu-Sheng; Liao, Ning-Fang; Lü, Hang; Wu, Wen-Min; Dong, Zhi-Gang

    2014-11-01

    In the premise of fulfilling the application requirement, the adjustment of spectral resolution can improve efficiency of data acquisition, data processing and data saving. So, by adjusting the spectral resolution, the performance of spectrometer can be improved, and its application range can be extended. To avoid the problems of the fixed spectral resolution of classical Fourier transform spectrometer, a novel type of spatial modulation Fourier transform spectrometer with adjustable spectral resolution is proposed in this paper. The principle of the novel spectrometer and its interferometer is described. The general expressions of the optical path difference and the lateral shear are induced by a ray tracing procedure. The equivalent model of the novel interferometer is analyzed. Meanwhile, the principle of the adjustment of spectral resolution is analyzed. The result shows that the novel spectrometer has the merits of adjustable spectral resolution, high stability, easy assemblage and adjustment etc. This theoretical study will provide the theoretical basis for the design of the spectrometer with adjustable spectral resolution and expand the application range of Fourier transform spectrometer.

  19. Study of $ \\bar{p} $ and $ \\bar{n} $ annihilations at LEAR with OBELIX, a large acceptance and high resolution detector based on the Open Axial Field Spectrometer

    CERN Multimedia

    2002-01-01

    % PS201 Study of $\\bar{p}$ and $\\bar{n}$ annihilations at LEAR with OBELIX, a large acceptance and high resolution detector based on the Open Axial Field Spectrometer \\\\ \\\\OBELIX is designed to study exclusive final states of antiproton and antineutron annihilations at low energies with protons and nuclei. \\\\ \\\\The physics motivations of the experiment are:\\\\ \\\\\\begin{itemize} \\item (gg, ggg), hybrids ($ q \\bar{q} g $), multiquarks ($ q q \\bar{q} \\bar{q} $) and light mesons ($ q \\bar{q} $) produced in $ N \\bar{N} $ annihilations and study of their spectroscopy and decays. Also broad structures will be searched for by comparing identical decay modes in exclusive final states of the same type occuring from initial states with different angular momentum or isospin. \\item Study of the dynamics of $ N \\bar{N} $ interactions and of the dependence of the final and intermediate resonant states of annihilation upon the quantum numbers of the initial $ N \\bar{N} $ state (angular momentum: S and P-wave in $\\bar{p}p $ at...

  20. Chemical Characteristics of Particulate Matter from Vehicle emission using High Resolution Time of Flight Aerosol Mass Spectrometer (HR-ToF-AMS)

    Science.gov (United States)

    Park, T.; Lee, T.; Kang, S.; Lee, J.; Kim, J.; Son, J.; Yoo, H. M.; Kim, K.; Park, G.

    2015-12-01

    Car emissions are major contributors of particulate matter (PM) in the urban environment and effects of air pollution, climate change, and human activities. By increasing of interest in research of car emission for assessment of the PM control, it became require to understand the chemical composition and characteristics of the car exhaust gases and particulate matter. To understand car emission characteristics of PM, we will study PM of car emissions for five driving modes (National Institute Environmental Research (NIER)-5, NIER-9, NIER-12, NIER-14) and three fixed speed driving modes (30km/h, 70km/h, 110km/h) using different fuel types (gasoline, diesel, and LPG) at Transportation Pollution Research Center (TPRC) of NIER in Incheon, South Korea. PM chemical composition of car emission was measured for concentrations of organics, sulfate, nitrate, ammonium, PAHs, oxidation states and size distribution using an Aerodyne High Resolution Time-of-Flight Aerosol Mass Spectrometer (HR-ToF-AMS) and engine exhaust particle sizer (EEPS) on real-time. In the study, organics concentration was dominated for all cases of driving modes and the concentration of organics was increased in 110km/h fixed speed mode for gasoline and diesel. The presentation will provide an overview of the chemical composition of PM in the car emissions.

  1. Improved instrumental line shape monitoring for the ground-based, high-resolution FTIR spectrometers of the Network for the Detection of Atmospheric Composition Change

    Directory of Open Access Journals (Sweden)

    F. Hase

    2012-03-01

    Full Text Available We propose an improved monitoring scheme for the instrumental line shape (ILS of high-resolution, ground-based FTIR (Fourier Transform InfraRed spectrometers used for chemical monitoring of the atmosphere by the Network for Detection of Atmospheric Composition Change (NDACC. Good ILS knowledge is required for the analysis of the recorded mid-infrared spectra. The new method applies a sequence of measurements using different gas cells instead of a single calibration cell. Three cells are used: cell C1 is a refillable cell offering 200 mm path length and equipped with a pressure gauge (filled with 100 Pa N2O, cells C2 and C3 are sealed cells offering 75 mm path length. C2 is filled with 5 Pa of pure N2O. Cell C3 is filled with 16 Pa N2O in 200 hPa technical air, so provides pressure-broadened N2O lines. We demonstrate that an ILS retrieval using C1 improves significantly the sensitivity of the ILS retrieval over the current calibration cells used in the network, because this cell provides narrow fully saturated N2O lines. The N2O columns derived from C2 and C3 allow the performance of a highly valuable closure experiment: adopting the ILS retrieved from C1, the N2O columns of C2 and C3 are derived. Because N2O is an inert gas, both columns should be constant on long timescales. Apparent changes in the columns would immediately attract attention and indicate either inconsistent ILS results or instrumental problems of other origin. Two different cells are applied for the closure experiment, because the NDACC spectrometers observe both stratospheric and tropospheric gases: C2 mimics signatures of stratospheric gases, whereas C3 mimics signatures of tropospheric gases.

  2. Characterization of x-ray imaging crystal spectrometer for high-resolution spatially-resolved x-ray Thomson scattering measurements in shock-compressed experiments

    Science.gov (United States)

    Lu, J.; Hill, K. W.; Bitter, M.; Pablant, N. A.; Delgado-Aparicio, L. F.; Efthimion, P. C.; Lee, H. J.; Zastrau, U.

    2017-01-01

    We have proposed, designed and built a dual-channel x-ray imaging crystal spectrometer (XICS) for spectrally- and spatially-resolved x-ray Thomson scattering (XRTS) measurements in the Matter in Extreme Conditions (MEC) end station at the Linac Coherent Light Source (LCLS). This spectrometer employs two spherically-bent germanium (Ge) 220 crystals, which are combined to form a large aperture dispersive element with a spectral bandwidth of 300 eV that enables both the elastic and inelastic x-ray scattering peaks to be simultaneously measured. The apparatus and its characterization are described. A resolving power of 1900 was demonstrated and a spatial resolution of 12 μm was achieved in calibration tests. For XRTS measurements, a narrow-bandwidth (ΔE/Ecarbon plasma produced in shock-compressed samples of different forms of carbon. Preliminary results of the scattering experiments from Pyrolytic Graphite samples that illustrate the utility of the instrument are presented.

  3. Size-resolved aerosol chemistry on Whistler Mountain, Canada with a High-Resolution Aerosol Mass Spectrometer during INTEX-B

    Directory of Open Access Journals (Sweden)

    Y. Sun

    2008-12-01

    Full Text Available An Aerodyne High Resolution Time-of-Flight Aerosol Mass Spectrometer (HR-ToF-AMS was deployed at the peak of Whistler Mountain (elevation 2182 m-MSL, British Columbia, from 19 April to 16 May 2006, as part of the Intercontinental Chemical Transport Experiment Phase B (INTEX-B campaign. The mass concentrations and size distributions of non-refractory submicron particle (NR-PM1 species (i.e., sulfate, nitrate, ammonium, chloride, and organics were measured in situ every 5 min. The HR-ToF-AMS results agreed well with collocated measurements. The average concentration of non-refractory submicron particulate matter (NR-PM1; 1.9 μg m−3 is similar to those observed at other remote, high elevation sites in North America. Episodes of enhanced aerosol loadings were observed, due to influences of regional and trans-Pacific transport of air pollution. Organics and sulfate were the dominant species, on average accounting for 55% and 30%, respectively, of the NR-PM1 mass. The average size distributions of sulfate and ammonium both showed a~large accumulation mode peaking around 500–600 nm in Dva while those of organic aerosol (OA and nitrate peaked at ~300 nm. The size differences suggest that sulfate and OA were mostly present in external mixtures from different source origins. We also quantitatively determined the elemental composition of OA using the high resolution mass spectra. Overall, OA at Whistler Peak was highly oxygenated, with an average organic-mass-to-organic-carbon ratio (OM/OC of 2.28±0.23 and an atomic ratio of oxygen-to-carbon (O/C of 0.83±0.17. The nominal formula for OA was C1H1.66N0.03O0.83 for the entire study. Two significant trans-Pacific dust events originated from Asia were observed at Whistler Peak during this study. While both events were characterized with significant enhancements of coarse mode particles and mineral

  4. A high-throughput neutron spectrometer

    Science.gov (United States)

    Stampfl, Anton; Noakes, Terry; Bartsch, Friedl; Bertinshaw, Joel; Veliscek-Carolan, Jessica; Nateghi, Ebrahim; Raeside, Tyler; Yethiraj, Mohana; Danilkin, Sergey; Kearley, Gordon

    2010-03-01

    A cross-disciplinary high-throughput neutron spectrometer is currently under construction at OPAL, ANSTO's open pool light-water research reactor. The spectrometer is based on the design of a Be-filter spectrometer (FANS) that is operating at the National Institute of Standards research reactor in the USA. The ANSTO filter-spectrometer will be switched in and out with another neutron spectrometer, the triple-axis spectrometer, Taipan. Thus two distinct types of neutron spectrometers will be accessible: one specialised to perform phonon dispersion analysis and the other, the filter-spectrometer, designed specifically to measure vibrational density of states. A summary of the design will be given along with a detailed ray-tracing analysis. Some preliminary results will be presented from the spectrometer.

  5. Optimization of fluorine determination via the molecular absorption of gallium mono-fluoride in a graphite furnace using a high-resolution continuum source spectrometer

    Energy Technology Data Exchange (ETDEWEB)

    Gleisner, Heike, E-mail: H.Gleisner@analytik-jena.d [Analytik Jena AG, Konrad-Zuse-Str. 1, 07745 Jena (Germany); Welz, Bernhard [Departamento de Quimica, Universidade Federal de Santa Catarina, 88040-900 Florianopolis-SC (Brazil); Instituto Nacional de Ciencia e Tecnologia do CNPq-INCT de Energia e Ambiente, Universidade Federal da Bahia, 40170 Salvador, BA (Brazil); Einax, Juergen W. [Department of Environmental Analysis, Institute of Inorganic und Analytical Chemistry, Friedrich Schiller University of Jena, Lessingstr. 8, 07743 Jena (Germany)

    2010-09-15

    The determination of fluorine using the molecular absorption of gallium mono-fluoride (GaF) at the 211.248 nm rotational line has been optimized using a commercially available high-resolution continuum source atomic absorption spectrometer with a transversely heated graphite tube furnace. The electron excitation spectrum of GaF was generated by adding 500 {mu}g Ga per injection into the graphite tube as molecule forming reagent. Best results were obtained by applying Zr as a permanent modifier and a mixed Pd/Zr modifier, thermally pretreated before each sample injection together with the Ga reagent at 1100 {sup o}C. The use of sodium acetate and Ru(III) nitrosyl nitrate as additional modifiers injected together with the sample further improved the performance. This way a maximum pyrolysis temperature of 550 {sup o}C could be used, and the optimum molecule forming temperature was 1550 {sup o}C. Several drinking water samples, a mineral water sample, and two certified reference materials were analyzed using the standard calibration technique; the absence of potential matrix effects was verified by measuring different dilutions and spiking with known fluorine mass. The results were in good agreement with the certified values and those measured by ion selective electrode; the recovery rate for the spiking experiments was between 97% and 106%. The results show that there was no matrix influence for that kind of samples containing relatively high concentrations of Ca, Mg and chloride, which are known to cause interference in GaF molecule absorption. The limit of detection and the characteristic mass of the method were 5.2 and 7.4 pg F, respectively, and were both about a factor of two better than recently published values.

  6. Detection of atmospheric gaseous amines and amides by a high-resolution time-of-flight chemical ionization mass spectrometer with protonated ethanol reagent ions

    Science.gov (United States)

    Yao, Lei; Wang, Ming-Yi; Wang, Xin-Ke; Liu, Yi-Jun; Chen, Hang-Fei; Zheng, Jun; Nie, Wei; Ding, Ai-Jun; Geng, Fu-Hai; Wang, Dong-Fang; Chen, Jian-Min; Worsnop, Douglas R.; Wang, Lin

    2016-11-01

    Amines and amides are important atmospheric organic-nitrogen compounds but high time resolution, highly sensitive, and simultaneous ambient measurements of these species are rather sparse. Here, we present the development of a high-resolution time-of-flight chemical ionization mass spectrometer (HR-ToF-CIMS) method, utilizing protonated ethanol as reagent ions to simultaneously detect atmospheric gaseous amines (C1 to C6) and amides (C1 to C6). This method possesses sensitivities of 5.6-19.4 Hz pptv-1 for amines and 3.8-38.0 Hz pptv-1 for amides under total reagent ion signals of ˜ 0.32 MHz. Meanwhile, the detection limits were 0.10-0.50 pptv for amines and 0.29-1.95 pptv for amides at 3σ of the background signal for a 1 min integration time. Controlled characterization in the laboratory indicates that relative humidity has significant influences on the detection of amines and amides, whereas the presence of organics has no obvious effects. Ambient measurements of amines and amides utilizing this method were conducted from 25 July to 25 August 2015 in urban Shanghai, China. While the concentrations of amines ranged from a few parts per trillion by volume to hundreds of parts per trillion by volume, concentrations of amides varied from tens of parts per trillion by volume to a few parts per billion by volume. Among the C1- to C6-amines, the C2-amines were the dominant species with concentrations up to 130 pptv. For amides, the C3-amides (up to 8.7 ppb) were the most abundant species. The diurnal and backward trajectory analysis profiles of amides suggest that in addition to the secondary formation of amides in the atmosphere, industrial emissions could be important sources of amides in urban Shanghai. During the campaign, photo-oxidation of amines and amides might be a main loss pathway for them in daytime, and wet deposition was also an important sink.

  7. High-resolution measurements of the DT neutron spectrum using new CD foils in the Magnetic Recoil neutron Spectrometer (MRS) on the National Ignition Facility

    Energy Technology Data Exchange (ETDEWEB)

    Gatu Johnson, M., E-mail: gatu@psfc.mit.edu; Frenje, J. A.; Li, C. K.; Petrasso, R. D.; Séguin, F. H. [Massachusetts Institute of Technology, Cambridge, Massachusetts 02139 (United States); Bionta, R. M.; Casey, D. T.; Eckart, M. J.; Grim, G. P.; Hartouni, E. P.; Hatarik, R.; Sayre, D. B.; Skulina, K.; Yeamans, C. B. [Lawrence Livermore National Laboratory, Livermore, California 94550 (United States); Farrell, M. P.; Hoppe, M.; Kilkenny, J. D.; Reynolds, H. G.; Schoff, M. E. [General Atomics, San Diego, California 92186 (United States)

    2016-11-15

    The Magnetic Recoil neutron Spectrometer (MRS) on the National Ignition Facility measures the DT neutron spectrum from cryogenically layered inertial confinement fusion implosions. Yield, areal density, apparent ion temperature, and directional fluid flow are inferred from the MRS data. This paper describes recent advances in MRS measurements of the primary peak using new, thinner, reduced-area deuterated plastic (CD) conversion foils. The new foils allow operation of MRS at yields 2 orders of magnitude higher than previously possible, at a resolution down to ∼200 keV FWHM.

  8. Characterization of submicron aerosols during a serious pollution month in Beijing (2013 using an aerodyne high-resolution aerosol mass spectrometer

    Directory of Open Access Journals (Sweden)

    J. K. Zhang

    2013-07-01

    Full Text Available In January 2013, Beijing experienced several serious haze events. To achieve a better understanding of the characteristics, sources and processes of aerosols during this month, an Aerodyne High-Resolution Time-of-Flight Aerosol Mass Spectrometer (HR-ToF-AMS was deployed at an urban site between 1 January and 1 February 2013 to obtain the size-resolved chemical composition of non-refractory submicron particles (NR-PM1. During this period, the mean measured NR-PM1 mass concentration was 87.4 μg m-3 and was composed of organics (49.8%, sulfate (21.4%, nitrate (14.6%, ammonium (10.4%, and chloride (3.8%. Moreover, inorganic matter, such as sulfate and nitrate comprised an increasing fraction of the NR-PM1 load as NR-PM1 loading increased, denoting their key roles in particulate pollution during this month. The average size distributions of the species were all dominated by an accumulation mode peaking at approximately 600 nm in vacuum aerodynamic diameter and organics characterized by an additional smaller size (∼200 nm. Elemental analyses showed that the average O/C, H/C, and N/C (molar ratio of organic matter were 0.34, 1.44 and 0.015, respectively, corresponding to an OM/OC ratio (mass ratio of organic matter to organic carbon of 1.60. Positive matrix factorization (PMF analyses of the high-resolution organic mass spectral dataset differentiated the organic aerosol into four components, i.e., oxygenated organic aerosols (OOA, cooking-related (COA, nitrogen-containing (NOA and hydrocarbon-like (HOA, which on average accounted for 40.0, 23.4, 18.1 and 18.5% of the total organic mass, respectively. Back trajectory clustering analyses indicated that the WNW air masses were associated with the highest NR-PM1 pollution during the campaign. Aerosol particles in southern air masses were especially rich in inorganic and oxidized organic species, whereas northern air masses contained a large fraction of primary species.

  9. Angle modulated surface plasmon resonance spectrometer for refractive index sensing with enhanced detection resolution

    Science.gov (United States)

    Zhou, Xinlei; Chen, Ke; Li, Li; Peng, Wei; Yu, Qingxu

    2017-01-01

    We design and manufacture an angle modulated surface plasmon resonance (SPR) spectrometer with high detection resolution for refractive index sensing. The presented SPR spectrometer is based on a five-layer Kretchmann configuration. To enhance the sensitivity and resolution of the SPR spectrometer, we introduce a reference beam into the system, which has improved the stability of the system by nearly one order of magnitude. Numerical simulation and experimental study are presented and the results show that a sensitivity of 85 degrees/RIU (refractive index unit) and a good repeatability (standard deviation=3.7×10-6 RIU) have been achieved.

  10. Resonant inelastic x-ray scattering spectrometer with 25 meV resolution at Cu K-edge

    CERN Document Server

    Ketenoglu, Didem; Klementiev, Konstantin; Upton, Mary; Taherkhani, Mehran; Spiwek, Manfred; Dill, Frank-Uwe; Wille, Hans-Christian; Yavaş, Hasan

    2014-01-01

    An unparalleled resolution is reported with an inelastic x-ray scattering instrument at the Cu K-edge. Based on a segmented concave analyzer, featuring single crystal quartz (SiO_{2}) pixels, the spectrometer delivers a resolution near 25 meV (FWHM) at 8981 eV. Besides the quartz analyzer, the performance of the spectrometer relies on a four-bounce Si(553) high-resolution monochromator and focusing Kirkpatrick-Baez optics. The measured resolution agrees with the ray tracing simulation of an ideal spectrometer. We demonstrated the performance of the spectrometer by reproducing the phonon dispersion curve of a beryllium (Be) single crystal.

  11. (r) Mass Resolution versus Chamber Resolution in ALICE Dimuon Forward Spectrometer

    Institute of Scientific and Technical Information of China (English)

    WU Tao

    2007-01-01

    The precisions and its sources of spatial resolutions of tracking chambers and mass resolutions of dimuon signals in ALICE Dimuon Forward Spectrometer are explored by tracking and reconstruction of AliRoot software. The dependences of (r) mass resolution on spatial resolution of tracking chambers are presented with and without background events through simulations.

  12. Temperature and pressure retrievals and mitigation of the impact of dust for a high-resolution Fourier transform spectrometer mission to Mars

    Science.gov (United States)

    Olsen, Kevin Sutherland

    On the path to sending a Fourier transform spectrometer (FTS) to Mars to measure the trace gas composition of the atmosphere, several critical elements of the analysis routine need to be adapted from Earth to Mars observation. I have developed new algorithms and software for retrieving vertical profiles of temperature and pressure from infrared spectra, and created interferograms simulating observations at Mars in the presence of dust. The temperature and pressure retrieval algorithm exploits the temperature dependence of absorption lines in CO2 vibration rotation bands. It was applied to terrestrial spectra from the Atmospheric Chemistry Experiment (ACE) FTS, a solar occultation instrument in orbit since 2003, and the basis for the instrument selected for a Mars mission. ACE-FTS makes multiple spectral measurements during an occultation, separated in altitude by 1.5-5 km, and ten CO2 bands are analyzed at each altitude, each with a different usable altitude range. I present an inter-comparison of temperature profiles retrieved from ACE-FTS using my algorithm and that of the ACE Science Team, and from the Constellation Observing System for Meteorology, Ionosphere, and Climate (COSMIC, coincident within 1.5 hours and 150 km). Compared to the ACE-FTS standard product, my retrievals exhibit mean differences between -5 and +2 K and compared to COSMIC, mean differences are between -4 and +1 K. A solar occultation FTS vertically scans the limb of the atmosphere continuously, and so the optical path for a Mars observation will move through layers of varying dust levels during a single interferogram acquisition, resulting in source intensity variations (SIVs), negatively impacting trace gas retrievals. I have simulated SIV using synthetic spectra for the Martian atmosphere, and investigated high-pass filters in the wavenumber domain, and smoothing methods in the optical path difference (OPD) domain. The use of a convolution operator in the OPD domain can isolate the SIV

  13. Characterization of the sources and processes of organic and inorganic aerosols in New York City with a high-resolution time-of-flight aerosol mass spectrometer

    Directory of Open Access Journals (Sweden)

    Y.-L. Sun

    2010-10-01

    Full Text Available Submicron aerosol particles (PM1 were measured in-situ using a High-Resolution Time-of-Flight Aerosol Mass Spectrometer (HR-ToF-AMS during the summer 2009 Field Intensive Study at Queens College in New York City. Organic aerosol (OA and sulfate are the two dominant species, accounting for 54% and 24%, respectively, of total PM1 mass on average. The average mass size distribution of OA presents a small mode peaking at ~150 nm (Dva in addition to an accumulation mode (~550 nm that is internally mixed with sulfate, nitrate, and ammonium. The diurnal cycles of sulfate and OA both show pronounced peaks between 01:00–02:00 p.m. EST due to photochemical production. The average (±1σ oxygen-to-carbon (O/C, hydrogen-to-carbon (H/C, and nitrogen-to-carbon (N/C ratios of OA in NYC are 0.36 (±0.09, 1.49 (±0.08, and 0.012(±0.005, respectively, corresponding to an average organic mass-to-carbon (OM/OC ratio of 1.62(±0.11. Positive matrix factorization (PMF of the high resolution mass spectra identified five OA components: a hydrocarbon-like OA (HOA, two types of oxygenated OA (OOA including a low-volatility OOA (LV-OOA and a semi-volatile OOA (SV-OOA, a cooking-emission related OA (COA, and a unique nitrogen-enriched OA (NOA. HOA appears to represent primary OA (POA from urban traffic emissions. It comprises primarily of reduced species (H/C=1.83; O/C=0.06 and shows a mass spectral pattern very similar to those of POA from fossil fuel combustion, and correlates tightly with traffic emission tracers including elemental carbon and NOx. LV-OOA, which is highly oxidized (O/C=0.63 and correlates well with sulfate, appears to be representative for regional, aged secondary OA (SOA. SV-OOA, which is less oxidized (O/C=0.38 and correlates well with non-refractory chloride, likely represents less photo-chemically aged, semi-volatile SOA. COA shows a similar spectral pattern to the reference spectra of POA from

  14. Sources and atmospheric processing of winter aerosols in Seoul, Korea: insights from real-time measurements using a high-resolution aerosol mass spectrometer

    Science.gov (United States)

    Kim, Hwajin; Zhang, Qi; Bae, Gwi-Nam; Kim, Jin Young; Bok Lee, Seung

    2017-02-01

    Highly time-resolved chemical characterization of nonrefractory submicrometer particulate matter (NR-PM1) was conducted in Seoul, the capital and largest metropolis of Korea, using an Aerodyne high-resolution time-of-flight aerosol mass spectrometer (HR-ToF-AMS). The measurements were performed during winter, when elevated particulate matter (PM) pollution events are often observed. This is the first time that detailed real-time aerosol measurement results have been reported from Seoul, Korea, and they reveal valuable insights into the sources and atmospheric processes that contribute to PM pollution in this region. The average concentration of submicron aerosol (PM1 = NR-PM1+ black carbon (BC)) was 27.5 µg m-3, and the total mass was dominated by organics (44 %), followed by nitrate (24 %) and sulfate (10 %). The average atomic ratios of oxygen to carbon (O / C), hydrogen to carbon (H / C), and nitrogen to carbon (N / C) of organic aerosols (OA) were 0.37, 1.79, and 0.018, respectively, which result in an average organic mass-to-carbon (OM / OC) ratio of 1.67. The concentrations (2.6-90.7 µg m-3) and composition of PM1 varied dynamically during the measurement period due to the influences of different meteorological conditions, emission sources, and air mass origins. Five distinct sources of OA were identified via positive matrix factorization (PMF) analysis of the HR-ToF-AMS data: vehicle emissions represented by a hydrocarbon-like OA factor (HOA, O / C = 0.06), cooking activities represented by a cooking OA factor (COA, O / C = 0.14), wood combustion represented by a biomass burning OA factor (BBOA, O / C = 0.34), and secondary organic aerosol (SOA) represented by a semivolatile oxygenated OA factor (SV-OOA, O / C = 0.56) and a low-volatility oxygenated OA factor (LV-OOA, O / C = 0.68). On average, primary OA (POA = HOA + COA + BBOA) accounted for 59 % the OA mass, whereas SV-OOA and LV-OOA contributed 15 and 26 %, respectively. Our results indicate that air

  15. Synchrotron X-ray tests of an L-shaped laterally graded multilayer mirror for the analyzer system of the ultra-high-resolution IXS spectrometer at NSLS-II.

    Science.gov (United States)

    Honnicke, Marcelo G; Keister, Jeffrey W; Conley, Raymond; Kaznatcheev, Konstantine; Takacs, Peter Z; Coburn, David Scott; Reffi, Leo; Cai, Yong Q

    2011-11-01

    Characterization and testing of an L-shaped laterally graded multilayer mirror are presented. This mirror is designed as a two-dimensional collimating optics for the analyzer system of the ultra-high-resolution inelastic X-ray scattering (IXS) spectrometer at National Synchrotron Light Source II (NSLS-II). The characterization includes point-to-point reflectivity measurements, lattice parameter determination and mirror metrology (figure, slope error and roughness). The synchrotron X-ray test of the mirror was carried out reversely as a focusing device. The results show that the L-shaped laterally graded multilayer mirror is suitable to be used, with high efficiency, for the analyzer system of the IXS spectrometer at NSLS-II.

  16. Primary support of high resolution space imaging spectrometer%空间成像光谱仪的主体支撑方式

    Institute of Scientific and Technical Information of China (English)

    张军强; 董得义; 颜昌翔

    2009-01-01

    为了改善空间成像光谱仪主体支撑方式对系统光机结构稳定性的影响,分析了成像光谱仪对主体支撑结构的要求,介绍了常用空间光学遥感仪器的支撑方式.在传统支耳支撑方式不能满足离轴非球面三反射镜(TMA)系统热稳定性的情况下,提出了一种新的双耦合的支撑方案并对其进行了理论分析.优化设计过程中,采用有限元分析软件MSC.PATRAN对其三维样机进行工程分析,结果显示,在正弦振动载荷作用下,主体一阶频率为95 Hz;在10 ℃均匀温降与自重耦合作用下,各反射镜的镜面变形RMS最大值为12 nm、PV最大值为60 nm,主镜绕Z轴的转角由原来的55″降低为12″,热真空环境下整机成像试验获得的光谱数据验证了工程分析的正确性,表明双耦合的支撑方案能满足整机刚度和光机系统对热稳定性的要求.%With the aim to improve the effect of the primary support of a space High Resolution Imaging Spectrometer (HRIS) on its stability of optic-mechanic system,the requirements were analyzed for the rigidity and heat stability of a common space remote sensor.The traditional support structures to the space optical remote sensors were introduced.As the traditional supports by lags could not meet the need of the three-mirror anastigmatic (TMA) imaging system,a new coupling support structure by two axes was presented and its theory was analyzed.The finite element analysis of a 3D model was realized by software MSC.PATRAN during the optimum designing.The results show that the first order natural frequency is 95 Hz under sine vibration loading.The maximum RMS value and the maximum PV value of the mirror surface aberration are 12 nm and 60 nm under both of a 10 "C temperature fall and the influence of the gravity,respectively.The angle rotation by the Z axis of primary mirror is reduced from 55" to 12".The spectral data of the optical system under the hot vacuum environments verify the analysis

  17. Ground-based remote sensing of O3 by high- and medium-resolution FTIR spectrometers over the Mexico City basin

    Science.gov (United States)

    Plaza-Medina, Eddy F.; Stremme, Wolfgang; Bezanilla, Alejandro; Grutter, Michel; Schneider, Matthias; Hase, Frank; Blumenstock, Thomas

    2017-07-01

    We present atmospheric ozone (O3) profiles measured over central Mexico between November 2012 and February 2014 from two different ground-based FTIR (Fourier transform infrared) solar absorption experiments. The first instrument offers very high-resolution spectra and contributes to NDACC (Network for the Detection of Atmospheric Composition Change). It is located at a mountain observatory about 1700 m above the Mexico City basin. The second instrument has a medium spectral resolution and is located inside Mexico City at a horizontal distance of about 60 km from the mountain observatory. It is documented that the retrieval with the high- and medium-resolution experiments provides O3 variations for four and three independent atmospheric altitude ranges, respectively, and the theoretically estimated errors of these profile data are mostly within 10 %. The good quality of the data is empirically demonstrated above the tropopause by intercomparing the two FTIR O3 data, and for the boundary layer by comparing the Mexico City FTIR O3 data with in situ O3 surface data. Furthermore, we develop a combined boundary layer O3 remote sensing product that uses the retrieval results of both FTIR experiments, and we use theoretical and empirical evaluations to document the improvements that can be achieved by such a combination.

  18. Ground-based remote sensing of O3 by high- and medium-resolution FTIR spectrometers over the Mexico City basin

    Directory of Open Access Journals (Sweden)

    E. F. Plaza-Medina

    2017-07-01

    Full Text Available We present atmospheric ozone (O3 profiles measured over central Mexico between November 2012 and February 2014 from two different ground-based FTIR (Fourier transform infrared solar absorption experiments. The first instrument offers very high-resolution spectra and contributes to NDACC (Network for the Detection of Atmospheric Composition Change. It is located at a mountain observatory about 1700 m above the Mexico City basin. The second instrument has a medium spectral resolution and is located inside Mexico City at a horizontal distance of about 60 km from the mountain observatory. It is documented that the retrieval with the high- and medium-resolution experiments provides O3 variations for four and three independent atmospheric altitude ranges, respectively, and the theoretically estimated errors of these profile data are mostly within 10 %. The good quality of the data is empirically demonstrated above the tropopause by intercomparing the two FTIR O3 data, and for the boundary layer by comparing the Mexico City FTIR O3 data with in situ O3 surface data. Furthermore, we develop a combined boundary layer O3 remote sensing product that uses the retrieval results of both FTIR experiments, and we use theoretical and empirical evaluations to document the improvements that can be achieved by such a combination.

  19. Ground-based Measurements of Vertical Profiles and Columns of Atmospheric Trace Gases Over Toronto Using a New High-Resolution Fourier Transform Infrared Spectrometer

    Science.gov (United States)

    Wiacek, A.; Yashcov, D.; Strong, K.; Boudreau, L.; Rochette, L.; Roy, C.

    2002-12-01

    The University of Toronto Atmospheric Observatory (TAO) has recently been established at Toronto, Canada. TAO includes several instruments, with a DA8 Fourier Transform Spectrometer (DA8 FTS, manufactured by ABB Bomem Inc., Québec, Canada) serving as the primary instrument at the facility. The geographic position of TAO (43.66°N, 79.40°W) makes it well suited for long-term measurements of mid-latitude stratospheric ozone and related species, while its urban setting enables measurements of tropospheric pollution. The DA8 FTS is based on a Michelson interferometer with a maximum optical path difference of 250 cm, providing a maximum unapodized resolution of 0.0026 cm-1. It is currently equipped with KBr and CaF2 beamsplitters, and InSb and HgCdTe detectors, for coverage of the spectral range from 700 to 4100 cm-1. A new heliostat (manufactured by Aim Controls Inc., California, USA) provides active solar tracking, collecting the incoming solar radiation and directing it into the FTS. The TAO DA8 FTS incorporates a new optical design recently developed by ABB Bomem Inc., which results in a fixed optical axis through the beamsplitter (and a fixed focal point on the detector) as well as a more stable modulation efficiency. The new instrument optics will be discussed. Next, the performance of the instrument will be examined in the context of standard NDSC (Network for the Detection of Stratospheric Change) trace gas column and vertical profile retrieval techniques, which use least squares fitting algorithms (SFIT, SFIT2). TAO has been operational (weather permitting) since October 2001. We have been retrieving columns and vertical profiles of HCl, HF, CH4, OCS, C2H6, CO, N2O and NO2 since May 2002. A detailed error analysis of retrieved columns and vertical profiles has been undertaken for the above species. Future plans for the TAO FTS include comparing our measurements with satellite measurements made by MOPITT, OSIRIS, and the upcoming ACE and MAESTRO instruments

  20. High-Resolution Gamma-Ray Spectrometers using Bulk Absorbers Coupled to Mo/Cu Multilayer Superconducting Transition-Edge Sensors

    Energy Technology Data Exchange (ETDEWEB)

    Chow, D.T.; Loshak, A.; Van Den Berg, M.L.; Frank, M.; Barbee Jr., T.W.; Labov, S.E.

    2000-07-04

    In x-ray and gamma-ray spectroscopy, it is desirable to have detectors with high energy resolution and high absorption efficiency. At LLNL, we have developed superconducting tunnel junction-based single photon x-ray detectors with thin film absorbers that have achieved these goals for photon energies up to 1 keV. However, for energies above 1 keV, the absorption efficiency of these thin-film detectors decreases drastically. We are developing the use of high-purity superconducting bulk materials as microcalorimeter absorbers for high-energy x-rays and gamma rays. The increase in absorber temperature due to incident photons is sensed by a superconducting transition-edge sensor (TES) composed of a Mo/Cu multilayer thin film. Films of Mo and Cu are mutually insoluble and therefore very stable and can be annealed. The multilayer structure allows scaling in thickness to optimize heat capacity and normal state resistance. We measured an energy resolution of 70 eV for 60 keV incident gamma-rays with a 1 x 1 x 0.25 mm{sup 3} Sn absorber. We present x-ray and gamma-ray results from this detector design with a Sn absorber. We also propose the use of an active negative feedback voltage bias to improve the performance of our detector and show preliminary results.

  1. First performance results of a mobile high-resolution MR-ToF mass spectrometer for in-situ analytical mass spectrometry

    Energy Technology Data Exchange (ETDEWEB)

    Lang, Johannes; Ebert, Jens [II. Physikalisches Institut, JLU Giessen (Germany); Dickel, Timo; Plass, Wolfgang; Geissel, Hans; Haettner, Emma; Scheidenberger, Christoph [II. Physikalisches Institut, JLU Giessen (Germany); GSI, Darmstadt (Germany); Yavor, Mikhail [RAS St. Petersburg (Russian Federation)

    2012-07-01

    A mobile multiple-reflection time-of-flight mass spectrometer (MR-TOF-MS) has been designed, built and commissioned. While other mobile mass spectrometers are restricted to low or medium mass resolving power, this MR-TOF-MS allows for the first time for a mass resolving power exceeding 100.000 and a sub ppm accuracy in a transportable format. It can thus resolve isobars and enables to accurately determine the composition and structure of biomolecules. An atmospheric pressure interface provides compatibility to various atmospheric ion sources. The mass spectrometer part comprises an RFQ mass filter, ion cooler, ion trap, time-of-flight analyzer and detector. Supply electronics, DAQ and control system are mounted together with the spectrometer into a single frame with a total volume of only 0.8 m{sup 3}. First results with the MR-TOF-MS are presented, and an overview of envisaged life science applications is given, such as realtime tissue recognition in electrosurgery, identification of mycotoxins and analysis of soil samples for environmental studies.

  2. Improving the energy resolution of bent crystal X-ray spectrometers with position-sensitive detectors.

    Science.gov (United States)

    Honkanen, Ari Pekka; Verbeni, Roberto; Simonelli, Laura; Moretti Sala, Marco; Al-Zein, Ali; Krisch, Michael; Monaco, Giulio; Huotari, Simo

    2014-07-01

    Wavelength-dispersive high-resolution X-ray spectrometers often employ elastically bent crystals for the wavelength analysis. In a preceding paper [Honkanen et al. (2014). J. Synchrotron Rad. 21, 104-110] a theory for quantifying the internal stress of a macroscopically large spherically curved analyser crystal was presented. Here the theory is applied to compensate for the corresponding decrease of the energy resolution. The technique is demonstrated with a Johann-type spectrometer using a spherically bent Si(660) analyser in near-backscattering geometry, where an improvement in the energy resolution from 1.0 eV down to 0.5 eV at 9.7 keV incident photon energy was observed.

  3. Preliminary results from the high resolution gamma-ray and hard x-ray spectrometer (HIREGS) '92-'93 long duration balloon flight in Antarctica

    Energy Technology Data Exchange (ETDEWEB)

    Lin, R.P.; Feffer, P.T.; Slassi, S.; Whiteside, W.; Smith, D.M.; Hurley, K.C.; Kane, S.R.; McBride, S.; Primbsch, J.H.; Youssefi, K.; Zimmer, G. (Univ. of California, Berkeley, CA (United States)); Pelling, R.M. (Univ. of California, San Diego, CA (United States)); Cotin, F.; Lavigne, J.M.; Rouaix, G.; Vedrenne, G.; Pehl, R.; Cork, C.; Luke, P.; Madden, N.; Malone, D.

    1993-01-01

    HIREGS consists of an array of twelve 6.7 cm diameter x 6.1 cm long liquid nitrogen-cooled segmented germanium detectors enclosed in a bismuth germanate (BGO) active anticoincidence shield. A CsI front collimator defines a 24 degree FWHM field-of-view. The energy resolution is one to several keV FWHM over the instrument energy range of 20 keV to 16 MeV. HIREGS was flown on a 10-day (31 Dec 92--10 Jan 93) circumpolar balloon flight from McMurdo Station, Antarctica. 30.5 hours of observation were obtained between 31 Dec 0400-2130 UT and 1 Jan 0600-1900 UT. Because the Sun was inactive during the flight, only one small flare was detected on 31 Dec 1933 UT. Excellent high resolution [open quotes]quiet[close quotes] Sun hard X-ray and gamma-ray spectra were obtained. These provide stringent upper limits for solar gamma-ray line and hard X-ray and gamma-ray continuum emission, which in turn can constrain the storage and/or continuous acceleration of ions and electrons by the Sun.

  4. Further development and application of a mobile multiple-reflection time-of-flight mass spectrometer for analytical high-resolution tandem mass spectrometry

    OpenAIRE

    Lippert, Wayne

    2016-01-01

    In this work, a mobile multiple-reflection time-of-flight mass spectrometer (MR-TOF-MS) for analytical mass spectrometry was enhanced in many important aspects. Technical as well as software-based improvements have been added to the instrument, thus greatly increasing its performance and applicability. Changes have been applied to the whole beam preparation system of the MR-TOF-MS. In this context, the electronic setup was completely overhauled and a quadrupole mass filter was commissioned. C...

  5. The Cosmic Infrared Background Experiment (CIBER): The Low Resolution Spectrometer

    CERN Document Server

    Tsumura, K; Battle, J; Bock, J; Brown, S; Cooray, A; Hristov, V; Keating, B; Kim, M G; Lee, D H; Levenson, L R; Lykke, K; Mason, P; Matsumoto, T; Matsuura, S; Murata, K; Nam, U W; Renbarger, T; Smith, A; Sullivan, I; Suzuki, K; Wada, T; Zemcov, M

    2011-01-01

    Absolute spectrophotometric measurements of diffuse radiation at 1 \\mu m to 2 \\mu m are crucial to our understanding of the radiative content of the Universe from nucleosynthesis since the epoch of reionization, the composition and structure of the Zodiacal dust cloud in our solar system, and the diffuse galactic light arising from starlight scattered by interstellar dust. The Low Resolution Spectrometer (LRS) on the rocket-borne Cosmic Infrared Background Experiment (CIBER) is a \\lambda / \\Delta \\lambda \\sim 15-30 absolute spectrophotometer designed to make precision measurements of the absolute near-infrared sky brightness between 0.75 \\mu m < \\lambda < 2.1 \\mu m. This paper presents the optical, mechanical and electronic design of the LRS, as well as the ground testing, characterization and calibration measurements undertaken before flight to verify its performance. The LRS is shown to work to specifications, achieving the necessary optical and sensitivity performance. We describe our understanding a...

  6. High Pressure XENON Gamma-Ray Spectrometers for Field Use

    Energy Technology Data Exchange (ETDEWEB)

    David K. Wehe; Zong He; Glenn K. Knoll

    2004-02-16

    This project explored a new concept for high-pressure xenon ionization chambers by replacing the Frisch grid with coplanar grid electrodes similar to those used in wide bandgap semiconductor gamma-ray spectrometers. This work is the first attempt to apply the coplanar grid anode design in a gas ionization chamber in order to achieve to improved energy resolution. Three prototype detectors, two cylindrical and one parallel plate configurations, were built and tested. While the detectors did not demonstrate energy resolutions as good as other high pressure xenon gamma-ray spectrometers, the results demonstrated that the concept of single polarity charge sending using coplanar grid electrodes will work in a gas detector.

  7. High-resolution glacial and deglacial record of atmospheric methane by continuous-flow and laser spectrometer analysis along the NEEM ice core

    Directory of Open Access Journals (Sweden)

    J. Chappellaz

    2013-05-01

    Full Text Available The Greenland NEEM (North Greenland Eemian Ice Drilling operation in 2010 provided the first opportunity to combine trace-gas measurements by laser spectroscopic instruments and continuous-flow analysis along a freshly drilled ice core in a field based setting. We present the resulting atmospheric methane (CH4 record covering the time period from 107.7 to 9.5 ka b2k (thousand years before 2000 AD. Companion discrete CH4 measurements are required to transfer the laser spectroscopic data from a relative to an absolute scale. However, even on a relative scale, the high-resolution CH4 dataset significantly improves our knowledge of past atmospheric methane concentration changes. New significant sub-millennial-scale features appear during interstadials and stadials, generally associated with similar changes in water isotopic ratios of the ice, a proxy for local temperature. In addition to the mid-point of Dansgaard/Oeschger (D/O CH4 transitions usually used for cross-dating, sharp definition of the start and end of these events brings precise depth markers (with ±20 cm uncertainty for further cross-dating with other ice core or paleo records, e.g. speleothems. The method also provides an estimate of CH4 rates of change. The onsets of D/O events in the methane signal show a more rapid rate of change than their endings. The rate of CH4 increase associated with the onsets of D/O events progressively declines from 1.7 to 0.6 ppbv yr−1 in the course of Marine Isotope Stage 3. The largest observed rate of increase takes place at the onset of D/O event #21 and reaches 2.5 ppbv yr−1.

  8. VAMOS: a VAriable MOde high acceptance Spectrometer

    CERN Document Server

    Savajols, H

    1999-01-01

    The study of reactions induced by the future SPIRAL beams at GANIL requires new techniques: the low intensity of secondary beams implies the need of a very high efficiency detection system ; the study of nearly or completely unknown nuclei, over a wide range of masses and energies, needs a very efficient method for attributing a reaction product to a nucleus. The VAriable MOde high acceptance Spectrometer VAMOS is being designed and built especially for this purpose.

  9. A high-resolution multi-parametric study of sup 239 Pu(n sub th , f) with the Cosi-Fan-Tutte spectrometer

    Energy Technology Data Exchange (ETDEWEB)

    Boucheneb, N. (Inst. de Physique, USTHB, Algiers (Algeria) Centre d' Etudes Nucleaires, 33 - Bordeaux-Gradignan (France)); Asghar, M. (Inst. de Physique, USTHB, Algiers (Algeria)); Barreau, G.; Doan, T.P.; Leroux, B.; Sicre, A. (Centre d' Etudes Nucleaires, 33 - Bordeaux-Gradignan (France)); Geltenbrot, P.; Oed, A. (Inst. Laue-Langevin, 38 - Grenoble (France))

    1991-12-09

    The Cosi-Fan-Tutte spectrometer has been used to measure for the first time in one go the mass-nuclear charge-energy correlations of well-resolved light group masses for {sup 239}Pu(n{sub th}, f). About 2x10{sup 6} events were collected and analysed. The global mass distribution is consistent with the Lohengrin data. The mean proton odd-even effects in yields and energy are {delta}{sub p}=(11.8{+-}0.3)% and {delta}E{sub K}{sup o-e}=0.49{+-}0.15 MeV respectively. The {delta}{sub p}(E{sub L}) varies from {approx equal}7% to {approx equal}25% for E{sub L}=90 to 116 MeV. The present analysis consists of 21 values of E{sub L} compared to only 5 values for Lohengrin. The apparent mean neutron odd-even effect {delta}{sub n}=(3.5{+-}0.1)% is much lower than the {delta}{sub n}=(6.5{+-}0.7)% for Lohengrin. The mean value of conditional variance <{sigma}{sub Z}{sup 2}(Zvertical strokeA)>=(0.42{+-}0.02); the <{sigma}{sub Z}{sup 2}(Zvertical strokeA)> increases from {sup 230}Th to {sup 250}Cf and this behaviour turns out to be important for understanding the dynamics of the fission process. (orig.).

  10. The Cosmic Infrared Background Experiment (CIBER): The Low Resolution Spectrometer

    Science.gov (United States)

    Tsumura, K.; Arai, T.; Battle, J.; Bock, J.; Brown, S.; Cooray, A.; Hristov, V.; Keating, B.; Kim, M. G.; Lee, D. H.; Levenson, L. R.; Lykke, K.; Mason, P.; Matsumoto, T.; Matsuura, S.; Murata, K.; Nam, U. W.; Renbarger, T.; Smith, A.; Sullivan, I.; Suzuki, K.; Wada, T.; Zemcov, M.

    2013-08-01

    Absolute spectrophotometric measurements of diffuse radiation at 1 μm to 2 μm are crucial to our understanding of the radiative content of the universe from nucleosynthesis since the epoch of reionization, the composition and structure of the zodiacal dust cloud in our solar system, and the diffuse galactic light arising from starlight scattered by interstellar dust. The Low Resolution Spectrometer (LRS) on the rocket-borne Cosmic Infrared Background Experiment is a λ/Δλ ~ 15-30 absolute spectrophotometer designed to make precision measurements of the absolute near-infrared sky brightness between 0.75 μm <λ < 2.1 μm. This paper presents the optical, mechanical, and electronic design of the LRS, as well as the ground testing, characterization, and calibration measurements undertaken before flight to verify its performance. The LRS is shown to work to specifications, achieving the necessary optical and sensitivity performance. We describe our understanding and control of sources of systematic error for absolute photometry of the near-infrared extragalactic background light.

  11. THE COSMIC INFRARED BACKGROUND EXPERIMENT (CIBER): THE LOW RESOLUTION SPECTROMETER

    Energy Technology Data Exchange (ETDEWEB)

    Tsumura, K.; Arai, T.; Matsumoto, T.; Matsuura, S.; Murata, K. [Department of Space Astronomy and Astrophysics, Institute of Space and Astronoutical Science (ISAS), Japan Aerospace Exploration Agency (JAXA), Sagamihara, Kanagawa 252-5210 (Japan); Battle, J.; Bock, J. [Jet Propulsion Laboratory (JPL), National Aeronautics and Space Administration (NASA), Pasadena, CA 91109 (United States); Brown, S.; Lykke, K.; Smith, A. [Optical Technology Division, National Institute of Standards and Technology (NIST), Gaithersburg, MD 20899 (United States); Cooray, A. [Center for Cosmology, University of California, Irvine, Irvine, CA 92697 (United States); Hristov, V.; Levenson, L. R.; Mason, P. [Department of Astronomy, California Institute of Technology, Pasadena, CA 91125 (United States); Keating, B.; Renbarger, T. [Department of Physics, University of California, San Diego, San Diego, CA 92093 (United States); Kim, M. G. [Department of Physics and Astronomy, Seoul National University, Seoul 151-742 (Korea, Republic of); Lee, D. H.; Nam, U. W. [Korea Astronomy and Space Science Institute (KASI), Daejeon 305-348 (Korea, Republic of); Sullivan, I., E-mail: tsumura@ir.isas.jaxa.jp [Department of Physics, The University of Washington, Seattle, WA 98195 (United States); and others

    2013-08-15

    Absolute spectrophotometric measurements of diffuse radiation at 1 {mu}m to 2 {mu}m are crucial to our understanding of the radiative content of the universe from nucleosynthesis since the epoch of reionization, the composition and structure of the zodiacal dust cloud in our solar system, and the diffuse galactic light arising from starlight scattered by interstellar dust. The Low Resolution Spectrometer (LRS) on the rocket-borne Cosmic Infrared Background Experiment is a {lambda}/{Delta}{lambda} {approx} 15-30 absolute spectrophotometer designed to make precision measurements of the absolute near-infrared sky brightness between 0.75 {mu}m <{lambda} < 2.1 {mu}m. This paper presents the optical, mechanical, and electronic design of the LRS, as well as the ground testing, characterization, and calibration measurements undertaken before flight to verify its performance. The LRS is shown to work to specifications, achieving the necessary optical and sensitivity performance. We describe our understanding and control of sources of systematic error for absolute photometry of the near-infrared extragalactic background light.

  12. High resolution measurements of mass, energy and nuclear charge correlations for sup 229 Th(n sub th ,f) with the COSI FAN TUTTE spectrometer

    Energy Technology Data Exchange (ETDEWEB)

    Boucheneb, N. (Bordeaux-1 Univ., 33 - Gradignan (France). Centre d' Etudes Nucleaires; Universite des Sciences et de la Technologie Houari Boumedienne, Algiers (Algeria). Inst. de Physique); Geltenbort, P.; Oed, A. (Institut Max von Laue - Paul Langevin, 38 - Grenoble (France)); Barreau, G.; Doan, T.P.; Leroux, B.; Sicre, A. (Institut Max von Laue - Paul Langevin, 38 - Grenoble (France)); Asghar, M. (Universite des Sciences et de la Technologie Houari Boumedienne, Algiers (Algeria). Inst. de Physique); Goennenwein, F. (Tuebingen Univ. (Germany, F.R.))

    1989-10-09

    The COSI FAN TUTTE spectrometer has been used to measure for the first time in one go the mass-charge-energy correlations for well-resolved light group masses for {sup 229}Th(n{sub th},f). About 4.8x10{sup 5} events were collected in a {approx equal} 3 months run. The global mass distribution shows structures and the distribution for E{sub L}=(112+-0.5) MeV is dominated by mass number A{sub L}=86 and 96. The mean kinetic energy shows strong fluctuations as a function of the light fragment mass A{sub L}. The mean proton odd-even effects in yields and energy are {delta}p=(40.0+-1.0)% and {delta}E{sub TKE}{sup o-e}=(1.35+-0.17) MeV, respectively. The {delta}p(E{sub L}) varies by a factor of {approx equal} 3 for E{sub L}=92 to 107 MeV with a plateau for E{sub L}{approx equal} 96 to 103 MeV. The mean neutron odd-even effect is {delta}n=(1.95+-0.5)%. The mean value of the conditional variance is <{sigma}{sup 2}(Zvertical strokeA)>=(0.33+-0.02) and it varies little with energy. The conditional variance seems to decrease as one goes from {sup 252}Cf to {sup 230}Th. These data are discussed in the context of existing results on other nuclei. (orig.).

  13. High Accuracy Wavelength Calibration For A Scanning Visible Spectrometer

    Energy Technology Data Exchange (ETDEWEB)

    Filippo Scotti and Ronald Bell

    2010-07-29

    Spectroscopic applications for plasma velocity measurements often require wavelength accuracies ≤ 0.2Â. An automated calibration for a scanning spectrometer has been developed to achieve a high wavelength accuracy overr the visible spectrum, stable over time and environmental conditions, without the need to recalibrate after each grating movement. The method fits all relevant spectrometer paraameters using multiple calibration spectra. With a steping-motor controlled sine-drive, accuracies of ~0.025 Â have been demonstrated. With the addition of high resolution (0.075 aresec) optical encoder on the grading stage, greater precision (~0.005 Â) is possible, allowing absolute velocity measurements with ~0.3 km/s. This level of precision requires monitoring of atmospheric temperature and pressure and of grating bulk temperature to correct for changes in the refractive index of air and the groove density, respectively.

  14. The method of improving the spatial resolution of the matrix spectrometer

    Science.gov (United States)

    Krot, Yury; Beliaev, Boris; Katkovsky, Leonid

    2014-10-01

    The videospectral system (VSS) intended for ecological space experiment on board of the International Space Station (ISS) has been developed by the Aerospace Researches Department of the Institute of Applied Physical Problems of the Belarusian State University. The system comprises three matrix spectrometers MP-15. The polychromator of each spectrometer includes the imaging fiber, the entrance slit, concave holographic diffraction grating, and a CCD array detector. The array photodetector measures the spectral radiation distribution in rows, and the spatial distribution (image) in columns. Astigmatism is a typical aberration of polychromators based on concave spherical gratings - rays in tangential and sagittal planes are focused at different points. This degrades as for spectral and spatial resolution along the entrance slit. The proposed method of obtaining high spatial resolution without spectral resolution loss consists in the displacement of the output end of the imaging fiber along the optical axis at a specified distance from the entrance slit. After that the rays in the tangential and sagittal planes focus at one point. The entrance slit operates as a one-dimensional aperture to obtain high spectral resolution.

  15. 大视场高分辨力星载成像光谱仪光学系统设计%Optical System Design of Wide-Angle and High-Resolution Spaceborne Imaging Spectrometer

    Institute of Scientific and Technical Information of China (English)

    薛庆生; 黄煜; 林冠宇

    2011-01-01

    大视场、高分辨力星载成像光谱仪已成为空间遥感的迫切需求.根据大视场、高分辨力的研究目标,提出了先视场分离分光再用分色片分光的设计方法,分析了视场分离分光的原理.设计了一个全反射式星载成像光谱仪光学系统,该系统由指向镜、11.42°远心离轴三反消像散(TMA)前置望远系统和4个Offner凸面光栅光谱成像系统组成,通过恰当选择4个光谱成像系统的变倍比来实现2种探测器的匹配.运用光学设计软件CODE V对成像光谱仪调制系统进行了光线追迹和优化,并对设计结果进行了分析.分析结果表明,光学系统在各个谱段的光学传递函数均达到0.7以上,完全满足设计指标要求;同时证明了设计方法是可行的.%Space remote sensing urgently requires wide-angle and high-resolution spaceborne imaging spectrometer. According to the research objective of wide angle and high resolution, the design method of firstly dividing field of view (FOV) and secondly dividing beam using dichroscope is developed. The principle of dividing FOV is analyzed. A reflective spaceborne imaging spectrometer is designed, which is composed of a pointing mirror, a 11.42° telecentric off-axis three-mirror anastigmatic (TMA) telescope and four Offner convex grating spectral imaging systems. The proper magnification is chosen for each spectral imaging system to match two types of detectors. Ray tracing and optimization are performed and analyzed by CODE V software. The results demonstrate that the modulation transfer function (MTF) for different spectral bands is more than 0. 7, which satisfies the pre-designed requirement. The design method is proved to be feasible.

  16. Chemical characterization of particle emissions from controlled burns of biomass fuels using a high resolution time-of-flight aerosol mass spectrometer

    Science.gov (United States)

    Qi, L.; Hosseini, S.; Jung, H.; Yokelson, B.; Weise, D.; Cocker, D., III; Huang, Y.

    2012-03-01

    A total of forty-nine burns were conducted at the Missoula Fire Sciences Lab consisting of nine fuel types; i.e., chamise scrub oak, ceanothus, maritime chaparral, coastal sage scrub, California sage brush, Manzanita, oak savanna, oak woodland and masticated mesquite. This paper focuses on the chemical characterization of fine particle emissions collected for flaming, mixed and smoldering phases using a HR ToF-AMS. The evolution of OM/OC, H/C, O/C and N/C from fire ignition to extinction was measured to capture the transient and integrated chemical composition of the non-refractory portion of bulk particles. Real time elemental ratios and empirical formulas derived with respect to modified combustion efficiency (MCE) are reported. For each fuel, the hydrogen fragment ions dominate the unit mass resolution (UMR) mass spectra with no specific fragment ions attributable to an individual ecological combination. An interference ion in the UMR m/z 73, a fragment normally attributed to levoglucosan, is noted. Therefore, the results imply that C2H4O2+ (m/z 60.021) plus C3H5O2+ (m/z 73.029) are more sufficient to estimate the contribution of levoglucosan. The results did not show significant variations of levoglucosan content in the organic particle with the overall average contribution fraction ranging from 0.74% for coastal sage to 1.93% for chamise.

  17. Chemical characterization of particle emissions from controlled burns of biomass fuels using a high resolution time-of-flight aerosol mass spectrometer

    Directory of Open Access Journals (Sweden)

    L. Qi

    2012-03-01

    Full Text Available A total of forty-nine burns were conducted at the Missoula Fire Sciences Lab consisting of nine fuel types; i.e., chamise scrub oak, ceanothus, maritime chaparral, coastal sage scrub, California sage brush, Manzanita, oak savanna, oak woodland and masticated mesquite. This paper focuses on the chemical characterization of fine particle emissions collected for flaming, mixed and smoldering phases using a HR ToF-AMS. The evolution of OM/OC, H/C, O/C and N/C from fire ignition to extinction was measured to capture the transient and integrated chemical composition of the non-refractory portion of bulk particles. Real time elemental ratios and empirical formulas derived with respect to modified combustion efficiency (MCE are reported. For each fuel, the hydrogen fragment ions dominate the unit mass resolution (UMR mass spectra with no specific fragment ions attributable to an individual ecological combination. An interference ion in the UMR m/z 73, a fragment normally attributed to levoglucosan, is noted. Therefore, the results imply that C2H4O2+ (m/z 60.021 plus C3H5O2+ (m/z 73.029 are more sufficient to estimate the contribution of levoglucosan. The results did not show significant variations of levoglucosan content in the organic particle with the overall average contribution fraction ranging from 0.74% for coastal sage to 1.93% for chamise.

  18. SPHERES, J\\"ulich's High-Flux Neutron Backscattering Spectrometer at FRM II

    CERN Document Server

    Wuttke, Joachim; Drochner, Matthias; Kämmerling, Hans; Kayser, Franz-Joseph; Pardo, Luis Carlos; Prager, Michael; Ossovyi, Vladimir; Schneider, Gerald J; Schneider, Harald; Staringer, Simon; Richter, Dieter

    2012-01-01

    SPHERES (SPectrometer with High Energy RESolution) is a third-generation neutron backscattering spectrometer, located at the 20 MW German neutron source FRM II and operated by the J\\"ulich Centre for Neutron Science. It offers an energy resolution (fwhm) better than 0.65 micro-eV, a dynamic range of +-31 micro-eV, and a signal-to-noise ratio of up to 1750:1.

  19. Design of thin-film filters for resolution improvements in filter-array based spectrometers using DSP

    Science.gov (United States)

    Lee, Woong-Bi; Kim, Cheolsun; Ju, Gun Wu; Lee, Yong Tak; Lee, Heung-No

    2016-05-01

    Miniature spectrometers have been widely developed in various academic and industrial applications such as bio-medical, chemical and environmental engineering. As a family of spectrometers, optical filter-array based spectrometers fabricated using CMOS or Nano technology provide miniaturization, superior portability and cost effectiveness. In filterarray based spectrometers, the resolution which represents the ability how closely resolve two neighboring spectra, depends on the number of filters and the characteristics of the transmission functions (TFs) of the filters. In practice, due to the small-size and low-cost fabrication, the number of filters is limited and the shape of the TF of each filter is nonideal. As a development of modern digital signal processing (DSP), the spectrometers are equipped with DSP algorithms not only to alleviate distortions due to unexpected noise or interferences among filters but also reconstruct the original signal spectrum. For a high-resolution spectrum reconstruction by the DSP, the TFs of the filters need to be sufficiently uncorrelated with each other. In this paper, we present a design of optical thin-film filters which have the uncorrelated TFs. Each filter consists of multiple layers of high- and low-refractive index materials deposited on a substrate. The proposed design helps the DSP algorithm to improve resolution with a small number of filters. We demonstrate that a resolution of 5 nm within a range from 500 nm to 1100 nm can be achieved with only 64 filters.

  20. High resolution study of U235(nsub(th),f) and Th229(nsub(th), f) with Cosi Fan Tutte mass spectrometer

    Energy Technology Data Exchange (ETDEWEB)

    Sicre, A.; Barreau, G.; Boukellal, A.

    1986-01-01

    The new built Cosi Fan Tutte facility installed at the High Flux Reactor of the ILL in Grenoble was used to obtain correlated mass, kinetic energy and nuclear charge of the fission fragments from U235(nsub(th),f) and Th229(nsub(th),f).

  1. Surpassing the Path-Limited Resolution of a Fourier Transform Spectrometer with Frequency Combs

    CERN Document Server

    Maslowski, Piotr; Johansson, Alexandra C; Khodabakhsh, Amir; Kowzan, Grzegorz; Rutkowski, Lucile; Mills, Andrew A; Mohr, Christian; Jiang, Jie; Fermann, Martin E; Foltynowicz, Aleksandra

    2015-01-01

    Fourier transform spectroscopy based on incoherent light sources is a well-established tool in research fields from molecular spectroscopy and atmospheric monitoring to material science and biophysics. It provides broadband molecular spectra and information about the molecular structure and composition of absorptive media. However, the spectral resolution is fundamentally limited by the maximum delay range ({\\Delta}$_{max}$) of the interferometer, so acquisition of high-resolution spectra implies long measurement times and large instrument size. We overcome this limit by combining the Fourier transform spectrometer with an optical frequency comb and measuring the intensities of individual comb lines by precisely matching the {\\Delta}$_{max}$ to the comb line spacing. This allows measurements of absorption lines narrower than the nominal (optical path-limited) resolution without ringing effects from the instrumental lineshape and reduces the acquisition time and interferometer length by orders of magnitude.

  2. The ALICE Dimuon Spectrometer High Level Trigger

    CERN Document Server

    Becker, B; Cicalo, Corrado; Das, Indranil; de Vaux, Gareth; Fearick, Roger; Lindenstruth, Volker; Marras, Davide; Sanyal, Abhijit; Siddhanta, Sabyasachi; Staley, Florent; Steinbeck, Timm; Szostak, Artur; Usai, Gianluca; Vilakazi, Zeblon

    2009-01-01

    The ALICE Dimuon Spectrometer High Level Trigger (dHLT) is an on-line processing stage whose primary function is to select interesting events that contain distinct physics signals from heavy resonance decays such as J/psi and Gamma particles, amidst unwanted background events. It forms part of the High Level Trigger of the ALICE experiment, whose goal is to reduce the large data rate of about 25 GB/s from the ALICE detectors by an order of magnitude, without loosing interesting physics events. The dHLT has been implemented as a software trigger within a high performance and fault tolerant data transportation framework, which is run on a large cluster of commodity compute nodes. To reach the required processing speeds, the system is built as a concurrent system with a hierarchy of processing steps. The main algorithms perform partial event reconstruction, starting with hit reconstruction on the level of the raw data received from the spectrometer. Then a tracking algorithm finds track candidates from the recon...

  3. High Resolution Elevation Contours

    Data.gov (United States)

    Minnesota Department of Natural Resources — This dataset contains contours generated from high resolution data sources such as LiDAR. Generally speaking this data is 2 foot or less contour interval.

  4. The High-Acceptance Dielectron Spectrometer HADES

    CERN Document Server

    Agakichiev, G; Bannier, B; Bassini, R; Belver, D; Belyaev, A V; Blanco, A; Boehmer, M; Boyard, J L; Braun-Munzinger, P; Cabanelas, P; Castro, E; Chernenko, S; Christ, T; Destefanis, M; Díaz, J; Dohrmann, F; Dybczak, A; Eberl, T; Enghardt, W; Fabbietti, L; Fateev, O V; Finocchiaro, P; Fonte, Paulo J R; Friese, J; Fröhlich, I; Galatyuk, T; Garzón, J A; Gernhäuser, R; Gil1, A; Gilardi, C; Golubeva, M; Gonzalez-Diaz, D; Guber, F; Heilmann, M; Heinz, T; Hennino, T; Holzmann, R; Ierusalimov, A; Iori, I; Ivashkin, A; Jurkovic, M; Kämpfer, B; Kanaki, K; Karavicheva, T; Kirschner, D; König, I; König, W; Kolb, B W; Kotte, R; Krizek, F; Krücken, R; Kühn, W; Kugler, A; Kurepin, A; Lang, S; Lange, J S; Lapidus, K; Liu, T; Lopes, L; Lorenz, M; Maier, L; Mangiarotti, A; Markert, J; Metag, V; Michalska, B; Michel, J; Mishra, D; Moriniere, E; Mousa, J; Müntz, C; Naumann, Lutz; Otwinowski, J; Pachmayer, Y C; Palka, M; Parpottas, Y; Pechenov, V; Pechenova, O; PerezCavalcanti, T; Pietraszko, J; Przygoda, W; Ramstein, B; Reshetin, A; Roy-Stephan, M; Rustamov, A; Sadovskii, A; Sailer, B; Salabura, P; Schmah, A; Schwab, E; Sobolev, Yu G; Spataro, S; Spruck, B; Ströbele, H; Stroth, J; Sturm, C; Sudol, M; Tarantola, A; Teilab, K; Tlustý, P; Traxler, M; Trebac, R; Tsertos, H; Wagner, V; Weber, M; Wisniowski, M; Wojcik, T; Wuestenfel, J; Yurevich, S; Zanevsky, Yu V; Zhou, P; Zumbruch, P

    2009-01-01

    HADES is a versatile magnetic spectrometer aimed at studying dielectron production in pion, proton and heavy-ion induced collisions. Its main features include a ring imaging gas Cherenkov detector for electron-hadron discrimination, a tracking system consisting of a set of 6 superconducting coils producing a toroidal field and drift chambers and a multiplicity and electron trigger array for additional electron-hadron discrimination and event characterization. A two-stage trigger system enhances events containing electrons. The physics program is focused on the investigation of hadron properties in nuclei and in the hot and dense hadronic matter. The detector system is characterized by an 85% azimuthal coverage over a polar angle interval from 18 to 85 degree, a single electron efficiency of 50% and a vector meson mass resolution of 2.5%. Identification of pions, kaons and protons is achieved combining time-of-flight and energy loss measurements over a large momentum range. This paper describes the main featur...

  5. The high-acceptance dielectron spectrometer HADES

    Energy Technology Data Exchange (ETDEWEB)

    Agakichiev, G.; Destefanis, M.; Gilardi, C.; Kirschner, D.; Kuehn, W.; Lange, J.S.; Lehnert, J.; Lichtblau, C.; Lins, E.; Metag, V.; Mishra, D.; Novotny, R.; Pechenov, V.; Pechenova, O.; Perez Cavalcanti, T.; Petri, M.; Ritman, J.; Salz, C.; Schaefer, D.; Skoda, M.; Spataro, S.; Spruck, B.; Toia, A. [Justus-Liebig-Univ. Giessen, II. Physikalisches Inst., Giessen (Germany); Agodi, C.; Coniglione, R.; Cosentino, L.; Finocchiaro, P.; Maiolino, C.; Piattelli, P.; Sapienza, P.; Vassiliev, D. [Lab. Nazionali del Sud, Istituto Nazionale di Fisica Nucleare, Catania (Italy); Alvarez-Pol, H.; Belver, D.; Cabanelas, P.; Castro, E.; Duran, I.; Fernandez, C.; Fuentes, B.; Garzon, J.A.; Kurtukian-Nieto, T.; Rodriguez-Prieto, G.; Sabin-Fernandez, J.; Sanchez, M.; Vazquez, A. [Univ. de Santiago de Compostela, Dept. de Fisica de Particulas, Santiago de Compostela (Spain); Atkin, E.; Volkov, Y. [State Univ., Moscow Engineering Physics Inst., Moscow (Russian Federation); Badura, E.; Bertini, D.; Bielcik, J.; Bokemeyer, H.; Dahlinger, M.; Daues, H.W.; Galatyuk, T.; Garabatos, C.; Gonzalez-Diaz, D.; Hehner, J.; Heinz, T.; Hoffmann, J.; Holzmann, R.; Koenig, I.; Koenig, W.; Kolb, B.W.; Kopf, U.; Lang, S.; Leinberger, U.; Magestro, D.; Muench, M.; Niebur, W.; Ott, W.; Pietraszko, J.; Rustamov, A.; Schicker, R.M.; Schoen, H.; Schoen, W.; Schroeder, C.; Schwab, E.; Senger, P.; Simon, R.S.; Stelzer, H.; Traxler, M.; Yurevich, S.; Zovinec, D.; Zumbruch, P. [GSI Helmholtzzentrum fuer Schwerionenforschung, Darmstadt (Germany); Balanda, A.; Kozuch, A.; Przygoda, W. [Jagiellonian Univ. of Krakow, Smoluchowski Inst. of Physics, Krakow (Poland); Pantwowa Wyzsza Szkola Zawodowa, Nowy Sacz (Poland); Bassi, A.; Bassini, R.; Boiano, C.; Bartolotti, A.; Brambilla, S. [Sezione di Milano, Istituto Nazionale di Fisica Nucleare, Milano (Italy); Bellia, G.; Migneco, E. [Lab. Nazionali del Sud, Istituto Nazionale di Fisica Nucleare, Catania (Italy); Univ. di Catania (Italy)] (and others)

    2009-08-15

    HADES is a versatile magnetic spectrometer aimed at studying dielectron production in pion, proton and heavy-ion-induced collisions. Its main features include a ring imaging gas Cherenkov detector for electron-hadron discrimination, a tracking system consisting of a set of 6 superconducting coils producing a toroidal field and drift chambers and a multiplicity and electron trigger array for additional electron-hadron discrimination and event characterization. A two-stage trigger system enhances events containing electrons. The physics program is focused on the investigation of hadron properties in nuclei and in the hot and dense hadronic matter. The detector system is characterized by an 85% azimuthal coverage over a polar angle interval from 18 to 85 , a single electron efficiency of 50% and a vector meson mass resolution of 2.5%. Identification of pions, kaons and protons is achieved combining time-of-flight and energy loss measurements over a large momentum range (0.1< p< 1.0 GeV/c). This paper describes the main features and the performance of the detector system. (orig.)

  6. The high-acceptance dielectron spectrometer HADES

    Science.gov (United States)

    Agakichiev, G.; Agodi, C.; Alvarez-Pol, H.; Atkin, E.; Badura, E.; Balanda, A.; Bassi, A.; Bassini, R.; Bellia, G.; Belver, D.; Belyaev, A. V.; Benovic, M.; Bertini, D.; Bielcik, J.; Böhmer, M.; Boiano, C.; Bokemeyer, H.; Bartolotti, A.; Boyard, J. L.; Brambilla, S.; Braun-Munzinger, P.; Cabanelas, P.; Castro, E.; Chepurnov, V.; Chernenko, S.; Christ, T.; Coniglione, R.; Cosentino, L.; Dahlinger, M.; Daues, H. W.; Destefanis, M.; Díaz, J.; Dohrmann, F.; Dressler, R.; Durán, I.; Dybczak, A.; Eberl, T.; Enghardt, W.; Fabbietti, L.; Fateev, O. V.; Fernández, C.; Finocchiaro, P.; Friese, J.; Fröhlich, I.; Fuentes, B.; Galatyuk, T.; Garabatos, C.; Garzón, J. A.; Genolini, B.; Gernhäuser, R.; Gilardi, C.; Gilg, H.; Golubeva, M.; González-Díaz, D.; Grosse, E.; Guber, F.; Hehner, J.; Heidel, K.; Heinz, T.; Hennino, T.; Hlavac, S.; Hoffmann, J.; Holzmann, R.; Homolka, J.; Hutsch, J.; Ierusalimov, A. P.; Iori, I.; Ivashkin, A.; Jaskula, M.; Jourdain, J. C.; Jurkovic, M.; Kämpfer, B.; Kajetanowicz, M.; Kanaki, K.; Karavicheva, T.; Kastenmüller, A.; Kidon, L.; Kienle, P.; Kirschner, D.; Koenig, I.; Koenig, W.; Körner, H. J.; Kolb, B. W.; Kopf, U.; Korcyl, K.; Kotte, R.; Kozuch, A.; Krizek, F.; Krücken, R.; Kühn, W.; Kugler, A.; Kulessa, R.; Kurepin, A.; Kurtukian-Nieto, T.; Lang, S.; Lange, J. S.; Lapidus, K.; Lehnert, J.; Leinberger, U.; Lichtblau, C.; Lins, E.; Lippmann, C.; Lorenz, M.; Magestro, D.; Maier, L.; Maier-Komor, P.; Maiolino, C.; Malarz, A.; Marek, T.; Markert, J.; Metag, V.; Michalska, B.; Michel, J.; Migneco, E.; Mishra, D.; Morinière, E.; Mousa, J.; Münch, M.; Müntz, C.; Naumann, L.; Nekhaev, A.; Niebur, W.; Novotny, J.; Novotny, R.; Ott, W.; Otwinowski, J.; Pachmayer, Y. C.; Palka, M.; Parpottas, Y.; Pechenov, V.; Pechenova, O.; Pérez Cavalcanti, T.; Petri, M.; Piattelli, P.; Pietraszko, J.; Pleskac, R.; Ploskon, M.; Pospísil, V.; Pouthas, J.; Prokopowicz, W.; Przygoda, W.; Ramstein, B.; Reshetin, A.; Ritman, J.; Roche, G.; Rodriguez-Prieto, G.; Rosenkranz, K.; Rosier, P.; Roy-Stephan, M.; Rustamov, A.; Sabin-Fernandez, J.; Sadovsky, A.; Sailer, B.; Salabura, P.; Salz, C.; Sánchez, M.; Sapienza, P.; Schäfer, D.; Schicker, R. M.; Schmah, A.; Schön, H.; Schön, W.; Schroeder, C.; Schroeder, S.; Schwab, E.; Senger, P.; Shileev, K.; Simon, R. S.; Skoda, M.; Smolyankin, V.; Smykov, L.; Sobiella, M.; Sobolev, Yu. G.; Spataro, S.; Spruck, B.; Stelzer, H.; Ströbele, H.; Stroth, J.; Sturm, C.; Sudoł, M.; Suk, M.; Szczybura, M.; Taranenko, A.; Tarantola, A.; Teilab, K.; Tiflov, V.; Tikhonov, A.; Tlusty, P.; Toia, A.; Traxler, M.; Trebacz, R.; Troyan, A. Yu.; Tsertos, H.; Turzo, I.; Ulrich, A.; Vassiliev, D.; Vázquez, A.; Volkov, Y.; Wagner, V.; Wallner, C.; Walus, W.; Wang, Y.; Weber, M.; Wieser, J.; Winkler, S.; Wisniowski, M.; Wojcik, T.; Wüstenfeld, J.; Yurevich, S.; Zanevsky, Y. V.; Zeitelhack, K.; Zentek, A.; Zhou, P.; Zovinec, D.; Zumbruch, P.

    2009-08-01

    HADES is a versatile magnetic spectrometer aimed at studying dielectron production in pion, proton and heavy-ion-induced collisions. Its main features include a ring imaging gas Cherenkov detector for electron-hadron discrimination, a tracking system consisting of a set of 6 superconducting coils producing a toroidal field and drift chambers and a multiplicity and electron trigger array for additional electron-hadron discrimination and event characterization. A two-stage trigger system enhances events containing electrons. The physics program is focused on the investigation of hadron properties in nuclei and in the hot and dense hadronic matter. The detector system is characterized by an 85% azimuthal coverage over a polar angle interval from 18° to 85° , a single electron efficiency of 50% and a vector meson mass resolution of 2.5%. Identification of pions, kaons and protons is achieved combining time-of-flight and energy loss measurements over a large momentum range ( 0.1 < p < 1.0 GeV/ c . This paper describes the main features and the performance of the detector system.

  7. Development of a new corona discharge based ion source for high resolution time-of-flight chemical ionization mass spectrometer to measure gaseous H2SO4 and aerosol sulfate

    Science.gov (United States)

    Zheng, Jun; Yang, Dongsen; Ma, Yan; Chen, Mindong; Cheng, Jin; Li, Shizheng; Wang, Ming

    2015-10-01

    A new corona discharge (CD) based ion source was developed for a commercial high-resolution time-of-flight chemical ionization mass spectrometer (HRToF-CIMS) (Aerodyne Research Inc.) to measure both gaseous sulfuric acid (H2SO4) and aerosol sulfate after thermal desorption. Nitrate core ions (NO3-) were used as reagent ions and were generated by a negative discharge in zero air followed by addition of excess nitrogen dioxide (NO2) to convert primary ions and hydroxyl radicals (OH) into NO3- ions and nitric acid (HNO3). The CD-HRToF-CIMS showed no detectable interference from hundreds parts per billion by volume (ppbv) of sulfur dioxide (SO2). Unlike the atmospheric pressure ionization (API) ToF-CIMS, the CD ion source was integrated onto the ion-molecule reaction (IMR) chamber and which made it possible to measure aerosol sulfate by coupling to a filter inlet for gases and aerosols (FIGAERO). Moreover, compared with a quadrupole-based mass spectrometer, the desired HSO4- signal was detected by its exact mass of m/z 96.960, which was well resolved from the potential interferences of HCO3-ṡ(H2O)2 (m/z 97.014) and O-ṡH2OṡHNO3 (m/z 97.002). In this work, using laboratory-generated standards the CD-HRToF-CIMS was demonstrated to be able to detect as low as 3.1 × 105 molecules cm-3 gaseous H2SO4 and 0.5 μg m-3 ammonium sulfate based on 10-s integration time and two times of the baseline noise. The CD ion source had the advantages of low cost and a simple but robust structure. Since the system was non-radioactive and did not require corrosive HNO3 gas, it can be readily field deployed. The CD-HRToF-CIMS can be a powerful tool for both field and laboratory studies of aerosol formation mechanism and the chemical processes that were critical to understand the evolution of aerosols in the atmosphere.

  8. The PNL high-transmission three-stage mass spectrometer

    Science.gov (United States)

    Stoffels, J. J.; Ells, D. R.; Bond, L. A.; Freedman, P. A.; Tattersall, B. N.; Lagergren, C. R.

    1992-12-01

    We have constructed a three-stage isotope-ratio mass spectrometer of unique ion-optical design that achieves high ion transmission efficiency and high abundance sensitivity. The spectrometer has tandem 90 deg deflection magnets with boundaries 18 deg off normal. The magnet drift lengths are 1.48 times the 27-cm radius of deflection. This extended geometry gives a mass dispersion equivalent to a 40-cm-radius magnet with normal boundaries. The first magnet renders the ion beam parallel in the vertical plane and provides a focus in the horizontal plane of mass dispersion. The second magnet brings the beam to a stigmatic focus. This novel ion-optical design gives 100 percent transmission without the need for intermediate focusing lenses. It also provides a 16 percent increase in mass resolution over the traditional tandem geometry with normal magnet boundaries. Complete transmission of ions is maintained through a third-stage cylindrical electric sector of 38-cm radius, which provides increased isotope-abundance sensitivity. The isotope-abundance sensitivity of the new mass spectrometer is an order of magnitude better than similar instruments with normal magnet boundaries. This is because the vertical focusing of the ion beam prevents ion scattering from the top and bottom of the flight tube. The measured values of the isotope-abundance sensitivity one-half mass unit away from the rhenium ion peaks at masses 185 and 187 are M - 1/2 = (6.5 +/- 0.5)(10)(exp -10) and M + 1/2 = (3.1 +/- 0.8)(10)(exp -10). By extrapolation, the uranium isotope-abundance sensitivity is M - 1 = 1(10)(exp -10). Construction of the instrument was facilitated by using standard commercial mass spectrometer components.

  9. Ultra high resolution tomography

    Energy Technology Data Exchange (ETDEWEB)

    Haddad, W.S.

    1994-11-15

    Recent work and results on ultra high resolution three dimensional imaging with soft x-rays will be presented. This work is aimed at determining microscopic three dimensional structure of biological and material specimens. Three dimensional reconstructed images of a microscopic test object will be presented; the reconstruction has a resolution on the order of 1000 A in all three dimensions. Preliminary work with biological samples will also be shown, and the experimental and numerical methods used will be discussed.

  10. A high-resolution time-of-flight chemical ionization mass spectrometer utilizing hydronium ions (H3O+ ToF-CIMS) for measurements of volatile organic compounds in the atmosphere

    Science.gov (United States)

    Yuan, Bin; Koss, Abigail; Warneke, Carsten; Gilman, Jessica B.; Lerner, Brian M.; Stark, Harald; de Gouw, Joost A.

    2016-07-01

    Proton transfer reactions between hydronium ions (H3O+) and volatile organic compounds (VOCs) provide a fast and highly sensitive technique for VOC measurements, leading to extensive use of proton-transfer-reaction mass spectrometry (PTR-MS) in atmospheric research. Based on the same ionization approach, we describe the development of a high-resolution time-of-flight chemical ionization mass spectrometer (ToF-CIMS) utilizing H3O+ as the reagent ion. The new H3O+ ToF-CIMS has sensitivities of 100-1000 cps ppb-1 (ion counts per second per part-per-billion mixing ratio of VOC) and detection limits of 20-600 ppt at 3σ for a 1 s integration time for simultaneous measurements of many VOC species of atmospheric relevance. The ToF analyzer with mass resolution (m/Δm) of up to 6000 allows the separation of isobaric masses, as shown in previous studies using similar ToF-MS. While radio frequency (RF)-only quadrupole ion guides provide better overall ion transmission than ion lens system, low-mass cutoff of RF-only quadrupole causes H3O+ ions to be transmitted less efficiently than heavier masses, which leads to unusual humidity dependence of reagent ions and difficulty obtaining a humidity-independent parameter for normalization. The humidity dependence of the instrument was characterized for various VOC species and the behaviors for different species can be explained by compound-specific properties that affect the ion chemistry (e.g., proton affinity and dipole moment). The new H3O+ ToF-CIMS was successfully deployed on the NOAA WP-3D research aircraft for the SONGNEX campaign in spring of 2015. The measured mixing ratios of several aromatics from the H3O+ ToF-CIMS agreed within ±10 % with independent gas chromatography measurements from whole air samples. Initial results from the SONGNEX measurements demonstrate that the H3O+ ToF-CIMS data set will be valuable for the identification and characterization of emissions from various sources, investigation of secondary

  11. High sensitivity field asymmetric ion mobility spectrometer

    Science.gov (United States)

    Chavarria, Mario A.; Matheoud, Alessandro V.; Marmillod, Philippe; Liu, Youjiang; Kong, Deyi; Brugger, Jürgen; Boero, Giovanni

    2017-03-01

    A high sensitivity field asymmetric ion mobility spectrometer (FAIMS) was designed, fabricated, and tested. The main components of the system are a 10.6 eV UV photoionization source, an ion filter driven by a high voltage/high frequency n-MOS inverter circuit, and a low noise ion detector. The ion filter electronics are capable to generate square waveforms with peak-to-peak voltages up to 1000 V at frequencies up to 1 MHz with adjustable duty cycles. The ion detector current amplifier has a gain up to 1012 V/A with an effective equivalent input noise level down to about 1 fA/Hz1/2 during operation with the ion filter at the maximum voltage and frequency. The FAIMS system was characterized by detecting different standard chemical compounds. Additionally, we investigated the use of a synchronous modulation/demodulation technique to improve the signal-to-noise ratio in FAIMS measurements. In particular, we implemented the modulation of the compensation voltage with the synchronous demodulation of the ion current. The analysis of the measurements at low concentration levels led to an extrapolated limit of detection for acetone of 10 ppt with an averaging time of 1 s.

  12. The resolution of the tof-backscattering spectrometer OSIRIS: Monte Carlo simulations and analytical calculations

    Science.gov (United States)

    Demmel, F.; Pokhilchuk, K.

    2014-12-01

    The energy resolution of an indirect time of flight (tof) spectrometer is determined mainly by the pulse shape of the incoming pulse and the contribution of the crystal analyser. We performed extensive Monte Carlo simulations for the indirect near-backscattering spectrometer OSIRIS utilising the McStas neutron ray-traycing package. The simulations are accompanied by analytical calculations for the energy resolution. From simulation and calculation an excellent description for the width of the line is achieved for the PG002 and PG004 energy setting. The simulations and calculations reveal that the secondary spectrometer and hence the analyser geometry is the dominating term for the energy resolution at zero energy transfer. The remaining differences in the lineshape can be traced to a not perfectly modeled hydrogen moderator. The simulations and calculations predict a superb energy resolution of less than 100 μeV at an energy transfer of 15 meV.

  13. The resolution of the tof-backscattering spectrometer OSIRIS: Monte Carlo simulations and analytical calculations

    Energy Technology Data Exchange (ETDEWEB)

    Demmel, F., E-mail: franz.demmel@stfc.ac.uk [ISIS Facility, Didcot, OX11 0QX (United Kingdom); Pokhilchuk, K. [ISIS Facility, Didcot, OX11 0QX (United Kingdom); Loughborough University, Loughborough (United Kingdom)

    2014-12-11

    The energy resolution of an indirect time of flight (tof) spectrometer is determined mainly by the pulse shape of the incoming pulse and the contribution of the crystal analyser. We performed extensive Monte Carlo simulations for the indirect near-backscattering spectrometer OSIRIS utilising the McStas neutron ray-traycing package. The simulations are accompanied by analytical calculations for the energy resolution. From simulation and calculation an excellent description for the width of the line is achieved for the PG002 and PG004 energy setting. The simulations and calculations reveal that the secondary spectrometer and hence the analyser geometry is the dominating term for the energy resolution at zero energy transfer. The remaining differences in the lineshape can be traced to a not perfectly modeled hydrogen moderator. The simulations and calculations predict a superb energy resolution of less than 100 μeV at an energy transfer of 15 meV.

  14. A Compact High-Energy Neutron Spectrometer

    CERN Document Server

    Brooks, F D; Buffler, A; Dangendorf, V; Herbert, M S; Jones, D T L; Nchodu, M R; Nolte, R; Smit, F D

    2007-01-01

    A compact liquid organic neutron spectrometer (CLONS) based on a single NE213 liquid scintillator (5 cm diam. x 5 cm) is described. The spectrometer is designed to measure neutron fluence spectra over the energy range 2-200 MeV and is suitable for use in neutron fields having any type of time structure. Neutron fluence spectra are obtained from measurements of two-parameter distributions (counts versus pulse height and pulse shape) using the Bayesian unfolding code MAXED. Calibration and test measurements made using a pulsed neutron beam with a continuous energy spectrum are described and the application of the spectrometer to radiation dose measurements is discussed.

  15. Micro-Spec: A High Performance Compact Spectrometer for Submillimeter Astronomy

    Science.gov (United States)

    Hsieh, Wen-Ting; Moseley, Harvey; Stevenson, Thomas; Brown, Ari; Patel, Amil; U-Yen, Kongpop; Ehsan, Negar; Caltado, Giuseppe; Wollock, Edward

    2012-01-01

    We describe the micro-Spec, an extremely compact high performance spectrometer for the submillimeter and millimeter spectral ranges. We have designed a fully integrated submillimeter spectrometer based on superconducting microstrip technology and fabricated its critical elements. Using low loss transmission lines, we can produce a fully integrated high resolution submillimeter spectrometer on a single four inch Si wafer. A resolution of 500 can readily be achieved with standard fabrication tolerance, higher with phase trimming. All functions of the spectrometer are integrated - light is coupled to the micro strip circuit with a planar antenna, the spectra discrimination is achieved using a synthetic grating, orders are separated using a built-in planar filter, and the light is detected using photon counting Microwave Kinetic Inductance Detectors (MKID). We will discus the design principle of the instrument, describe its technical advantages, and report the progress on the development of the instrument.

  16. Mu-Spec: A High Performance Compact Spectrometer for Submillimeter Astronomy

    Science.gov (United States)

    Hsieh, Wen-Ting; Moseley, Harvey; Stevenson, Thomas; Brown, Ari; Patel, Amil; U-yen, Kongpop; Ehsan, Negar; Cataldo, Giuseppe; Wollack, Ed

    2012-01-01

    We describe the Mu-Spec, an extremely compact high performance spectrometer for the submillimeter and millimeter spectral ranges. We have designed a fully integrated submillimeter spectrometer based on superconducting microstrip technology and fabricated its critical elements. Using low loss transmission lines, we can produce a fully integrated high resolution submillimeter spectrometer on a single four inch Si wafer. A resolution of 500 can readily be achieved with standard fabrication tolerance, higher with phase trimming. All functions of the spectrometer are integrated - light is coupled to the microstrip circuit with a planar antenna, the spectra discrimination is achieved using a synthetic grating, orders are separated using a built-in planar filter, and the light is detected using photon counting Microwave Kinetic Inductance Detectors (MKID). We will discus the design principle of the instrument, describe its technical advantages, and report the progress on the development of the instrument.

  17. High-resolution headlamp

    Science.gov (United States)

    Gut, Carsten; Cristea, Iulia; Neumann, Cornelius

    2016-04-01

    The following article shall describe how human vision by night can be influenced. At first, front lighting systems that are already available on the market will be described, followed by their analysis with respect to the positive effects on traffic safety. Furthermore, how traffic safety by night can be increased since the introduction of high resolution headlamps shall be discussed.

  18. High Resolution Acoustical Imaging

    Science.gov (United States)

    1989-05-01

    1028 (September 1982). 26 G. Arfken , Mathematical Methods for Physicists (Academic Press, New York, 1971), 2nd printing, pp.662-666. 27 W. R. Hahn...difference in the approach used by the two methods , as noted in the previous paragraph, forming a direct mathematical com- parison may be impossible...examines high resolution methods which use a linear array to locate stationary objects which have scattered the fressure waves. Several;- new methods

  19. High resolution differential thermometer

    Directory of Open Access Journals (Sweden)

    Gotra Z. Yu.

    2009-11-01

    Full Text Available Main schematic solutions of differential thermometers with measurement resolution about 0.001°C are considered. Differential temperature primary transducer realized on a transistor differential circuit in microampere mode. Analytic calculation and schematic mathematic simulation of primary transducer are fulfilled. Signal transducer is realized on a high precision Zero-Drift Single-Supply Rail-to-Rail operation amplifier AD8552 and 24-Bit S-D microconverter ADuC834.

  20. High Spectral Resolution, High Cadence, Imaging X-ray Microcalorimeters for Solar Physics - Phase 2 Project

    Data.gov (United States)

    National Aeronautics and Space Administration — Microcalorimeter x-ray instruments are non-dispersive, high spectral resolution, broad-band, high cadence imaging spectrometers. We have been developing these...

  1. Saturn's rings - high resolution

    Science.gov (United States)

    1981-01-01

    Voyager 2 obtained this high-resolution picture of Saturn's rings Aug. 22, when the spacecraft was 4 million kilometers (2.5 million miles) away. Evident here are the numerous 'spoke' features, in the B-ring; their very sharp, narrow appearance suggests short formation times. Scientists think electromagnetic forces are responsible in some way for these features, but no detailed theory has been worked out. Pictures such as this and analyses of Voyager 2's spoke movies may reveal more clues about the origins of these complex structures. The Voyager project is managed for NASA by the Jet Propulsion Laboratory, Pasadena, Calif.

  2. High Resolution Laboratory Spectroscopy

    CERN Document Server

    Brünken, Sandra

    2016-01-01

    In this short review we will highlight some of the recent advancements in the field of high-resolution laboratory spectroscopy that meet the needs dictated by the advent of highly sensitive and broadband telescopes like ALMA and SOFIA. Among these is the development of broadband techniques for the study of complex organic molecules, like fast scanning conventional absorption spectroscopy based on multiplier chains, chirped pulse instrumentation, or the use of synchrotron facilities. Of similar importance is the extension of the accessible frequency range to THz frequencies, where many light hydrides have their ground state rotational transitions. Another key experimental challenge is the production of sufficiently high number densities of refractory and transient species in the laboratory, where discharges have proven to be efficient sources that can also be coupled to molecular jets. For ionic molecular species sensitive action spectroscopic schemes have recently been developed to overcome some of the limita...

  3. The mid-infrared instrument for the James Webb Space telescope, VI: the medium resolution spectrometer

    NARCIS (Netherlands)

    Wells, M.; Pel, J.W.; Glasse, A.; Wright, G.S.; Aitink-Kroes, G.; Azzollini, R.; Beard, S.; Brandl, B.R.; Gallie, A.; Geers, V.C.; Glauser, A.M.; Hastings, P.; Henning, T.; Jager, R.; Justtanont, K.; Kruizinga, B.; Lahuis, F.; Lee, D.; Martinez-Delgado, I.; Martínez-Galarza, J.R.; Meijers, M.; Morrison, J.E.; Müller, F.; Nakos, T.; O’Sullivan, B.; Oudenhuysen, A.; Parr-Burman, P.; Pauwels, E.; Rohloff, R.R.; Schmalzl, E.; Sykes, J.; Thelen, M.P.; Dishoeck, E.F. van; Vandenbussche, B.; Venema, L.B.; Visser, H.; Waters, L.B.F.M.; Wright, D.

    2015-01-01

    We describe the design and performance of the Medium Resolution Spectrometer (MRS) for the JWST-MIRI instrument. The MRS incorporates four coaxial spectral channels in a compact opto-mechanical layout that generates spectral images over fields of view up to 7.7 × 7.7″ in extent and at spectral resol

  4. The Mid-Infrared Instrument for the James Webb Space Telescope, VI: The Medium Resolution Spectrometer

    NARCIS (Netherlands)

    Wells, M.; Pel, J.-W.; Glasse, A.; Wright, G.S.; Aitink-Kroes, G.; Azzollini, R.; Beard, S.; Brandl, B.R.; Gallie, A.; Geers, V.C.; Glauser, A.M.; Hastings, P.; Henning, Th.; Jager, R.; Justtanont, K.; Kruizinga, B.; Lahuis, F.; Lee, D.; Martinez-Delgado, I.; Martínez-Galarza, J.R.; Meijers, M.; Morrison, J.E.; Müller, F.; Nakos, T.; O'Sullivan, B.; Oudenhuysen, A.; Parr-Burman, P.; Pauwels, E.; Rohloff, R.R.; Schmalzl, E.; Sykes, J.; Thelen, M.P.; van Dishoeck, E.F.; Vandenbussche, B.; Venema, L.B.; Visser, H.; Waters, L.B.F.M.; Wright, D.

    2015-01-01

    We describe the design and performance of the Medium Resolution Spectrometer (MRS) for the JWST-MIRI instrument. The MRS incorporates four coaxial spectral channels in a compact opto-mechanical layout that generates spectral images over fields of view up to 7.7 × 7.7'' in extent and at spectral reso

  5. High-resolution spectroscopy of gamma-ray transients

    Energy Technology Data Exchange (ETDEWEB)

    Cline, T.L.

    1988-09-25

    The first high-resolution spectrometer flown to observe gamma-ray bursts was launched on the ISEE-3 spacecraft over nine years ago. It recorded two events before instrument failure, giving results that were suggestive but marginal. Other studies, with coarser energy resolution, also show evidence for spectral features as well as for spectral evolution on short time scales. Absolute source strength calibration will be possible only with source identification, but understanding of the burst emission processes will surely come only from the measurements having the best spectral and temporal precision. The only high- resolution gamma-ray spectrometer now planned, here or abroad, for space flight is an instrument sequel to the ISEE-3 spectrometer, to be flown on the interplanetary 'GGS Wind' mission. Much larger and higher-sensitivity, high-resolution instruments may have their optimum opportunities in conjunction with studies of solar flares in the time frame of the solar maximum of 2002.

  6. High Time Resolution Astrophysics

    CERN Document Server

    Phelan, Don; Shearer, Andrew

    2008-01-01

    High Time Resolution Astrophysics (HTRA) is an important new window to the universe and a vital tool in understanding a range of phenomena from diverse objects and radiative processes. This importance is demonstrated in this volume with the description of a number of topics in astrophysics, including quantum optics, cataclysmic variables, pulsars, X-ray binaries and stellar pulsations to name a few. Underlining this science foundation, technological developments in both instrumentation and detectors are described. These instruments and detectors combined cover a wide range of timescales and can measure fluxes, spectra and polarisation. These advances make it possible for HTRA to make a big contribution to our understanding of the Universe in the next decade.

  7. Study of the ATLAS MDT Spectrometer using High Energy CERN combined Test beam Data

    CERN Document Server

    Adorisio, C; Alexopoulos, T; Alviggi, M G; Amelung, C; Anastopoulos, C; Avolio, G; Bachas, K; Bagnaia, P; Ball, R; Barisonzi, M; Baroncelli, A; Barone, M; Bauer, F; Bellomo, M; Benhammou, Ya; Bensinger, J; Beretta, M; Bianchi, R M; Bianco, M; Bini, C; Bobbink, G; Borisov, A; Boterenbrood, H; Boyko, I; Branchini, P; Brambilla, Elena; Brandenburg, G; Bratzler, U; Bressler, S; Brouwer, G; Cambiaghi, M; Canale, V; Caprio, M; Cardarelli, R; Cerutti, F; Chapman, J W; Chelkov, G; Chevalier, L; Chiodini, G; Cirilli, M; Coco, R; Curatolo, M; Esposito, B; Etzion, E; Dai, T; De Asmundis, R; Dedovich, D; Della Pietra, M; Della Volpe, D; DeZorzi, G; Di Ciaccio, A; DiDomenico, A; Di Luise, S; Di Simone, A; Dris, M; Dushkin, A; Ernwein, J; Fakhrutdinov, R; Falciano, S; Fassouliotis, D; Ferrari, R; Formica, A; Fukunaga, C; Gaudio, G; Gazis, E; Giraud, PF; Gorini, E; Grancagnolo, F; Gregory, J A; Groenstege, H; Guimarães da Costa, J; Guyot, C; Harel, A; Hart, R; Hashemi, K S; Hassani, S; Herten, G; Horvat, S; Hurst, P; Ichimiya, R; Iengo, P; Ikeno, M; Ioannou, P; Iodice, M; Ishino, M; Iwasaki, H; Kataoka, Y; Khodinov, A; König, A; Kortner, O; Kotov, S; Kourkoumelis, C; Kozhin, A; Krepouri, A; Kroha, H; Krumshtein, Z; Kurashige, H; Landgraf, U; Lacava, F; Lançon, E; Lanza, A; Laporte, JF; Lellouch, D; Levin, D S; Levinson, L; Liberti, B; Lifshitz, R; Linde, F; Luci, C; Lupu, N; Maccarrone, G; Maeno, T; Mair, K; Maltezos, S; Manz, A; Marchesotti, M; Meoni, E; Mikenberg, G; Mohr, W; Mohrdieck-Möck, S; Nagano, K; Nikolaidou, R; Nikolaev, K; Nikolopoulos, K; Nisati, A; Nomoto, H; Oliver, J; Orestano, D; Osborne, LS; Ouraou, A; Palestini, S; Pasqualucci, E; Passeri, A; Pastore, F; Patricelli, S; Perrino, R; Petridou, C; Petrucci, F; Podkladkin, S; Policicchio, Antonio; Pomarède, D; Ponsot, P; Pontecorvo, L; Primavera, M; Rebuzzi, D; Richter, R; Rimoldi, A; Rosati, S; Rothberg, J E; Sakamoto, H; Salvatore, D; Sampsonidis, D; Santonico, R; Sasaki, O; Schricker, A; Schuh, S; Schune, P; Shoa, M; Skvorodnev, N; Sliwa, K; Solfaroli, E; Spagnolo, S; Spogli, L; Strauss, E; Sugaya, Y; Tanaka, S; Tarem, S; Taylor, F E; Todorova, S; Trigger, I; Tsiafis, I; Tsipolitis, G; Valderanis, C; Valente, P; Vandelli, W; van der Graaf, H; Vari, R; Veneziano, S; Ventura, A; Ventura, Sandro; Vermeulen, J; Vlachos, S; Vreeswijk, M; Yasu, Y; Wellenstein, H; Werneke, P; Wijnen, T; Wolter, M; Wotschack, J; Woudstra, M; Zema, P F; Zhao, Z; Zhemchugov, A; Zhou, B; Zimmerman, S

    2009-01-01

    In 2004, a combined system test was performed in the H8 beam line at the CERN SPS with a setup using muon chambers made of Monitored Drift Tubes (MDT) to form a spectrometer which represented 1% of the ATLAS detector. The basic design performances of the muon spectrometer were veried. The full ATLAS analysis chain was used to obtain the results presented in this paper. The stability of MDT calibration constants, the alignment system using optical devices and high energy tracks, as well as the intrinsic sagitta resolution of the Muon Spectrometer were studied and found to agree with expectations. The reconstruction of muon tracks using the combined information from both the Inner Detector and the Muon Spectrometer are also presented.

  8. A Liquid-Cryogen-Free Cryostat for Ultrahigh Resolution Gamma-Ray Spectrometers

    Energy Technology Data Exchange (ETDEWEB)

    Dreyer, J G; Hertrich, T; Drury, O B; Hohne, J; Friedrich, S

    2008-06-30

    We are developing ultra-high energy resolution gamma-ray detectors based on superconducting transition edge sensors (TESs) for nuclear non-proliferation and fundamental science applications. They use bulk tin absorbers attached to molybdenum-copper multilayer TESs, and have achieved an energy resolution between 50 and 90 eV FWHM for gamma-ray energies below 122 keV. For increased user-friendliness, we have built a cryostat that attains the required detector operating temperature of 0.1 K at the push of a button without the use of cryogenic liquids. It uses a two-stage mechanical pulse tube refrigerator for precooling to {approx}3 K, and a two-stage adiabatic demagnetization refrigerator for cooling to the base temperature. The cryostat is fully automated, attains a base temperature below 30 mK without the use of cryogenic liquids, and has a hold time of {approx}2 days at 0.1 K between 1-hour demagnetization cycles. Here we discuss the performance of the cryostat for operation in a Gamma-spectrometer with 112-pixel arrays of superconducting TES detectors.

  9. A design study of VOR: A versatile optimal resolution chopper spectrometer for the ESS

    Directory of Open Access Journals (Sweden)

    Deen P.P.

    2015-01-01

    Full Text Available VOR, the versatile optimal resolution chopper spectrometer, is designed to probe dynamic phenomena that are currently inaccessible for inelastic neutron scattering due to flux limitations. VOR is a short instrument by the standards of the European Spallation Source (ESS, 30.2 m moderator to sample, and provides instantaneous access to a broad dynamic range, 1–120 meV within each ESS period. The short instrument length combined with the long ESS pulse width enables a quadratic flux increase, even at longer wavelengths, by relaxing energy resolution from ΔE/E = 1% up to ΔE/E = 7%. This is impossible both on a long chopper spectrometer at the ESS and with instruments at short pulsed sources. In comparison to current day chopper spectrometers, VOR can offer an order of magnitude improvement in flux for equivalent energy resolutions, ΔE/E = 1–3%. Further relaxing the energy resolution enables VOR to gain an extra order of magnitude in flux. In addition, VOR has been optimised for repetition rate multiplication (RRM and is therefore able to measure, in a single ESS period, 6–14 incident wavelengths, across a wavelength band of 9 Å with a novel chopper configuration that transmits all incident wavelengths with equivalent counting statistics. The characteristics of VOR make it a unique instrument with capabilities to access small, limited-lifetime samples and transient phenomena with inelastic neutron scattering.

  10. Quadrupole magnetic mapping of the high resolution spectrometers of Thomas Jefferson National Accelerator Laboratory, Hall A. (Q.M.M. project: Quadrupole Magnetic Measurement); Cartographie magnetique des quadripoles des spectrometre a haute resolution du Thomas Jefferson National Accelerator Laboratory, Hall A. (Le projet Q.M.M.: Quadrupole Magnetic Measurement)

    Energy Technology Data Exchange (ETDEWEB)

    Quemener, Gilles [Ecole Doctorale des Science Fondamentales, Universite Blaise Pascal, U.F.R. de Recherche Scientifique et Technique, F-63177 Aubiere Cedex (France)

    1997-12-19

    This thesis describes the magnetic measurements that have been performed on the superconducting quadrupoles of the High Resolution Spectrometers of TJNAF, Hall A (USA), which are designed to measure particle momentum up to 4 GeV.c{sup -1} with a {sigma}p/p = 10{sup -4} resolution. The mapping method is based on rotating coil technique, the originality being a segmentation of the probe along the quad axis. Together with an accurate magnet modelling, the measurement of the flux variations through the set of rotating coils allows to determine the magnetic field at each point. We use the 3D field formalism, i.e., the Fourier-Bessel expansion of the field obtained by solving the Laplace equation. We describe the QMM method and then the apparatus consisting in two probes of length 1.6 m and 3.2 m built to map the three quadrupoles Q1, Q2, Q3. Data processing uses Fourier analysis. The mapping of the Electron Arm took place in situ in 1996. A first set of results concerns integral measurements including the properties of excitation cycle of the magnets (saturation and hysteresis). Second set of results in terms of local field yields the 3D field maps of the quadrupoles. After having applied corrections to the data we obtain a local field accuracy of 5 Gauss on each component, i.e. an uncertainty of 5.10{sup -4} relative to the quadrupole central field. We use SNAKE ray-tracing code with the implementation of QMM field maps and obtain preliminary results on HRS optics. (author) 48 refs., 93 figs., 41 tabs.

  11. Monte Carlo simulation of the resolution volume for the SEQUOIA spectrometer

    Directory of Open Access Journals (Sweden)

    Granroth G.E.

    2015-01-01

    Full Text Available Monte Carlo ray tracing simulations, of direct geometry spectrometers, have been particularly useful in instrument design and characterization. However, these tools can also be useful for experiment planning and analysis. To this end, the McStas Monte Carlo ray tracing model of SEQUOIA, the fine resolution fermi chopper spectrometer at the Spallation Neutron Source (SNS of Oak Ridge National Laboratory (ORNL, has been modified to include the time of flight resolution sample and detector components. With these components, the resolution ellipsoid can be calculated for any detector pixel and energy bin of the instrument. The simulation is split in two pieces. First, the incident beamline up to the sample is simulated for 1 × 1011 neutron packets (4 days on 30 cores. This provides a virtual source for the backend that includes the resolution sample and monitor components. Next, a series of detector and energy pixels are computed in parallel. It takes on the order of 30 s to calculate a single resolution ellipsoid on a single core. Python scripts have been written to transform the ellipsoid into the space of an oriented single crystal, and to characterize the ellipsoid in various ways. Though this tool is under development as a planning tool, we have successfully used it to provide the resolution function for convolution with theoretical models. Specifically, theoretical calculations of the spin waves in YFeO3 were compared to measurements taken on SEQUOIA. Though the overall features of the spectra can be explained while neglecting resolution effects, the variation in intensity of the modes is well described once the resolution is included. As this was a single sharp mode, the simulated half intensity value of the resolution ellipsoid was used to provide the resolution width. A description of the simulation, its use, and paths forward for this technique will be discussed.

  12. Monte Carlo simulation of the resolution volume for the SEQUOIA spectrometer

    Science.gov (United States)

    Granroth, G. E.; Hahn, S. E.

    2015-01-01

    Monte Carlo ray tracing simulations, of direct geometry spectrometers, have been particularly useful in instrument design and characterization. However, these tools can also be useful for experiment planning and analysis. To this end, the McStas Monte Carlo ray tracing model of SEQUOIA, the fine resolution fermi chopper spectrometer at the Spallation Neutron Source (SNS) of Oak Ridge National Laboratory (ORNL), has been modified to include the time of flight resolution sample and detector components. With these components, the resolution ellipsoid can be calculated for any detector pixel and energy bin of the instrument. The simulation is split in two pieces. First, the incident beamline up to the sample is simulated for 1 × 1011 neutron packets (4 days on 30 cores). This provides a virtual source for the backend that includes the resolution sample and monitor components. Next, a series of detector and energy pixels are computed in parallel. It takes on the order of 30 s to calculate a single resolution ellipsoid on a single core. Python scripts have been written to transform the ellipsoid into the space of an oriented single crystal, and to characterize the ellipsoid in various ways. Though this tool is under development as a planning tool, we have successfully used it to provide the resolution function for convolution with theoretical models. Specifically, theoretical calculations of the spin waves in YFeO3 were compared to measurements taken on SEQUOIA. Though the overall features of the spectra can be explained while neglecting resolution effects, the variation in intensity of the modes is well described once the resolution is included. As this was a single sharp mode, the simulated half intensity value of the resolution ellipsoid was used to provide the resolution width. A description of the simulation, its use, and paths forward for this technique will be discussed.

  13. High Resolution Formaldehyde Photochemistry

    Science.gov (United States)

    Ernest, C. T.; Bauer, D.; Hynes, A. J.

    2010-12-01

    Formaldehyde (HCHO) is the most abundant and most important organic carbonyl compound in the atmosphere. The sources of formaldehyde are the oxidation of methane, isoprene, acetone, and other volatile organic compounds (VOCs); fossil fuel combustion; and biomass burning. The dominant loss mechanism for formaldehyde is photolysis which occurs via two pathways: (R1) HCHO + hv → HCO + H (R2) HCHO + hv → H2 + CO The first pathway (R1) is referred to as the radical channel, while the second pathway (R2) is referred to as the molecular channel. The products of both pathways play a significant role in atmospheric chemistry. The CO that is produced in the molecular channel undergoes further oxidation to produce CO2. Under atmospheric conditions, the H atom and formyl radical that are produced in the radical channel undergo rapid reactions with O2 to produce the hydroperoxyl radical (HO2) via (R3) and (R4). (R3) HCO + O2 → HO2 + CO (R4) H + O2 → HO2 Thus, for every photon absorbed, the photolysis of formaldehyde can contribute one CO2 molecule to the global greenhouse budget or two HO2 radicals to the tropospheric HOx (OH + HO2) cycle. The HO2 radicals produced during formaldehyde photolysis have also been implicated in the formation of photochemical smog. The HO2 radicals act as radical chain carriers and convert NO to NO2, which ultimately results in the catalytic production of O3. Constraining the yield of HO2 produced via HCHO photolysis is essential for improving tropospheric chemistry models. In this study, both the absorption cross section and the quantum yield of the radical channel (R1) were measured at high resolution over the tropospherically relevant wavelength range 304-330 nm. For the cross section measurements a narrow linewidth Nd:YAG pumped dye laser was used with a multi-pass cell. Partial pressures of HCHO were kept below 0.3 torr. Simultaneous measurement of OH LIF in a flame allowed absolute calibration of the wavelength scale. Pressure

  14. Energy resolution methods efficiency depending on beam source position of potassium clusters in time-of-flight mass spectrometer

    Indian Academy of Sciences (India)

    Ş Şentürk; F Demiray; O Özsoy

    2007-09-01

    Energy resolution of the time-of-flight mass spectrometer was considered. The estimations indicate that the time-lag energy focusing method provides better resolution for the parallel case while the turnaround time is more convenient for the perpendicular position. Hence the applicability of the methods used for the energy resolution depends on beam source arrangement.

  15. Algorithmic Enhancement of Spectral Resolution of a LiNbO3 Waveguide-Based Miniature Fourier Transform Spectrometer.

    Science.gov (United States)

    Wang, Kun; Li, Jinyang; Lu, Dan-Feng; Qi, Zhi-Mei

    2016-07-08

    In a recent report we demonstrated a miniature static Fourier transform spectrometer (FTS) that was implemented with a LiNbO3 (LN) waveguide electro-optic modulator (EOM) combined with the dispersion relation between its half-wave voltage and wavelength. The FTS was verified to be able to measure laser wavelength and for low-resolution spectroscopy. In this report, we successfully applied the resolution enhancement algorithm to the FTS, resulting in at least a three-fold increase in its spectral resolution without causing obvious distortion of the measured spectra. The algorithm method used is based on an autoregressive (AR) model, singular value decomposition (SVD), and forward-backward linear prediction (FBLP). The combination of these methods allows the FTS to remain a small size but to possess good spectral resolution, effectively mitigating the conflict between the small size and high resolution of the device. This study opens the way to development of high-resolution miniature FTS. © The Author(s) 2016.

  16. An inelastic X-ray spectrometer with 2.2 meV energy resolution

    CERN Document Server

    Sinn, H; Alatas, A; Barraza, J; Bortel, G; Burkel, E; Shu, D; Sturhahn, W; Sutter, J P; Toellner, T S; Zhao, J

    2001-01-01

    We present a new spectrometer at the Advanced Photon Source for inelastic X-ray scattering with an energy resolution of 2.2 meV at an incident energy of 21.6 keV. For monochromatization, a nested structure of one silicon channel cut and one 'artificial' channel cut is used in forward-scattering geometry. The energy analysis is achieved by a two-dimensional focusing silicon analyzer in backscattering geometry. In the first demonstration experiments, elastic scattering from a Plexiglas sup T sup M sample and two dispersion curves in a beryllium single crystal were measured. Based on these data sets, the performance of the new spectrometer is discussed.

  17. Design of a single moderator-type neutron spectrometer with enhanced energy resolution in the energy range from a few to 100 keV

    Energy Technology Data Exchange (ETDEWEB)

    Tanimura, Y. [Japan Atomic Energy Research Institute, Tokai-mura, Naka-gun, Ibaraki 319-1195 (Japan)]. E-mail: tanimura@popsvr.tokai.jaeri.go.jp; Saegusa, J. [Japan Atomic Energy Research Institute, Tokai-mura, Naka-gun, Ibaraki 319-1195 (Japan); Yoshizawa, M. [Japan Atomic Energy Research Institute, Tokai-mura, Naka-gun, Ibaraki 319-1195 (Japan); Yoshida, M. [Japan Atomic Energy Research Institute, Tokai-mura, Naka-gun, Ibaraki 319-1195 (Japan)

    2005-08-01

    The moderator structure for a neutron spectrometer was optimized with the Monte Carlo code MCNP-4B. The spectrometer consists of a cylindrical moderator and a position-sensitive thermal neutron detector and obtains energy spectra from thermal neutron distribution along its cylindrical axis. The structure of the moderator was improved by using a low hydrogen density material on one end and a high hydrogen density on the other, and inserting a neutron absorber that eliminates thermal neutron diffusion. This design improves the energy resolution of the spectrometer, especially for low-energy neutrons from a few to 100 keV. The designed spectrometer can be applied to the measurement of energy spectra over a neutron energy range from a few keV to 20 MeV.

  18. Image Monitoring of Pharmaceutical Blending Processes and the Determination of an End Point by Using a Portable Near-Infrared Imaging Device Based on a Polychromator-Type Near-Infrared Spectrometer with a High-speed and High-Resolution Photo Diode Array Detector

    Directory of Open Access Journals (Sweden)

    Kodai Murayama

    2015-03-01

    Full Text Available In the present study we have developed a new version (ND-NIRs of a polychromator-type near-infrared (NIR spectrometer with a high-resolution photo diode array detector, which we built before (D-NIRs. The new version has four 5 W halogen lamps compared with the three lamps for the older version. The new version also has a condenser lens with a shorter focal point length. The increase in the number of the lamps and the shortening of the focal point of the condenser lens realize high signal-to-noise ratio and high-speed NIR imaging measurement. By using the ND-NIRs we carried out the in-line monitoring of pharmaceutical blending and determined an end point of the blending process. Moreover, to determinate a more accurate end point, a NIR image of the blending sample was acquired by means of a portable NIR imaging device based on ND-NIRs. The imaging result has demonstrated that the mixing time of 8 min is enough for homogeneous mixing. In this way the present study has demonstrated that ND-NIRs and the imaging system based on a ND-NIRs hold considerable promise for process analysis.

  19. Miniature high-performance infrared spectrometer for space applications

    Science.gov (United States)

    Kruzelecky, Roman V.; Haddad, Emile; Wong, Brian; Lafrance, Denis; Jamroz, Wes; Ghosh, Asoke K.; Zheng, Wanping; Phong, Linh

    2004-06-01

    Infrared spectroscopy probes the characteristic vibrational and rotational modes of chemical bonds in molecules to provide information about both the chemical composition and the bonding configuration of a sample. The significant advantage of the Infrared spectral technique is that it can be used with minimal consumables to simultaneously detect a large variety of chemical and biochemical species with high chemical specificity. To date, relatively large Fourier Transform (FT-IR) spectrometers employing variations of the Michelson interferometer have been successfully employed in space for various IR spectroscopy applications. However, FT-IR systems are mechanically complex, bulky (> 15 kg), and require considerable processing. This paper discusses the use of advanced integrated optics and smart optical coding techniques to significantly extend the performance of miniature IR spectrometers by several orders of magnitude in sensitivity. This can provide the next-generation of compact, high-performance IR spectrometers with monolithically integrated optical systems for robust optical alignment. The entire module can weigh under 3 kg to minimize the mass penalty for space applications. Miniaturized IR spectrometers are versatile and very convenient for small and micro satellite based missions. They can be dedicated to the monitoring of the CO2 in an Earth Observation mission, to Mars exobiology exploration, as well as to vital life support in manned space system; such as the cabin air quality and the quality of the recycled water supply.

  20. 大视场宽谱段高分辨率分波段机载紫外-可见光成像光谱仪设计%Design of Airborne Dual Channel Ultraviolet-Visible Imaging Spectrometer with Large Field of View,Wide Spectrum, and High Resolution

    Institute of Scientific and Technical Information of China (English)

    郝爱花; 胡炳樑; 白加光; 李立波; 于涛; 李思远

    2013-01-01

    紫外-可见光(200~500 nm )成像光谱仪是空间遥感的重要组成部分,本文基于机载紫外-可见成像光谱仪的特殊性和实际应用要求,提出了一种采用面阵CCD的摆扫式成像光谱仪,这样既克服了传统线阵CCD摆扫式成像光谱仪空间分辨率低的缺点,同时又弥补了推扫式成像光谱仪视场范围有限的缺点,能够满足大视场、宽谱段、高分辨率成像光谱仪的应用要求;此外,考虑400~500 nm波段中200~250 nm波段二级光谱的影响和<290 nm的短波区和>310 nm的长波区两个波段相差3个数量级的辐射波动,采用了分波段、分系统的方式独立进行消杂光光谱成像。在系统结构设计方面,本着高性能、低成本的设计理念,选用了两镜同心系统作为望远系统,Czerny-T urner平面光栅结构作为成像光谱仪系统的光学设计方案;设计了一种不使用任何辅助光学元件,全部采用球面镜结构的成像光谱仪。整个系统结构简单、紧凑,性能优良,可行性好。全谱段、全视场调制传递函数值在0.6以上。%The ultraviolet-visible (UV-Vis 200~500 nm) imaging spectrometer is an important part of space remote sensing . Based on special requirements and practical application of the airborne UV-VIS spectrometer ,a kind of scanning imaging spec-trometer using area array CCD is proposed ,which can meet the application requirements of large field of view ,wide spectrum and high resolution .It overcomes low spatial resolution of traditional line array CCD scanning imaging spectrometer ,and limited field of view of the pushbroom imaging spectrometer .In addition ,dual channel was designed to reduce stray light .400~500 nm band includes two order spectrum for 200~250 nm band ,and variation of radiance from earth between the shorter wavelength (310 nm) is above three orders of magnitude .In the structure design of the system , the imaging spectrometer is

  1. High resolution digital delay timer

    Science.gov (United States)

    Martin, Albert D.

    1988-01-01

    Method and apparatus are provided for generating an output pulse following a trigger pulse at a time delay interval preset with a resolution which is high relative to a low resolution available from supplied clock pulses. A first lumped constant delay (20) provides a first output signal (24) at predetermined interpolation intervals corresponding to the desired high resolution time interval. Latching circuits (26, 28) latch the high resolution data (24) to form a first synchronizing data set (60). A selected time interval has been preset to internal counters (142, 146, 154) and corrected for circuit propagation delay times having the same order of magnitude as the desired high resolution. Internal system clock pulses (32, 34) count down the counters to generate an internal pulse delayed by an interval which is functionally related to the preset time interval. A second LCD (184) corrects the internal signal with the high resolution time delay. A second internal pulse is then applied to a third LCD (74) to generate a second set of synchronizing data (76) which is complementary with the first set of synchronizing data (60) for presentation to logic circuits (64). The logic circuits (64) further delay the internal output signal (72) to obtain a proper phase relationship of an output signal (80) with the internal pulses (32, 34). The final delayed output signal (80) thereafter enables the output pulse generator (82) to produce the desired output pulse (84) at the preset time delay interval following input of the trigger pulse (10, 12).

  2. HAND-HELD GAMMA-RAY SPECTROMETER BASED ON HIGH-EFFICIENCY FRISCH-RING CdZnTe DETECTORS.

    Energy Technology Data Exchange (ETDEWEB)

    CUI,Y.

    2007-05-01

    Frisch-ring CdZnTe detectors have demonstrated good energy resolution, el% FWHM at 662 keV, and good efficiency for detecting gamma rays. This technique facilitates the application of CdZnTe materials for high efficiency gamma-ray detection. A hand-held gamma-ray spectrometer based on Frisch-ring detectors is being designed at Brookhaven National Laboratory. It employs an 8x8 CdZnTe detector array to achieve a high volume of 19.2 cm3, so that detection efficiency is significantly improved. By using the front-end ASICs developed at BNL, this spectrometer has a small profile and high energy resolution. The spectrometer includes signal processing circuit, digitization and storage circuit, high-voltage module, and USB interface. In this paper, we introduce the details of the system structure and report our test results with it.

  3. High Precision Momentum Calibration of the Magnetic Spectrometers at MAMI for Hypernuclear Binding Energy Determination

    CERN Document Server

    Margaryan, A; Achenbach, P; Ajvazyan, R; Elbakyan, H; Montgomery, R; Nakamura, S N; Pochodzalla, J; Schulz, F; Toyama, Y; Zhamkochyan, S

    2016-01-01

    We propose a new method for absolute momentum calibration of magnetic spectrometers used in nuclear physics, using the time-of-flight (TOF), differences of pairs of particles with different masses. In cases where the flight path is not known, a calibration can be determined by using the TOF differences of two pair combinations of three particles. A Cherenkov detector, read out by a radio frequency photomultiplier tube, is considered as the high-resolution and highly stable TOF detector. By means of Monte Carlo simulations it is demonstrated that the magnetic spectrometers at the MAMI electron-scattering facility can be calibrated absolutely with an accuracy $\\delta p/p\\leq 10^{-4}$, which will be crucial for high precision determination of hypernuclear masses.

  4. Resolution- and throughput-enhanced spectroscopy using high-throughput computational slit

    CERN Document Server

    Kazemzadeh, Farnoud

    2016-01-01

    There exists a fundamental tradeoff between spectral resolution and the efficiency or throughput for all optical spectrometers. The primary factors affecting the spectral resolution and throughput of an optical spectrometer are the size of the entrance aperture and the optical power of the focusing element. Thus far collective optimization of the above mentioned has proven difficult. Here, we introduce the concept of high-throughput computational slits (HTCS) for improving both the effective spectral resolution and efficiency of a spectrometer. The proposed HTCS approach was experimentally validated using an optical spectrometer configured with a 200 um entrance aperture, test, and a 50 um entrance aperture, control, demonstrating improvements in spectral resolution of the spectrum by ~20% over the control spectral resolution and improvements in efficiency of > 2 times the efficiency of the largest entrance aperture used in the study while producing highly accurate spectra.

  5. High-resolution detectors for soft X-ray spectroscopy

    OpenAIRE

    Soman, Matthew

    2014-01-01

    Resonant Inelastic X-ray Scattering (RIXS) is a modern soft X-ray spectroscopy technique used to investigate the structure of and excitations in materials. It requires high resolution spectrometers and a brilliant, tunable, X-ray source and therefore is carried out at spectrometers such as SAXES at the Swiss Light Source Light, a synchrotron at the Paul Scherrer Institut.\\ud \\ud SAXES uses a grating to disperse X-rays scattered from a sample across a position sensitive detector, a Charge-Coup...

  6. The Mid-Infrared Instrument for the James Webb Space Telescope, VI: The Medium Resolution Spectrometer

    CERN Document Server

    Wells, Martyn; Glasse, Alistair; Wright, G S; Aitink-Kroes, Gabby; Azzollini, Ruyman; Beard, Steven; Brandl, B R; Gallie, Angus; Geers, V C; Glauser, A M; Hastings, Peter; Henning, Th; Jager, Rieks; Justtanont, K; Kruizinga, Bob; Lahuis, Fred; Lee, David; Martinez-Delgado, I; Martinez-Galarza, J R; Meijers, M; Morrison, Jane E; Mueller, Friedrich; Nakos, Thodori; O'Sullivan, Brian; Oudenhuysen, Ad; Parr-Burman, P; Pauwels, Evert; Rohloff, R -R; Schmalzl, Eva; Sykes, Jon; Thelen, M P; van Dishoeck, E F; Vandenbussche, Bart; Venema, Lars B; Visser, Huib; Waters, L B F M; Wright, David

    2015-01-01

    We describe the design and performance of the Medium Resolution Spectrometer (MRS) for the JWST-MIRI instrument. The MRS incorporates four coaxial spectral channels in a compact opto-mechanical layout that generates spectral images over fields of view up to 7.7 X 7.7 arcseconds in extent and at spectral resolving powers ranging from 1,300 to 3,700. Each channel includes an all-reflective integral field unit (IFU): an 'image slicer' that reformats the input field for presentation to a grating spectrometer. Two 1024 X 1024 focal plane arrays record the output spectral images with an instantaneous spectral coverage of approximately one third of the full wavelength range of each channel. The full 5 to 28.5 micron spectrum is then obtained by making three exposures using gratings and pass-band-determining filters that are selected using just two three-position mechanisms. The expected on-orbit optical performance is presented, based on testing of the MIRI Flight Model and including spectral and spatial coverage an...

  7. High-resolution spectroscopy of gases for industrial applications

    DEFF Research Database (Denmark)

    Fateev, Alexander; Clausen, Sønnik

    High-resolution spectroscopy of gases is a powerful technique which has various fundamental and practical applications: in situ simultaneous measurements of gas temperature and gas composition, radiative transfer modeling, validation of existing and developing of new databases and etc. Existing...... for analysis of complex experimental data and further development of the databases. High-temperature gas cell facilities available at DTU Chemical Engineering are presented and described. The gas cells and high-resolution spectrometers allow us to perform high-quality reference measurements of gases relevant...

  8. Design of a transportable high efficiency fast neutron spectrometer

    Energy Technology Data Exchange (ETDEWEB)

    Roecker, C., E-mail: calebroecker@berkeley.edu [Department of Nuclear Engineering, University of California at Berkeley, CA 94720 (United States); Bernstein, A.; Bowden, N.S. [Nuclear and Chemical Sciences Division, Lawrence Livermore National Laboratory, Livermore, CA 94550 (United States); Cabrera-Palmer, B. [Radiation and Nuclear Detection Systems, Sandia National Laboratories, Livermore, CA 94550 (United States); Dazeley, S. [Nuclear and Chemical Sciences Division, Lawrence Livermore National Laboratory, Livermore, CA 94550 (United States); Gerling, M.; Marleau, P.; Sweany, M.D. [Radiation and Nuclear Detection Systems, Sandia National Laboratories, Livermore, CA 94550 (United States); Vetter, K. [Department of Nuclear Engineering, University of California at Berkeley, CA 94720 (United States); Nuclear Science Division, Lawrence Berkeley National Laboratory, Berkeley, CA 94720 (United States)

    2016-08-01

    A transportable fast neutron detection system has been designed and constructed for measuring neutron energy spectra and flux ranging from tens to hundreds of MeV. The transportability of the spectrometer reduces the detector-related systematic bias between different neutron spectra and flux measurements, which allows for the comparison of measurements above or below ground. The spectrometer will measure neutron fluxes that are of prohibitively low intensity compared to the site-specific background rates targeted by other transportable fast neutron detection systems. To measure low intensity high-energy neutron fluxes, a conventional capture-gating technique is used for measuring neutron energies above 20 MeV and a novel multiplicity technique is used for measuring neutron energies above 100 MeV. The spectrometer is composed of two Gd containing plastic scintillator detectors arranged around a lead spallation target. To calibrate and characterize the position dependent response of the spectrometer, a Monte Carlo model was developed and used in conjunction with experimental data from gamma ray sources. Multiplicity event identification algorithms were developed and used with a Cf-252 neutron multiplicity source to validate the Monte Carlo model Gd concentration and secondary neutron capture efficiency. The validated Monte Carlo model was used to predict an effective area for the multiplicity and capture gating analyses. For incident neutron energies between 100 MeV and 1000 MeV with an isotropic angular distribution, the multiplicity analysis predicted an effective area of 500 cm{sup 2} rising to 5000 cm{sup 2}. For neutron energies above 20 MeV, the capture-gating analysis predicted an effective area between 1800 cm{sup 2} and 2500 cm{sup 2}. The multiplicity mode was found to be sensitive to the incident neutron angular distribution.

  9. The Mid-Infrared Instrument for the James Webb Space Telescope: IV. The Low Resolution Spectrometer

    CERN Document Server

    Kendrew, S; Bouchet, P; Amiaux, J; Azzolini, R; Bouwman, J; Chen, C; Dubreuil, D; Fischer, S; Glasse, A; Greene, T; Lagage, P -O; Lahuis, F; Ronayette, S; Wright, D; Wright, G S

    2015-01-01

    The Low Resolution Spectrometer of the MIRI, which forms part of the imager module, will provide R~100 long-slit and slitless spectroscopy from 5 to 12 micron. The design is optimised for observations of compact sources, such as exoplanet host stars. We provide here an overview of the design of the LRS, and its performance as measured during extensive test campaigns, examining in particular the delivered image quality, dispersion, and resolving power, as well as spectrophotometric performance, flatfield accuracy and the effects of fringing. We describe the operational concept of the slitless mode, which is optimally suited to transit spectroscopy of exoplanet atmospheres. The LRS mode of the MIRI was found to perform consistently with its requirements and goals.

  10. High-resolution spectroscopy of gases at elevated temperatures for industrial applications

    DEFF Research Database (Denmark)

    development of existing and developing new databases. Measurements should be performed at well-controlled conditions in a highly temperature uniform heated gas cell with a high-resolution spectrometer. In this work some high-temperature, high-resolution IR absorption/transmission measurements gases relevant...

  11. High Resolution Orientation Imaging Microscopy

    Science.gov (United States)

    2012-05-02

    carbon distribution as it relates to the presence of Bainite phase (with small tetragonality) interspersed among the cubic ferrite. An example of the...preferentially segregate. The view offered by these high resolution methods differs from what has been considered before: grains thought to be Bainite

  12. High-Resolution Instrumentation Radar.

    Science.gov (United States)

    1986-09-30

    30 September 1986 Los Angeles Air Force Station 13. NUMBER OF PAGES Los Angeles, Calif. 90009-2960 36 74. MONITORING AGENCY NAME & ADDRESS(If...TREE PLMUT ",-20 -CUTLIASS DumpER SED AN... TREE TRUNK, -0 - MERC BUMPER f - 40 H!-I -50 iI Fig. 7. High-Resolution Instrumentation Radar View of

  13. High precision electric gate for time-of-flight ion mass spectrometers

    Science.gov (United States)

    Sittler, Edward C. (Inventor)

    2011-01-01

    A time-of-flight mass spectrometer having a chamber with electrodes to generate an electric field in the chamber and electric gating for allowing ions with a predetermined mass and velocity into the electric field. The design uses a row of very thin parallel aligned wires that are pulsed in sequence so the ion can pass through the gap of two parallel plates, which are biased to prevent passage of the ion. This design by itself can provide a high mass resolution capability and a very precise start pulse for an ion mass spectrometer. Furthermore, the ion will only pass through the chamber if it is within a wire diameter of the first wire when it is pulsed and has the right speed so it is near all other wires when they are pulsed.

  14. Requirements on high resolution detectors

    Energy Technology Data Exchange (ETDEWEB)

    Koch, A. [European Synchrotron Radiation Facility, Grenoble (France)

    1997-02-01

    For a number of microtomography applications X-ray detectors with a spatial resolution of 1 {mu}m are required. This high spatial resolution will influence and degrade other parameters of secondary importance like detective quantum efficiency (DQE), dynamic range, linearity and frame rate. This note summarizes the most important arguments, for and against those detector systems which could be considered. This article discusses the mutual dependencies between the various figures which characterize a detector, and tries to give some ideas on how to proceed in order to improve present technology.

  15. Simultaneous measurement of {sup 239}Pu, {sup 240}Pu, {sup 241}Pu, and {sup 242}Pu by high resolution inductively coupled plasma mass spectrometer (HR ICP-MS) in marine sediments; Mesure des isotopes du plutonium des sediments marins par spectrometrie de masse a plasma couple inductivement haute resolution (HR ICP-MS)

    Energy Technology Data Exchange (ETDEWEB)

    Bruneau, F

    1999-07-01

    Transuranics elements are of particular interest in radioecological studies because of their radiotoxicity and their potential use to decipher source fingerprints and transport processes. The simultaneous measurement of {sup 239}Pu, {sup 240}Pu, {sup 241}Pu, and {sup 242}Pu in environmental samples requires a specific chemical procedure. This work deals with an analytical procedure which yields a very high grade of purification of Pu suitable for ultra low level detection by HR ICP-MS, from marine sediments. After the elimination of major elements (Fe, Al, Mg...) by a first chromatographic separation, a new device of purification by solvent extraction and concentration by a second chromatographic separation is used to obtain a concentrated and high purified solution of plutonium. The chemical procedure have been validated on IAEA certified sediment samples and on sediment samples collected in the roads of Cherbourg which had been previously analysed by other techniques (a spectrometry and thermo-ionisation mass spectrometer). (author)

  16. Novel techniques in VUV high-resolution spectroscopy

    CERN Document Server

    Ubachs, W; Eikema, K S E; de Oliveira, N; Nahon, L

    2013-01-01

    Novel VUV sources and techniques for VUV spectroscopy are reviewed. Laser-based VUV sources have been developed via non-linear upconversion of laser pulses in the nanosecond (ns), the picosecond (ps), and femtosecond (fs) domain, and are applied in high-resolution gas phase spectroscopic studies. While the ns and ps pulsed laser sources, at Fourier-transform limited bandwidths, are used in wavelength scanning spectroscopy, the fs laser source is used in a two-pulse time delayed mode. In addition a Fourier-transform spectrometer for high resolution gas-phase spectroscopic studies in the VUV is described, exhibiting the multiplex advantage to measure many resonances simultaneously.

  17. High resolution tomographic instrument development

    Energy Technology Data Exchange (ETDEWEB)

    1992-08-01

    Our recent work has concentrated on the development of high-resolution PET instrumentation reflecting in part the growing importance of PET in nuclear medicine imaging. We have developed a number of positron imaging instruments and have the distinction that every instrument has been placed in operation and has had an extensive history of application for basic research and clinical study. The present program is a logical continuation of these earlier successes. PCR-I, a single ring positron tomograph was the first demonstration of analog coding using BGO. It employed 4 mm detectors and is currently being used for a wide range of biological studies. These are of immense importance in guiding the direction for future instruments. In particular, PCR-II, a volume sensitive positron tomograph with 3 mm spatial resolution has benefited greatly from the studies using PCR-I. PCR-II is currently in the final stages of assembly and testing and will shortly be placed in operation for imaging phantoms, animals and ultimately humans. Perhaps the most important finding resulting from our previous study is that resolution and sensitivity must be carefully balanced to achieve a practical high resolution system. PCR-II has been designed to have the detection characteristics required to achieve 3 mm resolution in human brain under practical imaging situations. The development of algorithms by the group headed by Dr. Chesler is based on a long history of prior study including his joint work with Drs. Pelc and Reiderer and Stearns. This body of expertise will be applied to the processing of data from PCR-II when it becomes operational.

  18. High resolution tomographic instrument development

    Energy Technology Data Exchange (ETDEWEB)

    1992-01-01

    Our recent work has concentrated on the development of high-resolution PET instrumentation reflecting in part the growing importance of PET in nuclear medicine imaging. We have developed a number of positron imaging instruments and have the distinction that every instrument has been placed in operation and has had an extensive history of application for basic research and clinical study. The present program is a logical continuation of these earlier successes. PCR-I, a single ring positron tomograph was the first demonstration of analog coding using BGO. It employed 4 mm detectors and is currently being used for a wide range of biological studies. These are of immense importance in guiding the direction for future instruments. In particular, PCR-II, a volume sensitive positron tomograph with 3 mm spatial resolution has benefited greatly from the studies using PCR-I. PCR-II is currently in the final stages of assembly and testing and will shortly be placed in operation for imaging phantoms, animals and ultimately humans. Perhaps the most important finding resulting from our previous study is that resolution and sensitivity must be carefully balanced to achieve a practical high resolution system. PCR-II has been designed to have the detection characteristics required to achieve 3 mm resolution in human brain under practical imaging situations. The development of algorithms by the group headed by Dr. Chesler is based on a long history of prior study including his joint work with Drs. Pelc and Reiderer and Stearns. This body of expertise will be applied to the processing of data from PCR-II when it becomes operational.

  19. HRSC: High resolution stereo camera

    Science.gov (United States)

    Neukum, G.; Jaumann, R.; Basilevsky, A.T.; Dumke, A.; Van Gasselt, S.; Giese, B.; Hauber, E.; Head, J. W.; Heipke, C.; Hoekzema, N.; Hoffmann, H.; Greeley, R.; Gwinner, K.; Kirk, R.; Markiewicz, W.; McCord, T.B.; Michael, G.; Muller, Jan-Peter; Murray, J.B.; Oberst, J.; Pinet, P.; Pischel, R.; Roatsch, T.; Scholten, F.; Willner, K.

    2009-01-01

    The High Resolution Stereo Camera (HRSC) on Mars Express has delivered a wealth of image data, amounting to over 2.5 TB from the start of the mapping phase in January 2004 to September 2008. In that time, more than a third of Mars was covered at a resolution of 10-20 m/pixel in stereo and colour. After five years in orbit, HRSC is still in excellent shape, and it could continue to operate for many more years. HRSC has proven its ability to close the gap between the low-resolution Viking image data and the high-resolution Mars Orbiter Camera images, leading to a global picture of the geological evolution of Mars that is now much clearer than ever before. Derived highest-resolution terrain model data have closed major gaps and provided an unprecedented insight into the shape of the surface, which is paramount not only for surface analysis and geological interpretation, but also for combination with and analysis of data from other instruments, as well as in planning for future missions. This chapter presents the scientific output from data analysis and highlevel data processing, complemented by a summary of how the experiment is conducted by the HRSC team members working in geoscience, atmospheric science, photogrammetry and spectrophotometry. Many of these contributions have been or will be published in peer-reviewed journals and special issues. They form a cross-section of the scientific output, either by summarising the new geoscientific picture of Mars provided by HRSC or by detailing some of the topics of data analysis concerning photogrammetry, cartography and spectral data analysis.

  20. High-resolution x-ray photoemission spectra of silver

    DEFF Research Database (Denmark)

    Barrie, A.; Christensen, N. E.

    1976-01-01

    An electron spectrometer fitted with an x-ray monochromator for Al Kα1,2 radiation (1486.6 eV) has been used to record high-resolution x-ray photoelectron spectra for the 4d valence band as well as the 3d spin doublet in silver. The core-level spectrum has a line shape that can be described...

  1. Section on High Resolution Optical Imaging (HROI)

    Data.gov (United States)

    Federal Laboratory Consortium — The Section on High Resolution Optical Imaging (HROI) develops novel technologies for studying biological processes at unprecedented speed and resolution. Research...

  2. High Resolution Muon Computed Tomography at Neutrino Beam Facilities

    CERN Document Server

    Suerfu, Burkhant

    2015-01-01

    X-ray computed tomography (CT) has an indispensable role in constructing 3D images of objects made from light materials. However, limited by absorption coefficients, X-rays cannot deeply penetrate materials such as copper and lead. Here we show via simulation that muon beams can provide high resolution tomographic images of dense objects and of structures within the interior of dense objects. The effects of resolution broadening from multiple scattering diminish with increasing muon momentum. As the momentum of the muon increases, the contrast of the image goes down and therefore requires higher resolution in the muon spectrometer to resolve the image. The variance of the measured muon momentum reaches a minimum and then increases with increasing muon momentum. The impact of the increase in variance is to require a higher integrated muon flux to reduce fluctuations. The flux requirements and level of contrast needed for high resolution muon computed tomography are well matched to the muons produced in the pio...

  3. High-resolution absorption measurements of NH3 at high temperatures: 500–2100cm−1

    DEFF Research Database (Denmark)

    Barton, Emma J.; Yurchenko, Sergei N.; Tennyson, Jonathan

    2015-01-01

    High-resolution absorption spectra of NH3 in the region 500–2100 cm -1 at temperatures up to1027 1C and approximately atmospheric pressure (1013±20 mbar) are measured. NH3 concentrations of 1000 ppm,0.5% and 1% in volume fraction were used in the measurements. Spectra are recorded in high...... temperature gas flow cells using a FourierTransform Infrared (FTIR) spectrometer at a nominal resolution of 0.09cm-1. Measurements at 22.7 °C are compared to high-resolution cross sections available from thePacific Northwest National Laboratory (PNNL). The higher temperature spectra are analysed by comparison...

  4. High-pressure duo-multichannel soft x-ray spectrometer for tokamak plasma diagnostics

    Energy Technology Data Exchange (ETDEWEB)

    Schwob, J.L.; Wouters, A.W.; Suckewer, S.

    1987-03-01

    A high-resolution, time-resolving soft X-ray multichannel spectrometer (SOXMOS) that permits the simultaneous measurement of emission in two different spectral ranges has been developed and tested extensively for tokamak plasma diagnostics. The basic instrument is a high-resolution, interferometrically adjusted, extreme grazing incidence Schwob-Fraenkel duochromator. The instrument is equipped with two multichannel detectors that are adjusted interferometrically and scan along the Rowland circle. Each consists of an MgF/sub 2/ coated, funneled microchannel plate, associated with a phosphor screen image intensifier that is coupled to a 1024-element photodiode array by a flexible fibrer optic conduit. The total wavelength coverage of the instrument is 5 to 340/sup 0/ A with a measured resolution (FWHM) of about 0.2 A when equipped with a 600 g/mm grating, and 5 to 85 A with a resolution of about 0.06 A using a 2400 g/mm grating. The simultaneous spectral coverage of each detector varies from 15 A at the short wavelength limit to 70 A at the long wavelength limit with the lower dispersion grating. The minimum read-out time for a full spectral portion is 17 ms, but several individual lines can be measured with 1 ms time resolution by selected pixel readout. Higher time resolution can be achieved by replacing one multichannel detector with a single channel electron multiplier detector. Examples of data from the PLT and TFTR tokamaks are presented to illustrate the instrument's versatility, high spectral resolution, and high signal-to-noise ratio even in the 10 A region. 44 refs., 20 figs.

  5. High-sensitivity, portable, tunable imaging X-ray spectrometer based on a spherical crystal and MCP

    CERN Document Server

    Monot, P; Dobosz, S; D'Oliveira, P; Hulin, S; Bougeard, M; Faenov, A Y; Pikuz, T A; Skobelev, I Y

    2002-01-01

    A portable (200x100x100 mm sup 3), high-luminosity, spherically bent crystal spectrometer was designed to measure very low emissivity X-ray spectra of different elements with spatial resolution in a wide spectral range (1.2-19.6 A). A large (50x15 mm sup 2) open aperture mica spherically bent crystal with R=150 mm was used as dispersive and focusing element. This spectrometer was associated with a large sensitive area (phi=40 mm) micro-channel plates assembly. This apparatus provides simultaneously high spectral (lambda/delta lambda approx 1800) and spatial (100-200 mu m) resolutions. Its large tunability allowed, without any adjustment of the spectrometer set-up, to record spectra in the 1.38-17.5 A wavelength range. We used the X-ray emission of femtosecond laser-produced plasmas from different materials ((CF sub 2) sub n , CaF sub 2 , Cu, Al) to test the spectrometer. Thanks to the high sensitivity (high collection efficiency) of the system, high quality space-resolved X-ray spectra of Fluorine and Aluminu...

  6. Detector tests in a high magnetic field and muon spectrometer triggering studies on a small prototype for an LHC experiment

    CERN Document Server

    Ambrosi, G; Basile, M; Battiston, R; Bergsma, F; Castro, H; Cifarelli, Luisa; Cindolo, F; Contin, A; De Pasquale, S; Gálvez, J; Gentile, S; Giusti, P; Laurent, G; Levi, G; Lin, Q; Maccarrone, G D; Mattern, D; Nania, R; Rivera, F; Schioppa, M; Sharma, A; CERN. Geneva. Detector Research and Development Committee

    1990-01-01

    The "Large Area Devices" group of the LAA project is working on R&D for muon detection at a future super-collider. New detectors are under development and the design of a muon spectrometer for an LHC experiment is under study. Our present choice is for a compact, high field, air-core toroidal muon spectrometer. Good momentum resolution is achievable in this compact solution, with at least one plane of detection elements inside the high field region. A new detector, the Blade Chamber, making use of blades instead of wires, has been developed for the forward and backward regions of the spectrometer, where polar coordinate readings are desirable.The assembling of a CERN high energy beam line, equipped with high resolution drift chambers and a strong field magnet could give us the opportunity to test our chambers in a high magnetic field and to study the muon trigger capabilities of a spectrometer, like the one proposed, on a small prototype.

  7. Qualification of a high-efficiency, gated spectrometer for x-ray Thomson scattering on the National Ignition Facility

    Energy Technology Data Exchange (ETDEWEB)

    Döppner, T.; Kritcher, A. L.; Bachmann, B.; Burns, S.; Hawreliak, J.; House, A.; Landen, O. L.; LePape, S.; Ma, T.; Pak, A.; Swift, D. [Lawrence Livermore National Laboratory, Livermore, California 94550 (United States); Neumayer, P. [Gesellschaft für Schwerionenphysik, 64291 Darmstadt (Germany); Kraus, D. [University of California, Berkeley, California 94720 (United States); Falcone, R. W. [University of California, Berkeley, California 94720 (United States); Lawrence Berkeley National Laboratory, Berkeley, California 94720 (United States); Glenzer, S. H. [SLAC National Accelerator Laboratory, Menlo Park, California 94309 (United States)

    2014-11-15

    We have designed, built, and successfully fielded a highly efficient and gated Bragg crystal spectrometer for x-ray Thomson scattering measurements on the National Ignition Facility (NIF). It utilizes a cylindrically curved Highly Oriented Pyrolytic Graphite crystal. Its spectral range of 7.4–10 keV is optimized for scattering experiments using a Zn He-α x-ray probe at 9.0 keV or Mo K-shell line emission around 18 keV in second diffraction order. The spectrometer has been designed as a diagnostic instrument manipulator-based instrument for the NIF target chamber at the Lawrence Livermore National Laboratory, USA. Here, we report on details of the spectrometer snout, its novel debris shield configuration and an in situ spectral calibration experiment with a Brass foil target, which demonstrated a spectral resolution of E/ΔE = 220 at 9.8 keV.

  8. Spatial heterodyne spectrometer for FLEX

    Science.gov (United States)

    Scott, Alan; Zheng, Sheng-Hai; Brown, Stephen; Bell, Andrew

    2007-10-01

    A spatial heterodyne spectrometer (SHS) has significant advantages for high spectral resolution imaging over narrow pre-selected bands compared to traditional solutions. Given comparable optical étendue at R~6500, a field-widened SHS will have a throughput-resolution product ~170 x larger than an air-spaced etalon spectrometer, and ~1000 x larger than a standard grating spectrometer. The monolithic glass Michelson design and lack of moving parts allows maximum stability of spectral calibration over the mission life. For these reasons, SHS offers considerable advantages for the core spectrometer instrument in the European Space Agency's (ESA) Fluorescence Explorer (FLEX) mission.

  9. High-resolution intravital microscopy.

    Directory of Open Access Journals (Sweden)

    Volker Andresen

    Full Text Available Cellular communication constitutes a fundamental mechanism of life, for instance by permitting transfer of information through synapses in the nervous system and by leading to activation of cells during the course of immune responses. Monitoring cell-cell interactions within living adult organisms is crucial in order to draw conclusions on their behavior with respect to the fate of cells, tissues and organs. Until now, there is no technology available that enables dynamic imaging deep within the tissue of living adult organisms at sub-cellular resolution, i.e. detection at the level of few protein molecules. Here we present a novel approach called multi-beam striped-illumination which applies for the first time the principle and advantages of structured-illumination, spatial modulation of the excitation pattern, to laser-scanning-microscopy. We use this approach in two-photon-microscopy--the most adequate optical deep-tissue imaging-technique. As compared to standard two-photon-microscopy, it achieves significant contrast enhancement and up to 3-fold improved axial resolution (optical sectioning while photobleaching, photodamage and acquisition speed are similar. Its imaging depth is comparable to multifocal two-photon-microscopy and only slightly less than in standard single-beam two-photon-microscopy. Precisely, our studies within mouse lymph nodes demonstrated 216% improved axial and 23% improved lateral resolutions at a depth of 80 µm below the surface. Thus, we are for the first time able to visualize the dynamic interactions between B cells and immune complex deposits on follicular dendritic cells within germinal centers (GCs of live mice. These interactions play a decisive role in the process of clonal selection, leading to affinity maturation of the humoral immune response. This novel high-resolution intravital microscopy method has a huge potential for numerous applications in neurosciences, immunology, cancer research and

  10. High-resolution image analysis.

    Science.gov (United States)

    Preston, K

    1986-01-01

    In many departments of cytology, cytogenetics, hematology, and pathology, research projects using high-resolution computerized microscopy are now being mounted for computation of morphometric measurements on various structural components, as well as for determination of cellular DNA content. The majority of these measurements are made in a partially automated, computer-assisted mode, wherein there is strong interaction between the user and the computerized microscope. At the same time, full automation has been accomplished for both sample preparation and sample examination for clinical determination of the white blood cell differential count. At the time of writing, approximately 1,000 robot differential counting microscopes are in the field, analyzing images of human white blood cells, red blood cells, and platelets at the overall rate of about 100,000 slides per day. This mammoth through-put represents a major accomplishment in the application of machine vision to automated microscopy for hematology. In other areas of automated high-resolution microscopy, such as cytology and cytogenetics, no commercial instruments are available (although a few metaphase-finding machines are available and other new machines have been announced during the past year). This is a disappointing product, considering the nearly half century of research effort in these areas. This paper provides examples of the state of the art in automation of cell analysis for blood smears, cervical smears, and chromosome preparations. Also treated are new developments in multi-resolution automated microscopy, where images are now being generated and analyzed by a single machine over a range of 64:1 magnification and from 10,000 X 20,000 to 500 X 500 in total picture elements (pixels). Examples of images of human lymph node and liver tissue are presented. Semi-automated systems are not treated, although there is mention of recent research in the automation of tissue analysis.

  11. High resolution spectroscopy from low altitude satellites. [gamma ray astronomy

    Science.gov (United States)

    Nakano, G. H.; Imhof, W. L.

    1978-01-01

    The P 78 1 satellite to be placed in a synchronous polar orbit at an altitude of 550-660 km will carry two identical high resolution spectrometers each consisting of a single (approximately 85 cc) intrinsic germanium IGE detector. The payload also includes a pair of phoswitch scintillators, an array of CdTe detectors and several particle detectors, all of which are mounted on the wheel of the satellite. The intrinsic high purity IGE detectors receive cooling from two Stirling cycle refrigerators and facilitate the assembly of large and complex detector arrays planned for the next generation of high sensitivity instruments such as those planned for the gamma ray observatory. The major subsystems of the spectrometer are discussed as well as its capabilities.

  12. Ultra-high resolution AMOLED

    Science.gov (United States)

    Wacyk, Ihor; Prache, Olivier; Ghosh, Amal

    2011-06-01

    AMOLED microdisplays continue to show improvement in resolution and optical performance, enhancing their appeal for a broad range of near-eye applications such as night vision, simulation and training, situational awareness, augmented reality, medical imaging, and mobile video entertainment and gaming. eMagin's latest development of an HDTV+ resolution technology integrates an OLED pixel of 3.2 × 9.6 microns in size on a 0.18 micron CMOS backplane to deliver significant new functionality as well as the capability to implement a 1920×1200 microdisplay in a 0.86" diagonal area. In addition to the conventional matrix addressing circuitry, the HDTV+ display includes a very lowpower, low-voltage-differential-signaling (LVDS) serialized interface to minimize cable and connector size as well as electromagnetic emissions (EMI), an on-chip set of look-up-tables for digital gamma correction, and a novel pulsewidth- modulation (PWM) scheme that together with the standard analog control provides a total dimming range of 0.05cd/m2 to 2000cd/m2 in the monochrome version. The PWM function also enables an impulse drive mode of operation that significantly reduces motion artifacts in high speed scene changes. An internal 10-bit DAC ensures that a full 256 gamma-corrected gray levels are available across the entire dimming range, resulting in a measured dynamic range exceeding 20-bits. This device has been successfully tested for operation at frame rates ranging from 30Hz up to 85Hz. This paper describes the operational features and detailed optical and electrical test results for the new AMOLED WUXGA resolution microdisplay.

  13. Electron spectrometer for gas-phase spectroscopy

    Energy Technology Data Exchange (ETDEWEB)

    Bozek, J.D.; Schlachter, A.S. [Ernest Orlando Lawrence Berkeley National Lab., CA (United States)

    1997-04-01

    An electron spectrometer for high-resolution spectroscopy of gaseous samples using synchrotron radiation has been designed and constructed. The spectrometer consists of a gas cell, cylindrical electrostatic lens, spherical-sector electron energy analyzer, position-sensitive detector and associated power supplies, electronics and vacuum pumps. Details of the spectrometer design are presented together with some representative spectra.

  14. High-resolution slug testing.

    Science.gov (United States)

    Zemansky, G M; McElwee, C D

    2005-01-01

    The hydraulic conductivity (K) variation has important ramifications for ground water flow and the transport of contaminants in ground water. The delineation of the nature of that variation can be critical to complete characterization of a site and the planning of effective and efficient remedial measures. Site-specific features (such as high-conductivity zones) need to be quantified. Our alluvial field site in the Kansas River valley exhibits spatial variability, very high conductivities, and nonlinear behavior for slug tests in the sand and gravel aquifer. High-resolution, multilevel slug tests have been performed in a number of wells that are fully screened. A general nonlinear model based on the Navier-Stokes equation, nonlinear frictional loss, non-Darcian flow, acceleration effects, radius changes in the wellbore, and a Hvorslev model for the aquifer has been used to analyze the data, employing an automated processing system that runs within the Excel spreadsheet program. It is concluded that slug tests can provide the necessary data to identify the nature of both horizontal and vertical K variation in an aquifer and that improved delineation or higher resolution of K structure is possible with shorter test intervals. The gradation into zones of higher conductivity is sharper than seen previously, and the maximum conductivity observed is greater than previously measured. However, data from this project indicate that well development, the presence of fines, and the antecedent history of the well are important interrelated factors in regard to slug-test response and can prevent obtaining consistent results in some cases.

  15. A High Resolution HPGeγ-ray Spectrometer

    Institute of Scientific and Technical Information of China (English)

    1994-01-01

    4.7AHighResolutionHPGeγ-raySpetrometerPanDajing;WuShaoyun;LuoYingxin;LiangQikai;LiuYongsheng;ChengBaoliuγ-rayspectrometerisus...

  16. Science with the XEUS High Time Resolution Spectrometer

    NARCIS (Netherlands)

    Barret, D.; Belloni, T.; Bhattacharyya, S.; Cackett, E.; Gilfanov, M.; G¨o˘g¨u¸s, E.; Homan, J.; M´endez, M.; Miller, J.M.; Miller, M.C.; Mereghettik, S.; Paltanil, S.; Poutanen, J.; Wilms, J.; Zdziarski, A.A.

    2008-01-01

    XEUS has been recently selected by ESA for an assessment study. XEUS is a large mission candidate for the Cosmic Vision program, aiming for a launch date as early as 2018. XEUS is a follow-on to ESA’s Cornerstone X-Ray Spectroscopy Mission (XMM–Newton). It will be placed in a halo orbit at L2, by a

  17. High-Resolution, Low-Cost Spectrometer-on-Chip

    Science.gov (United States)

    2015-01-02

    increase the performance of the devices. All the prototype chips were made using Electron Beam Lithography ( EBL ) and reactive ion etching (RIE). Specific...the input coupling efficiency when using inverted tapers. In total, more than 50 designs were fabricated by EBL and plasma etching in order to...performance (DPH reflectivity, channel numbers, etc…) of the imprinted chips are very close to the ones made by EBL . Around 100 chips were

  18. Alignment and Characterization of High Uniformity Imaging Spectrometers

    Science.gov (United States)

    Bender, Holly A.; Mouroulis, Pantazis; Eastwood, Michael L.; Green, Robert O.; Geier, Sven; Hochberg, Eric B.

    2011-01-01

    Imaging spectrometers require precise adjustments, in some cases at the sub-micrometer level, in order to achieve auniform response over both the spectral and spatial dimensions. We describe a set of measurement techniques and theircorresponding alignment adjustments to achieve the 95% or higher uniformity specifications required for Earthobservingimaging spectrometers. The methods are illustrated with measurements from the Next Generation Imaging Spectrometer system that has been built at the Jet Propulsion Laboratory, California Institute of Technology, under contract with the National Aeronautics and Space Administration.

  19. High-resolution land topography

    Science.gov (United States)

    Massonnet, Didier; Elachi, Charles

    2006-11-01

    After a description of the background, methods of production and some scientific uses of high-resolution land topography, we present the current status and the prospect of radar interferometry, regarded as one of the best techniques for obtaining the most global and the most accurate topographic maps. After introducing briefly the theoretical aspects of radar interferometry - principles, limits of operation and various capabilities -, we will focus on the topographic applications that resulted in an almost global topographic map of the earth: the SRTM map. After introducing the Interferometric Cartwheel system, we will build on its expected performances to discuss the scientific prospects of refining a global topographic map to sub-metric accuracy. We also show how other fields of sciences such as hydrology may benefit from the products generated by interferometric radar systems. To cite this article: D. Massonnet, C. Elachi, C. R. Geoscience 338 (2006).

  20. Note: Multi channel Doppler tuned spectrometer to study highly charged ions.

    Science.gov (United States)

    Karn, Ranjeet K; Mishra, C N; Ahmad, Nissar; Saini, S K; Safvan, C P; Nandi, T

    2014-06-01

    We describe the design and implementation of a multi channel Doppler tuned spectrometer setup to study physics of highly charged ions at high resolution in a direct way. A unique Soller slit assembly coupled with a long one dimensional position sensitive proportional counter enables us to get distinct x-ray peaks at different angles, which allows us to cover large number of angle in one shot. By using this setup, 1s2s (3)S1 - 1s(2) (1)S0 M1 transition in He-like Fe has been resolved from its satellite line 1s2s2p ⁴P(5/2)⁰ - 1s(2)2s (2)S(1/2) M2 transition in Li-like Fe and measured the lifetime of their respective upper levels with high precision.

  1. Spectroscopic Investigations of Highly Charged Ions using X-Ray Calorimeter Spectrometers

    Energy Technology Data Exchange (ETDEWEB)

    Thorn, Daniel Bristol [Univ. of California, Davis, CA (United States)

    2008-11-19

    Spectroscopy of K-shell transitions in highly charged heavy ions, like hydrogen-like uranium, has the potential to yield information about quantum electrodynamics (QED) in extremely strong nuclear fields as well as tests of the standard model, specifically parity violation in atomic systems. These measurements would represent the 'holy grail' in high-Z atomic spectroscopy. However, the current state-of-the-art detection schemes used for recording the K-shell spectra from highly charged heavy ions does not yet have the resolving power to be able to attain this goal. As such, to push the field of high-Z spectroscopy forward, new detectors must be found. Recently, x-ray calorimeter spectrometers have been developed that promise to make such measurements. In an effort to make the first steps towards attaining the 'holy grail', measurements have been performed with two x-ray calorimeter spectrometers (the XRS/EBIT and the ECS) designed and built at Goddard Space Flight Center in Greenbelt, MD. The calorimeter spectrometers have been used to record the K-shell spectra of highly charged ions produced in the SuperEBIT electron beam ion trap at Lawrence Livermore National Laboratory in Livermore, CA. Measurements performed with the XRS/EBIT calorimeter array found that the theoretical description of well-above threshold electron-impact excitation cross sections for hydrogen-like iron and nickel ions are correct. Furthermore, the first high-resolution spectrum of hydrogen-like through carbon-like praseodymium ions was recorded with a calorimeter. In addition, the new high-energy array on the EBIT Calorimeter Spectrometer (ECS) was used to resolve the K-shell x-ray emission spectrum of highly charged xenon ions, where a 40 ppm measurement of the energy of the K-shell resonance transition in helium-like xenon was achieved. This is the highest precision result, ever, for an element with such high atomic number. In addition, a first-of-its-kind measurement of

  2. High-resolution electron microscopy of advanced materials

    Energy Technology Data Exchange (ETDEWEB)

    Mitchell, T.E.; Kung, H.H.; Sickafus, K.E.; Gray, G.T. III; Field, R.D.; Smith, J.F. [Los Alamos National Lab., NM (United States). Materials Science and Technology Div.

    1997-11-01

    This final report chronicles a three-year, Laboratory Directed Research and Development (LDRD) project at Los Alamos National Laboratory (LANL). The High-Resolution Electron Microscopy Facility has doubled in size and tripled in quality since the beginning of the three-year period. The facility now includes a field-emission scanning electron microscope, a 100 kV field-emission scanning transmission electron microscope (FE-STEM), a 300 kV field-emission high-resolution transmission electron microscope (FE-HRTEM), and a 300 kV analytical transmission electron microscope. A new orientation imaging microscope is being installed. X-ray energy dispersive spectrometers for chemical analysis are available on all four microscopes; parallel electron energy loss spectrometers are operational on the FE-STEM and FE-HRTEM. These systems enable evaluation of local atomic bonding, as well as chemical composition in nanometer-scale regions. The FE-HRTEM has a point-to-point resolution of 1.6 {angstrom}, but the resolution can be pushed to its information limit of 1 {angstrom} by computer reconstruction of a focal series of images. HRTEM has been used to image the atomic structure of defects such as dislocations, grain boundaries, and interfaces in a variety of materials from superconductors and ferroelectrics to structural ceramics and intermetallics.

  3. A spectrometer for study of high mass objects created in relativistic heavy ion reactions

    Energy Technology Data Exchange (ETDEWEB)

    Armstrong, T.A.; Barish, K.N.; Batsouli, S.; Bennett, M.J.; Bennett, S.J.; Chikanian, A.; Coe, S.D.; Cormier, T.M.; Davies, R.R.; De Cataldo, G.; Dee, P.; Diebold, G.E.; Dover, C.B.; Ewell, L.A.; Emmet, W.; Fachini, P.; Fadem, B.; Finch, L.E.; George, N.K.; Giglietto, N.; Greene, S.V.; Haridas, P.; Hill, J.C. E-mail: jhill@iastate.edu; Hirsch, A.S.; Hoversten, R.A.; Huang, H.Z.; Jaradat, H.; Kim, B.; Kumar, B.S.; Lajoie, J.G.; Lainis, T.; Lewis, R.A.; Li, Q.; Li, Y.; Libby, B.; Majka, R.D.; Miller, T.E.; Munhoz, M.G.; Nagle, J.L.; Petridis, A.; Pless, I.A.; Pope, J.K.; Porile, N.T.; Pruneau, C.; Rabin, M.S.Z.; Reid, J.D.; Rimai, A.; Riso, J.; Rose, A.; Rotondo, F.S.; Sandweiss, J.; Scharenberg, R.P.; Skank, H.; Slaughter, A.J.; Sleage, G.; Smith, G.A.; Spinelli, P.; Srivastava, B.K.; Tincknell, M.L.; Toothacker, W.S.; Van Buren, G.; Wilson, W.K.; Wohn, F.K.; Wolin, E.J.; Xu, Z.; Zhao, K

    1999-11-21

    Experiment E864 at the Brookhaven AGS accelerator uses a high sensitivity, large acceptance spectrometer, designed to search for strangelets and other novel forms of matter produced in high-energy heavy ion collisions. The spectrometer has excellent acceptance and rate capabilities for measuring the production properties of known particles and nuclei such as p-bar, d-bar and {sup 6}He. The experiment uses a magnetic spectrometer and employs redundant time of flight and position detectors and a hadronic calorimeter. In this paper we describe the design and performance of the spectrometer.

  4. High Etendue Imaging Fourier Transform Spectrometer: initial results

    Science.gov (United States)

    Horton, Richard F.; Conger, Chris A.; Pelligrino, L. S.

    1997-10-01

    At the Denver meeting, last year, we presented the High Etendue Imaging Fourier Transform Spectrometer, (HEIFTS), theory and optical design. This device uses a new 'image plane interferometer' geometry to produce 'autocorrelation function modulation' in the image plane of a 2D imaging array, such that the phase offset of the modulation varies linearly across the image. As a 2D image is pushbroomed across the imaging, array, the record of an individual scene pixel is recorded for each autocorrelation phase offset. The 3D array of this data is processed to yield an 'autocorrelation function' data cube, which is Fourier transformed to yield a 'wavenumber' hyperspectral data curve. A phase I device has been demonstrated in the laboratory and initial results are presented. The significant increase in signal to noise ratio, which the HEIFTS optical design promises over conventional hyperspectral imaging schemes, has been simulated, and results will be discussed. A Phase II system is being prepared for initial field deployment, and will be described.

  5. High resolution emission tomography; Tomographie d`emission haute resolution

    Energy Technology Data Exchange (ETDEWEB)

    Charon, Y.; Laniece, P.; Mastrippolito, R.; Pinot, L.; Ploux, L.; Valda Ochoa, A.; Valentin, L. [Groupe I.P.B., Experimental Research Division, Inst. de Physique Nucleaire, Paris-11 Univ., 91 - Orsay (France)

    1999-11-01

    We have developed an original high resolution tomograph for in-vivo small animal imaging. A first prototype is under evaluation. Initial results of its characterisation are presented. (authors) 3 figs.

  6. A high-efficiency spin-resolved photoemission spectrometer combining time-of-flight spectroscopy with exchange-scattering polarimetry

    Energy Technology Data Exchange (ETDEWEB)

    Jozwiak, Chris M.; Graff, Jeff; Lebedev, Gennadi; Andresen, Nord; Schmid, Andreas; Fedorov, Alexei; El Gabaly, Farid; Wan, Weishi; Lanzara, Alessandra; Hussain, Zahid

    2010-04-13

    We describe a spin-resolved electron spectrometer capable of uniquely efficient and high energy resolution measurements. Spin analysis is obtained through polarimetry based on low-energy exchange scattering from a ferromagnetic thin-film target. This approach can achieve a similar analyzing power (Sherman function) as state-of-the-art Mott scattering polarimeters, but with as much as 100 times improved efficiency due to increased reflectivity. Performance is further enhanced by integrating the polarimeter into a time-of-flight (TOF) based energy analysis scheme with a precise and flexible electrostatic lens system. The parallel acquisition of a range of electron kinetic energies afforded by the TOF approach results in an order of magnitude (or more) increase in efficiency compared to hemispherical analyzers. The lens system additionally features a 90 degrees bandpass filter, which by removing unwanted parts of the photoelectron distribution allows the TOF technique to be performed at low electron drift energy and high energy resolution within a wide range of experimental parameters. The spectrometer is ideally suited for high-resolution spin- and angle-resolved photoemission spectroscopy (spin-ARPES), and initial results are shown. The TOF approach makes the spectrometer especially ideal for time-resolved spin-ARPES experiments.

  7. High Resolution Infrared Spectroscopy of Allene -D4.

    Science.gov (United States)

    Rousan, Khetam Ibrahim Khasawinah

    Two parallel bands of allene-d(,4), (nu)(,6) (occurring at 1920.2289 cm('-1)) and (nu)(,5) (occurring at 2228.4133 cm('-1)), and the perpendicular band, (nu)(,8) (occurring at 2321.2484 cm('-1)), were recorded by using two spectrometers under high resolution. The combination band, (nu)(,2) + (nu)(,7), was measured also; the band origin is located at 2276.0053 cm('-1), rather distant from the previously reported one at 2267.0 cm('-1). Initially, by using the 4.5 m grating spectrometer, deconvolution of the spectra achieved a resolution of (TURN)0.007 cm('-1). Although the resolution was high, a detailed analysis of the K structure could not be obtained. Other measurements were carried out by using a BOMEM Fourier transform spectrometer. Deconvolution of the spectra achieved a resolution of (TURN)0.002 cm(' -1). This made it possible to resolve and analyze these bands in detail. Successful ground state and upper state analyses were completed from this data. Combining all the three bands together, a ground state analysis has resulted in better values of. (DIAGRAM, TABLE OR GRAPHIC OMITTED...PLEASE SEE DAI). than the previously published works on the same molecule by others. A set of accurate spectroscopic constants was obtained for each band. The spectrum of the (nu)(,8) band was analyzed in detail, including the perturbations. The perturbed states for (nu)(,8) were assigned as 2(nu)(,9) + (nu)(,10), (nu)(,2) + (nu)(,9) + (nu)(,11) and 2(nu)(,3) + (nu)(,4), and the spectroscopic constants for those perturbed states were calculated.

  8. High-grade, compact spectrometers for Earth observation from SmallSats

    Science.gov (United States)

    van der Wal, L. F.; de Goeij, B. T. G.; Jansen, R.; Oosterling, J. A. J.; Snijders, B.

    2016-10-01

    The market for nano- and microsatellites is developing rapidly. There is a strong focus on 2D imaging of the Earth's surface, with limited possibilities to obtain spectral information. More demanding applications, such as monitoring trace gases, aerosols or water quality still require advanced imaging instruments, which are large, heavy and expensive. In recent years TNO has investigated and developed different innovative designs to realize advanced spectrometers for space applications in a more compact and cost-effective manner. This offers multiple advantages: a compact instrument can be flown on a much smaller platform (nano- or microsatellite); a low-cost instrument opens up the possibility to fly multiple instruments in a satellite constellation, improving both global coverage and temporal sampling (e.g. to study diurnal processes); a constellation of low-cost instruments may provide added value to the larger scientific and operational satellite missions (e.g. the Copernicus Sentinel missions); and a small, lightweight spectrometer can also be mounted easily on a high-altitude UAV (offering high spatial resolution). Last but not least, a low-cost instrument may allow to break through the `cost spiral': lower cost will allow to take more risk and thus progress more quickly. This may lead to a much faster development cycle than customary for current Earth Observation instruments. To explore the potential of a constellation of low-cost instruments a consortium of Dutch partners was formed, which currently consists of Airbus Defence and Space Netherlands, ISISpace, S and T and TNO. In this paper we will illustrate this new design approach by using the most advanced design of a hyperspectral imaging spectrometer (named `Spectrolite') as an example. We will discuss the different design and manufacturing techniques that were used to realize this compact and low-cost design. Laboratory tests as well as the first preliminary results of airborne measurements with the

  9. A high efficiency spectrometer for reflection (e,2e) experiments at surfaces

    Energy Technology Data Exchange (ETDEWEB)

    Liscio, A. [CNR - IMIP, Area della Ricerca di Roma, Via Salaria km 29.300, 00016 Monterotondo (Italy); Dip.to di Fisica Universita di Roma Tre, Via Vasca Navale 84, 00146 Roma (Italy); Ruocco, A.; Stefani, G. [Dip.to di Fisica Universita di Roma Tre, Via Vasca Navale 84, 00146 Roma (Italy); Iacobucci, S. [CNR - ISC, Area della Ricerca di Roma, Via Salaria km 29.300, 00016 Monterotondo (Italy)], E-mail: stefano.iacobucci@isc.cnr.it

    2007-10-15

    To study electron momentum densities in solids by grazing angle reflection kinematics has been shown to be feasible [S. Iacobucci, S. Rioual, A. Ruocco, M. Mastropietro, G. Stefani, Surf. Sci. 454 (2000) 1026], but development of this spectroscopy has been hampered by long acquisition time; to fully exploit potentialities of this method is mandatory to reduce duration of the experiment within times comparable with clean surface lifetimes in ultra-high vacuum. This paper reports on recent developments of the reflection (e,2e) spectrometer that make a sizeable step forward in attaining this goal. It operates in asymmetric kinematics and at small grazing angle, thus allowing to enhance the surface sensitivity. A drastic reduction in acquisition time has been achieved by implementing parallel acquisition, both in energy and angle, of the detected electron pairs. To achieve parallel acquisition in energy and momentum, each of the two electron analysers is equipped with a two-dimensional position sensitive detector. A custom-made electronic hardware and software have been developed for the automatic control of the experiment and for acquisition and storage of the coincidence events. After discussing in some details the relevant features of the new spectrometer, few examples of valence band mapping and electron momentum densities measured in highly oriented pyrolitic graphite with energy and momentum resolutions of 1.3 eV and 0.15 A{sup -1} are given.

  10. VT Hydrography Dataset - High Resolution NHD

    Data.gov (United States)

    Vermont Center for Geographic Information — (Link to Metadata) The Vermont Hydrography Dataset (VHD) is compliant with the local resolution (also known as High Resolution) National Hydrography Dataset (NHD)...

  11. High-resolution infrared imaging

    Science.gov (United States)

    Falco, Charles M.

    2010-08-01

    The hands and mind of an artist are intimately involved in the creative process of image formation, intrinsically making paintings significantly more complex than photographs to analyze. In spite of this difficulty, several years ago the artist David Hockney and I identified optical evidence within a number of paintings that demonstrated artists began using optical projections as early as c1425 - nearly 175 years before Galileo - as aids for producing portions of their images. In the course of our work, Hockney and I developed insights that I have been applying to a new approach to computerized image analysis. Recently I developed and characterized a portable high resolution infrared for capturing additional information from paintings. Because many pigments are semi-transparent in the IR, in a number of cases IR photographs ("reflectograms") have revealed marks made by the artists that had been hidden under paint ever since they were made. I have used this IR camera to capture photographs ("reflectograms") of hundreds of paintings in over a dozen museums on three continents and, in some cases, these reflectograms have provided new insights into decisions the artists made in creating the final images that we see in the visible.

  12. ONE-DIMENSIONAL LIGHT BEAM WIDENING USING PRISMS FOR INCREASE OF SPECTROMETER SPECTRAL RESOLUTION AND ANGULAR DISPERSION

    Directory of Open Access Journals (Sweden)

    I. M. Gulis

    2016-01-01

    Full Text Available The increase of angular dispersion and slit resolution limit of grating spectrometers by means of variation of grating parameters is limited by its period and allowable order of diffraction. The special solutions (echelle, holographic, immersion gratings are acceptable in a limited parameter range and are technologically complex in fabrication, thus hardly applicable to instruments of mass production. We propose to decrease slit resolution limit by one-dimensional beam widening in dispersion plane by means of passing it through oblique prism before incidence onto diffraction grating. The increase of angular dispersion can be achieved by narrowing of dispersed beams after grating while passing through other oblique prism. We prove that slit resolution limit in such a system changes approximately as multiplied by angular magnification of the first prism (that is less than 1 times. Also angular dispersion changed approximately as multiplied by angular magnification of the second prism. The Fresnel reflection from the faces of prisms is analyzed. Accounting for that factor gives the increase of resolution about 1,4–1,6 times without loss of light (and can be 2 and more times while using anti-reflective coating. The proposed method is different from the similar ones first of all by its simplicity because it uses simple optical elements – plane reflective grating and thin prisms. It can be applied to amend the analytical characteristics of dispersive spectrometers, first of all the small-sized ones. 

  13. Application of high-resolution MS for development of peptide and large-molecule drug candidates.

    Science.gov (United States)

    Kellie, John F; Kehler, Jonathan R; Szapacs, Matthew E

    2016-02-01

    For quantitative bioanalysis utilizing MS, the instrument of choice is typically a triple quadruple mass spectrometer. However, advances in high-resolution MS have allowed sensitivity and dynamic ranges to approach that of triple quadrupole instruments. A matrix-free protein digest, a digested therapeutic protein and the intact peptide therapeutic liraglutide were each analyzed on high-resolution and triple quadrupole mass spectrometers with data compared. Samples from a mouse PK study with liraglutide were analyzed using the two different instruments, and equivalent PK exposure data were demonstrated. High-resolution and triple quadrupole mass spectrometers can generate data resulting in identical PK parameters from an in-life sample set, thus giving confidence in either technique in support of biotherapeutic PK exposure studies.

  14. A High-Efficiency Electron Momentum Spectrometer for Direct Imaging of Orbital Electron Density

    Institute of Scientific and Technical Information of China (English)

    REN Xue-Guang; NING Chuan-Gang; DENG Jing-Kang; ZHANG Shu-Feng; SU Guo-Lin; LI Bin; CHEN Xue-Jun

    2005-01-01

    @@ Direct three-dimensional images for orbital electron density are obtained by using our newly developed electron momentum spectrometer with simultaneous detection in energy and momentum, and the instruments resolutions of Aθ = ±0.7°, △φ = ±1.9°, △E = 1.2 eV, and △T = 2.0ns. The detection efficiency is about 100 times higher than conventional spectrometers. The design and performance of the apparatus are reported together with the experimental results on argon to show the extensive improvements in experimental resolutions, detection efficiency and versatility.

  15. High-resolution neutron tomography

    Energy Technology Data Exchange (ETDEWEB)

    Mikerov, V.I. [P.N. Lebedev Physical Inst., RAN, Moscow (Russian Federation); Zhitnik, I.A. [P.N. Lebedev Physical Inst., RAN, Moscow (Russian Federation); Ignat`ev, A.P. [P.N. Lebedev Physical Inst., RAN, Moscow (Russian Federation); Isakov, A.I. [P.N. Lebedev Physical Inst., RAN, Moscow (Russian Federation); Korneev, V.V. [P.N. Lebedev Physical Inst., RAN, Moscow (Russian Federation); Krutov, V.V. [P.N. Lebedev Physical Inst., RAN, Moscow (Russian Federation); Kuzin, S.V. [P.N. Lebedev Physical Inst., RAN, Moscow (Russian Federation); Oparin, S.N. [P.N. Lebedev Physical Inst., RAN, Moscow (Russian Federation); Pertsov, A.A. [P.N. Lebedev Physical Inst., RAN, Moscow (Russian Federation); Podolyak, E.R. [P.N. Lebedev Physical Inst., RAN, Moscow (Russian Federation); Sobel`man, I.I. [P.N. Lebedev Physical Inst., RAN, Moscow (Russian Federation); Tindo, I.P. [P.N. Lebedev Physical Inst., RAN, Moscow (Russian Federation); Tukarev, B.A. [P.N. Lebedev Physical Inst., RAN, Moscow (Russian Federation)

    1995-12-31

    A neutron tomography technique with a coordinate resolution of several tens of micrometers has been developed. Our results indicate that the technique resolves details with dimensions less than 100 {mu}m and measures a linear attenuation of less than {approx} 0.1 cm{sup -1}. Tomograms can be reconstructed using incomplete data. Limits on the resolution of the restored pattern are analyzed, and ways to improve the sensitivity of the technique are discussed. (orig.).

  16. CUSB-II: A high precision electromagnetic spectrometer

    Energy Technology Data Exchange (ETDEWEB)

    Schamberger, R.D.; Heintz, U.; Lee-Franzini, J.; Lovelock, D.M.J.; Narain, M.; Willins, J.; Yanagisawa, C. (SUNY, Stony Brook, NY (United States)); Tuts, P.M.; Franzini, P.; Kanekal, S.; Wu, Q.W. (Columbia Univ., New York, NY (United States))

    1991-11-15

    The design, construction and performance of a very compact precision electromagnetic spectrometer is described. The CUSB-II detectors has been used to study {gamma} spectroscopy, search for exotic particles and measure properties of the B and B{sup *} mesons at the Cornell Electron Storage Ring. (orig.).

  17. High-resolution absorption measurements of NH3 at high temperatures: 2100–5500 cm−1

    DEFF Research Database (Denmark)

    Barton, Emma J.; Yurchenko, Sergei N.; Tennyson, Jonathan

    2017-01-01

    High-resolution absorption spectra of NH3 in the region 2100–5500 cm−1 at 1027 °C and approximately atmospheric pressure (1045±3 mbar) are measured. An NH3 concentration of 10% in volume fraction is used in the measurements. Spectra are recorded in a high-temperature gas-flow cell using a Fourier...... Transform Infrared (FTIR) spectrometer at a nominal resolution of 0.09 cm−1. The spectra are analysed by comparison to a variational line list, BYTe, and experimental energy levels determined using the MARVEL procedure. 2308 lines have been assigned to 45 different bands, of which 1755 and 15 have been...

  18. SPIDER Progress Towards High Resolution Correlated Fission Product Data

    Science.gov (United States)

    Shields, Dan; Meierbachtol, Krista; Tovesson, Fredrik; Arnold, Charles; Blackeley, Rick; Bredeweg, Todd; Devlin, Matt; Hecht, Adam; Jandel, Marian; Jorgenson, Justin; Nelson, Ron; White, Morgan; Spider Team

    2014-09-01

    The SPIDER detector (SPectrometer for Ion DEtermination in fission Research) is under development with the goal of obtaining high-resolution, high-efficiency, correlated fission product data needed for many applications including the modeling of next generation nuclear reactors, stockpile stewardship, and the fundamental understanding of the fission process. SPIDER simultaneously measures velocity and energy of both fission products to calculate fission product yields (FPYs), neutron multiplicity (ν), and total kinetic energy (TKE). A detailed description of the prototype SPIDER detector components will be presented. Characterization measurements with alpha and spontaneous fission sources will also be discussed. LA-UR-14-24875. The SPIDER detector (SPectrometer for Ion DEtermination in fission Research) is under development with the goal of obtaining high-resolution, high-efficiency, correlated fission product data needed for many applications including the modeling of next generation nuclear reactors, stockpile stewardship, and the fundamental understanding of the fission process. SPIDER simultaneously measures velocity and energy of both fission products to calculate fission product yields (FPYs), neutron multiplicity (ν), and total kinetic energy (TKE). A detailed description of the prototype SPIDER detector components will be presented. Characterization measurements with alpha and spontaneous fission sources will also be discussed. LA-UR-14-24875. This work is in part supported by LANL Laboratory Directed Research and Development Projects 20110037DR and 20120077DR.

  19. Cavity Enhanced Optical Vernier Spectroscopy, Broad Band, High Resolution, High Sensitivity

    CERN Document Server

    Gohle, Christoph; Schliesser, Albert; Udem, Thomas; Hänsch, Theodor W

    2007-01-01

    A femtosecond frequency comb provides a vast number of equidistantly spaced narrow band laser modes that can be simultaneously tuned and frequency calibrated with 15 digits accuracy. Our Vernier spectrometer utilizes all of theses modes in a massively parallel manner to rapidly record both absorption and dispersion spectra with a sensitivity that is provided by a high finesse broad band optical resonator and a resolution that is only limited by the frequency comb line width while keeping the required setup simple.

  20. Temperature-dependent high resolution absorption cross sections of propane

    Science.gov (United States)

    Beale, Christopher A.; Hargreaves, Robert J.; Bernath, Peter F.

    2016-10-01

    High resolution (0.005 cm-1) absorption cross sections have been measured for pure propane (C3H8). These cross sections cover the 2550-3500 cm-1 region at five temperatures (from 296 to 700 K) and were measured using a Fourier transform spectrometer and a quartz cell heated by a tube furnace. Calibrations were made by comparison to the integrated cross sections of propane from the Pacific Northwest National Laboratory. These are the first high resolution absorption cross sections of propane for the 3 μm region at elevated temperatures. The cross sections provided may be used to monitor propane in combustion environments and in astronomical sources such as the auroral regions of Jupiter, brown dwarfs and exoplanets.

  1. Miniature anastigmatic spectrometer design with a concave toroidal mirror.

    Science.gov (United States)

    Dong, Jianing; Chen, He; Zhang, Yinchao; Chen, Siying; Guo, Pan

    2016-03-01

    An advanced optical design for a low-cost and astigmatism-corrected spectrometer with a high resolution is presented. The theory and method of astigmatism correction are determined with the use of a concave toroidal mirror. The performances of a modified spectrometer and a traditional spectrometer are compared, and the analysis is verified. Experimentally, the limiting resolution of our spectrometer is 0.1 nm full width at half-maximum, as measured for 579.1 nm.

  2. High precision pointing with a multiline spectrometer at the VTT

    Science.gov (United States)

    Staiger, J.

    2012-12-01

    We are investigating the pointing quality of the VTT, Tenerife under the aspect of suitability for long-term heliosesimological observations. Tests have shown that thermal and mechanical loads within the telescope may create spurious image drifts with shift rates of up to 5 arcsec per hour. During daylong recordings this will reduce significantly the effective size of the field-of-view and may infer artificial lateral movements into the data. The underlying problem that not all image position offsets developing during a measurement may be compensated for is common to most high-resolution solar telescopes independently of the type of pointing system used. We are developing new approaches to address this problem which are to be tested in the near future at the VTT. The simulations established so far show that the problem may be reduced by more than 90 %.

  3. Scintillating Fiber Technology for a High Neutron Spectrometer

    Science.gov (United States)

    Kuznetsov, Evgeny; Adams, James, Jr.; Christl, Mark; Norwood, Joseph; Watts, John

    2014-01-01

    Develop a compact low-power neutron spectrometer that uniquely identifies neutrons in the mixed radiation field expected on crewed deep-space missions. Secondary neutrons are generated by cosmic rays striking heavy crewed spacecraft as well as lunar and planetary surfaces1,2. It has been shown that secondary neutrons can account for up to 50% if the total dose-equivalent received by the crew.

  4. High-resolution electron microscopy

    CERN Document Server

    Spence, John C H

    2013-01-01

    This new fourth edition of the standard text on atomic-resolution transmission electron microscopy (TEM) retains previous material on the fundamentals of electron optics and aberration correction, linear imaging theory (including wave aberrations to fifth order) with partial coherence, and multiple-scattering theory. Also preserved are updated earlier sections on practical methods, with detailed step-by-step accounts of the procedures needed to obtain the highest quality images of atoms and molecules using a modern TEM or STEM electron microscope. Applications sections have been updated - these include the semiconductor industry, superconductor research, solid state chemistry and nanoscience, and metallurgy, mineralogy, condensed matter physics, materials science and material on cryo-electron microscopy for structural biology. New or expanded sections have been added on electron holography, aberration correction, field-emission guns, imaging filters, super-resolution methods, Ptychography, Ronchigrams, tomogr...

  5. DESIR high resolution separator at GANIL, France

    Directory of Open Access Journals (Sweden)

    Toprek Dragan

    2012-01-01

    Full Text Available A high-resolution separator for the SPIRAL2/DESIR project at GANIL has been designed. The extracted isotopes from SPIRAL2 will be transported to and cooled in a RFQ cooler yielding beams with very low transverse emittance and energy spread. These beams will then be accelerated to 60 keV and sent to a high-resolution mass separator where a specific isotope will be selected. The good beam properties extracted from the RFQ cooler will allow one to obtain a mass resolution of č26000 with the high-resolution mass separator.

  6. Highly miniaturized laser ablation time-of-flight mass spectrometer for a planetary rover

    Science.gov (United States)

    Rohner, Urs; Whitby, James A.; Wurz, Peter; Barabash, Stas

    2004-05-01

    We report the development and testing of a highly miniaturized mass spectrometer and ion source intended to be deployed on an airless planetary surface to measure the elemental and isotopic composition of solids, e.g., rocks and soils. Our design concentrates at this stage on the proposed BepiColombo mission to the planet Mercury. The mass analyzer is a novel combination of an electrostatic analyzer and a reflectron time-of-flight design. The ion source utilizes a laser induced plasma, which is directly coupled into the mass analyzer. Laser ablation gives high spatial resolution and avoids the need for sample preparation. Our prototype instrument has a demonstrated mass resolution m/Δm full width at half maximum in excess of 180 and a predicted dynamic range of better than five orders of magnitude. We estimate that a flight instrument would have a mass of 280 g (including laser and all electronics), a volume of 84 cm3, and could operate on 3 W power.

  7. A High-Throughput, Arbitrary-Waveform, MPI Spectrometer and Relaxometer for Comprehensive Magnetic Particle Optimization and Characterization

    Science.gov (United States)

    Tay, Zhi Wei; Goodwill, Patrick W.; Hensley, Daniel W.; Taylor, Laura A.; Zheng, Bo; Conolly, Steven M.

    2016-09-01

    Magnetic Particle Imaging (MPI) is a promising new tracer modality with zero attenuation deep in tissue, high contrast and sensitivity, and an excellent safety profile. However, the spatial resolution of MPI is limited to around 1 mm currently and urgently needs to be improved for clinical applications such as angiography and brain perfusion. Although MPI resolution is highly dependent on tracer characteristics and the drive waveforms, optimization is limited to a small subset of possible excitation strategies by current MPI hardware that only does sinusoidal drive waveforms at very few frequencies. To enable a more comprehensive and rapid optimization of drive waveforms for multiple metrics like resolution and signal strength simultaneously, we demonstrate the first untuned MPI spectrometer/relaxometer with unprecedented 400 kHz excitation bandwidth and capable of high-throughput acquisition of harmonic spectra (100 different drive-field frequencies in only 500 ms). It is also capable of arbitrary drive-field waveforms which have not been experimentally evaluated in MPI to date. Its high-throughput capability, frequency-agility and tabletop size makes this Arbitrary Waveform Relaxometer/Spectrometer (AWR) a convenient yet powerfully flexible tool for nanoparticle experts seeking to characterize magnetic particles and optimize MPI drive waveforms for in vitro biosensing and in vivo imaging with MPI.

  8. A High-Throughput, Arbitrary-Waveform, MPI Spectrometer and Relaxometer for Comprehensive Magnetic Particle Optimization and Characterization

    Science.gov (United States)

    Tay, Zhi Wei; Goodwill, Patrick W.; Hensley, Daniel W.; Taylor, Laura A.; Zheng, Bo; Conolly, Steven M.

    2016-01-01

    Magnetic Particle Imaging (MPI) is a promising new tracer modality with zero attenuation deep in tissue, high contrast and sensitivity, and an excellent safety profile. However, the spatial resolution of MPI is limited to around 1 mm currently and urgently needs to be improved for clinical applications such as angiography and brain perfusion. Although MPI resolution is highly dependent on tracer characteristics and the drive waveforms, optimization is limited to a small subset of possible excitation strategies by current MPI hardware that only does sinusoidal drive waveforms at very few frequencies. To enable a more comprehensive and rapid optimization of drive waveforms for multiple metrics like resolution and signal strength simultaneously, we demonstrate the first untuned MPI spectrometer/relaxometer with unprecedented 400 kHz excitation bandwidth and capable of high-throughput acquisition of harmonic spectra (100 different drive-field frequencies in only 500 ms). It is also capable of arbitrary drive-field waveforms which have not been experimentally evaluated in MPI to date. Its high-throughput capability, frequency-agility and tabletop size makes this Arbitrary Waveform Relaxometer/Spectrometer (AWR) a convenient yet powerfully flexible tool for nanoparticle experts seeking to characterize magnetic particles and optimize MPI drive waveforms for in vitro biosensing and in vivo imaging with MPI. PMID:27686629

  9. High Resolution Silicon Deformable Mirrors Project

    Data.gov (United States)

    National Aeronautics and Space Administration — This proposal describes a plan to build a prototype small stroke, high precision deformable mirror suitable for space-based operation in systems for high-resolution...

  10. Broadening of a spectrum line by finite spectrometer resolution. [FORTRAN IV; SAL, KAL

    Energy Technology Data Exchange (ETDEWEB)

    Engleman, R. Jr.

    1978-12-01

    The distortion of a spectrum line by the finite resolving power of a spectrometer is discussed in terms of a mathematical model. Particular attention is given to the case where either a Gaussian or Cauchy slit function broadens an isolated Doppler, Lorentz, or Voigt absorption line. Corrections to the peak absorption, the line width, and the integrated absorption coefficient are calculated and discussed for different combinations of slit functions and line shapes. Several new series expansions for the corrections are derived. Two general FORTRAN IV programs that calculate these corrections are described and some sample correction curves are given. 27 references.

  11. High-energy x-ray imaging spectrometer (HEXIS)

    Science.gov (United States)

    Matteson, James L.; Gruber, Duane E.; Heindl, William A.; Pelling, Michael R.; Peterson, Laurence E.; Rothschild, Richard E.; Skelton, Robert E.; Hink, Paul L.; Slavis, Kimberly R.; Binns, W. Robert

    1998-11-01

    HEXIS is a MIDEX-class mission concept for x-ray astronomy. Its objectives are to improve our knowledge of the high energy x-ray sky by increasing the number of sources above 20 keV to > 2,000, discovering transient sources such as x-ray novae and gamma-ray bursts, and making spectral and temporal studies of the sources. With mission life > 3 years, a 1-year all-sky survey sensitivity of approximately 0.3 mCrab, and continuous monitoring of the entire visible sky, HEXIS will provide unprecedented capabilities. Source positions will be determined to accuracies of a few arcmin or better. Spectra will be determined with an energy resolution of a few keV and source variability will be studied on time scales from CZT detectors operating from approximately 5 keV to 200 keV. Detector planes are built with 41 cm(superscript 2) CZT detector modules which employ crossed-strip readout to obtain a pixel size of 0.5 mm. Nine modules are grouped in a 369 cm(superscript 2) array for each imager. In the past 2 years significant progress has been made on techniques requires for HEXIS: position-sensitive CZT detectors and ASIC readout, coded mask imaging, and background properties at balloon altitudes. Scientific and technical details of HEXIS are presented together with result form tests of detectors and a coded mask imager.

  12. High Resolution Spectroscopic Study of $^{10}_{\\Lambda}$Be

    CERN Document Server

    Gogami, T; Kawama, D; Achenbach, P; Ahmidouch, A; Albayrak, I; Androic, D; Asaturyan, A; Asaturyan, R; Ates, O; Baturin, P; Badui, R; Boeglin, W; Bono, J; Brash, E; Carter, P; Chiba, A; Christy, E; Danagoulian, S; De Leo, R; Doi, D; Elaasar, M; Ent, R; Fujii, Y; Fujita, M; Furic, M; Gabrielyan, M; Gan, L; Garibaldi, F; Gaskell, D; Gasparian, A; Han, Y; Hashimoto, O; Horn, T; Hu, B; Hungerford, Ed V; Jones, M; Kanda, H; Kaneta, M; Kato, S; Kawai, M; Khanal, H; Kohl, M; Liyanage, A; Luo, W; Maeda, K; Margaryan, A; Markowitz, P; Maruta, T; Matsumura, A; Maxwell, V; Mkrtchyan, A; Mkrtchyan, H; Nagao, S; Nakamura, S N; Narayan, A; Neville, C; Niculescu, G; Niculescu, M I; Nunez, A; Nuruzzaman,; Okayasu, Y; Petkovic, T; Pochodzalla, J; Qiu, X; Reinhold, J; Rodriguez, V M; Samanta, C; Sawatzky, B; Seva, T; Shichijo, A; Tadevosyan, V; Tang, L; Taniya, N; Tsukada, K; Veilleux, M; Vulcan, W; Wesselmann, F R; Wood, S A; Yamamoto, T; Ya, L; Ye, Z; Yokota, K; Yuan, L; Zhamkochyan, S; Zhu, L

    2015-01-01

    A spectroscopy of a $^{10}_{\\Lambda}$Be hypernucleus was carried out at JLab Hall C using the $(e,e^{\\prime}K^{+})$ reaction. A new magnetic spectrometer system (SPL+HES+HKS), specifically designed for high resolution hypernuclear spectroscopy, was used to obtain an energy spectrum with a resolution of 0.78 MeV (FWHM). The well-calibrated spectrometer system of the present experiment using the $p(e,e^{\\prime}K^{+})\\Lambda,\\Sigma^{0}$ reactions allowed us to determine the energy levels, and the binding energy of the ground state peak (mixture of 1$^{-}$ and 2$^{-}$ states) was obtained to be B$_{\\Lambda}$=8.55$\\pm$0.07(stat.)$\\pm$0.11(sys.) MeV. The result indicates that the ground state energy is shallower than that of an emulsion study by about 0.5 MeV which provides valuable experimental information on Charge Symmetry Breaking (CSB) effect in the $\\Lambda N$ interaction.

  13. Dewar cooler integrated MWIR spectrometer for high rates and high dynamic range measurements

    Science.gov (United States)

    Guérineau, N.; Rommeluère, S.; Ferrec, Y.; Druart, G.; Lasfargues, G.; de Borniol, E.; Magli, S.

    2015-06-01

    There is a need for compact, hand-held, spectrometers for the measurement of spectral signatures of chemicals or objects. To achieve this goal, a new concept of Fourier-transform interferometer (FTIR) directly integrated on the infrared focal plane array (FPA) has been developed at ONERA. The fundamental properties of this key element called MICROSPOC will be recalled and we will see how those properties can be exploited to get a snapshot, compact and cryogenic MWIR spectrometer. These design rules have been applied to develop a very compact device that combines the metrological properties of a FTIR-FPA of quantum HgCdTe technology with the radiometric performances of a last generation Sofradir detection block (Infrared Detector Dewar Cooler Assembly - IDDCA). The experimental performances of the prototype will be presented, in terms of spectral resolution, acquisition rate, dynamic range and noise equivalent spectral radiance. We will discuss at the end the potential of this technology to meet the requirements of different applications.

  14. High-Resolution Data for a Low-Resolution World

    Energy Technology Data Exchange (ETDEWEB)

    Brady, Brendan Williams [Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

    2016-05-10

    In the past 15 years, the upper section of Cañon de Valle has been severely altered by wildfires and subsequent runoff events. Loss of root structures on high-angle slopes results in debris flow and sediment accumulation in the narrow canyon bottom. The original intent of the study described here was to better understand the changes occurring in watershed soil elevations over the course of several post-fire years. An elevation dataset from 5 years post-Cerro Grande fire was compared to high-resolution LiDAR data from 14 years post-Cerro Grande fire (also 3 years post-Las Conchas fire). The following analysis was motivated by a problematic comparison of these datasets of unlike resolution, and therefore focuses on what the data reveals of itself. The objective of this study is to highlight the effects vegetation can have on remote sensing data that intends to read ground surface elevation.

  15. High performance gamma-ray spectrometer for runaway electron studies on the FT-2 tokamak

    Science.gov (United States)

    Shevelev, A. E.; Khilkevitch, E. M.; Lashkul, S. I.; Rozhdestvensky, V. V.; Altukhov, A. B.; Chugunov, I. N.; Doinikov, D. N.; Esipov, L. A.; Gin, D. B.; Iliasova, M. V.; Naidenov, V. O.; Nersesyan, N. S.; Polunovsky, I. A.; Sidorov, A. V.; Kiptily, V. G.

    2016-09-01

    A gamma-ray spectrometer based on LaBr3(Ce) scintillator has been used for measurements of hard X-ray emission generated by runaway electrons in the FT-2 tokamak plasmas. Using of the fast LaBr3(Ce) has allowed extending count rate range of the spectrometer by a factor of 10. A developed digital processing algorithm of the detector signal recorded with a digitizer sampling rate of 250 MHz has provided a pulse height analysis at count rates up to 107 s-1. A spectrum deconvolution code DeGaSum has been applied for inferring the energy distribution of runaway electrons escaping from the plasma and interacting with materials of the FT-2 limiter in the vacuum chamber. The developed digital signal processing technique for LaBr3(Ce) spectrometer has allowed studying the evolution of runaways energy distribution in the FT-2 plasma discharges with time resolution of 1-5 ms.

  16. A high etendue spectrometer suitable for core charge eXchange recombination spectroscopy on ITER.

    Science.gov (United States)

    Jaspers, R J E; Scheffer, M; Kappatou, A; van der Valk, N C J; Durkut, M; Snijders, B; Marchuk, O; Biel, W; Pokol, G I; Erdei, G; Zoletnik, S; Dunai, D

    2012-10-01

    A feasibility study for the use of core charge exchange recombination spectroscopy on ITER has shown that accurate measurements on the helium ash require a spectrometer with a high etendue of 1mm(2)sr to comply with the measurement requirements [S. Tugarinov et al., Rev. Sci. Instrum. 74, 2075 (2003)]. To this purpose such an instrument has been developed consisting of three separate wavelength channels (to measure simultaneously He/Be, C/Ne, and H/D/T together with the Doppler shifted direct emission of the diagnostic neutral beam, the beam emission (BES) signal), combining high dispersion (0.02 nm/pixel), sufficient resolution (0.2 nm), high efficiency (55%), and extended wavelength range (14 nm) at high etendue. The combined measurement of the BES along the same sightline within a third wavelength range provides the possibility for in situ calibration of the charge eXchange recombination spectroscopy signals. In addition, the option is included to use the same instrument for measurements of the fast fluctuations of the beam emission intensity up to 2 MHz, with the aim to study MHD activity.

  17. A high etendue spectrometer suitable for core charge eXchange recombination spectroscopy on ITER

    Energy Technology Data Exchange (ETDEWEB)

    Jaspers, R. J. E.; Scheffer, M. [Science and Technology of Nuclear Fusion, Eindhoven University of Technology, Eindhoven (Netherlands); Kappatou, A. [FOM Institute DIFFER - Dutch Institute for Fundamental Energy Research, Association EURATOM-FOM, Nieuwegein (Netherlands); Valk, N. C. J. van der; Durkut, M.; Snijders, B. [TNO Science and Industry, P.O. Box 155, 2600 AD Delft (Netherlands); Marchuk, O.; Biel, W. [Institut fuer Energie und Klimaforschung-IEK-4 Forschungszentrum, Juelich GmbH, 52425 Juelich (Germany); Pokol, G. I. [Institute of Nuclear Techniques, Budapest University of Technology and Economics, EURATOM Association, P. O. Box 91, H-1521 Budapest (Hungary); Erdei, G. [Department of Atomic Physics, Budapest University of Technology and Economics, EURATOM Association, P. O. Box 91, H-1521 Budapest (Hungary); Zoletnik, S.; Dunai, D. [WIGNER RCP, RMKI, EURATOM Association, P. O. Box 91, H-1521 Budapest (Hungary)

    2012-10-15

    A feasibility study for the use of core charge exchange recombination spectroscopy on ITER has shown that accurate measurements on the helium ash require a spectrometer with a high etendue of 1mm{sup 2}sr to comply with the measurement requirements [S. Tugarinov et al., Rev. Sci. Instrum. 74, 2075 (2003)]. To this purpose such an instrument has been developed consisting of three separate wavelength channels (to measure simultaneously He/Be, C/Ne, and H/D/T together with the Doppler shifted direct emission of the diagnostic neutral beam, the beam emission (BES) signal), combining high dispersion (0.02 nm/pixel), sufficient resolution (0.2 nm), high efficiency (55%), and extended wavelength range (14 nm) at high etendue. The combined measurement of the BES along the same sightline within a third wavelength range provides the possibility for in situ calibration of the charge eXchange recombination spectroscopy signals. In addition, the option is included to use the same instrument for measurements of the fast fluctuations of the beam emission intensity up to 2 MHz, with the aim to study MHD activity.

  18. High-resolution transmission measurements of CO2 at high temperatures for industrial applications

    DEFF Research Database (Denmark)

    Evseev, Vadim; Fateev, Alexander; Clausen, Sønnik

    2012-01-01

    . The spectra have been recorded in a high-temperature flow gas cell and using a Fourier transform infrared (FTIR) spectrometer at a nominal resolution of 0.125 cm-1. The volume fractions of CO2 in the measurements were 1,10 and 100%. The measurements have been validated by comparison with medium...

  19. High-resolution ionization detector and array of such detectors

    Energy Technology Data Exchange (ETDEWEB)

    McGregor, Douglas S. (Ypsilanti, MI); Rojeski, Ronald A. (Pleasanton, CA)

    2001-01-16

    A high-resolution ionization detector and an array of such detectors are described which utilize a reference pattern of conductive or semiconductive material to form interaction, pervious and measurement regions in an ionization substrate of, for example, CdZnTe material. The ionization detector is a room temperature semiconductor radiation detector. Various geometries of such a detector and an array of such detectors produce room temperature operated gamma ray spectrometers with relatively high resolution. For example, a 1 cm.sup.3 detector is capable of measuring .sup.137 Cs 662 keV gamma rays with room temperature energy resolution approaching 2% at FWHM. Two major types of such detectors include a parallel strip semiconductor Frisch grid detector and the geometrically weighted trapezoid prism semiconductor Frisch grid detector. The geometrically weighted detector records room temperature (24.degree. C.) energy resolutions of 2.68% FWHM for .sup.137 Cs 662 keV gamma rays and 2.45% FWHM for .sup.60 Co 1.332 MeV gamma rays. The detectors perform well without any electronic pulse rejection, correction or compensation techniques. The devices operate at room temperature with simple commercially available NIM bin electronics and do not require special preamplifiers or cooling stages for good spectroscopic results.

  20. Mu-Spec - A High Performance Ultra-Compact Photon Counting spectrometer for Space Submillimeter Astronomy

    Science.gov (United States)

    Moseley, H.; Hsieh, W.-T.; Stevenson, T.; Wollack, E.; Brown, A.; Benford, D.; Sadleir; U-Yen, I.; Ehsan, N.; Zmuidzinas, J.; Bradford, M.

    2011-01-01

    We have designed and are testing elements of a fully integrated submillimeter spectrometer based on superconducting microstrip technology. The instrument can offer resolving power R approximately 1500, and its high frequency cutoff is set by the gap of available high performance superconductors. All functions of the spectrometer are integrated - light is coupled to the microstrip circuit with a planar antenna, the spectra discrimination is achieved using a synthetic grating, orders are separated using planar filter, and detected using photon counting MKID detector. This spectrometer promises to revolutionize submillimeter spectroscopy from space. It replaces instruments with the scale of 1m with a spectrometer on a 10 cm Si wafer. The reduction in mass and volume promises a much higher performance system within available resource in a space mission. We will describe the system and the performance of the components that have been fabricated and tested.

  1. High-resolution absorption cross sections of C$_{2}$H$_{6}$ at elevated temperatures

    OpenAIRE

    2015-01-01

    Infrared absorption cross sections near 3.3 $\\mu$m have been obtained for ethane, C$_{2}$H$_{6}$. These were acquired at elevated temperatures (up to 773 K) using a Fourier transform infrared spectrometer and tube furnace with a resolution of 0.005 cm$^{-1}$. The integrated absorption was calibrated using composite infrared spectra taken from the Pacific Northwest National Laboratory (PNNL). These new measurements are the first high-resolution infrared C$_{2}$H$_{6}$ cross sections at elevate...

  2. High resolution studies of massive primordial haloes

    CERN Document Server

    Latif, M A; Schmidt, W; Niemeyer, J

    2012-01-01

    Atomic cooling haloes with T_vir > 10^4 K are the most plausible sites for the formation of the first galaxies. In this article, we aim to study the implications of gravity driven turbulence in protogalactic haloes. By varying the resolution per Jeans length, we explore whether the turbulent cascade is resolved well enough to obtain converged results. We have performed high resolution cosmological simulations using the adaptive mesh refinement code Enzo including a subgrid-scale turbulence model to study the role of unresolved turbulence. We compared the results of three different Jeans resolutions from 16 to 64 cells. While radially averaged profiles roughly agree at different resolutions, differences in the morphology reveal that even the highest resolution employed provides no convergence. Moreover, taking into account unresolved turbulence significantly influences the morphology of a halo. We have quantified the properties of the high-density clumps in the halo. These clumps are gravitationally unbound wi...

  3. Multichannel emission spectrometer for high dynamic range optical pyrometry of shock-driven materials

    Science.gov (United States)

    Bassett, Will P.; Dlott, Dana D.

    2016-10-01

    An emission spectrometer (450-850 nm) using a high-throughput, high numerical aperture (N.A. = 0.3) prism spectrograph with stepped fiberoptic coupling, 32 fast photomultipliers and thirty-two 1.25 GHz digitizers is described. The spectrometer can capture single-shot events with a high dynamic range in amplitude and time (nanoseconds to milliseconds or longer). Methods to calibrate the spectrometer and verify its performance and accuracy are described. When a reference thermal source is used for calibration, the spectrometer can function as a fast optical pyrometer. Applications of the spectrometer are illustrated by using it to capture single-shot emission transients from energetic materials or reactive materials initiated by kmṡs-1 impacts with laser-driven flyer plates. A log (time) data analysis method is used to visualize multiple kinetic processes resulting from impact initiation of HMX (octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine) or a Zr/CuO nanolaminate thermite. Using a gray body algorithm to interpret the spectral radiance from shocked HMX, a time history of temperature and emissivity was obtained, which could be used to investigate HMX hot spot dynamics. Finally, two examples are presented showing how the spectrometer can avoid temperature determination errors in systems where thermal emission is accompanied by atomic or molecular emission lines.

  4. High-resolution XAS/XES analyzing electronic structures of catalysts

    CERN Document Server

    Sa, Jacinto

    2014-01-01

    Photon-in-photon-out core level spectroscopy is an emerging approach to characterize the electronic structure of catalysts and enzymes, and it is either installed or planned for intense synchrotron beam lines and X-ray free electron lasers. This type of spectroscopy requires high-energy resolution spectroscopy not only for the incoming X-ray beam but also, in most applications, for the detection of the outgoing photons. Thus, the use of high-resolution X-ray crystal spectrometers whose resolving power ?E/E is typically about 10-4, is mandatory.High-Resolution XAS/XES: Analyzing Electronic Stru

  5. Measurements with the high flux lead slowing-down spectrometer at LANL

    Energy Technology Data Exchange (ETDEWEB)

    Danon, Y. [Rensselaer Polytechnic Intstitute, 110 8th Street, Troy, NY 12180 (United States)]. E-mail: danony@rpi.edu; Romano, C. [Rensselaer Polytechnic Intstitute, 110 8th Street, Troy, NY 12180 (United States); Thompson, J. [Rensselaer Polytechnic Intstitute, 110 8th Street, Troy, NY 12180 (United States); Watson, T. [Rensselaer Polytechnic Intstitute, 110 8th Street, Troy, NY 12180 (United States); Haight, R.C. [Los Alamos National Laboratory, Los Alamos, NM 87545 (United States); Wender, S.A. [Los Alamos National Laboratory, Los Alamos, NM 87545 (United States); Vieira, D.J. [Los Alamos National Laboratory, Los Alamos, NM 87545 (United States); Bond, E. [Los Alamos National Laboratory, Los Alamos, NM 87545 (United States); Wilhelmy, J.B. [Los Alamos National Laboratory, Los Alamos, NM 87545 (United States); O' Donnell, J.M. [Los Alamos National Laboratory, Los Alamos, NM 87545 (United States); Michaudon, A. [Los Alamos National Laboratory, Los Alamos, NM 87545 (United States); Bredeweg, T.A. [Los Alamos National Laboratory, Los Alamos, NM 87545 (United States); Schurman, T. [Los Alamos National Laboratory, Los Alamos, NM 87545 (United States); Rochman, D. [Brookhaven National Laboratory National Nuclear Data Center (NNDC), Upton, NY 11973-5000 (United States); Granier, T. [CEA-DAM, BP 12, 91680 Bruyeres-le-Chatel (France); Ethvignot, T. [CEA-DAM, BP 12, 91680 Bruyeres-le-Chatel (France); Taieb, J. [CEA-DAM, BP 12, 91680 Bruyeres-le-Chatel (France); Becker, J.A. [Lawrence Livermore National Laboratory, Livermore, CA 94550 (United States)

    2007-08-15

    A Lead Slowing-Down Spectrometer (LSDS) was recently installed at LANL [D. Rochman, R.C. Haight, J.M. O'Donnell, A. Michaudon, S.A. Wender, D.J. Vieira, E.M. Bond, T.A. Bredeweg, A. Kronenberg, J.B. Wilhelmy, T. Ethvignot, T. Granier, M. Petit, Y. Danon, Characteristics of a lead slowing-down spectrometer coupled to the LANSCE accelerator, Nucl. Instr. and Meth. A 550 (2005) 397]. The LSDS is comprised of a cube of pure lead 1.2 m on the side, with a spallation pulsed neutron source in its center. The LSDS is driven by 800 MeV protons with a time-averaged current of up to 1 {mu}A, pulse widths of 0.05-0.25 {mu}s and a repetition rate of 20-40 Hz. Spallation neutrons are created by directing the proton beam into an air-cooled tungsten target in the center of the lead cube. The neutrons slow down by scattering interactions with the lead and thus enable measurements of neutron-induced reaction rates as a function of the slowing-down time, which correlates to neutron energy. The advantage of an LSDS as a neutron spectrometer is that the neutron flux is 3-4 orders of magnitude higher than a standard time-of-flight experiment at the equivalent flight path, 5.6 m. The effective energy range is 0.1 eV to 100 keV with a typical energy resolution of 30% from 1 eV to 10 keV. The average neutron flux between 1 and 10 keV is about 1.7 x 10{sup 9} n/cm{sup 2}/s/{mu}A. This high flux makes the LSDS an important tool for neutron-induced cross section measurements of ultra-small samples (nanograms) or of samples with very low cross sections. The LSDS at LANL was initially built in order to measure the fission cross section of the short-lived metastable isotope of U-235, however it can also be used to measure (n, {alpha}) and (n, p) reactions. Fission cross section measurements were made with samples of {sup 235}U, {sup 236}U, {sup 238}U and {sup 239}Pu. The smallest sample measured was 10 ng of {sup 239}Pu. Measurement of (n, {alpha}) cross section with 760 ng of Li-6 was also

  6. Measurements with the high flux lead slowing-down spectrometer at LANL

    Science.gov (United States)

    Danon, Y.; Romano, C.; Thompson, J.; Watson, T.; Haight, R. C.; Wender, S. A.; Vieira, D. J.; Bond, E.; Wilhelmy, J. B.; O'Donnell, J. M.; Michaudon, A.; Bredeweg, T. A.; Schurman, T.; Rochman, D.; Granier, T.; Ethvignot, T.; Taieb, J.; Becker, J. A.

    2007-08-01

    A Lead Slowing-Down Spectrometer (LSDS) was recently installed at LANL [D. Rochman, R.C. Haight, J.M. O'Donnell, A. Michaudon, S.A. Wender, D.J. Vieira, E.M. Bond, T.A. Bredeweg, A. Kronenberg, J.B. Wilhelmy, T. Ethvignot, T. Granier, M. Petit, Y. Danon, Characteristics of a lead slowing-down spectrometer coupled to the LANSCE accelerator, Nucl. Instr. and Meth. A 550 (2005) 397]. The LSDS is comprised of a cube of pure lead 1.2 m on the side, with a spallation pulsed neutron source in its center. The LSDS is driven by 800 MeV protons with a time-averaged current of up to 1 μA, pulse widths of 0.05-0.25 μs and a repetition rate of 20-40 Hz. Spallation neutrons are created by directing the proton beam into an air-cooled tungsten target in the center of the lead cube. The neutrons slow down by scattering interactions with the lead and thus enable measurements of neutron-induced reaction rates as a function of the slowing-down time, which correlates to neutron energy. The advantage of an LSDS as a neutron spectrometer is that the neutron flux is 3-4 orders of magnitude higher than a standard time-of-flight experiment at the equivalent flight path, 5.6 m. The effective energy range is 0.1 eV to 100 keV with a typical energy resolution of 30% from 1 eV to 10 keV. The average neutron flux between 1 and 10 keV is about 1.7 × 109 n/cm2/s/μA. This high flux makes the LSDS an important tool for neutron-induced cross section measurements of ultra-small samples (nanograms) or of samples with very low cross sections. The LSDS at LANL was initially built in order to measure the fission cross section of the short-lived metastable isotope of U-235, however it can also be used to measure (n, α) and (n, p) reactions. Fission cross section measurements were made with samples of 235U, 236U, 238U and 239Pu. The smallest sample measured was 10 ng of 239Pu. Measurement of (n, α) cross section with 760 ng of Li-6 was also demonstrated. Possible future cross section measurements

  7. High Resolution Silicon Deformable Mirrors Project

    Data.gov (United States)

    National Aeronautics and Space Administration — In this proposal we describe a plan to build a deformable mirror suitable for space-based operation in systems for high-resolution imaging. The prototype DM will be...

  8. High range resolution micro-Doppler analysis

    Science.gov (United States)

    Cammenga, Zachary A.; Smith, Graeme E.; Baker, Christopher J.

    2015-05-01

    This paper addresses use of the micro-Doppler effect and the use of high range-resolution profiles to observe complex targets in complex target scenes. The combination of micro-Doppler and high range-resolution provides the ability to separate the motion of complex targets from one another. This ability leads to the differentiation of targets based on their micro-Doppler signatures. Without the high-range resolution, this would not be possible because the individual signatures would not be separable. This paper also addresses the use of the micro-Doppler information and high range-resolution profiles to generate an approximation of the scattering properties of a complex target. This approximation gives insight into the structure of the complex target and, critically, is created without using a pre-determined target model.

  9. Structure of high-resolution NMR spectra

    CERN Document Server

    Corio, PL

    2012-01-01

    Structure of High-Resolution NMR Spectra provides the principles, theories, and mathematical and physical concepts of high-resolution nuclear magnetic resonance spectra.The book presents the elementary theory of magnetic resonance; the quantum mechanical theory of angular momentum; the general theory of steady state spectra; and multiple quantum transitions, double resonance and spin echo experiments.Physicists, chemists, and researchers will find the book a valuable reference text.

  10. The mid-infrared instrument for the James Webb Space Telescope: performance and operation of the Low-Resolution Spectrometer

    Science.gov (United States)

    Kendrew, Sarah; Scheithauer, Silvia; Bouchet, Patrice; Amiaux, Jerome; Azzollini, Ruymán.; Bouwman, Jeroen; Chen, Christine; Dubreuil, Didier; Fischer, Sebastian; Fox, Ori D.; Glasse, Alistair; Gordon, Karl; Greene, Tom; Hines, Dean C.; Lagage, Pierre-Olivier; Lahuis, Fred; Ronayette, Samuel; Wright, David; Wright, Gillian S.

    2016-07-01

    We describe here the performance and operational concept for the Low Resolution Spectrometer (LRS) of the mid-infrared instrument (MIRI) for the James Webb Space Telescope. The LRS will provide R˜100 slit and slitless spectroscopy from 5 to 12 micron, and its design is optimised for observations of compact sources, such as exoplanet host stars. We provide here an overview of the design of the LRS, and its performance as measured during extensive test campaigns, examining in particular the delivered image quality, dispersion, and resolving power, as well as spectrophotometric performance. The instrument also includes a slitless spectroscopy mode, which is optimally suited for transit spectroscopy of exoplanet atmospheres. We provide an overview of the operational procedures and the differences ahead of the JWST launch in 2018.

  11. Modeling High Resolution Flare Spectra Using Hydrodynamic Simulations

    Science.gov (United States)

    Warren, Harry; Doschek, G.

    2006-06-01

    Understanding the hydrodynamic response of the solar atmosphere to the release of energy during a flare has been a long standing problem in solar physics. Early time-dependent hydrodynamic simulations were able to reproduce the high temperatures and densities observed in solar flares, but were not able to model the observations in any detail. For example, these simulations could not account for the relatively slow decay of the observed emission or the absence of blueshifts in high spectral resolution line profiles at flare onset. We have found that by representing the flare as a succession of independently heated filaments it is possible to reproduce both the evolution of line intensity and the shape of the line profile using hydrodynamic simulations. Here we present detailed comparisons between our simulation results and several flares observed with the Yohkoh Bragg Crystal Spectrometer (BCS). Comparisons with 3D MHD simulations will also be discussed.

  12. SPHERES, Jülich's high-flux neutron backscattering spectrometer at FRM II.

    Science.gov (United States)

    Wuttke, Joachim; Budwig, Alfred; Drochner, Matthias; Kämmerling, Hans; Kayser, Franz-Joseph; Kleines, Harald; Ossovyi, Vladimir; Pardo, Luis Carlos; Prager, Michael; Richter, Dieter; Schneider, Gerald J; Schneider, Harald; Staringer, Simon

    2012-07-01

    SPHERES is a third-generation neutron backscattering spectrometer, located at the 20 MW German neutron source FRM II and operated by the Jülich Centre for Neutron Science. It offers an energy resolution (fwhm) better than 0.65 μeV, a dynamic range of ± 31 μeV, and a signal-to-noise ratio of up to 1750:1.

  13. SPHERES, Juelich's high-flux neutron backscattering spectrometer at FRM II

    Energy Technology Data Exchange (ETDEWEB)

    Wuttke, Joachim; Budwig, Alfred; Drochner, Matthias; Kaemmerling, Hans; Kayser, Franz-Joseph; Kleines, Harald; Ossovyi, Vladimir; Pardo, Luis Carlos; Prager, Michael; Richter, Dieter; Schneider, Gerald J.; Schneider, Harald; Staringer, Simon [Forschungszentrum Juelich GmbH, 52425 Juelich (Germany)

    2012-07-15

    SPHERES is a third-generation neutron backscattering spectrometer, located at the 20 MW German neutron source FRM II and operated by the Juelich Centre for Neutron Science. It offers an energy resolution (fwhm) better than 0.65 {mu}eV, a dynamic range of {+-} 31 {mu}eV, and a signal-to-noise ratio of up to 1750:1.

  14. Conditioning the γ spectrometer for activity measurement at very high background

    Institute of Scientific and Technical Information of China (English)

    YAN Wei-Hua; ZHANG Li-Guo; ZHANG Zhao; XIAO Zhi-Gang

    2012-01-01

    The application of a high purity Germanium (HPGe) γ spectrometer in determining the fuel element burnup in a future reactor is studied.The HPGe detector is exposed by a 60Co source with varying irradiation rate from 10× 103 s-1 to 150× 103 s-1 to simulate the input counting rate in real reactor environment.A 137Cs and a 152Eu source are positioned at given distances to generate a certain event rate in the detector with the former being proposed as a labeling nuclide to measure the burnup of a fuel element.It is shown that both the energy resolution slightly increasing with the irradiation rate and the passthrough rate at high irradiation level match the requirement of the real application.The influence of the background is studied in the different parameter sets used in the specially developed procedure of background subtraction.It is demonstrated that with the typical input irradiation rate and 137Cs intensity relevant to a deep burnup situation,the precision of the 137Cs counting rate in the current experiment is consistently below 2.8%,indicating a promising feasibility of utilizing an HPGe detector in the burnup measurement in future bed-like reactors.

  15. High Rate and Ageing Studies for the Drift Tubes of the ATLAS Muon Spectrometer

    CERN Document Server

    Zimmermann, S

    2004-01-01

    The muon spectrometer of Atlas, one of the 4 experiments currently under construction at the Large Hadron Collider LHC, relies on Monitored Drift Tubes (MDTs) for track reconstruction in most of its regions. The MDTs will have to sustain count rates up to 1500 Hz/cm and must be able to survive an accumulated charge of up to 0.6 C/cm during 10 years of operation. This thesis presents results of high rate and ageing studies conducted at the CERN Gamma Irradiation Facility GIF; a series production Atlas muon chamber and a prototype of the gas recirculation system planned at LHC were used for the first time. Test beam muons were utilized to evaluate the MDT high rate behaviour; questions of resolution, efficiency and changes in the drift properties of the operating gas were addressed. The measurements were complemented by simulations with the program GARFIELD. For the ageing study the MDTs were irradiated over a period of several months, in which their performance was monitored weekly with cosmic muons. A loss in...

  16. High energy X-ray spectrometer on the Chandrayaan-1 mission to the Moon

    Indian Academy of Sciences (India)

    J N Goswami; D Banerjee; N Bhandari; M Shanmugam; Y B Acharya; D V Subhedar; M R Sharma; C N Umapathy; P Sreekumar; M Sudhakar; L Abraham; P C Agrawal

    2005-12-01

    The Chandrayaan-1 mission to the Moon scheduled for launch in late 2007 will include a high energy X-ray spectrometer (HEX) for detection of naturally occurring emissions from the lunar surface due to radioactive decay of the 238U and 232Th series nuclides in the energy region 20 –250 keV.The primary science objective is to study the transport of volatiles on the lunar surface by detection of the 46.5 keV line from radioactive 210Pb, a decay product of the gaseous 222Rn, both of which are members of the 238U decay series. Mapping of U and Th concentration over the lunar surface, particularly in the polar and U –Th rich regions will also be attempted through detection of prominent lines from the U and Th decay series in the above energy range.The low signal strengths of these emissions require a detector with high sensitivity and good energy resolution.Pixelated Cadmium – Zinc –Telluride (CZT)array detectors having these characteristics will be used in this experiment. Here we describe the science considerations that led to this experiment,anticipated flux and back- ground (lunar continuum),the choice of detectors,the proposed payload con figuration and plans for its realization.

  17. From BASIS to MIRACLES: Benchmarking and perspectives for high-resolution neutron spectroscopy at the ESS

    Science.gov (United States)

    Tsapatsaris, Nikolaos; Willendrup, Peter K.; Lechner, Ruep E.; Bordallo, Heloisa N.

    2015-01-01

    Results based on virtual instrument models for the first high-flux, high-resolution, spallation based, backscattering spectrometer, BASIS are presented in this paper. These were verified using the Monte Carlo instrument simulation packages McStas and VITESS. Excellent agreement of the neutron count rate at the sample position between the virtual instrument simulation and experiments was found, in both time and energy distributions. This achievement was only possible after a new component for a bent single crystal analyser in McStas, using a Gaussian approximation, was developed. These findings are pivotal to the conceptual design of the next generation backscattering spectrometer, MIRACLES at the European Spallation Source.

  18. High-resolution, flat-field, plane-grating, f/10 spectrograph with off-axis parabolic mirrors.

    Science.gov (United States)

    Schieffer, Stephanie L; Rimington, Nathan W; Nayyar, Ved P; Schroeder, W Andreas; Longworth, James W

    2007-06-01

    A high-resolution, flat-field, plane-grating, f/10 spectrometer based on the novel design proposed by Gil and Simon [Appl. Opt. 22, 152 (1983)] is demonstrated. The spectrometer design employs off-axis parabolic collimation and camera mirrors in a configuration that eliminates spherical aberrations and minimizes astigmatism, coma, and field curvature in the image plane. In accordance with theoretical analysis, the performance of this spectrometer achieves a high spatial resolution over the large detection area, which is shown to be limited only by the quality of its optics and their proper alignment within the spatial resolution of a 13 microm x 13 microm pixelated CCD detector. With a 1500 lines/mm grating in first order, the measured spectral resolving power of lambda/Dlambda = 2.5(+/-0.5) x 10(4) allows the clear resolution of the violet Ar(I) doublet at 419.07 and 419.10 nm.

  19. High resolution SAR applications and instrument design

    Science.gov (United States)

    Dionisio, C.; Torre, A.

    1993-01-01

    The Synthetic Aperture Radar (SAR) has viewed, in the last two years, a huge increment of interest from many preset and potential users. The good spatial resolution associated to the all weather capability lead to considering SAR not only a scientific instrument but a tool for verifying and controlling the daily human relationships with the Earth Environment. New missions were identified for SAR as spatial resolution became lower than three meters: disasters, pollution, ships traffic, volcanic eruptions, earthquake effect are only a few of the possible objects which can be effectively detected, controlled and monitored by SAR mounted on satellites. High resolution radar design constraints and dimensioning are discussed.

  20. High resolution tomography of objects with access to a single side

    Energy Technology Data Exchange (ETDEWEB)

    Thoe, R.S.

    1993-03-24

    The author is developing a technique which will enable one to obtain high-contrast, high-spatial resolution, three-dimensional images in opaque objects. The only constraint will be the radiation source and detector(s) will be located on the same side of the object. The goal is to obtain images with a spatial resolution of {approximately}1 mm at depths of 10 mm and {approximately}3 mm at depths of 30 mm in materials of moderate density (brass, steel, etc.). The author`s technique uses a highly-collimated beam of monochromatic gamma rays and a slit collimated high-resolution, high-efficiency, coaxial germanium spectrometer. If the geometry is well known, the spectrum of Compton scattered radiation can be used to map out the density as a function of depth. By scanning the object in two dimensions, a full three-dimensional image of the electron density can be reconstructed. The resolution is dependent on the incident beam collimation and the energy resolution of the spectrometer. For his system, the author anticipates a resolution of about 1 mm{sup 3}. The apparatus, reconstruction algorithms and current data verifying his predictions are presented here. Also included are the details on how the system can be modified to increase the efficiency by over two orders of magnitude. This system will have several advantages over conventional transmission radiographic and tomographic systems: (1) It requires the use of a high specific intensity isotopic source of modest activity (< 100 mCi). (2) It requires only a single high-resolution spectrometer used in conjunction with an array of low-resolution detectors (all readily available). (3) It allows for the recording of three-dimensional images of object even though both detector and source are located on the same side of the object.

  1. JPL Fourier transform ultraviolet spectrometer

    Science.gov (United States)

    Cageao, R. P.; Friedl, R. R.; Sander, Stanley P.; Yung, Y. L.

    1994-01-01

    The Fourier Transform Ultraviolet Spectrometer (FTUVS) is a new high resolution interferometric spectrometer for multiple-species detection in the UV, visible and near-IR. As an OH sensor, measurements can be carried out by remote sensing (limb emission and column absorption), or in-situ sensing (long-path absorption or laser-induced fluorescence). As a high resolution detector in a high repetition rate (greater than 10 kHz) LIF system, OH fluorescence can be discriminated against non-resonant background emission and laser scatter, permitting (0, 0) excitation.

  2. Non-invasive submilligram level quantification of in vivo blood components with slitless high-sensitivity spectrometer and noncooled NIR detector

    Science.gov (United States)

    Kuribayashi, Ryosuke; Furukawa, Hiromitsu

    2015-03-01

    By using a "slit-less" Fourier-transform spectrometer, we demonstrate that cardiac-pulsation amplitude of absorbance can be extracted from 3.5-level absorbance unit (AU) spectra of a human fingertip with a resolution of blood components (water, HbO2, and lipids/proteins) in a fingertip are deduced in the sub-milligram order. The results indicate the capacity of the spectrometer for a portable non-invasive blood monitor as well as for a high-end analytic instrument.

  3. 4MOST: the high-resolution spectrograph

    Science.gov (United States)

    Seifert, W.; Xu, W.; Buschkamp, P.; Feiz, C.; Saviauk, A.; Barden, S.; Quirrenbach, A.; Mandel, H.

    2016-08-01

    4MOST (4-meter Multi-Object Spectroscopic Telescope) is a wide-field, fiber-feed, high-multiplex spectroscopic survey facility to be installed on the 4-meter ESO telescope VISTA in Chile. It consists of two identical low resolution spectrographs and one high resolution spectrograph. The instrument is presently in the preliminary design phase and expected to get operational end of 2022. The high resolution spectrograph will afford simultaneous observations of up to 812 targets - over a hexagonal field of view of 4.1 sq.degrees on sky - with a spectral resolution R>18,000 covering a wavelength range from 393 to 679nm in three channels. In this paper we present the optical and mechanical design of the high resolution spectrograph (HRS) as prepared for the review at ESO, Garching. The expected performance including the highly multiplexed fiber slit concept is simulated and its impact on the optical performance given. We show the thermal and finite element analyses and the resulting stability of the spectrograph under operational conditions.

  4. High-Resolution PET Detector. Final report

    Energy Technology Data Exchange (ETDEWEB)

    Karp, Joel

    2014-03-26

    The objective of this project was to develop an understanding of the limits of performance for a high resolution PET detector using an approach based on continuous scintillation crystals rather than pixelated crystals. The overall goal was to design a high-resolution detector, which requires both high spatial resolution and high sensitivity for 511 keV gammas. Continuous scintillation detectors (Anger cameras) have been used extensively for both single-photon and PET scanners, however, these instruments were based on NaI(Tl) scintillators using relatively large, individual photo-multipliers. In this project we investigated the potential of this type of detector technology to achieve higher spatial resolution through the use of improved scintillator materials and photo-sensors, and modification of the detector surface to optimize the light response function.We achieved an average spatial resolution of 3-mm for a 25-mm thick, LYSO continuous detector using a maximum likelihood position algorithm and shallow slots cut into the entrance surface.

  5. Improving the spectral resolution of flat-field concave grating miniature spectrometers by dividing a wide spectral band into two narrow ones.

    Science.gov (United States)

    Zhou, Qian; Pang, Jinchao; Li, Xinghui; Ni, Kai; Tian, Rui

    2015-11-10

    In this study, a new flat-field concave grating miniature spectrometer is proposed with improved resolution across a wide spectral band. A mirror is added to a conventional concave grating spectrometer and placed near the existing detector array, allowing a wide spectral band to be divided into two adjacent subspectral bands. One of these bands is directly detected by the detector, and the other is indirectly analyzed by the same detector after being reflected by the mirror. These two subspectral bands share the same entrance slit, concave grating, and detector, which allows for a compact size, while maintaining an improved spectral resolution across the entire spectral band. The positions of the mirror and other parameters of the spectrometer are designed by a computer procedure and the optical design software ZEMAX. Simulation results show that the resolution of this kind of flat-field concave grating miniature spectrometer is better than 1.6 nm across a spectral band of 700 nm. Experiments based on three laser sources reveal that the measured resolutions are comparable to the simulated ones, with a maximum relative error between them of less than 19%.

  6. High Resolution Investigation of the Ethane Spectrum at 7 μ

    Science.gov (United States)

    Brown, Linda R.; Sung, K.; Di Lauro, C.; Lattanzi, F.; Vander Auwera, J.; Mantz, A. W.; Smith, M. A. H.

    2010-10-01

    A new theoretical analysis of the ethane spectrum between 1330 and 1610 cm-1 has been undertaken in order to create the first line-by-line database of molecular parameters for this spectral region. For this, high resolution spectra were obtained at room and cold (130 K) temperatures with two Bruker Fourier transform spectrometers (at 0.002 cm-1 resolution in Brussels and at 0.003 cm-1 resolution in Pasadena). Over 5000 lines were assigned to five bands in the region: v6, v8, v4+v12 and 2v4+v9 cold bands, and one hot band (v4+v8-v4). This new study employed a much improved theoretical Hamiltonian to reproduce the very complicated spectral structures resulting from numerous interactions between these vibrational modes. This advancement has enabled us to provide a quantum mechanical prediction of line positions and intensities of C2H6 at 7 micron long needed for remote sensing of outer planets and Titan. Two manuscripts are in preparation. Part of the research described in this paper was performed at the Jet Propulsion Laboratory, California Institute of Technology, Connecticut College, and NASA Langley under contract with the National Aeronautics and Space Administration, and with funding from FRS-FNRS in Belgium.

  7. A Miniature Mass Spectrometer for High-Flux Cosmic Dust Analysis

    Science.gov (United States)

    Austin, D. E.; Manning, H. L. K.; Beauchamp, J. L.

    2007-03-01

    We designed a novel mass spectrometer for in situ characterization of micro-particulates in regions of high concentration, such as a comet fly-by, planetary ring, or impact-generated plume. This device is based on novel ion optics that allow high performa

  8. High-resolution spectroscopic diagnostics of very high-temperature plasmas in the hard x-ray regime

    Energy Technology Data Exchange (ETDEWEB)

    Widmann, K

    1999-12-06

    Motivated by the need for establishing a reliable database useful for the application of x-ray spectroscopic tools for the diagnostic of very high temperature plasmas, high-resolution crystal spectrometer measurements have been performed investigating the characteristic K-shell radiation of highly charged krypton and xenon. The measurements, which have been performed at the Electron-Beam-Ion-Trap (EBIT) facility of the Lawrence Livermore National Laboratory, include the investigation of the n = 2 {yields} 1 transitions in heliumlike krypton (Kr{sup 34+}) and innershell excited lithiumlike krypton (Kr{sup 33+}) utilizing a conventional reflection-type crystal spectrometer of von Hamos geometry. The electron-excitation-energy selective measurements map the contribution of the dielectronic recombination lines providing the means of accurate interpretation of the line profiles of the characteristic K{alpha} x-ray emission of plasmas. The high-resolution measurements of the n = 2 {yields} 1 transitions in heliumlike xenon (Xe{sup 52+}) and hydrogenlike xenon (Xe{sup 53+}) were based on a new transmission-type crystal spectrometer of DuMond geometry. The resolving power of the developed spectrometer was sufficient for charge state specific observation allowing the determination of the electron-impact excitation cross section for the hydrogen- and heliumlike K{alpha} transitions. The disagreement with theoretically predicted values is a measure of the magnitude of the Breit interaction for the highly charged high-Z ions.

  9. A high-resolving-power x-ray spectrometer for the OMEGA EP Laser (invited)

    Science.gov (United States)

    Nilson, P. M.; Ehrne, F.; Mileham, C.; Mastrosimone, D.; Jungquist, R. K.; Taylor, C.; Stillman, C. R.; Ivancic, S. T.; Boni, R.; Hassett, J.; Lonobile, D. J.; Kidder, R. W.; Shoup, M. J.; Solodov, A. A.; Stoeckl, C.; Theobald, W.; Froula, D. H.; Hill, K. W.; Gao, L.; Bitter, M.; Efthimion, P.; Meyerhofer, D. D.

    2016-11-01

    A high-resolving-power x-ray spectrometer has been developed for the OMEGA EP Laser System based on a spherically bent Si [220] crystal with a radius of curvature of 330 mm and a Spectral Instruments (SI) 800 Series charge-coupled device. The instrument measures time-integrated x-ray emission spectra in the 7.97- to 8.11-keV range, centered on the Cu Kα1 line. To demonstrate the performance of the spectrometer under high-power conditions, Kα1,2 emission spectra were measured from Cu foils irradiated by the OMEGA EP laser with 100-J, 1-ps pulses at focused intensities above 1018 W/cm2. The ultimate goal is to couple the spectrometer to a picosecond x-ray streak camera and measure temperature-equilibration dynamics inside rapidly heated materials. The plan for these ultrafast streaked x-ray spectroscopy studies is discussed.

  10. A High Resolution Scale-of-four

    Science.gov (United States)

    Fitch, V.

    1949-08-25

    A high resolution scale-of-four has been developed to be used in conjunction with the nuclear particle detection devices in applications where the counting rate is unusually high. Specifically, it is intended to precede the commercially available medium resolution scaling circuits and so decrease the resolving time of the counting system. The circuit will function reliably on continuously recurring pulses separated by less than 0.1 microseconds. It will resolve two pulses (occurring at a moderate repetition rate) which are spaced at 0.04 microseconds. A five-volt input signal is sufficient to actuate the device.

  11. Single shot high resolution digital holography.

    Science.gov (United States)

    Khare, Kedar; Ali, P T Samsheer; Joseph, Joby

    2013-02-11

    We demonstrate a novel computational method for high resolution image recovery from a single digital hologram frame. The complex object field is obtained from the recorded hologram by solving a constrained optimization problem. This approach which is unlike the physical hologram replay process is shown to provide high quality image recovery even when the dc and the cross terms in the hologram overlap in the Fourier domain. Experimental results are shown for a Fresnel zone hologram of a resolution chart, intentionally recorded with a small off-axis reference beam angle. Excellent image recovery is observed without the presence of dc or twin image terms and with minimal speckle noise.

  12. Soft x-ray transmission grating spectrometer for X-ray Surveyor and smaller missions with high resolving power

    Science.gov (United States)

    Heilmann, Ralf K.; Bruccoleri, Alexander; Schattenburg, Mark; Kolodziejczak, jeffery; Gaskin, Jessica; O'Dell, Stephen L.

    2017-01-01

    A number of high priority subjects in astrophysics are addressed by a state-of-the-art soft x-ray grating spectrometer, e.g. the role of Active Galactic Nuclei in galaxy and star formation, characterization of the WHIM and the “missing baryon” problem, characterization of halos around the Milky Way and nearby galaxies, and stellar coronae and surrounding winds and disks. An Explorer-scale, large-area (A > 1,000 cm2), high resolving power (R > 3,000) soft x-ray grating spectrometer is highly feasible based on Critical-Angle Transmission (CAT) grating technology, even for telescopes with angular resolution of 5-10 arcsec. Significantly higher performance could be provided by a CAT grating spectrometer on an X-ray-Surveyor-type mission (A > 4,000 cm2, R > 5,000). CAT gratings combine advantages of blazed reflection gratings (high efficiency, use of higher orders) with those of transmission gratings (low mass, relaxed alignment tolerances and temperature requirements, transparent at higher energies) with minimal mission resource requirements. Blazing is achieved through grazing-incidence reflection off the smooth silicon grating bar sidewalls. Silicon is well matched to the soft x-ray band, and 30% absolute diffraction efficiency has been acheived with clear paths for further improvement. CAT gratings with sidewalls made of high-Z elements allow extension of blazing to higher energies and larger dispersion angles, enabling higher resolving power at shorter wavelengths. X-ray data from CAT gratings coated with a thin layer of platinum using atomic layer deposition demonstrate efficient blazing to higher energies and much larger blaze angles than possible with silicon alone. Measurements of the resolving power of a breadboard CAT grating spectrometer consisting of a Wolter-I slumped-glass focusing optic from GSFC and CAT gratings, taken at the MSFC Stray Light Facility, have demonstrated resolving power > 10,000. Thus currently fabricated CAT gratings are compatible

  13. ESSENSE: Ultra high resolution spectroscopy for the ESS

    Science.gov (United States)

    Pasini, Stefano; Monkenbusch, Michael; Kozielewski, Tadeusz

    2016-09-01

    The instrument concept for a very high intensity neutron spin-echo spectrometer with ultimate resolution properties has been developed and submitted as an instrument proposal to ESS. Effective intensity gain factors up to 30 compared to the best current instruments are anticipated. In addition the resolution will be boosted to the technical limits by newly designed superconducting precession solenoids. The intensity gain results from the use of an optimized guide transporting the high flux from the ESS cold moderator on the one side and from the utilization of an extended wavelength frame of 8 Å yielding a multiplication of information collection rate on the other side. The instrument thus enables novel views on soft matter systems ranging from polymers, functional gels and more to to dynamics of biological molecules with relevance for MD development; the employment of new techniques for surface NSE (GINSE) may contribute to new knowledge in tribology and lubrication and other surface phenomena that currently are hampered by low intensity. New developments in “intelligent” polymers as e.g. self-healing, the properties of which depend on molecular mobility and dynamics, require observation at many 100 ns of correlation times with high intensity, which can be made with ESSENSE.

  14. High resolution AMS imaging of radiocarbon in biomedical applications

    Science.gov (United States)

    Jiang, Z. X.; Bronk Ramsey, C.; Hedges, R. E. M.; Somogyi, P.; Roberts, J. D. B.; Cowey, A.

    1997-03-01

    Radiocarbon has been an important labelling element in biological metabolism studies. By interfacing an accelerator mass spectrometer (AMS) with a scanning microprobe secondary ion source, we have imaged the uptake of radiocarbon labelled metabolic or neurotransmitter amino acids by neurons and glial cells of rats and gerbils at high resolution (1 micron), high sensitivity and in a short time. The biological samples are prepared and sectioned serially at 0.5 μm thickness using standard histological procedures. The adjacent sections to those used for AMS imaging were either immunolabelled with antibodies to GABA to reveal GABA-containing cells, or stained with toluidine blue to visualise every cell. Therefore, the distribution of radiocarbon revealed by AMS could be matched to that of the cells. By simultaneously measuring the 14C, 13C and 12C signals, we can demonstrate that the localised peaks of radiocarbon could be readily identified and matched to GABA-immunopositive neurons and glial cells by aligning the radiocarbon deficient blood vessels with the vessels in the adjacent histologically stained section. The results revealed the selective uptake of the neurotransmitter, GABA and that of metabolic amino acid, leucine. The technique compares favourably with high resolution autoradiography and provides great potential for improving the analysis of molecular interactions in and between cells.

  15. Montecarlo simulation for a new high resolution elemental analysis methodology

    Energy Technology Data Exchange (ETDEWEB)

    Figueroa S, Rodolfo; Brusa, Daniel; Riveros, Alberto [Universidad de La Frontera, Temuco (Chile). Facultad de Ingenieria y Administracion

    1996-12-31

    Full text. Spectra generated by binary, ternary and multielement matrixes when irradiated by a variable energy photon beam are simulated by means of a Monte Carlo code. Significative jumps in the counting rate are shown when the photon energy is just over the edge associated to each element, because of the emission of characteristic X rays. For a given associated energy, the net height of these jumps depends mainly on the concentration and of the sample absorption coefficient. The spectra were obtained by a monochromatic energy scan considering all the emitted radiation by the sample in a 2{pi} solid angle, associating a single multichannel spectrometer channel to each incident energy (Multichannel Scaling (MCS) mode). The simulated spectra were made with Monte Carlo simulation software adaptation of the package called PENELOPE (Penetration and Energy Loss of Positrons and Electrons in matter). The results show that it is possible to implement a new high resolution spectroscopy methodology, where a synchrotron would be an ideal source, due to the high intensity and ability to control the energy of the incident beam. The high energy resolution would be determined by the monochromating system and not by the detection system and not by the detection system, which would basicalbe a photon counter. (author)

  16. Customized MFM probes with high lateral resolution

    Directory of Open Access Journals (Sweden)

    Óscar Iglesias-Freire

    2016-07-01

    Full Text Available Magnetic force microscopy (MFM is a widely used technique for magnetic imaging. Besides its advantages such as the high spatial resolution and the easy use in the characterization of relevant applied materials, the main handicaps of the technique are the lack of control over the tip stray field and poor lateral resolution when working under standard conditions. In this work, we present a convenient route to prepare high-performance MFM probes with sub-10 nm (sub-25 nm topographic (magnetic lateral resolution by following an easy and quick low-cost approach. This allows one to not only customize the tip stray field, avoiding tip-induced changes in the sample magnetization, but also to optimize MFM imaging in vacuum (or liquid media by choosing tips mounted on hard (or soft cantilevers, a technology that is currently not available on the market.

  17. High-resolution electrohydrodynamic jet printing

    Science.gov (United States)

    Park, Jang-Ung; Hardy, Matt; Kang, Seong Jun; Barton, Kira; Adair, Kurt; Mukhopadhyay, Deep Kishore; Lee, Chang Young; Strano, Michael S.; Alleyne, Andrew G.; Georgiadis, John G.; Ferreira, Placid M.; Rogers, John A.

    2007-10-01

    Efforts to adapt and extend graphic arts printing techniques for demanding device applications in electronics, biotechnology and microelectromechanical systems have grown rapidly in recent years. Here, we describe the use of electrohydrodynamically induced fluid flows through fine microcapillary nozzles for jet printing of patterns and functional devices with submicrometre resolution. Key aspects of the physics of this approach, which has some features in common with related but comparatively low-resolution techniques for graphic arts, are revealed through direct high-speed imaging of the droplet formation processes. Printing of complex patterns of inks, ranging from insulating and conducting polymers, to solution suspensions of silicon nanoparticles and rods, to single-walled carbon nanotubes, using integrated computer-controlled printer systems illustrates some of the capabilities. High-resolution printed metal interconnects, electrodes and probing pads for representative circuit patterns and functional transistors with critical dimensions as small as 1μm demonstrate potential applications in printed electronics.

  18. Smartphone microendoscopy for high resolution fluorescence imaging

    CERN Document Server

    Hong, Xiangqian; Mugler, Dale H; Yu, Bing

    2016-01-01

    High resolution optical endoscopes are increasingly used in diagnosis of various medical conditions of internal organs, such as the gastrointestinal tracts, but they are too expensive for use in resource-poor settings. On the other hand, smartphones with high resolution cameras and Internet access have become more affordable, enabling them to diffuse into most rural areas and developing countries in the past decade. In this letter we describe a smartphone microendoscope that can take fluorescence images with a spatial resolution of 3.1 {\\mu}m. Images collected from ex vivo, in vitro and in vivo samples using the device are also presented. The compact and cost-effective smartphone microendoscope may be envisaged as a powerful tool for detecting pre-cancerous lesions of internal organs in low and middle income countries.

  19. A miniature X-ray emission spectrometer (miniXES) for high-pressure studies in a diamond anvil cell.

    Science.gov (United States)

    Pacold, J I; Bradley, J A; Mattern, B A; Lipp, M J; Seidler, G T; Chow, P; Xiao, Y; Rod, Eric; Rusthoven, B; Quintana, J

    2012-03-01

    Core-shell X-ray emission spectroscopy (XES) is a valuable complement to X-ray absorption spectroscopy (XAS) techniques. However, XES in the hard X-ray regime is much less frequently employed than XAS, often as a consequence of the relative scarcity of XES instrumentation having energy resolutions comparable with the relevant core-hole lifetimes. To address this, a family of inexpensive and easily operated short-working-distance X-ray emission spectrometers has been developed. The use of computer-aided design and rapid prototype machining of plastics allows customization for various emission lines having energies from ∼3 keV to ∼10 keV. The specific instrument described here, based on a coarsely diced approximant of the Johansson optic, is intended to study volume collapse in Pr metal and compounds by observing the pressure dependence of the Pr Lα emission spectrum. The collection solid angle is ∼50 msr, roughly equivalent to that of six traditional spherically bent crystal analyzers. The miniature X-ray emission spectrometer (miniXES) methodology will help encourage the adoption and broad application of high-resolution XES capabilities at hard X-ray synchrotron facilities.

  20. The GRAVITY spectrometers: optical qualification

    Science.gov (United States)

    Yazici, Senol; Straubmeier, Christian; Wiest, Michael; Wank, Imke; Fischer, Sebastian; Horrobin, Matthew; Eisenhauer, Frank; Perrin, Guy; Perraut, Karine; Brandner, Wolfgang; Amorim, Antonio; Schöller, Markus; Eckart, Andreas

    2014-07-01

    the arrangement, direction of spectral dispersion and shift of polarization channels for both spectrometers, and the curvature of the spectra in the science spectrometer. In Section 2 we determine the best focus position of the detectors. The overall contrast of images at different positions of the detector stage is computed with the standard deviation of pixel values in the spectra containing region. In Section 3 we analyze high dynamic range images for each spectrometer and resolution obtained at the afore determined best focus positions. We deduce the ensquared energy from the FWHM of Gaussian fits perpendicular to the spectra.

  1. A high-field magnetic resonance imaging spectrometer using an oven-controlled crystal oscillator as the local oscillator of its radio frequency transceiver.

    Science.gov (United States)

    Liang, Xiao; Tang, Xin; Tang, Weinan; Gao, Jia-Hong

    2014-09-01

    A home-made high-field magnetic resonance imaging (MRI) spectrometer with multiple receiving channels is described. The radio frequency (RF) transceiver of the spectrometer consists of digital intermediate frequency (IF) circuits and corresponding mixing circuits. A direct digital synthesis device is employed to generate the IF pulse; the IF signal from a down-conversion circuit is sampled and followed by digital quadrature detection. Both the IF generation and the IF sampling use a 50 MHz clock. An oven-controlled crystal oscillator, which has outstanding spectral purity and a compact circuit, is used as the local oscillator of the RF transceiver. A digital signal processor works as the pulse programmer of the spectrometer, as a result, 32 control lines can be generated simultaneously while an event is triggered. Field programmable gate array devices are utilized as the auxiliary controllers of the IF generation, IF receiving, and gradient control. High performance, including 1 μs time resolution of the soft pulse, 1 MHz receiving bandwidth, and 1 μs time resolution of the gradient waveform, is achieved. High-quality images on a 1.5 T MRI system using the spectrometer are obtained.

  2. The future of high resolution electron microscopy

    Institute of Scientific and Technical Information of China (English)

    D Van Dyck

    2000-01-01

    The state of the art and the future in quantitative high resolution electron microscopy are discussed in the framework of parameter estimation. Reconstruction methods are then to be considered as direct methods to yield a starting structure for further refinement. With the increasing flexibility of the instruments, computer aided experimental strategy will become important.

  3. High resolution spectroscopy of planet bearing stars

    Directory of Open Access Journals (Sweden)

    M. C. Gálvez

    2007-01-01

    Full Text Available We present here the first steps of an extended spectroscopic survey in order to characterize the stellar hosts of extra-solar planets. We have selected several known stars with plan- ets and using high resolution spectroscopy, we have studied their properties.

  4. High-resolution seismic profiling on water

    OpenAIRE

    McGee, T.M.

    2000-01-01

    Herein is presented an overview of high-resolution seismic profiling on water. Included are basic concepts and terminology as well as discussions of types of sources and receivers, field practice, data recording and data processing. Emphasis is on digital single-channel profiling for engineering and environmental purposes.

  5. Compact high-resolution spectral phase shaper

    NARCIS (Netherlands)

    Postma, S.; Walle, van der P.; Offerhaus, H.L.; Hulst, van N.F.

    2005-01-01

    The design and operation of a high-resolution spectral phase shaper with a footprint of only 7×10 cm2 is presented. The liquid-crystal modulator has 4096 elements. More than 600 independent degrees of freedom can be positioned with a relative accuracy of 1 pixel. The spectral shaping of pulses fro

  6. A High-Resolution Stopwatch for Cents

    Science.gov (United States)

    Gingl, Z.; Kopasz, K.

    2011-01-01

    A very low-cost, easy-to-make stopwatch is presented to support various experiments in mechanics. The high-resolution stopwatch is based on two photodetectors connected directly to the microphone input of a sound card. Dedicated free open-source software has been developed and made available to download. The efficiency is demonstrated by a free…

  7. Compressive sensing for high resolution radar imaging

    NARCIS (Netherlands)

    Anitori, L.; Otten, M.P.G.; Hoogeboom, P.

    2010-01-01

    In this paper we present some preliminary results on the application of Compressive Sensing (CS) to high resolution radar imaging. CS is a recently developed theory which allows reconstruction of sparse signals with a number of measurements much lower than what is required by the Shannon sampling th

  8. High-resolution x-ray studies of an AXAF high-energy transmission grating

    DEFF Research Database (Denmark)

    Abdali, S.; Christensen, Finn Erland; Schnopper, H. W.

    1993-01-01

    A triple axis X-ray diffractometer, designed and built at the Danish Space Research Institute, was used to make a high resolution study of the performance of a 2000 angstroms period, high energy X-ray transmission grating developed at MIT for one of the grating spectrometers on the Advanced X-ray...... Astrophysics Facility. Data was obtained at CuK(alpha )1 (8.048 keV) and, using single reflection asymmetric Si(044) crystals for both the monochromator and analyzer, an angular resolution of 1.5 arcsec FWHM was achieved. The efficiency of the grating in all orders up to the 15th was measured using a 12 k......W rotating anode X-ray generator. These data provided the basis for a modelling of the grating structure....

  9. High-resolution absorption measurements of NH3 at high temperatures: 2100-5500 cm-1

    Science.gov (United States)

    Barton, Emma J.; Yurchenko, Sergei N.; Tennyson, Jonathan; Clausen, Sønnik; Fateev, Alexander

    2017-03-01

    High-resolution absorption spectra of NH3 in the region 2100-5500 cm-1 at 1027 °C and approximately atmospheric pressure (1045±3 mbar) are measured. An NH3 concentration of 10% in volume fraction is used in the measurements. Spectra are recorded in a high-temperature gas-flow cell using a Fourier Transform Infrared (FTIR) spectrometer at a nominal resolution of 0.09 cm-1. The spectra are analysed by comparison to a variational line list, BYTe, and experimental energy levels determined using the MARVEL procedure. 2308 lines have been assigned to 45 different bands, of which 1755 and 15 have been assigned or observed for the first time in this work.

  10. High-resolution x-ray studies of an AXAF high-energy transmission grating

    DEFF Research Database (Denmark)

    Abdali, S.; Christensen, Finn Erland; Schnopper, H. W.

    1993-01-01

    A triple axis X-ray diffractometer, designed and built at the Danish Space Research Institute, was used to make a high resolution study of the performance of a 2000 angstroms period, high energy X-ray transmission grating developed at MIT for one of the grating spectrometers on the Advanced X-ray...... Astrophysics Facility. Data was obtained at CuK(alpha )1 (8.048 keV) and, using single reflection asymmetric Si(044) crystals for both the monochromator and analyzer, an angular resolution of 1.5 arcsec FWHM was achieved. The efficiency of the grating in all orders up to the 15th was measured using a 12 k......W rotating anode X-ray generator. These data provided the basis for a modelling of the grating structure....

  11. A micromachined mass spectrometer

    Energy Technology Data Exchange (ETDEWEB)

    Petzold, G.; Siebert, P.; Mueller, J. [Technische Univ. Hamburg-Harburg, Hamburg (Germany). Dept. of Microsystemtechnology

    2001-07-01

    This paper presents the concept, the processing and the simulated and measured characteristics of a miniaturised mass spectrometer, with dimensions of approximately only a few cm{sup 3}. The mass spectrometer consists of three main parts to be manufactured by micro structuring: an electron source, an ionisation chamber including accelerating and focusing units and a mass analyser with detector. Its fabrication is based on techniques used in micro-system processing and in particular anisotropic etching, thin film deposition, electroplating, and anodic bonding. The aim of the concept for this micro mass spectrometer is not only to scale down a macroscopic system but it also takes advantage of the added features of a micro system, i.e. a high Knudsen number of about 3 at a pressure of a few Pascal, and high field strengths at a relatively low voltage. Therefore, the demands on the vacuum systems and the electrical circuits are much more simple compared to a macroscopic mass spectrometer. In the presented design of the micro mass spectrometer the resolution is in the range of 10 to 20 at a sensitivity of several tens of ppm. (orig.)

  12. Constructing a WISE High Resolution Galaxy Atlas

    Science.gov (United States)

    Jarrett, T. H.; Masci, F.; Tsai, C. W.; Petty, S.; Cluver, M.; Assef, Roberto J.; Benford, D.; Blain, A.; Bridge, C.; Donoso, E.; Eisenhardt, P.; Fowler, J.; Koribalski, B.; Lake, S.; Neill, James D.; Seibert, M.; Stanford, S.; Wright, E.

    2012-01-01

    After eight months of continuous observations, the Wide-field Infrared Survey Explorer (WISE) mapped the entire sky at 3.4 micron, 4.6 micron, 12 micron, and 22 micron. We have begun a dedicated WISE High Resolution Galaxy Atlas project to fully characterize large, nearby galaxies and produce a legacy image atlas and source catalog. Here we summarize the deconvolution techniques used to significantly improve the spatial resolution of WISE imaging, specifically designed to study the internal anatomy of nearby galaxies. As a case study, we present results for the galaxy NGC 1566, comparing the WISE enhanced-resolution image processing to that of Spitzer, Galaxy Evolution Explorer, and ground-based imaging. This is the first paper in a two-part series; results for a larger sample of nearby galaxies are presented in the second paper.

  13. High-resolution traction force microscopy.

    Science.gov (United States)

    Plotnikov, Sergey V; Sabass, Benedikt; Schwarz, Ulrich S; Waterman, Clare M

    2014-01-01

    Cellular forces generated by the actomyosin cytoskeleton and transmitted to the extracellular matrix (ECM) through discrete, integrin-based protein assemblies, that is, focal adhesions, are critical to developmental morphogenesis and tissue homeostasis, as well as disease progression in cancer. However, quantitative mapping of these forces has been difficult since there has been no experimental technique to visualize nanonewton forces at submicrometer spatial resolution. Here, we provide detailed protocols for measuring cellular forces exerted on two-dimensional elastic substrates with a high-resolution traction force microscopy (TFM) method. We describe fabrication of polyacrylamide substrates labeled with multiple colors of fiducial markers, functionalization of the substrates with ECM proteins, setting up the experiment, and imaging procedures. In addition, we provide the theoretical background of traction reconstruction and experimental considerations important to design a high-resolution TFM experiment. We describe the implementation of a new algorithm for processing of images of fiducial markers that are taken below the surface of the substrate, which significantly improves data quality. We demonstrate the application of the algorithm and explain how to choose a regularization parameter for suppression of the measurement error. A brief discussion of different ways to visualize and analyze the results serves to illustrate possible uses of high-resolution TFM in biomedical research. © 2014 Elsevier Inc. All rights reserved.

  14. Development of a high resolution and high dispersion Thomson parabola.

    Science.gov (United States)

    Jung, D; Hörlein, R; Kiefer, D; Letzring, S; Gautier, D C; Schramm, U; Hübsch, C; Öhm, R; Albright, B J; Fernandez, J C; Habs, D; Hegelich, B M

    2011-01-01

    Here, we report on the development of a novel high resolution and high dispersion Thomson parabola for simultaneously resolving protons and low-Z ions of more than 100 MeV/nucleon necessary to explore novel laser ion acceleration schemes. High electric and magnetic fields enable energy resolutions of ΔE∕E parabola for ion energies of more than 30 MeV/nucleon.

  15. Development of a high vacuum sample preparation system for helium mass spectrometer

    Science.gov (United States)

    Kumar, P.; Das, N. K.; Mallik, C.; Bhandari, R. K.

    2012-11-01

    A high vacuum sample preparation system for the 3He/4He ratio mass spectrometer (Helix SFT) has been developed to remove all the gaseous constituents excluding helium from the field gases. The sample preparation system comprises of turbo molecular pump, ion pump, zirconium getter, pipettes and vacuum gauges with controller. All these are fitted with cylindrical SS chamber using all metal valves. The field samples are initially treated with activated charcoal trap immersed in liquid nitrogen to cutoff major impurities and moisture present in the sample gas. A sample of 5 ml is collected out of this stage at a pressure of 10-2 mbar. This sample is subsequently purified at a reduced pressure of 10-7 mbar before it is injected into the ion source of the mass spectrometer. The sample pressure was maintained below 10-7 mbar with turbo molecular vacuum pumps and ion pumps. The sample gas passes through several getter elements and a cold finger with the help of manual high vacuum valves before it is fed to the mass spectrometer. Thus the high vacuum sample preparation system introduces completely clean, dry and refined helium sample to the mass spectrometer for best possible analysis of isotopic ratio of helium.

  16. High resolution 3D nonlinear integrated inversion

    Institute of Scientific and Technical Information of China (English)

    Li Yong; Wang Xuben; Li Zhirong; Li Qiong; Li Zhengwen

    2009-01-01

    The high resolution 3D nonlinear integrated inversion method is based on nonlinear theory. Under layer control, the log data from several wells (or all wells) in the study area and seismic trace data adjacent to the wells are input to a network with multiple inputs and outputs and are integratedly trained to obtain an adaptive weight function of the entire study area. Integrated nonlinear mapping relationships are built and updated by the lateral and vertical geologic variations of the reservoirs. Therefore, the inversion process and its inversion results can be constrained and controlled and a stable seismic inversion section with high resolution with velocity inversion, impedance inversion, and density inversion sections, can be gained. Good geologic effects have been obtained in model computation tests and real data processing, which verified that this method has high precision, good practicality, and can be used for quantitative reservoir analysis.

  17. Progress toward high resolution EUV spectroscopy

    Science.gov (United States)

    Korendyke, C.; Doschek, G. A.; Warren, H.; Young, P. R.; Chua, D.; Hassler, D. M.; Landi, E.; Davila, J. M.; Klimchuck, J.; Tun, S.; DeForest, C.; Mariska, J. T.; Solar C Spectroscopy Working Group; LEMUR; EUVST Development Team

    2013-07-01

    HIgh resolution EUV spectroscopy is a critical instrumental technique to understand fundamental physical processes in the high temperature solar atmosphere. Spectroscopic observations are used to measure differential emission measure, line of sight and turbulent flows, plasma densities and emission measures. Spatially resolved, spectra of these emission lines with adequate cadence will provide the necessary clues linking small scale structures with large scale, energetic solar phenomena. The necessary observations to determine underlying physical processes and to provide comprehensive temperature coverage of the solar atmosphere above the chromosphere will be obtained by the proposed EUVST instrument for Solar C. This instrument and its design will be discussed in this paper. Progress on the VEry high Resolution Imaging Spectrograph (VERIS) sounding rocket instrument presently under development at the Naval Research Laboratory will also be discussed.

  18. High performance gamma-ray spectrometer for runaway electron studies on the FT-2 tokamak

    Energy Technology Data Exchange (ETDEWEB)

    Shevelev, A.E., E-mail: Shevelev@cycla.ioffe.ru [Ioffe Institute, Politekhnicheskaya 26, St. Petersburg 194021 (Russian Federation); Khilkevitch, E.M.; Lashkul, S.I.; Rozhdestvensky, V.V.; Altukhov, A.B.; Chugunov, I.N.; Doinikov, D.N.; Esipov, L.A.; Gin, D.B.; Iliasova, M.V.; Naidenov, V.O.; Nersesyan, N.S.; Polunovsky, I.A.; Sidorov, A.V. [Ioffe Institute, Politekhnicheskaya 26, St. Petersburg 194021 (Russian Federation); Kiptily, V.G. [CCFE, Culham Science Centre, Abingdon, Oxon X14 3DB (United Kingdom)

    2016-09-11

    A gamma-ray spectrometer based on LaBr{sub 3}(Ce) scintillator has been used for measurements of hard X-ray emission generated by runaway electrons in the FT-2 tokamak plasmas. Using of the fast LaBr{sub 3}(Ce) has allowed extending count rate range of the spectrometer by a factor of 10. A developed digital processing algorithm of the detector signal recorded with a digitizer sampling rate of 250 MHz has provided a pulse height analysis at count rates up to 10{sup 7} s{sup −1}. A spectrum deconvolution code DeGaSum has been applied for inferring the energy distribution of runaway electrons escaping from the plasma and interacting with materials of the FT-2 limiter in the vacuum chamber. The developed digital signal processing technique for LaBr{sub 3}(Ce) spectrometer has allowed studying the evolution of runaways energy distribution in the FT-2 plasma discharges with time resolution of 1–5 ms.

  19. Understanding reconstructed Dante spectra using high resolution spectroscopy

    Science.gov (United States)

    May, M. J.; Weaver, J.; Widmann, K.; Kemp, G. E.; Thorn, D.; Colvin, J. D.; Schneider, M. B.; Moore, A.; Blue, B. E.

    2016-11-01

    The Dante is an 18 channel filtered diode array used at the National Ignition Facility (NIF) to measure the spectrally and temporally resolved radiation flux between 50 eV and 20 keV from various targets. The absolute flux is determined from the radiometric calibration of the x-ray diodes, filters, and mirrors and a reconstruction algorithm applied to the recorded voltages from each channel. The reconstructed spectra are very low resolution with features consistent with the instrument response and are not necessarily consistent with the spectral emission features from the plasma. Errors may exist between the reconstructed spectra and the actual emission features due to assumptions in the algorithm. Recently, a high resolution convex crystal spectrometer, VIRGIL, has been installed at NIF with the same line of sight as the Dante. Spectra from L-shell Ag and Xe have been recorded by both VIRGIL and Dante. Comparisons of these two spectroscopic measurements yield insights into the accuracy of the Dante reconstructions.

  20. Understanding reconstructed Dante spectra using high resolution spectroscopy

    Energy Technology Data Exchange (ETDEWEB)

    May, M. J., E-mail: may13@llnl.gov; Widmann, K.; Kemp, G. E.; Thorn, D.; Colvin, J. D.; Schneider, M. B.; Moore, A.; Blue, B. E. [L-170 Lawrence Livermore National Laboratory, 7000 East Ave., Livermore, California 94551 (United States); Weaver, J. [Naval Research Laboratory, 4555 Overlook Ave. SW, Washington, DC 20375 (United States)

    2016-11-15

    The Dante is an 18 channel filtered diode array used at the National Ignition Facility (NIF) to measure the spectrally and temporally resolved radiation flux between 50 eV and 20 keV from various targets. The absolute flux is determined from the radiometric calibration of the x-ray diodes, filters, and mirrors and a reconstruction algorithm applied to the recorded voltages from each channel. The reconstructed spectra are very low resolution with features consistent with the instrument response and are not necessarily consistent with the spectral emission features from the plasma. Errors may exist between the reconstructed spectra and the actual emission features due to assumptions in the algorithm. Recently, a high resolution convex crystal spectrometer, VIRGIL, has been installed at NIF with the same line of sight as the Dante. Spectra from L-shell Ag and Xe have been recorded by both VIRGIL and Dante. Comparisons of these two spectroscopic measurements yield insights into the accuracy of the Dante reconstructions.

  1. High-Resolution US of Rheumatologic Diseases.

    Science.gov (United States)

    Taljanovic, Mihra S; Melville, David M; Gimber, Lana H; Scalcione, Luke R; Miller, Margaret D; Kwoh, C Kent; Klauser, Andrea S

    2015-01-01

    For the past 15 years, high-resolution ultrasonography (US) is being routinely and increasingly used for initial evaluation and treatment follow-up of rheumatologic diseases. This imaging technique is performed by using high-frequency linear transducers and has proved to be a powerful diagnostic tool in evaluation of articular erosions, simple and complex joint and bursal effusions, tendon sheath effusions, and synovitis, with results comparable to those of magnetic resonance imaging, excluding detection of bone marrow edema. Crystal deposition diseases including gouty arthropathy and calcium pyrophosphate deposition disease (CPPD) have characteristic appearances at US, enabling differentiation between these two diseases and from inflammatory arthropathies. Enthesopathy, which frequently accompanies psoriatic and reactive arthritis, also has a characteristic appearance at high-resolution US, distinguishing these two entities from other inflammatory and metabolic arthropathies. The presence of Doppler signal in examined joints, bursae, and tendon sheaths indicates active synovitis. Microbubble echo contrast agents augment detection of tissue vascularity and may act in the future as a drug delivery vehicle. Frequently, joint, tendon sheath, and bursal fluid aspirations and therapeutic injections are performed under US guidance. The authors describe the high-resolution US technique including gray-scale, color or power Doppler, and contrast agent-enhanced US that is used in evaluation of rheumatologic diseases of the wrist and hand and the ankle and foot in their routine clinical practice. This article demonstrates imaging findings of normal joints, rheumatoid arthritis, gouty arthritis, CPPD, psoriatic and reactive arthritis, and osteoarthritis.

  2. High-resolution terahertz spectroscopy with a noise radiation source based on high-T c superconductors

    Science.gov (United States)

    Sobakinskaya, E.; Vaks, V. L.; Kinev, N.; Ji, M.; Li, M. Y.; Wang, H. B.; Koshelets, V. P.

    2017-01-01

    Stochastic fields can play a ‘constructive’ role in their interaction with quantum systems. In this paper, we demonstrate that the phase-diffusion field (PDF) in the terahertz range (THz) induces macroscopic polarization in molecular gas. We explain the observed effect using a simple model in which the PDF is treated as a series of ultrashort pulses of a regular signal, resulting in transient absorption in molecular gas. The experimental investigation of this effect is carried out using ammonia, and the PDF is generated by an oscillator based on stacks of Bi2Sr2CaCu2O8 intrinsic Josephson junctions. These radiation sources do not require a phase-lock loop system to provide high resolution, which simplifies the spectrometer considerably. The PDF radiation sources open up new horizons for the development of compact high-resolution THz spectrometers and applications thereof.

  3. Photonuclear reaction based high-energy x-ray spectrometer to cover from 2 MeV to 20 MeV.

    Science.gov (United States)

    Sakata, S; Arikawa, Y; Kojima, S; Ikenouchi, T; Nagai, T; Abe, Y; Inoue, H; Morace, A; Utsugi, M; Kato, R; Nishimura, H; Nakai, M; Shiraga, H; Fujioka, S; Azechi, H

    2014-11-01

    A photonuclear-reaction-based hard x-ray spectrometer is developed to measure the number and energy spectrum of fast electrons generated by interactions between plasma and intense laser light. In this spectrometer, x-rays are converted to neutrons through photonuclear reactions, and the neutrons are counted with a bubble detector that is insensitive to x-rays. The spectrometer consists of a bundle of hard x-ray detectors that respond to different photon-energy ranges. Proof-of-principle experiment was performed on a linear accelerator facility. A quasi-monoenergetic electron bunch (Ne = 1.0 × 10(-6) C, Ee = 16 ± 0.32 MeV) was injected into a 5-mm-thick lead plate. Bremsstrahlung x-rays, which emanate from the lead plate, were measured with the spectrometer. The measured spectral shape and intensity agree fairly well with those computed with a Monte Carlo simulation code. The result shows that high-energy x-rays can be measured absolutely with a photon-counting accuracy of 50%-70% in the energy range from 2 MeV to 20 MeV with a spectral resolution (Δhν/hν) of about 15%. Quantum efficiency of this spectrometer was designed to be 10(-7), 10(-4), 10(-5), respectively, for 2-10, 11-15, and 15-25 MeV of photon energy ranges.

  4. High-resolution flurescence spectroscopy in immunoanalysis

    Energy Technology Data Exchange (ETDEWEB)

    Grubor, Nenad M.

    2005-05-01

    The work presented in this dissertation combines highly sensitive and selective fluorescence line-narrowing spectroscopy (FLNS) detection with various modes of immunoanalytical techniques. It has been shown that FLNS is capable of directly probing molecules immunocomplexed with antibodies, eliminating analytical ambiguities that may arise from interferences that accompany traditional immunochemical techniques. Moreover, the utilization of highly cross-reactive antibodies for highly specific analyte determination has been demonstrated. Finally, they demonstrate the first example of the spectral resolution of diastereomeric analytes based on their interaction with a cross-reactive antibody.

  5. High-resolution flurescence spectroscopy in immunoanalysis

    Energy Technology Data Exchange (ETDEWEB)

    Grubor, Nenad M. [Iowa State Univ., Ames, IA (United States)

    2005-01-01

    The work presented in this dissertation combines highly sensitive and selective fluorescence line-narrowing spectroscopy (FLNS) detection with various modes of immunoanalytical techniques. It has been shown that FLNS is capable of directly probing molecules immunocomplexed with antibodies, eliminating analytical ambiguities that may arise from interferences that accompany traditional immunochemical techniques. Moreover, the utilization of highly cross-reactive antibodies for highly specific analyte determination has been demonstrated. Finally, they demonstrate the first example of the spectral resolution of diastereomeric analytes based on their interaction with a cross-reactive antibody.

  6. An electrospray ionization-ion mobility spectrometer as detector for high- performance liquid chromatography.

    Science.gov (United States)

    Zühlke, Martin; Riebe, Daniel; Beitz, Toralf; Löhmannsröben, Hans-Gerd; Zenichowski, Karl; Diener, Marc; Linscheid, Michael W

    2015-01-01

    The application of electrospray ionization (ESI) ion mobility (IM) spectrometry on the detection end of a high-performance liquid chromatograph has been a subject of study for some time. So far, this method has been limited to low flow rates or has required splitting of the liquid flow. This work presents a novel concept of an ESI source facilitating the stable operation of the spectrometer at flow rates between 10 μL mn(-1) and 1500 μL min(-1) without flow splitting, advancing the T-cylinder design developed by Kurnin and co-workers. Flow rates eight times faster than previously reported were achieved because of a more efficient dispersion of the liquid at increased electrospray voltages combined with nebulization by a sheath gas. Imaging revealed the spray operation to be in a rotationally symmetric multijet mode. The novel ESI-IM spectrometer tolerates high water contents (≤90%) and electrolyte concentrations up to 10mM, meeting another condition required of high-performance liquid chromatography (HPLC) detectors. Limits of detection of 50 nM for promazine in the positive mode and 1 μM for 1,3-dinitrobenzene in the negative mode were established. Three mixtures of reduced complexity (five surfactants, four neuroleptics, and two isomers) were separated in the millisecond regime in stand-alone operation of the spectrometer. Separations of two more complex mixtures (five neuroleptics and 13 pesticides) demonstrate the application of the spectrometer as an HPLC detector. The examples illustrate the advantages of the spectrometer over the established diode array detector, in terms of additional IM separation of substances not fully separated in the retention time domain as well as identification of substances based on their characteristic Ims.

  7. High-resolution TOF with RPCs

    Energy Technology Data Exchange (ETDEWEB)

    Fonte, P. E-mail: fonte@lipc.fis.uc.pt; Peskov, V

    2002-01-21

    In this work, we describe some recent results concerning the application of Resistive Plate Chambers operated in avalanche mode at atmospheric pressure for high-resolution time-of-flight measurements. A combination of multiple, mechanically accurate, thin gas gaps and state-of-the-art electronics yielded an overall (detector plus electronics) timing accuracy better than 50 ps {sigma} with a detection efficiency up to 99% for MIPs. Single gap chambers were also tested in order to clarify experimentally several aspects of the mode of operation of these detectors. These results open perspectives of affordable and reliable high granularity large area TOF detectors, with an efficiency and time resolution comparable to the existing scintillator-based TOF technology but with a significantly, up to an order of magnitude, lower price per channel.

  8. Structural High-resolution Satellite Image Indexing

    OpenAIRE

    Xia, Gui-Song; YANG, WEN; Delon, Julie; Gousseau, Yann; Sun, Hong; Maître, Henri

    2010-01-01

    International audience; Satellite images with high spatial resolution raise many challenging issues in image understanding and pattern recognition. First, they allow measurement of small objects maybe up to 0.5 m, and both texture and geometrical structures emerge simultaneously. Second, objects in the same type of scenes might appear at different scales and orientations. Consequently, image indexing methods should combine the structure and texture information of images and comply with some i...

  9. Stellar Tools for High Resolution Population Synthesis

    Science.gov (United States)

    Chávez, M.; Bertone, E.; Rodríguez-Merino, L.; Buzzoni, A.

    2005-12-01

    We present preliminary results of the application of a new stellar library of high-resolution synthetic spectra (based upon ATLAS9 and SYNTHE codes developed by R. L. Kurucz) in the calculation of the ultraviolet-optical spectral energy distribution of simple stellar populations (SSPs). For this purpose, the library has been coupled with Buzzoni's population synthesis code. Part of this paper is also devoted to illustrate quantitatively the extent to which synthetic stellar libraries represent real stars.

  10. Petrous apex mucocele: high resolution CT

    Energy Technology Data Exchange (ETDEWEB)

    Memis, A. [Dept. of Radiology, Hospital of Ege Univ., Bornova, Izmir (Turkey); Memis, A. [Dept. of Radiology, Hospital of Ege Univ., Bornova, Izmir (Turkey); Alper, H. [Dept. of Radiology, Hospital of Ege Univ., Bornova, Izmir (Turkey); Calli, C. [Dept. of Radiology, Hospital of Ege Univ., Bornova, Izmir (Turkey); Ozer, H. [Dept. of Radiology, Hospital of Ege Univ., Bornova, Izmir (Turkey); Ozdamar, N. [Dept. of Neurosurgery, Hospital of Ege Univ., Bornova, Izmir (Turkey)

    1994-11-01

    Mucocele of the petrous apex is very rare, only three cases having been reported. Since this area is inaccessible to direct examination, imaging, preferably high resolution computed tomography (HR CT) is essential. We report a case showing an eroding, non enhancing mass with sharp, lobulated contours, within the petrous apex. The presence of a large air cell on the opposite side suggested a mucocele. (orig.)

  11. High resolution NMR theory and chemical applications

    CERN Document Server

    Becker, Edwin D

    1969-01-01

    High Resolution NMR: Theory and Chemical Applications focuses on the applications of nuclear magnetic resonance (NMR), as well as chemical shifts, lattices, and couplings. The book first offers information on the theory of NMR, including nuclear spin and magnetic moment, spin lattice relaxation, line widths, saturation, quantum mechanical description of NMR, and ringing. The text then ponders on instrumentation and techniques and chemical shifts. Discussions focus on the origin of chemical shifts, reference compounds, empirical correlations of chemical shifts, modulation and phase detection,

  12. High Speed and High Resolution Table-Top Nanoscale Imaging

    CERN Document Server

    Tadesse, G K; Demmler, S; HÄdrich, S; Wahyutama, I; Steinert, M; Spielmann, C; ZÜrch, M; TÜnnermann, A; Limpert, J; Rothhardt, J

    2016-01-01

    We present a table-top coherent diffraction imaging (CDI) experiment based on high-order harmonics generated at 18 nm by a high average power femtosecond fiber laser system. The high photon flux, narrow spectral bandwidth and high degree of spatial coherence allow for ultra-high sub-wavelength resolution imaging at a high numerical aperture. Our experiments demonstrate a half-pitch resolution of 13.6 nm, very close to the actual Abbe-limit of 12.4 nm, which is the highest resolution achieved from any table-top XUV or X-ray microscope. In addition, 20.5 nm resolution was achieved with only 3 sec of integration time bringing live diffraction imaging and 3D tomography on the nanoscale one step closer to reality. The current resolution is solely limited by the wavelength and the detector size. Thus, table-top nanoscopes with only a few-nm resolutions are in reach and will find applications in many areas of science and technology.

  13. High Sensitivity, High Frequency and High Time Resolution Decimetric Spectroscope

    Science.gov (United States)

    Sawant, H. S.; Rosa, R. R.

    1990-11-01

    RESUMEN. Se ha desarrollado el primer espectroscopio decimetrico latino americano operando en una banda de 100 MHz con alta resoluci6n de fre- cuencia (100 KHz) y tiempo (10 ms), alrededor de cualquier centro de frecuencia en el intervalo de 2000-200 MHz. El prop6sito de esta nota es describir investigaciones solares y no solares que se planean, progra ma de investigaci6n y la situaci6n actual de desarrollo de este espectroscopio. ABSTRACT. First Latin American Decimetric Spectroscope operating over a band of 100 MHz with high resolution in frequency (100 KHz) and time (10 ms), around any center frequency in the range of 2000-200 MHz is being developed. The purpose of this note is to describe planned solar, and non-solar, research programmes and present status of development of this spectroscope. Keq wo : INSTRUMENTS - SPECTROSCOPY

  14. 21 Tesla Fourier Transform Ion Cyclotron Resonance Mass Spectrometer: A National Resource for Ultrahigh Resolution Mass Analysis.

    Science.gov (United States)

    Hendrickson, Christopher L; Quinn, John P; Kaiser, Nathan K; Smith, Donald F; Blakney, Greg T; Chen, Tong; Marshall, Alan G; Weisbrod, Chad R; Beu, Steven C

    2015-09-01

    We describe the design and initial performance of the first 21 tesla Fourier transform ion cyclotron resonance (FT-ICR) mass spectrometer. The 21 tesla magnet is the highest field superconducting magnet ever used for FT-ICR and features high spatial homogeneity, high temporal stability, and negligible liquid helium consumption. The instrument includes a commercial dual linear quadrupole trap front end that features high sensitivity, precise control of trapped ion number, and collisional and electron transfer dissociation. A third linear quadrupole trap offers high ion capacity and ejection efficiency, and rf quadrupole ion injection optics deliver ions to a novel dynamically harmonized ICR cell. Mass resolving power of 150,000 (m/Δm(50%)) is achieved for bovine serum albumin (66 kDa) for a 0.38 s detection period, and greater than 2,000,000 resolving power is achieved for a 12 s detection period. Externally calibrated broadband mass measurement accuracy is typically less than 150 ppb rms, with resolving power greater than 300,000 at m/z 400 for a 0.76 s detection period. Combined analysis of electron transfer and collisional dissociation spectra results in 68% sequence coverage for carbonic anhydrase. The instrument is part of the NSF High-Field FT-ICR User Facility and is available free of charge to qualified users.

  15. High Resolution Measurement of the Glycolytic Rate

    Science.gov (United States)

    Bittner, Carla X.; Loaiza, Anitsi; Ruminot, Iván; Larenas, Valeria; Sotelo-Hitschfeld, Tamara; Gutiérrez, Robin; Córdova, Alex; Valdebenito, Rocío; Frommer, Wolf B.; Barros, L. Felipe

    2010-01-01

    The glycolytic rate is sensitive to physiological activity, hormones, stress, aging, and malignant transformation. Standard techniques to measure the glycolytic rate are based on radioactive isotopes, are not able to resolve single cells and have poor temporal resolution, limitations that hamper the study of energy metabolism in the brain and other organs. A new method is described in this article, which makes use of a recently developed FRET glucose nanosensor to measure the rate of glycolysis in single cells with high temporal resolution. Used in cultured astrocytes, the method showed for the first time that glycolysis can be activated within seconds by a combination of glutamate and K+, supporting a role for astrocytes in neurometabolic and neurovascular coupling in the brain. It was also possible to make a direct comparison of metabolism in neurons and astrocytes lying in close proximity, paving the way to a high-resolution characterization of brain energy metabolism. Single-cell glycolytic rates were also measured in fibroblasts, adipocytes, myoblasts, and tumor cells, showing higher rates for undifferentiated cells and significant metabolic heterogeneity within cell types. This method should facilitate the investigation of tissue metabolism at the single-cell level and is readily adaptable for high-throughput analysis. PMID:20890447

  16. High resolution measurement of the glycolytic rate

    Directory of Open Access Journals (Sweden)

    Carla X Bittner

    2010-09-01

    Full Text Available The glycolytic rate is sensitive to physiological activity, hormones, stress, aging and malignant transformation. Standard techniques to measure the glycolytic rate are based on radioactive isotopes, are not able to resolve single cells and have poor temporal resolution, limitations that hamper the study of energy metabolism in the brain and other organs. A new method is described in this article, which makes use of a recently-developed FRET glucose nanosensor to measure the rate of glycolysis in single cells with high temporal resolution. Used in cultured astrocytes, the method showed for the first time that glycolysis can be activated within seconds by a combination of glutamate and K+, supporting a role for astrocytes in neurometabolic and neurovascular coupling in the brain. It was also possible to make a direct comparison of metabolism in neurons and astrocytes lying in close proximity, paving the way to a high-resolution characterization of brain energy metabolism. Single-cell glycolytic rates were also measured in fibroblasts, adipocytes, myoblasts and tumor cells, showing higher rates for undifferentiated cells and significant metabolic heterogeneity within cell types. This method should facilitate the investigation of tissue metabolism at the single-cell level and is readily adaptable for high-throughput analysis.

  17. Study of an electromagnetic calorimeter for HADES (High Acceptance Di-Electron Spectrometer); Etude d`un calorimetre electromagnetique pour HADES (High Acceptance Di-Electron Spectrometer)

    Energy Technology Data Exchange (ETDEWEB)

    Pienne, Cyril [Universite Blaise Pascal, Clermont-Ferrand 2, (CNRS), 63 - Aubiere (France). U.F.R. de Recherche Scientifique et Technique

    1996-11-27

    The physics context of this work is the study of heavy ion collisions at relativistic energies where dielectron are chosen as a probe of the produced hot and dense nuclear matter. The experimental set-up in construction, the HADES spectrometer, is designed to study the decays of {rho}, {omega}, {phi} mesons into e{sup +}e{sup -} pairs inside the excited medium. The goal is to show that restoration of chiral symmetry, theoretically predicted, manifests itself through the in-medium properties of particles, mesons in particular. Moreover, another goal is the study of electromagnetic form factors of hadrons which are involved in production of dileptons, test of a vector dominance model (VDM) in particular. In the case of the {omega}, its Dalitz decay is not well understood, and the use of a calorimeter could help to solve this mystery. In addition, a calorimeter could provide a redundant characterisation of electrons and positrons. Our work consisted in studying two materials: lead glass and lead tungstate. In the first case, only simulations have been made and led to the following conclusions: - energy resolution ({sigma}{sub E}/E) = 3.89/{radical}E+5.2(%); - spatial resolution ({sigma}{sub x,y}) = 0.14/{radical}E+0.73(cm); - possibility of separation e/h, e/{mu}; - accurate study of the {omega} for factor via its Dalitz decay. The study of lead tungstate began with test of quality and homogeneity of crystal samples in order to check that they have similar properties.. Experiments were performed at the MAMI microtron in Mainz (Germany) with electrons of 180, 450, 855 MeV energy and yielded the following results, never obtained so far: - energy resolution ({sigma}{sub E}/E) = 2.45/{radical}E+97(%); - spatial resolution ({approx_equal} 0.3 cm); - time resolution ({sigma}){approx}1.41 ps at 8.55 MeV for T = 20 deg. C. (author) 52 refs., 90 figs., 30 tabs.

  18. SPIRAL2/DESIR high resolution mass separator

    Energy Technology Data Exchange (ETDEWEB)

    Kurtukian-Nieto, T., E-mail: kurtukia@cenbg.in2p3.fr [Centre d’Études Nucléaires de Bordeaux Gradignan, Université Bordeaux 1-CNRS/IN2P3, BP 120, F-33175 Gradignan Cedex (France); Baartman, R. [TRIUMF, 4004 Wesbrook Mall, Vancouver B.C., V6T 2A3 (Canada); Blank, B.; Chiron, T. [Centre d’Études Nucléaires de Bordeaux Gradignan, Université Bordeaux 1-CNRS/IN2P3, BP 120, F-33175 Gradignan Cedex (France); Davids, C. [Physics Division, Argonne National Laboratory, Argonne, IL 60439 (United States); Delalee, F. [Centre d’Études Nucléaires de Bordeaux Gradignan, Université Bordeaux 1-CNRS/IN2P3, BP 120, F-33175 Gradignan Cedex (France); Duval, M. [GANIL, CEA/DSM-CNRS/IN2P3, Bd Henri Becquerel, BP 55027, F-14076 Caen Cedex 5 (France); El Abbeir, S.; Fournier, A. [Centre d’Études Nucléaires de Bordeaux Gradignan, Université Bordeaux 1-CNRS/IN2P3, BP 120, F-33175 Gradignan Cedex (France); Lunney, D. [CSNSM-IN2P3-CNRS, Université de Paris Sud, F-91405 Orsay (France); Méot, F. [BNL, Upton, Long Island, New York (United States); Serani, L. [Centre d’Études Nucléaires de Bordeaux Gradignan, Université Bordeaux 1-CNRS/IN2P3, BP 120, F-33175 Gradignan Cedex (France); Stodel, M.-H.; Varenne, F. [GANIL, CEA/DSM-CNRS/IN2P3, Bd Henri Becquerel, BP 55027, F-14076 Caen Cedex 5 (France); and others

    2013-12-15

    DESIR is the low-energy part of the SPIRAL2 ISOL facility under construction at GANIL. DESIR includes a high-resolution mass separator (HRS) with a designed resolving power m/Δm of 31,000 for a 1 π-mm-mrad beam emittance, obtained using a high-intensity beam cooling device. The proposed design consists of two 90-degree magnetic dipoles, complemented by electrostatic quadrupoles, sextupoles, and a multipole, arranged in a symmetric configuration to minimize aberrations. A detailed description of the design and results of extensive simulations are given.

  19. Moderate resolution spectrophotometry of high redshift quasars

    Science.gov (United States)

    Schneider, Donald P.; Schmidt, Maarten; Gunn, James E.

    1991-01-01

    A uniform set of photometry and high signal-to-noise moderate resolution spectroscopy of 33 quasars with redshifts larger than 3.1 is presented. The sample consists of 17 newly discovered quasars (two with redshifts in excess of 4.4) and 16 sources drawn from the literature. The objects in this sample have r magnitudes between 17.4 and 21.4; their luminosities range from -28.8 to -24.9. Three of the 33 objects are broad absorption line quasars. A number of possible high redshift damped Ly-alpha systems were found.

  20. Radiation length imaging with high resolution telescopes

    CERN Document Server

    Stolzenberg, U; Schwenker, B; Wieduwilt, P; Marinas, C; Lütticke, F

    2016-01-01

    The construction of low mass vertex detectors with a high level of system integration is of great interest for next generation collider experiments. Radiation length images with a sufficient spatial resolution can be used to measure and disentangle complex radiation length $X$/$X_0$ profiles and contribute to the understanding of vertex detector systems. Test beam experiments with multi GeV particle beams and high-resolution tracking telescopes provide an opportunity to obtain precise 2D images of the radiation length of thin planar objects. At the heart of the $X$/$X_0$ imaging is a spatially resolved measurement of the scattering angles of particles traversing the object under study. The main challenges are the alignment of the reference telescope and the calibration of its angular resolution. In order to demonstrate the capabilities of $X$/$X_0$ imaging, a test beam experiment has been conducted. The devices under test were two mechanical prototype modules of the Belle II vertex detector. A data sample of ...

  1. High Resolution Bathymetry Estimation Improvement with Single ImageSuper Resolution Algorithm Super Resolution Forests

    Science.gov (United States)

    2017-01-26

    process of the SRF algorithm, we were able to further increase the mean PSNR score of the high resolution estimated data from previously used bicubic...This meant that implementing the edited variance before the bicubic estimates were created caused the mean PSNR to increase the most, and all...interpolation (by about 1 dB). Figure 7: PSNR comparison (with mean scores) between Bicubic Interpolation and SRF Figure 7 shows the comparison between

  2. High-time Resolution Astrophysics and Pulsars

    CERN Document Server

    Shearer, Andy

    2008-01-01

    The discovery of pulsars in 1968 heralded an era where the temporal characteristics of detectors had to be reassessed. Up to this point detector integration times would normally be measured in minutes rather seconds and definitely not on sub-second time scales. At the start of the 21st century pulsar observations are still pushing the limits of detector telescope capabilities. Flux variations on times scales less than 1 nsec have been observed during giant radio pulses. Pulsar studies over the next 10 to 20 years will require instruments with time resolutions down to microseconds and below, high-quantum quantum efficiency, reasonable energy resolution and sensitive to circular and linear polarisation of stochastic signals. This chapter is review of temporally resolved optical observations of pulsars. It concludes with estimates of the observability of pulsars with both existing telescopes and into the ELT era.

  3. Novel high-resolution VGA QWIP detector

    Science.gov (United States)

    Kataria, H.; Asplund, C.; Lindberg, A.; Smuk, S.; Alverbro, J.; Evans, D.; Sehlin, S.; Becanovic, S.; Tinghag, P.; Höglund, L.; Sjöström, F.; Costard, E.

    2017-02-01

    Continuing with its legacy of producing high performance infrared detectors, IRnova introduces its high resolution LWIR IDDCA (Integrated Detector Dewar Cooler assembly) based on QWIP (quantum well infrared photodetector) technology. The Focal Plane Array (FPA) has 640×512 pixels, with small (15μm) pixel pitch, and is based on the FLIRIndigo ISC0403 Readout Integrated Circuit (ROIC). The QWIP epitaxial structures are grown by metal-organic vapor phase epitaxy (MOVPE) at IRnova. Detector stability and response uniformity inherent to III/V based material will be demonstrated in terms of high performing detectors. Results showing low NETD at high frame rate will be presented. This makes it one of the first 15μm pitch QWIP based LWIR IDDCA commercially available on the market. High operability and stability of our other QWIP based products will also be shared.

  4. High-Temporal-Resolution High-Spatial-Resolution Spaceborne SAR Based on Continuously Varying PRF.

    Science.gov (United States)

    Men, Zhirong; Wang, Pengbo; Li, Chunsheng; Chen, Jie; Liu, Wei; Fang, Yue

    2017-07-25

    Synthetic Aperture Radar (SAR) is a well-established and powerful imaging technique for acquiring high-spatial-resolution images of the Earth's surface. With the development of beam steering techniques, sliding spotlight and staring spotlight modes have been employed to support high-spatial-resolution applications. In addition to this strengthened high-spatial-resolution and wide-swath capability, high-temporal-resolution (short repeat-observation interval) represents a key capability for numerous applications. However, conventional SAR systems are limited in that the same patch can only be illuminated for several seconds within a single pass. This paper considers a novel high-squint-angle system intended to acquire high-spatial-resolution spaceborne SAR images with repeat-observation intervals varying from tens of seconds to several minutes within a single pass. However, an exponentially increased range cell migration would arise and lead to a conflict between the receive window and 'blind ranges'. An efficient data acquisition technique for high-temporal-resolution, high-spatial-resolution and high-squint-angle spaceborne SAR, in which the pulse repetition frequency (PRF) is continuously varied according to the changing slant range, is presented in this paper. This technique allows echo data to remain in the receive window instead of conflicting with the transmitted pulse or nadir echo. Considering the precision of hardware, a compromise and practical strategy is also proposed. Furthermore, a detailed performance analysis of range ambiguities is provided with respect to parameters of TerraSAR-X. For strong point-like targets, the range ambiguity of this technique would be better than that of uniform PRF technique. For this innovative technique, a resampling strategy and modified imaging algorithm have been developed to handle the non-uniformly sampled echo data. Simulations are performed to validate the efficiency of the proposed technique and the associated

  5. High-resolution absorption cross sections of C$_{2}$H$_{6}$ at elevated temperatures

    CERN Document Server

    Hargreaves, Robert J; Dulick, Michael; Bernath, Peter F

    2015-01-01

    Infrared absorption cross sections near 3.3 $\\mu$m have been obtained for ethane, C$_{2}$H$_{6}$. These were acquired at elevated temperatures (up to 773 K) using a Fourier transform infrared spectrometer and tube furnace with a resolution of 0.005 cm$^{-1}$. The integrated absorption was calibrated using composite infrared spectra taken from the Pacific Northwest National Laboratory (PNNL). These new measurements are the first high-resolution infrared C$_{2}$H$_{6}$ cross sections at elevated temperatures.

  6. High Resolution Continuous Flow Analysis System for Polar Ice Cores

    Science.gov (United States)

    Dallmayr, Remi; Azuma, Kumiko; Yamada, Hironobu; Kjær, Helle Astrid; Vallelonga, Paul; Azuma, Nobuhiko; Takata, Morimasa

    2014-05-01

    35.636 kyr b2k 7), respectively. The results show the conductivity measured upstream and downstream of the debubbler. We will calculate the depth resolution of our system and compare it with earlier studies. 1) Bigler at al, "Optimization of High-Resolution Continuous Flow Analysis For Transient Climate Signals in Ice Cores". Environ. Sci. Technol. 2011, 45, 4483-4489 2) Kaufmann et al, "An Improved Continuous Flow Analysis System for High Resolution Field Measurements on Ice Cores". Environmental Environ. Sci. Technol. 2008, 42, 8044-8050 3) Gkinis, V., T. J. Popp, S. J. Johnsen and T, Blunier, 2010: A continuous stream flash evaporator for the calibration of an IR cavity ring down spectrometer for the isotopic analysis of water. Isotopes in Environmental and Health Studies, 46(4), 463-475. 4) McConnell et al, "Continuous ice-core chemical analyses using inductively coupled plasma mass spectrometry. Environ. Sci. Technol. 2002, 36, 7-11 5) Rhodes et al, "Continuous methane measurements from a late Holocene Greenland ice core : Atmospheric and in-situ signals" Earth and Planetary Science Letters. 2013, 368, 9-19 6) Breton et al, "Quantifying Signal Dispersion in a Hybrid Ice Core Melting System". Environ. Sci. Technol. 2012, 46, 11922-11928 7) Rasmussen et al, " A first chronology for the NEEM ice core". Climate of the Past. 2013, 9, 2967--3013

  7. The research of digital circuit system for high accuracy CCD of portable Raman spectrometer

    Science.gov (United States)

    Yin, Yu; Cui, Yongsheng; Zhang, Xiuda; Yan, Huimin

    2013-08-01

    The Raman spectrum technology is widely used for it can identify various types of molecular structure and material. The portable Raman spectrometer has become a hot direction of the spectrometer development nowadays for its convenience in handheld operation and real-time detection which is superior to traditional Raman spectrometer with heavy weight and bulky size. But there is still a gap for its measurement sensitivity between portable and traditional devices. However, portable Raman Spectrometer with Shell-Isolated Nanoparticle-Enhanced Raman Spectroscopy (SHINERS) technology can enhance the Raman signal significantly by several orders of magnitude, giving consideration in both measurement sensitivity and mobility. This paper proposed a design and implementation of driver and digital circuit for high accuracy CCD sensor, which is core part of portable spectrometer. The main target of the whole design is to reduce the dark current generation rate and increase signal sensitivity during the long integration time, and in the weak signal environment. In this case, we use back-thinned CCD image sensor from Hamamatsu Corporation with high sensitivity, low noise and large dynamic range. In order to maximize this CCD sensor's performance and minimize the whole size of the device simultaneously to achieve the project indicators, we delicately designed a peripheral circuit for the CCD sensor. The design is mainly composed with multi-voltage circuit, sequential generation circuit, driving circuit and A/D transition parts. As the most important power supply circuit, the multi-voltage circuits with 12 independent voltages are designed with reference power supply IC and set to specified voltage value by the amplifier making up the low-pass filter, which allows the user to obtain a highly stable and accurate voltage with low noise. What's more, to make our design easy to debug, CPLD is selected to generate sequential signal. The A/D converter chip consists of a correlated

  8. Highly reproducible laser beam scanning device for an internal source laser desorption microprobe Fourier transform mass spectrometer

    Science.gov (United States)

    Scott, Jill R.; Tremblay, Paul L.

    2002-03-01

    Traditionally, mass spectrometry has relied on manipulating the sample target to provide scanning capabilities for laser desorption microprobes. This has been problematic for an internal source laser desorption Fourier transform mass spectrometer (LD-FTMS) because of the high magnetic field (7 Tesla) and geometric constraints of the superconducting magnet bore. To overcome these limitations, we have implemented a unique external laser scanning mechanism for an internal source LD-FTMS. This mechanism provides adjustable resolution enhancement so that the spatial resolution at the target is not limited to that of the stepper motors at the light source (˜5 μm/step). The spatial resolution is now limited by the practical optical diffraction limit of the final focusing lens. The scanning mechanism employs a virtual source that is wavelength independent up to the final focusing lens, which can be controlled remotely to account for focal length dependence on wavelength. A binary index provides an automatic alignment feature. The virtual source is located ˜9 ft from the sample; therefore, it is completely outside of the vacuum system and beyond the 50 G line of the fringing magnetic field. To eliminate reproducibility problems associated with vacuum pump vibrations, we have taken advantage of the magnetic field inherent to the FTMS to utilize Lenz's law for vibrational dampening. The LD-FTMS microprobe has exceptional reproducibility, which enables successive mapping sequences for depth-profiling studies.

  9. Integrated High Resolution Monitoring of Mediterranean vegetation

    Science.gov (United States)

    Cesaraccio, Carla; Piga, Alessandra; Ventura, Andrea; Arca, Angelo; Duce, Pierpaolo; Mereu, Simone

    2017-04-01

    The study of the vegetation features in a complex and highly vulnerable ecosystems, such as Mediterranean maquis, leads to the need of using continuous monitoring systems at high spatial and temporal resolution, for a better interpretation of the mechanisms of phenological and eco-physiological processes. Near-surface remote sensing techniques are used to quantify, at high temporal resolution, and with a certain degree of spatial integration, the seasonal variations of the surface optical and radiometric properties. In recent decades, the design and implementation of global monitoring networks involved the use of non-destructive and/or cheaper approaches such as (i) continuous surface fluxes measurement stations, (ii) phenological observation networks, and (iii) measurement of temporal and spatial variations of the vegetation spectral properties. In this work preliminary results from the ECO-SCALE (Integrated High Resolution Monitoring of Mediterranean vegetation) project are reported. The project was manly aimed to develop an integrated system for environmental monitoring based on digital photography, hyperspectral radiometry , and micrometeorological techniques during three years of experimentation (2013-2016) in a Mediterranean site of Italy (Capo Caccia, Alghero). The main results concerned the analysis of chromatic coordinates indices from digital images, to characterized the phenological patterns for typical shrubland species, determining start and duration of the growing season, and the physiological status in relation to different environmental drought conditions; then the seasonal patterns of canopy phenology, was compared to NEE (Net Ecosystem Exchange) patterns, showing similarities. However, maximum values of NEE and ER (Ecosystem respiration), and short term variation, seemed mainly tuned by inter annual pattern of meteorological variables, in particular of temperature recorded in the months preceding the vegetation green-up. Finally, green signals

  10. ABERRATIONS MINIMIZATION FOR IMPROVING CHARACTERISTICS OF COMPACT HIGH-APERTURE DISPERSIVE SPECTROMETERS

    Directory of Open Access Journals (Sweden)

    E. S. Voropay

    2010-01-01

    Full Text Available Schemes of high-aperture and compact optical spectrometers and giperspectrometer with minimized aberrations are presented. In the first scheme usage of inclined plane-parallel plate allows decreasing of astigmatism. In the second scheme off-axis aberrations are practically removed due to axial propagation of light. For giperspectrometer narrowing of light propagation angle through the object lens and turning the light out of dispersion plane lead to minimizing of picture aberrations.

  11. A Novel Spatial Modulation Fourier Transform Spectrometer with Adjustable Spectral Resolution%一种光谱分辨率可调的新型空间调制傅里叶变换光谱仪

    Institute of Scientific and Technical Information of China (English)

    廉玉生; 廖宁放; 吕航; 吴文敏; 董志刚

    2014-01-01

    In the premise of fulfilling the application requirement ,the adjustment of spectral resolution can improve efficiency of data acquisition ,data processing and data saving .So ,by adjusting the spectral resolution ,the performance of spectrometer can be improved ,and its application range can be extended .To avoid the problems of the fixed spectral resolution of classical Fourier transform spectrometer ,a novel type of spatial modulation Fourier transform spectrometer with adjustable spectral resolution is proposed in this paper .The principle of the novel spectrometer and its interferometer is described .The general expressions of the optical path difference and the lateral shear are induced by a ray tracing procedure .The equivalent model of the novel inter-ferometer is analyzed .Meanwhile ,the principle of the adjustment of spectral resolution is analyzed .The result shows that the novel spectrometer has the merits of adjustable spectral resolution ,high stability ,easy assemblage and adjustment etc .This the-oretical study will provide the theoretical basis for the design of the spectrometer with adjustable spectral resolution and expand the application range of Fourier transform spectrometer .%调整光谱仪的光谱分辨率,可使光谱仪在满足不同目标测量需求的同时,减少数据采集、处理和存储的时间,提高仪器的整体性能。为克服传统傅里叶变换光谱仪的光谱分辨率固定的缺点,提出了一种分辨率可调的空间调制傅里叶变换光谱仪。介绍了该新型光谱仪及其干涉仪的工作原理,利用光线追迹的方法推导了光程差和横向剪切量的计算公式,并分析了新型干涉仪的光程等效模型。在此基础上,分析了光谱分辨率的调节原理。结果表明,该光谱分辨率可调的新型空间调制傅里叶变换光谱仪克服了传统光谱仪分辨率固定、稳定性差等缺点,具有分辨率可调、高稳定性、结构灵活和

  12. High-resolution phylogenetic microbial community profiling

    Energy Technology Data Exchange (ETDEWEB)

    Singer, Esther; Coleman-Derr, Devin; Bowman, Brett; Schwientek, Patrick; Clum, Alicia; Copeland, Alex; Ciobanu, Doina; Cheng, Jan-Fang; Gies, Esther; Hallam, Steve; Tringe, Susannah; Woyke, Tanja

    2014-03-17

    The representation of bacterial and archaeal genome sequences is strongly biased towards cultivated organisms, which belong to merely four phylogenetic groups. Functional information and inter-phylum level relationships are still largely underexplored for candidate phyla, which are often referred to as microbial dark matter. Furthermore, a large portion of the 16S rRNA gene records in the GenBank database are labeled as environmental samples and unclassified, which is in part due to low read accuracy, potential chimeric sequences produced during PCR amplifications and the low resolution of short amplicons. In order to improve the phylogenetic classification of novel species and advance our knowledge of the ecosystem function of uncultivated microorganisms, high-throughput full length 16S rRNA gene sequencing methodologies with reduced biases are needed. We evaluated the performance of PacBio single-molecule real-time (SMRT) sequencing in high-resolution phylogenetic microbial community profiling. For this purpose, we compared PacBio and Illumina metagenomic shotgun and 16S rRNA gene sequencing of a mock community as well as of an environmental sample from Sakinaw Lake, British Columbia. Sakinaw Lake is known to contain a large age of microbial species from candidate phyla. Sequencing results show that community structure based on PacBio shotgun and 16S rRNA gene sequences is highly similar in both the mock and the environmental communities. Resolution power and community representation accuracy from SMRT sequencing data appeared to be independent of GC content of microbial genomes and was higher when compared to Illumina-based metagenome shotgun and 16S rRNA gene (iTag) sequences, e.g. full-length sequencing resolved all 23 OTUs in the mock community, while iTags did not resolve closely related species. SMRT sequencing hence offers various potential benefits when characterizing uncharted microbial communities.

  13. Novel high resolution tactile robotic fingertips

    DEFF Research Database (Denmark)

    Drimus, Alin; Jankovics, Vince; Gorsic, Matija

    2014-01-01

    This paper describes a novel robotic fingertip based on piezoresistive rubber that can sense pressure tactile stimuli with a high spatial resolution over curved surfaces. The working principle is based on a three-layer sandwich structure (conductive electrodes on top and bottom and piezoresistive...... with specialized data acquisition electronics that acquire 500 frames per second provides rich information regarding contact force, shape and angle for bio- inspired robotic fingertips. Furthermore, a model of estimating the force of contact based on values of the cells is proposed....

  14. Fast Backprojection Techniques for High Resolution Tomography

    CERN Document Server

    Koshev, Nikolay; Miqueles, Eduardo X

    2016-01-01

    Fast image reconstruction techniques are becoming important with the increasing number of scientific cases in high resolution micro and nano tomography. The processing of the large scale three-dimensional data demands new mathematical tools for the tomographic reconstruction task because of the big computational complexity of most current algorithms as the sizes of tomographic data grow with the development of more powerful acquisition hardware and more refined scientific needs. In the present paper we propose a new fast back-projection operator for the processing of tomographic data and compare it against other fast reconstruction techniques.

  15. Operating mode of high pressure straws with high spatial resolution

    CERN Document Server

    Davkov, K I; Peshekhonov, V D; Cholakov, V D

    2013-01-01

    The article presents results of studying the operating mode of thin-walled drift tubes (straws) at flushing it with a high-pressure gas mixture, which allowed obtaining extremely high spatial resolution for straw detectors. The results of studying the radiation ageing of straws operating in this mode are also described.

  16. Digital interface for high-resolution displays

    Science.gov (United States)

    Hermann, David J.; Gorenflo, Ronald L.

    1999-08-01

    Commercial display interfaces are currently transitioning from analog to digital. Although this transition is in the very early stages, the military needs to begin planning their own transition to digital. There are many problems with the analog interface in high-resolution display systems that are solved by changing to a digital interface. Also, display system cost can be lower with a digital interface to a high resolution display. Battelle is under contract with DARPA to develop an advanced Display Interface (ADI) to replace the analog RGB interfaces currently used in high definition workstation displays. The goal is to create a standard digital display interface for military applications that is based on emerging commercial standards. Support for military application- specific functionality is addressed, including display test and control. The main challenges to implementing a digital display interface are described, along with approaches to address the problems. Conceptual ADI architectures are described and contrasted. The current and emerging commercial standards for digital display interfaces are reviewed in detail. Finally, the tasks required to complete the ADI effort are outlined and described.

  17. High resolution electron scattering on {sup 96}Zr

    Energy Technology Data Exchange (ETDEWEB)

    Kremer, Christoph; Bassauer, Sergej; Krugmann, Andreas; Krumbholz, Anna Maria; Pietralla, Norbert; Singer, Maxim; Neumann-Cosel, Peter von [Institut fuer Kernphysik, TU Darmstadt (Germany)

    2015-07-01

    The low-energy structure of the nucleus {sup 96}Zr is interesting for numerous reasons - especially the strong octupole correlation leading to an excitation of the prominent 3{sup -}{sub 1} state with the largest known ground-state transition strength (B(E3, 3{sup +}{sub 1} → 0{sup +}{sub 1}) = 57(4) W.u.) of all nuclei. Even though this nucleus is a good testing ground for nuclear structure theories some low-energy observables are known with insufficient precision. Especially the transition strength of low-lying 2{sup +} states, which are important for the identification of mixed-symmetry states, have large uncertainties. Electron scattering at low impulse transfer has been shown to be capable of obtaining these B(E2) values with high precision. A {sup 96}Zr(e,e{sup '}) experiment has recently been performed at the superconducting electron linear accelerator S-DALINAC at Darmstadt using the high-resolution LINTOTT spectrometer. The experiment and preliminary results are presented.

  18. High Resolution Studies of Mass Loss from Massive Binary Stars

    Science.gov (United States)

    Corcoran, Michael F.; Gull, Theodore R.; Hamaguchi, Kenji; Richardson, Noel; Madura, Thomas; Post Russell, Christopher Michael; Teodoro, Mairan; Nichols, Joy S.; Moffat, Anthony F. J.; Shenar, Tomer; Pablo, Herbert

    2017-01-01

    Mass loss from hot luminous single and binary stars has a significant, perhaps decisive, effect on their evolution. The combination of X-ray observations of hot shocked gas embedded in the stellar winds and high-resolution optical/UV spectra of the cooler mass in the outflow provides unique ways to study the unstable process by which massive stars lose mass both through continuous stellar winds and rare, impulsive, large-scale mass ejections. The ability to obtain coordinated observations with the Hubble Space Telescope Imaging Spectrograph (HST/STIS) and the Chandra High-Energy Transmission Grating Spectrometer (HETGS) and other X-ray observatories has allowed, for the first time, studies of resolved line emisssion over the temperature range of 104- 108K, and has provided observations to confront numerical dynamical models in three dimensions. Such observations advance our knowledge of mass-loss asymmetries, spatial and temporal variabilities, and the fundamental underlying physics of the hot shocked outflow, providing more realistic constraints on the amount of mass lost by different luminous stars in a variety of evolutionary stages. We discuss the impact that these joint observational studies have had on our understanding of dynamical mass outflows from massive stars, with particular emphasis on two important massive binaries, Delta Ori Aa, a linchpin of the mass luminosity relation for upper HRD main sequence stars, and the supermassive colliding wind binary Eta Carinae.

  19. Crusta: Visualizing High-resolution Global Data

    Science.gov (United States)

    Bernardin, T. S.; Kreylos, O.; Bowles, C. J.; Cowgill, E.; Hamann, B.; Kellogg, L. H.

    2009-12-01

    Virtual globes have become indispensable tools for visualizing, understanding and presenting data from Earth and other planetary bodies. The scientific community has invested much effort into exploiting existing globes to their fullest potential by refining and adapting their capabilities to better satisfy specific needs. For example, Google Earth provides users with the ability to view hillshade images derived from airborne LiDAR data such as the 2007 Northern California GeoEarthScope data. However, because most available globes were not designed with the specific needs of geoscientists in mind, shortcomings are becoming increasingly evident in geoscience applications such as terrain visualization. In particular, earth scientists struggle to visualize digital elevation models with both high spatial resolution (0.5 - 1 square meters per sample) and large extent (>2000 square kilometers), such as those obtained with airborne LiDAR. To address the specific earth science need of real-time terrain visualization of LiDAR data, we are developing Crusta as part of a close collaboration involving earth and computer scientists. Crusta is a new virtual globe that differs from widely used globes by both providing accurate global data representation and the ability to easily visualize custom topographic and image data. As a result, Crusta enables real-time, interactive visualization of high resolution digital elevation data spanning thousands of square kilometers, such as the complete 2007 Northern California GeoEarthScope airborne LiDAR data set. To implement an accurate data representation and avoid distortion of the display at the poles, where other projections have singularities, Crusta represents the globe as a thirty-sided polyhedron. Each side of this polyhedron can be subdivided to an arbitrarily fine grid on the surface of the globe, which allows Crusta to accommodate input data of arbitrary resolution ranging from global (e.g., Blue Marble) to local (e.g., a tripod

  20. Quantum cascade laser-based spectrometer for high sensitive measurements of trace gases in air

    Institute of Scientific and Technical Information of China (English)

    Yuanyuan Tang; Wenqing Liu; Ruifeng Kan; Yujun Zhang; Dong Chen; Shuai Zhang; Jun Ruan

    2012-01-01

    A quantum cascade (QC) laser-based spectrometer is developed to measure trace gases in air.The proposed spectrometer is tested for N2O,and the results presented in this letter.This system takes advantage of recent technology in QC lasers by utilizing intra-pulse scan spectroscopy,which allows high sensitive measurement.Without calibration gases,the gas concentration can be calculated with scan integration and the corresponding values from the HITRAN04 database.By analyzing the Allan variance,a detection limit of 2 ppb is obtained.Continuous measurement of N2O sampled from ambient air shows the applicability of the proposed system for the field measurements of gases of environmental concern.

  1. Compact diode-laser spectrometer ISOWAT for highly sensitive airborne measurements of water-isotope ratios

    Science.gov (United States)

    Dyroff, C.; Fütterer, D.; Zahn, A.

    2010-02-01

    The tunable diode-laser absorption spectrometer ISOWAT for airborne measurements of the water-isotope ratios 18O/16O and D/H is described. The spectrometer uses a distributed feedback (DFB) diode laser to probe fundamental rovibrational water-absorption lines at around 2.66 μm. Very-low-noise system components along with signal averaging allow for a detection limit of 1.2 and 4.5 ‰ for measurements of 18O/16O and D/H, respectively, for a water-vapour mixing ratio of 100 ppmv and an averaging time of 60 s. This corresponds to a minimum detectable absorbance of ˜5×10-6 or ˜6.6×10-10 cm-1 when normalized to pathlength. In addition to its high sensitivity, the spectrometer is highly compact (19-inch rack at a height of 35 cm, excluding pump and calibration unit) and light weight (automated. ISOWAT will be calibrated during flight with known water-isotope ratios using a compact calibration-gas source.

  2. High spectral resolution observation of extended sources in future interplanetary missions

    Science.gov (United States)

    Hosseini, Sona

    2016-10-01

    The most commonly used technique for high spectral resolution (R) studies are grating spectrometers. They can achieve broad bandpasses but they have small FOV and relatively low étendue so they have to be paired with large aperture telescopes such Keck (10m), Hubble (2.4m) or JWST (6.5m). Fabry-Pérot Interferometers (FPI) and FTS are the other best known types of high étendue, high R spectrometers used in astronomy. But their opto-mechnical tolerances becomes challenging and they use transmitting optics, where transmission drops especially below 130 nm. Spatial Heterodyne Spectrometer (SHS) is a candidate for high étendue, high spectral R spectroscopy in compact low cost, low-mass, low-power architecture using no or small aperture telescope for UV to IR wavelengths. High R spectrometers are usually limited by the telescope aperture size and complicated opto-mechanical tolerances but that's not the case for SHS. SHS provides integrated spectra at high spectral R, over a wide FOV in compact designs in which it offers the ability to make key science measurements for a variety of planetary targets. SHS could be implemented on a dedicated SmallSat or ISS that can sit and stare at its target for long duration of time that cannot be done from the ground or on big missions. SmallSats are lower cost, faster to build, relatively easy to correct and upgrade. For UV observation, currently HST is the only telescope capable of collecting the necessary observations and the next major UV space telescope might be able to fly in 10 years or more. SHS instrument can quickly fill the technology gap for UV space spectrometers.

  3. High-resolution noncontact atomic force microscopy.

    Science.gov (United States)

    Pérez, Rubén; García, Ricardo; Schwarz, Udo

    2009-07-01

    original papers authored by many of the leading groups in the field with the goal of providing a well-balanced overview on the state-of-the-art in this rapidly evolving field. These papers, many of which are based on notable presentations given during the Madrid conference, feature highlights such as (1) the development of sophisticated force spectroscopy procedures that are able to map the complete 3D tip-sample force field on different surfaces; (2) the considerable resolution improvement of Kelvin probe force microscopy (reaching, in some cases, the atomic scale), which is accompanied by a thorough, quantitative understanding of the contrast observed; (3) the perfecting of atomic resolution imaging on insulating substrates, which helps reshape our microscopic understanding of surface properties and chemical activity of these surfaces; (4) the description of instrumental and methodological developments that pave the way to the atomic-scale characterization of magnetic and electronic properties of nanostructures, and last but not least (5) the extension of dynamic imaging modes to high-resolution operation in liquids, ultimately achieving atomic resolution. The latter developments are already having a significant impact in the highly competitive field of biological imaging under physiological conditions. This special issue of Nanotechnology would not have been possible without the highly professional support from Nina Couzin, Amy Harvey, Alex Wotherspoon and the entire Nanotechnology team at IOP Publishing. We are thankful for their help in pushing this project forward. We also thank the authors who have contributed their excellent original articles to this issue, the referees whose comments have helped make the issue an accurate portrait of this rapidly moving field, and the entire NC-AFM community that continues to drive NC-AFM to new horizons.

  4. Principles of high resolution NMR in solids

    CERN Document Server

    Mehring, Michael

    1983-01-01

    The field of Nuclear Magnetic Resonance (NMR) has developed at a fascinating pace during the last decade. It always has been an extremely valuable tool to the organic chemist by supplying molecular "finger print" spectra at the atomic level. Unfortunately the high resolution achievable in liquid solutions could not be obtained in solids and physicists and physical chemists had to live with unresolved lines open to a wealth of curve fitting procedures and a vast amount of speculations. High resolution NMR in solids seemed to be a paradoxon. Broad structure­ less lines are usually encountered when dealing with NMR in solids. Only with the recent advent of mUltiple pulse, magic angle, cross-polarization, two-dimen­ sional and multiple-quantum spectroscopy and other techniques during the last decade it became possible to resolve finer details of nuclear spin interactions in solids. I have felt that graduate students, researchers and others beginning to get involved with these techniques needed a book which trea...

  5. Limiting liability via high resolution image processing

    Energy Technology Data Exchange (ETDEWEB)

    Greenwade, L.E.; Overlin, T.K.

    1996-12-31

    The utilization of high resolution image processing allows forensic analysts and visualization scientists to assist detectives by enhancing field photographs, and by providing the tools and training to increase the quality and usability of field photos. Through the use of digitized photographs and computerized enhancement software, field evidence can be obtained and processed as `evidence ready`, even in poor lighting and shadowed conditions or darkened rooms. These images, which are most often unusable when taken with standard camera equipment, can be shot in the worst of photographic condition and be processed as usable evidence. Visualization scientists have taken the use of digital photographic image processing and moved the process of crime scene photos into the technology age. The use of high resolution technology will assist law enforcement in making better use of crime scene photography and positive identification of prints. Valuable court room and investigation time can be saved and better served by this accurate, performance based process. Inconclusive evidence does not lead to convictions. Enhancement of the photographic capability helps solve one major problem with crime scene photos, that if taken with standard equipment and without the benefit of enhancement software would be inconclusive, thus allowing guilty parties to be set free due to lack of evidence.

  6. High-Resolution Scintimammography: A Pilot Study

    Energy Technology Data Exchange (ETDEWEB)

    Rachel F. Brem; Joelle M. Schoonjans; Douglas A. Kieper; Stan Majewski; Steven Goodman; Cahid Civelek

    2002-07-01

    This study evaluated a novel high-resolution breast-specific gamma camera (HRBGC) for the detection of suggestive breast lesions. Methods: Fifty patients (with 58 breast lesions) for whom a scintimammogram was clinically indicated were prospectively evaluated with a general-purpose gamma camera and a novel HRBGC prototype. The results of conventional and high-resolution nuclear studies were prospectively classified as negative (normal or benign) or positive (suggestive or malignant) by 2 radiologists who were unaware of the mammographic and histologic results. All of the included lesions were confirmed by pathology. Results: There were 30 benign and 28 malignant lesions. The sensitivity for detection of breast cancer was 64.3% (18/28) with the conventional camera and 78.6% (22/28) with the HRBGC. The specificity with both systems was 93.3% (28/30). For the 18 nonpalpable lesions, sensitivity was 55.5% (10/18) and 72.2% (13/18) with the general-purpose camera and the HRBGC, respectively. For lesions 1 cm, 7 of 15 were detected with the general-purpose camera and 10 of 15 with the HRBGC. Four lesions (median size, 8.5 mm) were detected only with the HRBGC and were missed by the conventional camera. Conclusion: Evaluation of indeterminate breast lesions with an HRBGC results in improved sensitivity for the detection of cancer, with greater improvement shown for nonpalpable and 1-cm lesions.

  7. High-resolution light microscopy of nanoforms

    Science.gov (United States)

    Vodyanoy, Vitaly; Pustovyy, Oleg; Vainrub, Arnold

    2007-09-01

    We developed a high resolution light imaging system. Diffraction gratings with 100 nm width lines as well as less than 100 nm size features of different-shaped objects are clearly visible on a calibrated microscope test slide (Vainrub et al., Optics Letters, 2006, 31, 2855). The two-point resolution increase results from a known narrowing of the central diffraction peak for the annular aperture. Better visibility and advanced contrast of the smallest features in the image are due to enhancement of high spatial frequencies in the optical transfer function. The imaging system is portable, low energy, and battery operated. It has been adapted to use in both transmitting and reflecting light. It is particularly applicable for motile nanoform systems where structure and functions can be depicted in real time. We have isolated micrometer and submicrometer particles, termed proteons, from human and animal blood. Proteons form by reversible seeded aggregation of proteins around proteon nucleating centers (PNCs). PNCs are comprised of 1-2nm metallic nanoclusters containing 40-300 atoms. Proteons are capable of spontaneous assembling into higher nanoform systems assuming structure of complicated topology. The arrangement of complex proteon system mimics the structure of a small biological cell. It has structures that imitate membrane and nucleolus or nuclei. Some of these nanoforms are motile. They interact and divide. Complex nanoform systems can spontaneously reduce to simple proteons. The physical properties of these nanoforms could shed some light on the properties of early life forms or forms at extreme conditions.

  8. Venus gravity - A high-resolution map

    Science.gov (United States)

    Reasenberg, R. D.; Goldberg, Z. M.; Macneil, P. E.; Shapiro, I. I.

    1981-01-01

    The Doppler data from the radio tracking of the Pioneer Venus Orbiter (PVO) have been used in a two-stage analysis to develop a high-resolution map of the gravitational potential of Venus, represented by a central mass and a surface mass density. The two-stage procedure invokes a Kalman filter-smoother to determine the orbit of the spacecraft, and a stabilized linear inverter to estimate the surface mass density. The resultant gravity map is highly correlated with the topographic map derived from the PVO radar altimeter data. However, the magnitudes of the gravity variations are smaller than would be expected if the topography were uncompensated, indicating that at least partial compensation has taken place.

  9. Ultra-high resolution computed tomography imaging

    Energy Technology Data Exchange (ETDEWEB)

    Paulus, Michael J. (Knoxville, TN); Sari-Sarraf, Hamed (Knoxville, TN); Tobin, Jr., Kenneth William (Harriman, TN); Gleason, Shaun S. (Knoxville, TN); Thomas, Jr., Clarence E. (Knoxville, TN)

    2002-01-01

    A method for ultra-high resolution computed tomography imaging, comprising the steps of: focusing a high energy particle beam, for example x-rays or gamma-rays, onto a target object; acquiring a 2-dimensional projection data set representative of the target object; generating a corrected projection data set by applying a deconvolution algorithm, having an experimentally determined a transfer function, to the 2-dimensional data set; storing the corrected projection data set; incrementally rotating the target object through an angle of approximately 180.degree., and after each the incremental rotation, repeating the radiating, acquiring, generating and storing steps; and, after the rotating step, applying a cone-beam algorithm, for example a modified tomographic reconstruction algorithm, to the corrected projection data sets to generate a 3-dimensional image. The size of the spot focus of the beam is reduced to not greater than approximately 1 micron, and even to not greater than approximately 0.5 microns.

  10. Concept for a new high resolution high intensity diffractometer

    Energy Technology Data Exchange (ETDEWEB)

    Stuhr, U. [Paul Scherrer Inst. (PSI), Villigen (Switzerland)

    1997-09-01

    A concept of a new time-of-flight powder-diffractometer for a thermal neutral beam tube at SINQ is presented. The design of the instrument optimises the contradictory conditions of high intensity and high resolution. The high intensity is achieved by using many neutron pulses simultaneously. By analysing the time-angle-pattern of the detected neutrons an assignment of the neutrons to a single pulse is possible. (author) 3 figs., tab., refs.

  11. High sensitivity stand-off detection and quantification of chemical mixtures using an active coherent laser spectrometer (ACLaS)

    Science.gov (United States)

    MacLeod, Neil A.; Weidmann, Damien

    2016-05-01

    High sensitivity detection, identification and quantification of chemicals in a stand-off configuration is a highly sought after capability across the security and defense sector. Specific applications include assessing the presence of explosive related materials, poisonous or toxic chemical agents, and narcotics. Real world field deployment of an operational stand-off system is challenging due to stringent requirements: high detection sensitivity, stand-off ranges from centimeters to hundreds of meters, eye-safe invisible light, near real-time response and a wide chemical versatility encompassing both vapor and condensed phase chemicals. Additionally, field deployment requires a compact, rugged, power efficient, and cost-effective design. To address these demanding requirements, we have developed the concept of Active Coherent Laser Spectrometer (ACLaS), which can be also described as a middle infrared hyperspectral coherent lidar. Combined with robust spectral unmixing algorithms, inherited from retrievals of information from high-resolution spectral data generated by satellitebased spectrometers, ACLaS has been demonstrated to fulfil the above-mentioned needs. ACLaS prototypes have been so far developed using quantum cascade lasers (QCL) and interband cascade lasers (ICL) to exploit the fast frequency tuning capability of these solid state sources. Using distributed feedback (DFB) QCL, demonstration and performance analysis were carried out on narrow-band absorbing chemicals (N2O, H2O, H2O2, CH4, C2H2 and C2H6) at stand-off distances up to 50 m using realistic non cooperative targets such as wood, painted metal, and bricks. Using more widely tunable external cavity QCL, ACLaS has also been demonstrated on broadband absorbing chemicals (dichloroethane, HFC134a, ethylene glycol dinitrate and 4-nitroacetanilide solid) and on complex samples mixing narrow-band and broadband absorbers together in a realistic atmospheric background.

  12. Tables of wavenumbers for the calibration of infrared spectrometers

    CERN Document Server

    Cole, ARH

    1977-01-01

    Tables of Wavenumbers for the Calibration of Infrared Spectrometers, Second Edition is a compilation of tables of wavenumber values for the calibration of infrared spectrometers. It makes the best use of high resolution results and integrates the far infrared data with the higher frequency values. This book is organized in two parts, one for high to medium-resolution spectrometers used by physical chemists and physicists, and the other for medium to low-resolution instruments employed by organic and inorganic chemists. The first part includes tables of wavenumber of infrared absorption lines

  13. A rapid reflectance-difference spectrometer for real-time semiconductor growth monitoring with sub-second time resolution.

    Science.gov (United States)

    Núñez-Olvera, O; Balderas-Navarro, R E; Ortega-Gallegos, J; Guevara-Macías, L E; Armenta-Franco, A; Lastras-Montaño, M A; Lastras-Martínez, L F; Lastras-Martínez, A

    2012-10-01

    We report on a rapid, 32-channel reflectance-difference (RD) spectrometer with sub-second spectra acquisition times and ΔR/R sensitivity in the upper 10(-4) range. The spectrometer is based on a 50 kHz photo-elastic modulator for light polarization modulation and on a lock-in amplifier for signal harmonic analysis. Multichannel operation is allowed by multiplexing the 32 outputs of the spectrometer into the input of the lock-in amplifier. The spectrometer spans a wavelength range of 230 nm that can be tuned to cover E(1) and E(1) + Δ(1) transitions for a number of III-V semiconductors at epitaxial growth temperatures, including GaAs, InAs, AlAs, and their alloys. We present two examples of real-time measurements to demonstrate the performance of the RD spectrometer, namely, the evolution of the RD spectrum of GaAs (001) annealed at 500 °C and the time-dependent RD spectrum during the first stages of the epitaxial growth of In(0.3)Ga(0.7)As on GaAs (001) substrates.

  14. High-Resolution Spectroscopy of the Lunar Sodium Exosphere

    Science.gov (United States)

    Mierkiewicz, E. J.; Oliversen, R. J.; Roesler, F. L.; Lupie, O. L.

    2014-01-01

    We have applied high-resolution Fabry-Perot spectroscopy to the study of the lunar sodium exosphere for the study of exospheric effective temperature and velocity variations. Observing from the National Solar Observatory McMath-Pierce Telescope, we used a dual-etalon Fabry-Perot spectrometer with a resolving power of 180,000 to measure line widths and Doppler shifts of the sodium D2 (5889.95 Å) emission line. Our field of view was 360 km, and measurements were made in equatorial and polar regions from 500 km to 3500 km off the limb. Data were obtained from full moon to 3 days following full moon (waning phase) in March 2009. Measured Doppler line widths within 1100 km of the sunlit east and south lunar limbs for observations between 5 and 40 deg lunar phase imply effective temperatures ranging between 3260 +/- 190 and 1000 +/- 135 K. Preliminary line center analysis indicates velocity displacements between different locations off the lunar limb ranging between 100 and 600 m/s from the lunar rest velocity with a precision of +/-20 to +/-50 m/s depending on brightness. Based on the success of these exploratory observations, an extensive program has been initiated that is expected to constrain lunar atmospheric and surface-process modeling and help quantify source and escape mechanisms.

  15. High-resolution spectroscopy of the lunar sodium exosphere

    Science.gov (United States)

    Mierkiewicz, E. J.; Oliversen, R. J.; Roesler, F. L.; Lupie, O. L.

    2014-06-01

    We have applied high-resolution Fabry-Perot spectroscopy to the study of the lunar sodium exosphere for the study of exospheric effective temperature and velocity variations. Observing from the National Solar Observatory McMath-Pierce Telescope, we used a dual-etalon Fabry-Perot spectrometer with a resolving power of 180,000 to measure line widths and Doppler shifts of the sodium D2 (5889.95 Å) emission line. Our field of view was 360 km, and measurements were made in equatorial and polar regions from 500 km to 3500 km off the limb. Data were obtained from full moon to 3 days following full moon (waning phase) in March 2009. Measured Doppler line widths within 1100 km of the sunlit east and south lunar limbs for observations between 5 and 40° lunar phase imply effective temperatures ranging between 3260 ± 190 and 1000 ± 135 K. Preliminary line center analysis indicates velocity displacements between different locations off the lunar limb ranging between 100 and 600 m/s from the lunar rest velocity with a precision of ±20 to ±50 m/s depending on brightness. Based on the success of these exploratory observations, an extensive program has been initiated that is expected to constrain lunar atmospheric and surface-process modeling and help quantify source and escape mechanisms.

  16. a Highly-Integrated Supersonic-Jet Fourier Transform Microwave Spectrometer

    Science.gov (United States)

    Gou, Qian; Feng, Gang; Grabow, Jens-Uwe

    2017-06-01

    A highly integrated supersonic-jet Fourier-transform microwave spectrometer of coaxially oriented beam-resonator arrangement (COBRA) type, covering 2-20GHz, has been recently built at Chongqing University, China. Built up almost entirely in an NI PXIe chassis, we take the advantage of the NI PXIe-5451 Dual-channel arbitrary waveform generator and the PXIe-5654 RF signal generator to create a spectrometer with wobbling capacity for fast resonator tuning. Based on the I/Q modulation, associate with PXI control and sequence boards built at the Leibniz Universitat Hannover, the design of the spectrometer is much simpler and very compact. The Fabry-Pérot resonator is semi-confocal with a spherical reflector of 630 mm diameter and a radius of 900 mm curvature and one circulator plate reflector of 630 mm diameter. The vacuum is effectuated by a three-stage mechanical (two-stage rotary vane and roots booster) pump at the fore line of a DN630 ISO-F 20000 L/s oil-diffusion pump. The supersonic-jet expansion is pulsed by a general valve Series 9 solenoid valve which is controlled by a general valve IOTA one driver governed by the experiment-sequence generation. First molecular examples to illustrate the performance of the new setup will include OCS and CF_3CHFCl.

  17. High-resolution colorimetric imaging of paintings

    Science.gov (United States)

    Martinez, Kirk; Cupitt, John; Saunders, David R.

    1993-05-01

    With the aim of providing a digital electronic replacement for conventional photography of paintings, a scanner has been constructed based on a 3000 X 2300 pel resolution camera which is moved precisely over a 1 meter square area. Successive patches are assembled to form a mosaic which covers the whole area at c. 20 pels/mm resolution, which is sufficient to resolve the surface textures, particularly craquelure. To provide high color accuracy, a set of seven broad-band interference filters are used to cover the visible spectrum. A calibration procedure based upon a least-mean-squares fit to the color of patches from a Macbeth Colorchecker chart yields an average color accuracy of better than 3 units in the CMC uniform color space. This work was mainly carried out as part of the VASARI project funded by the European Commission's ESPRIT program, involving companies and galleries from around Europe. The system is being used to record images for conservation research, for archival purposes and to assist in computer-aided learning in the field of art history. The paper will describe the overall system design, including the selection of the various hardware components and the design of controlling software. The theoretical basis for the color calibration methodology is described as well as the software for its practical implementation. The mosaic assembly procedure and some of the associated image processing routines developed are described. Preliminary results from the research will be presented.

  18. High resolution CT of temporal bone trauma

    Energy Technology Data Exchange (ETDEWEB)

    Youn, Eun Kyung [Korea General Hospital, Seoul (Korea, Republic of)

    1986-10-15

    Radiographic studies of the temporal bone following head trauma are indicated when there is cerebrospinal fluid otorrhea or rhinorrhoea, hearing loss, or facial nerve paralysis. Plain radiography displays only 17-30% of temporal bone fractures and pluridirectional tomography is both difficult to perform, particularly in the acutely ill patient, and less satisfactory for the demonstration of fine fractures. Consequently, high resolution CT is the imaging method of choice for the investigation of suspected temporal bone trauma and allows special resolution of fine bony detail comparable to that attainable by conventional tomography. Eight cases of temporal bone trauma examined at Korea General Hospital April 1985 through May 1986. The results were as follows: Seven patients (87%) suffered longitudinal fractures. In 6 patients who had purely conductive hearing loss, CT revealed various ossicular chain abnormality. In one patient who had neuro sensory hearing loss, CT demonstrated intract ossicular with a fracture nearing lateral wall of the lateral semicircular canal. In one patient who had mixed hearing loss, CT showed complex fracture.

  19. High Resolution Radar Measurements of Snow Avalanches

    Science.gov (United States)

    McElwaine, Jim; Sovilla, Betty; Vriend, Nathalie; Brennan, Paul; Ash, Matt; Keylock, Chris

    2013-04-01

    Geophysical mass flows, such as snow avalanches, are a major hazard in mountainous areas and have a significant impact on the infrastructure, economy and tourism of such regions. Obtaining a thorough understanding of the dynamics of snow avalanches is crucial for risk assessment and the design of defensive structures. However, because the underlying physics is poorly understood there are significant uncertainties concerning current models, which are poorly validated due to a lack of high resolution data. Direct observations of the denser core of a large avalanche are particularly difficult, since it is frequently obscured by the dilute powder cloud. We have developed and installed a phased array FMCW radar system that penetrates the powder cloud and directly images the dense core with a resolution of around 1 m at 50 Hz over the entire slope. We present data from recent avalanches at Vallee de la Sionne that show a wealth of internal structure and allow the tracking of individual fronts, roll waves and surges down the slope for the first time. We also show good agreement between the radar results and existing measurement systems that record data at particular points on the avalanche track.

  20. Pyramidal fractal dimension for high resolution images

    Science.gov (United States)

    Mayrhofer-Reinhartshuber, Michael; Ahammer, Helmut

    2016-07-01

    Fractal analysis (FA) should be able to yield reliable and fast results for high-resolution digital images to be applicable in fields that require immediate outcomes. Triggered by an efficient implementation of FA for binary images, we present three new approaches for fractal dimension (D) estimation of images that utilize image pyramids, namely, the pyramid triangular prism, the pyramid gradient, and the pyramid differences method (PTPM, PGM, PDM). We evaluated the performance of the three new and five standard techniques when applied to images with sizes up to 8192 × 8192 pixels. By using artificial fractal images created by three different generator models as ground truth, we determined the scale ranges with minimum deviations between estimation and theory. All pyramidal methods (PM) resulted in reasonable D values for images of all generator models. Especially, for images with sizes ≥1024 ×1024 pixels, the PMs are superior to the investigated standard approaches in terms of accuracy and computation time. A measure for the possibility to differentiate images with different intrinsic D values did show not only that the PMs are well suited for all investigated image sizes, and preferable to standard methods especially for larger images, but also that results of standard D estimation techniques are strongly influenced by the image size. Fastest results were obtained with the PDM and PGM, followed by the PTPM. In terms of absolute D values best performing standard methods were magnitudes slower than the PMs. Concluding, the new PMs yield high quality results in short computation times and are therefore eligible methods for fast FA of high-resolution images.

  1. A high-speed automatic spectrometer based on a solid-state non-collinear acousto-optic tunable filter

    Institute of Scientific and Technical Information of China (English)

    Jianhua Zhu(朱建华); Andrew Y.S.Cheng(郑玉臣)

    2003-01-01

    An automatic visible spectrometer based on a non-collinear acousto-optic tunable filter (AOTF) isconstructed for high-speed spectrometry. Its spectral filtering characteristics, such as relationshipsbetween the radio-frequency (RF) driving frequency and the output central wavelength, the outputbandwidth and the central wavelength, its typical spectral point spread function (PSF), and so on, arestudied systematically. The preliminary measurement results of AOTF spectrometer show that it is asolid-state, high-speed, easily controllable by computer-programming, rugged and compact spectroscopicdevice in comparison with a conventional grating spectrometer, and has the potential for widespreadspectrometric applications.

  2. Detection of proximal caries with high-resolution and standard resolution digital radiographic systems

    NARCIS (Netherlands)

    Berkhout, W.E.R.; Verheij, H.G.C.; Syriopoulos, K.; Li, G.; Sanderink, G.C.H.; van der Stelt, P.F.

    2007-01-01

    Aims: The aim of this study was to: (1) compare the diagnostic accuracy of the high-resolution and standard resolution settings of four digital imaging systems for caries diagnosis and (2) compare the effect on the diagnostic accuracy of reducing the high-resolution image sizes to the standard

  3. Improved methods for high resolution electron microscopy

    Energy Technology Data Exchange (ETDEWEB)

    Taylor, J.R.

    1987-04-01

    Existing methods of making support films for high resolution transmission electron microscopy are investigated and novel methods are developed. Existing methods of fabricating fenestrated, metal reinforced specimen supports (microgrids) are evaluated for their potential to reduce beam induced movement of monolamellar crystals of C/sub 44/H/sub 90/ paraffin supported on thin carbon films. Improved methods of producing hydrophobic carbon films by vacuum evaporation, and improved methods of depositing well ordered monolamellar paraffin crystals on carbon films are developed. A novel technique for vacuum evaporation of metals is described which is used to reinforce microgrids. A technique is also developed to bond thin carbon films to microgrids with a polymer bonding agent. Unique biochemical methods are described to accomplish site specific covalent modification of membrane proteins. Protocols are given which covalently convert the carboxy terminus of papain cleaved bacteriorhodopsin to a free thiol. 53 refs., 19 figs., 1 tab.

  4. A new high-resolution TOF technology

    CERN Document Server

    Fonte, Paulo J R; Williams, M C S

    2000-01-01

    In the framework of the ALICE collaboration we have recently studied the performance of multigap Resistive Plate Chambers operated in avalanche mode and at atmospheric pressure for time-of-flight measurements. The detector provided an overall (detector plus electronics) timing accuracy of 120 ps sigma at an efficiency of 98% for MIPs. The chambers had 4 gas gaps of 0.3 mm, each limited by a metallised ceramic plate and a glass plate, with an active dimension of 4'4cm2. The gas mixture contained C2H2F4+5%isobutane+10%SF6. A few percent of streamer discharges, each releasing about 20 pC, was tolerated without any noticeable inconvenience. This detector opens perspectives of affordable and reliable high granularity large area TOF detectors, with an efficiency and a time resolution comparable to existing scintillator-based TOF technology but with significantly, up to an order of magnitude, lower price per channel.

  5. Capillary detectors for high resolution tracking

    CERN Document Server

    Annis, P

    1997-01-01

    We present a new tracking device based on glass capillary bundles or layers filled with highly purified liquid scintillator and read out at one end by means of image intensifiers and CCD devices. A large-volume prototype consisting of 5 × 105 capillaries with a diameter of 20 μm and a length of 180 cm and read out by a megapixel CCD has been tested with muon and neutrino beams at CERN. With this prototype a two track resolution of 33 μm was achieved with passing through muons. Images of neutrino interactions in a capillary bundle have also been acquired and analysed. Read-out chains based on Electron Bombarded CCD (EBCCD) and image pipeline devices are also investigated. Preliminary results obtained with a capillary bundle read out by an EBCCD are presented.

  6. Speleothems as high-resolution paleoflood archives

    Science.gov (United States)

    Denniston, Rhawn F.; Luetscher, Marc

    2017-08-01

    Over the last two decades, speleothems have become widely utilized records of past environmental variability, typically through their stable isotopic and trace elemental chemistry. Numerous speleothem researchers have identified evidence of flooding recorded by detrital layers trapped within speleothems, but few studies have developed paleoflood reconstructions from such samples. Because they can be precisely dated, are generally immune to post-depositional distortion or erosion, and can be tied to a fixed elevational baseline, speleothems hold enormous potential as high-resolution archives of cave floods, and thus as proxies for extreme rainfall or other hydrologic drivers of cave flooding. Here we review speleothem-based paleoflood reconstruction methods, identify potential biases and pitfalls, and suggest standard practices for future studies.

  7. High-resolution CT of otosclerosis

    Energy Technology Data Exchange (ETDEWEB)

    Dewen, Yang; Kodama, Takao; Tono, Tetsuya; Ochiai, Reiji; Kiyomizu, Kensuke; Suzuki, Yukiko; Yano, Takanori; Watanabe, Katsushi [Miyazaki Medical Coll., Kiyotake (Japan)

    1997-11-01

    High-resolution CT (HRCT) scans of thirty-two patients (60 ears) with the clinical diagnosis of fenestral otosclerosis were evaluated retrospectively. HRCT was performed with 1-mm-thick targeted sections and 1-mm (36 ears) or 0.5-mm (10 ears) intervals in the semiaxial projection. Seven patients (14 ears) underwent helical scanning with a 1-mm slice thickness and 1-mm/sec table speed. Forty-five ears (75%) were found to have one or more otospongiotic or otosclerotic foci on HRCT. In most instances (30 ears), the otospongiotic foci were found in the region of the fissula ante fenestram. No significant correlations between CT findings and air conduction threshold were observed. We found a significant relationship between lesions of the labyrinthine capsule and sensorineural hearing loss. We conclude that HRCT is a valuable modality for diagnosing otosclerosis, especially when otospongiotic focus is detected. (author)

  8. High resolution imaging detectors and applications

    CERN Document Server

    Saha, Swapan K

    2015-01-01

    Interferometric observations need snapshots of very high time resolution of the order of (i) frame integration of about 100 Hz or (ii) photon-recording rates of several megahertz (MHz). Detectors play a key role in astronomical observations, and since the explanation of the photoelectric effect by Albert Einstein, the technology has evolved rather fast. The present-day technology has made it possible to develop large-format complementary metal oxide–semiconductor (CMOS) and charge-coupled device (CCD) array mosaics, orthogonal transfer CCDs, electron-multiplication CCDs, electron-avalanche photodiode arrays, and quantum-well infrared (IR) photon detectors. The requirements to develop artifact-free photon shot noise-limited images are higher sensitivity and quantum efficiency, reduced noise that includes dark current, read-out and amplifier noise, smaller point-spread functions, and higher spectral bandwidth. This book aims to address such systems, technologies and design, evaluation and calibration, control...

  9. GRANULOMETRIC MAPS FROM HIGH RESOLUTION SATELLITE IMAGES

    Directory of Open Access Journals (Sweden)

    Catherine Mering

    2011-05-01

    Full Text Available A new method of land cover mapping from satellite images using granulometric analysis is presented here. Discontinuous landscapes such as steppian bushes of semi arid regions and recently growing urban settlements are especially concerned by this study. Spatial organisations of the land cover are quantified by means of the size distribution analysis of the land cover units extracted from high resolution remotely sensed images. A granulometric map is built by automatic classification of every pixel of the image according to the granulometric density inside a sliding neighbourhood. Granulometric mapping brings some advantages over traditional thematic mapping by remote sensing by focusing on fine spatial events and small changes in one peculiar category of the landscape.

  10. High resolution CT of Meckel's cave.

    Science.gov (United States)

    Chui, M; Tucker, W; Hudson, A; Bayer, N

    1985-01-01

    High resolution CT of the parasellar region was carried out in 50 patients studied for suspected pituitary microadenoma, but who showed normal pituitary gland or microadenoma on CT. This control group of patients all showed an ellipsoid low-density area in the posterior parasellar region. Knowledge of the gross anatomy and correlation with metrizamide cisternography suggest that the low density region represents Meckel's cave, rather than just the trigeminal ganglion alone. Though there is considerable variation in the size of Meckel's cave in different patients as well as the two sides of the same patient, the rather constant ellipsoid configuration of the cave in normal subjects will aid in diagnosing small pathological lesions, thereby obviating more invasive cisternography via the transovale or lumbar route. Patients with "idiopathic" tic douloureux do not show a Meckel's cave significantly different from the control group.

  11. Georadar - high resolution geophysical electromagnetic device

    Directory of Open Access Journals (Sweden)

    Janez Stern

    1995-12-01

    Full Text Available Georadar is a high resolution geophysical electromagnetic device that was developed in the first part of the 1980's. In Slovenia it was first tested in 1991 on several objects of economicgeological, geotechnical and hydrogeologic nature.Here its usefulness in karst studied is presented. The first part of the paper deals with description of measurement procedure and methodological bases, and the second part with experience and results of case histories. Shown are radargrams from ornamental stone quarry Hotavlje, calcite mine Stahovica, Golobja jama karstcave near Divača and from highway construction site Razdrto-Čebulovica. All measurements were performed with the georadar instrument Pulse EKKO IV with a lOOMHz antenna according to the method of reflection profiling.

  12. Potential High Resolution Dosimeters For MRT

    Science.gov (United States)

    Bräuer-Krisch, E.; Rosenfeld, A.; Lerch, M.; Petasecca, M.; Akselrod, M.; Sykora, J.; Bartz, J.; Ptaszkiewicz, M.; Olko, P.; Berg, A.; Wieland, M.; Doran, S.; Brochard, T.; Kamlowski, A.; Cellere, G.; Paccagnella, A.; Siegbahn, E. A.; Prezado, Y.; Martinez-Rovira, I.; Bravin, A.; Dusseau, L.; Berkvens, P.

    2010-07-01

    Microbeam Radiation Therapy (MRT) uses highly collimated, quasi-parallel arrays of X-ray microbeams of 50-600 keV, produced by 2nd and 3rd generation synchrotron sources, such as the National Synchrotron Light Source (NSLS) in the U.S., and the European Synchrotron Radiation Facility (ESRF) in France, respectively. High dose rates are necessary to deliver therapeutic doses in microscopic volumes, to avoid spreading of the microbeams by cardiosynchronous movement of the tissues. A small beam divergence and a filtered white beam spectrum in the energy range between 30 and 250 keV results in the advantage of steep dose gradients with a sharper penumbra than that produced in conventional radiotherapy. MRT research over the past 20 years has allowed a vast number of results from preclinical trials on different animal models, including mice, rats, piglets and rabbits. Microbeams in the range between 10 and 100 micron width show an unprecedented sparing of normal radiosensitive tissues as well as preferential damage to malignant tumor tissues. Typically, MRT uses arrays of narrow (˜25-100 micron-wide) microplanar beams separated by wider (100-400 microns centre-to-centre, c-t-c) microplanar spaces. We note that thicker microbeams of 0.1-0.68 mm used by investigators at the NSLS are still called microbeams, although some invesigators in the community prefer to call them minibeams. This report, however, limits it discussion to 25-100 μm microbeams. Peak entrance doses of several hundreds of Gy are surprisingly well tolerated by normal tissues. High resolution dosimetry has been developed over the last two decades, but typical dose ranges are adapted to dose delivery in conventional Radiation Therapy (RT). Spatial resolution in the sub-millimetric range has been achieved, which is currently required for quality assurance measurements in Gamma-knife RT. Most typical commercially available detectors are not suitable for MRT applications at a dose rate of 16000 Gy/s, micron

  13. High-Resolution Movement EEG Classification

    Directory of Open Access Journals (Sweden)

    Jakub Štastný

    2007-01-01

    Full Text Available The aim of the contribution is to analyze possibilities of high-resolution movement classification using human EEG. For this purpose, a database of the EEG recorded during right-thumb and little-finger fast flexion movements of the experimental subjects was created. The statistical analysis of the EEG was done on the subject's basis instead of the commonly used grand averaging. Statistically significant differences between the EEG accompanying movements of both fingers were found, extending the results of other so far published works. The classifier based on hidden Markov models was able to distinguish between movement and resting states (classification score of 94–100%, but it was unable to recognize the type of the movement. This is caused by the large fraction of other (nonmovement related EEG activities in the recorded signals. A classification method based on advanced EEG signal denoising is being currently developed to overcome this problem.

  14. A high-resolution neutron spectra unfolding method using the Genetic Algorithm technique

    CERN Document Server

    Mukherjee, B

    2002-01-01

    The Bonner sphere spectrometers (BSS) are commonly used to determine the neutron spectra within various nuclear facilities. Sophisticated mathematical tools are used to unfold the neutron energy distribution from the output data of the BSS. This paper highlights a novel high-resolution neutron spectra-unfolding method using the Genetic Algorithm (GA) technique. The GA imitates the biological evolution process prevailing in the nature to solve complex optimisation problems. The GA method was utilised to evaluate the neutron energy distribution, average energy, fluence and equivalent dose rates at important work places of a DIDO class research reactor and a high-energy superconducting heavy ion cyclotron. The spectrometer was calibrated with a sup 2 sup 4 sup 1 Am/Be (alpha,n) neutron standard source. The results of the GA method agreed satisfactorily with the results obtained by using the well-known BUNKI neutron spectra unfolding code.

  15. From BASIS to MIRACLES: Benchmarking and perspectives for high-resolution neutron spectroscopy at the ESS

    Directory of Open Access Journals (Sweden)

    Tsapatsaris Nikolaos

    2015-01-01

    Full Text Available Results based on virtual instrument models for the first high-flux, high-resolution, spallation based, backscattering spectrometer, BASIS are presented in this paper. These were verified using the Monte Carlo instrument simulation packages McStas and VITESS. Excellent agreement of the neutron count rate at the sample position between the virtual instrument simulation and experiments was found, in both time and energy distributions. This achievement was only possible after a new component for a bent single crystal analyser in McStas, using a Gaussian approximation, was developed. These findings are pivotal to the conceptual design of the next generation backscattering spectrometer, MIRACLES at the European Spallation Source.

  16. High-resolution transcriptome of human macrophages.

    Directory of Open Access Journals (Sweden)

    Marc Beyer

    Full Text Available Macrophages are dynamic cells integrating signals from their microenvironment to develop specific functional responses. Although, microarray-based transcriptional profiling has established transcriptional reprogramming as an important mechanism for signal integration and cell function of macrophages, current knowledge on transcriptional regulation of human macrophages is far from complete. To discover novel marker genes, an area of great need particularly in human macrophage biology but also to generate a much more thorough transcriptome of human M1- and M1-like macrophages, we performed RNA sequencing (RNA-seq of human macrophages. Using this approach we can now provide a high-resolution transcriptome profile of human macrophages under classical (M1-like and alternative (M2-like polarization conditions and demonstrate a dynamic range exceeding observations obtained by previous technologies, resulting in a more comprehensive understanding of the transcriptome of human macrophages. Using this approach, we identify important gene clusters so far not appreciated by standard microarray techniques. In addition, we were able to detect differential promoter usage, alternative transcription start sites, and different coding sequences for 57 gene loci in human macrophages. Moreover, this approach led to the identification of novel M1-associated (CD120b, TLR2, SLAMF7 as well as M2-associated (CD1a, CD1b, CD93, CD226 cell surface markers. Taken together, these data support that high-resolution transcriptome profiling of human macrophages by RNA-seq leads to a better understanding of macrophage function and will form the basis for a better characterization of macrophages in human health and disease.

  17. Surface Plasmon Based Spectrometer

    Science.gov (United States)

    Wig, Andrew; Passian, Ali; Boudreaux, Philip; Ferrell, Tom

    2008-03-01

    A spectrometer that uses surface plasmon excitation in thin metal films to separate light into its component wavelengths is described. The use of surface plasmons as a dispersive medium sets this spectrometer apart from prism, grating, and interference based variants and allows for the miniaturization of this device. Theoretical and experimental results are presented for two different operation models. In the first case surface plasmon tunneling in the near field is used to provide transmission spectra of different broad band-pass, glass filters across the visible wavelength range with high stray-light rejection at low resolution as well as absorption spectra of chlorophyll extracted from a spinach leaf. The second model looks at the far field components of surface plasmon scattering.

  18. A simplified spectrometer based on a fast digital oscilloscope for the measurement of high energy $\\gamma$-rays

    CERN Document Server

    Markochev, S S

    2014-01-01

    A simplified digital spectrometer for the study of $\\gamma$-rays with energies up to $\\sim100$ MeV is presented and tested. The spectrometer is only consisted of a fast digital oscilloscope and three scintillation detectors which can work in single or in coincidence modes: two BGO-detectors comprising $\\varnothing\\,7.62\\times7.62$ cm BGO-crystalls and one plastic detector which includes an organic polystyrene-based scintillator. The basic properties of the spectrometer (energy resolution, time resolution, $\\gamma$-rays detection efficiency) were studied exhaustively also using a Geant4-based Monte-Carlo simulation. Several numerical algorithms for processing of waveforms in offline mode were proposed and tested to perform digital timing, pulse area measurement and processing of pile-up events without rejection. As a result, the spectrometer demonstrated $\\sim10\\%$ better energy resolution than was obtained by a common 10-bit CAMAC ADC with the same detectors. And the developed algorithm based on the pulse sha...

  19. HCN Polymers: Toward Structure Comprehension Using High Resolution Mass Spectrometry

    Science.gov (United States)

    Bonnet, Jean-Yves; Thissen, Roland; Frisari, Ma; Vuitton, Veronique; Quirico, Eric; Le Roy, Léna; Fray, Nicolas; Cottin, Hervé; Horst, Sarah; Yelle, Roger

    A lot of solar system materials, including cometary ices and Titan aerosols, contain dark matter that can be interpreted as complex nitrogen bearing organic matter [1]. In laboratory experi-ments, HCN polymers are thus analogs of great interest. In fact they may be present in Titan atmosphere and in comet nuclei and then reprocessed as a CN distributed source [2], when ices began to sublimate and ejects from the nucleus organic matter grains [3]. The presence of HCN polymers is suggested because HCN molecule has been directly observed in 1P/Halley comet [4] and others. HCN polymers are also of prebiotic interest [5] as it can form amino acid under hydrolysis conditions. Even if they have been studied during the last decades, their chemical composition and structure are still poorly understood, and a great analytical effort has to be continued. In this way we present a high resolution mass spectrometry (HRMS) and a high resolution tandem mass spectrometry (MS/HRMS) analysis of HCN polymers. It was shown [6] that this is a suitable technique to elucidate composition and structure of the soluble part of tholins analogs of Titan's atmosphere aerosols. HCN polymers have never been studied by HRMS, thus we used a LTQ-Orbitrap XL high resolution mass spectrometer to analyse the HCN polymers. These are produced at LISA by direct polymerisation of pure liquid HCN, catalyzed by ammonia. HCN polymers have been completely dissolved in methanol and then injected in the mass spectrometer by ElectroSpray Ionization (ESI). This atmospheric pressure ionization process produces protonated or deprotonated ions, but it does not fragment molecules. Thus HRMS, allows a direct access to the stoechiometry of all the ionizable molecules present in the samples. Fragmentation analyses (MS/MS) of selected ions have also been performed. Thess analysis provide information about the different chemical fonctionnalities present in HCN poly-mers and also about their structure. Thus we are able to

  20. Soft x-ray blazed transmission grating spectrometer with high resolving power and extended bandpass

    Science.gov (United States)

    Heilmann, Ralf K.; Bruccoleri, Alexander Robert; Schattenburg, Mark

    2016-04-01

    A number of high priority questions in astrophysics can be addressed by a state-of-the-art soft x-ray grating spectrometer, such as the role of Active Galactic Nuclei in galaxy and star formation, characterization of the Warm-Hot Intergalactic Medium and the “missing baryon” problem, characterization of halos around the Milky Way and nearby galaxies, as well as stellar coronae and surrounding winds and disks. An Explorer-scale, large-area (> 1,000 cm2), high resolving power (R = λ/Δλ > 3,000) soft x-ray grating spectrometer is highly feasible based on Critical-Angle Transmission (CAT) grating technology. Still significantly higher performance can be provided by a CAT grating spectrometer on an X-ray-Surveyor-type mission. CAT gratings combine the advantages of blazed reflection gratings (high efficiency, use of higher diffraction orders) with those of conventional transmission gratings (low mass, relaxed alignment tolerances and temperature requirements, transparent at higher energies) with minimal mission resource requirements. They are high-efficiency blazed transmission gratings that consist of freestanding, ultra-high aspect-ratio grating bars fabricated from silicon-on-insulator (SOI) wafers using advanced anisotropic dry and wet etch techniques. Blazing is achieved through grazing-incidence reflection off the smooth grating bar sidewalls. The reflection properties of silicon are well matched to the soft x-ray band. Nevertheless, CAT gratings with sidewalls made of higher atomic number elements allow extension of the CAT grating principle to higher energies and larger dispersion angles. We show x-ray data from metal-coated CAT gratings and demonstrate efficient blazing to higher energies and larger blaze angles than possible with silicon alone. We also report on measurements of the resolving power of a breadboard CAT grating spectrometer consisting of a Wolter-I slumped-glass focusing mirror pair from Goddard Space Flight Center and CAT gratings, to be

  1. Nanograting-based compact VUV spectrometer and beam profiler for in-situ characterization of high-order harmonic generation light sources

    Energy Technology Data Exchange (ETDEWEB)

    Kornilov, Oleg; Wilcox, Russell; Gessner, Oliver

    2010-07-09

    A compact, versatile device for VUV beam characterization is presented. It combines the functionalities of a VUV spectrometer and a VUV beam profiler in one unit and is entirely supported by a standard DN200 CF flange. The spectrometer employs a silicon nitride transmission nanograting in combination with a micro-channel plate based imaging detector. This enables the simultaneous recording of wavelengths ranging from 10 nm to 80 nm with a resolution of 0.25 nm to 0.13 nm. Spatial beam profiles with diameters up to 10 mm are imaged with 0.1 mm resolution. The setup is equipped with an in-vacuum translation stage that allows for in situ switching between the spectrometer and beam profiler modes and for moving the setup out of the beam. The simple, robust design of the device is well suited for non-intrusive routine characterization of emerging laboratory- and accelerator-based VUV light sources. Operation of the device is demonstrated by characterizing the output of a femtosecond high-order harmonic generation light source.

  2. Nanograting-based compact vacuum ultraviolet spectrometer and beam profiler for in situ characterization of high-order harmonic generation light sources.

    Science.gov (United States)

    Kornilov, Oleg; Wilcox, Russell; Gessner, Oliver

    2010-06-01

    A compact, versatile device for vacuum ultraviolet (VUV) beam characterization is presented. It combines the functionalities of a VUV spectrometer and a VUV beam profiler in one unit and is entirely supported by a standard DN200 CF flange. The spectrometer employs a silicon nitride transmission nanograting in combination with a microchannel plate-based imaging detector. This enables the simultaneous recording of wavelengths ranging from 10 to 80 nm with a resolution of 0.25-0.13 nm. Spatial beam profiles with diameters up to 10 mm are imaged with 0.1 mm resolution. The setup is equipped with an in-vacuum translation stage that allows for in situ switching between the spectrometer and beam profiler modes and for moving the setup out of the beam. The simple, robust design of the device is well suited for nonintrusive routine characterization of emerging laboratory- and accelerator-based VUV light sources. Operation of the device is demonstrated by characterizing the output of a femtosecond high-order harmonic generation light source.

  3. First measurements of highly ionized impurity emission distribution by grazing-incidence flat-field extreme ultraviolet spectrometer in HL-2A.

    Science.gov (United States)

    Cui, Zhengying; Dong, Chunfeng; Zhou, Hangyu; Morita, Shigeru; Sun, Ping; Fu, Bingzhong; Lu, Ping; Ding, Xuantong; Yang, Qingwei; Duan, Xuru

    2014-11-01

    A space-resolved grazing-incidence flat-field extreme ultraviolet (EUV) spectrometer has been developed in the HL-2A tokamak to measure vertical impurity emission profiles with simultaneous spectral, temporal, and spatial resolution. The spectrometer working in the wavelength range of 30-500 Å has been equipped with a gold-coated varied-line-spacing holographic grating with curvature of 5606 mm and a back illuminated charge-coupled device with size of 6.6 × 26.6 mm(2) (255 × 1024 pixels). A lower half of the HL-2A plasma with averaged minor radius of 40 cm is observed when the spectrometer with horizontal dispersion is placed at a distance of 7.5 m away from the plasma center. An excellent spatial resolution of 12 mm is achieved when a space-resolved slit with vertical width of 0.5 mm is adopted. The radial profiles of intrinsic impurities in several ionization stages have been measured with high throughput and extremely low stray light.

  4. Development of Fast High-Resolution Muon Drift-Tube Detectors for High Counting Rates

    CERN Document Server

    INSPIRE-00287945; Dubbert, J.; Horvat, S.; Kortner, O.; Kroha, H.; Legger, F.; Richter, R.; Adomeit, S.; Biebel, O.; Engl, A.; Hertenberger, R.; Rauscher, F.; Zibell, A.

    2011-01-01

    Pressurized drift-tube chambers are e?cient detectors for high-precision tracking over large areas. The Monitored Drift-Tube (MDT) chambers of the muon spectrometer of the ATLAS detector at the Large Hadron Collider (LHC) reach a spatial resolution of 35 micons and almost 100% tracking e?ciency with 6 layers of 30 mm diameter drift tubes operated with Ar:CO2 (93:7) gas mixture at 3 bar and a gas gain of 20000. The ATLAS MDT chambers are designed to cope with background counting rates due to neutrons and gamma-rays of up to about 300 kHz per tube which will be exceeded for LHC luminosities larger than the design value of 10-34 per square cm and second. Decreasing the drift-tube diameter to 15 mm while keeping the other parameters, including the gas gain, unchanged reduces the maximum drift time from about 700 ns to 200 ns and the drift-tube occupancy by a factor of 7. New drift-tube chambers for the endcap regions of the ATLAS muon spectrometer have been designed. A prototype chamber consisting of 12 times 8 l...

  5. High-resolution downscaling for hydrological management

    Science.gov (United States)

    Ulbrich, Uwe; Rust, Henning; Meredith, Edmund; Kpogo-Nuwoklo, Komlan; Vagenas, Christos

    2017-04-01

    Hydrological modellers and water managers require high-resolution climate data to model regional hydrologies and how these may respond to future changes in the large-scale climate. The ability to successfully model such changes and, by extension, critical infrastructure planning is often impeded by a lack of suitable climate data. This typically takes the form of too-coarse data from climate models, which are not sufficiently detailed in either space or time to be able to support water management decisions and hydrological research. BINGO (Bringing INnovation in onGOing water management; ) aims to bridge the gap between the needs of hydrological modellers and planners, and the currently available range of climate data, with the overarching aim of providing adaptation strategies for climate change-related challenges. Producing the kilometre- and sub-daily-scale climate data needed by hydrologists through continuous simulations is generally computationally infeasible. To circumvent this hurdle, we adopt a two-pronged approach involving (1) selective dynamical downscaling and (2) conditional stochastic weather generators, with the former presented here. We take an event-based approach to downscaling in order to achieve the kilometre-scale input needed by hydrological modellers. Computational expenses are minimized by identifying extremal weather patterns for each BINGO research site in lower-resolution simulations and then only downscaling to the kilometre-scale (convection permitting) those events during which such patterns occur. Here we (1) outline the methodology behind the selection of the events, and (2) compare the modelled precipitation distribution and variability (preconditioned on the extremal weather patterns) with that found in observations.

  6. The high resolution neutrino calorimeter KARMEN

    Energy Technology Data Exchange (ETDEWEB)

    Drexlin, G.; Eberhard, V.; Gemmeke, H.; Giorginis, G.; Grandegger, W.; Gumbsheimer, R.; Hucker, H.; Husson, L.; Kleinfeller, J.; Maschuw, R.; Plischke, P.; Spohrer, G.; Schmidt, F.K.; Wochele, J.; Woelfle, S.; Zeitnitz, B. (Kernforschungszentrum Karlsruhe GmbH (Germany, F.R.). Inst. fuer Kernphysik 1 Karlsruhe Univ. (T.H.) (Germany, F.R.). Inst. fuer Experimentelle Kernphysik); Bodman, B.; Burtak, F.; Finckh, E.; Glombik, A.; Kretschmer, W.; Schilling, F.; Voetisch, D. (Erlangen-Nuernberg Univ., Erlangen (Germany, F.R.). Physikalisches Inst.); Edgington, J.A.; Gorringe, T.; Malik, A. (Queen Mary Coll., London (UK)); Booth, N.E. (Oxford Univ. (UK)); Dodd, A.; Payne, A.G.D. (Rutherford Appleton Lab., Chilton (UK))

    1990-04-15

    KARMEN is a 56 t scintillation calorimeter designed for beam dump neutrino experiments at the neutron spallation facility ISIS of the Rutherford Appleton Laboratory. The calorimetric properties are demonstrated by cosmic muons and laser calibration. The measured energy resolution of the detector is {sigma}{sub E}/E{approx equal}11.5%/{radical}E(MeV), the position resolution {sigma}{sub x}=5 cm and the timing resolution {sigma}{sub t}{approx equal}350 ps. (orig.).

  7. Applications of High Resolution Mid-Infrared Spectroscopy for Atmospheric and Environmental Measurements

    Science.gov (United States)

    Roscioli, Joseph R.; McManus, J. Barry; Nelson, David; Zahniser, Mark; Herndon, Scott C.; Shorter, Joanne; Yacovitch, Tara I.; Jervis, Dylan; Dyroff, Christoph; Kolb, Charles E.

    2016-06-01

    For the past 20 years, high resolution infrared spectroscopy has served as a valuable tool to measure gas-phase concentrations of ambient gas samples. We review recent advances in atmospheric sampling using direct absorption high resolution mid-infrared spectroscopy from the perspective of light sources, detectors, and optical designs. Developments in diode, quantum cascade and interband cascade laser technology have led to thermoelectrically-cooled single-mode laser sources capable of operation between 800 wn and 3100 wn, with 10 mW power. Advances in detector and preamplifier technology have yielded thermoelectriocally-cooled sensors capable of room-temperature operation with extremely high detectivities. Finally, novel spectrometer optical designs have led to robust multipass absorption cells capable of >400 m effective pathlength in a compact package. In combination with accurate spectroscopic databases, these developments have afforded dramatic improvements in measurement sensitivity, accuracy, precision, and selectivity. We will present several examples of the applications of high resolution mid-IR spectrometers in real-world field measurements at sampling towers and aboard mobile platforms such as vehicles and airplanes.

  8. High resolution image reconstruction from projection of low resolution images differing in subpixel shifts

    Science.gov (United States)

    Mareboyana, Manohar; Le Moigne, Jacqueline; Bennett, Jerome

    2016-05-01

    In this paper, we demonstrate simple algorithms that project low resolution (LR) images differing in subpixel shifts on a high resolution (HR) also called super resolution (SR) grid. The algorithms are very effective in accuracy as well as time efficiency. A number of spatial interpolation techniques using nearest neighbor, inverse-distance weighted averages, Radial Basis Functions (RBF) etc. are used in projection. For best accuracy of reconstructing SR image by a factor of two requires four LR images differing in four independent subpixel shifts. The algorithm has two steps: i) registration of low resolution images and (ii) shifting the low resolution images to align with reference image and projecting them on high resolution grid based on the shifts of each low resolution image using different interpolation techniques. Experiments are conducted by simulating low resolution images by subpixel shifts and subsampling of original high resolution image and the reconstructing the high resolution images from the simulated low resolution images. The results of accuracy of reconstruction are compared by using mean squared error measure between original high resolution image and reconstructed image. The algorithm was tested on remote sensing images and found to outperform previously proposed techniques such as Iterative Back Projection algorithm (IBP), Maximum Likelihood (ML) algorithms. The algorithms are robust and are not overly sensitive to the registration inaccuracies.

  9. High Resolution Image Reconstruction from Projection of Low Resolution Images DIffering in Subpixel Shifts

    Science.gov (United States)

    Mareboyana, Manohar; Le Moigne-Stewart, Jacqueline; Bennett, Jerome

    2016-01-01

    In this paper, we demonstrate a simple algorithm that projects low resolution (LR) images differing in subpixel shifts on a high resolution (HR) also called super resolution (SR) grid. The algorithm is very effective in accuracy as well as time efficiency. A number of spatial interpolation techniques using nearest neighbor, inverse-distance weighted averages, Radial Basis Functions (RBF) etc. used in projection yield comparable results. For best accuracy of reconstructing SR image by a factor of two requires four LR images differing in four independent subpixel shifts. The algorithm has two steps: i) registration of low resolution images and (ii) shifting the low resolution images to align with reference image and projecting them on high resolution grid based on the shifts of each low resolution image using different interpolation techniques. Experiments are conducted by simulating low resolution images by subpixel shifts and subsampling of original high resolution image and the reconstructing the high resolution images from the simulated low resolution images. The results of accuracy of reconstruction are compared by using mean squared error measure between original high resolution image and reconstructed image. The algorithm was tested on remote sensing images and found to outperform previously proposed techniques such as Iterative Back Projection algorithm (IBP), Maximum Likelihood (ML), and Maximum a posterior (MAP) algorithms. The algorithm is robust and is not overly sensitive to the registration inaccuracies.

  10. Photoacoustic absorption spectrometer for highly transparent dielectrics with parts-per-million sensitivity

    Science.gov (United States)

    Waasem, Niklas; Fieberg, Stephan; Hauser, Janosch; Gomes, Gregory; Haertle, Daniel; Kühnemann, Frank; Buse, Karsten

    2013-02-01

    A sensitive photoacoustic absorption spectrometer for highly transparent solids has been built and tested. As the light source an optical parametrical oscillator pumped by a nanosecond pulse laser with 10 Hz repetition rate is employed, covering the complete wavelength range from 407 to 2600 nm. A second-harmonic-generation unit extends the range of accessible wavelengths down to 212 nm. A lead-zirconate-titanate piezo transducer, directly coupled to the sample, detects the photoacoustically generated sound waves. Absorption spectra of lithium triborate, lithium niobate, and alpha barium borate crystals with absorption coefficients down to 10-5 cm-1 are presented.

  11. High Resolution Airborne Shallow Water Mapping

    Science.gov (United States)

    Steinbacher, F.; Pfennigbauer, M.; Aufleger, M.; Ullrich, A.

    2012-07-01

    In order to meet the requirements of the European Water Framework Directive (EU-WFD), authorities face the problem of repeatedly performing area-wide surveying of all kinds of inland waters. Especially for mid-sized or small rivers this is a considerable challenge imposing insurmountable logistical efforts and costs. It is therefore investigated if large-scale surveying of a river system on an operational basis is feasible by employing airborne hydrographic laser scanning. In cooperation with the Bavarian Water Authority (WWA Weilheim) a pilot project was initiated by the Unit of Hydraulic Engineering at the University of Innsbruck and RIEGL Laser Measurement Systems exploiting the possibilities of a new LIDAR measurement system with high spatial resolution and high measurement rate to capture about 70 km of riverbed and foreland for the river Loisach in Bavaria/Germany and the estuary and parts of the shoreline (about 40km in length) of lake Ammersee. The entire area surveyed was referenced to classic terrestrial cross-section surveys with the aim to derive products for the monitoring and managing needs of the inland water bodies forced by the EU-WFD. The survey was performed in July 2011 by helicopter and airplane and took 3 days in total. In addition, high resolution areal images were taken to provide an optical reference, offering a wide range of possibilities on further research, monitoring, and managing responsibilities. The operating altitude was about 500 m to maintain eye-safety, even for the aided eye, the airspeed was about 55 kts for the helicopter and 75 kts for the aircraft. The helicopter was used in the alpine regions while the fixed wing aircraft was used in the plains and the urban area, using appropriate scan rates to receive evenly distributed point clouds. The resulting point density ranged from 10 to 25 points per square meter. By carefully selecting days with optimum water quality, satisfactory penetration down to the river bed was achieved

  12. Logging Data High-Resolution Sequence Stratigraphy

    Institute of Scientific and Technical Information of China (English)

    Li Hongqi; Xie Yinfu; Sun Zhongchun; Luo Xingping

    2006-01-01

    The recognition and contrast of bed sets in parasequence is difficult in terrestrial basin high-resolution sequence stratigraphy. This study puts forward new methods for the boundary identification and contrast of bed sets on the basis of manifold logging data. The formation of calcareous interbeds, shale resistivity differences and the relation of reservoir resistivity to altitude are considered on the basis of log curve morphological characteristics, core observation, cast thin section, X-ray diffraction and scanning electron microscopy. The results show that the thickness of calcareous interbeds is between 0.5 m and 2 m, increasing on weathering crusts and faults. Calcareous interbeds occur at the bottom of Reservoir resistivity increases with altitude. Calcareous interbeds may be a symbol of recognition for the boundary of bed sets and isochronous contrast bed sets, and shale resistivity differences may confirm the stack relation and connectivity of bed sets. Based on this, a high-rcsolution chronostratigraphic framework of Xi-1 segment in Shinan area, Junggar basin is presented, and the connectivity of bed sets and oil-water contact is confirmed. In this chronostratigraphic framework, the growth order, stack mode and space shape of bed sets are qualitatively and quantitatively described.

  13. High resolution low frequency ultrasonic tomography.

    Science.gov (United States)

    Lasaygues, P; Lefebvre, J P; Mensah, S

    1997-10-01

    Ultrasonic reflection tomography results from a linearization of the inverse acoustic scattering problem, named the inverse Born approximation. The goal of ultrasonic reflection tomography is to obtain reflectivity images from backscattered measurements. This is a Fourier synthesis problem and the first step is to correctly cover the frequency space of the object. For this inverse problem, we use the classical algorithm of tomographic reconstruction by summation of filtered backprojections. In practice, only a limited number of views are available with our mechanical rig, typically 180, and the frequency bandwidth of the pulses is very limited, typically one octave. The resolving power of the system is them limited by the bandwidth of the pulse. Low and high frequencies can be restored by use of a deconvolution algorithm that enhances resolution. We used a deconvolution technique based on the Papoulis method. The advantage of this technique is conservation of the overall frequency information content of the signals. The enhancement procedure was tested by imaging a square aluminium rod with a cross-section less than the wavelength. In this application, the central frequency of the transducer was 250 kHz so that the central wavelength was 6 mm whereas the cross-section of the rod was 4 mm. Although the Born approximation was not theoretically valid in this case (high contrast), a good reconstruction was obtained.

  14. Automatic abundance analysis of high resolution spectra

    CERN Document Server

    Bonifacio, P; Bonifacio, Piercarlo; Caffau, Elisabetta

    2003-01-01

    We describe an automatic procedure for determining abundances from high resolution spectra. Such procedures are becoming increasingly important as large amounts of data are delivered from 8m telescopes and their high-multiplexing fiber facilities, such as FLAMES on ESO-VLT. The present procedure is specifically targeted for the analysis of spectra of giants in the Sgr dSph; however, the procedure may be, in principle, tailored to analyse stars of any type. Emphasis is placed on the algorithms and on the stability of the method; the external accuracy rests, ultimately, on the reliability of the theoretical models (model-atmospheres, synthetic spectra) used to interpret the data. Comparison of the results of the procedure with the results of a traditional analysis for 12 Sgr giants shows that abundances accurate at the level of 0.2 dex, comparable with that of traditional analysis of the same spectra, may be derived in a fast and efficient way. Such automatic procedures are not meant to replace the traditional ...

  15. Supporting observation campaigns with high resolution modeling

    Science.gov (United States)

    Klocke, Daniel; Brueck, Matthias; Voigt, Aiko

    2017-04-01

    High resolution simulation in support of measurement campaigns offers a promising and emerging way to create large-scale context for small-scale observations of clouds and precipitation processes. As these simulation include the coupling of measured small-scale processes with the circulation, they also help to integrate the research communities from modeling and observations and allow for detailed model evaluations against dedicated observations. In connection with the measurement campaign NARVAL (August 2016 and December 2013) simulations with a grid-spacing of 2.5 km for the tropical Atlantic region (9000x3300 km), with local refinement to 1.2 km for the western part of the domain, were performed using the icosahedral non-hydrostatic (ICON) general circulation model. These simulations are again used to drive large eddy resolving simulations with the same model for selected days in the high definition clouds and precipitation for advancing climate prediction (HD(CP)2) project. The simulations are presented with the focus on selected results showing the benefit for the scientific communities doing atmospheric measurements and numerical modeling of climate and weather. Additionally, an outlook will be given on how similar simulations will support the NAWDEX measurement campaign in the North Atlantic and AC3 measurement campaign in the Arctic.

  16. High-resolution infrared flash kinetic spectroscopy of OH radicals

    Energy Technology Data Exchange (ETDEWEB)

    Schiffman, A.; Nelson, D.D. Jr.; Robinson, M.S.; Nesbitt, D.J. (Univ. of Colorado, Boulder (United States) National Inst. of Standards and Tech., Boulder, CO (United States))

    1991-04-04

    A high-resolution infrared flash kinetic spectrometer is used for time- and frequency-resolved studies of the OH radical. OH is produced by 193-nm excimer laser photolysis of HNO{sub 3}/buffer gas mixtures in a 100-cm flow tube and is probed via weak fractional absorption of light from a widely tunable (2.35-3.59 {mu}m) single-mode ({Delta}{nu} {le} 2 MHz) color center laser. The IR absorption technique allows fast ({le}10{sup {minus}6} s), sensitive (<10{sup 9} radicals/cm{sup 3} per quantum state) detection of OH and is designed to permit determination of absolute OH number densities. The spectrometer is used to measure rate constants for the reactions of OH with ethane (k{sub 1}), propane (k{sub 2}), n-butane (k{sub 3}), and isobutane (k{sub 4}). The reliability of these measurements is tested on a variety of rotational, spin-orbit, and {lambda}-doublet states, with several buffer gases, and over more than an order of magnitude of alkane concentrations. The resulting rate constants are, in units of 10{sup {minus}12} cm{sup 3} molecule{sup {minus}1} s{sup {minus}1}, k{sub 1} = 0.243 {plus minus} 0.012, k{sub 2} = 1.02 {plus minus} 0.05, k{sub 3} = 2.35 {plus minus} 0.08, and k{sub 4} = 2.11 {plus minus} 0.09. The rate constants for the ethane, n-butane, and isobutane reactions agree with some previous determinations but are found to be between 10% and 25% lower than values currently used in atmospheric modeling; it is recommended that these values be revised to reflect the lower rates from this study. Current models of atmospheric air flow based on these rate constants, as well as those previously accepted values, are found to be inconsistent with daily changes in observed atmospheric alkane concentrations.

  17. Resolution enhancement of low quality videos using a high-resolution frame

    NARCIS (Netherlands)

    Pham, T.Q.; Van Vliet, L.J.; Schutte, K.

    2006-01-01

    This paper proposes an example-based Super-Resolution (SR) algorithm of compressed videos in the Discrete Cosine Transform (DCT) domain. Input to the system is a Low-Resolution (LR) compressed video together with a High-Resolution (HR) still image of similar content. Using a training set of correspo

  18. Airborne ROWS data report for the high resolution experiment, June 1993

    Science.gov (United States)

    Vandemark, D.; Hines, D.; Bailey, S.; Stewart, K.

    1994-01-01

    Airborne radar ocean wave spectrometer (ROWS) data collected during the Office of Naval Research's High Resolution Remote Sensing Experiment of June 1993 are presented. This data summary covers six flights made using NASA's T-39 aircraft over a region of the North Atlantic off the coast of North Carolina and includes multiple crossings of the gulf stream. The Ku-band ROWS was operated in a configuration which continuously switched between an altimeter and a spectrometer channel. Data derived from the two channels include altimeter radar cross section, altimeter-derived sea surface mean square slope and wind speed, and directional and nondirectional longwave spectra. Discussion is provided for several events of particular interest.

  19. Molecular beam mass spectrometer equipped with a catalytic wall reactor for in situ studies in high temperature catalysis research

    Science.gov (United States)

    Horn, R.; Ihmann, K.; Ihmann, J.; Jentoft, F. C.; Geske, M.; Taha, A.; Pelzer, K.; Schlögl, R.

    2006-05-01

    A newly developed apparatus combining a molecular beam mass spectrometer and a catalytic wall reactor is described. The setup has been developed for in situ studies of high temperature catalytic reactions (>1000°C), which involve besides surface reactions also gas phase reactions in their mechanism. The goal is to identify gas phase radicals by threshold ionization. A tubular reactor, made from the catalytic material, is positioned in a vacuum chamber. Expansion of the gas through a 100μm sampling orifice in the reactor wall into differentially pumped nozzle, skimmer, and collimator chambers leads to the formation of a molecular beam. A quadrupole mass spectrometer with electron impact ion source designed for molecular beam inlet and threshold ionization measurements is used as the analyzer. The sampling time from nozzle to detector is estimated to be less than 10ms. A detection time resolution of up to 20ms can be reached. The temperature of the reactor is measured by pyrometry. Besides a detailed description of the setup components and the physical background of the method, this article presents measurements showing the performance of the apparatus. After deriving the shape and width of the energy spread of the ionizing electrons from measurements on N2 and He we estimated the detection limit in threshold ionization measurements using binary mixtures of CO in N2 to be in the range of several hundreds of ppm. Mass spectra and threshold ionization measurements recorded during catalytic partial oxidation of methane at 1250°C on a Pt catalyst are presented. The detection of CH3• radicals is successfully demonstrated.

  20. The High Time Resolution Radio Sky

    Science.gov (United States)

    Thornton, D.

    2013-11-01

    Pulsars are laboratories for extreme physics unachievable on Earth. As individual sources and possible orbital companions can be used to study magnetospheric, emission, and superfluid physics, general relativistic effects, and stellar and binary evolution. As populations they exhibit a wide range of sub-types, with parameters varying by many orders of magnitude signifying fundamental differences in their evolutionary history and potential uses. There are currently around 2200 known pulsars in the Milky Way, the Magellanic clouds, and globular clusters, most of which have been discovered with radio survey observations. These observations, as well as being suitable for detecting the repeating signals from pulsars, are well suited for identifying other transient astronomical radio bursts that last just a few milliseconds that either singular in nature, or rarely repeating. Prior to the work of this thesis non-repeating radio transients at extragalactic distances had possibly been discovered, however with just one example status a real astronomical sources was in doubt. Finding more of these sources was a vital to proving they were real and to open up the universe for millisecond-duration radio astronomy. The High Time Resolution Universe survey uses the multibeam receiver on the 64-m Parkes radio telescope to search the whole visible sky for pulsars and transients. The temporal and spectral resolution of the receiver and the digital back-end enable the detection of relatively faint, and distant radio sources. From the Parkes telescope a large portion of the Galactic plane can be seen, a rich hunting ground for radio pulsars of all types, while previously poorly surveyed regions away from the Galactic plane are also covered. I have made a number of pulsar discoveries in the survey, including some rare systems. These include PSR J1226-6208, a possible double neutron star system in a remarkably circular orbit, PSR J1431-471 which is being eclipsed by its companion with

  1. Bulk and integrated acousto-optic spectrometers for molecular astronomy with heterodyne spectrometers

    Science.gov (United States)

    Chin, G.; Buhl, D.; Florez, J. M.

    1981-01-01

    A survey of acousto-optic spectrometers for molecular astronomy is presented, noting a technique of combining the acoustic bending of a collimated coherent light beam with a Bragg cell followed by an array of sensitive photodetectors. This acousto-optic spectrometer has a large bandwidth, a large number of channels, high resolution, and is energy efficient. Receiver development has concentrated on high-frequency heterodyne systems for the study of the chemical composition of the interstellar medium. RF spectrometers employing acousto-optic diffraction cells are described. Acousto-optic techniques have been suggested for applications to electronic warfare, electronic countermeasures and electronic support systems. Plans to use integrated optics for the further miniaturization of acousto-optic spectrometers are described. Bulk acousto-optic spectrometers with 300 MHz and 1 GHz bandwidths are being developed for use in the back-end of high-frequency heterodyne receivers for astronomical research.

  2. Pulse Rise Time Characterization of a High Pressure Xenon Gamma Detector for use in Resolution Enhancement

    CERN Document Server

    Troyer, G L

    2000-01-01

    High pressure xenon ionization chamber detectors are possible alternatives to traditional thallium doped sodium iodide (NaI(Tl)) and hyperpure germanium as gamma spectrometers in certain applications. Xenon detectors incorporating a Frisch grid exhibit energy resolutions comparable to cadmium/zinc/telluride (CZT) (e.g. 2% (at) 662keV) but with far greater sensitive volumes. The Frisch grid reduces the position dependence of the anode pulse risetimes, but it also increases the detector vibration sensitivity, anode capacitance, voltage requirements and mechanical complexity. We have been investigating the possibility of eliminating the grid electrode in high-pressure xenon detectors and preserving the high energy resolution using electronic risetime compensation methods. A two-electrode cylindrical high pressure xenon gamma detector coupled to time-to-amplitude conversion electronics was used to characterize the pulse rise time of deposited gamma photons. Time discrimination was used to characterize the pulse r...

  3. Photonuclear reaction based high-energy x-ray spectrometer to cover from 2 MeV to 20 MeV

    Energy Technology Data Exchange (ETDEWEB)

    Sakata, S., E-mail: sakata-s@ile.osaka-u.ac.jp; Arikawa, Y.; Kojima, S.; Ikenouchi, T.; Nagai, T.; Abe, Y.; Inoue, H.; Morace, A.; Utsugi, M.; Nishimura, H.; Nakai, M.; Shiraga, H.; Fujioka, S.; Azechi, H. [Institute of Laser Engineering, Osaka University, Suita 565-0871 (Japan); Kato, R. [Institute of Scientific and Industrial Research, Osaka University, Ibaraki 565-0047 (Japan)

    2014-11-15

    A photonuclear-reaction-based hard x-ray spectrometer is developed to measure the number and energy spectrum of fast electrons generated by interactions between plasma and intense laser light. In this spectrometer, x-rays are converted to neutrons through photonuclear reactions, and the neutrons are counted with a bubble detector that is insensitive to x-rays. The spectrometer consists of a bundle of hard x-ray detectors that respond to different photon-energy ranges. Proof-of-principle experiment was performed on a linear accelerator facility. A quasi-monoenergetic electron bunch (N{sub e} = 1.0 × 10{sup −6} C, E{sub e} = 16 ± 0.32 MeV) was injected into a 5-mm-thick lead plate. Bremsstrahlung x-rays, which emanate from the lead plate, were measured with the spectrometer. The measured spectral shape and intensity agree fairly well with those computed with a Monte Carlo simulation code. The result shows that high-energy x-rays can be measured absolutely with a photon-counting accuracy of 50%–70% in the energy range from 2 MeV to 20 MeV with a spectral resolution (Δhν/hν) of about 15%. Quantum efficiency of this spectrometer was designed to be 10{sup −7}, 10{sup −4}, 10{sup −5}, respectively, for 2–10, 11–15, and 15–25 MeV of photon energy ranges.

  4. The development of a wide-field, high-resolution UV Raman hyperspectral imager

    Science.gov (United States)

    Gomer, Nathaniel R.; Nelson, Matthew P.; Angel, S. M.

    2015-05-01

    Raman spectroscopy is a valuable tool for the investigation and analysis of explosive and biological analytes because it provides a unique molecular fingerprint that allows for unambiguous target identification. Raman can be advantageous when utilized with deep UV excitation, but typical deep UV Raman systems have numerous limitations that hinder their performance and make their potential integration onto a field portable platform difficult. These systems typically offer very low throughput, are physically large and heavy, and can only probe an area the size of a tightly focused laser, severely diminishing the ability of the system to investigate large areas efficiently. The majority of these limitations are directly related to a system's spectrometer, which is typically dispersive grating based and requires a very narrow slit width and long focal length optics to achieve high spectral resolution. To address these shortcomings, ChemImage Sensor Systems (CISS), teaming with the University of South Carolina, are developing a revolutionary wide-field Raman hyperspectral imaging system capable of providing wide-area, high resolution measurements with greatly increased throughput in a small form factor, which would revolutionize the way Raman is conducted and applied. The innovation couples a spatial heterodyne spectrometer (SHS), a novel slit-less spectrometer that operates similar to Michelson interferometer, with a fiber array spectral translator (FAST) fiber array, a two-dimensional imaging fiber for hyperspectral imagery. This combination of technologies creates a novel wide-field, high throughput Raman hyperspectral imager capable of yielding very high spectral resolution measurements using defocused excitation, giving the system a greater area coverage and faster search rate than traditional Raman systems. This paper will focus on the need for an innovative UV Raman system, provide an overview of spatial heterodyne Raman spectroscopy, and discuss the development

  5. AIRBORNE HIGH-RESOLUTION DIGITAL IMAGING SYSTEM

    Directory of Open Access Journals (Sweden)

    Prado-Molina, J.

    2006-04-01

    Full Text Available A low-cost airborne digital imaging system capable to perform aerial surveys with small-format cameras isintroduced. The equipment is intended to obtain high-resolution multispectral digital photographs constituting so aviable alternative to conventional aerial photography and satellite imagery. Monitoring software handles all theprocedures involved in image acquisition, including flight planning, real-time graphics for aircraft position updatingin a mobile map, and supervises the main variables engaged in the imaging process. This software also creates fileswith the geographical position of the central point of every image, and the flight path followed by the aircraftduring the entire survey. The cameras are mounted on a three-axis stabilized platform. A set of inertial sensorsdetermines platform's deviations independently from the aircraft and an automatic control system keeps thecameras at a continuous nadir pointing and heading, with a precision better than ± 1 arc-degree in three-axis. Thecontrol system is also in charge of saving the platform’s orientation angles when the monitoring software triggersthe camera. These external orientation parameters, together with a procedure for camera calibration give theessential elements for image orthocorrection. Orthomosaics are constructed using commercial GIS software.This system demonstrates the feasibility of large area coverage in a practical and economical way using smallformatcameras. Monitoring and automatization reduce the work while increasing the quality and the amount ofuseful images.

  6. High spatial resolution probes for neurobiology applications

    Science.gov (United States)

    Gunning, D. E.; Kenney, C. J.; Litke, A. M.; Mathieson, K.

    2009-06-01

    Position-sensitive biological neural networks, such as the brain and the retina, require position-sensitive detection methods to identify, map and study their behavior. Traditionally, planar microelectrodes have been employed to record the cell's electrical activity with device limitations arising from the electrode's 2-D nature. Described here is the development and characterization of an array of electrically conductive micro-needles aimed at addressing the limitations of planar electrodes. The capability of this array to penetrate neural tissue improves the electrode-cell electrical interface and allows more complicated 3-D networks of neurons, such as those found in brain slices, to be studied. State-of-the-art semiconductor fabrication techniques were used to etch and passivate conformally the metal coat and fill high aspect ratio holes in silicon. These are subsequently transformed into needles with conductive tips. This process has enabled the fabrication of arrays of unprecedented dimensions: 61 hexagonally close-packed electrodes, ˜200 μm tall with 60 μm spacing. Electroplating the tungsten tips with platinum ensure suitable impedance values (˜600 kΩ at 1 kHz) for the recording of neuronal signals. Without compromising spatial resolution of the neuronal recordings, this array adds a new and exciting dimension to the study of biological neural networks.

  7. High Spectral Resolution Lidar (HSRL) Instrument Handbook

    Energy Technology Data Exchange (ETDEWEB)

    Goldsmith, John [Sandia National Lab. (SNL-CA), Livermore, CA (United States)

    2016-04-01

    High Spectral Resolution Lidar (HSRL) systems provide vertical profiles of optical depth, backscatter cross-section, depolarization, and backscatter phase function. All HSRL measurements are absolutely calibrated by reference to molecular scattering, which is measured at each point in the lidar profile. Like the Raman lidar but unlike simple backscatter lidars such as the micropulse lidar, the HSRL can measure backscatter cross-sections and optical depths without prior assumptions about the scattering properties of the atmosphere. The depolarization observations also allow robust discrimination between ice and water clouds. In addition, rigorous error estimates can be computed for all measurements. A very narrow, angular field of view reduces multiple scattering contributions. The small field of view, coupled with a narrow optical bandwidth, nearly eliminates noise due to scattered sunlight. There are two operational U.S. Department of Energy (DOE) Atmospheric Radiation Measurement (ARM) Climate Research Facility HSRL systems, one at the Barrow North Slope of Alaska (NSA) site and the other in the second ARM Mobile Facility (AMF2) collection of instrumentation.

  8. Holographic high-resolution endoscopic image recording

    Science.gov (United States)

    Bjelkhagen, Hans I.

    1991-03-01

    Endoscopic holography or endoholography combines the features of endoscopy and holography. The purpose of endoholographic imaging is to provide the physician with a unique means of extending diagnosis by providing a life-like record of tissue. Endoholographic recording will provide means for microscopic examination of tissue and in some cases may obviate the need to excise specimens for biopsy. In this method holograms which have the unique properties of three-dimensionality large focal depth and high resolution are made with a newly designed endoscope. The endoscope uses a single-mode optical fiber for illumination and single-beam reflection holograms are recorded in close contact with the tissue at the distal end of the endoscope. The holograms are viewed under a microscope. By using the proper combinations of dyes for staining specific tissue types with various wavelengths of laser illumination increased contrast on the cellular level can be obtained. Using dyes such as rose bengal in combination with the 514. 5 nm line of an argon ion laser and trypan blue or methylene blue with the 647. 1 nm line of a krypton ion laser holograms of the stained colon of a dog showed the architecture of the colon''s columnar epithelial cells. It is hoped through chronological study using this method in-vivo an increased understanding of the etiology and pathology of diseases such as Crohn''s diseases colitis proctitis and several different forms of cancer will help

  9. High-resolution imaging using endoscopic holography

    Science.gov (United States)

    Bjelkhagen, Hans I.

    1990-08-01

    Endoscopic holography or endoholography combines the features of endoscopy and holography. The purpose of endoholographic imaging is to provide the physician with a unique means of extending diagnosis by providing a life-like record of tissue. Endoholographic recording will provide means for microscopic examination of tissue and in some cases may obviate the need to excise specimens for biopsy. In this method holograms which have the unique properties of three-dimensionality large focal depth and high resolution are made with a newly designed endoscope. The endoscope uses a single-mode optical fiber for illumination and single-beam reflection holograms are recorded in close contact with the tissue at the distal end of the endoscope. The holograms are viewed under a microscope. By using the proper combinations of dyes for staining specific tissue types with various wavelengths of laser illumination increased contrast on the cellular level can be obtained. Using dyes such as rose bengal in combination with the 514. 5 nm line of an argon ion laser and trypan blue or methylene blue with the 647. 1 nm line of a krypton ion laser holograms of the stained colon of a dog showed the architecture of the colon''s columnar epithelial cells. It is hoped through chronological study using this method in-vivo an increased understanding of the etiology and pathology of diseases such as Crohn''s diseases colitis proctitis and several different forms of cancer will help to their control. 1.

  10. DUACS: Toward High Resolution Sea Level Products

    Science.gov (United States)

    Faugere, Y.; Gerald, D.; Ubelmann, C.; Claire, D.; Pujol, M. I.; Antoine, D.; Desjonqueres, J. D.; Picot, N.

    2016-12-01

    The DUACS system produces, as part of the CNES/SALP project, and the Copernicus Marine Environment and Monitoring Service, high quality multimission altimetry Sea Level products for oceanographic applications, climate forecasting centers, geophysic and biology communities... These products consist in directly usable and easy to manipulate Level 3 (along-track cross-calibrated SLA) and Level 4 products (multiple sensors merged as maps or time series) and are available in global and regional version (Mediterranean Sea, Arctic, European Shelves …).The quality of the products is today limited by the altimeter technology "Low Resolution Mode" (LRM), and the lack of available observations. The launch of 2 new satellites in 2016, Jason-3 and Sentinel-3A, opens new perspectives. Using the global Synthetic Aperture Radar mode (SARM) coverage of S3A and optimizing the LRM altimeter processing (retracking, editing, ...) will allow us to fully exploit the fine-scale content of the altimetric missions. Thanks to this increase of real time altimetry observations we will also be able to improve Level-4 products by combining these new Level-3 products and new mapping methodology, such as dynamic interpolation. Finally these improvements will benefit to downstream products : geostrophic currents, Lagrangian products, eddy atlas… Overcoming all these challenges will provide major upgrades of Sea Level products to better fulfill user needs.

  11. Laser wavelength comparison by high resolution interferometry.

    Science.gov (United States)

    Layer, H P; Deslattes, R D; Schweitzer, W G

    1976-03-01

    High resolution interferometry has been used to determine the wavelength ratio between two molecularly stabilized He-Ne lasers, one locked to a methane absorption at 3.39 microm and the other locked to the k peak of (129)I(2) at 633 nm. An optical beat frequency technique gave fractional orders while a microwave sideband method yielded the integer parts. Conventional (third derivative) peak seeking servoes stabilized both laser and cavity lengths. Reproducibility of the electronic control system and optics was a few parts in 10(12), while systematic errors associated with curvature of the cavity mirrors limited the accuracy of the wavelength ratio measurement to 2 parts in 10(10). The measured wavelength ratio of the methane stabilized He-Ne laser at 3.39 microm [P(7) line, nu(3) band] to the (129)I(2) (k peak) stabilized He-Ne laser at 633 nm was 5.359 049 260 6 (0.000 2 ppm). This ratio agrees with that calculated from the (lower accuracy) results of earlier wavelength measurements made relative to the (86)Kr standard. Its higher accuracy thus permits a provisional extension of the frequency scale based on the cesium oscillator into the visible spectrum.

  12. Analysis of X-ray Spectra of High-Z Elements obtained on Nike with high spectral and spatial resolution

    Science.gov (United States)

    Aglitskiy, Yefim; Weaver, J. L.; Karasik, M.; Serlin, V.; Obenschain, S. P.; Ralchenko, Yu.

    2014-10-01

    The spectra of multi-charged ions of Hf, Ta, W, Pt, Au and Bi have been studied on Nike krypton-fluoride laser facility with the help of two kinds of X-ray spectrometers. First, survey instrument covering a spectral range from 0.5 to 19.5 angstroms which allows simultaneous observation of both M- and N- spectra of above mentioned elements with high spectral resolution. Second, an imaging spectrometer with interchangeable spherically bent Quartz crystals that added higher efficiency, higher spectral resolution and high spatial resolution to the qualities of the former one. Multiple spectral lines with X-ray energies as high as 4 keV that belong to the isoelectronic sequences of Fe, Co, Ni, Cu and Zn were identified with the help of NOMAD package developed by Dr. Yu. Ralchenko and colleagues. In our continuous effort to support DOE-NNSA's inertial fusion program, this campaign covered a wide range of plasma conditions that result in production of relatively energetic X-rays. Work supported by the US DOE/NNSA.

  13. A High Rigidity Spectrometer for the Facility for Rare Isotope Beams.

    Science.gov (United States)

    Zegers, Remco

    2017-01-01

    The High Rigidity Spectrometer (HRS) will be the centerpiece experimental tool of the Facility for Rare-Isotope Beams (FRIB) fast-beam program. The fast-beam program has tremendous discovery potential, enabling experiments with beam intensities of a few ions per second or less through the luminosity afforded by thick targets. The high magnetic rigidity of the HRS (up to 8 Tm) will match the rigidities at which rare-isotope production yields at the FRIB fragment separator are maximum across the entire chart of nuclei and enable experiments with the most neutron-rich nuclei available at FRIB. Gain factors in luminosity of ten or more are achievable compared to running with existing spectrometers, which have a maximum rigidity of 4 Tm, with the highest gains for the most neutron-rich unstable isotopes. To enable a broad spectrum of experiments, the HRS will accommodate different ion-optical modes and provide the flexibility to run in coincidence with a diverse set of other detector systems, such as the Gamma Ray Energy Tracking Array (GRETA) and the Modular Neutron Array (MoNA-LISA). In the presentation, an overview of the scientific opportunities with the HRS and the present layout, based on ion-optical and magnet-feasibility studies, will be given. This material is based upon work supported by the U.S. Department of Energy, Office of Science, Office for Nuclear Physics, under Award Number DE-SC0014554.

  14. Micro-Spec: An Ultracompact, High-sensitivity Spectrometer for Far-Infrared and Submillimeter Astronomy

    Science.gov (United States)

    Cataldo, Giuseppe; Hsieh, Wen-Ting; Huang, Wei-Chung; Moseley, S. Harvey; Stevenson, Thomas R.; Wollack, Edward J.

    2014-01-01

    High-performance, integrated spectrometers operating in the far-infrared and submillimeter ranges promise to be powerful tools for the exploration of the epochs of reionization and initial galaxy formation. These devices, using high-efficiency superconducting transmission lines, can achieve the performance of a meter-scale grating spectrometer in an instrument implemented on a 4 inch silicon wafer. Such a device, when combined with a cryogenic telescope in space, provides an enabling capability for studies of the early universe. Here, the optical design process for Micro-Spec (micron-Spec) is presented, with particular attention given to its two-dimensional diffractive region, where the light of different wavelengths is focused on the different detectors. The method is based on the stigmatization and minimization of the light path function in this bounded region, which results in an optimized geometrical configuration. A point design with an efficiency of (is) approximately 90% has been developed for initial demonstration and can serve as the basis for future instruments. Design variations on this implementation are also discussed, which can lead to lower efficiencies due to diffractive losses in the multimode region.

  15. High-resolution ophthalmic imaging system

    Science.gov (United States)

    Olivier, Scot S.; Carrano, Carmen J.

    2007-12-04

    A system for providing an improved resolution retina image comprising an imaging camera for capturing a retina image and a computer system operatively connected to the imaging camera, the computer producing short exposures of the retina image and providing speckle processing of the short exposures to provide the improved resolution retina image. The system comprises the steps of capturing a retina image, producing short exposures of the retina image, and speckle processing the short exposures of the retina image to provide the improved resolution retina image.

  16. Upgrading a high-throughput spectrometer for high-frequency (<400 kHz) measurements

    Energy Technology Data Exchange (ETDEWEB)

    Nishizawa, T., E-mail: nishizawa@wisc.edu; Nornberg, M. D.; Den Hartog, D. J. [University of Wisconsin–Madison, Madison, Wisconsin 53706 (United States); Craig, D. [Wheaton College, Wheaton, Illinois 60187 (United States)

    2016-11-15

    The upgraded spectrometer used for charge exchange recombination spectroscopy on the Madison Symmetric Torus resolves emission fluctuations up to 400 kHz. The transimpedance amplifier’s cutoff frequency was increased based upon simulations comparing the change in the measured photon counts for time-dynamic signals. We modeled each signal-processing stage of the diagnostic and scanned the filtering frequency to quantify the uncertainty in the photon counting rate. This modeling showed that uncertainties can be calculated based on assuming each amplification stage is a Poisson process and by calibrating the photon counting rate with a DC light source to address additional variation.

  17. Upgrading a high-throughput spectrometer for high-frequency (<400 kHz) measurements

    Science.gov (United States)

    Nishizawa, T.; Nornberg, M. D.; Den Hartog, D. J.; Craig, D.

    2016-11-01

    The upgraded spectrometer used for charge exchange recombination spectroscopy on the Madison Symmetric Torus resolves emission fluctuations up to 400 kHz. The transimpedance amplifier's cutoff frequency was increased based upon simulations comparing the change in the measured photon counts for time-dynamic signals. We modeled each signal-processing stage of the diagnostic and scanned the filtering frequency to quantify the uncertainty in the photon counting rate. This modeling showed that uncertainties can be calculated based on assuming each amplification stage is a Poisson process and by calibrating the photon counting rate with a DC light source to address additional variation.

  18. Calculation of Resolution Function for Triple-Axis Neutron Spectrometer%中子三轴谱仪分辨函数的模拟计算

    Institute of Scientific and Technical Information of China (English)

    刘丽鹃; 谢超美; 徐家云; 阳剑; 谢雷

    2009-01-01

    The theory of triple-axis neutron spectrometer (TAS) was described briefly. With MCSTAS code based on Monte-Carlo method, the resolution function was calculated at elastic scattering. The energy resolution, the scan of vanadium sample scattering experiment and the resolution function shape of different transferred energy were simulated. The relation between the choice of measuring position in real experiment and the shape of the resolution ellipse was analysed. The result shows that simulation calculation can calculate the shape of resolution function rapidly.%阐述了中子三轴谱仪的工作原理,利用MCSTAS程序模拟计算了分辨函数,分别计算了在弹性散射下能量分辨率、钒样品散射实验的转移能量的扫描和不同转移能量下的分辨函数形态.分析了实验中测量位置的选取与分辨椭圆状态的关系.结果表明,模拟计算能快速地计算出分辨函数形态.

  19. Modified Thomson spectrometer design for high energy, multi-species ion sources

    Energy Technology Data Exchange (ETDEWEB)

    Gwynne, D.; Kar, S., E-mail: s.kar@qub.ac.uk; Doria, D.; Ahmed, H.; Hanton, F. [Centre for Plasma Physics, School of Mathematics and Physics, Queen' s University Belfast, Belfast BT7 1NN (United Kingdom); Cerchez, M.; Swantusch, M.; Willi, O. [Institut für Laser-und Plasmaphysik, Heinrich-Heine-Universität, Düsseldorf (Germany); Fernandez, J. [Instituto de Fusión Nuclear UPM, Jose Gutierrez Abascal 2, E28006 Madrid (Spain); Central Laser Facility, Rutherford Appleton Laboratory, Didcot, Oxfordshire OX11 0QX (United Kingdom); Gray, R. J.; MacLellan, D. A.; McKenna, P. [Department of Physics, SUPA, University of Strathclyde, Glasgow G4 0NG (United Kingdom); Green, J. S.; Neely, D. [Central Laser Facility, Rutherford Appleton Laboratory, Didcot, Oxfordshire OX11 0QX (United Kingdom); Najmudin, Z.; Streeter, M. [Blackett Laboratory, Imperial College, London SW7 2AZ (United Kingdom); Ruiz, J. A. [Instituto de Fusión Nuclear UPM, Jose Gutierrez Abascal 2, E28006 Madrid (Spain); Schiavi, A. [Dipartimento SBAI, Università di Roma “La Sapienza,” 00161 Rome (Italy); Zepf, M. [Centre for Plasma Physics, School of Mathematics and Physics, Queen' s University Belfast, Belfast BT7 1NN (United Kingdom); Helmholtz Institut Jena, D-07743 Jena (Germany); Borghesi, M. [Centre for Plasma Physics, School of Mathematics and Physics, Queen' s University Belfast, Belfast BT7 1NN (United Kingdom); Institute of Physics of the ASCR, ELI-Beamlines Project, Na Slovance 2, 18221 Prague (Czech Republic)

    2014-03-15

    A modification to the standard Thomson parabola spectrometer is discussed, which is designed to measure high energy (tens of MeV/nucleon), broad bandwidth spectra of multi-species ions accelerated by intense laser plasma interactions. It is proposed to implement a pair of extended, trapezoidal shaped electric plates, which will not only resolve ion traces at high energies, but will also retain the lower energy part of the spectrum. While a longer (along the axis of the undeflected ion beam direction) electric plate design provides effective charge state separation at the high energy end of the spectrum, the proposed new trapezoidal shape will enable the low energy ions to reach the detector, which would have been clipped or blocked by simply extending the rectangular plates to enhance the electrostatic deflection.

  20. High-Precision Mass Measurements of Exotic Nuclei with the Triple-Trap Mass Spectrometer Isoltrap

    CERN Multimedia

    Blaum, K; Zuber, K T; Stanja, J

    2002-01-01

    The masses of close to 200 short-lived nuclides have already been measured with the mass spectrometer ISOLTRAP with a relative precision between 1$\\times$10$^{-7}$ and 1$\\times$10^{-8}$. The installatin of a radio-frequency quadrupole trap increased the overall efficiency by two orders of magnitude which is at present about 1%. In a recent upgrade, we installed a carbon cluster laser ion source, which will allow us to use carbon clusters as mass references for absolute mass measurements. Due to these improvements and the high reliability of ISOLTRAP we are now able to perform accurate high-precision mass measurements all over the nuclear chart. We propose therefore mass measurements on light, medium and heavy nuclides on both sides of the valley of stability in the coming four years. ISOLTRAP is presently the only instrument capable of the high precision required for many of the proposed studies.