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Sample records for high field esr

  1. Direct observation of the edge spin structure and chain length dependence of a finite haldane chain by high field ESR measurements

    International Nuclear Information System (INIS)

    Yoshida, Makoto; Ohta, Hitoshi; Ito, Toshimitsu; Ajiro, Yoshitami

    2006-01-01

    We have performed high field and multi-frequency ESR measurements of finite length S=1 antiferromagnetic chains in Y 2 BaNi 0.96 Mg 0.04 O 5 . Owing to the high spectral resolution by high fields and high frequencies, observed ESR signals can be separated into the contributions of the finite chains with various chain lengths. Our results clearly show that the edge spins actually interact with each other through the quantum spin chain and the interaction depends on the chain length N. (author)

  2. High-dose dosimetry using electron spin resonance (ESR) spectroscopy

    International Nuclear Information System (INIS)

    Kojima, Takuji; Tanaka, Ryuichi

    1992-01-01

    An electron spin resonance (ESR) dosimeter capable of measuring large doses of radiation in radiotherapy and radiation processing is outlined. In particular, an alanine/ESR dosimeter is discussed, focusing on the development of elements, the development of the ESR dosimetric system, the application of alanine/ESR dosimeter, and basic researches. Rod elements for gamma radiation and x radiation and film elements for electron beams are described in detail. The following recent applications of the alanine/ESR dosimeter are introduced: using as a transfer dosimeter, applying to various types of radiation, diagnosing the deterioration of radiological materials and equipments, and applying to ESR imaging. The future subjects to be solved in the alanine/ESR dosimetric system are referred to as follows: (1) improvement of highly accurate elements suitable for the measurement of various types of radiation, (2) establishment of sensitive calibration method of the ESR equipment itself, and (3) calibration and standardization of radiation doses. (K.N.) 65 refs

  3. Exotic spin phases in the one-dimensional spin-1/2 quantum magnet LiCuSbO{sub 4} as seen by high-field NMR and ESR spectroscopies

    Energy Technology Data Exchange (ETDEWEB)

    Iakovleva, Margarita [IFW Dresden, Dresden (Germany); TU Dresden, Dresden (Germany); Zavoisky Physical Technical Institute, Kazan (Russian Federation); Grafe, Hans-Joachim; Kataev, Vladislav; Alfonsov, Alexey; Sturza, Mihai I.; Wurmehl, Sabine [IFW Dresden, Dresden (Germany); Vavilova, Evgeniia [Zavoisky Physical Technical Institute, Kazan (Russian Federation); Nojiri, Hiroyuki [Institute of Materials Research, Sendai (Japan); Buechner, Bernd [IFW Dresden, Dresden (Germany); TU Dresden, Dresden (Germany)

    2016-07-01

    We will present our recent results of high-field NMR and sub-THz ESR studies of the quantum magnet LiCuSbO{sub 4} (LCSO) that presents an excellent model system of a one-dimensional spin-1/2 quantum magnet with frustrated exchange interactions. Such networks are predicted to exhibit a plethora of novel ground states beyond classical ferro- or antiferromagnetic phases. In LCSO the absence of a long-range magnetic order down to sub-Kelvin temperatures is suggestive of the realization of a quantum spin liquid state. Our NMR and ESR measurements in strong magnetic fields up to 16 Tesla reveal clear indications for the occurrence of an exotic field-induced hidden phase which we will discuss in terms of multipolar physics.

  4. Superconductivity and magnetism in the oxypnictides: high field ESR and {mu}SR studies of (La,Gd)FeAsO{sub 1-x}F{sub x} compounds

    Energy Technology Data Exchange (ETDEWEB)

    Muranyi, Ferenc [Physics Institute, University of Zuerich (Switzerland); IFW Dresden (Germany); Alfonsov, Alexey; Kataev, Vladislav; Koehler, Anke; Werner, Jochen; Behr, Guenter; Leps, Norman; Klingeler, Ruediger; Kondrat, Agnieszka; Hess, Christian; Buechner, Bernd [IFW Dresden (Germany); Khasanov, Rustem; Luetkens, Hubertus [Paul Scherrer Institut, Villigen PSI (Switzerland); Klaus, Hans-Henning [IFP, TU Dresden (Germany)

    2009-07-01

    The discovery of a new class of superconducting materials, ReFeAsO{sub 1-x}F{sub x}, stirred up the scientific community. Here we report the Gd{sup 3+} high field ESR study of differently doped (La,Gd)FeAsO{sub 1-x}F{sub x} compounds. In lightly Gd-doped LaFeAsO samples the SDW transition yields line-broadening at the transition temperature, the SDW transition is then suppressed upon F-doping. In the dense compound, GdFeAsO, with SDW transition around 140 K, the Gd-ESR was also studied. With 15% F-doping superconductivity appears at {proportional_to} 21 K. The SDW and SC transitions are clearly seen in ESR and in {mu} SR as well. Surprisingly the reminiscence of the SDW transition of the undoped material (GdFeAsO) was identified in the doped (15% F) compound at lower temperature ({proportional_to} 80 K). This indicates the importance of the the interplay between superconductivity and magnetism in oxypnictides.

  5. High field ESR study of the pi-d interaction effect in beta-(BDA-TTP)2MCl4 (M=Fe, Ga)

    Science.gov (United States)

    Tokumoto, Takahisa; Vantol, J.; Brunel, L.-C.; Choi, E. S.; Brooks, J. S.; Kaihatsu, T.; Akutsu, H.; Yamada, J.

    2007-03-01

    Novel magnetic organic conductors with pi-d interaction have commanded attention since the discovery of field induced superconductivity. One of them, beta-(BDA-TTP)2FeCl4, has alternating donor molecules and quasi 2D electrical properties. Previous studies of electrical and magnetic properties show an M-I transition at 120K and an AF transition at TN=8.5K, suggesting an exchange interaction between the conduction electrons and the Fe^3+ d-electrons. The properties of beta-(BDA-TTP)2GaCl4 are similar with exception of the absence of the AF transition, which is apparently due to the absence of pi-d exchange interaction. We report angular/temperature dependent 240GHz quasi optical ESR measurements on both compounds to probe the magnetic properties. The Ga compound signals follow the donor molecule structure, and show no magnetic order at any temperature. The Fe compound signals are quite different from the Ga compound, and exhibit AF behavior below TN. The difference of Fe and Ga compounds will be discussed in terms of the interaction between localized and itinerant magnetic moments.

  6. QED in highly-charged high Z ions - experiments at the storage ring ESR

    International Nuclear Information System (INIS)

    Mokler, P.H.

    1996-01-01

    A survey on the fundamental structure aspects of very heavy few -electron ions, in particular H-like systems, is presented. Special emphasis is given to contribution from quantum-electro-dynamics at strong central potentials. The technical possibilities to produce highly-charged heavy ions are reviewed and the ground-state Lamb-shift experiments performed at the heavy ion storage ring ESR are summarized. A short outlook on further developments in this field is added. (author). 23 refs, 9 figs

  7. Electron spin resonance (ESR) spectroscopy applied to radiation dosimetry and other fields

    International Nuclear Information System (INIS)

    Schneider, C.C.J.

    1994-12-01

    A short introduction to the theory and practice of ESR spectroscopy is given. ESR alanine dosimetry for low and high LET (linear energy transfer) ionising radiation is described, indicating its advantages over traditional methods. Problems arising in the therapy dose range (below 5 Gy), and possible future developments, are mentioned. The application of ESR to the radiation processing of materials and foodstuffs, to geological dating, biology, molecular chemistry and to medicine is discussed. Some examples of chemical analyses are also presented. (orig.)

  8. Metal ion-organic compound for high sensitive ESR dosimetry

    International Nuclear Information System (INIS)

    Hassan, G.M.; Ikeya, Motoji

    2000-01-01

    A systematic study to find a tissue equivalent and high sensitive dosimeter material has been made to stimulate the field of ESR dosimetry. Lithium acetate dihydrate (Li-Ac·2H 2 O:CH 3 COOLi·2H 2 O) and lithium phosphate (Li-phosphate:Li 3 PO 4 ) were irradiated by γ-rays to study radicals with (ESR) in addition to magnesium lactate (Mg-lactate (CH 3 CH(OH)COO) 2 Mg) doped with nominal pure lithium lactate (Mg(Li)-lactate) and lithium lactate (CH 3 CH(OH)COOLi) doped with Mg-lactate (Li(Mg)-lactate). A triplet spectrum with intensity ratio of 1:2:1 in Li-Ac·2H 2 O was ascribed to acetate radical which has g=2.0031±0.0004 and hyperfine splitting of A/gβ=2.12±0.1 mT. The Li-phosphate spectrum shows splitting due to anisotropic g-factors of g par =2.0190±0.0005 and g perp =1.9974±0.0004. Quartet spectra with the intensity ratio of 1:3:3:1 in Mg(Li)-lactate and Li(Mg)-lactate were ascribed to lactate radicals with g-factors of 2.0032 ± 0.0004 and 2.0029 ± 0.0004 and the intensity ratio of 1:3:3:1 and A/gβ=1.92±0.06 and 1.82 ± 0.06 mT, respectively. The response to γ-ray dose and the thermal stability as well as the effect of UV-illumination have been studied. The obtained number of free radicals per 100 eV (G-values) were 0.4 ± 0.13, 1.02 ± 0.31, 1.35 ± 0.35 and 0.78 ± 0 for Li-Ac.2H 2 O, Li-phosphate, Mg(Li)-lactate, and Li(Mg)-lactate, respectively. The lifetimes were estimated from Arrhenius plots to be approximately 2.0 ± 0.6, 50.7 ± 20 and 10 ± 3.5 years for Li-phosphate, Mg(Li)-lactate and Li(Mg)-lactate, respectively. The lifetime for Li-Ac·2H 2 O cannot be estimated because of the decomposition by heating

  9. ESR-dosimetry in thermal and epithermal neutron fields for application in boron neutron capture therapy

    Energy Technology Data Exchange (ETDEWEB)

    Schmitz, Tobias

    2016-01-22

    Dosimetry is essential for every form of radiotherapy. In Boron Neutron Capture Therapy (BNCT) mixed neutron and gamma fields have to be considered. Dose is deposited in different neutron interactions with elements in the penetrated tissue and by gamma particles, which are always part of a neutron field. The therapeutic dose in BNCT is deposited by densely ionising particles, originating from the fragmentation of the isotope boron-10 after capture of a thermal neutron. Despite being investigated for decades, dosimetry in neutron beams or fields for BNCT remains complex, due to the variety in type and energy of the secondary particles. Today usually ionisation chambers combined with metal foils are used. The applied techniques require extensive effort and are time consuming, while the resulting uncertainties remain high. Consequently, the investigation of more effective techniques or alternative dosimeters is an important field of research. In this work the possibilities of ESR-dosimeters in those fields have been investigated. Certain materials, such as alanine, generate stable radicals upon irradiation. Using Electron Spin Resonance (ESR) spectrometry the amount of radicals, which is proportional to absorbed dose, can be quantified. Different ESR detector materials have been irradiated in the thermal neutron field of the research reactor TRIGA research reactor in Mainz, Germany, with five setups, generating different secondary particle spectra. Further irradiations have been conducted in two epithermal neutron beams. The detector response, however, strongly depends on the dose depositing particle type and energy. It is hence necessary to accompany measurements by computational modelling and simulation. In this work the Monte Carlo code FLUKA was used to calculate absorbed doses and dose components. The relative effectiveness (RE), linking absorbed dose and detector response, has been calculated using amorphous track models. For the simulation, detailed models of

  10. ESR studies of high-energy phosphorus-ion implanted synthetic diamond crystals

    Energy Technology Data Exchange (ETDEWEB)

    Isoya, J [University of Library and Information Science, Tsukuba, Ibaraki (Japan); Kanda, H; Morita, Y; Ohshima, T

    1997-03-01

    Phosphorus is among potential n-type dopants in diamond. High pressure synthetic diamond crystals of type IIa implanted with high energy (9-18 MeV) phosphorus ions have been studied by using electron spin resonance (ESR) technique. The intensity and the linewidth of the ESR signal attributed to the dangling bond of the amorphous phase varied with the implantation dose, suggesting the nature of the amorphization varies with the dose. The ESR signals of point defects have been observed in the low dose as-implanted crystals and in the high dose crystals annealed at high temperature and at high pressure. (author)

  11. Production of High Quality Die Steels from Large ESR Slab Ingots

    Science.gov (United States)

    Geng, Xin; Jiang, Zhou-hua; Li, Hua-bing; Liu, Fu-bin; Li, Xing

    With the rapid development of manufacture industry in China, die steels are in great need of large slab ingot of high quality and large tonnage, such as P20, WSM718R and so on. Solidification structure and size of large slab ingots produced with conventional methods are not satisfied. However, large slab ingots manufactured by ESR process have a good solidification structure and enough section size. In the present research, the new slab ESR process was used to produce the die steels large slab ingots with the maximum size of 980×2000×3200mm. The compact and sound ingot can be manufactured by the slab ESR process. The ultra-heavy plates with the maximum thickness of 410 mm can be obtained after rolling the 49 tons ingots. Due to reducing the cogging and forging process, the ESR for large slab ingots process can increase greatly the yield and production efficiency, and evidently cut off product costs.

  12. High Energy Electron Dosimetry by Alanine/ESR Spectroscopy

    International Nuclear Information System (INIS)

    Chu, Sung Sil

    1989-01-01

    Dosimetry based on electron spin resonance(ESR) analysis of radiation induced free radicals in amino acids is relevant to biological dosimetry applications. Alanine detectors are without walls and are tissue equivalent. Therefore, alanine ESR dosimetry looks promising for use in the therapy level. The dose range of the alanine/ESR dosimetry system can be extended down to l Gy. In a water phantom the absorbed dose of electrons generated by a medical linear accelerator of different initial energies (6-21 MeV) and therapeutic dose levels(1-60 Gy) was measured. Furthermore, depth dose measurements carried out with alanine dosimeters were compared with ionization chamber measurements. As the results, the measured absorbed doses for shallow depth of initial electron energies above 15 MeV were higher by 2-5% than those calculated by nominal energy CE factors. This seems to be caused by low energy scattered beams generated from the scattering foil and electron cones of beam projecting device in medical linear accelerator

  13. Crystal field effects in the ESR spectra of Dysup(3+), Ersup(3+) and Ybsup(3+) in YPd3

    International Nuclear Information System (INIS)

    Rettori, C.; Weber, E.; Donoso, J.P.; Gandra, F.C.G.; Barberis, G.E.

    1981-01-01

    Low temperature ESR experiments of diluted Dy, Er and Yb in YPd 3 are reported. The host cubic crystal field leaves a GAMMA 7 ground state in the case of Yb 3+ , a GAMMA 7 excited state for Er 3+ and a broad and undefined resonance for Dy 3+ . A comparison with Inelastic Neutron Scattering and Magnetic Susceptibility data is given. (orig.)

  14. Storing quantum information in spins and high-sensitivity ESR.

    Science.gov (United States)

    Morton, John J L; Bertet, Patrice

    2018-02-01

    Quantum information, encoded within the states of quantum systems, represents a novel and rich form of information which has inspired new types of computers and communications systems. Many diverse electron spin systems have been studied with a view to storing quantum information, including molecular radicals, point defects and impurities in inorganic systems, and quantum dots in semiconductor devices. In these systems, spin coherence times can exceed seconds, single spins can be addressed through electrical and optical methods, and new spin systems with advantageous properties continue to be identified. Spin ensembles strongly coupled to microwave resonators can, in principle, be used to store the coherent states of single microwave photons, enabling so-called microwave quantum memories. We discuss key requirements in realising such memories, including considerations for superconducting resonators whose frequency can be tuned onto resonance with the spins. Finally, progress towards microwave quantum memories and other developments in the field of superconducting quantum devices are being used to push the limits of sensitivity of inductively-detected electron spin resonance. The state-of-the-art currently stands at around 65 spins per Hz, with prospects to scale down to even fewer spins. Copyright © 2017. Published by Elsevier Inc.

  15. Storing quantum information in spins and high-sensitivity ESR

    Science.gov (United States)

    Morton, John J. L.; Bertet, Patrice

    2018-02-01

    Quantum information, encoded within the states of quantum systems, represents a novel and rich form of information which has inspired new types of computers and communications systems. Many diverse electron spin systems have been studied with a view to storing quantum information, including molecular radicals, point defects and impurities in inorganic systems, and quantum dots in semiconductor devices. In these systems, spin coherence times can exceed seconds, single spins can be addressed through electrical and optical methods, and new spin systems with advantageous properties continue to be identified. Spin ensembles strongly coupled to microwave resonators can, in principle, be used to store the coherent states of single microwave photons, enabling so-called microwave quantum memories. We discuss key requirements in realising such memories, including considerations for superconducting resonators whose frequency can be tuned onto resonance with the spins. Finally, progress towards microwave quantum memories and other developments in the field of superconducting quantum devices are being used to push the limits of sensitivity of inductively-detected electron spin resonance. The state-of-the-art currently stands at around 65 spins per √{ Hz } , with prospects to scale down to even fewer spins.

  16. Multi-frequency ESR studies on a Haldane magnet in a field-induced phase at ultra-low temperatures

    International Nuclear Information System (INIS)

    Hagiwara, Masayuki; Kashiwagi, Takanari; Idutsu, Yuichi; Honda, Zentaro; Miyazaki, Hiroshi; Harada, Isao

    2010-01-01

    We report the results of multi-frequency electron spin resonance (ESR) measurements on single crystals of Ni(C 5 H 14 N 2 ) 2 N 3 (PF 6 ) which is regarded as the one-dimensional Heisenberg antiferromagnet with spin one, namely the Haldane magnet, at very low temperatures down to about 100 mK. We observed the lowest resonance branch below about 500 mK for the field along the chain direction (H||c), which was observed previously only in an inelastic neutron scattering experiment at 30 mK. We compare the resonance branch with that calculated by a phenomenological field theory, and discuss the field dependence and the temperature sensitivity of this ESR branch.

  17. Investigation of the isochronous mode of the experimental storage ring (ESR) and the collector ring (CR). Decay spectroscopy of highly charged stored 140Pr ions at the FRS-ESR facility

    International Nuclear Information System (INIS)

    Litvinov, Sergey A.

    2008-11-01

    The combination of the present fragment separator FRS and the cooler-storage ring ESR at GSI provides conditions for accurate mass and unique half-life measurements of exotic nuclei. A major part of this doctoral work has been devoted to investigations of the isochronous ion-optical operating mode of the present ESR facility and the planned Collector Ring (CR) facility at FAIR. A detailed ion-optical study of the isochronous storage ring with the emphasis on the main parameters has been done. For example, a simple scaling law providing a quantitative estimate for the mass resolving power as a function of the transverse acceptance has been derived. The ion-optical matching of the FRS-ESR has been calculated and experimentally verified for both the standard and the isochronous operating modes of the ESR. In addition, the dispersion function of a stored ion beam has been measured for both ion-optical modes at the straight section. The improved setting for higher transmission in the standard mode has been used in an experiment on the half-life measurements of highly-charged ions. Orbital electron capture (EC) and/or β + -decay rates of 140 Pr ions with zero-, one- and two- bound electrons have been measured. A complementary future study of EC-decay in highly-charged 64 Cu ions is discussed. Based on the present experience, the ion-optical matching between the future in-flight fragment separator Super-FRS and the CR has been calculated. The isochronous mode of the CR has been calculated. A dedicated Monte-Carlo code (ISOCHRON) has been developed in order to investigate the influence of the transverse acceptance, the closed orbit distortions, the fringe fields of the quadrupoles, the magnetic field imperfections of the magnets on the mass resolving power. The influence of chromaticity on the isochronicity has been investigated. The correction of the chromaticity and of second-order isochronicity has been performed employing sextupole magnets in the arcs of the CR. The

  18. Investigation of the isochronous mode of the experimental storage ring (ESR) and the collector ring (CR). Decay spectroscopy of highly charged stored {sup 140}Pr ions at the FRS-ESR facility

    Energy Technology Data Exchange (ETDEWEB)

    Litvinov, Sergey A.

    2008-11-15

    The combination of the present fragment separator FRS and the cooler-storage ring ESR at GSI provides conditions for accurate mass and unique half-life measurements of exotic nuclei. A major part of this doctoral work has been devoted to investigations of the isochronous ion-optical operating mode of the present ESR facility and the planned Collector Ring (CR) facility at FAIR. A detailed ion-optical study of the isochronous storage ring with the emphasis on the main parameters has been done. For example, a simple scaling law providing a quantitative estimate for the mass resolving power as a function of the transverse acceptance has been derived. The ion-optical matching of the FRS-ESR has been calculated and experimentally verified for both the standard and the isochronous operating modes of the ESR. In addition, the dispersion function of a stored ion beam has been measured for both ion-optical modes at the straight section. The improved setting for higher transmission in the standard mode has been used in an experiment on the half-life measurements of highly-charged ions. Orbital electron capture (EC) and/or {beta}{sup +}-decay rates of {sup 140}Pr ions with zero-, one- and two- bound electrons have been measured. A complementary future study of EC-decay in highly-charged {sup 64}Cu ions is discussed. Based on the present experience, the ion-optical matching between the future in-flight fragment separator Super-FRS and the CR has been calculated. The isochronous mode of the CR has been calculated. A dedicated Monte-Carlo code (ISOCHRON) has been developed in order to investigate the influence of the transverse acceptance, the closed orbit distortions, the fringe fields of the quadrupoles, the magnetic field imperfections of the magnets on the mass resolving power. The influence of chromaticity on the isochronicity has been investigated. The correction of the chromaticity and of second-order isochronicity has been performed employing sextupole magnets in the

  19. ESR Dosimetry

    International Nuclear Information System (INIS)

    Baffa, Oswaldo; Rossi, Bruno; Graeff, Carlos; Kinoshita, Angela; Chen Abrego, Felipe; Santos, Adevailton Bernardo dos

    2004-01-01

    ESR dosimetry is widely used for several applications such as dose assessment in accidents, medical applications and sterilization of food and other materials. In this work the dosimetric properties of natural and synthetic Hydroxyapatite, Alanine, and 2-Methylalanine are presented. Recent results on the use of a K-Band (24 GHz) ESR spectrometer in dosimetry are also presented

  20. Experiments with highly-charged heavy-ions performed at the storage ring ESR

    International Nuclear Information System (INIS)

    Mokler, P.H.

    1992-01-01

    The new heavy ion accelerator facility SIS/ESR was inaugurated in April 1990. During 1991 the experimental storage ring, ESR, has been commissioned. Highly-charged heavy ions from O 8+ up to Bi 82+ were successfully accumulated, cooled, and stored in the ring. Now all highly-charged, heavy ions can be provided for experiments at comfortable storage times and at energies roughly between 100 and 500 MeV/u. A report on the achievements and on the first experimental results will be given. For the experiments, special emphasis is put on capture processes in the electron cooler, i.e. on radiative and dielectronic recombination processes as well as on capture events of bound target electrons from a gas jet. In this case, the capture leads either directly (REC) or by cascading to X-ray emission, which is also exploited for a precision spectroscopy of the structure of the heaviest ions. Another exciting topic is the radioactive decay of highly charged ions: For instance the β-decay into bound atomic states, which is not possible for neutral atoms, was studied for stored naked Dy ions. (orig.)

  1. Development of multi-frequency ESR system for high-pressure measurements up to 2.5 GPa

    Science.gov (United States)

    Sakurai, T.; Fujimoto, K.; Matsui, R.; Kawasaki, K.; Okubo, S.; Ohta, H.; Matsubayashi, K.; Uwatoko, Y.; Tanaka, H.

    2015-10-01

    A new piston-cylinder pressure cell for electron spin resonance (ESR) has been developed. The pressure cell consists of a double-layer hybrid-type cylinder with internal components made of the ZrO2-based ceramics. It can generate a pressure of 2 GPa repeatedly and reaches a maximum pressure of around 2.5 GPa. A high-pressure ESR system using a cryogen-free superconducting magnet up 10 T has also been developed for this hybrid-type pressure cell. The frequency region is from 50 GHz to 400 GHz. This is the first time a pressure above 2 GPa has been achieved in multi-frequency ESR system using a piston-cylinder pressure cell. We demonstrate its potential by showing the results of the high-pressure ESR of the S = 1 system with the single ion anisotropy NiSnCl6 · 6H2O and the S = 1 / 2 quantum spin system CsCuCl3. We performed ESR measurements of these systems above 2 GPa successfully.

  2. Cantilever-detected high-frequency ESR measurement using a backward travelling wave oscillator

    International Nuclear Information System (INIS)

    Tokuda, Y; Hirano, S; Ohmichi, E; Ohta, H

    2012-01-01

    Our cantilever-detected electron spin resonance (ESR) technique is motivated for terahertz ESR spectroscopy of a tiny single crystal at low temperature. In this technique, ESR signal is detected as deflection of a sample-mounted cantilever, which is sensitively detected by built-in piezoresistors. So far, ESR detection at 315 GHz was succeeded using Gunn oscillator. In this study, we combine our ESR technique with a backward traveling wave oscillator (BWO), which can cover a wide frequency range 120-1200 GHz, to achieve better spectral resolution. Experiments were carried out at 4.2 K for a single crystal of Co Tutton salt with a newly constructed optical system. We successfully observed two ESR absorption lines in BWO frequencies up to 370 GHz. From multi-frequency measurements, the observed ESR lines shifted linearly with BWO frequency, being consistent with paramagnetic resonance. The estimated g values are g 1 = 3.00 and g 2 = 3.21. The spin sensitivity was estimated to ∼10 12 spins/gauss at 370 GHz.

  3. Submillimeter wave ESR of copper-oxides

    International Nuclear Information System (INIS)

    Ohta, Hitoshi; Motokawa, Mitsuhiro

    1993-01-01

    Since the discovery of high T c superconductors the magnetism of various copper-oxides has attracted much interest. Especially the magnetism of strong spin correlation systems in various CuO 4 networks is of great interest because it is well known that the superconductivity is occurring in the CuO 2 plane of the high T c superconductors. Here the authors will show some of their work done on copper-oxides by submillimeter wave ESR. The submillimeter wave ESR can provide the frequency region of 90 ∼ 3,100 GHz and the pulse magnetic field up to 30T

  4. Simultaneous high- and low-latitude reconnection: ESR and DMSP observations

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    F. Pitout

    2002-09-01

    Full Text Available We present EISCAT Svalbard Radar and DMSP observations of a double cusp during an interval of predominantly northward IMF on 26 November 2000. In the cusp region, the ESR dish, pointing northward, recorded sun-ward ionospheric flow at high latitudes (above 82° GL, indicating reconnection occuring in the magnetospheric lobe. Meanwhile, the same dish also recorded bursts of poleward flow, indicative of bursty reconnection at the subsolar magnetopause. Within this time interval, the DMSP F13 satellite passed in the close vicinity of the Svalbard archipelago. The particle measurement on board exhibited a double cusp structure in which two oppositely oriented ion dispersions are recorded. We interpret this set of data in terms of simultaneous merging at low- and high-latitude magnetopause. We discuss the conditions for which such simultaneous high-latitude and low-latitude reconnection can be anticipated. We also discuss the consequences of the presence of two X-lines in the dayside polar ionosphere.Key words. Magnetospheric physics (solar wind-magnetosphere interactions – Ionosphere (polar ionosphere; plasma convection

  5. From dating to biophysics -- 20 years of progress in applied ESR spectroscopy

    International Nuclear Information System (INIS)

    Regulla, Dieter

    2000-01-01

    ESR spectroscopy represents a tool for quantitative radiation analysis that was developed somehow simultaneously for dating purposes in Japan and in Germany for high-level standardization, in the mid-seventies. Meanwhile, ESR dosimetry has reached an established metrology level. Present research fields of ESR dosimetry consider post-accident dose reconstruction in the environment, and biophysical dosimetry using human tissues. The latter promises a re-definition of radiation risk for chronicle exposure to be derived from individuals of the early nuclear facilities in Russia, and hopefully United States in the future. An attempt is made to sketch development and potential future of the ESR technique

  6. Effect of Low Nickel Dopant on Torque Transducer Response Function in High-Chromium Content ESR Stainless Tool Steels

    Science.gov (United States)

    Wiewel, Joseph L.; Hecox, Bryan G.; Orris, Jason T.; Boley, Mark S.

    2007-03-01

    The change in magnetoelastic torque transducer response was investigated as a low nickel content (up to 0.2%) is alloyed into an ESR (Electro-Slag-Refining) stainless tool steel with a chromium content of around 13%, which our previous studies have proven to be the ideal level of chromium content for optimal transducer performance. Two separate hollow steel 3/4-inch diameter shafts were prepared from ESR 416 and ESR 420 steel, respectively, the first having no nickel content and the second having 0.2% nickel content. The heat treatment of these steels consisted of a hardening process conducted in a helium atmosphere at 1038^oC, followed by an annealing at 871^oC for 5h and a 15^oC cool down rate. Prior and subsequent to the heat treatment processes, the circumferential and axial magnetic hysteresis properties of the samples were measured and their external field signals were mapped over the magnetically polarized regions both with and without applied shear stress up to 2500 psi on the samples. It was found that the effect of the low nickel dopant was to improve torque transducer sensitivity and linearity, but heat treatment worsened the performance of both samples.

  7. Construction of imaging system for wide-field-range ESR spectra using localized microwave field and its case study of crystal orientation in suspension of copper sulfate pentahydrate (CuSO4.5H2O)

    International Nuclear Information System (INIS)

    Tani, Atsushi; Ueno, Takehiro; Yamanaka, Chihiro; Katsura, Makoto; Ikeya, Motoji

    2005-01-01

    A scanning electron spin resonance (ESR) microscope using a localized microwave field was redesigned to measure ESR spectra from 0 to 400mT using electromagnets. Divalent copper ion (Cu 2+ ) in copper sulfate pentahydrate (CuSO 4 .5H 2 O) was imaged, after the powdered samples were cemented in silicone rubber under a magnetic field. The ratio of the two signal intensities at g=2.27 and 2.08 clearly indicates the orientation of the particles. This method can be used for mapping the local magnetic field and its direction

  8. Construction of imaging system for wide-field-range ESR spectra using localized microwave field and its case study of crystal orientation in suspension of copper sulfate pentahydrate (CuSO{sub 4}.5H{sub 2}O)

    Energy Technology Data Exchange (ETDEWEB)

    Tani, Atsushi [Department of Earth and Space Science, Graduate School of Science, Osaka University, 1-1 Machikaneyama Toyonaka, Osaka 560-0043 (Japan)]. E-mail: atani@ess.sci.osaka-u.ac.jp; Ueno, Takehiro [Department of Earth and Space Science, Graduate School of Science, Osaka University, 1-1 Machikaneyama Toyonaka, Osaka 560-0043 (Japan); Yamanaka, Chihiro [Department of Earth and Space Science, Graduate School of Science, Osaka University, 1-1 Machikaneyama Toyonaka, Osaka 560-0043 (Japan); Katsura, Makoto [Department of Earth and Space Science, Graduate School of Science, Osaka University, 1-1 Machikaneyama Toyonaka, Osaka 560-0043 (Japan); Ikeya, Motoji [Department of Earth and Space Science, Graduate School of Science, Osaka University, 1-1 Machikaneyama Toyonaka, Osaka 560-0043 (Japan)

    2005-02-01

    A scanning electron spin resonance (ESR) microscope using a localized microwave field was redesigned to measure ESR spectra from 0 to 400mT using electromagnets. Divalent copper ion (Cu{sup 2+}) in copper sulfate pentahydrate (CuSO{sub 4}.5H{sub 2}O) was imaged, after the powdered samples were cemented in silicone rubber under a magnetic field. The ratio of the two signal intensities at g=2.27 and 2.08 clearly indicates the orientation of the particles. This method can be used for mapping the local magnetic field and its direction.

  9. Construction of imaging system for wide-field-range ESR spectra using localized microwave field and its case study of crystal orientation in suspension of copper sulfate pentahydrate (CuSO4 . 5H2O).

    Science.gov (United States)

    Tani, Atsushi; Ueno, Takehiro; Yamanaka, Chihiro; Katsura, Makoto; Ikeya, Motoji

    2005-02-01

    A scanning electron spin resonance (ESR) microscope using a localized microwave field was redesigned to measure ESR spectra from 0 to 400 mT using electromagnets. Divalent copper ion (Cu2+) in copper sulfate pentahydrate (CuSO4 . 5H2O) was imaged, after the powdered samples were cemented in silicone rubber under a magnetic field. The ratio of the two signal intensities at g=2.27 and 2.08 clearly indicates the orientation of the particles. This method can be used for mapping the local magnetic field and its direction.

  10. The high-frequency ESR spectra of the syntetic diamond and nanodiamonds type Ib at low temperature

    International Nuclear Information System (INIS)

    Khatsko, E.; Kobets, M.; Dergachev, K.; Kulbickas, A.; Rasteniene, L.; Vaisnoras, R.

    2013-01-01

    The ESR absorption spectra of nonirradiated and irradiated (by electrons with an energy of 2 MeV) bulk diamond and nanodiamond powder of type Ib have been studied at a wide range of frequencies (70-20 GHz) and temperature (4.2-0 K) by ESR method. It is shown, that in the ESR spectrum of bulk diamond absorption lines of ion nickel catalyst Ni +a nd a paramagnetic single center of the nitrogen N 0 is observed. Absorption lines of the paramagnetic centers with dangling bonds on the nanodiamond surface (surface defects) in the ESR spectra are obtained.

  11. Electron beam dose measurements with alanine/ESR dosimeter

    International Nuclear Information System (INIS)

    Rodrigues, O. Jr.; Galante, O.L.; Campos, L.L.

    2001-01-01

    When the aminoacid alanine, CH 3 -CH(NH 2 )-COOH, is exposed to radiation field, stable free radicals are produced. The predominant paramagnetic specie found at room temperature is the CH 3 -CH-COOH. Electron Spin Resonance - ESR is a technique used for quantification and analysis of radicals in solid and liquid samples. The evaluation of the amount of produced radicals can be associated with the absorbed dose . The alanine/ESR is an established dosimetry method employed for high doses evaluation, it presents good performance for X-rays, gamma, electrons, and protons radiation detection. The High Doses Dosimetry Laboratory of Ipen developed a dosimetric system based on alanina/ESR that presents good characteristics for use in gamma fields such as: wide dose range from 10 to 10 5 Gy, low fading, low uncertainty (<5%), no dose rate dependence and non-destructive ESR single readout. The detector is encapsulated in a special polyethylene tube that reduces the humidity problems and improves the mechanical resistance. The IPEN dosimeter was investigated for application in electron beam fields dosimetry

  12. A comment upon the use of two criteria in the identification of intrinsic ESR in high T sub c oxides

    Energy Technology Data Exchange (ETDEWEB)

    Deville, A.; Gaillard, B. (Aix-Marseille-3 Univ., 13 - Marseille (FR))

    1990-12-15

    An ESR signal detected in a Bi compound has recently been attributed to the SC phase, arguing that two criteria (value and thermal behaviour of the intensity) were met. We draw attention to the weakness of this argument, recalling a canonical example.

  13. Highly sensitive detection of ESR1 mutations in cell-free DNA from patients with metastatic breast cancer using molecular barcode sequencing.

    Science.gov (United States)

    Masunaga, Nanae; Kagara, Naofumi; Motooka, Daisuke; Nakamura, Shota; Miyake, Tomohiro; Tanei, Tomonori; Naoi, Yasuto; Shimoda, Masafumi; Shimazu, Kenzo; Kim, Seung Jin; Noguchi, Shinzaburo

    2018-01-01

    We aimed to develop a highly sensitive method to detect ESR1 mutations in cell-free DNA (cfDNA) using next-generation sequencing with molecular barcode (MB-NGS) targeting the hotspot segment (c.1600-1713). The sensitivity of MB-NGS was tested using serially diluted ESR1 mutant DNA and then cfDNA samples from 34 patients with metastatic breast cancer were analyzed with MB-NGS. The results of MB-NGS were validated in comparison with conventional NGS and droplet digital PCR (ddPCR). MB-NGS showed a higher sensitivity (0.1%) than NGS without barcode (1%) by reducing background errors. Of the cfDNA samples from 34 patients with metastatic breast cancer, NGS without barcode revealed seven mutations in six patients (17.6%) and MB-NGS revealed six additional mutations including three mutations not reported in the COSMIC database of breast cancer, resulting in total 13 ESR1 mutations in ten patients (29.4%). Regarding the three hotspot mutations, all the patients with mutations detected by MB-NGS had identical mutations detected by droplet digital PCR (ddPCR), and mutant allele frequency correlated very well between both (r = 0.850, p < 0.01). Moreover, all the patients without these mutations by MB-NGS were found to have no mutations by ddPCR. In conclusion, MB-NGS could successfully detect ESR1 mutations in cfDNA with a higher sensitivity of 0.1% than conventional NGS and was considered as clinically useful as ddPCR.

  14. ESR signal changes recorded in γ-irradiated bovine livers

    International Nuclear Information System (INIS)

    Kikuchi, Masahiro; Kobayashi, Yasuhiko

    2015-01-01

    After fresh raw livers of bovine were exposed to γ-rays on ice, radiation-induced radicals in the livers were measured in liquid nitrogen using electron spin resonance spectroscopy. In the magnetic field of 320.5 to 335.5 mT, the signals responsible to absorbed doses were found. The signal intensity from a main peak was increased up to 5 kGy. The side peaks existing both low and high magnetic field of the main peak showed linear responses as increasing absorbed doses. Radiation-induced radicals were found in a tissue without bones from animals. Without complicated sample preparations, the raw bovine livers can be easily measured on ESR at liquid nitrogen temperature. The ESR method may be applicable to distinguish irradiated fresh raw livers within a few days after irradiation. (author)

  15. ESR Dating Research of Glacial Tills in Tibetan Plateau

    Science.gov (United States)

    Bi, W.; Yi, C.

    2016-12-01

    In recent years, Quaternary Glacial-chronology has been made remarkable progress in the Tibetan Platean(TP) with the development of several numeric dating techniques, such as cosmogenic nuclides(NC), optically stimulated luminescence(OSL) and 14C. In constrast, the dating of Quaternary glacial tills in 100,000 years even more than million-year has been a challenge, just because the techniques has defects themselves and the sediments were stransformed during the geological and geomorphology progress later. Electron Spin Resonance(ESR) has been becoming one of the key methods of Quaternary Glacial-chronology with wide range of dating, expecially for the sample older than 100,000 years up to million-year scale. The accurate measurement of equivalent dose significantly impacts on accuracy and reliability of ESR dating method. Therefore, the study of the mechanisms of resetting processes is fundamental for accurate and reliable ESR dating. To understand the mechanism and characteristics of quartz ESR signal resetting of different samples, a series of laboratory simulation and field observation studies were carried out, which made lots of important breakthrough. But the research in quartz ESR signal of moraines is less and the test of ESR dating method is still in the qualitative investigation. Therefor, we use ESR dating and study on the mechanism and characteristics of quartz ESR signals in tills in the Tibetan Platean. In the adjust method of Modern, the quartz ESR signals in Modern glacial tills represent residual values which can be adjusted signals in the older glacial tills. As a consequence, ESR dating of the quartz in moraines needs to be explored in deep with building models to adjust ages which are measured by ESR dating. Therefore, ESR dating will become the trusted one of the cross dating methods in Quaternary Glacial-chronology with the adjust mothod improving the accuracy of ESR dating ages.

  16. Cooled heavy ion beams at the ESR

    International Nuclear Information System (INIS)

    Steck, M.; Beckert, K.; Bosch, F.; Eickhoff, H.; Franzke, B.; Klepper, O.; Nolden, F.; Reich, H.; Schlitt, B.; Spaedtke, P.; Winkler, T.

    1996-01-01

    The storage ring ESR has been used in various operational modes for experiments with electron cooled heavy ion beams. Besides the standard storage mode including injection and beam accumulation the deceleration of highly charged ions has been demonstrated. Beams of highly charged ions have been injected and accumulated and finally decelerated to a minimum energy of 50 MeV/u. An ultraslow extraction method using charge changing processes is now also available for cooled beams of highly charged ions. For in ring experiments the internal gas jet and the cold electron beam of the cooling system are applied as targets. High precision mass spectrometry by Schottky noise detection has been demonstrated. Operation at transition energy has been achieved with cooled beams opening the field for experiments which require an isochronous revolution of the ions. (orig.)

  17. Experimental Progress in Fast Cooling in the ESR

    CERN Document Server

    Steck, Markus; Beller, Peter; Franzke, Bernhard; Nolden, Fritz

    2005-01-01

    The ESR storage ring at GSI is operated with highly charged heavy ions. Due to the high electric charge the ions interact much stronger with electromagnetic fields. Therefore both cooling methods which are applied to stored ions in the ESR, stochastic cooling and electron cooling, are more powerful than for singly charged particles. The experimental results exhibit cooling times for stochastic cooling of a few seconds. For cold ion beams, electron cooling provides cooling times which are one to two orders of magnitude smaller. The beams are cooled to beam parameters which are limited by intrabeam scattering. At small ion numbers, however, intrabeam scattering is suppressed by electron cooling, clear evidence was found that the ion beam forms a one-dimensional ordered structure, a linear chain of ions. The strengths of stochastic cooling and electron cooling are complementary and can be combined favorably. Stochastic cooling is employed for pre-cooling of hot secondary beams followed by electron cooling to pro...

  18. Development of force-detected THz-ESR measurement system and its application to metal porphyrin complexes

    Science.gov (United States)

    Takahashi, Hideyuki; Okamoto, Tsubasa; Ohmichi, Eiji; Ohta, Hitoshi

    Electron spin resonance spectroscopy in the terahertz region (THz-ESR) is a promising technique to study biological materials such as metalloproteins because it directly probes the metal ion sites that play an important role in the emergence of functionality. By combining THz-ESR with force detection, the samples mass is reduced to the order of ng. This feature is of great advantage because the sample preparation process of biological materials is time-consuming. We developed a force-detected THz-ESR system utilizing optical interferometry for precise cantilever displacement measurement. In order to suppress the sensitivity fluctuation and instability of cantilever dynamics under high magnetic field, the tuning of interferometer is feedback-controlled during a measurement. By using this system, we successfully observed the ESR signal of hemin, which is a model substance of hemoglobin and myoglobin, in THz region.

  19. Correlation of ESR with lyoluminescence dosimetry using some sugars

    International Nuclear Information System (INIS)

    Azorin, Juan; Gutierrez, Alicia; Munoz, Eduardo; Gleason, Roberto

    1989-01-01

    Most applications involving ESR dosimetry currently center on aminoacids because of their relative tissue equivalence. Sugars, however, in addition to possessing high sensitivity and stability in their ESR and LL responses, are widely available as chemical reagents and as commercial sugar. In the present study, dosimetric characteristics of mannose, trehalose, sucrose and commercial sugar obtained by means of ESR and LL techniques are reported. Doses measured by both methods showed agreement within 5%. (author)

  20. Exchange and crystal field effects in the ESR spectra of Eu2+ in LaB6

    Science.gov (United States)

    Duque, J. G. S.; Urbano, R. R.; Venegas, P. A.; Pagliuso, P. G.; Rettori, C.; Fisk, Z.; Oseroff, S. B.

    2007-09-01

    Electron spin resonance of Eu2+ ( 4f7 , S=7/2 ) in a La hexaboride (LaB6) single crystal shows a single anisotropic Dysonian resonance. From the observed negative g shift of the resonance, it is inferred that the Eu2+ ions are covalent exchange coupled to the B2p -like host conduction electrons. From the anisotropy of the spectra (linewidth and field for resonance), we found that the S ground state of Eu2+ ions experience a cubic crystal field of a negative fourth order crystal field parameter (CFP), b4=-11.5(2.0)Oe , in agreement with the negative fourth order CFP, A4 , found for the non- S ground state R hexaborides. These results support covalency as the dominant contribution to the fourth order CFP for the whole R hexaboride family.

  1. ESR application to radiation chemistry of polymers

    International Nuclear Information System (INIS)

    Kashiwabara, H.

    1988-01-01

    Important results obtained in our group in the field of ESR application to the study of irradiated polymers are summarized. They are the analysis of the decay reaction of the free radicals, spur-like trapping of the free radicals and the related discussions. A diffusion controlled bimolecular reaction scheme was a good way of analyzing the data of the decay reaction. Power saturation phenomenon of ESR spectra of the free radicals showed a circumstance of the spur-like trapping of the free radicals in irradiated polyethylene. The phenomenon of spur-like trapping was quite consistent with the interpretation of the decay reaction of the free radicals. (author)

  2. Development of portable ESR spectrometer as a reader for alanine dosimeters

    International Nuclear Information System (INIS)

    Kojima, T.; Haruyama, Y.; Tachibana, H.; Tanaka, R.; Okamoto, J.

    1993-01-01

    A prototype portable electron spin resonance (ESR) spectrometer was designed and tested, and its feasibility as a reader of alanine dosimeters was studied from the two standpoints of reproducibility of readings and sensitivity sufficient for dosimetry in the absorbed dose range 1-100 kGy. It has two main components: a permanent magnet and resonator; and a unit box with a microwave and auto-frequency control (AFC) circuit, a sweep controller of magnetic field, display, etc. In the present preliminary study, reproducibility values are measured with the same ESR parameters and alanine-polystyrene (alanine-PS) dosimeter at a dose of 1 kGy: repeatedly measuring without removing dosimeter from the cavity; individual measurement with removing and inserting again into the cavity with readjustment of ESR parameters. Alanine/ESR dosimetry using this spectrometer has a measurable dose range from 1 to 100 kGy with relatively high precision within ± 3% (1σ) as a preliminary result. The portable ESR spectrometer may also be modified as an automatic, more precise, dedicated alanine dosimeter reader. (author)

  3. ESR identification of irradiated foodstuffs: LARQUA research

    International Nuclear Information System (INIS)

    Raffi, J.

    1996-01-01

    As electron spin resonance (ESR) spectroscopy is the leading method for identification of irradiated foodstuffs, meat and fish bones, fruit and relative products (of vegetable origin), sea-food etc. were studied. In order to prepare a large co-trial on ESR identification of irradiation of irradiated foodstuffs, experiments were carried out at LARQUA, especially on fruits and vegetables. The radicals induced in the fruit pulp are not stable because the water content of fruit is generally high, but ESR can be used with dried fruit or dry components such as achenes, pips or stones. Different responses are observed, depending on the fruit. In ''sugatype'' fruits (papaya, dried grapes), an ESR multicomponent signal is radio-induced, but the non-irradiated fruit presents no ESR signal or a single-line, while in ''cellulose type'' fruits (pistachio nut, berries), a triplet is induced. But a six line signal due to Mn 2+ and a central single line may also be present both in irradiated and non-irradiated samples. In the case of aromatic herbs, the proposed official CEN protocol for irradiated food containing cellulose was used. (author)

  4. ESR identification of irradiated foodstuffs: LARQUA research

    Energy Technology Data Exchange (ETDEWEB)

    Raffi, J [Laboratoire de Recherche sur la Qualite des Aliments, Marseille (France)

    1997-12-31

    As electron spin resonance (ESR) spectroscopy is the leading method for identification of irradiated foodstuffs, meat and fish bones, fruit and relative products (of vegetable origin), sea-food etc. were studied. In order to prepare a large co-trial on ESR identification of irradiation of irradiated foodstuffs, experiments were carried out at LARQUA, especially on fruits and vegetables. The radicals induced in the fruit pulp are not stable because the water content of fruit is generally high, but ESR can be used with dried fruit or dry components such as achenes, pips or stones. Different responses are observed, depending on the fruit. In ``sugatype`` fruits (papaya, dried grapes), an ESR multicomponent signal is radio-induced, but the non-irradiated fruit presents no ESR signal or a single-line, while in ``cellulose type`` fruits (pistachio nut, berries), a triplet is induced. But a six line signal due to Mn{sup 2+} and a central single line may also be present both in irradiated and non-irradiated samples. In the case of aromatic herbs, the proposed official CEN protocol for irradiated food containing cellulose was used. (author).

  5. Screening of irradiated food using ESR measurement of paper

    International Nuclear Information System (INIS)

    Goto, Michiko; Yamazaki, Masao

    2005-01-01

    As paper has high content of cellulose, sensibility of ESR measurements of paper should be high. We examined stability of ESR signals in irradiated recycled copying paper, and estimated the possibility to utilize ESR measurement of paper for the detection of irradiated food. Cellulose radicals in paper irradiated at 1kGy and stored at 40degC in water was detected for 20 days. Cellulose radicals in irradiated paper stored at 90degC in water were more stable than that stored in air. ESR measurements of 50mg paper are simple and easy, so ESR measurement of rapping paper or corrugated box is good screening method for the detection of irradiated food. (author)

  6. Physics book: CRYRING'a'ESR

    International Nuclear Information System (INIS)

    Lestinsky, M.; Aurand, B.; Bagnoud, V.; Andrianov, V.

    2016-01-01

    CRYRING is a heavy ion storage ring, formerly located in Stockholm University. During close to two decades of operation in Sweden, many significant scientific contributions to atomic and molecular physics were achieved using CRYRING. To further leverage its capabilities into the realm of intense beams of highly charged ions, of exotic isotopes, and antiprotons, it has for long been proposed to relocate CRYRING from Sweden to GSI/FAIR, which is the CRYRING'a'ESR project. In Darmstadt, the ring is being modernized and adapted to the GSI/FAIR standards and set up downstream of ESR. In the different chapters we sketch out a broad scientific program in the fields of atomic and nuclear physics and at their intersection. The realization will allow for exciting high-precision spectroscopy studies of atomic systems and their dynamics where special emphasis is given to the effects of quantum electrodynamics (QED) and electron-correlation in the strong field domain (Chap. 2). The intersection of atomic and nuclear physics is addressed where the imprint of nuclear effects on the electronic shell are investigated with spectroscopic methods (Chap. 3), and exploring the nuclear structure, nuclear dynamical processes and quantitative measurements of astrophysically relevant (p, γ)-reaction rates (Chap. 4). These experiments are of prime interest for testing modern theoretical methods on fundamental processes as well as for applications in astrophysics and for modelling plasmas. In the domain of slow collisions in of heavy ions at highest charge-states where atomic processes are prevailed by large perturbations, these studies are expected to refine substantially our understanding of the physics of extreme electromagnetic fields. Also, CRYRINGaESR will offer extracted high-quality ion beams, thus enabling novel research opportunities for external-target experiments with slow highly-charged ions. The experimental boundary conditions and suggested future instrumentation

  7. High Field Workshop

    Energy Technology Data Exchange (ETDEWEB)

    Anon.

    1984-12-15

    A Workshop was held in Frascati at the end of September under the title 'Generation of High Fields for Particle Acceleration to Very High Energies'. It was organized by the CERN Accelerator School, the European Committee for Future Accelerators (ECFA) and the Italian INFN and was a further stage in the exploratory moves towards new techniques of acceleration. Such techniques might become necessary to respond to the needs of high energy physics some decades from now when the application of conventional techniques will probably have reached their limits.

  8. Status and outlook of the CRYRING@ESR project

    Energy Technology Data Exchange (ETDEWEB)

    Geithner, W., E-mail: w.geithner@gsi.de; Andelkovic, Z.; Beck, D.; Bräuning, H.; Bräuning-Demian, A. [GSI Helmholtzzentrum für Schwerionenforschung (Germany); Danared, H. [European Spallation Source ESS (Sweden); Dimopoulou, C. [GSI Helmholtzzentrum für Schwerionenforschung (Germany); Engström, M. [Fysikum, Stockholm University (Sweden); Fedotova, S.; Gorda, O.; Herfurth, F.; Hess, R. [GSI Helmholtzzentrum für Schwerionenforschung (Germany); Källberg, A. [Fysikum, Stockholm University (Sweden); Kleffner, C.; Kotovskiy, N.; Kraus, I.; Lestinsky, M.; Litvinov, S.; Nolden, F.; Reiter, A. [GSI Helmholtzzentrum für Schwerionenforschung (Germany); and others

    2017-11-15

    Once operational, CRYRING@ESR will store and decelerate ions delivered by the experimental storage ring ESR at energies well below those of ESR. In addition to that, CRYRING@ESR has an electron cooler operating with an ultracold electron beam, allowing to provide cooled ion beams for precision experiments. These ions will be delivered to a broad range of experiments presently in preparation; either in-ring or extracted to a dedicated beamline for experiments. An overview and status report of the installation and commissioning of the CRYRING-@ESR storage ring for highly charged ions at the GSI Helmholtzzentrum für Schwerionenforschung is presented. The installation of this storage ring started in 2014 and was completing end of 2016, when this publication was written.

  9. ESR dating a quaternary travertine

    International Nuclear Information System (INIS)

    Lopez Carranza, E.; Amosse, J.; Bouchez, R.

    1987-10-01

    To study the chronology of the quarternary glaciations in the high Peruvian Andes (3.5-4.0 Km high) a number of samples of travertines was collected in the Oroya-Tarma-Huancayo region. We report, in particular, the ESR measurements realized on samples from Santa Rosa de Sacco, which contain 99% of calcite and show a line of g=2.0046 and of width 8.3G, stable, at least, until ∼ 270 deg C. Using the additive dose method to obtain the paleodose and measuring the annual dose by spectrometry gamma of high resolution we obtain for the samples, as a preliminary result, an age between 260,000 and 340,000 a. (author). 7 refs, 6 figs

  10. ESR teleradiology survey: results.

    Science.gov (United States)

    2016-08-01

    With recent developments of teleradiology technology and services, it has become necessary to better evaluate its extent and use among different countries in Europe. With this goal in mind, the ESR launched two specific surveys intended to gather the current state of adoption and implementation of teleradiology in clinical practice. A special focus on differentiating between insourcing teleradiology services among partners of the same organisation and outsourcing to external services was an essential part of the design of these surveys. The first survey was addressed to 44 national societies of different countries in Europe, while the second survey was intended for all practicing radiologist ESR members. While the results of these surveys reported here may provide a wealth of information to better understand the trends in adoption of teleradiology in Europe, they only represent a snapshot at a certain point in time. The rapid development of telecommunication tools as well as a fundamental change in practice and healthcare economics will certainly influence these observations in the upcoming years. These data, however, will provide objective and relevant parameters for supporting the efforts of experts and policy makers in promoting appropriate criteria and guidelines for adequate use of teleradiology in clinical practice. Main Messages • Understand concepts and challenges of teleradiology • Provide insight into current trends and solutions for teleradiology • Compare differences in teleradiolgy strategies between countries in Europe • Establish a reference on statistical data of usage of teleradiology in Europe.

  11. ESR detection of irradiated seashells

    Energy Technology Data Exchange (ETDEWEB)

    Raffi, J. [Laboratoire de Recherche sur la Qualite des Aliments, Faculte de Saint-Jerome, Marseille (France); Hasbany, C. [Laboratoire de Recherche sur la Qualite des Aliments, Faculte de Saint-Jerome, Marseille (France)]|[Laboratoire de Chimie des Produits Naturels, Faculte de Saint-Jerome, Marseille (France); Lesgards, G. [Laboratoire de Chimie des Produits Naturels, Faculte de Saint-Jerome, Marseille (France); Ochin, D. [Institut Agricol et Alimentaire de Lille (France). Lab. de Microbiologie et d`Hygiene Alimentaire

    1996-11-01

    Among the protocols for identification of irradiated foodstuffs submitted to the European Committee of Standardization, two using ESR (food containing bone or cellulose) were finally accepted as official `draft European standards` in Berlin on 9-10 June 1994. We present here some new results for oyster and mussel shells, and an ESR draft protocol is proposed. (author).

  12. High field electron linacs

    International Nuclear Information System (INIS)

    Le Duff, J.

    1985-12-01

    High field electron linacs are considered as potential candidates to provide very high energies beyond LEP. Since almost twenty years not much improvement has been made on linac technologies as they have been mostly kept at low and medium energies to be used as injectors for storage rings. Today, both their efficiency and their performances are being reconsidered, and for instance the pulse compression sheme developed at SLAC and introduced to upgrade the energy of that linac is a first step towards a new generation of linear accelerators. However this is not enough in terms of power consumption and more development is needed to improve both the efficiency of accelerating structures and the performances of RF power sources

  13. ESR dating of fault rocks

    International Nuclear Information System (INIS)

    Lee, Hee Kwon

    2002-03-01

    Past movement on faults can be dated by measurement of the intensity of ESR signals in quartz. These signals are reset by local lattice deformation and local frictional heating on grain contacts at the time of fault movement. The ESR signals then trow back as a result of bombardment by ionizing radiation from surrounding rocks. The age is obtained from the ratio of the equivalent dose, needed to produce the observed signal, to the dose rate. Fine grains are more completely reset during faulting, and a plot of age vs grain size shows a plateau for grains below critical size : these grains are presumed to have been completely zeroed by the last fault activity. We carried out ESR dating of fault rocks collected from the Yangsan fault system. ESR dates from the this fault system range from 870 to 240 ka. Results of this research suggest that long-term cyclic fault activity continued into the pleistocene

  14. ESR dating of fault rocks

    Energy Technology Data Exchange (ETDEWEB)

    Lee, Hee Kwon [Kangwon National Univ., Chuncheon (Korea, Republic of)

    2002-03-15

    Past movement on faults can be dated by measurement of the intensity of ESR signals in quartz. These signals are reset by local lattice deformation and local frictional heating on grain contacts at the time of fault movement. The ESR signals then trow back as a result of bombardment by ionizing radiation from surrounding rocks. The age is obtained from the ratio of the equivalent dose, needed to produce the observed signal, to the dose rate. Fine grains are more completely reset during faulting, and a plot of age vs grain size shows a plateau for grains below critical size : these grains are presumed to have been completely zeroed by the last fault activity. We carried out ESR dating of fault rocks collected from the Yangsan fault system. ESR dates from the this fault system range from 870 to 240 ka. Results of this research suggest that long-term cyclic fault activity continued into the pleistocene.

  15. Evaluation of flux-trapping and magneto-resistibility of superconductors by ESR spectroscopy; ESR ho ni yoru chodendotai no jisoku hosoku to taijiba tokusei no hyoka

    Energy Technology Data Exchange (ETDEWEB)

    Kusumori, T; Matsuura, K; Muto, H [National Industrial Research Institute of Nagoya, Nagoya (Japan)

    1995-09-28

    The abnormal sisal, which was observed in the ESR measurement of superconductors, was confirmed to be a non-ESR (non resonant) signal, from an ESR experiment applying parallel and vertically polarized microwave fields and from the calculation of the ESR transition probabilities. The field modulation dependence of the spectra revealed that the signal was composed of two components. From the modulation-scheme analysis and a study of type I and II superconductors, two components were assigned to the microwave responses to magnetizations trapped in the crystalline portion and at intergranular Josephson junctions. The former B and the batter J components are observed in the first derivative and absorption a form, respectively, and their polarities differently behave for the field sweep reversal. Based on these results, we have improved an ESR spectrometer, which makes it possible to measure separately two kinds of magnetization and to study the trapping ability and quantum flux. 11 refs., 12 figs., 1 tab.

  16. HPLC-ESR techniques for detection of complex trapped radicals

    International Nuclear Information System (INIS)

    Tu Tiecheng; Dong Jirong; Lin Nianyun; Xie Leidong; Liu Rengzhong

    1992-01-01

    High performance liquid chromatography (HPLC) and ESR combined examination of radical species is an advanced techniques for separation and identification of complex radical species. At SRCL, Waters 990 HPLC has been used to separate the complex trapped radicals and Varian E-112 ESR spectrometer to record the spectra of single trapped radicals after HPLC separation. The advantages of the combined techniques are described as bellow: HPLC is used to separate the long-lived complex trapped radicals derived from reaction of short-lived radicals with spin trap. ESR spectra from single trapped radicals, obtained following HPLC separation of complex trapped radicals, are recorded one by one and well resolved. The structures of short-lived radicals can be inferred from the ESR spectra of the long-lived trapped radicals

  17. Effect of estrogen receptor-alpha (ESR1 gene polymorphism on high density lipoprotein levels in response to hormone replacement therapy

    Directory of Open Access Journals (Sweden)

    N.C. Nogueira-de-Souza

    2009-12-01

    Full Text Available Studies have shown that estrogen replacement therapy and estrogen plus progestin replacement therapy alter serum levels of total, LDL and HDL cholesterol levels. However, HDL cholesterol levels in women vary considerably in response to hormone replacement therapy (HRT. A significant portion of the variability of these levels has been attributed to genetic factors. Therefore, we investigated the influence of estrogen receptor-alpha (ESR1 gene polymorphisms on HDL levels in response to postmenopausal HRT. We performed a prospective cohort study on 54 postmenopausal women who had not used HRT before the study and had no significant general medical illness. HRT consisted of conjugated equine estrogen and medroxyprogesterone acetate continuously for 1 year. The lipoprotein levels were measured from blood samples taken before the start of therapy and after 1 year of HRT. ESR1 polymorphism (MspI C>T, HaeIII C>T, PvuII C>T, and XbaI A>G frequencies were assayed by restriction fragment length polymorphism. A general linear model was used to describe the relationships between HDL levels and genotypes after adjusting for age. A significant increase in HDL levels was observed after HRT (P = 0.029. Women with the ESR1 PvuII TT genotype showed a statistically significant increase in HDL levels after HRT (P = 0.032. No association was found between other ESR1 polymorphisms and HDL levels. According to our results, the ESR1 PvuII TT genotype was associated with increased levels of HDL after 1 year of HRT.

  18. ESR modes in a Strong-Leg Ladder in the Tomonaga-Luttinger Liquid Phase

    Science.gov (United States)

    Zvyagin, S.; Ozerov, M.; Maksymenko, M.; Wosnitza, J.; Honecker, A.; Landee, C. P.; Turnbull, M.; Furuya, S. C.; Giamarchi, T.

    Magnetic excitations in the strong-leg quantum spin ladder compound (C7H10N)2CuBr4 (known as DIMPY) in the field-induced Tomonaga-Luttinger spin liquid phase are studied by means of high-field electron spin resonance (ESR) spectroscopy. The presence of a gapped ESR mode with unusual non-linear frequency-field dependence is revealed experimentally. Using a combination of analytic and exact diagonalization methods, we compute the dynamical structure factor and identify this mode with longitudinal excitations in the antisymmetric channel. We argue that these excitations constitute a fingerprint of the spin dynamics in a strong-leg spin-1/2 Heisenberg antiferromagnetic ladder and owe its ESR observability to the uniform Dzyaloshinskii-Moriya interaction. This work was partially supported by the DFG and Helmholtz Gemeinschaft (Germany), Swiss SNF under Division II, and ERC synergy UQUAM project. We acknowledge the support of the HLD at HZDR, member of the European Magnetic Field Laboratory (EMFL).

  19. High magnetic field MRI system

    International Nuclear Information System (INIS)

    Maeda, Hideaki; Urata, Masami; Satoh, Kozo

    1990-01-01

    A high field superconducting magnet, 4-5 T in central magnetic field, is required for magnetic resonance spectroscopic imaging (MRSI) on 31 P, essential nuclei for energy metabolism of human body. This paper reviews superconducting magnets for high field MRSI systems. Examples of the cross-sectional image and the spectrum of living animals are shown in the paper. (author)

  20. ESR identification of gamma-irradiated albendazole

    Science.gov (United States)

    Çolak, Seyda

    2010-01-01

    The use of ionizing radiation for sterilization of pharmaceuticals is a well-established technology. In the present work, the spectroscopic and kinetic features of the radicals induced in gamma-irradiated solid albendazole samples is investigated at different temperatures in the dose range of 3-34 kGy by electron spin resonance (ESR) spectroscopy. Irradiation with gamma radiation produced two different radical species in albendazole. They were fairly stable at room temperature but relatively unstable above room temperature, giving rise to an unresolved ESR spectrum consisting of three resonance peaks centered at g=2.0057. Decay activation energies of the contributing radical species were calculated to be 47.8 (±13.5) and 50.5 (±9.7) kJ/mol using the signal intensity decay data derived from annealing studies performed at high temperatures. A linear function of the applied dose was found to best describe the experimental dose-response data. Albendazole does not present the characteristics of good dosimetric materials. However, the discrimination of irradiated albendazole from its unirradiated form was possible even 6 months after storage in normal conditions. Based on these findings, it is concluded that albendazole and albendazole-containing drugs can be safely sterilized by gamma radiation and that ESR spectroscopy could be successfully used as a potential technique for monitoring their radiosterilization.

  1. ESR dating of fault rocks

    International Nuclear Information System (INIS)

    Lee, Hee Kwon

    2003-02-01

    Past movement on faults can be dated by measurement of the intensity of ESR signals in quartz. These signals are reset by local lattice deformation and local frictional heating on grain contacts at the time of fault movement. The ESR signals then grow back as a result of bombardment by ionizing radiation from surrounding rocks. The age is obtained from the ratio of the equivalent dose, needed to produce the observed signal, to the dose rate. Fine grains are more completely reset during faulting, and a plot of age vs. grain size shows a plateau for grains below critical size; these grains are presumed to have been completely zeroed by the last fault activity. We carried out ESR dating of fault rocks collected near the Gori nuclear reactor. Most of the ESR signals of fault rocks collected from the basement are saturated. This indicates that the last movement of the faults had occurred before the Quaternary period. However, ESR dates from the Oyong fault zone range from 370 to 310 ka. Results of this research suggest that long-term cyclic fault activity of the Oyong fault zone continued into the Pleistocene

  2. ESR dating of fault rocks

    Energy Technology Data Exchange (ETDEWEB)

    Lee, Hee Kwon [Kangwon National Univ., Chuncheon (Korea, Republic of)

    2003-02-15

    Past movement on faults can be dated by measurement of the intensity of ESR signals in quartz. These signals are reset by local lattice deformation and local frictional heating on grain contacts at the time of fault movement. The ESR signals then grow back as a result of bombardment by ionizing radiation from surrounding rocks. The age is obtained from the ratio of the equivalent dose, needed to produce the observed signal, to the dose rate. Fine grains are more completely reset during faulting, and a plot of age vs. grain size shows a plateau for grains below critical size; these grains are presumed to have been completely zeroed by the last fault activity. We carried out ESR dating of fault rocks collected near the Gori nuclear reactor. Most of the ESR signals of fault rocks collected from the basement are saturated. This indicates that the last movement of the faults had occurred before the Quaternary period. However, ESR dates from the Oyong fault zone range from 370 to 310 ka. Results of this research suggest that long-term cyclic fault activity of the Oyong fault zone continued into the Pleistocene.

  3. CH{sub 3} and CD{sub 3} radicals isolated in argon: high resolution ESR spectra and analysis by three-dimensional quantum rotor model. A case study of low temperature quantum effects on radicals

    Energy Technology Data Exchange (ETDEWEB)

    Shiotani, Masaru; Yamada, Tomoya; Komaguchi, Kenji [Hiroshima Univ., Higashi-Hiroshima (Japan). Faculty of Engineering; Benetis, N.P.; Lund, A.; Soernes, A.R.

    1998-10-01

    The present study deals with high resolution isotropic ESR spectra of the CH{sub 3} and CD{sub 3} radicals isolated in solid argon matrix at low temperature from 4 K to 40 K. Argon gases mixed with methane (Ar/methane {approx_equal} 500 mole ratio) were condensed at the end of Suprasile ESR tube at 4.2 K. Methyl radicals were generated by X-ray irradiation at 4 K and subjected to an ESR study. The 6.0 K ESR spectrum of the CH{sub 4}/Ar system is shown in Fig. 1. For CH{sub 3} radical the {sup 1}H hyperfine (hf) quartet was observed with an equal intensity (A-lines). The E-lines were absent at 4 K, but became visible at m{sub F} = {+-}1/2 positions above 12 K increased with temperature. The CD{sub 3} gave a peculiar spectrum at 4 K with an abnormally strong central singlet superimposed on a much weaker seven line spectrum of a freely rotating CD{sub 3}. The temperature dependent spectra showed clear quantum effects due to three-dimensional spin-rotation couplings. The spectra were analyzed with the following assumptions: (a) a planar D{sub 3} geometry, (b) a free and three-dimensional quantum rotation and (c) a thermally isolated radical. Application of the Pauli principle in combination to the D{sub 3} point group resulted in interesting selections for ESR-transitions for both the CH{sub 3} and CD{sub 3} spectra. That is, the {sup 1}H hf quartet of CH{sub 3} radical (A-lines) was attributed to the rotational ground state, J=0, with totally symmetric A{sub 1} nuclear states. The central strong singlet of CD{sub 3} was attributed to one spin-rotation state with A{sub 2} antisymmetric nuclear states at the lowest rotational level of J=0. (author)

  4. High field superconducting magnets

    Science.gov (United States)

    Hait, Thomas P. (Inventor); Shirron, Peter J. (Inventor)

    2011-01-01

    A superconducting magnet includes an insulating layer disposed about the surface of a mandrel; a superconducting wire wound in adjacent turns about the mandrel to form the superconducting magnet, wherein the superconducting wire is in thermal communication with the mandrel, and the superconducting magnet has a field-to-current ratio equal to or greater than 1.1 Tesla per Ampere; a thermally conductive potting material configured to fill interstices between the adjacent turns, wherein the thermally conductive potting material and the superconducting wire provide a path for dissipation of heat; and a voltage limiting device disposed across each end of the superconducting wire, wherein the voltage limiting device is configured to prevent a voltage excursion across the superconducting wire during quench of the superconducting magnet.

  5. ESR signals of irradiated insects

    International Nuclear Information System (INIS)

    Ukai, Mitsuko; Kameya, Hiromi; Imamura, Taro; Miyanoshita, Akihiro; Todoriki, Setsuko; Shimoyama, Yuhei

    2009-01-01

    Analysis of irradiated insects using Electron Spin Resonance (ESR) spectroscopy was reported. The insects were maize weevil, red flour beetle, Indian meal moth and cigarette beetle that are hazardous to crops. The ESR spectra were consisted of a singlet at g=2 and a sextet centered at the similar g-value. The singlet signal is due to an organic free radical. The sextet signal is attributable to the hyperfine interactions from Mn 2+ ions. Upon irradiation, new signals were not detected. The relaxation times, T 1 and T 2 , showed no variations before and after irradiation. (author)

  6. Time-resolved ESR spectroscopy

    International Nuclear Information System (INIS)

    Beckert, D.

    1986-06-01

    The time-resolved ESR spectroscopy is one of the modern methods in radiospectroscopy and plays an important role in solving various problems in chemistry and biology. Proceeding from the basic ideas of time-resolved ESR spectroscopy the experimental equipment is described generally including the equipment developed at the Central Institute of Isotope and Radiation Research. The experimental methods applied to the investigation of effects of chemically induced magnetic polarization of electrons and to kinetic studies of free radicals in polymer systems are presented. The theory of radical pair mechanism is discussed and theoretical expressions are summarized in a computer code to compute the theoretical polarization for each pair of the radicals

  7. Development of an ESR/MR dual-imaging system as a tool to detect bioradicals

    International Nuclear Information System (INIS)

    Fujii, Hirotada; Aoki, Masaaki; Haishi, Tomoyuki; Itoh, Kouichi; Sakata, Motomichi

    2006-01-01

    A system combining electron spin resonance imaging (ESRI) with another imaging modality capable of enabling visualization of the distribution of bioradicals on an anatomical map of the specimens would be a superior biomedical imaging system. We describe the development of an electron spin resonance ESR/MR dual-imaging system with one permanent magnet and the biomedical applications of this system. The magnetic circuit developed for the ESR/MR dual-imaging system consisted of the permanent magnet made of Fe-Nd-B, pole pieces, and poke. The permanent magnet was installed on the MR side only, and the ESR side was made of pole pieces only. The magnetic field was adjusted to 0.5T at MR and to 0.042T at ESR. The overall dimensions of the magnet developed for the ESR/MR imaging system were 460 (W) x 440 (D) x 460 (H) mm, and it weighed 220 kg. The distance of each center for the magnet for ESR and MR imaging could be set as close as 200 mm. The entire ESR/MR imaging system can be installed in a common laboratory without magnetic shielding. MR images of plants (myoga) and small animals (mice and rats) were successfully acquired with or without ESR operation. ESR spectra of nitroxyl spin probes were also measured, even with MRI operation. ESR signals of triarylmethyl derivatives with narrow line-width (0.026 mT) were observed in living mice while MRI was operating. The ESR/MR imaging dual functions work properly with no electric or magnetic interference. The ESR/MR dual images demonstrate that this system enables visualization of the distribution of bioradicals on the anatomical map of the object. (author)

  8. Evolution of ESR Technology and Equipment for Long Hollow Ingots Manufacture

    Science.gov (United States)

    Medovar, Lev; Stovpchenko, Ganna; Dudka, Grigory; Kozminskiy, Alexander; Fedorovskii, Borys; Lebid, Vitalii; Gusiev, Iaroslav

    In this paper development of both ESR technology and equipment for hollow ingot manufacture review and analysis are presented. The real complications of hollow ingot manufacture and some tendentious issues which restrict process dissemination are discussed. An actual data of modern manufacture of as-cast pipes for heat and power engineering by traditional ESR with consumable electrode are given. Results of microstructure and nonmetal inclusion investigations have shown the high quality of as-cast ESR pipes. On the basis of these results the possibility to produce huge ESR hollows (up 5000 mm in dia) with final goal drastically to reduce setting ratio on forged shells and rings or even replace it by ESR hollows as-cast is grounded. Two new ESR technologies — consumable electrodes change and liquid metal usage — have passed pilot tests for heavy hollow production and shown very prospective results to be presented.

  9. Status report of the ESR/alanine project of the IAEA Dosimetry Laboratory

    International Nuclear Information System (INIS)

    Girzikowsky, R.

    1990-01-01

    The main tasks of the Dosimetry Laboratory of the IAEA are in the field of therapy-level dosimetry. Other dose ranges, i.e. protection-level standardization and calibration, are partly covered, too. On high-dose level the laboratory has been offering a Fricke-dosimetry service to Member States on request since 1965. In 1985 the Dosimetry Section has initiated an International Dose Assurance Service (IDAS). This service is an important part of the Agency's high-dose standardization programme and is based on Electron-Spin-Resonance (ESR) analysis of radiation-induced free radicals in alanine. This ESR/alanine dosimetry system was initially developed for high-dose application by GSF/Munich as the Agency's outside contractor. Although efforts were undertaken to equip the Agency Laboratory with an ESR analyzer since 1984, the purchase of an adequate unit was postponed until the end of 1988. From the date of establishment of the IDAS programme until today, the handling of all technical aspects, i.e. dosimeter production and evaluation was and is carried out by GSP/Munich under IAEA contract. As mentioned above, the IAEA Dosimetry Laboratory is in possession of its own ESR analyzer since December 1988. It was then installed in May 1989. Only one staff member of the laboratory was assigned to this project. He made himself acquainted with the analyzer, the measuring technique, and the application of alanine as dosimeter material. The ESR spectrometric analyzer is a CW ESR type ESP 300 manufactured by Bruker GmbH/FRG. It consists of a 9''/2,7 kW magnet, an X-band microwave bridge, a field regulator unit, a signal channel unit and a data system ESP 1620 based on the 68020 CPU. The probe material selected for measurement of concentration of radiation-induced free radicals is L-Alanine. This amino acid is a suitable material for transfer dosimeters due to its properties, i.e. wide sensitivity range (10 Gy to 100 kGy), energy independence for high-energy photons and electron

  10. An ESR study of radicals induced in irradiated fresh mango

    International Nuclear Information System (INIS)

    Kikuchi, Masahiro; Hussain, Mohammed S.; Morishita, Norio; Kobayashi, Yasuhiko; Ukai, Mitsuko; Shimoyama, Yuhei

    2009-01-01

    An electron spin resonance (ESR) spectroscopic study was performed on the radicals induced irradiated fresh mangoes. Fresh Philippine mangoes were irradiated by the γ-rays, lyophilized and powdered. The ESR spectrum of the dry specimen showed a strong main peak at g=2.004 and a pair of peaks at both magnetic fields of the main peak. The main peak detected from flesh and skin specimens faded away in a few days after the irradiation. On the other hand, the side peaks showed a well-defined dose response even 9 days after the irradiation. The side-peak is a useful mean to define the irradiation on fresh mangoes. (author)

  11. ESR dating: is it still an 'experimental' technique?

    International Nuclear Information System (INIS)

    Skinner, A.R.

    2000-01-01

    Nearly 25 years ago, Motoji Ikeya demonstrated the potential of ESR dating. From a single substance (stalagmitic carbonate) and a single site (Akiyoshi Cavern), the field has grown to include materials from all over the world and time periods from a few thousand years ago to several million years ago. A vigorous program of instrumentation development has increased the precision of measurements as well as opening up new ways of collecting and interpreting spectra. Yet there are still references to ESR dating as an 'experimental' technique, one which cannot be trusted to produce dates that are accurate or precise. This paper discusses areas for which this is true and suggests what should be done to convince skeptics. Other areas for which the evidence suggests that ESR is at least as reliable as 'standard' methods will also be covered

  12. High-Field Accelerator Magnets

    International Nuclear Information System (INIS)

    Rijk, G de

    2014-01-01

    In this lecture an overview is given of the present technology for high field accelerator magnets. We indicate how to get high fields and what are the most important parameters. The available conductors and their limitations are presented followed by the most relevant types of coils and support structures. We conclude by showing a number of recent examples of development magnets which are either pure R&D objects or models for the LHC luminosity upgrade

  13. Study of free-radical centers in lignin with 2-mm band ESR spectroscopy

    International Nuclear Information System (INIS)

    Kuzina, S.I.; Demidov, S.V.; Brezgunov, A.Yu.; Poluehktov, O.G.; Grinberg, O.Ya.; Dubinskij, A.A.; Mikhajlov, A.I.; Lebedev, Ya.S.

    1993-01-01

    The nature of paramagnetic centers in pristine lignin and lignin, treated with molecular chlorine, aqueous solutions of acids and alkalis, and γ- and UV-irradiated, was studied with 2-mm band ESR spectroscopy. Most of the observed singlet ESR lines are accounted for by radicals with conjugated bonds. High reactivity of double bonds of polyconjugated systems was in the processes studied

  14. Detection of irradiated strawberries by identifying ESR peak of irradiated cellulose component

    International Nuclear Information System (INIS)

    Goto, Michiko; Tanabe, Hiroko

    2002-01-01

    The method of detecting low-dose irradiated strawberries by identifying ESR peak of irradiated cellulose component was studied. Ratio of peak height (S) of high magnetic field cellulose component, and noise width (N) of either irradiated or unirradiated seeds of strawberries were compared. In this study, sample was identified to be irradiated when S/N ratio of ESR spectrum of 4 min. sweep time was above 0.7. In the case of S/N ratio below 0.7, when the S/N ratio of integrated ESR spectrum, obtained from measuring 10 times with 1 min. sweep time was above 1.0, the sample was identified to be irradiated. The result suggests that S/N ratio is a good marker to detect the irradiation. The strawberries irradiated above 0.5kGy was able to be detected after 3 days storage at room temperature, after 21 days refrigeration and after 60 days freezing, respectively. (author)

  15. Criticality accident dosimetry with ESR spectroscopy.

    Science.gov (United States)

    d'Errico, F; Fattibene, P; Onori, S; Pantaloni, M

    1996-01-01

    The suitability of the ESR alanine and sugar detectors for criticality accident dosimetry was experimentally investigated during an intercomparison of dosimetry techniques. Tests were performed irradiating detectors both free-in-air and on-phantom during controlled critcality excursions at the SILENE reactor in Valduc, France. Several grays of absorbed dose were imparted in neutron gamma-ray fields of various relative intensities and spectral distributions. Analysed results confirmed the potential of these systems which can immediately provide an acute dose assessment with an average underestimate of 30%in the various fields. This performance allows for the screening of severely exposed individuals and meets the IAEA recommendations on the early estimate of accident absorbed doses.

  16. Unconventional spin dynamics in the honeycomb-lattice material α -RuCl3 : High-field electron spin resonance studies

    Science.gov (United States)

    Ponomaryov, A. N.; Schulze, E.; Wosnitza, J.; Lampen-Kelley, P.; Banerjee, A.; Yan, J.-Q.; Bridges, C. A.; Mandrus, D. G.; Nagler, S. E.; Kolezhuk, A. K.; Zvyagin, S. A.

    2017-12-01

    We present high-field electron spin resonance (ESR) studies of the honeycomb-lattice material α -RuCl3 , a prime candidate to exhibit Kitaev physics. Two modes of antiferromagnetic resonance were detected in the zigzag ordered phase, with magnetic field applied in the a b plane. A very rich excitation spectrum was observed in the field-induced quantum paramagnetic phase. The obtained data are compared with the results of recent numerical calculations, strongly suggesting a very unconventional multiparticle character of the spin dynamics in α -RuCl3 . The frequency-field diagram of the lowest-energy ESR mode is found consistent with the behavior of the field-induced energy gap, revealed by thermodynamic measurements.

  17. ESR response of powder samples of clear fused quartz material to high doses of 10 MeV electrons: possible applications for industrial radiation processing

    International Nuclear Information System (INIS)

    Aliabadi, R.; Amraei, R.; Ranjbar, A.H.; Rafieian, Sh.; Nasirimoghadam, S.

    2010-01-01

    Powder samples of clear fused quartz were irradiated by 10 MeV electrons at doses between 6-15 kGy and 25-37 kGy and analyzed with electron spin resonance. The reproducibility of the material dose response curve was studied, in which the irradiated samples were annealed and reused for further investigations. Results indicate a good linearity between the absorbed dose and the ESR intensity of the signals. They also showed that in the reuse processes, the electron spin resonance signal intensity, in both dose ranges was decreased. The thermal fading represented a relative sharp decay at room temperature through 15 days, after which the decay-rate was negligible for a measurement period of 60 days.

  18. Electric-Field Effects in ESR Spectrum of Low-Spin Center Ni3+ in KTaO3 Crystals (Preprint)

    National Research Council Canada - National Science Library

    Sochava, L. S; Basun, S. A; Bursian, V. E; Razdobarin, A. G; Evans, Dean R

    2007-01-01

    ...+ was studied in KTaO3 single crystals. Orientation of the centers as well as splitting of the resonance lines was found resulting from the external E-field interaction with the electric dipole moment of the center...

  19. Novel spin excitation in the high field phase of an S=1 antiferromagnetic chain

    International Nuclear Information System (INIS)

    Hagiwara, M.; Kashiwagi, T.; Kimura, S.; Honda, Z.; Kindo, K.

    2007-01-01

    We report the results of high-field multi-frequency ESR experiment on the S=1 Heisenberg antiferromagnetic chain Ni(C 5 H 14 N 2 ) 2 N 3 (PF 6 ) for the fields up to about 55T and the frequencies up to about 2THz. We have found that excitation branches above the critical field (H c ) where the energy gap closes change into one branch around 15T which becomes close to the paramagnetic line at high fields. The branch above 15T fits well the conventional antiferromagnetic resonance mode with easy planar anisotropy. We compare the results with those in a weakly coupled antiferromagnetic dimer compound KCuCl 3 and discuss the origin of the branches observed above H c

  20. Relaxation behavior of radicals produced in irradiated black pepper under various moisture conditions by ESR

    International Nuclear Information System (INIS)

    Kameya, Hiromi; Kawauchi, Risa; Shimoyama, Yuhei; Kaeda, Yoko; Ogawa, Satoko; Nakamura, Hideo; Ukai, Mitsuko

    2008-01-01

    Black pepper is easy to be contaminated by microorganism and often processed to γ-irradiation. ESR has been used for the detection of radicals induced in irradiated spices. Using ESR, we revealed the effects of moisture condition during storage of irradiated black pepper on the saturation behavior of ESR signal. The ESR spectrum of black pepper consists of a broad sextet centered at g=2.0, a singlet as same g-value and a singlet at g=4.0. The irradiation causes two new signals, one is the strong and sharp singlet signal at g=2.0 and the other is the side signal. We found that the signal intensity originated by the radicals of black pepper with and without radiation decayed in the high humidity condition during storage. The ESR signal intensity of irradiated black pepper decayed during storage and showed almost the same intensity level as that of non-irradiated black pepper during storage. (author)

  1. Effect of surfactant coating on magnetic properties of Fe3O4 nanoparticles: ESR study

    International Nuclear Information System (INIS)

    Koeseoglu, Yueksel

    2006-01-01

    Magnetic properties of surfactant-coated and uncoated superparamagnetic iron oxide nanoparticles, Fe 3 O 4 (SPION) were investigated by electron spin resonance (ESR) technique. For all samples, a strong and broad single ESR signal has been observed at all temperatures. A strong temperature dependence of ESR linewidth and resonance field is observed. Also, there is a strong effect of surfactant coating on magnetic properties of Fe 3 O 4 nanoparticles. While the resonance field is decreasing by coating, the linewidth of the ESR spectra is increasing. These changes in resonance field and the linewidth are attributed to the decrease in effective magnetic moment due to a non-collinear spin structure originated from the pinning of the surface spins and coated surfactant at the interface of nanoparticles. Also, the changes are due to the contribution of the volume of the diamagnetic coating mass to the sample volume

  2. Computer enhancement of ESR spectra of magnetite nanoparticles

    Energy Technology Data Exchange (ETDEWEB)

    Dobosz, B.; Krzyminiewski, R. [Medical Physics Division, Faculty of Physics, Adam Mickiewicz University, Umultowska 85, 61-614 Poznan (Poland); Koralewski, M. [Optics Laboratory, Faculty of Physics, Adam Mickiewicz University, Umultowska 85, 61-614 Poznan (Poland); Hałupka-Bryl, M. [Medical Physics Division, Faculty of Physics, Adam Mickiewicz University, Umultowska 85, 61-614 Poznan (Poland); The PhD Program in Nanoscience and Nanotechnology, The Nanobiomedical Centre, Umultowska 85, 61-614 Poznan (Poland)

    2016-06-01

    We present ESR measurements of non-interacting magnetic nanoparticle systems. Temperature and orientational dependence of ESR spectra were measured for Fe{sub 3}O{sub 4} nanoparticle coated by dextran or oleic acid, frozen in different magnetic field. Several parameters describing magnetic properties such as g-factor, line width, the anisotropy constant were calculated and discussed. The ESR spectra of investigated nanoparticles were also subjected to Computer Resolution Enhancement Method (CREM). This procedure allows to separate a narrow line on the background of the broad line, which presence in this type of materials was recognized in the recent literature and have been further discussed in the paper. CREM is a valuable tool for monitoring of changes on the surface of magnetic core of nanoparticles. - Highlights: • CREM – a new tool for monitoring of changes on the surface of magnetic core of nanoparticles. • CREM allows to separate a narrow line on the background of the broad line. • Temperature and orientational dependence of ESR spectra of Fe{sub 3}O{sub 4} nanoparticles were measured. • Parameters describing magnetic properties were calculated and discussed.

  3. Expression of estrogen receptor α 36 (ESR36) in the hamster ovary throughout the estrous cycle: effects of gonadotropins.

    Science.gov (United States)

    Chakraborty, Prabuddha; Roy, Shyamal K

    2013-01-01

    Estradiol-17β (E) plays an important role in ovarian follicular development. Evidence indicates that some of the effect of E is mediated by the transmembrane estrogen receptor. In this study, we examined the spatio-temporal expression of recently discovered ERα36 (ESR36), a splice variant of Esr1 and a receptor for non-genomic E signaling, in the hamster ovary during the estrous cycle and the role of gonadotropins and ovarian steroid hormones in ESR36 expression. ESR36 expression was high on estrus (D1:0900 h) and declined precipitously by proestrus (D4:0900 h) and remained low up to D4:1600 h. Immunofluorescence findings corroborated immunoblot findings and revealed that ESR36 was expressed only in the cell membrane of both follicular and non-follicular cells, except the oocytes. Ovarian ESR36 was capable of binding to the E-affinity matrix, and have different molecular weight than that of the ESR1 or GPER. Hypophysectomy (Hx) resulted in a marked decline in ESR36 protein levels. FSH and LH, alone or combined, markedly upregulated ESR36 protein in Hx hamsters to the levels observed in D1 hamsters, but neither E nor P had any effect. Inhibition of the gonadotropin surge by phenobarbital treatment on D4:1100 h attenuated ESR36 expression in D1:0900 h ovaries, but the decline was restored by either FSH or LH replacement on D4 afternoon. This is the first report to show that ESR36, which is distinct from ESR1 or GPER is expressed in the plasma membrane of ovarian follicular and non-follicular cells, binds to E and its expression is regulated directly by the gonadotropins. In light of our previous findings, the results suggest that ovarian cells contain at least two distinct membrane estrogen receptors, such as GPER and ESR36, and strongly suggest for a non-genomic action of E regulating ovarian follicular functions.

  4. ESR identification of irradiated foodstuffs

    International Nuclear Information System (INIS)

    Raffi, J.

    1993-01-01

    The conditions required to use Electron Spin Resonance (ESR) in identification of irradiated foods is first described. Then we present the results of an intercomparison sponsored by the Community Bureau of Reference involving 22 european laboratories. Qualitative identification of irradiated beef bones, dried grapes and papaya is very easy. Kinetical studies are necessary in case of fish species. Further researches are required in case of pistachio-nuts. Although all laboratories could distinguish between the two dose ranges used in case of meat bones (i.e. 1-3 and 7-10 kGy), there is an overlap of the results from the different laboratories. 2 tabs., 3 figs

  5. Comparative Study of Erythrocyte Sedimentation Rate (ESR) Using ...

    African Journals Online (AJOL)

    MICHAEL

    significant difference between the ESR values obtained using trisodium citrate and whole blood (P< 0.05). Males had lower ESR ... The ESR is governed by the balance between pro- ... 1999). When an inflammatory process is present, the.

  6. Current topics in ESR dating

    International Nuclear Information System (INIS)

    Skinner, Anne R.

    2011-01-01

    After over 25 years, the use of electron spin resonance (ESR) is well-established in dating sites of geological, paleontological and archaeological interest. Like any scientific technique, there have been changes in understanding and in methodology. Improvements have not, however, changed the observation that external dose calculations are still a significant source of uncertainty in ages. Examples from Europe, Africa and the Americans illustrate this point. For Pradayrol Cave (France), the occupation age, 330 ka, is unchallenged, making this the oldest known Neanderthal site in France. For Roc de Marsal, also in France, on the other hand, discrepancies between TL and sedimentary dose rates imply substantial differences in interpretation. In the Western Egyptian Desert, where artifacts and datable material are not well-correlated, the dating results show consistency with expectations based on global climate change, even in deflated sites. Climate change is also the question in geological studies in the Bahamas where, despite concerns about cosmic dose history, ESR dates confirm other evidence for sea level changes. We show that an uncertain age is not the same as an impossible one.

  7. Luminescence and ESR properties of Brazilian feldspars

    International Nuclear Information System (INIS)

    Bitencourt, J.F.S.; Silva, D.M.; Silva, P.H.; Kinoshita, A.; Munita, C.S.; Tatumi, S.H.

    2006-01-01

    The IRSL and TL responses of three different feldspar crystals have been analysed. TL measurements were taken in the ultraviolet UV (290-370nm) and the visible VIS (340-610nm) regions of the spectrum. For the UV region and for a natural sample, peaks were observed at 283, 287 and 310 deg. C for grey, white and pink crystals, respectively. For samples irradiated after prior preheating, it was noted that TL peaks occurred at about 200 deg. C for all the samples; irradiation with high doses above 500Gy induced the formation of one additional peak at 170 deg. C. The VIS region results were similar to those for the UV. ESR experiments have been developed to verify the influence of radiation and heat treatments on the centres and preliminary results showed great variation in the intensities of [TiO 4 ] - , Al-O - -Al and Fe 3+ centres

  8. Electron cooling experiments at the ESR

    International Nuclear Information System (INIS)

    Steck, M.; Beller, P.; Beckert, K.; Franzke, B.; Nolden, F.

    2004-01-01

    The properties of electron cooled beams of highly charged ions have been studied at the ESR. New experiments using a beam scraper to determine the transverse beam size provide the beam parameters in the intrabeam scattering dominated intensity regime, but also at very low intensity when the ion beam enters into an ultra-cold state. Extremely low values of longitudinal and transverse beam temperature on the order of meV were achieved for less than 1000 stored ions. An experiment with bunched ultra-cold beam showed a limit of the line density which agrees with the one observed for coasting beams. Cooling of decelerated ions at a minimum energy of 3 MeV/u has been demonstrated recently

  9. SDSL-ESR-based protein structure characterization.

    Science.gov (United States)

    Strancar, Janez; Kavalenka, Aleh; Urbancic, Iztok; Ljubetic, Ajasja; Hemminga, Marcus A

    2010-03-01

    As proteins are key molecules in living cells, knowledge about their structure can provide important insights and applications in science, biotechnology, and medicine. However, many protein structures are still a big challenge for existing high-resolution structure-determination methods, as can be seen in the number of protein structures published in the Protein Data Bank. This is especially the case for less-ordered, more hydrophobic and more flexible protein systems. The lack of efficient methods for structure determination calls for urgent development of a new class of biophysical techniques. This work attempts to address this problem with a novel combination of site-directed spin labelling electron spin resonance spectroscopy (SDSL-ESR) and protein structure modelling, which is coupled by restriction of the conformational spaces of the amino acid side chains. Comparison of the application to four different protein systems enables us to generalize the new method and to establish a general procedure for determination of protein structure.

  10. ESR dating of tooth enamel samples

    International Nuclear Information System (INIS)

    Chen Tiemei; Yang quan; Wu En

    1993-01-01

    Five tooth samples from the palaeoanthropological site of Jinniushan were dated with both electron-spin-resonance (ESR) and uranium-series techniques. The ESR age of about 230 ka is in good agreement with the U-series dating result, which confirms the hypothesis of possible coexistence of Homo erect us and Homo sapiens in China. Problems in ESR dating are discussed such as: 1) inappropriate of simple exponential extrapolation for accumulated dose determination; 2)experimental measurement of alpha detection efficiency and radon emanation and 3)selection of U-uptake model

  11. High-resolution spectroscopy of deeply-bound pionic atoms in heavy nuclei by pion-transfer reactions of inverse kinematics using the GSI cooler ring ESR

    International Nuclear Information System (INIS)

    Yamazaki, Toshimitsu.

    1991-02-01

    Many studies published in the past are reviewed first in relation to high-resolution spectroscopy of deeply-bound pionic atoms in heavy nuclei. The report then describes a procedure for applying the method of inverse kinematics to the case of (d, 3 He) reactions. The (d, 3 He) reaction in inverse kinematics is feasible from practical viewpoints. Thus a discussion is made of the inverse kinematics in which a heavy-ion beam ( 208 Pb for instance) with a projectile kinetic energy hits a deuteron target and ejected recoil 3 He nuclei are measured in the forward direction. The recoil momentum is calculated as a function of the Q value. Analysis shows that the recoil spectroscopy with inverse kinematics can be applied to the case of (d, 3 He) reaction, which will yield a very high mass resolution. The experimental setup for use in the first stage is then outlined, and a simple detector configuration free of magnetic field is discussed. These investigations demonstrate that the (d, 3 He) reaction in inverse kinematics provides a promising tool for obtaining high-resolution spectra of deeply-bound pionic atoms. (N.K.)

  12. [Identification of irradiated abalone by ESR spectroscopy].

    Science.gov (United States)

    Song, Yeping; Wang, Chuanxian; Yang, Zhenyu; Zhong, Weike; Geng, Jinpei; Lu, Di; Ding, Zhuoping

    2012-05-01

    To establish an analytical method for the detection and identification of irradiated abalone by electron spin resonance spectroscopy. Electron spin resonance (ESR) was used to study the spectral characteristics of abalone and the characteristic peak for quantitation. There were obvious different ESR spectra between unirradiated and irradiated abalone. The g factor for unirradiated abalone was 2.0055-2.0060, the g1 and g2 factor for irradiated abalone were (2.0027 +/- 0.0001) and (1.9994 +/- 0.0001), respectively. The ESR signal intensity of characteristic peak was positively correlated with absorbed dose in the range of 0.5 - 10 kGy, left peak was the characteristic peak for quantitation and the detection limit was abalone. ESR spectroscopy is an effective method to determine whether the abalone being irradiated or not.

  13. A 3D- and 4D-ESR imaging system for small animals

    International Nuclear Information System (INIS)

    Oikawa, K.; Ogata, T.; Togashi, H.; Yokoyama, H.; Ohya-Nishiguchi, H.; Kamada, H.

    1996-01-01

    A new version of in vivo ESR-CT system composed of custom-made 0.7 GHz ESR spectrometer, air-core magnet with a field-scanning coil, three field-gradient coils, and two computers enables up-and down-field, and rapid magnetic-field scanning linearly controlled by computer. 3D-pictures of distribution of nitroxide radicals injected in brains and livers of rats and mice were obtained in 1.5 min with resolution of 1 mm. We have also succeeded in obtaining spatial-time imagings of the animals. (author)

  14. ESR dating of the fault rocks

    Energy Technology Data Exchange (ETDEWEB)

    Lee, Hee Kwon [Kangwon National Univ., Chuncheon (Korea, Republic of)

    2004-01-15

    Past movement on faults can be dated by measurement of the intensity of ESR signals in quartz. These signals are reset by local lattice deformation and local frictional heating on grain contacts at the time of fault movement. The ESR signals then grow back as a result of bombardment by ionizing radiation from surrounding rocks. The age is obtained from the ratio of the equivalent dose, needed to produce the observed signal, to the dose rate. Fine grains are more completely reset during faulting, and a plot of age vs, grain size shows a plateau for grains below critical size : these grains are presumed to have been completely zeroed by the last fault activity. We carried out ESR dating of fault rocks collected near the Ulzin nuclear reactor. ESR signals of quartz grains separated from fault rocks collected from the E-W trend fault are saturated. This indicates that the last movement of these faults had occurred before the quaternary period. ESR dates from the NW trend faults range from 300ka to 700ka. On the other hand, ESR date of the NS trend fault is about 50ka. Results of this research suggest that long-term cyclic fault activity near the Ulzin nuclear reactor continued into the pleistocene.

  15. Dosimetric calibration of humidity chamber inside the 60Co-PANBIT irradiator using alanine ESR dosimeter

    International Nuclear Information System (INIS)

    Murali, S.; Venkataramani, R.; Pushparaja; Natarajan, V.; Sastry, M.D.; Bora, J.S.; Venkatacharyulu, K.

    1998-01-01

    In the present work the suitability of the electron spin resonance (ESR) technique, using DL - α - alanine sample is examined. It is well documented that radiation induced free radicals in alanine give strong ESR spectrum which can be used for dosimetry purposes. The aspects that are relevant to the present work are: (I) stability of the radicals in temperature and humidity conditions in which the experiments were carried out; (II) linearity at high doses; and (III) establishing the utility of alanine ESR dosimeter by cross checking the dose values with more established dosimeters. The details of these investigations are presented and it is shown that alanine ESR dosimeter will meet all the required conditions satisfactorily

  16. Diffusion studies on permeable nitroxyl spin probes through bilayer lipid membranes: A low frequency ESR study

    International Nuclear Information System (INIS)

    Meenakumari, V.; Benial, A. Milton Franklin; Utsumi, Hideo; Ichikawa, Kazuhiro; Yamada, Ken-ichi; Hyodo, Fuminori; Jawahar, A.

    2015-01-01

    Electron spin resonance (ESR) studies were carried out for permeable 2mM 14 N-labeled deutrated 3 Methoxy carbonyl-2,2,5,5-tetramethyl-pyrrolidine-1-oxyl (MC-PROXYL) in pure water and 1mM, 2mM, 3mM, 4mM concentration of 14N-labeled deutrated MC-PROXYL in 400mM concentration of liposomal solution by using a 300 MHz ESR spectrometer. The ESR parameters such as linewidth, hyperfine coupling constant, g-factor, partition parameter and permeability were reported for these samples. The line broadening was observed for the nitroxyl spin probe in the liposomal solution. The line broadening indicates that the high viscous nature of the liposomal solution. The partition parameter and permeability values indicate the maximum diffusion of nitroxyl spin probes in the bilayer lipid membranes at 2 mM concentration of nitroxyl radical. This study illustrates that ESR can be used to differentiate between the intra and extra- membrane water by loading the liposome vesicles with a lipid-permeable nitroxyl spin probe. From the ESR results, the spin probe concentration was optimized as 2mM in liposomal solution for ESR phantom studies/imaging, invivo and invitro experiments

  17. ESR spectroscopy of blood serum in thalassemia: computer simulation of methemalbumin spectrum

    International Nuclear Information System (INIS)

    Preoteasa, E.A.; Duliu, O.G.; Grecu, V.V.; Schianchi, G.; Giori, D.C.; Pedrazzi, G.

    1997-01-01

    In pathological states with severe hemolysis such as homozygous β-thalassemia, human serum albumin (HSA) binds ferric heme to form the methemalbumin (MHA) molecular complex. Low-temperature X-band ESR monitored MHA in patients' serum, while in vitro studies prompted a molecular model for the complex. On the assumption of axial symmetry with small rhombic distortion for high spin Fe (III) in MHA, we used a simulation program written in FORTRAN V for ESR spectra of vitreous samples containing subsystems with effective electronic spin S' = 1/2 and nuclear spin I ≥ 0. We have take also into account the individual resonance line shape and half-width, and the magnetic field dependence of the transition probability. Two distinct forms of MHA were found in patients' serum, the second one showing a stronger rhombic distortion around Fe (III) as compared to the in-vitro complex. This suggested a conformational change of HSA around heme binding site, possibly produced by free radicals occurring in thalassemia intense oxidative stress; these could generate more forms of MHA. (authors)

  18. Electron Spin Resonance (ESR) studies of returned comet nucleus samples

    International Nuclear Information System (INIS)

    Tsay, Fundow; Kim, S.S.; Liang, R.H.

    1989-01-01

    The most important objective of the Comet Nucleus Sample Returm Mission is to return samples which could reflect formation conditions and evolutionary processes in the early solar nebula. It is expected that the returned samples will consist of fine-grained silicate materials mixed with ices composed of simple molecules such as H 2 O, NH 3 , CH 4 as well as organics and/or more complex compounds. Because of the exposure to ionizing radiation from cosmic-ray, gamma-ray, and solar wind protons at low temperature, free radicals are expected to be formed and trapped in the solid ice matrices. The kind of trapped radical species together with their concentration and thermal stability can be used as a dosimeter as well as a geothermometer to determine thermal and radiation histories as well as outgassing and other possible alternation effects since the nucleus material was formed. Since free radicals that are known to contain unpaired electrons are all paramagnetic in nature, they can be readily detected and characterized in their native form by the Electron Spin Resonance (ESR) method. In fact, ESR has been shown to be a non-destructive, highly sensitive tool for the detection and characterization of paramagnetic, ferromagnetic, and radiation damage centers in terrestrial and extraterrestrial geological samples. The potential use of ESR as an effective method in the study of returned comet nucleus samples, in particular, in the analysis of fine-grained solid state icy samples is discussed

  19. ESR dating of the fault rocks

    International Nuclear Information System (INIS)

    Lee, Hee Kwon

    2005-01-01

    We carried out ESR dating of fault rocks collected near the nuclear reactor. The Upcheon fault zone is exposed close to the Ulzin nuclear reactor. The space-time pattern of fault activity on the Upcheon fault deduced from ESR dating of fault gouge can be summarised as follows : this fault zone was reactivated between fault breccia derived from Cretaceous sandstone and tertiary volcanic sedimentary rocks about 2 Ma, 1.5 Ma and 1 Ma ago. After those movements, the Upcheon fault was reactivated between Cretaceous sandstone and fault breccia zone about 800 ka ago. This fault zone was reactivated again between fault breccia derived form Cretaceous sandstone and Tertiary volcanic sedimentary rocks about 650 ka and after 125 ka ago. These data suggest that the long-term(200-500 k.y.) cyclic fault activity of the Upcheon fault zone continued into the Pleistocene. In the Ulzin area, ESR dates from the NW and EW trend faults range from 800 ka to 600 ka NE and EW trend faults were reactivated about between 200 ka and 300 ka ago. On the other hand, ESR date of the NS trend fault is about 400 ka and 50 ka. Results of this research suggest the fault activity near the Ulzin nuclear reactor fault activity continued into the Pleistocene. One ESR date near the Youngkwang nuclear reactor is 200 ka

  20. Basic ESR studies on recent corals

    Science.gov (United States)

    Walther, Ralf; Barabas, Michael; Mangini, Augusto

    Experiments on recent corals ( Acropora palmata, Barbados) were carried out to study the dating relevant properties of the characteristic ESR signals. Highly resolved signal growth curves (55 aliquots of a sieve fraction 125-250 μm) were obtained by γ-irradiation in small steps up to 20 kGy. The signal growth curve of the 'dating signal' at g = 2.0006 can only be approximated by a single exponential saturation function in a certain dose range. Thus, ADs derived with this function tend to be overestimated. A better analytical description by two different functions was tested. Isothermal annealing experiments were carried out at various temperatures before and after irradiation with a definite γ-dose respectively. The thermal decay of the dating signal is not 1st order. Furthermore, the decay process is strongly influenced by the decay of the traps themselves. The behaviour of the signals at g = 2.0057 and g = 2.0031 was compared with that of the dating signal. A surprising result was the growth of the signal at g = 2.0057 with γ-irradiation.

  1. Reflectivity quenching of ESR multilayer polymer film reflector in optically bonded scintillator arrays

    Science.gov (United States)

    Loignon-Houle, Francis; Pepin, Catherine M.; Charlebois, Serge A.; Lecomte, Roger

    2017-04-01

    The 3M-ESR multilayer polymer film is a widely used reflector in scintillation detector arrays. As specified in the datasheet and confirmed experimentally by measurements in air, it is highly reflective (> 98 %) over the entire visible spectrum (400-1000 nm) for all angles of incidence. Despite these outstanding characteristics, it was previously found that light crosstalk between pixels in a bonded LYSO scintillator array with ESR reflector can be as high as ∼30-35%. This unexplained light crosstalk motivated further investigation of ESR optical performance. Analytical simulation of a multilayer structure emulating the ESR reflector showed that the film becomes highly transparent to incident light at large angles when surrounded on both sides by materials of refractive index higher than air. Monte Carlo simulations indicate that a considerable fraction (∼25-35%) of scintillation photons are incident at these leaking angles in high aspect ratio LYSO scintillation crystals. The film transparency was investigated experimentally by measuring the scintillation light transmission through the ESR film sandwiched between a scintillation crystal and a photodetector with or without layers of silicone grease. Strong light leakage, up to nearly 30%, was measured through the reflector when coated on both sides with silicone, thus elucidating the major cause of light crosstalk in bonded arrays. The reflector transparency was confirmed experimentally for angles of incidence larger than 60 ° using a custom designed setup allowing illumination of the bonded ESR film at selected grazing angles. The unsuspected ESR film transparency can be beneficial for detector arrays exploiting light sharing schemes, but it is highly detrimental for scintillator arrays designed for individual pixel readout.

  2. Identification of irradiated pepper by ESR measurement

    International Nuclear Information System (INIS)

    Morishita, Norio; Kume, Tamikazu; Kawakami, Waichiro; Ishigaki, Isao

    1988-01-01

    The possibility of using electron spin resonance (ESR) for identification of irradiated black and white pepper was examined. The ESR spectra induced by irradiation with 10 kGy are clearly distinguishable from that of unirradiated samples. The intensity of signal induced by irradiation was markedly reduced during 2 weeks storage but it was slowly reduced on further storage. The difference of intensity between the irradiated and unirradiated samples can be distinguished after 13 weeks storage. In this experiment, ground black pepper, ground white pepper and whole white pepper can be identified after 13 weeks. On the other hand, whole black pepper cannot be identified after 8 weeks because of the variation of values. It suggests that the suitable method for sample preparation such as separation of pellicle of whole black pepper is required before ESR measurement. (author)

  3. LLNL high-field coil program

    International Nuclear Information System (INIS)

    Miller, J.R.

    1986-01-01

    An overview is presented of the LLNL High-Field Superconducting Magnet Development Program wherein the technology is being developed for producing fields in the range of 15 T and higher for both mirror and tokamak applications. Applications requiring less field will also benefit from this program. In addition, recent results on the thermomechanical performance of cable-in-conduit conductor systems are presented and their importance to high-field coil design discussed

  4. Dynamics of Gauge Fields at High Temperature

    NARCIS (Netherlands)

    Nauta, B.J.

    2000-01-01

    An effective description of dynamical Bose fields is provided by the classical (high-temperature) limit of thermal field theory. The main subject of this thesis is to improve the ensuing classical field theory, that is, to include the dominant quantum corrections and to add counter terms for the

  5. Stabilized high-field superconductor

    International Nuclear Information System (INIS)

    Marancik, W.G.; Ormand, F.T.; Gregory, E.

    1976-01-01

    A superconducting compound of the A-15 crystal structure type is obtained in a composite by a high temperature diffusion between a first metallic component and a second metallic component contained in a bronze alloy. Stability is achieved by including in the composite a quantity of high-conductivity normal material. Diffusion of the second metallic component into the normal material with a resultant degradation of conductivity of the normal material is prevented by placing an impervious barrier layer between the bronze alloy and the normal material. In a specific embodiment, the barrier layer takes the form of an annular shell comprising at least two sectors of dissimilar metals, one of which reacts with a component of the bronze alloy to form a layer of said superconducting compound, and the other of which is substantially non-reactive. Thus, a discontinuous superconducting ring is formed on the barrier layer which prevents flux trapping. 3 claims, 10 figures

  6. New Approach For Detection Of Irradiated Spices Using Electron Spin Resonance (ESR)

    International Nuclear Information System (INIS)

    FARAG, S.A.; SHAMS EL DIEEN, N.M.M.

    2010-01-01

    Black pepper and anise samples were irradiated with different doses of gamma rays (5, 10 and 20 kGy) then the irradiated samples were stored at room temperature (20 0 C, 70-75 % RH) for one year. The measurements of free radicals were carried out by electron spin resonance (ESR) at different intervals (3, 6, 9 and 12 months). A series of signals tentatively described as cellulose-like and complex radical observed at G values were 2.01027 for black pepper and 2.01019 for anise. The ESR signals of irradiated spices showed a directly proportional relationship for increasing dose with increasing intensity of signal. A relationship was noticed as polynomial regression analysis resulted between signals of ESR intensity and applied doses with significant values of correlation coefficient (R 2 ). All combination treatments of thermal and irradiation beside long storage caused significant reduction of ESR intensity of irradiated black pepper and anise. Upon using low doses as 1, 2 and 3 kGy for re-irradiation, the irradiated samples (10 and 20 kGy) increased the power of ESR intensity. The enhancement effect was markedly increased. For example, the irradiated black pepper (10 kGy) increased the ESR intensity with high percentages as 49.19%, 69.23% and 89.68% while the high dose (20 kGy) caused increase by 39.96%, 69.05% and 96.90% for irradiated black pepper samples. This approach with that technique can be used easily to overcome the main disadvantages of ESR signals fading especially at the end of storage period.

  7. Investigations of radical primary processes by ESR pulse radiolysis and ESR laser photolysis experiments

    International Nuclear Information System (INIS)

    Beckert, D.; Mehler, K.; Naumann, W.

    1984-08-01

    The Chemically Induced Magnetic Polarization of Electrons (CIDEP) describes the anomalies of ESR intensities of free radicals which react chemically. In this paper the fundamentals and some experimental results of the CIDEP effect are summarized. (author)

  8. High field MRI in the diagnosis of multiple sclerosis: high field-high yield?

    International Nuclear Information System (INIS)

    Wattjes, Mike P.; Barkhof, Frederik

    2009-01-01

    Following the approval of the U.S. Food and Drug Administration (FDA), high field magnetic resonance imaging (MRI) has been increasingly incorporated into the clinical setting. Especially in the field of neuroimaging, the number of high field MRI applications has been increased dramatically. Taking advantage on increased signal-to-noise ratio (SNR) and chemical shift, higher magnetic field strengths offer new perspectives particularly in brain imaging and also challenges in terms of several technical and physical consequences. Over the past few years, many applications of high field MRI in patients with suspected and definite multiple sclerosis (MS) have been reported including conventional and quantitative MRI methods. Conventional pulse sequences at 3 T offers higher lesion detection rates when compared to 1.5 T, particularly in anatomic regions which are important for the diagnosis of patients with MS. MR spectroscopy at 3 T is characterized by an improved spectral resolution due to increased chemical shift allowing a better quantification of metabolites. It detects significant axonal damage already in patients presenting with clinically isolated syndromes and can quantify metabolites of special interest such as glutamate which is technically difficult to quantify at lower field strengths. Furthermore, the higher susceptibility and SNR offer advantages in the field of functional MRI and diffusion tensor imaging. The recently introduced new generation of ultra-high field systems beyond 3 T allows scanning in submillimeter resolution and gives new insights into in vivo MS pathology on MRI. The objectives of this article are to review the current knowledge and level of evidence concerning the application of high field MRI in MS and to give some ideas of research perspectives in the future. (orig.)

  9. Progress in ESR dating of fossils

    International Nuclear Information System (INIS)

    Ikeya, M.

    1983-01-01

    In this review the progress of ESR dating is briefly described together with its historical development. Examples of fossil dating include shells and corals in geological sediments, fossil bones and teeth in anthropology and fossil woods in geology. The total dose of natural radiation (TD) equivalent to the archaeological dose in TL dating was obtained by the additive dose method. Initially, the TDs were plotted against the known ages; using the apparent annual dose-rate thus obtained gives the ESR age within a factor of 2 or 3 for a fossil. Precise assessment of the radiation environment was made later taking the disequilibrium of uranium series disintegration into account. ESR ages of corals agreed well with those obtained by radiocarbon and uranium-thorium methods. The time-independent accumulation rate or a linear accumulation or uranium was adopted as a first sensible model for the opensystem fossil bones: the relation between the TD and the age explains the ages of anthropologically important bones. Lastly, geological assessment of fossil woods was made by ESR based on the organic radicals and electron traps in the silicified part. (author)

  10. Radiation dosimetry by ESR in bone

    Energy Technology Data Exchange (ETDEWEB)

    Gallegos, R. (Universidad de San Agustin de Arequipa (Peru)); Marticorena, B. (Instituto Peruano de Energia Nuclear, Lima)

    1983-05-01

    The absorption speed in bovine bone samples irradiated with a /sup 90/Sr ..beta..-source of 45 mCi is studied with ESR. The signal changes linearly with the absorbed quantity of radiation to a maximum dose of 1.5 x 10/sup 6/ rads. This positive result allows to foresee the use of bone as a radiation dosimeter.

  11. Radiation dosimetry by ESR in bone

    International Nuclear Information System (INIS)

    Gallegos, R.; Marticorena, B.

    1983-01-01

    The absorption speed in bovine bone samples irradiated with a 90 Sr β-source of 45 mCi is studied with ESR. The signal changes linearly with the absorbed quantity of radiation to a maximum dose of 1.5 x 10 6 rads. This positive result allows to foresee the use of bone as a radiation dosimeter

  12. ESR dating of marine fossil shells

    International Nuclear Information System (INIS)

    Radtke, U.; Mangini, A.; Gruen, R.

    1985-01-01

    In order to establish the relatively new ESR dating method for marine shells a detailed comparison with the independent U-series technique was carried out. Agreement of both dating methods with the geological classification is strongly dependent on the species investigated and environmental conditions. Several problems encountered in the determination of the accumulated dose as well as the annual dose are discussed. (author)

  13. ESR dating of marine fossil shells

    Energy Technology Data Exchange (ETDEWEB)

    Radtke, U; Mangini, A; Gruen, R

    1985-01-01

    In order to establish the relatively new ESR dating method for marine shells a detailed comparison with the independent U-series technique was carried out. Agreement of both dating methods with the geological classification is strongly dependent on the species investigated and environmental conditions. Several problems encountered in the determination of the accumulated dose as well as the annual dose are discussed.

  14. ESR investigations of gamma irradiated beryllium ceramics

    International Nuclear Information System (INIS)

    Ryabikin, Yu.A.; Polyakov, A.I.; Petukhov, Yu.V.; Bitenbaev, M.I.; Zashkvara, O.V.

    2000-01-01

    In this report the result of ESR- investigation of kinetics of radiation paramagnetic defects accumulated in beryllium ceramics under gamma irradiation are presented. The data on quantum yield and destruction rate constants of these defects under ionizing irradiation are obtained. (orig.)

  15. ESR investigations of gamma irradiated beryllium ceramics

    Energy Technology Data Exchange (ETDEWEB)

    Ryabikin, Yu A; Polyakov, A I; Petukhov, Yu V; Bitenbaev, M I; Zashkvara, O V [Physical-Technical Inst., Almaty (Kazakhstan)

    2000-04-01

    In this report the result of ESR- investigation of kinetics of radiation paramagnetic defects accumulated in beryllium ceramics under gamma irradiation are presented. The data on quantum yield and destruction rate constants of these defects under ionizing irradiation are obtained. (orig.)

  16. ESR dosimetric properties of some biomineral materials

    International Nuclear Information System (INIS)

    Hassan, Gamal M.; Sharaf, M.A.

    2005-01-01

    Dosimetric properties of g-irradiated modern coral and bioactive glass (Bio-G) samples analyzed with electron spin resonance (ESR) have been separately reported (Hassan et al., 2004; Sharaf and Hassan, 2004) and compared with alanine. These are combined here to allow a three-way comparison between these materials

  17. ESR dosimetric properties of some biomineral materials

    Energy Technology Data Exchange (ETDEWEB)

    Hassan, Gamal M. [Department of Ionizing Radiation Metrology, National Institute for Standards (NIS), Tersa Street, El-Haram, El-Giza, P.O. Box 136 Giza, El-Giza (Egypt)]. E-mail: gamalhassan65@hotmail.com; Sharaf, M.A. [Department of Ionizing Radiation Metrology, National Institute for Standards (NIS), Tersa Street, El-Haram, El-Giza, P.O. Box 136 Giza, El-Giza (Egypt)

    2005-02-01

    Dosimetric properties of g-irradiated modern coral and bioactive glass (Bio-G) samples analyzed with electron spin resonance (ESR) have been separately reported (Hassan et al., 2004; Sharaf and Hassan, 2004) and compared with alanine. These are combined here to allow a three-way comparison between these materials.

  18. Expression of estrogen receptor α 36 (ESR36 in the hamster ovary throughout the estrous cycle: effects of gonadotropins.

    Directory of Open Access Journals (Sweden)

    Prabuddha Chakraborty

    Full Text Available Estradiol-17β (E plays an important role in ovarian follicular development. Evidence indicates that some of the effect of E is mediated by the transmembrane estrogen receptor. In this study, we examined the spatio-temporal expression of recently discovered ERα36 (ESR36, a splice variant of Esr1 and a receptor for non-genomic E signaling, in the hamster ovary during the estrous cycle and the role of gonadotropins and ovarian steroid hormones in ESR36 expression. ESR36 expression was high on estrus (D1:0900 h and declined precipitously by proestrus (D4:0900 h and remained low up to D4:1600 h. Immunofluorescence findings corroborated immunoblot findings and revealed that ESR36 was expressed only in the cell membrane of both follicular and non-follicular cells, except the oocytes. Ovarian ESR36 was capable of binding to the E-affinity matrix, and have different molecular weight than that of the ESR1 or GPER. Hypophysectomy (Hx resulted in a marked decline in ESR36 protein levels. FSH and LH, alone or combined, markedly upregulated ESR36 protein in Hx hamsters to the levels observed in D1 hamsters, but neither E nor P had any effect. Inhibition of the gonadotropin surge by phenobarbital treatment on D4:1100 h attenuated ESR36 expression in D1:0900 h ovaries, but the decline was restored by either FSH or LH replacement on D4 afternoon. This is the first report to show that ESR36, which is distinct from ESR1 or GPER is expressed in the plasma membrane of ovarian follicular and non-follicular cells, binds to E and its expression is regulated directly by the gonadotropins. In light of our previous findings, the results suggest that ovarian cells contain at least two distinct membrane estrogen receptors, such as GPER and ESR36, and strongly suggest for a non-genomic action of E regulating ovarian follicular functions.

  19. The result of Alanine/ESR dosimetry at Wolsung unit 1

    International Nuclear Information System (INIS)

    Park, Byeong Ryong; Choi, Hoon; Lim, Young Khi

    2008-01-01

    It needs accurate estimation of radiation level for verifying machinery and cable in Nuclear Power Plant. Therefore, in this study, we used ESR(Electron Spin Resonance) system for estimate dose of Alanine dosimeter. Alanine/ESR dosimetry, already known as a dosimetric method in medical and industrial field, was applied to estimate dose quantity at cable locations within a nuclear power plant as a part of equipment qualification program. Alanine/ESR dosimetry of absorbed dose range is 1 - 100 KGy. The alanine dosimeter is not significantly affected by temperature and fading is limited to 1% per year. The alanine dosimeters were fixed on the targeted cable or nearest position to measure dose quantity to get accurate value. Alanine dosimeters were scanned by commercially used two different ESR systems, e-scan and EMX series for alanine dosimeters. To estimate more accurate dose, two environmental correction factors, irradiation temperature and dosimeter weight, were used in calculation of absorbed dose quantity. In this study, dose values which are alinine dosimeter from Wolsong unit 1 are measured by two ESR systems. And then the results was compared each other

  20. Synchrotron Applications of High Magnetic Fields

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    2006-07-01

    This workshop aims at discussing the scientific potential of X-ray diffraction and spectroscopy in magnetic fields above 30 T. Pulsed magnetic fields in the range of 30 to 40 T have recently become available at Spring-8 and the ESRF (European synchrotron radiation facility). This document gathers the transparencies of the 6 following presentations: 1) pulsed magnetic fields at ESRF: first results; 2) X-ray spectroscopy and diffraction experiments by using mini-coils: applications to valence state transition and frustrated magnet; 3) R{sub 5}(Si{sub x}Ge{sub 1-x}){sub 4}: an ideal system to be studied in X-ray under high magnetic field?; 4) high field studies at the Advanced Photon Source: present status and future plans; 5) synchrotron X-ray diffraction studies under extreme conditions; and 6) projects for pulsed and steady high magnetic fields at the ESRF.

  1. Neutron Scattering and High Magnetic Fields

    Energy Technology Data Exchange (ETDEWEB)

    Winn, Barry L. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Stone, Matthew B. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)

    2014-11-01

    The workshop “Neutron Scattering and High Magnetic Fields” was held September 4-5, 2014 at the Oak Ridge National Laboratory (ORNL). The workshop was held in response to a recent report by the National Research Council of the National Academy of Sciences entitled “High Magnetic Field Science and Its Application in the United States: Current Status and Future Directions.”1 This report highlights the fact that neutron scattering measurements carried out in high magnetic fields provide important opportunities for new science. The workshop explored the range of the scientific discoveries that could be enabled with neutron scattering measurements at high fields (25 Tesla or larger), the various technologies that might be utilized to build specialized instruments and sample environment equipment to enable this research at ORNL, and possible routes to funding and constructing these facilities and portable high field sample environments.

  2. Ultra high field magnetic resonance imaging

    International Nuclear Information System (INIS)

    Lethimonnier, F.; Vedrine, P.

    2007-01-01

    Understanding human brain function, brain development and brain dysfunction is one of the great challenges of the twenty first century. Biomedical imaging has now run up against a number of technical constraints that are exposing limits to its potential. In order to overcome the current limits to high-field magnetic resonance cerebral imaging (MRI) and unleash its fullest potential, the Cea has built NeuroSpin, an ultra-high-field neuroimaging facility at its Saclay centre (in the Essonne). NeuroSpin already boasts three fully operational MRI systems. The first is a 3-tesla high-field system and the second is a very-high-field 7-tesla system, both of which are dedicated to clinical studies and investigations in humans, while the third is an ultra-high-field 17.65-tesla system designed for studies on small animals. In 2011, NeuroSpin will be commissioning an 11.7-tesla ultra-high-field system of unprecedented power that is designed for research on human subjects. The level of the magnetic field and the scale required will make this joint French-German project to build the magnet a breakthrough in the international arena. (authors)

  3. Phase transitions of natural corals monitored by ESR spectroscopy

    Energy Technology Data Exchange (ETDEWEB)

    Vongsavat, V. [Department of Chemistry, Faculty of Science, Mahidol University, Rama VI Road, Rajathevi, Bangkok 10400 (Thailand); Winotai, P. [Department of Chemistry, Faculty of Science, Mahidol University, Rama VI Road, Rajathevi, Bangkok 10400 (Thailand); Meejoo, S. [Department of Chemistry, Faculty of Science, Mahidol University, Rama VI Road, Rajathevi, Bangkok 10400 (Thailand)]. E-mail: scsmj@mahidol.ac.th

    2006-01-15

    The main purpose of this work is to present a systematic study of structure of marine exoskeletons, Acropora coral and its structural transformation upon heat treatments. The coralline sample was ground and characterized as powder throughout this work. Structural identifications of all samples have been confirmed using X-ray diffraction and IR spectroscopy. It was clearly found that the fresh specimen is made of aragonite, a common phase of the mineral CaCO{sub 3}. Thermal analyses, DSC and TGA were used to monitor structural and thermal decompositions and an irreversible solid-state phase transition from aragonite to calcite of the marine carbonate. Next, the coral powder was annealed at specific temperatures over the range 350-900 deg. C, and the effects of heat treatment on the structure of coralline samples were carefully studied by Rietveld refinement method. In addition, we have examined Mn{sup 2+} paramagnetic ions and free radicals present in the coral and changes of those upon heating by using ESR spectroscopy. The local environments of Mn{sup 2+} ions were verified from the calculated ESR spectra using appropriate spin Hamiltonian parameters, i.e. gyromagnetic tensor g , zero-field splitting D and hyperfine tensor A . This work reported structures and compositions as well as physical, chemical and thermal properties of the coralline material upon heat treatments qualitatively and quantitatively.

  4. Phase transitions of natural corals monitored by ESR spectroscopy

    International Nuclear Information System (INIS)

    Vongsavat, V.; Winotai, P.; Meejoo, S.

    2006-01-01

    The main purpose of this work is to present a systematic study of structure of marine exoskeletons, Acropora coral and its structural transformation upon heat treatments. The coralline sample was ground and characterized as powder throughout this work. Structural identifications of all samples have been confirmed using X-ray diffraction and IR spectroscopy. It was clearly found that the fresh specimen is made of aragonite, a common phase of the mineral CaCO 3 . Thermal analyses, DSC and TGA were used to monitor structural and thermal decompositions and an irreversible solid-state phase transition from aragonite to calcite of the marine carbonate. Next, the coral powder was annealed at specific temperatures over the range 350-900 deg. C, and the effects of heat treatment on the structure of coralline samples were carefully studied by Rietveld refinement method. In addition, we have examined Mn 2+ paramagnetic ions and free radicals present in the coral and changes of those upon heating by using ESR spectroscopy. The local environments of Mn 2+ ions were verified from the calculated ESR spectra using appropriate spin Hamiltonian parameters, i.e. gyromagnetic tensor g , zero-field splitting D and hyperfine tensor A . This work reported structures and compositions as well as physical, chemical and thermal properties of the coralline material upon heat treatments qualitatively and quantitatively

  5. Development of high field superconducting magnet

    International Nuclear Information System (INIS)

    Irie, Fujio; Takeo, Masakatsu.

    1986-01-01

    Recently, in connection with nuclear fusion research, the development of high field superconducting magnets showed rapid progress. The development of high field magnets of 15 T class by the techniques of winding after heat treatment has been continued in various places, as these techniques are suitable to make large magnets. In 1985, Kyushu University attained the record of 15.5 T. However in high field magnets, there are many problems peculiar to them, and the basic research related to those is demanded. In this report, these general problems, the experience of the design and manufacture in Kyushu University and the related problems are described. The superconducting magnet installed in the Superconducting Magnet Research Center of Kyushu University attained the record of 15.5 T for the first time in March, 1985. In superconducting magnets, very difficult problem must be solved since superconductivity, heat and mechanical force are inter related. The problems of the wire materials for high field, the scale of high field magnets, the condition limiting mean current density, and the development of high field magnets in Kyushu University are described. (Kako, I.)

  6. ESR studies on degradation processes in polyethyleneterephtalate

    International Nuclear Information System (INIS)

    Chipara, M.; Chipara, M.D.; Georgescu, L.; Constantinescu, L.; Morosanu, C.

    2002-01-01

    Complete text of publication follows. The generation of free radicals by degradation processes (thermal, plasma and radiation induced) is analyzed. Details regarding the generation of free radicals, their interactions, and kinetics, as revealed by electron spin resonance (ESR), with emphasis on laser beam degradation, are discussed. Some ESR lines of laser-irradiated polyethyleneterephtalate (PET), recorded at room temperature, are shown in Figure 1. The lines are narrow singlets located around g=2.003. The resonance line amplitude, width and double integral of the resonance line are affected by the power of the incident beam. The common features of these degradation processes (universal behavior) as well as the fingerprints of each degradation process are analyzed in detail

  7. ESR study of free radicals in mango

    Science.gov (United States)

    Kikuchi, Masahiro; Hussain, Mohammad S.; Morishita, Norio; Ukai, Mitsuko; Kobayashi, Yasuhiko; Shimoyama, Yuhei

    2010-01-01

    An electron spin resonance (ESR) spectroscopic study of radicals induced in irradiated fresh mangoes was performed. Mangoes in the fresh state were irradiated with γ-rays, lyophilized and then crushed into a powder. The ESR spectrum of the powder showed a strong main peak at g = 2.004 and a pair of peaks centered at the main peak. The main peak was detected from both flesh and skin specimens. This peak height gradually decreased during storage following irradiation. On the other hand, the side peaks showed a well-defined dose-response relationship even at 9 days post-irradiation. The side peaks therefore provide a useful means to define the irradiation of fresh mangoes.

  8. ESR dosimetry of optically bleached quartz grains extracted from Plio-Quaternary sediment: Evaluating some key aspects of the ESR signals associated to the Ti-centers

    International Nuclear Information System (INIS)

    Duval, Mathieu; Guilarte, Verónica

    2015-01-01

    The present study aims at investigating several key aspects of ESR dose reconstruction of quartz grains based on the analysis of the Ti-center: (i) the evaluation of the ESR intensity, (ii) its impact on measurements precision, and (iii) the potential of various fitting functions to describe the behavior of the signal with the radiation absorbed dose. In contrast with the Al center, the various Ti centers have quite low ESR signal intensities. It is thus crucial to adapt the experimental conditions for the optimization of the signal-to-noise ratio and to perform repeated measurements in order to take into consideration the uncertainty associated to angular dependence of the signal as well as day-to-day variations. Several options (named A to E) for evaluating the ESR intensity of the Ti–Li and Ti–H centers are explored and some of them yield too much experimental uncertainty (e.g. options C and E) and are apparently not suitable for accurate ESR dosimetry. In contrast, options A and D usually provide similar equivalent dose (D E ) results and can be used together for assessing the dose absorbed by the Ti–Li center. Our results show a systematic non-monotonic behavior of the ESR signal of the Ti center with the dose, which raise some questions about the suitability of the single saturating exponential (SSE) function that is classically used in ESR dating. Consequently, we explored the potential of other functions that can describe the “radiation bleaching” phenomenon observed at high doses. We recommend the use of a specific fitting function (called Ti-2 in the present paper) previously proposed by Woda and Wagner (2007) for any dose reconstruction, and define some criteria to ensure a good fitting. The SSE function provides D E results that are, in most cases, relatively consistent with those derived from the Ti-2, suggesting that the Ti centers apparently follow a SSE behavior up to, at least, 6.0–6.5 kGy However, the reliability of the D E values

  9. Critical fields in high temperature superconductors

    International Nuclear Information System (INIS)

    Finnemore, D.K.

    1991-01-01

    An analysis of various methods to obtain the critical fields of the high temperature superconductors from experimental data is undertaken in order to find definitions of these variables that are consistent with the models used to define them. Characteristic critical fields of H c1 , H c2 and H c that occur in the Ginsburg-Landau theory are difficult to determine experimentally in the high temperature superconductors because there are additional physical phenomena that obscure the results. The lower critical field is difficult to measure because there are flux pinning and surface barrier effects to flux entry; the upper critical field is difficult because fluctuation effects are large at this phase boundary; the thermodynamic critical field is difficult because fluctuations make it difficult to know the field where the magnetization integral should be terminated. In addition to these critical fields there are at least two other cross-over fields. There is the so called irreversibility line where the vortices transform from a rigid flux line lattice to a fluid lattice and there is a second cross-over field associated with the transition from the fluctuation to the Abrikosov vortex regime. The presence of these new physical effects may require new vocabulary

  10. Idea Generation in Highly Institutionalized Fields

    DEFF Research Database (Denmark)

    Agoguè, Marine; Boxenbaum, Eva

    innovation. An important question facing innovation research is thus how actors can generate ideas that break with the field frame in highly institutionalized fields? To answer this question, we draw on insights into dual process modeling from cognitive sciences. Dual process modeling emphasizes...... the different nature of the conscious (deliberate) and subconscious (implicit) systems involved in ideation. We further elaborate on how these two systems relate to four streams of research that management scholars evoke to model microprocesses of generating new ideas, namely metaphors, conceptual blending......The early phase of innovation processes in highly institutionalized fields relies on the capabilities of actors to generate new ideas that break with the field frame. Informed by a dominant logic, a field frame shapes collective cognition and can thus prevent the generation of new ideas and block...

  11. High-field superferric MR magnet

    International Nuclear Information System (INIS)

    Huson, F.R.; Carcagno, R.; Colvin, J.

    1987-01-01

    Current large-bore (>20 cm), high-field (2-T) MR magnets have major implementation disadvantages, mostly related to the extensive stray field of traditional air-core superconducting magnets. To circumvent this problem, the authors designed, constructed, and tested a 30-cm prototype superconducting, self-shielded, high field magnet. This unshimmed superferric magnet can operate between 0.5 and 4 T with a field quality of about one part per million over one quarter of its aperture. The magnet can be ramped from one field strength to another in approximately 10 minutes. The 5-Gauss line extends less than 1 meter outside the magnet structure. Further details, including MR measurements and images, are demonstrated, as well as 1-meter bore scale-up projections

  12. High-magnetic field atomic physics

    International Nuclear Information System (INIS)

    Gay, J.C.

    1984-01-01

    This chapter discusses both the traditional developments of Zeeman techniques at strong fields and the fundamental concepts of diamagnetism. Topics considered include historical aspects, the production of high fields, the atom in a magnetic field (Hamiltonian and symmetries, the various magnetic regimes in atomic spectra), applications of the Zeeman effect at strong B fields, the Landau regime for loosely bound particles, theoretical concepts of atomic diamagnetism, and the ultra-high-field regime and quantum electrodynamics. It is concluded that the wide implications of the problem of the strongly magnetized hydrogen atom in various domains of physics and its conceptual importance concerning theoretical methods of classical and quantum mechanics justify the experimental and theoretical efforts in atomic physics

  13. The influence of surface modification, coating agents and pH value of aqueous solutions on physical properties of magnetite nanoparticles investigated by ESR method

    Energy Technology Data Exchange (ETDEWEB)

    Dobosz, Bernadeta, E-mail: benia@amu.edu.pl [Medical Physics Division, Faculty of Physics, Adam Mickiewicz University, Umultowska 85, 61-614 Poznań (Poland); Krzyminiewski, Ryszard [Medical Physics Division, Faculty of Physics, Adam Mickiewicz University, Umultowska 85, 61-614 Poznań (Poland); Kurczewska, Joanna; Schroeder, Grzegorz [Faculty of Chemistry, Adam Mickiewicz University, Umultowska 89B, 61-614 Poznań (Poland)

    2017-05-01

    The article presents the results of electron spin resonance (ESR) studies for aqueous solutions of functionalized superparamagnetic iron(II,III) oxide nanoparticles. The samples studied differed in type of organic ligands at the magnetite surface, type of coating agent and pH value of aqueous solutions. The ESR spectra of the samples were obtained at room temperature and at 230 K. The field cooling (FC) experiment was performed for selected samples, and the effective anisotropy field (H{sub K2}) and the first order magnetocrystalline anisotropy constant (K{sub 1}) was calculated. The process of the nanoparticles diffusion in different environments (human blood, human serum) forced by an inhomogeneous magnetic field was monitored and their interactions with different solvents have been discussed. It has been shown that ESR method is useful to observe the impact of organic ligands at the magnetite surface, type of coating agent and pH value of aqueous solutions on the properties of iron(II,III) oxide nanoparticles. - Highlights: • The influence of different organic ligands, coatings and pH values of aqueous solutions on the physical properties of the magnetite nanoparticles studied by ESR method. • Nanoparticles diffusion forced by inhomogeneous magnetic field monitored by ESR and explained. • A narrow line separated in ESR spectra by CREM. • The influence of different coatings and pH values of aqueous solutions on ESR spectra of TEMPO attached to the magnetite core.

  14. IAEA reference dosimeter: Alanine-ESR

    International Nuclear Information System (INIS)

    Mehta, K.; Girzikowsky, R.

    1999-01-01

    Since 1985, the IAEA has been using alanine-ESR as a transfer dosimeter for its dose quality audit service, namely the International Dose Assurance Service. The alanine dosimeters are rod-type containing 70 wt% DL--α-alanine and 30 wt% polystyrene. We have two self-shielded gamma facilities for the calibration of the dosimetry system, where the temperature within the irradiation chamber can be controlled by a specially designed unit. A 4th order polynomial is fitted to the 16 data points in the dose range of 100 Gy to 50 kGy. The measured value of the irradiation temperature coefficient at two dose values (15 and 45 kGy) is 0.23 %/deg. C. Also, the ESR-response was followed for several dosimeters for about 8 months to study the post-irradiation effect. A value of 0.008 %/day was observed for the fading of the response for two dose values (15 and 45 kGy) and three irradiation temperatures (15, 27 and 40 deg. C). The effect of the analysis temperature on the ESR response was also studied. The combined relative uncertainty for the IAEA alanine-ESR dosimetry system is 1.5% (k=1). This includes that transferred from the primary laboratory for the dose rate measurements of the gamma facilities, dosimetry system calibration uncertainties, batch variability and uncertainty in the curve fitting procedure. This value however does not include the contribution due to the irradiation temperature correction which is applied when it differs from that during calibration; this component being specific for each dose measurement. (author)

  15. Background field coils for the High Field Test Facility

    International Nuclear Information System (INIS)

    Zbasnik, J.P.; Cornish, D.N.; Scanlan, R.M.; Jewell, A.M.; Leber, R.L.; Rosdahl, A.R.; Chaplin, M.R.

    1980-01-01

    The High Field Test Facility (HFTF), presently under construction at LLNL, is a set of superconducting coils that will be used to test 1-m-o.d. coils of prototype conductors for fusion magnets in fields up to 12 T. The facility consists of two concentric sets of coils; the outer set is a stack of Nb-Ti solenoids, and the inner set is a pair of solenoids made of cryogenically-stabilized, multifilamentary Nb 3 Sn superconductor, developed for use in mirror-fusion magnets. The HFTF system is designed to be parted along the midplane to allow high-field conductors, under development for Tokamak fusion machines, to be inserted and tested. The background field coils were wound pancake-fashion, with cold-welded joints at both the inner and outer diameters. Turn-to-turn insulation was fabricated at LLNL from epoxy-fiberglass strip. The coils were assembled and tested in our 2-m-diam cryostat to verify their operation

  16. ESR of Gd3+ in magnetically ordered Eu2CuO4

    International Nuclear Information System (INIS)

    Rettori, C.; Oseroff, S.B.; Rao, D.; Valdivia, J.A.; Barberis, G.E.; Martins, G.B.; Sarrao, J.; Fisk, Z.; Tovar, M.

    1996-01-01

    Electron spin resonance (ESR) experiments of Gd 3+ in the antiferromagnetic (AF) ordered phase (T N ) of Eu 2 CuO 4 can be interpreted in terms of four magnetically nonequivalent rare-earth sites with local internal fields H i =±310(30) Oe along the [100] and [010] directions. The internal field is well described by a dipolar magnetic field of a noncollinear AF array of 0.35(4) μ B per Cu moment aligned along the [100] and [010] directions. This is consistent with recent results of magnetic-field-dependent neutron-diffraction experiments. From the ESR and magnetic susceptibility data, the crystal field parameters for Gd 3+ and Eu 3+ in Eu 2 CuO 4 are determined. The exchange parameters between the rare earths are also estimated. copyright 1996 The American Physical Society

  17. The ESR dating of fossil enamel samples from palaeo-anthropological and Palaeolithic sites of Early Pleistocene

    International Nuclear Information System (INIS)

    Chen Qi; Chen Tiemei; Li Jiuqiang

    1999-01-01

    The following problems regarding the ESR dating of fossil enamel samples from palaeo-anthropological and Palaeolithic sites of Early Pleistocene are discussed: 1) the applicability of exponential fitting in the additive method for reliable AD determination; 2) the thermo-stability of the g = 2.0018 line of hydroxyapatite and its influence on apparent ESR ages; 3) the right selection of U-uptake models; and 4) the effect of high U-content in enamel on the ESR ages. It is concluded that the ESR-EU ages of Early Pleistocene enamel samples can only be regarded as the lower limit of the true ages if no appropriate corrections for the factors discussed above are made

  18. Individual Dosimetry for High Energy Radiation Fields

    International Nuclear Information System (INIS)

    Spurny, F.

    1999-01-01

    The exposure of individuals on board aircraft increased interest in individual dosimetry in high energy radiation fields. These fields, both in the case of cosmic rays as primary radiation and at high energy particle accelerators are complex, with a large diversity of particle types, their energies, and linear energy transfer (LET). Several already existing individual dosemeters have been tested in such fields. For the component with high LET (mostly neutrons) etched track detectors were tested with and without fissile radiators, nuclear emulsions, bubble detectors for both types available and an albedo dosemeter. Individual dosimetry for the low LET component has been performed with thermoluminescent detectors (TLDs), photographic film dosemeters and two types of electronic individual dosemeters. It was found that individual dosimetry for the low LET component was satisfactory with the dosemeters tested. As far as the high LET component is concerned, there are problems with both the sensitivity and the energy response. (author)

  19. Coordinated research efforts for establishing an international radiotherapy dose intercomparison service based on the alanine/ESR system

    International Nuclear Information System (INIS)

    Nette, H.P.; Onori, S.; Fattibene, P.; Regulla, D.; Wieser, A.

    1993-01-01

    The IAEA has long been active in the field of high-dose standardization. An International Dose Assurance Service (IDAS) was established based on alanine/ESR dosimetry. This service operates over the range of 100 Gy to 100 kGy and is directed towards industrial radiation processing in IAEA member states. It complements the IAEA/WHO TLD postal dose intercomparison service for dose assurance in hospital radiotherapy departments. Experience with the alanine high dose service suggests that the alanine dosimeter might provide superior performance to TLD in the therapy dose range. Preliminary test measurements with the participation of GSF/Germany, Istituto Superiore di Sanita/Italy (both providing alanine dosimeters and their evaluation) and IAEA (providing reference irradiations) seems to justify research efforts through an IAEA Coordinated Research Programme (CRP). This CRP, entitled ''Therapy Level Dosimetry with the Alanine/ESR System'' is presently under set-up. It will include general work common to all assigned/potential contract holders as well as some specific research topics in accordance to individual proposals of each participant. (author)

  20. High Accelerating Field Superconducting Radio Frequency Cavities

    Science.gov (United States)

    Orr, R. S.; Saito, K.; Furuta, F.; Saeki, T.; Inoue, H.; Morozumi, Y.; Higo, T.; Higashi, Y.; Matsumoto, H.; Kazakov, S.; Yamaoka, H.; Ueno, K.; Sato, M.

    2008-06-01

    We have conducted a study of a series of single cell superconducting RF cavities at KEK. These tests were designed to investigate the effect of surface treatment on the maximum accelerating field attainable. All of these cavities are of the ICHIRO shape, based on the Low Loss shape. Our results indicate that accelerating fields as high as the theoretical maximum of 50MV/m are attainable.

  1. Moderate and high intensity pulsed electric fields

    OpenAIRE

    Timmermans, Rian Adriana Hendrika

    2018-01-01

    Pulsed Electric Field (PEF) processing has gained a lot of interest the last decades as mild processing technology as alternative to thermal pasteurisation, and is suitable for preservation of liquid food products such as fruit juices. PEF conditions typically applied at industrial scale for pasteurisation are high intensity pulsed electric fields aiming for minimal heat load, with an electric field strength (E) in the range of 15 − 20 kV/cm and pulse width (τ) between 2 − 20 μs. Alternativel...

  2. High magnetic fields science and technology

    CERN Document Server

    Miura, Noboru

    2003-01-01

    This three-volume book provides a comprehensive review of experiments in very strong magnetic fields that can only be generated with very special magnets. The first volume is entirely devoted to the technology of laboratory magnets: permanent, superconducting, high-power water-cooled and hybrid; pulsed magnets, both nondestructive and destructive (megagauss fields). Volumes 2 and 3 contain reviews of the different areas of research where strong magnetic fields are an essential research tool. These volumes deal primarily with solid-state physics; other research areas covered are biological syst

  3. Advances in high field laser physics

    CERN Document Server

    Sheng, Zhengming; Chen, Liming; Lu, Wei; Shen, Baifei

    2019-01-01

    High field laser physics emerged with the advent of ultrashort intense lasers about 25 years ago. It has developed into a frontier of cross-disciplinary studies, covering attosecond X-ray physics, particle accelerator physics, and physics of inertial confined fusion, etc., with prospects of wide applications. Because this is a new and rapidly developing field, so far there are only 2-3 related books available. There are a few review articles in some journals, which are limited to specific topics in high field physics. There are quite a few conference proceedings in this field, which are the collections of papers presented at conferences. In this book, a few leading experts working on different subjects in this field are invited to introduce the key topics in high field laser physics, which cover the involved fundamental physics, the recent advances, as well as the prospects of future applications. It shall be very useful to graduate students, young researchers, and people who want to have an overview of thi...

  4. High-field dipoles for future accelerators

    International Nuclear Information System (INIS)

    Wipf, S.L.

    1984-09-01

    This report presents the concept for building superconducting accelerator dipoles with record high fields. Economic considerations favor the highest possible current density in the windings. Further discussion indicates that there is an optimal range of pinning strength for a superconducting material and that it is not likely for multifilamentary conductors to ever equal the potential performance of tape conductors. A dipole design with a tape-wound, inner high-field winding is suggested. Methods are detailed to avoid degradation caused by flux jumps and to overcome problems with the dipole ends. Concerns for force support structure and field precision are also addressed. An R and D program leading to a prototype 11-T dipole is outlined. Past and future importance of superconductivity to high-energy physics is evident from a short historical survey. Successful dipoles in the 10- to 20-T range will allow interesting options for upgrading present largest accelerators

  5. ESR analysis of irradiated frogs' legs and fishes

    International Nuclear Information System (INIS)

    Raffi, J.; Agnel, J.-P.; Evans, J.C.; Rowlands, C.C.; Lesgards, G.

    1989-01-01

    Electron spin resonance (ESR) spectral analysis of different parts (bones, scales, jaw, etc.) from ionized (irradiated) frozen frogs' legs and fishes (brown trout and sardine) were recorded. There is always present, after treatment, a signal due to the irradiation. ESR and ENDOR experiments lead us to assign it to h 1 centers from hydroxyapatite, as in the case of other irradiated meat bones. The use of ESR to prove whether one of these foods has been irradiated or not is discussed. (author)

  6. Field and frequency modulated sub-THz electron spin resonance spectrometer

    Directory of Open Access Journals (Sweden)

    Christian Caspers

    2016-05-01

    Full Text Available 260-GHz radiation is used for a quasi-optical electron spin resonance (ESR spectrometer which features both field and frequency modulation. Free space propagation is used to implement Martin-Puplett interferometry with quasi-optical isolation, mirror beam focusing, and electronic polarization control. Computer-aided design and polarization pathway simulation lead to the design of a compact interferometer, featuring lateral dimensions less than a foot and high mechanical stability, with all components rated for power levels of several Watts suitable for gyrotron radiation. Benchmark results were obtained with ESR standards (BDPA, DPPH using field modulation. Original high-field ESR of 4f electrons in Sm3+-doped Ceria was detected using frequency modulation. Distinct combinations of field and modulation frequency reach a signal-to-noise ratio of 35 dB in spectra of BDPA, corresponding to a detection limit of about 1014 spins.

  7. Molecular dynamics in high electric fields

    International Nuclear Information System (INIS)

    Apostol, M.; Cune, L.C.

    2016-01-01

    Highlights: • New method for rotation molecular spectra in high electric fields. • Parametric resonances – new features in spectra. • New elementary excitations in polar solids from dipolar interaction (“dipolons”). • Discussion about a possible origin of the ferroelectricity from dipolar interactions. - Abstract: Molecular rotation spectra, generated by the coupling of the molecular electric-dipole moments to an external time-dependent electric field, are discussed in a few particular conditions which can be of some experimental interest. First, the spherical-pendulum molecular model is reviewed, with the aim of introducing an approximate method which consists in the separation of the azimuthal and zenithal motions. Second, rotation spectra are considered in the presence of a static electric field. Two particular cases are analyzed, corresponding to strong and weak fields. In both cases the classical motion of the dipoles consists of rotations and vibrations about equilibrium positions; this motion may exhibit parametric resonances. For strong fields a large macroscopic electric polarization may appear. This situation may be relevant for polar matter (like pyroelectrics, ferroelectrics), or for heavy impurities embedded in a polar solid. The dipolar interaction is analyzed in polar condensed matter, where it is shown that new polarization modes appear for a spontaneous macroscopic electric polarization (these modes are tentatively called “dipolons”); one of the polarization modes is related to parametric resonances. The extension of these considerations to magnetic dipoles is briefly discussed. The treatment is extended to strong electric fields which oscillate with a high frequency, as those provided by high-power lasers. It is shown that the effect of such fields on molecular dynamics is governed by a much weaker, effective, renormalized, static electric field.

  8. Iron chalcogenide superconductors at high magnetic fields

    Science.gov (United States)

    Lei, Hechang; Wang, Kefeng; Hu, Rongwei; Ryu, Hyejin; Abeykoon, Milinda; Bozin, Emil S; Petrovic, Cedomir

    2012-01-01

    Iron chalcogenide superconductors have become one of the most investigated superconducting materials in recent years due to high upper critical fields, competing interactions and complex electronic and magnetic phase diagrams. The structural complexity, defects and atomic site occupancies significantly affect the normal and superconducting states in these compounds. In this work we review the vortex behavior, critical current density and high magnetic field pair-breaking mechanism in iron chalcogenide superconductors. We also point to relevant structural features and normal-state properties. PMID:27877518

  9. Identification of irradiated mangoes by means of ESR spectroscopy

    International Nuclear Information System (INIS)

    Bustos, M.E.; Romero, M.E.; Gutierrez, A.; Azorin, J.

    1996-01-01

    Samples of mango varieties Tommy Atkins, Haiden and Ataulfo were irradiated with 60 Co gamma radiation at doses in the range 0.15-1.0 kGy, and stored at room temperature for lapses of time up to 72 h. They were then studied by ESR spectrometry. Results show that the ESR signal of the irradiated samples is higher than that of the unirradiated samples, and this is found even at the minimum radiation dose of 0.15 kGy. The ESR signal remained stable during the storage time. The ESR signals obtained for hydroheated mangoes show insignificant differences with respect to the control samples. (author)

  10. An Endogenous Electron Spin Resonance (ESR signal discriminates nevi from melanomas in human specimens: a step forward in its diagnostic application.

    Directory of Open Access Journals (Sweden)

    Eleonora Cesareo

    Full Text Available Given the specific melanin-associated paramagnetic features, the Electron Spin Resonance (ESR, called also Electron Paramagnetic Resonance, EPR analysis has been proposed as a potential tool for non-invasive melanoma diagnosis. However, studies comparing human melanoma tissues to the most appropriate physiological counterpart (nevi have not been performed, and ESR direct correlation with melanoma clinical features has never been investigated. ESR spectrum was obtained from melanoma and non-melanoma cell-cultures as well as mouse melanoma and non-melanoma tissues and an endogenous ESR signal (g = 2.005 was found in human melanoma cells and in primary melanoma tissues explanted from mice, while it was always absent in non-melanoma samples. These characteristics of the measured ESR signal strongly suggested its connection with melanin. Quantitative analyses were then performed on paraffin-embedded human melanoma and nevus sections, and validated on an independent larger validation set, for a total of 112 sections (52 melanomas, 60 nevi. The ESR signal was significantly higher in melanomas (p = 0.0002 and was significantly different between "Low Breslow's and "High Breslow's" depth melanomas (p<0.0001. A direct correlation between ESR signal and Breslow's depth, expressed in millimetres, was found (R = 0.57; p<0.0001. The eu/pheomelanin ratio was found to be significantly different in melanomas "Low Breslow's" vs melanomas "High Breslow's" depth and in nevi vs melanomas "High Breslow's depth". Finally, ROC analysis using ESR data discriminated melanomas sections from nevi sections with up to 90% accuracy and p<0.0002. In the present study we report for the first time that ESR signal in human paraffin-embedded nevi is significantly lower than signal in human melanomas suggesting that spectrum variations may be related to qualitative melanin differences specifically occurring in melanoma cells. We therefore conclude that this ESR signal

  11. Fiber optics in high dose radiation fields

    International Nuclear Information System (INIS)

    Partin, J.K.

    1985-01-01

    A review of the behavior of state-of-the-art optical fiber waveguides in high dose (greater than or equal to 10 5 rad), steady state radiation fields is presented. The influence on radiation-induced transmission loss due to experimental parameters such as dose rate, total dose, irradiation history, temperature, wavelength, and light intensity, for future work in high dose environments are given

  12. Strain sensors for high field pulse magnets

    Energy Technology Data Exchange (ETDEWEB)

    Martinez, Christian [Los Alamos National Laboratory; Zheng, Yan [Los Alamos National Laboratory; Easton, Daniel [Los Alamos National Laboratory; Farinholt, Kevin M [Los Alamos National Laboratory; Park, Gyuhae [Los Alamos National Laboratory

    2009-01-01

    In this paper we present an investigation into several strain sensing technologies that are being considered to monitor mechanical deformation within the steel reinforcement shells used in high field pulsed magnets. Such systems generally operate at cryogenic temperatures to mitigate heating issues that are inherent in the coils of nondestructive, high field pulsed magnets. The objective of this preliminary study is to characterize the performance of various strain sensing technologies at liquid nitrogen temperatures (-196 C). Four sensor types are considered in this investigation: fiber Bragg gratings (FBG), resistive foil strain gauges (RFSG), piezoelectric polymers (PVDF), and piezoceramics (PZT). Three operational conditions are considered for each sensor: bond integrity, sensitivity as a function of temperature, and thermal cycling effects. Several experiments were conducted as part of this study, investigating adhesion with various substrate materials (stainless steel, aluminum, and carbon fiber), sensitivity to static (FBG and RFSG) and dynamic (RFSG, PVDF and PZT) load conditions, and sensor diagnostics using PZT sensors. This work has been conducted in collaboration with the National High Magnetic Field Laboratory (NHMFL), and the results of this study will be used to identify the set of sensing technologies that would be best suited for integration within high field pulsed magnets at the NHMFL facility.

  13. Physics of semiconductors in high magnetic fields

    CERN Document Server

    Miura, Noboru

    2008-01-01

    This book summarizes most of the fundamental physical phenomena which semiconductors and their modulated structures exhibit in high magnetic fields. Readers can learn not only the basic theoretical background but also the present state of the art from the most advanced data in this rapidly growing research area.

  14. High-performance phase-field modeling

    KAUST Repository

    Vignal, Philippe

    2015-04-27

    Many processes in engineering and sciences involve the evolution of interfaces. Among the mathematical frameworks developed to model these types of problems, the phase-field method has emerged as a possible solution. Phase-fields nonetheless lead to complex nonlinear, high-order partial differential equations, whose solution poses mathematical and computational challenges. Guaranteeing some of the physical properties of the equations has lead to the development of efficient algorithms and discretizations capable of recovering said properties by construction [2, 5]. This work builds-up on these ideas, and proposes novel discretization strategies that guarantee numerical energy dissipation for both conserved and non-conserved phase-field models. The temporal discretization is based on a novel method which relies on Taylor series and ensures strong energy stability. It is second-order accurate, and can also be rendered linear to speed-up the solution process [4]. The spatial discretization relies on Isogeometric Analysis, a finite element method that possesses the k-refinement technology and enables the generation of high-order, high-continuity basis functions. These basis functions are well suited to handle the high-order operators present in phase-field models. Two-dimensional and three dimensional results of the Allen-Cahn, Cahn-Hilliard, Swift-Hohenberg and phase-field crystal equation will be presented, which corroborate the theoretical findings, and illustrate the robustness of the method. Results related to more challenging examples, namely the Navier-Stokes Cahn-Hilliard and a diusion-reaction Cahn-Hilliard system, will also be presented. The implementation was done in PetIGA and PetIGA-MF, high-performance Isogeometric Analysis frameworks [1, 3], designed to handle non-linear, time-dependent problems.

  15. High trapped fields in bulk YBCO superconductors

    Science.gov (United States)

    Fuchs, Günter; Gruss, Stefan; Krabbes, Gernot; Schätzle, Peter; Verges, Peter; Müller, Karl-Hartmut; Fink, Jörg; Schultz, Ludwig

    The trapped field properties of bulk melt-textured YBCO material were investigated at different temperatures. In the temperature range of liquid nitrogen, maximum trapped fields of 1.1 T were found at 77 K by doping of YBCO with small amounts of zinc. The improved pinning of zinc-doped YBa2Cu3O7-x (YBCO) results in a pronounced peak effect in the field dependence of the critical current density. the trapped field at lower temperatures increases due to the increasing critical current density, however, at temperatures around 50 K cracking of the material is observed which is exposed to considerably tensile stresses due to Lorentz forces. Very high trapped fields up to 14.4 T were achieved at 22.5 K for a YBCO disk pair by the addition of silver improving the tensile strength of YBCO and by using a bandage made of a steel tube. The steel tube produces a compressive stress on YBCO after cooling down from 300 K to the measuring temperature, which is due to the higher coeeficient of thermal expansion of steel compared with that of YBCO in the a,b plane. The application of superconducting permanent magnets with trapped fields of 10 T and more in superconducting bearings would allow to obtain very high levitation pressures up to 2500 N/cm2 which is two orders of magnitude higher than the levitation pressure achievable in superconducting bearings with conventional permanent magnets. The most important problem for the application of superconducting permanent magnets is the magnetizing procedure of the YBCO material. Results of magnetizing YBCO disks by using of pulsed magnetic fields will be presented.

  16. High-field electron-photon interactions

    International Nuclear Information System (INIS)

    Hartemann, F V.

    1999-01-01

    Recent advances in novel technologies (including chirped-pulse amplification, femtosecond laser systems operating in the TW-PW range, high-gradient rf photoinjectors, and synchronized relativistic electron bunches with subpicosecond durations and THz bandwidths) allow experimentalists to study the interaction of relativistic electrons with ultrahigh-intensity photon fields. Ponderomotive scattering can accelerate these electrons with extremely high gradients in a three-dimensional vacuum laser focus. The nonlinear Doppler shift induced by relativistic radiation pressure in Compton backscattering is shown to yield complex nonlinear spectra which can be modified by using temporal laser pulse shaping techniques. Colliding laser pulses, where ponderomotive acceleration and Compton backscattering are combined, could also yield extremely short wavelength photons. Finally, one expects strong radiative corrections when the Doppler-upshifted laser wavelength approaches the Compton scale. These are discussed within the context of high-field classical electrodynamics, a new discipline borne out of the aforementioned innovations

  17. Sultan - forced flow, high field test facility

    International Nuclear Information System (INIS)

    Horvath, I.; Vecsey, G.; Weymuth, P.; Zellweger, J.

    1981-01-01

    Three European laboratories: CNEN (Frascati, I) ECN (Petten, NL) and SIN (Villigen, CH) decided to coordinate their development efforts and to install a common high field forced flow test facility at Villigen Switzerland. The test facility SULTAN (Supraleiter Testanlage) is presently under construction. As a first step, an 8T/1m bore solenoid with cryogenic periphery will be ready in 1981. The cryogenic system, data acquisition system and power supplies which are contributed by SIN are described. Experimental feasibilities, including cooling, and instrumentation are reviewed. Progress of components and facility construction is described. Planned extension of the background field up to 12T by insert coils is outlined. 5 refs

  18. High energy approximations in quantum field theory

    International Nuclear Information System (INIS)

    Orzalesi, C.A.

    1975-01-01

    New theoretical methods in hadron physics based on a high-energy perturbation theory are discussed. The approximated solutions to quantum field theory obtained by this method appear to be sufficiently simple and rich in structure to encourage hadron dynamics studies. Operator eikonal form for field - theoretic Green's functions is derived and discussion is held on how the eikonal perturbation theory is to be renormalized. This method is extended to massive quantum electrodynamics of scalar charged bosons. Possible developments and applications of this theory are given [pt

  19. Silicon Photomultiplier Performance in High ELectric Field

    Science.gov (United States)

    Montoya, J.; Morad, J.

    2016-12-01

    Roughly 27% of the universe is thought to be composed of dark matter. The Large Underground Xenon (LUX) relies on the emission of light from xenon atoms after a collision with a dark matter particle. After a particle interaction in the detector, two things can happen: the xenon will emit light and charge. The charge (electrons), in the liquid xenon needs to be pulled into the gas section so that it can interact with gas and emit light. This allows LUX to convert a single electron into many photons. This is done by applying a high voltage across the liquid and gas regions, effectively ripping electrons out of the liquid xenon and into the gas. The current device used to detect photons is the photomultiplier tube (PMT). These devices are large and costly. In recent years, a new technology that is capable of detecting single photons has emerged, the silicon photomultiplier (SiPM). These devices are cheaper and smaller than PMTs. Their performance in a high electric fields, such as those found in LUX, are unknown. It is possible that a large electric field could introduce noise on the SiPM signal, drowning the single photon detection capability. My hypothesis is that SiPMs will not observe a significant increase is noise at an electric field of roughly 10kV/cm (an electric field within the range used in detectors like LUX). I plan to test this hypothesis by first rotating the SiPMs with no applied electric field between two metal plates roughly 2 cm apart, providing a control data set. Then using the same angles test the dark counts with the constant electric field applied. Possibly the most important aspect of LUX, is the photon detector because it's what detects the signals. Dark matter is detected in the experiment by looking at the ratio of photons to electrons emitted for a given interaction in the detector. Interactions with a low electron to photon ratio are more like to be dark matter events than those with a high electron to photon ratio. The ability to

  20. Consideration on detection of irradiated rainbow trout by ESR method and 2-alkylcyclobutanone analysis

    International Nuclear Information System (INIS)

    Tanabe, Hiroko; Goto, Michiko

    2002-01-01

    Relative ESR strength of rib, backbone and opercular bone from irradiated culture rainbow trout was direct proportional to dose between 0.56kGy and 5.7kGy. Relative ESR strength of rib was higher than that of backbone. Although only 5mg of otolith was obtained from one rainbow trout, bone density of otolith is so high that relative ESR strength of otolith showed about 20-fold higher value than that of rib. In GCMS-SIM analysis of RCB, radiolytic compounds of lipid of fish meat, the amount of both DCB and TCB formed, estimated from ion concentrations of m/z98, were direct proportional to dose between 1.1kGy and 11.1kGy. Neither DCB nor TCB was detected in unirradiated sample. The ratio of amount of DCB formed to amount of TCB formed was nearly 4.4, which is the ratio of palmitic acid content to stearic acid content in rainbow trout, denoted in Standard Tables of Food Composition in Japan; Lipid composition of Foods. Finally, we propose to use detection of radiolytic compound, RCB, and measurement of ESR of high-density bone together for reliable identification of irradiated fish. (author)

  1. Consideration on detection of irradiated rainbow trout by ESR method and 2-alkylcyclobutanone analysis

    International Nuclear Information System (INIS)

    Tanabe, H.; Goto, M.

    2002-01-01

    R elative ESR strength of rib, backbone and opercular bone from irradiated culture rainbow trout was direct proportional to dose between 0.56kGy and 5.7kGy. Relative ESR strength of rib was higher than that of backbone. Although only 5mg of otolith was obtained from one rainbow trout, bone density of otolith is so high that relative ESR strength of otolith showed about 20-fold higher value than that of rib. In GCMS-SIM analysis of RGB, radiolytic compounds of lipid of fish meat, the amount of both DCB and TCB formed, estimated from ion concentrations of m/z98, were direct proportional to dose between 1.1kGy and 11.1kGy. Neither DCB nor TCB was detected in unirradiated sample. The ratio of amount of DCB formed to amount of TCB formed was nearly 4.4, which is the ratio of palmitic acid content to stearic acid content in rainbow trout, denoted in Standard Tables of Food Composition in Japan; Lipid composition of Foods. Finally, we propose to use detection of radiolytic compound, RCB, and measurement of ESR of high-density bone together for reliable identification of irradiated fish

  2. The Pioneer XI high field fluxgate magnetometer

    Science.gov (United States)

    Acuna, M. A.; Ness, N. F.

    1975-01-01

    The high field fluxgate magnetometer experiment flown aboard the Pioneer XI spacecraft is described. This extremely simple instrument was used to extend the spacecraft's upper-limit measurement capability by approximately an order of magnitude (from 0.14 mT to 1.00 mT) with minimum power and volume requirements. This magnetometer was designed to complement the low-field measurements provided by a helium vector magnetometer and utilizes magnetic ring core sensors with biaxial orthogonal sense coils. The instrument is a single-range, triaxial-fluxgate magnetometer capable of measuring fields of up to 1 mT along each orthogonal axis, with a maximum resolution of 1 microT.

  3. ESR studies of heat denaturation in Cu myoglobin complexes

    International Nuclear Information System (INIS)

    Louro, S.R.W.; Ribeiro, S.C.; Bemski, G.

    1975-01-01

    An investigation is made on the behaviour of Cu2 + and Fe3 + in copper doped myoglobin, subjected to heat treatment. ESR is observed at X-band. The amplitude of the g = 5.9 line of the high spin F 3 + in met-myoglobin is studied as a function of the temperature of the heat treatment, the pH and the length of time of exposure to the heat treatment. These experiments are performed for both the pure protein and for the copper-myoglobin complex, at pH between 5 and 8.5. Results concerning the decrease of the amplitude of Fe 3+ high spin signal are discussed in comparison with Hollocher's results in hemoglobin. The Cu spectra obtained are interpreted, with the aid of a computer program, Kivelson and Neiman's results being used to analyse the authors data

  4. ESR dosimetric properties of modern coral reef

    Energy Technology Data Exchange (ETDEWEB)

    Sharaf, M.A. E-mail: mokhtar_sharaf@yahoo.com; Hassan, Gamal M

    2004-06-01

    Modern coral reef samples from Egypt were irradiated with {sup 60}Co{gamma}-rays to study radicals for dosimetric materials with electron spin resonance (ESR). The ESR spectrum for the radical species in unirradiated coral is characterized by four signals with spectroscopic splitting factors of g=2.0056, 2.0030, 2.0006 and 1.997. The signal at g=2.0006{+-}0.0005 is ascribed to free rotation CO{sub 2}{sup -} radicals and used as a dosimetric one. The response to {gamma}-ray doses ranging from 5 to 10{sup 3} Gy and the thermal stability has been studied. The number of free radicals per 100 eV (G-value) was found to be 0.45 {+-} 0.1 and 0.9 {+-} 0.18 for coral and alanine, respectively. The lifetime of radicals and the activation energy were estimated from Arrhenius plots to be approximately 8 x 10{sup 5} {+-} 1.6 x 10{sup 5} years, and 1.12 eV, respectively.

  5. Application of ESR to identification of irradiated foodstuffs

    Energy Technology Data Exchange (ETDEWEB)

    Raffi, J. [Aix-Marseille-3 Univ., 13 - Marseille (France); Agnel, J.P. [CEA Centre d`Etudes de Cadarache, 13 - Saint-Paul-lez-Durance (France). Dept. de Physiologie Vegetale et Ecosystemes; Belliardo, J.J. [BCR, Bruxelles (Belgium)

    1994-11-01

    The conditions required to use Electron Spin Resonance (ESR) in identification of irradiated foods is first described. Then we present the results of an intercomparison sponsored by the Community Bureau of Reference involving 22 european laboratories on meat and fish bones and fruits. Then the ESR protocols given to the BCR are described. (authors). 14 refs., 8 figs., 5 annexes.

  6. Experimental microdosimetry in high energy radiation fields

    International Nuclear Information System (INIS)

    Spurny, F.; Bednar, J.; Vlcek, B.; Bottollier-Depois, J.-F.; Molokanov, A.G.

    2000-01-01

    To determine microdosimetric characteristics in the beams and fields of high energy panicles with the goal, also, to compare the classical method of experimental microdosimetry, a tissue equivalent low pressure proportional counter (TEPC) with the linear energy transfer (LET) spectrometer based on a chemically etched polyallyldiglycolcarbonate as a track etched detector (TED). To test the use of TED LET spectrometer in the conditions, where the use or TEPC is not possible (high energy charged particle beams at high dose rates). The results obtained with the TEPC NAUSICAA were used in this work to compare them with other data. This TEPC measures directly the linear energy in the interval between 0.15 and 1500 keV/μm in tissue, the low gas pressure (propan based TE mixture) permits to simulate a tissue element of about 3 μm. It can be used in the fields with instantaneous dose equivalent rates between 1 μSv/hour and 1 mSv/ hour. TED LET spectrometer developed to determine LET spectra between 10 and 700 keV/μm in tissue. Primarily, track-to-bulk etch rate ratios are determined through the track parameters measurements, the spectra of these ratios are convened to LET spectra using the calibration curve established by means of heavy charge panicles. The critical volume of thi spectrometer is supposed to be a few nm. There is no limit of use for the dose rate, the background tracks limit the lowest threshold to about 1 mSv, the overlapping of tracks (the highest one) to 100 mSv. Both experimental microdosimetry methods have been used in on board aircraft radiation fields, in on-Earth high energy radiation reference fields, and in the beams of protons with energies up to 300 MeV (Dubna, Moscow, Loma Linda). First, it should be emphasized, that in all high energy radiation fields studied, we concentrated our analysis on the region, where both methods overlap, i.e. between 10 and 1000 keV/μm in tissue. It should be also stressed, that the events observed in this region

  7. High-field, high-density tokamak power reactor

    International Nuclear Information System (INIS)

    Cohn, D.R.; Cook, D.L.; Hay, R.D.; Kaplan, D.; Kreischer, K.; Lidskii, L.M.; Stephany, W.; Williams, J.E.C.; Jassby, D.L.; Okabayashi, M.

    1977-11-01

    A conceptual design of a compact (R 0 = 6.0 m) high power density (average P/sub f/ = 7.7 MW/m 3 ) tokamak demonstration power reactor has been developed. High magnetic field (B/sub t/ = 7.4 T) and moderate elongation (b/a = 1.6) permit operation at the high density (n(0) approximately 5 x 10 14 cm -3 ) needed for ignition in a relatively small plasma, with a spatially-averaged toroidal beta of only 4%. A unique design for the Nb 3 Sn toroidal-field magnet system reduces the stress in the high-field trunk region, and allows modularization for simpler disassembly. The modest value of toroidal beta permits a simple, modularized plasma-shaping coil system, located inside the TF coil trunk. Heating of the dense central plasma is attained by the use of ripple-assisted injection of 120-keV D 0 beams. The ripple-coil system also affords dynamic control of the plasma temperature during the burn period. A FLIBE-lithium blanket is designed especially for high-power-density operation in a high-field environment, and gives an overall tritium breeding ratio of 1.05 in the slowly pumped lithium

  8. High-performance phase-field modeling

    KAUST Repository

    Vignal, Philippe; Sarmiento, Adel; Cortes, Adriano Mauricio; Dalcin, L.; Collier, N.; Calo, Victor M.

    2015-01-01

    and phase-field crystal equation will be presented, which corroborate the theoretical findings, and illustrate the robustness of the method. Results related to more challenging examples, namely the Navier-Stokes Cahn-Hilliard and a diusion-reaction Cahn-Hilliard system, will also be presented. The implementation was done in PetIGA and PetIGA-MF, high-performance Isogeometric Analysis frameworks [1, 3], designed to handle non-linear, time-dependent problems.

  9. High field dipole magnet design concepts

    International Nuclear Information System (INIS)

    Nicol, T.H.

    1988-12-01

    High field dipole magnets will play a crucial role in the development of future accelerators whether at Fermilab or elsewhere. This paper presents conceptual designs for two such dipoles; 6.6 and 8.8 Tesla, with special focus on their suitability for upgrades to the Fermilab Tevatron. Descriptions and cross-sectional views will be presented as will preliminary estimates of heat loads and costs. 3 refs., 2 figs., 2 tabs

  10. Establishment of estrogen receptor 1 (ESR1)-knockout medaka: ESR1 is dispensable for sexual development and reproduction in medaka, Oryzias latipes.

    Science.gov (United States)

    Tohyama, Saki; Ogino, Yukiko; Lange, Anke; Myosho, Taijun; Kobayashi, Tohru; Hirano, Yu; Yamada, Gen; Sato, Tomomi; Tatarazako, Norihisa; Tyler, Charles R; Iguchi, Taisen; Miyagawa, Shinichi

    2017-08-01

    Estrogens play fundamental roles in regulating reproductive activities and they act through estrogen receptor (ESR) in all vertebrates. Most vertebrates have two ESR subtypes (ESR1 and ESR2), whereas teleost fish have at least three (Esr1, Esr2a and Esr2b). Intricate functionalization has been suggested among the Esr subtypes, but to date, distinct roles of Esr have been characterized in only a limited number of species. Study of loss-of-function in animal models is a powerful tool for application to understanding vertebrate reproductive biology. In the current study, we established esr1 knockout (KO) medaka using a TALEN approach and examined the effects of Esr1 ablation. Unexpectedly, esr1 KO medaka did not show any significant defects in their gonadal development or in their sexual characteristics. Neither male or female esr1 KO medaka exhibited any significant changes in sexual differentiation or reproductive activity compared with wild type controls. Interestingly, however, estrogen-induced vitellogenin gene expression, an estrogen-responsive biomarker in fish, was limited in the liver of esr1 KO males. Our findings, in contrast to mammals, indicate that Esr1 is dispensable for normal development and reproduction in medaka. We thus provide an evidence for estrogen receptor functionalization between mammals and fish. Our findings will also benefit interpretation of studies into the toxicological effects of estrogenic chemicals in fish. © 2017 Japanese Society of Developmental Biologists.

  11. High field superconductor development and understanding

    Energy Technology Data Exchange (ETDEWEB)

    Larbalestier, David C. [Florida State Univ., Tallahassee, FL (United States); Lee, Peter J. [Florida State Univ., Tallahassee, FL (United States); Tarantini, Chiara [Florida State Univ., Tallahassee, FL (United States)

    2014-09-28

    All present circular accelerators use superconducting magnets to bend and to focus the particle beams. The most powerful of these machines is the large hadron collider (LHC) at CERN. The main ring dipole magnets of the LHC are made from Nb-Ti but, as the machine is upgraded to higher luminosity, more powerful magnets made of Nb3Sn will be required. Our work addresses how to make the Nb3Sn conductors more effective and more suitable for use in the LHC. The most important property of the superconducting conductor used for an accelerator magnet is that it must have very high critical current density, the property that allows the generation of high magnetic fields in small spaces. Nb3Sn is the original high field superconductor, the material which was discovered in 1960 to allow a high current density in the field of about 9 T. For the high luminosity upgrade of the LHC, much higher current densities in fields of about 12 Tesla will be required. The critical value of the current density is of order 2600 A/mm2 in a field of 12 Tesla. But there are very important secondary factors that complicate the attainment of this critical current density. The first is that the effective filament diameter must be no larger than about 40 µm. The second factor is that 50% of the cross-section of the Nb3Sn conductor that is pure copper must be protected from any poisoning by any Sn leakage through the diffusion barrier that protects the package of niobium and tin from which the Nb3Sn is formed by a high temperature reaction. These three, somewhat conflicting requirements, mean that optimization of the conductor is complex. The work described in this contract report addresses these conflicting requirements. They show that very sophisticated characterizations can uncover the way to satisfy all 3 requirements and they also suggest that the ultimate optimization of Nb3Sn is still not yet in sight

  12. Super high field ohmically heated tokamak operation

    International Nuclear Information System (INIS)

    Cohn, D.R.; Bromberg, L.; Leclaire, R.J.; Potok, R.E.; Jassby, D.L.

    1986-01-01

    The authors discuss a super high field mode of tokamak operation that uses ohmic heating or near ohmic heating to ignition. The super high field mode of operation uses very high values of Β/sup 2/α, where Β is the magnetic field and a is the minor radius (Β/sup 2/α > 100 T/sup 2/m). We analyze copper magnet devices with major radii from 1.7 to 3.0 meters. Minimizing or eliminating the need for auxiliary heating has the potential advantages of reducing uncertainty in extrapolating the energy confinement time of current tokamak devices, and reducing engineering problems associated with large auxiliary heating requirements. It may be possible to heat relatively short pulse, inertially cooled tokamaks to ignition with ohmic power alone. However, there may be advantages in using a very small amount of auxiliary power (less than the ohmic heating power) to boost the ohmic heating and provide a faster start-up, expecially in relatively compact devices

  13. Alanine-ESR dosimeter: application for dosimetry in industrial electron beam accelerator

    International Nuclear Information System (INIS)

    Murali, S.; Venkataramani, R.; Pushparaja; Sarma, K.S.S.; Natarajan, V.; Sastry, M.D.

    2000-01-01

    The feasibility of DL-α-alanine, as ESR dosimeter in powder form, was examined under the conditions of pulse electron accelerator used as an industrial irradiator. The investigations were carried out to examine the following aspects: (i) Alanine-ESR dose response in irradiator characteristics viz. various beam energies, beam currents, product conveying speeds, (ii) linearity of dose response of irradiated alanine signal for suitable range, (iii) dose uniformity of the irradiated samples and (iv) depth dose measurements using alanine powder dosimeters sandwiched between polyethylene layers. Experiments were carried out by varying some of the irradiator parameters at mobile mode of the conveyor (product under movement) and also at stationary mode for different EB energies and pulse rates. For estimation of EB dose, signal intensities of gamma irradiated DL--alanine powder calibrated with Fricke dosimetry have been used. Feasibility of application of alanine ESR dosimeter for low dose measurement down to 350 Gy has been experimentally established. The present studies show that under variable operating conditions of irradiator, alanine ESR dosimetry is suitable for dosimetric applications from low dose (350 Gy) to high dose (53 kgy). (author)

  14. High field conditioning of cryogenic RF cavities

    International Nuclear Information System (INIS)

    Cole, M.; Debiak, T.; Lom, C.; Shephard, W.; Sredniawski, J.

    1993-01-01

    Space-based and other related accelerators have conditioning and operation requirements that are not found in most machines. The use of cryogenic copper, relatively poor vacuum, and limited power storage and operating time put unusual demands on the high-field conditioning process and present some concerns. Two CW cryogenic engineering model open-quotes sparkerclose quotes cavities have been fabricated and tested to fairly high field levels. Tests included initial and repeated conditioning as well as sustained RF operations. The two cavities were an engineering model TDL and an engineering model RFQ. Both cavities operated at 425 MHz. The DTL was conditioned to 46 MV/m at 100% duty factor (CW) at cryogenic temperature. This corresponds to a gap voltage of 433 kV and a real estate accelerating gradient (energy gain/total cavity length) of 6.97 MV/m. The authors believe this to be record performance for cryo CW operation. During cryo pulsed operation, the same cavity reached 48 MV/m with 200 μsec pulses at 0.5% DF. The RFQ was conditioned to 30 MV/m CW at cryo, 85 kV gap voltage. During a brief period of cryo pulsed operation, the RFQ operated at 46 MV/m, or 125 kV gap voltage. Reconditioning experiments were performed on both cavities and no problems were encountered. It should be noted that the vacuum levels were not very stringent during these tests and no special cleanliness or handling procedures were followed. The results of these tests indicate that cavities can run CW without difficulty at cryogenic temperatures at normal conservative field levels. Higher field operation may well be possible, and if better vacuums are used and more attention is paid to cleanliness, much higher fields may be attainable

  15. Uses of polymer-alanine film/ESR dosimeters in dosimetry of ionizing radiation

    International Nuclear Information System (INIS)

    Xie Liqing; Zhang Yinfeng; Dai Jinxian; Lu Ting; Chen Ruyi; Yang Hua

    1993-01-01

    Alanine ESR dosimetry is a reliable method, used in a various fields of ionizing radiation. The polymer-alanine film/ESR dosimeters of 0.3 -0.4 mm thickness were prepared and their dosimetric properties were studied for 60 Co γ photons and 3 - 5 MeV electrons in the dose range from 20 Gy to 100 kGy. The results show that under normal conditions the alanine calibration curves are linear in the dose range from 100 Gy to 10kGy. The dose profiles at the electron radiation field were measured with the film alanine dosimeters. The polymer-alanine film dosimeters were used for ion implantation of 400 keV ion implantor. Their dose response and energy dependence were investigated initially. (Author)

  16. Empirical high-latitude electric field models

    International Nuclear Information System (INIS)

    Heppner, J.P.; Maynard, N.C.

    1987-01-01

    Electric field measurements from the Dynamics Explorer 2 satellite have been analyzed to extend the empirical models previously developed from dawn-dusk OGO 6 measurements (J.P. Heppner, 1977). The analysis embraces large quantities of data from polar crossings entering and exiting the high latitudes in all magnetic local time zones. Paralleling the previous analysis, the modeling is based on the distinctly different polar cap and dayside convective patterns that occur as a function of the sign of the Y component of the interplanetary magnetic field. The objective, which is to represent the typical distributions of convective electric fields with a minimum number of characteristic patterns, is met by deriving one pattern (model BC) for the northern hemisphere with a +Y interplanetary magnetic field (IMF) and southern hemisphere with a -Y IMF and two patterns (models A and DE) for the northern hemisphere with a -Y IMF and southern hemisphere with a +Y IMF. The most significant large-scale revisions of the OGO 6 models are (1) on the dayside where the latitudinal overlap of morning and evening convection cells reverses with the sign of the IMF Y component, (2) on the nightside where a westward flow region poleward from the Harang discontinuity appears under model BC conditions, and (3) magnetic local time shifts in the positions of the convection cell foci. The modeling above was followed by a detailed examination of cases where the IMF Z component was clearly positive (northward). Neglecting the seasonally dependent cases where irregularities obscure pattern recognition, the observations range from reasonable agreement with the new BC and DE models, to cases where different characteristics appeared primarily at dayside high latitudes

  17. Pulsed-High Field/High-Frequency EPR Spectroscopy

    Science.gov (United States)

    Fuhs, Michael; Moebius, Klaus

    Pulsed high-field/high-frequency electron paramagnetic resonance (EPR) spectroscopy is used to disentangle many kinds of different effects often obscured in continuous wave (cw) EPR spectra at lower magnetic fields/microwave frequencies. While the high magnetic field increases the resolution of G tensors and of nuclear Larmor frequencies, the high frequencies allow for higher time resolution for molecular dynamics as well as for transient paramagnetic intermediates studied with time-resolved EPR. Pulsed EPR methods are used for example for relaxation-time studies, and pulsed Electron Nuclear DOuble Resonance (ENDOR) is used to resolve unresolved hyperfine structure hidden in inhomogeneous linewidths. In the present article we introduce the basic concepts and selected applications to structure and mobility studies on electron transfer systems, reaction centers of photosynthesis as well as biomimetic models. The article concludes with an introduction to stochastic EPR which makes use of an other concept for investigating resonance systems in order to increase the excitation bandwidth of pulsed EPR. The limited excitation bandwidth of pulses at high frequency is one of the main limitations which, so far, made Fourier transform methods hardly feasible.

  18. High-magnetic-field research collaborations

    International Nuclear Information System (INIS)

    Goettee, J.

    1998-01-01

    This is the final report of a two-year, Laboratory Directed Research and Development (LDRD) project at the Los Alamos National Laboratory (LANL). The purpose of this project was to develop collaborations with the academic community to exploit scientific research potential of the pulsed magnetic fields that might be possible with electrically pulsed devices, as well as magneto-cumulative generators. The author started with a campaign of experiments using high-explosive-driven flux compression generators. The campaign's objective was to explore completely novel ideas in condensed-matter physics and chemistry. The initiative was very successful in pulling together top researchers from around the world

  19. Pubertal Escape From Estradiol Negative Feedback in Ewe Lambs Is Not Accounted for by Decreased ESR1 mRNA or Protein in Kisspeptin Neurons.

    Science.gov (United States)

    Bedenbaugh, Michelle N; D'Oliveira, Marcella; Cardoso, Rodolfo C; Hileman, Stanley M; Williams, Gary L; Amstalden, Marcel

    2018-01-01

    In this study, we investigated whether decreased sensitivity to estradiol negative feedback is associated with reduced estrogen receptor α (ESR1) expression in kisspeptin neurons as ewe lambs approach puberty. Lambs were ovariectomized and received no implant (OVX) or an implant containing estradiol (OVX+E). In the middle arcuate nucleus (mARC), ESR1 messenger RNA (mRNA) was greater in OVX than OVX+E lambs but did not differ elsewhere. Post hoc analysis of luteinizing hormone (LH) secretion from OVX+E lambs revealed three patterns of LH pulsatility: low [1 to 2 pulses per 12 hours; low frequency (LF), n = 3], moderate [6 to 7 pulses per 12 hours; moderate frequency (MF), n = 6], and high [>10 pulses per 12 hours; high frequency (HF), n = 5]. The percentage of kisspeptin neurons containing ESR1 mRNA in the preoptic area did not differ among HF, MF, or LF groups. However, the percentage of kisspeptin neurons containing ESR1 mRNA in the mARC was greater in HF (57%) than in MF (36%) or LF (27%) lambs and did not differ from OVX (50%) lambs. A higher percentage of kisspeptin neurons contained ESR1 protein in all regions of the arcuate nucleus (ARC) in OVX compared with OVX+E lambs. There were no differences in ESR1 protein among the HF, MF, or LF groups in the preoptic area or ARC. Contrary to our hypothesis, increases in LH pulsatility were associated with enhanced ESR1 mRNA abundance in kisspeptin neurons in the ARC, and absence of estradiol increased the percentage of kisspeptin neurons containing ESR1 protein in the ARC. Therefore, changes in the expression of ESR1, particularly in kisspeptin neurons in the ARC, do not explain the pubertal escape from estradiol negative feedback in ewe lambs. Copyright © 2018 Endocrine Society.

  20. Structural alloys for high field superconducting magnets

    International Nuclear Information System (INIS)

    Morris, J.W. Jr.

    1985-08-01

    Research toward structural alloys for use in high field superconducting magnets is international in scope, and has three principal objectives: the selection or development of suitable structural alloys for the magnet support structure, the identification of mechanical phenomena and failure modes that may influence service behavior, and the design of suitable testing procedures to provide engineering design data. This paper reviews recent progress toward the first two of these objectives. The structural alloy needs depend on the magnet design and superconductor type and differ between magnets that use monolithic and those that employ force-cooled or ICCS conductors. In the former case the central requirement is for high strength, high toughness, weldable alloys that are used in thick sections for the magnet case. In the latter case the need is for high strength, high toughness alloys that are used in thin welded sections for the conductor conduit. There is productive current research on both alloy types. The service behavior of these alloys is influenced by mechanical phenomena that are peculiar to the magnet environment, including cryogenic fatigue, magnetic effects, and cryogenic creep. The design of appropriate mechanical tests is complicated by the need for testing at 4 0 K and by rate effects associated with adiabatic heating during the tests. 46 refs

  1. Assessment of the lower ESR dating range in Greek speleothems

    International Nuclear Information System (INIS)

    Bassiakos, Y.

    2001-01-01

    Pilot ESR dating studies on geologically young calcitic sinters were carried out, aiming at assessment of the lower ESR dating range in characteristic Greek speleoenvironments. Five stalactites were dated, coming from an ancient mining gallery, idle for the last 2,500 years, found on Siphnos island (Aegean). The calculated ages range between 1,7-2,0 ka. Medium to low measured external dose rates (aprox. 900 μGy/a) and very low measured radioelement concentration in samples are very usual in the Mediterranean environments. The study concludes that ESR dating of speleothems younger than two millenia is practically unattainable. Some geoarchaeological implications of the obtained ages are discussed. (author)

  2. Radicals in DNA as seen by ESR spectroscopy

    International Nuclear Information System (INIS)

    Symons, M.C.R.

    1997-01-01

    This is a review of ESR studies, mainly of DNA systems, after exposure to ionising radiation at low temperatures. Under this conditions 'direct' damage is of major significance, and ESR evidence for the concept of the initial formation of electron-gain and electron-loss centers localised within DNA bases, and deeply trapped by proton-gain and loss, will be discussed. It is stressed that 'negative' evidence, showing that various phosphate and sugar centred radicals are not detected, is of major importance since the ESR 'fingerprints' of base-radicals are relatively ill defined. (author)

  3. ESR measurements and the detection of radiosterilization of drugs

    International Nuclear Information System (INIS)

    Gibella, M.; Crucq, A.S.; Tilquin, B.

    1993-01-01

    The ESR spectrum of trapped radicals in irradiated solid antibiotics could permit the detection of the radiosterilization. The ESR signal is detected only after radiolysis; at room temperature, this ESR spectrum is observable for a few hours or until several years. The rate of the metathesis reactions can be fast or very slow, the reaction path is unknown,. However, in many cases, the polycrystalline solid phase exhibits its ability to keep radicals for a long period of time and the detection of the radiolysis is possible during this period. 10 figs., 1 tab

  4. High-field Magnet Development toward the High Luminosity LHC

    Energy Technology Data Exchange (ETDEWEB)

    Apollinari, Giorgio [Fermilab

    2014-07-01

    The upcoming Luminosity upgrade of the LHC (HL-LHC) will rely on the use of Accelerator Quality Nb3Sn Magnets which have been the focus of an intense R&D effort in the last decade. This contribution will describe the R&D and results of Nb3Sn Accelerator Quality High Field Magnets development efforts, with emphasis on the activities considered for the HL-LHC upgrades.

  5. Ribavirin restores ESR1 gene expression and tamoxifen sensitivity in ESR1 negative breast cancer cell lines

    Directory of Open Access Journals (Sweden)

    Sappok Anne

    2011-12-01

    Full Text Available Abstract Tumor growth is estrogen independent in approximately one-third of all breast cancers, which makes these patients unresponsive to hormonal treatment. This unresponsiveness to hormonal treatment may be explained through the absence of the estrogen receptor alpha (ESR1. The ESR1 gene re-expression through epigenetic modulators such as DNA methyltransferase inhibitors and/or histone deacetylase inhibitors restores tamoxifen sensitivity in ESR1 negative breast cancer cell lines and opens new treatment horizons in patients who were previously associated with a poor prognosis. In the study presented herein, we tested the ability of ribavirin, which shares some structural similarities with the DNA-methyltransferase inhibitor 5-azacytidine and which is widely known as an anti-viral agent in the treatment of hepatitis C, to restore ESR1 gene re-expression in ESR1 negative breast cancer cell lines. In our study we identified ribavirin to restore ESR1 gene re-expression alone and even more in combination with suberoylanilide hydroxamic acid (SAHA - up to 276 fold induction. Ribavirin and analogs could pave the way to novel translational research projects that aim to restore ESR1 gene re-expression and thus the susceptibility to tamoxifen-based endocrine treatment strategies.

  6. High Performance Clocks and Gravity Field Determination

    Science.gov (United States)

    Müller, J.; Dirkx, D.; Kopeikin, S. M.; Lion, G.; Panet, I.; Petit, G.; Visser, P. N. A. M.

    2018-02-01

    Time measured by an ideal clock crucially depends on the gravitational potential and velocity of the clock according to general relativity. Technological advances in manufacturing high-precision atomic clocks have rapidly improved their accuracy and stability over the last decade that approached the level of 10^{-18}. This notable achievement along with the direct sensitivity of clocks to the strength of the gravitational field make them practically important for various geodetic applications that are addressed in the present paper. Based on a fully relativistic description of the background gravitational physics, we discuss the impact of those highly-precise clocks on the realization of reference frames and time scales used in geodesy. We discuss the current definitions of basic geodetic concepts and come to the conclusion that the advances in clocks and other metrological technologies will soon require the re-definition of time scales or, at least, clarification to ensure their continuity and consistent use in practice. The relative frequency shift between two clocks is directly related to the difference in the values of the gravity potential at the points of clock's localization. According to general relativity the relative accuracy of clocks in 10^{-18} is equivalent to measuring the gravitational red shift effect between two clocks with the height difference amounting to 1 cm. This makes the clocks an indispensable tool in high-precision geodesy in addition to laser ranging and space geodetic techniques. We show how clock measurements can provide geopotential numbers for the realization of gravity-field-related height systems and can resolve discrepancies in classically-determined height systems as well as between national height systems. Another application of clocks is the direct use of observed potential differences for the improved recovery of regional gravity field solutions. Finally, clock measurements for space-borne gravimetry are analyzed along with

  7. Tritium system for compact high field devices

    International Nuclear Information System (INIS)

    Roccella, M.; Bonizzoni, G.; Chiesa, P.; Ghezzi, F.; Nassi, M.; Pavesi, U.; Amedeo, P.; Boschetti, G.; Giffanti, F.; Moriggio, A.

    1988-01-01

    Some theoretical results and the current status of the work on a prototype plant for the Tritium cycle of compact high-field tokamaks (such as, Ignitor, CIT, etc.), using the SAES Getter St 707 getter material, are described in this report. The schematics and present status of the main subplants of the cycle are reported together with some experimental results demostrating the possibility of utilizing the St 707 material to purify the inert atmosphere of the glove-boxes and the secondary containment of the double-containment metal canalization which is to eventually house the various parts of the plant. Finally, as an example, the FTU machine, under construction at ENEA Frascati, has been taken as a reference, and theoretical evaluations are given for the inventory, permeation and release of the Tritium from the first wall and the thermal shieldes of such a tokamak

  8. High range electromagnetic fields. Experimental investigations

    International Nuclear Information System (INIS)

    Comino, E.; Boccardo, D.; Quaglino, A.

    2001-01-01

    It has been often discussed on the health effects from the electromagnetic fields, and nowadays this theme is particularly controlled and studied by the research-workers. It needs to know what is the risk connected to the exposure to the electromagnetism during a short or a long quantity of time and what are the health pathologies caused by the continue exposure. On one hand the results from epidemiological research can not still define the effect of the dose, on the other hand the legislative frame is variously fragmented and based on cautious concepts. But in this work, under the collaboration of Energy Resources Laboratory in Lausanne and the Geo resources and Territory Department in Turin University, are presented the early results on the experiments got out on high frequency (950 MHZ) in order to give a contribution to the debate between the scientific community and the public opinion [it

  9. Erythrocyte Sedimentation Rate (ESR): MedlinePlus Lab Test Information

    Science.gov (United States)

    ... K. Brunner & Suddarth's Handbook of Laboratory and Diagnostic Tests. 2 nd Ed, Kindle. Philadelphia: Wolters Kluwer Health, Lippincott Williams & Wilkins; c2014. Erythrocyte Sedimentation Rate (ESR); p. 267– ...

  10. Study on identification of irradiated food containing cellulose by ESR

    International Nuclear Information System (INIS)

    Wan Xiaojuan; Dou Daying; Xu Gang; Jiao Zheng; Wang Jia; Zheng Jianfei; Jiao Zheng; Wu Minghong; Ding Guoji

    2008-01-01

    The fast development and application of food irradiation technology signify the necessity and urgency to research on effective detection method for irradiated food. In this paper, we report a preliminary study in this area with dried chili powder, peanuts and strawberry seeds. The food samples were irradiated to 0.5, 1.0, 3.0, 5.0 and 10.0 kGy by 60 Co gamma rays. The relation between ESR intensity and irradiation dose, and correlation R 2 , were studied. The results showed that the ESR signal intensity is positively related with the dose. ESR intensity of the strawberry increased the slowest with the dose, and the chili powder had the most accurate calculation. Accurate dose-effect curves, however, require repeating tests and further studies are needed to verify the ESR results. (authors)

  11. Modeling membrane protein structure through site-directed ESR spectroscopy

    NARCIS (Netherlands)

    Kavalenka, A.A.

    2009-01-01

    Site-directed spin labeling (SDSL) electron spin resonance (ESR) spectroscopy is a
    relatively new biophysical tool for obtaining structural information about proteins. This
    thesis presents a novel approach, based on powerful spectral analysis techniques (multicomponent
    spectral

  12. ESR and TL age determination of caliche nodules

    Energy Technology Data Exchange (ETDEWEB)

    Oezer, A.M. (Middle East Technical Univ., Ankara (Turkey)); Wieser, A.; Goeksu, H.Y.; Mueller, P.; Regulla, D.F. (Gesellschaft fuer Strahlen- und Umweltforschung mbH Muenchen, Neuherberg (Germany, F.R.). Inst. fuer Strahlenschutz); Erol, O. (Istanbul Univ. (Turkey). School of Geography and Marine Sciences)

    1989-01-01

    Feasibility of dating caliche nodules by ESR and TL is investigated. For both methods the properties of the dating signal are described. Chemical composition as well as TL glow curves of caliches originating from different localities exhibit some differences. Due to the complexity of the TL glow curves, some samples required a special post-annealing procedure in order to resolve the main TL peak for age determination. Typical ESR calcite signals do not exist in caliche, therefore usefulness of the g=2.0040 ESR signal is studied. The results of TL and ESR ages are found to be compatible except for two samples. Possible causes of the discrepancy in these samples are discussed. It is shown that, with proper treatment of the radiation-induced signals, it was possible to date caliche formations older than 350 ka, which is not achievable with other methods like uranium series disequilibrium and/or radiocarbon dating. (author).

  13. ESR and TL age determination of caliche nodules

    International Nuclear Information System (INIS)

    Oezer, A.M.; Wieser, A.; Goeksu, H.Y.; Mueller, P.; Regulla, D.F.; Erol, O.

    1989-01-01

    Feasibility of dating caliche nodules by ESR and TL is investigated. For both methods the properties of the dating signal are described. Chemical composition as well as TL glow curves of caliches originating from different localities exhibit some differences. Due to the complexity of the TL glow curves, some samples required a special post-annealing procedure in order to resolve the main TL peak for age determination. Typical ESR calcite signals do not exist in caliche, therefore usefulness of the g=2.0040 ESR signal is studied. The results of TL and ESR ages are found to be compatible except for two samples. Possible causes of the discrepancy in these samples are discussed. It is shown that, with proper treatment of the radiation-induced signals, it was possible to date caliche formations older than 350 ka, which is not achievable with other methods like uranium series disequilibrium and/or radiocarbon dating. (author)

  14. Irradiation detection of coffee mate by electron spin resonance (ESR)

    Energy Technology Data Exchange (ETDEWEB)

    Ozsayin, Fulya [Physics Engineering Department, Hacettepe University, 06800 Ankara (Turkey); Polat, Mustafa, E-mail: polat@hacettepe.edu.t [Physics Engineering Department, Hacettepe University, 06800 Ankara (Turkey)

    2011-06-15

    Un-irradiated coffee mate samples do not exhibit any ESR signal. However, the samples exposed to UV and gamma radiation exhibit an ESR singlet and a large unresolved ESR signal, respectively. The dose-response curves of the samples exposed to UV and gamma radiations were found to be described well by an exponential and linear functions, respectively. Variable temperature and fading studies at room temperature showed that the radiation-induced radicals in coffee mate sample are very sensitive to temperature. The discrimination between un-irradiated and irradiated coffee mate samples can be done just comparing their ESR spectra. However, determination of the radiation dose received by the sample cannot be possible because of the fast decay of signal intensity at room temperature.

  15. Analysis of radicals induced in irradiated cereal flour using ESR

    International Nuclear Information System (INIS)

    Kawamura, Shoei; Kishita, Keigo; Ukai, Mitsuko; Kikuchi, Masahiro; Kobayashi, Yasuhiko

    2013-01-01

    Using electron spin resonance (ESR) spectroscopy, we revealed radicals induced in cereal flour irradiated with gamma-ray or electron beam. Sample was wheat and rice. We detected a broad singlet signal at g = 2.0. It consists of a singlet signal and a triplet signal. It suggested that the singlet signal is originated from organic free radicals and the triplet signal is from 14 N. There were no differences of ESR spectra between irradiated wheat flour and rice flour. The signal intensity of radiation induced radical was tend to increase following with the increase of radiation dose level. After radiation treatment, relaxation time of radiation induced radical was changed during storage. T 1 was decreased and T 2 was increased. In this study, the relaxation time is calculated using the parameters obtained from the ESR signal. It is necessary to analyze the relaxation time directly with pulsed ESR spectroscopy in future. (author)

  16. The nitrogen acceptor in 2H-Polytype synthetic MoS2. Frequency and temperature dependent ESR analysis

    International Nuclear Information System (INIS)

    Schoenaers, Ben; Stesmans, Andre; Afanas'ev, Valery V.

    2017-01-01

    In extending on recent electron spin resonance (ESR) work which has revealed the N acceptor (N substituting for S site) in 2H-polytype bulk synthetic MoS 2 , the dopant is extensively analyzed in terms of its frequency, temperature (T), and magnetic field B angular dependent ESR spectral characteristics. For B parallel c-axis, the multi-frequency analysis confirms the ESR spectrum as being composed of a 14 N hyperfine (hf) triplet with hf splitting constant A parallel = 14.7 ± 0.2 G (B parallel c-axis) and making up ∼74% of the total spectrum intensity, superimposed on a central line centered at about equal g-value [g parallel = 2.032(2)]. The presence of the latter signal, points to some non-uniformity in dopant distribution, that is, clustering, with about ∼26% of the total N response not originating from N incorporated in the preferred ''isolated'' dopant configuration. Angular dependent measurements reveal distinct anisotropy of the hf matrix, whereas ESR probing over a wide T-range exposes drastic signal broadening with increasing T above ∼150 K. Detailed study of the N acceptor signal intensity versus T at Q-band reveals an activation energy E a = 50 ± 10 meV, herewith consolidating the value reported initially. Besides unveiling the S-site substitutional N impurity as an appropriate p-type dopant for MoS 2 , the total of the ESR work establishes a basic frame of the N acceptor ESR characteristics, giving way for further in-depth theoretical perusal. (copyright 2017 WILEY-VCH Verlag GmbH and Co. KGaA, Weinheim)

  17. Changes in molecular structure and properties of irradiated polymers of different compositions - ESR and NMR study

    International Nuclear Information System (INIS)

    Carswell-Pomerantz, T.; Babanalbandi, A.; Dong, L.; Hill, D.J.T.; Perera, M.C.S.; Pomery, P.J.; Saadat, G.; Whittaker, A.K.

    1999-01-01

    Investigations of molecular structural changes in polymers during exposure to high energy radiation is the long term interest of the Polymer Materials and Radiation Group at the University of Queensland. Recently, the group had looked at a range of polymers including natural and synthetic rubbers, methacrylates and polyesters. The objective of the work has been to investigate the relationships between polymer structure and sensitivity towards high energy radiation, including gamma radiation. This report will focus on the Electron Spin Resonance (ESR) and Nuclear Magnetic Resonance (NMR) studies of the effects of gamma irradiation on these polymers. Other methods such as Gas Chromatography (GC), Gel Permeation Chromatography (GPC), Fourier Transformed Infra Red (FTIR), Differential Scanning Calorimetry (DSC), Thermogravimetric Analysis (TGA) and Dynamic Mechanical Analysis (DMA) have also been used as these methods combine with ESR and NMR, to provide a more complete picture of the mechanism of the structural changes. (author)

  18. Electric field measurements in high pressure discharges

    International Nuclear Information System (INIS)

    Mitko, S.V.; Ochkin, V.N.; Serdyuchenko, A.Yu.; Tskhai, S.N.

    2001-01-01

    Electric fields define a wide range of interactions and phenomena at different phases of matter both on micro- and macro-level. Investigation of electric fields behavior provides a key for understanding of these phenomena and their application

  19. High density, high magnetic field concepts for compact fusion reactors

    International Nuclear Information System (INIS)

    Perkins, L.J.

    1996-01-01

    One rather discouraging feature of our conventional approaches to fusion energy is that they do not appear to lend themselves to a small reactor for developmental purposes. This is in contrast with the normal evolution of a new technology which typically proceeds to a full scale commercial plant via a set of graduated steps. Accordingly' several concepts concerned with dense plasma fusion systems are being studied theoretically and experimentally. A common aspect is that they employ: (a) high to very high plasma densities (∼10 16 cm -3 to ∼10 26 cm -3 ) and (b) magnetic fields. If they could be shown to be viable at high fusion Q, they could conceivably lead to compact and inexpensive commercial reactors. At least, their compactness suggests that both proof of principle experiments and development costs will be relatively inexpensive compared with the present conventional approaches. In this paper, the following concepts are considered: (1) The staged Z-pinch, (2) Liner implosion of closed-field-line configurations, (3) Magnetic ''fast'' ignition of inertial fusion targets, (4) The continuous flow Z-pinch

  20. Lactose and ''tris'' lyoluminescence dosimetry systems and ESR correlation studies

    International Nuclear Information System (INIS)

    Oommen, I.K.; Nambi, K.S.V.; Sengupta, S.; Rao, T.K.G.; Ravikumar, M.

    1989-01-01

    Lyoluminescence (LL) dosimeters have been developed using lactose monohydrate (disaccharide) and tris(hydroxymethyl)aminomethane (''Tris'') systems and attempts have been made to understand the LL mechanism through ESR correlation studies. Tris LL dosimeter has a γ-ray sensitivity with a linear response in the absorbed-dose range 0.05-200 Gy (5-2 x 10 4 rad), while the lactose response extends to a higher range from 1 to 10 4 Gy (10 2 -10 6 rad). The LL output of lactose and Tris did not show any appreciable decay for a period of 6 months after irradiation. ESR measurements show that free-radical concentration in both the systems increases with γ-ray dose in the range 10 2 -10 5 Gy. The minimum dose required to measure the radiation-induced ESR signal for Tris is ∼ 500 Gy, the dose at which the LL output saturates, while lactose shows a radiation-induced ESR signal right at the minimum dose where LL could be detected. The estimated spin density on the radical carbon atom is 0.7. ESR signal stabilities of lactose and Tris were also studied. Lactose did not show any appreciable ESR decay for a period of 3 months after irradiation, while, for Tris, one of the radicals showed a decay of 45% for the same period. (author)

  1. Dosimetry of blood irradiation using an alanine/ESR dosimeter

    International Nuclear Information System (INIS)

    Chen, F.; Covas, D.T.; Baffa, O.

    2001-01-01

    A batch of 80 DL-alanine dosimeters was supplied to Hemocentro of the Hospital and Clinics of Faculdade de Medicina de Ribeirao Preto (HC-FMRP) SP, Brazil for the purpose of quality control of the radiation dose delivered to blood bags. The irradiation was made using two (40x40) cm 2 parallel opposed radiation fields each with 80 cm of source to surface distance in the Radiotherapy Section of HC-FMRP with the 60 Co teletherapy unit. The calculated radiation absorbed dose at the center of the box was 20 Gy. The dosimeter readings were performed using a Varian E-4 ESR Spectrometer operating in X-band. For the 80 dosimeters and over the irradiation volume throughout a blood bag, the minimum and maximum doses were 14 and 23 Gy, respectively. The mean dose was (18±2) Gy (1σ), and the coefficient of variability was 11.1%. Alanine dosimeters demonstrated easy handling, good precision and adequate sensitivity for this application

  2. Measurement of radical scavenging activity of irradiated Kampo extracts using ESR spin-trap method

    International Nuclear Information System (INIS)

    Ohta, Yui; Kawamura, Shoei; Ukai, Mitsuko; Nakamura, Hideo; Kikuchi, Masahiro; Kobayashi, Yasuhiko

    2014-01-01

    The radical scavenging activity (RSA) of 13 kinds of γ-ray irradiated Kampo extracts were studied by ESR spin-trap method. The RSA against alkoxy radical and hydroxyl radical were measured using new spin trapping reagent CYPMPO. The RSA against these two radicals were evaluated using GSH for alkoxy RSA and L-ascorbic acid for hydroxy RSA as a standard antioxidant reagent. We revealed that a few Kampo extracts showed high RSA against alkoxy radical and also hydroxy radical. This RSA of Kampo extracts was changed by γ-ray irradiation treatment. Using ESR spin-trap method, it is concluded that the effect of radiation treatment on RSA of Kampo extracts were able to detect. (author)

  3. The SIS-ESR project of GSI

    International Nuclear Information System (INIS)

    Kienle, P.

    1985-05-01

    During the last years GSI developed plans for future accelerators and experimental facilities with the intention to extend heavy ion research in a wide scope to higher energies and into new fields of research using novel techniques for acceleration, accumulation, storage and phase space density increase of heavy ion beams up to 238 U. The prime goals of this development plan using as a first step a synchrotron acceleration ring connected with an accumulator-, storage-, cooling- and experimental ring are the following: 1. Provide completely stripped heavy ion beams up to U 92+ with the highest phase space densities using various cooling techniques in a storage ring. 2. Provide radioactive heavy ion beams by accumulation, storage and cooling of fragmentation or fission products from beams of the synchrotron. 3. Provide facilities for internal target experiments using simultaneously cooled circulating beams. 4. Provide two merging beams in the storage ring with well defineable collision energies up to the Coulomb barrier of the heaviest ions like U 92+ in order to study atomic collision processes in high Coulomb fields with both nuclei highly ionized. 5. Provide a beam of heavy ions up to U 92+ with best phase space density for further acceleration and collisions in superconducting collider rings at very high c.m. energies (>20 GeV/u) and as high as possible luminosities. (orig.)

  4. Polarized neutron reflectometry in high magnetic fields

    International Nuclear Information System (INIS)

    Fritzsche, H.

    2005-01-01

    A simple method is described to maintain the polarization of a neutron beam on its way through the large magnetic stray fields produced by a vertical field of a cryomagnet with a split-coil geometry. The two key issues are the proper shielding of the neutron spin flippers and an additional radial field component in order to guide the neutron spin through the region of the null point (i.e., point of reversal for the vertical field component). Calculations of the neutron's spin rotation as well as polarized neutron reflectometry experiments on an ErFe 2 /DyFe 2 multilayer show the perfect performance of the used setup. The recently commissioned cryomagnet M5 with a maximum vertical field of up to 7.2 T in asymmetric mode for polarized neutrons and 9 T in symmetric mode for unpolarized neutrons was used on the C5 spectrometer in reflectometry mode, at the NRU reactor in Chalk River, Canada

  5. Relationship of white blood cell counts, haemoglobin and ESR with IHD

    International Nuclear Information System (INIS)

    Shahzad, F.; Shahzad Tawwab, S.; Abbas, A.

    2009-01-01

    To find any association of white blood cells, haemoglobin and ESR with ischemic heart disease in high risk native population. Methodology: The study included 93 male patients with Ischemic heart disease, between 40 and 60 years of age; 96 age and gender matched subjects. All study participants were non-diabetics. Complete blood cells count, haemoglobin and ESR levels were compared between the patient and control groups. Results: Total leukocyte counts along with neutrophils were significantly higher in the test group compared to the control population (p<0.001) and lymphocytes were significantly lower (p<0.001) in the patient group as compared to the control group. Haemoglobin levels were significantly lower (p<0.001) and ESR was higher (p=0.030) in the patient group as compared to the control group. Conclusion: Although, our findings of the study variables extend previous reports, the prevalence and prognostic importance of theses variables in IHD should be assessed in future experimental studies. These parameters could be important in public health because they are routinely measured by clinicians and may be helpful to predict the risk of future and secondary ischemic events in a high risk population. (author)

  6. On the connection of the ESR characteristics of zircons with the degree of their defectiveness

    International Nuclear Information System (INIS)

    Matyash, I.V.; Brik, A.E.; Derski, L.S.; Larikov, A.L.; Ponomarenko, A.N.

    1989-01-01

    The dynamic characteristics of the electron-hole centres (EHC) in zircons with various degree of defectiveness have been studied. Crystalline and amorphous regions are typical of different sets of EHC, having essentially different relaxation characteristics. Lack of cross-relaxation between these centres shows that they are localized in different parts of the crystal. The influence of autoirradiation and of corresponding defectiveness of the matrix upon the intensity of the EHC signals (V i ) has been studied. In the specimens of high crystallinity V i increases as the content of radioactive elements and defectiveness increases. In the essentially metamict specimens the situation reverses. Interpretation of this effect is given considering the dose dependence of the ESR signals and the ratio of the crystal and metamict volumes in the studied object. The transformations of the EHC set is traced along the amorphization of the zircon matrix due to the autoirradiation. ESR signals corresponding to different phases in zircon have been recorded. The correlation of the zircon grain size and the static magnetic susceptibility with V i have been studied. In the specimens of high crystallinity such correlation is absent and in metamict specimens the intensities V i decrease as the grain sizes decrease. The interpretation of this fact is proposed. It has been shown that the ESR studies reflect the processes of income and migration of the impurity elements in zircons and the ways of the zircon crystal matrix decay in a geological time scale. The factors controlling such a decay have been found. (author)

  7. Investigating High Field Gravity using Astrophysical Techniques

    Energy Technology Data Exchange (ETDEWEB)

    Bloom, Elliott D.; /SLAC

    2008-02-01

    The purpose of these lectures is to introduce particle physicists to astrophysical techniques. These techniques can help us understand certain phenomena important to particle physics that are currently impossible to address using standard particle physics experimental techniques. As the subject matter is vast, compromises are necessary in order to convey the central ideas to the reader. Many general references are included for those who want to learn more. The paragraphs below elaborate on the structure of these lectures. I hope this discussion will clarify my motivation and make the lectures easier to follow. The lectures begin with a brief review of more theoretical ideas. First, elements of general relativity are reviewed, concentrating on those aspects that are needed to understand compact stellar objects (white dwarf stars, neutron stars, and black holes). I then review the equations of state of these objects, concentrating on the simplest standard models from astrophysics. After these mathematical preliminaries, Sec. 2(c) discusses 'The End State of Stars'. Most of this section also uses the simplest standard models. However, as these lectures are for particle physicists, I also discuss some of the more recent approaches to the equation of state of very dense compact objects. These particle-physics-motivated equations of state can dramatically change how we view the formation of black holes. Section 3 focuses on the properties of the objects that we want to characterize and measure. X-ray binary systems and Active Galactic Nuclei (AGN) are stressed because the lectures center on understanding very dense stellar objects, black hole candidates (BHCs), and their accompanying high gravitational fields. The use of x-ray timing and gamma-ray experiments is also introduced in this section. Sections 4 and 5 review information from x-ray and gamma-ray experiments. These sections also discuss the current state of the art in x-ray and gamma-ray satellite

  8. Investigating High Field Gravity using Astrophysical Techniques

    International Nuclear Information System (INIS)

    Bloom, Elliott D.

    2008-01-01

    The purpose of these lectures is to introduce particle physicists to astrophysical techniques. These techniques can help us understand certain phenomena important to particle physics that are currently impossible to address using standard particle physics experimental techniques. As the subject matter is vast, compromises are necessary in order to convey the central ideas to the reader. Many general references are included for those who want to learn more. The paragraphs below elaborate on the structure of these lectures. I hope this discussion will clarify my motivation and make the lectures easier to follow. The lectures begin with a brief review of more theoretical ideas. First, elements of general relativity are reviewed, concentrating on those aspects that are needed to understand compact stellar objects (white dwarf stars, neutron stars, and black holes). I then review the equations of state of these objects, concentrating on the simplest standard models from astrophysics. After these mathematical preliminaries, Sec. 2(c) discusses 'The End State of Stars'. Most of this section also uses the simplest standard models. However, as these lectures are for particle physicists, I also discuss some of the more recent approaches to the equation of state of very dense compact objects. These particle-physics-motivated equations of state can dramatically change how we view the formation of black holes. Section 3 focuses on the properties of the objects that we want to characterize and measure. X-ray binary systems and Active Galactic Nuclei (AGN) are stressed because the lectures center on understanding very dense stellar objects, black hole candidates (BHCs), and their accompanying high gravitational fields. The use of x-ray timing and gamma-ray experiments is also introduced in this section. Sections 4 and 5 review information from x-ray and gamma-ray experiments. These sections also discuss the current state of the art in x-ray and gamma-ray satellite experiments and

  9. Superconducting niobium in high rf magnetic fields

    International Nuclear Information System (INIS)

    Mueller, G.

    1988-01-01

    The benefit of superconducting cavities for accelerator applications depends on the field and Q/sub 0/ levels which can be achieved reliably in mass producible multicell accelerating structures. The presently observed field and Q/sub 0/ limitations are caused by anomalous loss mechanisms which are not correlated with the intrinsic properties of the pure superconductor but rather due to defects or contaminants on the superconducting surface. The ultimate performance levels of clean superconducting cavities built from pure Nb will be given by the rf critical field and the surface resistance of the superconductor. In the first part of this paper a short survey is given of the maximum surface magnetic fields achieved in single-cell cavities. The results of model calculations for the thermal breakdown induced by very small defects and for the transition to the defect free case is discussed in part 2. In the last chapter, a discussion is given for the rf critical field of Nb on the basis of the Ginzburg-Landau Theory. It is shown that not only purity but also the homogeneity of the material should become important for the performance of superconducting Nb cavities at field levels beyond 100mT. Measurement results of the upper critical field for different grades of commercially available Nb sheet materials are given. 58 references, 20 figures, 1 table

  10. Threats to ultra-high-field MRI

    Science.gov (United States)

    Le Bihan, Denis

    2009-08-01

    In 2004 the European Commission (EC) adopted a directive restricting occupational exposure to electromagnetic fields. This directive (2004/40/CE), which examines the possible health risks of the electromagnetic fields from mobile phones, Wi-Fi, Bluetooth and other devices, concluded that upper limits on radiation and applied electromagnetic fields are necessary to prevent workers from suffering any undue acute health effects. But although not initially intended, the biggest impact of the directive could be on magnetic resonance imaging (MRI), which is used in hospitals worldwide to produce images of unrivalled quality of the brain and other soft tissues.

  11. National High Magnetic Field Laboratory (NHMFL)

    Data.gov (United States)

    Federal Laboratory Consortium — The Pulsed Field Program is located in Northern New Mexico at Los Alamos National Laboratory. The user program is designed to provide researchers with a balance of...

  12. High Field Magnetization of Tb Single Crystals

    DEFF Research Database (Denmark)

    Roeland, L. W.; Cock, G. J.; Lindgård, Per-Anker

    1975-01-01

    Hamiltonian including isotropic exchange interactions, effective single-ion anisotropy and magnetoelastic contributions. The parameters of this Hamiltonian were determined by fitting the theoretical results for the spin wave dispersion and energy gap as a function of temperature and magnetic field to existing...... data on Tb. The conduction-electron polarization at zero field and temperature is (0.33+or-0.05) mu B/ion, and the susceptibility is greater than the Pauli susceptibility calculated from the band-structure....

  13. Study on detection of electron beam irradiated food by ESR spectroscopy and comparison of the ESR spectrum of electron beams and γ-rays

    International Nuclear Information System (INIS)

    Li Weiming; Ha Yiming; Wang Feng

    2012-01-01

    The study was conducted to detect electron beam irradiated food by ESR spectroscopy. The white pepper powder, paprika powder, cumin powder and pistachios were used as test materials to study the feature changes of ESR spectrum and the relationship between ESR intensity and irradiation dose in different doses, the shape variation of ESR spectrum in γ-rays and electron beams in the same sample was also compared. The results showed that the ESR spectrum of 4 kinds of irradiated samples was obviously different before and after irradiation, the intensity of ESR signal increased with the increasing of the absorbed dose. The dose above 432 Gy could be detected in white pepper powder and pistachios, the dose above 875 Gy could be detected in paprika powder and cumin powder. The ESR intensity of all samples decreased during the storage time (200 d), even after 200 days the ESR method could also be used to detect whether or not the samples have been irradiated. The same dosage of y-rays and electron beams has no significant influence on the shape of ESR spectrum, however, the difference of irradiation mechanism caused slight impact on ESR intensity. The results could provide the technical basis for the application of ESR method in detecting electron beam irradiated food. (authors)

  14. Study on detection of electron beam irradiated food by ESR spectroscopy and comparison of the ESR spectrum of electron beams and γ-rays

    International Nuclear Information System (INIS)

    Li Weiming; Ha Yiming; Wang Feng

    2011-01-01

    The study was conducted to detect electron beam irradiated food by ESR spectroscopy. The white pepper powder, paprika powder, cumin powder and pistachios were used as test materials to study the feature changes of ESR spectrum and the relationship between ESR intensity and irradiation dose in different doses, the shape variation of ESR spectrum in γ-rays and electron beams in the same sample was also compared. The results showed that the ESR spectrum of 4 kinds of irradiated samples was obviously different before and after irradiation, the intensity of ESR signal increased with the increasing of the absorbed dose. The dose above 432 Gy could be detected in white pepper powder and pistachios, the dose above 875 Gy could be detected in paprika powder and cumin powder. The ESR intensity of all samples decreased during the storage time (200 d), even after 200 days the ESR method could also be used to detect whether or not the samples have been irradiated. The same dosage of γ-rays and electron beams has no significant influence on the shape of ESR spectrum, however, the difference of irradiation mechanism caused slight impact on ESR intensity. The results could provide the technical basis for the application of ESR method in detecting electron beam irradiated food. (authors)

  15. Detection of electron beam irradiated crude drugs by electron spin resonance (ESR)

    International Nuclear Information System (INIS)

    Yamaoki, Rumi; Kimura, Shojiro; Aoki, Kenji; Nishimoto, Susumu

    2007-01-01

    Perillae Herba, Sennae Folium, Cinnamomi Cortex, Phellodendri Cortex, Ginseng Radix, Glycyrrhizae Radix, Paeoniae Radix, and Zingiberis Rhizoma were irradiated with electron beam (5 MeV) and organic radicals were detected by ESR measurement, before and after irradiation (10 kGy). A single line spectrum was detected at around g=2.005 in non-irradiated crude drugs, and radical concentrations were high in the leaf varieties of crude drugs. After irradiation, the signal intensity around g=2.005 increased, and a new subsignal was detected as a 3 mT shoulder of this signal. Broad, asymmetrically divided signals were also detected in irradiated root varieties of crude drugs. The free radical localized on the organic components of irradiated crude drugs tended to decrease with the water content. After irradiation, signal intensity reduced and reached a steady state after about 1 to 2 months. However, specificity of the ESR signal shape appearing after irradiation continued to be detectable for 6 months in leaf varieties and for a year in bark and root varieties of crude drugs. Consequently, it was concluded that ESR could be applied as an initial screening procedure to detect irradiated crude drugs. (author)

  16. ESR (Electronic Spin Resonance Spectroscopy) study of irradiated paper for biomedical material wrapping

    International Nuclear Information System (INIS)

    Huarte, Monica; Rubin de Celis, Emilio; Kairiyama, Eulogia; Zapata, Miguel; Santoro, Natalia; Magnavacca, Cecilia

    2009-01-01

    Ionising radiation treatments are used for sterilization, microbiological decontamination, disinfection, insect disinfestation and food preservation. This ionising radiation generates free radicals (FR) in matter, which can be detected by Electronic Spin Resonance Spectroscopy (ESR). For this work it had analysed different kind of irradiated package papers of syringes, surgical gloves and dressings by ESR. These were irradiated with doses between 20 and 35 kGy of gamma radiation (Cobalt 60). The processed samples were measured in a Bruker ECS 106 spectrometer. The obtained results were: 1-) The irritated samples showed a central peak and two satellites induced by the applied radiation; 2-) The non-irradiated samples did not show the characteristic satellite peaks of the irritated ones; 3-) A linear relationship between the signal heights per unit mass and the applied doses was found; and 4-) The signals were highly stable, with half-time values between 240 and 370 days for 20 and 30 kGy, permitting more than one year of monitoring proceedings. In conclusion, the ESR allows the detection, quantification and time monitoring processes of this kind of irradiated materials. (author) [es

  17. Quantifying the impact of µCT-scanning of human fossil teeth on ESR age results.

    Science.gov (United States)

    Duval, Mathieu; Martín-Francés, Laura

    2017-05-01

    Fossil human teeth are nowadays systematically CT-scanned by palaeoanthropologists prior to any further analysis. It has been recently demonstrated that this noninvasive technique has, in most cases, virtually no influence on ancient DNA preservation. However, it may have nevertheless an impact on other techniques, like Electron Spin Resonance (ESR) dating, by artificially ageing the apparent age of the sample. To evaluate this impact, we µCT-scanned several modern enamel fragments following the standard analytical procedures employed by the Dental Anthropology Group at CENIEH, Spain, and then performed ESR dose reconstruction for each of them. The results of our experiment demonstrate that the systematic high-resolution µCT-scanning of fossil hominin remains introduces a nonnegligible X-ray dose into the tooth enamel, equivalent to 15-30 Gy depending on the parameters used. This dose may be multiplied by a factor of ∼8 if no metallic filter is used. However, this dose estimate cannot be universally extrapolated to any µCT-scan experiment but has instead to be specifically assessed for each device and set of parameters employed. The impact on the ESR age results is directly dependent on the magnitude of the geological dose measured in fossil enamel but could potentially lead to an age overestimation up to 40% in case of Late Pleistocene samples, if not taken into consideration. © 2017 Wiley Periodicals, Inc.

  18. Free radicals in cellulose containing food detected by ESR

    International Nuclear Information System (INIS)

    Abe, Aika; Yogo, Satsuki; Ichii, Akane; Ukai, Mitsuko

    2003-01-01

    Using electron spin resonance (ESR) spectroscopy, we revealed three radical species in cellulose containing foods, pepper and green tea. These are commercially available in Japan. The representative ESR spectrum is composed of a sextet centered at g=2.0, a singlet at the same g-value, and a singlet at g=4.0. The first one is attributable to a signal with hyperfine (hf) interactions of Mn 2+ ion (hf constant: 7.4 mT). The second one is due to an organic free radical, the third one may be originated from Fe 3+ ion. The progressive saturation behavior (PSB) of the ESR at various microwave power levels were indicated different relaxation behaviors of in those radicals. Namely, the peak intensity of the organic free radical component decreases in a monotonic fashion, whereas the Mn 2+ and Fe 3+ ESR signals substantially keep constant. This reflects the evidence of three independent radical species. The ESR spectrum of the cellulose containing foods shows the same spectral feature irrespective of the tea or pepper. Upon gamma irradiation, a new pair of signals appeared. The PSB of the pair peaks after the irradiation showed a quite different as compared with the free radical centered at g=2. (author)

  19. ESR in a disordered network of nanographene sheets

    Science.gov (United States)

    Hagiwara, M.; Tsugeno, H.; Yamaguchi, H.; Joly, V. L. J.; Takai, K.; Enoki, T.

    2011-12-01

    Randomly networked nanographene sheets have been studied by electron spin resonance (ESR) technique at 20 GHz (K-band) and 35 GHz (Q-band). Nanographene has spin-polarized non-bonding π-electron states (edge-state spins) localized in the zigzag edge region. We have investigated the temperature dependence of an ESR signal of activated carbon fibers at two different microwave powers for each frequency. The signal intensity smoothly increases with decreasing temperature at any microwave power. The line width of ESR signal with a Lorentzian line shape decreases linearly upon cooling, and then increases steeply after taking a minimum at about 20 K irrespective of microwave power. The former is interpreted as the Korringa relation in the localized edge spins and conduction π carriers. The latter may be caused by inhomogeneous line broadening of the ESR signal from randomly distributed nanographene sheets with different sizes due to the suppression of electron hopping between nanographene sheets, i.e. electron localization. The discontinuous line broadening and the signal intensity drop at around 20 K reported in the previous X-band ESR at 1 μW were not observed, probably because of either higher microwave power than 1 μW or some amount of oxygen adsorption in our sample in the present study.

  20. [Relations between plasma-erythrocyte viscosity factors and ESR].

    Science.gov (United States)

    Cortinovis, A; Crippa, A; Crippa, M; Bosoni, T; Moratti, R

    1992-09-01

    The ESR is usually put in relationship: to the real density of the RBCs (erythrocytes) (difference between the RBC specific gravity and the plasma one), and to the resistance that the RBCs meet moving in a medium, which is due to the plasma viscosity and to the total external RBC surface. When the RBCs take shape of aggregates, their external surface is decreased and ESR increases. The most important plasma factor causing changes in ESR is the fibrinogen level followed by the plasma globulins and by the products arising from the tissue damage. The resistance that the RBCs meet moving in the plasma is well expressed by the measurement of the plasma-RBC viscosity considering that is inclusive of both factors that are the plasma viscosity and the external RBC surface. The plasma-RBC viscosity is the resultant of several factors: Fa = Fb - Fe - Fs - Fm, were: Fa is the resultant, Fb the attracting forces due to the proteic macromolecules, Fe the repulsing forces due the negative charges. Fs the repulsing forces due to the shear-stress, Fm the force which opposes itself against the surface tension of the aggregation; it depends on the RBC morphology and on the RBC rigidity. The ESR has been recently used like an index of the RBC aggregation. The Authors study the relationship between several hemorheological parameters and the ESR in infective and inflammatory processes.(ABSTRACT TRUNCATED AT 250 WORDS)

  1. Highly educated but in the wrong field?

    DEFF Research Database (Denmark)

    Reimer, David; Steinmetz, Stephanie

    2009-01-01

      This paper investigates the impact of gender differences in tertiary education, i.e., field of study and level of tertiary degree, on two selected labour market risks: unemployment and low-status jobs. Using Labour Force Survey data from the year 2000, results of the logistic regression models...... and non-linear decomposition analyses generally confirm our expectation that the field of study explains a sizable portion of the gender gap in unemployment and low-status jobs in both countries. However, the level of tertiary degree earned explains only part of the female disadvantage behind holding...

  2. The 4π-collaboration at SIS/ESR

    International Nuclear Information System (INIS)

    Rami, F.

    1991-01-01

    A new generation of 4π experiments aiming at the investigation of the properties of compressed and heated nuclear matter produced in heavy-ion collisions in the incident energy range .1 to 2. GeV/nucleon, is presently starting at the SIS/ESR facility at GSI-Darmstadt. The new 4π-instrument is described. A first experiment was focused on the production of composite particles in central and semi central collisions of 197 Au+ 197 Au at incident energies between 100 and 800 MeV/nucleon. Preliminary results indicate that the charged particle multiplicity measurement alone cannot be used to select the most central collisions, and new selection criteria are suggested. They also show the ability of the detection system to sort out, with reasonable statistics, high degree multifragment events, i.e. events where a large fraction of the total initial charge is going into a few big clusters (Z≥6). (R.P.) 20 refs., 14 figs

  3. Electrical resistivity of UBe13 in high magnetic fields

    International Nuclear Information System (INIS)

    Schmiedeshoff, G.M.; Lacerda, A.; Fisk, Z.; Smith, J.L.

    1996-01-01

    We have measured the temperature dependent electrical resistivity of single and polycrystal samples of UBe 13 in high magnetic fields. Two maxima in the resistivity are observed at T M1 and T M2 . T M1 , the temperature of the colder maximum, increases quadratically with magnetic field H, a field dependence previously observed under hydrostatic pressure. The high temperature maximum at T M2 emerges in fields above about 4 T and increases linearly with H, a behavior which may be due to a sharpening of the crystal field levels associated with a depression of the Kondo effect by high magnetic fields. copyright 1996 The American Physical Society

  4. High-intensity, focused ultrasonic fields

    DEFF Research Database (Denmark)

    Jensen, Leif Bjørnø

    1988-01-01

    The use of extracorporeal shock wave lithotripsy (ESWL) for disintegration of body stones has increased considerably during recent years. A worldwide activity in this field is reflected in a growing number of international publications and in the development and manufacturing of several ESWL...... essential pressure wave parameters, their relation to the focal system data, and their significance to stone disintegration efficiency....

  5. Moderate and high intensity pulsed electric fields

    NARCIS (Netherlands)

    Timmermans, Rian Adriana Hendrika

    2018-01-01

    Pulsed Electric Field (PEF) processing has gained a lot of interest the last decades as mild processing technology as alternative to thermal pasteurisation, and is suitable for preservation of liquid food products such as fruit juices. PEF conditions typically applied at industrial scale for

  6. High-field superconducting nested coil magnet

    Science.gov (United States)

    Laverick, C.; Lobell, G. M.

    1970-01-01

    Superconducting magnet, employed in conjunction with five types of superconducting cables in a nested solenoid configuration, produces total, central magnetic field strengths approaching 70 kG. The multiple coils permit maximum information on cable characteristics to be gathered from one test.

  7. Plasma instabilities in high electric fields

    DEFF Research Database (Denmark)

    Morawetz, K.; Jauho, Antti-Pekka

    1994-01-01

    expression is derived for the nonequilibrium dielectric function epsilon(K, omega). For certain values of momenta K and frequency omega, Imepsilon(K, omega) becomes negative, implying a plasma instability. This new instability exists only for strong electric fields, underlining its nonequilibrium origin....

  8. Carrier tunneling in high magnetic fields

    NARCIS (Netherlands)

    Christianen, P.C.M.; Bruggink, I.E.M.; Maan, J.C.; Vleuten, van der W.C.

    1995-01-01

    Proceedings of the XXIV International School of Semiconducting Coinpounds, Jaszowiec 1995. A magnetic field induced coupling is observed between the Landau levels with different quantum number of two GaAs quantum wells separated by a thin (Ga,Al)As tunnel barrier using

  9. Analysis of ESR measurement parameters for detecting irradiated spices

    International Nuclear Information System (INIS)

    Kameya, Hiromi; Hagiwara, Shoji; Todoriki, Setsuko

    2015-01-01

    The side signals from irradiated cellulose radical are used for detecting irradiated spices with the electron spin resonance (ESR). The side signals are two signals observed on both sides of a singlet signal (g≒2.00) from organic free radicals. Since the intensities of the side signals are weak, if the width of the singlet signal is large, these signals are covered and cannot be observed. In this study, we analyzed ESR measurement parameters of seven kinds spices (oregano, basil, parsley, coriander, cumin, white pepper, and black pepper) that would lead to narrow width of the singlet signal for detecting side signals. The results were as follows: 4 mW microwave power for basil, parsley, oregano, coriander, and cumin, and 8 mW for white pepper and black pepper, while modulation amplitude of 4 G, time constant of 20 ms were determined to be the optimal ESR measurement parameters. (author)

  10. Dose determination by ESR in an accident, using cotton fabric

    International Nuclear Information System (INIS)

    Venkataramani, R.; Mehta, S.K.; Iyer, M.R.; Natarajan, V.; Sastry, M.D.

    1993-01-01

    Accidental exposure dose assessment by electron spin resonance (ESR) technique from the free radicals generated in a cotton handkerchief has been attempted in this investigation. The cotton handkerchief, a common material carried by individuals, was taken as the medium for free radical estimation. About 55 mg of the irradiated piece of cloth was loaded into a quartz tube and the dose dependence of the ESR signal at g = 2.0026 was measured at room temperature, using a Bruker ESP-300 ESR spectrometer in X-band (9.74 GHz). The intensity of this signal was found to be proportional to the dose in the range of 1-1000 Gy. The stability of the free radicals with time of storage was followed. Dependence of dose rate as well as the presence of water on the yield of free radicals were also investigated. (author) 5 refs.; 4 figs.; 2 tabs

  11. Novel Electrochemical Phenomena in Magnetic Fields(Research in High Magnetic Fields)

    OpenAIRE

    Mogi, Iwao; Kamiko, Masao

    1996-01-01

    Recent two topics are given of electrochemical studies in steady magnetic fields at the High Field Laboratory of Tohoku University. One is the magnetic-field-induced diffusion-limited-aggregation in the pattern formation of silver electrodeposits . The other is the magnetic field effect on the learning effect in a dopant-exchange process of an organic conducting polymer polypyrrole.

  12. A Nb3Sn high field dipole

    International Nuclear Information System (INIS)

    McClusky, R.; Robins, K.E.; Sampson, W.B.

    1990-01-01

    A dipole magnet approximately 1 meter long with an 8 cm bore has been fabricated from cable made from Nb 3 Sn multifilamentary strands. The coil consists of four layers of conductor wound in pairs to eliminate internal joints. Each set of layers is separately constrained with Kevlar-epoxy bands and the complete assembly clamped in a split laminated iron yoke. The inner coil pairs were wound before heat treating while the outer coils were formed from pre-reacted cable using conventional insulation. A NbTi version of the magnet was fabricated using SSC version of the magnet was fabricated using SSC conductor to test the construction techniques. This magnet reached a maximum central field of 7.6 Tesla, at 4.4K which is very close to the limit estimated from conductor measurements. The Nb 3 Sn magnet, however, only reached a maximum field at 8.1T considerably short of the field expected from measurements on the inner cable. 7 refs., 5 figs

  13. ESR studies of electron irradiated K3Ir(CN)6 in KCl single crystals

    International Nuclear Information System (INIS)

    Vugman, N.V.; Pinhal, N.M.

    1983-01-01

    ESR studies of KCl single crystals doped with small amounts of K 3 Ir(CN) 6 and submitted to a prolongued 2 MeV electron irradiation at room temperature reveal the presence of the [IR(CN) 5 Cl] 4- and [Ir(CN) 4 Cl 2 ] 4- new molecular species. Ligand spin densities and ligand field parameters are calculated from the experimental hyperfine and superhyperfine interactions and compared to previous data on the [Ir(CN) 5 ] 4- species. (Author) [pt

  14. Alanine-ESR dosimetry for radiotherapy IAEA experience

    International Nuclear Information System (INIS)

    Mehta, K.; Girzikowsky, R.; )

    1997-01-01

    At present, the most commonly used transfer dosimeters for radiotherapy applications are TL dosemeters. They are being used for intercomparison between SSDLs (about 70) and the IAEA dosimetry laboratory. However, there are some undesirable characteristics of this dosimetry system. We have a study in progress at the IAEA to evaluate the alanine-ESR systems as an alternative to TLDs. There are several desirable qualities which make alanine an attractive dosemeter. Preliminary data suggest that the alanine-ESR dosimetry system has the potential to replace TLDs for intercomparison amongst SSDLs in the therapy-level dose regions. (Author)

  15. ESR dating studies on fossil of elaphurus davidianus horn

    International Nuclear Information System (INIS)

    Chen Shiming; Wang Hong; Tang Jingjuan; Yan Xiaomin; Guo Shiqing

    1991-01-01

    On the basis of studies on elephant tooth fossil, ESR dating of elaphurus davidianus horn fossil found in Anhui Province was reported. The sample examined by TEM electron spectrum is composed of hydroxyapatite. ESR experiments showed that the solid bone sample can be chosen as dating material. According to the contents of U, Th and K in the sample determined by ICP, the annual dose of radiation was calculated by using the linear uranium accumulation model and disequilibrium decay. The age of this fossil was determined to be 2.5 x 10 4 years

  16. An ESR study of defects in irradiated hydroxyapatite

    International Nuclear Information System (INIS)

    Murata, T.; Shiraishi, K.; Ebina, Y.; Miki, T.

    1996-01-01

    Radiation-induced defects in synthetic hydroxyapatite (HAp) of six different origins have been investigated by electron spin resonance (ESR), X-ray diffraction (XRD), Raman scattering and IR measurements. The orthorhombic CO 2 - radicals were detected in almost all of the samples examined, but the isotropic CO 2 - was produced only in water-containing HAp with low crystallinity. The doublet signal due to H 0 was clearly detected in HAp with extreme calcium deficiency as compared to the stoichiometry. The results of ESR and FTIR suggest that water molecules in low crystalline HAp are not on the surface but embedded in the HAp crystalline lattice. (author)

  17. Attempt at ESR dating of tooth enamel of French middle pleistocene sites

    International Nuclear Information System (INIS)

    Bahain, J.J.; Sarcia, M.N.; Falgueres, C.; Yokoyama, Y.

    1993-01-01

    Tooth enamel samples from four important French middle Pleistocene sites are analyzed by the ESR method. ESR ages were calculated using uranium uptake mathematical models and compared with U-series results. (author)

  18. Photoluminescence and ESR of glasses of the Ge-S system

    International Nuclear Information System (INIS)

    Cernoskova, E.; Cernosek, Z.; Holubova, J.

    1999-01-01

    In this work the chalcogenide glasses were studied by photoluminescence, electron spin resonance (ESR) as well as optically induce ESR (LESR) methods. Dependence of energy of luminescence and Stokes shift on glass composition was determined

  19. High-field magnetization of dilute rare earths in yttrium

    DEFF Research Database (Denmark)

    Touborg, P.; Høg, J.; Cock, G. J.

    1974-01-01

    Magnetization measurements have been performed on single crystals of Y containing small amounts of Tb, Dy, or Er at 4.2 K in fields up to 295 × 105 A/m (370 kOe). Crystal-field and molecular-field parameters obtained from measurements of the initial susceptibility versus temperature give a satisf...... a satisfactory quantitative account of the high-field magnetization. This includes characteristic features due to the crossing and mixing of crystal-field levels....

  20. Simple method for quantification of gadolinium magnetic resonance imaging contrast agents using ESR spectroscopy.

    Science.gov (United States)

    Takeshita, Keizo; Kinoshita, Shota; Okazaki, Shoko

    2012-01-01

    To develop an estimation method of gadolinium magnetic resonance imaging (MRI) contrast agents, the effect of concentration of Gd compounds on the ESR spectrum of nitroxyl radical was examined. A solution of either 4-oxo-2,2,6,6-tetramethylpiperidine-N-oxyl (TEMPONE) or 4-hydroxy-2,2,6,6-tetramethylpiperidine-N-oxyl (TEMPOL) was mixed with a solution of Gd compound and the ESR spectrum was recorded. Increased concentration of gadolinium-diethylenetriamine pentaacetic acid chelate (Gd-DTPA), an MRI contrast agent, increased the peak-to-peak line widths of ESR spectra of the nitroxyl radicals, in accordance with a decrease of their signal heights. A linear relationship was observed between concentration of Gd-DTPA and line width of ESR signal, up to approximately 50 mmol/L Gd-DTPA, with a high correlation coefficient. Response of TEMPONE was 1.4-times higher than that of TEMPOL as evaluated from the slopes of the lines. The response was slightly different among Gd compounds; the slopes of calibration curves for acua[N,N-bis[2-[(carboxymethyl)[(methylcarbamoyl)methyl]amino]ethyl]glycinato(3-)]gadolinium hydrate (Gd-DTPA-BMA) (6.22 μT·L/mmol) and gadolinium-1,4,7,10-tetraazacyclododecane-1,4,7,10-tetraacetic acid chelate (Gd-DOTA) (6.62 μT·L/mmol) were steeper than the slope for Gd-DTPA (5.45 μT·L/mmol), whereas the slope for gadolinium chloride (4.94 μT·L/mmol) was less steep than that for Gd-DTPA. This method is simple to apply. The results indicate that this method is useful for rough estimation of the concentration of Gd contrast agents if calibration is carried out with each standard compound. It was also found that the plot of the reciprocal square root of signal height against concentrations of contrast agents could be useful for the estimation if a constant volume of sample solution is taken and measured at the same position in the ESR cavity every time.

  1. Non-linear effects in the radiolysis-optically detected ESR of radical-ion pairs in liquid and glassy solutions. Reactions and motion of organic radicals as studied by ESR and OD ESR spectroscopy

    International Nuclear Information System (INIS)

    Antzutkin, O.

    1992-01-01

    This thesis is divided into two sections. The first part covers an introduction to the Optically Detected Electron Spin Resonance (OD ESR) spectroscopy and a short description of the OD ESR spectrometer built in Linkoeping University in 1991. In the second section the following topics are discussed: Non-linear effects in OD ESR spectroscopy and Reactions and motion of organic radicals trapped in freon matrices. (19 refs.)

  2. Magnetic memory effects in high temperature superconductors

    International Nuclear Information System (INIS)

    Rockenbauer, A.

    1989-01-01

    Microwave absorption of high temperature oxide superconductors MBa 2 Cu 3 O 7 (M = Y, Er, Dy, Ho, Lu, Tm, Gd) at 77 K have been studied by ESR. In granular samples diamagnetic zero-field resonance and strong ESR baseline hysteresis have been observed: for increasing field sweep - a high, for decreasing one - a low, while in constant field the baseline approaches the middle position with kinetics typical of spin-glasses. The hysteresis amplitude, i.e. the deviation of high and low baselines, possesses maximum at zero field if the sample is cooled down in zero field. In case of field cooling both the diamagnetic resonance and hysteresis maximum are shifted as a function of relative direction of the fields where the samples are cooled and measured, respectively. The shift is caused by the remanent diamagnetism of trapped fluxons. The hysteresis critically depends on the modulation amplitude of magnetic field, and no hysteresis can be observed if the microwave absorption is detected without field modulation. By applying saw-tooth sweep the spin-glass can be driven between two extreme hysteresis states, and the ESR response is rectangular for large saw-tooth amplitude and linear - for small one, while for intermediate amplitudes the recording shows characteristic memory effects. The hysteresis memory is explained in terms of loop distribution of fluxons. In the single crystal the fluxon absorptions are also detected and the separation of fluxon lines can be related to the hysteresis in granular samples. (author)

  3. Elevated seminal plasma estradiol and epigenetic inactivation of ESR1 and ESR2 is associated with CP/CPPS.

    Science.gov (United States)

    Nesheim, Nils; Ellem, Stuart; Dansranjavin, Temuujin; Hagenkötter, Christina; Berg, Elena; Schambeck, Rupert; Schuppe, Hans-Christian; Pilatz, Adrian; Risbridger, Gail; Weidner, Wolfgang; Wagenlehner, Florian; Schagdarsurengin, Undraga

    2018-04-13

    Chronic prostatitis/chronic pelvic pain syndrome (CP/CPPS) is associated with urinary tract symptoms and hormonal imbalances amongst others. The heterogeneous clinical presentation, unexplored molecular background and lack of prostate biopsies complicate therapy. Here, using liquid biopsies, we performed a comprehensive translational study on men diagnosed with CP/CPPS type III ( n = 50; median age 39.8, range 23-65) and age-matched controls ( n = 61; median age 36.8, range 20-69), considering biochemical parameters of blood and ejaculates, and epigenetic regulation of the estrogen receptor genes ( ESR1 and ESR2 ) in leukocytes isolated from blood (systemic regulation) and in somatic cells isolated from ejaculates (local regulation). We found elevated 17β-estradiol (E 2 ) levels in seminal plasma, but not in blood plasma, that was significantly associated with CP/CPPS and impaired urinary tract symptoms. In ejaculated somatic cells of CP/CPPS patients we found that ESR1 and ESR2 were both significantly higher methylated in CpG-promoters and expressionally down-regulated in comparison to controls. Mast cells are reported to contribute to CP/CPPS and are estrogen responsive. Consistent with this, we found that E 2 -treatment of human mast cell lines (HMC-1 and LAD2) resulted in altered cytokine and chemokine expression. Interestingly, in HMC-1 cells, possessing epigenetically inactivated ESR1 and ESR2, E 2 -treatment led to a reduced transcription of a number of inflammatory genes. Overall, these data suggest that elevated local E 2 levels associate with an epigenetic down-regulation of the estrogen receptors and have a prominent role in CP/CPPS. Investigating E 2 levels in semen could therefore serve as a promising biomarker to select patients for estrogen targeted therapy.

  4. ESR, thermoelectrical and positron annihilation Doppler broadening studies of CuZnFe{sub 2}O{sub 4}-BaTiO{sub 3} composite

    Energy Technology Data Exchange (ETDEWEB)

    Hemeda, O.M. [Physics Department, Faculty of Science, Tanta University, Tanta (Egypt); Mahmoud, K.R. [Physics Department, Faculty of Science, Kafrelsheikh University, Kafr El-Sheikh (Egypt); Sharshar, T. [Physics Department, Faculty of Science, Kafrelsheikh University, Kafr El-Sheikh (Egypt); Physics Department, Faculty of Science, Taif University, Al-Hawiah, Taif, P.O. Box 888 Zip Code 21974 (Saudi Arabia); Elsheshtawy, M. [Physics Department, Faculty of Science, Tanta University, Tanta (Egypt); Hamad, Mahmoud A., E-mail: m_hamad76@yahoo.com [Physics Department, Faculty of Science, Tanta University, Tanta (Egypt); King Marriott Academy for Engineering & Technology, Alexandria (Egypt)

    2017-05-01

    Composite materials of Cu{sub 0.6}Zn{sub 0.4}Fe{sub 2}O{sub 4} (CZF) and barium titanate (BT) with different concentrations were prepared by high energy ball milling method. The composite samples of CZF and BT were studied using Infrared, ESR and positron annihilation Doppler broadening (PADB) spectroscopy techniques as well as thermo-electric power measurements. The results confirm formation of the composite, and presence of two ferrimagnetic and ferroelectric phases, simultaneously. In addition, Fe–O bond for both tetrahedral and octahedral sites, population and distribution of cations at A and B sites are varied with BT content. The values of resonance field, line width of ESR spectrum and charge carrier concentration increase by increasing BT content. The value of the g factor for our samples with low BT content is greater than g-factor value of the isolated free electron. On the contrary, the g-factor values for samples with high BT content are smaller than the free isolated electron. PADB line-shape S-parameter suggests that there are increases of the density of the delocalized electrons, defect size and concentration caused by highly adding BT phase. In addition, PADB results confirm the homogeneity of composite phases and same structure of defects in BT-CZF composite samples. - Highlights: • Composite materials of Cu{sub 0.6}Zn{sub 0.4}Fe{sub 2}O{sub 4} (CZF) and barium titanate (BT) were prepared. • The resonance field and charge carrier concentration increase by increasing BT. • there is increase of the density of delocalized electrons by highly adding BT. • In addition, PADB results confirm the homogeneity of composite phases.

  5. Estimate of landslide deformation and failure time by ESR technique of. alpha. -quartz

    Energy Technology Data Exchange (ETDEWEB)

    Xingzhong, Liang; Mingdong, Chen [Chengdu Coll. of Geology, SC (China); Jiyong, Chen; Jiamin, Feng [Sichuan Univ., Chengdu, SC (China)

    1991-02-01

    ESR dating has been applied to study landslides. A method of dose-difference to determine the landslide age has been developed. The ESR spectra of annealled quartz grain samples and the optimum conditions of thermal activation were studied. The signifcance of ESR dating of landslide in geological research was discussed.

  6. High Magnetic Field Vortex Microscopy by NMR

    Science.gov (United States)

    Mitrović, V. F.; Sigmund, E. E.; Bachman, H. N.; Halperin, W. P.; Reyes, A. P.; Kuhns, P.; Moulton, W. G.

    2001-03-01

    At low temperatures the ^17O NMR spectrum of HTS exhibits a characteristic vortex lattice line shape. Measurements of spin-lattice relaxation rate, T_1-1, across the vortex spectrum represent a probe of low-energy quasiparticle excitations as a function of distance from the vortex core. We report ^17O(2,3) T_1-1 measurements of YBa_2Cu_3O7 at low temperatures in magnetic fields up to 37 T. We find that the rate increases on approaching the vortex core. In the vortex core region at 37 T we observe an additional increase in the relaxation rate. The temperature dependence of the rate will also be discussed. Work at Northwestern University is supported by the NSF (DMR 91-20000) through the Science and Technology Center for Superconductivity.

  7. Investigation of free radicals in paprika with the ESR method

    International Nuclear Information System (INIS)

    Kispeter, J.; Szabo, I.; Horvath, L.J.

    1998-01-01

    Complete text of publication follows. The ESR method is the one of the most successfully applied method among the physical methods for the identification of radiation or ionising treatment of foods. The identification of free radicals having short and long lifetimes is the base of the measurement. The quantitative determination makes possible the determination of the absorbed dose deriving from 60 Co radiation treatment. It has to be noted that the treatment of the foods with ionising radiation and other treatments (milling, frying, baking) and the oxidative process result free radicals in paprika samples as a function of absorbed radiation dose (2.5; 5 and 10 kGy) on the different particle size and on storage time. The intensities of the samples given after each of the seven stages of the paprika milling increased till the fifth stage corresponding to the effect of a 2 kGy absorbed dose. After conditioning and increasing the water content by 5-8% the ESR intensity shows significant lowering. This value characterises the ESR intensity of not irradiated sample. As an effect of the irradiation the ESR intensities increased along with the increase of the absorbed dose. The samples having lower particle size are more sensible for the identification of the irradiation. Evaluating the art of the decline we concluded that there are free radicals having short and long shelf lifetimes in paprika samples at the same time

  8. Absolute rate measurement by light modulation - ESR technique

    Energy Technology Data Exchange (ETDEWEB)

    Choo, K Y; Gaspar, P P

    1977-01-01

    A rate constant is deduced for the reaction of tert-butoxy radicals and trimethylsilane from the measurement of the phase shift between the modulated light source and the ESR signal of trimethylsilyl radical. The rate constant was found to be 3 x 10/sup -2/M/sup -1/. sec/sup -1/ at -50/sup 0/C.

  9. ESR spectroscopy - an analytical tool for the glass industry

    International Nuclear Information System (INIS)

    Elvers, A.; Weissmann, R.

    2001-01-01

    In the past, wet chemical methods have been developed for the quantitative analysis of polyvalent elements in glasses. The major disadvantage of these chemical methods is that all structural information is lost during analysis. In addition, the analysis of species by wet chemical methods is unreliable due to possible redox reactions during the decomposition process. Therefore, the emphasis is on the physical methods which can directly detect species in bulk glasses. Especially optical and ESR spectroscopy are suitable methods due to their wide range of applications and sensitivity. Concerning quantitative measurements, no comparison between ESR results and chemical analysis of species has been published so far. This work discusses the possible application of ESR spectroscopy in the glass industry by focussing on routine interpretation, the correlation to chemical procedures and quantitative analysis. Results are presented and discussed for iron and chromium in packaging glasses. For example an excellent correlation was found between the Fe 3+ ESR signal and the chemically determined Fe 3+ concentration in glass. (orig.)

  10. Influence of Thermal Homogenization Treatment on Structure and Impact Toughness of H13 ESR Steel

    Institute of Scientific and Technical Information of China (English)

    MA Dang-shen; ZHOU Jian; CHEN Zai-zhi; ZHANG Zhong-kan; CHEN Qi-an; LI De-hui

    2009-01-01

    The as-cast microstrueture of H13 ESR ingot and the influence of high temperature diffusion treatment on the structure and impact toughness have been investigated. The results show that the dendrite arm spacing gradually becomes wide from the surface to the center of ingot, and the large primary carbide particles always exist in interdendritic segregation areas; by means of high temperature diffusion treatment of ingot prior to hot forging, the banded segregation is nearly eliminated, the annealed structure is more uniform and the isotropic properties have been improved remarkably.

  11. High field Tokamaks: The why's and how's

    International Nuclear Information System (INIS)

    Sestero, A.

    1989-01-01

    After expressing the input power into the plasma through the energy confinement time τ E (by invoking thermal equilibrium), and in turn expressing τ E through the LAWSON parameter L, power-law type scalings can be manipulated into the form G(L,T,m)=M(α,B,A,q,β) (1) where G and M are monomial functions of their arguments. The function G can be labelled goal factor in that by assigning numerical values to its arguments L (Lawson's parameter), T (temperature) and m (ion mass), one is typically identifying specific goals on the way to fusion. Conversely, the function M can be labelled merit factor in that, whichever merit exists in the discharge parameters appearing as its arguments, it is expressed by the particular combination of values that M represents. Please note that, of the usual variables appearing in scaling laws, the minor radius α and the magnetic field B are maintained as such in relation (1), while the major radius R, the plasma current I and the plasma density n are respectively expressed in terms of the aspect ratio A, the safety factor q and the plasma β: consequently, arguments of M are one extensive variable (namely α) and one intensive variable (namely B), plus a set of three dimensionless variables (namely A,q,β). (author) 6 refs., 2 figs

  12. Simultaneous CXCL12 and ESR1 CpG island hypermethylation correlates with poor prognosis in sporadic breast cancer

    International Nuclear Information System (INIS)

    Ramos, Edneia AS; Klassen, Giseli; Camargo, Anamaria A; Braun, Karin; Slowik, Renata; Cavalli, Iglenir J; Ribeiro, Enilze MSF; Pedrosa, Fábio de O; Souza, Emanuel M de; Costa, Fabrício F

    2010-01-01

    CXCL12 is a chemokine that is constitutively expressed in many organs and tissues. CXCL12 promoter hypermethylation has been detected in primary breast tumours and contributes to their metastatic potential. It has been shown that the oestrogen receptor α (ESR1) gene can also be silenced by DNA methylation. In this study, we used methylation-specific PCR (MSP) to analyse the methylation status in two regions of the CXCL12 promoter and ESR1 in tumour cell lines and in primary breast tumour samples, and correlated our results with clinicopathological data. First, we analysed CXCL12 expression in breast tumour cell lines by RT-PCR. We also used 5-aza-2'-deoxycytidine (5-aza-CdR) treatment and DNA bisulphite sequencing to study the promoter methylation for a specific region of CXCL12 in breast tumour cell lines. We evaluated CXCL12 and ESR1 methylation in primary tumour samples by methylation-specific PCR (MSP). Finally, promoter hypermethylation of these genes was analysed using Fisher's exact test and correlated with clinicopathological data using the Chi square test, Kaplan-Meier survival analysis and Cox regression analysis. CXCL12 promoter hypermethylation in the first region (island 2) and second region (island 4) was correlated with lack of expression of the gene in tumour cell lines. In the primary tumours, island 2 was hypermethylated in 14.5% of the samples and island 4 was hypermethylated in 54% of the samples. The ESR1 promoter was hypermethylated in 41% of breast tumour samples. In addition, the levels of ERα protein expression diminished with increased frequency of ESR1 methylation (p < 0.0001). This study also demonstrated that CXCL12 island 4 and ESR1 methylation occur simultaneously at a high frequency (p = 0.0220). This is the first study showing a simultaneous involvement of epigenetic regulation for both CXCL12 and ESR1 genes in Brazilian women. The methylation status of both genes was significantly correlated with histologically advanced

  13. Super-high magnetic fields in spatially inhomogeneous plasma

    International Nuclear Information System (INIS)

    Nastoyashchiy, Anatoly F.

    2012-01-01

    The new phenomenon of a spontaneous magnetic field in spatially inhomogeneous plasma is found. The criteria for instability are determined, and both the linear and nonlinear stages of the magnetic field growth are considered; it is shown that the magnetic field can reach a considerable magnitude, namely, its pressure can be comparable with the plasma pressure. Especially large magnetic fields can arise in hot plasma with a high electron density, for example, in laser-heated plasma. In steady-state plasma, the magnetic field can be self-sustaining. The considered magnetic fields may play an important role in thermal insulation of the plasma. (author)

  14. Investigation of radiosterilization feasibility of sulfamethoxazole by ESR spectroscopy

    Science.gov (United States)

    Çolak, Şeyda

    2017-12-01

    In the present study, the spectroscopic features of the radiolytic intermediates that were produced in gamma-irradiated (5, 10, 25 and 50 kGy) sulfamethoxazole (SMX) have been investigated by electron spin resonance (ESR) spectroscopy and the radiation sterilization feasibility of SMX by ionizing radiation was examined. Gamma-irradiated SMX exhibited a complex ESR spectrum consisting of 13 resonance lines where spectral parameters for the central resonance line were found to be g = 2.0062 and ΔHpp = 0.6 mT. The radiation yield of SMX was calculated to be relatively low (G = 0.1) by ESR spectroscopy and no meaningful difference was observed in the comparison of unirradiated and 50 kGy gamma irradiated SMX by the Fourier transform infrared (FT-IR) technique, confirming that SMX is a radioresistive material. Although SMX could not be accepted to be a good dosimetric material, the identification of irradiated SMX from the unirradiated sample was possible even for the low absorbed radiation doses and for a relatively long time (three months) after the irradiation process. Decay activation energy of the radical species, which is mostly responsible for the central intense resonance line, is calculated to be 45.15 kJ/mol by using the signal intensity decay data derived from annealing studies. Four radical species with different spectroscopic properties were accepted to be responsible for the ESR spectra of gamma-irradiated SMX, by simulation calculations. It is concluded that SMX and SMX-containing drugs can be sterilized by gamma radiation and ESR spectroscopy is an appropriate technique for the characterization of these induced radical intermediates during the gamma irradiation process of SMX. Toxicology tests should also be done for its safe usage.

  15. Elaboration And Study Of Transfer Alanine/ESR Dosemeters

    International Nuclear Information System (INIS)

    Torres G, Luz A.

    1996-01-01

    The dosimetry is the dose measure imparted by the energy from the ionizing radiation to the matter. The dosemeters is the means used for the determination of such a dose. Diverse dosimetric classes exist, this classification depends in essence of the energy involved in the irradiation process and of its application necessity. It is as well as in radiological protection movie dosemeter is used, and TLD, in the calibration of units, as those of cobalt, the ionization cameras are used, in the detection of superficial contamination the accountants Geiger Muller and proportional etc. The transfer dosimeter Alanine/ESR is used, object of the present work, is characterized because after reading the registered dose, the information is conserved and it can be transferred and read in any team of ESR. Likewise the following dose that is imparted will be added to the previous one registered, this indicates that the dosemeters is of integral character. In the spectra taken ESR, it is determined that the integral double or area under the curve of the spectrum ESR is proportional to the concentration of free radicals generated by the radiation ionization and in turn this concentration is proportional to the dose received by the pills; in last, these proportionality relationships take to that the area under the curve of the spectrum main ESR is proportional to the radiation dose received by the alanine dosemeters. This dosemeter seeks to be an economic alternative that it will lend the calibration service that today offers the ionization Cameras or the acrylic red industrial dosemeters

  16. ESR as a method for the characterization of alluvial sediments

    International Nuclear Information System (INIS)

    Tissoux, H.; Voinchet, P.; Lacquement, F.; Despriée, J.

    2015-01-01

    The possibility of using the parameters involved in the ESR dating of optically bleached quartz grains in a purpose of source determination was checked. In that aim, samples previously taken in different sedimentary formations of the Middle Loire Basin (Central France) and dated by ESR have been observed. First discrimination was made using the thorium and potassium content in the sediments obtained by gamma spectrometry. The plot of these 119 data on the Th/K Schlumberger diagram clearly demonstrated that it was possible to discriminate the clays associations included in the sediment from which the dated quartz are extracted. Clay's nature could then be indicative of the geological nature of the substratum of rivers from their sources. Second discrimination was made using the ESR intensities calculated from Al, Ti–H and Ti–Li paramagnetic centres on 18 samples. It appears that the combination of the non-bleachable aluminum trap (DAT) saturation intensity and the Ti–H/Ti–Li ratio intensities make possible the discrimination of the two main sources of the sediment: Massif Central and Paris Basin. More deeply, The Ti/OBAT (Optically bleachable aluminum traps) intensities made possible the discrimination of quartz grains of different geological sources or with different geothermal history within the Massif Central group. - Highlights: • We used ESR and gamma spectrometry for source determination of alluvial quartz grains. • Th/K ratio distinguishes sediments from rivers flowing in various geological contexts. • Al, Ti–H and Ti–Li ESR centers discriminate quartz of different geological sources.

  17. Electron spin resonance (ESR) studies on irradiated cocoa beans and niger seeds

    International Nuclear Information System (INIS)

    Mangaonkar, S.R.; Natarajan, V.; Sastry, M.D.; Desai, S.R.P.; Kulkarni, P.R.

    1997-01-01

    Electron spin resonance (ESR) spectra of irradiated (10kGy) and unirradiated cocoa beans and niger seeds have been compared. Unirradiated cocoa beans failed to give any ESR signal, whereas after irradiation (10kGy) an ESR signal at g = 2.0042 was observed. However, ESR signals are given by both irradiated and unirradiated niger seeds. The intensity of signal was found to be dose-dependent up to 10kGy for both seeds. The signals were stable up to 180 days in both cases. The results indicate the possibility of using ESR for distinguishing between irradiated and unirradiated cocoa beans but not for niger seeds

  18. Final report: High current capacity high temperature superconducting film based tape for high field magnets

    International Nuclear Information System (INIS)

    Ying Xin

    2000-01-01

    The primary goal of the program was to establish the process parameters for the continuous deposition of high quality, superconducting YBCO films on one meter lengths of buffered RABiTS tape using MOCVD and to characterize the potential utility of the resulting tapes in high field magnet applications

  19. High School Students' Representations and Understandings of Electric Fields

    Science.gov (United States)

    Cao, Ying; Brizuela, Bárbara M.

    2016-01-01

    This study investigates the representations and understandings of electric fields expressed by Chinese high school students 15 to 16 years old who have not received high school level physics instruction. The physics education research literature has reported students' conceptions of electric fields post-instruction as indicated by students'…

  20. Radiofrequency solutions in clinical high field magnetic resonance

    NARCIS (Netherlands)

    Andreychenko, A.

    2013-01-01

    Magnetic resonance imaging (MRI) and spectroscopy (MRS) benefit from the sensitivity gain at high field (≥7T). However, high field brings also certain challenges associated with growing frequency and spectral dispersion. Frequency growth results in degraded performance of large volume radiofrequency

  1. A field-sweep/field-lock system for superconducting magnets--Application to high-field EPR.

    Science.gov (United States)

    Maly, Thorsten; Bryant, Jeff; Ruben, David; Griffin, Robert G

    2006-12-01

    We describe a field-lock/field-sweep system for the use in superconducting magnets. The system is based on a commercially available field mapping unit and a custom designed broad-band 1H NMR probe. The NMR signal of a small water sample is used in a feedback loop to set and control the magnetic field to high accuracy. The current instrumental configuration allows field sweeps of +/-0.4 T and a resolution of up to 10(-5) T (0.1 G) and the performance of the system is demonstrated in a high-field electron paramagnetic resonance (EPR) application. The system should also be of utility in other experiments requiring precise and reproducible sweeps of the magnetic field such as DNP, ENDOR or PELDOR.

  2. A Field-Sweep/Field-Lock System for Superconducting Magnets-Application to High-Field EPR

    Science.gov (United States)

    Maly, Thorsten; Bryant, Jeff; Ruben, David; Griffin, Robert G.

    2007-01-01

    We describe a field-lock/field-sweep system for the use in superconducting magnets. The system is based on a commercially available field mapping unit and a custom designed broad-band 1H-NMR probe. The NMR signal of a small water sample is used in a feedback loop to set and control the magnetic field to high accuracy. The current instrumental configuration allows field sweeps of ± 0.4 T and a resolution of up to 10-5 T (0.1 G) and the performance of the system is demonstrated in a high-field electron paramagnetic resonance (EPR) application. The system should also be of utility in other experiments requiring precise and reproducible sweeps of the magnetic field such as DNP, ENDOR or PELDOR. PMID:17027306

  3. Large field-of-view transmission line resonator for high field MRI

    DEFF Research Database (Denmark)

    Zhurbenko, Vitaliy; Johannesson, Kristjan Sundgaard; Boer, Vincent

    2016-01-01

    Transmission line resonators is often a preferable choice for coils in high field magnetic resonance imaging (MRI), because they provide a number of advantages over traditional loop coils. The size of such resonators, however, is limited to shorter than half a wavelength due to high standing wave....... Achieved magnetic field distribution is compared to the conventional transmission line resonator. Imaging experiments are performed using 7 Tesla MRI system. The developed resonator is useful for building coils with large field-of-view....

  4. High field, low current operation of engineering test reactors

    International Nuclear Information System (INIS)

    Schwartz, J.; Cohn, D.R.; Bromberg, L.; Williams, J.E.C.

    1987-06-01

    Steady state engineering test reactors with high field, low current operation are investigated and compared to high current, lower field concepts. Illustrative high field ETR parameters are R = 3 m, α ∼ 0.5 m, B ∼ 10 T, β = 2.2% and I = 4 MA. For similar wall loading the fusion power of an illustrative high field, low current concept could be about 50% that of a lower field device like TIBER II. This reduction could lead to a 50% decrease in tritium consumption, resulting in a substantial decrease in operating cost. Furthermore, high field operation could lead to substantially reduced current drive requirements and cost. A reduction in current drive source power on the order of 40 to 50 MW may be attainable relative to a lower field, high current design like TIBER II implying a possible cost savings on the order of $200 M. If current drive is less efficient than assumed, the savings could be even greater. Through larger β/sub p/ and aspect ratio, greater prospects for bootstrap current operation also exist. Further savings would be obtained from the reduced size of the first wall/blanket/shield system. The effects of high fields on magnet costs are very dependent on technological assumptions. Further improvements in the future may lie with advances in superconducting and structural materials

  5. Periodic permanent magnet focusing system with high peak field

    International Nuclear Information System (INIS)

    Zhang Hong; Liu Weiwei; Bai Shuxin; Chen Ke

    2008-01-01

    In this study, hybrid periodic permanent magnet (PPM) system is studied, which has high axial magnetic field and low magnetic leakage. By simulation computation, some laws of magnetic field distribution vs. structure dimensions were obtained. A hybrid PPM is designed and constructed whose peak field reaches 0.6 T. The factors inducing discrepancies between computational results and practical measurements are analyzed. The magnetic field distribution is very sensitive to the variations of constructional parameters. Construction accuracy greatly influences the magnetic field distribution. Research results obtained here are potentially valuable for future work

  6. Analysis of a high brightness photo electron beam with self field and wake field effects

    International Nuclear Information System (INIS)

    Parsa, Z.

    1991-01-01

    High brightness sources are the basic ingredients in the new accelerator developments such as Free-Electron Laser experiments. The effects of the interactions between the highly charged particles and the fields in the accelerating structure, e.g. R.F., Space charge and Wake fields can be detrimental to the beam and the experiments. We present and discuss the formulation used, some simulation and results for the Brookhaven National Laboratory high brightness beam that illustrates effects of the accelerating field, space charge forces (e.g. due to self field of the bunch), and the wake field (e.g. arising from the interaction of the cavity surface and the self field of the bunch)

  7. High gain requirements and high field Tokamak experiments

    International Nuclear Information System (INIS)

    Cohn, D.R.

    1994-01-01

    Operation at sufficiently high gain (ratio of fusion power to external heating power) is a fundamental requirement for tokamak power reactors. For typical reactor concepts, the gain is greater than 25. Self-heating from alpha particles in deuterium-tritium plasmas can greatly reduce ητ/temperature requirements for high gain. A range of high gain operating conditions is possible with different values of alpha-particle efficiency (fraction of alpha-particle power that actually heats the plasma) and with different ratios of self heating to external heating. At one extreme, there is ignited operation, where all of the required plasma heating is provided by alpha particles and the alpha-particle efficiency is 100%. At the other extreme, there is the case of no heating contribution from alpha particles. ητ/temperature requirements for high gain are determined as a function of alpha-particle heating efficiency. Possibilities for high gain experiments in deuterium-tritium, deuterium, and hydrogen plasmas are discussed

  8. High magnetic field {mu}SR instrument scientific case

    Energy Technology Data Exchange (ETDEWEB)

    Amato, A

    2005-10-15

    In order to gain more insight into the specific behavior of materials, it is often necessary to perform measurements as a function of different external parameters. Despite its high sensitivity to internal fields, this simple observation also applies for the {mu}SR technique. The most common parameter which can be tuned during an experiment is the sample temperature. By using a range of cryostats, temperatures between 0.02 and 900 K can be covered at the PSI {mu}SR Facility. On the other hand, and by using high-energy muons, pressures as high as 10'000 bars can nowadays be reached during {mu}SR experiments. As will be demonstrated in the following Sections, the magnetic field is an additional external parameter playing a fundamental role when studying the ground state properties of materials in condensed matter physics and chemistry. However, the availability of high magnetic fields for {mu}SR experiments is still rather limited. Hence, if on one hand the high value of the gyromagnetic ratio of the muon provides the high magnetic sensitivity of the method, on the other hand it can lead to very high muon-spin precession frequencies when performing measurements in applied fields (the muon-spin precession frequency in a field of 1 Tesla s 135.5 MHz). Consequently, the use of ultra-fast detectors and electronics is mandatory when measuring in magnetic fields exceeding 1 Tesla. If such fields are very intense when compared to the Earth magnetic field < 10{sup -4} Tesla), the energy associated with them is still modest in view of the thermal energy. Hence, the Zeeman energy splitting of a free electron in a magnetic field of 1 Tesla corresponds to a thermal energy as low as 0.67 Kelvin. It is worth mentioning that nowadays magnetic fields of the order of 10 to 15 Tesla are quite common in condensed matter laboratories and have opened up vast new exciting experimental possibilities. (author)

  9. High magnetic field μSR instrument scientific case

    International Nuclear Information System (INIS)

    Amato, A.

    2005-10-01

    In order to gain more insight into the specific behavior of materials, it is often necessary to perform measurements as a function of different external parameters. Despite its high sensitivity to internal fields, this simple observation also applies for the μSR technique. The most common parameter which can be tuned during an experiment is the sample temperature. By using a range of cryostats, temperatures between 0.02 and 900 K can be covered at the PSI μSR Facility. On the other hand, and by using high-energy muons, pressures as high as 10'000 bars can nowadays be reached during μSR experiments. As will be demonstrated in the following Sections, the magnetic field is an additional external parameter playing a fundamental role when studying the ground state properties of materials in condensed matter physics and chemistry. However, the availability of high magnetic fields for μSR experiments is still rather limited. Hence, if on one hand the high value of the gyromagnetic ratio of the muon provides the high magnetic sensitivity of the method, on the other hand it can lead to very high muon-spin precession frequencies when performing measurements in applied fields (the muon-spin precession frequency in a field of 1 Tesla s 135.5 MHz). Consequently, the use of ultra-fast detectors and electronics is mandatory when measuring in magnetic fields exceeding 1 Tesla. If such fields are very intense when compared to the Earth magnetic field -4 Tesla), the energy associated with them is still modest in view of the thermal energy. Hence, the Zeeman energy splitting of a free electron in a magnetic field of 1 Tesla corresponds to a thermal energy as low as 0.67 Kelvin. It is worth mentioning that nowadays magnetic fields of the order of 10 to 15 Tesla are quite common in condensed matter laboratories and have opened up vast new exciting experimental possibilities. (author)

  10. HIFI - a dedicated HIgh-FIeld diffraction and spectroscopy instrument

    International Nuclear Information System (INIS)

    Steffens, P.; Enderle, M.; Boehm, M.; Roux, S.

    2011-01-01

    The outstanding scientific impact of single-crystal neutron diffraction and spectroscopy in steady state vertical magnetic fields up to 15 T (17 T without dilution fringe) is reflected in numerous high-profile publications. Magnetic fields 30 T - 35 T in vertical geometry allow to address enigmatic questions without equivalence at lower fields. The constraints implied by such magnetic fields demand a specially designed dedicated instrument. Since the vertical field geometry is crucial for single-crystal diffraction as well as spectroscopy, the solid angle of scattered neutrons is restricted, and a high-flux reactor is best suited to host a corresponding instrument. We propose a world-wide unique versatile instrument for diffraction and spectroscopy in vertical steady fields of 30 T. (authors)

  11. Advanced measurements and techniques in high magnetic fields

    International Nuclear Information System (INIS)

    Campbell, L.J.; Rickel, D.G.; Lacerda, A.H.; Kim, Y.

    1997-01-01

    This is the final report of a one-year, Laboratory-Directed Research and Development (LDRD) project at the Los Alamos National Laboratory (LANL). High magnetic fields present a unique environment for studying the electronic structure of materials. Two classes of materials were chosen for experiments at the national high Magnetic Field Laboratory at Los Alamos: highly correlated electron systems and semiconductors. Magnetotransport and thermodynamic experiments were performed on the renormalized ground states of highly correlated electron systems (such as heavy fermion materials and Kondo insulators) in the presence of magnetic fields that are large enough to disrupt the many-body correlations. A variety of optical measurements in high magnetic fields were performed on semiconductor heterostructures including GaAs/AlGaAs single heterojunctions (HEMT structure), coupled double quantum wells (CDQW), asymmetric coupled double quantum wells (ACDQW), multiple quantum wells and a CdTe single crystal thin film

  12. Improving Magnet Designs With High and Low Field Regions

    DEFF Research Database (Denmark)

    Bjørk, Rasmus; Bahl, Christian Robert Haffenden; Smith, Anders

    2011-01-01

    A general scheme for increasing the difference in magnetic flux density between a high and a low magnetic field region by removing unnecessary magnet material is presented. This is important in, e.g., magnetic refrigeration where magnet arrays have to deliver high field regions in close proximity...... to low field regions. Also, a general way to replace magnet material with a high permeability soft magnetic material where appropriate is discussed. As an example, these schemes are applied to a two dimensional concentric Halbach cylinder design resulting in a reduction of the amount of magnet material...

  13. Design of a high field uniformity electromagnet for Penning trap

    International Nuclear Information System (INIS)

    Itteera, Janvin; Singh, Kumud; Teotia, Vikas; Ukarde, Priti; Malhotra, Sanjay; Taly, Y.K.; Joshi, Manoj; Rao, Pushpa

    2013-01-01

    An ion trap (Penning trap) facility is being developed at BARC for spectroscopy studies. This requires the design of an iron core electromagnet capable of generating high magnetic fields (∼1.7T) at the centre of an 88 mm long air gap. This electromagnet provides the requisite dipole magnetic field which when superimposed on the electrostatic quadrupoles ensures a stable trapping of ions. To conduct high precision spectroscopy studies, we need to ensure a high degree of magnetic field uniformity ( 3 volume (Trap zone). Various pole shoe profiles were studied and modelled, FEM simulation of the same were conducted to compute the magnetic field intensity and field uniformity. Owing to the large air gap and requirement of high field intensity in the GFR, the exciting coils need to handle high current densities, which require water cooled systems. Double Pan-Cake coil design is selected for powering the magnet. Electrical, thermal and hydraulic designs of the coils are completed and a prototype double pancake coil was fabricated and tested for verifying the electrical and thermal parameter. The spatial field homogeneity is achieved by shimming the pole tip. Temporal stability of magnet requires a highly stable power supply for exciting the coils and its stability class is derived from FEM simulations. This paper discusses the electromagnetic design and development of the penning trap magnet being developed at BARC. (author)

  14. High electric field conduction in low-alkali boroaluminosilicate glass

    Science.gov (United States)

    Dash, Priyanka; Yuan, Mengxue; Gao, Jun; Furman, Eugene; Lanagan, Michael T.

    2018-02-01

    Electrical conduction in silica-based glasses under a low electric field is dominated by high mobility ions such as sodium, and there is a transition from ionic transport to electronic transport as the electric field exceeds 108 V/m at low temperatures. Electrical conduction under a high electric field was investigated in thin low-alkali boroaluminosilicate glass samples, showing nonlinear conduction with the current density scaling approximately with E1/2, where E is the electric field. In addition, thermally stimulated depolarization current (TSDC) characterization was carried out on room-temperature electrically poled glass samples, and an anomalous discharging current flowing in the same direction as the charging current was observed. High electric field conduction and TSDC results led to the conclusion that Poole-Frenkel based electronic transport occurs in the mobile-cation-depleted region adjacent to the anode, and accounts for the observed anomalous current.

  15. Probing High Temperature Superconductors with Magnetometry in Ultrahigh Magnetic Fields

    Energy Technology Data Exchange (ETDEWEB)

    Li, Lu [Univ. of Michigan, Ann Arbor, MI (United States)

    2017-07-26

    The objective of this research is to investigate the high-field magnetic properties of high temperature superconductors, materials that conduct electricity without loss. A technique known as high-resolution torque magnetometry that was developed to directly measure the magnetization of high temperature superconductors. This technique was implemented using the 65 Tesla pulsed magnetic field facility that is part of the National High Magnetic Field Laboratory at Los Alamos National Laboratory. This research addressed unanswered questions about the interplay between magnetism and superconductivity, determine the electronic structure of high temperature superconductors, and shed light on the mechanism of high temperature superconductivity and on potential applications of these materials in areas such as energy generation and power transmission. Further applications of the technology resolve the novel physical phenomena such as correlated topological insulators, and spin liquid state in quantum magnets.

  16. ESR accident dosimetry using medicine tablets coated with sugar

    International Nuclear Information System (INIS)

    Kai, A.; Miki, T.; Ikeya, M.

    1990-01-01

    Properties of radiation-induced radicals in medicine tablets were investigated using electron spin resonance (ESR). A sharp ESR signal sensitive to gamma ray irradiation was observed in the sugar coating part of the tablets. The signal has anisotropic g values of g 1 = 2.0009, g 2 = 2.0007 and g 3 = 2.0002. The signal grows linearly with dose at least up to about 20 Gy. No fading was observed at room temperature even when exposed to sunlight. The dose to artificially irradiated tablets was estimated using the signal intensity and a previously determined calibration curve. The signal in sugar coated tablets can be utilised for dose measurements. In particular, the wide distribution of sugar coated tablets allows the use of the tablets as accident dosemeters. (author)

  17. The ESR dating of the Nanjing Homo erectus stratigraphy

    International Nuclear Information System (INIS)

    Chen Tiemei; Wu En; Yang Quan; Hu Yanqiu

    1997-01-01

    Five fossil tooth enamel samples collected from the stratum of the Nanjing Homo erectus were ESR dated. The average age is 355 +- 42 ka, based on the early uranium-uptake model. Additional uranium series measurement of fossil teeth confirms the appropriateness of the early uranium-uptake model for these ESR samples. Considering also the uranium-series ages of two calcite samples from the flow stone covering the fossil-containing stratum, an age value of 350 +- 50 ka for the Nanjing Homo erectus stratum is evaluated, which means that the Nanjing Homo erectus appeared in the late stage of Peking Man and also in the stage of human evolution earlier than Hexian Homo erectus

  18. Lyoluminescence and ESR correlation studies of trehalose dihydrate

    Energy Technology Data Exchange (ETDEWEB)

    Raman, Anand E-mail: anandr@apsara.barc.ernet.in; Oommen, Issac K.; Gundu Rao, T.K.; Sharma, D.N

    2002-07-01

    ESR studies of irradiated lyoluminescence (LL) phosphor, trehalose dihydrate showed a linear free radical growth up to a dose of 11 kGy. The LL output measured under oxygen equilibrated conditions showed an extension of the dosimetric response from 0.6 to 6 kGy. ESR spectral analysis indicates the formation of two radical species viz., 'a' and 'b' and their involvement in the LL process. The estimated free radical concentrations of radicals 'a' and 'b' were found to be 6.81x10{sup 15} and 1.35x10{sup 16} g{sup -1}, respectively, for a gamma dose of 10.8 kGy.

  19. ESR studies of the radiation effects on polystyrene

    International Nuclear Information System (INIS)

    Garrett, R.W.; O'Donnell, J.H.; Pomery, P.J.

    1976-01-01

    The aim of this work was to investigate the polystyrene system (both pure and commercial samples) to elucidate the type and percentage of each paramagnetic species upon exposure to various irradiation doses. The size of dose plays a vital role in the type of spectra obtained. Upon irradiation in vacuo, polystyrene displays ESR spectra which are basically triplet in character but the line spacing and intensities of components are observed to depend on the magnitude of the irradiation dose. G value for the total radicals present and for the individual species present as a function of dose have been obtained. The relative concentration of each paramagnetic species has been determined through computer simulation of the observed ESR spectra. The relative stability of the different species with respect to temperature is discussed. The results for deuterated polystyrene is used to support those obtained for the unsubstituted polystyrene system. (author)

  20. ESR spectroscopic investigations of the radiation-grafting of fluoropolymers

    Energy Technology Data Exchange (ETDEWEB)

    Huebner, G; Roduner, E [University of Stuttgart (Germany); Brack, H P; Scherer, G G [Paul Scherrer Inst. (PSI), Villigen (Switzerland)

    1999-08-01

    ESR spectroscopic investigations have clarified the influence of several preparative parameters on the reaction rates and yields obtained in the radiation-grafting method used at PSI to prepare proton-conducting polymer membranes. At a given irradiation dose, a higher concentration of reactive radical sites was detected in ETFE films than in FEP films. This higher concentration explains the higher grafting levels and rates of the ETFE films found in our previous grafting experiments. Taken together, the in-situ ESR experiments and grafting experiments show that the rates of disappearance of radical species and grafting rates and final grafting levels depend strongly on the reaction temperature and the oxygen content of the system. Average grafted chain lengths were calculated to contain about 1,000 monomer units. (author) 2 figs., 4 refs.

  1. Dose determination in irradiated chicken meat by ESR method

    International Nuclear Information System (INIS)

    Polat, M.

    1996-01-01

    In this work, the properties of the radicals produced in chicken bones have been investigated by ESR technique to determine the amount of dose applied to the chicken meats during the food irradiation. For this goal, the drumsticks from 6-8 weeks old chickens purchased from a local market were irradiated at dose levels of 0; 2; 4; 6; 8 and 10 kGy. Then, the ESR spectra of the powder samples prepared from the bones of the drumsticks have been investigated. Unirradiated chicken bones have been observed to show a weak ESR signal of single line character. CO-2 ionic radicals of axial symmetry with g=1.9973 and g=2.0025 were observed to be produced in irradiated samples which would give rise to a three peaks ESR spectrum. In addition, the signal intensities of the samples were found to depend linearly on the irradiation dose in the dose range of 0-10 kGy. The powder samples prepared from chicken leg bones cleaned from their meats and marrow and irradiated at dose levels of 1, 2, 3, 4, 5, 6, B, 10, 12,14, 16, 1B, 20 and 22 kGy were used to get the dose-response curve. It was found that this curve has biphasic character and that the dose yield was higher in the 12-1B kGy dose range and a decrease appears in this curve over 18 kGy. The radical produced in the bones were found to be the same whether the irradiation was performed after stripping the meat and removing the marrow from the bone or before the stripping. The ESR spectra of both irradiated and non irradiated samples were investigated in the temperature range of 100 K-450 K and changes in the ESR spectra of CO-2 radical have been studied. For non irradiated samples (controls). the signal intensities were found to decrease when the temperature was increased. The same investigation has been carried out for irradiated samples and it was concluded that the signal intensities relative to the peaks of the radical spectrum increase in the temperature range of 100 K-330 K, then they decrease over 330 K. The change in the

  2. The Uncertainty estimation of Alanine/ESR dosimetry

    International Nuclear Information System (INIS)

    Kim, Bo Rum; An, Jin Hee; Choi, Hoon; Kim, Young Ki

    2008-01-01

    Machinery, tools and cable etc are in the nuclear power plant which environment is very severe. By measuring actual dose, it needs for extending life expectancy of the machinery and tools and the cable. Therefore, we estimated on dose (gamma ray) of Wolsong nuclear power division 1 by dose estimation technology for three years. The dose estimation technology was secured by ESR(Electron Spin Resonance) dose estimation using regression analysis. We estimate uncertainty for secure a reliability of results. The uncertainty estimation will be able to judge the reliability of measurement results. The estimation of uncertainty referred the international unified guide in order; GUM(Guide to the Expression of Uncertainty in Measurement). It was published by International Standardization for Organization (ISO) in 1993. In this study the uncertainty of e-scan and EMX those are ESR equipment were evaluated and compared. Base on these results, it will improve the reliability of measurement

  3. High pressure apparatus transport properties study in high magnetic field

    Czech Academy of Sciences Publication Activity Database

    Honda, F.; Sechovský, V.; Mikulina, O.; Kamarád, Jiří; Alsmadi, A. M.; Nakotte, H.; Lacerda, A. H.

    2002-01-01

    Roč. 16, 20, 21 & 22 (2002), s. 3330-3333 ISSN 0217-9792 R&D Projects: GA ČR GP202/01/D045; GA ČR GA202/00/1217; GA MŠk ME 165 Grant - others:NSF(XX) DMR-0094241 Institutional research plan: CEZ:AV0Z1010914 Keywords : high-pressure apparatus Subject RIV: BM - Solid Matter Physics ; Magnetism Impact factor: 0.604, year: 2002

  4. High-field EPR spectroscopy of thermal donors in silicon

    DEFF Research Database (Denmark)

    Dirksen, R.; Rasmussen, F.B.; Gregorkiewicz, T.

    1997-01-01

    Thermal donors generated in p-type boron-doped Czochralski-grown silicon by a 450 degrees C heat treatment have been studied by high-field magnetic resonance spectroscopy. In the experiments conducted at a microwave frequency of 140 GHz and in a magnetic field of approximately 5 T four individual...

  5. The Pioneer 11 high-field fluxgate magnetometer

    Science.gov (United States)

    Acuna, M. H.; Ness, N. F.

    1973-01-01

    The High Field Fluxgate Magnetometer Experiment flow aboard the Pioneer 11 spacecraft to investigate Jupiter's magnetic field is described. The instrument extends the spacecraft's upper limit measurement capability by more than an order of magnitude to 17.3 gauss with minimum power and volume requirements.

  6. High-field magnetization of UCuGe single crystal

    Czech Academy of Sciences Publication Activity Database

    Andreev, Alexander V.; Mushnikov, N. V.; Gozo, T.; Honda, F.; Sechovský, V.; Prokeš, K.

    346-347, - (2004), s. 132-136 ISSN 0921-4526 R&D Projects: GA ČR GA202/02/0739 Institutional research plan: CEZ:AV0Z1010914 Keywords : uranium intermetallics * UCuGe * high fields * magnetic anisotropy * field-induced phase transition Subject RIV: BM - Solid Matter Physics ; Magnetism Impact factor: 0.679, year: 2004

  7. High-Redshift Radio Galaxies from Deep Fields

    Indian Academy of Sciences (India)

    2016-01-27

    Jan 27, 2016 ... High-Redshift Radio Galaxies from Deep Fields ... Here we present results from the deep 150 MHz observations of LBDS-Lynx field, which has been imaged at 327, ... Articles are also visible in Web of Science immediately.

  8. High field Moessbauer spectroscopy using water-cooled magnets

    Energy Technology Data Exchange (ETDEWEB)

    Chappert, J.; Regnard, J. R.

    1974-07-01

    A high field Moessbauer spectrometer using a Bitter coil producing fields of up to 155 kOe is described. Problems encountered in the design of this type of equipment are discussed and preliminary results demonstrating the performance of the spectrometer are presented.

  9. Ultra high energy cosmic rays and magnetic fields

    Energy Technology Data Exchange (ETDEWEB)

    Stanev, Todor; Engel, Ralph; Alvarez-Muniz, Jaime; Seckel, David

    2002-07-01

    We follow the propagation of ultra high energy protons in the presence of random and regular magnetic fields and discuss some of the changes in the angular and energy distributions of these particles introduced by the scattering in the magnetic fields.

  10. Ultra high energy cosmic rays and magnetic fields

    International Nuclear Information System (INIS)

    Stanev, Todor; Engel, Ralph; Alvarez-Muniz, Jaime; Seckel, David

    2002-01-01

    We follow the propagation of ultra high energy protons in the presence of random and regular magnetic fields and discuss some of the changes in the angular and energy distributions of these particles introduced by the scattering in the magnetic fields

  11. High mobility polymer gated organic field effect transistor using zinc ...

    Indian Academy of Sciences (India)

    Organic thin film transistors were fabricated using evaporated zinc phthalocyanine as the active layer. Parylene film ... At room temperature, these transistors exhibit p-type conductivity with field-effect ... Keywords. Organic semiconductor; field effect transistor; phthalocyanine; high mobility. ... The evaporation rate was kept at ...

  12. The nuclear physics program at SIS/ESR

    International Nuclear Information System (INIS)

    Henning, W.

    1991-01-01

    The present workshop discusses the physics program to be addressed with the new photon spectrometer TAPS. Part of this program will be carried out at the new accelerator facility SIS/ESR at GSI Darmstadt. To put the TAPS activities at SIS into perspective, an overview is given in the following discussing the new GSI facility, the research program under consideration and the various experimental facilities besides TAPS to carry out these studies. (orig.)

  13. Rapid screening for anthocyanins in cane sugars using ESR spectroscopy.

    Science.gov (United States)

    Thamaphat, Kheamrutai; Goodman, Bernard A; Limsuwan, Pichet; Smith, Siwaporn Meejoo

    2015-03-15

    Anthocyanin, which is soluble in water and released into sugar steam during extraction, was investigated in this study. The anthocyanin content in refined sugar, plantation white sugar, soft brown sugar and raw sugar was determined using electron spin resonance (ESR) spectroscopy, which was operated at room temperature, and compared with spectra from standard anthocyanin. The ESR spectra of red and violet anthocyanins was predominantly g ≈ 2.0055, which corresponded to an unpaired electron located in the pyrylium ring. Signals for Fe(III) and Mn(II), which naturally occur in plants, were found in raw sugar, soft brown sugar and standard anthocyanin but were absent from refined sugar and plantation white sugar due to the refining process. In addition, the ESR results were correlated with the apparent colour of the sugar, which was determined using the method of the International Commission for Uniform Methods of Sugar Analysis and inductively coupled plasma optical emission spectroscopy. Copyright © 2014 Elsevier Ltd. All rights reserved.

  14. Estimation of dose in irradiated chicken bone by ESR method

    International Nuclear Information System (INIS)

    Tanabe, Hiroko; Hougetu, Daisuke

    1998-01-01

    The author studied the conditions needed to routinely estimate the radiation dose in chicken bone by repeated re-irradiation and measuring ESR signals. Chicken meat containing bone was γ-irradiated at doses of up to 3kGy, accepted as the commercially used dose. The results show that points in sample preparation and ESR measurement are as follows: Both ends of bone are cut off and central part of compact bone is used for experiment. To obtain accurate ESR spectrum, marrow should be scraped out completely. Sample bone fragments of 1-2mm particle size and ca.100mg are recommended to obtain stable and maximum signal. In practice, by re-irradiating up to 5kGy and extrapolating data of the signal intensity to zero using linear regression analysis, radiation dose is estimated. For example, in one experiment, estimated doses of chicken bones initially irradiated at 3.0kGy, 1.0kGy, 0.50kGy and 0.25kGy were 3.4kGy, 1.3kGy, 0.81kGy and 0.57kGy. (author)

  15. An ESR study on biological dosimeters: Human hair

    International Nuclear Information System (INIS)

    Colak, Seyda; Ozbey, Turan

    2011-01-01

    In the present work, characteristic features of the radicals found in untreated, gamma and UV-irradiated and mechanical damaged human hair samples were investigated by ESR spectroscopy. Heights of the resonance peaks measured with respect to the spectrum base line were used to monitor microwave power, dose-response, storage time and temperature dependent kinetic features of the radical species contributing to the formation of recorded experimental ESR spectra. Peak heights and g-values (2.0037-2.0052) determined from recorded spectra of hair were color dependent with ΔHpp-0.47 mT. The act of cutting hair samples gene rates sulfur centered radicals which are found in the a-keratin structure of hair. The variations of the peak heights with temperature were related with the water content found in the hair samples. In the 6-1100 Gy dose range, a linear + quadratic dose-response curve was recorded for hair and the mean radiation yield (G mean ) was calculated to be 0.4. The gamma radiation induced radicals were stable for a several hours at room temperature storage conditions. Based on these findings it was concluded that human hair samples could be used as biological/personnel dosimeters and that ESR spectroscopy could be successfully used as a potential technique for monitoring its dosimetric behaviours.

  16. Overlay control methodology comparison: field-by-field and high-order methods

    Science.gov (United States)

    Huang, Chun-Yen; Chiu, Chui-Fu; Wu, Wen-Bin; Shih, Chiang-Lin; Huang, Chin-Chou Kevin; Huang, Healthy; Choi, DongSub; Pierson, Bill; Robinson, John C.

    2012-03-01

    Overlay control in advanced integrated circuit (IC) manufacturing is becoming one of the leading lithographic challenges in the 3x and 2x nm process nodes. Production overlay control can no longer meet the stringent emerging requirements based on linear composite wafer and field models with sampling of 10 to 20 fields and 4 to 5 sites per field, which was the industry standard for many years. Methods that have emerged include overlay metrology in many or all fields, including the high order field model method called high order control (HOC), and field by field control (FxFc) methods also called correction per exposure. The HOC and FxFc methods were initially introduced as relatively infrequent scanner qualification activities meant to supplement linear production schemes. More recently, however, it is clear that production control is also requiring intense sampling, similar high order and FxFc methods. The added control benefits of high order and FxFc overlay methods need to be balanced with the increased metrology requirements, however, without putting material at risk. Of critical importance is the proper control of edge fields, which requires intensive sampling in order to minimize signatures. In this study we compare various methods of overlay control including the performance levels that can be achieved.

  17. Design of High Field Solenoids made of High Temperature Superconductors

    Energy Technology Data Exchange (ETDEWEB)

    Bartalesi, Antonio; /Pisa U.

    2010-12-01

    This thesis starts from the analytical mechanical analysis of a superconducting solenoid, loaded by self generated Lorentz forces. Also, a finite element model is proposed and verified with the analytical results. To study the anisotropic behavior of a coil made by layers of superconductor and insulation, a finite element meso-mechanic model is proposed and designed. The resulting material properties are then used in the main solenoid analysis. In parallel, design work is performed as well: an existing Insert Test Facility (ITF) is adapted and structurally verified to support a coil made of YBa{sub 2}Cu{sub 3}O{sub 7}, a High Temperature Superconductor (HTS). Finally, a technological winding process was proposed and the required tooling is designed.

  18. Beneficial use of off-specification fly ashes to increase the shear strength and stiffness of expansive soil-rubber (ESR) mixtures.

    Science.gov (United States)

    2011-07-01

    The use of off-specification fly ashes to increase the shear strength and stiffness of an expansive soil-rubber (ESR) mixture is investigated systematically in this study. The off-specification fly ashes used include a high-sulfur content and a high-...

  19. Generation of high magnetic fields using superconducting magnets

    International Nuclear Information System (INIS)

    Kiyoshi, T.; Otsuka, A.; Kosuge, M.; Yuyama, M.; Nagai, H.; Matsumoto, F.

    2006-01-01

    High-field superconducting magnets have opened new frontiers for several kinds of applications, such as fusion reactors, particle accelerators, and nuclear magnetic resonance (NMR) spectrometers. The present record for the highest field in a fully superconducting state is 23.4 T. It was achieved with a combination of NbTi, Nb 3 Sn, and Bi-2212 conductors in 1999. Since high T c (critical temperature) superconductors (HTS) have sufficiently high critical current density even in excess of 30 T, they are promising for use as high-field superconducting magnets. However, several problems still remain to be resolved for practical applications, and the use of HTS coils will be limited to the inner part of a high-field magnet system in the near future. The required technologies to develop a high-field superconducting magnet with a field of up to 28 T have already been established. Such a magnet is certain to provide information to all leading research areas

  20. ESR and X-ray diffraction studies on thin films of poly-3-hexylthiophene: Molecular orientation and magnetic interactions

    International Nuclear Information System (INIS)

    Sugiyama, Keisuke; Kojima, Takashi; Fukuda, Hisashi; Yashiro, Hisashi; Matsuura, Toshihiko; Shimoyama, Yuhei

    2008-01-01

    Poly-3-hexylthiophene (P3HT) thin films were investigated by X-ray diffraction (XRD) and electron spin resonance (ESR) to reveal the film structure and molecular organization. The XRD data showed a diffraction pattern with a plane separation between the planes containing thiophene rings of 16.0 A. Comparison between the XRD patterns of powder and thin films of P3HT suggests that the main chains are folded on the substrate. Angular variation of the line position (g-value) of ESR spectra revealed that thiophene ring of P3HT orients along the substrate normal axis. The ESR linewidth varied by the angular rotation, indicating the one-dimensional spin-chain interactions in the P3HT thin films with a linear network of spin-chains. An organic thin-film transistor (OTFT) with P3HT film as a channel layer was then demonstrated. The P3HT films showed conducting characteristics with holes as carriers. The OTFTs indicated a field-effect mobility of 4.93 x 10 -3 cm 2 /Vs and an on/off ratio of 73 in the accumulation mode

  1. ESR investigation of alkali metal complexes of galvinoxyl-labeled benzo-15-crown-5 in frozen solution

    International Nuclear Information System (INIS)

    Mukai, Kazuo; Iida, Nobuhito; Ishizu, Kazuhiko

    1982-01-01

    A stable galvinoxyl derivative (1) of benzo-15-crown-5 was prepared and the complex formation between the spin labeled crown ether 1 and the alkali metal and ammonium salts was studied by the ESR technique. Existence of the (2:1) complex of 1 with potassium, rubidium, and ammonium salts was confirmed by the observation of the triplet ESR spectra in ethanol rigid matrix at 77K. Essentially the same g- and D-tensor values are observed for all the (2:1) complexes, indicating similar conformation of the ligand mole cule 1. The zero-field splitting parameters (D and E) are calculated on the basis of the spin distribution of 1 and the assumed molecular structures for the (2:1) complex. By comparing the observed D and E parameters with the calculated ones, the structure of the (2:1) complex in ethanol rigid matrix is discussed. On the other hand, the sodium complexes of 1 show a slightly asymmetric single line, suggesting the (1:1) complex formation btween 1 and the sodium salts. No anions (SCN - , Br - , and I - ) have any appreciable effect on the ESR spectra of both the (2:1) and (1:1) complexes. (author)

  2. High-electric-field quantum transport theory for semiconductor superlattices

    International Nuclear Information System (INIS)

    Nguyen Hong Shon; Nazareno, H.N.

    1995-12-01

    Based on the Baym-Kadanoff-Keldysh nonequilibrium Green's functions technique, a quantum transport theory for semiconductor superlattices under high-electric field is developed. This theory is capable of considering collisional broadening, intra-collisional field effects and band transport and hopping regimes simultaneously. Numerical calculations for narrow-miniband superlattices in high electric field, when the hopping regime dominates are in reasonable agreement with experimental results and show a significant deviation from the Boltzmann theory. A semiphenomenological formula for current density in hopping regime is proposed. (author). 60 refs, 4 figs

  3. Field emission from the surface of highly ordered pyrolytic graphite

    Energy Technology Data Exchange (ETDEWEB)

    Knápek, Alexandr, E-mail: knapek@isibrno.cz [Institute of Scientific Instruments of the ASCR, v.v.i., Královopolská 147, Brno (Czech Republic); Sobola, Dinara; Tománek, Pavel [Department of Physics, FEEC, Brno University of Technology, Technická 8, Brno (Czech Republic); Pokorná, Zuzana; Urbánek, Michal [Institute of Scientific Instruments of the ASCR, v.v.i., Královopolská 147, Brno (Czech Republic)

    2017-02-15

    Highlights: • HOPG shreds were created and analyzed in the UHV conditions. • Current-voltage measurements have been done to confirm electron tunneling, based on the Fowler-Nordheim theory. • Surface was characterized by other surface evaluation methods, in particular by: SNOM, SEM and AFM. - Abstract: This paper deals with the electrical characterization of highly ordered pyrolytic graphite (HOPG) surface based on field emission of electrons. The effect of field emission occurs only at disrupted surface, i.e. surface containing ripped and warped shreds of the uppermost layers of graphite. These deformations provide the necessary field gradients which are required for measuring tunneling current caused by field electron emission. Results of the field emission measurements are correlated with other surface characterization methods such as scanning near-field optical microscopy (SNOM) or atomic force microscopy.

  4. Field emission from the surface of highly ordered pyrolytic graphite

    International Nuclear Information System (INIS)

    Knápek, Alexandr; Sobola, Dinara; Tománek, Pavel; Pokorná, Zuzana; Urbánek, Michal

    2017-01-01

    Highlights: • HOPG shreds were created and analyzed in the UHV conditions. • Current-voltage measurements have been done to confirm electron tunneling, based on the Fowler-Nordheim theory. • Surface was characterized by other surface evaluation methods, in particular by: SNOM, SEM and AFM. - Abstract: This paper deals with the electrical characterization of highly ordered pyrolytic graphite (HOPG) surface based on field emission of electrons. The effect of field emission occurs only at disrupted surface, i.e. surface containing ripped and warped shreds of the uppermost layers of graphite. These deformations provide the necessary field gradients which are required for measuring tunneling current caused by field electron emission. Results of the field emission measurements are correlated with other surface characterization methods such as scanning near-field optical microscopy (SNOM) or atomic force microscopy.

  5. Association of ESR1 gene tagging SNPs with breast cancer risk

    Science.gov (United States)

    Dunning, Alison M.; Healey, Catherine S.; Baynes, Caroline; Maia, Ana-Teresa; Scollen, Serena; Vega, Ana; Rodríguez, Raquel; Barbosa-Morais, Nuno L.; Ponder, Bruce A.J.; Low, Yen-Ling; Bingham, Sheila; Haiman, Christopher A.; Le Marchand, Loic; Broeks, Annegien; Schmidt, Marjanka K.; Hopper, John; Southey, Melissa; Beckmann, Matthias W.; Fasching, Peter A.; Peto, Julian; Johnson, Nichola; Bojesen, Stig E.; Nordestgaard, Børge; Milne, Roger L.; Benitez, Javier; Hamann, Ute; Ko, Yon; Schmutzler, Rita K.; Burwinkel, Barbara; Schürmann, Peter; Dörk, Thilo; Heikkinen, Tuomas; Nevanlinna, Heli; Lindblom, Annika; Margolin, Sara; Mannermaa, Arto; Kosma, Veli-Matti; Chen, Xiaoqing; Spurdle, Amanda; Change-Claude, Jenny; Flesch-Janys, Dieter; Couch, Fergus J.; Olson, Janet E.; Severi, Gianluca; Baglietto, Laura; Børresen-Dale, Anne-Lise; Kristensen, Vessela; Hunter, David J.; Hankinson, Susan E.; Devilee, Peter; Vreeswijk, Maaike; Lissowska, Jolanta; Brinton, Louise; Liu, Jianjun; Hall, Per; Kang, Daehee; Yoo, Keun-Young; Shen, Chen-Yang; Yu, Jyh-Cherng; Anton-Culver, Hoda; Ziogoas, Argyrios; Sigurdson, Alice; Struewing, Jeff; Easton, Douglas F.; Garcia-Closas, Montserrat; Humphreys, Manjeet K.; Morrison, Jonathan; Pharoah, Paul D.P.; Pooley, Karen A.; Chenevix-Trench, Georgia

    2009-01-01

    We have conducted a three-stage, comprehensive single nucleotide polymorphism (SNP)-tagging association study of ESR1 gene variants (SNPs) in more than 55 000 breast cancer cases and controls from studies within the Breast Cancer Association Consortium (BCAC). No large risks or highly significant associations were revealed. SNP rs3020314, tagging a region of ESR1 intron 4, is associated with an increase in breast cancer susceptibility with a dominant mode of action in European populations. Carriers of the c-allele have an odds ratio (OR) of 1.05 [95% Confidence Intervals (CI) 1.02–1.09] relative to t-allele homozygotes, P = 0.004. There is significant heterogeneity between studies, P = 0.002. The increased risk appears largely confined to oestrogen receptor-positive tumour risk. The region tagged by SNP rs3020314 contains sequence that is more highly conserved across mammalian species than the rest of intron 4, and it may subtly alter the ratio of two mRNA splice forms. PMID:19126777

  6. ESR Study of PE, HDPE and UHMWPE Irradiated with Ion Beams and Neutrons

    International Nuclear Information System (INIS)

    Reyes-Romero, J.

    2006-01-01

    We report the Electron Spin Resonance (RES) studies on the effects produced by bombarding with accelerated Sulfur ions, Protons and Neutrons on the Polyethylene, PE, (Hostalen and Romanian), ultra-high molecular weight polyethylene, UHMWPE, ( GUR 1050, medical grade Lennite), and high density polyethylene, HDPE, (HDPE-7000F, Polinter de Venezuela, PDVSA). The resonance spectra have been recorded using a Varian E-line-X ESR spectrometer at 100 KHz modulation frequency. In thin films of Polyethylene (Hostalen and UHMWPE) have been irradiated with Sulfur ions, S, accelerated at about 7 MeV/nucleons, and Protons at about 5 MeV/nucleons (IFIN, Romania). Samples of Polyethylene ( HDPE 7000-F) were irradiate with neutrons from a Pu-Be source (flux of 1.19 x 10 6 n/s. cm 2 , 5.65 MeV, IVIC, Venezuela) from 0 to 8 hours in the presence of air and at room temperature (RT). The ESR measurements were performed after a storage time of about 7 months, in air at room temperature. The nature of the free radicals induced by irradiation as well as the dependence of resonance line, resonance line shape and radicals concentration has been studied

  7. Magnetoresistance peculiarities of bismuth wires in high magnetic field

    Energy Technology Data Exchange (ETDEWEB)

    Condrea, E., E-mail: condrea@nano.asm.md [Institute of Electronic Engineering and Nanotechnologies, Academy of Science of Moldova, 2028 Chisinau, Republic of Moldova (Moldova, Republic of); International Laboratory of High Magnetic Fields and Low Temperatures, Gajowicka 95, 51-421 Wroclaw (Poland); Gilewski, A. [International Laboratory of High Magnetic Fields and Low Temperatures, Gajowicka 95, 51-421 Wroclaw (Poland); MagNet, 50-421 Wroclaw (Poland); Nicorici, A. [Institute of Electronic Engineering and Nanotechnologies, Academy of Science of Moldova, 2028 Chisinau, Republic of Moldova (Moldova, Republic of)

    2016-03-11

    Magnetoresistance measurements of Bi wires performed in the magnetic field oriented along the bisector axis revealed unexpected anomalous peaks in a high magnetic field far above the quantum limit of the electrons. By combining a magnetic field and an uniaxial strain, we obtained a modification of the electronic structure; as a result, the quantum limit for light and heavy electrons is changed in a different way. For the case where heavy electrons are in the quantum limit, a correlation between the exit of the lowest Landau level of light electrons and the Lifshitz transition was found. - Highlights: • Glass-coated single-crystalline Bi wires attain high limit of elastic strain of up to 3.0%. • Selective modification of the electronic structure of Bi wires is obtained by combining a high magnetic field and uniaxial strain. • The correlation between the exit of the lowest Landau level of electrons and Lifshitz transition was found.

  8. Magnetoresistance peculiarities of bismuth wires in high magnetic field

    International Nuclear Information System (INIS)

    Condrea, E.; Gilewski, A.; Nicorici, A.

    2016-01-01

    Magnetoresistance measurements of Bi wires performed in the magnetic field oriented along the bisector axis revealed unexpected anomalous peaks in a high magnetic field far above the quantum limit of the electrons. By combining a magnetic field and an uniaxial strain, we obtained a modification of the electronic structure; as a result, the quantum limit for light and heavy electrons is changed in a different way. For the case where heavy electrons are in the quantum limit, a correlation between the exit of the lowest Landau level of light electrons and the Lifshitz transition was found. - Highlights: • Glass-coated single-crystalline Bi wires attain high limit of elastic strain of up to 3.0%. • Selective modification of the electronic structure of Bi wires is obtained by combining a high magnetic field and uniaxial strain. • The correlation between the exit of the lowest Landau level of electrons and Lifshitz transition was found.

  9. Preliminary study on the detection of irradiated food containing bone by ESR spectroscopy

    International Nuclear Information System (INIS)

    Zhao Yongfu; Ha Yiming; Liu Ting; Wang Rongfu; Wang Changbao

    2007-01-01

    Electron spin resonance (ESR) spectroscopy is one of the most effective technique for detection of irradiated food containing bone. It was found that the radiation -induced ESR signal (Spectrum, g factor and peak-to-peak line width AH) in bone before and after irradiation was significantly different and could be easily distinguished from the endogenous ESR signal. Sample preparation studies showed vacuum drying and grinding at frozen temperature was an ideal method. A linear relationship was observed between ESR signal intensity and the absorbed dose (0.3-10.1kGy). It can be proposed that 0.5kGy absorbed doses can be detected by ESR for irradiated food containing bone though detecting sensitivity is very different at the same irradiated dosage with different food such as pork, beef, duck, chicken and fish. The ultimate purpose of this work is to establish a national criterion for detection of irradiated foodstuffs by use of ESR. (authors)

  10. SDSL-ESR-based protein structure characterization

    NARCIS (Netherlands)

    Strancar, J.; Kavalenka, A.A.; Urbancic, I.; Ljubetic, A.; Hemminga, M.A.

    2010-01-01

    As proteins are key molecules in living cells, knowledge about their structure can provide important insights and applications in science, biotechnology, and medicine. However, many protein structures are still a big challenge for existing high-resolution structure-determination methods, as can be

  11. High-field proton MRS of human brain

    Energy Technology Data Exchange (ETDEWEB)

    Di Costanzo, Alfonso E-mail: alfonso.dicostanzo@unina2.it; Trojsi, F.; Tosetti, M.; Giannatempo, G.M.; Nemore, F.; Piccirillo, M.; Bonavita, S.; Tedeschi, G.; Scarabino, T

    2003-11-01

    Proton magnetic resonance spectroscopy ({sup 1}H-MRS) of the brain reveals specific biochemical information about cerebral metabolites, which may support clinical diagnoses and enhance the understanding of neurological disorders. The advantages of performing {sup 1}H-MRS at higher field strengths include better signal to noise ratio (SNR) and increased spectral, spatial and temporal resolution, allowing the acquisition of high quality, easily quantifiable spectra in acceptable imaging times. In addition to improved measurement precision of N-acetylaspartate, choline, creatine and myo-inositol, high-field systems allow the high-resolution measurement of other metabolites, such as glutamate, glutamine, {gamma}-aminobutyric acid, scyllo-inositol, aspartate, taurine, N-acetylaspartylglutamate, glucose and branched amino acids, thus extending the range of metabolic information. However, these advantages may be hampered by intrinsic field-dependent technical difficulties, such as decreased T2 signal, chemical shift dispersion errors, J-modulation anomalies, increased magnetic susceptibility, eddy current artifacts, limitations in the design of homogeneous and sensitive radiofrequency (RF) coils, magnetic field instability and safety issues. Several studies demonstrated that these limitations could be overcome, suggesting that the appropriate optimization of high-field {sup 1}H-MRS would expand the application in the fields of clinical research and diagnostic routine.

  12. ESR1 gene promoter region methylation in free circulating DNA and its correlation with estrogen receptor protein expression in tumor tissue in breast cancer patients

    International Nuclear Information System (INIS)

    Martínez-Galán, Joaquina; Ríos, Sandra; Delgado, Juan Ramón; Torres-Torres, Blanca; Núñez, María Isabel; López-Peñalver, Jesús; Del Moral, Rosario; Ruiz De Almodóvar, José Mariano; Menjón, Salomón; Concha, Ángel; Chamorro, Clara

    2014-01-01

    Tumor expression of estrogen receptor (ER) is an important marker of prognosis, and is predictive of response to endocrine therapy in breast cancer. Several studies have observed that epigenetic events, such methylation of cytosines and deacetylation of histones, are involved in the complex mechanisms that regulate promoter transcription. However, the exact interplay of these factors in transcription activity is not well understood. In this study, we explored the relationship between ER expression status in tumor tissue samples and the methylation of the 5′ CpG promoter region of the estrogen receptor gene (ESR1) isolated from free circulating DNA (fcDNA) in plasma samples from breast cancer patients. Patients (n = 110) with non-metastatic breast cancer had analyses performed of ER expression (luminal phenotype in tumor tissue, by immunohistochemistry method), and the ESR1-DNA methylation status (fcDNA in plasma, by quantitative methylation specific PCR technique). Our results showed a significant association between presence of methylated ESR1 in patients with breast cancer and ER negative status in the tumor tissue (p = 0.0179). There was a trend towards a higher probability of ESR1-methylation in those phenotypes with poor prognosis i.e. 80% of triple negative patients, 60% of HER2 patients, compared to 28% and 5.9% of patients with better prognosis such as luminal A and luminal B, respectively. Silencing, by methylation, of the promoter region of the ESR1 affects the expression of the estrogen receptor protein in tumors of breast cancer patients; high methylation of ESR1-DNA is associated with estrogen receptor negative status which, in turn, may be implicated in the patient’s resistance to hormonal treatment in breast cancer. As such, epigenetic markers in plasma may be of interest as new targets for anticancer therapy, especially with respect to endocrine treatment

  13. High field dielectric properties of anisotropic polymer-ceramic composites

    International Nuclear Information System (INIS)

    Tomer, V.; Randall, C. A.

    2008-01-01

    Using dielectrophoretic assembly, we create anisotropic composites of BaTiO 3 particles in a silicone elastomer thermoset polymer. We study a variety of electrical properties in these composites, i.e., permittivity, dielectric breakdown, and energy density as function of ceramic volume fraction and connectivity. The recoverable energy density of these electric-field-structured composites is found to be highly dependent on the anisotropy present in the system. Our results indicate that x-y-aligned composites exhibit higher breakdown strengths along with large recoverable energy densities when compared to 0-3 composites. This demonstrates that engineered anisotropy can be employed to control dielectric breakdown strengths and nonlinear conduction at high fields in heterogeneous systems. Consequently, manipulation of anisotropy in high-field dielectric properties can be exploited for the development of high energy density polymer-ceramic systems

  14. Homogenous BSCCO-2212 Round Wires for Very High Field Magnets

    International Nuclear Information System (INIS)

    Campbell, Scott; Holesinger, Terry; Huang, Ybing

    2012-01-01

    The performance demands on modern particle accelerators generate a relentless push towards higher field magnets. In turn, advanced high field magnet development places increased demands on superconducting materials. Nb3Sn conductors have been used to achieve 16 T in a prototype dipole magnet and are thought to have the capability for ∼18 T for accelerator magnets (primarily dipoles but also higher order multipole magnets). However there have been suggestions and proposals for such magnets higher than 20 T. The High Energy Physics Community (HEP) has identified important new physics opportunities that are enabled by extremely high field magnets: 20 to 50 T solenoids for muon cooling in a muon collider (impact: understanding of neutrinos and dark matter); and 20+ T dipoles and quadrupoles for high energy hadron colliders (impact: discovery reach far beyond present). This proposal addresses the latest SBIR solicitation that calls for grant applications that seek to develop new or improved superconducting wire technologies for magnets that operate at a minimum of 12 Tesla (T) field, with increases up to 15 to 20 T sought in the near future (three to five years). The long-term development of accelerator magnets with fields greater than 20 T will require superconducting wires having significantly better high-field properties than those possessed by current Nb 3 Sn or other A15 based wires. Given the existing materials science base for Bi-2212 wire processing, we believe that Bi 2 Sr 2 CaCu 2 O y (Bi-2212) round wires can be produced in km-long piece lengths with properties suitable to meet both the near term and long term needs of the HEP community. The key advance will be the translation of this materials science base into a robust, high-yield wire technology. While the processing and application of A15 materials have advanced to a much higher level than those of the copper oxide-based, high T c (HTS) counterparts, the HTS materials have the very significant advantage

  15. The Humboldt High Magnetic Field Center at Berlin

    International Nuclear Information System (INIS)

    Hansel, S; Mueller, H-U; Anh, T T; Richter, B; Rossmann, H; Ortenberg, M von

    2006-01-01

    The Humboldt High Magnetic Field Center is operated by the Chair for Magnetotransport in Solids of the Department of Physics of the Humboldt-Universitaet zu Berlin. It provides DC-magnetic fields up to 20 T, pulsed nondestructive fields of up to 60 T and megagauss fields of up to 331 T using a single-turn coil generator for experimental application focusing on solid state physics. Magneto-optical investigations are carried out in the MIR, NIR and visible wavelength range as well as transport and magnetization experiments. The facility is open to the scientific community and welcomes users within the European project EuroMagNET. The laboratory will be closed in fall 2006 but its experimental facilities will be further accessible to the community in other labs. The single-turn coil generator will be transferred to LNCMP, Toulouse, France, continuing to provide applicable megagauss fields to the European Community

  16. Properties of partially ionized hydrogen plasmas in high electric fields

    International Nuclear Information System (INIS)

    Morawetz, K.

    1993-03-01

    In this thesis the fundamental equations of many-particle quantum-statistics of nonequilibrium are treated in respect to arbitrary high electric fields. Generalizations are found for the T-matrix approximation as well as for the shielded potential approximation valid for any field strength. These result in a non-Markovian behavior of the obtained collision integrals, also known as intra-collisional-field-effect (ICFE), and in a broadening of the energy conservation, the so-called collisional broadening (CB), caused by applied electric fields. In linear response it is shown in a new way, how the Debye-Onsager relaxation effect can be rederived from these collision integrals. Furthermore the complete quantum result is presented. Both effects, ICFE and CB, contribute to the right classical limit. The quantum result yields an surprising maximum of this field effects in dependence of the interacting mass ratio, which may be important in exciton-plasmas and semiconductors. (orig.)

  17. High speed pulsed magnetic fields measurements, using the Faraday effect

    International Nuclear Information System (INIS)

    Dillet, A.

    1964-12-01

    For these measures, the information used is the light polarization plane rotation induced by the magnetic field in a glass probe. This rotation is detected using a polarizer-analyzer couple. The detector is a photomultiplier used with high-current and pulsed light. In a distributed magnet (gap: 6 x 3 x 3 cm) magnetic fields to measure are 300 gauss, lasting 0.1 μs, with rise times ≤ 35 ns, repetition rate: 1/s. An oscilloscope is used to view the magnetic field from the P.M. plate signal. The value of the field is computed from a previous static calibration. Magnetic fields from 50 to 2000 gauss (with the probe now used) can be measured to about 20 gauss ± 5 per cent, with a frequency range of 30 MHz. (author) [fr

  18. High-Performance Field Emission from a Carbonized Cork.

    Science.gov (United States)

    Lee, Jeong Seok; Lee, Hak Jun; Yoo, Jae Man; Kim, Taewoo; Kim, Yong Hyup

    2017-12-20

    To broaden the range of application of electron beams, low-power field emitters are needed that are miniature and light. Here, we introduce carbonized cork as a material for field emitters. The light natural cork becomes a graphitic honeycomb upon carbonization, with the honeycomb cell walls 100-200 nm thick and the aspect ratio larger than 100, providing an ideal structure for the field electron emission. Compared to nanocarbon field emitters, the cork emitter produces a high current density and long-term stability with a low turn-on field. The nature of the cork material makes it quite simple to fabricate the emitter. Furthermore, any desired shape of the emitter tailored for the final application can easily be prepared for point, line, or planar emission.

  19. A design proposal for high field dipole magnet

    International Nuclear Information System (INIS)

    Hirabayashi, H.; Kobayashi, M.; Shintomi, T.; Tsuchiya, K.; Wake, M.

    1981-06-01

    A design of the high field dipole magnet which is going to be constructed in the KEK-Fermilab collaboration program is proposed. The central field of the magnet is meant to achieve 10 T by the use of ternary alloy conductor in the 1.8 K superfluid environment under atmospheric pressure. Since the electro-magnetic force in such a high field region is strong enough to give a fatal problem, a careful calculation is necessary for the magnet design. The program POISSON and LINDA were used for the magnetic field calculation. The computer code ISAS which is originated from NASTRAN developed at NASA was applied to calculate the stress and the deformation. A horizontal cryostat desigh for the operation of the 10 T dipole magnet is also proposed. (author)

  20. Microchip Electrophoresis at Elevated Temperatures and High Separation Field Strengths

    Science.gov (United States)

    Mitra, Indranil; Marczak, Steven P.; Jacobson, Stephen C.

    2014-01-01

    We report free-solution microchip electrophoresis performed at elevated temperatures and high separation field strengths. We used microfluidic devices with 11-cm long separation channels to conduct separations at temperatures between 22 (ambient) and 45 °C and field strengths from 100 to 1000 V/cm. To evaluate separation performance, N-glycans were used as a model system and labeled with 8-aminopyrene-1,3,6-trisulfonic acid to impart charge for electrophoresis and render them fluorescent. Typically, increased diffusivity at higher temperatures leads to increased axial dispersion and poor separation performance; however, we demonstrate that sufficiently high separation field strengths can be used to offset the impact of increased diffusivity in order to maintain separation efficiency. Efficiencies for these free-solution separations are the same at temperatures of 25, 35, and 45 °C with separation field strengths ≥500 V/cm. PMID:24114979

  1. MR equipment acquisition strategies: low-field or high-field scanners

    International Nuclear Information System (INIS)

    Marti-Bonmati, L.; Kormano, M.

    1997-01-01

    Magnetic resonance (MR) field strength is one of the key aspects to consider when purchasing MR equipment. Other aspects include the gradient system, coil design, computer and pulse sequence availability, purchase cost, local reimbursement policies, and current opinion within the medical community. Our objective here is to evaluate the decision-influencing aspects of the MR market, with a focus on some specific areas such as high resolution studies, examination times, special techniques, instrumentation, open design magnets, costs and reimbursement policies, academic and industrial interests, contrast media, clinical efficacy, and finally, clinicians' preferences. Certainly the advantage of high-field is a higher signal-to-noise ratio and improved resolution. With a high-field unit, higher spatial resolution images and higher temporal resolution images can be obtained. Typical imaging times needed to produce clinically diagnostic images are about 3 times longer at 0.1 T than at 1.0 or 1.5 T. High-field-related advanced techniques, such as functional imaging, spectroscopy and microscopy, may become clinically useful in the near future. As long as there is an unlimited demand for MR examinations, it appears financially profitable to run a high-field system, despite the associated higher costs. However, if demand for MR becomes saturated, low-field systems will cause less financial strain on the reimbursement organisation and service provider. Recent emphasis on cost containment, the development of interventional techniques, the increased use of MR for patients in intensive care and operating suites, the deployment of magnets in office suites, and the development of new magnet configurations, all favour the supplementary use of low-field systems. Hence, MR units of all field strengths have a role in radiology. (orig.)

  2. Influences of different sample preparation methods on tooth enamel ESR signals

    International Nuclear Information System (INIS)

    Zhang Wenyi; Jiao Ling; Zhang Liang'an; Pan Zhihong; Zeng Hongyu

    2005-01-01

    Objective: To study the influences of different sample preparation methods on tooth enamel ESR signals in order to reduce the effect of dentine on their sensitivities to radiation. Methods: The enamel was separated from dentine of non-irradiated adult teeth by mechanical, chemical, or both methods. The samples of different preparations were scanned by an ESR spectrometer before and after irradiation. Results: The response of ESR signals of samples prepared with different methods to radiation dose was significantly different. Conclusion: The selection of sample preparation method is very important for dose reconstruction by tooth enamel ESR dosimetry, especially in the low dose range. (authors)

  3. Detection of gamma-irradiated peanuts by ESR spectroscopy and GC analysis of hydrocarbons

    Energy Technology Data Exchange (ETDEWEB)

    Wei Mingli; An Li [Institute of Agro-food Science and Technology, Chinese Academy of Agricultural Sciences, 100193 Beijing (China); Yi Mingha, E-mail: wangyilwm@163.co [Institute of Agro-food Science and Technology, Chinese Academy of Agricultural Sciences, 100193 Beijing (China); Feng Wang [Institute of Agro-food Science and Technology, Chinese Academy of Agricultural Sciences, 100193 Beijing (China); Yan Lizhang [Division of Metrology in Ionizing Radiation and Medicine, National Institute of Metrology, 100013 Beijing (China)

    2011-03-15

    Peanuts were analyzed by electron spin resonance (ESR) spectroscopy and gas chromatography (GC) before and after gamma irradiation. Using European protocols, the validity and effectiveness of these two techniques were compared with regard to sample preparation, sample and solvent consumption and dose-response curves after irradiation. The results showed the possibility of using ESR and GC for distinguishing between irradiated and unirradiated peanuts. A radiation dose of 0.1 kGy could be detected by ESR but not by GC. The results also indicated that GC is an effective method for qualitative analysis of irradiated peanut, while ESR is suitable for the rapid detection of irradiated peanuts.

  4. ESR Spectroscopy for the Study of Oxidative Processes in Food and Beverages

    DEFF Research Database (Denmark)

    Andersen, Mogens Larsen; Skibsted, Leif Horsfelt

    2018-01-01

    Radicals are intermediates in many reactions that deteriorate foods. The detection of radicals by electron spin resonance, ESR, can provide mechanistic and uantitative information about these reactions, which has led to ESR-based methods for early prediction of shelf life of foods and beverages....... ESR is also used for monitoring irradiated foods, since the generated radicals are often quite stable. ESR can moreover give important information about oxidation mechanisms and microscopic physical structural aspects, which is useful for developing protective measures against oxidation in food....

  5. Ultra-high-field magnets for future hadron colliders

    International Nuclear Information System (INIS)

    McIntyre, P.M.; Shen, W.

    1997-01-01

    Several new concepts in magnetic design and coil fabrication are being incorporated into designs for ultra-high field collider magnets: a 16 Tesla block-coil dual dipole, also using Nb 3 Sn cable, featuring simple pancake coil construction and face-loaded prestress geometry; a 330 T/m block-coil quadrupole; and a ∼ 20 Tesla pipe-geometry dual dipole, using A15 or BSCCO tape. Field design and fabrication issues are discussed for each magnet

  6. Tunable filter imaging of high-redshift quasar fields

    NARCIS (Netherlands)

    Swinbank, J.; Baker, J.; Barr, J.; Hook, I.; Bland-Hawthorn, J.

    2012-01-01

    We have used the Taurus Tunable Filter to search for Lyα emitters in the fields of three high-redshift quasars: two at z∼ 2.2 (MRC B1256−243 and MRC B2158−206) and one at z∼ 4.5 (BR B0019−1522). Our observations had a field of view of around 35 arcmin2, and reached AB magnitudes of ∼21 (MRC

  7. Artificial terraced field extraction based on high resolution DEMs

    Science.gov (United States)

    Na, Jiaming; Yang, Xin; Xiong, Liyang; Tang, Guoan

    2017-04-01

    With the increase of human activities, artificial landforms become one of the main terrain features with special geographical and hydrological value. Terraced field, as the most important artificial landscapes of the loess plateau, plays an important role in conserving soil and water. With the development of digital terrain analysis (DTA), there is a current and future need in developing a robust, repeatable and cost-effective research methodology for terraced fields. In this paper, a novel method using bidirectional DEM shaded relief is proposed for terraced field identification based on high resolution DEM, taking Zhifanggou watershed, Shannxi province as the study area. Firstly, 1m DEM is obtained by low altitude aerial photogrammetry using Unmanned Aerial Vehicle (UAV), and 0.1m DOM is also obtained as the test data. Then, the positive and negative terrain segmentation is done to acquire the area of terraced field. Finally, a bidirectional DEM shaded relief is simulated to extract the ridges of each terraced field stages. The method in this paper can get not only polygon feature of the terraced field areas but also line feature of terraced field ridges. The accuracy is 89.7% compared with the artificial interpretation result from DOM. And additional experiment shows that this method has a strong robustness as well as high accuracy.

  8. Nonlinear piezoelectricity in epitaxial ferroelectrics at high electric fields.

    Science.gov (United States)

    Grigoriev, Alexei; Sichel, Rebecca; Lee, Ho Nyung; Landahl, Eric C; Adams, Bernhard; Dufresne, Eric M; Evans, Paul G

    2008-01-18

    Nonlinear effects in the coupling of polarization with elastic strain have been predicted to occur in ferroelectric materials subjected to high electric fields. Such predictions are tested here for a PbZr0.2Ti0.8O3 ferroelectric thin film at electric fields in the range of several hundred MV/m and strains reaching up to 2.7%. The piezoelectric strain exceeds predictions based on constant piezoelectric coefficients at electric fields from approximately 200 to 400 MV/m, which is consistent with a nonlinear effect predicted to occur at corresponding piezoelectric distortions.

  9. A commercial tokamak reactor using super high field superconducting magnets

    International Nuclear Information System (INIS)

    Schwartz, J.; Bromberg, L.; Cohn, D.R.; Williams, J.E.C.

    1988-01-01

    This paper explores the range of possibilities for producing super high fields with advanced superconducting magnets. Obtaining magnetic fields greater than about 18 T at the coil in a large superconducting magnet system will require advances in many areas of magnet technology. These needs are discussed and potential solutions (advanced superconductors, structural materials and design methods) evaluated. A point design for a commercial reactor with magnetic field at the coil of 24 T and fusion power of 1800 MW is presented. Critical issues and parameters for magnet design are identified. 20 refs., 9 figs., 4 tabs

  10. Magnetoresistance peculiarities of bismuth wires in high magnetic field

    Science.gov (United States)

    Condrea, E.; Gilewski, A.; Nicorici, A.

    2016-03-01

    Magnetoresistance measurements of Bi wires performed in the magnetic field oriented along the bisector axis revealed unexpected anomalous peaks in a high magnetic field far above the quantum limit of the electrons. By combining a magnetic field and an uniaxial strain, we obtained a modification of the electronic structure; as a result, the quantum limit for light and heavy electrons is changed in a different way. For the case where heavy electrons are in the quantum limit, a correlation between the exit of the lowest Landau level of light electrons and the Lifshitz transition was found.

  11. Design considerations for a large aperture high field superconducting dipole

    International Nuclear Information System (INIS)

    Harfoush, F.; Ankenbrandt, C.; Harrison, M.; Kerby, J.; Koepke, K.; Mantsch, P.; Nicol, T.; Riddiford, A.; Theilacker, J.

    1989-03-01

    The final phase of the Fermilab upgrade proposal calls for a new ring of superconducting magnets to be placed in the existing Main Accelerator tunnel. The goal of this design study is to specify a high field dipole (HFD) that is capable of supporting fixed target operation (ramping, resonant extraction) at a field of 6.6T (1.5 Tev) and colliding beam physics at 8.0T (1.8 Tev). The magnetic field quality at high field is set by the large amplitude orbits associated with resonant extraction. The field quality must therefore be at least as good as the existing Tevatron magnets which fulfill these criteria. The high fields and large aperture of this magnet result in large forces on the coil and collar assemblies. Therefore, the cold mass design must be able to sustain these forces while providing sufficient cooling to the coils during 4.2 K fixed target operation, and a minimum heat load during 1.8 K collider operation. The design work is still in progress but a cosine-theta, cold-iron dipole with a 70mm inner diameter coil has been tentatively adopted. This report presents details on the conductor and cable parameters, coil cross-section, projected manufacturing tolerances, iron yoke design, and cold mass assembly. 4 refs., 5 figs., 1 tab

  12. Design considerations for a large aperture high field superconducting dipole

    Energy Technology Data Exchange (ETDEWEB)

    Harfoush, F.; Ankenbrandt, C.; Harrison, M.; Kerby, J.; Koepke, K.; Mantsch, P.; Nicol, T.; Riddiford, A.; Theilacker, J.

    1989-03-01

    The final phase of the Fermilab upgrade proposal calls for a new ring of superconducting magnets to be placed in the existing Main Accelerator tunnel. The goal of this design study is to specify a high field dipole (HFD) that is capable of supporting fixed target operation (ramping, resonant extraction) at a field of 6.6T (1.5 Tev) and colliding beam physics at 8.0T (1.8 Tev). The magnetic field quality at high field is set by the large amplitude orbits associated with resonant extraction. The field quality must therefore be at least as good as the existing Tevatron magnets which fulfill these criteria. The high fields and large aperture of this magnet result in large forces on the coil and collar assemblies. Therefore, the cold mass design must be able to sustain these forces while providing sufficient cooling to the coils during 4.2 K fixed target operation, and a minimum heat load during 1.8 K collider operation. The design work is still in progress but a cosine-theta, cold-iron dipole with a 70mm inner diameter coil has been tentatively adopted. This report presents details on the conductor and cable parameters, coil cross-section, projected manufacturing tolerances, iron yoke design, and cold mass assembly. 4 refs., 5 figs., 1 tab.

  13. Disintegration and field evaporation of thiolate polymers in high electric fields

    International Nuclear Information System (INIS)

    Nickerson, B.S.; Karahka, M.; Kreuzer, H.J.

    2015-01-01

    High electrostatic fields cause major changes in polymers, structural (e.g. electrostriction) and electronic (e.g. reduction of the “band gap” with final metallization). Using density functional theory we have studied field effects on amino-alkane-thiols and perfluoro-alkane-thiols adsorbed on a metal substrate. Our results agree well with the APT fragmentation spectra obtained by Stoffers, Oberdorfer and Schmitz and shed light on disintegration pathways. We demonstrate that in SAMs the HOMO/LUMO gap is again reduced as a function of the field strength and vanishes at evaporation. We also follow the field dependence of the dielectric constant and polarizability. - Highlights: • Simple model of thiolate polymers is used to understand trends leading to field evaporation. • Potential energy curves followed by dipole moment, electric polarizability and dielectric constant are examined. • Features including coil, tilt and electrostriction are featured alongside evaporated species and HOMO/LUMO gap.

  14. Disintegration and field evaporation of thiolate polymers in high electric fields

    Energy Technology Data Exchange (ETDEWEB)

    Nickerson, B.S., E-mail: brenden.nickerson@dal.ca; Karahka, M.; Kreuzer, H.J.

    2015-12-15

    High electrostatic fields cause major changes in polymers, structural (e.g. electrostriction) and electronic (e.g. reduction of the “band gap” with final metallization). Using density functional theory we have studied field effects on amino-alkane-thiols and perfluoro-alkane-thiols adsorbed on a metal substrate. Our results agree well with the APT fragmentation spectra obtained by Stoffers, Oberdorfer and Schmitz and shed light on disintegration pathways. We demonstrate that in SAMs the HOMO/LUMO gap is again reduced as a function of the field strength and vanishes at evaporation. We also follow the field dependence of the dielectric constant and polarizability. - Highlights: • Simple model of thiolate polymers is used to understand trends leading to field evaporation. • Potential energy curves followed by dipole moment, electric polarizability and dielectric constant are examined. • Features including coil, tilt and electrostriction are featured alongside evaporated species and HOMO/LUMO gap.

  15. Improving NASICON Sinterability through Crystallization under High Frequency Electrical Fields

    Directory of Open Access Journals (Sweden)

    Ilya eLisenker

    2016-03-01

    Full Text Available The effect of high frequency (HF electric fields on the crystallization and sintering rates of a lithium aluminum germanium phosphate (LAGP ion conducting ceramic was investigated. LAGP with the nominal composition Li1.5Al0.5Ge1.5(PO43 was crystallized and sintered, both conventionally and under effect of electrical field. Electrical field application, of 300V/cm at 1MHz, produced up to a 40% improvement in sintering rate of LAGP that was crystallized and sintered under the HF field. Heat sink effect of the electrodes appears to arrest thermal runaway and subsequent flash behavior. Sintered pellets were characterized using XRD, SEM, TEM and EIS to compare conventionally and field sintered processes. The as-sintered structure appears largely unaffected by the field as the sintering curves tend to converge beyond initial stages of sintering. Differences in densities and microstructure after 1 hour of sintering were minor with measured sintering strains of 31% vs. 26% with and without field, respectively . Ionic conductivity of the sintered pellets was evaluated and no deterioration due to the use of HF field was noted, though capacitance of grain boundaries due to secondary phases was significantly increased.

  16. Association with litter size of new polymorphisms on ESR1 and ESR2 genes in a Chinese-European pig line

    Directory of Open Access Journals (Sweden)

    Rodriguez Carmen

    2007-02-01

    Full Text Available Abstract The objective of this study was to search for polymorphisms in the coding region of the estrogen receptors 1 and 2 (ESR1 and ESR2 and to analyze the effects of these variants and the well known intronic ESR1 Pvu II polymorphism on litter size in a Chinese-European pig line. We identified five silent single nucleotide polymorphisms (SNP in the ESR1 cDNA: c.669T > C (exon 3, c.1227C > T (exon 5, c.1452C > T (exon 7, c.1665T > C and c.1755A > G (exon 8. One pair of these SNP (c.1665T > C and c.1755A > G co-segregated in the analyzed line, and the SNP c.669T > C showed the same segregation pattern as the Pvu II polymorphism. These polymorphisms were tested in this study, although the c.1452C > T SNP within exon 7 was not analyzed due to its low informativeness. In the ESR2 cDNA, one missense SNP was found within exon 5, which caused an amino acid substitution in the coded protein: "c.949G > A (p.Val317Met" and was tested on sow litter size. Information on 1622 litter records from 408 genotyped sows was analyzed to determine whether these SNP influenced the total number of piglets born (TNB or the number of born alive (NBA. The polymorphisms ESR1: [Pvu II; c.669T > C], ESR1: [c.1665T > C; c.1755A > G] and ESR2: c.949G > A showed no statistically significant association with litter size. However, the ESR1: c.1227T allele was significantly associated with TNB. The additive substitution effect was estimated to be 0.40 piglets born per litter (P

  17. Field-effect transistor having a superlattice channel and high carrier velocities at high applied fields

    Science.gov (United States)

    Chaffin, R.J.; Dawson, L.R.; Fritz, I.J.; Osbourn, G.C.; Zipperian, T.E.

    1987-06-08

    A field effect transistor comprises a semiconductor having a source, a drain, a channel and a gate in operational relationship. The semiconductor is a strained layer superlattice comprising alternating quantum well and barrier layers, the quantum well layers and barrier layers being selected from the group of layer pairs consisting of InGaAs/AlGaAs, InAs/InAlGaAs, and InAs/InAlAsP. The layer thicknesses of the quantum well and barrier layers are sufficiently thin that the alternating layers constitute a superlattice which has a superlattice conduction band energy level structure in k-vector space. The layer thicknesses of the quantum well layers are selected to provide a superlattice L/sub 2D/-valley which has a shape which is substantially more two-dimensional than that of said bulk L-valley. 2 figs.

  18. Study of HTS Wires at High Magnetic Fields

    Energy Technology Data Exchange (ETDEWEB)

    Turrioni, D.; Barzi, E.; Lamm, M.J.; Yamada, R.; Zlobin, A.V.; Kikuchi, A.; /Fermilab

    2009-01-01

    Fermilab is working on the development of high field magnet systems for ionization cooling of muon beams. The use of high temperature superconducting (HTS) materials is being considered for these magnets using Helium refrigeration. Critical current (I{sub c}) measurements of HTS conductors were performed at FNAL and at NIMS up to 28 T under magnetic fields at zero to 90 degree with respect to the sample face. A description of the test setups and results on a BSCCO-2223 tape and second generation (2G) coated conductors are presented.

  19. Energy confinement in a high-current reversed field pinch

    International Nuclear Information System (INIS)

    An, Z.G.; Lee, G.S.; Diamond, P.H.

    1985-07-01

    The ion temperature gradient driven (eta/sub i/) mode is proposed as a candidate for the cause of anomalous transport in high current reversed field pinches. A 'four-field' fluid model is derived to describe the coupled nonlinear evolution of resistive interchange and eta/sub i/ modes. A renormalized theory is discussed, and the saturation level of the fluctuations is analytically estimated. Transport scalings are obtained, and their implications discussed. In particular, these results indicate that pellet injection is a potentially viable mechanism for improving energy confinement in a high temperature RFP

  20. Low-field MRI can be more sensitive than high-field MRI

    Science.gov (United States)

    Coffey, Aaron M.; Truong, Milton L.; Chekmenev, Eduard Y.

    2013-12-01

    MRI signal-to-noise ratio (SNR) is the key factor for image quality. Conventionally, SNR is proportional to nuclear spin polarization, which scales linearly with magnetic field strength. Yet ever-stronger magnets present numerous technical and financial limitations. Low-field MRI can mitigate these constraints with equivalent SNR from non-equilibrium ‘hyperpolarization' schemes, which increase polarization by orders of magnitude independently of the magnetic field. Here, theory and experimental validation demonstrate that combination of field independent polarization (e.g. hyperpolarization) with frequency optimized MRI detection coils (i.e. multi-turn coils using the maximum allowed conductor length) results in low-field MRI sensitivity approaching and even rivaling that of high-field MRI. Four read-out frequencies were tested using samples with identical numbers of 1H and 13C spins. Experimental SNRs at 0.0475 T were ∼40% of those obtained at 4.7 T. Conservatively, theoretical SNRs at 0.0475 T 1.13-fold higher than those at 4.7 T were possible despite an ∼100-fold lower detection frequency, indicating feasibility of high-sensitivity MRI without technically challenging, expensive high-field magnets. The data at 4.7 T and 0.0475 T was obtained from different spectrometers with different RF probes. The SNR comparison between the two field strengths accounted for many differences in parameters such as system noise figures and variations in the probe detection coils including Q factors and coil diameters.

  1. open-quotes High magnetic fields in the USAclose quotes

    International Nuclear Information System (INIS)

    Campbell, L.J.; Parkin, D.M.; Crow, J.E.; Schneider-Muntau, H.J.; Sullivan, N.S.

    1994-01-01

    During the past thirty years research using high magnetic fields has technically evolved in the manner, but not the magnitude, of the so-called big science areas of particle physics, plasma physics, neutron scattering, synchrotron light scattering, and astronomy. Starting from the laboratories of individual researchers it moved to a few larger universities, then to centralized national facilities with research and maintenance staffs, and, finally, to joint international ventures to build unique facilities, as illustrated by the subject of this conference. To better understand the nature of this type of research and its societal justification it is helpful to compare it, in general terms, with the aforementioned big-science fields. High magnetic field research differs from particle physics, plasma physics, and astronomy in three respects: (1) It is generic research that cuts across a wide range of scientific disciplines in physics, chemistry, biology, medicine, and engineering; (2) It studies materials and processes that are relevant for a variety of technological applications and it gives insight into biological processes; (3) It has produced, at least, comparably significant results with incomparably smaller resources. Unlike neutron and synchrotron light scattering, which probe matter, high magnetic fields change the thermodynamic state of matter. This change of state is fundamental and independent of other state variables, such as pressure and temperature. After the magnetic field is applied, various techniques are then used to study the new state

  2. Temperature dependence of high field electromechanical coupling in ferroelectric ceramics

    Energy Technology Data Exchange (ETDEWEB)

    Weaver, P M; Cain, M G; Stewart, M, E-mail: paul.weaver@npl.co.u [National Physical Laboratory, Hampton Road, Teddington, Middlesex, TW11 0LW (United Kingdom)

    2010-04-28

    A study of the temperature dependence of the electromechanical response of ferroelectric lead zirconate titanate (PZT) ceramics at high electric fields (up to 1.3 kV mm{sup -1}) is reported. Simultaneous measurements were performed of strain, electric field and polarization to form a complete response map from room temperature up to 200 {sup 0}C. An electrostrictive model is shown to provide an accurate description of the electromechanical response to high levels of induced polarization and electric field. This provides a method for decoupling strain contributions from thermal expansion and polarization changes. Direct measurements of electrostriction and thermal expansion, above and below the Curie temperature, are reported. Electrostriction coefficients are shown to be temperature dependent in these ceramic materials, with different values above and below the Curie temperature.

  3. Nb3Sn High Field Magnets for the High Luminosity LHC Upgrade Project

    Energy Technology Data Exchange (ETDEWEB)

    Ambrosio, Giorgio

    2015-06-01

    The High Luminosity upgrade of the Large Hadron Collider at CERN requires a new generation of high field superconducting magnets. High field large aperture quadrupoles (MQXF) are needed for the low-beta triplets close to the ATLAS and CMS detectors, and high field two-in-one dipoles (11 T dipoles) are needed to make room for additional collimation. The MQXF quadrupoles, with a field gradient of 140 T/m in 150 mm aperture, have a peak coil field of 12.1 T at nominal current. The 11 T dipoles, with an aperture of 60 mm, have a peak coil field of 11.6 T at nominal current. Both magnets require Nb3Sn conductor and are the first applications of this superconductor to actual accelerator magnets.

  4. High performance field emission of silicon carbide nanowires and their applications in flexible field emission displays

    Science.gov (United States)

    Cui, Yunkang; Chen, Jing; Di, Yunsong; Zhang, Xiaobing; Lei, Wei

    2017-12-01

    In this paper, a facile method to fabricate the flexible field emission devices (FEDs) based on SiC nanostructure emitters by a thermal evaporation method has been demonstrated. The composition characteristics of SiC nanowires was characterized by X-ray diffraction (XRD), selected area electron diffraction (SAED) and energy dispersive X-ray spectrometer (EDX), while the morphology was revealed by field emission scanning electron microscopy (SEM) and high resolution transmission electron microscopy (HRTEM). The results showed that the SiC nanowires grew along the [111] direction with the diameter of ˜110 nm and length of˜30 μm. The flexible FEDs have been fabricated by transferring and screen-printing the SiC nanowires onto the flexible substrates exhibited excellent field emission properties, such as the low turn-on field (˜0.95 V/μm) and threshold field (˜3.26 V/μm), and the high field enhancement factor (β=4670). It is worth noting the current density degradation can be controlled lower than 2% per hour during the stability tests. In addition, the flexible FEDs based on SiC nanowire emitters exhibit uniform bright emission modes under bending test conditions. As a result, this strategy is very useful for its potential application in the commercial flexible FEDs.

  5. High performance field emission of silicon carbide nanowires and their applications in flexible field emission displays

    Directory of Open Access Journals (Sweden)

    Yunkang Cui

    2017-12-01

    Full Text Available In this paper, a facile method to fabricate the flexible field emission devices (FEDs based on SiC nanostructure emitters by a thermal evaporation method has been demonstrated. The composition characteristics of SiC nanowires was characterized by X-ray diffraction (XRD, selected area electron diffraction (SAED and energy dispersive X-ray spectrometer (EDX, while the morphology was revealed by field emission scanning electron microscopy (SEM and high resolution transmission electron microscopy (HRTEM. The results showed that the SiC nanowires grew along the [111] direction with the diameter of ∼110 nm and length of∼30 μm. The flexible FEDs have been fabricated by transferring and screen-printing the SiC nanowires onto the flexible substrates exhibited excellent field emission properties, such as the low turn-on field (∼0.95 V/μm and threshold field (∼3.26 V/μm, and the high field enhancement factor (β=4670. It is worth noting the current density degradation can be controlled lower than 2% per hour during the stability tests. In addition, the flexible FEDs based on SiC nanowire emitters exhibit uniform bright emission modes under bending test conditions. As a result, this strategy is very useful for its potential application in the commercial flexible FEDs.

  6. Individual monitoring in high-energy stray radiation fields

    International Nuclear Information System (INIS)

    Hoefert, M.; Stevenson, G.R.

    1995-01-01

    Due to the lack of passive or active devices that could be considered as personal dosemeters in high-energy stray fields one can at present only perform individual monitoring around high energy accelerators. Of all detectors currently available it is shown that the NTA film is the most suitable method for individually monitoring the neutron exposure of more than 3000 persons regularly, reliably, and cost effectively like at CERN. (author)

  7. Submillimetre wave spectroscopy of semiconductors in high magnetic fields

    International Nuclear Information System (INIS)

    Maan, J.C.

    1979-01-01

    Two types of cyclotron resonance studies with far infrared radiation and at high magnetic fields in semiconductors are discussed. Firstly, the phenomenon of the change in the static conductivity at cyclotron resonance conditions in pure semiconductors, in this case n-GaAs, is investigated. Secondly, the results of cyclotron resonance experiments in an n-InAs-GaSb superlattice are discussed. (Auth.)

  8. The high field superconducting magnet program at LLNL: Annual report

    International Nuclear Information System (INIS)

    Miller, J.R.; Chaplin, M.R.; Kerns, J.A.; Leber, R.L.; Rosdahl, A.R.; Slack, D.S.; Summers, L.T.; Zbasnik, J.P.

    1986-01-01

    In FY 86 the program continued along several interrelated thrust areas. These thrust areas have been broadly labeled as follows: (1) Superconductor Research and Technology; (2) Magnet Systems Materials Technology; (3) Magnet Systems Design Technology; (4) High Field Test Facility; and (5) Technology Transfer

  9. High field MRI of axillary lymph nodes and breast cancer

    NARCIS (Netherlands)

    Korteweg, M.A.

    2011-01-01

    In this thesis nodal characteristics have been assessed with high field Magnetic Resonance Imaging (MRI) using a clinical scanner in order to discriminate non-metastatic from metastatic nodes of breast cancer patients. The final goal is to non-invasively determine nodal and tumor stage of breast

  10. Magnetic field structure of experimental high beta tokamak equilibria

    International Nuclear Information System (INIS)

    Deniz, A.V.

    1986-01-01

    The magnetic field structure of several low and high β tokamaks in the Columbia High Beta Tokamak (HBT) was determined by high-impedance internal magnetic probes. From the measurement of the magnetic field, the poloidal flux, toroidal flux, toroidal current, and safety factor are calculated. In addition, the plasma position and cross-sectional shape are determined. The extent of the perturbation of the plasma by the probe was investigated and was found to be acceptably small. The tokamaks have major radii of approx.0.24 m, minor radii of approx.0.05 m, toroidal plasma current densities of approx.10 6 A/m 2 , and line-integrated electron densities of approx.10 20 m -2 . The major difference between the low and high β tokamaks is that the high β tokamak was observed to have an outward shift in major radius of both the magnetic center and peak of the toroidal current density. The magnetic center moves inward in major radius after 20 to 30 μsec, presumably because the plasma maintains major radial equilibrium as its pressure decreases from radiation due to impurity atoms. Both the equilibrium and the production of these tokamaks from a toroidal field stabilized z-pinch are modeled computationally. One tokamak evolves from a state with low β features, through a possibly unstable state, to a state with high β features

  11. Effects of a homogeneous magnetic field on erythrocyte sedimentation and aggregation

    Energy Technology Data Exchange (ETDEWEB)

    Iino, Masaaki [Nippon Medical School, Tokyo (Japan). Dept. of Physiology I

    1997-05-01

    Effects of a homogeneous static magnetic field on erythrocyte sedimentation rate (ESR) have been assessed by using the standard Westergren method. A magnetic field of 6.3 T in the vertical direction only slightly enhanced ESR in saline solution, which was consistent with an effect on cell orientation. On the other hand, the magnetic field greatly enhanced ESR in plasma. It took a long time (about 20 min) for an ESR change to occur in plasma in response to the magnetic field. The effects in plasma were too large to originate only from cell orientation and were clearly distinct from a magnetic field-induced Boycott effect under an inhomogeneous magnetic field. A morphological examination and the nonlinear time course of the sedimentation in plasma indicated that the magnetic field increased cell aggregation and thereby enhanced ESR in plasma.

  12. Report on the high magnetic field tokamak TRIAM-1

    Energy Technology Data Exchange (ETDEWEB)

    Ito, T; Kawai, Y; Toi, K; Hiraki, N; Nakamure, K [Kyushu Univ., Fukuoke (Japan). Research Inst. for Applied Mechanics

    1981-02-01

    A high magnetic field tokamak has been constructed at Kyushu University to study the confinement of high magnetic field tokamak plasma and turbulent heating. The tokamak device consists of toroidal field coils, vertical field coils, horizontal field coils, primary windings, a transformer iron core, turbulent heating coils, and a vacuum chamber. For the observation of plasma, plasma monitors, a micro-wave interferometer, a laser scattering system, a neutral particle energy analyzer, a soft X-ray detector, and a visible spectrometer were installed on the vacuum chamber. The experimental results showed that the central electron temperature was about 640 eV, the central ion temperature 280 eV and mean electron density 2.2 x 10/sup 14//cm/sup 3/. It was found that the proportionality law of electron density and confinement time was valid for this small plasma system. By the turbulent heating, the central ion temperature increased from 170 eV to 580 eV.

  13. Design of High Field Multipole Wiggler at PLS

    International Nuclear Information System (INIS)

    Kim, D. E.; Park, K. H.; Lee, H. G.; Suh, H. S.; Han, H. S.; Jung, Y. G.; Chung, C. W.

    2007-01-01

    Pohang Accelerator Laboratory (PAL) is developing a high field multipole wiggler for new EXAFS beamline. The beamline is planning to utilize very high photon energy (∼40keV) synchrotron radiation at Pohang Light Source (PLS). To achieve higher critical photon energy, the wiggler field need to be maximized. A magnetic structure with wedged pole and blocks with additional side blocks which are similar to asymmetric wiggler of ESRF are designed to achieve higher flux density. The end structures were designed to be asymmetric along the beam direction to ensure systematic zero 1st field integral. The thickness of the last magnets were adjusted to minimize the transition sequence to the fully developed periodic field. This approach is more convenient to control than adjusting the strength of the end magnets. The final design features 140mm period, 2.5 Tesla peak flux density at 12mm pole gap, 1205mm magnetic structure length with 16 full field poles. In this article, all the design, engineering efforts for the HFMSII wiggler will be described

  14. ESR study on free radicals trapped in crosslinked polytetrafluoroethylene (PTFE)

    International Nuclear Information System (INIS)

    Oshima, Akihiro; Tabata, Yoneho; Seguchi, Tadao

    1997-01-01

    Free radicals in crosslinked PTFE which formed by 60 Co γ-rays irradiation at 77 K and at room temperature were studied by electron spin resonance (ESR) spectroscopy. The crosslinked PTFE specimens with different crosslinking density were prepared by electron beam irradiation in the molten state. The ESR spectra observed in the irradiated crosslinked PTFE are much different from those in non-crosslinked PTFE (virgin); a broad singlet component increases with increasing the crosslinking density, G-value of radicals is much higher in crosslinked PTFE than in non-crosslinked one. Free radicals related to the broad component are trapped in the non-crystalline region of crosslinked PTFE and rather stable at room temperature, whereas radicals trapped in amorphous non-crosslinked PTFE are unstable at room temperature. It is thought that most of free radicals trapped in the crosslinked PTFE are formed in the crosslinked amorphous region. The trapped radicals decays around 383 K (110 o C) due to the molecular motion of α-relaxation. (Author)

  15. Second interlaboratory-comparison project on ESR dating

    International Nuclear Information System (INIS)

    Barabas, M.; Walther, R.; Radtke, U.

    1993-01-01

    An intercomparison project on ESR dating in which 14 ESR groups participated was initiated. Each group was provided with two samples of a coral powder, one of which (Sample A) was a fossil coral with a mass spectrometric determined U/Th age. Sample B was a recent coral, irradiated with a definite γ-dose (checked by alanine dosimetry). In both cases the accumulated dose (AD) had to be determined (for sample A the U-content and age as well). Additionally, the chance of a calibration of γ-sources by alanine dosimeters was offered. The results show that the γ-source calibration is better then ± 5%, the mean value of the AD from sample A seems to agree with the expected AD but the mean AD value from sample B is overestimated, systematic errors occur due to the fitting procedure: the AD estimate depends on the maximum γ-dose used for the irradiation curve, the AD determination including the smallest systematic error gives correct values for sample B but too low values for sample A which may be caused by fading of the signal g = 2.0006. (author)

  16. Magnetic resonance imaging and spectroscopy at ultra high fields

    International Nuclear Information System (INIS)

    Neuberger, Thomas

    2009-01-01

    The goal of the work presented in this thesis was to explore the possibilities and limitations of MRI / MRS using an ultra high field of 17.6 tesla. A broad range of specific applications and MR methods, from MRI to MRSI and MRS were investigated. The main foci were on sodium magnetic resonance spectroscopic imaging of rodents, magnetic resonance spectroscopy of the mouse brain, and the detection of small amounts of iron labeled stem cells in the rat brain using MRI Sodium spectroscopic imaging was explored since it benefits tremendously from the high magnetic field. Due to the intrinsically low signal in vivo, originating from the low concentrations and short transverse relaxation times, only limited results have been achieved by other researchers until now. Results in the literature include studies conducted on large animals such as dogs to animals as small as rats. No studies performed on mice have been reported, despite the fact that the mouse is the most important laboratory animal due to the ready availability of transgenic strains. Hence, this study concentrated on sodium MRSI of small rodents, mostly mice (brain, heart, and kidney), and in the case of the brain on young rats. The second part of this work concentrated on proton magnetic resonance spectroscopy of the rodent brain. Due to the high magnetic field strength not only the increasing signal but also the extended spectral resolution was advantageous for such kind of studies. The difficulties/limitations of ultra high field MRS were also investigated. In the last part of the presented work detection limits of iron labeled stem cells in vivo using magnetic resonance imaging were explored. The studies provided very useful benchmarks for future researchers in terms of the number of labeled stem cells that are required for high-field MRI studies. Overall this work has shown many of the benefits and the areas that need special attention of ultra high fields in MR. Three topics in MRI, MRS and MRSI were

  17. Magnetic resonance imaging and spectroscopy at ultra high fields

    Energy Technology Data Exchange (ETDEWEB)

    Neuberger, Thomas

    2009-06-23

    The goal of the work presented in this thesis was to explore the possibilities and limitations of MRI / MRS using an ultra high field of 17.6 tesla. A broad range of specific applications and MR methods, from MRI to MRSI and MRS were investigated. The main foci were on sodium magnetic resonance spectroscopic imaging of rodents, magnetic resonance spectroscopy of the mouse brain, and the detection of small amounts of iron labeled stem cells in the rat brain using MRI Sodium spectroscopic imaging was explored since it benefits tremendously from the high magnetic field. Due to the intrinsically low signal in vivo, originating from the low concentrations and short transverse relaxation times, only limited results have been achieved by other researchers until now. Results in the literature include studies conducted on large animals such as dogs to animals as small as rats. No studies performed on mice have been reported, despite the fact that the mouse is the most important laboratory animal due to the ready availability of transgenic strains. Hence, this study concentrated on sodium MRSI of small rodents, mostly mice (brain, heart, and kidney), and in the case of the brain on young rats. The second part of this work concentrated on proton magnetic resonance spectroscopy of the rodent brain. Due to the high magnetic field strength not only the increasing signal but also the extended spectral resolution was advantageous for such kind of studies. The difficulties/limitations of ultra high field MRS were also investigated. In the last part of the presented work detection limits of iron labeled stem cells in vivo using magnetic resonance imaging were explored. The studies provided very useful benchmarks for future researchers in terms of the number of labeled stem cells that are required for high-field MRI studies. Overall this work has shown many of the benefits and the areas that need special attention of ultra high fields in MR. Three topics in MRI, MRS and MRSI were

  18. The Impact of ESR1 Mutations on the Treatment of Metastatic Breast Cancer.

    Science.gov (United States)

    Pejerrey, Sasha M; Dustin, Derek; Kim, Jin-Ah; Gu, Guowei; Rechoum, Yassine; Fuqua, Suzanne A W

    2018-05-07

    After nearly 20 years of research, it is now established that mutations within the estrogen receptor (ER) gene, ESR1, frequently occur in metastatic breast cancer and influence response to hormone therapy. Though early studies presented differing results, sensitive sequencing techniques now show that ESR1 mutations occur at a frequency between 20 and 40% depending on the assay method. Recent studies have focused on several "hot spot mutations," a cluster of mutations found in the hormone-binding domain of the ESR1 gene. Throughout the course of treatment, tumor evolution can occur, and ESR1 mutations emerge and become enriched in the metastatic setting. Sensitive techniques to continually monitor mutant burden in vivo are needed to effectively treat patients with mutant ESR1. The full impact of these mutations on tumor response to different therapies remains to be determined. However, recent studies indicate that mutant-bearing tumors may be less responsive to specific hormonal therapies, and suggest that aromatase inhibitor (AI) therapy may select for the emergence of ESR1 mutations. Additionally, different mutations may respond discretely to targeted therapies. The need for more preclinical mechanistic studies on ESR1 mutations and the development of better agents to target these mutations are urgently needed. In the future, sequential monitoring of ESR1 mutational status will likely direct personalized therapeutic regimens appropriate to each tumor's unique mutational landscape.

  19. ESR study of weakly irradiated organic conductors: TMTSF-DMTCNQ and (TMTSF)2PF6

    International Nuclear Information System (INIS)

    Forro, L.; Beuneu, F.

    1982-01-01

    ESR experiments are presented on irradiated TMTSF-DMTCNQ and (TMTSF) 2 PF 6 . They suggest that a weak disorder extends the metallic phases to low temperatures. Surprisingly, disorder has no effect on the ESR linewidth of (TMTSF) 2 PF 6 between 20 and 30 K, where the d.c. conductivity changes a lot with disorder. (author)

  20. High field superconductor development and understanding project, Final Report

    Energy Technology Data Exchange (ETDEWEB)

    Larbalestier, David C.; Lee, Peter J.

    2009-07-15

    Over 25 years the Applied Superconductivity Center at the University of Wisconsin-Madison provided a vital technical resource to the High Energy Physics community covering development in superconducting strand for HEP accelerator magnet development. In particular the work of the group has been to develop the next generation of high field superconductors for high field application. Grad students Mike Naus, Chad Fischer, Arno Godeke and Matt Jewell improved our understanding of the microstructure and microchemistry of Nb3Sn and their impact on the physical and mechanical properties. The success of this work has led to the continued funding of this work at the ASC after it moved to the NHMFL and also to direct funding from BNL for some aspects of Nb3Sn cable evaluation.

  1. Mechanical design of a high field common coil magnet

    CERN Document Server

    Caspi, S; Dietderich, D R; Gourlay, S A; Gupta, R; McInturff, A; Millos, G; Scanlan, R M

    1999-01-01

    A common coil design for high field 2-in-1 accelerator magnets has been previously presented as a "conductor-friendly" option for high field magnets applicable for a Very Large Hadron Collider. This paper presents the mechanical design for a 14 tesla 2-in-1 dipole based on the common coil design approach. The magnet will use a high current density Nb/sub 3/Sn conductor. The design addresses mechanical issues particular to the common coil geometry: horizontal support against coil edges, vertical preload on coil faces, end loading and support, and coil stresses and strains. The magnet is the second in a series of racetrack coil magnets that will provide experimental verification of the common coil design approach. (9 refs).

  2. Resonator as high frequency electromagnetic field oscillation generator

    International Nuclear Information System (INIS)

    Svoroba, O.V.; Scherbina, V.O.

    2007-01-01

    The problem of finding the u(x-vector) field potential in a specific waveguide with generalized corrugated core geometry is considered. The perturbation is brought to the system by high energy electron beam, injected in a waveguide. It is shown that the Neumann spectral problem can be reduced to finding Green approximation solution, and how it can be solved by the discretization technique. Considered parameterization allow to optimize the u(x-vector) field for specific frequency tuning. This method can be used as plasma heating method for thermonuclear temperature control

  3. Functional magnetic resonance imaging with ultra-high fields

    International Nuclear Information System (INIS)

    Windischberger, C.; Schoepf, V.; Sladky, R.; Moser, E.; Fischmeister, F.P.S.

    2010-01-01

    Functional magnetic resonance imaging (fMRI) is currently the primary method for non-invasive functional localization in the brain. With the emergence of MR systems with field strengths of 4 Tesla and above, neuronal activation may be studied with unprecedented accuracy. In this article we present different approaches to use the improved sensitivity and specificity for expanding current fMRT resolution limits in space and time based on several 7 Tesla studies. In addition to the challenges that arise with ultra-high magnetic fields possible solutions will be discussed. (orig.) [de

  4. High-field susceptibility in ferromagnetic NpOs2

    International Nuclear Information System (INIS)

    Dunlap, B.D.; Aldred, A.T.; Lam, D.J.; Davidson, G.R.

    1975-01-01

    NpOs 2 is known to be a ferromagnet with a Curie temperature of 7.5 0 K. Previous bulk magnetization measurements indicated a field-induced magnetization even well below the transition temperature. By a measurement of the local high-field susceptibility, using the Moessbauer effect in 237 Np, a susceptibility of (1.2 +- 0.2) x 10 -2 emu/mole at 1.6 0 K is obtained, in general agreement with the bulk measurement. Such a large susceptibility is best understood by a model f itinerant magnetism, although other properties of the material indicate localized behavior

  5. High critical magnetic field superconductor La3S4

    International Nuclear Information System (INIS)

    Westerholt, K.; Bach, H.; Wendemuth, R.; Methfessel, S.

    1979-01-01

    A report is presented on electrical conductivity, specific heat and magnetization measurements on La 3 S 4 single crystals. The results show that La 3 S 4 is a strong coupling superconductor with a BCS coherence length of 132 A. This extremely low value makes La 3 S 4 an intrinsic high critical magnetic field superconductor with a Landau-Ginsburg parameter of 20. For the temperature gradient of the upper critical magnetic field at the transition temperature values are found up to 35 kG/K. (author)

  6. Review - X-ray diffraction measurements in high magnetic fields and at high temperatures

    Directory of Open Access Journals (Sweden)

    Yoshifuru Mitsui, Keiichi Koyama and Kazuo Watanabe

    2009-01-01

    Full Text Available A system was developed measuring x-ray powder diffraction in high magnetic fields up to 5 T and at temperatures from 283 to 473 K. The stability of the temperature is within 1 K over 6 h. In order to examine the ability of the system, the high-field x-ray diffraction measurements were carried out for Si and a Ni-based ferromagnetic shape-memory alloy. The results show that the x-ray powder diffraction measurements in high magnetic fields and at high temperatures are useful for materials research.

  7. Quantitative detection of absorbed dose of irradiated dried fruit by ESR spectroscopy method

    International Nuclear Information System (INIS)

    Li Weiming; Ha Yiming; Zhao Yongfu; Zhang Yanli

    2011-01-01

    Sunflower seeds, walnuts, pistachios, and hazelnuts were used as experimental materials which were irradiated at 1.0, 3.0, 5.0 and 10.0 kGy, respectively. The relationships and correlations between ESR signal intensity and irradiation dosages were studied. The results showed that ESR spectra of irradiated samples were obviously different from that of CK, and the ESR signal intensity was positively related with the irradiation dose. After irradiation, the ESR intensity and spectrum shapes all changed and all four samples were clearly identified irradiated or unirradiated. The appearances of the two weak satellite lines which situated left and right to the intense singlet line in walnuts and pistachios proved the existence of cellulose radical. The detection dose limit of irradiated walnut was 1 kGy, and the detection limits of the other three samples were lower than 1 kGy. In conclusion, the ESR method could be used to irradiated. (authors)

  8. Ultra-High Field Magnets for X-Ray and Neutron Scattering using High Temperature Superconductors

    Energy Technology Data Exchange (ETDEWEB)

    Winn, Barry L. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Broholm, C. [Johns Hopkins Univ., Baltimore, MD (United States); Bird, M. [Florida State Univ., Tallahassee, FL (United States). National High Magnetic Field Lab. (MagLab); Breneman, Bruce C. [General Atomics, San Diego, CA (United States); Coffey, Michael [Cryomagnetics, Oak Ridge, TN (United States); Cutler, Roy I. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Duckworth, Robert C. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Erwin, R. [National Inst. of Standards and Technology (NIST), Gaithersburg, MD (United States); Hahn, Seungyong [Florida State Univ., Tallahassee, FL (United States). National High Magnetic Field Lab. (MagLab); Hernandez, Yamali [National Inst. of Standards and Technology (NIST), Gaithersburg, MD (United States); Herwig, Kenneth W. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Holland, Leo D. [General Atomics, San Diego, CA (United States); Lonergan, Kevin M. [Oxford Instruments, Abingdon (United Kingdom); Melhem, Ziad [Oxford Instruments, Abingdon (United Kingdom); Minter, Stephen J. [Cryomagnetics, Oak Ridge, TN (United States); Nelson, C. [Brookhaven National Lab. (BNL), Upton, NY (United States); Paranthaman, M. Parans [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Pierce, Josh [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Ruff, Jacob [Cornell Univ., Ithaca, NY (United States); Shen, Tengming [Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States); Sherline, Todd E. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Smeibidl, Peter G. [Helmholtz-Zentrum Berlin (HZB), (Germany); Tennant, David [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); van der Laan, Danko [Advanced Conductor Technologies, LLC, Boulder, CO (United States); Wahle, Robert J. [Helmholtz-Zentrum Berlin (HZB), (Germany); Zhang, Yifei [SuperPower, Inc., Schenectady, NY (United States)

    2017-01-01

    X-ray and neutron scattering techniques are capable of acquiring information about the structure and dynamics of quantum matter. However, the high-field magnet systems currently available at x-ray and neutron scattering facilities in the United States are limited to fields of 16 tesla (T) at maximum, which precludes applications that require and/or study ultra-high field states of matter. This gap in capability—and the need to address it—is a central conclusion of the 2005 National Academy of Sciences report by the Committee on Opportunities in High Magnetic Field Science. To address this gap, we propose a magnet development program that would more than double the field range accessible to scattering experiments. With the development and use of new ultra-high field–magnets, the program would bring into view new worlds of quantum matter with profound impacts on our understanding of advanced electronic materials.

  9. High-Density Near-Field Optical Disc Recording

    Science.gov (United States)

    Shinoda, Masataka; Saito, Kimihiro; Ishimoto, Tsutomu; Kondo, Takao; Nakaoki, Ariyoshi; Ide, Naoki; Furuki, Motohiro; Takeda, Minoru; Akiyama, Yuji; Shimouma, Takashi; Yamamoto, Masanobu

    2005-05-01

    We developed a high-density near-field optical recording disc system using a solid immersion lens. The near-field optical pick-up consists of a solid immersion lens with a numerical aperture of 1.84. The laser wavelength for recording is 405 nm. In order to realize the near-field optical recording disc, we used a phase-change recording media and a molded polycarbonate substrate. A clear eye pattern of 112 GB capacity with 160 nm track pitch and 50 nm bit length was observed. The equivalent areal density is 80.6 Gbit/in2. The bottom bit error rate of 3 tracks-write was 4.5× 10-5. The readout power margin and the recording power margin were ± 30.4% and ± 11.2%, respectively.

  10. Rf Gun with High-Current Density Field Emission Cathode

    International Nuclear Information System (INIS)

    Jay L. Hirshfield

    2005-01-01

    High current-density field emission from an array of carbon nanotubes, with field-emission-transistor control, and with secondary electron channel multiplication in a ceramic facing structure, have been combined in a cold cathode for rf guns and diode guns. Electrodynamic and space-charge flow simulations were conducted to specify the cathode configuration and range of emission current density from the field emission cold cathode. Design of this cathode has been made for installation and testing in an existing S-band 2-1/2 cell rf gun. With emission control and modulation, and with current density in the range of 0.1-1 kA/cm2, this cathode could provide performance and long-life not enjoyed by other currently-available cathodes

  11. Safety aspects in high-field magnetic resonance imaging

    International Nuclear Information System (INIS)

    Muehlenweg, M.; Trattnig, S.; Schaefers, G.

    2008-01-01

    With more and more 3 Tesla high-field magnetic resonance (MR) scanners entering clinical routine, the safety notion in MR imaging has also reached a new dimension. The first part of this paper deals with the three most important sources of physical interaction (static magnetic field, gradient and HF fields). The paper discusses the differences compared with the traditional clinical 1.5 T standard scanners, the impact on human beings, the interactions with metallic objects and the relevant safety standards. The second part of the paper examines the issue of MR safety as seen in clinical practice and tries to demonstrate optimization potentials. This includes structural optimization in information distribution and hospital organization as well as test standards and labeling guidelines. (orig.) [de

  12. Field experimental observations of highly graded sediment plumes

    DEFF Research Database (Denmark)

    Hjelmager Jensen, Jacob; Saremi, Sina; Jimenez, Carlos

    2015-01-01

    A field experiment in the waters off the south-eastern coast of Cyprus was carried out to study near-field formation of sediment plumes from dumping. Different loads of sediment were poured into calm and limpid waters one at the time from just above the sea surface. The associated plumes......-bed positions gives unique insight into the dynamics of the descending plume and near-field dispersion processes, and enables good understanding of flow and sediment transport processes involved from-release-to-deposition of the load in a non-scaled environment. The high resolution images and footages...... are available through the link provided herein. Observations support the development of a detailed multi-fractional sediment plume model....

  13. Field calibration of a TLD albedo dosemeter in the high-energy neutron field of CERF

    International Nuclear Information System (INIS)

    Haninger, T.; Kleinau, P.; Haninger, S.

    2017-01-01

    The new albedo dosemeter-type AWST-TL-GD 04 has been calibrated in the CERF neutron field (CERN-EU high-energy Reference Field). This type of albedo dosemeter is based on thermoluminescent detectors (TLDs) and used by the individual monitoring service of the Helmholtz Zentrum Muenchen (AWST) since 2015 for monitoring persons, who are exposed occupationally against photon and neutron radiation. The motivation for this experiment was to gain a field specific neutron correction factor N n for workplaces at high-energy particle accelerators. N n is a dimensionless factor relative to a basic detector calibration with 137 Cs and is used to calculate the personal neutron dose in terms of H p (10) from the neutron albedo signal. The results show that the sensitivity of the albedo dosemeter for this specific neutron field is not significantly lower as for fast neutrons of a radionuclide source like 252 Cf. The neutron correction factor varies between 0.73 and 1.16 with a midrange value of 0.94. The albedo dosemeter is therefore appropriate to monitor persons, which are exposed at high-energy particle accelerators. (authors)

  14. Electron-electron interactions in graphene field-induced quantum dots in a high magnetic field

    DEFF Research Database (Denmark)

    Orlof, A.; Shylau, Artsem; Zozoulenko, I. V.

    2015-01-01

    We study the effect of electron-electron interaction in graphene quantum dots defined by an external electrostatic potential and a high magnetic field. To account for the electron-electron interaction, we use the Thomas-Fermi approximation and find that electron screening causes the formation...... of compressible strips in the potential profile and the electron density. We numerically solve the Dirac equations describing the electron dynamics in quantum dots, and we demonstrate that compressible strips lead to the appearance of plateaus in the electron energies as a function of the magnetic field. Finally...

  15. High-energy behavior of field-strength interactions

    International Nuclear Information System (INIS)

    Levin, D.N.

    1976-01-01

    It is known that spontaneously broken gauge theories are the only renormalizable theories of massive spin-one particles with mass dimension less than or equal to 4. This paper describes a search for renormalizable interactions with higher mass dimension. Specifically, we examine the high-energy behavior of a class of models which involve field-strength interactions. Power counting shows that the high-energy behavior of these models is no worse than the naively estimated high-energy behavior of a gauge theory in the U gauge. Therefore, there may be a ''soft'' symmetry-breaking mechanism (for instance, a soft divergence of an antisymmetric tensor current) which enforces renormalizable high-energy behavior in the same way that spontaneously broken gauge invariance guarantees the renormalizability of gauge theories. This hope is supported by the existence of ''gauge theories'' of strings, which describe analogous interactions of strings and field strengths. Unfortunately, this idea is tarnished by explicit calculations in which renormalizability is imposed in the form of unitarity bounds. These unitarity bounds imply that all possible field-strength couplings must be zero and that the remaining interactions describe a spontaneously broken gauge theory. Thus this result supports an earlier conjecture that gauge theories are the only renormalizable theories of massive vector bosons

  16. Seasonal dependence of high-latitude electric fields

    International Nuclear Information System (INIS)

    de la Beaujardiere, O.; Leger, C.; Alcayde, D.; Fontanari, J.

    1991-01-01

    The seasonal dependence of the high-latitude electric field was investigated using Sondrestrom incoherent scatter radar data. Average ExB drifts were derived from 5 years of measurements centered around solar minimum. The electrostatic potentials that best fit the observed average electric field were calculated. It was found that the large-scale convection pattern significantly changes with season. This change involves the overall shape of the convection pattern, as well as the electric field intensity, and thus the total dawn-dusk potential across the polar cap. The cross polar cap potential drop is largest in fall, followed by winter, spring and summer. The small difference found between the summer and winter cross polar cap potential can be attributed to differing field-aligned potential drops. In view of the well-known relationship between field-aligned currents and parallel potential drop, this is consistent with the observations that Birkeland currents are larger in the summer than in winter. Changes in the overall shape of the convection pattern are consistent with the simple notion that the whole pattern is shifted toward the nightside as well as, to a lesser extent, toward the dawnside in summer as compared to winter. This assumption is based on the following observed effects: (1) The rotation of the overall convection pattern toward earlier local times with respect to the noon-midnight direction is maximum for summer on the dayside. (2) On the nightside, the Harang discontinuity is typically located within the radar field of view (Λ=67 to 82) in the winter averaged patterns, but it is equatorward of the field of view in summer. (3) The line that joins the dawn and dusk potential maxima is shifted toward the midnight sector in summer as compared to winter by about 5 degree. (4) In the dawn cell, the latitude of the convection reversal is the lowest during summer; in the dusk cell the latitude of the reversal is the lowest during winter

  17. The Evaluation of IL6 and ESR1 Gene Polymorphisms in Primary Dysmenorrhea.

    Science.gov (United States)

    Ozsoy, Asker Zeki; Karakus, Nevin; Yigit, Serbulent; Cakmak, Bulent; Nacar, Mehmet Can; Yılmaz Dogru, Hatice

    2016-01-01

    Primary dysmenorrhea is the most common gynecological complaint with painful menstrual cramps in pelvis without any pathology. It affects about half of menstruating women, and it causes significant disruption in quality of life. We investigated the association between IL6 gene promoter and ESR1 gene XbaI and PvuII polymorphisms and primary dysmenorrhea. In this case-control study, 152 unrelated young women with primary dysmenorrhea and 150 unrelated healthy age-matched controls participated. Genomic DNA was isolated and IL6 and ESR1 gene polymorphisms were genotyped using PCR-based RFLP assay. The distribution of genotype and allele frequencies of IL6 gene promoter and ESR1 gene XbaI polymorphisms were not statistically different between patients and controls (p > 0.05). However, the genotype and allele frequencies of ESR1 gene PvuII polymorphism showed statistically significant differences between primary dysmenorrhea patients and controls (p = 0.009 and p = 0.021, respectively). Statistically significant associations were also observed between age and married status of primary dysmenorrhea patients and ESR1 gene PvuII polymorphism (p = 0.044 and p = 0.023, respectively). In combined genotype analyses, AG at ESR1 XbaI and TC at ESR1 PvuII loci encoded a p-value of 0.027. Thus, individuals who are heterozygote at both loci have a lower risk of developing primary dysmenorrhea. Our study suggests no strong association between IL6 gene promoter and ESR1 gene XbaI polymorphisms and primary dysmenorrhea in Turkish women. However, ESR1 gene PvuII polymorphism showed statistically significant differences between primary dysmenorrhea patients and controls. The potential association between ESR1 gene PvuII polymorphism and age and married status of dysmenorrhea patients deserves further consideration.

  18. Compact high-field superconducting quadrupole magnet with holmium poles

    Energy Technology Data Exchange (ETDEWEB)

    Barlow, D.B.; Kraus, R.H. Jr.; Lobb, C.T.; Menzel, M.T. (Los Alamos National Lab., NM (United States)); Walstrom, P.L. (Grumman Space Systems, Los Alamos, NM (United States))

    1992-03-15

    A compact high-field superconducting quadrupole magnet was designed and built with poles made of the rare-earth metal holmium. The magnet is intended for use in superconducting coupled-cavity linear accelerators where compact high-field quadrupoles are needed, but where the use of permanent magnets is ruled out because of trapped-flux losses. The magnet has a clear bore diameter of 1.8 cm, outside diameter of 11 cm, length of 11 cm, and pole tip length of 6 cm. The effect of using holmium, a material with a higher saturation field than iron, was investigated by replacing poles made of iron with identical poles made of holmium. The magnet was operated at a temperature of 4.2 K and reached a peak quadrupole field gradient of 355 T/m, a 10% increase over the same magnet with iron poles. This increase in performance is consistent with calculations based on B-H curves that were measured for holmium at 4.2 K. (orig.).

  19. ESR characterization of point defects in amber colored c-BN super abrasive powders

    International Nuclear Information System (INIS)

    Nistor, S.V.; Ghica, D.; Stefan, M.; Bouwen, A.; Goovaerts, E.

    2004-01-01

    Cubic boron nitride (c-BN) crystalline superabrasive powder (Borazon ** CBN 400), consisting of 200-300 microns sized amber colored crystallites prepared by HP/HT synthesis, has been examined from 2.1 K to 293 K by X-band ESR spectroscopy. The observed spectrum consists of a component line A1, visible in the whole temperature range, and two component lines A2 and A3, visible at high and low temperatures, respectively. The A1 and A3 lines originate from transitions inside S = 1/2 ground states of distinct paramagnetic species and A2 from transitions inside an excited state of another paramagnetic center. The intensity of the A1 and A3 lines changes differently during in situ low temperature illumination in the UV-VIS range. * Borazon is a registered trademark of Diamond Innovations, Inc. (copyright 2004 WILEY-VCH Verlag GmbH and Co. KGaA, Weinheim) (orig.)

  20. Molecular organization and dynamics of micellar phase of polyelectrolyte-surfactant complexes: ESR spin probe study

    Science.gov (United States)

    Wasserman, A. M.; Kasaikin, V. A.; Zakharova, Yu. A.; Aliev, I. I.; Baranovsky, V. Yu.; Doseva, V.; Yasina, L. L.

    2002-04-01

    Molecular dynamics and organization of the micellar phase of complexes of linear polyelectrolytes with ionogenic and non-ionogenic surfactants was studied by the ESR spin probe method. Complexes of polyacrylic acid (PAA) and sodium polystyrenesulfonate (PSS) with alkyltrimethylammonium bromides (ATAB), as well as complexes of poly- N, N'-dimethyldiallylammonium chloride (PDACL) with sodium dodecylsulfate (SDS) were studied. The micellar phase of such complexes is highly organized molecular system, molecular ordering of which near the polymeric chain is much higher than in the 'center' of the micelle, it depends on the polymer-detergent interaction, flexibility of polymeric chain and length of carbonic part of the detergent molecule. Complexes of polymethacrylic acid (PMAA) with non-ionic detergent (dodecyl-substituted polyethyleneglycol), show that the local mobility of surfactant in such complexes is significantly lower than in 'free' micelles and depends on the number of micellar particles participating in formation of complexes.

  1. Sudden flux change studies in high field superconducting accelerator magnets

    International Nuclear Information System (INIS)

    Feher, S.; Bordini, B.; Carcagno, R.; Makulski, A.; Orris, D.F.; Pischalnikov, Y.M.; Sylvester, C.; Tartaglia, M.; Tompkins, J.C.; Zlobin, A.V.

    2004-01-01

    As part of the High Field Magnet Program at Fermilab many magnets have been tested which utilize multi strand Rutherford type cable made of state-of-the art Nb 3 Sn strands. During these magnet tests we observed sudden flux changes by monitoring coil voltages and the magnetic field close to the magnets. These flux changes might be linked to magnet instabilities. The voltage spike signals were correlated with quench antenna signals, a strong indication that these are magnet phenomena. With a new high resolution voltage spike detection system, we were able to observe the detailed structure of the spikes. Two fundamentally different signal shapes were distinguished, most likely generated by different mechanisms

  2. High resolution NMR imaging using a high field yokeless permanent magnet.

    Science.gov (United States)

    Kose, Katsumi; Haishi, Tomoyuki

    2011-01-01

    We measured the homogeneity and stability of the magnetic field of a high field (about 1.04 tesla) yokeless permanent magnet with 40-mm gap for high resolution nuclear magnetic resonance (NMR) imaging. Homogeneity was evaluated using a 3-dimensional (3D) lattice phantom and 3D spin-echo imaging sequences. In the central sphere (20-mm diameter), peak-to-peak magnetic field inhomogeneity was about 60 ppm, and the root-mean-square was 8 ppm. We measured room temperature, magnet temperature, and NMR frequency of the magnet simultaneously every minute for about 68 hours with and without the thermal insulator of the magnet. A simple mathematical model described the magnet's thermal property. Based on magnet performance, we performed high resolution (up to [20 µm](2)) imaging with internal NMR lock sequences of several biological samples. Our results demonstrated the usefulness of the high field small yokeless permanent magnet for high resolution NMR imaging.

  3. High resolution NMR imaging using a high field yokeless permanent magnet

    International Nuclear Information System (INIS)

    Kose, Katsumi; Haishi, Tomoyuki

    2011-01-01

    We measured the homogeneity and stability of the magnetic field of a high field (about 1.04 tesla) yokeless permanent magnet with 40-mm gap for high resolution nuclear magnetic resonance (NMR) imaging. Homogeneity was evaluated using a 3-dimensional (3D) lattice phantom and 3D spin-echo imaging sequences. In the central sphere (20-mm diameter), peak-to-peak magnetic field inhomogeneity was about 60 ppm, and the root-mean-square was 8 ppm. We measured room temperature, magnet temperature, and NMR frequency of the magnet simultaneously every minute for about 68 hours with and without the thermal insulator of the magnet. A simple mathematical model described the magnet's thermal property. Based on magnet performance, we performed high resolution (up to [20 μm] 2 ) imaging with internal NMR lock sequences of several biological samples. Our results demonstrated the usefulness of the high field small yokeless permanent magnet for high resolution NMR imaging. (author)

  4. Excitation thresholds of field-aligned irregularities and associated ionospheric hysteresis at very high latitudes observed using SPEAR-induced HF radar backscatter

    Directory of Open Access Journals (Sweden)

    D. M. Wright

    2009-07-01

    Full Text Available On 10 October 2006 the SPEAR high power radar facility was operated in a power-stepping mode where both CUTLASS radars were detecting backscatter from the SPEAR-induced field-aligned irregularities (FAIs. The effective radiated power of SPEAR was varied from 1–10 MW. The aim of the experiment was to investigate the power thresholds for excitation (Pt and collapse (Pc of artificially-induced FAIs in the ionosphere over Svalbard. It was demonstrated that FAI could be excited by a SPEAR ERP of only 1 MW, representing only 1/30th of SPEAR's total capability, and that once created the irregularities could be maintained for even lower powers. The experiment also demonstrated that the very high latitude ionosphere exhibits hysteresis, where the down-going part of the power cycle provided a higher density of irregularities than for the equivalent part of the up-going cycle. Although this second result is similar to that observed previously by CUTLASS in conjunction with the Tromsø heater, the same is not true for the equivalent incoherent scatter measurements. The EISCAT Svalbard Radar (ESR failed to detect any hysteresis in the plasma parameters over Svalbard in stark contract with the measurements made using the Tromsø UHF.

  5. Excitation thresholds of field-aligned irregularities and associated ionospheric hysteresis at very high latitudes observed using SPEAR-induced HF radar backscatter

    Directory of Open Access Journals (Sweden)

    D. M. Wright

    2009-07-01

    Full Text Available On 10 October 2006 the SPEAR high power radar facility was operated in a power-stepping mode where both CUTLASS radars were detecting backscatter from the SPEAR-induced field-aligned irregularities (FAIs. The effective radiated power of SPEAR was varied from 1–10 MW. The aim of the experiment was to investigate the power thresholds for excitation (Pt and collapse (Pc of artificially-induced FAIs in the ionosphere over Svalbard. It was demonstrated that FAI could be excited by a SPEAR ERP of only 1 MW, representing only 1/30th of SPEAR's total capability, and that once created the irregularities could be maintained for even lower powers. The experiment also demonstrated that the very high latitude ionosphere exhibits hysteresis, where the down-going part of the power cycle provided a higher density of irregularities than for the equivalent part of the up-going cycle. Although this second result is similar to that observed previously by CUTLASS in conjunction with the Tromsø heater, the same is not true for the equivalent incoherent scatter measurements. The EISCAT Svalbard Radar (ESR failed to detect any hysteresis in the plasma parameters over Svalbard in stark contract with the measurements made using the Tromsø UHF.

  6. High-field spin dynamics of antiferromagnetic quantum spin chains

    DEFF Research Database (Denmark)

    Enderle, M.; Regnault, L.P.; Broholm, C.

    2000-01-01

    present recent work on the high-field spin dynamics of the S = I antiferromagnetic Heisenberg chains NENP (Haldane ground state) and CsNiCl3 (quasi-1D HAF close to the quantum critical point), the uniform S = 1/2 chain CTS, and the spin-Peierls system CuGeO3. (C) 2000 Elsevier Science B,V. All rights...

  7. Breakdown of highly excited oxygen in a DC electric field

    International Nuclear Information System (INIS)

    Vagin, N.P.; Ionin, A.A.; Klimachev, Yu.M.; Sinitsin, D.V.; Yuryshev, N.N.; Deryugin, A.A.; Kochetov, I.V.; Napartovich, A.P.

    2000-01-01

    The breakdown of oxygen in a dc electric field is studied. A high concentration of oxygen molecules in the a 1 Δ g excited state is obtained in a purely chemical reactor. A decrease in the breakdown voltage at degrees of excitation exceeding 50% is observed. The theoretical decrement in the breakdown voltage obtained by solving the Boltzmann equation is in good agreement with the experimental data

  8. High magnetic field induced otolith fusion in the zebrafish larvae.

    Science.gov (United States)

    Pais-Roldán, Patricia; Singh, Ajeet Pratap; Schulz, Hildegard; Yu, Xin

    2016-04-11

    Magnetoreception in animals illustrates the interaction of biological systems with the geomagnetic field (geoMF). However, there are few studies that identified the impact of high magnetic field (MF) exposure from Magnetic Resonance Imaging (MRI) scanners (>100,000 times of geoMF) on specific biological targets. Here, we investigated the effects of a 14 Tesla MRI scanner on zebrafish larvae. All zebrafish larvae aligned parallel to the B0 field, i.e. the static MF, in the MRI scanner. The two otoliths (ear stones) in the otic vesicles of zebrafish larvae older than 24 hours post fertilization (hpf) fused together after the high MF exposure as short as 2 hours, yielding a single-otolith phenotype with aberrant swimming behavior. The otolith fusion was blocked in zebrafish larvae under anesthesia or embedded in agarose. Hair cells may play an important role on the MF-induced otolith fusion. This work provided direct evidence to show that high MF interacts with the otic vesicle of zebrafish larvae and causes otolith fusion in an "all-or-none" manner. The MF-induced otolith fusion may facilitate the searching for MF sensors using genetically amenable vertebrate animal models, such as zebrafish.

  9. Strong-field relativistic processes in highly charged ions

    Energy Technology Data Exchange (ETDEWEB)

    Postavaru, Octavian

    2010-12-08

    In this thesis we investigate strong-field relativistic processes in highly charged ions. In the first part, we study resonance fluorescence of laser-driven highly charged ions in the relativistic regime by solving the time-dependent master equation in a multi-level model. Our ab initio approach based on the Dirac equation allows for investigating highly relativistic ions, and, consequently, provides a sensitive means to test correlated relativistic dynamics, bound-state quantum electrodynamic phenomena and nuclear effects by applying coherent light with x-ray frequencies. Atomic dipole or multipole moments may be determined to unprecedented accuracy by measuring the interference-narrowed fluorescence spectrum. Furthermore, we investigate the level structure of heavy hydrogenlike ions in laser beams. Interaction with the light field leads to dynamic shifts of the electronic energy levels, which is relevant for spectroscopic experiments. We apply a fully relativistic description of the electronic states by means of the Dirac equation. Our formalism goes beyond the dipole approximation and takes into account non-dipole effects of retardation and interaction with the magnetic field components of the laser beam. We predicted cross sections for the inter-shell trielectronic recombination (TR) and quadruelectronic recombination processes which have been experimentally confirmed in electron beam ion trap measurements, mainly for C-like ions, of Ar, Fe and Kr. For Kr{sup 30}+, inter-shell TR contributions of nearly 6% to the total resonant photorecombination rate were found. (orig.)

  10. Irradiation of graphene field effect transistors with highly charged ions

    Energy Technology Data Exchange (ETDEWEB)

    Ernst, P.; Kozubek, R.; Madauß, L.; Sonntag, J.; Lorke, A.; Schleberger, M., E-mail: marika.schleberger@uni-due.de

    2016-09-01

    In this work, graphene field-effect transistors are used to detect defects due to irradiation with slow, highly charged ions. In order to avoid contamination effects, a dedicated ultra-high vacuum set up has been designed and installed for the in situ cleaning and electrical characterization of graphene field-effect transistors during irradiation. To investigate the electrical and structural modifications of irradiated graphene field-effect transistors, their transfer characteristics as well as the corresponding Raman spectra are analyzed as a function of ion fluence for two different charge states. The irradiation experiments show a decreasing mobility with increasing fluences. The mobility reduction scales with the potential energy of the ions. In comparison to Raman spectroscopy, the transport properties of graphene show an extremely high sensitivity with respect to ion irradiation: a significant drop of the mobility is observed already at fluences below 15 ions/μm{sup 2}, which is more than one order of magnitude lower than what is required for Raman spectroscopy.

  11. New developments in pulsed fields at the US National High Magnetic Field Laboratory

    International Nuclear Information System (INIS)

    Campbell, L.J.; Parkin, D.M.; Rickel, D.G.; Pernambuco-Wise, P.

    1996-01-01

    Los Alamos National Laboratory is a member of a consortium (with Florida State University and the University of Florida) to operate the National High Magnetic Field Laboratory (NHMFL), with funding from the National Science Foundation and the State of Florida. Los Alamos provides unique resources for its component of NHMFL in the form of a 1.4 GW inertial storage motor-generator for high field pulsed magnets and infrastructure for fields generated by flux compression. The NHMFL provides a user facility open to all qualified users, develops magnet technology in association with the private sector, and advances science and technology opportunities. The magnets in service at Los Alamos are of three types. Starting with the pre-existing explosive flux compression capability in 1991, NHMFL added capacitor-driven magnets in December, 1992, and a 20 tesla superconducting magnet in January, 1993. The capacitor-driven magnets continue to grow in diversity and accessibility, with four magnet stations now available for several different magnet types. Two magnets of unprecedented size and strength are nearing completion of assembly and design, respectively. Under final assembly is a quasi-continuous magnet that contains 90 MJ of magnetic energy at full field, and being designed is a non-destructive 100 T magnet containing 140 MJ

  12. Young's moduli of cables for high field superconductive dipole magnet

    International Nuclear Information System (INIS)

    Yamada, Shunji; Shintomi, Takakazu.

    1983-01-01

    Superconductive dipole magnets for big accelerators are subjected to enormous electro-magnetic force, when they are operated with high field such as 10 Tesla. They should be constructed by means of superconductive cables, which have high Young's modulus, to obtain good performance. To develop such cables we measured the Young's moduli of cables for practical use of accelerator magnets. They are monolithic and compacted strand cables. We measured also Young's moduli of monolithic copper and brass cables for comparison. The obtained data showed the Young's moduli of 35 and 15 GPa for the monolithic and compacted strand cables, respectively. (author)

  13. Quasi permanent superconducting magnet of very high field

    Science.gov (United States)

    Ren, Y.; Liu, J.; Weinstein, R.; Chen, I. G.; Parks, D.; Xu, J.; Obot, V.; Foster, C.

    1993-01-01

    We report on persistent field in a quasi-permanent magnet made of high temperature superconductor. The material has an average of 40 percent molar excess of Y, relative to Y1Ba2Cu3O7 and has been irradiated with high energy light ions at 200 MeV. The magnet, which traps 1.52 T at 77.3 K, traps nearly 4 T at 64.5 K. No evidence of giant flux jump or sample cracking was observed.

  14. The Mechanical Design Optimization of a High Field HTS Solenoid

    Energy Technology Data Exchange (ETDEWEB)

    Lalitha, SL; Gupta, RC

    2015-06-01

    This paper describes the conceptual design optimization of a large aperture, high field (24 T at 4 K) solenoid for a 1.7 MJ superconducting magnetic energy storage device. The magnet is designed to be built entirely of second generation (2G) high temperature superconductor tape with excellent electrical and mechanical properties at the cryogenic temperatures. The critical parameters that govern the magnet performance are examined in detail through a multiphysics approach using ANSYS software. The analysis results formed the basis for the performance specification as well as the construction of the magnet.

  15. The High Field Path to Practical Fusion Energy

    Science.gov (United States)

    Mumgaard, Robert; Whyte, D.; Greenwald, M.; Hartwig, Z.; Brunner, D.; Sorbom, B.; Marmar, E.; Minervini, J.; Bonoli, P.; Irby, J.; Labombard, B.; Terry, J.; Vieira, R.; Wukitch, S.

    2017-10-01

    We propose a faster, lower cost development path for fusion energy enabled by high temperature superconductors, devices at high magnetic field, innovative technologies and modern approaches to technology development. Timeliness, scale, and economic-viability are the drivers for fusion energy to combat climate change and aid economic development. The opportunities provided by high-temperature superconductors, innovative engineering and physics, and new organizational structures identified over the last few years open new possibilities for realizing practical fusion energy that could meet mid-century de-carbonization needs. We discuss re-factoring the fusion energy development path with an emphasis on concrete risk retirement strategies utilizing a modular approach based on the high-field tokamak that leverages the broader tokamak physics understanding of confinement, stability, and operational limits. Elements of this plan include development of high-temperature superconductor magnets, simplified immersion blankets, advanced long-leg divertors, a compact divertor test tokamak, efficient current drive, modular construction, and demountable magnet joints. An R&D plan culminating in the construction of an integrated pilot plant and test facility modeled on the ARC concept is presented.

  16. ESR1 Is Co-Expressed with Closely Adjacent Uncharacterised Genes Spanning a Breast Cancer Susceptibility Locus at 6q25.1

    Science.gov (United States)

    Dunbier, Anita K.; Anderson, Helen; Ghazoui, Zara; Lopez-Knowles, Elena; Pancholi, Sunil; Ribas, Ricardo; Drury, Suzanne; Sidhu, Kally; Leary, Alexandra; Martin, Lesley-Ann; Dowsett, Mitch

    2011-01-01

    Approximately 80% of human breast carcinomas present as oestrogen receptor α-positive (ER+ve) disease, and ER status is a critical factor in treatment decision-making. Recently, single nucleotide polymorphisms (SNPs) in the region immediately upstream of the ER gene (ESR1) on 6q25.1 have been associated with breast cancer risk. Our investigation of factors associated with the level of expression of ESR1 in ER+ve tumours has revealed unexpected associations between genes in this region and ESR1 expression that are important to consider in studies of the genetic causes of breast cancer risk. RNA from tumour biopsies taken from 104 postmenopausal women before and after 2 weeks treatment with an aromatase (oestrogen synthase) inhibitor was analyzed on Illumina 48K microarrays. Multiple-testing corrected Spearman correlation revealed that three previously uncharacterized open reading frames (ORFs) located immediately upstream of ESR1, C6ORF96, C6ORF97, and C6ORF211 were highly correlated with ESR1 (Rs = 0.67, 0.64, and 0.55 respectively, FDRaccount for the correlations. The correlations were maintained in cultured cells. An ERα antagonist did not affect the ORFs' expression or their correlation with ESR1, suggesting their transcriptional co-activation is not directly mediated by ERα. siRNA inhibition of C6ORF211 suppressed proliferation in MCF7 cells, and C6ORF211 positively correlated with a proliferation metagene in tumours. In contrast, C6ORF97 expression correlated negatively with the metagene and predicted for improved disease-free survival in a tamoxifen-treated published dataset, independently of ESR1. Our observations suggest that some of the biological effects previously attributed to ER could be mediated and/or modified by these co-expressed genes. The co-expression and function of these genes may be important influences on the recently identified relationship between SNPs in this region and breast cancer risk. PMID:21552322

  17. ESR1 is co-expressed with closely adjacent uncharacterised genes spanning a breast cancer susceptibility locus at 6q25.1.

    Directory of Open Access Journals (Sweden)

    Anita K Dunbier

    2011-04-01

    Full Text Available Approximately 80% of human breast carcinomas present as oestrogen receptor α-positive (ER+ve disease, and ER status is a critical factor in treatment decision-making. Recently, single nucleotide polymorphisms (SNPs in the region immediately upstream of the ER gene (ESR1 on 6q25.1 have been associated with breast cancer risk. Our investigation of factors associated with the level of expression of ESR1 in ER+ve tumours has revealed unexpected associations between genes in this region and ESR1 expression that are important to consider in studies of the genetic causes of breast cancer risk. RNA from tumour biopsies taken from 104 postmenopausal women before and after 2 weeks treatment with an aromatase (oestrogen synthase inhibitor was analyzed on Illumina 48K microarrays. Multiple-testing corrected Spearman correlation revealed that three previously uncharacterized open reading frames (ORFs located immediately upstream of ESR1, C6ORF96, C6ORF97, and C6ORF211 were highly correlated with ESR1 (Rs =  0.67, 0.64, and 0.55 respectively, FDR<1 × 10(-7. Publicly available datasets confirmed this relationship in other groups of ER+ve tumours. DNA copy number changes did not account for the correlations. The correlations were maintained in cultured cells. An ERα antagonist did not affect the ORFs' expression or their correlation with ESR1, suggesting their transcriptional co-activation is not directly mediated by ERα. siRNA inhibition of C6ORF211 suppressed proliferation in MCF7 cells, and C6ORF211 positively correlated with a proliferation metagene in tumours. In contrast, C6ORF97 expression correlated negatively with the metagene and predicted for improved disease-free survival in a tamoxifen-treated published dataset, independently of ESR1. Our observations suggest that some of the biological effects previously attributed to ER could be mediated and/or modified by these co-expressed genes. The co-expression and function of these genes may be

  18. Enhanced Field Emission Studies on Niobium Surfaces Relevant to High Field Superconducting Radio-Frequency Devices

    International Nuclear Information System (INIS)

    Tong Wang

    2002-01-01

    Enhanced field emission (EFE) presents the main impediment to higher acceleration gradients in superconducting niobium (Nb) radio frequency cavities for particle accelerators. The strength, number and sources of EFE sites strongly depend on surface preparation and handling. The main objective of this thesis project is to systematically investigate the sources of EFE from Nb, to evaluate the best available surface preparation techniques with respect to resulting field emission, and to establish an optimized process to minimize or eliminate EFE. To achieve these goals, a scanning field emission microscope (SFEM) was designed and built as an extension to an existing commercial scanning electron microscope (SEM). In the SFEM chamber of ultra high vacuum, a sample is moved laterally in a raster pattern under a high voltage anode tip for EFE detection and localization. The sample is then transferred under vacuum to the SEM chamber equipped with an energy-dispersive x-ray spectrometer for individual emitting site characterization. Compared to other systems built for similar purposes, this apparatus has low cost and maintenance, high operational flexibility, considerably bigger scan area, as well as reliable performance. EFE sources from planar Nb have been studied after various surface preparation, including chemical etching and electropolishing, combined with ultrasonic or high-pressure water rinse. Emitters have been identified, analyzed and the preparation process has been examined and improved based on EFE results. As a result, field-emission-free or near field-emission-free surfaces at ∼140 MV/m have been consistently achieved with the above techniques. Characterization on the remaining emitters leads to the conclusion that no evidence of intrinsic emitters, i.e., no fundamental electric field limit induced by EFE, has been observed up to ∼140 MV/m. Chemically etched and electropolished Nb are compared and no significant difference is observed up to ∼140 MV

  19. Enhanced Field Emission Studies on Niobium Surfaces Relevant to High Field Superconducting Radio-Frequency Devices

    Energy Technology Data Exchange (ETDEWEB)

    Wang, Tong [Virginia Polytechnic Inst. and State Univ. (Virginia Tech), Blacksburg, VA (United States)

    2002-09-18

    Enhanced field emission (EFE) presents the main impediment to higher acceleration gradients in superconducting niobium (Nb) radiofrequency cavities for particle accelerators. The strength, number and sources of EFE sites strongly depend on surface preparation and handling. The main objective of this thesis project is to systematically investigate the sources of EFE from Nb, to evaluate the best available surface preparation techniques with respect to resulting field emission, and to establish an optimized process to minimize or eliminate EFE. To achieve these goals, a scanning field emission microscope (SFEM) was designed and built as an extension to an existing commercial scanning electron microscope (SEM). In the SFEM chamber of ultra high vacuum, a sample is moved laterally in a raster pattern under a high voltage anode tip for EFE detection and localization. The sample is then transferred under vacuum to the SEM chamber equipped with an energy-dispersive x-ray spectrometer for individual emitting site characterization. Compared to other systems built for similar purposes, this apparatus has low cost and maintenance, high operational flexibility, considerably bigger scan area, as well as reliable performance. EFE sources from planar Nb have been studied after various surface preparation, including chemical etching and electropolishing, combined with ultrasonic or high-pressure water rinse. Emitters have been identified, analyzed and the preparation process has been examined and improved based on EFE results. As a result, field-emission-free or near field-emission-free surfaces at ~140 MV/m have been consistently achieved with the above techniques. Characterization on the remaining emitters leads to the conclusion that no evidence of intrinsic emitters, i.e., no fundamental electric field limit induced by EFE, has been observed up to ~140 MV/m. Chemically etched and electropolished Nb are compared and no significant difference is observed up to ~140 MV/m. To

  20. Operation of cold-cathode gauges in high magnetic fields

    International Nuclear Information System (INIS)

    Thomas, S.R. Jr.; Goerz, D.A.; Pickles, W.L.

    1985-01-01

    The Mirror Fusion Test Facility (MFTF-B), under construction at LLNL, requires measurement of the neutral gas density in high magnetic fields near the plasma at several axial regions. This Background Gas Pressure (BGP) diagnostic will help us understand the role of background neutrals in particle and power balance, particularly in the maintenance of the cold halo plasma that shields the hot core plasma from the returning neutrals. It consists of several cold-cathode, magnetron-type gauges stripped of their permanent magnets, and utilizes the MFTF-B ambient B-field in strengths of 5 to 25 kG. Similar gauges have operated in TMX-U in B-fields up to 3 kG. To determine how well the gauges will perform, we assembled a test stand which operated magnetron gauges in an external, uniform magnetic field of up to 30 kG, over a pressure range of 1E-8 T to 1E-5 T, at several cathode voltages. This paper describes the test stand and presents the results of the tests

  1. ESR imaging investigations of two-phase systems.

    Science.gov (United States)

    Herrmann, Werner; Stösser, Reinhard; Borchert, Hans-Hubert

    2007-06-01

    The possibilities of electron spin resonance (ESR) and electron spin resonance imaging (ESRI) for investigating the properties of the spin probes TEMPO and TEMPOL in two-phase systems have been examined in the systems water/n-octanol, Miglyol/Miglyol, and Precirol/Miglyol. Phases and regions of the phase boundary could be mapped successfully by means of the isotropic hyperfine coupling constants, and, moreover, the quantification of rotational and lateral diffusion of the spin probes was possible. For the quantitative treatment of the micropolarity, a simplified empirical model was established on the basis of the Nernst distribution and the experimentally determined isotropic hyperfine coupling constants. The model does not only describe the summarized micropolarities of coexisting phases, but also the region of the phase boundary, where solvent molecules of different polarities and tendencies to form hydrogen bonds compete to interact with the NO group of the spin probe. Copyright 2007 John Wiley & Sons, Ltd.

  2. Human estrogen receptor (ESR) gene locus: PssI dimorphism

    Energy Technology Data Exchange (ETDEWEB)

    Coleman, R T; Taylor, J E; Frossard, P M [California Biotechnology Inc., Mountain View, CA (USA); Shine, J J [Garvan Institute, Darlinghurst (Australia)

    1988-07-25

    pESR-2, a 2.1 kb partial cDNA containing the entire translated sequence of the human estrogen receptor mRNA isolated from MCF-7 human breast cancer cells, was subcloned in the Eco RI site of pBR322. PssI (PuGGNCCPy) identifies a single two-allele polymorphism with bands at either 1.7 or 1.4 kb, as well as invariant bands at 12.6, 9.3, 4.1, 3.7, 2.4, 2.2, and 1.2 kb. Its frequency was studied in 77 unrelated North American Caucasians. The human estrogen receptor gene has been localized to 6q24 -- q27 by in situ hybridization. Co-dominant segregation is demonstrated in one family (8 individuals).

  3. Broadband lasercooling of relativistic ions at the ESR

    Energy Technology Data Exchange (ETDEWEB)

    Winters, Danyal; Ullmann, Johannes; Clark, Colin; Dimopoulou, Christina; Nolden, Fritz; Steck, Markus [GSI Darmstadt (Germany); Bussmann, Michael; Siebold, Mathias; Seltmann, Michael; Schramm, Ulrich [HZDR Dresden (Germany); Wen, Weiqiang [GSI Darmstadt (Germany); IMP CAS Lanzhou (China); Sanchez, Rodolfo; Lochmann, Matthias [GSI Darmstadt (Germany); Uni Mainz (Germany); Beck, Tobias; Rein, Benjamin; Tichelmann, Sascha; Birkl, Gerhard; Walther, Thomas [TU Darmstadt (Germany); Zhang, Dacheng; Yang, Jie; Ma, Xinwen [IMP CAS Lanzhou (China); Noertershaeuser, Wilfried [GSI Darmstadt (Germany); Uni Mainz (Germany); TU Darmstadt (Germany); Kuehl, Thomas [GSI Darmstadt (Germany); Uni Mainz (Germany); HI Jena (Germany); Stoehlker, Thomas [GSI Darmstadt (Germany); Uni Jena (Germany); HI Jena (Germany)

    2013-07-01

    We present new results on broadband laser cooling of stored relativistic C{sup 3+} ion beams at the ESR in Darmstadt. For the first time we could show laser cooling of bunched relativistic ion beams using a UV-laser which could scan over a very large range and thus cool all the ions in the 'bucket'. This scheme is much more versatile than a previous scheme, where the bunching frequency was scanned relative to a fixed laser frequency. We have also demonstrated that this cooling scheme works without pre-electron cooling, which is a prerequisite for its general application to future storage rings and synchrotrons, such as the HESR and the SIS100 at FAIR. We also present results from in vacuo VUV-fluorescence detectors, which have proven to be very effective.

  4. An ESR study on the detection of irradiated red lentil

    International Nuclear Information System (INIS)

    Ercan, I.; Eken, M.

    2001-01-01

    The purpose of this work is to investigate in detail detection of irradiated red lentil. In this way, red lentil powder was analysed by using Bruker EMX ESR spectrometer before and after irradiation between the doses 1-9 kGy at ambient conditions. It was observed that seeds of non-irradiated and irradiated red lentil have a signal having six lines due to Mn''+''2 content. However hull of the red lentil has a single line whose origin is still unknown. Besides, this signal has superposed with the radiation induced one. It was also found that the intensity of radiation induced signal was decreased logarithmically in time, and the change in the intensity was minimal at low doses

  5. ESR concept paper on value-based radiology.

    Science.gov (United States)

    2017-10-01

    The European Society of Radiology (ESR) established a Working Group on Value-Based Imaging (VBI WG) in August 2016 in response to developments in European healthcare systems in general, and the trend within radiology to move from volume- to value-based practice in particular. The value-based healthcare (VBH) concept defines "value" as health outcomes achieved for patients relative to the costs of achieving them. Within this framework, value measurements start at the beginning of therapy; the whole diagnostic process is disregarded, and is considered only if it is the cause of errors or complications. Making the case for a new, multidisciplinary organisation of healthcare delivery centred on the patient, this paper establishes the diagnosis of disease as a first outcome in the interrelated activities of the healthcare chain. Metrics are proposed for measuring the quality of radiologists' diagnoses and the various ways in which radiologists provide value to patients, other medical specialists and healthcare systems at large. The ESR strongly believes value-based radiology (VBR) is a necessary complement to existing VBH concepts. The Society is determined to establish a holistic VBR programme to help European radiologists deal with changes in the evolution from volume- to value-based evaluation of radiological activities. Main Messages • Value-based healthcare defines value as patient's outcome over costs. • The VBH framework disregards the diagnosis as an outcome. • VBH considers diagnosis only if wrong or a cause of complications. • A correct diagnosis is the first outcome that matters to patients. • Metrics to measure radiologists' impacts on patient outcomes are key. • The value provided by radiology is multifaceted, going beyond exam volumes.

  6. Field experimental observations of highly graded sediment plumes.

    Science.gov (United States)

    Jensen, Jacob Hjelmager; Saremi, Sina; Jimenez, Carlos; Hadjioannou, Louis

    2015-06-15

    A field experiment in the waters off the south-eastern coast of Cyprus was carried out to study near-field formation of sediment plumes from dumping. Different loads of sediment were poured into calm and limpid waters one at the time from just above the sea surface. The associated plumes, gravitating towards the seafloor, were filmed simultaneously by four divers situated at different depths in the water column, and facing the plume at different angles. The processes were captured using GoPro-Hero-series cameras. The high-quality underwater footage from near-surface, mid-depth and near-bed positions gives unique insight into the dynamics of the descending plume and near-field dispersion processes, and enables good understanding of flow and sediment transport processes involved from-release-to-deposition of the load in a non-scaled environment. The high resolution images and footages are available through the link provided herein. Observations support the development of a detailed multi-fractional sediment plume model. Copyright © 2015 Elsevier Ltd. All rights reserved.

  7. High ionization radiation field remote visualization device - shielding requirements

    International Nuclear Information System (INIS)

    Fernandez, Antonio P. Rodrigues; Omi, Nelson M.; Silveira, Carlos Gaia da; Calvo, Wilson A. Pajero

    2011-01-01

    The high activity sources manipulation hot-cells use special and very thick leaded glass windows. This window provides a single sight of what is being manipulated inside the hot-cell. The use of surveillance cameras would replace the leaded glass window, provide other sights and show more details of the manipulated pieces, using the zoom capacity. Online distant manipulation may be implemented, too. The limitation is their low ionizing radiation resistance. This low resistance also limited the useful time of robots made to explore or even fix problematic nuclear reactor core, industrial gamma irradiators and high radioactive leaks. This work is a part of the development of a high gamma field remote visualization device using commercial surveillance cameras. These cameras are cheap enough to be discarded after the use for some hours of use in an emergency application, some days or some months in routine applications. A radiation shield can be used but it cannot block the camera sight which is the shield weakness. Estimates of the camera and its electronics resistance may be made knowing each component behavior. This knowledge is also used to determine the optical sensor type and the lens material, too. A better approach will be obtained with the commercial cameras working inside a high gamma field, like the one inside of the IPEN Multipurpose Irradiator. The goal of this work is to establish the radiation shielding needed to extend the camera's useful time to hours, days or months, depending on the application needs. (author)

  8. ESR technique for noninvasive way to quantify cyclodextrins effect on cell membranes

    International Nuclear Information System (INIS)

    Grammenos, A.; Mouithys-Mickalad, A.; Guelluy, P.H.; Lismont, M.; Piel, G.; Hoebeke, M.

    2010-01-01

    Research highlights: → ESR: a new tool for cyclodextrins study on living cells. → Cholesterol and phospholipid extraction by Rameb in a dose- and time-dependent way. → Extracted phospholipids and cholesterol form stable aggregates. → ESR spectra show that lipid rafts are damaged by Rameb. → Quantification of the cholesterol extraction on cell membranes in a noninvasive way. -- Abstract: A new way to study the action of cyclodextrin was developed to quantify the damage caused on cell membrane and lipid bilayer. The Electron Spin Resonance (ESR) spectroscopy was used to study the action of Randomly methylated-beta-cyclodextrin (Rameb) on living cells (HCT-116). The relative anisotropy observed in ESR spectrum of nitroxide spin probe (5-DSA and cholestane) is directly related to the rotational mobility of the probe, which can be further correlated with the microviscosity. The use of ESR probes clearly shows a close correlation between cholesterol contained in cells and cellular membrane microviscosity. This study also demonstrates the Rameb ability to extract cholesterol and phospholipids in time- and dose-dependent ways. In addition, ESR spectra enabled to establish that cholesterol is extracted from lipid rafts to form stable aggregates. The present work supports that ESR is an easy, reproducible and noninvasive technique to study the effect of cyclodextrins on cell membranes.

  9. High current superconductors for tokamak toroidal field coils

    International Nuclear Information System (INIS)

    Fietz, W.A.

    1976-01-01

    Conductors rated at 10,000 A for 8 T and 4.2 K are being purchased for the first large coil segment tests at ORNL. Requirements for these conductors, in addition to the high current rating, are low pulse losses, cryostatic stability, and acceptable mechanical properties. The conductors are required to have losses less than 0.4 W/m under pulsed fields of 0.5 T with a rise time of 1 sec in an ambient 8-T field. Methods of calculating these losses and techniques for verifying the performance by direct measurement are discussed. Conductors stabilized by two different cooling methods, pool boiling and forced helium flow, have been proposed. Analysis of these conductors is presented and a proposed definition and test of stability is discussed. Mechanical property requirements, tensile and compressive, are defined and test methods are discussed

  10. High-resolution field shaping utilizing a masked multileaf collimator.

    Science.gov (United States)

    Williams, P C; Cooper, P

    2000-08-01

    Multileaf collimators (MLCs) have become an important tool in the modern radiotherapy department. However, the current limit of resolution (1 cm at isocentre) can be too coarse for acceptable shielding of all fields. A number of mini- and micro-MLCs have been developed, with thinner leaves to achieve approved resolution. Currently however, such devices are limited to modest field sizes and stereotactic applications. This paper proposes a new method of high-resolution beam collimation by use of a tertiary grid collimator situated below the conventional MLC. The width of each slit in the grid is a submultiple of the MLC width. A composite shaped field is thus built up from a series of subfields, with the main MLC defining the length of each strip within each subfield. Presented here are initial findings using a prototype device. The beam uniformity achievable with such a device was examined by measuring transmission profiles through the grid using a diode. Profiles thus measured were then copied and superposed to generate composite beams, from which the uniformity achievable could be assessed. With the average dose across the profile normalized to 100%, hot spots up to 5.0% and troughs of 3% were identified for a composite beam of 2 x 5.0 mm grids, as measured at Dmax for a 6 MV beam. For a beam composed from 4 x 2.5 mm grids, the maximum across the profile was 3.0% above the average, and the minimum 2.5% below. Actual composite profiles were also formed using the integrating properties of film, with the subfield indexing performed using an engineering positioning stage. The beam uniformity for these fields compared well with that achieved in theory using the diode measurements. Finally sine wave patterns were generated to demonstrate the potential improvements in field shaping and conformity using this device as opposed to the conventional MLC alone. The scalloping effect on the field edge commonly seen on MLC fields was appreciably reduced by use of 2 x 5.0 mm

  11. 2 mm range ESR of the transmutation-produced phosphorus impurity in 6HSiC

    International Nuclear Information System (INIS)

    Kalabukhova, E.N.; Lukin, S.N.; Mokhov, E.N.

    1993-01-01

    Phosphorus impurity is introduced into 6HSiC monocrystals via neutron transmutation doping. Parameters of ESR two spectra referred to ESR spectra of separated phosphorus atoms in the lattice cubic and hexagonal position are detected and determined in the specimens at T=4.2 K. variation dynamics of ESR spectra of phosphorus and nitrogen within 4.2-73 K temperature range is studied. Ionization energies of phosphorus atoms are determined to be less, than those of nitrogen atoms, and ionization energy of phosphorus atoms in hexagonal position is higher, than that of phosphorus atoms in cubic position

  12. μSR spectroscopy on free radicals: a complement to ESR spectroscopy

    International Nuclear Information System (INIS)

    Cox, S.F.J.; Symons, M.C.R.

    1986-12-01

    The paper on ''μSR spectroscopy on free radicals'' was presented to the conference on ''Muon spin, rotation, relaxation and resonance'' Uppsala, 1986. The spectroscopic techniques for both ESR and μSR are described, along with the interpretation of the spectra, hyperfine coupling constants and radical structure. A comparison of ESR and μSR data is carried out with respect: to 1) isotope effects in organic radicals, 2) isotope effects in solids, -the isotropic muonium defect centres, and 3) the muonium defect centres in semiconductors. Radical categories examined using ESR and μSR are discussed, including new species, formation mechanisms, and ionic species. (U.K.)

  13. High Field Magnet R and D in the USA

    International Nuclear Information System (INIS)

    Gourlay, Stephen A.

    2003-01-01

    Accelerator magnet technology is currently dominated by the use of NbTi superconductor. New and more demanding applications for superconducting accelerator magnets require the use of alternative materials. Several programs in the US are taking advantage of recent improvements in Nb 3 Sn to develop high field magnets for new applications. Highlights and challenges of the US R and D program are presented along with the status of conductor development. In addition, a new R and D focus, the US LHC Accelerator Research Program, will be discussed

  14. High Field Magnet R and D in the USA

    International Nuclear Information System (INIS)

    Gourlay, S.A.

    2003-01-01

    Accelerator magnet technology is currently dominated by the use of NbTi superconductor. New and more demanding applications for superconducting accelerator magnets require the use of alternative materials. Several programs in the US are taking advantage of recent improvements in Nb 3 Sn to develop high field magnets for new applications. Highlights and challenges of the US R and D program are presented along with the status of conductor development. In addition, a new R and D focus, the US LHC Accelerator Research Program, will be discussed.

  15. High magnetic field magnetization of a new triangular lattice antiferromagnet

    Energy Technology Data Exchange (ETDEWEB)

    Zhou, H. D. [Univ. of Tennessee, Knoxville, TN (United States); Los Alamos National Lab. (LANL), Los Alamos, NM (United States). National High Magnetic Field Lab. (MagLab); Stritzinger, Laurel Elaine Winter [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Harrison, Neil [Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

    2017-03-23

    In CsV(MoO4)2, the magnetic V3+ ions with octahedral oxygen-coordination form a geometrically frustrated triangular lattice. So fare, there is no magnetic properties reported on it. Recently, we successfully grew single crystals of CsV(MoO4)2 by using flux method. The susceptibility shows a sharp drop around 24 K, representing a long range magnetic ordering. To understand the physical properties of this new triangular lattice antiferromagnet (TLAF), we pursued high field magnetization measurements to answer two questions: (i) what is the saturation field, which will be very useful to calculate the exchange interaction of the system? (ii) Will it exhibit spin state transition, such as the up up down phase with 1/3-saturation moment as other TLAFs? Recently, we performed VSM measurements in Cell 8, Tallahassee, NHMFL, the results show that the magnetization reaches 0.38 MuB at 34 T, which is just 19% of the full moment of 2 MuB for V3+ (3d2) ions. Apparently we need higher field to reach 1/3 value or full moment.

  16. Avo analysis in the high impedance reservoir of Chuchupa Field

    International Nuclear Information System (INIS)

    Cediel Mauricio; Almanza Ovidio; Montes Luis

    2012-01-01

    The technique of bright spot as a direct indicator of hydrocarbons has been widely used since the work of Ostrander (1984), particularly in gas fields. Located at north of Colombia, the Chuchupa field has produced gas continuously during 30 years, but despite the coverage with 2D seismic, amplitude anomalies associated with gas accumulation have not been observed. In order to find the relationships between the amplitude information and the gas accumulation, an AVO analysis was performed to describe the seismic reservoir response. The raw data of a 2D seismic line that crosses the field from East to West and a well log data set were used. In a first approach the seismic response was modeled using well logs, so a comparative analysis between the furnished synthetic seismograms and the real CDP gathers was done. The results indicated that the reservoirs top is represented by a low amplitude peak which decreases when the offset increases but whose phase remains unchanged. In the well, where the reservoir has 100% gas saturation, a high correlation between the synthetic and real CDP gathers was observed. In a second approach, anomalous clustered points in the IV quadrant were discriminated through intercept versus gradient cross plot analysis. A weak Class-I anomaly was identified, which could not be observed in stacked sections and hence it should be analyzed using pre-stack data.

  17. High magnetic field properties of Fe-pnictide thin films

    Energy Technology Data Exchange (ETDEWEB)

    Kurth, Fritz

    2015-11-20

    The recent discovery of high-temperature superconductivity in Fe-based materials triggered worldwide efforts to investigate their fundamental properties. Despite a lot of similarities to cuprates and MgB{sub 2}, important differences like near isotropic behaviour in contrast to cuprates and the peculiar pairing symmetry of the order parameter (OP) have been reported. The OP symmetry of Fe-based superconductors (FBS) was theoretically predicted to be of so-called s± state prior to various experimental works. Still, most of the experimental results favour the s± scenario; however, definitive evidence has not yet been reported. Although no clear understanding of the superconducting mechanisms yet exists, potential applications such as high-field magnets and Josephson devices have been explored. Indeed, a lot of reports about FBS tapes, wires, and even SQUIDs have been published to this date. In this thesis, the feasibility of high-field magnet applications of FBS is addressed by studying their transport properties, involving doped BaFe{sub 2}As{sub 2} (Ba-122) and LnFeAs(O,F) [Ln=Sm and Nd]. Particularly, it is important to study physical properties in a sample form (i.e. thin films) that is close to the conditions found in applications. However, the realisation of epitaxial FBS thin films is not an easy undertaking. Recent success in growing epitaxial FBS thin films opens a new avenue to delve into transport critical current measurements. The information obtained through this research will be useful for exploring high-field magnet applications. This thesis consists of 7 chapters: Chapter 1 describes the motivation of this study, the basic background of superconductivity, and a brief summary of the thin film growth of FBS. Chapter 2 describes experimental methods employed in this study. Chapter 3 reports on the fabrication of Co-doped Ba-122 thin films on various substrates. Particular emphasis lies on the discovery of fluoride substrates to be beneficial for

  18. Contribution of polymorphisms in ESR1, ESR2, FSHR, CYP19A1 ...

    Indian Academy of Sciences (India)

    2016-03-04

    Mar 4, 2016 ... 1Department of Medical Genetics, and 2Department of Neurology, Dicle University, Medical Faculty, ... analysis was performed only in women, the GG genotype of ... tor interacting protein 1 (NRIP1) negatively regulates the ... High FSH levels and low oestrogen levels have been asso- ...... meta-analysis.

  19. Production of highly charged ions of argon by optical field ionization in a relativistic laser field

    International Nuclear Information System (INIS)

    Sagisaka, Akito; Akahane, Yutaka; Aoyama, Makoto; Nakano, Fumihiko; Yamakawa, Koichi

    2001-01-01

    We observed the highly charged ions of argon by optical field ionization in a relativistic intensity regime. Charge states up to Ar 15+ were produced at the highest intensity of 800 nm, linearly polarized 20 fs Ti: sapphire laser pulses. The peak intensity of the pulse is determined by comparing the measured ion production curve for Ar 9+ with ADK theory. The results of these measurements of the ionization indicate that the maximum peak intensity is achieved to ∼2x10 19 W/cm 2 . (author)

  20. Flow field design for high-pressure PEM electrolysis cells

    DEFF Research Database (Denmark)

    Olesen, Anders Christian; Kær, Søren Knudsen

    -water distributes. Water not only serves a reactant, it also aids in cooling due to its high specific heat capacity. The movement of liquid water at the anode is difficult to model, since it is highly coupled to the formation of gas bubbles. To capture the complex two-phase flow behaviour that takes place within...... micro-channels and porous media, our research group has developed an Euler-Euler model in the computational fluid dynamics modelling framework of ANSYS CFX. In addition to two-phase flow, the model accounts for turbulence, species transport in the gas phase, heat transport in all three phases (i.......e. solid, gas and liquid), as well as charge transport of electrons and ions. Our recent improvements have focused on the models ability to account for phase change and electrochemistry as well as the modelling of two-phase flow regimes. For comparison, an interdigitated and parallel channel flow field...

  1. Internal Stresses in Wires for High Field Magnets

    International Nuclear Information System (INIS)

    Han, K.; Embury, J.D.; Lawson, A.C.; Von Dreele, R.B.; Wood, J.T.; Richardson, J.W. Jr.

    1998-01-01

    The codeformation of Cu-Ag or Cu-Nb composite wires used for high field magnets has a number of important microstructural consequences, including the production of very fine scale structures, the development of very high internal surface area to volume ratios during the drawing and the storage of defects at interphase interfaces. In addition, the fabrication and codeformation of phases which differ in crystal structure, thermal expansion, elastic modulus and lattice parameter lead to the development of short wavelength internal stresses. These internal stresses are measured by neutron diffraction and transmission electron microscopy as a function of the imposed drawing strain. The internal stresses lead to important changes in elastic plastic response which can be related to both magnet design and service life and these aspects will be described in detail

  2. Fusion Performance of High Magnetic Field Expe-riments

    Science.gov (United States)

    Airoldi, A.; Cenacchi, G.; Coppi, B.

    1997-11-01

    High magnetic field machines have the characteristic of operating well within the usual limitations known as density and beta limits. This feature is highlighted in the Ignitor concept thanks to its reference field of up to 13 T on the magnetic axis and its high current densities. The two reference scenarios with plasma currents of 12 MA and 11 MA respectively, are discussed. The ramp time is 4 sec for both scenarios, whereas the following programmed time dependence of the current is different. The results of an extensive series of numerical simulations using an appropriate version of the 1+1/2D JETTO transport code show that in any case optimal fusion performances are reacheable without needing enhancement over the values of the energy replacement time predicted by the most pessimistic scalings (for the so-called L-mode regime). The density is the crucial parameter involved on the path to ignition that can be achieved provided the density rise is carefully programmed. The density profiles can be controlled by the proper use of the pellet injector that is included in the machine design.

  3. Velocity field measurements on high-frequency, supersonic microactuators

    Science.gov (United States)

    Kreth, Phillip A.; Ali, Mohd Y.; Fernandez, Erik J.; Alvi, Farrukh S.

    2016-05-01

    The resonance-enhanced microjet actuator which was developed at the Advanced Aero-Propulsion Laboratory at Florida State University is a fluidic-based device that produces pulsed, supersonic microjets by utilizing a number of microscale, flow-acoustic resonance phenomena. The microactuator used in this study consists of an underexpanded source jet that flows into a cylindrical cavity with a single, 1-mm-diameter exhaust orifice through which an unsteady, supersonic jet issues at a resonant frequency of 7 kHz. The flowfields of a 1-mm underexpanded free jet and the microactuator are studied in detail using high-magnification, phase-locked flow visualizations (microschlieren) and two-component particle image velocimetry. These are the first direct measurements of the velocity fields produced by such actuators. Comparisons are made between the flow visualizations and the velocity field measurements. The results clearly show that the microactuator produces pulsed, supersonic jets with velocities exceeding 400 m/s for roughly 60 % of their cycles. With high unsteady momentum output, this type of microactuator has potential in a range of ow control applications.

  4. Development of high temperature superconductors for magnetic field applications

    International Nuclear Information System (INIS)

    Larbalestier, D.C.

    1991-01-01

    The key requirement for magnetic field applications of high temperature superconductor (HTS) materials is to have conductors with high transport critical current density available for magnet builders. After 3 or 4 years of being without any such object, conductor makers have had recent success in producing simple conductor prototypes. These have permitted the construction of simple HTS magnets having self fields exceeding 1 tesla at 4K. Thus the scientific feasibility of making powerful HTS magnets has been demonstrated. Attention to the technological aspects of making HTS conductors for magnets with strong flux pinning and reduced superconducting granularity is now sensible and attractive. However, extrinsic defects such as filament sausaging, cracking, misaligned grains and other perturbations to long range current flow must be controlled at a low level if the benefit of intrinsic improvements to the critical current density is to be maintained in the conductor form. Due to the great complexity of HTS materials, there is sometimes confusion as to whether a given sample has an intrinsically or extrinsically limited critical current density. Systematic microstructure variation experiments and resistive transition analysis are shown to be particularly helpful in this phase of conductor development

  5. Tokamak-like confinement at high beta and low field in the reversed field pinch

    International Nuclear Information System (INIS)

    Sarff, J S; Anderson, J K; Biewer, T M; Brower, D L; Chapman, B E; Chattopadhyay, P K; Craig, D; Deng, B; Hartog, D J Den; Ding, W X; Fiksel, G; Forest, C B; Goetz, J A; O'Connell, R; Prager, S C; Thomas, M A

    2003-01-01

    For several reasons, improved-confinement achieved in the reversed field pinch (RFP) during the last few years can be characterized as 'tokamak-like'. Historically, RFP plasmas have had relatively poor confinement due to tearing instability which causes magnetic stochasticity and enhanced transport. Tearing reduction is achieved through modification of the inductive current drive, which dramatically improves confinement. The electron temperature increases to >1 keV and the electron heat diffusivity decreases to approx. 5 m 2 s -1 , comparable with the transport level expected in a tokamak plasma of the same size and current. This corresponds to a 10-fold increase in global energy confinement. Runaway electrons are confined, and Fokker-Planck modelling of the electron distribution reveals that the diffusion at high energy is independent of the parallel velocity, uncharacteristic of stochastic transport. Improved-confinement occurs simultaneously with increased beta approx. 15%, while maintaining a magnetic field strength ten times weaker than a comparable tokamak. Measurements of the current, magnetic, and electric field profiles show that a simple Ohm's Law applies to this RFP sustained without dynamo relaxation

  6. Progress with High-Field Superconducting Magnets for High-Energy Colliders

    Science.gov (United States)

    Apollinari, Giorgio; Prestemon, Soren; Zlobin, Alexander V.

    2015-10-01

    One of the possible next steps for high-energy physics research relies on a high-energy hadron or muon collider. The energy of a circular collider is limited by the strength of bending dipoles, and its maximum luminosity is determined by the strength of final focus quadrupoles. For this reason, the high-energy physics and accelerator communities have shown much interest in higher-field and higher-gradient superconducting accelerator magnets. The maximum field of NbTi magnets used in all present high-energy machines, including the LHC, is limited to ˜10 T at 1.9 K. Fields above 10 T became possible with the use of Nb3Sn superconductors. Nb3Sn accelerator magnets can provide operating fields up to ˜15 T and can significantly increase the coil temperature margin. Accelerator magnets with operating fields above 15 T require high-temperature superconductors. This review discusses the status and main results of Nb3Sn accelerator magnet research and development and work toward 20-T magnets.

  7. Efficiency and rate capability studies of the time-of-flight detector for isochronous mass measurements of stored short-lived nuclei with the FRS-ESR facility

    Energy Technology Data Exchange (ETDEWEB)

    Kuzminchuk-Feuerstein, Natalia; Fabian, Benjamin [II. Physikalisches Institut, Justus-Liebig-Universität, 35392 Gießen (Germany); GSI Helmholtzzentrum für Schwerionenforschung, 64291 Darmstadt (Germany); Diwisch, Marcel [II. Physikalisches Institut, Justus-Liebig-Universität, 35392 Gießen (Germany); Plaß, Wolfgang R., E-mail: Wolfgang.R.Plass@exp2.physik.uni-giessen.de [II. Physikalisches Institut, Justus-Liebig-Universität, 35392 Gießen (Germany); GSI Helmholtzzentrum für Schwerionenforschung, 64291 Darmstadt (Germany); Geissel, Hans; Ayet San Andrés, Samuel; Dickel, Timo; Knöbel, Ronja; Scheidenberger, Christoph [II. Physikalisches Institut, Justus-Liebig-Universität, 35392 Gießen (Germany); GSI Helmholtzzentrum für Schwerionenforschung, 64291 Darmstadt (Germany); Sun, Baohua [II. Physikalisches Institut, Justus-Liebig-Universität, 35392 Gießen (Germany); Weick, Helmut [GSI Helmholtzzentrum für Schwerionenforschung, 64291 Darmstadt (Germany)

    2016-06-11

    A time-of-flight (TOF) detector is used for Isochronous Mass Spectrometry (IMS) with the projectile fragment separator FRS and the heavy-ion storage ring ESR. Exotic nuclei are spatially separated in flight with the FRS at about 70% of the speed of light and are injected into the ESR. The revolution times of the stored ions circulating in the ESR are measured with a thin transmission foil detector. When the ions penetrate the thin detector foil, secondary electrons (SEs) are emitted from the surface and provide the timing information in combination with microchannel plate (MCP) detectors. The isochronous transport of the SEs is performed by perpendicular superimposed electric and magnetic fields. The detection efficiency and the rate capability of the TOF detector have been studied in simulations and experiments. As a result the performance of the TOF detector has been improved substantially: (i) The SE collection efficiency was doubled by use of an optimized set of electric and magnetic field values; now SEs from almost the full area of the foil are transmitted to the MCP detectors. (ii) The rate capability of the TOF detector was improved by a factor of four by the use of MCPs with 5 μm pore size. (iii) With these MCPs and a carbon foil with a reduced thickness of 10 μg/cm{sup 2} the number of recorded revolutions in the ESR has been increased by nearly a factor of 10. The number of recorded revolutions determine the precision of the IMS experiments. Heavy-ion measurements were performed with neon ions at 322 MeV/u and uranium fission fragments at about 370 MeV/u. In addition, measurements with an alpha source were performed in the laboratory with a duplicate of the TOF detector.

  8. Efficiency and rate capability studies of the time-of-flight detector for isochronous mass measurements of stored short-lived nuclei with the FRS-ESR facility

    International Nuclear Information System (INIS)

    Kuzminchuk-Feuerstein, Natalia; Fabian, Benjamin; Diwisch, Marcel; Plaß, Wolfgang R.; Geissel, Hans; Ayet San Andrés, Samuel; Dickel, Timo; Knöbel, Ronja; Scheidenberger, Christoph; Sun, Baohua; Weick, Helmut

    2016-01-01

    A time-of-flight (TOF) detector is used for Isochronous Mass Spectrometry (IMS) with the projectile fragment separator FRS and the heavy-ion storage ring ESR. Exotic nuclei are spatially separated in flight with the FRS at about 70% of the speed of light and are injected into the ESR. The revolution times of the stored ions circulating in the ESR are measured with a thin transmission foil detector. When the ions penetrate the thin detector foil, secondary electrons (SEs) are emitted from the surface and provide the timing information in combination with microchannel plate (MCP) detectors. The isochronous transport of the SEs is performed by perpendicular superimposed electric and magnetic fields. The detection efficiency and the rate capability of the TOF detector have been studied in simulations and experiments. As a result the performance of the TOF detector has been improved substantially: (i) The SE collection efficiency was doubled by use of an optimized set of electric and magnetic field values; now SEs from almost the full area of the foil are transmitted to the MCP detectors. (ii) The rate capability of the TOF detector was improved by a factor of four by the use of MCPs with 5 μm pore size. (iii) With these MCPs and a carbon foil with a reduced thickness of 10 μg/cm 2 the number of recorded revolutions in the ESR has been increased by nearly a factor of 10. The number of recorded revolutions determine the precision of the IMS experiments. Heavy-ion measurements were performed with neon ions at 322 MeV/u and uranium fission fragments at about 370 MeV/u. In addition, measurements with an alpha source were performed in the laboratory with a duplicate of the TOF detector.

  9. Neutron diffraction and ESR studies of pseudocubic Nd0.75Ba0.25MnO3 and its unusual critical behavior above TC

    International Nuclear Information System (INIS)

    Lazuta, A.V.; Ryzhov, V.A.; Smirnov, O.P.; Kiselev, I.A.; Chernenkov, Yu.P.; Borisov, S.A.; Troaynchuk, I.O.; Khalyavin, D.D.

    2006-01-01

    Results of structural neutron diffraction study and electron spin resonance (ESR) measurements are presented for insulating Nd 1-x Ba x MnO 3 (x=0.25) with the Curie temperature T C ∼129K. Its pseudocubic structure reveals the definite distortions to a lower symmetry. Detailed analysis of the data is performed in the frame of Pbnm space group in a temperature range 4.2-300K. The compound is found to exhibit the Jahn-Teller (JT) transition at T JT ∼250K. Character of the coherent JT distortions and their temperature evolution differ from those of the x=0.23 manganite. The ESR results correspond to behavior of a 3D isotropic ferromagnet above T*∼143K (τ*∼0.12= C )/T C ). It is shown that an anisotropic exchange coupling of the Mn and Nd magnetic moments may give a substantial contribution in ESR linewidth masking its critical enhancement. The different temperature treatments (slow/fast cooling/heating with/without external magnetic field) of the sample reveal a temperature hysteresis of the ESR spectra below T* indicating an anomalous response in the paramagnetic region. The study of the magnetic phase transition in the x=0.23 and 0.25 NdBa manganites suggests a change in its character from the second to first order at T*. The conventional free energy including the magnetization and magnetic field failed to describe this first-order transition. The unconventional critical behavior is attributed to an orbital liquid metallic phase that begins to coexist with the initial orbital-ordered phases below T*

  10. Longitudinal wake field for an electron beam accelerated through a ultra-high field gradient

    Energy Technology Data Exchange (ETDEWEB)

    Geloni, G.; Saldin, E.; Schneidmiller, E.; Yurkov, M.

    2006-12-15

    Electron accelerators with higher and higher longitudinal field gradients are desirable, as they allow for the production of high energy beams by means of compact and cheap setups. The new laser-plasma acceleration technique appears to constitute the more promising breakthrough in this direction, delivering unprecedent field gradients up to TV/m. In this article we give a quantitative description of the impact of longitudinal wake fields on the electron beam. Our paper is based on the solution of Maxwell's equations for the longitudinal field. Our conclusions are valid when the acceleration distance is much smaller than the the overtaking length, that is the length that electrons travel as a light signal from the tail of the bunch overtakes the head of the bunch. This condition is well verified for laser-plasma devices. We calculate a closed expression for the impedance and the wake function that may be evaluated numerically. It is shown that the rate of energy loss in the bunch due to radiative interaction is equal to the energy emitted through coherent radiation in the far-zone. Furthermore, an expression is found for the asymptotic limit of a large distance of the electron beam from the accelerator compared with the overtaking length. Such expression allows us to calculate analytical solutions for a Gaussian transverse and longitudinal bunch shape. Finally, we study the feasibility of Table-Top Free-Electron Lasers in the Vacuum Ultra-Violet (TT-VUV FEL) and X-ray range (TT-XFEL), respectively based on 100 MeV and 1 GeV laser-plasma accelerator drivers. Numerical estimations presented in this paper indicate that the effects of the time-dependent energy change induced by the longitudinal wake pose a serious threat to the operation of these devices. (orig.)

  11. The characteristics of ESR and 3-D TL spectra of diamonds

    International Nuclear Information System (INIS)

    Liu Shunsheng; Lu Xu; Fu Huifang

    2003-01-01

    Electron Spin Resonance (ESR) and 3-dimensional Thermoluminescence (3-D TL) spectra of natural diamond, high temperature-high pressure artificial diamond and high temperature-low pressure chemical vapor deposited (CVD) diamond were determined. The characteristics of spectra have been studied. It is found that isolated nitrogen, nitrogen exchange pair and nitrogen atom pair (S=1) are main forms of electron spin resonance nitrogen in natural and high temperature-high pressure artificial diamonds. The spectrum of CVD diamond is sampler, and contains only one peak caused by suspended bond of unsaturated carbon ones. For 3-D TL spectra, natural diamond has two peaks (∼370 nm and ∼510 nm) in 100-200 degree C temperature range, high temperature-high pressure artificial diamond only has ∼370 nm peak, and CVD diamond only has ∼500 nm peak. These characteristics would be useful for the quality inspection and classification of diamonds, as well as for the study of geologic actions associated with natural diamond

  12. ESR study on the interaction between carbon blacks and oxygen molecules; ESR ho ni yoru carbon black to sanso bunshi tono sogo sayo no kenkyu

    Energy Technology Data Exchange (ETDEWEB)

    Okazaki, M.; Toriyama, K.; Konishi, Y. [National Industrial Research Institute of Nagoya, Nagoya (Japan)

    2000-02-24

    Interaction between carbon blacks and oxygen molecules has been studied by means of electron spin resonance (ESR) spectroscopy. The ESR spectra of the carbon blacks appears at the g-value of free spin, which are contributed by both isolated electrons and conduction electrons. Upon introducing oxygen to the system the ESR linewidth was broadened in proportion to the partial pressure of oxygen. In case of lampblack (LB 101, Degussa) the interaction was not so strong that it took a tong time at 77K for the linewidth to reach the maxmum value. In case of gassblack (P 140 V, Degussa), on the other hand, the oxygen was easily adsorbed at 298K and the linewidth at 77K became its maximum immediately after cooling. The number of unpaired electrons decreased when the system was kept at 298 K and the decrease was prominent for the local spins. These phenomena have been explained with a simple band model for the electron. (author)

  13. Whole-globe biomechanics using high-field MRI.

    Science.gov (United States)

    Voorhees, Andrew P; Ho, Leon C; Jan, Ning-Jiun; Tran, Huong; van der Merwe, Yolandi; Chan, Kevin; Sigal, Ian A

    2017-07-01

    The eye is a complex structure composed of several interconnected tissues acting together, across the whole globe, to resist deformation due to intraocular pressure (IOP). However, most work in the ocular biomechanics field only examines the response to IOP over smaller regions of the eye. We used high-field MRI to measure IOP induced ocular displacements and deformations over the whole globe. Seven sheep eyes were obtained from a local abattoir and imaged within 48 h using MRI at multiple levels of IOP. IOP was controlled with a gravity perfusion system and a cannula inserted into the anterior chamber. T2-weighted imaging was performed to the eyes serially at 0 mmHg, 10 mmHg, 20 mmHg and 40 mmHg of IOP using a 9.4 T MRI scanner. Manual morphometry was conducted using 3D visualization software to quantify IOP-induced effects at the globe scale (e.g. axial length and equatorial diameters) or optic nerve head scale (e.g. canal diameter, peripapillary sclera bowing). Measurement sensitivity analysis was conducted to determine measurement precision. High-field MRI revealed an outward bowing of the posterior sclera and anterior bulging of the cornea due to IOP elevation. Increments in IOP from 10 to 40 mmHg caused measurable increases in axial length in 6 of 7 eyes of 7.9 ± 5.7% (mean ± SD). Changes in equatorial diameter were minimal, 0.4 ± 1.2% between 10 and 40 mmHg, and in all cases less than the measurement sensitivity. The effects were nonlinear, with larger deformations at normal IOPs (10-20 mmHg) than at elevated IOPs (20-40 mmHg). IOP also caused measurable increases in the nasal-temporal scleral canal diameter of 13.4 ± 9.7% between 0 and 20 mmHg, but not in the superior-inferior diameter. This study demonstrates that high-field MRI can be used to visualize and measure simultaneously the effects of IOP over the whole globe, including the effects on axial length and equatorial diameter, posterior sclera displacement and bowing, and even

  14. Identification of irradiated sage tea (Salvia officinalis L.) by ESR spectroscopy

    International Nuclear Information System (INIS)

    Tepe Cam, Semra; Engin, Birol

    2010-01-01

    The use of electron spin resonance (ESR) spectroscopy to accurately distinguish irradiated from unirradiated sage tea was examined. Before irradiation, sage tea samples exhibit one asymmetric singlet ESR signal centered at g=2.0037. Besides this central signal, two weak satellite signals situated about 3 mT left and right to it in radiation-induced spectra. Irradiation with increasing doses caused a significant increase in radiation-induced ESR signal intensity at g=2.0265 (the left satellite signal) and this increase was found to be explained by a polynomial varying function. The stability of that radiation-induced ESR signal at room temperature was studied over a storage period of 9 months. Also, the kinetic of signal at g=2.0265 was studied in detail over a temperature range 313-353 K by annealing samples at different temperatures for various times.

  15. DETECTION OF SOME IRRADIATED NUTS BY ELECTRON SPIN RESONANCE (ESR) TECHNIQUE

    International Nuclear Information System (INIS)

    KHALLAF, M.F.; YASIN, N.M.N.; EL-NASHABY, F.M.; ALI, H.G.M.; EL-SHIEMY, S.M.

    2008-01-01

    The present investigation was carried out to establish the electron spin resonance (ESR) detection method for identifying irradiated nuts (almond and pistachio). Samples were irradiated with 2, 4 and 6 kGy and stored at room temperature (25± 2 0 C) for six months to study the possibility of detecting its previous irradiation treatments by ESR spectroscopy. Analysis was carried out just after irradiation treatment and during ambient storage period. The ESR signal intensities of irradiated samples were markedly increased correspondingly with irradiation dose as a result of free radicals generated by gamma irradiation so, all irradiated samples under investigation could be differentiated from non-irradiated ones immediately after irradiation treatment. The decay in radicals responsible of ESR signals showed the identification of irradiated almond (shell or edible part) and pistachio (edible part) was impossible after six months of ambient storage

  16. DETECTION OF SOME IRRADIATED NUTS BY ELECTRON SPIN RESONANCE (ESR) TECHNIQUE

    Energy Technology Data Exchange (ETDEWEB)

    KHALLAF, M F; YASIN, N M.N. [Food Science Dept., Faculty of Agriculture, Ain Shams University, Cairo (Egypt); EL-NASHABY, F M; ALI, H G.M.; EL-SHIEMY, S M [Nuclear Research Centre, Atomic Energy Authority, Cairo (Egypt)

    2008-07-01

    The present investigation was carried out to establish the electron spin resonance (ESR) detection method for identifying irradiated nuts (almond and pistachio). Samples were irradiated with 2, 4 and 6 kGy and stored at room temperature (25{+-} 2{sup 0}C) for six months to study the possibility of detecting its previous irradiation treatments by ESR spectroscopy. Analysis was carried out just after irradiation treatment and during ambient storage period. The ESR signal intensities of irradiated samples were markedly increased correspondingly with irradiation dose as a result of free radicals generated by gamma irradiation so, all irradiated samples under investigation could be differentiated from non-irradiated ones immediately after irradiation treatment. The decay in radicals responsible of ESR signals showed the identification of irradiated almond (shell or edible part) and pistachio (edible part) was impossible after six months of ambient storage.

  17. Dose response of artificial irradiation of fluvial sediment sample for ESR dating

    International Nuclear Information System (INIS)

    Liu Chunru; Yin Gongming; Gao Lu; Li Jianping; Han Fei; Lin Min

    2011-01-01

    ESR dating samples need be irradiated to obtain dose response curve and the equivalent dose. The artificial dose rate is about 1 x 10 -1 -1 x 10 2 Gy/min, whereas the natural dose rate is about 3 Gy/ka. Therefore, one must be sure whether the much higher artificial dose rate is suitable for the ESR dating study. In this paper, we use different artificial dose rate to irradiate the same fluvial sample and measure the quartz Al centre ESR signal under the same conditions. The dose response curves are compared, in an attempt to gain a preliminary knowledge on that problem and build a good foundation for our ESR dating studies on fluvial samples. (authors)

  18. ESR analysis of natural and gamma irradiated coriander (Coriandrum sativum L.) seeds

    Science.gov (United States)

    Sezer, M. Özgür; Kaplan, Necati; Sayin, Ulku

    2017-12-01

    Electron spin resonance (ESR) is a powerful technique to detect radicals trapped in cellulosic food products and has been suggested as a useful method for identification of irradiated herbal foodstuffs. Coriander spice which has important medicinal properties was investigated using ESR spectroscopy. Radicals in natural and irradiated coriander samples were determined at room temperature. ESR spectra of natural sample were characterized by a single central signal with ? value and gamma irradiation produced satellite peaks attributed to cellulose-like radical which is used as a marker for detection of irradiated cellulosic plant products. The spectroscopic splitting values of radicals were determined. Dose dependency and stability of this center were analyzed by dose response and kinetic measurements. The reported results about activation energy, thermal life time and dose response relationship of the cellulose-like radical accurately prove that ESR can be used for identification of irradiated coriander spice seeds.

  19. Identification of irradiated sage tea (Salvia officinalis L.) by ESR spectroscopy

    Energy Technology Data Exchange (ETDEWEB)

    Tepe Cam, Semra, E-mail: stepe06@gmail.co [Gazi University, Faculty of Medicine, Biophysics Department, 06500 Besevler, Ankara (Turkey); Engin, Birol [Turkish Atomic Energy Authority, Saraykoey Nuclear Research and Training Center, 06983 Ankara (Turkey)

    2010-04-15

    The use of electron spin resonance (ESR) spectroscopy to accurately distinguish irradiated from unirradiated sage tea was examined. Before irradiation, sage tea samples exhibit one asymmetric singlet ESR signal centered at g=2.0037. Besides this central signal, two weak satellite signals situated about 3 mT left and right to it in radiation-induced spectra. Irradiation with increasing doses caused a significant increase in radiation-induced ESR signal intensity at g=2.0265 (the left satellite signal) and this increase was found to be explained by a polynomial varying function. The stability of that radiation-induced ESR signal at room temperature was studied over a storage period of 9 months. Also, the kinetic of signal at g=2.0265 was studied in detail over a temperature range 313-353 K by annealing samples at different temperatures for various times.

  20. ESR-spin trapping studies on the interaction between anthraquinone triplets and aromatic compounds

    International Nuclear Information System (INIS)

    Moger, G.; Rockenbauer, A.; Simon, P.

    1980-01-01

    The ESR spin trapping technique was used for the detection of transient C-centered radicals in the photochemical interaction between triplet anthraquinone and aromatic hydroperoxide and alcohol. (author)

  1. White paper of the European Association of Nuclear Medicine (EANM) and the European Society of Radiology (ESR) on multimodality imaging

    International Nuclear Information System (INIS)

    Bischof Delaloye, Angelika; Carrio, Ignasi; Cuocolo, Alberto; Knapp, Wolfram; Gourtsoyiannis, Nicholas; McCall, Iain; Reiser, Maximilian; Silberman, Bruno

    2007-01-01

    New multimodality imaging systems bring together anatomical and molecular information and require the competency and accreditation of individuals from both nuclear medicine and radiology. This paper sets out the positions and aspirations of the European Association of Nuclear Medicine (EANM) and the European Society of Radiology (ESR) working together on an equal and constructive basis for the future benefit of both specialties. EANM and ESR recognise the importance of coordinating working practices for multimodality imaging systems and that undertaking the nuclear medicine and radiology components of imaging with hybrid systems requires different skills. It is important to provide adequate and appropriate training in the two disciplines in order to offer a proper service to the patient using hybrid systems. Training models are proposed with the overall objective of providing opportunities for acquisition of special competency certification in multimodality imaging. Both organisations plan to develop common procedural guidelines and recognise the importance of coordinating the purchasing and management of hybrid systems to maximise the benefits to both specialties and to ensure appropriate reimbursement of these examinations. European multimodality imaging research is operating in a highly competitive environment. The coming years will decide whether European research in this area manages to defend its leading position or whether it falls behind research in other leading economies. Since research teams in the Member States are not always sufficiently interconnected, more European input is necessary to create interdisciplinary bridges between research institutions in Europe and to stimulate excellence. EANM and ESR will work with the European Institute for Biomedical Imaging Research (EIBIR) to develop further research opportunities across Europe. European Union grant-funding bodies should allocate funds to joint research initiatives that encompass clinical research

  2. White paper of the European Society of Radiology (ESR) and the European Association of Nuclear Medicine (EANM) on multimodality imaging

    International Nuclear Information System (INIS)

    Gourtsoyiannis, Nicholas; McCall, Iain; Reiser, Maximilian; Silberman, Bruno; Bischof Delaloye, Angelika; Carrio, Ignacio; Cuocolo, Alberto; Knapp, Wolfram

    2007-01-01

    New multimodality imaging systems bring together anatomical and molecular information and require the competency and accreditation of individuals from both radiology and nuclear medicine. This paper sets out the positions and aspirations of the European Society of Radiology (ESR) and the European Association of Nuclear Medicine (EANM) working together on an equal and constructive basis for the future benefit of both specialties. ESR and EANM recognise the importance of coordinating working practices for multimodality imaging systems and that undertaking the radiology and nuclear medicine components of imaging with hybrid systems requires different skills. It is important to provide adequate and appropriate training in the two disciplines in order to offer a proper service to the patient using hybrid systems. Training models are proposed with the overall objective of providing opportunities for acquisition of special competency certification in multimodality imaging. Both organisations plan to develop common procedural guidelines and recognise the importance of coordinating the purchasing and management of hybrid systems to maximise the benefits to both specialties and to ensure appropriate reimbursement of these examinations. European multimodality imaging research is operating in a highly competitive environment. The coming years will decide whether European research in this area manages to defend its leading position or whether it falls behind research in other leading economies. Since research teams in the member states are not always sufficiently interconnected, more European input is necessary to create interdisciplinary bridges between research institutions in Europe and to stimulate excellence. ESR and EANM will work with the European Institute for Biomedical Imaging Research (EIBIR) to develop further research opportunities across Europe. European Union grant-funding bodies should allocate funds to joint research initiatives that encompass clinical research

  3. ESR/Alanine {gamma}-dosimetry in the 10-30 Gy range

    Energy Technology Data Exchange (ETDEWEB)

    Fainstein, C. E-mail: cfainstein@cab.cnea.gov.ar; Winkler, E.; Saravi, M

    2000-05-15

    We report Alanine Dosimeter preparation, procedures for using the ESR/Dosimetry method, and the resulting calibration curve for {gamma}-irradiation in the range from 10-30 Gy. We use calibration curve to measure the irradiation dose in {gamma}-irradiation of human blood, as required in Blood Transfusion Therapy. The ESR/Alanine results are compared against those obtained using the thermoluminescent dosimetry (TLD) method.

  4. Study by electron spin resonance (ESR) of 60 Co irradiated grains and farinaceous derivatives

    International Nuclear Information System (INIS)

    Catanni, Marta Mattos.

    1995-01-01

    The electron spin resonance (ESR) spectroscopy is being pointed out as one of the most promising techniques to determine whether a food has been irradiated. In this work, the ESR spectrum of paramagnetic radicals produced by gamma irradiation of grains and flour derivatives using a 60 Co source was investigated. Samples of grains (wheat and barley), flours (wheat, maniac, rye, soy bean and maize), bran and starch have been irradiated with doses between 0.2 and 70 KGy. It was shown that all varieties of grains and flours presented similar ESR spectra with variation in the free radicals signal intensity. Measurements at 9.5 and 34.5 GHz shown that spectra were composed probably by the superposition of four paramagnetic species with g-factors closed to that of the free electron (2 triplets, 1 doublet and 1 singlet). Hyperfine interactions and the correspondingly line widths were estimated through an spectrum computer simulation. It was established that ESR signal intensities increased with the irradiation dose for all samples. Up to the commercial admissible dose limit (1 kGy), the increase of ESR signal shown a linear behavior with the dose. The signal stability varied significantly with storage conditions and sample humidity. For 1 kGy-irradiated samples stored at room temperature and 14% humidity, the ESR radiation signals were possible to be detected up to 5 days after irradiation. When the same samples were stored at low temperatures (0 0 C) or freeze-dried (almost 0% humidity) the ESR signals were detected until 6 months after irradiation. Similar ESR spectrum found for grains and flours was obtained for diverse starchy food products. It was verified that it is possible to identify for a long time irradiated starchy foods when they are commercialized dehydrated or frozen. (author). 66 refs., 35 figs., 17 tabs

  5. The influence of measurement and storage conditions on alanine ESR dosimeters

    International Nuclear Information System (INIS)

    Alexandre, A.C.

    1992-01-01

    Alanine has several desirable properties as an ESR dosemeter e.g. tissue equivalence, low fading and an approximately linear response for doses up to 10 kGy. This work reports on a simple system to produce the alanine dosemeter, the signal intensity for a range of doses and energies, and the effect of the air humidity and the spectrometer settings on the ESR signal. (Author)

  6. Cooling history of the Valles Caldera, New Mexico using ESR dating method

    International Nuclear Information System (INIS)

    Ogoh, K.; Toyoda, S.; Ikeda, S.; Ikeya, M.; Goff, F.

    1993-01-01

    ESR dating was made at the Valles caldera by using the Al center and Ti center in quartz grains separated from the layers of the Valles Rhyolite. Obtained ESR ages were much younger than those by other methods (fission track and 39 Ar- 40 Ar). A reported thermal event of about 10-40 ka ago might explain the difference between the above ages. (author)

  7. Upper critical field measurements in high-Tc superconducting oxides

    Science.gov (United States)

    Ousset, J. C.; Bobo, J. F.; Ulmet, J. P.; Rakoto, H.; Cheggour, N.

    We present upper critical field measurements on the superconducting oxides RE Ba2Cu3O7-δ (RE = Y, Gd) performed in a pulsed magnetic field up to 43 T. Values for Hc2 as high as 52 T and 77 T for Y and Gd respectively, are expected at 77 K. However, in order to observe no resistive behaviour up to 43 T the temperature must be decreased down to 50 K. In the case of oxygen deficient systems the magnetoresistance reveals two superconducting phases wich could be related to two different orders of oxygen vacancies. Nous présentons des mesures de champ critique Hc2 sur les supraconducteurs TR Ba 2Cu3O7-δ (TR = Y, Gd) réalisées en champ magnétique pulsé jusqu'à 43 T. Elles permettent de prévoir des valeurs de H c2 de 52 T et 77 T respectivement pour Y et Gd à 77 K. Cependant, pour ne pas observer de comportement résistif jusqu'au champ maximum, il est nécessaire de refroidir l'échantillon jusqu'à 50 K. Dans le cas des systèmes déficients en oxygène (δ important) nous mettons en évidence l'existence de deux phases supraconductrices qui pourraient être dues à deux ordres différents des lacunes d'oxygène.

  8. Dynamics of Coulomb correlations in semiconductors in high magnetic fields

    International Nuclear Information System (INIS)

    Fromer, Neil Alan

    2002-01-01

    Current theories have been successful in explaining many nonlinear optical experiments in undoped semiconductors. However, these theories require a ground state which is assumed to be uncorrelated. Strongly correlated systems of current interest, such as a two dimensional electron gas in a high magnetic field, cannot be explained in this manner because the correlations in the ground state and the low energy collective excitations cause a breakdown of the conventional techniques. We perform ultrafast time-resolved four-wave mixing on $n$-modulation doped quantum wells, which contain a quasi-two dimensional electron gas, in a large magnetic field, when only a single Landau level is excited and also when two levels are excited together. We find evidence for memory effects and as strong coupling between the Landau levels induced by the electron gas. We compare our results with simulations based on a new microscopic approach capable of treating the collective effects and correlations of the doped electrons, and find a good qualitative agreement. By looking at the individual contributions to the model, we determine that the unusual correlation effects seen in the experiments are caused by the scattering of photo-excited electron-hole pairs with the electron gas, leading to new excited states which are not present in undoped semiconductors, and also by exciton-exciton interactions mediated by the long-lived collective excitations of the electron gas, inter-Landau level magnetoplasmons

  9. The optimal use of contrast agents at high field MRI

    International Nuclear Information System (INIS)

    Trattnig, Siegfried; Pinker, Kathia; Ba-Ssalamah, Ahmed; Noebauer-Huhmann, Iris-Melanie

    2006-01-01

    The intravenous administration of a standard dose of conventional gadolinium-based contrast agents produces higher contrast between the tumor and normal brain at 3.0 Tesla (T) than at 1.5 T, which allows reducing the dose to half of the standard one to produce similar contrast at 3.0 T compared to 1.5 T. The assessment of cumulative triple-dose 3.0 T images obtained the best results in the detection of brain metastases compared to other sequences. The contrast agent dose for dynamic susceptibility-weighted contrast-enhanced perfusion MR imaging at 3.0 T can be reduced to 0.1 mmol compared to 0.2 mmol at 1.5 T due to the increased susceptibility effects at higher magnetic field strengths. Contrast agent application makes susceptibility-weighted imaging (SWI) at 3.0 T clinically attractive, with an increase in spatial resolution within the same scan time. Whereas a double dose of conventional gadolinium-based contrast agents was optimal in SWI with respect to sensitivity and image quality, a standard dose of gadobenate dimeglumine, which has a two-fold higher T1-relaxivity in blood, produced the same effect. For MR-arthrography, optimized concentrations of gadolinium-based contrast agents are similar at 3.0 and 1.5 T. In summary, high field MRI requires the optimization of the contrast agent dose in different clinical applications. (orig.)

  10. High-field MR imaging of spinal cord multiple sclerosis

    International Nuclear Information System (INIS)

    De La Paz, R.L.; Floris, R.; Norman, D.; Enzmann, D.R.

    1987-01-01

    Fifty-one high-field MR imaging studies (1.5 T, General Electric Signa) of the spinal cord were performed in 42 patients (27 female, 15 male; mean age, 40 years) with clinically definitive (n = 34) or probable (n = 8) multiple sclerosis and suspected spinal cord lesions. MR imaging showed focal spinal cord abnormalities in 38 (75%) of 51 studies. T2-weighted images were abnormal (showing foci of high signal intensity) in 38 studies, T1-weighted images were abnormal (showing areas of low signal intensity or mass effect) in 16 (42%) of 38, and GRASS images were abnormal (showing foci of high signal intensity) in 9 (82%) of 11 cases. Brain MR imaging showed periventricular lesions typical of multiple sclerosis in 34 (81%) of 42 studies. Spinal cord studies were positive in eight cases with normal brain MR images, and brain studies were positive in 13 instances of normal spinal cord MR images. Four lesions were at the cervicomedullary junction, 44 in the cervical spinal cord, and three in the thoracic cord. Mass effect in cord lesions, simulating neoplasm, was seen in seven patients during the acute symptomatic phase. Serial studies in three patients with decreasing symptoms showed a reduction after 3-4 weeks and resolution of the mass effect after 2-6 months

  11. Highly air stable passivation of graphene based field effect devices.

    Science.gov (United States)

    Sagade, Abhay A; Neumaier, Daniel; Schall, Daniel; Otto, Martin; Pesquera, Amaia; Centeno, Alba; Elorza, Amaia Zurutuza; Kurz, Heinrich

    2015-02-28

    The sensitivity of graphene based devices to surface adsorbates and charge traps at the graphene/dielectric interface requires proper device passivation in order to operate them reproducibly under ambient conditions. Here we report on the use of atomic layer deposited aluminum oxide as passivation layer on graphene field effect devices (GFETs). We show that successful passivation produce hysteresis free DC characteristics, low doping level GFETs stable over weeks though operated and stored in ambient atmosphere. This is achieved by selecting proper seed layer prior to deposition of encapsulation layer. The passivated devices are also demonstrated to be robust towards the exposure to chemicals and heat treatments, typically used during device fabrication. Additionally, the passivation of high stability and reproducible characteristics is also shown for functional devices like integrated graphene based inverters.

  12. High field nuclear magnetic resonance application to polysaccharide chemistry

    International Nuclear Information System (INIS)

    Vincendon, Marc

    1972-01-01

    Nuclear magnetic resonance has been applied to polysaccharide chemistry using time averaging technique and high fields (100 and 250 MHz). The three methyl signals of methyl cellulose and cellulose triacetate are separated, and the C-6 substituent has been identified. Biosynthesis of bacterial cellulose has been performed using deuterium labelled D-glucose and Acetobacter xylinum. Per-acetylated derivative of bacterial cellulose has been studied by NMR; this study permitted us to determine the quantity of deuterium on each position of the anhydro-glucose unit in the polymer. NMR has also been used to see the anomeric end chain of cellulose and amylose derivatives and to show the fixation of bromine and t-butyl group on the free anomeric end chain of cellulose triacetate. (author) [fr

  13. Voltage spike detection in high field superconducting accelerator magnets

    Energy Technology Data Exchange (ETDEWEB)

    Orris, D.F.; Carcagno, R.; Feher, S.; Makulski, A.; Pischalnikov, Y.M.; /Fermilab

    2004-12-01

    A measurement system for the detection of small magnetic flux changes in superconducting magnets, which are due to either mechanical motion of the conductor or flux jump, has been developed at Fermilab. These flux changes are detected as small amplitude, short duration voltage spikes, which are {approx}15mV in magnitude and lasts for {approx}30 {micro}sec. The detection system combines an analog circuit for the signal conditioning of two coil segments and a fast data acquisition system for digitizing the results, performing threshold detection, and storing the resultant data. The design of the spike detection system along with the modeling results and noise analysis will be presented. Data from tests of high field Nb{sub 3}Sn magnets at currents up to {approx}20KA will also be shown.

  14. Voltage spike detection in high field superconducting accelerator magnets

    International Nuclear Information System (INIS)

    Orris, D.F.; Carcagno, R.; Feher, S.; Makulski, A.; Pischalnikov, Y.M.

    2004-01-01

    A measurement system for the detection of small magnetic flux changes in superconducting magnets, which are due to either mechanical motion of the conductor or flux jump, has been developed at Fermilab. These flux changes are detected as small amplitude, short duration voltage spikes, which are ∼15mV in magnitude and lasts for ∼30(micro)sec. The detection system combines an analog circuit for the signal conditioning of two coil segments and a fast data acquisition system for digitizing the results, performing threshold detection, and storing the resultant data. The design of the spike detection system along with the modeling results and noise analysis will be presented. Data from tests of high field Nb3Sn magnets at currents up to ∼20KA will also be shown

  15. An example of remote maintenance in high radiation fields

    International Nuclear Information System (INIS)

    Pothier, N.E.; Brisbois, L.U.

    Six auxiliary low pressure small (diameter <=5.0 cm) pipes located inside the reactor vault of the Douglas Point Nuclear Generating Station failed due to fretting wear at U-bolt supports: two had worn through the wall and developed leaks, and the others had worn <= 50% through the pipe wall. Human entry into the vault was not possible because of high radiation fields; hence, hands-on repair was not possible. The pipes were repaired and resupported to prevent further fretting wear failures during February-September, 1980. The repair work was performed using custom designed and developed remotely operated tooling and closed-circuit TV viewing. Three main groups were involved in the repair work: Atomic Energy of Canada Engineering Company (AECEC) - the reactor owner; Ontario Hydro - the reactor operator; and, Chalk River Nuclear Laboratories (CRNL). In this report, the contributions made by CRNL are summarized and discussed

  16. Characterization of phenolic pellets for ESR dosimetry in photon beam radiotherapy

    International Nuclear Information System (INIS)

    Gallo, Salvatore; Veronese, Ivan; Iacoviello, Giuseppina; Panzeca, Salvatore; Bartolotta, Antonio; Longo, Anna; Dondi, Daniele; Gueli, Anna Maria; Loi, Gianfranco; Mones, Eleonora; Marrale, Maurizio

    2017-01-01

    This work deals with the dosimetric features of a particular phenolic compound (IRGANOX 1076 registered ) for dosimetry of clinical photon beams by using electron spin resonance (ESR) spectroscopy. After the optimization of the ESR readout parameters (namely modulation amplitude and microwave power) to maximise the signal without excessive spectrum distortions, basic dosimetric properties of laboratory-made phenolic dosimeters in pellet form, such as reproducibility, dose-response, sensitivity, linearity and dose rate dependence were investigated. The dosimeters were tested by measuring the depth dose profile of a 6 MV photon beam. A satisfactory intra-batch reproducibility of the ESR signal of the manufactured dosimeters was obtained. The ESR signal proved to increase linearly with increasing dose in the investigated dose range 1-13 Gy. The presence of an intrinsic background signal limits the minimum detectable dose to a value of approximately 0.6 Gy. Reliable and accurate assessment of the dose was achieved, independently of the dose rate. Such characteristics, together with the fact that IRGANOX 1076 registered is almost tissue-equivalent, and the stability of the ESR signal, make these dosimeters promising materials for ESR dosimetric applications in radiotherapy. (orig.)

  17. Characterization of phenolic pellets for ESR dosimetry in photon beam radiotherapy

    Energy Technology Data Exchange (ETDEWEB)

    Gallo, Salvatore; Veronese, Ivan [Universita degli Studi di Milano, Department of Physics, Milan (Italy); Istituto Nazionale di Fisica Nucleare, Sezione di Milano (Italy); Iacoviello, Giuseppina [Hospital ARNAS-Civico, Medical Physics Department, Palermo (Italy); Panzeca, Salvatore [Universita degli Studi di Palermo, Department of Physics and Chemistry, Palermo (Italy); Istituto Nazionale di Fisica Nucleare-Sezione di Catania, Catania (Italy); Bartolotta, Antonio; Longo, Anna [Universita degli Studi di Palermo, Department of Physics and Chemistry, Palermo (Italy); Dondi, Daniele [Universita degli Studi di Pavia, Department of Chemistry, Pavia (Italy); Istituto Nazionale di Fisica Nucleare, Sezione di Pavia (Italy); Gueli, Anna Maria [Istituto Nazionale di Fisica Nucleare-Sezione di Catania, Catania (Italy); Universita degli Studi di Catania, Department of Physics and Astronomy, PH3DRA Laboratories, Catania (Italy); Loi, Gianfranco; Mones, Eleonora [Azienda Ospedaliero Universitaria Maggiore della Carita, Medical Physics Department, Novara (Italy); Marrale, Maurizio [Universita degli Studi di Palermo, Department of Physics and Chemistry, Palermo (Italy); Istituto Nazionale di Fisica Nucleare-Sezione di Catania, Catania (Italy); Universita degli Studi di Palermo, Advanced Technologies Network Center (ATeN Center), Palermo (Italy)

    2017-11-15

    This work deals with the dosimetric features of a particular phenolic compound (IRGANOX 1076 {sup registered}) for dosimetry of clinical photon beams by using electron spin resonance (ESR) spectroscopy. After the optimization of the ESR readout parameters (namely modulation amplitude and microwave power) to maximise the signal without excessive spectrum distortions, basic dosimetric properties of laboratory-made phenolic dosimeters in pellet form, such as reproducibility, dose-response, sensitivity, linearity and dose rate dependence were investigated. The dosimeters were tested by measuring the depth dose profile of a 6 MV photon beam. A satisfactory intra-batch reproducibility of the ESR signal of the manufactured dosimeters was obtained. The ESR signal proved to increase linearly with increasing dose in the investigated dose range 1-13 Gy. The presence of an intrinsic background signal limits the minimum detectable dose to a value of approximately 0.6 Gy. Reliable and accurate assessment of the dose was achieved, independently of the dose rate. Such characteristics, together with the fact that IRGANOX 1076 {sup registered} is almost tissue-equivalent, and the stability of the ESR signal, make these dosimeters promising materials for ESR dosimetric applications in radiotherapy. (orig.)

  18. Field test investigation of high sensitivity fiber optic seismic geophone

    Science.gov (United States)

    Wang, Meng; Min, Li; Zhang, Xiaolei; Zhang, Faxiang; Sun, Zhihui; Li, Shujuan; Wang, Chang; Zhao, Zhong; Hao, Guanghu

    2017-10-01

    Seismic reflection, whose measured signal is the artificial seismic waves ,is the most effective method and widely used in the geophysical prospecting. And this method can be used for exploration of oil, gas and coal. When a seismic wave travelling through the Earth encounters an interface between two materials with different acoustic impedances, some of the wave energy will reflect off the interface and some will refract through the interface. At its most basic, the seismic reflection technique consists of generating seismic waves and measuring the time taken for the waves to travel from the source, reflect off an interface and be detected by an array of geophones at the surface. Compared to traditional geophones such as electric, magnetic, mechanical and gas geophone, optical fiber geophones have many advantages. Optical fiber geophones can achieve sensing and signal transmission simultaneously. With the development of fiber grating sensor technology, fiber bragg grating (FBG) is being applied in seismic exploration and draws more and more attention to its advantage of anti-electromagnetic interference, high sensitivity and insensitivity to meteorological conditions. In this paper, we designed a high sensitivity geophone and tested its sensitivity, based on the theory of FBG sensing. The frequency response range is from 10 Hz to 100 Hz and the acceleration of the fiber optic seismic geophone is over 1000pm/g. sixteen-element fiber optic seismic geophone array system is presented and the field test is performed in Shengli oilfield of China. The field test shows that: (1) the fiber optic seismic geophone has a higher sensitivity than the traditional geophone between 1-100 Hz;(2) The low frequency reflection wave continuity of fiber Bragg grating geophone is better.

  19. Diffuse axonal injury at ultra-high field MRI.

    Directory of Open Access Journals (Sweden)

    Christoph Moenninghoff

    Full Text Available Diffuse axonal injury (DAI is a specific type of traumatic brain injury caused by shearing forces leading to widespread tearing of axons and small vessels. Traumatic microbleeds (TMBs are regarded as a radiological marker for DAI. This study aims to compare DAI-associated TMBs at 3 Tesla (T and 7 T susceptibility weighted imaging (SWI to evaluate possible diagnostic benefits of ultra-high field (UHF MRI.10 study participants (4 male, 6 female, age range 20-74 years with known DAI were included. All MR exams were performed with a 3 T MR system (Magnetom Skyra and a 7 T MR research system (Magnetom 7 T, Siemens AG, Healthcare Sector, Erlangen, Germany each in combination with a 32-channel-receive coil. The average time interval between trauma and imaging was 22 months. Location and count of TMBs were independently evaluated by two neuroradiologists on 3 T and 7 T SWI images with similar and additionally increased spatial resolution at 7 T. Inter- and intraobserver reliability was assessed using the interclass correlation coefficient (ICC. Count and diameter of TMB were evaluated with Wilcoxon signed rank test.Susceptibility weighted imaging revealed a total of 485 TMBs (range 1-190, median 25 at 3 T, 584 TMBs (plus 20%, range 1-262, median 30.5 at 7 T with similar spatial resolution, and 684 TMBs (plus 41%, range 1-288, median 39.5 at 7 T with 10-times higher spatial resolution. Hemorrhagic DAI appeared significantly larger at 7 T compared to 3 T (p = 0.005. Inter- and intraobserver correlation regarding the counted TMB was high and almost equal 3 T and 7 T.7 T SWI improves the depiction of small hemorrhagic DAI compared to 3 T and may be supplementary to lower field strengths for diagnostic in inconclusive or medicolegal cases.

  20. ESR spectrometer with a loop-gap resonator for cw and time resolved studies in a superconducting magnet.

    Science.gov (United States)

    Simon, Ferenc; Murányi, Ferenc

    2005-04-01

    The design and performance of an electron spin resonance spectrometer operating at 3 and 9 GHz microwave frequencies combined with a 9-T superconducting magnet are described. The probehead contains a compact two-loop, one gap resonator, and is inside the variable temperature insert of the magnet enabling measurements in the 0-9T magnetic field and 1.5-400 K temperature range. The spectrometer allows studies on systems where resonance occurs at fields far above the g approximately 2 paramagnetic condition such as in antiferromagnets. The low quality factor of the resonator allows time resolved experiments such as, e.g., longitudinally detected ESR. We demonstrate the performance of the spectrometer on the NaNiO2 antiferromagnet, the MgB2 superconductor, and the RbC60 conducting alkaline fulleride polymer.

  1. Current and field distribution in high temperature superconductors

    International Nuclear Information System (INIS)

    Johnston, M.D.

    1998-01-01

    The manufacture of wires from HTS materials containing copper-oxide planes is difficult because their physical and electrical properties are highly anisotropic. The electrical connectivity depends on the nearest-neighbour grain alignment and although a high degree of grain texture is achieved through processing, the tape microstructure is generally far from uniform, with weak links and porosity also complicating the picture. In order to optimise the processing, the microstructural features common to good tapes must be identified, requiring knowledge of the local properties. The preferential path taken by transport current is determined by the properties of the local microstructure and as such can be used to measure the variation in quality across the tape cross-section. By measuring the self-field profile generated by a current-carrying tape, it is possible to extract the associated current distribution. I have designed and built a Scanning Hall Probe Microscope to measure the normal field distribution above superconductor tapes carrying DC currents, operating at liquid nitrogen temperature and zero applied magnetic field. It has a spatial resolution of 50*50 μm and a field sensitivity of 5 μT, and can scan over a distance of 6 mm. The current extraction is performed by means of a deconvolution procedure based on Legendre functions. This allows a nondestructive, non-invasive method of evaluating the effects of the processing on the tapes - especially when correlated with transport and magnetisation measurement data. Conductors fabricated from Bi 2 Sr 2 Ca 2 Cu 3 O 10 , Bi 2 Sr 2 CaCu 2 O 8 and (Tl 0.78 Bi 0.22 )(Sr 0.8 Ba 0.2 ) 2 Ca 2 Cu 3 O x , have been investigated. I have confirmed the reports that in Bi-2223/Ag mono-core conductors produced by the oxide-powder-in-tube (OPIT) technique, the current flows predominantly at the edges of the tape, where the grains are long and well-aligned. This is in contrast to Bi-2212 ribbons, where the better microstructure

  2. High field high frequency EPR techniques and their application to single molecule magnets

    International Nuclear Information System (INIS)

    Edwards, R.S.; Hill, S.; Goy, P.; Wylde, R.; Takahashi, S.

    2004-01-01

    We present details of a new high-field/high-frequency EPR technique, and its application to measurements of single-molecule magnets (SMMs). By using a quasi-optical set-up and microwave sources covering a continuous frequency range from 170 to 600 GHz, in conjunction with a millimetre-wave vector network analyser, we are able to measure EPR to high magnetic fields. For example, a g=2 system will exhibit EPR at about 14 T at a frequency of 400 GHz. We illustrate the technique by presenting details of recent high-frequency experiments on several SMMs which are variations of the well-known SMM Mn 12 -Ac. This material has a spin ground state of S=10 and large uniaxial anisotropy, hence frequencies above 300 GHz are required in order to observe EPR from the ground state

  3. Joint analysis of ESR lineshapes and 1H NMRD profiles of DOTA-Gd derivatives by means of the slow motion theory

    Science.gov (United States)

    Kruk, D.; Kowalewski, J.; Tipikin, D. S.; Freed, J. H.; Mościcki, M.; Mielczarek, A.; Port, M.

    2011-01-01

    The "Swedish slow motion theory" [Nilsson and Kowalewski, J. Magn. Reson. 146, 345 (2000)] applied so far to Nuclear Magnetic Relaxation Dispersion (NMRD) profiles for solutions of transition metal ion complexes has been extended to ESR spectral analysis, including in addition g-tensor anisotropy effects. The extended theory has been applied to interpret in a consistent way (within one set of parameters) NMRD profiles and ESR spectra at 95 and 237 GHz for two Gd(III) complexes denoted as P760 and P792 (hydrophilic derivatives of DOTA-Gd, with molecular masses of 5.6 and 6.5 kDa, respectively). The goal is to verify the applicability of the commonly used pseudorotational model of the transient zero field splitting (ZFS). According to this model the transient ZFS is described by a tensor of a constant amplitude, defined in its own principal axes system, which changes its orientation with respect to the laboratory frame according to the isotropic diffusion equation with a characteristic time constant (correlation time) reflecting the time scale of the distortional motion. This unified interpretation of the ESR and NMRD leads to reasonable agreement with the experimental data, indicating that the pseudorotational model indeed captures the essential features of the electron spin dynamics.

  4. ADX: a high field, high power density, Advanced Divertor test eXperiment

    Science.gov (United States)

    Vieira, R.; Labombard, B.; Marmar, E.; Irby, J.; Shiraiwa, S.; Terry, J.; Wallace, G.; Whyte, D. G.; Wolfe, S.; Wukitch, S.; ADX Team

    2014-10-01

    The MIT PSFC and collaborators are proposing an advanced divertor experiment (ADX) - a tokamak specifically designed to address critical gaps in the world fusion research program on the pathway to FNSF/DEMO. This high field (6.5 tesla, 1.5 MA), high power density (P/S ~ 1.5 MW/m2) facility would utilize Alcator magnet technology to test innovative divertor concepts for next-step DT fusion devices (FNSF, DEMO) at reactor-level boundary plasma pressures and parallel heat flux densities while producing high performance core plasma conditions. The experimental platform would also test advanced lower hybrid current drive (LHCD) and ion-cyclotron range of frequency (ICRF) actuators and wave physics at the plasma densities and magnetic field strengths of a DEMO, with the unique ability to deploy launcher structures both on the low-magnetic-field side and the high-field side - a location where energetic plasma-material interactions can be controlled and wave physics is most favorable for efficient current drive, heating and flow drive. This innovative experiment would perform plasma science and technology R&D necessary to inform the conceptual development and accelerate the readiness-for-deployment of FNSF/DEMO - in a timely manner, on a cost-effective research platform. Supported by DE-FC02-99ER54512.

  5. Evaluation of the new ESR network software for the retrieval of direct sun products from CIMEL CE318 and PREDE POM01 sun-sky radiometers

    Directory of Open Access Journals (Sweden)

    V. Estellés

    2012-12-01

    Full Text Available The European Skynet Radiometers network (EuroSkyRad or ESR has been recently established as a research network of European PREDE sun-sky radiometers. Moreover, ESR is federated with SKYNET, an international network of PREDE sun-sky radiometers mostly present in East Asia. In contrast to SKYNET, the European network also integrates users of the CIMEL CE318 sky–sun photometer. Keeping instrumental duality in mind, a set of open source algorithms has been developed consisting of two modules for (1 the retrieval of direct sun products (aerosol optical depth, wavelength exponent and water vapor from the sun extinction measurements; and (2 the inversion of the sky radiance to derive other aerosol optical properties such as size distribution, single scattering albedo or refractive index. In this study we evaluate the ESR direct sun products in comparison with the AERosol RObotic NETwork (AERONET products. Specifically, we have applied the ESR algorithm to a CIMEL CE318 and PREDE POM simultaneously for a 4-yr database measured at the Burjassot site (Valencia, Spain, and compared the resultant products with the AERONET direct sun measurements obtained with the same CIMEL CE318 sky–sun photometer. The comparison shows that aerosol optical depth differences are mostly within the nominal uncertainty of 0.003 for a standard calibration instrument, and fall within the nominal AERONET uncertainty of 0.01–0.02 for a field instrument in the spectral range 340 to 1020 nm. In the cases of the Ångström exponent and the columnar water vapor, the differences are lower than 0.02 and 0.15 cm, respectively. Therefore, we present an open source code program that can be used with both CIMEL and PREDE sky radiometers and whose results are equivalent to AERONET and SKYNET retrievals.

  6. Self-interacting scalar fields at high-temperature

    Energy Technology Data Exchange (ETDEWEB)

    Deur, Alexandre [University of Virginia, Charlottesville, VA (United States)

    2017-06-15

    We study two self-interacting scalar field theories in their high-temperature limit using path integrals on a lattice. We first discuss the formalism and recover known potentials to validate the method. We then discuss how these theories can model, in the high-temperature limit, the strong interaction and General Relativity. For the strong interaction, the model recovers the known phenomenology of the nearly static regime of heavy quarkonia. The model also exposes a possible origin for the emergence of the confinement scale from the approximately conformal Lagrangian. Aside from such possible insights, the main purpose of addressing the strong interaction here - given that more sophisticated approaches already exist - is mostly to further verify the pertinence of the model in the more complex case of General Relativity for which non-perturbative methods are not as developed. The results have important implications on the nature of Dark Matter. In particular, non-perturbative effects naturally provide flat rotation curves for disk galaxies, without need for non-baryonic matter, and explain as well other observations involving Dark Matter such as cluster dynamics or the dark mass of elliptical galaxies. (orig.)

  7. High magnetic field generation for laser-plasma experiments

    International Nuclear Information System (INIS)

    Pollock, B. B.; Froula, D. H.; Davis, P. F.; Ross, J. S.; Fulkerson, S.; Bower, J.; Satariano, J.; Price, D.; Krushelnick, K.; Glenzer, S. H.

    2006-01-01

    An electromagnetic solenoid was developed to study the effect of magnetic fields on electron thermal transport in laser plasmas. The solenoid, which is driven by a pulsed power system supplying 30 kJ, achieves magnetic fields of 13 T. The field strength was measured on the solenoid axis with a magnetic probe and optical Zeeman splitting. The measurements agree well with analytical estimates. A method for optimizing the solenoid design to achieve magnetic fields exceeding 20 T is presented

  8. High performance ultrasonic field simulation on complex geometries

    Science.gov (United States)

    Chouh, H.; Rougeron, G.; Chatillon, S.; Iehl, J. C.; Farrugia, J. P.; Ostromoukhov, V.

    2016-02-01

    Ultrasonic field simulation is a key ingredient for the design of new testing methods as well as a crucial step for NDT inspection simulation. As presented in a previous paper [1], CEA-LIST has worked on the acceleration of these simulations focusing on simple geometries (planar interfaces, isotropic materials). In this context, significant accelerations were achieved on multicore processors and GPUs (Graphics Processing Units), bringing the execution time of realistic computations in the 0.1 s range. In this paper, we present recent works that aim at similar performances on a wider range of configurations. We adapted the physical model used by the CIVA platform to design and implement a new algorithm providing a fast ultrasonic field simulation that yields nearly interactive results for complex cases. The improvements over the CIVA pencil-tracing method include adaptive strategies for pencil subdivisions to achieve a good refinement of the sensor geometry while keeping a reasonable number of ray-tracing operations. Also, interpolation of the times of flight was used to avoid time consuming computations in the impulse response reconstruction stage. To achieve the best performance, our algorithm runs on multi-core superscalar CPUs and uses high performance specialized libraries such as Intel Embree for ray-tracing, Intel MKL for signal processing and Intel TBB for parallelization. We validated the simulation results by comparing them to the ones produced by CIVA on identical test configurations including mono-element and multiple-element transducers, homogeneous, meshed 3D CAD specimens, isotropic and anisotropic materials and wave paths that can involve several interactions with interfaces. We show performance results on complete simulations that achieve computation times in the 1s range.

  9. A feasibility study of high-strength Bi-2223 conductor for high-field solenoids

    Science.gov (United States)

    Godeke, A.; Abraimov, D. V.; Arroyo, E.; Barret, N.; Bird, M. D.; Francis, A.; Jaroszynski, J.; Kurteva, D. V.; Markiewicz, W. D.; Marks, E. L.; Marshall, W. S.; McRae, D. M.; Noyes, P. D.; Pereira, R. C. P.; Viouchkov, Y. L.; Walsh, R. P.; White, J. M.

    2017-03-01

    We performed a feasibility study on a high-strength Bi{}2-xPb x Sr2Ca2Cu3O{}10-x(Bi-2223) tape conductor for high-field solenoid applications. The investigated conductor, DI-BSCCO Type HT-XX, is a pre-production version of Type HT-NX, which has recently become available from Sumitomo Electric Industries. It is based on their DI-BSCCO Type H tape, but laminated with a high-strength Ni-alloy. We used stress-strain characterizations, single- and double-bend tests, easy- and hard-way bent coil-turns at various radii, straight and helical samples in up to 31.2 T background field, and small 20-turn coils in up to 17 T background field to systematically determine the electro-mechanical limits in magnet-relevant conditions. In longitudinal tensile tests at 77 K, we found critical stress- and strain-levels of 516 MPa and 0.57%, respectively. In three decidedly different experiments we detected an amplification of the allowable strain with a combination of pure bending and Lorentz loading to ≥slant 0.92 % (calculated elastically at the outer tape edge). This significant strain level, and the fact that it is multi-filamentary conductor and available in the reacted and insulated state, makes DI-BSCCO HT-NX highly suitable for very high-field solenoids, for which high current densities and therefore high loads are required to retain manageable magnet dimensions.

  10. ENDOR/ESR of Mn atoms and MnH molecules in solid argon

    Science.gov (United States)

    van Zee, R. J.; Garland, D. A.; Weltner, W., Jr.

    1986-09-01

    Mn atoms and MnH molecules, the latter formed by reaction between metal and hydrogen atoms, were trapped in solid argon and their ESR/ENDOR spectra measured at 4 K. At each pumping magnetic field two ENDOR lines were observed for 55Mn(I=5/2) atoms, corresponding to hyperfine transitions within the MS =±1/2 levels. Values of the hyperfine interaction constant and nuclear moment of 55Mn were derived from the six sets of data. For MnH, three sets of signals were detected: a proton ``matrix ENDOR'' line, transitions in the MS =0,±1 levels involving MI (55Mn)=1/2, 3/2, 5/2 levels, and proton transitions corresponding to νH and νH±aH. Analysis yielded the hyperfine constant aH =6.8(1) MHz and the nuclear quadrupole coupling constant Q'(55Mn)=-11.81(2) MHz. The latter compared favorably with a theoretical value derived earlier by Bagus and Schaefer. A higher term in the spin Hamiltonian appeared to be necessary to fit the proton hyperfine data.

  11. High field Moessbauer study of dilute Ir-(Fe) alloys

    International Nuclear Information System (INIS)

    Takabatake, Toshiro; Mazaki, Hiromasa; Shinjo, Teruya.

    1981-01-01

    The magnetic behavior of very dilute Fe impurities in Ir has been studied by means of Moessbauer measurement in external fields up to 80 kOe at 4.2 K. The saturation hyperfine field increases in proportion to the external field up to the maximum magnetic field available. This means that for a localized spin fluctuation system IrFe, the effective magnetic moment associated with Fe impurities is induced in proportion to the external field. No anomalous spectrum was observed with a very dilute sample (--10 ppm 57 Co), indicating that the interaction between impurities is responsible for the anomalous spectrum previously observed with a less homogeneous sample. (author)

  12. Characterization of free radicals in γ-irradiated polycrystalline uridine 5'-monophosphate: a study combining ESR, spin-trapping and HPLC

    International Nuclear Information System (INIS)

    Hiraoka, W.; Kuwabara, M.; Sato, F.

    1991-01-01

    Free radicals generated in γ-irradiated polycrystalline uridine 5'-monophosphate (5'-UMP) were studied by ESR, spin-trapping and high-performance liquid chromatography (HPLC). Although HPLC ultimately gave four spin-adducts, one component that was originally present disappeared during HPLC. Spin adducts due to two types of C6 radials were identified. One of these was thought to be formed by electron addition and subsequent protonation at the C6 position, and the other was presumed to be produced by electron addition and subsequent protonation at the O 4 position. The spin adducts derived from the C5 and C5' radicals were also identified. The spin adduct that disappeared during HPLC was thought to correspond to the C4'-centred radical. Computer simulation of ESR spectra was carried out to estimate the hyperfine splitting constants. (author)

  13. ESR signal features of 60Co γ-ray irradiated bone tissue and its dose response relationship

    International Nuclear Information System (INIS)

    Wu Ke; Sun Zunpu; Shi Yuanming

    1993-01-01

    Electron spin resonance (ESR) technique was used to study the radiation-induced ESR signal features of different paramagnetic species of 60 Co γ-ray irradiated bone tissue. The results showed that the intensity of an ESR signal at that the intensity of an ESR signal at g 2.0022 of human bones exposed to a dose range of 0-50 Gy had linear dose response relationships. The lower limit of detectable dose was about 2 Gy and the detecting error was about 10%. The signal was stable at room temperature during 60 days, and the effect of radiation dose rate of 0.5-8.0 Gy/min could be neglected. This signal was insensitive to microwave power and temperature, which was suitable for rapid and direct detection with ESR technique. These features suggest that human bones could be used for radiation accident dose evaluation by ESR

  14. R and D status and requirements for PIE in the fields of the HTGR fuel and the innovative basic research on High-Temperature Engineering

    Energy Technology Data Exchange (ETDEWEB)

    Sawa, Kazuhiro; Tobita, Tsutomu; Sumita, Junya [Japan Atomic Energy Research Inst., Oarai, Ibaraki (Japan). Oarai Research Establishment; Ishihara, Masahiro; Hayashi, Kimio; Hoshiya, Taiji; Sekino, Hajime; Ooeda, Etsurou

    1999-09-01

    The High Temperature Engineering Test Reactor (HTTR), which is the first high temperature gas-cooled reactor (HTGR) in Japan, achieved its first criticality in November 1998 at the Oarai Research Establishment of the Japan Atomic Energy Research Institute (JAERI). In the field of HTGR fuel development, JAERI will proceed research and development (R and D) works by the following steps: (STEP-1) confirmation of irradiation performance of the first-loading fuel of the HTTR, (STEP-2) study on irradiation performance of high burnup SiC-coated fuel particle and (STEP-3) development of ZrC-coated fuel particle. Requirements for post-irradiation examination (PIE) are different for each R and D step. In STEP-1, firstly, hot cells will be prepared in the HTTR reactor building to handle spent fuels. In parallel, general equipments such as those for deconsolidation of fuel compacts and for handling coated fuel particles will be installed in the Hot Laboratory at Oarai. In STEP-2, precise PIE techniques, for example, Raman spectroscopy for measurement of stress on irradiated SiC layer, will be investigated. In STEP-3, new PIE techniques should be developed to investigate irradiation behavior of ZrC-coated particle. In the field of the innovative basic research on high-temperature engineering, some preliminary tests have been made on the research areas of (1) new materials development, (2) fusion technology, (3) radiation chemistry and (4) high-temperature in-core instrumentation. Requirements for PIE are under investigation, in particular in the field of the new materials development. Besides more general apparatuses including transmission electron microscopy (TEM), some special apparatuses such as an electron spin resonance (ESR) spectrometer, a specific resistance/Hall coefficient measuring system and a differential scanning calorimeter (DSC) are planned to install in the Hot Laboratory at Oarai. Acquisition of advanced knowledge on the irradiation behavior is expected in

  15. Double disordered YBCO coated conductors of industrial scale: high currents in high magnetic field

    International Nuclear Information System (INIS)

    Abraimov, D; Francis, A; Jaroszynski, J; McCallister, J; Polyanskii, A; Santos, M; Viouchkov, Y L; Ballarino, A; Bottura, L; Rossi, L; Barth, C; Senatore, C; Dietrich, R; Rutt, A; Schlenga, K; Usoskin, A; Majkic, G S; Selvamanickam, V

    2015-01-01

    A significant increase of critical current in high magnetic field, up to 31 T, was recorded in long tapes manufactured by employing a double-disorder route. In a double-disordered high-temperature superconductor (HTS), a superimposing of intrinsic and extrinsic disorder takes place in a way that (i) the intrinsic disorder is caused by local stoichiometry deviations that lead to defects of crystallinity that serve as pining centers in the YBa 2 Cu 3 O x−δ matrix and (ii) the extrinsic disorder is introduced via embedded atoms or particles of foreign material (e.g. barium zirconate), which create a set of lattice defects. We analyzed possible technological reasons for this current gain. The properties of these tapes over a wider field-temperature range as well as field anisotropy were also studied. Record values of critical current as high as 309 A at 31 T, 500 A at 18 Tm and 1200 A at 5 T were found in 4 mm wide tape at 4.2 K and B perpendicular to tape surface. HTS layers were processed in medium-scale equipment that allows a maximum batch length of 250 m while 22 m long batches were provided for investigation. Abnormally high ratios (up to 10) of critical current density measured at 4.2 K, 19 T to critical current density measured at 77 K, self-field were observed in tapes with the highest in-field critical current. Anisotropy of the critical current as well as angular dependences of n and α values were investigated. The temperature dependence of critical current is presented for temperatures between 4.2 and 40 K. Prospects for the suppression of the dog-bone effect by Cu plating and upscale of processing chain to >500 m piece length are discussed. (paper)

  16. Double disordered YBCO coated conductors of industrial scale: high currents in high magnetic field

    Science.gov (United States)

    Abraimov, D.; Ballarino, A.; Barth, C.; Bottura, L.; Dietrich, R.; Francis, A.; Jaroszynski, J.; Majkic, G. S.; McCallister, J.; Polyanskii, A.; Rossi, L.; Rutt, A.; Santos, M.; Schlenga, K.; Selvamanickam, V.; Senatore, C.; Usoskin, A.; Viouchkov, Y. L.

    2015-11-01

    A significant increase of critical current in high magnetic field, up to 31 T, was recorded in long tapes manufactured by employing a double-disorder route. In a double-disordered high-temperature superconductor (HTS), a superimposing of intrinsic and extrinsic disorder takes place in a way that (i) the intrinsic disorder is caused by local stoichiometry deviations that lead to defects of crystallinity that serve as pining centers in the YBa2Cu3O x-δ matrix and (ii) the extrinsic disorder is introduced via embedded atoms or particles of foreign material (e.g. barium zirconate), which create a set of lattice defects. We analyzed possible technological reasons for this current gain. The properties of these tapes over a wider field-temperature range as well as field anisotropy were also studied. Record values of critical current as high as 309 A at 31 T, 500 A at 18 Tm and 1200 A at 5 T were found in 4 mm wide tape at 4.2 K and B perpendicular to tape surface. HTS layers were processed in medium-scale equipment that allows a maximum batch length of 250 m while 22 m long batches were provided for investigation. Abnormally high ratios (up to 10) of critical current density measured at 4.2 K, 19 T to critical current density measured at 77 K, self-field were observed in tapes with the highest in-field critical current. Anisotropy of the critical current as well as angular dependences of n and α values were investigated. The temperature dependence of critical current is presented for temperatures between 4.2 and 40 K. Prospects for the suppression of the dog-bone effect by Cu plating and upscale of processing chain to >500 m piece length are discussed.

  17. Survey of Processing Methods for High Strength High Conductivity Wires for High Field Magnet Applications

    Energy Technology Data Exchange (ETDEWEB)

    Han, K.; Embury, J.D.

    1998-10-01

    This paper will deal with the basic concepts of attaining combination of high strength and high conductivity in pure materials, in-situ composites and macrocomposites. It will survey current attainments, and outline where some future developments may lie in developing wire products that are close to the theoretical strength of future magnet applications.

  18. Survey of Processing Methods for High Strength High Conductivity Wires for High Field Magnet Applications

    International Nuclear Information System (INIS)

    Han, K.; Embury, J.D.

    1998-01-01

    This paper will deal with the basic concepts of attaining combination of high strength and high conductivity in pure materials, in-situ composites and macrocomposites. It will survey current attainments, and outline where some future developments may lie in developing wire products that are close to the theoretical strength of future magnet applications

  19. Comparison of ESR1 Mutations in Tumor Tissue and Matched Plasma Samples from Metastatic Breast Cancer Patients

    Directory of Open Access Journals (Sweden)

    Takashi Takeshita

    2017-10-01

    Full Text Available BACKGROUND: ESR1 mutation in circulating cell-free DNA (cfDNA is emerging as a noninvasive biomarker of acquired resistance to endocrine therapy, but there is a paucity of data comparing the status of ESR1 gene in cfDNA with that in its corresponding tumor tissue. The objective of this study is to validate the degree of concordance of ESR1 mutations between plasma and tumor tissue. METHODS: ESR1 ligand-binding domain mutations Y537S, Y537N, Y537C, and D538G were analyzed using droplet digital PCR in 35 patients with metastatic breast cancer (MBC (35 tumor tissue samples and 67 plasma samples. RESULTS: Of the 35 paired samples, 26 (74.3% were concordant: one patient had detectable ESR1 mutations both plasma (ESR1 Y537S/Y537N and tumor tissue (ESR1 Y537S/Y537C, and 25 had WT ESR1 alleles in both. Nine (25.7% had discordance between the plasma and tissue results: five had mutations detected only in their tumor tissue (two Y537S, one Y537C, one D538G, and one Y537S/Y537N/D538G, and four had mutations detected only in their plasma (one Y537S, one Y537N, and two Y537S/Y537N/D538G. Furthermore, longitudinal plasma samples from 19 patients were used to assess changes in the presence of ESR1 mutations during treatment. Eleven patients had cfDNA ESR1 mutations over the course of treatment. A total of eight of 11 patients with MBC with cfDNA ESR1 mutations (72.7% had the polyclonal mutations. CONCLUSION: We have shown the independent distribution of ESR1 mutations between plasma and tumor tissue in 35 patients with MBC.

  20. Low field-low cost: Can low-field magnetic resonance systems replace high-field magnetic resonance systems in the diagnostic assessment of multiple sclerosis patients?

    International Nuclear Information System (INIS)

    Ertl-Wagner, B.B.; Reith, W.; Sartor, K.

    2001-01-01

    As low-field MR imaging is becoming a widely used imaging technique, we aimed at a prospective assessment of differences in imaging quality between low- and high-field MR imaging in multiple sclerosis patients possibly interfering with diagnostic or therapeutic decision making. Twenty patients with clinically proven multiple sclerosis were examined with optimized imaging protocols in a 1.5- and a 0.23-T MR scanner within 48 h. Images were assessed independently by two neuroradiologists. No statistically significant interrater discrepancies were observed. A significantly lower number of white matter lesions could be identified in low-field MR imaging both on T1- and on T2-weighted images (T2: high field 700, low field 481; T1: high field 253, low field 177). A total of 114 enhancing lesions were discerned in the high-field MR imaging as opposed to 45 enhancing lesions in low-field MR imaging. Blood-brain barrier disruption was identified in 11 of 20 patients in the high-field MR imaging, but only in 4 of 20 patients in low-field MR imaging. Since a significantly lower lesion load is identified in low-field MR imaging than in high-field MR imaging, and blood-brain barrier disruption is frequently missed, caution must be exercised in interpreting a normal low-field MR imaging scan in a patient with clinical signs of multiple sclerosis and in interpreting a scan without enhancing lesions in a patient with known multiple sclerosis and clinical signs of exacerbation. (orig.)

  1. Combined ESR and U-series isochron dating of fossil tooth from Longgupo cave

    International Nuclear Information System (INIS)

    Han Fei; Yin Gongming; Liu Chunru; Jean-Jacques Bahain

    2012-01-01

    Background: In ESR and luminescence archaeological dating, the assessment of external radiation dose rate is one of the constant sources of uncertainty because of its variation in the past time and it cannot be determined accurately using the present-day measurements. Purpose: ESR isochron protocol was proposed to solve this uncertainty for the tooth samples. This protocol is applicable wherever multiple samples with different internal doses have all experienced a common external dose. The variable uranium concentration of tooth samples makes it possible to plot the equivalent dose versus the internal dose rate of each sample, and the slope of isochron line gives hence the age. For isochron dating of teeth, combined ESR/U-series dating analysis must be done together with isochron protocol. Methods: In this study, we try to use combined ESR/U-series isochron method on 5 tooth samples collected from immediate adjacent square in layer C Ⅲ'6 of Longgupo archaeological site, Chongqing, China. Combined ESR/U-series analysis with in situ external dose rate shows recent uranium uptake of all the samples. Results: The time-averaged external dose rate was iterative calculated by isochron protocol, and gives an isochron age of 1.77±0.09 Ma for layer C Ⅲ'6, which consistent with the mean US-ESR ages of 5 samples (1.64+0.16/-0.21 Ma) in the error range. The calculated time-averaged external dose rate(∼807 μGy/a) was basically in agreement with the in situ measured gamma dose rate value (8.50 μGy/a) in 2006, indicating the geochemical alterations may not occurred or do not affect the environmental dose rate obviously during the burial history. Conclusions: This study indicates the potential of solving both internal and external dose rate problems of ESR dating of fossil teeth by combining with U-series analysis and isochron protocol. (authors)

  2. Gene Expression Analyses of HER-2/neu and ESR1 in Patients with Breast Cancer

    Directory of Open Access Journals (Sweden)

    Omid Kheyri Nadergoli

    2017-10-01

    Full Text Available ABSTRACT Background: Her-2 and ESR1 genes, that interact in the cell signaling pathway, are the most important molecular markers of breast cancer, which have been amplified or overexpressed in 30% and 70%, respectively. This study was performed to evaluate the gene expression levels of Her-2 and ESR1 genes in tumor cells and its adjacent normal tissue of breast cancer patients and compared them whit clinical-pathological features. Methods: In total, 80 tissue specimens from 40 patients, with an average age of 48.47 years, were examined by Real-time PCR technique, and ultimately evaluated the expression level of Her-2 and ESR1genes. The data were analyzed by REST 2009 V2.0.13 statistical software. Results: HER2 and ESR1 overexpression was identified in 19 (48% and 12 (30% of 40 patients respectively, which was higher and lower than that recorded in international statistics, respectively. ESR1 overexpression was associated with Stage 3A and lymph node involvement 2 (N2 (P = 0.04 and P = 0.047, respectively. No significant correlation was observed between the expression of HER2 and ESR1 and other clinical-pathological features, however, the relative differences were identified in the expression levels of genes between main group and groups that were classified according to the clinical-pathological features and age. Conclusions: Overexpression of Her-2 and ESR1 genes in the patients of our study are higher and lower than international statistics, respectively, indicating the differences in genetic, environmental and ethnic factors that involved in the developing of breast cancer.

  3. Investigation and dating of gypsum crystals from Sivrihisar region in Eskisehir by ESR and TL techniques

    International Nuclear Information System (INIS)

    2011-01-01

    Gypsum crystals taken from Sivrihisar-Eskisehir district were investigated and dated by Electron Spin Resonance (ESR) and Thermoluminescence (TL) techniques. The natural ESR spectra of gypsum samples had also the signals of Mn 2 + in addition to the signal at g=2.009. It was observed that the intensity of ESR signal at g=2.009 increased with gamma irradiation dose. This ESR signal (g=2.009) was used as a dating signal in dating of gypsum samples. The only one TL peak at about 278 degree Celsius was observed in TL glow curves of nonirradiated gypsum sample. In the case of irradiated sample, TL peak at 157 degree Celsius was observed in addition of TL peak at 278 degree Celsius. Gypsum samples were irradiated with a 6 0Co gamma source. The ESR spectra and TL glow curve of gypsum samples were recorded by X-band ESR spectrometer and Risφ TL/OSL reader, respectively. For samples, ESR/TL dose-response curves was constructed. Dose-response curves were fitted with an exponential saturation function. Based on this model, accumulated dose (AD) values for dating are determined. 2 38U, 2 32Th and 4 0K analysis was carried out for gypsum crystals and dolomite which enveloped these gypsum crystals. The internal dose rate was calculated from 2 38U, 2 32Th and 4 0K analysis results of gypsum sample. The external dose rate was calculated by using 2 38U, 2 32Th and 4 0K analysis results of dolomite and cosmic dose rate. Internal and external gamma dose-rate was used for dating calculations. Because of successive recrystallization of gypsum sample after formation, calculated age values of gypsum is smaller than expected formation age.

  4. Endocrine-Therapy-Resistant ESR1 Variants Revealed by Genomic Characterization of Breast-Cancer-Derived Xenografts

    Directory of Open Access Journals (Sweden)

    Shunqiang Li

    2013-09-01

    Full Text Available To characterize patient-derived xenografts (PDXs for functional studies, we made whole-genome comparisons with originating breast cancers representative of the major intrinsic subtypes. Structural and copy number aberrations were found to be retained with high fidelity. However, at the single-nucleotide level, variable numbers of PDX-specific somatic events were documented, although they were only rarely functionally significant. Variant allele frequencies were often preserved in the PDXs, demonstrating that clonal representation can be transplantable. Estrogen-receptor-positive PDXs were associated with ESR1 ligand-binding-domain mutations, gene amplification, or an ESR1/YAP1 translocation. These events produced different endocrine-therapy-response phenotypes in human, cell line, and PDX endocrine-response studies. Hence, deeply sequenced PDX models are an important resource for the search for genome-forward treatment options and capture endocrine-drug-resistance etiologies that are not observed in standard cell lines. The originating tumor genome provides a benchmark for assessing genetic drift and clonal representation after transplantation.

  5. Structure of very heavy few-electron ions - new results from the heavy ion storage ring, ESR

    International Nuclear Information System (INIS)

    Mokler, P.H.; Stoehlker, T.; Kozhuharov, C.; Moshammer, R.; Rymuza, P.; Bosch, F.; Kandler, T.

    1993-08-01

    The heavy ion synchrotron/storage ring facility at GSI, SIS/ESR, provides intense beams of cooled, highly-charged ions up to naked uranium (U 92+ ). By electron capture during ion-atom collisions in the gas target of the ESR or by recombination at ion-electron encounters in the ''electron cooler'' excited states are populated. The detailed structure of very heavy one-, two- and three-electron ions is studied. The different mechanisms leading to the excited states are described, as well as the new experimental tools now available for a detailed spectroscopy of these interesting systems. Special emphasis is given to X-ray transitions to the groundstates in H- and He-like systems. For the heaviest species the groundstate Lambshift can now be probed on an accuracy level of better than 10% using solid-state X-ray detectors. Applying dispersive X-ray analyzing techniques, this accuracy will certainly be improved in future. However, utilizing the dielectronic resonances for a spectroscopy, the structure in Li-like heavy ions can already be probed now on the sub eV level. (orig.)

  6. A high-gain high-power L-band antenna for field test applications

    Science.gov (United States)

    Abe, David K.; Tran, George T.; Knop, C. M.

    1995-09-01

    A high-gain, prime-focus parabolic dish antenna system was designed and constructed for experimental use in the field. The antenna was designed to radiate in L-band at peak power levels exceeding 1 X 106 watts. A 3.6 m diameter, commercial off-the-shelf parabolic dish antenna was modified with a custom-designed waveguide horn feed. The system was mounted on an antenna pedestal to allow for fine (approximately 0.001 degrees) elevation and azimuth control; the antenna and pedestal were mounted on a 4.3 m long trailer for mobility in the field. The antenna has a measured gain of 32 dBi and a 3-dB beamwidth of approximately 4.5 degrees. The system was successfully operated in the field in L-band at peak power levels exceeding 5 MW. The design, calibration, and testing of the antenna system will be presented.

  7. Low and High-Frequency Field Potentials of Cortical Networks ...

    Science.gov (United States)

    Neural networks grown on microelectrode arrays (MEAs) have become an important, high content in vitro assay for assessing neuronal function. MEA experiments typically examine high- frequency (HF) (>200 Hz) spikes, and bursts which can be used to discriminate between different pharmacological agents/chemicals. However, normal brain activity is additionally composed of integrated low-frequency (0.5-100 Hz) field potentials (LFPs) which are filtered out of MEA recordings. The objective of this study was to characterize the relationship between HF and LFP neural network signals, and to assess the relative sensitivity of LFPs to selected neurotoxicants. Rat primary cortical cultures were grown on glass, single-well MEA chips. Spontaneous activity was sampled at 25 kHz and recorded (5 min) (Multi-Channel Systems) from mature networks (14 days in vitro). HF (spike, mean firing rate, MFR) and LF (power spectrum, amplitude) components were extracted from each network and served as its baseline (BL). Next, each chip was treated with either 1) a positive control, bicuculline (BIC, 25μM) or domoic acid (DA, 0.3μM), 2) or a negative control, acetaminophen (ACE, 100μM) or glyphosate (GLY, 100μM), 3) a solvent control (H2O or DMSO:EtOH), or 4) a neurotoxicant, (carbaryl, CAR 5, 30μM ; lindane, LIN 1, 10μM; permethrin, PERM 25, 50μM; triadimefon, TRI 5, 65μM). Post treatment, 5 mins of spontaneous activity was recorded and analyzed. As expected posit

  8. Workshop on High-Field NMR and Biological Applications

    Science.gov (United States)

    Scientists at the Pacific Northwest Laboratory have been working toward the establishment of a new Molecular Science Research Center (MSRC). The primary scientific thrust of this new research center is in the areas of theoretical chemistry, chemical dynamics, surface and interfacial science, and studies on the structure and interactions of biological macromolecules. The MSRC will provide important new capabilities for studies on the structure of biological macromolecules. The MSRC program includes several types of advanced spectroscopic techniques for molecular structure analysis, and a theory and modeling laboratory for molecular mechanics/dynamics calculations and graphics. It is the goal to closely integrate experimental and theoretical studies on macromolecular structure, and to join these research efforts with those of the molecular biological programs to provide new insights into the structure/function relationships of biological macromolecules. One of the areas of structural biology on which initial efforts in the MSRC will be focused is the application of high field, 2-D NMR to the study of biological macromolecules. First, there is interest in obtaining 3-D structural information on large proteins and oligonucleotides. Second, one of the primary objectives is to closely link theoretical approaches to molecular structure analysis with the results obtained in experimental research using NMR and other spectroscopies.

  9. The design of a large aperture high field dipole

    International Nuclear Information System (INIS)

    Harfoush, F.; Harrison, M.; Kerby, J.; Koepke, K.; Mantsch, P.; Nicol, T.; Riddiford, A.; Theilacker, J.

    1989-12-01

    The impetus for this design report originated in the Snowmass 88 meeting where the subject of higher energies within the constraints of the existing Tevatron tunnel enclosure was investigated. It was determined that beam transport to the fixed target experimental areas was possible up to an energy of ∼1.5 Tev. Collider operation was feasible at somewhat higher energies (1.8 Tev), primarily limited by the ability to design a single turn beam abort system within the constraints of the straight section length. A new accelerator in the existing tunnel would, of necessity, have a similar though not identical lattice and straight section layout to the present Tevatron. Thus when issues arose in the magnet design requiring input from the accelerator standpoint we have assumed a Tevatron like machine. The possibility of using these high field magnets as elements in the existing Tevatron to create new 'warm space,' for another Interaction Region for example, also emphasizes compatibility with the present machine. 16 refs., 62 figs., 23 tabs

  10. High resolution geomagnetic field observations at Terra Nova bay, Antarctica

    Directory of Open Access Journals (Sweden)

    P. Palangio

    1996-06-01

    Full Text Available he preliminary results obtained from the analysis in the micropulsation frequency range of high time resolution magnetic field data recorded at the Antarctic Italian geomagnetic observatory at Terra Nova Bay for 11 consecutive days in February 1994 are reported. The spectral index over the whole Pcl-Pc5 frequency range is of the order of 3.5 and its value significantly increases beyond about 50 mHz. Spectral peaks in the Pc3 frequency range are common, especially during the daytime hours, and are probably due to the direct penetration of upstream waves in the cusp region. From the local time distribution of the micro pulsation power, a signifi - cant activity enhancement around the local magnetic noon emerges, in agreement with previous observations. The analysis of the signal polarisation characteristics in the horizontal plane shows a predominant CW polarisation in the Pcl-Pc3 frequency ranges with the major axis of the polarisation ellipse in the first quadrant.

  11. Radiation distribution sensor with optical fibers for high radiation fields

    International Nuclear Information System (INIS)

    Takada, Eiji; Kimura, Atsushi; Hosono, Yoneichi; Takahashi, Hiroyuki; Nakazawa, Masaharu

    1999-01-01

    Radiation distribution sensors with their feasibilities have been described in earlier works. However, due to large radiation induced transmission losses in optical fibers, especially in the visible wavelength region, it has been difficult to apply these techniques to high radiation fields. In this study, we proposed a new concept of optical fiber based radiation distribution measurements with near infrared (IR) emission. Near IR scintillators were attached to the ends of optical fibers, where the fibers were bundled and connected to an N-MOS line sensor or a cooled CCD camera. From the measurements of each area density, the radiation levels at the positions of the scintillators can be known. The linearity between the gamma dose rate at each scintillator and the registered counts has been examined. For correcting the radiation induced loss effects, we applied the Optical Time Domain Reflectometry technique to measure the loss distribution and from the results, a possibility for correction of the loss effect has been demonstrated. The applicable dose rate range was evaluated to be from 0.1 to 10 3 Gy/h. This system can be a promising tool as a flexible dose rate distribution monitor in radiation facilities like nuclear plants and accelerator facilities. (author)

  12. Ultrafast outflows disappear in high-radiation fields

    Science.gov (United States)

    Pinto, C.; Alston, W.; Parker, M. L.; Fabian, A. C.; Gallo, L. C.; Buisson, D. J. K.; Walton, D. J.; Kara, E.; Jiang, J.; Lohfink, A.; Reynolds, C. S.

    2018-05-01

    Ultrafast outflows (UFOs) are the most extreme winds launched by active galactic nuclei (AGN) due to their mildly relativistic speeds (˜0.1-0.3c) and are thought to significantly contribute to galactic evolution via AGN feedback. Their nature and launching mechanism are however not well understood. Recently, we have discovered the presence of a variable UFO in the narrow-line Seyfert 1 IRAS 13224-3809. The UFO varies in response to the brightness of the source. In this work we perform flux-resolved X-ray spectroscopy to study the variability of the UFO and found that the ionization parameter is correlated with the luminosity. In the brightest states the gas is almost completely ionized by the powerful radiation field and the UFO is hardly detected. This agrees with our recent results obtained with principal component analysis. We might have found the tip of the iceberg: the high ionization of the outflowing gas may explain why it is commonly difficult to detect UFOs in AGN and possibly suggest that we may underestimate their actual feedback. We have also found a tentative correlation between the outflow velocity and the luminosity, which is expected from theoretical predictions of radiation-pressure-driven winds. This trend is rather marginal due to the Fe XXV-XXVI degeneracy. Further work is needed to break such degeneracy through time-resolved spectroscopy.

  13. A Shared Compliance Control for Application in High Radiation Fields

    International Nuclear Information System (INIS)

    Ahn, Sung Ho; Jung, Hoan Sung; Lee, Kye Hong; Kim, Young Ki; Kim, Hark Rho

    2005-01-01

    Bilateral control systems present a technical alternative for intelligent robotic systems performing dexterous tasks in unstructured environments such as a nuclear facility, outer space and underwater. A shared compliance control scheme is proposed for application in high radiation fields in which the force sensor can not be installed because of a radiation effect. A position difference between the master system and the slave system is treated as an equivalent contact force and used for an input to the compliance controller. The compliance controller is implemented by a first order low pass filter and it modifies the position of the master to the reference position. Thus the compliance control task is shared by both the human operator's direct manual control and the autonomous compliance control of the slave system. Consequently, the position of a slave system tracks well the reference position and the compliance of the slave system is autonomously controlled in a contact condition. The simulation results show the excellence of the proposed scheme

  14. The New High Magnetic Field Laboratory at Dresden: a Pulsed-Field Laboratory at an IR Free-Electron-Laser

    International Nuclear Information System (INIS)

    Pobell, F.; Bianchi, A. D.; Herrmannsdoerfer, T.; Krug, H.; Zherlitsyn, S.; Zvyagin, S.; Wosnitza, J.

    2006-01-01

    We report on the construction of a new high magnetic field user laboratory which will offer pulsed-field coils in the range (60 T, 500 ms, 40 mm) to (100 T, 10 ms, 20 mm) for maximum field, pulse time, and bore diameter of the coils. These coils will be energized by a modular 50 MJ/24 kV capacitor bank. Besides many other experimental techniques, as unique possibilities NMR in pulsed fields as well as infrared spectroscopy at 5 to 150 μm will be available by connecting the pulsed field laboratory to a nearby free-electron-laser facility

  15. High field superconducting magnets for accelerators and particle beams

    International Nuclear Information System (INIS)

    Allinger, J.; Danby, G.; Jackson, J.

    1975-01-01

    Experience in designing precision superconducting magnets for fields up to 60 kG is described. Realizable construction tolerances and their impact on field accuracy are discussed. For dipole fields up to 60 kG or more, rectangular coil window frame type magnets are compared with circular or elliptical coil designs. In all cases, the same superconductor current density versus maximum field performance is assumed. The comparison will include field quality and correction required as a function of aperture size, stored energy, ampere turns required, and overall magnet size. In quadrupole design the impact of the allowed superconductor current density being roughly inversely proportional to peak field is severe. For gradients up to one Tesla/cm or greater, similar comparisons for different types of quadrupole construction are made. (U.S.)

  16. ADX: a high field, high power density, advanced divertor and RF tokamak

    Science.gov (United States)

    LaBombard, B.; Marmar, E.; Irby, J.; Terry, J. L.; Vieira, R.; Wallace, G.; Whyte, D. G.; Wolfe, S.; Wukitch, S.; Baek, S.; Beck, W.; Bonoli, P.; Brunner, D.; Doody, J.; Ellis, R.; Ernst, D.; Fiore, C.; Freidberg, J. P.; Golfinopoulos, T.; Granetz, R.; Greenwald, M.; Hartwig, Z. S.; Hubbard, A.; Hughes, J. W.; Hutchinson, I. H.; Kessel, C.; Kotschenreuther, M.; Leccacorvi, R.; Lin, Y.; Lipschultz, B.; Mahajan, S.; Minervini, J.; Mumgaard, R.; Nygren, R.; Parker, R.; Poli, F.; Porkolab, M.; Reinke, M. L.; Rice, J.; Rognlien, T.; Rowan, W.; Shiraiwa, S.; Terry, D.; Theiler, C.; Titus, P.; Umansky, M.; Valanju, P.; Walk, J.; White, A.; Wilson, J. R.; Wright, G.; Zweben, S. J.

    2015-05-01

    The MIT Plasma Science and Fusion Center and collaborators are proposing a high-performance Advanced Divertor and RF tokamak eXperiment (ADX)—a tokamak specifically designed to address critical gaps in the world fusion research programme on the pathway to next-step devices: fusion nuclear science facility (FNSF), fusion pilot plant (FPP) and/or demonstration power plant (DEMO). This high-field (⩾6.5 T, 1.5 MA), high power density facility (P/S ˜ 1.5 MW m-2) will test innovative divertor ideas, including an ‘X-point target divertor’ concept, at the required performance parameters—reactor-level boundary plasma pressures, magnetic field strengths and parallel heat flux densities entering into the divertor region—while simultaneously producing high-performance core plasma conditions that are prototypical of a reactor: equilibrated and strongly coupled electrons and ions, regimes with low or no torque, and no fuelling from external heating and current drive systems. Equally important, the experimental platform will test innovative concepts for lower hybrid current drive and ion cyclotron range of frequency actuators with the unprecedented ability to deploy launch structures both on the low-magnetic-field side and the high-magnetic-field side—the latter being a location where energetic plasma-material interactions can be controlled and favourable RF wave physics leads to efficient current drive, current profile control, heating and flow drive. This triple combination—advanced divertors, advanced RF actuators, reactor-prototypical core plasma conditions—will enable ADX to explore enhanced core confinement physics, such as made possible by reversed central shear, using only the types of external drive systems that are considered viable for a fusion power plant. Such an integrated demonstration of high-performance core-divertor operation with steady-state sustainment would pave the way towards an attractive pilot plant, as envisioned in the ARC concept

  17. WISH: Wide-field Imaging Durvayor for High-redshift

    Science.gov (United States)

    Yamada, Toru

    2015-08-01

    We introduce the concept and current status of WISH project and discuss the science cases. WISH is a proposed space science mission for JAXA, which is dedicated for the deep and wide-field near-infrared imaging surveys. The mission contains the 1.5m cooled telescope as well as the imager with the FoV of ~850 square arcmin. The main goal of WISH is to detect and study galaxies at z=8-15 in the earliest history of structure formation in the universe. The key feature is to conduct WISH Ultra Deep Survey, which images in total of 100 square degrees in 6 broad-band filters at 0.9-4.5 micron down to 28AB magnitude. While more than 10^5 galaxies at z=8-9, 10^4 galaxies at z=11-12 will be detected, WISH-UDS is designed to constrain UV luminosity function at z=15. Depending on the models of the earliest evolution history, 1-1000 galaxies at z~15 (~100 galaxies for the moderate cases) will be detected. The UV spectral properties as well as the clustering properties of galaxies at z=8-15 can be studied as well; UV slope can be measured up to z=15, and the stellar and dark-matter-halo masses can be obtained up to z=9. WISH UDS can provide excellent opportunities for studying SNe at high redshift. Up to ~7000 type Ia SNe at z>1 can be detected and the distance modulus can be constrained with the precision of 0.9-1.5% at z>1.5. More than 100 Super Luminous SNe at z>6, and 10 SLSN at z>10 can also be detected, which allow us to study the earliest history of massive star formation in the universe. WISH imaging surveys as well as WISHSpec, which is an optional parallel-operation simple IFU spectrograph, also provide unique opportunities in various astronomical fields. WISH mission proposal was submitted to JAXA in February 2015 for the first down selection of JAXA Large Strategic Science Mission targeting the launch date in 2020-22. International collaborations including SAO (G.Fazio et al.), LAM (D. Burgarella et al.) and Canada (M.Sawicki et al.) are also actively coordinated.

  18. Fabrication of highly ordered nanoporous alumina films by stable high-field anodization

    International Nuclear Information System (INIS)

    Li Yanbo; Zheng Maojun; Ma Li; Shen Wenzhong

    2006-01-01

    Stable high-field anodization (1500-4000 A m -2 ) for the fabrication of highly ordered porous anodic alumina films has been realized in a H 3 PO 4 -H 2 O-C 2 H 5 OH system. By maintaining the self-ordering voltage and adjusting the anodizing current density, high-quality self-ordered alumina films with a controllable inter-pore distance over a large range are achieved. The high anodizing current densities lead to high-speed film growth (4-10 μm min -1 ). The inter-pore distance is not solely dependent on the anodizing voltage, but is also influenced by the anodizing current density. This approach is simple and cost-effective, and is of great value for applications in diverse areas of nanotechnology

  19. Frequency dependent power fluctuations: a feature of the ESR system or physical?

    Directory of Open Access Journals (Sweden)

    Y. Ogawa

    Full Text Available The k-dependence of the received power in high signal-to-noise ratio (SNR conditions, occurring for naturally enhanced ion-acoustic lines (NEIALs and for real satellites, is investigated by using the EISCAT Svalbard Radar (ESR, where the data are recorded in eight separate channels using different frequencies. For the real satellites we find large variations of the relative powers from event to event, which is probably due to a different number of pulses catching the satellite over the integration period. However, the large power difference remains unexpected in one case. Over short time scale (< 10 s the relative power difference seems to be highly stable. For most NEIAL events the differences between channels are within noise level. In a few cases variations of the relative power well above both the estimated and expected 1-sigma level occur over a signal preintegrated profile. We thus suggest that the frequency dependence of the power in NEIAL events has its origin in the scattering medium itself as the most plausible explanation.

    Key words: Ionosphere (auroral ionosphere; plasma waves and instabilities; instruments and techniques

  20. Frequency dependent power fluctuations: a feature of the ESR system or physical?

    Directory of Open Access Journals (Sweden)

    Y. Ogawa

    2000-09-01

    Full Text Available The k-dependence of the received power in high signal-to-noise ratio (SNR conditions, occurring for naturally enhanced ion-acoustic lines (NEIALs and for real satellites, is investigated by using the EISCAT Svalbard Radar (ESR, where the data are recorded in eight separate channels using different frequencies. For the real satellites we find large variations of the relative powers from event to event, which is probably due to a different number of pulses catching the satellite over the integration period. However, the large power difference remains unexpected in one case. Over short time scale (< 10 s the relative power difference seems to be highly stable. For most NEIAL events the differences between channels are within noise level. In a few cases variations of the relative power well above both the estimated and expected 1-sigma level occur over a signal preintegrated profile. We thus suggest that the frequency dependence of the power in NEIAL events has its origin in the scattering medium itself as the most plausible explanation.Key words: Ionosphere (auroral ionosphere; plasma waves and instabilities; instruments and techniques