Atomic physics with hard X-rays from high brilliance synchrotron light sources

Energy Technology Data Exchange (ETDEWEB)

Southworth, S.; Gemmell, D.

1996-08-01

A century after the discovery of x rays, the experimental capability for studying atomic structure and dynamics with hard, bright synchrotron radiation is increasing remarkably. Tempting opportunities arise for experiments on many-body effects, aspects of fundamental photon-atom interaction processes, and relativistic and quantum-electrodynamic phenomena. Some of these possibilities are surveyed in general terms.

A novel probe of intrinsic electronic structure: hard X-ray photoemission spectroscopy

International Nuclear Information System (INIS)

Takata, Y.; Tamasaku, K.; Nishino, Y.; Miwa, D.; Yabashi, M.; Ikenaga, E.; Horiba, K.; Arita, M.; Shimada, K.; Namatame, H.; Nohira, H.; Hattori, T.; Soedergren, S.; Wannberg, B.; Taniguchi, M.; Shin, S.; Ishikawa, T.; Kobayashi, K.

2005-01-01

We have realized hard X-ray (HX) photoemission spectroscopy (PES) with high throughput and high-energy resolution for core level and valence band studies using high-energy and high-brilliance synchrotron radiation at SPring-8. This is a brand new method because large escape depth of high-energy photoelectrons enables us to probe intrinsic bulk states free from surface condition. By use of a newly developed electron energy analyzer and well-focused X-rays, high-energy resolution of 75 meV (E/ΔE 79,000) was realized for 5.95 keV photoelectrons

Three-Dimensional X-Ray Diffraction Technique for Metals Science

DEFF Research Database (Denmark)

Zhang, Yubin; Fan, Guohua

2017-01-01

The three-dimensional X-ray diffraction (3DXRD) is a new, advanced technique for materials characterization. This technique utilizes high-energy synchrotron X-rays to characterize the 3D crystallographic structure and strain/stress state of bulk materials. As the measurement is non......-destructive, the microstructural evolution as a function of time can be followed, i.e. it allows 4D (x, y, z characterizations, t). The high brilliance of synchrotron X-rays ensures that diffraction signals from volumes of micrometer scale can be quickly detected and distinguished from the background noise, i.e. its spatial...... implemented in several large synchrotron facilities, e.g. the Advanced Photon Source (APS) in USA and the Spring-8 in Japan. Another family of 3DXRD technique that utilizes white beam synchrotron X-rays has also been developed in parallel in cooperation between Oak Ridge National Laboratory and APS...

High-resolution X-ray imaging - a powerful nondestructive technique for applications in semiconductor industry

International Nuclear Information System (INIS)

Zschech, Ehrenfried; Yun, Wenbing; Schneider, Gerd

2008-01-01

The availability of high-brilliance X-ray sources, high-precision X-ray focusing optics and very efficient CCD area detectors has contributed essentially to the development of transmission X-ray microscopy (TXM) and X-ray computed tomography (XCT) with sub-50 nm resolution. Particularly, the fabrication of high aspect ratio Fresnel zone plates with zone widths approaching 15 nm has contributed to the enormous improvement in spatial resolution during the previous years. Currently, Fresnel zone plates give the ability to reach spatial resolutions of 15 to 20 nm in the soft and of about 30 to 50 nm in the hard X-ray energy range. X-ray microscopes with rotating anode X-ray sources that can be installed in an analytical lab next to a semiconductor fab have been developed recently. These unique TXM/XCT systems provide an important new capability of nondestructive 3D imaging of internal circuit structures without destructive sample preparation such as cross sectioning. These lab systems can be used for failure localization in micro- and nanoelectronic structures and devices, e.g., to visualize voids and residuals in on-chip metal interconnects without physical modification of the chip. Synchrotron radiation experiments have been used to study new processes and materials that have to be introduced into the semiconductor industry. The potential of TXM using synchrotron radiation in the soft X-ray energy range is shown for the nondestructive in situ imaging of void evolution in embedded on-chip copper interconnect structures during electromigration and for the imaging of different types of insulating thin films between the on-chip interconnects (spectromicroscopy). (orig.)

Soft X-ray radiation damage in EM-CCDs used for Resonant Inelastic X-ray Scattering

Science.gov (United States)

Gopinath, D.; Soman, M.; Holland, A.; Keelan, J.; Hall, D.; Holland, K.; Colebrook, D.

2018-02-01

Advancement in synchrotron and free electron laser facilities means that X-ray beams with higher intensity than ever before are being created. The high brilliance of the X-ray beam, as well as the ability to use a range of X-ray energies, means that they can be used in a wide range of applications. One such application is Resonant Inelastic X-ray Scattering (RIXS). RIXS uses the intense and tuneable X-ray beams in order to investigate the electronic structure of materials. The photons are focused onto a sample material and the scattered X-ray beam is diffracted off a high resolution grating to disperse the X-ray energies onto a position sensitive detector. Whilst several factors affect the total system energy resolution, the performance of RIXS experiments can be limited by the spatial resolution of the detector used. Electron-Multiplying CCDs (EM-CCDs) at high gain in combination with centroiding of the photon charge cloud across several detector pixels can lead to sub-pixel spatial resolution of 2-3 μm. X-ray radiation can cause damage to CCDs through ionisation damage resulting in increases in dark current and/or a shift in flat band voltage. Understanding the effect of radiation damage on EM-CCDs is important in order to predict lifetime as well as the change in performance over time. Two CCD-97s were taken to PTB at BESSY II and irradiated with large doses of soft X-rays in order to probe the front and back surfaces of the device. The dark current was shown to decay over time with two different exponential components to it. This paper will discuss the use of EM-CCDs for readout of RIXS spectrometers, and limitations on spatial resolution, together with any limitations on instrument use which may arise from X-ray-induced radiation damage.

A water-cooled x-ray monochromator for using off-axis undulator beam

International Nuclear Information System (INIS)

Khounsary, A.; Maser, J.

2000-01-01

Undulator beamlines at third-generation synchrotrons x-ray sources are designed to use the high-brilliance radiation that is contained in the central cone of the generated x-ray beams. The rest of the x-ray beam is often unused. Moreover, in some cases, such as in the zone-plate-based microfocusing beamlines, only a small part of the central radiation cone around the optical axis is used. In this paper, a side-station branch line at the Advanced Photon Source that takes advantage of some of the unused off-axis photons in a microfocusing x-ray beamline is described. Detailed information on the design and analysis of a high-heat-load water-cooled monochromator developed for this beamline is provided

High spatial resolution grain orientation and strain mapping in thin films using polychromatic submicron x-ray diffraction

Science.gov (United States)

Tamura, N.; MacDowell, A. A.; Celestre, R. S.; Padmore, H. A.; Valek, B.; Bravman, J. C.; Spolenak, R.; Brown, W. L.; Marieb, T.; Fujimoto, H.; Batterman, B. W.; Patel, J. R.

2002-05-01

The availability of high brilliance synchrotron sources, coupled with recent progress in achromatic focusing optics and large area two-dimensional detector technology, has allowed us to develop an x-ray synchrotron technique that is capable of mapping orientation and strain/stress in polycrystalline thin films with submicron spatial resolution. To demonstrate the capabilities of this instrument, we have employed it to study the microstructure of aluminum thin film structures at the granular and subgranular levels. Due to the relatively low absorption of x-rays in materials, this technique can be used to study passivated samples, an important advantage over most electron probes given the very different mechanical behavior of buried and unpassivated materials.

A compact x-ray free electron laser

International Nuclear Information System (INIS)

Barletta, W.; Attac, M.; Cline, D.B.

1988-01-01

We present a design concept and simulation of the performance of a compact x-ray, free electron laser driven by ultra-high gradient rf-linacs. The accelerator design is based on recent advances in high gradient technology by a LLNL/SLAC/LBL collaboration and on the development of bright, high current electron sources by BNL and LANL. The GeV electron beams generated with such accelerators can be concerted to soft x-rays in the range from 2--10 nm by passage through short period, high fields strength wigglers as are being designed at Rocketdyne. Linear light sources of this type can produce trains of picosecond (or shorter) pulses of extremely high spectral brilliance suitable for flash holography of biological specimens in vivo and for studies of fast chemical reactions. 12 refs., 8 figs., 4 tabs

X-ray and neutron scattering studies of complex confined fluids

International Nuclear Information System (INIS)

Sinha, S. K.

1999-01-01

We review recent X-ray and neutron scattering studies of the structure and dynamics of confined complex fluids. This includes the study of polymer conformations and binary fluid phase transitions in porous media using Small Angle Neutron scattering, and the use of synchrotrons radiation to study ordering and fluctuation phenomena at solid/liquid and liquid/air interfaces. Ordering of liquids near a solid surface or in confinement will be discussed, and the study, via specular and off-specular X-ray reflectivity, of capillary wave fluctuations on liquid polymer films. Finally, we shall discuss the use of high-brilliance beams from X-ray synchrotrons to study via photon correlation spectroscopy the slow dynamics of soft condensed matter systems

Soft x-ray photoionization of atoms and molecules

International Nuclear Information System (INIS)

Svensson, Svante

2005-01-01

A review of resonant and non-resonant electron spectroscopy on atoms and molecules at third generation synchrotron radiation facilities is given. The high brilliance of the soft x-ray radiation has made possible new types of experiments giving information on the fundamental behaviour of photoionization. The relevance of Einstein's photoelectric law, and notably the question of when electron energies disperse or do not disperse with the photon energy, is given special attention

High-Resolution X-ray Emission and X-ray Absorption Spectroscopy

NARCIS (Netherlands)

Groot, F.M.F. de

2000-01-01

In this review, high-resolution X-ray emission and X-ray absorption spectroscopy will be discussed. The focus is on the 3d transition-metal systems. To understand high-resolution X-ray emission and reso-nant X-ray emission, it is first necessary to spend some time discussing the X-ray absorption

X-ray diffraction and imaging with a coherent beam: application to X-ray optical elements and to crystals exhibiting phase inhomogeneities

International Nuclear Information System (INIS)

Masiello, F.

2011-05-01

The exceptional properties of synchrotron light sources have been exploited in very different disciplines, from archaeology to chemistry, from material science to biology, from medicine to physics. Among these properties it is important to mention the high brilliance, continuum spectrum, high degree of polarization, time structure, small source size and divergence of the beam, the last resulting in a high transversal coherence of the produced radiation. This high transversal coherence of the synchrotron sources has permitted the development of new techniques, e.g. phase contrast imaging, X-ray photon correlation spectroscopy and coherent X-ray diffraction imaging (CXDI). This thesis work will consist essentially of three parts. In the first part it will be presented the work done as a member of the X-ray Optics Group of ESRF in the characterization of high quality diamond crystals foreseen as X-ray optical elements. The characterization has been done using different complementary X-ray techniques, such as high resolution diffraction, topography, grazing incidence diffraction, reflectivity and measurements of the coherence preservation using the Talbot effect. In the second part, I will show the result obtained in the study of the temperature behaviours of the domain in periodically poled ferroelectrics crystals. This type of measurements, based on Bragg-Fresnel diffraction, are possible only thanks to the high degree of coherence of the beam. In the third part, I will present the results obtained in the characterization of diamonds foreseen for applications other than X-ray optical elements. (author)

Time-dependent nonequilibrium soft x-ray response during a spin crossover

Energy Technology Data Exchange (ETDEWEB)

van Veenendaal, Michel

2018-03-01

The rapid development of high-brilliance pulsed X-ray sources with femtosecond time resolution has created a need for a better theoretical understanding of the time-dependent soft-X-ray response of dissipative many-body quantum systems. It is demonstrated how soft-X-ray spectroscopies, such as X-ray absorption and resonant inelastic X-ray scattering at transition-metal L-edges, can provide insight into intersystem crossings, such as a spin crossover. The photoinduced doublet-to-quartet spin crossover on cobalt in Fe-Co Prussian blue analogues is used as an example to demonstrate how the X-ray response is affected by the dissipative nonequilibrium dynamics. The time-dependent soft-X-ray spectra provide a wealth of information that reflect the changes in the nonequilibrium initial state via continuously changing spectral lineshapes that cannot be decomposed into initial photoexcited and final metastable spectra, strong broadenings, a collapse of clear selection rules during the intersystem crossing, strong fluctuations in the isotropic branching ratio in X-ray absorption, and crystal-field collapse/oscillations and strongly time-dependent anti-Stokes processes in RIXS.

Hard X-ray quantum optics in thin films nanostructures

Energy Technology Data Exchange (ETDEWEB)

Haber, Johann Friedrich Albert

2017-05-15

This thesis describes quantum optical experiments with X-rays with the aim of reaching the strong-coupling regime of light and matter. We make use of the interaction which arises between resonant matter and X-rays in specially designed thin-film nanostructures which form X-ray cavities. Here, the resonant matter are Tantalum atoms and the Iron isotope {sup 57}Fe. Both limit the number of modes available to the resonant atoms for interaction, and enhances the interaction strength. Thus we have managed to observe a number of phenomena well-known in quantum optics, which are the building blocks for sophisticated applications in e.g. metrology. Among these are the strong coupling of light and matter and the concurrent exchange of virtual photons, often called Rabi oscillations. Furthermore we have designed and tested a type of cavity hitherto unused in X-ray optics. Finally, we develop a new method for synchrotron Moessbauer spectroscopy, which not only promises to yield high-resolution spectra, but also enables the retrieval of the phase of the scattered light. The results open new avenues for quantum optical experiments with X-rays, particularly with regards to the ongoing development of high-brilliance X-ray free-electron lasers.

Hard X-ray quantum optics in thin films nanostructures

International Nuclear Information System (INIS)

Haber, Johann Friedrich Albert

2017-05-01

This thesis describes quantum optical experiments with X-rays with the aim of reaching the strong-coupling regime of light and matter. We make use of the interaction which arises between resonant matter and X-rays in specially designed thin-film nanostructures which form X-ray cavities. Here, the resonant matter are Tantalum atoms and the Iron isotope "5"7Fe. Both limit the number of modes available to the resonant atoms for interaction, and enhances the interaction strength. Thus we have managed to observe a number of phenomena well-known in quantum optics, which are the building blocks for sophisticated applications in e.g. metrology. Among these are the strong coupling of light and matter and the concurrent exchange of virtual photons, often called Rabi oscillations. Furthermore we have designed and tested a type of cavity hitherto unused in X-ray optics. Finally, we develop a new method for synchrotron Moessbauer spectroscopy, which not only promises to yield high-resolution spectra, but also enables the retrieval of the phase of the scattered light. The results open new avenues for quantum optical experiments with X-rays, particularly with regards to the ongoing development of high-brilliance X-ray free-electron lasers.

Structural analysis with high brilliance synchrotron radiation

Energy Technology Data Exchange (ETDEWEB)

Ohno, Hideo [Japan Atomic Energy Research Inst., Kamigori, Hyogo (Japan). Kansai Research Establishment

1997-11-01

The research subjects in diffraction and scattering of materials with high brilliance synchrotron radiation such as SPring-8 (Super Photon ring 8 GeV) are summarized. The SPring-8 project is going well and 10 public beamlines will be opened for all users in October, 1997. Three JAERI beamlines are also under construction for researches of heavy element science, physical and structural properties under extreme conditions such as high temperature and high pressure. (author)

Microscale X-ray Absorption Spectroscopy on the GSECARS Sector 13 at the APS

CERN Document Server

Stephen-Sutto

2000-01-01

GeoSoilEnviroCARS (GSECARS) is a national user facility for frontier research in the earth sciences using synchrotrons radiation at the Advanced Photon Source, Argonne National Laboratory. GSECARS provides earth scientists with access to the high-brilliance hard x-rays from this third-generation synchrotrons light source. The research conducted at this facility will advance our knowledge of the composition, structure and properties of earth materials, the processes they control and the processes that produce them. All principal synchrotron-based analytical techniques in demand by earth scientists are being brought to bear on earth science problems: (1) high-pressure/high-temperature crystallography and spectroscopy using the diamond anvil cell; (2) high-pressure/high-temperature crystallography using the large-volume press; (3) powder, single crystal and interface diffraction; (4) x-ray absorption fine structure (XAFS) spectroscopy; (5) x-ray fluorescence microprobe analysis and microspectroscopy; and (6) mic...

An electromagnetic helical undulator for polarized X-rays

International Nuclear Information System (INIS)

Gluskin, E.; Vinokurov, N.; Tcheskidov, V.; Medvedko, A.; Evtushenko, Y.; Kolomogorov, V.; Vobly, P.; Antokhin, E.; Ivanov, P.; Vasserman, I. B.; Trakhtenberg, E. M.; Den Hartog, P. K.; Deriy, B.; Erdmann, M.; Makarov, O.; Moog, E. R.

1999-01-01

Linearly and circularly polarized x-rays have been very successfully applied to the study of the properties of materials. Many applications can benefit from the availability of energy-turnable, high-brilliance x-ray beams with adjustable polarization properties. A helical undulator that can generate beams of variable (linear to circular) polarization has been designed and built by the Budker Institute of Nuclear Physics and the Advanced Photon Source. The first harmonic of this 12.8-cm-period device will cover the energy range from 0.4 keV to 3.5 keV. An important feature of this fully electromagnetic device is that it will allow one to generate 100% horizontally (K x =O)or vertically (K y =O) plane-polarized radiation, which will enable many experiments otherwise not technically feasible. With symmetric deflection parameters (K x =K y ), the on-axis radiation will be circularly polarized, with a user-selectable handedness. The polarization can be changed at rates up to 10 Hz

High-speed X-ray topography

International Nuclear Information System (INIS)

Eckers, W.; Oppolzer, H.

1977-01-01

The investigation of lattice defects in semiconductor crystals by conventional X-ray diffraction topography is very time-consuming. Exposure times can be reduced by using high-intensity X-rays and X-ray image intensifiers. The described system comprises a high-power rotating-anode X-ray tube, a remote-controlled X-ray topography camera, and a television system operating with an X-ray sensing VIDICON. System performance is demonstrated with reference to exploratory examples. The exposure time for photographic plates is reduced to 1/20 and for the X-ray TV system (resolution of the order of 30 μm) to 1/100 relative to that required when using a conventional topography system. (orig.) [de

CARNAÚBA: The Coherent X-Ray Nanoprobe Beamline for the Brazilian Synchrotron SIRIUS/LNLS

Science.gov (United States)

Tolentino, Hélio C. N.; Soares, Márcio M.; Perez, Carlos A.; Vicentin, Flávio C.; Abdala, Dalton B.; Galante, Douglas; Teixeira, Verônica de C.; de Araújo, Douglas H. C.; Westfahl, Harry, Jr.

2017-06-01

The CARNAÚBA beamline is the tender-to-hard X-ray (2 - 15 keV) scanning nanoprobe planned for the 4th generation storage ring SIRIUS at the LNLS. CARNAÚBA uses an undulator source with vertical linear polarization in a low-beta straight section and grazing incidence-focusing mirrors to create a nanoprobe at 143 m from the source. The beamline optic is based on KB mirrors and provides high brilliance at an achromatic focal spot down to the diffraction limit diameter of ˜30 nm with a working distance of ˜6 cm. These characteristics are crucial for studying nanometric samples in experiments involving complex stages and environments. The CARNAÚBA beamline aims to perform raster scans using x-ray fluorescence, x-ray absorption spectroscopy, x-ray diffraction and coherent x-ray imaging techniques. Computed tomography will extend these methods to three dimensions.

HPHT growth and x-ray characterization of high-quality type IIa diamond.

Science.gov (United States)

Burns, R C; Chumakov, A I; Connell, S H; Dube, D; Godfried, H P; Hansen, J O; Härtwig, J; Hoszowska, J; Masiello, F; Mkhonza, L; Rebak, M; Rommevaux, A; Setshedi, R; Van Vaerenbergh, P

2009-09-09

The trend in synchrotron radiation (x-rays) is towards higher brilliance. This may lead to a very high power density, of the order of hundreds of watts per square millimetre at the x-ray optical elements. These elements are, typically, windows, polarizers, filters and monochromators. The preferred material for Bragg diffracting optical elements at present is silicon, which can be grown to a very high crystal perfection and workable size as well as rather easily processed to the required surface quality. This allows x-ray optical elements to be built with a sufficient degree of lattice perfection and crystal processing that they may preserve transversal coherence in the x-ray beam. This is important for the new techniques which include phase-sensitive imaging experiments like holo-tomography, x-ray photon correlation spectroscopy, coherent diffraction imaging and nanofocusing. Diamond has a lower absorption coefficient than silicon, a better thermal conductivity and lower thermal expansion coefficient which would make it the preferred material if the crystal perfection (bulk and surface) could be improved. Synthetic HPHT-grown (high pressure, high temperature) type Ib material can readily be produced in the necessary sizes of 4-8 mm square and with a nitrogen content of typically a few hundred parts per million. This material has applications in the less demanding roles such as phase plates: however, in a coherence-preserving beamline, where all elements must be of the same high quality, its quality is far from sufficient. Advances in HPHT synthesis methods have allowed the growth of type IIa diamond crystals of the same size as type Ib, but with substantially lower nitrogen content. Characterization of this high purity type IIa material has been carried out with the result that the crystalline (bulk) perfection of some of the HPHT-grown materials is approaching the quality required for the more demanding applications such as imaging applications and imaging

Harmonic lasing in X-ray FELs

Energy Technology Data Exchange (ETDEWEB)

Schneidmiller, E.A.; Yurkov, M.V.

2012-05-15

Harmonic lasing in a free electron laser with a planar undulator (under the condition that the fundamental frequency is suppressed) might be a cheap and efficient way of extension of wavelength ranges of existing and planned X-ray FEL facilities. Contrary to nonlinear harmonic generation, harmonic lasing can provide much more intense, stable, and narrow-band FEL beam which is easier to handle due to the suppressed fundamental frequency. In this paper we perform a parametrization of the solution of the eigenvalue equation for lasing at odd harmonics, and present an explicit expression for FEL gain length, taking into account all essential effects. We propose and discuss methods for suppression of the fundamental harmonic. We also suggest a combined use of harmonic lasing and lasing at the retuned fundamental wavelength in order to reduce bandwidth and to increase brilliance of X-ray beam at saturation. Considering 3rd harmonic lasing as a practical example, we come to the conclusion that it is much more robust than usually thought, and can be widely used in the existing or planned X-ray FEL facilities. In particular, LCLS after a minor modification can lase to saturation at the 3rd harmonic up to the photon energy of 25-30 keV providing multi-gigawatt power level and narrow bandwidth. As for the European XFEL, harmonic lasing would allow to extend operating range (ultimately up to 100 keV), to reduce FEL bandwidth and to increase brilliance, to enable two-color operation for pump-probe experiments, and to provide more flexible operation at different electron energies. Similar improvements can be realized in other X-ray FEL facilities with gap-tunable undulators like FLASH II, SACLA, LCLS II, etc. Harmonic lasing can be an attractive option for compact X-ray FELs (driven by electron beams with a relatively low energy), allowing the use of the standard undulator technology instead of small-gap in-vacuum devices. Finally, in this paper we discover that in a part of the

Pixel array detector for X-ray free electron laser experiments

Energy Technology Data Exchange (ETDEWEB)

Philipp, Hugh T., E-mail: htp2@cornell.edu [Department of Physics, Laboratory of Solid State Physics, Cornell University, Ithaca, NY 14853 (United States); Hromalik, Marianne [Electrical and Computer Engineering, SUNY Oswego, Oswego, NY 13126 (United States); Tate, Mark; Koerner, Lucas [Department of Physics, Laboratory of Solid State Physics, Cornell University, Ithaca, NY 14853 (United States); Gruner, Sol M. [Department of Physics, Laboratory of Solid State Physics, Cornell University, Ithaca, NY 14853 (United States); Wilson Laboratory, Cornell University, CHESS, Ithaca, NY 14853 (United States)

2011-09-01

X-ray free electron lasers (XFELs) promise to revolutionize X-ray science with extremely high peak brilliances and femtosecond X-ray pulses. This will require novel detectors to fully realize the potential of these new sources. There are many current detector development projects aimed at the many challenges of meeting the XFEL requirements . This paper describes a pixel array detector (PAD) that has been developed for the Coherent X-ray Imaging experiment at the Linac Coherent Light Source (LCLS) at the SLAC National Laboratory . The detector features 14-bit in-pixel digitization; a 2-level in-pixel gain setting that can be used to make an arbitrary 2-D gain pattern that is adaptable to a particular experiment; the ability to handle instantaneous X-ray flux rates of 10{sup 17} photons per second; and continuous frames rates in excess of 120 Hz. The detector uses direct detection of X-rays in a silicon diode. The charge produced by the diode is integrated in a pixilated application specific integrated circuit (ASIC) which digitizes collected holes with single X-ray photon capability. Each ASIC is 194x185 pixels, each pixel is 110{mu}mx110{mu}m on a side. Each pixel can detect up to 2500 X-rays per frame in low-gain mode, yet easily detects single photons at high-gain. Cooled, single-chip detectors have been built and meet all the required specifications. SLAC National Laboratory is engaged in constructing a tiled, multi-chip 1516x1516 pixel detector.

Performance of a high-resolution x-ray microprobe at the Advanced Photon Source

International Nuclear Information System (INIS)

Cai, Z.; Lai, B.; Yun, W.; McNulty, I.; Khounsary, A.; Maser, J.; Ilinski, P.; Legnini, D.; Trakhtenberg, E.; Xu, S.; Tieman, B.; Wiemerslage, G.; Gluskin, E.

1999-01-01

The authors have developed a x-ray microprobe in the energy region from 6 to 20 keV using undulator radiation and zone-plate optics for microfocusing-based techniques and applications at a beamline at the Advanced Photon Source (APS). The performance of the beamline was shown to meet the design objectives, including preservation of the source brilliance and coherence, selectable transverse coherence length and energy bandwidth, high angular stability, and harmonic suppression of the beam. These objectives were achieved by careful thermal management and use of a novel mirror and crystal monochromator cooling geometry. All beamline optical components are water cooled, and the x-ray beam in the experiment station is stable in beam intensity, energy, and position over many days with no active feedback. Using a double-crystal Si(111) monochromator, they have obtained a focal spot size (FWHM) of 0.15 (micro)m (v) x 1.0 (micro)m (h), and a photon flux of 4 x 10 9 photons/sec at the focal spot, and thus a photon flux density gain of 15,000. A circular beam spot of 0.15 (micro)m in diameter can be achieved by reducing the horizontal source size using a white beam slit located 43.5 meters upstream of the zone plate, with an order of magnitude less flux in the focal spot

Small-angle X-ray scattering at high brilliance european synchrotrons for biotechnology and nano-technology

International Nuclear Information System (INIS)

Svergun, D.; Malfois, M.; Svergun, D.; Douka, M.; Riekel, Ch.; Perez, J.; Roessle, M.; Amenitsch, H.; Gunter Grossman, J.; Vestergaard, B.; Receveur-Brechot, V.; Roth, St.V.; Ferrari, E.

2007-01-01

Different issues such as micro-fluidic devices for SAXS (small-angle X-ray diffraction), the use of electro-spray and ion trapping for SAXS in the gas phase, the study of flexible and disordered proteins through SAXS, the time-resolved SAXS studies in solution, or the study of nano-structured soft materials, were addressed in this workshop. This document gathers the transparencies of the presentations

Small-angle X-ray scattering at high brilliance european synchrotrons for biotechnology and nano-technology

Energy Technology Data Exchange (ETDEWEB)

Svergun, D.; Malfois, M. [EMBL c/o DESY, Hamburg (Germany); Svergun, D. [Institute of Crystallography, Russian Academy of Sciences, Moscow (Russian Federation); Douka, M. [Commission Europeenne, DG III, Bruxelles (Belgium); Riekel, Ch. [European Synchrotron Radiation Facility (ESRF), 38 - Grenoble (France); Perez, J. [Soleil, 91 - Saclay (France); Roessle, M. [European Molecular Biology Laboratory (EMBL), 38 - Grenoble (France); Amenitsch, H. [IBN/Elettra (Germany); Gunter Grossman, J. [Daresbury Synchrotron Radiation Source (SRS) (United Kingdom); Vestergaard, B. [University of Pharmaceutical Sciences, Copenhagen (Denmark); Receveur-Brechot, V. [Centre National de la Recherche Scientifique (CNRS/AFMB), 13 - Marseille (France); Roth, St.V. [Deutsches Elektronen Synchrotron (HASYLAB), Hamburg (Germany); Ferrari, E. [National Institute for the Physics of Matter (CNR-INFM), Trieste (Italy)

2007-07-01

Different issues such as micro-fluidic devices for SAXS (small-angle X-ray diffraction), the use of electro-spray and ion trapping for SAXS in the gas phase, the study of flexible and disordered proteins through SAXS, the time-resolved SAXS studies in solution, or the study of nano-structured soft materials, were addressed in this workshop. This document gathers the transparencies of the presentations.

X-ray grazing incidence studies of the 2D crystallization of monolayers of 1-alcohols at the air water interface

DEFF Research Database (Denmark)

Legrand, J.F.; Renault, A.; Konovalov, O.

1994-01-01

A new undulator producing an X-ray beam of high brilliance has been used at the European Synchrotron Radiation Facility (ESRF, Beamline-9, Troika) for investigating the structure of two-dimensional crystals of 1-tetradecanol, 1-dodecanol, 1-decanol and 1-nonanol. These fatty alcohols with relativ...

Submicron x-ray diffraction and its applications to problems in materials and environmental science

Science.gov (United States)

Tamura, N.; Celestre, R. S.; MacDowell, A. A.; Padmore, H. A.; Spolenak, R.; Valek, B. C.; Meier Chang, N.; Manceau, A.; Patel, J. R.

2002-03-01

The availability of high brilliance third generation synchrotron sources together with progress in achromatic focusing optics allows us to add submicron spatial resolution to the conventional century-old x-ray diffraction technique. The new capabilities include the possibility to map in situ, grain orientations, crystalline phase distribution, and full strain/stress tensors at a very local level, by combining white and monochromatic x-ray microbeam diffraction. This is particularly relevant for high technology industry where the understanding of material properties at a microstructural level becomes increasingly important. After describing the latest advances in the submicron x-ray diffraction techniques at the Advanced Light Source, we will give some examples of its application in material science for the measurement of strain/stress in metallic thin films and interconnects. Its use in the field of environmental science will also be discussed.

Submicron X-Ray Diffraction and its Applications to Problems in Materials and Environmental Science

Energy Technology Data Exchange (ETDEWEB)

Patel, J. R.

2002-08-16

The availability of high brilliance 3rd generation synchrotron sources together with progress in achromatic focusing optics allow to add submicron spatial resolution to the conventional century-old X-ray diffraction technique. The new capabilities include the possibility to map in-situ, grain orientations, crystalline phase distribution and full strain/stress tensors at a very local level, by combining white and monochromatic X-ray microbeam diffraction. This is particularly relevant for high technology industry where the understanding of material properties at a microstructural level becomes increasingly important. After describing the latest advances in the submicron X-ray diffraction techniques at the ALS, we will give some examples of its application in material science for the measurement of strain/stress in metallic thin films and interconnects. Its use in the field of environmental science will also be discussed.

Submicron X-ray diffraction and its applications to problems in materials and environmental science

Energy Technology Data Exchange (ETDEWEB)

Tamura, N.; Celestre, R.S.; MacDowell, A.A.; Padmore, H.A.; Spolenak, R.; Valek, B.C.; Meier Chang, N.; Manceau, A.; Patel, J.R.

2002-03-26

The availability of high brilliance 3rd generation synchrotron sources together with progress in achromatic focusing optics allow to add submicron spatial resolution to the conventional century-old X-ray diffraction technique. The new capabilities include the possibility to map in-situ, grain orientations, crystalline phase distribution and full strain/stress tensors at a very local level, by combining white and monochromatic X-ray microbeam diffraction. This is particularly relevant for high technology industry where the understanding of material properties at a microstructural level becomes increasingly important. After describing the latest advances in the submicron X-ray diffraction techniques at the ALS, we will give some examples of its application in material science for the measurement of strain/stress in metallic thin films and interconnects. Its use in the field of environmental science will also be discussed.

Ultrafast X-ray Imaging of Fuel Sprays

Science.gov (United States)

Wang, Jin

2007-01-01

Detailed analysis of fuel sprays has been well recognized as an important step for optimizing the operation of internal combustion engines to improve efficiency and reduce emissions. Ultrafast radiographic and tomographic techniques have been developed for probing the fuel distribution close to the nozzles of direct-injection diesel and gasoline injectors. The measurement was made using x-ray absorption of monochromatic synchrotron-generated radiation, allowing quantitative determination of the fuel distribution in this optically impenetrable region with a time resolution on the order of 1 μs. Furthermore, an accurate 3-dimensional fuel-density distribution, in the form of fuel volume fraction, was obtained by the time-resolved computed tomography. These quantitative measurements constitute the most detailed near-nozzle study of a fuel spray to date. With high-energy and high-brilliance x-ray beams available at the Advanced Photon Source, propagation-based phase-enhanced imaging was developed as a unique metrology technique to visualize the interior of an injection nozzle through a 3-mm-thick steel with a 10-μs temporal resolution, which is virtually impossible by any other means.

Ultrafast X-ray Imaging of Fuel Sprays

International Nuclear Information System (INIS)

Wang Jin

2007-01-01

Detailed analysis of fuel sprays has been well recognized as an important step for optimizing the operation of internal combustion engines to improve efficiency and reduce emissions. Ultrafast radiographic and tomographic techniques have been developed for probing the fuel distribution close to the nozzles of direct-injection diesel and gasoline injectors. The measurement was made using x-ray absorption of monochromatic synchrotron-generated radiation, allowing quantitative determination of the fuel distribution in this optically impenetrable region with a time resolution on the order of 1 μs. Furthermore, an accurate 3-dimensional fuel-density distribution, in the form of fuel volume fraction, was obtained by the time-resolved computed tomography. These quantitative measurements constitute the most detailed near-nozzle study of a fuel spray to date. With high-energy and high-brilliance x-ray beams available at the Advanced Photon Source, propagation-based phase-enhanced imaging was developed as a unique metrology technique to visualize the interior of an injection nozzle through a 3-mm-thick steel with a 10-μs temporal resolution, which is virtually impossible by any other means

X-ray spectral meter of high voltages for X-ray apparatuses

International Nuclear Information System (INIS)

Zubkov, I.P.; Larchikov, Yu.V.

1993-01-01

Design of the X-ray spectral meter of high voltages (XRSMHV) for medical X-ray apparatuses permitting to conduct the voltage measurements without connection to current circuits. The XRSMHV consists of two main units: the detector unit based on semiconductor detector and the LP4900B multichannel analyzer (Afora, Finland). The XRSMYV was tested using the pilot plant based on RUM-20 X-ray diagnostic apparatus with high-voltage regulator. It was shown that the developed XRSMHV could be certify in the range of high constant voltages form 40 up to 120 kV with the basic relative error limits ±0.15%. The XRSMHV is used at present as the reference means for calibration of high-voltage medical X-ray equipment

The APS x-ray undulator photon beam position monitor and tests at CHESS and NSLS

International Nuclear Information System (INIS)

Shu, D.; Rodricks, B.; Barraza, J.; Sanchez, T.; Kuzay, T.M.

1992-01-01

The advent of third generation synchrotron radiation sources, like the Advanced Photon Source (APS), will provide significant increases in brilliance over existing synchrotron sources. The APS x-ray undulators will increase the brilliance in the 3-40 KeV range by several orders of magnitude. Thus, the design of the photon beam position monitor is a challenging engineering task. The beam position monitors must withstand the high thermal load, be able to achieve sub-micron spatial resolution while maintaining their stability, and be compatible with both undulators and wigglers. A preliminary APS prototype photon beam position monitor consisting of a CVD-diamond-based, tungsten-coated blade was tested on the APS/CHESS undulator at the Cornell High Energy Synchrotron Radiation Source (CHESS) and on the NSLS X-13 undulator beamline. Results from these tests, as well as the design of this prototype APS photon beam position monitor, will be discussed in this paper

The APS X-ray undulator photon beam position monitor and tests at CHESS and NSLS

International Nuclear Information System (INIS)

Shu, D.; Rodricks, B.; Barraza, J.; Sanchez, T.; Kuzay, T.M.

1992-01-01

The advent of thirs generation synchrotron sources, like the Advanced Photon Source (APS), will provide significant increases in brilliance over existing synchrotron sources. The APS X-ray undulators will increase the brilliance in the 3-40 keV range by several orders of magnitude. Thus, the design of the photon beam position monitor is a challenging engineering task. The beam position monitors must withstand the high thermal load, be able to achieve submicron spatial resolution while maintaining their stability, and be compatible with both undulators and wigglers. A preliminary APS prototype photon beam position monitor consisting of a CVD-diamond-based, tungsten-coated blade was tested on the APS/CHESS undulator at the Cornell High Energy Synchrotron Radiation Source (CHESS) and on the NSLS X-13 undulator beamline. Results from these tests, as well as the design of this prototype APS photon beam position monitor, will be discussed in this paper. (orig.)

Toward a fourth-generation X-ray source

International Nuclear Information System (INIS)

Monction, D. E.

1999-01-01

The field of synchrotron radiation research has grown rapidly over the last 25 years due to both the push of the accelerator and magnet technology that produces the x-ray beams and the pull of the extraordinary scientific research that is possible with them. Three successive generations of synchrotrons radiation facilities have resulted in beam brilliances 11 to 12 orders of magnitude greater than the standard laboratory x-ray tube. However, greater advances can be easily imagined given the fact that x-ray beams from present-day facilities do not exhibit the coherence or time structure so familiar with the optical laser. Theoretical work over the last ten years or so has pointed to the possibility of generating hard x-ray beams with laser-like characteristics. The concept is based on self-amplified spontaneous emission (SASE) in flee-electron lasers. A major facility of this type based upon a superconducting linac could produce a cost-effective facility that spans wave-lengths from the ultraviolet to the hard x-ray regime, simultaneously servicing large numbers experimenters from a wide range of disciplines. As with each past generation of synchrotrons facilities, immense new scientific opportunities would result from fourth-generation sources.

On the image formation in x-ray radiography using aligned carbon nanofibers

International Nuclear Information System (INIS)

Okuyama, F.

2017-01-01

Evidence is presented that field electrons emitted from vertically-aligned carbon nanofibers (CNFs) yield clearer x-ray images than do thermionic electrons, under the identical electron-optical condition. Specifically, the same sample, an LSI circuit, mounted on the same x-ray chamber could be imaged far more sharply with a CNF emitter than with a thermionic one. It is hypothesized that electrons discharged from CNF tips hit the target to form “discrete focal points” thereon, thereby generating multiple x-ray beams that interplay to form a brilliant, sharply-delineated x-ray image. This hypothesis may stimulate open discussion on how to define the “focal point” for the x-ray imaging using nano-structured electron sources. Also, the improved resolution attained with CNFs might indicate that the heat generation originating in electron-target interactions is not so serious in the present field-emission mode. - Highlights: • Field-emission (FE) x-ray radiography (XR) is based on nanotechnology. • FE-XR surpasses thermionic XR in image resolution and brilliance. • Highly-resolved FE-XR images are due possibly to a discrete array of x-ray spots. • This hypothesis stimulates open discussion on how to define the focal-point in FE-XR.

On the image formation in x-ray radiography using aligned carbon nanofibers

Energy Technology Data Exchange (ETDEWEB)

Okuyama, F., E-mail: okuya@mui.biglobe.ne.jp

2017-04-11

Evidence is presented that field electrons emitted from vertically-aligned carbon nanofibers (CNFs) yield clearer x-ray images than do thermionic electrons, under the identical electron-optical condition. Specifically, the same sample, an LSI circuit, mounted on the same x-ray chamber could be imaged far more sharply with a CNF emitter than with a thermionic one. It is hypothesized that electrons discharged from CNF tips hit the target to form “discrete focal points” thereon, thereby generating multiple x-ray beams that interplay to form a brilliant, sharply-delineated x-ray image. This hypothesis may stimulate open discussion on how to define the “focal point” for the x-ray imaging using nano-structured electron sources. Also, the improved resolution attained with CNFs might indicate that the heat generation originating in electron-target interactions is not so serious in the present field-emission mode. - Highlights: • Field-emission (FE) x-ray radiography (XR) is based on nanotechnology. • FE-XR surpasses thermionic XR in image resolution and brilliance. • Highly-resolved FE-XR images are due possibly to a discrete array of x-ray spots. • This hypothesis stimulates open discussion on how to define the focal-point in FE-XR.

X-ray generation in an ion channel

International Nuclear Information System (INIS)

Kostyukov, I.; Kiselev, S.; Pukhov, A.

2003-01-01

X-ray generation by relativistic electrons in an ion channel is studied. The emission process is analyzed in the regime of high harmonic generation when the plasma wiggler strength is large. Like for the conventional free electron laser, the synchrotron-like broadband spectrum is generated in this regime. An asymptotic expression for the radiation spectrum of the spontaneous emission is derived. The radiation spectrum emitted from an axisymmetric monoenergetic electron beam is analyzed. The stimulated emission in the ion channel is studied and the gain of the ion-channel synchrotron-radiation laser is calculated. It is shown that the use of laser-produced ion channels leads to a much higher power of x-ray radiation than the one in a self-generated channel. In addition, the mean photon energy, the number of emitted photons and the brilliance of the photon beam increase dramatically. Three-dimensional particle-in-cell simulations of a 25-GeV electron bunch propagating in a laser-produced ion channel are made. Several GeV γ-quants are produced in a good agreement with the analytical results

Harmonic lasing in x-ray free electron lasers

Directory of Open Access Journals (Sweden)

E. A. Schneidmiller

2012-08-01

Full Text Available Harmonic lasing in a free electron laser with a planar undulator (under the condition that the fundamental frequency is suppressed might be a cheap and efficient way of extension of wavelength ranges of existing and planned x-ray free electron laser (FEL facilities. Contrary to nonlinear harmonic generation, harmonic lasing can provide much more intense, stable, and narrow-band FEL beam which is easier to handle due to the suppressed fundamental frequency. In this paper we perform a parametrization of the solution of the eigenvalue equation for lasing at odd harmonics, and present an explicit expression for FEL gain length, taking into account all essential effects. We propose and discuss methods for suppression of the fundamental harmonic. We also suggest a combined use of harmonic lasing and lasing at the retuned fundamental wavelength in order to reduce bandwidth and to increase brilliance of x-ray beam at saturation. Considering 3rd harmonic lasing as a practical example, we come to the conclusion that it is much more robust than usually thought, and can be widely used in the existing or planned x-ray FEL (XFEL facilities. In particular, Linac Coherent Light Source (LCLS after a minor modification can lase to saturation at the 3rd harmonic up to the photon energy of 25–30 keV providing multigigawatt power level and narrow bandwidth. As for the European XFEL, harmonic lasing would allow one to extend operating range (ultimately up to 100 keV, to reduce FEL bandwidth and to increase brilliance, to enable two-color operation for pump-probe experiments, and to provide more flexible operation at different electron energies. Similar improvements can be realized in other x-ray FEL facilities with gap-tunable undulators like FLASH II, SACLA, LCLS II, etc. Harmonic lasing can be an attractive option for compact x-ray FELs (driven by electron beams with a relatively low energy, allowing the use of the standard undulator technology instead of

Development of Compton X-ray spectrometer for high energy resolution single-shot high-flux hard X-ray spectroscopy

Energy Technology Data Exchange (ETDEWEB)

Kojima, Sadaoki, E-mail: kojima-s@ile.osaka-u.ac.jp, E-mail: sfujioka@ile.osaka-u.ac.jp; Ikenouchi, Takahito; Arikawa, Yasunobu; Sakata, Shohei; Zhang, Zhe; Abe, Yuki; Nakai, Mitsuo; Nishimura, Hiroaki; Shiraga, Hiroyuki; Fujioka, Shinsuke, E-mail: kojima-s@ile.osaka-u.ac.jp, E-mail: sfujioka@ile.osaka-u.ac.jp; Azechi, Hiroshi [Institute of Laser Engineering, Osaka University, 2-6 Yamada-oka, Suita, Osaka 565-0871 (Japan); Ozaki, Tetsuo [National Institute for Fusion Science, 322-6 Oroshi, Toki, Gifu 509-5292 (Japan); Miyamoto, Shuji; Yamaguchi, Masashi; Takemoto, Akinori [Laboratory of Advanced Science and Technology for Industry, University of Hyogo, 3-1-2 Kouto, Kamigori-cho, Ako-gun, Hyogo 678-1205 (Japan)

2016-04-15

Hard X-ray spectroscopy is an essential diagnostics used to understand physical processes that take place in high energy density plasmas produced by intense laser-plasma interactions. A bundle of hard X-ray detectors, of which the responses have different energy thresholds, is used as a conventional single-shot spectrometer for high-flux (>10{sup 13} photons/shot) hard X-rays. However, high energy resolution (Δhv/hv < 0.1) is not achievable with a differential energy threshold (DET) X-ray spectrometer because its energy resolution is limited by energy differences between the response thresholds. Experimental demonstration of a Compton X-ray spectrometer has already been performed for obtaining higher energy resolution than that of DET spectrometers. In this paper, we describe design details of the Compton X-ray spectrometer, especially dependence of energy resolution and absolute response on photon-electron converter design and its background reduction scheme, and also its application to the laser-plasma interaction experiment. The developed spectrometer was used for spectroscopy of bremsstrahlung X-rays generated by intense laser-plasma interactions using a 200 μm thickness SiO{sub 2} converter. The X-ray spectrum obtained with the Compton X-ray spectrometer is consistent with that obtained with a DET X-ray spectrometer, furthermore higher certainly of a spectral intensity is obtained with the Compton X-ray spectrometer than that with the DET X-ray spectrometer in the photon energy range above 5 MeV.

Radiation processing with high-energy X-rays

International Nuclear Information System (INIS)

Cleland, Marshall R.; Stichelbaut, Frederic

2009-01-01

The physical, chemical or biological characteristics of selected commercial products and materials can be improved by radiation processing. The ionizing energy can be provided by accelerated electrons with energies between 75 keV and 10 MeV, gamma rays from cobalt-60 with average energies of 1.25 MeV or X-rays with maximum energies up to 7.5 MeV. Electron beams are preferred for thin products, which are processed at high speeds. Gamma rays are used for products that are too thick for treatment with electron beams. High-energy X-rays can also be used for these purposes because their penetration in solid materials is similar to or even slightly greater than that of gamma rays. Previously, the use of X-rays had been inhibited by their slower processing rates and higher costs when compared with gamma rays. Since then, the price of cobalt-60 sources has been increased and the radiation intensity from high-energy, high-power X-ray generators has also increased. For facilities requiring at least 2 MCi of cobalt-60, the capital and operating costs of X-ray facilities with equivalent processing rates can be less than that of gamma-ray irradiators. Several high-energy electron beam facilities have been equipped with removable X-ray targets so that irradiation processes can be done with either type of ionizing energy. A new facility is now being built which will be used exclusively in the X-ray mode to sterilize medical products. Operation of this facility will show that high-energy, high-power X-ray generators are practical alternatives to large gamma-ray sources. (author)

Prospects of high-resolution resonant X-ray inelastic scattering studies on solid materials, liquids and gases at diffraction-limited storage rings

International Nuclear Information System (INIS)

Schmitt, Thorsten; Groot, Frank M. F. de; Rubensson, Jan-Erik

2014-01-01

Diffraction-limited storage rings will allow for pushing the achievable energy resolution, signal intensity and the sampled spot size in resonant inelastic X-ray scattering (RIXS) experiments to new limits. In this article the types of improved soft X-ray RIXS studies that will become possible with these instrumental improvements are envisioned. The spectroscopic technique of resonant inelastic X-ray scattering (RIXS) will particularly profit from immensely improved brilliance of diffraction-limited storage rings (DLSRs). In RIXS one measures the intensities of excitations as a function of energy and momentum transfer. DLSRs will allow for pushing the achievable energy resolution, signal intensity and the sampled spot size to new limits. With RIXS one nowadays probes a broad range of electronic systems reaching from simple molecules to complex materials displaying phenomena like peculiar magnetism, two-dimensional electron gases, superconductivity, photovoltaic energy conversion and heterogeneous catalysis. In this article the types of improved RIXS studies that will become possible with X-ray beams from DLSRs are envisioned

Direct observation of organic layer growth by dynamic spectro-microscopy using high-brilliance synchrotron

International Nuclear Information System (INIS)

Umbach, E.

2004-01-01

It was always the dream of scientists to watch microscopic objects directly on an atomic scale, to follow their dynamical behaviour, and to know everything about them, i.e. to get as much spectroscopic information as possible. While instruments have become available which may fulfill two of these wishes simultaneously, it is much more difficult to get all three at once. The development of so called spectro-microscopes which operate at 3rd generation synchrotron sources nourishes the hope that this dream will become true in the near future. The talk intends to show how much can be learned about organic thin films and interfaces if high-brilliance synchrotron radiation is combined with new instruments, for instance a high energy resolution beamline and a high-spatial resolution spectro-microscope. While the former is standard technology of today, the latter is a new development, combining brilliant undulator radiation of variable polarization with a specially developed, energy-filtered low energy electron microscope. First, it will be shown that many new details about the electronic structure of organic materials and their interaction with one another or with an interface can be obtained using high-resolution photoemission and x-ray absorption. For instance, from a careful analysis of the fine structure of photoemission spectra one can derive details about the interface bonding, about the interaction between molecules, and about the dynamic response of the molecular system upon creation of a core hole. Or, from a careful analysis of the fine structure of high resolution x-ray absorption spectra one gets insight into the intermolecular interaction, the coupling between electronic and vibronic excitations, and even about the shapes of potential curves. Second, the dynamic growth of highly-ordered organic thin films will be followed as a function of molecule and preparation conditions. The formation of islands, the inner structure of organic crystallites, diffusion

Soft X-ray reflectivity: from quasi-perfect mirrors to accelerator walls

CERN Document Server

Schäfers, F.

2013-04-22

Reflection of light from surfaces is a very common, but complex phenomenon not only in science and technology, but in every day life. The underlying basic optical principles have been developed within the last five centuries using visible light available from the sun or other laboratory light sources. X-rays were detected in 1895, and the full potential of soft- and hard-x ray radiation as a probe for the electronic and geometric properties of matter, for material analysis and its characterisation is available only since the advent of synchrotron radiation sources some 50 years ago. On the other hand high-brilliance and high power synchrotron radiation of present-days 3rd and 4th generation light sources is not always beneficial. Highenergy machines and accelerator-based light sources can suffer from a serious performance drop or limitations due to interaction of the synchrotron radiation with the accelerator walls, thus producing clouds of photoelectrons (e-cloud) which in turn interact with the accelerated ...

The X-ray transition radiation; Le rayonnement de transition X

Energy Technology Data Exchange (ETDEWEB)

Couillaud, Ch

2000-07-01

The interest of producing high-energy radiation using a small-size electron accelerator is growing since many years. It appeared that such accelerators should drive x-ray sources to produce a high flux of radiation. The range of photon-energy available when using electron linacs, for example, is between a few tens of eV and the maximum electron kinetic energy. The transition radiation, which is produced when a charged particle crosses the interface between two media of different permittivities, is a very promising way due to its high production rate. We present here a study of this physical process involving moderate-energy relativistic electrons (20 MeV). We recall the main characteristics of the radiation when the interface is crossed at normal incidence and derive the analytical production yields when the interaction takes place at grazing incidence. The results for both geometries are compared. Finally, the scale laws allowing the optimization of the spectral source brilliance are presented. (author)

A free-electron laser fourth-generation X-ray source

International Nuclear Information System (INIS)

Moncton, D. E.

1999-01-01

The field of synchrotrons radiation research has grown rapidly over the last 25 years due to both the push of the accelerator and magnet technology that produces the x-ray beams and the pull of the extraordinary scientific research those beams make possible. Three successive generations of synchrotrons radiation facilities have resulted in beam brilliances 11 to 12 orders of magnitude greater than the standard laboratory x-ray tube. However, greater advances can be easily imagined given the fact that x-ray beams from present-day facilities do not exhibit the coherence or time structure so familiar with the.optical laser. Theoretical work over the last ten years or so has pointed to the possibility of generating hard x-ray beams with laser-like characteristics. The concept is based on self-amplified spontaneous emission in free electron lasers. The use of a superconducting linac could produce a major, cost-effective facility that spans wavelengths from the ultraviolet to the hard x-ray regime, simultaneously servicing large numbers experimenters from a wide range of disciplines. As with each past generation of synchrotron facilities, immense new scientific opportunities from fourth-generation sources

X-ray diffraction at high pressure and high/low temperatures using synchrotron radiation. Applications in the study of spinel structures

International Nuclear Information System (INIS)

Gerward, L.; Jiang, J.Z.; Olsen, J.S.; Recio, J.M.; Wakowska, A.

2004-01-01

High-pressure x-ray diffraction made a quantum leap in the 1960's with the advent of the diamond-anvil cell. This ingenious device, where two opposing diamond faces apply pressure to a tiny sample, made it possible to replicate the pressure near the core of the Earth by turning a thumbscrew. Multianvil cells, such as the Japanese MAX80 press, were developed for combined high-pressure and high-temperature studies. The availability n at about the same time n of dedicated synchrotron radiation sources of hard x-rays was another big step forward. Since then, the white-beam energy-dispersive method has been the workhorse for high pressure, high-temperature x-ray diffraction, although it is now gradually being replaced by high-resolution monochromatic methods based on the image plate, the CCD camera or other electronic area detectors. The first part of the paper is a review of high-pressure x-ray diffraction (HPXRD), covering roughly the last three decades. Physical parameters, such as the bulk modulus, the compressibility and the equation of state, are defined. The diamond-anvil cell, the multianvil press and other high-pressure devices are described, as well as synchrotron radiation sources and recording techniques. Examples are drawn from current experimental and theoretical research on crystal structures of the spinel type. Accurate structural parameters have been determined at ambient conditions and at low temperatures using single-crystal diffraction and four-circle diffractometers. The uniform high-pressure behavior of the oxide spinels has been investigated in detail and compared with the corresponding behavior of selenium-based spinels. The synthesis of advanced novel materials is exemplified in the case of the cubic spinel Si 3 N 4 . This and other nitrogen spinels, which have a bulk modulus of about 300 GPa modulated by the actual cation, are opening a road towards superhard materials. The paper finishes off with an outlook into the future, where new

High brilliance multicusp ion source for hydrogen microscopy at SNAKE

Energy Technology Data Exchange (ETDEWEB)

Moser, M., E-mail: marcus.moser@unibw.de [Universitaet der Bundeswehr Muenchen, Institut fuer Angewandte Physik und Messtechnik, LRT2, Department fuer Luft- und Raumfahrttechnik, 85577 Neubiberg (Germany); Reichart, P. [Universitaet der Bundeswehr Muenchen, Institut fuer Angewandte Physik und Messtechnik, LRT2, Department fuer Luft- und Raumfahrttechnik, 85577 Neubiberg (Germany); Carli, W. [Maier-Leibniz-Laboraturium der LMU und TU Muenchen, 85478 Garching (Germany); Greubel, C.; Peeper, K. [Universitaet der Bundeswehr Muenchen, Institut fuer Angewandte Physik und Messtechnik, LRT2, Department fuer Luft- und Raumfahrttechnik, 85577 Neubiberg (Germany); Hartung, P. [Maier-Leibniz-Laboraturium der LMU und TU Muenchen, 85478 Garching (Germany); Dollinger, G. [Universitaet der Bundeswehr Muenchen, Institut fuer Angewandte Physik und Messtechnik, LRT2, Department fuer Luft- und Raumfahrttechnik, 85577 Neubiberg (Germany)

2012-02-15

In order to improve the lateral resolution of the 3D hydrogen microscopy by proton-proton scattering at the Munich microprobe SNAKE, we have installed a new multicusp ion source for negative hydrogen ions manufactured by HVEE at the Munich 14 MV tandem accelerator that boosts the proton beam brilliance with the potential to reduce the beam diameter at the focal plane of SNAKE. We measured a beam brilliance B = 27 A m{sup -2} rad{sup -2} eV{sup -1} directly behind the ion source that is at the space charge limit for conventional ion sources. After preacceleration to in total 180 keV beam energy we measure a slightly reduced beam brilliance of B = 10 {mu}A mm{sup -2} mrad{sup -2} MeV{sup -1}. For injection into the tandem accelerator, the extracted H{sup -}-current of the multicusp source of 1 mA is reduced to about 10 {mu}A because of radiation safety regulations and heating problems at the object slits of SNAKE. Due to beam oscillations and influences of the terminal stripper of the tandem we measured a reduced beam brilliance of 0.8 {mu}A mm{sup -2} mrad{sup -2} MeV{sup -1} in front of SNAKE at 25 MeV but still being nearly 10 times larger than measured with any other ion source.

Beam brilliance investigation of high current ion beams at GSI heavy ion accelerator facility.

Science.gov (United States)

Adonin, A A; Hollinger, R

2014-02-01

In this work the emittance measurements of high current Ta-beam provided by VARIS (Vacuum Arc Ion Source) ion source are presented. Beam brilliance as a function of beam aperture at various extraction conditions is investigated. Influence of electrostatic ion beam compression in post acceleration gap on the beam quality is discussed. Use of different extraction systems (single aperture, 7 holes, and 13 holes) in order to achieve more peaked beam core is considered. The possible ways to increase the beam brilliance are discussed.

High pressure X-ray studies

International Nuclear Information System (INIS)

Sikka, S.K.

1981-01-01

High pressure research has already led to new insights in the physical properties of materials and at times to the synthesis of new ones. In all this, X-ray diffraction has been a valuable diagnostic experimental tool. In particular, X-rays in high pressure field have been used (a) for crystallographic identification of high pressure polymorphs and (b) for study of the effect of pressure on lattice parameters and volume under isothermal conditions. The results in the area (a) are reviewed. The techniques of applying high pressures are described. These include both static and dynamic shockwave X-ray apparatus. To illustrate the effect of pressure, some of the pressure induced phase transitions in pure metals are described. It has been found that there is a clear trend for elements in any group of the periodic table to adopt similar structures at high pressures. These studies have enabled to construct generalized phase diagrams for many groups. In the case of alloys, the high pressure work done on Ti-V alloys is presented. (author)

High-temperature x-ray camera

Energy Technology Data Exchange (ETDEWEB)

Il' inskii, A G; Romanova, A V; Prikhod' ko, N P

1974-03-25

A high-temperature x-ray chamber for taking x-ray photographs of flat horizontally set samples in a vacuum or gas medium is described. The chamber is fitted out with a water-cooled vacuum closed hull with a window letting the x-rays pass, a centering mechanism and a device for heating the samples. To widen its functional abilities the chamber is provided with a goniometric device, fixed immovably to the body foundation by means of two stands. Bearings are mounted to the stands; one of them is equipped with a screw wheel and an endless screw with a limb in the ring; a traverse to which a counter for the x-ray radiation is installed is attached to the shafts of both the bearings. The centering mechanism has a cooled metalic rod, which is connected through a spiral screw thread with the limb fixable by a fork. The position of the shaft of rotation of the counter is adjusted with the help of a nit, extended through the plug openings, positioned on the stands. The chamber can be applied for x-ray structural analyses.

Treatment of foods with high-energy X rays

International Nuclear Information System (INIS)

Cleland, M.R.; Meissner, J.; Herer, A.S.; Beers, E.W.

2001-01-01

The treatment of foods with ionizing energy in the form of gamma rays, accelerated electrons, and X rays can produce beneficial effects, such as inhibiting the sprouting in potatoes, onions, and garlic, controlling insects in fruits, vegetables, and grains, inhibiting the growth of fungi, pasteurizing fresh meat, poultry, and seafood, and sterilizing spices and food additives. After many years of research, these processes have been approved by regulatory authorities in many countries and commercial applications have been increasing. High-energy X rays are especially useful for treating large packages of food. The most attractive features are product penetration, absorbed dose uniformity, high utilization efficiency and short processing time. The ability to energize the X-ray source only when needed enhances the safety and convenience of this technique. The availability of high-energy, high-power electron accelerators, which can be used as X-ray generators, makes it feasible to process large quantities of food economically. Several industrial accelerator facilities already have X-ray conversion equipment and several more will soon be built with product conveying systems designed to take advantage of the unique characteristics of high-energy X rays. These concepts will be reviewed briefly in this paper

Treatment of foods with high-energy X rays

Science.gov (United States)

Cleland, M. R.; Meissner, J.; Herer, A. S.; Beers, E. W.

2001-07-01

The treatment of foods with ionizing energy in the form of gamma rays, accelerated electrons, and X rays can produce beneficial effects, such as inhibiting the sprouting in potatoes, onions, and garlic, controlling insects in fruits, vegetables, and grains, inhibiting the growth of fungi, pasteurizing fresh meat, poultry, and seafood, and sterilizing spices and food additives. After many years of research, these processes have been approved by regulatory authorities in many countries and commercial applications have been increasing. High-energy X rays are especially useful for treating large packages of food. The most attractive features are product penetration, absorbed dose uniformity, high utilization efficiency and short processing time. The ability to energize the X-ray source only when needed enhances the safety and convenience of this technique. The availability of high-energy, high-power electron accelerators, which can be used as X-ray generators, makes it feasible to process large quantities of food economically. Several industrial accelerator facilities already have X-ray conversion equipment and several more will soon be built with product conveying systems designed to take advantage of the unique characteristics of high-energy X rays. These concepts will be reviewed briefly in this paper.

Three-dimensional x-ray stereometry from paired coplanar images: a progress report.

Science.gov (United States)

Baumrind, S; Moffitt, F H; Curry, S

1983-10-01

More than fifty years ago, Broadbent reported the development of a three-dimensional cephalometric method which complexed information from pairs of x-ray images oriented in two planes at right angles to each other. Empirical problems have prevented the routine clinical use of this "biplanar" method, notwithstanding its obvious conceptual brilliance. The present article reports on recent work toward the development of an alternative method of three-dimensional cephalometry in which the two images of each x-ray pair are positioned in the same plane rather than being at right angles to each other. It is believed that this "coplanar" method avoids many of the technical problems that have limited the use of the Broadbent method.

A full-field transmission x-ray microscope for time-resolved imaging of magnetic nanostructures

Energy Technology Data Exchange (ETDEWEB)

Ewald, J.; Nisius, T.; Abbati, G.; Baumbach, S.; Overbuschmann, J.; Wilhein, T. [Institute for X-Optics (IXO), Hochschule Koblenz, Joseph-Rovan-Allee 2, 53424 Remagen (Germany); Wessels, P.; Wieland, M.; Drescher, M. [The Hamburg Centre for Ultrafast Imaging (CUI), University of Hamburg, Luruper Chaussee 149, 22761 Hamburg (Germany); Institut für Experimentalphysik, University of Hamburg, Luruper Chaussee 149, 22761 Hamburg (Germany); Vogel, A. [Institut für Angewandte Physik, University of Hamburg, Jungiusstraße 11, 20355 Hamburg (Germany); Viefhaus, J. [Deutsches Elektronen-Synchrotron (DESY), Notkestraße 85, 22607 Hamburg (Germany); Meier, G. [The Hamburg Centre for Ultrafast Imaging (CUI), University of Hamburg, Luruper Chaussee 149, 22761 Hamburg (Germany); Max Planck Institute for the Structure and Dynamics of Matter, Luruper Chaussee 149, 22761 Hamburg (Germany)

2016-01-28

Sub-nanosecond magnetization dynamics of small permalloy (Ni{sub 80}Fe{sub 20}) elements has been investigated with a new full-field transmission microscope at the soft X-ray beamline P04 of the high brilliance synchrotron radiation source PETRA III. The soft X-ray microscope generates a flat-top illumination field of 20 μm diameter using a grating condenser. A tilted nanostructured magnetic sample can be excited by a picosecond electric current pulse via a coplanar waveguide. The transmitted light of the sample plane is directly imaged by a micro zone plate with < 65 nm resolution onto a 2D gateable X-ray detector to select one particular bunch in the storage ring that probes the time evolution of the dynamic information successively via XMCD spectromicroscopy in a pump-probe scheme. In the experiments it was possible to generate a homogeneously magnetized state in patterned magnetic layers by a strong magnetic Oersted field pulse of 200 ps duration and directly observe the recovery to the initial flux-closure vortex patterns.

High-speed image converter x-ray studies

International Nuclear Information System (INIS)

Bryukhnevitch, G.I.; Kas'yanov, Yu.S.; Korobkin, V.V.; Prokhorov, A.M.; Stepanov, B.M.; Chevokin, V.K.; Schelev, M.Ya.

1975-01-01

Two X-ray high-speed image-converter cameras (ICC) have been developed. In the first one a soft X-ray radiation is converted into visible light with the aid of a 0.5ns response time, plastic scintillator. The second camera incorporates a photocathode which is sensitive to visible and X-ray radiation. Its calculated temporal resolution approaches 5 to 7ps. Both developed cameras were employed for studies of X-ray radiation emitted by laser plasma. For the smooth nanosecond excited laser pulses, a noticeable amplitude modulation was recorded in all laser pulses reflected by plasma as well as in each third pulse of X-ray plasma radiation. It was also observed that the duration of X-ray plasma radiation is 20 to 40% shorter than that of the incident nanosecond laser pulses and this duration being 3 to 6 times longer than that of the picosecond irradiating pulses. The half-width of the recorded X-ray plasma pulses was 30 to 60ps. (author)

EMA beamline at SIRIUS: extreme condition X-ray methods of analysis

International Nuclear Information System (INIS)

Souza Neto, Narcizo

2016-01-01

Full text: The EMA beamline (Extreme condition X-ray Methods of Analysis) is one of the hard x-ray undulator beamlines within the first phase of the new synchrotron source in Brazil (Sirius project). This beamline is thought to make a difference where a high brilliance (high flux of up to 2 x 10 14 photons/sec with beam size down to 0.5 x 0.5 μm 2 ) is essential, which is the case for extreme pressures that require small focus and time-resolved that require high photon flux. With that in mind we propose the beamline to have two experimental hutches to cover most of the extreme condition techniques today employed at synchrotron laboratories worldwide. These two stations are thought to provide the general infrastructure for magnets and lasers experiments, which may evolve as new scientific problems appear. In addition to the hutches, support laboratories will be strongly linked and supportive to the experiments at the beamline, covering high pressure instrumentations using diamond anvil cells and pump-and-probe requirements for ultrafast and high power lasers. Along these lines, we will describe the following techniques covered at this beamline: magnetic spectroscopy (XMCD) and scattering (XRMS) under high pressure and very low temperature in order to fully probe both ferromagnetic and antiferromagnetic materials and the dependence with pressure; extreme pressure and temperature XRD and XAS experiments using very small diamond culet anvils and high power lasers. (author)

EMA beamline at SIRIUS: extreme condition X-ray methods of analysis

Energy Technology Data Exchange (ETDEWEB)

Souza Neto, Narcizo, E-mail: narcizo.souza@lnls.br [Centro Nacional de Pesquisa em Energia e Materiais (CNPEM), Campinas, SP (Brazil)

2016-07-01

Full text: The EMA beamline (Extreme condition X-ray Methods of Analysis) is one of the hard x-ray undulator beamlines within the first phase of the new synchrotron source in Brazil (Sirius project). This beamline is thought to make a difference where a high brilliance (high flux of up to 2 x 10{sup 14} photons/sec with beam size down to 0.5 x 0.5 μm{sup 2}) is essential, which is the case for extreme pressures that require small focus and time-resolved that require high photon flux. With that in mind we propose the beamline to have two experimental hutches to cover most of the extreme condition techniques today employed at synchrotron laboratories worldwide. These two stations are thought to provide the general infrastructure for magnets and lasers experiments, which may evolve as new scientific problems appear. In addition to the hutches, support laboratories will be strongly linked and supportive to the experiments at the beamline, covering high pressure instrumentations using diamond anvil cells and pump-and-probe requirements for ultrafast and high power lasers. Along these lines, we will describe the following techniques covered at this beamline: magnetic spectroscopy (XMCD) and scattering (XRMS) under high pressure and very low temperature in order to fully probe both ferromagnetic and antiferromagnetic materials and the dependence with pressure; extreme pressure and temperature XRD and XAS experiments using very small diamond culet anvils and high power lasers. (author)

Correlation between X-ray and high energy gamma-ray emission form Cygnus X-3

International Nuclear Information System (INIS)

Weekes, T.C.; Danaher, S.; Fegan, D.J.; Porter, N.A.

1981-01-01

In May-June 1980, the 4.8 hour modulated X-ray flux from Cygnus X-3 underwent a significant change in the shape of the light curve; this change correlates with the peak in the high-energy (E > 2 x 10 12 eV) gamma ray emission at the same epoch. (orig.)

BioSAXS Sample Changer: a robotic sample changer for rapid and reliable high-throughput X-ray solution scattering experiments

Energy Technology Data Exchange (ETDEWEB)

Round, Adam, E-mail: around@embl.fr; Felisaz, Franck [European Molecular Biology Laboratory, Grenoble Outstation, 71 Avenue des Martyrs, CS 90181, 38042 Grenoble (France); Université Grenoble Alpes–EMBL–CNRS, 71 Avenue des Martyrs, CS 90181, 38042 Grenoble (France); Fodinger, Lukas; Gobbo, Alexandre [European Molecular Biology Laboratory, Grenoble Outstation, 71 Avenue des Martyrs, CS 90181, 38042 Grenoble (France); Huet, Julien [European Molecular Biology Laboratory, Grenoble Outstation, 71 Avenue des Martyrs, CS 90181, 38042 Grenoble (France); Université Grenoble Alpes–EMBL–CNRS, 71 Avenue des Martyrs, CS 90181, 38042 Grenoble (France); Villard, Cyril [European Molecular Biology Laboratory, Grenoble Outstation, 71 Avenue des Martyrs, CS 90181, 38042 Grenoble (France); Blanchet, Clement E., E-mail: around@embl.fr [EMBL c/o DESY, Notkestrasse 85, 22603 Hamburg (Germany); Pernot, Petra; McSweeney, Sean [ESRF, 6 Rue Jules Horowitz, 38000 Grenoble (France); Roessle, Manfred; Svergun, Dmitri I. [EMBL c/o DESY, Notkestrasse 85, 22603 Hamburg (Germany); Cipriani, Florent, E-mail: around@embl.fr [European Molecular Biology Laboratory, Grenoble Outstation, 71 Avenue des Martyrs, CS 90181, 38042 Grenoble (France); Université Grenoble Alpes–EMBL–CNRS, 71 Avenue des Martyrs, CS 90181, 38042 Grenoble (France)

2015-01-01

A robotic sample changer for solution X-ray scattering experiments optimized for speed and to use the minimum amount of material has been developed. This system is now in routine use at three high-brilliance European synchrotron sites, each capable of several hundred measurements per day. Small-angle X-ray scattering (SAXS) of macromolecules in solution is in increasing demand by an ever more diverse research community, both academic and industrial. To better serve user needs, and to allow automated and high-throughput operation, a sample changer (BioSAXS Sample Changer) that is able to perform unattended measurements of up to several hundred samples per day has been developed. The Sample Changer is able to handle and expose sample volumes of down to 5 µl with a measurement/cleaning cycle of under 1 min. The samples are stored in standard 96-well plates and the data are collected in a vacuum-mounted capillary with automated positioning of the solution in the X-ray beam. Fast and efficient capillary cleaning avoids cross-contamination and ensures reproducibility of the measurements. Independent temperature control for the well storage and for the measurement capillary allows the samples to be kept cool while still collecting data at physiological temperatures. The Sample Changer has been installed at three major third-generation synchrotrons: on the BM29 beamline at the European Synchrotron Radiation Facility (ESRF), the P12 beamline at the PETRA-III synchrotron (EMBL@PETRA-III) and the I22/B21 beamlines at Diamond Light Source, with the latter being the first commercial unit supplied by Bruker ASC.

High-intensity laser synchrotron x-ray source

International Nuclear Information System (INIS)

Pogorelsky, I.V.

1995-10-01

A laser interacting with a relativistic electron beam behaves like a virtual wiggler of an extremely short period equal to half of the laser wavelength. This approach opens a route to relatively compact, high-brightness x-ray sources alternative or complementary to conventional synchrotron light sources. Although not new, the Laser Synchrotron Light Source (LSLS) concept is still waiting for a convincing demonstration. Available at the BNL's Accelerator Test Facility (ATF), a high-brightness electron beam and the high-power C0 2 laser may be used as prototype LSLS brick stones. In a feasible demonstration experiment, 10-GW, 100-ps C0 2 laser beam will be brought to a head-on collision with a 10-ps, 0.5-nC, 70 MeV electron bunch. Flashes of well-collimated, up to 9.36-keV (∼ Angstrom) x-rays of 10-ps pulse duration, with a flux of ∼10 19 photons/sec will be produced via linear Compton backscattering. The x-ray spectrum is tunable proportionally to a variable e-beam energy. A natural short-term extension of the proposed experiment would be further enhancement of the x-ray flux to a 10 21 -10 22 photons/sec level, after the ongoing ATF CO 2 laser upgrade to 1 TW peak power and electron bunch shortening to 3 ps. The ATF LSLS x-ray beamline, exceeding by orders of magnitude the peak fluxes attained at the National Synchrotron Light Source (NSLS) x-ray storage ring, may become attractive for certain users, e.g., for biological x-ray microscopy. In addition, a terawatt CO 2 laser will enable harmonic multiplication of the x-ray spectrum via nonlinear Compton scattering

Progress in high-resolution x-ray holographic microscopy

International Nuclear Information System (INIS)

Jacobsen, C.; Kirz, J.; Howells, M.; McQuaid, K.; Rothman, S.; Feder, R.; Sayre, D.

1987-07-01

Among the various types of x-ray microscopes that have been demonstrated, the holographic microscope has had the largest gap between promise and performance. The difficulties of fabricating x-ray optical elements have led some to view holography as the most attractive method for obtaining the ultimate in high resolution x-ray micrographs; however, we know of no investigations prior to 1987 that clearly demonstrated submicron resolution in reconstructed images. Previous efforts suffered from problems such as limited resolution and dynamic range in the recording media, low coherent x-ray flux, and aberrations and diffraction limits in visible light reconstruction. We have addressed the recording limitations through the use of an undulator x-ray source and high-resolution photoresist recording media. For improved results in the readout and reconstruction steps, we have employed metal shadowing and transmission electron microscopy, along with numerical reconstruction techniques. We believe that this approach will allow holography to emerge as a practical method of high-resolution x-ray microscopy. 30 refs., 4 figs

Progress in high-resolution x-ray holographic microscopy

Energy Technology Data Exchange (ETDEWEB)

Jacobsen, C.; Kirz, J.; Howells, M.; McQuaid, K.; Rothman, S.; Feder, R.; Sayre, D.

1987-07-01

Among the various types of x-ray microscopes that have been demonstrated, the holographic microscope has had the largest gap between promise and performance. The difficulties of fabricating x-ray optical elements have led some to view holography as the most attractive method for obtaining the ultimate in high resolution x-ray micrographs; however, we know of no investigations prior to 1987 that clearly demonstrated submicron resolution in reconstructed images. Previous efforts suffered from problems such as limited resolution and dynamic range in the recording media, low coherent x-ray flux, and aberrations and diffraction limits in visible light reconstruction. We have addressed the recording limitations through the use of an undulator x-ray source and high-resolution photoresist recording media. For improved results in the readout and reconstruction steps, we have employed metal shadowing and transmission electron microscopy, along with numerical reconstruction techniques. We believe that this approach will allow holography to emerge as a practical method of high-resolution x-ray microscopy. 30 refs., 4 figs.

A high resolution position sensitive X-ray MWPC for small angle X-ray diffraction

International Nuclear Information System (INIS)

Bateman, J.E.; Connolly, J.F.; Stephenson, R.; Tappern, G.J.

1981-02-01

A small sealed-off delay line readout MWPC X-ray detector has been designed and built for small angle X-ray diffraction applications. Featuring a sensitive area of 100 mm x 25 mm it yields a spatial resolution of 0.13 mm (standard deviation) with a high rate capability and good quantum efficiency for copper K radiation. (author)

High-intensity, subkilovolt x-ray calibration facility

International Nuclear Information System (INIS)

Kuckuck, R.W.; Gaines, J.L.; Ernst, R.D.

1976-01-01

A high-intensity subkilovolt x-ray calibration source utilizing proton-induced inner-shell atomic fluorescence of low-Z elements is described. The high photon yields and low bremsstrahlung background associated with this phenomenon are ideally suited to provide intense, nearly monoenergetic x-ray beams. The proton accelerator is a 3 mA, 300 kV Cockroft-Walton using a conventional rf hydrogen ion source. Seven remotely-selectable targets capable of heat dissipation of 5 kW/cm 2 are used to provide characteristic x-rays with energies between 100 and 1000 eV. Source strengths are of the order of 10 13 to 10 14 photons/sec. Methods of reducing spectral contamination due to hydrocarbon build-up on the target are discussed. Typical x-ray spectra (Cu-L, C-K and B-K) are shown

X-ray fluorescence in Member States (Italy): Full field X-ray fluorescence imaging with high-energy and high-spatial resolution

Energy Technology Data Exchange (ETDEWEB)

Romano, F. P.; Masini, N.; Pappalardo, L., E-mail: romanop@lns.infn.it [IBAM, CNR, Via Biblioteca 4, 95124 Catania (Italy); Cosentino, L.; Gammino, S.; Mascali, D.; Rizzo, F. [INFN-LNS, Via S. Sofia 62, 95123 Catania (Italy)

2014-02-15

A full field X-ray camera for the X-Ray Fluorescence imaging of materials with high-energy and high-spatial resolution was designed and developed. The system was realized by coupling a pinhole collimator with a positionsensitive CCD detector. X-Ray fluorescence is induced on the samples by irradiation with an external X-ray tube. The characteristic X-ray spectra of the investigated materials are obtained by using a multi-frames acquisition in single-photon counting. The energy resolution measured at the Fe-Kα line was 157 eV. The spatial resolution of the system was determined by the analysis of a sharp-edge at different magnification values; it was estimated to be 90 μm at a magnification value of 3.2x and 190 μm at 0.8x. The present set-up of the system is suited to analyze samples with dimensions up to 5x4 cm{sup 2}. Typical measurement time is in the range between 1h to 4 h. (author)

Synchrotron X-ray imaging applied to solar photovoltaic silicon

International Nuclear Information System (INIS)

Lafford, T A; Villanova, J; Plassat, N; Dubois, S; Camel, D

2013-01-01

Photovoltaic (PV) cell performance is dictated by the material of the cell, its quality and purity, the type, quantity, size and distribution of defects, as well as surface treatments, deposited layers and contacts. A synchrotron offers unique opportunities for a variety of complementary X-ray techniques, given the brilliance, spectrum, energy tunability and potential for (sub-) micron-sized beams. Material properties are revealed within in the bulk and at surfaces and interfaces. X-ray Diffraction Imaging (X-ray Topography), Rocking Curve Imaging and Section Topography reveal defects such as dislocations, inclusions, misorientations and strain in the bulk and at surfaces. Simultaneous measurement of micro-X-Ray Fluorescence (μ-XRF) and micro-X-ray Beam Induced Current (μ-XBIC) gives direct correlation between impurities and PV performance. Together with techniques such as microscopy and Light Beam Induced Current (LBIC) measurements, the correlation between structural properties and photovoltaic performance can be deduced, as well as the relative influence of parameters such as defect type, size, spatial distribution and density (e.g [1]). Measurements may be applied at different stages of solar cell processing in order to follow the evolution of the material and its properties through the manufacturing process. Various grades of silicon are under study, including electronic and metallurgical grades in mono-crystalline, multi-crystalline and mono-like forms. This paper aims to introduce synchrotron imaging to non-specialists, giving example results on selected solar photovoltaic silicon samples.

Introduction. From a first-generation synchrotron radiation to an x-ray free electron laser

International Nuclear Information System (INIS)

Mizuki, Jun'ichiro

2013-01-01

The fruitful and remarkable research results in materials science during the past more than ten years have been continuously obtained by the advent of synchrotron radiation (SR) sources, especially the third-generation SR source. This is easily understood by considering that the SR beams provide not only five to ten orders of magnitude brilliance more in the continuum vacuum ultraviolet and X-ray regions of the electromagnetic spectrum than conventional sources, but also natural collimation, high polarization, pulsed time structure and high stability. In this paper we present a brief history of SR sources, especially in Japan to know how the SR sources developed, and a view of the future research direction regarding the use of SR beams. (author)

High-resolution X-ray television and high-resolution video recorders

International Nuclear Information System (INIS)

Haendle, J.; Horbaschek, H.; Alexandrescu, M.

1977-01-01

The improved transmission properties of the high-resolution X-ray television chain described here make it possible to transmit more information per television image. The resolution in the fluoroscopic image, which is visually determined, depends on the dose rate and the inertia of the television pick-up tube. This connection is discussed. In the last few years, video recorders have been increasingly used in X-ray diagnostics. The video recorder is a further quality-limiting element in X-ray television. The development of function patterns of high-resolution magnetic video recorders shows that this quality drop may be largely overcome. The influence of electrical band width and number of lines on the resolution in the X-ray television image stored is explained in more detail. (orig.) [de

Miniaturized High-Speed Modulated X-Ray Source

Science.gov (United States)

Gendreau, Keith C. (Inventor); Arzoumanian, Zaven (Inventor); Kenyon, Steven J. (Inventor); Spartana, Nick Salvatore (Inventor)

2015-01-01

A miniaturized high-speed modulated X-ray source (MXS) device and a method for rapidly and arbitrarily varying with time the output X-ray photon intensities and energies. The MXS device includes an ultraviolet emitter that emits ultraviolet light, a photocathode operably coupled to the ultraviolet light-emitting diode that emits electrons, an electron multiplier operably coupled to the photocathode that multiplies incident electrons, and an anode operably coupled to the electron multiplier that is configured to produce X-rays. The method for modulating MXS includes modulating an intensity of an ultraviolet emitter to emit ultraviolet light, generating electrons in response to the ultraviolet light, multiplying the electrons to become more electrons, and producing X-rays by an anode that includes a target material configured to produce X-rays in response to impact of the more electrons.

Isolated elliptically polarized attosecond soft X-ray with high-brilliance using polarization gating of harmonics from relativistic plasmas at oblique incidence.

Science.gov (United States)

Chen, Zi-Yu; Li, Xiao-Ya; Li, Bo-Yuan; Chen, Min; Liu, Feng

2018-02-19

The production of intense isolated attosecond pulse is a major goal in ultrafast research. Recent advances in high harmonic generation from relativistic plasma mirrors under oblique incidence interactions gave rise to photon-rich attosecond pulses with circular or elliptical polarization. However, to achieve an isolated elliptical attosecond pulse via polarization gating using currently available long driving pulses remains a challenge, because polarization gating of high harmonics from relativistic plasmas is assumed only possible at normal or near-normal incidence. Here we numerically demonstrate a scheme around this problem. We show that via control of plasma dynamics by managing laser polarization, it is possible to gate an intense single attosecond pulse with high ellipticity extending to the soft X-ray regime at oblique incidence. This approach thus paves the way towards a powerful tool enabling high-time-resolution probe of dynamics of chiral systems and magnetic materials with current laser technology.

Geoscience Applications of Synchrotron X-ray Computed Microtomography

Science.gov (United States)

Rivers, M. L.

2009-05-01

Computed microtomography is the extension to micron spatial resolution of the CAT scanning technique developed for medical imaging. Synchrotron sources are ideal for the method, since they provide a monochromatic, parallel beam with high intensity. High energy storage rings such as the Advanced Photon Source at Argonne National Laboratory produce x-rays with high energy, high brilliance, and high coherence. All of these factors combine to produce an extremely powerful imaging tool for earth science research. Techniques that have been developed include: - Absorption and phase contrast computed tomography with spatial resolution approaching one micron - Differential contrast computed tomography, imaging above and below the absorption edge of a particular element - High-pressure tomography, imaging inside a pressure cell at pressures above 10GPa - High speed radiography, with 100 microsecond temporal resolution - Fluorescence tomography, imaging the 3-D distribution of elements present at ppm concentrations. - Radiographic strain measurements during deformation at high confining pressure, combined with precise x- ray diffraction measurements to determine stress. These techniques have been applied to important problems in earth and environmental sciences, including: - The 3-D distribution of aqueous and organic liquids in porous media, with applications in contaminated groundwater and petroleum recovery. - The kinetics of bubble formation in magma chambers, which control explosive volcanism. - Accurate crystal size distributions in volcanic systems, important for understanding the evolution of magma chambers. - The equation-of-state of amorphous materials at high pressure using both direct measurements of volume as a function of pressure and also by measuring the change x-ray absorption coefficient as a function of pressure. - The formation of frost flowers on Arctic sea-ice, which is important in controlling the atmospheric chemistry of mercury. - The distribution of

High-speed radiography and x-ray cinematography by high-current betatrons

International Nuclear Information System (INIS)

Akimochkin, Yu.V.; Akulov, G.V.; Leunov, F.G.; Moskalev, V.A.; Ryabukhin, V.L.

1979-01-01

The paper provides a description of an equipment system comprising a pair of 25 MeV high-current betatrons and an X-ray drum-type cinecamera for high-speed radiography and X-ray cinematography for use when studying dynamics of objects moving at a rate of 0.5 - 3.0 km/s as well as in X-ray cinematography of processes at a rate of up to 1 m/s. (author)

Dosimetry of x-rays from high-temperature plasmas

International Nuclear Information System (INIS)

Yamamoto, Takayoshi; Abe, Nobuyuki; Kawanishi, Masaharu

1980-01-01

Study on the dosimetry of ionizing radiations, especially of X-rays, emitted from high-temperature plasms has been made. As to the unpolarized Bremsstrahlung, a brief method to estimate electron temperatures with TLD is described and evaluation of average energy and current of the run-away electrons in the turbulent heating Tokamak is made by observing the half-value layer of the emitted X-rays and the total exposure per one shot of the Tokamak discharge. As to the polarized one, it is shown that the anisotropic electron temperature is related to the degree of polarization of the X-rays. Furthermore, reference is made to the possibility of developing such X-ray generators as can emit nearly monochromatic X-rays (characteristic X-rays) or polarized ones arbitrarily. (author)

A quasi-realtime x-ray microtomography system at the Advanced Photon Source

International Nuclear Information System (INIS)

DeCarlo, F.; Foster, I.; Insley, J.; Kesselman, C.; Lane, P.; Mancini, D.; McNulty, I.; Su, M.; Tieman, B.; Wang, Y.; Laszewski, G. von

1999-01-01

The combination of high-brilliance x-ray sources, fast detector systems, wide-bandwidth networks, and parallel computers can substantially reduce the time required to acquire, reconstruct, and visualize high-resolution three-dimensional tomographic datasets. A quasi-realtime computed x-ray microtomography system has been implemented at the 2-BM beamline at the Advanced Photon Source at Argonne National Laboratory. With this system, a complete tomographic data set can be collected in about 15 minutes. Immediately after each projection is obtained, it is rapidly transferred to the Mathematics and Computing Sciences Division where preprocessing and reconstruction calculations are performed concurrently with the data acquisition by a SGI parallel computer. The reconstruction results, once completed, are transferred to a visualization computer that performs the volume rendering calculations. Rendered images of the reconstructed data are available for viewing back at the beamline experiment station minutes after the data acquisition was complete. The fully pipelined data acquisition and reconstruction system also gives us the option to acquire the tomographic data set in several cycles, initially with coarse then with fine angular steps. At present the projections are acquired with a straight-ray projection imaging scheme using 5-20 keV hard x rays in either phase or amplitude contrast mode at a 1-10 pm resolution. In the future, we expect to increase the resolution of the projections to below 100 nm by using a focused x-ray beam at the 2-ID-B beamline and to reduce the combined acquisition and computation time to the 1 min scale with improvements in the detectors, network links, software pipeline, and computation algorithms

A new X-ray pinhole camera for energy dispersive X-ray fluorescence imaging with high-energy and high-spatial resolution

Energy Technology Data Exchange (ETDEWEB)

Romano, F.P., E-mail: romanop@lns.infn.it [IBAM, CNR, Via Biblioteca 4, 95124 Catania (Italy); INFN-LNS, Via S. Sofia 62, 95123 Catania (Italy); Altana, C. [INFN-LNS, Via S. Sofia 62, 95123 Catania (Italy); Dipartimento di Fisica e Astronomia, Università di Catania, Via S. Sofia 64, 95123 Catania (Italy); Cosentino, L.; Celona, L.; Gammino, S.; Mascali, D. [INFN-LNS, Via S. Sofia 62, 95123 Catania (Italy); Pappalardo, L. [IBAM, CNR, Via Biblioteca 4, 95124 Catania (Italy); INFN-LNS, Via S. Sofia 62, 95123 Catania (Italy); Rizzo, F. [INFN-LNS, Via S. Sofia 62, 95123 Catania (Italy); Dipartimento di Fisica e Astronomia, Università di Catania, Via S. Sofia 64, 95123 Catania (Italy)

2013-08-01

A new X-ray pinhole camera for the Energy Dispersive X-ray Fluorescence (ED-XRF) imaging of materials with high-energy and high-spatial resolution, was designed and developed. It consists of a back-illuminated and deep depleted CCD detector (composed of 1024 × 1024 pixels with a lateral size of 13 μm) coupled to a 70 μm laser-drilled pinhole-collimator, positioned between the sample under analysis and the CCD. The X-ray pinhole camera works in a coaxial geometry allowing a wide range of magnification values. The characteristic X-ray fluorescence is induced on the samples by irradiation with an external X-ray tube working at a maximum power of 100 W (50 kV and 2 mA operating conditions). The spectroscopic capabilities of the X-ray pinhole camera were accurately investigated. Energy response and energy calibration of the CCD detector were determined by irradiating pure target-materials emitting characteristic X-rays in the energy working-domain of the system (between 3 keV and 30 keV). Measurements were performed by using a multi-frame acquisition in single-photon counting. The characteristic X-ray spectra were obtained by an automated processing of the acquired images. The energy resolution measured at the Fe–Kα line is 157 eV. The use of the X-ray pinhole camera for the 2D resolved elemental analysis was investigated by using reference-patterns of different materials and geometries. The possibility of the elemental mapping of samples up to an area of 3 × 3 cm{sup 2} was demonstrated. Finally, the spatial resolution of the pinhole camera was measured by analyzing the profile function of a sharp-edge. The spatial resolution determined at the magnification values of 3.2 × and 0.8 × (used as testing values) is about 90 μm and 190 μm respectively. - Highlights: • We developed an X-ray pinhole camera for the 2D X-ray fluorescence imaging. • X-ray spectra are obtained by a multi-frame acquisition in single photon mode. • The energy resolution in the X-ray

Differential phase contrast setup for a non coherent beamline at HASYLAB using hard X-ray grating interferometer

Energy Technology Data Exchange (ETDEWEB)

Herzen, Julia; Beckmann, Felix; Haibel, Astrid; Schreyer, Andreas [GKSS Research Centre, Geesthacht (Germany); Donath, Tilman; David, Christian; Gruenzweig, Christian [Paul Scherrer Institute, Villigen PSI (Switzerland); Pfeiffer, Franz [Paul Scherrer Institute, Villigen PSI (Switzerland); EPF Lausanne, Lausanne (Switzerland)

2009-07-01

Phase-contrast imaging is a common technique to visualize soft tissue with much higher contrast than the conventional absorption-contrast imaging. Differential phase contrast (DPC), developed at PSI, Switzerland, makes use of a hard x-ray grating interferometer and allows for phase-contrast imaging with high brilliance synchrotron sources as well as with conventional x-ray tubes. It is recently reported also to provide dark field information that is very sensitive to micro structures like porosity within the materials. Here we present the plans to adopt the DPC technique to the HARWI-II materials science beamline, operated by GKSS Research Centre, in cooperation with DESY, Hamburg. This will offer an amount of new applications especially in the field of materials science like for example characterizing new light weight materials like magnesium and studying its corrosion as implant material.

Kinetics of the main phase transition of hydrated lecithin monitored by real-time x-ray diffraction

International Nuclear Information System (INIS)

Caffrey, M.; Bilderback, D.H.

1984-01-01

A method is described for observing and recording in real-time x-ray diffraction from an unoriented hydrated membrane lipid, dipalmitoylphosphatidylcholine (DPPC), through its thermotropic gel/liquid crystal phase transition. Synchrotron radiation from the Cornell High Energy Synchrotron Source (Ithaca, New York) was used as an x-ray source of extremely high brilliance and the dynamic display of the diffraction image was effected using a three-stage image intensifier tube coupled to an external fluorescent screen. The image on the output phosphor was sufficiently intense to be recorded cinematographically and to be displayed on a television monitor using a vidicon camera at 30 frames x s -1 . These measurements set an upper limit of 2 s on the DPPC gel → liquid crystal phase transition and indicate that the transition is a two-state process. The real-time method couples the power of x-ray diffraction as a structural probe with the ability to follow kinetics of structural changes. The method does not require an exogenous probe, is relatively nonperturbing, and can be used with membranes in a variety of physical states and with unstable samples. The method has the additional advantage over its static measurement counterpart in that it is more likely to detect transiently stable intermediates if present

Ultra-high-resolution inelastic X-ray scattering at high-repetition-rate self-seeded X-ray free-electron lasers

Energy Technology Data Exchange (ETDEWEB)

Chubar, Oleg [Brookhaven National Laboratory, Upton, NY 11973 (United States); Geloni, Gianluca [European X-ray Free-Electron Laser, Albert-Einstein-Ring 19, 22761 Hamburg (Germany); Kocharyan, Vitali [Deutsches Elektronen-Synchrotron, 22761 Hamburg (Germany); Madsen, Anders [European X-ray Free-Electron Laser, Albert-Einstein-Ring 19, 22761 Hamburg (Germany); Saldin, Evgeni; Serkez, Svitozar [Deutsches Elektronen-Synchrotron, 22761 Hamburg (Germany); Shvyd’ko, Yuri, E-mail: shvydko@aps.anl.gov [Argonne National Laboratory, Argonne, IL 60439 (United States); Sutter, John [Diamond Light Source Ltd, Didcot OX11 0DE (United Kingdom)

2016-02-12

This article explores novel opportunities for ultra-high-resolution inelastic X-ray scattering (IXS) at high-repetition-rate self-seeded XFELs. These next-generation light sources are promising a more than three orders of magnitude increase in average spectral flux compared with what is possible with storage-ring-based radiation sources. In combination with the advanced IXS spectrometer described here, this may become a real game-changer for ultra-high-resolution X-ray spectroscopies, and hence for the studies of dynamics in condensed matter systems. Inelastic X-ray scattering (IXS) is an important tool for studies of equilibrium dynamics in condensed matter. A new spectrometer recently proposed for ultra-high-resolution IXS (UHRIX) has achieved 0.6 meV and 0.25 nm{sup −1} spectral and momentum-transfer resolutions, respectively. However, further improvements down to 0.1 meV and 0.02 nm{sup −1} are required to close the gap in energy–momentum space between high- and low-frequency probes. It is shown that this goal can be achieved by further optimizing the X-ray optics and by increasing the spectral flux of the incident X-ray pulses. UHRIX performs best at energies from 5 to 10 keV, where a combination of self-seeding and undulator tapering at the SASE-2 beamline of the European XFEL promises up to a 100-fold increase in average spectral flux compared with nominal SASE pulses at saturation, or three orders of magnitude more than what is possible with storage-ring-based radiation sources. Wave-optics calculations show that about 7 × 10{sup 12} photons s{sup −1} in a 90 µeV bandwidth can be achieved on the sample. This will provide unique new possibilities for dynamics studies by IXS.

High-resolution X-ray diffraction studies of multilayers

DEFF Research Database (Denmark)

Christensen, Finn Erland; Hornstrup, Allan; Schnopper, H. W.

1988-01-01

High-resolution X-ray diffraction studies of the perfection of state-of-the-art multilayers are presented. Data were obtained using a triple-axis perfect-crystal X-ray diffractometer. Measurements reveal large-scale figure errors in the substrate. A high-resolution triple-axis set up is required...

A laboratory-based hard x-ray monochromator for high-resolution x-ray emission spectroscopy and x-ray absorption near edge structure measurements

Energy Technology Data Exchange (ETDEWEB)

Seidler, G. T., E-mail: seidler@uw.edu; Mortensen, D. R.; Remesnik, A. J.; Pacold, J. I.; Ball, N. A.; Barry, N.; Styczinski, M.; Hoidn, O. R. [Physics Department, University of Washington, Seattle, Washington 98195-1560 (United States)

2014-11-15

We report the development of a laboratory-based Rowland-circle monochromator that incorporates a low power x-ray (bremsstrahlung) tube source, a spherically bent crystal analyzer, and an energy-resolving solid-state detector. This relatively inexpensive, introductory level instrument achieves 1-eV energy resolution for photon energies of ∼5 keV to ∼10 keV while also demonstrating a net efficiency previously seen only in laboratory monochromators having much coarser energy resolution. Despite the use of only a compact, air-cooled 10 W x-ray tube, we find count rates for nonresonant x-ray emission spectroscopy comparable to those achieved at monochromatized spectroscopy beamlines at synchrotron light sources. For x-ray absorption near edge structure, the monochromatized flux is small (due to the use of a low-powered x-ray generator) but still useful for routine transmission-mode studies of concentrated samples. These results indicate that upgrading to a standard commercial high-power line-focused x-ray tube or rotating anode x-ray generator would result in monochromatized fluxes of order 10{sup 6}–10{sup 7} photons/s with no loss in energy resolution. This work establishes core technical capabilities for a rejuvenation of laboratory-based hard x-ray spectroscopies that could have special relevance for contemporary research on catalytic or electrical energy storage systems using transition-metal, lanthanide, or noble-metal active species.

High speed gated x-ray imagers

International Nuclear Information System (INIS)

Kilkenny, J.D.; Bell, P.; Hanks, R.; Power, G.; Turner, R.E.; Wiedwald, J.

1988-01-01

Single and multi-frame gated x-ray images with time-resolution as fast as 150 psec are described. These systems are based on the gating of microchannel plates in a stripline configuration. The gating voltage comes from the avalanche breakdown of reverse biased p-n junction producing high power voltage pulses as short as 70 psec. Results from single and four frame x-ray cameras used on Nova are described. 8 refs., 9 figs

Bright circularly polarized soft X-ray high harmonics for X-ray magnetic circular dichroism.

Science.gov (United States)

Fan, Tingting; Grychtol, Patrik; Knut, Ronny; Hernández-García, Carlos; Hickstein, Daniel D; Zusin, Dmitriy; Gentry, Christian; Dollar, Franklin J; Mancuso, Christopher A; Hogle, Craig W; Kfir, Ofer; Legut, Dominik; Carva, Karel; Ellis, Jennifer L; Dorney, Kevin M; Chen, Cong; Shpyrko, Oleg G; Fullerton, Eric E; Cohen, Oren; Oppeneer, Peter M; Milošević, Dejan B; Becker, Andreas; Jaroń-Becker, Agnieszka A; Popmintchev, Tenio; Murnane, Margaret M; Kapteyn, Henry C

2015-11-17

We demonstrate, to our knowledge, the first bright circularly polarized high-harmonic beams in the soft X-ray region of the electromagnetic spectrum, and use them to implement X-ray magnetic circular dichroism measurements in a tabletop-scale setup. Using counterrotating circularly polarized laser fields at 1.3 and 0.79 µm, we generate circularly polarized harmonics with photon energies exceeding 160 eV. The harmonic spectra emerge as a sequence of closely spaced pairs of left and right circularly polarized peaks, with energies determined by conservation of energy and spin angular momentum. We explain the single-atom and macroscopic physics by identifying the dominant electron quantum trajectories and optimal phase-matching conditions. The first advanced phase-matched propagation simulations for circularly polarized harmonics reveal the influence of the finite phase-matching temporal window on the spectrum, as well as the unique polarization-shaped attosecond pulse train. Finally, we use, to our knowledge, the first tabletop X-ray magnetic circular dichroism measurements at the N4,5 absorption edges of Gd to validate the high degree of circularity, brightness, and stability of this light source. These results demonstrate the feasibility of manipulating the polarization, spectrum, and temporal shape of high harmonics in the soft X-ray region by manipulating the driving laser waveform.

Low Mass X-ray Binary 4U1705-44 Exiting an Extended High X-ray State

Science.gov (United States)

Phillipson, Rebecca; Boyd, Patricia T.; Smale, Alan P.

2017-09-01

The neutron-star low-mass X-ray binary 4U1705-44, which exhibited high amplitude long-term X-ray variability on the order of hundreds of days during the 16-year continuous monitoring by the RXTE ASM (1995-2012), entered an anomalously long high state in July 2012 as observed by MAXI (2009-present).

Compton spectra of atoms at high x-ray intensity

Science.gov (United States)

Son, Sang-Kil; Geffert, Otfried; Santra, Robin

2017-03-01

Compton scattering is the nonresonant inelastic scattering of an x-ray photon by an electron and has been used to probe the electron momentum distribution in gas-phase and condensed-matter samples. In the low x-ray intensity regime, Compton scattering from atoms dominantly comes from bound electrons in neutral atoms, neglecting contributions from bound electrons in ions and free (ionized) electrons. In contrast, in the high x-ray intensity regime, the sample experiences severe ionization via x-ray multiphoton multiple ionization dynamics. Thus, it becomes necessary to take into account all the contributions to the Compton scattering signal when atoms are exposed to high-intensity x-ray pulses provided by x-ray free-electron lasers (XFELs). In this paper, we investigate the Compton spectra of atoms at high x-ray intensity, using an extension of the integrated x-ray atomic physics toolkit, xatom. As the x-ray fluence increases, there is a significant contribution from ionized electrons to the Compton spectra, which gives rise to strong deviations from the Compton spectra of neutral atoms. The present study provides not only understanding of the fundamental XFEL-matter interaction but also crucial information for single-particle imaging experiments, where Compton scattering is no longer negligible. , which features invited work from the best early-career researchers working within the scope of J. Phys. B. This project is part of the Journal of Physics series’ 50th anniversary celebrations in 2017. Sang-Kil Son was selected by the Editorial Board of J. Phys. B as an Emerging Leader.

High Resolution Energetic X-ray Imager (HREXI)

Science.gov (United States)

Grindlay, Jonathan

We propose to design and build the first imaging hard X-ray detector system that incorporates 3D stacking of closely packed detector readouts in finely-spaced imaging arrays with their required data processing and control electronics. In virtually all imaging astronomical detectors, detector readout is done with flex connectors or connections that are not vertical but rather horizontal , requiring loss of focal plane area. For high resolution pixel detectors needed for high speed event-based X-ray imaging, from low energy applications (CMOS) with focusing X-ray telescopes, to hard X-ray applications with pixelated CZT for large area coded aperture telescopes, this new detector development offers great promise. We propose to extend our previous and current APRA supported ProtoEXIST program that has developed the first large area imaging CZT detectors and demonstrated their astrophysical capabilities on two successful balloon flight to a next generation High Resolution Energetic X-ray Imager (HREXI), which would incorporate microvia technology for the first time to connect the readout ASIC on each CZT crystal directly to its control and data processing system. This 3-dimensional stacking of detector and readout/control system means that large area (>2m2) imaging detector planes for a High Resolution Wide-field hard X-ray telescope can be built with initially greatly reduced detector gaps and ultimately with no gaps. This increases detector area, efficiency, and simplicity of detector integration. Thus higher sensitivity wide-field imagers will be possible at lower cost. HREXI will enable a post-Swift NASA mission such as the EREXS concept proposed to PCOS to be conducted as a future MIDEX mission. This mission would conduct a high resolution (<2 arcmin) , broad band (5 200 keV) hard X-ray survey of black holes on all scales with ~10X higher sensitivity than Swift. In the current era of Time Domain Astrophysics, such a survey capability, in conjunction with a n

Diagnostic Spectrometers for High Energy Density X-Ray Sources

International Nuclear Information System (INIS)

Hudson, L. T.; Henins, A.; Seely, J. F.; Holland, G. E.

2007-01-01

A new generation of advanced laser, accelerator, and plasma confinement devices are emerging that are producing extreme states of light and matter that are unprecedented for laboratory study. Examples of such sources that will produce laboratory x-ray emissions with unprecedented characteristics include megajoule-class and ultrafast, ultraintense petawatt laser-produced plasmas; tabletop high-harmonic-generation x-ray sources; high-brightness zeta-pinch and magnetically confined plasma sources; and coherent x-ray free electron lasers and compact inverse-Compton x-ray sources. Characterizing the spectra, time structure, and intensity of x rays emitted by these and other novel sources is critical to assessing system performance and progress as well as pursuing the new and unpredictable physical interactions of interest to basic and applied high-energy-density (HED) science. As these technologies mature, increased emphasis will need to be placed on advanced diagnostic instrumentation and metrology, standard reference data, absolute calibrations and traceability of results.We are actively designing, fabricating, and fielding wavelength-calibrated x-ray spectrometers that have been employed to register spectra from a variety of exotic x-ray sources (electron beam ion trap, electron cyclotron resonance ion source, terawatt pulsed-power-driven accelerator, laser-produced plasmas). These instruments employ a variety of curved-crystal optics, detector technologies, and data acquisition strategies. In anticipation of the trends mentioned above, this paper will focus primarily on optical designs that can accommodate the high background signals produced in HED experiments while also registering their high-energy spectral emissions. In particular, we review the results of recent laboratory testing that explores off-Rowland circle imaging in an effort to reclaim the instrumental resolving power that is increasingly elusive at higher energies when using wavelength

21 CFR 892.1700 - Diagnostic x-ray high voltage generator.

Science.gov (United States)

2010-04-01

... 21 Food and Drugs 8 2010-04-01 2010-04-01 false Diagnostic x-ray high voltage generator. 892.1700... (CONTINUED) MEDICAL DEVICES RADIOLOGY DEVICES Diagnostic Devices § 892.1700 Diagnostic x-ray high voltage generator. (a) Identification. A diagnostic x-ray high voltage generator is a device that is intended to...

ICF ignition capsule neutron, gamma ray, and high energy x-ray images

Science.gov (United States)

Bradley, P. A.; Wilson, D. C.; Swenson, F. J.; Morgan, G. L.

2003-03-01

Post-processed total neutron, RIF neutron, gamma-ray, and x-ray images from 2D LASNEX calculations of burning ignition capsules are presented. The capsules have yields ranging from tens of kilojoules (failures) to over 16 MJ (ignition), and their implosion symmetry ranges from prolate (flattest at the hohlraum equator) to oblate (flattest towards the laser entrance hole). The simulated total neutron images emphasize regions of high DT density and temperature; the reaction-in-flight neutrons emphasize regions of high DT density; the gamma rays emphasize regions of high shell density; and the high energy x rays (>10 keV) emphasize regions of high temperature.

Large aperture Fizeau interferometer commissioning and preliminary measurements of a long x-ray mirror at European X-ray Free Electron Laser

Energy Technology Data Exchange (ETDEWEB)

Vannoni, M., E-mail: maurizio.vannoni@xfel.eu; Freijo Martín, I. [European XFEL GmbH, Albert-Einstein-Ring 19, 22761 Hamburg (Germany)

2016-05-15

The European XFEL (X-ray Free Electron Laser) is a large facility under construction in Hamburg, Germany. It will provide a transversally fully coherent x-ray radiation with outstanding characteristics: high repetition rate (up to 2700 pulses with a 0.6 ms long pulse train at 10 Hz), short wavelength (down to 0.05 nm), short pulse (in the femtoseconds scale), and high average brilliance (1.6 ⋅ 10{sup 25} (photons s{sup −1} mm{sup −2} mrad{sup −2})/0.1% bandwidth). The beam has very high pulse energy; therefore, it has to be spread out on a relatively long mirror (about 1 m). Due to the very short wavelength, the mirrors need to have a high quality surface on their entire length, and this is considered very challenging even with the most advanced polishing methods. In order to measure the mirrors and to characterize their interaction with the mechanical mount, we equipped a metrology laboratory with a large aperture Fizeau interferometer. The system is a classical 100 mm diameter commercial Fizeau, with an additional expander providing a 300 mm diameter beam. Despite the commercial nature of the system, special care has been taken in the polishing of the reference flats and in the expander quality. We report the first commissioning of the instrument, its calibration, and performance characterization, together with some preliminary results with the measurement of a 950 mm silicon substrate. The intended application is to characterize the final XFEL mirrors with nanometer accuracy.

Simple, compact, high brightness source for x-ray lithography and x-ray radiography

International Nuclear Information System (INIS)

Hawryluk, A.M.

1986-01-01

A simple, compact, high brightness x-ray source has recently been built. This source utilizes a commercially available, cylindrical geometry electron beam evaporator, which has been modified to enhance the thermal cooling to the anode. Cooling is accomplished by using standard, low-conductivity laboratory water, with an inlet pressure of less than 50 psi, and a flow rate of approx.0.3 gal/min. The anode is an inverted cone geometry for efficient cooling. The x-ray source has a measured sub-millimeter spot size (FWHM). The anode has been operated at 1 KW e-beam power (10 KV, 100 ma). Higher operating levels will be investigated. A variety of different x-ray lines can be obtained by the simple interchange of anodes of different materials. Typical anodes are made from easily machined metals, or materials which are vacuum deposited onto a copper anode. Typically, a few microns of material is sufficient to stop 10 KV electrons without significantly decreasing the thermal conductivity through the anode. The small size and high brightness of this source make it useful for step and repeat exposures over several square centimeter areas, especially in a research laboratory environment. For an aluminum anode, the estimated Al-K x-ray flux at 10 cms from the source is 70 μW/cm 2

High-energy X-ray diffraction studies of disordered materials

International Nuclear Information System (INIS)

Kohara, Shinji; Suzuya, Kentaro

2003-01-01

With the arrival of the latest generation of synchrotron sources and the introduction of advanced insertion devices (wigglers and undulators), the high-energy (E≥50 keV) X-ray diffraction technique has become feasible, leading to new approaches in the quantitative study of the structure of disordered materials. High-energy X-ray diffraction has several advantages: higher resolution in real space due to a wide range of scattering vector Q, smaller correction terms (especially the absorption correction), reduction of truncation errors, the feasibility of running under extreme environments, including high-temperatures and high-pressures, and the ability to make direct comparisons between X-ray and neutron diffraction data. Recently, high-energy X-ray diffraction data have been combined with neutron diffraction data from a pulsed source to provide more detailed and reliable structural information than that hitherto available

Diamond x-ray optics: Transparent, resilient, high-resolution, and wavefront preserving

International Nuclear Information System (INIS)

Shvyd’ko, Yuri; Blank, Vladimir; Terentyev, Sergey

2017-01-01

Diamond features a unique combination of outstanding physical properties perfect for numerous x-ray optics applications, where traditional materials such as silicon fail to perform. In the last two decades, impressive progress has been achieved in synthesizing diamond with high crystalline perfection, in manufacturing efficient, resilient, high-resolution, wavefront-preserving diamond optical components, and in implementing them in cutting-edge x-ray instruments. Diamond optics are essential for tailoring x-rays to the most challenging needs of x-ray research. Furthermore, they are becoming vital for the generation of fully coherent hard x-rays by seeded x-ray free-electron lasers. In this article, we review progress in manufacturing flawless diamond crystal components and their applications in diverse x-ray optical devices, such as x-ray monochromators, beam splitters, high-reflectance backscattering mirrors, lenses, phase plates, diffraction gratings, bent-crystal spectrographs, and windows.

Flash X-ray

International Nuclear Information System (INIS)

Sato, Eiichi

2003-01-01

Generation of quasi-monochromatic X-ray by production of weakly ionized line plasma (flash X-ray), high-speed imaging by the X-ray and high-contrast imaging by the characteristic X-ray absorption are described. The equipment for the X-ray is consisted from the high-voltage power supply and condenser, turbo molecular pump, and plasma X-ray tube. The tube has a long linear anticathode to produce the line plasma and flash X-ray at 20 kA current at maximum. X-ray spectrum is measured by the imaging plate equipped in the computed radiography system after diffracted by a LiF single crystal bender. Cu anticathode generates sharp peaks of K X-ray series. The tissue images are presented for vertebra, rabbit ear and heart, and dog heart by X-ray fluoroscopy with Ce anticathode. Generation of K-orbit characteristic X-ray with extremely low bremsstrahung is to be attempted for medical use. (N.I.)

High power X-ray welding of metal-matrix composites

Energy Technology Data Exchange (ETDEWEB)

Rosenberg, Richard A.; Goeppner, George A.; Noonan, John R.; Farrell, William J.; Ma, Qing

1997-12-01

A method for joining metal-matrix composites (MMCs) by using high power x-rays as a volumetric heat source is provided. The method involves directing an x-ray to the weld line between two adjacent MMCs materials to create an irradiated region or melt zone. The x-rays have a power density greater than about 10{sup 4} watts/cm{sup 2} and provide the volumetric heat required to join the MMC materials. Importantly, the reinforcing material of the metal-matrix composites remains uniformly distributed in the melt zone, and the strength of the MMCs are not diminished. In an alternate embodiment, high power x-rays are used to provide the volumetric heat required to weld metal elements, including metal elements comprised of metal alloys. In an alternate embodiment, high power x-rays are used to provide the volumetric heat required to weld metal elements, including metal elements comprised of metal alloys.

Pair distribution functions of amorphous organic thin films from synchrotron X-ray scattering in transmission mode

Directory of Open Access Journals (Sweden)

Chenyang Shi

2017-09-01

Full Text Available Using high-brilliance high-energy synchrotron X-ray radiation, for the first time the total scattering of a thin organic glass film deposited on a strongly scattering inorganic substrate has been measured in transmission mode. The organic thin film was composed of the weakly scattering pharmaceutical substance indomethacin in the amorphous state. The film was 130 µm thick atop a borosilicate glass substrate of equal thickness. The atomic pair distribution function derived from the thin-film measurement is in excellent agreement with that from bulk measurements. This ability to measure the total scattering of amorphous organic thin films in transmission will enable accurate in situ structural studies for a wide range of materials.

X-ray radiography with highly charged ions

Science.gov (United States)

Marrs, Roscoe E.

2000-01-01

An extremely small (1-250 micron FWHM) beam of slow highly charged ions deexciting on an x-ray production target generates x-ray monochromatic radiation that is passed through a specimen and detected for imaging. The resolution of the x-ray radiograms is improved and such detection is achieved with relatively low dosages of radiation passing through the specimen. An apparatus containing an electron beam ion trap (and modifications thereof) equipped with a focusing column serves as a source of ions that generate radiation projected onto an image detector. Electronic and other detectors are able to detect an increased amount of radiation per pixel than achieved by previous methods and apparati.

X-ray absorption intensity at high-energy region

International Nuclear Information System (INIS)

Fujikawa, Takashi; Kaneko, Katsumi

2012-01-01

We theoretically discuss X-ray absorption intensity in high-energy region far from the deepest core threshold to explain the morphology-dependent mass attenuation coefficient of some carbon systems, carbon nanotubes (CNTs), highly oriented pyrolytic graphite (HOPG) and fullerenes (C 60 ). The present theoretical approach is based on the many-body X-ray absorption theory including the intrinsic losses (shake-up losses). In the high-energy region the absorption coefficient has correction term dependent on the solid state effects given in terms of the polarization part of the screened Coulomb interaction W p . We also discuss the tail of the valence band X-ray absorption intensity. In the carbon systems C 2s contribution has some influence on the attenuation coefficient even in the high energy region at 20 keV.

Plasma instability control toward high fluence, high energy x-ray continuum source

Science.gov (United States)

Poole, Patrick; Kirkwood, Robert; Wilks, Scott; Blue, Brent

2017-10-01

X-ray source development at Omega and NIF seeks to produce powerful radiation with high conversion efficiency for material effects studies in extreme fluence environments. While current K-shell emission sources can achieve tens of kJ on NIF up to 22 keV, the conversion efficiency drops rapidly for higher Z K-alpha energies. Pulsed power devices are efficient generators of MeV bremsstrahlung x-rays but are unable to produce lower energy photons in isolation, and so a capability gap exists for high fluence x-rays in the 30 - 100 keV range. A continuum source under development utilizes instabilities like Stimulated Raman Scattering (SRS) to generate plasma waves that accelerate electrons into high-Z converter walls. Optimizing instabilities using existing knowledge on their elimination will allow sufficiently hot and high yield electron distributions to create a superior bremsstrahlung x-ray source. An Omega experiment has been performed to investigate the optimization of SRS and high energy x-rays using Au hohlraums with parylene inner lining and foam fills, producing 10× greater x-ray yield at 50 keV than conventional direct drive experiments on the facility. Experiment and simulation details on this campaign will be presented. This work was performed under the auspices of the US DoE by LLNL under Contract No. DE-AC52-07NA27344.

Development of high resolution x-ray CT technique for irradiated fuel assembly

Energy Technology Data Exchange (ETDEWEB)

Ishimi, Akihiro; Katsuyama, Kozo; Maeda, Koji; Asaga, Takeo [Japan Atomic Energy Agency, Oarai Research and Development Center, Oarai, Ibaraki (Japan)

2012-03-15

High X-ray CT technique was developed to observe the irradiation performance of FBR fuel assembly and MOX fuel. In this technique, the high energy X-ray pulse (12MeV) was used synchronizing detection system with the X-ray pulse to reduce the effect of the gamma ray emissions from the irradiated fuel assembly. In this study, this technique was upgraded to obtain high resolution X-ray CT image. In this upgrading, the collimator which had slit width of 0.1 mm and X-ray detector of a highly sensitive silicon semiconductor detector (100 channels) was introduced in the X-ray CT system. As a result of these developments, high resolution X-ray CT images could be obtained on the transverse cross section of irradiated fuel assembly. (author)

Final Report - X-ray Studies of Highly Correlated Systems

Energy Technology Data Exchange (ETDEWEB)

Burns, Clement [Western Michigan Univ., Kalamazoo MI (United States)

2017-11-27

The overall goal of the research was to improve the capabilities of x-ray synchrotron instrumentation to enable cutting-edge research in condensed matter physics. The main goal of the current grant cycle was to find a method to measure the polarization of the scattered x-ray in resonant inelastic x-ray scattering. To do this, we developed a polarization analysis apparatus using a thin, toroidally bent single crystal, which could be set to reflect one or the other of the two polarization components in the scattered x-ray beam. Resonant x-ray scattering measurements were also carried out on interfaces and the charge density wave in high temperature superconducting materials.

Byzantine Parthenogenesis as Hierotopy of Fluid Brilliance

DEFF Research Database (Denmark)

Isar, Nicoletta

2014-01-01

Images Borne on Dewy Lightning Byzantine παρθένογένεσις as Hierotopy of Fluid Brilliance......Images Borne on Dewy Lightning Byzantine παρθένογένεσις as Hierotopy of Fluid Brilliance...

High resolution projection X-ray microscope equipped with fluorescent X-ray analyzer and its applications

International Nuclear Information System (INIS)

Minami, K; Saito, Y; Kai, H; Shirota, K; Yada, K

2009-01-01

We have newly developed an open type fine-focus X-ray tube 'TX-510' to realize a spatial resolution of 50nm and to radiate low energy characteristic X-rays for giving high absorption contrast to images of microscopic organisms. The 'TX-510' employs a ZrO/W(100) Schottky emitter and an 'In-Lens Field Emission Gun'. The key points of the improvements are (1) reduced spherical aberration coefficient of magnetic objective lens, (2) easy and accurate focusing, (3) newly designed astigmatism compensator, (4) segmented thin film target for interchanging the target materials by electron beam shift and (5) fluorescent X-ray analysis system.

[High-Performance Active Pixel X-Ray Sensors for X-Ray Astronomy

Science.gov (United States)

Bautz, Mark; Suntharalingam, Vyshnavi

2005-01-01

The subject grants support development of High-Performance Active Pixel Sensors for X-ray Astronomy at the Massachusetts Institute of Technology (MIT) Center for Space Research and at MIT's Lincoln Laboratory. This memo reports our progress in the second year of the project, from April, 2004 through the present.

Design study on a high brilliance lattice of the PF storage ring

International Nuclear Information System (INIS)

Katoh, M.; Araki, A.; Kobayashi, Y.; Hori, Y.

1994-01-01

A high brilliance lattice of the PF storage ring is proposed. A small beam emittance of 27 nm-rad (about one fifth of the present value) can be achieved by doubling the number of the quadrupoles in the FODO cells. This emittance reduction will result in ten times brighter synchrotron light from the existing insertion devices. The problems incidental to the low emittance lattice, the small dynamic aperture and the short Touschek lifetime, will be discussed. (author)

DETECTING RELATIVISTIC X-RAY JETS IN HIGH-REDSHIFT QUASARS

Energy Technology Data Exchange (ETDEWEB)

McKeough, Kathryn [Department of Statistics, Harvard University, Cambridge, MA 02138 (United States); Siemiginowska, Aneta; Kashyap, Vinay L.; Lee, N. P.; Harris, D. E.; Schwartz, D. A. [Harvard-Smithsonian Center for Astrophysics, 60 Garden Street, Cambridge, MA 02138 (United States); Cheung, C. C. [Space Science Division, Naval Research Laboratory, Washington, DC 20375-5352 (United States); Stawarz, Łukasz [Astronomical Observatory, Jagiellonian University, ul. Orla 171, 30-244, Kraków (Poland); Stein, Nathan [Department of Statistics, The Wharton School, University of Pennsylvania, 400 Jon M. Huntsman Hall, 3730 Walnut Street, Philadelphia, PA 19104-6340 (United States); Stampoulis, Vasileios; Dyk, David A. van [Statistics Section, Imperial College London, Huxley Building, South Kensington Campus, London SW7 (United Kingdom); Wardle, J. F. C. [Department of Physics, MS 057, Brandeis University, Waltham, MA 02454 (United States); Donato, Davide [CRESST and Astroparticle Physics Laboratory NASA/GSFC, Greenbelt, MD 20771 (United States); Maraschi, Laura; Tavecchio, Fabrizio, E-mail: kathrynmckeough@g.harvard.edu [INAF Osservatorio Astronomico di Brera, via Brera 28, I-20124, Milano (Italy)

2016-12-10

We analyze Chandra X-ray images of a sample of 11 quasars that are known to contain kiloparsec scale radio jets. The sample consists of five high-redshift ( z  ≥ 3.6) flat-spectrum radio quasars, and six intermediate redshift (2.1 <  z  < 2.9) quasars. The data set includes four sources with integrated steep radio spectra and seven with flat radio spectra. A total of 25 radio jet features are present in this sample. We apply a Bayesian multi-scale image reconstruction method to detect and measure the X-ray emission from the jets. We compute deviations from a baseline model that does not include the jet, and compare observed X-ray images with those computed with simulated images where no jet features exist. This allows us to compute p -value upper bounds on the significance that an X-ray jet is detected in a pre-determined region of interest. We detected 12 of the features unambiguously, and an additional six marginally. We also find residual emission in the cores of three quasars and in the background of one quasar that suggest the existence of unresolved X-ray jets. The dependence of the X-ray to radio luminosity ratio on redshift is a potential diagnostic of the emission mechanism, since the inverse Compton scattering of cosmic microwave background photons (IC/CMB) is thought to be redshift dependent, whereas in synchrotron models no clear redshift dependence is expected. We find that the high-redshift jets have X-ray to radio flux ratios that are marginally inconsistent with those from lower redshifts, suggesting that either the X-ray emissions are due to the IC/CMB rather than the synchrotron process, or that high-redshift jets are qualitatively different.

Effective high voltage at X-ray tube in hard X-ray chest imaging

International Nuclear Information System (INIS)

Klein, J.

1987-01-01

The FRG standard TGL 36 661 (March 1980) for synoptical chest pictures of large size in adults specifies the 120 kV voltage at the X-ray tube together with maximal, 100% use of the capacity of the tube (hard picture, short exposure time). By means of circular recording and by measuring the high voltage at the X-ray tube it was quantitatively shown that the effective voltage during exposure is (according to the exposure time and the attenuation phase of the generator) always lower than the set-up voltage of 120 kV. This phenomenon is the more marked the shorter the actual exposure time in comparison with the attenuation phase of the generator. The typical characteristic of a hard X-ray chest picture is thus not given only by the setting-up of voltage. The impact of the reduction in voltage is thus quantitatively shown also from the aspect of the radiation burden for the patient. (author). 7 figs., 8 refs

Portable X-ray fluorescence analyzer of high sensitivity using X-ray tube excitation

International Nuclear Information System (INIS)

Vatai, E.; Ando, L.

1982-01-01

A review of the three main methods of X-ray fluorescence analysis and their problems is given. The attainable accuracy and effectiveness of each method are discussed. The main properties of portable X-ray analyzers required by the industry are described. The results and experiences of R and D activities in ATOMKI (Debrecen, Hungary) for developing portable X-ray analyzers are presented. The only way for increasing the accuracy and decreasing the measuring time is the application of X-ray tube excitation instead of radioactive sources. The new ATOMKI equipment presently under construction and patenting uses X-ray tube excitation; it will increase the accuracy of concentration determination by one order of magnitude. (D.Gy.)

High energy resolution off-resonant X-ray spectroscopy

Energy Technology Data Exchange (ETDEWEB)

Wojciech, Blachucki [Univ. of Fribourg (Switzerland). Dept. of Physics

2015-10-16

This work treats of the high energy resolution off-resonant X-ray spectroscopy (HEROS) method of determining the density of unoccupied electronic states in the vicinity of the absorption edge. HEROS is an alternative to the existing X-ray absorption spectroscopy (XAS) methods and opens the way for new studies not achievable before.

Generation of x-ray radiation in a storage ring by a superconductive cold-bore in-vacuum undulator

Directory of Open Access Journals (Sweden)

S. Casalbuoni

2006-01-01

Full Text Available The first beam measurements with a cold-bore superconducting in-vacuum undulator in a storage ring are reported. Undulators are x-ray generators in light sources. The physical limitations of these devices limit the intensity and the brilliance of the x-ray beam. At present the undulators are made from permanent magnets. It was shown in earlier papers that at low electron beam intensities superconductive wires in the vacuum beam pipe can overcome the limitations inherent to permanent magnet undulators. It was argued that the use of these novel devices in light sources with high beam currents may be limited by the extreme anomalous skin effect regime in Cu at 4.2 K, which has so far undergone very little investigation, and the power deposited by the infrared part of the synchrotron radiation. The purpose of this paper is to present measurements of these effects at the synchrotron light source ANKA with stored currents up to 200 mA.

Evaluation on correction factor for in-line X-ray phase contrast computed tomography

Energy Technology Data Exchange (ETDEWEB)

Jin, Mingli; Huang, Zhifeng; Zhang, Li; Zhang, Ran [Tsinghua Univ., Beijing (China). Dept. of Engineering Physics; Ministry of Education, Beijing (China). Key Laboratory of Particle and Radiation Imaging; Yin, Hongxia; Liu, Yunfu; Wang, Zhenchang [Capital Medical Univ., Beijing (China). Medical Imaging Center; Xiao, Tiqiao [Chinese Academy of Sciences, Shanghai (China). Shanghai Inst. of Applied Physics

2011-07-01

X-ray in-line phase contrast computed tomography (CT) is an effective nondestructive tool, providing 3D distribution of the refractive index of weakly absorbing low-Z object with high resolution and image contrast, especially with high-brilliance third-generation synchrotron radiation sources. Modified Bronnikov's algorithm (MBA), one of the in-line phase contrast CT reconstruction algorithms, can reconstruct the refractive index distribution of a pure phase object with a single computed tomographic data set. The key idea of the MBA is to use a correction factor in the filter function to stabilize the behavior at low frequencies. In this paper, we evaluate the influences of the correction factor to the final reconstruction results of the absorption-phase-mixed objects with analytical simulation and actual experiments. The limitations of the MBA are discussed finally. (orig.)

Micro controller application as x-ray machine's high voltage controller

International Nuclear Information System (INIS)

Wiranto Budi Santoso; Beny Syawaludin

2010-01-01

The micro controller application as x-ray machine's high voltage controller has been carried out. The purpose of this micro controller application is to give an accurate high voltage supply to the x-ray tube so that the x ray machine could produce the result as expected. The micro controller based X-ray machine's high voltage controller receives an input voltage from the keypad. This input value is displayed in the LCD (Liquid Crystal Display) screen. Then micro controller uses this input data to drive the stepper motor. The stepper motor adjusts the high voltage auto transformer's output according to the input value. The micro controller is programmed using BASCOM-B051 compiler. The test results show that the stepper motor could rotate according to an input value. (author)

Review - X-ray diffraction measurements in high magnetic fields and at high temperatures

Directory of Open Access Journals (Sweden)

Yoshifuru Mitsui, Keiichi Koyama and Kazuo Watanabe

2009-01-01

Full Text Available A system was developed measuring x-ray powder diffraction in high magnetic fields up to 5 T and at temperatures from 283 to 473 K. The stability of the temperature is within 1 K over 6 h. In order to examine the ability of the system, the high-field x-ray diffraction measurements were carried out for Si and a Ni-based ferromagnetic shape-memory alloy. The results show that the x-ray powder diffraction measurements in high magnetic fields and at high temperatures are useful for materials research.

Brilliance and flux reduction in imperfect inclined crystals

International Nuclear Information System (INIS)

Lee, W.K.; Blasdell, R.C.; Fernandez, P.B.; Macrander, A.T.; Mills, D.M.

1996-01-01

The inclined crystal geometry has been suggested as a method of reducing the surface absorbed power density of high-heat-load monochromators for third-generation synchrotron radiation sources. Computer simulations have shown that if the crystals are perfectly aligned and have no strains then the diffraction properties of a pair of inclined crystals are very similar to a pair of conventional flat crystals with only subtle effects differentiating the two configurations. However, if the crystals are strained, these subtle differences in the behavior of inclined crystals can result in large beam divergences causing brilliance and flux losses. This manuscript elaborates on these issues and estimates potential brilliance and flux losses from strained inclined crystals at the APS

Temporally coherent x-ray laser with the high order harmonic light

International Nuclear Information System (INIS)

Hasegawa, Noboru; Kawachi, Tetsuya; Kishimoto, Maki; Sukegawa, Kouta; Tanaka, Momoko; Ochi, Yoshihiro; Nishikino, Masaharu; Kawazome, Hayato; Nagashima, Keisuke

2005-01-01

We obtained the neon-like manganese x-ray laser with the injection of the high order harmonic light as the seed x-ray at the wavelength of 26.9 nm for the purpose of generation of the temporally coherent x-ray laser. The x-ray amplifier, which has quite narrow spectral width, selected and amplified the temporally coherent mode of the harmonic light. The temporal coherence of the mode selected harmonic light was nearly transform limited pulse, and the obtained x-ray laser with the seed x-ray expected to be nearly temporally coherent x-ray. (author)

High temperature GaAs X-ray detectors

Science.gov (United States)

Lioliou, G.; Whitaker, M. D. C.; Barnett, A. M.

2017-12-01

Two GaAs p+-i-n+ mesa X-ray photodiodes were characterized for their electrical and photon counting X-ray spectroscopic performance over the temperature range of 100 °C to -20 °C. The devices had 10 μm thick i layers with different diameters: 200 μm (D1) and 400 μm (D2). The electrical characterization included dark current and capacitance measurements at internal electric field strengths of up to 50 kV/cm. The determined properties of the two devices were compared with previously reported results that were made with a view to informing the future development of photon counting X-ray spectrometers for harsh environments, e.g., X-ray fluorescence spectroscopy of planetary surfaces in high temperature environments. The best energy resolution obtained (Full Width at Half Maximum at 5.9 keV) decreased from 2.00 keV at 100 °C to 0.66 keV at -20 °C for the spectrometer with D1, and from 2.71 keV at 100 °C to 0.71 keV at -20 °C for the spectrometer with D2. Dielectric noise was found to be the dominant source of noise in the spectra, apart from at high temperatures and long shaping times, where the main source of photopeak broadening was found to be the white parallel noise.

A measurement-based X-ray source model characterization for CT dosimetry computations.

Science.gov (United States)

Sommerville, Mitchell; Poirier, Yannick; Tambasco, Mauro

2015-11-08

The purpose of this study was to show that the nominal peak tube voltage potential (kVp) and measured half-value layer (HVL) can be used to generate energy spectra and fluence profiles for characterizing a computed tomography (CT) X-ray source, and to validate the source model and an in-house kV X-ray dose computation algorithm (kVDoseCalc) for computing machine- and patient-specific CT dose. Spatial variation of the X-ray source spectra of a Philips Brilliance and a GE Optima Big Bore CT scanner were found by measuring the HVL along the direction of the internal bow-tie filter axes. Third-party software, Spektr, and the nominal kVp settings were used to generate the energy spectra. Beam fluence was calculated by dividing the integral product of the spectra and the in-air NIST mass-energy attenuation coefficients by in-air dose measurements along the filter axis. The authors found the optimal number of photons to seed in kVDoseCalc to achieve dose convergence. The Philips Brilliance beams were modeled for 90, 120, and 140 kVp tube settings. The GE Optima beams were modeled for 80, 100, 120, and 140 kVp tube settings. Relative doses measured using a Capintec Farmer-type ionization chamber (0.65 cc) placed in a cylindrical polymethyl methacrylate (PMMA) phantom and irradiated by the Philips Brilliance, were compared to those computed with kVDoseCalc. Relative doses in an anthropomorphic thorax phantom (E2E SBRT Phantom) irradiated by the GE Optima were measured using a (0.015 cc) PTW Freiburg ionization chamber and compared to computations from kVDoseCalc. The number of photons required to reduce the average statistical uncertainty in dose to measurement over all 12 PMMA phantom positions was found to be 1.44%, 1.47%, and 1.41% for 90, 120, and 140 kVp, respectively. The maximum percent difference between calculation and measurement for all energies, measurement positions, and phantoms was less than 3.50%. Thirty-five out of a total of 36 simulation conditions were

Gas scintillation glass GEM detector for high-resolution X-ray imaging and CT

Energy Technology Data Exchange (ETDEWEB)

Fujiwara, T., E-mail: fujiwara-t@aist.go.jp [Research Institute for Measurement and Analytical Instrumentation, National Institute of Advanced Industrial Science and Technology (AIST), Tsukuba, Ibaraki 305-8568 (Japan); Mitsuya, Y. [Nuclear Professional School, The University of Tokyo, Tokai, Naka, Ibaraki 319-1188 (Japan); Fushie, T. [Radiment Lab. Inc., Setagaya, Tokyo 156-0044 (Japan); Murata, K.; Kawamura, A.; Koishikawa, A. [XIT Co., Naruse, Machida, Tokyo 194-0045 (Japan); Toyokawa, H. [Research Institute for Measurement and Analytical Instrumentation, National Institute of Advanced Industrial Science and Technology (AIST), Tsukuba, Ibaraki 305-8568 (Japan); Takahashi, H. [Institute of Engineering Innovation, School of Engineering, The University of Tokyo, Bunkyo, Tokyo 113-8654 (Japan)

2017-04-01

A high-spatial-resolution X-ray-imaging gaseous detector has been developed with a single high-gas-gain glass gas electron multiplier (G-GEM), scintillation gas, and optical camera. High-resolution X-ray imaging of soft elements is performed with a spatial resolution of 281 µm rms and an effective area of 100×100 mm. In addition, high-resolution X-ray 3D computed tomography (CT) is successfully demonstrated with the gaseous detector. It shows high sensitivity to low-energy X-rays, which results in high-contrast radiographs of objects containing elements with low atomic numbers. In addition, the high yield of scintillation light enables fast X-ray imaging, which is an advantage for constructing CT images with low-energy X-rays.

Nanoscopium: a Scanning Hard X-ray Nanoprobe Beamline at Synchrotron Soleil

Science.gov (United States)

Somogyi, A.; Polack, F.; Moreno, T.

2010-06-01

Nanoscopium is the single scanning hard X-ray nano-probe beamline planned at SOLEIL. This ˜155 m long beamline will fully exploit the high brilliance and coherence characteristics of the X-ray beam both for diffraction limited focusing and for contrast formation. It will offer the most advanced imaging techniques in multimodal mode and will be a research tool for a wide user community working in the fields of earth-, environmental-, and life-sciences. The different μ-μnano-probe techniques offered by the beamline will permit elemental mapping at trace (ppm) levels (scanning XRF), speciation mapping (XANES), phase gradient mapping (scanning differential phase contrast), and density-contrast based imaging of internal structures (coherent diffraction imaging) in the 30 nm to 1 μm spatial resolution range, also in "in situ conditions". Nanoscopium will cover the 5-20 keV energy range. The stability of the nanobeam will be ensured by horizontally reflecting beamline optics (a sagitally and a tangentially pre-focusing mirror, horizontally reflecting monochromators) in front of the overfilled secondary source. Trade-off between high energy resolution (ΔE/E˜10-4) and high flux (1011 ph/s with ΔE/E˜10-2) will be achieved by two interchangeable monochromators (a double crystal and a double multilayer one). KB mirror and FZP lenses will be used as focusing devices. The beamline is in the design and construction phase. It is foreseen to be open for users at the beginning of 2013.

Novel X-ray imaging diagnostics of high energy nanosecond pulse accelerators

International Nuclear Information System (INIS)

Smith, Graham W.; Gallegos, Roque Rosauro; Hohlfelder, Robert James; Beutler, David Eric; Dudley, John; Seymour, Calvin L.G.; Bell, John D.

2004-01-01

Pioneering x-ray imaging has been undertaken on a number of AWE's and Sandia National Laboratories radiation effects x-ray simulators. These simulators typically yield a single very short (<50ns) pulse of high-energy (MeV endpoint energy bremsstrahlung) x-ray radiation with doses in the kilorad (krad(Si)) region. X-ray source targets vary in size from 2 to 25cm diameter, dependent upon the particular simulator. Electronic imaging of the source x-ray emission under dynamic conditions yields valuable information upon how the simulator is performing. The resultant images are of interest to the simulator designer who may configure new x-ray source converter targets and diode designs. The images can provide quantitative information about machine performance during radiation effects testing of components under active conditions. The effects testing program is a valuable interface for validation of high performance computer codes and models for the radiation effects community. A novel high-energy x-ray imaging spectrometer is described whereby the spectral energy (0.1 to 2.5MeV) profile may be discerned from the digitally recorded and viewable images via a pinhole/scintillator/CCD imaging system and knowledge of the filtration parameters. Unique images, analysis and a preliminary evaluation of the capability of the spectrometer are presented. Further, a novel time resolved imaging system is described that captures a sequence of high spatial resolution temporal images, with zero interframe time, in the nanosecond timeframe, of our source x-rays.

High spatial resolution soft-x-ray microscopy

Energy Technology Data Exchange (ETDEWEB)

Meyer-Ilse, W.; Medecki, H.; Brown, J.T. [Ernest Orlando Lawrence Berkeley National Lab., CA (United States)] [and others

1997-04-01

A new soft x-ray microscope (XM-1) with high spatial resolution has been constructed by the Center for X-ray Optics. It uses bending magnet radiation from beamline 6.1 at the Advanced Light Source, and is used in a variety of projects and applications in the life and physical sciences. Most of these projects are ongoing. The instrument uses zone plate lenses and achieves a resolution of 43 nm, measured over 10% to 90% intensity with a knife edge test sample. X-ray microscopy permits the imaging of relatively thick samples, up to 10 {mu}m thick, in water. XM-1 has an easy to use interface, that utilizes visible light microscopy to precisely position and focus the specimen. The authors describe applications of this device in the biological sciences, as well as in studying industrial applications including structured polymer samples.

Laser-powered dielectric-structures for the production of high-brightness electron and x-ray beams

Science.gov (United States)

Travish, Gil; Yoder, Rodney B.

2011-05-01

Laser powered accelerators have been under intensive study for the past decade due to their promise of high gradients and leveraging of rapid technological progress in photonics. Of the various acceleration schemes under examination, those based on dielectric structures may enable the production of relativistic electron beams in breadbox sized systems. When combined with undulators having optical-wavelength periods, these systems could produce high brilliance x-rays which find application in, for instance, medical and industrial imaging. These beams also may open the way for table-top atto-second sciences. Development and testing of these dielectric structures faces a number of challenges including complex beam dynamics, new demands on lasers and optical coupling, beam injection schemes, and fabrication. We describe one approach being pursued at UCLA-the Micro Accelerator Platform (MAP). A structure similar to the MAP has also been designed which produces periodic deflections and acts as an undulator for radiation production, and the prospects for this device will be considered. The lessons learned from the multi-year effort to realize these devices will be presented. Challenges remain with acceleration of sub-relativistic beams, focusing, beam phase stability and extension of these devices to higher beam energies. Our progress in addressing these hurdles will be summarized. Finally, the demands on laser technology and optical coupling will be detailed.

X-Rays from NGC 3256: High-Energy Emission in Starburst Galaxies and Their Contribution to the Cosmic X-Ray Background

International Nuclear Information System (INIS)

Moran, Edward C.; Lehnert, Matthew D.; Helfand, David J.

1999-01-01

The infrared-luminous galaxy NGC 3256 is a classic example of a merger-induced nuclear starburst system. We find here that it is the most X-ray-luminous star-forming galaxy yet detected (L 0.5-10keV =1.6x10 42 ergs s-1). Long-slit optical spectroscopy and a deep, high-resolution ROSAT X-ray image show that the starburst is driving a ''superwind'' which accounts for ∼20% of the observed soft X-ray emission. Analysis of X-ray spectral data from ASCA indicates this gas has a characteristic temperature of kT≅0.3 keV. Our model for the broadband X-ray emission of NGC 3256 contains two additional components: a warm thermal plasma (kT≅0.8 keV) associated with the central starburst, and a hard power-law component with an energy index of α X ≅0.7. We discuss the energy budget for the two thermal plasmas and find that the input of mechanical energy from the starburst is more than sufficient to sustain the observed level of emission. We also examine possible origins for the power-law component, concluding that neither a buried AGN nor the expected population of high-mass X-ray binaries can account for this emission. Inverse Compton scattering, involving the galaxy's copious flux of infrared photons and the relativistic electrons produced by supernovae, is likely to make a substantial contribution to the hard X-ray flux. Such a model is consistent with the observed radio and IR fluxes and the radio and X-ray spectral indices. We explore the role of X-ray-luminous starbursts in the production of the cosmic X-ray background radiation. The number counts and spectral index distribution of the faint radio source population, thought to be dominated by star-forming galaxies, suggest that a significant fraction of the hard X-ray background could arise from starbursts at moderate redshift. (c) (c) 1999. The American Astronomical Society

High-resolution accelerator alignment using x-ray optics

Directory of Open Access Journals (Sweden)

Bingxin Yang

2006-03-01

Full Text Available We propose a novel alignment technique utilizing the x-ray beam of an undulator in conjunction with pinholes and position-sensitive detectors for positioning components of the accelerator, undulator, and beam line in an x-ray free-electron laser. Two retractable pinholes at each end of the undulator define a stable and reproducible x-ray beam axis (XBA. Targets are precisely positioned on the XBA using a pinhole camera technique. Position-sensitive detectors responding to both x-ray and electron beams enable direct transfer of the position setting from the XBA to the electron beam. This system has the potential to deliver superior alignment accuracy (1–3   μm for target pinholes in the transverse directions over a long distance (200 m or longer. It can be used to define the beam axis of the electron-beam–based alignment, enabling high reproducibility of the latter. This x-ray–based concept should complement the electron-beam–based alignment and the existing survey methods to raise the alignment accuracy of long accelerators to an unprecedented level. Further improvement of the transverse accuracy using x-ray zone plates will be discussed. We also propose a concurrent measurement scheme during accelerator operation to allow real-time feedback for transverse position correction.

High-resolution measurements of x rays from ion-atom collisions

International Nuclear Information System (INIS)

Knudson, A.R.

1974-01-01

High resolution measurements of K x-ray spectra produced by ion-atom collisions at MeV energies are presented. These measurements indicate that a distribution of L-shell vacancies accompanies K-shell excitation. The variation of these spectra as a function of incident ion energy and atomic number is discussed. Difficulties in the analysis of these spectra due to rearrangement of vacancies between the time of the collision and the time of x-ray emission are considered. The use of high resolution x-ray measurements to obtain information on projectile ion vacancy configurations is demonstrated by data for Ar ions in KCl. X-ray spectra from Al projectiles in a variety of targets were measured and the effect of target composition on these spectra is discussed

Active x-ray optics for high resolution space telescopes

Science.gov (United States)

Doel, Peter; Atkins, Carolyn; Brooks, D.; Feldman, Charlotte; Willingale, Richard; Button, Tim; Rodriguez Sanmartin, Daniel; Meggs, Carl; James, Ady; Willis, Graham; Smith, Andy

2017-11-01

The Smart X-ray Optics (SXO) Basic Technology project started in April 2006 and will end in October 2010. The aim is to develop new technologies in the field of X-ray focusing, in particular the application of active and adaptive optics. While very major advances have been made in active/adaptive astronomical optics for visible light, little was previously achieved for X-ray optics where the technological challenges differ because of the much shorter wavelengths involved. The field of X-ray astronomy has been characterized by the development and launch of ever larger observatories with the culmination in the European Space Agency's XMM-Newton and NASA's Chandra missions which are currently operational. XMM-Newton uses a multi-nested structure to provide modest angular resolution ( 10 arcsec) but large effective area, while Chandra sacrifices effective area to achieve the optical stability necessary to provide sub-arc second resolution. Currently the European Space Agency (ESA) is engaged in studies of the next generation of X-ray space observatories, with the aim of producing telescopes with increased sensitivity and resolution. To achieve these aims several telescopes have been proposed, for example ESA and NASA's combined International X-ray Observatory (IXO), aimed at spectroscopy, and NASA's Generation-X. In the field of X-ray astronomy sub 0.2 arcsecond resolution with high efficiency would be very exciting. Such resolution is unlikely to be achieved by anything other than an active system. The benefits of a such a high resolution would be important for a range of astrophysics subjects, for example the potential angular resolution offered by active X-ray optics could provide unprecedented structural imaging detail of the Solar Wind bowshock interaction of comets, planets and similar objects and auroral phenomena throughout the Solar system using an observing platform in low Earth orbit. A major aim of the SXO project was to investigate the production of thin

Copper L X-ray spectra measured by a high resolution ion-induced X-ray spectrometer

Energy Technology Data Exchange (ETDEWEB)

Takahashi, Ryohei; Hamaguchi, Dai; Kageyama, Hiroyoshi [Kyoto Inst. of Tech. (Japan); and others

1997-03-01

High resolution L X-ray emission spectra of Cu have been measured by 0.75 MeV/u H, He, and F, 0.73 MeV/u Ar, 0.64 MeV/u Si, and 0.073 MeV/u Si ion impacts with a crystal spectrometer. The X-ray transition energies in the Cu target for L{iota}, L{eta}, L{alpha}{sub 1,2}, L{beta}{sub 1}, and L{beta}{sub 3,4} diagram lines induced by light ion impacts are determined, which are in good agreement with those given in the reference. The difference in L X-ray emission spectra produced by H, He, F, Si, and Ar ions are considered and the L{alpha}{sub 1,2} and L{beta}{sub 1} emission spectra are compared with the calculated ones based on the multiconfiguration Dirac-Fock method. (author)

Production of hollow atoms by high brightness x-ray sources and its applications

International Nuclear Information System (INIS)

Moribayashi, Kengo

2004-01-01

We study x-ray emissions from the (multi-)inner-shell states and hollow atoms of Si ions excited by high intensity x-ray sources. It is found that the x-ray number from multi-inner-shell excited states (1s 2 2s 2 2p k 3s 2 3p 2 , k=1-4) and hollow atoms (1s 2 2s 2 3p 2 ) is affected greatly by the high intensity short-pulse x-rays and little by weak intensity post-long pulse x-rays. The ratio of the x-ray intensities from hollow atoms to those from the multi-inner-shell excited states becomes almost independent of the pulses and dependent on the intensities of x-ray sources. This ratio may be used for the measurement of intensities of high intensity short pulse x-ray sources. (author)

A MEMS-based high frequency x-ray chopper

Energy Technology Data Exchange (ETDEWEB)

Siria, A; Schwartz, W; Chevrier, J [Institut Neel, CNRS-Universite Joseph Fourier Grenoble, BP 166, F-38042 Grenoble Cedex 9 (France); Dhez, O; Comin, F [ESRF, 6 rue Jules Horowitz, F-38043 Grenoble Cedex 9 (France); Torricelli, G [Department of Physics and Astronomy, University of Leicester, University Road, Leicester LE1 7RH (United Kingdom)

2009-04-29

Time-resolved x-ray experiments require intensity modulation at high frequencies (advanced rotating choppers have nowadays reached the kHz range). We here demonstrate that a silicon microlever oscillating at 13 kHz with nanometric amplitude can be used as a high frequency x-ray chopper. We claim that using micro-and nanoelectromechanical systems (MEMS and NEMS), it will be possible to achieve higher frequencies in excess of hundreds of megahertz. Working at such a frequency can open a wealth of possibilities in chemistry, biology and physics time-resolved experiments.

High-brightness beamline for x-ray spectroscopy at the ALS

Energy Technology Data Exchange (ETDEWEB)

Perera, R.C.C.; Jones, G. [Ernest Orlando Lawrence Berkeley National Lab., CA (United States); Lindle, D.W. [Univ. of Nevada, Las Vegas, NV (United States)

1997-04-01

Beamline 9.3.1 at the Advanced Light Source (ALS) is a windowless beamline, covering the 1-6 keV photon-energy range, designed to achieve the goals of high energy resolution, high flux, and high brightness at the sample. When completed later this year, it will be the first ALS monochromatic hard x-ray beamline, and its brightness will be an order of magnitude higher than presently available in this energy range. In addition, it will provide flux and resolution comparable to any other beamline now in operation. To achieve these goals, two technical improvements, relative to existing x-ray beamlines, were incorporated. First, a somewhat novel optical design for x-rays, in which matched toroidal mirrors are positioned before and after the double-crystal monochromator, was adopted. This configuration allows for high resolution by passing a collimated beam through the monochromator, and for high brightness by focusing the ALS source on the sample with unit magnification. Second, a new {open_quotes}Cowan type{close_quotes} double-crystal monochromator based on the design used at NSLS beamline X-24A was developed. The measured mechanical precision of this new monochromator shows significant improvement over existing designs, without using positional feedback available with piezoelectric devices. Such precision is essential because of the high brightness of the radiation and the long distance (12 m) from the source (sample) to the collimating (focusing) mirror. This combination of features will provide a bright, high resolution, and stable x-ray beam for use in the x-ray spectroscopy program at the ALS.

Inelastic X-ray scattering experiments at extreme conditions: high temperatures and high pressures

Directory of Open Access Journals (Sweden)

S.Hosokawa

2008-03-01

Full Text Available In this article, we review the present status of experimental techniques under extreme conditions of high temperature and high pressure used for inelastic X-ray scattering (IXS experiments of liquid metals, semiconductors, molten salts, molecular liquids, and supercritical water and methanol. For high temperature experiments, some types of single-crystal sapphire cells were designed depending on the temperature of interest and the sample thickness for the X-ray transmission. Single-crystal diamond X-ray windows attached to the externally heated high-pressure vessel were used for the IXS experiment of supercritical water and methanol. Some typical experimental results are also given, and the perspective of IXS technique under extreme conditions is discussed.

Multilayer optics for x-ray analysis: design - fabrication - application

International Nuclear Information System (INIS)

Dietsch, R.; Holz, Th.; Bruegemann, L.

2002-01-01

Full text: The use of multilayer optics induced a decisive extension of opportunities in laboratory based X-ray analysis. With the growing number of different applications, more and more dedicated X-ray optics are required, optimized for the spectral range they are intended to be used for. Both the characteristic of the used X-ray source and the design of the multilayer optics finally define the performance of the conditioned incident beam for the application. In any case, qualified spacer and absorber materials have to be selected for the deposition of the multilayer in respect to the designated X-ray wavelength. X-ray optical devices based on uniform multilayers have the advantage of a wide acceptance angle but show chromatic aberrations. This effect can be avoided by synthesizing a multilayer with a lateral thickness gradient. The gradient ensures that any beam of a certain wavelength emitted from an infinite narrow X-ray source impinging the multilayer optics fulfills the Bragg condition. Three different types of curvature of laterally graded multilayer mirrors are used for X-ray analysis experiments: parabolic, elliptic and planar, which result in parallel, focusing and divergent beam conditions, respectively. Furthermore, the X-ray beam characteristics: intensity, monochromasy, divergence, beam width and brilliance can be additionally conditioned by combining one multilayer optics with either a different optic and/or with a crystal monochromator. The deposition of nanometer-multilayers, used as X-ray optical components, result in extraordinary requirements of the deposition process concerning precision, reproducibility and long term stability. Across a stack of more than 150 individual layers with thicknesses in the range between 1 to 10 nm, a variation of single layer thickness considerably lower than σ D = 0.1 nm and an interface roughness below σ R = 0.25 nm have to be achieved. Thickness homogeneity Δd/d -8 have to be guaranteed across macroscopic

High energy X-ray observations of COS-B gamma-ray sources from OSO-8

Science.gov (United States)

Dolan, J. F.; Crannell, C. J.; Dennis, B. R.; Frost, K. J.; Orwig, L. E.; Caraveo, P. A.

1985-01-01

During the three years between satellite launch in June 1975 and turn-off in October 1978, the high energy X-ray spectrometer on board OSO-8 observed nearly all of the COS-B gamma-ray source positions given in the 2CG catalog (Swanenburg et al., 1981). An X-ray source was detected at energies above 20 keV at the 6-sigma level of significance in the gamma-ray error box containing 2CG342 - 02 and at the 3-sigma level of significance in the error boxes containing 2CG065 + 00, 2CG195 + 04, and 2CG311 - 01. No definite association between the X-ray and gamma-ray sources can be made from these data alone. Upper limits are given for the 2CG sources from which no X-ray flux was detected above 20 keV.

Ultraprecision motion control technique for high-resolution x-ray instrumentation

Energy Technology Data Exchange (ETDEWEB)

Shu, D.; Toellner, T. S.; Alp, E. E.

2000-07-17

With the availability of third-generation hard x-ray synchrotron radiation sources, such as the Advanced Photon Source (APS) at Argonne National Laboratory, x-ray inelastic scattering and x-ray nuclear resonant scattering provide powerful means for investigating the vibrational dynamics of a variety of materials and condensed matter systems. Novel high-resolution hard x-ray optics with meV energy resolution requires a compact positioning mechanism with 20--50-nrad angular resolution and stability. In this paper, the authors technical approach to this design challenge is presented. Sensitivity and stability test results are also discussed.

Extending the methodology of X-ray crystallography to allow X-ray microscopy without X-ray optics

International Nuclear Information System (INIS)

Miao Jianwei; Kirz, Janos; Sayre, David; Charalambous, Pambos

2000-01-01

We demonstrate that the soft X-ray diffraction pattern from a micron-size noncrystalline specimen can be recorded and inverted to form a high-resolution image. The phase problem is overcome by oversampling the diffraction pattern. The image is obtained using an iterative algorithm. The technique provides a method for X-ray microscopy requiring no high-resolution X-ray optical elements or detectors. In the present work, a resolution of approximately 60 nm was obtained, but we believe that considerably higher resolution can be achieved

Superiority of Low Energy 160 KV X-Rays Compared to High Energy 6 MV X-Rays in Heavy Element Radiosensitization for Cancer Treatment

Science.gov (United States)

Lim, Sara N.; Pradhan, Anil K.; Nahar, Sultana N.; Barth, Rolf F.; Yang, Weilian; Nakkula, Robin J.; Palmer, Alycia; Turro, Claudia

2013-06-01

High energy X-rays in the MeV range are generally employed in conventional radiation therapy from linear accelerators (LINAC) to ensure sufficient penetration depths. However, lower energy X-rays in the keV range may be more effective when coupled with heavy element (high-Z or HZ) radiosensitizers. Numerical simulations of X-ray energy deposition for tumor phantoms sensitized with HZ radiosensitizers were performed using the Monte Carlo code Geant4. The results showed enhancement in energy deposition to radiosensitized phantoms relative to unsensitized phantoms for low energy X-rays in the keV range. In contrast, minimal enhancement was seen using high energy X-rays in the MeV range. Dose enhancement factors (DEFs) were computed and showed radiosensitization only in the low energy range nitrate, was initially used because it was 7x less toxic that an equivalent amount of carboplatin in vitro studies. This would allow us to separate the radiotoxic and the chemotoxic effects of HZ sensitizers. Results from this study showed a 10-fold dose dependent reduction in surviving fractions (SF) of radiosensitized cells treated with low energy 160 kV X-rays compared to those treated with 6 MV X-rays. This is in agreement with our simulations that show an increase in dose deposition in radiosensitized tumors for low energy X-rays. Due to unforeen in vivo toxicity, however, another in vitro study was performed using the commonly used, Pt-based chemotherapeutic drug carboplatin which confirmed earlier results. This lays the ground work for a planned in vivo study using F98 glioma bearing rats. This study demonstrates that while high energy X-rays are commonly used in cancer radiotherapy, low energy keV X-rays might be much more effective with HZ radiosensitization.

Stress Free Multilayer Coating for High Resolution X-ray Mirrors

Data.gov (United States)

National Aeronautics and Space Administration — Most of X-ray optics research and development in the US is to build a high resolution, large collecting area and light-weight optic, namely an soft X-ray mirror for...

Time-resolved x-ray spectra of laser irradiated high-Z targets

International Nuclear Information System (INIS)

Lee, P.H.Y.; Attwood, D.T.; Boyle, M.J.; Campbell, E.M.; Coleman, L.C.; Kornblum, H.N.

1977-01-01

Recent results obtained by using the Livermore 15 psec x-ray streak camera to record x-ray emission from laser-irradiated high-z targets in the 1-20 keV range are reported. Nine to eleven K-edge filter channels were used for the measurements. In the lower energy channels, a dynamic range of x-ray emission intensity of better than three orders of magnitude have been recorded. Data will be presented which describe temporally and spectrally resolved x-ray spectra of gold disk targets irradiated by laser pulses from the Argus facility, including the temporal evolution of the superthermal x-ray tail

On the origin of highly ionized X-ray absorbers detected in the galactic X-ray binaries

International Nuclear Information System (INIS)

Luo, Yang; Fang, Taotao

2014-01-01

X-ray observations of the Galactic X-ray binaries (XRBs) revealed numerous highly ionized metal absorption lines. However, it is unclear whether such lines are produced by the hot interstellar medium (ISM) or the circumstellar medium intrinsic to the binaries. Here we present a Chandra X-ray absorption line study of 28 observations of 12 XRBs, with a focus on the Ne IX and Fe XVII lines. We report the first detections of these lines in a significant amount of observations. We do not find a significant dependence of the line equivalent width on the distance of the XRBs, but we do see a weak dependence on the source X-ray luminosity. We also find 2 out of 12 selected targets show strong temporal variation of the Ne IX absorbers. While the line ratio between the two ion species suggests a temperature consistent with the previous predictions of the ISM, comparing with two theoretical models of the ISM shows the observed column densities are significantly higher than predictions. On the other hand, photoionization by the XRBs provides a reasonably good fit to the data. Our findings suggest that a significant fraction of these X-ray absorbers may originate in the hot gas intrinsic to the XRBs, and that the ISM makes small, if not negligible, contribution. We briefly discuss the implications to the study of the Milky Way hot gas content.

High intensity line source for x-ray spectrometer calibration

International Nuclear Information System (INIS)

Thoe, R.S.

1986-06-01

A high intensity electron-impact x-ray source using a one-dimensional Pierce lens has been built for the purpose of calibrating a bent crystal x-ray spectrometer. This source focuses up to 100 mA of 20-keV electrons to a line on a liquid-cooled anode. The line (which can serve as a virtual slit for the spectrometer) measures approximately 800 μ x 2 cm. The source is portable and therefore adaptable to numerous types of spectrometer applications. One particular application, the calibration of a high resolution (r = 10 4 ) time-resolved cyrstal spectrometer, will be discussed in detail

High energy x-ray scattering studies of strongly correlated oxides

International Nuclear Information System (INIS)

Hatton, Peter D; Wilkins, S B; Spencer, P D; Zimmermann, M v; D'Almeida, T

2003-01-01

Many transition metal oxides display strongly correlated charge, spin, or orbital ordering resulting in varied phenomena such as colossal magnetoresistance, high temperature superconductivity, metal-insulator transitions etc. X-ray scattering is one of the principle techniques for probing the structural response to such effects. In this paper, we discuss and review the use of synchrotron radiation high energy x-rays (50-200 keV) for the study of transition metal oxides such as nickelates (La 2-x Sr x NiO 4 ) and manganites (La 2-2x Sr 1+2x Mn 2 O 7 ). High energy x-rays have sufficient penetration to allow us to study large flux-grown single crystals. The huge increase in sample scattering volume means that extremely weak peaks can be observed. This allows us to study very weak charge ordering. Measurements of the intensity, width and position of the charge ordering satellites as a function of temperature provide us with quantitative measures of the charge amplitude, inverse correlation length and wavevector of the charge ordering

A Chandra High-Resolution X-ray Image of Centaurus A.

Science.gov (United States)

Kraft; Forman; Jones; Kenter; Murray; Aldcroft; Elvis; Evans; Fabbiano; Isobe; Jerius; Karovska; Kim; Prestwich; Primini; Schwartz; Schreier; Vikhlinin

2000-03-01

We present first results from a Chandra X-Ray Observatory observation of the radio galaxy Centaurus A with the High-Resolution Camera. All previously reported major sources of X-ray emission including the bright nucleus, the jet, individual point sources, and diffuse emission are resolved or detected. The spatial resolution of this observation is better than 1&arcsec; in the center of the field of view and allows us to resolve X-ray features of this galaxy not previously seen. In particular, we resolve individual knots of emission in the inner jet and diffuse emission between the knots. All of the knots are diffuse at the 1&arcsec; level, and several exhibit complex spatial structure. We find the nucleus to be extended by a few tenths of an arcsecond. Our image also suggests the presence of an X-ray counterjet. Weak X-ray emission from the southwest radio lobe is also seen, and we detect 63 pointlike galactic sources (probably X-ray binaries and supernova remnants) above a luminosity limit of approximately 1.7x1037 ergs s-1.

Wire array z-pinch insights for high X-ray power generation

International Nuclear Information System (INIS)

Sanford, T.W.L.; Marder, B.M.; Desjarlais, M.P.

1998-01-01

The discovery that the use of very large numbers of wires enables high x-ray power to be generated from wire-array z-pinches represents a breakthrough in load design for large pulsed power generators, and has permitted high temperatures to be generated in radiation cavities on Saturn and Z. In this paper, changes in x-ray emission characteristics as a function of wire number, array mass, and load radius, for 20-mm-long aluminum arrays on Saturn that led to these breakthrough hohlraum results, are discussed and compared with a few related emission characteristics of high-wire-number aluminum and tungsten arrays on Z. X-ray measurement comparisons with analytic models and 2-D radiation-magnetohydrodynamic (RMHC) code simulations in the x-y and r-z planes provide confidence in the ability of the models and codes to predict future x-ray performance with very-large-number wire arrays

Wire array z-pinch insights for high X-ray power generation

Energy Technology Data Exchange (ETDEWEB)

Sanford, T.W.L.; Marder, B.M.; Desjarlais, M.P. [and others

1998-12-31

The discovery that the use of very large numbers of wires enables high x-ray power to be generated from wire-array z-pinches represents a breakthrough in load design for large pulsed power generators, and has permitted high temperatures to be generated in radiation cavities on Saturn and Z. In this paper, changes in x-ray emission characteristics as a function of wire number, array mass, and load radius, for 20-mm-long aluminum arrays on Saturn that led to these breakthrough hohlraum results, are discussed and compared with a few related emission characteristics of high-wire-number aluminum and tungsten arrays on Z. X-ray measurement comparisons with analytic models and 2-D radiation-magnetohydrodynamic (RMHC) code simulations in the x-y and r-z planes provide confidence in the ability of the models and codes to predict future x-ray performance with very-large-number wire arrays.

Wire array z-pinch insights for high x-ray power generation

Energy Technology Data Exchange (ETDEWEB)

Sanford, T.W.L.; Mock, R.C.; Marder, B.M. [and others

1997-12-31

The discovery that the use of very large numbers of wires enables high x-ray power to be generated from wire-array z-pinches represents a breakthrough in load design for large pulsed power generators, and has permitted high temperatures to be generated in radiation cavities on Saturn and Z. In this paper, changes in x-ray emission characteristics as a function of wire number, array mass, and load radius, for 20-mm-long aluminum arrays on Saturn that led to these breakthrough hohlraum results, are discussed and compared with a few related emission characteristics of high-wire-number aluminum and tungsten arrays on Z. X-ray measurement comparisons with analytic models and 2-D radiation-magnetohydrodynamic (RMHC) code simulations in the x-y and r-z planes provide confidence in the ability of the models and codes to predict future x-ray performance with very-large-number wire arrays.

Wire array z-pinch insights for high x-ray power generation

Energy Technology Data Exchange (ETDEWEB)

Sanford, T.W.L.; Mock, R.C.; Nash, T.J. [and others

1998-08-01

The discovery that the use of very large numbers of wires enables high x-ray power to be generated from wire-array z-pinches represents a breakthrough in load design for large pulsed power generators, and has permitted high temperatures to be generated in radiation cavities on Saturn. In this paper, changes in x-ray emission characteristics as a function of wire number, array mass, and load radius, for 20-mm-long aluminum arrays on Saturn that led to these breakthrough hohlraum results, are discussed and compared with a few related emission characteristics of high-wire-number aluminum and tungsten arrays on Z. X=ray measurement comparisons with analytic models and 2-D radiation-magnetohydrodynamic (RMHC) code simulations in the x-y and r-z planes provide confidence in the ability of the models and codes to predict future x-ray performance with very-large-number wire arrays.

Wire array z-pinch insights for high x-ray power generation

International Nuclear Information System (INIS)

Sanford, T.W.L.; Mock, R.C.; Marder, B.M.

1998-08-01

The discovery that the use of very large numbers of wires enables high x-ray power to be generated from wire-array z-pinches represents a breakthrough in load design for large pulsed power generators, and has permitted high temperatures to be generated in radiation cavities on Saturn and Z. In this paper, changes in x-ray emission characteristics as a function of wire number, array mass, and load radius, for 20-mm-long aluminum arrays on Saturn that led to these breakthrough hohlraum results, are discussed and compared with a few related emission characteristics of high-wire-number aluminum and tungsten arrays on Z. X=ray measurement comparisons with analytic models and 2-D radiation-magnetohydrodynamic (RMHC) code simulations in the x-y and r-z planes provide confidence in the ability of the models and codes to predict future x-ray performance with very-large-number wire arrays

High-energy synchrotron X-ray radiography of shock-compressed materials

Science.gov (United States)

Rutherford, Michael E.; Chapman, David J.; Collinson, Mark A.; Jones, David R.; Music, Jasmina; Stafford, Samuel J. P.; Tear, Gareth R.; White, Thomas G.; Winters, John B. R.; Drakopoulos, Michael; Eakins, Daniel E.

2015-06-01

This presentation will discuss the development and application of a high-energy (50 to 250 keV) synchrotron X-ray imaging method to study shock-compressed, high-Z samples at Beamline I12 at the Diamond Light Source synchrotron (Rutherford-Appleton Laboratory, UK). Shock waves are driven into materials using a portable, single-stage gas gun designed by the Institute of Shock Physics. Following plate impact, material deformation is probed in-situ by white-beam X-ray radiography and complimentary velocimetry diagnostics. The high energies, large beam size (13 x 13 mm), and appreciable sample volumes (~ 1 cm3) viable for study at Beamline I12 compliment existing in-house pulsed X-ray capabilities and studies at the Dynamic Compression Sector. The authors gratefully acknowledge the ongoing support of Imperial College London, EPSRC, STFC and the Diamond Light Source, and AWE Plc.

High-Performance X-ray Detection in a New Analytical Electron Microscope

Science.gov (United States)

Lyman, C. E.; Goldstein, J. I.; Williams, D. B.; Ackland, D. W.; vonHarrach, S.; Nicholls, A. W.; Statham, P. J.

1994-01-01

X-ray detection by energy-dispersive spectrometry in the analytical electron microscope (AEM) is often limited by low collected X-ray intensity (P), modest peak-to-background (P/B) ratios, and limitations on total counting time (tau) due to specimen drift and contamination. A new AFM has been designed with maximization of P. P/B, and tau as the primary considerations. Maximization of P has been accomplished by employing a field-emission electron gun, X-ray detectors with high collection angles, high-speed beam blanking to allow only one photon into the detector at a time, and simultaneous collection from two detectors. P/B has been maximized by reducing extraneous background signals generated at the specimen holder, the polepieces and the detector collimator. The maximum practical tau has been increased by reducing specimen contamination and employing electronic drift correction. Performance improvments have been measured using the NIST standard Cr thin film. The 0-3 steradian solid angle of X-ray collection is the highest value available. The beam blanking scheme for X-ray detection provides 3-4 times greater throughput of X-rays at high count rates into a recorded spectrum than normal systems employing pulse-pileup rejection circuits. Simultaneous X-ray collection from two detectors allows the highest X-ray intensity yet recorded to be collected from the NIST Cr thin film. The measured P/B of 6300 is the highest level recorded for an AEM. In addition to collected X-ray intensity (cps/nA) and P/B measured on the standard Cr film, the product of these can be used as a figure-of-merit to evaluate instruments. Estimated minimum mass fraction (MMF) for Cr measured on the standard NIST Cr thin film is also proposed as a figure-of-merit for comparing X-ray detection in AEMs. Determinations here of the MMF of Cr detectable show at least a threefold improvement over previous instruments.

High-energy X-ray production in a boundary layer of an accreting neutron star

International Nuclear Information System (INIS)

Hanawa, Tomoyuki

1991-01-01

It is shown by Monte Carlo simulation that high-energy X-rays are produced through Compton scattering in a boundary layer of an accreting neutron star. The following is the mechanism for the high-energy X-ray production. An accreting neutron star has a boundary layer rotating rapidly on the surface. X-rays radiated from the star's surface are scattered in part in the boundary layer. Since the boundary layer rotates at a semirelativistic speed, the scattered X-ray energy is changed by the Compton effect. Some X-rays are scattered repeatedly between the neutron star and the boundary layer and become high-energy X-rays. This mechanism is a photon analog of the second-order Fermi acceleration of cosmic rays. When the boundary layer is semitransparent, high-energy X-rays are produced efficiently. 17 refs

Providing x-rays

International Nuclear Information System (INIS)

Mallozzi, P.J.; Epstein, H.M.

1985-01-01

This invention provides an apparatus for providing x-rays to an object that may be in an ordinary environment such as air at approximately atmospheric pressure. The apparatus comprises: means (typically a laser beam) for directing energy onto a target to produce x-rays of a selected spectrum and intensity at the target; a fluid-tight enclosure around the target; means for maintaining the pressure in the first enclosure substantially below atmospheric pressure; a fluid-tight second enclosure adjoining the first enclosure, the common wall portion having an opening large enough to permit x-rays to pass through but small enough to allow the pressure reducing means to evacuate gas from the first enclosure at least as fast as it enters through the opening; the second enclosure filled with a gas that is highly transparent to x-rays; the wall of the second enclosure to which the x-rays travel having a portion that is highly transparent to x-rays (usually a beryllium or plastic foil), so that the object to which the x-rays are to be provided may be located outside the second enclosure and adjacent thereto and thus receive the x-rays substantially unimpeded by air or other intervening matter. The apparatus is particularly suited to obtaining EXAFS (extended x-ray fine structure spectroscopy) data on a material

The high energy X-ray spectra of supernova remnants

Science.gov (United States)

Pravdo, S. H.; Nugent, J. J.

The results of fitting an ionization-nonequilibrium (INE) model to the high-energy (above 5-keV) X-ray spectra of the young supernova remnants Cas A and Tycho are presented. As an additional constraint, the models must simultaneously fit lower-energy, higher-resolution data. For Cas A, a single INE component cannot adequately reproduce the features for the entire X-ray spectrum because the ionization structure of iron ions responsible for the K emission is inconsistent with that of the ions responsible for the lower-energy lines, and the flux of the highest-energy X-rays is underestimated. The iron K line and the high-energy continuum could arise from the same INE component, but the identification of this component with either the blast wave or the ejecta in the standard model is difficult. In Tycho, the high-energy data rule out a class of models for the lower-energy data which have too large a continuum contribution.

X-ray Spectroscopy of High-Z Elements on Nike

Science.gov (United States)

Aglitskiy, Y.; Weaver, J. L.; Karasik, M.; Serlin, V.; Obenschain, S. P.; Ralchenko, Yu.

2013-10-01

Survey X-ray spectrometer covering a spectral range from 0.5 to 19.5 angstroms has been added to the spectroscopic suite of Nike diagnostics. That allows simultaneous observation of both M- and N- spectra of W, Ta and Au with high spectral resolution. Low energy test shots confirmed strong presence of 3-4 transitions of Ni-like W, Ta and Au with X-ray energies as high as 3.5 keV when above mentioned elements were used as the targets. In our continuous effort to support DOE-NNSA's inertial fusion program, the future campaign will cover a wide range of plasma conditions that result in relatively energetic X-ray production. Eventually, absolutely calibrated spectrometers of similar geometry will be fielded at NIF in cooperation with NIF diagnostic group. Work supported by US DOE, Defense Programs.

High resolution X-ray detector for synchrotron-based microtomography

CERN Document Server

Stampanoni, M; Wyss, P; Abela, R; Patterson, B; Hunt, S; Vermeulen, D; Rueegsegger, P

2002-01-01

Synchrotron-based microtomographic devices are powerful, non-destructive, high-resolution research tools. Highly brilliant and coherent X-rays extend the traditional absorption imaging techniques and enable edge-enhanced and phase-sensitive measurements. At the Materials Science Beamline MS of the Swiss Light Source (SLS), the X-ray microtomographic device is now operative. A high performance detector based on a scintillating screen optically coupled to a CCD camera has been developed and tested. Different configurations are available, covering a field of view ranging from 715x715 mu m sup 2 to 7.15x7.15 mm sup 2 with magnifications from 4x to 40x. With the highest magnification 480 lp/mm had been achieved at 10% modulation transfer function which corresponds to a spatial resolution of 1.04 mu m. A low-noise fast-readout CCD camera transfers 2048x2048 pixels within 100-250 ms at a dynamic range of 12-14 bit to the file server. A user-friendly graphical interface gives access to the main parameters needed for ...

TH-AB-209-07: High Resolution X-Ray-Induced Acoustic Computed Tomography

Energy Technology Data Exchange (ETDEWEB)

Xiang, L; Tang, S [University of Oklahoma, Norman, OK (United States); Ahmad, M [Stanford University, Palo Alto, CA (United States); Xing, L [Stanford University School of Medicine, Stanford, CA (United States)

2016-06-15

Purpose: X-ray radiographic absorption imaging is an invaluable tool in medical diagnostics, biology and materials science. However, the use of conventional CT is limited by two factors: the detection sensitivity to weak absorption material and the radiation dose from CT scanning. The purpose of this study is to explore X-ray induced acoustic computed tomography (XACT), a new imaging modality, which combines X-ray absorption contrast and high ultrasonic resolution to address these challenges. Methods: First, theoretical models was built to analyze the XACT sensitivity to X-ray absorption and calculate the minimal radiation dose in XACT imaging. Then, an XACT system comprised of an ultrashort X-ray pulse, a low noise ultrasound detector and a signal acquisition system was built to evaluate the X-ray induced acoustic signal generation. A piece of chicken bone and a phantom with two golden fiducial markers were exposed to 270 kVp X-ray source with 60 ns exposure time, and the X-ray induced acoustic signal was received by a 2.25MHz ultrasound transducer in 200 positions. XACT images were reconstructed by a filtered back-projection algorithm. Results: The theoretical analysis shows that X-ray induced acoustic signals have 100% relative sensitivity to X-ray absorption, but not to X-ray scattering. Applying this innovative technology to breast imaging, we can reduce radiation dose by a factor of 50 compared with newly FDA approved breast CT. The reconstructed images of chicken bone and golden fiducial marker phantom reveal that the spatial resolution of the built XACT system is 350µm. Conclusion: In XACT, the imaging sensitivity to X-ray absorption is improved and the imaging dose is dramatically reduced by using ultrashort pulsed X-ray. Taking advantage of the high ultrasonic resolution, we can also perform 3D imaging with a single X-ray pulse. This new modality has the potential to revolutionize x-ray imaging applications in medicine and biology.

X-ray spectroscopy for high energy-density X pinch density and temperature measurements (invited)

International Nuclear Information System (INIS)

Pikuz, S.A.; Shelkovenko, T.A.; Chandler, K.M.; Mitchell, M.D.; Hammer, D.A.; Skobelev, I.Y.; Shlyaptseva, A.S.; Hansen, S.B.

2004-01-01

X pinch plasmas produced from fine metal wires can reach near solid densities and temperatures of 1 keV or even more. Plasma conditions change on time scales as short as 5-10 ps as determined using an x-ray streak camera viewing a focusing crystal spectrograph or directly viewing the plasma through multiple filters on a single test. As a result, it is possible to determine plasma conditions from spectra with ∼10 ps time resolution. Experiments and theory are now coming together to give a consistent picture of the dynamics and kinetics of these high energy density plasmas with very high temporal and spatial precision. A set of diagnostic techniques used in experiments for spectrally, temporally, and spatially resolved measurements of X pinch plasmas is described. Results of plasma parameter determination from these measurements are presented. X ray backlighting of one x-pinch by another with ∼30 ps x-ray pulses enables the dynamics and kinetics to be correlated in time

Joint European x-ray monitor (JEM-X): x-ray monitor for ESA's

DEFF Research Database (Denmark)

Schnopper, H.W.; Budtz-Joergensen, C.; Westergaard, Niels Jørgen Stenfeldt

1996-01-01

JEM-X will extend the energy range of the gamma ray instruments on ESA's INTEGRAL mission (SPI, IBIS) to include the x-ray band. JEM-X will provide images with arcminute angular resolution in the 2 - 60 keV band. The baseline photon detection system consists of two identical, high pressure, imagi...

Overview of high intensity x-ray and gamma-ray sources

International Nuclear Information System (INIS)

Prestwich, K.R.; Lee, J.R.; Ramirez, J.J.; Sanford, T.W.L.; Agee, F.J.; Frazier, G.B.; Miller, A.R.

1987-01-01

The requirements for intense x-ray and gamma-ray sources to simulate the radiation effects from nuclear weapons has led to the development of several types of terawatt-pulsed power systems. One example of a major gamma-ray source is Aurora, a 10-MV, 1.6-MA, 120-ns four-module, electron-beam generator. Recent requirements to improve the dose rate has led to the Aurora upgrade program and to the development of the 20-MV, 800-kA, 40-ns Hermes-III electron-beam accelerator. The Aurora program includes improvements to the pulsed power system and research on techniques to improve the pulse shape of the electron beam. Hermes III will feature twenty 1-MV, 800-kA induction accelerator cavities supplying energy to a magnetically insulated transmission line adder. Hermes III will become operational in 1988. Intense x-ray sources consist of pulsed power systems that operate with 1-MV to 2-MV output voltages and up to 25-TW output powers. These high powers are achieved with either low impedance electron-beam generators or multimodular pulsed power systems. The low-impedance generators have high voltage Marx generators that store the energy and then sequentially transfer this energy to pulse-forming transmission lines with lower and lower impedance until the high currents are reached. In the multimode machines, each module produces 0.7-TW to 4-TW output pulses, and all of the modules are connected together to supply energy to a single diode

Apparatus with a cooled X-ray source and a high voltage generator

Energy Technology Data Exchange (ETDEWEB)

1977-02-01

Apparatus, especially for a dental application, with an X-ray source and a high voltage generator, whereby the X-ray source and a high voltage generator are contained in a housing, which is filled with a coolant medium, characterised by the housing being divided into two chambers, whereby the X-ray source is in the first chamber and the high voltage generator is in the second chamber and between the chambers a dividing wall is placed for the screening of the X-ray irradiation from the first chamber from the second, whereby at least one of the walls of the second chamber is elastic to accommodate the expansion of the coolant medium.

Measurement of soft X-ray power from high-power Z-pinch plasma

International Nuclear Information System (INIS)

Wang Wensheng; Qiu Aici; Sun Fengrong; Luo Jianhui; Zhou Haisheng; He Duohui

2003-01-01

A Ni-film bolometer driven by the pulsed constant-voltage supply was developed for measuring soft X-ray energy under 1 keV generated from the Qiang-Guang-I, while the measuring system of the soft X-ray power was established with an X-ray diode detector. Results of the soft X-ray energy and power measurements were obtained at the experiment of Kr gas-puff high-power Z-pinch plasma

Catalogue of high-mass X-ray binaries in the Galaxy (4th edition)

NARCIS (Netherlands)

Liu, Q.Z.; van Paradijs, J.; van den Heuvel, E.P.J.

2006-01-01

We present a new edition of the catalogue of high-mass X-ray binaries in the Galaxy. The catalogue contains source name(s), coordinates, finding chart, X-ray luminosity, system parameters, and stellar parameters of the components and other characteristic properties of 114 high-mass X-ray binaries,

High resolution x-ray microscope

OpenAIRE

Gary, C. K.; Park, H.; Lombardo, L. W.; Piestrup, M. A.; Cremer, J. T.; Pantell, R. H.; Dudchik, Y. I.

2007-01-01

The authors present x-ray images of grid meshes and biological material obtained using a microspot x-ray tube with a multilayer optic and a 92-element parabolic compound refractive lens CRL made of a plastic containing only hydrogen and carbon. Images obtained using this apparatus are compared with those using an area source with a spherical lens and a spherical lens with multilayer condenser. The authors found the best image quality using the multilayer condenser with a parabolic lens, com...

Pulsed x-ray imaging of high-density objects using a ten picosecond high-intensity laser driver

Science.gov (United States)

Rusby, D. R.; Brenner, C. M.; Armstrong, C.; Wilson, L. A.; Clarke, R.; Alejo, A.; Ahmed, H.; Butler, N. M. H.; Haddock, D.; Higginson, A.; McClymont, A.; Mirfayzi, S. R.; Murphy, C.; Notley, M.; Oliver, P.; Allott, R.; Hernandez-Gomez, C.; Kar, S.; McKenna, P.; Neely, D.

2016-10-01

Point-like sources of X-rays that are pulsed (sub nanosecond), high energy (up to several MeV) and bright are very promising for industrial and security applications where imaging through large and dense objects is required. Highly penetrating X-rays can be produced by electrons that have been accelerated by a high intensity laser pulse incident onto a thin solid target. We have used a pulse length of 10ps to accelerate electrons to create a bright x-ray source. The bremsstrahlung temperature was measured for a laser intensity from 8.5-12×1018 W/cm2. These x-rays have sequentially been used to image high density materials using image plate and a pixelated scintillator system.

Novel X-ray telescopes for wide-field X-ray monitoring

International Nuclear Information System (INIS)

Hudec, R.; Inneman, A.; Pina, L.; Sveda, L.

2005-01-01

We report on fully innovative very wide-field of view X-ray telescopes with high sensitivity as well as large field of view. The prototypes are very promising, allowing the proposals for space projects with very wide-field Lobster-eye X-ray optics to be considered. The novel telescopes will monitor the sky with unprecedented sensitivity and angular resolution of order of 1 arcmin. They are expected to contribute essentially to study and to understand various astrophysical objects such as AGN, SNe, Gamma-ray bursts (GRBs), X-ray flashes (XRFs), galactic binary sources, stars, CVs, X-ray novae, various transient sources, etc. The Lobster optics based X-ray All Sky Monitor is capable to detect around 20 GRBs and 8 XRFs yearly and this will surely significantly contribute to the related science

High-resolution x-ray photoemission spectra of silver

DEFF Research Database (Denmark)

Barrie, A.; Christensen, N. E.

1976-01-01

An electron spectrometer fitted with an x-ray monochromator for Al Kα1,2 radiation (1486.6 eV) has been used to record high-resolution x-ray photoelectron spectra for the 4d valence band as well as the 3d spin doublet in silver. The core-level spectrum has a line shape that can be described...... successfully in terms of the many-body theory of Mahan, Nozières, and De Dominicis. The 4d spectrum agrees well with predictions based on a relativistic-augmented-plane-wave band-structure calculation....

A microcontroller application as X-ray machine's high voltage controller

International Nuclear Information System (INIS)

Wiranto Budi Santoso; Beny Syawaludin

2010-01-01

A micro controller application as x-ray machine's high voltage controller has been carried out. The purpose of this micro controller application is to give an accurate high voltage supply to the x-ray tube so that the x-ray machine could produce the result as expected. The micro controller based X-ray machine's high voltage controller receives an input voltage from the keypad. This input value is displayed in the LCD (Liquid Crystal Display) screen. Then micro controller uses this input data to drive a stepper motor. The stepper motor adjusts the high voltage auto transformer's output according to the input value. The micro controller is programmed using BASCOM-8051 compiler. The test results show that the stepper motor could rotate according to an input value (author)

Highly porous nanoberyllium for X-ray beam speckle suppression

Energy Technology Data Exchange (ETDEWEB)

Goikhman, Alexander, E-mail: agoikhman@ymail.com; Lyatun, Ivan; Ershov, Petr [Immanuel Kant Baltic Federal University, Nevskogo str. 14, Kaliningrad 236041 (Russian Federation); Snigireva, Irina [European Synchrotron Radiation Facility, BP 220, 38043 Grenoble (France); Wojda, Pawel [Immanuel Kant Baltic Federal University, Nevskogo str. 14, Kaliningrad 236041 (Russian Federation); Gdańsk University of Technology, 11/12 G. Narutowicza, Gdańsk 80-233 (Poland); Gorlevsky, Vladimir; Semenov, Alexander; Sheverdyaev, Maksim; Koletskiy, Viktor [A. A. Bochvar High-Technology Scientific Research Institute for Inorganic Materials, Rogova str. 5a, Moscow 123098 (Russian Federation); Snigirev, Anatoly [Immanuel Kant Baltic Federal University, Nevskogo str. 14, Kaliningrad 236041 (Russian Federation); European Synchrotron Radiation Facility, BP 220, 38043 Grenoble (France)

2015-04-09

A speckle suppression device containing highly porous nanoberyllium is proposed for manipulating the spatial coherence length and removing undesirable speckle structure during imaging experiments. This paper reports a special device called a ‘speckle suppressor’, which contains a highly porous nanoberyllium plate squeezed between two beryllium windows. The insertion of the speckle suppressor in an X-ray beam allows manipulation of the spatial coherence length, thus changing the effective source size and removing the undesirable speckle structure in X-ray imaging experiments almost without beam attenuation. The absorption of the nanoberyllium plate is below 1% for 1 mm thickness at 12 keV. The speckle suppressor was tested on the ID06 ESRF beamline with X-rays in the energy range from 9 to 15 keV. It was applied for the transformation of the phase–amplitude contrast to the pure amplitude contrast in full-field microscopy.

Highly porous nanoberyllium for X-ray beam speckle suppression

International Nuclear Information System (INIS)

Goikhman, Alexander; Lyatun, Ivan; Ershov, Petr; Snigireva, Irina; Wojda, Pawel; Gorlevsky, Vladimir; Semenov, Alexander; Sheverdyaev, Maksim; Koletskiy, Viktor; Snigirev, Anatoly

2015-01-01

A speckle suppression device containing highly porous nanoberyllium is proposed for manipulating the spatial coherence length and removing undesirable speckle structure during imaging experiments. This paper reports a special device called a ‘speckle suppressor’, which contains a highly porous nanoberyllium plate squeezed between two beryllium windows. The insertion of the speckle suppressor in an X-ray beam allows manipulation of the spatial coherence length, thus changing the effective source size and removing the undesirable speckle structure in X-ray imaging experiments almost without beam attenuation. The absorption of the nanoberyllium plate is below 1% for 1 mm thickness at 12 keV. The speckle suppressor was tested on the ID06 ESRF beamline with X-rays in the energy range from 9 to 15 keV. It was applied for the transformation of the phase–amplitude contrast to the pure amplitude contrast in full-field microscopy

X-ray scattering measurements from thin-foil x-ray mirrors

DEFF Research Database (Denmark)

Christensen, Finn Erland; BYRNAK, BP; Hornstrup, Allan

1992-01-01

Thin foil X-ray mirrors are to be used as the reflecting elements in the telescopes of the X-ray satellites Spectrum-X-Gamma (SRG) and ASTRO-D. High resolution X-ray scattering measurements from the Au coated and dip-lacquered Al foils are presented. These were obtained from SRG mirrors positioned...... in a test quadrant of the telescope structure and from ASTRO-D foils held in a simple fixture. The X-ray data is compared with laser data and other surface structure data such as STM, atomic force microscopy (AFM), TEM, and electron micrography. The data obtained at Cu K-alpha(1), (8.05 keV) from all...

High energy X-ray phase and dark-field imaging using a random absorption mask.

Science.gov (United States)

Wang, Hongchang; Kashyap, Yogesh; Cai, Biao; Sawhney, Kawal

2016-07-28

High energy X-ray imaging has unique advantage over conventional X-ray imaging, since it enables higher penetration into materials with significantly reduced radiation damage. However, the absorption contrast in high energy region is considerably low due to the reduced X-ray absorption cross section for most materials. Even though the X-ray phase and dark-field imaging techniques can provide substantially increased contrast and complementary information, fabricating dedicated optics for high energies still remain a challenge. To address this issue, we present an alternative X-ray imaging approach to produce transmission, phase and scattering signals at high X-ray energies by using a random absorption mask. Importantly, in addition to the synchrotron radiation source, this approach has been demonstrated for practical imaging application with a laboratory-based microfocus X-ray source. This new imaging method could be potentially useful for studying thick samples or heavy materials for advanced research in materials science.

Miniature x-ray source

Science.gov (United States)

Trebes, James E.; Bell, Perry M.; Robinson, Ronald B.

2000-01-01

A miniature x-ray source utilizing a hot filament cathode. The source has a millimeter scale size and is capable of producing broad spectrum x-ray emission over a wide range of x-ray energies. The miniature source consists of a compact vacuum tube assembly containing the hot filament cathode, an anode, a high voltage feedthru for delivering high voltage to the cathode, a getter for maintaining high vacuum, a connector for initial vacuum pump down and crimp-off, and a high voltage connection for attaching a compact high voltage cable to the high voltage feedthru. At least a portion of the vacuum tube wall is fabricated from highly x-ray transparent materials, such as sapphire, diamond, or boron nitride.

Method for spatially modulating X-ray pulses using MEMS-based X-ray optics

Science.gov (United States)

Lopez, Daniel; Shenoy, Gopal; Wang, Jin; Walko, Donald A.; Jung, Il-Woong; Mukhopadhyay, Deepkishore

2015-03-10

A method and apparatus are provided for spatially modulating X-rays or X-ray pulses using microelectromechanical systems (MEMS) based X-ray optics. A torsionally-oscillating MEMS micromirror and a method of leveraging the grazing-angle reflection property are provided to modulate X-ray pulses with a high-degree of controllability.

High-Resolution Detector For X-Ray Diffraction

Science.gov (United States)

Carter, Daniel C.; Withrow, William K.; Pusey, Marc L.; Yost, Vaughn H.

1988-01-01

Proposed x-ray-sensitive imaging detector offers superior spatial resolution, counting-rate capacity, and dynamic range. Instrument based on laser-stimulated luminescence and reusable x-ray-sensitive film. Detector scans x-ray film line by line. Extracts latent image in film and simultaneously erases film for reuse. Used primarily for protein crystallography. Principle adapted to imaging detectors for electron microscopy and fluorescence spectroscopy and general use in astronomy, engineering, and medicine.

X-ray photoelectron spectroscopy, high-resolution X-ray diffraction ...

Indian Academy of Sciences (India)

the crystalline quality through full-width at half-maximum values. .... angular divergence of ∆α = 12 arc sec. X-rays generated from the monochromator were diffracted from (0 0 6) LiNbO3 atomic planes with the (+, −, −, +, +) geometry. [8].

X-ray optics and X-ray microscopes: new challenges

International Nuclear Information System (INIS)

Susini, J.

2004-01-01

main fields of applications are driven by the unique attributes of X-ray microscopy in the multi-keV energy range: i) access to K-absorption edges and fluorescence emission lines of medium-light elements and L,M - edges of heavy materials for micro-spectroscopy (e.g. XANES), chemical or trace element mapping ii) higher penetration depths compared to soft X-rays allowing imaging of thicker samples, iii) favorable wavelengths for diffraction studies and iv) generally large focal lengths and depths of focus which are advantageous for the use of specific sample environments (high pressure, controlled temperatures....). Typical experiments can be broadly divided into two categories: i) morphological studies which require high spatial resolution and are therefore well adapted to 2D or 3D transmission full-field microscopy. ii) studies dealing with co-localization and/or speciation of trace elements in heterogeneous matrices at the micron scale. Following a brief account on the basic principles and methods, strengths and weaknesses of X-ray microscopy and spectro-microscopy techniques in the 1 - 30 keV range will be discussed and illustrated by examples of applications. The main technical developments, involving new focusing lenses or novel phase contrast geometry, will be presented. (author)

Development of confocal micro X-ray fluorescence instrument using two X-ray beams

International Nuclear Information System (INIS)

Tsuji, Kouichi; Nakano, Kazuhiko; Ding Xunliang

2007-01-01

A new confocal micro X-ray fluorescence instrument was developed. This instrument has two independent micro X-ray tubes with Mo targets. A full polycapillary X-ray lens was attached to each X-ray tube. Another half polycapillary lens was attached to a silicon drift X-ray detector (SDD). The focal spots of the three lenses were adjusted to a common position. The effects of the excitation of two X-ray beams were investigated. The instrument enabled highly sensitive three-dimensional X-ray fluorescence analysis. We confirmed that the X-ray fluorescence intensity from the sample increased by applying the two independent X-ray tubes in confocal configuration. Elemental depth profiling of black wheat was demonstrated with the result that each element in the surface coat of a wheat grain showed unique distribution

Miniature x-ray point source for alignment and calibration of x-ray optics

International Nuclear Information System (INIS)

Price, R.H.; Boyle, M.J.; Glaros, S.S.

1977-01-01

A miniature x-ray point source of high brightness similar to that of Rovinsky, et al. is described. One version of the x-ray source is used to align the x-ray optics on the Argus and Shiva laser systems. A second version is used to determine the spatial and spectral transmission functions of the x-ray optics. The spatial and spectral characteristics of the x-ray emission from the x-ray point source are described. The physical constraints including size, intensity and thermal limitations, and useful lifetime are discussed. The alignment and calibration techniques for various x-ray optics and detector combinations are described

Innovation of High Voltage Supply Adjustment Device on Diagnostic X-Ray Machine

International Nuclear Information System (INIS)

Sujatno; Wiranto Budi Santoso

2010-01-01

Innovation of high voltage supply adjustment device on diagnostic x-ray machine has been carried out. The innovation is conducted by utilizing an electronic circuit as a high voltage adjustment device. Usually a diagnostic x-ray machine utilizes a transformer or an auto-transformer as a high voltage supply adjustment device. A high power diagnostic x-ray machine needs a high power transformer which has big physical dimension. Therefore a box control where the transformer is located has to have big physical dimension. Besides, the price of the transformer is expensive and hardly found in local markets. In this innovation, the transformer is replaced by an electronic circuit. The main component of the electronic circuit is Triac BTA-40. As adjustment device, the triac is controlled by a variable resistor which is coupled by a stepper motor. A step movement of stepper motor varies a value of resistor. The resistor value determines the triac gate voltage. Furthermore the triac will open according to the value of electrical current flowing to the gate. When the gate is open, electrical voltage and current will flow from cathode to anode of the triac. The value of these electrical voltage and current depend on gate open condition. Then this triac output voltage is feed to diagnostic x-ray machine high voltage supply. Therefore the high voltage value of diagnostic x-ray machine is adjusted by the output voltage of the electronic circuit. By using this electronic circuit, the physical dimension of diagnostic x-ray machine box control and the price of the equipment can be reduced. (author)

Bismuth Passivation Technique for High-Resolution X-Ray Detectors

Science.gov (United States)

Chervenak, James; Hess, Larry

2013-01-01

The Athena-plus team requires X-ray sensors with energy resolution of better than one part in 3,000 at 6 keV X-rays. While bismuth is an excellent material for high X-ray stopping power and low heat capacity (for large signal when an X-ray is stopped by the absorber), oxidation of the bismuth surface can lead to electron traps and other effects that degrade the energy resolution. Bismuth oxide reduction and nitride passivation techniques analogous to those used in indium passivation are being applied in a new technique. The technique will enable improved energy resolution and resistance to aging in bismuth-absorber-coupled X-ray sensors. Elemental bismuth is lithographically integrated into X-ray detector circuits. It encounters several steps where the Bi oxidizes. The technology discussed here will remove oxide from the surface of the Bi and replace it with nitridized surface. Removal of the native oxide and passivating to prevent the growth of the oxide will improve detector performance and insulate the detector against future degradation from oxide growth. Placing the Bi coated sensor in a vacuum system, a reduction chemistry in a plasma (nitrogen/hydrogen (N2/H2) + argon) is used to remove the oxide and promote nitridization of the cleaned Bi surface. Once passivated, the Bi will perform as a better X-ray thermalizer since energy will not be trapped in the bismuth oxides on the surface. A simple additional step, which can be added at various stages of the current fabrication process, can then be applied to encapsulate the Bi film. After plasma passivation, the Bi can be capped with a non-diffusive layer of metal or dielectric. A non-superconducting layer is required such as tungsten or tungsten nitride (WNx).

Metallic magnetic calorimeters for high resolution X-ray spectroscopy

Energy Technology Data Exchange (ETDEWEB)

Krantz, M.; Hengstler, D.; Geist, J.; Schoetz, C.; Hassel, K.; Hendricks, S.; Keller, M.; Kempf, S.; Gastaldo, L.; Fleischmann, A.; Enss, C. [Heidelberg Univ. (Germany). KIP

2015-07-01

We develop microfabricated, energy dispersive particle detector arrays based on metallic magnetic calorimeters (MMCs) for high resolution X-ray spectroscopy to challenge bound-state QED calculations. Our MMCs are operated at about T=30 mK and use a paramagnetic temperature sensor, read-out by a SQUID, to measure the energy deposited by single X-ray photons. We discuss the physics of MMCs, the detector performance and the cryogenic setups for two different detector arrays. We present their microfabrication layouts with focus on challenges like the heatsinking of each pixel of the detector and the overhanging absorbers. The maXs-20 detector is a linear 1x8-pixel array with excellent linearity in its designated energy range up to 20 keV and unsurpassed energy resolution of 1.6 eV for 6 keV x-rays. MaXs-20 operated in a highly portable pulse tube cooled ADR setup has already been used at the EBIT facilities of the MPI-K for new reference measurements of V-like and Ti-like tungsten. The maXs-30 detector currently in development is a 8x8-pixel 2d-array with an active detection area of 16 mm{sup 2} and is designed to detect X-rays up to 50 keV with a designated energy resolution below 5 eV. MaXs-30 will be operated in a cryogen free 3He/4He-dilution refrigerator at the tip of a 40 cm long cold finger at T=20 mK.

X-ray detector array

International Nuclear Information System (INIS)

Houston, J.M.

1980-01-01

The object of the invention (an ionization chamber X-ray detector array for use with high speed computerised tomographic imaging apparatus) is to reduce the time required to produce a tomographic image. The detector array described determines the distribution of X-ray intensities in one or more flat, coplanar X-ray beams. It comprises three flat anode sheets parallel to the X-ray beam, a plurality of rod-like cathodes between the anodes, a detector gas between the electrodes and a means for applying a potential between the electrodes. Each of the X-ray sources is collimated to give a narrow, planar section of X-ray photons. Sets of X-ray sources in the array are pulsed simultaneously to obtain X-ray transmission data for tomographic image reconstruction. (U.K.)

Comparison of neutron and high-energy X-ray dual-beam radiography for air cargo inspection

International Nuclear Information System (INIS)

Liu, Y.; Sowerby, B.D.; Tickner, J.R.

2008-01-01

Dual-beam radiography techniques utilising various combinations of high-energy X-rays and neutrons are attractive for screening bulk cargo for contraband such as narcotics and explosives. Dual-beam radiography is an important enhancement to conventional single-beam X-ray radiography systems in that it provides additional information on the composition of the object being imaged. By comparing the attenuations of transmitted dual high-energy beams, it is possible to build a 2D image, colour coded to indicate material. Only high-energy X-rays, gamma-rays and neutrons have the required penetration to screen cargo containers. This paper reviews recent developments and applications of dual-beam radiography for air cargo inspection. These developments include dual high-energy X-ray techniques as well as fast neutron and gamma-ray (or X-ray) radiography systems. High-energy X-ray systems have the advantage of generally better penetration than neutron systems, depending on the material being interrogated. However, neutron systems have the advantage of much better sensitivity to material composition compared to dual high-energy X-ray techniques. In particular, fast neutron radiography offers the potential to discriminate between various classes of organic material, unlike dual energy X-ray techniques that realistically only offer the ability to discriminate between organic and metal objects

High-pressure X-ray diffraction studies of potassium chlorate

Energy Technology Data Exchange (ETDEWEB)

Pravica, Michael; Bai, Ligang; Bhattacharya, Neelanjan (UNLV)

2012-03-15

Two static high-pressure X-ray diffraction (XRD) studies of potassium chlorate have been performed at pressures of up to {approx}14.3 GPa in a diamond anvil cell at ambient temperature using the 16 ID-B undulator beamline at the Advanced Photon Source for the X-ray source. The first experiment was conducted to ascertain decomposition rates of potassium chlorate as a function of pressure. Below 2 GPa, the sample was observed to decompose rapidly in the presence of the X-ray beam and release oxygen. Above 2 GPa (near the phase I phase II transition), the decomposition rate dramatically slowed so that good quality XRD patterns could be acquired. This suggests a phase-dependent decomposition rate. In the second study, X-ray diffraction spectra were collected at pressures from 2 to 14.3 GPa by aligning virgin portions of the sample into the focused X-ray beam at each pressure. The results suggest the co-existence of mixed monoclinic (I) and rhombohedral (II) phases of potassium chlorate near 2 GPa. At pressures beyond 4 GPa, the XRD patterns show a very good fit to KClO{sub 3} in the rhombohedral phase with space group R3m, in agreement with earlier studies. No further phase transitions were observed with pressure. Decompression of the sample to ambient pressure indicated mixed phases I and II coupled with a small amount of synchrotron X-ray-induced decomposition product. The equation of state within this pressure regime has been determined.

Soft-X-Ray Projection Lithography Using a High-Repetition-Rate Laser-Induced X-Ray Source for Sub-100 Nanometer Lithography Processes

NARCIS (Netherlands)

E. Louis,; F. Bijkerk,; Shmaenok, L.; Voorma, H. J.; van der Wiel, M. J.; Schlatmann, R.; Verhoeven, J.; van der Drift, E. W. J. M.; Romijn, J.; Rousseeuw, B. A. C.; Voss, F.; Desor, R.; Nikolaus, B.

1993-01-01

In this paper we present the status of a joint development programme on soft x-ray projection lithography (SXPL) integrating work on high brightness laser plasma sources. fabrication of multilayer x-ray mirrors. and patterning of reflection masks. We are in the process of optimization of a

High temperature X-ray topography on silicon and gallium arsenide

International Nuclear Information System (INIS)

Krueger, H.E.

1976-01-01

Beginning with a review of the different theories of X-ray scattering on perfect and deformed crystals, results of the dynamic theory relevant specifically for X-ray topography are presented. The reflected intensity recorded in a X-ray topogram is discussed as a function of the angle of incidence, crystal thickness and lateral distribution. These results, together with fundamental relations of the DT which are developed in the annex, give insight into the contrasts induced by defects. Using practical examples Borrmann contrast, contrast produced by point defect agglomerates and dislocations and the Burgers vector method are explained. Thus the whole spectrum of contrast phenomena observed in the experimental part of the paper is presented. The experimental results were achieved with a high-temperature X-ray topography facility constructed for this purpose. The facility is described. (orig./HPOE) [de

Atomic physics at high brilliance synchrotron sources: Proceedings

International Nuclear Information System (INIS)

Berry, G.; Cowan, P.; Gemmell, D.

1994-08-01

This report contains papers on the following topics: present status of SPring-8 and the atomic physics undulator beamline; recent photoabsorption measurements in the rare gases and alkalis in the 3 to 15 keV proton energy region; atomic and molecular physics at LURE; experiments on atoms, ions and small molecules using the new generation of synchrotron radiation sources; soft x-ray fluorescence spectroscopy using tunable synchrotron radiation; soft x-ray fluorescence spectroscopy excited by synchrotron radiation: Inelastic and resonant scattering near threshold; outer-shell photoionization of ions; overview of the APS BESSRC beamline development; the advanced light source: Research opportunities in atomic and molecular physics; Photoionization of the Ba + ion by 4d shell excitation; decay dynamics of inner-shell excited atoms and molecules; absorption of atomic Ca, Cr, Mn and Cu; High-resolution photoelectron studies of resonant molecular photoionization; radiative and radiationless resonant raman scattering by synchrotron radiation; auger spectrometry of atoms and molecules; some thoughts of future experiments with the new generation of storage rings; Electron spectroscopy studies of argon K-shell excitation and vacancy cascades; ionization of atoms by high energy photons; ion coincidence spectroscopy on rare gas atoms and small molecules after photoexcitation at energies of several keV; an EBIS for use with synchrotron radiation photoionization of multiply charged ions and PHOBIS; gamma-2e coincidence measurements the wave of the future in inner-shell electron spectroscopy; recoil momentum spectroscopy in ion-atom and photon-atom collisions; a study of compton ionization of helium; future perspectives of photoionization studies at high photon energies; and status report on the advanced photon source. These papers have been cataloged separately elsewhere

High thermal efficiency x-ray energy conversion scheme for advanced fusion reactors

International Nuclear Information System (INIS)

Quimby, D.C.; Taussig, R.T.; Hertzberg, A.

1977-01-01

This paper reports on a new radiation energy conversion scheme which appears to be capable of producing electricity from the high quality x-ray energy with efficiencies of 60 to 70 percent. This new reactor concept incorporates a novel x-ray radiation boiler and a new thermal conversion device known as an energy exchanger. The low-Z first walls of the radiation boiler are semi-transparent to x-rays, and are kept cool by incoming working fluid, which is subsequently heated to temperatures of 2000 to 3000 0 K in the interior of the boiler by volumetric x-ray absorption. The radiation boiler may be a compact part of the reactor shell since x-rays are readily absorbed in high-Z materials. The energy exchanger transfers the high-temperature working fluid energy to a lower temperature gas which drives a conventional turbine. The overall efficiency of the cycle is characterized by the high temperature of the working fluid. The high thermal efficiencies which appear achievable with this cycle would make an otherwise marginal advanced fusion reactor into an attractive net power producer. The operating principles, initial conceptual design, and engineering problems of the radiation boiler and thermal cycle are presented

X-ray emission in slow highly charged ion-surface collisions

International Nuclear Information System (INIS)

Watanabe, H; Abe, T; Fujita, Y; Sun, J; Takahashi, S; Tona, M; Yoshiyasu, N; Nakamura, N; Sakurai, M; Yamada, C; Ohtani, S

2007-01-01

X-rays emitted in the collisions of highly charged ions with a surface have been measured to investigate dissipation schemes of their potential energies. While 8.1% of the potential energy was dissipated in the collisions of He-like I ions with a W surface, 29.1% has been dissipated in the case of He-like Bi ions. The x-ray emissions play significant roles in the dissipation of the potential energies in the interaction of highly charged heavy ions with the surface

A planar parabolic refractive nickel lens for high-energy X-rays

International Nuclear Information System (INIS)

Andrejczuk, Andrzej; Nagamine, Masaru; Sakurai, Yoshiharu; Itou, Masayoshi

2013-01-01

A compound refractive nickel lens focusing 174 keV X-rays to 5 µm with a gain of 4 is presented. A compound refractive lens made of nickel and designed for focusing high-energy synchrotron X-rays is presented. The lens consists of 600 parabolic grooves and focuses X-rays in one plane only (planar lens). The lenses made and investigated by us earlier exhibited low transmission and irregularities in the focused beam profile. Since then, improvements in lens manufacturing technology have been made. The present lens gives an almost Gaussian profile and produces four times higher intensity at its maximum compared with the intensity of primary X-ray beams of 174 keV

High spectral resolution X-ray observations of AGN

NARCIS (Netherlands)

Kaastra, J.S.

2008-01-01

brief overview of some highlights of high spectral resolution X-ray observations of AGN is given, mainly obtained with the RGS of XMM-Newton. Future prospects for such observations with XMM-Newton are given.

Silicon detectors for x and gamma-ray with high radiation resistance

International Nuclear Information System (INIS)

Cimpoca, Valerica; Popescu, Ion V.; Ruscu, Radu

2001-01-01

Silicon detectors are widely used in X and gamma-ray spectroscopy for direct detection or coupled with scintillators in high energy nuclear physics (modern collider experiments are representative), medicine and industrial applications. In X and gamma dosimetry, a low detection limit (under 6 KeV) with silicon detectors becomes available. Work at the room temperature is now possible due to the silicon processing evolution, which assures low reverse current and high life time of carriers. For several years, modern semiconductor detectors have been the primary choice for the measurement of nuclear radiation in various scientific fields. Nowadays the recently developed high resolution silicon detectors found their way in medical applications. As a consequence many efforts have been devoted to the development of high sensitivity and radiation hardened X and gamma-ray detectors for the energy range of 5 - 150 keV. The paper presents some results concerning the technology and behaviour of X and Gamma ray silicon detectors used in physics research, industrial and medical radiography. The electrical characteristics of these detectors, their modification after exposure to radiation and the results of spectroscopic X and Gamma-ray measurements are discussed. The results indicated that the proposed detectors enables the development of reliable silicon detectors to be used in controlling the low and high radiation levels encountered in a lot of application

Development of X-ray excitable luminescent probes for scanning X-ray microscopy

International Nuclear Information System (INIS)

Moronne, M.M.

1999-01-01

Transmission soft X-ray microscopy is now capable of achieving resolutions that are typically 5 times better than the best-visible light microscopes. With expected improvements in zone plate optics, an additional factor of two may be realized within the next few years. Despite the high resolution now available with X-ray microscopes and the high X-ray contrast provided by biological molecules in the soft X-ray region (λ=2-5 nm), molecular probes for localizing specific biological targets have been lacking. To circumvent this problem, X-ray excitable molecular probes are needed that can target unique biological features. In this paper we report our initial results on the development of lanthanide-based fluorescent probes for biological labeling. Using scanning luminescence X-ray microscopy (SLXM, Jacobsen et al., J. Microscopy 172 (1993) 121-129), we show that lanthanide organo-polychelate complexes are sufficiently bright and radiation resistant to be the basis of a new class of X-ray excitable molecular probes capable of providing at least a fivefold improvement in resolution over visible light microscopy. Lanthanide probes, able to bind 80-100 metal ions per molecule, were found to give strong luminescent signals with X-ray doses exceeding 10 8 Gy, and were used to label actin stress fibers and in vitro preparations of polymerized tubulin. (Copyright (c) 1999 Elsevier Science B.V., Amsterdam. All rights reserved.)

New tubes and techniques for flash X-ray diffraction and high contrast radiography

International Nuclear Information System (INIS)

Charbonnier, F.M.; Barbour, J.P.; Brewster, J.L.

High energy electrons are particularly efficient in producing characteristic X-rays and soft polychromatic. A line of wide spectrum beryllium window flash X-ray tubes, ranging from 150 to 600kV, has been developed to exploit this property. Laue and Debye Scherrer flash X-ray diffraction patterns have been obtained using a single 30 ns pulse exposure. X-ray diffraction tests obtained are shown. Extremely high contrast flash radiography of small, low density objects has been obtained using industrial film without screen. Alternatively, particularly at high voltages and for subjects which include a broad range of materials and thicknesses, special film techniques can be used to produce extremely wide latitudes. Equipment, techniques and results are discussed

Novel Hybrid CMOS X-ray Detector Developments for Future Large Area and High Resolution X-ray Astronomy Missions

Science.gov (United States)

Falcone, Abe

In the coming years, X-ray astronomy will require new soft X-ray detectors that can be read very quickly with low noise and can achieve small pixel sizes over a moderately large focal plane area. These requirements will be present for a variety of X-ray missions that will attempt to address science that was highly ranked by the 2010 Decadal Survey, including missions with science that overlaps with that of IXO and Athena, as well as other missions addressing science topics beyond those of IXO and Athena. An X-ray Surveyor mission was recently chosen by NASA for study by a Science & Technology Definition Team (STDT) so it can be considered as an option for an upcom-ing flagship mission. A mission such as this was endorsed by the NASA long term planning document entitled "Enduring Quests, Daring Visions," and a detailed description of one possible reali-zation of such a mission has been referred to as SMART-X, which was described in a recent NASA RFI response. This provides an example of a future mission concept with these requirements since it has high X-ray throughput and excellent spatial resolution. We propose to continue to modify current active pixel sensor designs, in particular the hybrid CMOS detectors that we have been working with for several years, and implement new in-pixel technologies that will allow us to achieve these ambitious and realistic requirements on a timeline that will make them available to upcoming X-ray missions. This proposal is a continuation of our program that has been work-ing on these developments for the past several years. The first 3 years of the program led to the development of a new circuit design for each pixel, which has now been shown to be suitable for a larger detector array. The proposed activity for the next four years will be to incorporate this pixel design into a new design of a full detector array (2k×2k pixels with digital output) and to fabricate this full-sized device so it can be thoroughly tested and

Ultrafast coherent diffractive imaging of nanoparticles using X-ray free-electron laser radiation

International Nuclear Information System (INIS)

Kassemeyer, Stephan

2014-01-01

Coherent diffractive imaging with X-ray free-electron lasers (X-FEL) promises high-resolution structure determination of single microscopic particles without the need for crystallization. The diffraction signal of small samples can be very weak, a difficulty that can not be countered by merely increasing the number of photons because the sample would be damaged by a high absorbed radiation dose. Traditional X-ray crystallography avoids this problem by bringing many sample particles into a periodic arrangement, which amplifies the individual signals while distributing the absorbed dose. Depending on the sample, however, crystallization can be very difficult or even impossible. This thesis presents algorithms for a new imaging approach using X-FEL radiation that works with single, non-crystalline sample particles. X-FELs can deliver X-rays with a peak brilliance many orders of magnitude higher than conventional X-ray sources, compensating for their weak interaction cross sections. At the same time, FELs can produce ultra-short pulses down to a few femtoseconds. In this way it is possible to perform ultra-fast imaging, essentially ''freezing'' the atomic positions in time and terminating the imaging process before the sample is destroyed by the absorbed radiation. This thesis primarily focuses on the three-dimensional reconstruction of single (and not necessarily crystalline) particles using coherent diffractive imaging at X-FELs: in order to extract three-dimensional information from scattering data, two-dimensional diffraction patterns from many different viewing angles must be combined. Therefore, the diffraction signal of many identical sample copies in random orientations is measured. The main result of this work is a globally optimal algorithm that can recover the sample orientations solely based on the diffraction signal, enabling three-dimensional imaging for arbitrary samples. The problem of finding three-dimensional orientations is

Cosmic and solar gamma-ray x-ray and particle measurements from high altitude balloons in Antarctica

International Nuclear Information System (INIS)

Lin, R.P.

1990-01-01

For measurements of cosmic and solar gamma-rays, hard X-rays, and particles, Antarctica offers the potential for very long, 10--20 day, continuous, twenty-four-hour-a-day observations, with balloon flights circling the South Pole during austral summer. For X-ray/gamma-ray sources at high south latitude the overlying atmosphere is minimized, and for cosmic ray measurements the low geomagnetic cutoff permits entry of low rigidity particles. The first Antarctic flight of a heavy (∼2400 lb.) payload on a large (11.6x10 6 cu. ft.) balloon took place in January, 1988, to search for the gamma-ray lines of 56 Co produced in the new supernova SN 1987A in the Large Magellanic Cloud. The long duration balloon flights presently planned from Antarctica include those for further gamma-ray/hard X-ray studies of SN 1987A and for the NASA Max '91 program for solar flare studies

A high-resolution multiwire area detector for X-ray scattering

Energy Technology Data Exchange (ETDEWEB)

Faruqi, A R; Andrews, H [Medical Research Council, Cambridge (UK). Lab. of Molecular Biology

1989-11-10

A high-resolution multiwire area detector has been developed for recording X-ray scattering from biological specimens. The detector is 100x100 mm{sup 2} and, under the present operating conditions, has a spatial resolution of about 250 {mu}m in both directions. The detector is set up on a double-mirror focusing camera on a rotating anode X-ray generator and has been used in a number of small-angle experiments, two of which are described in this paper. (orig.).

Femtosecond X-ray magnetic circular dichroism absorption spectroscopy at an X-ray free electron laser

Energy Technology Data Exchange (ETDEWEB)

Higley, Daniel J., E-mail: dhigley@stanford.edu; Yuan, Edwin [SLAC National Accelerator Laboratory, 2575 Sand Hill Road, Menlo Park, California 94025 (United States); Department of Applied Physics, Stanford University, Stanford, California 94305 (United States); Hirsch, Konstantin; Dakovski, Georgi L.; Jal, Emmanuelle; Lutman, Alberto A.; Coslovich, Giacomo; Hart, Philip; Hoffmann, Matthias C.; Mitra, Ankush; Moeller, Stefan; Ohldag, Hendrik; Seaberg, Matthew; Stöhr, Joachim; Nuhn, Heinz-Dieter; Reid, Alex H.; Dürr, Hermann A.; Schlotter, William F. [SLAC National Accelerator Laboratory, 2575 Sand Hill Road, Menlo Park, California 94025 (United States); Liu, Tianmin; MacArthur, James P. [SLAC National Accelerator Laboratory, 2575 Sand Hill Road, Menlo Park, California 94025 (United States); Department of Physics, Stanford University, Stanford, California 94305 (United States); and others

2016-03-15

X-ray magnetic circular dichroism spectroscopy using an X-ray free electron laser is demonstrated with spectra over the Fe L{sub 3,2}-edges. The high brightness of the X-ray free electron laser combined with high accuracy detection of incident and transmitted X-rays enables ultrafast X-ray magnetic circular dichroism studies of unprecedented sensitivity. This new capability is applied to a study of all-optical magnetic switching dynamics of Fe and Gd magnetic sublattices in a GdFeCo thin film above its magnetization compensation temperature.

X-ray microscopy with high resolution zone plates -- Recent developments

International Nuclear Information System (INIS)

Schneider, G.; Wilhein, T.; Niemann, B.; Guttmann, P.

1995-01-01

In order to expand the applications of X-ray microscopy, developments in the fields of zone plate technology, specimen preparation and imaging techniques have been made. A new cross-linked polymer chain electron beam resist allows to record zone plate pattern down to 19 nm outermost zone width. High resolution zone plates in germanium with outermost zone widths down to 19 nm have been developed. In addition, phase zone plates in nickel down to 30 nm zone width have been made by electroplating. In order to enhance the image contrast for weak absorbing objects, the phase contrast method for X-ray microscopy was developed and implemented on the Goettingen X-ray microscope at BESSY. The effects of X-ray absorption on the structure of biological specimen limits the maximum applicable radiation dose and therefore the achievable signal to noise ratio for an artifact-free X-ray image. To improve the stability especially of biological specimen, a cryogenic object chamber has been developed and tested. It turns out that at the operating temperature T ≤ 130 K unfixed biological specimen can be exposed to a radiation dose of 10 9 --10 10 Gy without any observable structural changes. A multiple-angle viewing stage allows to take stereoscopic images with the X-ray microscope, giving a 3D-impression of the object

A high time resolution x-ray diagnostic on the Madison Symmetric Torus

Science.gov (United States)

DuBois, Ami M.; Lee, John David; Almagri, Abdulgadar F.

2015-07-01

A new high time resolution x-ray detector has been installed on the Madison Symmetric Torus (MST) to make measurements around sawtooth events. The detector system is comprised of a silicon avalanche photodiode, a 20 ns Gaussian shaping amplifier, and a 500 MHz digitizer with 14-bit sampling resolution. The fast shaping time diminishes the need to restrict the amount of x-ray flux reaching the detector, limiting the system dead-time. With a much higher time resolution than systems currently in use in high temperature plasma physics experiments, this new detector has the versatility to be used in a variety of discharges with varying flux and the ability to study dynamics on both slow and fast time scales. This paper discusses the new fast x-ray detector recently installed on MST and the improved time resolution capabilities compared to the existing soft and hard x-ray diagnostics. In addition to the detector hardware, improvements to the detector calibration and x-ray pulse identification software, such as additional fitting parameters and a more sophisticated fitting routine are discussed. Finally, initial data taken in both high confinement and standard reversed-field pinch plasma discharges are compared.

High-Resolution and Lightweight X-ray Optics for the X-Ray Surveyor

Science.gov (United States)

Zhang, William

Envisioned in "Enduring Quest, Daring Visions" and under study by NASA as a potential major mission for the 2020s, the X-ray Surveyor mission will likely impose three requirements on its optics: (1) high angular resolution: 0.5 PSF, (2) large effective area: e10,000 cm2 or more, and (3) affordable production cost: $500M. We propose a technology that can meet these requirements by 2020. It will help the X-ray Surveyor secure the endorsement of the coming decadal survey and enable its implementation following WFIRST. The technology comprises four elements: (1) fabrication of lightweight single crystal silicon mirrors, (2) coating these mirrors with iridium to maximize effective area without figure degradation, (3) alignment and bonding of these mirrors to form meta-shells that will be integrated to make a mirror assembly, and (4) systems engineering to ensure that the mirror assembly meet all science performance and spaceflight environmental requirements. This approach grows out of our existing approach based on glass slumping. Using glass slumping technology, we have been able to routinely build and test mirror modules of 10half-power diameter (HPD). While comparable in HPD to XMM-Newtons electroformed nickel mirrors, these mirror modules are 10 times lighter. Likewise, while comparable in weight to Suzakus epoxy-replicated aluminum foil mirrors, these modules have 10 times better HPD. These modules represent the current state of the art of lightweight X-ray optics. Although both successful and mature, the glass slumping technology has reached its limit and cannot achieve sub-arc second HPD. Therefore, we are pursuing the new approach based on polishing single crystal silicon. The new approach will enable the building and testing of mirror modules, called meta-shells, capable of 3HPD by 2018 and 1HPD by 2020, and has the potential to reach diffraction limits ( 0.1) in the 2020s.

X-ray spectroscopic study of high-temperature plasmas by curved crystal spectrometer

International Nuclear Information System (INIS)

Morita, Shigeru.

1983-07-01

Extensive studies have been carried out on the structure of X-ray spectra from the highly stripped ions of first transition elements and their behavior in high temperature plasma, using a high resolution crystal spectrometer. Calculation was made on the design and the use of a curved crystal spectrometer for plasma diagnostics. A Johann type crystal spectrometer for measuring X-ray lines was constructed on the basis of the calculation. The characteristics of curved crystals of LiF, Ge and quartz used for the measurement of Kα lines from first transition elements were investigated. Vacuum sparks have been formed for producing high temperature plasma which emits X-ray lines from highly stripped ions. Two different structures of vacuum spark plasma were shown, that is, thermalized point plasma and extended plasma associated with non-thermal electrons. The X-ray lines from the extended plasma, those associated with the K shell from the point plasma and the Kα lines of Ti through Zn from the point plasma have been observed. (Kako, I.)

Femtosecond X-ray Absorption Spectroscopy at a Hard X-ray Free Electron Laser

DEFF Research Database (Denmark)

Lemke, Henrik T.; Bressler, Christian; Chen, Lin X.

2013-01-01

X-ray free electron lasers (XFELs) deliver short (current (SASE based) XFELs, they can be used for measuring high......-quality X-ray absorption data and we report femtosecond time-resolved X-ray absorption near-edge spectroscopy (XANES) measurements of a spin-crossover system, iron(II) tris(2,2'-bipyridine) in water. The data indicate that the low-spin to high-spin transition can be modeled by single-exponential kinetics...

Si(Li) X-ray detector

International Nuclear Information System (INIS)

Yuan Xianglin; Li Zhiyong; Hong Xiuse

1990-08-01

The fabrication technology of the 10∼80 mm 2 Si(Li) X-ray detectors are described and some problems concerning technology and measurement are discussed. The specifications of the detectors are shown as well. The Si(Li) X-ray detector is a kind of low energy X-ray detectors. Owing to very high energy resolution, fine linearity and high detection efficiency in the range of low energy X-rays, it is widely used in the fields of nuclear physics, medicine, geology and environmental protection, etc,. It is also a kernel component for the scanning electron microscope and X-ray fluorescence analysis systems

Project Title: Radiochemical Analysis by High Sensitivity Dual-Optic Micro X-ray Fluorescence

International Nuclear Information System (INIS)

Havrilla, George J.; Gao, Ning

2002-01-01

A novel dual-optic micro X-ray fluorescence instrument will be developed to do radiochemical analysis of high-level radioactive wastes at DOE sites such as Savannah River Site and Hanford. This concept incorporates new X-ray optical elements such as monolithic polycapillaries and double bent crystals, which focus X-rays. The polycapillary optic can be used to focus X-rays emitted by the X-ray tube thereby increasing the X-ray flux on the sample over 1000 times. Polycapillaries will also be used to collect the X-rays from the excitation site and screen the radiation background from the radioactive species in the specimen. This dual-optic approach significantly reduces the background and increases the analyte signal thereby increasing the sensitivity of the analysis. A doubly bent crystal used as the focusing optic produces focused monochromatic X-ray excitation, which eliminates the bremsstrahlung background from the X-ray source. The coupling of the doubly bent crystal for monochromatic excitation with a polycapillary for signal collection can effectively eliminate the noise background and radiation background from the specimen. The integration of these X-ray optics increases the signal-to-noise and thereby increases the sensitivity of the analysis for low-level analytes. This work will address a key need for radiochemical analysis of high-level waste using a non-destructive, multi-element, and rapid method in a radiation environment. There is significant potential that this instrumentation could be capable of on-line analysis for process waste stream characterization at DOE sites

High-pressure pair distribution function (PDF) measurement using high-energy focused x-ray beam

Energy Technology Data Exchange (ETDEWEB)

Hong, Xinguo, E-mail: xhong@bnl.gov; Weidner, Donald J. [Mineral Physics Institute, Stony Brook University, Stony Brook, NY 11794 (United States); Ehm, Lars [Mineral Physics Institute, Stony Brook University, Stony Brook, NY 11794 (United States); National Synchrotron Light Source II, Brookhaven National Laboratory, Upton, NY 11973 (United States); Zhong, Zhong; Ghose, Sanjit [National Synchrotron Light Source II, Brookhaven National Laboratory, Upton, NY 11973 (United States); Duffy, Thomas S. [Department of Geosciences, Princeton University, Princeton, NJ 08544 (United States)

2016-07-27

In this paper, we report recent development of the high-pressure pair distribution function (HP-PDF) measurement technique using a focused high-energy X-ray beam coupled with a diamond anvil cell (DAC). The focusing optics consist of a sagittally bent Laue monochromator and Kirkpatrick-Baez (K–B) mirrors. This combination provides a clean high-energy X-ray beam suitable for HP-PDF research. Demonstration of the HP-PDF technique for nanocrystalline platinum under quasi-hydrostatic condition above 30 GPa is presented.

Empirical electro-optical and x-ray performance evaluation of CMOS active pixels sensor for low dose, high resolution x-ray medical imaging

International Nuclear Information System (INIS)

Arvanitis, C. D.; Bohndiek, S. E.; Royle, G.; Blue, A.; Liang, H. X.; Clark, A.; Prydderch, M.; Turchetta, R.; Speller, R.

2007-01-01

Monolithic complementary metal oxide semiconductor (CMOS) active pixel sensors with high performance have gained attention in the last few years in many scientific and space applications. In order to evaluate the increasing capabilities of this technology, in particular where low dose high resolution x-ray medical imaging is required, critical electro-optical and physical x-ray performance evaluation was determined. The electro-optical performance includes read noise, full well capacity, interacting quantum efficiency, and pixels cross talk. The x-ray performance, including x-ray sensitivity, modulation transfer function, noise power spectrum, and detection quantum efficiency, has been evaluated in the mammographic energy range. The sensor is a 525x525 standard three transistor CMOS active pixel sensor array with more than 75% fill factor and 25x25 μm pixel pitch. Reading at 10 f/s, it is found that the sensor has 114 electrons total additive noise, 10 5 electrons full well capacity with shot noise limited operation, and 34% interacting quantum efficiency at 530 nm. Two different structured CsI:Tl phosphors with thickness 95 and 115 μm, respectively, have been optically coupled via a fiber optic plate to the array resulting in two different system configurations. The sensitivity of the two different system configurations was 43 and 47 electrons per x-ray incident on the sensor. The MTF at 10% of the two different system configurations was 9.5 and 9 cycles/mm with detective quantum efficiency of 0.45 and 0.48, respectively, close to zero frequency at ∼0.44 μC/kg (1.72 mR) detector entrance exposure. The detector was quantum limited at low spatial frequencies and its performance was comparable with high resolution a:Si and charge coupled device based x-ray imagers. The detector also demonstrates almost an order of magnitude lower noise than active matrix flat panel imagers. The results suggest that CMOS active pixel sensors when coupled to structured CsI:Tl can

X-ray CT high-density artefact suppression in cryosurgery

International Nuclear Information System (INIS)

Wei Jikun; Sandison, George A; Chen Laigao; Liang Yun; Xu, Lisa X

2002-01-01

Advantages of x-ray CT for imaging guidance of cryosurgery include 3D visualization of frozen and unfrozen tissue and calibration of temperature in the tissue water-ice interface (0-10 deg. C) to Hounsfield units. However, use of x-ray CT images and their thermal calibration can be compromised by the cryoprobes generating high-density streak artefacts. A new subtraction technique for artefact suppression is proposed and tested in prostate cryosurgery simulations. By subtracting the measured CT x-ray projection profile without cryoprobes from the profile with cryoprobes plus iceballs, one obtains the combined profile of the cryoprobes and a low value background. Polynomial interpolation to obtain the background profile allows its addition to the original profile without probes. The result may then be fed to a conventional filtered back-projection routine to reconstruct the probe-free image. Finally the cryoprobe pixels in the originally constructed image with probes and iceballs are added back to the probe-free image to get the final artefact-suppressed image. The major advantage of this subtraction technique is that it can successfully suppress the high-density artefacts in bone-abundant body regions such as the pelvis. X-ray CT images of cryoprobe arrays in a homogeneous gelatin phantom and the pelvic region of an anthropomorphic Rando phantom containing a human skeleton were generated. After suppression, cryoprobe metal artefact streaks are reduced and visualization of the positions and dimensions of the cryoprobes are well preserved. (note)

Phase contrast imaging with coherent high energy X-rays

Energy Technology Data Exchange (ETDEWEB)

Snigireva, I. [ESRF, Grenoble (France)

1997-02-01

X-ray imaging concern high energy domain (>6 keV) like a contact radiography, projection microscopy and tomography is used for many years to discern the features of the internal structure non destructively in material science, medicine and biology. In so doing the main contrast formation is absorption that makes some limitations for imaging of the light density materials and what is more the resolution of these techniques is not better than 10-100 {mu}m. It was turned out that there is now way in which to overcome 1{mu}m or even sub-{mu}m resolution limit except phase contrast imaging. It is well known in optics that the phase contrast is realised when interference between reference wave front and transmitted through the sample take place. Examples of this imaging are: phase contrast microscopy suggested by Zernike and Gabor (in-line) holography. Both of this techniques: phase contrast x-ray microscopy and holography are successfully progressing now in soft x-ray region. For imaging in the hard X-rays to enhance the contrast and to be able to resolve phase variations across the beam the high degree of the time and more importantly spatial coherence is needed. Because of this it was reasonable that the perfect crystal optics was involved like Bonse-Hart interferometry, double-crystal and even triple-crystal set-up using Laue and Bragg geometry with asymmetrically cut crystals.

OSO-7 observations of high galactic latitude x-ray sources

International Nuclear Information System (INIS)

Markert, T.H.; Canizares, C.R.; Clark, G.W.; Li, F.K.; Northridge, P.L.; Sprott, G.F.; Wargo, G.F.

1976-01-01

Six hundred days of observations by the MIT X-ray detectors aboard OSO-7 have been analyzed. All-sky maps of X-ray intensity have been constructed from these data. A sample map is displayed. Seven sources with galactic latitude vertical-barb/subi//subi/vertical-bar>10degree, discovered during the mapping process, are reported, and upper limits are set on other high-latitude sources. The OSO-7 results are compared with those of Uhuru and an implication of this comparison, that many of the high-latitude sources may be variable, is discussed

High-energy X-ray observations of extragalactic objects

International Nuclear Information System (INIS)

Pietsch, W.; Reppin, C.; Truemper, J.; Voges, W.; Lewin, W.; Kendziorra, E.; Staubert, R.

1981-01-01

During a balloon flight from Alice Springs, Australia, six extragalactic sources which are known as potential X-ray sources have been observed in hard X-rays (E > 20 keV). We present X-ray spectra of 3C 273 and Cen-A as well as upper limits on 3C 120, MKN 509, NGC 5506, and MR 2251-178. (orig.)

On the limitations and optimisation of high-resolution 3D medical X-ray imaging systems

International Nuclear Information System (INIS)

Zhou Shuang; Brahme, Anders

2011-01-01

Based on a quantitative analysis of both attenuation and refractive properties of X-ray propagation in human body tissues and the introduction of a mathematical model for image quality analysis, some limitations and optimisation of high-resolution three-dimensional (3D) medical X-ray imaging techniques are studied. A comparison is made of conventional attenuation-based X-ray imaging methods with the phase-contrast X-ray imaging modalities that have been developed recently. The results indicate that it is theoretically possible through optimal design of the X-ray imaging system to achieve high spatial resolution (<100 μm) in 3D medical X-ray imaging of the human body at a clinically acceptable dose level (<10 mGy) by introducing a phase-contrast X-ray imaging technique.

Diamond monochromator for high heat flux synchrotron x-ray beams

International Nuclear Information System (INIS)

Khounsary, A.M.; Smither, R.K.; Davey, S.; Purohit, A.

1992-12-01

Single crystal silicon has been the material of choice for x-ray monochromators for the past several decades. However, the need for suitable monochromators to handle the high heat load of the next generation synchrotron x-ray beams on the one hand and the rapid and on-going advances in synthetic diamond technology on the other make a compelling case for the consideration of a diamond mollochromator system. In this Paper, we consider various aspects, advantage and disadvantages, and promises and pitfalls of such a system and evaluate the comparative an monochromator subjected to the high heat load of the most powerful x-ray beam that will become available in the next few years. The results of experiments performed to evaluate the diffraction properties of a currently available synthetic single crystal diamond are also presented. Fabrication of diamond-based monochromator is within present technical means

High-resolution X-ray crystal structure of bovine H-protein using the high-pressure cryocooling method

International Nuclear Information System (INIS)

Higashiura, Akifumi; Ohta, Kazunori; Masaki, Mika; Sato, Masaru; Inaka, Koji; Tanaka, Hiroaki; Nakagawa, Atsushi

2013-01-01

Using the high-pressure cryocooling method, the high-resolution X-ray crystal structure of bovine H-protein was determined at 0.86 Å resolution. This is the first ultra-high-resolution structure obtained from a high-pressure cryocooled crystal. Recently, many technical improvements in macromolecular X-ray crystallography have increased the number of structures deposited in the Protein Data Bank and improved the resolution limit of protein structures. Almost all high-resolution structures have been determined using a synchrotron radiation source in conjunction with cryocooling techniques, which are required in order to minimize radiation damage. However, optimization of cryoprotectant conditions is a time-consuming and difficult step. To overcome this problem, the high-pressure cryocooling method was developed (Kim et al., 2005 ▶) and successfully applied to many protein-structure analyses. In this report, using the high-pressure cryocooling method, the X-ray crystal structure of bovine H-protein was determined at 0.86 Å resolution. Structural comparisons between high- and ambient-pressure cryocooled crystals at ultra-high resolution illustrate the versatility of this technique. This is the first ultra-high-resolution X-ray structure obtained using the high-pressure cryocooling method

Editorial: Focus on X-ray Beams with High Coherence

Science.gov (United States)

Robinson, Ian; Gruebel, Gerhard; Mochrie, Simon

2010-03-01

This editorial serves as the preface to a special issue of New Journal of Physics, which collects together solicited papers on a common subject, x-ray beams with high coherence. We summarize the issue's content, and explain why there is so much current interest both in the sources themselves and in the applications to the study of the structure of matter and its fluctuations (both spontaneous and driven). As this collection demonstrates, the field brings together accelerator physics in the design of new sources, particle physics in the design of detectors, and chemical and materials scientists who make use of the coherent beams produced. Focus on X-ray Beams with High Coherence Contents Femtosecond pulse x-ray imaging with a large field of view B Pfau, C M Günther, S Schaffert, R Mitzner, B Siemer, S Roling, H Zacharias, O Kutz, I Rudolph, R Treusch and S Eisebitt The FERMI@Elettra free-electron-laser source for coherent x-ray physics: photon properties, beam transport system and applications E Allaria, C Callegari, D Cocco, W M Fawley, M Kiskinova, C Masciovecchio and F Parmigiani Beyond simple exponential correlation functions and equilibrium dynamics in x-ray photon correlation spectroscopy Anders Madsen, Robert L Leheny, Hongyu Guo, Michael Sprung and Orsolya Czakkel The Coherent X-ray Imaging (CXI) instrument at the Linac Coherent Light Source (LCLS) Sébastien Boutet and Garth J Williams Dynamics and rheology under continuous shear flow studied by x-ray photon correlation spectroscopy Andrei Fluerasu, Pawel Kwasniewski, Chiara Caronna, Fanny Destremaut, Jean-Baptiste Salmon and Anders Madsen Exploration of crystal strains using coherent x-ray diffraction Wonsuk Cha, Sanghoon Song, Nak Cheon Jeong, Ross Harder, Kyung Byung Yoon, Ian K Robinson and Hyunjung Kim Coherence properties of the European XFEL G Geloni, E Saldin, L Samoylova, E Schneidmiller, H Sinn, Th Tschentscher and M Yurkov Fresnel coherent diffractive imaging: treatment and analysis of data G J

The superconducting high-resolution soft X-ray spectrometer at the advanced biological and environmental X-ray facility

Energy Technology Data Exchange (ETDEWEB)

Friedrich, S. [Advanced Detector Group, Lawrence Livermore National Laboratory, 7000 East Avenue, L-188, Livermore, CA 94550 (United States); Advanced Biological and Environmental X-ray Facility, Lawrence Berkeley National Laboratory, 1 Cyclotron Road, MS 6-2100, Berkeley, CA 94720 (United States)], E-mail: Friedrich1@llnl.gov; Drury, O.B. [Advanced Detector Group, Lawrence Livermore National Laboratory, 7000 East Avenue, L-188, Livermore, CA 94550 (United States); Advanced Biological and Environmental X-ray Facility, Lawrence Berkeley National Laboratory, 1 Cyclotron Road, MS 6-2100, Berkeley, CA 94720 (United States); Biophysics Group, University of California, 1 Shields Avenue, EU-III, Davis, CA 95616 (United States); George, S.J. [Advanced Biological and Environmental X-ray Facility, Lawrence Berkeley National Laboratory, 1 Cyclotron Road, MS 6-2100, Berkeley, CA 94720 (United States); Cramer, S.P. [Advanced Biological and Environmental X-ray Facility, Lawrence Berkeley National Laboratory, 1 Cyclotron Road, MS 6-2100, Berkeley, CA 94720 (United States); Biophysics Group, University of California, 1 Shields Avenue, EU-III, Davis, CA 95616 (United States)

2007-11-11

We have built a 36-pixel superconducting tunnel junction X-ray spectrometer for chemical analysis of dilute samples in the soft X-ray band. It offers an energy resolution of {approx}10-20 eV FWHM below 1 keV, a solid angle coverage of {approx}10{sup -3}, and can be operated at total rates of up to {approx}10{sup 6} counts/s. Here, we describe the spectrometer performance in speciation measurements by fluorescence-detected X-ray absorption spectroscopy at the Advanced Biological and Environmental X-ray facility at the ALS synchrotron.

X-ray imaging for studying behavior of liquids at high pressures and high temperatures using Paris-Edinburgh press

International Nuclear Information System (INIS)

Kono, Yoshio; Kenney-Benson, Curtis; Park, Changyong; Shen, Guoyin; Shibazaki, Yuki; Wang, Yanbin

2015-01-01

Several X-ray techniques for studying structure, elastic properties, viscosity, and immiscibility of liquids at high pressures have been integrated using a Paris-Edinburgh press at the 16-BM-B beamline of the Advanced Photon Source. Here, we report the development of X-ray imaging techniques suitable for studying behavior of liquids at high pressures and high temperatures. White X-ray radiography allows for imaging phase separation and immiscibility of melts at high pressures, identified not only by density contrast but also by phase contrast imaging in particular for low density contrast liquids such as silicate and carbonate melts. In addition, ultrafast X-ray imaging, at frame rates up to ∼10 5 frames/second (fps) in air and up to ∼10 4 fps in Paris-Edinburgh press, enables us to investigate dynamics of liquids at high pressures. Very low viscosities of melts similar to that of water can be reliably measured. These high-pressure X-ray imaging techniques provide useful tools for understanding behavior of liquids or melts at high pressures and high temperatures

X-ray imaging for studying behavior of liquids at high pressures and high temperatures using Paris-Edinburgh press

Energy Technology Data Exchange (ETDEWEB)

Kono, Yoshio; Kenney-Benson, Curtis; Park, Changyong; Shen, Guoyin [HPCAT, Geophysical Laboratory, Carnegie Institution of Washington, 9700 S. Cass Ave., Argonne, Illinois 60439 (United States); Shibazaki, Yuki [Frontier Research Institute for Interdisciplinary Sciences, Tohoku University, Aramaki aza Aoba 6-3, Aoba-ku, Sendai 980-8578 (Japan); Wang, Yanbin [GeoSoilEnviroCARS, Center for Advanced Radiation Sources, The University of Chicago, 5640 S. Ellis Avenue, Chicago, Illinois 60637 (United States)

2015-07-15

Several X-ray techniques for studying structure, elastic properties, viscosity, and immiscibility of liquids at high pressures have been integrated using a Paris-Edinburgh press at the 16-BM-B beamline of the Advanced Photon Source. Here, we report the development of X-ray imaging techniques suitable for studying behavior of liquids at high pressures and high temperatures. White X-ray radiography allows for imaging phase separation and immiscibility of melts at high pressures, identified not only by density contrast but also by phase contrast imaging in particular for low density contrast liquids such as silicate and carbonate melts. In addition, ultrafast X-ray imaging, at frame rates up to ∼10{sup 5} frames/second (fps) in air and up to ∼10{sup 4} fps in Paris-Edinburgh press, enables us to investigate dynamics of liquids at high pressures. Very low viscosities of melts similar to that of water can be reliably measured. These high-pressure X-ray imaging techniques provide useful tools for understanding behavior of liquids or melts at high pressures and high temperatures.

Dual-energy X-ray radiography for automatic high-Z material detection

International Nuclear Information System (INIS)

Chen Gongyin; Bennett, Gordon; Perticone, David

2007-01-01

There is an urgent need for high-Z material detection in cargo. Materials with Z > 74 can indicate the presence of fissile materials or radiation shielding. Dual (high) energy X-ray material discrimination is based on the fact that different materials have different energy dependence in X-ray attenuation coefficients. This paper introduces the basic physics and analyzes the factors that affect dual-energy material discrimination performance. A detection algorithm is also discussed

Differences of X-ray exposure between X-ray diagnostics with a conventional X-ray screen-system and with an image-intensifier-television-unit

International Nuclear Information System (INIS)

Loehr, H.; Vogel, H.; Reinhart, J.; Jantzen, R.

1977-01-01

During X-ray diagnostics of patients in the II. Medizinische Poliklinik the X-ray exposure was determined. It corresponded to the data described in literature. Two groups were compared: 518 patients examined with a conventional X-ray screen-system and 642 patients examined with an image-intensifier-television-system. The results demonstrated that with exception of thoracical X-ray examination the replacing of the old system by the television system brought a remarkable increase of the X-ray exposure. The doses depended of the patients constitution to a high degree. (orig.) [de

X pinch a point x-ray source

International Nuclear Information System (INIS)

Garg, A.B.; Rout, R.K.; Shyam, A.; Srinivasan, M.

1993-01-01

X ray emission from an X pinch, a point x-ray source has been studied using a pin-hole camera by a 30 kV, 7.2 μ F capacitor bank. The wires of different material like W, Mo, Cu, S.S.(stainless steel) and Ti were used. Molybdenum pinch gives the most intense x-rays and stainless steel gives the minimum intensity x-rays for same bank energy (∼ 3.2 kJ). Point x-ray source of size (≤ 0.5 mm) was observed using pin hole camera. The size of the source is limited by the size of the pin hole camera. The peak current in the load is approximately 150 kA. The point x-ray source could be useful in many fields like micro lithography, medicine and to study the basic physics of high Z plasmas. (author). 4 refs., 3 figs

High-energy X-ray diffraction studies of short- and intermediate-range structure in oxide glasses

International Nuclear Information System (INIS)

Suzuya, Kentaro

2002-01-01

The feature of high-energy X-ray diffraction method is explained. The oxide glasses studies by using BL04B2, high-energy X-ray diffraction beam line of SPring-8, and the random system materials by high-energy monochromatic X-ray diffraction are introduced. An advantage of third generation synchrotron radiation is summarized. On SPring-8, the high-energy X-ray diffraction experiments of random system are carried out by BL04B2 and BL14B1 beam line. BL04B2 can select Si (111)(E=37.8 keV, λ=0.033 nm) and Si(220)(E=61.7 keV, λ=0.020 nm) as Si monochromator. The intermediate-range structure of (MgO) x (P 2 O 5 ) 1-x glass ,MgP 2 O 6 glass, B 2 O 3 glass, SiO 2 and GeO 2 are explained in detail. The future and application of high-energy X-ray diffraction are stated. (S.Y.)

Special issue on compact x-ray sources

Science.gov (United States)

Hooker, Simon; Midorikawa, Katsumi; Rosenzweig, James

2014-04-01

Journal of Physics B: Atomic, Molecular and Optical Physics is delighted to announce a forthcoming special issue on compact x-ray sources, to appear in the winter of 2014, and invites you to submit a paper. The potential for high-brilliance x- and gamma-ray sources driven by advanced, compact accelerators has gained increasing attention in recent years. These novel sources—sometimes dubbed 'fifth generation sources'—will build on the revolutionary advance of the x-ray free-electron laser (FEL). New radiation sources of this type have widespread applications, including in ultra-fast imaging, diagnostic and therapeutic medicine, and studies of matter under extreme conditions. Rapid advances in compact accelerators and in FEL techniques make this an opportune moment to consider the opportunities which could be realized by bringing these two fields together. Further, the successful development of compact radiation sources driven by compact accelerators will be a significant milestone on the road to the development of high-gradient colliders able to operate at the frontiers of particle physics. Thus the time is right to publish a peer-reviewed collection of contributions concerning the state-of-the-art in: advanced and novel acceleration techniques; sophisticated physics at the frontier of FELs; and the underlying and enabling techniques of high brightness electron beam physics. Interdisciplinary research connecting two or more of these fields is also increasingly represented, as exemplified by entirely new concepts such as plasma based electron beam sources, and coherent imaging with fs-class electron beams. We hope that in producing this special edition of Journal of Physics B: Atomic, Molecular and Optical Physics (iopscience.iop.org/0953-4075/) we may help further a challenging mission and ongoing intellectual adventure: the harnessing of newly emergent, compact advanced accelerators to the creation of new, agile light sources with unprecedented capabilities

Ultra-high vacuum compatible optical chopper system for synchrotron x-ray scanning tunneling microscopy

Energy Technology Data Exchange (ETDEWEB)

Chang, Hao, E-mail: hc000211@ohio.edu [Advanced Photon Source, Argonne National Laboratory, 9700 South Cass Avenue, Argonne, Illinois 60439 (United States); Nanoscale and Quantum Phenomena Institute, Physics & Astronomy Department, Ohio University, Athens, Ohio 45701 (United States); Cummings, Marvin; Shirato, Nozomi; Stripe, Benjamin; Preissner, Curt; Freeland, John W. [Advanced Photon Source, Argonne National Laboratory, 9700 South Cass Avenue, Argonne, Illinois 60439 (United States); Rosenmann, Daniel [Center for Nanoscale Materials, Argonne National Laboratory, 9700 South Cass Avenue, Argonne, Illinois 60439 (United States); Kersell, Heath; Hla, Saw-Wai [Nanoscale and Quantum Phenomena Institute, Physics & Astronomy Department, Ohio University, Athens, Ohio 45701 (United States); Center for Nanoscale Materials, Argonne National Laboratory, 9700 South Cass Avenue, Argonne, Illinois 60439 (United States); Rose, Volker, E-mail: vrose@anl.gov [Advanced Photon Source, Argonne National Laboratory, 9700 South Cass Avenue, Argonne, Illinois 60439 (United States); Center for Nanoscale Materials, Argonne National Laboratory, 9700 South Cass Avenue, Argonne, Illinois 60439 (United States)

2016-01-28

High-speed beam choppers are a crucial part of time-resolved x-ray studies as well as a necessary component to enable elemental contrast in synchrotron x-ray scanning tunneling microscopy (SX-STM). However, many chopper systems are not capable of operation in vacuum, which restricts their application to x-ray studies with high photon energies, where air absorption does not present a significant problem. To overcome this limitation, we present a fully ultra-high vacuum (UHV) compatible chopper system capable of operating at variable chopping frequencies up to 4 kHz. The lightweight aluminum chopper disk is coated with Ti and Au films to provide the required beam attenuation for soft and hard x-rays with photon energies up to about 12 keV. The chopper is used for lock-in detection of x-ray enhanced signals in SX-STM.

X-ray speckle correlation interferometer

International Nuclear Information System (INIS)

Eisenhower, Rachel; Materlik, Gerhard

2000-01-01

Speckle Pattern Correlation Interferometry (SPCI) is a well-established technique in the visible-light regime for observing surface disturbances. Although not a direct imaging technique, SPCI gives full-field, high-resolution information about an object's motion. Since x-ray synchrotron radiation beamlines with high coherent flux have allowed the observation of x-ray speckle, x-ray SPCI could provide a means to measure strains and other quasi-static motions in disordered systems. This paper therefore examines the feasibility of an x-ray speckle correlation interferometer

X-ray filter for x-ray powder diffraction

Science.gov (United States)

Sinsheimer, John Jay; Conley, Raymond P.; Bouet, Nathalie C. D.; Dooryhee, Eric; Ghose, Sanjit

2018-01-23

Technologies are described for apparatus, methods and systems effective for filtering. The filters may comprise a first plate. The first plate may include an x-ray absorbing material and walls defining first slits. The first slits may include arc shaped openings through the first plate. The walls of the first plate may be configured to absorb at least some of first x-rays when the first x-rays are incident on the x-ray absorbing material, and to output second x-rays. The filters may comprise a second plate spaced from the first plate. The second plate may include the x-ray absorbing material and walls defining second slits. The second slits may include arc shaped openings through the second plate. The walls of the second plate may be configured to absorb at least some of second x-rays and to output third x-rays.

Computerized tomography using high resolution X-ray imaging system with a microfocus source

International Nuclear Information System (INIS)

Zaprazny, Z.; Korytar, D.; Konopka, P.; Ac, V.; Bielecki, J.

2011-01-01

In recent years there is an effort to image an internal structure of an object by using not only conventional 2D X-ray radiography but also using high resolution 3D tomography which is based on reconstruction of multiple 2D projections at various angular positions of the object. We have previously reported [1] the development and basic parameters of a high resolution x-ray imaging system with a microfocus source. We report the recent progress using this high resolution X-ray laboratory system in this work. These first findings show that our system is particularly suitable for light weight and nonmetallic objects such as biological objects, plastics, wood, paper, etc. where phase contrast helps to increase the visibility of the finest structures of the object. Phase-contrast X-ray Computerized Tomography is of our special interest because it is an emerging imaging technique that can be implemented at third generation synchrotron radiation sources and also in laboratory conditions using a microfocus X-ray tube or beam conditioning optics. (authors)

Molybdenum cell for x-ray diffraction measurements of fluid alkali metals at high temperatures and high pressures

Science.gov (United States)

Matsuda, Kazuhiro; Tamura, Kozaburo; Katoh, Masahiro; Inui, Masanori

2004-03-01

We have developed a sample cell for x-ray diffraction measurements of fluid alkali metals at high temperatures and high pressures. All parts of the cell are made of molybdenum which is resistant to the chemical corrosion of alkali metals. Single crystalline molybdenum disks electrolytically thinned down to 40 μm were used as the walls of the cell through which x rays pass. The crystal orientation of the disks was controlled in order to reduce the background from the cell. All parts of the cell were assembled and brazed together using a high-temperature Ru-Mo alloy. Energy dispersive x-ray diffraction measurements have been successfully carried out for fluid rubidium up to 1973 K and 16.2 MPa. The obtained S(Q) demonstrates the applicability of the molybdenum cell to x-ray diffraction measurements of fluid alkali metals at high temperatures and high pressures.

Stabilized x-ray generator power supply

International Nuclear Information System (INIS)

Saha, Subimal; Purushotham, K.V.; Bose, S.K.

1986-01-01

X-ray diffraction and X-ray fluorescence analysis are very much adopted in laboratories to determine the type and structure of the constituent compounds in solid materials, chemical composition of materials, stress developed on metals etc. These experiments need X-ray beam of fixed intensity and wave length. This can only be achieved by X-ray generator having highly stabilized tube voltage and tube current. This paper describes how X-ray tube high voltage and electron beam current are stabilized. This paper also highlights generation of X-rays, diffractometry and X-ray fluorescence analysis and their wide applications. Principle of operation for stabilizing the X-ray tube voltage and current, different protection circuits adopted, special features of the mains H.V. transformer and H.T. tank are described in this report. (author)

A versatile, highly-efficient, high-resolution von Hamos Bragg crystal x-ray spectrometer

International Nuclear Information System (INIS)

Vane, C.R.; Smith, M.S.; Raman, S.

1988-01-01

An efficient, high-resolution, vertical-focusing, Bragg crystal x-ray spectrometer has been specifically designed and constructed for use in measurements of x rays produced in collisions of energetic heavy ions. In this report the design and resulting operational characteristics of the final instrument are fully described. A wide variety of sample data is also included to illustrate the utility of this device in several areas of research. 14 refs., 38 figs

A POPULATION OF X-RAY WEAK QUASARS: PHL 1811 ANALOGS AT HIGH REDSHIFT

International Nuclear Information System (INIS)

Wu Jianfeng; Brandt, W. N.; Schneider, Donald P.; Hall, Patrick B.; Gibson, Robert R.; Schmidt, Sarah J.; Richards, Gordon T.; Shemmer, Ohad; Just, Dennis W.

2011-01-01

We report the results from Chandra and XMM-Newton observations of a sample of 10 type 1 quasars selected to have unusual UV emission-line properties (weak and blueshifted high-ionization lines; strong UV Fe emission) similar to those of PHL 1811, a confirmed intrinsically X-ray weak quasar. These quasars were identified by the Sloan Digital Sky Survey at high redshift (z ∼ 2.2); eight are radio quiet while two are radio intermediate. All of the radio-quiet PHL 1811 analogs, without exception, are notably X-ray weak by a mean factor of ∼13. These sources lack broad absorption lines and have blue UV/optical continua, supporting the hypothesis that they are intrinsically X-ray weak like PHL 1811 itself. However, their average X-ray spectrum appears to be harder than those of typical quasars, which may indicate the presence of heavy intrinsic X-ray absorption. Our sample of radio-quiet PHL 1811 analogs supports a connection between an X-ray weak spectral energy distribution and PHL 1811-like UV emission lines; this connection provides an economical way to identify X-ray weak type 1 quasars. The fraction of radio-quiet PHL 1811 analogs in the radio-quiet quasar population is estimated to be ∼< 1.2%. We have investigated correlations between relative X-ray brightness and UV emission-line properties (e.g., C IV equivalent width and blueshift) for a sample combining our radio-quiet PHL 1811 analogs, PHL 1811 itself, and typical type 1 quasars. These correlation analyses suggest that PHL 1811 analogs may have extreme wind-dominated broad emission-line regions. Observationally, the radio-quiet PHL 1811 analogs appear to be a subset (∼30%) of radio-quiet weak-line quasars (WLQs). The existence of a subset of quasars in which high-ionization 'shielding gas' covers most of the broad emission-line region (BELR), but little more than the BELR, could potentially unify the PHL 1811 analogs and WLQs. The two radio-intermediate PHL 1811 analogs are X-ray bright. X-ray

Advances in indirect detector systems for ultra high-speed hard X-ray imaging with synchrotron light

Science.gov (United States)

Olbinado, M. P.; Grenzer, J.; Pradel, P.; De Resseguier, T.; Vagovic, P.; Zdora, M.-C.; Guzenko, V. A.; David, C.; Rack, A.

2018-04-01

We report on indirect X-ray detector systems for various full-field, ultra high-speed X-ray imaging methodologies, such as X-ray phase-contrast radiography, diffraction topography, grating interferometry and speckle-based imaging performed at the hard X-ray imaging beamline ID19 of the European Synchrotron—ESRF. Our work highlights the versatility of indirect X-ray detectors to multiple goals such as single synchrotron pulse isolation, multiple-frame recording up to millions frames per second, high efficiency, and high spatial resolution. Besides the technical advancements, potential applications are briefly introduced and discussed.

X-ray fluorescence imaging with polycapillary X-ray optics

International Nuclear Information System (INIS)

Yonehara, Tasuku; Yamaguchi, Makoto; Tsuji, Kouichi

2010-01-01

X-ray fluorescence spectrometry imaging is a powerful tool to provide information about the chemical composition and elemental distribution of a specimen. X-ray fluorescence spectrometry images were conventionally obtained by using a μ-X-ray fluorescence spectrometry spectrometer, which requires scanning a sample. Faster X-ray fluorescence spectrometry imaging would be achieved by eliminating the process of sample scanning. Thus, we developed an X-ray fluorescence spectrometry imaging instrument without sample scanning by using polycapillary X-ray optics, which had energy filter characteristics caused by the energy dependence of the total reflection phenomenon. In the present paper, we show that two independent straight polycapillary X-ray optics could be used as an energy filter of X-rays for X-ray fluorescence. Only low energy X-rays were detected when the angle between the two optical axes was increased slightly. Energy-selective X-ray fluorescence spectrometry images with projection mode were taken by using an X-ray CCD camera equipped with two polycapillary optics. It was shown that Fe Kα (6.40 keV) and Cu Kα (8.04 keV) could be discriminated for Fe and Cu foils.

Short-time X-ray diffraction with an efficient-optimized, high repetition-rate laser-plasma X-ray-source

International Nuclear Information System (INIS)

Kaehle, Stephan

2009-01-01

This thesis deals with the production and application of ultrashort X-ray pulses. In the beginning different possibilities for the production of X-ray pulses with pulse durations of below one picosecond are presented, whereby the main topic lies on the so called laser-plasma X-ray sources with high repetition rate. In this case ultrashort laser pulses are focused on a metal, so that in the focus intensities of above 10 16 W/cm 2 dominate. In the ideal case in such way ultrafast electrons are produced, which are responsible for line radiation. In these experiments titanium K α radiation is produced, thes photons possess an energy of 4.51 keV. For the efficient production of line radiation here the Ti:Sa laser is optimized in view of the laser energy and the pulse shape and the influence of the different parameters on the K α production systematically studied. The influences of laser intensity, system-conditioned pre-pulses and of phase modulation are checked. It turns out that beside the increasement of the K α radiation by a suited laser intensity a reduction of the X-ray background radiation is of deciding importance for the obtaining of clear diffraction images. This background radiation is mainly composed of bremsstrahlung. It can be suppressed by the avoidance of intrinsic pre-pulses and by means of 2nd-order phase modulation. By means of optical excitation and X-ray exploration experiments the production of acoustic waves after ultrashort optical excitation in a 150 nm thick Ge(111) film on Si(111) is studied. These acoustic waves are driven by thermal (in this time scale time-independent) and electronic (time dependent) pressure amounts. As essential results it turns out that the relative amount of the electronic pressure increases with decreasing excitation density [de

High resolution krypton M/sub 4,5/ x-ray emission spectra

International Nuclear Information System (INIS)

Perera, R.C.C.; Hettrick, M.C.; Lindle, D.W.

1987-10-01

High resolution M/sub 4,5/ (3d → 4p) x-ray emission spectra from a krypton plasma were measured using a recently developed grazing-incidence reflection-grating monochromator/spectrometer with very high flux rates at extreme ultraviolet and soft x-ray wave lengths. The nominal resolving power of the instrument, E/ΔE, is about 300 in this energy range (∼80 eV). Three dipole-allowed 3d → 4p emission lines were observed at 80.98 eV, 80.35 eV and 79.73 eV. A broad peak at about 82.3 eV is tentatively assigned to transitions resulting from Kr 2+ , and effects of excitation energy on M/sub 4,5/ x-ray emission were observed. 9 refs., 3 figs., 1 tab

High-speed X-ray phase tomography with Talbot interferometer and fringe scanning method

International Nuclear Information System (INIS)

Kibayashi, Shunsuke; Harasse, Sébastien; Yashiro, Wataru; Momose, Atsushi

2012-01-01

High-speed X-ray phase tomography based on the Fourier-transform method has been demonstrated with an X-ray Talbot interferometer using white synchrotron radiation. We report the experimental results of high-speed X-ray phase tomography with fringe-scanning method instead of Fourier-transform method to improve spatial resolution without a considerable increase of scan time. To apply fringe-scanning method to high speed tomography, we tested a scan that is a synchronous combination of one-way continuous movements of the sample rotation and the grating displacement. When this scanning method was combined with X-ray phase tomography, we were able to obtain a scan time of 5 s. A comparison of the image quality derived with the conventional approach and with the proposed approach using the fringe-scanning method showed that the latter had better spatial resolution.

High-resolution X-ray spectra from low-temperature, highly charged ions

International Nuclear Information System (INIS)

Beiersdorfer, P.

1996-09-01

The electron beam ion traps (EBIT) at Livermore were designed for studying the x-ray emission of highly charged ions produced and excited by a monoenergetic electron beam. The precision with which the x-ray emission can be analyzed has recently been increased markedly when it became possible to decouple the temperature of the ions from the energy of the electron beam by several orders of magnitude. By adjusting the trap parameters, ion temperatures as low as 15.8±4.4 eV for Ti 20+ and 59.4±9.9 eV for Cs 45+ were achieved. These temperatures were more than two orders of magnitude lower than the energy of the multi-keV electron beam used for the production and excitation of the ions. A discussion of the techniques used to produce and study low-temperature highly charged ions is presented in this progress report. The low ion temperatures enabled measurements heretofore impossible. As an example, a direct observation of the natural line width of fast electric dipole allowed x-ray transitions is described. From the observed natural line width and b making use of the time-energy relations of the uncertainty principle we were able to determine a radiative transition rate of 1.65 fs for the 2p-3d resonance transition in neonlike Cs 45+ . A brief discussion of other high-precision measurements enabled by our new technique is also given

TU-G-207-03: High Spatial Resolution and High Sensitivity X-Ray Fluorescence Imaging

International Nuclear Information System (INIS)

Xing, L.

2015-01-01

Last few years has witnessed the development of novel of X-ray imaging modalities, such as spectral CT, phase contrast CT, and X-ray acoustic/fluorescence/luminescence imaging. This symposium will present the recent advances of these emerging X-ray imaging modalities and update the attendees with knowledge in various related topics, including X-ray photon-counting detectors, X-ray physics underlying the emerging applications beyond the traditional X-ray imaging, image reconstruction for the novel modalities, characterization and evaluation of the systems, and their practical implications. In addition, the concept and practical aspects of X-ray activatable targeted nanoparticles for molecular X-ray imaging will be discussed in the context of X-ray fluorescence and luminescence CT. Learning Objectives: Present background knowledge of various emerging X-ray imaging techniques, such as spectral CT, phase contrast CT and X-ray fluorescence/luminescence CT. Discuss the practical need, technical aspects and current status of the emerging X-ray imaging modalities. Describe utility and future impact of the new generation of X-ray imaging applications

Modulated High-Energy Gamma-Ray Emission from the Micro-quasar Cygnus X-3

International Nuclear Information System (INIS)

Abdo, A.A.; Cheung, C.C.; Dermer, C.D.; Grove, J.E.; Johnson, W.N.; Lovellette, M.N.; Makeev, A.; Ray, P.S.; Strickman, M.S.; Wood, K.S.; Abdo, A.A.; Cheung, C.C.; Ackermann, M.; Ajello, M.; Bechtol, K.; Berenji, B.; Blandford, R.D.; Bloom, E.D.; Borgland, A.W.; Cameron, R.A.; Chiang, J.; Claus, R.; Digel, S.W.; Silva, E.D.E.; Drell, P.S.; Dubois, R.; Focke, W.B.; Glanzman, T.; Godfrey, G.; Hayashida, M.; Johannesson, G.; Johnson, A.S.; Kamae, T.; Kocian, M.L.; Lande, J.; Madejski, G.M.; Michelson, P.F.; Mitthumsiri, W.; Monzani, M.E.; Moskalenko, I.V.; Murgia, S.; Nolan, P.L.; Paneque, D.; Reimer, A.; Reimer, O.; Rochester, L.S.; Romani, R.W.; Tanaka, T.; Thayer, J.B.; Tramacere, A.; Uchiyama, Y.; Usher, T.L.; Waite, A.P.; Wang, P.; Ackermann, M.; Ajello, M.; Bechtol, K.; Berenji, B.; Blandford, R.D.; Bloom, E.D.; Borgland, A.W.; Cameron, R.A.; Chiang, J.; Claus, R.; Digel, S.W.; Silva, E.D.E.; Drell, P.S.; Dubois, R.; Focke, W.B.; Glanzman, T.; Godfrey, G.; Hayashida, M.; Johannesson, G.; Johnson, A.S.; Kamae, T.; Kocian, M.L.; Lande, J.; Madejski, G.M.; Michelson, P.F.; Mitthumsiri, W.; Monzani, M.E.; Moskalenko, I.V.; Murgia, S.; Nolan, P.L.; Paneque, D.; Reimer, A.; Reimer, O.; Rochester, L.S.; Romani, R.W.; Tanaka, T.; Thayer, J.B.; Tramacere, A.; Uchiyama, Y.; Usher, T.L.; Waite, A.P.; Wang, P.; Axelsson, M.; Hjalmarsdotter, L.; Axelsson, M.; Conrad, J.; Hjalmarsdotter, L.; Jackson, M.S.; Meurer, C.; Ryde, F.; Ylinen, T.; Baldini, L.; Bellazzini, R.; Brez, A.; Kuss, M.; Latronico, L.; Omodei, N.; Pesce-Rollins, M.; Razzano, M.; Sgro, C.; Ballet, J.; Casandjian, J.M.; Chaty, S.; Corbel, S.; Grenier, I.A.; Koerding, E.; Rodriguez, J.; Starck, J.L.; Tibaldo, L.

2009-01-01

Micro-quasars are accreting black holes or neutron stars in binary systems with associated relativistic jets. Despite their frequent outburst activity, they have never been unambiguously detected emitting high-energy gamma rays. The Fermi Large Area Telescope (LAT) has detected a variable high-energy source coinciding with the position of the x-ray binary and micro-quasar Cygnus X-3. Its identification with Cygnus X-3 is secured by the detection of its orbital period in gamma rays, as well as the correlation of the LAT flux with radio emission from the relativistic jets of Cygnus X-3. The gamma-ray emission probably originates from within the binary system, opening new areas in which to study the formation of relativistic jets. (authors)

X-ray apparatus

International Nuclear Information System (INIS)

Bernstein, S.; Stagg, L.; Lambert, T.W.; Griswa, P.J.

1976-01-01

A patient support system for X-ray equipment in arteriographic studies of the heart is described in detail. The support system has been designed to overcome many of the practical problems encountered in using previous types of arteriographic X-ray equipment. The support system is capable of horizontal movement and, by a series of shafts attached to the main support system, the X-ray source and image intensifier or detector may be rotated through the same angle. The system is highly flexible and details are given of several possible operational modes. (U.K.)

Simulation of high-resolution X-ray microscopic images for improved alignment

International Nuclear Information System (INIS)

Song Xiangxia; Zhang Xiaobo; Liu Gang; Cheng Xianchao; Li Wenjie; Guan Yong; Liu Ying; Xiong Ying; Tian Yangchao

2011-01-01

The introduction of precision optical elements to X-ray microscopes necessitates fine realignment to achieve optimal high-resolution imaging. In this paper, we demonstrate a numerical method for simulating image formation that facilitates alignment of the source, condenser, objective lens, and CCD camera. This algorithm, based on ray-tracing and Rayleigh-Sommerfeld diffraction theory, is applied to simulate the X-ray microscope beamline U7A of National Synchrotron Radiation Laboratory (NSRL). The simulations and imaging experiments show that the algorithm is useful for guiding experimental adjustments. Our alignment simulation method is an essential tool for the transmission X-ray microscope (TXM) with optical elements and may also be useful for the alignment of optical components in other modes of microscopy.

Digital signal processors for cryogenic high-resolution x-ray detector readout

International Nuclear Information System (INIS)

Friedrich, Stephan; Drury, Owen B.; Bechstein, Sylke; Hennig, Wolfgang; Momayezi, Michael

2003-01-01

We are developing fast digital signal processors (DSPs) to read out superconducting high-resolution X-ray detectors with on-line pulse processing. For superconducting tunnel junction (STJ) detector read-out, the DSPs offer online filtering, rise time discrimination and pile-up rejection. Compared to analog pulse processing, DSP readout somewhat degrades the detector resolution, but improves the spectral purity of the detector response. We discuss DSP performance with our 9-channel STJ array for synchrotron-based high-resolution X-ray spectroscopy. (author)

Cellulose/inorganic-composite fibers for producing textile fabrics of high X-ray absorption properties

Energy Technology Data Exchange (ETDEWEB)

Günther, Karoline; Giebing, Christina; Askani, Antonia [FTB, Hochschule Niederrhein – University of Applied Science, Faculty of Textile and Clothing Technology, Webschulstr. 31, 41065 Mönchengladbach (Germany); Leisegang, Tilmann [Saxray GmbH, Maria-Reiche-Str. 1, 01109 Dresden (Germany); Krieg, Marcus [TITK, Thüringisches Institut für Textil- und Kunststoff-Forschung e.V., Breitscheidstraße 97, 07407 Rudolstadt (Germany); Kyosev, Yordan; Weide, Thomas [FTB, Hochschule Niederrhein – University of Applied Science, Faculty of Textile and Clothing Technology, Webschulstr. 31, 41065 Mönchengladbach (Germany); Mahltig, Boris, E-mail: Boris.Mahltig@hs-niederrhein.de [FTB, Hochschule Niederrhein – University of Applied Science, Faculty of Textile and Clothing Technology, Webschulstr. 31, 41065 Mönchengladbach (Germany)

2015-11-01

Common textile materials as cotton or polyester do not possess reliable X-ray absorption properties. This is due to their morphology and chemical composition in particular. Common fibers are built up from organic polymers containing mainly the elements carbon, hydrogen, oxygen and nitrogen. These “light” elements only have low X-ray absorption coefficients. In contrast, inorganic materials composed of “heavy” elements with high atomic numbers, e.g. barium or bismuth, exhibit X-ray absorption coefficients higher by up to two orders of magnitude. To obtain a flexible yarn with high X-ray absorption properties both these materials, the organic polymer and the inorganic X-ray absorber, are combined to an inorganic/organic composite fiber material. Hence, as the organic component cellulose from modified Lyocell-process is used as carrier fiber and blended with inorganic absorber particles of low toxicity and high absorption coefficients, as bariumsulphate, bariumtitanate or bismuthoxide. A content of inorganic absorber particles equally distributed in the whole fiber of up to 20% is achieved. The composite fibers are produced as staple or filament fibers and processed to multifilament or staple fiber yarns. The staple fiber yarns are rotor-spinned to increase the comfort of the subsequent textile material. Several woven fabrics, considering multilayer structure and different warp/weft density, are developed. The energy dependent X-ray shielding properties are determined in dependence on the different yarn compositions, yarn types and structural parameters of the woven fabrics. As a result, a production process of textile materials with comfortable and dedicated X-ray absorption properties is established. It offers a promising opportunity for manufacturing of specialized textiles, working clothes or uniforms applicable for medicine, air craft and security personal, mining as well as for innovative composite materials. - Highlights: • Preparation of cellulosic

Cellulose/inorganic-composite fibers for producing textile fabrics of high X-ray absorption properties

International Nuclear Information System (INIS)

Günther, Karoline; Giebing, Christina; Askani, Antonia; Leisegang, Tilmann; Krieg, Marcus; Kyosev, Yordan; Weide, Thomas; Mahltig, Boris

2015-01-01

Common textile materials as cotton or polyester do not possess reliable X-ray absorption properties. This is due to their morphology and chemical composition in particular. Common fibers are built up from organic polymers containing mainly the elements carbon, hydrogen, oxygen and nitrogen. These “light” elements only have low X-ray absorption coefficients. In contrast, inorganic materials composed of “heavy” elements with high atomic numbers, e.g. barium or bismuth, exhibit X-ray absorption coefficients higher by up to two orders of magnitude. To obtain a flexible yarn with high X-ray absorption properties both these materials, the organic polymer and the inorganic X-ray absorber, are combined to an inorganic/organic composite fiber material. Hence, as the organic component cellulose from modified Lyocell-process is used as carrier fiber and blended with inorganic absorber particles of low toxicity and high absorption coefficients, as bariumsulphate, bariumtitanate or bismuthoxide. A content of inorganic absorber particles equally distributed in the whole fiber of up to 20% is achieved. The composite fibers are produced as staple or filament fibers and processed to multifilament or staple fiber yarns. The staple fiber yarns are rotor-spinned to increase the comfort of the subsequent textile material. Several woven fabrics, considering multilayer structure and different warp/weft density, are developed. The energy dependent X-ray shielding properties are determined in dependence on the different yarn compositions, yarn types and structural parameters of the woven fabrics. As a result, a production process of textile materials with comfortable and dedicated X-ray absorption properties is established. It offers a promising opportunity for manufacturing of specialized textiles, working clothes or uniforms applicable for medicine, air craft and security personal, mining as well as for innovative composite materials. - Highlights: • Preparation of cellulosic

Fine-pitch glass GEM for high-resolution X-ray imaging

International Nuclear Information System (INIS)

Fujiwara, T.; Toyokawa, H.; Mitsuya, Y.

2016-01-01

We have developed a fine-pitch glass gas electron multiplier (G-GEM) for high-resolution X-ray imaging. The fine-pitch G-GEM is made of a 400 μm thick photo-etchable glass substrate with 150 μm pitch holes. It is fabricated using the same wet etching technique as that for the standard G-GEM. In this work, we present the experimental results obtained with a single fine-pitch G-GEM with a 50 × 50 mm 2 effective area. We recorded an energy resolution of 16.2% and gas gain up to 5,500 when the detector was irradiated with 5.9 keV X-rays. We present a 50 × 50 mm 2 X-ray radiograph image acquired with a scintillation gas and optical readout system.

Effects of X-ray tube parameters on thickness measure precision in X-ray profile gauge

International Nuclear Information System (INIS)

Miao Jichen; Wu Zhifang; Xing Guilai

2011-01-01

Instantaneous profile gauge technology has been widely used in metallurgy industry because it can on-line get the profile of steel strip. It has characters of high measure precision and wide measure range, but the X-ray tube parameters only can be set few different values during measurement. The relations of thickness measure precision and X-ray tube current, X-ray tube voltage were analyzed. The results show that the X-ray tube current affects the thickness measure precision and the X-ray tube voltage determines the thickness measure range. The method of estimating the X-ray current by thickness measure precision was provided in the end. This method is the base of X-ray source selection and X-ray source parameter's setting in the instantaneous profile gauge. (authors)

X-ray Diffraction Study of Arsenopyrite at High Pressure

Energy Technology Data Exchange (ETDEWEB)

D Fan; M Ma; W Zhou; S Wei; Z Chen; H Xie

2011-12-31

The high-pressure X-ray diffraction study of a natural arsenopyrite was investigated up to 28.2 GPa using in situ angle-dispersive X-ray diffraction and a diamond anvil cell at National Synchrotron Light Source, Brookhaven National Laboratory. The 16:3:1 methanol-ethanol-water mixture was used as a pressure-transmitting medium. Pressures were measured using the ruby-fluorescence method. No phase change has been observed up to 28.2 GPa. The isothermal equation of state (EOS) was determined. The values of K{sub 0}, and K'{sub 0} refined with a third-order Birch-Murnaghan EOS are K{sub 0} = 123(9) GPa, and K'{sub 0} = 5.2(8). Furthermore, we confirm that the linear compressibilities ({beta}) along a, b and c directions of arsenopyrite is elastically isotropic ({beta}{sub a} = 6.82 x 10{sup -4}, {beta}{sub b} = 6.17 x 10{sup -4} and {beta}{sub c} = 6.57 x 10{sup -4} GPa{sup -1}).

High-intensity, subkolovolt x-ray calibration facility using a Cockroft--Walton proton accelerator

International Nuclear Information System (INIS)

Kuckuck, R.W.; Gaines, J.L.; Ernst, R.D.

1976-01-01

Considerable need has arisen for the development of well-calibrated x-ray detectors capable of detecting photons with energies between 100 and 1000 electron-volts. This energy region is of significant interest since the x-ray emission from high-temperature (kT approximately 1.0 keV), laser-produced plasmas is predominantly in this range. A high-intensity, subkilovolt x-ray calibration source was developed which utilizes proton-induced inner-shell atomic fluorescence of low-Z elements. The high photon yields and low bremsstrahlung background associated with this phenomenon are ideally suited to provide an intense, nearly monoenergetic x-ray calibration source for detector development applications. The proton accelerator is a 3 mA, 300 kV Cockroft-Walton using a conventional rf hydrogen ion source. Seven remotely-selectable liquid-cooled targets capable of heat dissipation of 5 kW/cm 2 are used to provide characteristic x-rays with energies between 100 and 1000 eV. Source strengths are of the order of 10 13 to 10 14 photons/sec. A description of the facility is presented. Typical x-ray spectra (B-K, C-K, Ti-L, Fe-L and Cu-L) and flux values will be shown. Problems such as spectral contamination due to carbon buildup on the target and to backscattered particles are discussed

Workshop on high heat load x-ray optics

Energy Technology Data Exchange (ETDEWEB)

1990-01-01

A workshop on High Heat Load X-Ray Optics'' was held at Argonne National Laboratory on August 3--5, 1989. The object of this workshop was to discuss recent advances in the art of cooling x-ray optics subject to high heat loads from synchrotron beams. The cooling of the first optical element in the intense photon beams that will be produced in the next generation of synchrotron sources is recognized as one of the major challenges that must be faced before one will be able to use these very intense beams in future synchrotron experiments. Considerable advances have been made in this art during the last few years, but much work remains to be done before the heating problem can be said to be completely solved. Special emphasis was placed on recent cooling experiments and detailed finite element'' and finite difference'' calculations comparing experiment with theory and extending theory to optimize performance.

Workshop on high heat load x-ray optics

International Nuclear Information System (INIS)

1990-01-01

A workshop on ''High Heat Load X-Ray Optics'' was held at Argonne National Laboratory on August 3--5, 1989. The object of this workshop was to discuss recent advances in the art of cooling x-ray optics subject to high heat loads from synchrotron beams. The cooling of the first optical element in the intense photon beams that will be produced in the next generation of synchrotron sources is recognized as one of the major challenges that must be faced before one will be able to use these very intense beams in future synchrotron experiments. Considerable advances have been made in this art during the last few years, but much work remains to be done before the heating problem can be said to be completely solved. Special emphasis was placed on recent cooling experiments and detailed ''finite element'' and ''finite difference'' calculations comparing experiment with theory and extending theory to optimize performance

Automatic X-ray television rig for high-speed radiography of polycrystals

International Nuclear Information System (INIS)

Bezbakh, V.D.; Garasim, Yu.A.; Oshkaderov, S.P.; Pet'kov, V.V.

1993-01-01

The high-speed radiography method is used for studying the phase and structural transformation in metals and alloys during rapid changes in temperature. In order to improve the effectiveness of this method the Institute of Metal Physics, Ukrainian Academy of Sciences, has developed an automatic rig for high-speed radiography of polycrystalline materials using a television method for recording the x-ray diffraction patterns. The rig, described here, consists of an x-ray block, a vacuum chamber, a device for programmed electro-contact heating of specimens, a system for imaging and scanning x-ray diffraction patterns, and a system for collecting and analyzing the data. Focusing is carried out by the Zeeman-Bolin method. The new rig helps to significantly reduce the recording time and ensures adequate quality and reliability of the recorded diffraction image over a wide range of temperatures. Data using the rig is presented for high-speed radiography for cooling a specimen of G20 steel. 4 refs., 4 figs

X-ray electromagnetic application technology

International Nuclear Information System (INIS)

2011-01-01

The investigating committee aimed at research on electromagnetic fields in functional devices and X-ray fibers for efficient coherent X-ray generation and their material science, high-precision manufacturing, particularly for X-ray electromagnetic application technology from January 2006 to December 2008. In this report, we describe our research results, in particular, on the topics of synchrotron radiation and free-electron laser, Saga Synchrotron Project, X-ray waveguides and waveguide-based lens-less hard-X-ray imaging, X-ray nanofocusing for capillaries and zone plates, dispersion characteristics in photonics crystal consisting of periodic atoms for nanometer waveguides, electromagnetic characteristics of grid structures for scattering fields of nano-meter electromagnetic waves and X-rays, FDTD parallel computing of fundamental scattering and attenuation characteristics of X-ray for medical imaging diagnosis, orthogonal relations of electromagnetic fields including evanescent field in dispersive medium. (author)

Experimental demonstration of high resolution three-dimensional x-ray holography

International Nuclear Information System (INIS)

McNulty, I.; Trebes, J.E.; Brase, J.M.; Yorkey, T.J.; Levesque, R.; Szoke, H.; Anderson, E.H.; Jacobsen, C.

1992-01-01

Tomographic x-ray holography may make possible the imaging of biological objects at high resolution in three dimensions. We performed a demonstration experiment with soft x-rays to explore the feasibility of this technique. Coherent 3.2-nm undulator radiation was used to record Fourier transform holograms of a microfabricated test object from various illumination angles. The holograms were numerically reconstructed according to the principles of diffraction tomography, yielding images of the object that are well resolved in three dimensions

X-Ray Absorption with Transmission X-Ray Microscopes

NARCIS (Netherlands)

de Groot, F.M.F.

2016-01-01

In this section we focus on the use of transmission X-ray microscopy (TXM) to measure the XAS spectra. In the last decade a range of soft X-ray and hard X-ray TXM microscopes have been developed, allowing the measurement of XAS spectra with 10–100 nm resolution. In the hard X-ray range the TXM

Optical and X-ray studies of Compact X-ray Binaries in NGC 5904

Science.gov (United States)

Bhalotia, Vanshree; Beck-Winchatz, Bernhard

2018-06-01

Due to their high stellar densities, globular cluster systems trigger various dynamical interactions, such as the formation of compact X-ray binaries. Stellar collisional frequencies have been correlated to the number of X-ray sources detected in various clusters and we hope to measure this correlation for NGC 5904. Optical fluxes of sources from archival HST images of NGC 5904 have been measured using a DOLPHOT PSF photometry in the UV, optical and near-infrared. We developed a data analysis pipeline to process the fluxes of tens of thousands of objects using awk, python and DOLPHOT. We plot color magnitude diagrams in different photometric bands in order to identify outliers that could be X-ray binaries, since they do not evolve the same way as singular stars. Aligning previously measured astrometric data for X-ray sources in NGC 5904 from Chandra with archival astrometric data from HST will filter out the outlier objects that are not X-ray producing, and provide a sample of compact binary systems that are responsible for X-ray emission in NGC 5904. Furthermore, previously measured X-ray fluxes of NGC 5904 from Chandra have also been used to measure the X-ray to optical flux ratio and identify the types of compact X-ray binaries responsible for the X-ray emissions in NGC 5904. We gratefully acknowledge the support from the Illinois Space Grant Consortium.

X-CHIP: an integrated platform for high-throughput protein crystallization and on-the-chip X-ray diffraction data collection

International Nuclear Information System (INIS)

Kisselman, Gera; Qiu, Wei; Romanov, Vladimir; Thompson, Christine M.; Lam, Robert; Battaile, Kevin P.; Pai, Emil F.; Chirgadze, Nickolay Y.

2011-01-01

The X-CHIP (X-ray Crystallography High-throughput Integrated Platform) is a novel microchip that has been developed to combine multiple steps of the crystallographic pipeline from crystallization to diffraction data collection on a single device to streamline the entire process. The X-CHIP (X-ray Crystallization High-throughput Integrated Platform) is a novel microchip that has been developed to combine multiple steps of the crystallographic pipeline from crystallization to diffraction data collection on a single device to streamline the entire process. The system has been designed for crystallization condition screening, visual crystal inspection, initial X-ray screening and data collection in a high-throughput fashion. X-ray diffraction data acquisition can be performed directly on-the-chip at room temperature using an in situ approach. The capabilities of the chip eliminate the necessity for manual crystal handling and cryoprotection of crystal samples, while allowing data collection from multiple crystals in the same drop. This technology would be especially beneficial for projects with large volumes of data, such as protein-complex studies and fragment-based screening. The platform employs hydrophilic and hydrophobic concentric ring surfaces on a miniature plate transparent to visible light and X-rays to create a well defined and stable microbatch crystallization environment. The results of crystallization and data-collection experiments demonstrate that high-quality well diffracting crystals can be grown and high-resolution diffraction data sets can be collected using this technology. Furthermore, the quality of a single-wavelength anomalous dispersion data set collected with the X-CHIP at room temperature was sufficient to generate interpretable electron-density maps. This technology is highly resource-efficient owing to the use of nanolitre-scale drop volumes. It does not require any modification for most in-house and synchrotron beamline systems and offers

X-CHIP: an integrated platform for high-throughput protein crystallization and on-the-chip X-ray diffraction data collection

Energy Technology Data Exchange (ETDEWEB)

Kisselman, Gera; Qiu, Wei; Romanov, Vladimir; Thompson, Christine M.; Lam, Robert [Ontario Cancer Institute, Princess Margaret Hospital, University Health Network, Toronto, Ontario M5G 2C4 (Canada); Battaile, Kevin P. [Argonne National Laboratory, Argonne, Illinois 60439 (United States); Pai, Emil F.; Chirgadze, Nickolay Y., E-mail: nchirgad@uhnresearch.ca [Ontario Cancer Institute, Princess Margaret Hospital, University Health Network, Toronto, Ontario M5G 2C4 (Canada); University of Toronto, Toronto, Ontario M5S 1A8 (Canada)

2011-06-01

The X-CHIP (X-ray Crystallography High-throughput Integrated Platform) is a novel microchip that has been developed to combine multiple steps of the crystallographic pipeline from crystallization to diffraction data collection on a single device to streamline the entire process. The X-CHIP (X-ray Crystallization High-throughput Integrated Platform) is a novel microchip that has been developed to combine multiple steps of the crystallographic pipeline from crystallization to diffraction data collection on a single device to streamline the entire process. The system has been designed for crystallization condition screening, visual crystal inspection, initial X-ray screening and data collection in a high-throughput fashion. X-ray diffraction data acquisition can be performed directly on-the-chip at room temperature using an in situ approach. The capabilities of the chip eliminate the necessity for manual crystal handling and cryoprotection of crystal samples, while allowing data collection from multiple crystals in the same drop. This technology would be especially beneficial for projects with large volumes of data, such as protein-complex studies and fragment-based screening. The platform employs hydrophilic and hydrophobic concentric ring surfaces on a miniature plate transparent to visible light and X-rays to create a well defined and stable microbatch crystallization environment. The results of crystallization and data-collection experiments demonstrate that high-quality well diffracting crystals can be grown and high-resolution diffraction data sets can be collected using this technology. Furthermore, the quality of a single-wavelength anomalous dispersion data set collected with the X-CHIP at room temperature was sufficient to generate interpretable electron-density maps. This technology is highly resource-efficient owing to the use of nanolitre-scale drop volumes. It does not require any modification for most in-house and synchrotron beamline systems and offers

Asymmetrically cut crystal pair as x-ray magnifier for imaging at high intensity laser facilities

Energy Technology Data Exchange (ETDEWEB)

Szabo, C. I.; Feldman, U. [Artep Inc., 2922 Excelsior Spring Circle, Ellicott City, Maryland 21042 (United States); Seely, J. F. [Space Science Division, Naval Research Laboratory, Washington, DC 20375-5352 (United States); Curry, J. J.; Hudson, L. T.; Henins, A. [National Institute of Standards and Technology, Gaithersburg, Maryland 20899 (United States)

2010-10-15

The potential of an x-ray magnifier prepared from a pair of asymmetrically cut crystals is studied to explore high energy x-ray imaging capabilities at high intensity laser facilities. OMEGA-EP and NIF when irradiating mid and high Z targets can be a source of high-energy x-rays whose production mechanisms and use as backlighters are a subject of active research. This paper studies the properties and potential of existing asymmetric cut crystal pairs from the National Institute of Standards and Technology (NIST) built in a new enclosure for imaging x-ray sources. The technique of the x-ray magnifier has been described previously. This new approach is aimed to find a design that could be used at laser facilities by magnifying the x-ray source into a screen far away from the target chamber center, with fixed magnification defined by the crystals' lattice spacing and the asymmetry angles. The magnified image is monochromatic and the imaging wavelength is set by crystal asymmetry and incidence angles. First laboratory results are presented and discussed.

Trial fabrication of a secondary x-ray spectrometer with high energy resolution for use in x-ray resonant inelastic scattering experiments

International Nuclear Information System (INIS)

Iwazumi, Toshiaki

2004-01-01

An instrument was fabricated for use of x-ray resonant inelastic scattering with high-energy resolution in expectation of finding new physical phenomena in strongly correlated electron systems. In the scattering x-ray spectrometer, an asymmetric Johanson crystal spectrometer, which was deployed in an asymmetric Rowland configuration, was designed, fabricated and assessed. The performance expected theoretically for the Johanson spectrometer was recognized from experiments by use of synchrotron radiation. (Y. Kazumata)

13.1 micrometers hard X-ray focusing by a new type monocapillary X-ray optic designed for common laboratory X-ray source

Science.gov (United States)

Sun, Xuepeng; zhang, Xiaoyun; Zhu, Yu; Wang, Yabing; Shang, Hongzhong; Zhang, Fengshou; Liu, Zhiguo; Sun, Tianxi

2018-04-01

A new type of monocapillary X-ray optic, called 'two bounces monocapillary X-ray optics' (TBMXO), is proposed for generating a small focal spot with high power-density gain for micro X-ray analysis, using a common laboratory X-ray source. TBMXO is consists of two parts: an ellipsoidal part and a tapered part. Before experimental testing, the TBMXO was simulated by the ray tracing method in MATLAB. The simulated results predicted that the proposed TBMXO would produce a smaller focal spot with higher power-density gain than the ellipsoidal monocapillary X-ray optic (EMXO). In the experiment, the TBMXO performance was tested by both an optical device and a Cu target X-ray tube with focal spot of 100 μm. The results indicated that the TBMXO had a slope error of 57.6 μrad and a 13.1 μm focal spot and a 1360 gain in power density were obtained.

The X-ray Astronomy Recovery Mission

Science.gov (United States)

Tashiro, M.; Kelley, R.

2017-10-01

On 25 March 2016, the Japanese 6th X-ray astronomical satellite ASTRO-H (Hitomi), launched on February 17, lost communication after a series of mishap in its attitude control system. In response to the mishap the X-ray astronomy community and JAXA analyzed the direct and root cause of the mishap and investigated possibility of a recovery mission with the international collaborator NASA and ESA. Thanks to great effort of scientists, agencies, and governments, the X-ray Astronomy Recovery Mission (XARM) are proposed. The recovery mission is planned to resume high resolution X-ray spectroscopy with imaging realized by Hitomi under the international collaboration in the shortest time possible, simply by focusing one of the main science goals of Hitomi Resolving astrophysical problems by precise high-resolution X-ray spectroscopy'. XARM will carry a 6 x 6 pixelized X-ray micro-calorimeter on the focal plane of an X-ray mirror assembly, and an aligned X-ray CCD camera covering the same energy band and wider field of view, but no hard X-ray or soft gamma-ray instruments are onboard. In this paper, we introduce the science objectives, mission concept, and schedule of XARM.

Compton backscattered collmated X-ray source

Science.gov (United States)

Ruth, Ronald D.; Huang, Zhirong

2000-01-01

A high-intensity, inexpensive and collimated x-ray source for applications such as x-ray lithography is disclosed. An intense pulse from a high power laser, stored in a high-finesse resonator, repetitively collides nearly head-on with and Compton backscatters off a bunched electron beam, having relatively low energy and circulating in a compact storage ring. Both the laser and the electron beams are tightly focused and matched at the interaction region inside the optical resonator. The laser-electron interaction not only gives rise to x-rays at the desired wavelength, but also cools and stabilizes the electrons against intrabeam scattering and Coulomb repulsion with each other in the storage ring. This cooling provides a compact, intense bunch of electrons suitable for many applications. In particular, a sufficient amount of x-rays can be generated by this device to make it an excellent and flexible Compton backscattered x-ray (CBX) source for high throughput x-ray lithography and many other applications.

Compton backscattered collimated x-ray source

Science.gov (United States)

Ruth, R.D.; Huang, Z.

1998-10-20

A high-intensity, inexpensive and collimated x-ray source is disclosed for applications such as x-ray lithography is disclosed. An intense pulse from a high power laser, stored in a high-finesse resonator, repetitively collides nearly head-on with and Compton backscatters off a bunched electron beam, having relatively low energy and circulating in a compact storage ring. Both the laser and the electron beams are tightly focused and matched at the interaction region inside the optical resonator. The laser-electron interaction not only gives rise to x-rays at the desired wavelength, but also cools and stabilizes the electrons against intrabeam scattering and Coulomb repulsion with each other in the storage ring. This cooling provides a compact, intense bunch of electrons suitable for many applications. In particular, a sufficient amount of x-rays can be generated by this device to make it an excellent and flexible Compton backscattered x-ray (CBX) source for high throughput x-ray lithography and many other applications. 4 figs.

High resolution x-ray lensless imaging by differential holographic encoding

Energy Technology Data Exchange (ETDEWEB)

Zhu, D.; Guizar-Sicairos, M.; Wu, B.; Scherz, A.; Acremann, Y.; Tylisczcak, T.; Fischer, P.; Friedenberger, N.; Ollefs, K.; Farle, M.; Fienup, J. R.; Stohr, J.

2009-11-02

X-ray free electron lasers (X-FEL{sub s}) will soon offer femtosecond pulses of laterally coherent x-rays with sufficient intensity to record single-shot coherent scattering patterns for nanoscale imaging. Pulse trains created by splitand-delay techniques even open the door for cinematography on unprecedented nanometer length and femtosecond time scales. A key to real space ultrafast motion pictures is fast and reliable inversion of the recorded reciprocal space scattering patterns. Here we for the first time demonstrate in the x-ray regime the power of a novel technique for lensless high resolution imaging, previously suggested by Guizar-Sicairos and Fienup termed holography with extended reference by autocorrelation linear differential operation, HERALD0. We have achieved superior resolution over conventional x-ray Fourier transform holography (FTH) without sacrifices in SNR or significant increase in algorithmic complexity. By combining images obtained from individual sharp features on an extended reference, we further show that the resolution can be even extended beyond the reference fabrication limits. Direct comparison to iterative phase retrieval image reconstruction and images recorded with stateof- the-art zone plate microscopes is presented. Our results demonstrate the power of HERALDO as a favorable candidate for robust inversion of single-shot coherent scattering patterns.

High-Resolution X-Ray Lensless Imaging by Differential Holographic Encoding

Energy Technology Data Exchange (ETDEWEB)

Zhu, Diling [Stanford Univ., CA (United States). Dept. of Applied Physics; SLAC National Accelerator Lab., Menlo Park, CA (United States). Stanford Inst. for Material and Energy Science; Guizar-Sicairos, Manuel [Univ. of Rochester, NY (United States). Inst. of Optics; Wu, Benny [Stanford Univ., CA (United States). Dept. of Applied Physics; SLAC National Accelerator Lab., Menlo Park, CA (United States). Stanford Inst. for Material and Energy Science; Scherz, Andreas [SLAC National Accelerator Lab., Menlo Park, CA (United States). Stanford Inst. for Material and Energy Science; Acremann, Yves [SLAC National Accelerator Lab., Menlo Park, CA (United States). Photon Ultrafast Laser Science and Engineering Inst. (PULSE); Tyliszczak, Tolek [Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States). Advanced Light Source (ALS); Fischer, Peter [Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States). Center for X-ray Optics; Friedenberger, Nina [Universitat Duisburg-Essen (Germany). Dept. of Physics and Center for Nanointegration Duisburg-Essen (CeNIDE); Ollefs, Katharina [Universitat Duisburg-Essen (Germany). Dept. of Physics and Center for Nanointegration Duisburg-Essen (CeNIDE); Farle, Michael [Universitat Duisburg-Essen (Germany). Dept. of Physics and Center for Nanointegration Duisburg-Essen (CeNIDE); Fienup, James R. [Univ. of Rochester, NY (United States). Inst. of Optics; Stöhr, Joachim [SLAC National Accelerator Lab., Menlo Park, CA (United States). Linac Coherent Light Source (LCLS)

2010-07-01

X-ray free electron lasers (X-FELs) will soon offer femtosecond pulses of laterally coherent x-rays with sufficient intensity to record single-shot coherent scattering patterns for nanoscale imaging. Pulse trains created by split and- delay techniques even open the door for cinematography on unprecedented nanometer length and femtosecond time scales. A key to real space ultrafast motion pictures is fast and reliable inversion of the recorded reciprocal space scattering patterns. Here we for the first time demonstrate in the x-ray regime the power of a novel technique for lensless high resolution imaging, previously suggested by Guizar-Sicairos and Fienup termed holography with extended reference by autocorrelation linear differential operation, HERALD0. We have achieved superior resolution over conventional x-ray Fourier transform holography (FTH) without sacrifices in SNR or significant increase in algorithmic complexity. By combining images obtained from individual sharp features on an extended reference, we further show that the resolution can be even extended beyond the reference fabrication limits. Direct comparison to iterative phase retrieval image reconstruction and images recorded with state of-the-art zone plate microscopes is presented. Our results demonstrate the power of HERALDO as a favorable candidate for robust inversion of single-shot coherent scattering patterns.

Temporal characteristic analysis of laser-modulated pulsed X-ray source for space X-ray communication

Science.gov (United States)

Hang, Shuang; Liu, Yunpeng; Li, Huan; Tang, Xiaobin; Chen, Da

2018-04-01

X-ray communication (XCOM) is a new communication type and is expected to realize high-speed data transmission in some special communication scenarios, such as deep space communication and blackout communication. This study proposes a high-speed modulated X-ray source scheme based on the laser-to-X-ray conversion. The temporal characteristics of the essential components of the proposed laser-modulated pulsed X-ray source (LMPXS) were analyzed to evaluate its pulse emission performance. Results show that the LMPXS can provide a maximum modulation rate up to 100 Mbps which is expected to significantly improve the data rate of XCOM.

Applications of phase-contrast x-ray imaging to medicine using an x-ray interferometer

Science.gov (United States)

Momose, Atsushi; Yoneyama, Akio; Takeda, Tohoru; Itai, Yuji; Tu, Jinhong; Hirano, Keiichi

1999-10-01

We are investigating possible medical applications of phase- contrast X-ray imaging using an X-ray interferometer. This paper introduces the strategy of the research project and the present status. The main subject is to broaden the observation area to enable in vivo observation. For this purpose, large X-ray interferometers were developed, and 2.5 cm X 1.5 cm interference patterns were generated using synchrotron X-rays. An improvement of the spatial resolution is also included in the project, and an X-ray interferometer designed for high-resolution phase-contrast X-ray imaging was fabricated and tested. In parallel with the instrumental developments, various soft tissues are observed by phase- contrast X-ray CT to find correspondence between the generated contrast and our histological knowledge. The observation done so far suggests that cancerous tissues are differentiated from normal tissues and that blood can produce phase contrast. Furthermore, this project includes exploring materials that modulate phase contrast for selective imaging.

High pressure X-ray preionized TEMA-CO2 laser

NARCIS (Netherlands)

Bonnie, R.J.M.; Witteman, W.J.

1987-01-01

The construction of a high-pressure (up to 20 atm) transversely excited CO2 laser using transverse X-ray preionization is described. High pressure operation was found to be greatly improved in comparison to UV-preionized systems. Homogeneous discharges have been achieved in the pressure range 5–20

HIGH-RESOLUTION X-RAY SPECTROSCOPY REVEALS THE SPECIAL NATURE OF WOLF-RAYET STAR WINDS

Energy Technology Data Exchange (ETDEWEB)

Oskinova, L. M.; Hamann, W.-R. [Institute for Physics and Astronomy, University Potsdam, 14476 Potsdam (Germany); Gayley, K. G. [Department of Physics and Astronomy, University of Iowa, Iowa City, IA 52245 (United States); Huenemoerder, D. P. [Massachusetts Institute of Technology, Kavli Institute for Astrophysics and Space Research, 70 Vassar St., Cambridge, MA 02139 (United States); Ignace, R. [Department of Physics and Astronomy, East Tennessee State University, Johnson City, TN 37663 (United States); Pollock, A. M. T., E-mail: lida@astro.physik.uni-potsdam.de [European Space Agency XMM-Newton Science Operations Centre, European Space Astronomy Centre, Apartado 78, Villanueva de la Canada, 28691 Madrid (Spain)

2012-03-10

We present the first high-resolution X-ray spectrum of a putatively single Wolf-Rayet (WR) star. 400 ks observations of WR 6 by the XMM-Newton telescope resulted in a superb quality high-resolution X-ray spectrum. Spectral analysis reveals that the X-rays originate far out in the stellar wind, more than 30 stellar radii from the photosphere, and thus outside the wind acceleration zone where the line-driving instability (LDI) could create shocks. The X-ray emitting plasma reaches temperatures up to 50 MK and is embedded within the unshocked, 'cool' stellar wind as revealed by characteristic spectral signatures. We detect a fluorescent Fe line at Almost-Equal-To 6.4 keV. The presence of fluorescence is consistent with a two-component medium, where the cool wind is permeated with the hot X-ray emitting plasma. The wind must have a very porous structure to allow the observed amount of X-rays to escape. We find that neither the LDI nor any alternative binary scenario can explain the data. We suggest a scenario where X-rays are produced when the fast wind rams into slow 'sticky clumps' that resist acceleration. Our new data show that the X-rays in single WR star are generated by some special mechanism different from the one operating in the O-star winds.

High precision instrumentation for measuring the true exposure time in diagnostic X-ray examinations

International Nuclear Information System (INIS)

Silva, Danubia B.; Santos, Marcus A.P.; Barros, Fabio R.; Santos, Luiz A.P.

2013-01-01

One of the most important physical quantities to be evaluated in diagnostic radiology is the radiation exposure time experimented by the patient during the X-ray examination. IAEA and WHO organizations have suggested that any country must create a quality surveillance program to verify if each type of ionizing radiation equipment used in the hospitals and medical clinics are in conformity with the accepted uncertainties following the international standards. The purpose of this work is to present a new high precision methodology for measuring true exposure time in diagnostic X-ray examinations: pulsed, continuous or digital one. An electronic system named CronoX, which will be soon registered at the Brazilian Patent Office (INPI), is the equipment that provides such a high precision measurement. The principle of measurement is based on the electrical signal captured by a sensor that enters in a regeneration amplifier to transform it in a digital signal, which is treated by a microprocessor (uP). The signal treatment results in a two measured times: 1) T rx , the true X-ray exposure time; 2) T nx , the time in which the X-ray machine is repeatedly cut off during the pulsed irradiation and there is no delivery dose to the patient. Conventional Polymat X-ray equipment and dental X-ray machines were used to generate X-ray photons and take the measurements with the electronic systems. The results show that such a high precision instrumentation displays the true exposure time in diagnostic X-ray examinations and indicates a new method to be purposed for the quality surveillance programs in radiology. (author)

Development of a Watt-level gamma-ray source based on high-repetition-rate inverse Compton scattering

Energy Technology Data Exchange (ETDEWEB)

Mihalcea, D.; Murokh, A.; Piot, P.; Ruan, J.

2017-07-01

A high-brilliance (~10²² photon s^-1 mm^-2 mrad^-2 /0.1%) gamma-ray source experiment is currently being planned at Fermilab (E_γ≃1.1 MeV). The source implements a high-repetition-rate inverse Compton scattering by colliding electron bunches formed in a ~300-MeV superconducting linac with a high-intensity laser pulse. This paper describes the design rationale along with some of technical challenges associated to producing high-repetition-rate collision. The expected performances of the gamma-ray source are also presented.

Z-pinches as intense x-ray sources for high energy density physics application

International Nuclear Information System (INIS)

Matzen, M.K.

1997-01-01

Fast z-pinch implosions can convert more than 10% of the stored electrical energy in a pulsed-power accelerator into x rays. These x rays are produced when an imploding cylindrical plasma, driven by the magnetic field pressure associated with very large axial currents, stagnates upon the cylindrical axis of symmetry. On the Saturn pulsed-power accelerator at Sandia National Laboratories, for example, currents of 6 to 8 MA with a risetime of less than 50 ns are driven through cylindrically-symmetric loads, producing implosions velocities as high as 100 cm/μs and x-ray energies as high as 500 kJ. The keV component of the resulting x-ray spectrum has been used for many years 8 a radiation source for material response studies. Alternatively, the x-ray output can be thermalized into a near-Planckian x-ray source by containing it within a large cylindrical radiation case. These large volume, long-lived radiation sources have recently been used for ICF-relevant ablator physics experiments as well as astrophysical opacity and radiation-material interaction experiments. Hydromagnetic Rayleigh-Taylor instabilities and cylindrical load symmetry are critical, limiting factors in determining the assembled plasma densities and temperatures, and thus in the x-ray pulse widths that can be produced on these accelerators. In recent experiments on the Saturn accelerator, these implosion nonuniformities have been minimized by using uniform-fill gas puff loads or by using wire arrays with as many a 192 wires. These techniques produced significant improvements in the pinched plasma quality, Zn reproducibility, and x-ray output power. X-ray pulse widths of less than 5 ns and peak powers of 75±10 TW have been achieved with arrays of 120 tungsten wires. These powers represent greater than a factor of three in power amplification over the electrical power of the Saturn n accelerator, and are a record for x-ray powers in the laboratory

Extracting chemical information from high-resolution Kβ X-ray emission spectroscopy

Science.gov (United States)

Limandri, S.; Robledo, J.; Tirao, G.

2018-06-01

High-resolution X-ray emission spectroscopy allows studying the chemical environment of a wide variety of materials. Chemical information can be obtained by fitting the X-ray spectra and observing the behavior of some spectral features. Spectral changes can also be quantified by means of statistical parameters calculated by considering the spectrum as a probability distribution. Another possibility is to perform statistical multivariate analysis, such as principal component analysis. In this work the performance of these procedures for extracting chemical information in X-ray emission spectroscopy spectra for mixtures of Mn2+ and Mn4+ oxides are studied. A detail analysis of the parameters obtained, as well as the associated uncertainties is shown. The methodologies are also applied for Mn oxidation state characterization of double perovskite oxides Ba1+xLa1-xMnSbO6 (with 0 ≤ x ≤ 0.7). The results show that statistical parameters and multivariate analysis are the most suitable for the analysis of this kind of spectra.

Deposition and characterization of multilayers on thin foil x-ray mirrors for high-throughput x-ray telescopes

DEFF Research Database (Denmark)

Hussain, Ahsen M.; Joensen, Karsten D.; Hoeghoej, P.

1996-01-01

W/Si and Co/C multilayers have been deposited on epoxy- replicated Au mirrors from the ASTRO-E telescope project, SPectrum Roentgen Gamma (SRG) flight mirrors, DURAN glass substrates and Si witness wafers. A characterization of the multilayers with both hard x-rays and soft x-rays is presented....... This clearly indicates the effectiveness of the epoxy-replication process for the production of smooth substrates for multilayer deposition to be used in future x-ray telescopes....

X-ray Fourier-transform holographic microscope

International Nuclear Information System (INIS)

Haddad, W.S.; Cullen, D.; Solem, J.C.; Boyer, K.; Rhodes, C.K.

1988-01-01

The properties of an x-ray Fourier-transform holographic instrument suitable for imaging hydrated biological samples are described. Recent advances in coherent x-ray source technology are making diffraction-limited holograms of microscopic structures, with corresponding high spatial resolution, a reality. A high priority application of snapshot x-ray holography is the study of microscopic biological structures in the hydrated living state. X-rays offer both high resolution and high contrast for important structures within living organisms, thereby rendering unnecessary the staining of specimens, essential for optical and electron microscopy. If the wavelength is properly chosen. Furthermore, the snapshot feature, arising from picosecond or subpicosecond exposure times, eliminates blurring occurring from either thermal heating or normal biological activity of the sample. Finally, with sufficiently high photon fluxes, such as those available from x-ray lasers, the x-ray snapshot can be accomplished with a single pulse, thereby yielding complete three-dimensional information on a sample having normal biological integrity at the moment of exposure. 10 refs., 6 figs

High efficiency spectro graphs for the EUV and soft x-rays

International Nuclear Information System (INIS)

Cash, W.

1983-01-01

A basic need of modern UV and x-ray astronomy is the capability to perform high resolution spectroscopy of faint stars. The use of modern grazing incidence optics can be coupled to high blaze angle reflection gratings used in the conical diffraction mount to offer a versatile, efficient approach to the design problem. The authors discuss two designs of interest: an echelle spectrograph for use longward of 100 A, and an Objective Reflection Grating Spectrograph for use in the soft x-rays. General design considerations and measurements of grating efficiencies are also presented

The nuclear spectroscopic telescope array (NuSTAR) high-energy X-ray mission

DEFF Research Database (Denmark)

Madsen, Kristin K.; Harrison, Fiona A.; Hongjun An

2014-01-01

The Nuclear Spectroscopic Telescope Array (NuSTAR) mission was launched on 2012 June 13 and is the first focusing high-energy X-ray telescope in orbit operating above ~10 keV. NuSTAR flies two co-aligned Wolter-I conical approximation X-ray optics, coated with Pt/C and W/Si multilayers...

High-resolution X-ray crystal structure of bovine H-protein using the high-pressure cryocooling method.

Science.gov (United States)

Higashiura, Akifumi; Ohta, Kazunori; Masaki, Mika; Sato, Masaru; Inaka, Koji; Tanaka, Hiroaki; Nakagawa, Atsushi

2013-11-01

Recently, many technical improvements in macromolecular X-ray crystallography have increased the number of structures deposited in the Protein Data Bank and improved the resolution limit of protein structures. Almost all high-resolution structures have been determined using a synchrotron radiation source in conjunction with cryocooling techniques, which are required in order to minimize radiation damage. However, optimization of cryoprotectant conditions is a time-consuming and difficult step. To overcome this problem, the high-pressure cryocooling method was developed (Kim et al., 2005) and successfully applied to many protein-structure analyses. In this report, using the high-pressure cryocooling method, the X-ray crystal structure of bovine H-protein was determined at 0.86 Å resolution. Structural comparisons between high- and ambient-pressure cryocooled crystals at ultra-high resolution illustrate the versatility of this technique. This is the first ultra-high-resolution X-ray structure obtained using the high-pressure cryocooling method.

High-spatial resolution and high-spectral resolution detector for use in the measurement of solar flare hard x rays

International Nuclear Information System (INIS)

Desai, U.D.; Orwig, L.E.

1988-01-01

In the areas of high spatial resolution, the evaluation of a hard X-ray detector with 65 micron spatial resolution for operation in the energy range from 30 to 400 keV is proposed. The basic detector is a thick large-area scintillator faceplate, composed of a matrix of high-density scintillating glass fibers, attached to a proximity type image intensifier tube with a resistive-anode digital readout system. Such a detector, combined with a coded-aperture mask, would be ideal for use as a modest-sized hard X-ray imaging instrument up to X-ray energies as high as several hundred keV. As an integral part of this study it was also proposed that several techniques be critically evaluated for X-ray image coding which could be used with this detector. In the area of high spectral resolution, it is proposed to evaluate two different types of detectors for use as X-ray spectrometers for solar flares: planar silicon detectors and high-purity germanium detectors (HPGe). Instruments utilizing these high-spatial-resolution detectors for hard X-ray imaging measurements from 30 to 400 keV and high-spectral-resolution detectors for measurements over a similar energy range would be ideally suited for making crucial solar flare observations during the upcoming maximum in the solar cycle

Center for X-Ray Optics, 1986

International Nuclear Information System (INIS)

1987-07-01

The Center for X-Ray Optics has made substantial progress during the past year on the development of very high resolution x-ray technologies, the generation of coherent radiation at x-ray wavelengths, and, based on these new developments, had embarked on several scientific investigations that would not otherwise have been possible. The investigations covered in this report are topics on x-ray sources, x-ray imaging and applications, soft x-ray spectroscopy, synchrotron radiation, advanced light source and magnet structures for undulators and wigglers

Next Generation Astronomical X-ray Optics: High Angular Resolution, Light Weight, and Low Production Cost

Science.gov (United States)

Zhang. W. W.; Biskach, M. P.; Blake, P. N.; Chan, K. W.; Gaskin, J. A.; Hong, M. L.; Jones, W. D.; Kolos, L. D.; Mazzarella, J. R.; McClelland, R. S.;

X-ray detector

International Nuclear Information System (INIS)

Whetten, N.R.; Houston, J.M.

1977-01-01

An ionization chamber for use in determining the spatial distribution of x-ray photons in tomography systems comprises a plurality of substantially parallel, planar anodes separated by parallel, planar cathodes and enclosed in a gas of high atomic weight at a pressure from approximately 10 atmospheres to approximately 50 atmospheres. The cathode and anode structures comprise metals which are substantially opaque to x-ray radiation and thereby tend to reduce the resolution limiting effects of x-ray fluoresence in the gas. In another embodiment of the invention the anodes comprise parallel conductive bars disposed between two planar cathodes. Guard rings eliminate surface leakage currents between adjacent electrodes. 8 figures

X-ray astronomy

International Nuclear Information System (INIS)

Giacconi, R.; Gursky, H.

1974-01-01

This text contains ten chapters and three appendices. Following an introduction, chapters two through five deal with observational techniques, mechanisms for the production of x rays in a cosmic setting, the x-ray sky and solar x-ray emission. Chapters six through ten include compact x-ray sources, supernova remnants, the interstellar medium, extragalactic x-ray sources and the cosmic x-ray background. Interactions of x rays with matter, units and conversion factors and a catalog of x-ray sources comprise the three appendices. (U.S.)

First results from the high-brightness x-ray spectroscopy beamline at ALS

Energy Technology Data Exchange (ETDEWEB)

Perera, R.C.C.; Ng, W.; Jones, G. [Lawrence Berkeley National Lab., CA (United States)] [and others

1997-04-01

Beamline 9.3.1 at the Advanced Light Source (ALS) is a windowless beamline, covering the 1-6 keV photon-energy range, designed to achieve the goal of high brightness at the sample for use in the X-ray Atomic and Molecular Spectroscopy (XAMS) science, surface and interface science, biology and x-ray optical development programs at ALS. X-ray absorption and time of flight photo emission measurements in 2 - 5 keV photon energy in argon along with the flux, resolution, spot size and stability of the beamline will be discussed. Prospects for future XAMS measurements will also be presented.

High-Resolution X-Ray Spectra of the Symbiotic Star SS73 17

Science.gov (United States)

Eze, R. N. C.; Luna, G. J. M.; Smith, R. K.

2010-01-01

SS73 17 was an innocuous Mira-type symbiotic star until the International Gamma-Ray Astrophysics Laboratory and Swift discovered its bright hard X-ray emission, adding it to the small class of "hard X-ray emitting symbiotics." Suzaku observations in 2006 then showed it emits three bright iron lines as well, with little to no emission in the 0.3-2.0 keV bandpass. We present here follow-up observations with the Chandra High Energy Transmission Grating and Suzaku that confirm the earlier detection of strong emission lines of Fe K(alpha) fluorescence, Fe XXV and Fe XXVI but also show significantly more soft X-ray emission. The high-resolution spectrum also shows emission lines of other highly ionized ions as Si xiv and possibly S XVI. In addition, a re-analysis of the 2006 Suzaku data using the latest calibration shows that the hard (15-50 keV) X-ray emission is brighter than previously thought and remains constant in both the 2006 and 2008 data. The G ratio calculated from the Fe xxv lines shows that these lines are thermal, not photoionized, in origin.With the exception of the hard X-ray emission, the spectra from both epochs can be fit using thermal radiation assuming a differential emission measure based on a cooling-flow model combined with a full and partial absorber. We show that acceptable fits can be obtained for all the data in the 1-10 keV band varying only the partial absorber. Based on the temperature and accretion rate, the thermal emission appears to be arising from the boundary layer between the accreting white dwarf and the accretion disk.

HIGH-RESOLUTION X-RAY SPECTRA OF THE SYMBIOTIC STAR SS73 17

International Nuclear Information System (INIS)

Eze, R. N. C.; Luna, G. J. M.; Smith, R. K.

2010-01-01

SS73 17 was an innocuous Mira-type symbiotic star until the International Gamma-Ray Astrophysics Laboratory and Swift discovered its bright hard X-ray emission, adding it to the small class of 'hard X-ray emitting symbiotics'. Suzaku observations in 2006 then showed it emits three bright iron lines as well, with little to no emission in the 0.3-2.0 keV bandpass. We present here follow-up observations with the Chandra High Energy Transmission Grating and Suzaku that confirm the earlier detection of strong emission lines of Fe Kα fluorescence, Fe XXV and Fe XXVI but also show significantly more soft X-ray emission. The high-resolution spectrum also shows emission lines of other highly ionized ions as Si XIV and possibly S XVI. In addition, a re-analysis of the 2006 Suzaku data using the latest calibration shows that the hard (15-50 keV) X-ray emission is brighter than previously thought and remains constant in both the 2006 and 2008 data. The G ratio calculated from the Fe XXV lines shows that these lines are thermal, not photoionized, in origin. With the exception of the hard X-ray emission, the spectra from both epochs can be fit using thermal radiation assuming a differential emission measure based on a cooling-flow model combined with a full and partial absorber. We show that acceptable fits can be obtained for all the data in the 1-10 keV band varying only the partial absorber. Based on the temperature and accretion rate, the thermal emission appears to be arising from the boundary layer between the accreting white dwarf and the accretion disk.

Imaging of exploding wire plasmas by high-luminosity monochromatic X-ray backlighting using an X-pinch radiation source

Energy Technology Data Exchange (ETDEWEB)

Pikuz, S A; Shelkovenko, T A; Romanova, V M [Russian Academy of Sciences, Moscow (Russian Federation). P.N. Lebedev Physical Inst.; Hammer, D A [Cornell Univ., Ithaca, NY (United States). Laboratory of Plasma Studies; Faenov, A Ya; Pikuz, T A [VNIIFTRI, Mendeleevo (Russian Federation). Multicharged Ions Spectral Data Center

1997-12-31

A new diagnostic method for dense plasmas, monochromatic x-ray backlighting, is described. In this method, shadow images of a bright, dense plasma can be obtained with high spatial resolution using monochromatic radiation from a separate plasma, permitting a major reduction in the required backlighting source power. The object plasma is imaged utilizing spherically bent mica crystals as the x-ray optical elements. Images of test objects obtained using x-ray radiation having different photon energies are presented. Shadow images of exploding Al wire plasmas in the ls{sup 2}-1s3p line radiation of He-like Al XII are also shown. Spatial resolution as fine as 4 {mu}m is demonstrated. The scheme described is useful for backlighting extended high density plasmas, and could be a less costly alternative to using X-ray lasers for such purposes. (author). 7 figs., 10 refs.

Differential dose albedo for high-energy X-rays on concrete slab

International Nuclear Information System (INIS)

Kato, Hideki

2006-01-01

We computed the differential dose albedo (α D ) for high-energy X-rays on a concrete slab when the incident angle, reflection angle, and azimuth angle were changed, by means of Monte Carlo simulation. We found that α D changed with incident, reflection, and azimuth angles to the concrete slab. On the whole, the larger the incident angle, the larger α D tended to become. If the incident angle and reflection angle were the same, the larger the azimuth angle, the smaller α D tended to become. When the incident, reflection, and azimuth angles were the same, the smaller the X-ray energy was, the larger α D became, in the order of 10 MV, 6 MV, and 4 MV X-rays. (author)

Material Discriminated X-Ray CT System by Using New X-Ray Imager with Energy Discriminate Function

Directory of Open Access Journals (Sweden)

Toru Aoki

2008-04-01

Full Text Available Material discriminated X-ray CT system has been constructed by using conventional X-ray tube (white X-ray source and photon-counting X-ray imager as an application with energy band detection. We have already reported material identify X-ray CT using K-shell edge method elsewhere. In this report the principle of material discrimination was adapted the separation of electron-density and atomic number from attenuation coefficient mapping in X-ray CT reconstructed image in two wavelength X-ray CT method using white X-ray source and energy discriminated X-ray imager by using two monochrome X-ray source method. The measurement phantom was prepared as four kinds material rods (Carbon(C, Iron(Fe, Copper(Cu, Titanium(Ti rods of 3mm-diameter inside an aluminum(Al rod of 20mm-diameter. We could observed material discriminated X-ray CT reconstructed image, however, the discrimination properties were not good than two monochrome X-ray CT method. This results was could be explained because X-ray scattering, beam-hardening and so on based on white X-ray source, which could not observe in two monochrome X-ray CT method. However, since our developed CdTe imager can be detect five energy-bands at the same time, we can use multi-band analysis to decrease the least square error margin. We will be able to obtain more high separation in atomic number mapping in X-ray CT reconstructed image by using this system.

New techniques provide low-cost X-ray inspection of highly attenuating materials

International Nuclear Information System (INIS)

Stupin, D.M.; Mueller, K.H.; Viskoe, D.A.; Howard, B.; Poland, R.W.; Schneberk, D.; Dolan, K.; Thompson, K.; Stoker, G.

1995-01-01

As a result of an arms reduction treaty between the United States and the Russian Federation, both countries will each be storing over 40,000 containers of plutonium. To help detect any deterioration of the containers and prevent leakage, the authors are designing a digital radiography and computed tomography system capable of handling this volume reliably, efficiently, and at a lower cost. The materials to be stored have very high x-ray attenuations, and, in the past, were inspected using 1- to 24-MV x-ray sources. This inspection system, however, uses a new scintillating (Lockheed) glass and an integrating CCD camera. Preliminary experiments show that this will permit the use of a 450-kV x-ray source. This low-energy system will cost much less than others designed to use a higher-energy x-ray source because it will require a less expensive source, less shielding, and less floor space. Furthermore, they can achieve a tenfold improvement in spatial resolution by using their knowledge of the point-spread function of the x-ray imaging system and a least-squares fitting technique

Novel opportunities for sub-meV inelastic X-ray scattering at high-repetition rate self-seeded X-ray free-electron lasers

International Nuclear Information System (INIS)

Chubar, Oleg; Kocharyan, Vitali; Saldin, Evgeni; Serkez, Svitozar; Shvyd'ko, Yuri

2015-08-01

Inelastic X-ray scattering (IXS) is an important tool for studies of equilibrium dynamics in condensed matter. A new spectrometer recently proposed for ultra-high-resolution IXS (UHRIX) has achieved 0.6 meV and 0.25 nm -1 spectral and momentum transfer resolutions, respectively. However, further improvements down to 0.1 meV and 0.02 nm -1 are required to close the gap in energy-momentum space between high and low frequency probes. We show that this goal can be achieved by further optimizing the X-ray optics and by increasing the spectral flux of the incident X-ray pulses. UHRIX performs best at energies from 5 to 10 keV, where a combination of self-seeding and undulator tapering at the SASE-2 beamline of the European XFEL promises up to a hundred-fold increase in average spectral flux compared with nominal SASE pulses at saturation, or three orders of magnitude more than possible with storage-ring based radiation sources. Wave-optics propagation shows that about 7 x 10 12 ph/s in a 90-μeV bandwidth can be achieved on the sample. This will provide unique new possibilities for dynamics studies by IXS.

High resolution solar soft X-ray spectrometer

International Nuclear Information System (INIS)

Zhang Fei; Wang Huanyu; Peng Wenxi; Liang Xiaohua; Zhang Chunlei; Cao Xuelei; Jiang Weichun; Zhang Jiayu; Cui Xingzhu

2012-01-01

A high resolution solar soft X-ray spectrometer (SOX) payload onboard a satellite is developed. A silicon drift detector (SDD) is adopted as the detector of the SOX spectrometer. The spectrometer consists of the detectors and their readout electronics, a data acquisition unit and a payload data handling unit. A ground test system is also developed to test SOX. The test results show that the design goals of the spectrometer system have been achieved. (authors)

X-ray outbursts and high-state episodes of HETE J1900.1-2455

Science.gov (United States)

Šimon, Vojtěch

2018-06-01

HETE J1900.1-2455 is an ultra-compact low-mass X-ray binary that underwent a long-lasting (about 10 yr) active state. The analysis presented here of its activity uses the observations of RXTE/ASM, Swift/BAT, and ISS/MAXI for investigating this active state and the relation of time evolution of fluxes in the hard and medium X-ray bands. We show that the variations of the flux of HETE J1900.1-2455 on the time-scales of days and weeks have the form both of the outbursts and occasional high-state episodes. These outbursts are accompanied by the large changes of the hardness of the spectrum in the surroundings of the peaks of their soft X-ray flux. The very strong peaks of these outbursts occur in the soft X-ray band (2-4 keV) and are accompanied by a large depression in the 15-50 keV band flux. We interpret these events as an occasional occurrence of a thermal-viscous instability of the accretion disc that gives rise to the outbursts similar to those in the soft X-ray transients. On the other hand, the 2-4 and the 15-50 keV band fluxes are mutually correlated in the high-state episodes, much longer than the outbursts. In the interpretation, the episodes of the X-ray high states of HETE J1900.1-2455 during the active state bear some analogy with the standstills in the Z Cam type of cataclysmic variables.

Surface slope metrology of highly curved x-ray optics with an interferometric microscope

Science.gov (United States)

Gevorkyan, Gevork S.; Centers, Gary; Polonska, Kateryna S.; Nikitin, Sergey M.; Lacey, Ian; Yashchuk, Valeriy V.

2017-09-01

The development of deterministic polishing techniques has given rise to vendors that manufacture high quality threedimensional x-ray optics. The surface metrology on these optics remains a difficult task. For the fabrication, vendors usually use unique surface metrology tools, generally developed on site, that are not available in the optical metrology labs at x-ray facilities. At the Advanced Light Source X-Ray Optics Laboratory, we have developed a rather straightforward interferometric-microscopy-based procedure capable of sub microradian characterization of sagittal slope variation of x-ray optics for two-dimensionally focusing and collimating (such as ellipsoids, paraboloids, etc.). In the paper, we provide the mathematical foundation of the procedure and describe the related instrument calibration. We also present analytical expression describing the ideal surface shape in the sagittal direction of a spheroid specified by the conjugate parameters of the optic's beamline application. The expression is useful when analyzing data obtained with such optics. The high efficiency of the developed measurement and data analysis procedures is demonstrated in results of measurements with a number of x-ray optics with sagittal radius of curvature between 56 mm and 480 mm. We also discuss potential areas of further improvement.

Total Reflection X-ray Fluorescence Analysis (TXRF) using the high flux SAXS camera

CERN Document Server

Wobrauschek, P; Pepponi, G; Bergmann, A; Glatter, O

2002-01-01

Combining the high photon flux from a rotating anode X-ray tube with an X-ray optical component to focus and monochromatize the X-ray beam is the most promising instrumentation for best detection limits in the modern XRF laboratory. This is realized by using the design of a high flux SAXS camera in combination with a 4 kW high brilliant rotating Cu anode X-ray tube with a graded elliptically bent multilayer and including a new designed module for excitation in total reflection geometry within the beam path. The system can be evacuated thus reducing absorption and scattering of air and removing the argon peak in the spectra. Another novelty is the use of a Peltier cooled drift detector with an energy resolution of 148 eV at 5.9 keV and 5 mm sup 2 area. For Co detection limits of about 300 fg determined by a single element standard have been achieved. Testing a real sample NIST 1643d led to detection limits in the range of 300 ng/l for the medium Z.

A hard x-ray spectrometer for high angular resolution observations of cosmic sources

International Nuclear Information System (INIS)

Hailey, C.J.; Ziock, K.P.; Harrison, F.; Kahn, S.M.; Liedahl, D.; Lubin, P.M.; Seiffert, M.

1988-01-01

LAXRIS (large area x-ray imaging spectrometer) is an experimental, balloon-borne, hard x-ray telescope that consists of a coaligned array of x-ray imaging spectrometer modules capable of obtaining high angular resolution (1--3 arcminutes) with moderate energy resolution in the 20- to 300-keV region. Each spectrometer module consists of a CsI(Na) crystal coupled to a position-sensitive phototube with a crossed-wire, resistive readout. Imaging is provided by a coded aperture mask with a 4-m focal length. The high angular resolution is coupled with rather large area (/approximately/800 cm 2 ) to provide good sensitivity. Results are presented on performance and overall design. Sensitivity estimates are derived from a Monte-Carlo code developed to model the LAXRIS response to background encountered at balloon altitudes. We discuss a variety of observations made feasible by high angular resolution. For instance, spatially resolving the nonthermal x-ray emission from clusters of galaxies is suggested as an ideal program for LAXRIS. 15 refs., 5 figs

Development of X-ray CCD camera system with high readout rate using ASIC

International Nuclear Information System (INIS)

Nakajima, Hiroshi; Matsuura, Daisuke; Anabuki, Naohisa; Miyata, Emi; Tsunemi, Hiroshi; Doty, John P.; Ikeda, Hirokazu; Katayama, Haruyoshi

2009-01-01

We report on the development of an X-ray charge-coupled device (CCD) camera system with high readout rate using application-specific integrated circuit (ASIC) and Camera Link standard. The distinctive ΔΣ type analog-to-digital converter is introduced into the chip to achieve effective noise shaping and to obtain a high resolution with relatively simple circuits. The unit test proved moderately low equivalent input noise of 70μV with a high readout pixel rate of 625 kHz, while the entire chip consumes only 100 mW. The Camera Link standard was applied for the connectivity between the camera system and frame grabbers. In the initial test of the whole system, we adopted a P-channel CCD with a thick depletion layer developed for X-ray CCD camera onboard the next Japanese X-ray astronomical satellite. The characteristic X-rays from 109 Cd were successfully read out resulting in the energy resolution of 379(±7)eV (FWHM) at 22.1 keV, that is, ΔE/E=1.7% with a readout rate of 44 kHz.

Phase-contrast X-ray CT

Energy Technology Data Exchange (ETDEWEB)

Momose, Atsushi [Hitachi Ltd., Saitama (Japan). Advanced Research Laboratory; Takeda, Tohoru; Itai, Yuji

1995-12-01

Phase-contrast X-ray computed tomography (CT) enabling the observation of biological soft tissues without contrast enhancement has been developed. The X-ray phase shift caused by an object is measured and input to a standard CT reconstruction algorithm. A thousand times increase in the image sensitivity to soft tissues is achieved compared with the conventional CT using absorption contrast. This is because the X-ray phase shift cross section of light elements is about a thousand times larger than the absorption cross section. The phase shift is detected using an X-ray interferometer and computer analyses of interference patterns. Experiments were performed using a synchrotron X-ray source. Excellent image sensitivity is demonstrated in the observation of cancerous rabbit liver. The CT images distinguish cancer lesion from normal liver tissue and, moreover, visualize the pathological condition in the lesion. Although the X-ray energy employed and the present observation area size are not suitable for medical applications as they are, phase-contrast X-ray CT is promising for investigating the internal structure of soft tissue which is almost transparent for X-rays. The high sensitivity also provides the advantage of reducing X-ray doses. (author).

High-speed videography combined with an x-ray image intensifier for dynamic radiography

International Nuclear Information System (INIS)

Bryant, L.E. Jr.

1983-01-01

The Spin Physics SP-2000 high-speed video system can be combined with an x-ray source, a dynamic event having internal (not directly visible) movement and an x-ray image intensifier to perform dynamic radiography. The cesium iodide input fluor and P-20 output fluor of the image intensifier have rapid decay to allow x-ray imaging up to 12,000 pictures per second. Applications of this technique include internal functioning of a compressor, turbulent-water action, and other mechanical actions

High resolution X-ray diffraction studies on unirradiated

Indian Academy of Sciences (India)

High-resolution X-ray diffraction technique, employing a three-crystal monochromator–collimator combination is used to study the irradiation induced defects in flux grown Sr-hexaferrite crystals irradiated with 50 MeV Li3+ ion beams at room temperature with a fluence value of 1 × 1014 ions/cm2. The diffraction curves of the ...

Advanced ceramic matrix composites for high energy x-ray generation

International Nuclear Information System (INIS)

Khan, Amir Azam; Labbe, Jean Claude

2011-01-01

High energy x-ray targets are the anodes used in high performance tubes, designed to work for long operating times and at high power. Such tubes are used in computed tomography (CT) scan machines. Usually the tubes used in CT scanners have to continuously work at high temperatures and for longer scan durations in order to get maximum information during a single scan. These anodes are composed of a refractory substrate which supports a refractory metallic coating. The present work is a review of the development of a ceramic metal composite based on aluminium nitride (AlN) and molybdenum for potential application as the substrate. This composite is surface engineered by coating with tungsten, the most popular material for high energy x-ray targets. To spray metallic coatings on the surface of ceramic matrix composites dc blown arc plasma is employed. The objective is to increase the performance and the life of an x-ray tube. Aluminium nitride-molybdenum ceramic matrix composites were produced by uniaxial hotpressing mixtures of AlN and Mo powders. These composites were characterized for their mechanical, thermal, electrical and micro-structural properties. An optimized composition was selected which contained 25 vol.% of metallic phase dispersed in the AlN matrix. These composites were produced in the actual size of an anode and coated with tungsten through dc blown arc plasma spraying. The results have shown that sintering of large size anodes is possible through uniaxial pressing, using a modified sintering cycle

The Athena X-ray Integral Field Unit (X-IFU)

NARCIS (Netherlands)

Barret, Didier; Lam Trong, Thien; den Herder, Jan-Willem; Piro, Luigi; Barcons, Xavier; Huovelin, Juhani; Kelley, Richard; Mas-Hesse, J. Miguel; Mitsuda, Kazuhisa; Paltani, Stéphane; Rauw, Gregor; RoŻanska, Agata; Wilms, Joern; Barbera, Marco; Bozzo, Enrico; Ceballos, Maria Teresa; Charles, Ivan; Decourchelle, Anne; den Hartog, Roland; Duval, Jean-Marc; Fiore, Fabrizio; Gatti, Flavio; Goldwurm, Andrea; Jackson, Brian; Jonker, Peter; Kilbourne, Caroline; Macculi, Claudio; Mendez, Mariano; Molendi, Silvano; Orleanski, Piotr; Pajot, François; Pointecouteau, Etienne; Porter, Frederick; Pratt, Gabriel W.; Prêle, Damien; Ravera, Laurent; Renotte, Etienne; Schaye, Joop; Shinozaki, Keisuke; Valenziano, Luca; Vink, Jacco; Webb, Natalie; Yamasaki, Noriko; Delcelier-Douchin, Françoise; Le Du, Michel; Mesnager, Jean-Michel; Pradines, Alice; Branduardi-Raymont, Graziella; Dadina, Mauro; Finoguenov, Alexis; Fukazawa, Yasushi; Janiuk, Agnieszka; Miller, Jon; Nazé, Yaël; Nicastro, Fabrizio; Sciortino, Salvatore; Torrejon, Jose Miguel; Geoffray, Hervé; Hernandez, Isabelle; Luno, Laure; Peille, Philippe; André, Jérôme; Daniel, Christophe; Etcheverry, Christophe; Gloaguen, Emilie; Hassin, Jérémie; Hervet, Gilles; Maussang, Irwin; Moueza, Jérôme; Paillet, Alexis; Vella, Bruno; Campos Garrido, Gonzalo; Damery, Jean-Charles; Panem, Chantal; Panh, Johan; Bandler, Simon; Biffi, Jean-Marc; Boyce, Kevin; Clénet, Antoine; DiPirro, Michael; Jamotton, Pierre; Lotti, Simone; Schwander, Denis; Smith, Stephen; van Leeuwen, Bert-Joost; van Weers, Henk; Brand, Thorsten; Cobo, Beatriz; Dauser, Thomas; de Plaa, Jelle; Cucchetti, Edoardo

2016-01-01

The X-ray Integral Field Unit (X-IFU) on board the Advanced Telescope for High-ENergy Astrophysics (Athena) will provide spatially resolved high-resolution X-ray spectroscopy from 0.2 to 12 keV, with 5" pixels over a field of view of 5 arc minute equivalent diameter and a spectral resolution of 2.5

HIGH ENERGY, HIGH BRIGHTNESS X-RAYS PRODUCED BY COMPTON BACKSCATTERING AT THE LIVERMORE PLEIADES FACILITY

International Nuclear Information System (INIS)

Tremaine, A M; Anderson, S G; Betts, S; Crane, J; Gibson, D J; Hartemann, F V; Jacob, J S; Frigola, P; Lim, J; Rosenzweig, J; Travish, G

2005-01-01

PLEIADES (Picosecond Laser Electron Interaction for the Dynamic Evaluation of Structures) produces tunable 30-140 keV x-rays with 0.3-5 ps pulse lengths and up to 10 7 photons/pulse by colliding a high brightness electron beam with a high power laser. The electron beam is created by an rf photo-injector system, accelerated by a 120 MeV linac, and focused to 20 (micro)m with novel permanent magnet quadrupoles. To produce Compton back scattered x-rays, the electron bunch is overlapped with a Ti:Sapphire laser that delivers 500 mJ, 100 fs, pulses to the interaction point. K-edge radiography at 115 keV on Uranium has verified the angle correlated energy spectrum inherent in Compton scattering and high-energy tunability of the Livermore source. Current upgrades to the facility will allow laser pumping of targets synchronized to the x-ray source enabling dynamic diffraction and time-resolved studies of high Z materials. Near future plans include extending the radiation energies to >400 keV, allowing for nuclear fluorescence studies of materials

X-ray imaging system

International Nuclear Information System (INIS)

Houston, J.M.

1980-01-01

A novel, high-speed apparatus for use in X-ray computerised tomography is described in detail. It consists of a semi-circular array of X-ray sources, collimators and an ion chamber array for detection of the X-rays. The X-ray sources may be pulsed in salvos such that the corresponding detectors in the array are only illuminated by one source. The use of computer controlled salvos speeds up the image processing by at least a factor of two. The ion chamber array is designed to have a constant detection efficiency for varying angles of X-ray incidence. A detailed description of the detector construction and suggested gaseous fillings are given. It is claimed that the present tomographic system allows fast and accurate imaging of internal body organs and is insensitive to the blurring effects which motion of these organs tends to produce. (UK)

Precision mechanical structure of an ultra-high-resolution spectrometer for inelastic X-ray scattering instrument

Science.gov (United States)

Shu, Deming; Shvydko, Yuri; Stoupin, Stanislav A.; Khachatryan, Ruben; Goetze, Kurt A.; Roberts, Timothy

2015-04-14

A method and an ultrahigh-resolution spectrometer including a precision mechanical structure for positioning inelastic X-ray scattering optics are provided. The spectrometer includes an X-ray monochromator and an X-ray analyzer, each including X-ray optics of a collimating (C) crystal, a pair of dispersing (D) element crystals, anomalous transmission filter (F) and a wavelength (W) selector crystal. A respective precision mechanical structure is provided with the X-ray monochromator and the X-ray analyzer. The precision mechanical structure includes a base plate, such as an aluminum base plate; positioning stages for D-crystal alignment; positioning stages with an incline sensor for C/F/W-crystal alignment, and the positioning stages including flexure-based high-stiffness structure.

Small scale soft x-ray lasers

International Nuclear Information System (INIS)

Skinner, C.H.; DiCicco, D.S.; Kim, D.; Voorhees, D.; Suckewer, S.

1990-01-01

The widespread application of soft x-ray laser technology is contingent on the development of small scale soft x-ray lasers that do not require large laser facilities. Progress in the development of soft x-ray lasers pumped by a Nd laser of energy 6-12J is reported below. Application of an existing soft x-ray laser to x-ray microscopy has begun. A soft x-ray laser of output energy 1-3 mJ at 18,2 nm has been used to record high resolution images of biological specimens. The contact images were recorded on photoresist which was later viewed in a scanning electron microscope. The authors present a composite optical x-ray laser microscope design

High Resolution, Non-Dispersive X-Ray Calorimeter Spectrometers on EBITs and Orbiting Observatories

Science.gov (United States)

Porter, Frederick S.

2010-01-01

X-ray spectroscopy is the primary tool for performing atomic physics with Electron beam ion trap (EBITs). X-ray instruments have generally fallen into two general categories, 1) dispersive instruments with very high spectral resolving powers but limited spectral range, limited count rates, and require an entrance slit, generally, for EBITs, defined by the electron beam itself, and 2) non-dispersive solid-state detectors with much lower spectral resolving powers but that have a broad dynamic range, high count rate ability and do not require a slit. Both of these approaches have compromises that limit the type and efficiency of measurements that can be performed. In 1984 NASA initiated a program to produce a non-dispersive instrument with high spectral resolving power for x-ray astrophysics based on the cryogenic x-ray calorimeter. This program produced the XRS non-dispersive spectrometers on the Astro-E, Astro-E2 (Suzaku) orbiting observatories, the SXS instrument on the Astro-H observatory, and the planned XMS instrument on the International X-ray Observatory. Complimenting these spaceflight programs, a permanent high-resolution x-ray calorimeter spectrometer, the XRS/EBIT, was installed on the LLNL EBIT in 2000. This unique instrument was upgraded to a spectral resolving power of 1000 at 6 keV in 2003 and replaced by a nearly autonomous production-class spectrometer, the EBIT Calorimeter Spectrometer (ECS), in 2007. The ECS spectrometer has a simultaneous bandpass from 0.07 to over 100 keV with a spectral resolving power of 1300 at 6 keV with unit quantum efficiency, and 1900 at 60 keV with a quantum efficiency of 30%. X-ray calorimeters are event based, single photon spectrometers with event time tagging to better than 10 us. We are currently developing a follow-on instrument based on a newer generation of x-ray calorimeters with a spectral resolving power of 3000 at 6 keV, and improved timing and measurement cadence. The unique capabilities of the x-ray

Toward Adaptive X-Ray Telescopes

Science.gov (United States)

O'Dell, Stephen L.; Atkins, Carolyn; Button, Tim W.; Cotroneo, Vincenzo; Davis, William N.; Doel, Peer; Feldman, Charlotte H.; Freeman, Mark D.; Gubarev, Mikhail V.; Kolodziejczak, Jeffrey J.;

High-energy Neutrino Flares from X-Ray Bright and Dark Tidal Disruption Events

Energy Technology Data Exchange (ETDEWEB)

Senno, Nicholas; Murase, Kohta; Mészáros, Peter [Department of Physics, The Pennsylvania State University, University Park, PA 16802 (United States)

2017-03-20

X-ray and γ-ray observations by the Swift satellite revealed that a fraction of tidal disruption events (TDEs) have relativistic jets. Jetted TDEs have been considered to be potential sources of very-high-energy cosmic-rays and neutrinos. In this work, using semi-analytical methods, we calculate neutrino spectra of X-ray bright TDEs with powerful jets and dark TDEs with possible choked jets, respectively. We estimate their neutrino fluxes and find that non-detection would give us an upper limit on the baryon loading of the jet luminosity contained in cosmic-rays ξ {sub cr} ≲ 20–50 for Sw J1644+57. We show that X-ray bright TDEs make a sub-dominant (≲5%–10%) contribution to IceCube’s diffuse neutrino flux, and study possible contributions of X-ray dark TDEs given that particles are accelerated in choked jets or disk winds. We discuss future prospects for multi-messenger searches of the brightest TDEs.

X-ray area monitor

International Nuclear Information System (INIS)

Nintrakit, N.

1983-01-01

The X-ray area monitor is a nuclear electronic device that is essential in radiation protection in high radiation laboratories, e.g. in medical diagnosis using X-rays and in industrial X-radiography. Accidentally the level of X-radiator may arise above the safe permissible level and in such a case the alarm system of the area monitor will work and disconnect the ac power supply form the X-ray unit. Principally the device is a radiation counter using G.M.tube as radiation detector with high voltage supply variable form 200 to 2,000 volts. The maximum count rate of the scaler is 1.5 MHz and the total count is displayed on 4 digit LED's. A time base is used to control the counting time, the frequency multiplier, radiation safety limit, comparator and the radiation hazard warning signal. The reliability of the instrument is further enhanced through the addition of the random correction circuit, and it is applicable both in X- and γ -radiation

X-ray astronomy

International Nuclear Information System (INIS)

Giacconi, R.; Setti, G.

1980-01-01

This book contains the lectures, and the most important seminars held at the NATO meeting on X-Ray astronomy in Erice, July 1979. The meeting was an opportune forum to discuss the results of the first 8-months of operation of the X-ray satellite, HEAO-2 (Einstein Observatory) which was launched at the end of 1978. Besides surveying these results, the meeting covered extragalactic astronomy, including the relevant observations obtained in other portions of the electromagnetic spectrum (ultra-violet, optical, infrared and radio). The discussion on galactic X-ray sources essentially covered classical binaries, globular clusters and bursters and its significance to extragalactic sources and to high energy astrophysics was borne in mind. (orig.)

Quasimonochromatic x-ray computed tomography by the balanced filter method using a conventional x-ray source

International Nuclear Information System (INIS)

Saito, Masatoshi

2004-01-01

A quasimonochromatic x-ray computed tomography (CT) system utilizing balanced filters has recently been developed for acquiring quantitative CT images. This system consisted of basic components such as a conventional x-ray generator for radiography, a stage for mounting and rotating objects, and an x-ray line sensor camera. Metallic sheets of Er and Yb were used as the balanced filters for obtaining quasimonochromatic incident x rays that include the characteristic lines of the W Kα doublet from a tungsten target. The mean energy and energy width of the quasimonochromatic x rays were determined to be 59.0 and 1.9 keV, respectively, from x-ray spectroscopic measurements using a high-purity Ge detector. The usefulness of the present x-ray CT system was demonstrated by obtaining spatial distributions of the linear attenuation coefficients of three selected samples--a 20 cm diameter cylindrical water phantom, a 3.5 cm diameter aluminum rod, and a human head phantom. The results clearly indicate that this apparatus is surprisingly effective for estimating the distribution of the linear attenuation coefficients without any correction of the beam-hardening effect. Thus, implementing the balanced filter method on an x-ray CT scanner has promise in producing highly quantitative CT images

Discovery of Hard Nonthermal Pulsed X-Ray Emission from the Anomalous X-Ray Pulsar 1E 1841-045

NARCIS (Netherlands)

Kuiper, L.; Hermsen, W.; Méndez, R.M.

2004-01-01

We report the discovery of nonthermal pulsed X-ray/soft gamma-ray emission up to ~150 keV from the anomalous 11.8 s X-ray pulsar AXP 1E 1841-045 located near the center of supernova remnant Kes 73 using Rossi X-Ray Timing Explorer (RXTE) Proportional Counter Array and High Energy X-Ray Timing

X-Ray

Science.gov (United States)

... enema. What you can expect During the X-ray X-rays are performed at doctors' offices, dentists' offices, ... as those using a contrast medium. Your child's X-ray Restraints or other techniques may be used to ...

Total-reflection x-ray fluorescence with a brillant undulator x-ray source

International Nuclear Information System (INIS)

Sakurai, K.; Eba, H.; Numako, C.; Suzuki, M.; Inoue, K.; Yagi, N.

2000-01-01

Total-reflection x-ray fluorescence (TXRF) is a highly sensitive technique for analyzing trace elements, because of the very low background from the sample support. Use of third-generation synchrotron x-ray source could further enhance the detection power. However, while such high sensitivity permits the detection of signals from trace elements of interest, it also means that one can observe weak parasitic x-rays as well. If the sample surface becomes even slightly contaminated, owing to air particulates near the beamline, x-ray fluorescence lines of iron, zinc, copper, nickel, chromium, and titanium can be observed even for a blank sample. Another critical problem is the low-energy-side tail of the scattering x-rays, which ultimately restricts the detection capability of the technique using a TXRF spectrometer based on a Si(Li) detector. The present paper describes our experiments with brilliant undulator x-ray beams at BL39XU and BL40XU, at the SPring-8, Harima, Japan. The emphasis is on the development of instruments to analyze a droplet of 0.1 μl containing trace elements of ppb level. Although the beamline is not a clean room, we have employed equipment for preparing a clean sample and also for avoiding contamination during transferring the sample into the spectrometer. We will report on the successful detection of the peak from 0.8 ppb selenium in a droplet (absolute amount 80 fg). We will also present the results of recent experiments obtained from a Johansson spectrometer rather than a Si(Li) detector. (author)

Higher coherent x-ray laser

International Nuclear Information System (INIS)

Hasegawa, Noboru; Nagashima, Keisuke; Kawachi, Tetsuya

2001-01-01

X-ray lasers generated by an ultra short pulse laser have advantages such as monochromatic, short pulse duration, small beam divergence, high intensity, and coherence. Spatial coherence is most important for applications, we have investigated the transient collisional excitation (TCE) scheme x-ray laser lasing from Ne-like titanium (31.6 nm), Ne-like silver (13.9 nm) and tin (11.9 nm). However, the spatial coherence was not so good with this scheme. We have been studying to improve the spatial coherence of the x-ray laser and have proposed to use coherent seed light tuned to the x-ray laser wavelength generated from higher harmonics generation (HHG), which is introduced to the x-ray laser medium (Ne-like titanium, Ni-like silver plasmas). We present about the theoretical study of the coupling efficiency HHG light with x-ray laser medium. (author)

Design of a compact high-energy setup for x-ray phase-contrast imaging

Science.gov (United States)

Schüttler, Markus; Yaroshenko, Andre; Bech, Martin; Potdevin, Guillaume; Malecki, Andreas; Chabior, Michael; Wolf, Johannes; Tapfer, Arne; Meiser, Jan; Kunka, Danays; Amberger, Maximilian; Mohr, Jürgen; Pfeiffer, Franz

2014-03-01

The main shortcoming of conventional biomedical x-ray imaging is the weak soft-tissue contrast caused by the small differences in the absorption coefficients between different materials. This issue can be addressed by x-ray phasesensitive imaging approaches, e.g. x-ray Talbot-Lau grating interferometry. The advantage of the three-grating Talbot-Lau approach is that it allows to acquire x-ray phase-contrast and dark-field images with a conventional lab source. However, through the introduction of the grating interferometer some constraints are imposed on the setup geometry. In general, the grating pitch and the mean x-ray energy determine the setup dimensions. The minimal length of the setup increases linearly with energy and is proportional to p2, where p is the grating pitch. Thus, a high-energy (100 keV) compact grating-based setup for x-ray imaging can be realized only if gratings with aspect-ratio of approximately 300 and a pitch of 1-2 μm were available. However, production challenges limit the availability of such gratings. In this study we consider the use of non-binary phase-gratings as means of designing a more compact grating interferometer for phase-contrast imaging. We present simulation and experimental data for both monochromatic and polychromatic case. The results reveal that phase-gratings with triangular-shaped structures yield visibilities that can be used for imaging purposes at significantly shorter distances than binary gratings. This opens the possibility to design a high-energy compact setup for x-ray phase-contrast imaging. Furthermore, we discuss different techniques to achieve triangular-shaped phase-shifting structures.

Soft x-ray streak cameras

International Nuclear Information System (INIS)

Stradling, G.L.

1988-01-01

This paper is a discussion of the development and of the current state of the art in picosecond soft x-ray streak camera technology. Accomplishments from a number of institutions are discussed. X-ray streak cameras vary from standard visible streak camera designs in the use of an x-ray transmitting window and an x-ray sensitive photocathode. The spectral sensitivity range of these instruments includes portions of the near UV and extends from the subkilovolt x- ray region to several tens of kilovolts. Attendant challenges encountered in the design and use of x-ray streak cameras include the accommodation of high-voltage and vacuum requirements, as well as manipulation of a photocathode structure which is often fragile. The x-ray transmitting window is generally too fragile to withstand atmospheric pressure, necessitating active vacuum pumping and a vacuum line of sight to the x-ray signal source. Because of the difficulty of manipulating x-ray beams with conventional optics, as is done with visible light, the size of the photocathode sensing area, access to the front of the tube, the ability to insert the streak tube into a vacuum chamber and the capability to trigger the sweep with very short internal delay times are issues uniquely relevant to x-ray streak camera use. The physics of electron imaging may place more stringent limitations on the temporal and spatial resolution obtainable with x-ray photocathodes than with the visible counterpart. Other issues which are common to the entire streak camera community also concern the x-ray streak camera users and manufacturers

Time-resolved X-ray PIV technique for diagnosing opaque biofluid flow with insufficient X-ray fluxes.

Science.gov (United States)

Jung, Sung Yong; Park, Han Wook; Kim, Bo Heum; Lee, Sang Joon

2013-05-01

X-ray imaging is used to visualize the biofluid flow phenomena in a nondestructive manner. A technique currently used for quantitative visualization is X-ray particle image velocimetry (PIV). Although this technique provides a high spatial resolution (less than 10 µm), significant hemodynamic parameters are difficult to obtain under actual physiological conditions because of the limited temporal resolution of the technique, which in turn is due to the relatively long exposure time (~10 ms) involved in X-ray imaging. This study combines an image intensifier with a high-speed camera to reduce exposure time, thereby improving temporal resolution. The image intensifier amplifies light flux by emitting secondary electrons in the micro-channel plate. The increased incident light flux greatly reduces the exposure time (below 200 µs). The proposed X-ray PIV system was applied to high-speed blood flows in a tube, and the velocity field information was successfully obtained. The time-resolved X-ray PIV system can be employed to investigate blood flows at beamlines with insufficient X-ray fluxes under specific physiological conditions. This method facilitates understanding of the basic hemodynamic characteristics and pathological mechanism of cardiovascular diseases.

The SWARF high energy flash X-ray facility

International Nuclear Information System (INIS)

Gilbert, J.F.; Dove, E.W.D.

1976-06-01

A description is presented of the SWARF flash radiography facility at AWRE Foulness, which is stated to be the most powerful flash x-ray system available, in the U.K. The machine consists essentially of a Marx generator, a coaxial Blumlein system and an x-ray tube. The voltage output from the Marx generator (about 2.5 MV from an 80 kV input) is applied to a large re-entrant Blumlein pulse-forming line. Near maximum voltage, an adjustable oil switch short-circuits one end of the Blumlein generator and so applies a square voltage pulse of 65 ns duration to the x-ray tube. The x-rays are produced from a tantalum target which forms the anode of a vacuum field emission diode. The facility consists of two field machines positioned so that radiographs can be obtained from different angles. The description is given under the following heads: modus operandi; constructional details; oil installation; electrical details; commissioning, calibration and electrical data; flash radiography in explosives research; operational control of facility, film packs; radiographic results; further developments; overall performance. (U.K.)

The Nuclear Spectroscopic Telescope Array (NuSTAR) High-Energy X-ray Mission

Science.gov (United States)

Harrison, Fiona A.; Craig, Willliam W.; Christensen, Finn E.; Hailey, Charles J.; Zhang, William W.; Boggs, Steven E.; Stern, Daniel; Cook, W. Rick; Forster, Karl; Giommi, Paolo;

Black hole and neutron star soft X-ray transients: a hard X-ray view of their outbursts

International Nuclear Information System (INIS)

Yu, W.

2004-01-01

The RXTE public observations of the outbursts of black hole soft X-ray transients XTE J1550-564, XTE J1859+226, 4U 1630-47, XTE J1118+480, XTE J1650-500, and the neutron star soft X-ray transients 4U 1608-52, Aquila X-1, including a variable 'persistent' neutron star low mass X-ray binary 4U 1705-44, are summarized in this paper. The hard X-ray view of those outbursts, which is quite different from that of the soft X-ray band, suggests that there are several types of outbursts which result in different hard X-ray outburst profile - the outburst profiles are energy dependent. One type is the low/hard state outbursts, the other type is the outburst showing transitions from the low/hard state to the high/soft state, or to the intermediate or to the very high state. The later has an initial low/hard state, introducing the phenomena that the hard X-ray precedes the soft X-ray in the outburst rise. Such outbursts in XTE J1550-564, Aql X-1 and 4U 1705-44 support a two-accretion-flow model which involves one Keplerian disk flow and one sub-Keplerian flow for the initial outburst rise

High-current Rhodotron for X-ray facility

International Nuclear Information System (INIS)

Umezu, Toru; Tsujiura, Yuichiro; Bol, Jean Louis

2009-01-01

The Rhodotron is a widely employed high-power industrial accelerator developed and exclusively distributed by IBA. Most early examples of the accelerator were optimized to operate at 10 MeV. A new Rhodotron configuration recently advanced produces a lower-energy higher-current beam dedicated with x-ray to sterilize and enhancement materials. Core elements of this system's evolution include a higher performance RF electron gun (operating range, response control, and cathode lifetime). This operational machine is now producing 100 mA at 7 MeV (700 kW of beam) and treat medical devices, thick cable and pipes with a high efficiency. (author)

Refractive x-ray lens for high pressure diffraction

International Nuclear Information System (INIS)

Ohishi, Yasuo

2001-01-01

A stacked compound refractive x-ray lens was designed to produce a efficiently focused (φ 2 and a peak gain of 12, is well matched to these requirements. It is composed of many plastic chips made by molding, which is allowing many identical chips to be made precisely. Other advantages of this lens include high throughput, simple energy tunability and easy installation. (author)

Plastic nuclear track detectors as high x-ray and gamma dosimeters

International Nuclear Information System (INIS)

Chong Chon Sing

1995-01-01

A brief review of recent studies on the effects of high doses of x-ray and gamma ray on the track registration properties of several plastic track detectors is presented. The bulk etching rates and the etched track sizes have been found to increase with the dose in the range up to 100 Mrad. These results suggest that the changes in track registration characteristics can be employed as an index of the radiation dose in the megarad region. In particular, recent results on the effect of X-ray irradiation on two types of cellulose nitrate track detectors obtained in our laboratory are reported in this paper. (author)

X-ray emission from comets

International Nuclear Information System (INIS)

Dennerl, Konrad

1999-01-01

When comet Hyakutake (C/1996 B2) encountered Earth in March 1996 at a minimum distance of only 15 million kilometers (40 times the distance of the moon), x-ray and extreme ultraviolet emission was discovered for the first time from a comet. The observations were performed with the astronomy satellites ROSAT and EUVE. A systematic search for x-rays from comets in archival data, obtained during the ROSAT all-sky survey in 1990/91, resulted in the discovery of x-ray emission from four additional comets. They were detected at seven occasions in total, when they were optically 300 to 30 000 times fainter than Hyakutake. These findings indicated that comets represent a new class of celestial x-ray sources. Subsequent detections of x-ray emission from additional comets with the satellites ROSAT, EUVE, and BeppoSAX confirmed this conclusion. The x-ray observations have obviously revealed the presence of a process in comets which had escaped attention until recently. This process is most likely charge exchange between highly charged heavy ions in the solar wind and cometary neutrals. The solar wind, a stream of particles continuously emitted from the sun with ≅ 400 km s -1 , consists predominantly of protons, electrons, and alpha particles, but contains also a small fraction (≅0.1%) of highly charged heavier ions, such as C 6+ ,O 6+ ,Ne 8+ ,Si 9+ ,Fe 11+ . When these ions capture electrons from the cometary gas, they attain highly excited states and radiate a large fraction of their excitation energy in the extreme ultraviolet and x-ray part of the spectrum. Charge exchange reproduces the intensity, the morphology and the spectrum of the observed x-ray emission from comets very well

Electromechanical x-ray generator

Science.gov (United States)

Watson, Scott A; Platts, David; Sorensen, Eric B

2016-05-03

An electro-mechanical x-ray generator configured to obtain high-energy operation with favorable energy-weight scaling. The electro-mechanical x-ray generator may include a pair of capacitor plates. The capacitor plates may be charged to a predefined voltage and may be separated to generate higher voltages on the order of hundreds of kV in the AK gap. The high voltage may be generated in a vacuum tube.

Synchrotron x-ray microbeam characteristics for x-ray fluorescence analysis

International Nuclear Information System (INIS)

Iida, Atsuo; Noma, Takashi

1995-01-01

X-ray fluorescence analysis using a synchrotron x-ray microprobe has become an indispensable technique for non-destructive micro-analysis. One of the most important parameters that characterize the x-ray microbeam system for x-ray fluorescence analysis is the beam size. For practical analysis, however, the photon flux, the energy resolution and the available energy range are also crucial. Three types of x-ray microbeam systems, including monochromatic and continuum excitation systems, were compared with reference to the sensitivity, the minimum detection limit and the applicability to various types of x-ray spectroscopic analysis. 16 refs., 5 figs

X-ray generation by femtosecond laser pulses and its application to soft X-ray imaging microscope

International Nuclear Information System (INIS)

Ikeda, Kenichi; Kotaki, Hideyuki; Nakajima, Kazuhisa

2002-01-01

We have developed laser-produced plasma X-ray sources using femtosecond laser pulses at 10Hz repetition rate in a table-top size in order to investigate basic mechanism of X-ray emission from laser-matter interactions and its application to a X-ray microscope. In a soft X-ray region over 5 nm wavelength, laser-plasma X-ray emission from a solid target achieved an intense flux of photons of the order of 1011 photons/rad per pulse with duration of a few 100 ps, which is intense enough to make a clear imaging in a short time exposure. As an application of laser-produced plasma X-ray source, we have developed a soft X-ray imaging microscope operating in the wavelength range around 14 nm. The microscope consists of a cylindrically ellipsoidal condenser mirror and a Schwarzshird objective mirror with highly-reflective multilayers. We report preliminary results of performance tests of the soft X-ray imaging microscope with a compact laser-produced plasma X-ray source

Small Pixel Hybrid CMOS X-ray Detectors

Science.gov (United States)

Hull, Samuel; Bray, Evan; Burrows, David N.; Chattopadhyay, Tanmoy; Falcone, Abraham; Kern, Matthew; McQuaide, Maria; Wages, Mitchell

2018-01-01

Concepts for future space-based X-ray observatories call for a large effective area and high angular resolution instrument to enable precision X-ray astronomy at high redshift and low luminosity. Hybrid CMOS detectors are well suited for such high throughput instruments, and the Penn State X-ray detector lab, in collaboration with Teledyne Imaging Sensors, has recently developed new small pixel hybrid CMOS X-ray detectors. These prototype 128x128 pixel devices have 12.5 micron pixel pitch, 200 micron fully depleted depth, and include crosstalk eliminating CTIA amplifiers and in-pixel correlated double sampling (CDS) capability. We report on characteristics of these new detectors, including the best read noise ever measured for an X-ray hybrid CMOS detector, 5.67 e- (RMS).

SMART-X: Square Meter, Arcsecond Resolution Telescope for X-rays

Science.gov (United States)

Vikhlinin, Alexey; SMART-X Collaboration

2013-04-01

SMART-X is a concept for a next-generation X-ray observatory with large-area, 0.5" angular resolution grazing incidence adjustable X-ray mirrors, high-throughput critical angle transmission gratings, and X-ray microcalorimeter and CMOS-based imager in the focal plane. High angular resolution is enabled by new technology based on controlling the shape of mirror segments using thin film piezo actuators deposited on the back surface. Science applications include observations of growth of supermassive black holes since redshifts of ~10, ultra-deep surveys over 10's of square degrees, galaxy assembly at z=2-3, as well as new opportunities in the high-resolution X-ray spectroscopy and time domains. We also review the progress in technology development, tests, and mission design over the past year.

Workshop on cooling of x-ray monochromators on high power beamlines

International Nuclear Information System (INIS)

Matsushita, T.; Ishikawa, T.

1989-03-01

This report is a Workshop on Cooling of X-ray Monochromators on High Power Beamlines held on August 31, 1988 at the Photon Factory during the Third International Conference on Synchrotron Radiation Instrumentation (SRI88). On high power beamlines, especially on insertion device beamlines, heating of crystal monochromators is becoming a serious problem: Researchers observe that the intensity of the X-ray beam on the sample is not proportional to the source intensity because of thermal distortion of the monochromator crystal. This problem will be even more serious on beamlines for the next generation X-ray rings. In the very tight program of the SRI88 conference, only 2 speakers were able to give invited talks closely related to this problem in the session of OPTICAL COMPONENTS FOR HIGH POWER BEAMLINES on Wednesday morning of August 31, 1988. We held this workshop in the afternoon of the same day with the intention of offering further opportunities to exchange information on efforts underway at various laboratories and to discuss ideas how to solve this problem. We also intended that the workshop would be a 'follow-up' to the X-ray optics workshop held at ESRF, Grenoble in September 1987, where the importance of crystal cooling was strongly pointed out. There were 32 participants from 7 countries. 12 people represented their experiences and ideas for reducing thermal distortion of crystal monochromators. Following those presentations, there were discussions on collaborations for solving this important problem. The attendees agreed that exchange of information should be continued by holding such meetings at reasonable intervals. (J.P.N.)

X-ray sky

International Nuclear Information System (INIS)

Gruen, M.; Koubsky, P.

1977-01-01

The history is described of the discoveries of X-ray sources in the sky. The individual X-ray detectors are described in more detail, i.e., gas counters, scintillation detectors, semiconductor detectors, and the principles of X-ray spectrometry and of radiation collimation aimed at increased resolution are discussed. Currently, over 200 celestial X-ray sources are known. Some were identified as nebulae, in some pulsations were found or the source was identified as a binary star. X-ray bursts of novae were also observed. The X-ray radiation is briefly mentioned of spherical star clusters and of extragalactic X-ray sources. (Oy)

Small-Size High-Current Generators for X-Ray Backlighting

Science.gov (United States)

Chaikovsky, S. A.; Artyomov, A. P.; Zharova, N. V.; Zhigalin, A. S.; Lavrinovich, I. V.; Oreshkin, V. I.; Ratakhin, N. A.; Rousskikh, A. G.; Fedunin, A. V.; Fedushchak, V. F.; Erfort, A. A.

2017-12-01

The paper deals with the soft X-ray backlighting based on the X-pinch as a powerful tool for physical studies of fast processes. Proposed are the unique small-size pulsed power generators operating as a low-inductance capacitor bank. These pulse generators provide the X-pinch-based soft X-ray source (hν = 1-10 keV) of micron size at 2-3 ns pulse duration. The small size and weight of pulse generators allow them to be transported to any laboratory for conducting X-ray backlighting of test objects with micron space resolution and nanosecond exposure time. These generators also allow creating synchronized multi-frame radiographic complexes with frame delay variation in a broad range.

High pressure X-ray preionized TEMA-CO2 laser

Science.gov (United States)

Bonnie, R. J. M.; Witteman, W. J.

1987-09-01

The construction of a high-pressure (up to 20 atm) transversely excited CO2 laser using transverse X-ray preionization is described. High pressure operation was found to be greatly improved in comparison to UV-preionized systems. Homogeneous discharges have been achieved in the pressure range 5-20 atm, yielding a specific laser output in the order of 35 J/l.

Very high resolution UV and X-ray spectroscopy and imagery of solar active regions

Science.gov (United States)

Bruner, M.; Brown, W. A.; Haisch, B. M.

1987-01-01

A scientific investigation of the physics of the solar atmosphere, which uses the techniques of high resolution soft X-ray spectroscopy and high resolution UV imagery, is described. The experiments were conducted during a series of three sounding rocket flights. All three flights yielded excellent images in the UV range, showing unprecedented spatial resolution. The second flight recorded the X-ray spectrum of a solar flare, and the third that of an active region. A normal incidence multi-layer mirror was used during the third flight to make the first astronomical X-ray observations using this new technique.

Ultra high resolution X-ray detectors

International Nuclear Information System (INIS)

Hess, U.; Buehler, M.; Hentig, R. von; Hertrich, T.; Phelan, K.; Wernicke, D.; Hoehne, J.

2001-01-01

CSP Cryogenic Spectrometers GmbH is developing cryogenic energy dispersive X-ray spectrometers based on superconducting detector technology. Superconducting sensors exhibit at least a 10-fold improvement in energy resolution due to their low energy gap compared to conventional Si(Li) or Ge detectors. These capabilities are extremely valuable for the analysis of light elements and in general for the analysis of the low energy range of the X-ray spectrum. The spectrometer is based on a mechanical cooler needing no liquid coolants and an adiabatic demagnetization refrigerator (ADR) stage which supplies the operating temperature of below 100 mK for the superconducting sensor. Applications include surface analysis in semiconductor industry as well material analysis for material composition e.g. in ceramics or automobile industry

Einstein pictures the x-ray sky

International Nuclear Information System (INIS)

Hartline, B.K.

1979-01-01

The second High Energy Astronomy Observatory (HEAO-2, Einstein) is revolutionizing x-ray astronomy just as its namesake revolutionized physics. Earlier x-ray observatories, including HEAO-1, were designed to scan the sky for x-ray emitters. With Einstein, the challenge has shifted from discovering x-ray sources to understanding the processes producing the x-rays. But having 500 times the sensitivity of previous detectors, Einstein makes more than its share of discoveries, too. For example, it sees distant quasars and clusters of galaxies that can barely be detected by the largest optical telescopes

Novel opportunities for sub-meV inelastic X-ray scattering at high-repetition rate self-seeded X-ray free-electron lasers

Energy Technology Data Exchange (ETDEWEB)

Chubar, Oleg [Brookhaven National Laboratory, Upton, NY (United States). National Synchrotron Light Source II; Geloni, Gianluca; Madsen, Anders [European XFEL GmbH, Hamburg (Germany); Kocharyan, Vitali; Saldin, Evgeni; Serkez, Svitozar [Deutsches Elektronen-Synchrotron (DESY), Hamburg (Germany); Shvyd' ko, Yuri [Argonne National Laboratory, IL (United States). Advanced Photon Source; Sutter, John [Diamond Light Source Ltd., Didcot (United Kingdom)

2015-08-15

Inelastic X-ray scattering (IXS) is an important tool for studies of equilibrium dynamics in condensed matter. A new spectrometer recently proposed for ultra-high-resolution IXS (UHRIX) has achieved 0.6 meV and 0.25 nm{sup -1} spectral and momentum transfer resolutions, respectively. However, further improvements down to 0.1 meV and 0.02 nm{sup -1} are required to close the gap in energy-momentum space between high and low frequency probes. We show that this goal can be achieved by further optimizing the X-ray optics and by increasing the spectral flux of the incident X-ray pulses. UHRIX performs best at energies from 5 to 10 keV, where a combination of self-seeding and undulator tapering at the SASE-2 beamline of the European XFEL promises up to a hundred-fold increase in average spectral flux compared with nominal SASE pulses at saturation, or three orders of magnitude more than possible with storage-ring based radiation sources. Wave-optics propagation shows that about 7 x 10{sup 12} ph/s in a 90-μeV bandwidth can be achieved on the sample. This will provide unique new possibilities for dynamics studies by IXS.

A hybrid concept (segmented plus monolithic fused silica shells) for a high-throughput and high-angular resolution x-ray mission (Lynx/X-Ray Surveyor like)

Science.gov (United States)

Basso, Stefano; Civitani, Marta; Pareschi, Giovanni; Parodi, Giancarlo

2017-09-01

Lynx is a large area and high angular resolution X-ray mission being studied by NASA to be presented to the next Decadal Survey for the implementation in the next decade. It aims to realize an X-ray telescope with the effective area similar to Athena (2 m2 at 1 keV) but with the same angular resolution of Chandra and a much larger Field Of View (up 20 arcmin x 20 arcmin). The science of X-ray Surveyor requires a large-throughput mirror assembly with sub-arcsec angular resolution. These future X-ray mirrors have a set of requirements which, collectively, represents very substantial advances over any currently in operation or planned for missions other than X-ray Surveyor. Of particular importance is achieving low mass per unit collecting area, while maintaining Chandra like angular resolution. Among the possible solutions under study, the direct polishing of both thin monolithic pseudo-cylindrical shells and segments made of fused silica are being considered as viable solutions for the implementation of the mirrors. Fused silica has very good thermomechanical parameters (including a very low CTE), making the material particularly well suited for for the production of the Lynx mirrors. It should be noted that the use of close shells is also very attractive, since the operations for the integration of the shells will be greatly simplified and the area lost due to the vignetting from the interfacing structures minimized even if the management of such big (diameter of 3 m) and thin shells have to be demonstrated. In this paper we will discuss a possible basic layout for a full shell mirror and a hybrid concept (segmented plus monolithic shells made of fused silica) as a second solution, for the Lynx/XRS telescope, discussing preliminary results in terms of optical and mechanical performance.

Hohlraums energy balance and x-ray drive

International Nuclear Information System (INIS)

Kilkenny, J.D.

1994-01-01

For many years there has been an active ICF program in the US concentrating on x-ray drive. X-ray drive is produced by focusing laser beams into a high Z hohlraum. Conceptually, the radiation field comes close to thermodynamic equilibrium, that is it becomes isotropic and Planckian. These properties lead to the benefits of x-ray drive--it is relatively easy to obtain drive symmetry on a capsule with no small scalelengths drive perturbations. Other advantages of x-ray drive is the higher mass ablation rate, leading to lower growth rates for hydrodynamic instabilities. X-ray drive has disadvantages, principally the loss of energy to the walls of the hohlraum. This report is divided into the following sections: (1) review of blackbody radiation; (2) laser absorption and conversion to x-rays; (3) x-ray absorption coefficient in matter and Rosseland mean free path; (4) Marshak waves in high Z material; (5) x-ray albedo; and (6) power balance and hohlraum temperature

Prospects for compact high-intensity laser synchrotron x-ray and gamma sources

International Nuclear Information System (INIS)

Pogorelsky, I.V.

1996-11-01

A laser interacting with a relativistic electron beam behaves like a virtual wiggler of an extremely short period equal to half of the laser wavelength. This approach opens a route to relatively compact, high-brightness x-ray sources alternative or complementary to conventional synchrotron light sources. Although not new, the laser synchrotron source (LSS) concept is still waiting for a convincing demonstration. Available at the BNL Accelerator Test Facility (ATF), a high-brightness electron beam and the high-power CO 2 laser may be used as prototype LSS brick stones. In a feasible demonstration experiment, 10-GW, 100-ps CO 2 laser beam will be brought to a head-on collision with a 10-ps, 0.5-nC, 50 MeV electron bunch. Flashes of collimated 4.7 keV (2.6 angstrom) x-rays of 10-ps pulse duration, with a flux of ∼ 10 19 photons/sec, will be produced via linear Compton backscattering. The x-ray spectrum is tunable proportionally to the e-beam energy. A rational short-term extension of the proposed experiment would be further enhancement of the x-ray flux to the 10 22 photons/sec level, after the ongoing ATF CO 2 laser upgrade to 5 TW peak power and electron bunch shortening to 3 ps is realized. In the future, exploiting the promising approach of a high-gradient laser wake field accelerator, a compact ''table-top'' LSS of monochromatic gamma radiation may become feasible

Prospects for compact high-intensity laser synchrotron x-ray and gamma sources

International Nuclear Information System (INIS)

Pogorelsky, I.V.

1997-01-01

A laser interacting with a relativistic electron beam behaves like a virtual wiggler of an extremely short period equal to half of the laser wavelength. This approach opens a route to relatively compact, high- brightness x-ray sources alternative or complementary to conventional synchrotron light sources. Although not new, the laser synchrotron source (LSS) concept is still waiting for a convincing demonstration. Available at the BNL Accelerator Test Facility (ATF), a high- brightness electron beam and the high-power C0 2 laser may be used as prototype LSS brick stones. In a feasible demonstration experiment, 10 GW, 100 ps C0 2 laser beam will be brought to a head-on collision with a 10 ps, 0.5 nC, 50 MeV electron bunch. Flashes of collimated 4.7 keV (2.6 A) x-rays of 10-ps pulse duration, with a flux of ∼10 19 photons/sec, will be produced via linear Compton backscattering. The x-ray spectra is tunable proportionally to the e- beam energy. A rational short-term extension of the proposed experiment would be further enhancement of the x-ray flux to the 10 22 photon/sec level, after the ongoing ATF C0 2 laser upgrade to 5 TW peak power and electron bunch shortening to 3 ps is realized. In the future, exploiting the promising approach of a high-gradient laser wake field accelerator, a compact ''table- top'' LSS of monochromatic gamma radiation may become feasible

Handbook Of X-ray Astronomy

Science.gov (United States)

Arnaud, Keith A.; Smith, R. K.; Siemiginowska, A.; Edgar, R. J.; Grant, C. E.; Kuntz, K. D.; Schwartz, D. A.

2011-09-01

This poster advertises a book to be published in September 2011 by Cambridge University Press. Written for graduate students, professional astronomers and researchers who want to start working in this field, this book is a practical guide to x-ray astronomy. The handbook begins with x-ray optics, basic detector physics and CCDs, before focussing on data analysis. It introduces the reduction and calibration of x-ray data, scientific analysis, archives, statistical issues and the particular problems of highly extended sources. The book describes the main hardware used in x-ray astronomy, emphasizing the implications for data analysis. The concepts behind common x-ray astronomy data analysis software are explained. The appendices present reference material often required during data analysis.

High-energy synchrotron radiation x-ray microscopy: Present status and future prospects

International Nuclear Information System (INIS)

Jones, K.W.; Gordon, B.M.; Spanne, P.; Rivers, M.L.; Sutton, S.R.

1991-01-01

High-energy radiation synchrotron x-ray microscopy is used to characterize materials of importance to the chemical and materials sciences and chemical engineering. The x-ray microscope (XRM) forms images of elemental distributions fluorescent x rays or images of mass distributions by measurement of the linear attenuation coefficient of the material. Distributions of sections through materials are obtained non-destructively using the technique of computed microtomography. The energy range of the x rays used for the XRM ranges from a few keV at the minimum value to more than 100 keV, which is sufficient to excite the K-edge of all naturally occurring elements. The work in progress at the Brookhaven NSLS X26 and X17 XRM is described in order to show the current status of the XRM. While there are many possible approaches to the XRM instrumentation, this instrument gives state-of-the-art performance in most respects and serves as a reasonable example of the present status of the instrumentation in terms of the spatial resolution and minimum detection limits obtainable. The examples of applications cited give an idea of the types of research fields that are currently under investigation. They can be used to illustrate how the field of x-ray microscopy will benefit from the use of bending magnets and insertion devices at the Advanced Photon Source. 8 refs., 5 figs

High-energy synchrotron radiation x-ray microscopy: Present status and future prospects

International Nuclear Information System (INIS)

Jones, K.W.; Gordon, B.M.; Spanne, P.; Rivers, M.L.; Sutton, S.R.

1991-01-01

High-energy radiation synchrotron x-ray microscopy is used to characterize materials of importance to the chemical and materials sciences and chemical engineering. The x-ray microscope (XRM) forms images of elemental distributions fluorescent x rays or images of mass distributions by measurement of the linear attenuation coefficient of the material. Distributions of sections through materials are obtained non-destructively using the technique of computed microtomography (CMT). The energy range of the x rays used for the XRM ranges from a few keV at the minimum value to more than 100 keV, which is sufficient to excite the K-edge of all naturally occurring elements. The work in progress at the Brookhaven NSLS X26 and X17 XRM is described in order to show the current status of the XRM. While there are many possible approaches to the XRM instrumentation, this instrument gives state-of-the-art performance in most respects and serves as a reasonable example of the present status of the instrumentation in terms of the spatial resolution and minimum detection limits (MDLs) obtainable. The examples of applications cited give an idea of the types of research fields that are currently under investigation. They can be used to illustrate how the field of x-ray microscopy will benefit from the use of bending magnets and insertion devices at the Advanced Photon Source (APS)

High energy X-ray observation of Cyg X-3

International Nuclear Information System (INIS)

Kendziorra, E.; Pietsch, W.; Staubert, R.; Truemper, J.

1975-01-01

On Feb. 20, 1975 Cyg X-3 was observed in the energy range of 29-70 keV during a 5 hour observation of the Cyg region. An intensity variation consistent with a 4.8 h sinusoidal modulation has been found, in phase with low energy X-ray observations and with a relative amplitude of 0.37 +- 0.19. (orig.) [de

Generation of plasma X-ray sources via high repetition rate femtosecond laser pulses

Science.gov (United States)

Baguckis, Artūras; Plukis, Artūras; Reklaitis, Jonas; Remeikis, Vidmantas; Giniūnas, Linas; Vengris, Mikas

2017-12-01

In this study, we present the development and characterization of Cu plasma X-ray source driven by 20 W average power high repetition rate femtosecond laser in ambient atmosphere environment. The peak Cu- Kα photon flux of 2.3 × 109 photons/s into full solid angle is demonstrated (with a process conversion efficiency of 10-7), using pulses with peak intensity of 4.65 × 1014 W/cm2. Such Cu- Kα flux is significantly larger than others found in comparable experiments, performed in air environment. The effects of resonance plasma absorption process, when optimized, are shown to increase measured flux by the factor of 2-3. The relationship between X-ray photon flux and plasma-driving pulse repetition rate is quasi-linear, suggesting that fluxes could further be increased to 1010 photons/s using even higher average powers of driving radiation. These results suggest that to fully utilize the potential of high repetition rate laser sources, novel target material delivery systems (for example, jet-based ones) are required. On the other hand, this study demonstrates that high energy lasers currently used for plasma X-ray sources can be conveniently and efficiently replaced by high average power and repetition rate laser radiation, as a way to increase the brightness of the generated X-rays.

High-resolution x-ray computed tomography to understand ruminant phylogeny

Science.gov (United States)

Costeur, Loic; Schulz, Georg; Müller, Bert

2014-09-01

High-resolution X-ray computed tomography has become a vital technique to study fossils down to the true micrometer level. Paleontological research requires the non-destructive analysis of internal structures of fossil specimens. We show how X-ray computed tomography enables us to visualize the inner ear of extinct and extant ruminants without skull destruction. The inner ear, a sensory organ for hearing and balance has a rather complex three-dimensional morphology and thus provides relevant phylogenetical information what has been to date essentially shown in primates. We made visible the inner ears of a set of living and fossil ruminants using the phoenix x-ray nanotom®m (GE Sensing and Inspection Technologies GmbH). Because of the high absorbing objects a tungsten target was used and the experiments were performed with maximum accelerating voltage of 180 kV and a beam current of 30 μA. Possible stem ruminants of the living families are known in the fossil record but extreme morphological convergences in external structures such as teeth is a strong limitation to our understanding of the evolutionary history of this economically important group of animals. We thus investigate the inner ear to assess its phylogenetical potential for ruminants and our first results show strong family-level morphological differences.

X-ray astronomy

International Nuclear Information System (INIS)

Culhane, J.L.; Sanford, P.W.

1981-01-01

X-ray astronomy has been established as a powerful means of observing matter in its most extreme form. The energy liberated by sources discovered in our Galaxy has confirmed that collapsed stars of great density, and with intense gravitational fields, can be studied by making observations in the X-ray part of the electromagnetic spectrum. The astronomical objects which emit detectable X-rays include our own Sun and extend to quasars at the edge of the Universe. This book describes the history, techniques and results obtained in the first twenty-five years of exploration. Space rockets and satellites are essential for carrying the instruments above the Earth's atmosphere where it becomes possible to view the X-rays from stars and nebulae. The subject is covered in chapters, entitled: the birth of X-ray astronomy; the nature of X-radiation; X-rays from the Sun; solar-flare X-rays; X-rays from beyond the solar system; supernovae and their remnants; X-rays from binary stars; white dwarfs and neutron stars; black holes; X-rays from galaxies and quasars; clusters of galaxies; the observatories of the future. (author)

Irradiated ISM : Discriminating between cosmic rays and X-rays

NARCIS (Netherlands)

Meijerink, R.; Spaans, M.; Israel, F. P.

2006-01-01

The interstellar medium ( ISM) at the centers of active galaxies is exposed to a combination of cosmic-ray, far-ultraviolet (FUV), and X-ray radiation. We apply photodissociation region (PDR) models to this ISM with both "normal" and highly elevated (5 x 10(-15) s(-1)) cosmic- ray (CR) rates and

High resolution hard x-ray microscope on a second generation synchrotron source

International Nuclear Information System (INIS)

Tian Yangchao; Li Wenjie; Chen Jie; Liu Longhua; Liu Gang; Tian Jinping; Xiong Ying; Tkachuk, Andrei; Gelb, Jeff; Hsu, George; Yun Wenbing

2008-01-01

A full-field, transmission x-ray microscope (TXM) operating in the energy range of 7-11 keV has been installed at the U7A beamline at the National Synchrotron Radiation Laboratory, a second generation synchrotron source operating at 0.8 GeV. Although the photon flux at sample position in the operating energy range is significantly low due to its relatively large emittance, the TXM can get high quality x-ray images with a spatial resolution down to 50 nm with acceptable exposure time. This TXM operates in either absorption or Zernike phase contrast mode with similar resolution. This TXM is a powerful analytical tool for a wide range of scientific areas, especially studies on nanoscale phenomena and structural imaging in biology, materials science, and environmental science. We present here the property of the x-ray source, beamline design, and the operation and key optical components of the x-ray TXM. Plans to improve the throughput of the TXM will be discussed.

Semiconductor-based narrow-line and high-brilliance 193-nm laser system for industrial applications

Science.gov (United States)

Opalevs, D.; Scholz, M.; Stuhler, J.; Gilfert, C.; Liu, L. J.; Wang, X. Y.; Vetter, A.; Kirner, R.; Scharf, T.; Noell, W.; Rockstuhl, C.; Li, R. K.; Chen, C. T.; Voelkel, R.; Leisching, P.

2018-02-01

We present a novel industrial-grade prototype version of a continuous-wave 193 nm laser system entirely based on solid state pump laser technology. Deep-ultraviolet emission is realized by frequency-quadrupling an amplified diode laser and up to 20 mW of optical power were generated using the nonlinear crystal KBBF. We demonstrate the lifetime of the laser system for different output power levels and environmental conditions. The high stability of our setup was proven in > 500 h measurements on a single spot, a crystal shifter multiplies the lifetime to match industrial requirements. This laser improves the relative intensity noise, brilliance, wall-plug efficiency and maintenance cost significantly. We discuss first lithographic experiments making use of this improvement in photon efficiency.

Ultra high resolution soft x-ray tomography

International Nuclear Information System (INIS)

Haddad, W.S.; Trebes, J.E.; Goodman, D.M.

1995-01-01

Ultra high resolution three dimensional images of a microscopic test object were made with soft x-rays using a scanning transmission x-ray microscope. The test object consisted of two different patterns of gold bars on silicon nitride windows that were separated by ∼5μm. A series of nine 2-D images of the object were recorded at angles between -50 to +55 degrees with respect to the beam axis. The projections were then combined tomographically to form a 3-D image by means of an algebraic reconstruction technique (ART) algorithm. A transverse resolution of ∼1000 Angstrom was observed. Artifacts in the reconstruction limited the overall depth resolution to ∼6000 Angstrom, however some features were clearly reconstructed with a depth resolution of ∼1000 Angstrom. A specially modified ART algorithm and a constrained conjugate gradient (CCG) code were also developed as improvements over the standard ART algorithm. Both of these methods made significant improvements in the overall depth resolution bringing it down to ∼1200 Angstrom overall. Preliminary projection data sets were also recorded with both dry and re-hydrated human sperm cells over a similar angular range

Ultra high resolution soft x-ray tomography

International Nuclear Information System (INIS)

Haddad, W.S.; Trebes, J.E.; Goodman, D.M.; Lee, H.R.; McNulty, I.; Zalensky, A.O.

1995-01-01

Ultra high resolution three dimensional images of a microscopic test object were made with soft x-rays using a scanning transmission x-ray microscope. The test object consisted of two different patterns of gold bars on silicon nitride windows that were separated by ∼5 microm. A series of nine 2-D images of the object were recorded at angles between -50 to +55 degrees with respect to the beam axis. The projections were then combined tomographically to form a 3-D image by means of an algebraic reconstruction technique (ART) algorithm. A transverse resolution of ∼ 1,000 angstrom was observed. Artifacts in the reconstruction limited the overall depth resolution to ∼ 6,000 angstrom, however some features were clearly reconstructed with a depth resolution of ∼ 1,000 angstrom. A specially modified ART algorithm and a constrained conjugate gradient (CCG) code were also developed as improvements over the standard ART algorithm. Both of these methods made significant improvements in the overall depth resolution, bringing it down to ∼ 1,200 angstrom overall. Preliminary projection data sets were also recorded with both dry and re-hydrated human sperm cells over a similar angular range

High average power, highly brilliant laser-produced plasma source for soft X-ray spectroscopy.

Science.gov (United States)

Mantouvalou, Ioanna; Witte, Katharina; Grötzsch, Daniel; Neitzel, Michael; Günther, Sabrina; Baumann, Jonas; Jung, Robert; Stiel, Holger; Kanngiesser, Birgit; Sandner, Wolfgang

2015-03-01

In this work, a novel laser-produced plasma source is presented which delivers pulsed broadband soft X-radiation in the range between 100 and 1200 eV. The source was designed in view of long operating hours, high stability, and cost effectiveness. It relies on a rotating and translating metal target and achieves high stability through an on-line monitoring device using a four quadrant extreme ultraviolet diode in a pinhole camera arrangement. The source can be operated with three different laser pulse durations and various target materials and is equipped with two beamlines for simultaneous experiments. Characterization measurements are presented with special emphasis on the source position and emission stability of the source. As a first application, a near edge X-ray absorption fine structure measurement on a thin polyimide foil shows the potential of the source for soft X-ray spectroscopy.

High Spectral Resolution, High Cadence, Imaging X-ray Microcalorimeters for Solar Physics - Phase 2 Project

Data.gov (United States)

National Aeronautics and Space Administration — Microcalorimeter x-ray instruments are non-dispersive, high spectral resolution, broad-band, high cadence imaging spectrometers. We have been developing these...

X-ray Optics Development at MSFC

Science.gov (United States)

Sharma, Dharma P.

2017-01-01

Development of high resolution focusing telescopes has led to a tremendous leap in sensitivity, revolutionizing observational X-ray astronomy. High sensitivity and high spatial resolution X-ray observations have been possible due to use of grazing incidence optics (paraboloid/hyperboloid) coupled with high spatial resolution and high efficiency detectors/imagers. The best X-ray telescope flown so far is mounted onboard Chandra observatory launched on July 23,1999. The telescope has a spatial resolution of 0.5 arc seconds with compatible imaging instruments in the energy range of 0.1 to 10 keV. The Chandra observatory has been responsible for a large number of discoveries and has provided X-ray insights on a large number of celestial objects including stars, supernova remnants, pulsars, magnetars, black holes, active galactic nuclei, galaxies, clusters and our own solar system.

Skull x-ray

Science.gov (United States)

X-ray - head; X-ray - skull; Skull radiography; Head x-ray ... There is low radiation exposure. X-rays are monitored and regulated to provide the minimum amount of radiation exposure needed to produce the image. Most ...

Neck x-ray

Science.gov (United States)

X-ray - neck; Cervical spine x-ray; Lateral neck x-ray ... There is low radiation exposure. X-rays are monitored so that the lowest amount of radiation is used to produce the image. Pregnant women and ...

Design and Tests of the Hard X-ray Polarimeter X-Calibur

Directory of Open Access Journals (Sweden)

M. Beilicke

2014-12-01

Full Text Available X-ray polarimetry promises to give qualitatively new information bout high-energy astrophysical sources, such as binary black hole  systems, micro-quasars, active galactic nuclei, and gamma-ray bursts. We designed, built and tested ahard X-ray polarimeter, X-Calibur, to be used in the focal plane of the InFOCuS grazing incidence hard X-ray telescope.X-Calibur combines a low-Z Compton scatterer with a CZT detector assembly to measure the polarization of 20−60 keV X-rays making use of the fact that polarized photons Compton scatter preferentially perpendicular to the electric field orientation; in principal, a similar space-borne experiment could be operated in the 5−100 keV regime. X-Calibur achieves a high detection efficiency of order unity.

Distortion of absorption-line velocity curves due to x-ray heating in x-ray binaries

International Nuclear Information System (INIS)

Milgrom, M.

1976-01-01

The effects of X-ray heating on the measured absorption line velocities, in X-ray binaries with low X-rays to optical luminosities ratio are considered. These effects may be appreciable even for such binaries where the effect of X-ray heating on the light-curve is negligible. The effects are studied qualitatively and suggest possible ways to partially eliminate the systematic errors introduced by them. The individual systems Cyg x-1 and SMC x-1 are treated and the results of numerical calculations are presented for them. For Cyg x-1 it is found that the effect is detectable during the X-ray 'high' state in all regions of the spectrum. During the 'low' state it may be important in the red region of the spectrum. The results for the case in which soft X-ray fluxes (E < or approximately .4 keV, suggested by theoretical models) are present are also given. For SMC x-1 a strong effect for Hα, Hβ, Hγ had been found. This effect may be responsible for the observed variable velocity curve. We also find for SMC x-1 that the average X-ray intensity falling on the primary must be considerably smaller than what is derived from the detected flux, or else the effect is too large. (author)

Masks for high aspect ratio x-ray lithography

International Nuclear Information System (INIS)

Malek, C.K.; Jackson, K.H.; Bonivert, W.D.; Hruby, J.

1997-01-01

Fabrication of very high aspect ratio microstructures, as well as ultra-high precision manufacturing is of increasing interest in a multitude of applications. Fields as diverse as micromechanics, robotics, integrated optics, and sensors benefit from this technology. The scale-length of this spatial regime is between what can be achieved using classical machine tool operations and that which is used in microelectronics. This requires new manufacturing techniques, such as the LIGA process, which combines x-ray lithography, electroforming, and plastic molding

Fabrication of high-aspect-ratio nano structures using a nano x-ray shadow mask

International Nuclear Information System (INIS)

Kim, Yong Chul; Lee, Seung S

2008-01-01

This paper describes a novel method for the fabrication of high-aspect-ratio nano structures (HAR-nano structures) using a nano x-ray shadow mask and deep x-ray lithography (DXRL). The nano x-ray shadow mask is fabricated by depositing an x-ray absorber layer (Au, 3 µm) onto the back side of a nano shadow mask. The nano shadow mask is produced with nano-sized apertures whose dimensions are reduced to several tens of nanometers by the accumulation of low-stress silicon nitride (Si x N y ) using the LPCVD process on the shadow mask. A shadow mask containing apertures with a size of 1 µm is fabricated on a bulk micromachined Si x N y membrane. The thickness of an absorber layer must be in the range of several tens of micrometers in order to obtain a contrast of more than 100 for the conventional DXRL process at the Pohang Light Source (PLS). However, a 3 µm thick absorber layer can provide a sufficient contrast if the modified DXRL of the central beam-stop method is used, which blocks high-energy x-rays. A nano shadow mask with 30 nm sized apertures is fabricated and a nano x-ray shadow mask with 250 nm sized apertures is fabricated by depositing a 3 µm thick absorber layer on a nano shadow mask with 500 nm sized apertures. HAR-nano structures (circles with a diameter of 420 nm and lines with a width of 274 nm) with aspect ratios of over 10:1 on a 3.2 µm SU-8 are successfully fabricated by using the nano x-ray shadow mask and the central beam-stop method

X-ray filter for chest X-rays

International Nuclear Information System (INIS)

Ferlic, D.J.

1984-01-01

A description is given of an X-ray filter comprised of a sheet of radiation absorbing material with an opening corresponding to the spine and central portion of the heart. The upper portion of the filter exhibits a relatively narrow opening which becomes gradually wider toward the lower portion of the filter. This filter will permit an acceptable density level of x-ray exposure for the lungs while allowing a higher level of x-ray exposure for the mediastinum areas of the body. (author)

Energy spectrum measurement of high power and high energy(6 and 9 MeV) pulsed x-ray source for industrial use

Energy Technology Data Exchange (ETDEWEB)

Takagi, Hiroyuki [Hitachi, Ltd. Power Systems Company, Ibaraki (Japan); Murata, Isao [Graduate School of Engineering, Osaka University, Osaka (Japan)

2016-06-15

Industrial X-ray CT system is normally applied to non-destructive testing (NDT) for industrial product made from metal. Furthermore there are some special CT systems, which have an ability to inspect nuclear fuel assemblies or rocket motors, using high power and high energy (more than 6 MeV) pulsed X-ray source. In these case, pulsed X-ray are produced by the electron linear accelerator, and a huge number of photons with a wide energy spectrum are produced within a very short period. Consequently, it is difficult to measure the X-ray energy spectrum for such accelerator-based X-ray sources using simple spectrometry. Due to this difficulty, unexpected images and artifacts which lead to incorrect density information and dimensions of specimens cannot be avoided in CT images. For getting highly precise CT images, it is important to know the precise energy spectrum of emitted X-rays. In order to realize it we investigated a new approach utilizing the Bayesian estimation method combined with an attenuation curve measurement using step shaped attenuation material. This method was validated by precise measurement of energy spectrum from a 1 MeV electron accelerator. In this study, to extend the applicable X-ray energy range we tried to measure energy spectra of X-ray sources from 6 and 9 MeV linear accelerators by using the recently developed method. In this study, an attenuation curves are measured by using a step-shaped attenuation materials of aluminum and steel individually, and the each X-ray spectrum is reconstructed from the measured attenuation curve by the spectrum type Bayesian estimation method. The obtained result shows good agreement with simulated spectra, and the presently developed technique is adaptable for high energy X-ray source more than 6 MeV.

Survey on the parameters influencing X-ray picture quality

International Nuclear Information System (INIS)

Stender, H.S.

1985-01-01

Survey on factors influencing X-ray picture quality: 1) identification of patient and imaged body part. 2) Object properties - thickness, density, built; spatial expansion and arrangement of anatomical parts; object parts in a homogenic and an inhomogenic environment; object movements. 3) Examination technique - matching to medical issue; positioning and adjustment; projection; picture format in keeping with the medical issue; object-related fade-in; distance ratios; contrast medium distribution or deposition; compression. 4) Technical factors of picture production - radiation quality tube voltage; reproducible mAs and mR/mAs; automatic exposure equipment; focal spot size; scattered radiation grid; image intensifier and indirect radiography system; exposure time, dose-to-exposure-time ratio; film-screen combination; cassette with uniform pressure contact; film processing system; radiation safety and light safety. 5) Physical imaging parameters - mean optical density; resolution capacity; contrast reproduction; noise; modulation transmission function. 6) Perceptible picture properties - luminance density; picture contrast; recognizability of details; impression of grain structure; blurred picture structure; visually conspicuous elements. 7) Requirements on picture viewing - viewing device with high luminance density and equalized illumination; possible modification of brilliance; possible fade-in operations and prevention of ambient glare; spot light with iris diaphragm; possible viewing by magnifying lens; selection of correct viewing distances; repeated picture viewing or evaluation by two or more viewers. (orig./HP) [de

High vacuum high temperature x-ray camera (1961)

International Nuclear Information System (INIS)

Baron, J.L.

1961-01-01

- This camera makes it possible to carry out X-ray studies on highly oxidisable materials, up to about 900 deg. C. Most of the existing models do not provide sufficient protection against the formation of surface oxide or carbide films on the sample. The present arrangement makes it possible to operate at very low pressures: 5 x 10 -8 to 10 -7 torr, thanks to an entirely metallic apparatus. The radiation heating system consists of an incandescent lamp, outside the evacuated portion, and a reflector which concentrates the energetic flux into the sample through a silica window. The heated parts have thus only a small thermal inertia. With the apparatus it has been possible to determine the phase parameters of uranium-α up to 650 deg. C with a precision of ± 0.0015 A. A similar study has been carried out on a uranium-chromium alloy in the β-phase up to 740 deg. C. (author) [fr

X-ray image subtracting system

International Nuclear Information System (INIS)

Wesbey, W.H.; Keyes, G.S.; Georges, J.-P.J.

1982-01-01

An X-ray image subtracting system for making low contrast structures in the images more conspicuous is described. An X-ray source projects successive high and low energy X-ray beam pulses through a body and the resultant X-ray images are converted to optical images. Two image pick-up devices such as TV cameras that have synchronously operated shutters receive the alternate images and convert them to corresponding analog video signals. In some embodiments, the analog signals are converted to a matrix of digital pixel signals that are variously processed and subtracted and converted to signals for driving a TV monitor display and analog storage devices. In other embodiments the signals are processed and subtracted in analog form for display. The high and low energy pulses can follow each other immediately so good registration between subtracted images is obtainable even though the anatomy is in motion. The energy levels of the X-ray pulses are chosen to maximize the difference in attenuation between the anatomical structure which is to be subtracted out and that which remains. (author)

Transforming Our Understanding of the X-ray Universe: The Imaging X-ray Polarimeter Explorer (IXPE)

Science.gov (United States)

Weisskopf, Martin C.; Bellazzini, Ronaldo; Costa, Enrico; Matt, Giorgio; Marshall, Herman; ODell, Stephen L.; Pavlov, George; Ramsey, Brian; Romani, Roger

2014-01-01

Accurate X-ray polarimetry can provide unique information on high-energy-astrophysical processes and sources. As there have been no meaningful X-ray polarization measurements of cosmic sources since our pioneering work in the 1970's, the time is ripe to explore this new parameter space in X-ray astronomy. To accomplish this requires a well-calibrated and well understood system that-particularly for an Explorer mission-has technical, cost, and schedule credibility. The system that we shall present satisfies these conditions, being based upon completely calibrated imaging- and polarization-sensitive detectors and proven X-ray-telescope technology.

A high resolution, high counting rate bidimensional, MWPC imaging detector for small angle X-ray diffraction studies

International Nuclear Information System (INIS)

Bateman, J.E.; Connolly, J.F.; Sawyer, E.C.; Stephenson, R.

1981-07-01

The performance is reported of a 200 mm x 200 mm X-ray imaging MWPC aimed at applications in small angle X-ray diffraction and scattering. With quantum energies of approximately 8 keV high spatial resolution (+- 0.5 mm x +- 0.14 mm) with a capability for data taking at >approximately 350 kHz is reported. The detection efficiency is approximately 75% and the detector operates as a sealed unit with a long lifetime. (author)

Development of the super high angular resolution principle for X-ray imaging

International Nuclear Information System (INIS)

Zhang Chen; Zhang Shuangnan

2011-01-01

Development of the Super High Angular Resolution Principle (SHARP) for coded-mask X-ray imaging is presented. We prove that SHARP can be considered as a generalized coded mask imaging method with a coding pattern comprised of diffraction-interference fringes in the mask pattern. The angular resolution of SHARP can be improved by detecting the fringes more precisely than the mask's element size, i.e. by using a detector with a pixel size smaller than the mask's element size. The proposed mission SHARP-X for solar X-ray observations is also briefly discussed. (research papers)

Exploratory X-ray monitoring of luminous radio-quiet quasars at high redshift: Initial results

Energy Technology Data Exchange (ETDEWEB)

Shemmer, Ohad; Stein, Matthew S. [Department of Physics, University of North Texas, Denton, TX 76203 (United States); Brandt, W. N.; Schneider, Donald P. [Department of Astronomy and Astrophysics, The Pennsylvania State University, University Park, PA 16802 (United States); Paolillo, Maurizio [Dipartimento di Scienze Fisiche, Università Federico II di Napoli, via Cinthia 6, I-80126 Napoli (Italy); Kaspi, Shai [School of Physics and Astronomy and the Wise Observatory, Tel Aviv University, Tel Aviv 69978 (Israel); Vignali, Cristian [Dipartimento di Astronomia, Università degli studi di Bologna, via Ranzani 1, I-40127 Bologna (Italy); Lira, Paulina [Departamento de Astronomia, Universidad de Chile, Camino del Observatorio 1515, Santiago (Chile); Gibson, Robert R., E-mail: ohad@unt.edu [Department of Astronomy, University of Washington, Box 351580, Seattle, WA 98195 (United States)

2014-03-10

We present initial results from an exploratory X-ray monitoring project of two groups of comparably luminous radio-quiet quasars (RQQs). The first consists of four sources at 4.10 ≤ z ≤ 4.35, monitored by Chandra, and the second is a comparison sample of three sources at 1.33 ≤ z ≤ 2.74, monitored by Swift. Together with archival X-ray data, the total rest-frame temporal baseline spans ∼2-4 yr and ∼5-13 yr for the first and second group, respectively. Six of these sources show significant X-ray variability over rest-frame timescales of ∼10{sup 2}-10{sup 3} days; three of these also show significant X-ray variability on rest-frame timescales of ∼1-10 days. The X-ray variability properties of our variable sources are similar to those exhibited by nearby and far less luminous active galactic nuclei (AGNs). While we do not directly detect a trend of increasing X-ray variability with redshift, we do confirm previous reports of luminous AGNs exhibiting X-ray variability above that expected from their luminosities, based on simplistic extrapolation from lower luminosity sources. This result may be attributed to luminous sources at the highest redshifts having relatively high accretion rates. Complementary UV-optical monitoring of our sources shows that variations in their optical-X-ray spectral energy distribution are dominated by the X-ray variations. We confirm previous reports of X-ray spectral variations in one of our sources, HS 1700+6416, but do not detect such variations in any of our other sources in spite of X-ray flux variations of up to a factor of ∼4. This project is designed to provide a basic assessment of the X-ray variability properties of RQQs at the highest accessible redshifts that will serve as a benchmark for more systematic monitoring of such sources with future X-ray missions.

Examining the X-ray Properties of Lenticular Galaxies: Rollins S0 X-ray Sample (RS0X)

Science.gov (United States)

Fuse, Christopher R.; Malespina, Alysa