Subgroup report on hard x-ray microprobes

International Nuclear Information System (INIS)

Ice, G.E.; Barbee, T.; Bionta, R.; Howells, M.; Thompson, A.C.; Yun, W.

1994-01-01

The increasing availability of synchrotron x-ray sources has stimulated the development of advanced hard x-ray (E≥5 keV) microprobes. New x-ray optics have been demonstrated which show promise for achieving intense submicron hard x-ray probes. These probes will be used for extraordinary elemental detection by x-ray fluorescence/absorption and for microdiffraction to identify phase and strain. The inherent elemental and crystallographic sensitivity of an x-ray microprobe and its inherently nondestructive and penetrating nature makes the development of an advanced hard x-ray microprobe an important national goal. In this workshop state-of-the-art hard x-ray microprobe optics were described and future directions were discussed. Gene Ice, Oak Ridge National Laboratory (ORNL), presented an overview of the current status of hard x-ray microprobe optics and described the use of crystal spectrometers to improve minimum detectable limits in fluorescent microprobe experiments. Al Thompson, Lawrence Berkeley Laboratory (LBL), described work at the Center for X-ray Optics to develop a hard x-ray microprobe based on Kirkpatrick-Baez (KB) optics. Al Thompson also showed the results of some experimental measurements with their KB optics. Malcolm Howells presented a method for bending elliptical mirrors and Troy Barbee commented on the use of graded d spacings to achieve highest efficiency in KB multilayer microfocusing. Richard Bionta, Lawrence Livermore National Laboratory (LLNL), described the development of the first hard x-ray zone plates and future promise of so called open-quotes jelly rollclose quotes or sputter slice zone plates. Wenbing Yun, Argonne National Laboratory (ANL), described characterization of jelly roll and lithographically produced zone plates and described the application of zone plates to focus extremely narrow bandwidths by nuclear resonance. This report summarizes the presentations of the workshop subgroup on hard x-ray microprobes

Generation of relativistic electron bunches in plasma synchrotron Gyrac-x for hard x-ray production

International Nuclear Information System (INIS)

Andreev, V.V.; Umnov, A.M.

2000-01-01

Experiment performed on plasma synchrotron Gyrac-X operating on synchrotron gyromagnetic autoresonance (SGA) is described. Gyrac-X is a compact plasma x-ray source in which kinetic energy of relativistic electrons obtained under SGA converts into x-ray by falling e-bunches on to a heavy metal target. The plasma synchrotron acts in a regime of a magnetic field pulse packet under constant level of microwave power. Experiments and numerical modeling of the process showed that such a regime allowed obtaining dense short lived relativistic electron bunches with average electron energy of 500 keV - 4.5 MeV. Parameters of the relativistic electron bunch (energy, density and volume) and dynamics of the electron bunches can be controlled by varying the parameters of the SGA process. Possibilities of x-ray intensity increase are also discussed

Hard X-ray Microscopic Imaging Of Human Breast Tissues

Science.gov (United States)

Park, Sung H.; Kim, Hong T.; Kim, Jong K.; Jheon, Sang H.; Youn, Hwa S.

2007-01-01

X-ray microscopy with synchrotron radiation will be a useful tool for innovation of x-ray imaging in clinical and laboratory settings. It helps us observe detailed internal structure of material samples non-invasively in air. And, it also has the potential to solve some tough problems of conventional breast imaging if it could evaluate various conditions of breast tissue effectively. A new hard x-ray microscope with a spatial resolution better than 100 nm was installed at Pohang Light Source, a third generation synchrotron radiation facility in Pohang, Korea. The x-ray energy was set at 6.95 keV, and the x-ray beam was monochromatized by W/B4C monochromator. Condenser and objective zone plates were used as x-ray lenses. Zernike phase plate next to condenser zone plate was introduced for improved contrast imaging. The image of a sample was magnified 30 times by objective zone plate and 20 times by microscope objective, respectively. After additional 10 times digital magnification, the total magnifying power was up to 6000 times in the end. Phase contrast synchrotron images of 10-μm-thick female breast tissue of the normal, fibroadenoma, fibrocystic change and carcinoma cases were obtained. By phase contrast imaging, hard x-rays enable us to observe many structures of breast tissue without sample preparations such as staining or fixation.

Hard X-ray Microscopic Imaging Of Human Breast Tissues

International Nuclear Information System (INIS)

Park, Sung H.; Kim, Hong T.; Kim, Jong K.; Jheon, Sang H.; Youn, Hwa S.

2007-01-01

X-ray microscopy with synchrotron radiation will be a useful tool for innovation of x-ray imaging in clinical and laboratory settings. It helps us observe detailed internal structure of material samples non-invasively in air. And, it also has the potential to solve some tough problems of conventional breast imaging if it could evaluate various conditions of breast tissue effectively. A new hard x-ray microscope with a spatial resolution better than 100 nm was installed at Pohang Light Source, a third generation synchrotron radiation facility in Pohang, Korea. The x-ray energy was set at 6.95 keV, and the x-ray beam was monochromatized by W/B4C monochromator. Condenser and objective zone plates were used as x-ray lenses. Zernike phase plate next to condenser zone plate was introduced for improved contrast imaging. The image of a sample was magnified 30 times by objective zone plate and 20 times by microscope objective, respectively. After additional 10 times digital magnification, the total magnifying power was up to 6000 times in the end. Phase contrast synchrotron images of 10-μm-thick female breast tissue of the normal, fibroadenoma, fibrocystic change and carcinoma cases were obtained. By phase contrast imaging, hard x-rays enable us to observe many structures of breast tissue without sample preparations such as staining or fixation

Hard X-ray Emission and Efficient Particle Acceleration by Supernova Remnants

International Nuclear Information System (INIS)

Vink, Jacco

2009-01-01

I discuss the non-thermal X-ray emission from young supernova remnants. Over the last decade it has become clear from both X-ray and γ-ray observations that young supernovae accelerate particles up to 100 TeV. In soft X-rays the accelerated >10 TeV electrons produce synchrotron radiation, coming from narrow filaments located at the shock fronts. The width of these filaments shows that the magnetic fields are relatively high, thus providing evidence for magnetic field amplification.The synchrotron radiation of several remnants is known to extend into the hard X-ray regime. In particular Cas A, has a spectrum that appears as a power law up to almost 100 TeV. This is very surprising, as a steepening is expected going from the soft to the hard X-ray band. The spectrum is likely a result of many superimposed individual spectra, each steepening at different energies. This implies considerable spatial variation in hard X-rays, an obvious target for Simbol-X. The variations will be important to infer local shock acceleration properties, but also magnetic field fluctuations may cause spatial and temporal variations.Finally, I draw the attention to super bubbles and supernovae as sources of cosmic rays. As such they may be sources of hard X-ray emission. In particular, supernovae exploding inside the dense red supergiants winds of their progenitors ares promising candidates for hard X-ray emission.

Hard X-ray Emission and Efficient Particle Acceleration by Supernova Remnants

Science.gov (United States)

Vink, Jacco

2009-05-01

I discuss the non-thermal X-ray emission from young supernova remnants. Over the last decade it has become clear from both X-ray and γ-ray observations that young supernovae accelerate particles up to 100 TeV. In soft X-rays the accelerated >10 TeV electrons produce synchrotron radiation, coming from narrow filaments located at the shock fronts. The width of these filaments shows that the magnetic fields are relatively high, thus providing evidence for magnetic field amplification. The synchrotron radiation of several remnants is known to extend into the hard X-ray regime. In particular Cas A, has a spectrum that appears as a power law up to almost 100 TeV. This is very surprising, as a steepening is expected going from the soft to the hard X-ray band. The spectrum is likely a result of many superimposed individual spectra, each steepening at different energies. This implies considerable spatial variation in hard X-rays, an obvious target for Simbol-X. The variations will be important to infer local shock acceleration properties, but also magnetic field fluctuations may cause spatial and temporal variations. Finally, I draw the attention to super bubbles and supernovae as sources of cosmic rays. As such they may be sources of hard X-ray emission. In particular, supernovae exploding inside the dense red supergiants winds of their progenitors ares promising candidates for hard X-ray emission.

The Emerging Population of Pulsar Wind Nebulae in Hard X-rays

Science.gov (United States)

Mattana, F.; Götz, D.; Terrier, R.; Renaud, M.; Falanga, M.

2009-05-01

The hard X-ray synchrotron emission from Pulsar Wind Nebulae probes energetic particles, closely related to the pulsar injection power at the present time. INTEGRAL has disclosed the yet poorly known population of hard X-ray pulsar/PWN systems. We summarize the properties of the class, with emphasys on the first hard X-ray bow-shock (CTB 80 powered by PSR B1951+32), and highlight some prospects for the study of Pulsar Wind Nebulae with the Simbol-X mission.

Hard X-ray techniques suitable for polymer experiments

Energy Technology Data Exchange (ETDEWEB)

Bras, W; Goossens, H; Goderis, B, E-mail: Wim.Bras@esrf.fr [Netherlands Organisation for Scientific Research (NWO) (Netherlands); DUBBLE-ESRF, BP 220, F38043 Grenoble Cedex (France); Department of Chemical Engineering and Chemistry, Eindhoven University of Technology, PO Box 513, 5600 MB Eindhoven (Netherlands); Molecular and Nanomaterials, Chemistry Department, Catholic University of Leuven, Celestijnenlaan 200F (Belgium)

2010-11-15

Polymers have been studied since 1979 with 8-12 keV synchrotron radiation X-ray scattering methods and the number and sophistication of the experiments have rapidly grown ever since. More recently, new experimental techniques have been developed that use softer or harder X-rays in less conventional ways. This article provides a brief overview of the possibilities of hard X-ray techniques and indicates some areas that might gain from further developments.

Hard X-ray techniques suitable for polymer experiments

International Nuclear Information System (INIS)

Bras, W; Goossens, H; Goderis, B

2010-01-01

Polymers have been studied since 1979 with 8-12 keV synchrotron radiation X-ray scattering methods and the number and sophistication of the experiments have rapidly grown ever since. More recently, new experimental techniques have been developed that use softer or harder X-rays in less conventional ways. This article provides a brief overview of the possibilities of hard X-ray techniques and indicates some areas that might gain from further developments.

Microfabrication of hard x-ray lenses

DEFF Research Database (Denmark)

Stöhr, Frederik

This thesis deals with the development of silicon compound refractive lenses (Si-CRLs) for shaping hard x-ray beams. The CRLs are to be fabricated using state of the art microfabrication techniques. The primary goal of the thesis work is to produce Si-CRLs with considerably increased structure...... and characterized with respect to their shape. Their optical performances were tested at the European Synchrotron Radiation Facility (ESRF). Two 1D-focusing Si-CRLs suitable as condensers in hard-XRM were developed utilizing the aforementioned two different strategies. The first Si-condenser showed focusing of a 56...... of space for sample surroundings and ensure low-divergent and wide x-ray beams with narrow waists. Both results are substantial improvements to what was available at the start of this thesis work. The challenge of making x-ray objectives in silicon by interdigitation of lenslets alternately focusing...

High resolution hard x-ray microscope on a second generation synchrotron source

International Nuclear Information System (INIS)

Tian Yangchao; Li Wenjie; Chen Jie; Liu Longhua; Liu Gang; Tian Jinping; Xiong Ying; Tkachuk, Andrei; Gelb, Jeff; Hsu, George; Yun Wenbing

2008-01-01

A full-field, transmission x-ray microscope (TXM) operating in the energy range of 7-11 keV has been installed at the U7A beamline at the National Synchrotron Radiation Laboratory, a second generation synchrotron source operating at 0.8 GeV. Although the photon flux at sample position in the operating energy range is significantly low due to its relatively large emittance, the TXM can get high quality x-ray images with a spatial resolution down to 50 nm with acceptable exposure time. This TXM operates in either absorption or Zernike phase contrast mode with similar resolution. This TXM is a powerful analytical tool for a wide range of scientific areas, especially studies on nanoscale phenomena and structural imaging in biology, materials science, and environmental science. We present here the property of the x-ray source, beamline design, and the operation and key optical components of the x-ray TXM. Plans to improve the throughput of the TXM will be discussed.

Micro-structural characterization of materials using synchrotron hard X-ray imaging techniques

International Nuclear Information System (INIS)

Agrawal, Ashish; Singh, Balwant; Kashyap, Yogesh; Sarkar, P. S.; Shukla, Mayank; Sinha, Amar

2015-01-01

X-ray imaging has been an important tool to study the materials microstructure with the laboratory based sources however the advent of third generation synchrotron sources has introduced new concepts in X-ray imaging such as phase contrast imaging, micro-tomography, fluorescence imaging and diffraction enhance imaging. These techniques are being used to provide information of materials about their density distribution, porosity, geometrical and morphological characteristics at sub-micron scalewith improved contrast. This paper discusses the development of various imaging techniques at synchrotron based imaging beamline Indus-2 and few recent experiments carried out at this facility

Synchrotron x-ray fluorescence and extended x-ray absorption fine structure analysis

International Nuclear Information System (INIS)

Chen, J.R.; Gordon, B.M.; Hanson, A.L.; Jones, K.W.; Kraner, H.W.; Chao, E.C.T.; Minkin, J.A.

1984-01-01

The advent of dedicated synchrotron radiation sources has led to a significant increase in activity in many areas of science dealing with the interaction of x-rays with matter. Synchrotron radiation provides intense, linearly polarized, naturally collimated, continuously tunable photon beams, which are used to determine not only the elemental composition of a complex, polyatomic, dilute material but also the chemical form of the elements with improved accuracy. Examples of the application of synchrotron radiation include experiments in synchrotron x-ray fluorescence (SXRF) analysis and extended x-ray absorption fine structure (EXAFS) analysis. New synchrotron radiation x-ray microprobes for elemental analysis in the parts per billion range are under construction at several laboratories. 76 references, 24 figures

Blazars in Hard X-rays

Science.gov (United States)

Ghisellini, Gabriele

2009-05-01

Although blazars are thought to emit most of their luminosity in the γ-ray band, there are subclasses of them very prominent in hard X-rays. These are the best candidates to be studied by Simbol-X. They are at the extremes of the blazar sequence, having very small or very high jet powers. The former are the class of TeV emitting BL Lacs, whose synchrotron emission often peaks at tens of keV or more. The latter are the blazars with the most powerful jets, have high black hole masses accreting at high (i.e. close to Eddington) rates. These sources are predicted to have their high energy peak even below the MeV band, and therefore are very promising candidates to be studied with Simbol-X.

Coherent hard x-ray focusing optics and applications

Energy Technology Data Exchange (ETDEWEB)

Yun, W.B.; Viccaro, P.J.; Chrzas, J.; Lai, B.

1991-01-01

Coherent hard x-ray beams with a flux exceeding 10{sup 9} photons/second with a bandwidth of 0.1% will be provided by the undulator at the third generation synchrotron radiation sources such as APS, ESRF, and Spring-8. The availability of such high flux coherent x-ray beams offers excellent opportunities for extending the coherence-based techniques developed in the visible and soft x-ray part of the electromagnetic spectrum to the hard x-rays. These x-ray techniques (e.g., diffraction limited microfocusing, holography, interferometry, phase contrast imaging and signal enhancement), may offer substantial advantages over non-coherence-based x-ray techniques currently used. For example, the signal enhancement technique may be used to enhance an anomalous x-ray or magnetic x-ray scattering signal by several orders of magnitude. Coherent x-rays can be focused to a very small (diffraction-limited) spot size, thus allowing high spatial resolution microprobes to be constructed. The paper will discuss the feasibility of the extension of some coherence-based techniques to the hard x-ray range and the significant progress that has been made in the development of diffraction-limited focusing optics. Specific experimental results for a transmission Fresnel phase zone plate that can focus 8.2 keV x-rays to a spot size of about 2 microns will be briefly discussed. The comparison of measured focusing efficiency of the zone plate with that calculated will be made. Some specific applications of zone plates as coherent x-ray optics will be discussed. 17 refs., 4 figs.

Synchrotron hard X-ray imaging of shock-compressed metal powders

Science.gov (United States)

Rutherford, Michael E.; Chapman, David J.; Collinson, Mark A.; Jones, David R.; Music, Jasmina; Stafford, Samuel J. P.; Tear, Gareth R.; White, Thomas G.; Winters, John B. R.; Drakopoulos, Michael; Eakins, Daniel E.

2015-06-01

This poster will present the application of a new, high-energy (50 to 250 keV) synchrotron X-ray radiography technique to the study of shock-compressed granular materials. Following plate-impact loading, transmission radiography was used to quantitatively observe the compaction and release processes in a range of high-Z metal powders (e.g. Fe, Ni, Cu). By comparing the predictions of 3D numerical models initialized from X-ray tomograms-captured prior to loading-with experimental results, this research represents a new approach to refining mesoscopic compaction models. The authors gratefully acknowledge the ongoing support of Imperial College London, EPSRC, STFC and the Diamond Light Source, and AWE Plc.

Synchrotron radiation X-ray microfluorescence techniques

Indian Academy of Sciences (India)

Synchrotron X-ray imaging systems with fluorescence techniques was developed for biomedical researches in Brazilian Synchrotron Laboratory. An X-ray fluorescence microtomography system was implemented to analyse human prostate and breast samples and an X-ray microfluorescence system was implemented to ...

Synchrotron-Radiation Induced X-Ray Emission (SRIXE)

Energy Technology Data Exchange (ETDEWEB)

Jones, Keith W.

1999-09-01

Elemental analysis using emission of characteristic x rays is a well-established scientific method. The success of this analytical method is highly dependent on the properties of the source used to produce the x rays. X-ray tubes have long existed as a principal excitation source, but electron and proton beams have also been employed extensively. The development of the synchrotron radiation x-ray source that has taken place during the past 40 years has had a major impact on the general field of x-ray analysis. Even tier 40 years, science of x-ray analysis with synchrotron x-ray beams is by no means mature. Improvements being made to existing synchrotron facilities and the design and construction of new facilities promise to accelerate the development of the general scientific use of synchrotron x-ray sources for at least the next ten years. The effective use of the synchrotron source technology depends heavily on the use of high-performance computers for analysis and theoretical interpretation of the experimental data. Fortunately, computer technology has advanced at least as rapidly as the x-ray technology during the past 40 years and should continue to do so during the next decade. The combination of these technologies should bring about dramatic advances in many fields where synchrotron x-ray science is applied. It is interesting also to compare the growth and rate of acceptance of this particular research endeavor to the rates for other technological endeavors. Griibler [1997] cataloged the time required for introduction, diffusion,and acceptance of technological, economic, and social change and found mean values of 40 to 50 years. The introduction of the synchrotron source depends on both technical and non-technical factors, and the time scale at which this seems to be occurring is quite compatible with what is seen for other major innovations such as the railroad or the telegraph. It will be interesting to see how long the present rate of technological change

Synchrotron-Radiation Induced X-Ray Emission (SRIXE)

International Nuclear Information System (INIS)

Jones, Keith W.

1999-01-01

Elemental analysis using emission of characteristic x rays is a well-established scientific method. The success of this analytical method is highly dependent on the properties of the source used to produce the x rays. X-ray tubes have long existed as a principal excitation source, but electron and proton beams have also been employed extensively. The development of the synchrotron radiation x-ray source that has taken place during the past 40 years has had a major impact on the general field of x-ray analysis. Even tier 40 years, science of x-ray analysis with synchrotron x-ray beams is by no means mature. Improvements being made to existing synchrotron facilities and the design and construction of new facilities promise to accelerate the development of the general scientific use of synchrotron x-ray sources for at least the next ten years. The effective use of the synchrotron source technology depends heavily on the use of high-performance computers for analysis and theoretical interpretation of the experimental data. Fortunately, computer technology has advanced at least as rapidly as the x-ray technology during the past 40 years and should continue to do so during the next decade. The combination of these technologies should bring about dramatic advances in many fields where synchrotron x-ray science is applied. It is interesting also to compare the growth and rate of acceptance of this particular research endeavor to the rates for other technological endeavors. Griibler [1997] cataloged the time required for introduction, diffusion,and acceptance of technological, economic, and social change and found mean values of 40 to 50 years. The introduction of the synchrotron source depends on both technical and non-technical factors, and the time scale at which this seems to be occurring is quite compatible with what is seen for other major innovations such as the railroad or the telegraph. It will be interesting to see how long the present rate of technological change

Optoelectronic Picosecond Detection of Synchrotron X-rays

Energy Technology Data Exchange (ETDEWEB)

Durbin, Stephen M. [Purdue Univ., West Lafayette, IN (United States)

2017-08-04

The goal of this research program was to develop a detector that would measure x-ray time profiles with picosecond resolution. This was specifically aimed for use at x-ray synchrotrons, where x-ray pulse profiles have Gaussian time spreads of 50-100 ps (FWHM), so the successful development of such a detector with picosecond resolution would permit x-ray synchrotron studies to break through the pulse width barrier. That is, synchrotron time-resolved studies are currently limited to pump-probe studies that cannot reveal dynamics faster than ~50 ps, whereas the proposed detector would push this into the physically important 1 ps domain. The results of this research effort, described in detail below, are twofold: 1) the original plan to rely on converting electronic signals from a semiconductor sensor into an optical signal proved to be insufficient for generating signals with the necessary time resolution and sensitivity to be widely applicable; and 2) an all-optical method was discovered whereby the x-rays are directly absorbed in an optoelectronic material, lithium tantalate, which can then be probed by laser pulses with the desired picosecond sensitivity for detection of synchrotron x-rays. This research program has also produced new fundamental understanding of the interaction of x-rays and optical lasers in materials that has now created a viable path for true picosecond detection of synchrotron x-rays.

Hard X-ray nano-focusing with Montel mirror optics

Energy Technology Data Exchange (ETDEWEB)

Liu Wenjun, E-mail: wjliu@anl.gov [Advanced Photon Source, Argonne National Laboratory, Argonne, IL 60439 (United States); Ice, Gene E. [Oak Ridge National Laboratory, Oak Ridge, TN 37831 (United States); Assoufid, Lahsen; Liu Chian; Shi Bing; Zschack, Paul [Advanced Photon Source, Argonne National Laboratory, Argonne, IL 60439 (United States); Tischler, Jon [Oak Ridge National Laboratory, Oak Ridge, TN 37831 (United States); Qian Jun; Khachartryan, Ruben; Shu Deming [Advanced Photon Source, Argonne National Laboratory, Argonne, IL 60439 (United States)

2011-09-01

Kirkpatrick-Baez mirrors in the Montel (or nested) configuration were tested for hard X-ray nanoscale focusing at a third generation synchrotron beamline. In this scheme, two mirrors, mounted side-by-side and perpendicular to each other, provide for a more compact focusing system and a much higher demagnification and flux than the traditional sequential K-B mirror arrangement. They can accept up to a 120 {mu}mx120 {mu}m incident X-ray beam with a long working distance of 40 mm and broad-bandpass of energies up to {approx}30 keV. Initial test demonstrated a focal spot of about 150 nm in both horizontal and vertical directions with either polychromatic or monochromatic beam. Montel mirror optics is important and very appealing for achromatic X-ray nanoscale focusing in conventional non-extra-long synchrotron beamlines.

Real world issues for the new soft x-ray synchrotron sources

International Nuclear Information System (INIS)

Kincaid, B.M.

1991-05-01

A new generation of synchrotron radiation light sources covering the VUV, soft x-ray and hard x-ray spectral regions is under construction in several countries. They are designed specifically to use periodic magnetic undulators and low-emittance electron or positron beams to produce high-brightness near-diffraction-limited synchrotron radiation beams. An introduction to the properties of undulator radiation is followed by a discussion of some of the challenges to be faced at the new facilities. Examples of predicted undulator output from the Advanced Light Source, a third generation 1--2 GeV storage ring optimized for undulator use, are used to highlight differences from present synchrotron radiation sources, including high beam power, partial coherence, harmonics, and other unusual spectral and angular properties of undulator radiation. 8 refs., 2 figs

Non-thermal Hard X-Ray Emission from Coma and Several Abell Clusters

International Nuclear Information System (INIS)

Correa, C

2004-01-01

We report results of hard X-Ray observations of the clusters Coma, Abell 496, Abell754, Abell 1060, Abell 1367, Abell2256 and Abell3558 using RXTE data from the NASA HEASARC public archive. Specifically we searched for clusters with hard x-ray emission that can be fitted by a power law because this would indicate that the cluster is a source of non-thermal emission. We are assuming the emission mechanism proposed by Vahk Petrosian where the inter cluster space contains clouds of relativistic electrons that by themselves create a magnetic field and emit radio synchrotron radiation. These relativistic electrons Inverse-Compton scatter Microwave Background photons up to hard x-ray energies. The clusters that were found to be sources of non-thermal hard x-rays are Coma, Abell496, Abell754 and Abell 1060

Hard X-ray mirrors for Nuclear Security

Energy Technology Data Exchange (ETDEWEB)

Descalle, M. A. [Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States); Brejnholt, N. [Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States); Hill, R. [Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States); Decker, T. [Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States); Alameda, J. [Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States); Soufli, R. [Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States); Pivovaroff, M. [Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States); Pardini, T. [Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States)

2016-01-07

Research performed under this LDRD aimed to demonstrate the ability to detect and measure hard X-ray emissions using multilayer X-ray reflective optics above 400 keV, to enable the development of inexpensive and high-accuracy mirror substrates, and to investigate applications of hard X-ray mirrors of interest to the nuclear security community. Experiments conducted at the European Synchrotron Radiation Facility demonstrated hard X-ray mirror reflectivity up to 650 keV for the first time. Hard X-ray optics substrates must have surface roughness under 3 to 4 Angstrom rms, and three materials were evaluated as potential substrates: polycarbonates, thin Schott glass and a new type of flexible glass called Willow Glass®. Chemical smoothing and thermal heating of the surface of polycarbonate samples, which are inexpensive but have poor intrinsic surface characteristics, did not yield acceptable surface roughness. D263 Schott glass was used for the focusing optics of the NASA NuSTAR telescope. The required specialized hardware and process were costly and motivated experiments with a modified non-contact slumping technique. The surface roughness of the glass was preserved and the process yielded cylindrical shells with good net shape pointing to the potential advantage of this technique. Finally, measured surface roughness of 200 and 130 μm thick Willow Glass sheets was between 2 and 2.5 A rms. Additional results of flexibility tests and multilayer deposition campaigns indicated it is a promising substrate for hard X-ray optics. The detection of U and Pu characteristics X-ray lines and gamma emission lines in a high background environment was identified as an area for which X-ray mirrors could have an impact and where focusing optics could help reduce signal to noise ratio by focusing signal onto a smaller detector. Hence the first one twelvetant of a Wolter I focusing optics for the 90 to 140 keV energy range based on aperiodic multilayer coating was designed. Finally

X-ray beam splitting design for concurrent imaging at hard X-ray FELs and synchrotron facilities

Czech Academy of Sciences Publication Activity Database

Oberta, Peter; Mokso, R.

2013-01-01

Roč. 729, NOV (2013), s. 85-89 ISSN 0168-9002 R&D Projects: GA MPO FR-TI1/412 Institutional research plan: CEZ:AV0Z10100522 Keywords : diffractive-refractive optics * hard X-ray FEL * X-ray imaging Subject RIV: BH - Optics, Masers, Lasers Impact factor: 1.316, year: 2013 http://www.sciencedirect.com/science/article/pii/S0168900213009613

Hard alpha-keratin degradation inside a tissue under high flux X-ray synchrotron micro-beam: a multi-scale time-resolved study.

Science.gov (United States)

Leccia, Emilie; Gourrier, Aurélien; Doucet, Jean; Briki, Fatma

2010-04-01

X-rays interact strongly with biological organisms. Synchrotron radiation sources deliver very intense X-ray photon fluxes within micro- or submicro cross-section beams, resulting in doses larger than the MGy. The relevance of synchrotron radiation analyses of biological materials is therefore questionable since such doses, million times higher than the ones used in radiotherapy, can cause huge damages in tissues, with regard to not only DNA, but also proteic and lipid organizations. Very few data concerning the effect of very high X-ray doses in tissues are available in the literature. We present here an analysis of the structural phenomena which occur when the model tissue of human hair is irradiated by a synchrotron X-ray micro-beam. The choice of hair is supported by its hierarchical and partially ordered keratin structure which can be analysed inside the tissue by X-ray diffraction. To assess the damages caused by hard X-ray micro-beams (1 microm(2) cross-section), short exposure time scattering SAXS/WAXS patterns have been recorded at beamline ID13 (ESRF) after various irradiation times. Various modifications of the scattering patterns are observed, they provide fine insight of the radiation damages at various hierarchical levels and also unexpectedly provide information about the stability of the various hierarchical structural levels. It appears that the molecular level, i.e. the alpha helices which are stabilized by hydrogen bonds and the alpha-helical coiled coils which are stabilized by hydrophobic interactions, is more sensitive to radiation than the supramolecular architecture of the keratin filament and the filament packing within the keratin associated proteins matrix, which is stabilized by disulphide bonds. (c) 2009 Elsevier Inc. All rights reserved.

Techniques for materials research with synchrotron radiation x-rays

International Nuclear Information System (INIS)

Bowen, D.K.

1983-01-01

A brief introductory survey is presented of the properties and generation of synchrotron radiation and the main techniques developed so far for its application to materials problems. Headings are:synchrotron radiation; X-ray techniques in synchrotron radiation (powder diffraction; X-ray scattering; EXAFS (Extended X-ray Absorption Fine Structure); X-ray fluorescent analysis; microradiography; white radiation topography; double crystal topography); future developments. (U.K.)

Historical development of synchrotron x-ray diffraction topography

International Nuclear Information System (INIS)

Kawado, Seiji

2011-01-01

After a short history of X-ray diffraction topography, from the early stage of laboratory X-ray topography to recent synchrotron-radiation applications, is described, the development of science and technology for the synchrotron X-ray topography and its industrial applications are reviewed in more detail. In addition, the recent trend to synchrotron topography research is clarified on the basis of several data obtained from 256 papers which have been published since 2000. (author)

A HARD X-RAY POWER-LAW SPECTRAL CUTOFF IN CENTAURUS X-4

Energy Technology Data Exchange (ETDEWEB)

Chakrabarty, Deepto; Nowak, Michael A. [MIT Kavli Institute for Astrophysics and Space Research, Massachusetts Institute of Technology, Cambridge, MA 02139 (United States); Tomsick, John A.; Boggs, Steven E.; Craig, William W. [Space Sciences Laboratory, University of California, Berkeley, CA 94720 (United States); Grefenstette, Brian W.; Fürst, Felix; Harrison, Fiona A.; Rana, Vikram [Cahill Center for Astronomy and Astrophysics, California Institute of Technology, Pasadena, CA 91125 (United States); Psaltis, Dimitrios [Department of Astronomy, University of Arizona, Tucson, AZ 85721 (United States); Bachetti, Matteo; Barret, Didier [Observatoire Midi-Pyrénées, Université de Toulouse III - Paul Sabatier, F-31400 Toulouse (France); Christensen, Finn E. [Division of Astrophysics, National Space Institute, Technical University of Denmark, DK-2800 Lyngby (Denmark); Hailey, Charles J. [Columbia Astrophysics Laboratory, Columbia University, New York, NY 10027 (United States); Kaspi, Victoria M. [Department of Physics, McGill University, Montreal, PQ H3A 2T8 (Canada); Miller, Jon M. [Department of Astronomy, University of Michigan, Ann Arbor, MI 48109 (United States); Stern, Daniel [Jet Propulsion Laboratory, California Institute of Technology, Pasadena, CA 91109 (United States); Wik, Daniel R.; Zhang, William W. [Astrophysics Science Division, NASA Goddard Space Flight Center, Greenbelt, MD 20771 (United States); Wilms, Jörn, E-mail: deepto@mit.edu [Dr. Karl-Remeis-Sternwarte and Erlangen Centre for Astroparticle Physics, Universität Erlangen-Nürnberg, D-96049 Bamberg (Germany)

2014-12-20

The low-mass X-ray binary (LMXB) Cen X-4 is the brightest and closest (<1.2 kpc) quiescent neutron star transient. Previous 0.5-10 keV X-ray observations of Cen X-4 in quiescence identified two spectral components: soft thermal emission from the neutron star atmosphere and a hard power-law tail of unknown origin. We report here on a simultaneous observation of Cen X-4 with NuSTAR (3-79 keV) and XMM-Newton (0.3-10 keV) in 2013 January, providing the first sensitive hard X-ray spectrum of a quiescent neutron star transient. The 0.3-79 keV luminosity was 1.1×10{sup 33} D{sub kpc}{sup 2} erg s{sup –1}, with ≅60% in the thermal component. We clearly detect a cutoff of the hard spectral tail above 10 keV, the first time such a feature has been detected in this source class. We show that thermal Comptonization and synchrotron shock origins for the hard X-ray emission are ruled out on physical grounds. However, the hard X-ray spectrum is well fit by a thermal bremsstrahlung model with kT{sub e} = 18 keV, which can be understood as arising either in a hot layer above the neutron star atmosphere or in a radiatively inefficient accretion flow. The power-law cutoff energy may be set by the degree of Compton cooling of the bremsstrahlung electrons by thermal seed photons from the neutron star surface. Lower thermal luminosities should lead to higher (possibly undetectable) cutoff energies. We compare Cen X-4's behavior with PSR J1023+0038, IGR J18245–2452, and XSS J12270–4859, which have shown transitions between LMXB and radio pulsar modes at a similar X-ray luminosity.

Evaluating scintillator performance in time-resolved hard X-ray studies at synchrotron light sources.

Science.gov (United States)

Rutherford, Michael E; Chapman, David J; White, Thomas G; Drakopoulos, Michael; Rack, Alexander; Eakins, Daniel E

2016-05-01

The short pulse duration, small effective source size and high flux of synchrotron radiation is ideally suited for probing a wide range of transient deformation processes in materials under extreme conditions. In this paper, the challenges of high-resolution time-resolved indirect X-ray detection are reviewed in the context of dynamic synchrotron experiments. In particular, the discussion is targeted at two-dimensional integrating detector methods, such as those focused on dynamic radiography and diffraction experiments. The response of a scintillator to periodic synchrotron X-ray excitation is modelled and validated against experimental data collected at the Diamond Light Source (DLS) and European Synchrotron Radiation Facility (ESRF). An upper bound on the dynamic range accessible in a time-resolved experiment for a given bunch separation is calculated for a range of scintillators. New bunch structures are suggested for DLS and ESRF using the highest-performing commercially available crystal LYSO:Ce, allowing time-resolved experiments with an interframe time of 189 ns and a maximum dynamic range of 98 (6.6 bits).

The application of synchrotron radiation to X-ray lithography

International Nuclear Information System (INIS)

Spiller, E.; Eastman, D.E.; Feder, R.; Grobman, W.D.; Gudat, W.; Topalian, J.

1976-06-01

Synchrotron radiation from the German electron synchrotron DESY in Hamburg has been used for X-ray lithograpgy. Replications of different master patterns (for magnetic bubble devices, fresnel zone plates, etc.) were made using various wavelengths and exposures. High quality lines down to 500 A wide have been reproduced using very soft X-rays. The sensitivities of X-ray resists have been evaluated over a wide range of exposures. Various critical factors (heating, radiation damage, etc.) involved with X-ray lithography using synchrotron radiation have been studied. General considerations of storage ring sources designed as radiation sources for X-ray lithography are discussed, together with a comparison with X-ray tube sources. The general conclusion is that X-ray lithography using synchrotron radiation offers considerable promise as a process for forming high quality sub-micron images with exposure times as short as a few seconds. (orig.) [de

Studies in useful hard x-ray induced chemistry

Science.gov (United States)

Pravica, Michael; Bai, Ligang; Sneed, Daniel; Park, Changyong

2013-06-01

The observed rapid decomposition of potassium chlorate (via 2KClO3 + h ν --> 2KCl +3O2) via synchrotron hard x-ray irradiation (>10 keV) has enabled experiments that are developing novel and useful hard x-ray chemistry. We have observed a number of radiation-induced in situ decomposition reactions in various substances which release O2, H2, N2, NH3, and H2O in a diamond anvil cell (DAC) at ambient and high pressures. These novel acatalytic and isothermal reactions represent a highly controllable, penetrating, and focused method to initiate chemistry (including x-ray induced combustion) in sealed and/or isolated chambers which maintain matter under extreme conditions. During our studies, we have typically observed a slowing of decomposition with pressure including phase dependent decomposition of KClO3. Energy dependent studies have observed an apparent resonance near 15 keV at which the decomposition rate is maximized. This may enable use of much lower flux and portable x-ray sources (e.g. x-ray tubes) in larger scale experiments. These developments support novel means to load DACs and control chemical reactions providing novel routes of synthesis of novel materials under extreme conditions.

Synchrotron x-ray microbeam characteristics for x-ray fluorescence analysis

International Nuclear Information System (INIS)

Iida, Atsuo; Noma, Takashi

1995-01-01

X-ray fluorescence analysis using a synchrotron x-ray microprobe has become an indispensable technique for non-destructive micro-analysis. One of the most important parameters that characterize the x-ray microbeam system for x-ray fluorescence analysis is the beam size. For practical analysis, however, the photon flux, the energy resolution and the available energy range are also crucial. Three types of x-ray microbeam systems, including monochromatic and continuum excitation systems, were compared with reference to the sensitivity, the minimum detection limit and the applicability to various types of x-ray spectroscopic analysis. 16 refs., 5 figs

Applications of Hard X-ray Full-Field Transmission X-ray Microscopy at SSRL

International Nuclear Information System (INIS)

Liu, Y.; Andrews, J. C.; Mehta, A.; Pianetta, P.; Meirer, F.; Gil, S. Carrasco; Sciau, P.; Mester, Z.

2011-01-01

State-of-the-art hard x-ray full-field transmission x-ray microscopy (TXM) at beamline 6-2C of Stanford Synchrotron Radiation Lightsource has been applied to various research fields including biological, environmental, and material studies. With the capability of imaging a 32-micron field-of-view at 30-nm resolution using both absorption mode and Zernike phase contrast, the 3D morphology of yeast cells grown in gold-rich media was investigated. Quantitative evaluation of the absorption coefficient was performed for mercury nanoparticles in alfalfa roots exposed to mercury. Combining XANES and TXM, we also performed XANES-imaging on an ancient pottery sample from the Roman pottery workshop at LaGraufesenque (Aveyron).

Applications of Hard X-ray Full-Field Transmission X-ray Microscopy at SSRL

Science.gov (United States)

Liu, Y.; Andrews, J. C.; Meirer, F.; Mehta, A.; Gil, S. Carrasco; Sciau, P.; Mester, Z.; Pianetta, P.

2011-09-01

State-of-the-art hard x-ray full-field transmission x-ray microscopy (TXM) at beamline 6-2C of Stanford Synchrotron Radiation Lightsource has been applied to various research fields including biological, environmental, and material studies. With the capability of imaging a 32-micron field-of-view at 30-nm resolution using both absorption mode and Zernike phase contrast, the 3D morphology of yeast cells grown in gold-rich media was investigated. Quantitative evaluation of the absorption coefficient was performed for mercury nanoparticles in alfalfa roots exposed to mercury. Combining XANES and TXM, we also performed XANES-imaging on an ancient pottery sample from the Roman pottery workshop at LaGraufesenque (Aveyron).

A novel synthesis of polymeric CO via useful hard X-ray photochemistry

Directory of Open Access Journals (Sweden)

Michael Pravica

2016-12-01

Full Text Available We report on the synchrotron hard X-ray-induced decomposition of strontium oxalate (SrC2O4 pressurized to 7 GPa inside a diamond anvil cell (DAC. After some 4 h of irradiation in a white X-ray synchrotron beam, a dark reddish/brown region formed in the area of irradiation which was surrounded by a yellowish brown remainder in the rest of the sample. Upon depressurization of the sample to ambient conditions, the reacted/decomposed sample was recoverable as a dark brown/red and yellow waxy solid. Synchrotron infrared spectroscopy confirmed the strong presence of CO2 even under ambient conditions with the sample exposed to air and other strongly absorbing regions, suggesting that the sample may likely be polymerized CO (in part with dispersed CO2 and SrO trapped within the polymer. These results will have significant implications in the ability to readily produce and trap CO2 in situ via irradiation of a simple powder for useful hard X-ray photochemistry and in the ability to easily manufacture polymeric CO (via loading of powders in a DAC or high volume press without the need for the dangerous and complex loading of toxic CO. A novel means of X-ray-induced polymerization under extreme conditions has also been demonstrated.

Hard X-ray Microscopy with Elemental, Chemical and Structural Contrast

International Nuclear Information System (INIS)

Schroer, C.G.; Boye, P.; Feldkamp, J.P.

2010-01-01

We review hard X-ray microscopy techniques with a focus on scanning microscopy with synchrotron radiation. Its strength compared to other microscopies is the large penetration depth of hard x rays in matter that allows one to investigate the interior of an object without destructive sample preparation. In combination with tomography, local information from inside of a specimen can be obtained, even from inside special non-ambient sample environments. Different X-ray analytical techniques can be used to produce contrast, such as X-ray absorption, fluorescence, and diffraction, to yield chemical, elemental, and structural information about the sample, respectively. This makes X-ray microscopy attractive to many fields of science, ranging from physics and chemistry to materials, geo-, and environmental science, biomedicine, and nanotechnology. Our scanning microscope based on nanofocusing refractive X-ray lenses has a routine spatial resolution of about 100 nm and supports the contrast mechanisms mentioned above. In combination with coherent X-ray diffraction imaging, the spatial resolution can be improved to the 10 nm range. The current state-of-the-art of this technique is illustrated by several examples, and future prospects of the technique are given. (author)

Hard X-ray irradiation of cosmic silicate analogs: structural evolution and astrophysical implications

Science.gov (United States)

Gavilan, L.; Jäger, C.; Simionovici, A.; Lemaire, J. L.; Sabri, T.; Foy, E.; Yagoubi, S.; Henning, T.; Salomon, D.; Martinez-Criado, G.

2016-03-01

Context. Protoplanetary disks, interstellar clouds, and active galactic nuclei contain X-ray-dominated regions. X-rays interact with the dust and gas present in such environments. While a few laboratory X-ray irradiation experiments have been performed on ices, X-ray irradiation experiments on bare cosmic dust analogs have been scarce up to now. Aims: Our goal is to study the effects of hard X-rays on cosmic dust analogs via in situ X-ray diffraction. By using a hard X-ray synchrotron nanobeam, we seek to simulate cumulative X-ray exposure on dust grains during their lifetime in these astrophysical environments and provide an upper limit on the effect of hard X-rays on dust grain structure. Methods: We prepared enstatite (MgSiO3) nanograins, which are analogs to cosmic silicates, via the melting-quenching technique. These amorphous grains were then annealed to obtain polycrystalline grains. These were characterized via scanning electron microscopy (SEM) and high-resolution transmission electron microscopy (HRTEM) before irradiation. Powder samples were prepared in X-ray transparent substrates and were irradiated with hard X-rays nanobeams (29.4 keV) provided by beamline ID16B of the European Synchrotron Radiation Facility (Grenoble). X-ray diffraction images were recorded in transmission mode, and the ensuing diffractograms were analyzed as a function of the total X-ray exposure time. Results: We detected the amorphization of polycrystalline silicates embedded in an organic matrix after an accumulated X-ray exposure of 6.4 × 1027 eV cm-2. Pure crystalline silicate grains (without resin) do not exhibit amorphization. None of the amorphous silicate samples (pure and embedded in resin) underwent crystallization. We analyze the evolution of the polycrystalline sample embedded in an organic matrix as a function of X-ray exposure. Conclusions: Loss of diffraction peak intensity, peak broadening, and the disappearance of discrete spots and arcs reveal the amorphization

X-ray fluorescence imaging with synchrotron radiation

International Nuclear Information System (INIS)

Rivers, M.L.

1987-01-01

The micro-distribution of trace elements is of great interest in fields such as geochemistry, biology and material science. The synchrotron x-ray fluorescence microprobe provides a technique to quantitatively measure trace element compositions at individual points and to construct semiquantitative two dimensional maps of trace element compositions. This paper describes an x-ray fluorescence system used at the National Synchrotron Light Source

Using acoustic levitation in synchrotron based laser pump hard x-ray probe experiments

Science.gov (United States)

Hu, Bin; Lerch, Jason; Suthar, Kamlesh; Dichiara, Anthony

Acoustic levitation provides a platform to trap and hold a small amount of material by using standing pressure waves without a container. The technique has a potential to be used for laser pump x-ray probe experiments; x-ray scattering and laser distortion from the container can be avoided, sample consumption can be minimized, and unwanted chemistry that may occur at the container interface can be avoided. The method has been used at synchrotron sources for studying protein and pharmaceutical solutions using x-ray diffraction (XRD) and small angle x-ray scattering (SAXS). However, pump-probe experiments require homogeneously excited samples, smaller than the absorption depth of the material that must be held stably at the intersection of both the laser and x-ray beams. We discuss 1) the role of oscillations in acoustic levitation and the optimal acoustic trapping conditions for x-ray/laser experiments, 2) opportunities to automate acoustic levitation for fast sample loading and manipulation, and 3) our experimental results using SAXS to monitor laser induced thermal expansion in gold nanoparticles solution. We also performed Finite Element Analysis to optimize the trapping performance and stability of droplets ranging from 0.4 mm to 2 mm. Our early x-ray/laser demonstrated the potential of the technique for time-resolved X-ray science.

Diamond detectors for synchrotron radiation X-ray applications

Energy Technology Data Exchange (ETDEWEB)

De Sio, A. [Laboratori Nazionali di Frascati, INFN, 00044 Frascati, Roma (Italy); Department of Astronomy and Space Science, Universita di Firenze, L.go E. Fermi 2, 50125 Firenze (Italy)], E-mail: desio@arcetri.astro.it; Pace, E. [Department of Astronomy and Space Science, Universita di Firenze, L.go E. Fermi 2, 50125 Firenze (Italy); INFN, Sezione di Firenze, v. G. Sansone 1, Sesto Fiorentino, Firenze (Italy); Cinque, G.; Marcelli, A. [Laboratori Nazionali di Frascati, INFN, 00044 Frascati, Roma (Italy); Achard, J.; Tallaire, A. [LIMHP-CNRS, University of Paris XIII, 99 Avenue JB Clement, 93430 Villetaneuse (France)

2007-07-15

Due to its unique physical properties, diamond is a very appealing material for the development of electronic devices and sensors. Its wide band gap (5.5 eV) endows diamond based devices with low thermal noise, low dark current levels and, in the case of radiation detectors, high visible-to-X-ray signal discrimination (visible blindness) as well as high sensitivity to energies greater than the band gap. Furthermore, due to its radiation hardness diamond is very interesting for applications in extreme environments, or as monitor of high fluency radiation beams. In this work the use of diamond based detectors for X-ray sensing is discussed. On purpose, some photo-conductors based on different diamond types have been tested at the DAFNE-L synchrotron radiation laboratory at Frascati. X-ray sensitivity spectra, linearity and stability of the response of these diamond devices have been measured in order to evidence the promising performance of such devices.

Diamond detectors for synchrotron radiation X-ray applications

International Nuclear Information System (INIS)

De Sio, A.; Pace, E.; Cinque, G.; Marcelli, A.; Achard, J.; Tallaire, A.

2007-01-01

Due to its unique physical properties, diamond is a very appealing material for the development of electronic devices and sensors. Its wide band gap (5.5 eV) endows diamond based devices with low thermal noise, low dark current levels and, in the case of radiation detectors, high visible-to-X-ray signal discrimination (visible blindness) as well as high sensitivity to energies greater than the band gap. Furthermore, due to its radiation hardness diamond is very interesting for applications in extreme environments, or as monitor of high fluency radiation beams. In this work the use of diamond based detectors for X-ray sensing is discussed. On purpose, some photo-conductors based on different diamond types have been tested at the DAFNE-L synchrotron radiation laboratory at Frascati. X-ray sensitivity spectra, linearity and stability of the response of these diamond devices have been measured in order to evidence the promising performance of such devices

Synchrotron X-Ray Footprinting on Tour

OpenAIRE

Bohon, Jen; Ralston, Corie; D'Mello, Rhijuta; Gupta, Sayan; Chance, Mark R.

2014-01-01

Synchrotron X-ray footprinting resources were investigated at a variety of beamlines and synchrotron facilities to understand their potential for a mobile general user. Results indicate that viable resources exist at each synchrotron investigated such that a prospective user need only provide a simple flow apparatus and sample handling accessories to perform this technique.

Time-resolved X-ray studies using third generation synchrotron radiation sources

International Nuclear Information System (INIS)

Mills, D.M.

1991-10-01

The third generation, high-brilliance, hard x-ray, synchrotron radiation (SR) sources currently under construction (ESRF at Grenoble, France; APS at Argonne, Illinois; and SPring-8 at Harima, Japan) will usher in a new era of x-ray experimentation for both physical and biological sciences. One of the most exciting areas of experimentation will be the extension of x-ray scattering and diffraction techniques to the study of transient or time-evolving systems. The high repetition rate, short-pulse duration, high brilliance, and variable spectral bandwidth of these sources make them ideal for x-ray time-resolved studies. The temporal properties (bunch length, interpulse period, etc.) of these new sources will be summarized. Finally, the scientific potential and the technological challenges of time-resolved x-ray scattering from these new sources will be described. 13 refs., 4 figs

Hard X-ray Emission from Galaxy Clusters Observed with INTEGRAL and Prospects for Simbol-X

Science.gov (United States)

Eckert, D.; Paltani, S.; Courvoisier, T. J.-L.

2009-05-01

Some galaxy clusters are known to contain a large population of relativistic electrons, which produce radio emission through synchrotron radiation. Therefore, it is expected that inverse-Compton scattering of the relativistic electrons with the CMB produce non-thermal emission which should be observable in the hard X-ray domain. Here we focus on the recent results by INTEGRAL, which shed a new light on the non-thermal emission thanks to its angular resolution and sensitivity in the hard X-ray range. We also present the exciting prospects in this field for Simbol-X, which will allow us to detect the non-thermal emission in a number of clusters and map the magnetic field throughout the intra-cluster medium.

A submicron synchrotron X-ray beam generated by capillary optics

International Nuclear Information System (INIS)

Engstroem, P.; Larsson, S.; Rindby, A.; Buttkewitz, A.; Garbe, S.; Gaul, G.; Knoechel, A.; Lechtenberg, F.; Deutsches Elektronen-Synchrotron

1991-01-01

A novel capillary optics technique for focusing synchrotron X-ray beams has been applied in an experiment performed at the DORIS storage ring at HASYLAB. This new technqiue, which utilizes the total reflection properties of X-rays inside small capillaries, has recently been applied to generate microbeams of X-rays, with a beam size down to about 10 μm using conventional X-ray tubes. The result from our recent experiment shows that capillary optics can also be used to generate a submicron beam of X-rays from a synchrotron light source. A description of the capillary unit, and the alignment procedure is given. The influence of the thermal load on the device caused by the intense flux of synchrotron radiation will be discussed. Future perspectives of the capillary techniques as applied to synchrotron radiation will be discussed. (orig.)

Synchrotron X-ray induced solution precipitation of nanoparticles

CERN Document Server

Lee, H J; Hwu, Y; Tsai, W L

2003-01-01

By irradiating a solution in electroless Ni deposition using synchrotron X-rays, Ni composite was found to nucleate homogeneously and eventually precipitate in the form of nanoparticles. The size of the nanoparticles precipitated is rather uniform (100-300 nm depending on the applied temperature). By the addition of an organic acid, well-dispersed nanoparticles could be effectively deposited on glass substrate. The hydrated electrons (e sub a sub q sup -), products of radiolysis of water molecules by synchrotron X-rays, may be responsible for the effective reduction of the metal ions, resulting in homogeneous nucleation and nanoparticle formation. Our results suggest that synchrotron X-ray can be used to induce solution precipitation of nanoparticles and therefore lead to a new method of producing nanostructured particles and coating.

X-ray energy-dispersive diffractometry using synchrotron radiation

International Nuclear Information System (INIS)

Buras, B.; Staun Olsen, J.; Gerward, L.

1977-03-01

In contrast to bremsstrahlung from X-ray tubes, synchrotron radiation is very intense, has a smooth spectrum, its polarization is well defined, and at DESY the range of useful photon energies can be extended to about 70 keV and higher. In addition the X-ray beam is very well collimated. Thus synchrotron radiation seems to be an ideal X-ray source for energy-dispersive diffractometry. This note briefly describes the experimental set up at DESY, shows examples of results, and presents the underlying 'philosophy' of the research programme. (Auth.)

High-intensity laser synchrotron x-ray source

International Nuclear Information System (INIS)

Pogorelsky, I.V.

1995-10-01

A laser interacting with a relativistic electron beam behaves like a virtual wiggler of an extremely short period equal to half of the laser wavelength. This approach opens a route to relatively compact, high-brightness x-ray sources alternative or complementary to conventional synchrotron light sources. Although not new, the Laser Synchrotron Light Source (LSLS) concept is still waiting for a convincing demonstration. Available at the BNL's Accelerator Test Facility (ATF), a high-brightness electron beam and the high-power C0 2 laser may be used as prototype LSLS brick stones. In a feasible demonstration experiment, 10-GW, 100-ps C0 2 laser beam will be brought to a head-on collision with a 10-ps, 0.5-nC, 70 MeV electron bunch. Flashes of well-collimated, up to 9.36-keV (∼ Angstrom) x-rays of 10-ps pulse duration, with a flux of ∼10 19 photons/sec will be produced via linear Compton backscattering. The x-ray spectrum is tunable proportionally to a variable e-beam energy. A natural short-term extension of the proposed experiment would be further enhancement of the x-ray flux to a 10 21 -10 22 photons/sec level, after the ongoing ATF CO 2 laser upgrade to 1 TW peak power and electron bunch shortening to 3 ps. The ATF LSLS x-ray beamline, exceeding by orders of magnitude the peak fluxes attained at the National Synchrotron Light Source (NSLS) x-ray storage ring, may become attractive for certain users, e.g., for biological x-ray microscopy. In addition, a terawatt CO 2 laser will enable harmonic multiplication of the x-ray spectrum via nonlinear Compton scattering

Time-resolved materials science opportunities using synchrotron x-ray sources

International Nuclear Information System (INIS)

Larson, B.C.; Tischler, J.Z.

1995-06-01

The high brightness, high intensity, and pulsed time-structure of synchrotron sources provide new opportunities for time-resolved x-ray diffraction investigations. With third generation synchrotron sources coming on line, high brilliance and high brightness are now available in x-ray beams with the highest flux. In addition to the high average flux, the instantaneous flux available in synchrotron beams is greatly enhanced by the pulsed time structure, which consists of short bursts of x-rays that are separated by ∼tens to hundreds of nanoseconds. Time-resolved one- and two-dimensional position sensitive detection techniques that take advantage of synchrotron radiation for materials science x-ray diffraction investigations are presented, and time resolved materials science applications are discussed in terms of recent diffraction and spectroscopy results and materials research opportunities

Quantitative X-ray microtomography with synchrotron radiation

Energy Technology Data Exchange (ETDEWEB)

Donath, T. [GKSS-Forschungszentrum Geesthacht GmbH (Germany). Inst. fuer Materialforschung

2007-07-01

Synchrotron-radiation-based computed microtomography (SR{sub {mu}}CT) is an established method for the examination of volume structures. It allows to measure the x-ray attenuation coefficient of a specimen three-dimensionally with a spatial resolution of about one micrometer. In contrast to conventional x-ray sources (x-ray tubes), the unique properties of synchrotron radiation enable quantitative measurements that do not suffer from beam-hardening artifacts. During this work the capabilities for quantitative SR{sub {mu}}CT measurements have been further improved by enhancements that were made to the SR{sub {mu}}CT apparatus and to the reconstruction chain. For high-resolution SR{sub {mu}}CT an x-ray camera consisting of luminescent screen (x-ray phosphor), lens system, and CCD camera was used. A significant suppression of blur that is caused by reflections inside the luminescent screen could be achieved by application of an absorbing optical coating to the screen surface. It is shown that blur and ring artifacts in the tomographic reconstructions are thereby drastically reduced. Furthermore, a robust and objective method for the determination of the center of rotation in projection data (sinograms) is presented that achieves sub-pixel precision. By implementation of this method into the reconstruction chain, complete automation of the reconstruction process has been achieved. Examples of quantitative SR{sub {mu}}CT studies conducted at the Hamburger Synchrotronstrahlungslabor HASYLAB at the Deutsches Elektronen-Synchrotron DESY are presented and used for the demonstration of the achieved enhancements. (orig.)

Quantitative X-ray microtomography with synchrotron radiation

International Nuclear Information System (INIS)

Donath, T.

2007-01-01

Synchrotron-radiation-based computed microtomography (SR μ CT) is an established method for the examination of volume structures. It allows to measure the x-ray attenuation coefficient of a specimen three-dimensionally with a spatial resolution of about one micrometer. In contrast to conventional x-ray sources (x-ray tubes), the unique properties of synchrotron radiation enable quantitative measurements that do not suffer from beam-hardening artifacts. During this work the capabilities for quantitative SR μ CT measurements have been further improved by enhancements that were made to the SR μ CT apparatus and to the reconstruction chain. For high-resolution SR μ CT an x-ray camera consisting of luminescent screen (x-ray phosphor), lens system, and CCD camera was used. A significant suppression of blur that is caused by reflections inside the luminescent screen could be achieved by application of an absorbing optical coating to the screen surface. It is shown that blur and ring artifacts in the tomographic reconstructions are thereby drastically reduced. Furthermore, a robust and objective method for the determination of the center of rotation in projection data (sinograms) is presented that achieves sub-pixel precision. By implementation of this method into the reconstruction chain, complete automation of the reconstruction process has been achieved. Examples of quantitative SR μ CT studies conducted at the Hamburger Synchrotronstrahlungslabor HASYLAB at the Deutsches Elektronen-Synchrotron DESY are presented and used for the demonstration of the achieved enhancements. (orig.)

The Variable Crab Nebula: Evidence for a Connection Between GeV Flares and Hard X-ray Variations

Science.gov (United States)

Wilson-Hodge, Colleen A.; Harding, A. K.; Hays, E. A.; Cherry, M. L.; Case, G. L.; Finger, M. H.; Jenke, P.; Zhang, X.

2016-01-01

In 2010, hard X-ray variations (Wilson-Hodge et al. 2011) and GeV flares (Tavani et al 2011, Abdo et al. 2011) from the Crab Nebula were discovered. Connections between these two phenomena were unclear, in part because the timescales were quite different, with yearly variations in hard X-rays and hourly to daily variations in the GeV flares. The hard X-ray flux from the Crab Nebula has again declined since 2014, much like it did in 2008-2010. During both hard X-ray decline periods, the Fermi LAT detected no GeV flares, suggesting that injection of particles from the GeV flares produces the much slower and weaker hard X-ray variations. The timescale for the particles emitting the GeV flares to lose enough energy to emit synchrotron photons in hard X-rays is consistent with the yearly variations observed in hard X-rays and with the expectation that the timescale for variations slowly increases with decreasing energy. This hypothesis also predicts even slower and weaker variations below 10 keV, consistent with the non-detection of counterparts to the GeV flares by Chandra (Weisskopf et al 2013). We will present a comparison of the observed hard X-ray variations and a simple model of the decay of particles from the GeV flares to test our hypothesis.

Investigation of biomedical inner microstructures with hard X-ray phase-contrast imaging

Energy Technology Data Exchange (ETDEWEB)

Shu Hang [Beijing Synchrotron Radiation Facility, Institute of High Energy Physics, CAS, 100049 Beijing (China); Graduate University of the Chinese Academy of Sciences, 100864 Beijing (China); Zhu Peiping [Beijing Synchrotron Radiation Facility, Institute of High Energy Physics, CAS, 100049 Beijing (China); Chen Bo [Department of Physics, University of Science and Technology of China, Hefei 230026 (China); Liu Bo; Yin Hongxia [Capital University of Medical Sciences, 100054 Beijing (China); Li Enrong [Beijing Synchrotron Radiation Facility, Institute of High Energy Physics, CAS, 100049 Beijing (China); Graduate University of the Chinese Academy of Sciences, 100864 Beijing (China); Liu Yijin [Department of Physics, University of Science and Technology of China, Hefei 230026 (China); Wang Junyue [Beijing Synchrotron Radiation Facility, Institute of High Energy Physics, CAS, 100049 Beijing (China); Graduate University of the Chinese Academy of Sciences, 100864 Beijing (China); Yuan Qingxi; Huang Wanxia; Fang Shouxian [Beijing Synchrotron Radiation Facility, Institute of High Energy Physics, CAS, 100049 Beijing (China); Wu Ziyu [Beijing Synchrotron Radiation Facility, Institute of High Energy Physics, CAS, 100049 Beijing (China); National Center for NanoScience and Technology, 100080 Beijing (China)], E-mail: wuzy@ihep.ac.cn

2007-09-21

Hard X-ray Phase-Contrast Imaging (HX-PCI) is a new and valuable method that may provide information of the inner parts of an opaque object. Previous reports demonstrated its applicability in soft and hard tissue imaging. Here we provide further evidence for improved image quality and the effective capability to distinguish inner microstructures in real biomedical systems such as cochlea. Experiments performed both at the 4W1A beamline of the Beijing Synchrotron Radiation Facility (BSRF) and at the Taiwan National Synchrotron Radiation Research Center (NSRRC) clearly show details of samples' inner microstructure with a resolution of a few microns. The improved spatial resolution is a relevant achievement for future improved understanding and clinical trials.

Development and application of cryogenic radiometry with hard X-rays

International Nuclear Information System (INIS)

Gerlach, Martin

2008-01-01

To establish cryogenic radiometry with hard X-ray radiation for photon energies of up to 60 keV, a novel type of cavity absorber had to be developed for the cryogenic radiometer SYRES I, which is deployed by the Physikalisch-Technische Bundesanstalt (PTB) as primary standard detector at the electron storage ring BESSY II. This new type of cavity absorber allows for the complete absorption of hard X-ray radiation in combination with an appropriate sensitivity and an adequate time constant for the measurement of synchrotron radiation at BESSY II. As the process of fabrication of different types of absorbers is very time-consuming, the interaction of hard X-ray radiation with different absorber materials and geometries was studied intensively by using the Monte Carlo simulation code Geant4. The accuracy of the simulations was verified comparing them to scattering experiments performed at a wavelength shifter beamline at BESSY II with a calibrated energy dispersive detector. It was shown that Geant4 describes the photo-effect, including fluorescence as well as Compton- and Rayleigh scattering, with high accuracy. The simulations and experiments resulted in a cavity absorber with a gold base 550 μm in thickness and a cylindrical shell made of copper 90 μm in thickness to reduce losses caused by fluorescence and scattered radiation. Monochromatized synchrotron radiation of high spectral purity was then used to calibrate semiconductor photodiodes, which can be used as compact and inexpensive secondary standard detectors, against a cryogenic radiometer, covering the entire photon energy range of three beamlines from 50 eV to 60 keV with relative uncertainties of less than 0.5 %. Furthermore the spatial homogeneity of the spectral responsivity, the transmittance and the linearity of the photodiodes was investigated. Through a direct comparison of the free-air ionization chamber PK100, a primary detector standard of PTB used in dosimetry, and the cryogenic radiometer SYRES

A novel probe of intrinsic electronic structure: hard X-ray photoemission spectroscopy

International Nuclear Information System (INIS)

Takata, Y.; Tamasaku, K.; Nishino, Y.; Miwa, D.; Yabashi, M.; Ikenaga, E.; Horiba, K.; Arita, M.; Shimada, K.; Namatame, H.; Nohira, H.; Hattori, T.; Soedergren, S.; Wannberg, B.; Taniguchi, M.; Shin, S.; Ishikawa, T.; Kobayashi, K.

2005-01-01

We have realized hard X-ray (HX) photoemission spectroscopy (PES) with high throughput and high-energy resolution for core level and valence band studies using high-energy and high-brilliance synchrotron radiation at SPring-8. This is a brand new method because large escape depth of high-energy photoelectrons enables us to probe intrinsic bulk states free from surface condition. By use of a newly developed electron energy analyzer and well-focused X-rays, high-energy resolution of 75 meV (E/ΔE 79,000) was realized for 5.95 keV photoelectrons

Broad-band hard X-ray reflectors

DEFF Research Database (Denmark)

Joensen, K.D.; Gorenstein, P.; Hoghoj, P.

1997-01-01

Interest in optics for hard X-ray broad-band application is growing. In this paper, we compare the hard X-ray (20-100 keV) reflectivity obtained with an energy-dispersive reflectometer, of a standard commercial gold thin-film with that of a 600 bilayer W/Si X-ray supermirror. The reflectivity...... of the multilayer is found to agree extraordinarily well with theory (assuming an interface roughness of 4.5 Angstrom), while the agreement for the gold film is less, The overall performance of the supermirror is superior to that of gold, extending the band of reflection at least a factor of 2.8 beyond...... that of the gold, Various other design options are discussed, and we conclude that continued interest in the X-ray supermirror for broad-band hard X-ray applications is warranted....

A laboratory-based hard x-ray monochromator for high-resolution x-ray emission spectroscopy and x-ray absorption near edge structure measurements

Energy Technology Data Exchange (ETDEWEB)

Seidler, G. T., E-mail: seidler@uw.edu; Mortensen, D. R.; Remesnik, A. J.; Pacold, J. I.; Ball, N. A.; Barry, N.; Styczinski, M.; Hoidn, O. R. [Physics Department, University of Washington, Seattle, Washington 98195-1560 (United States)

2014-11-15

We report the development of a laboratory-based Rowland-circle monochromator that incorporates a low power x-ray (bremsstrahlung) tube source, a spherically bent crystal analyzer, and an energy-resolving solid-state detector. This relatively inexpensive, introductory level instrument achieves 1-eV energy resolution for photon energies of ∼5 keV to ∼10 keV while also demonstrating a net efficiency previously seen only in laboratory monochromators having much coarser energy resolution. Despite the use of only a compact, air-cooled 10 W x-ray tube, we find count rates for nonresonant x-ray emission spectroscopy comparable to those achieved at monochromatized spectroscopy beamlines at synchrotron light sources. For x-ray absorption near edge structure, the monochromatized flux is small (due to the use of a low-powered x-ray generator) but still useful for routine transmission-mode studies of concentrated samples. These results indicate that upgrading to a standard commercial high-power line-focused x-ray tube or rotating anode x-ray generator would result in monochromatized fluxes of order 10{sup 6}–10{sup 7} photons/s with no loss in energy resolution. This work establishes core technical capabilities for a rejuvenation of laboratory-based hard x-ray spectroscopies that could have special relevance for contemporary research on catalytic or electrical energy storage systems using transition-metal, lanthanide, or noble-metal active species.

Upgrading multilayer zone plate technology for hard x-ray focusing

Energy Technology Data Exchange (ETDEWEB)

Hirotomo, Toshiki; Konishi, Shigeki [Graduate School of Material Science, University of Hyogo, Kamigori, Hyogo 678-1297 (Japan); SPring-8 Service Co., Ltd (Japan); Takano, Hidekazu, E-mail: htakano@sci.u-hyogo.ac.jp; Sumida, Kazuhiro; Tsusaka, Yoshiyuki; Kagoshima, Yasushi [Graduate School of Material Science, University of Hyogo, Kamigori, Hyogo 678-1297 (Japan); Koyama, Takahisa [Graduate School of Material Science, University of Hyogo, Kamigori, Hyogo 678-1297 (Japan); Japan Synchrotron Radiation Research Institute (JASRI/SPring-8) (Japan); Ichimaru, Satoshi; Ohchi, Tadayuki [NTT Advanced Technology Corporation (Japan); Takenaka, Hisataka [NTT Advanced Technology Corporation (Japan); TOYAMA Corporation (Japan)

2016-01-28

Multilayer zone plate (MZP) technology for hard X-ray focusing was upgraded and its focusing performance was evaluated using 20-keV X-rays at the synchrotron beamline (BL24XU) of SPring-8. The MZP consists of MoSi{sub 2} and Si layers alternately deposited on a glass fiber by magnetron sputtering so that all zone boundaries satisfy the Fresnel zone configuration. The focused beam was evaluated using knife-edge scanning in which the measured intensity distribution is identical to the line spread function (LSF) in the focal plane. The focused beamsize of about 30 nm was estimated by oscillation peaks observed in the measured LSF according to Rayleigh’s criterion.

A preliminary study of synchrotron light sources for x-ray lithography

International Nuclear Information System (INIS)

Hoffmann, C.R.; Bigham, C.B.; Ebrahim, N.A.; Sawicki, J.A.; Taylor, T.

1989-02-01

A preliminary study of synchrotron light sources has been made, primarily oriented toward x-ray lithography. X-ray lithography is being pursued vigorously in several countries, with a goal of manufacturing high-density computer chips (0.25 μm feature sizes), and may attain commercial success in the next decade. Many other applications of soft x-rays appear worthy of investigation as well. The study group visited synchrotron radiation facilities and had discussions with members of the synchrotron radiation community, particularly Canadians. It concluded that accelerator technology for a conventional synchrotron light source appropriate for x-ray lithography is well established and is consistent with skills and experience at Chalk River Nuclear Laboratories. Compact superconducting systems are being developed also. Their technical requirements overlap with capabilities at Chalk River. (32 refs)

Application of synchrotron radiation to x-ray fluorescence analysis of trace elements

International Nuclear Information System (INIS)

Gordon, B.M.; Jones, K.W.; Hanson, A.L.

1986-08-01

The development of synchrotron radiation x-ray sources has provided the means to greatly extend the capabilities of x-ray fluorescence analysis for determinations of trace element concentrations. A brief description of synchrotron radiation properties provides a background for a discussion of the improved detection limits compared to existing x-ray fluorescence techniques. Calculated detection limits for x-ray microprobes with micrometer spatial resolutions are described and compared with experimental results beginning to appear from a number of laboratories. The current activities and future plans for a dedicated x-ray microprobe beam line at the National Synchrotron Light Source (NSLS) of Brookhaven National Laboratory are presented

Synchrotron radiation calibration for soft X-ray detector

International Nuclear Information System (INIS)

Ning, Jiamin; Guo, Cun; Xu, Rongkun; Jiang, Shilun; Xu, Zeping; Chen, Jinchuan; Xia, Guangxin; Xue, Feibiao; Qin, Yi

2009-04-01

The calibration experiments were carried out to X-ray film, scintillator and transmission grating by employing the soft X-ray station at 3W1B beam-line in Beijing synchrotron Radiation Facility. The experiments presented the black intensity curve and energy response curve of soft X-ray film. And the experimental results can be used in diagnosis of X-ray radiation characterization of Z-pinch, such as in the measurement of soft X-ray Power Meter, grating spectrometer, pinhole camera and one-dimension imaging system which can ensure precision of Z-pinch results. (authors)

Ultra-high vacuum compatible optical chopper system for synchrotron x-ray scanning tunneling microscopy

Energy Technology Data Exchange (ETDEWEB)

Chang, Hao, E-mail: hc000211@ohio.edu [Advanced Photon Source, Argonne National Laboratory, 9700 South Cass Avenue, Argonne, Illinois 60439 (United States); Nanoscale and Quantum Phenomena Institute, Physics & Astronomy Department, Ohio University, Athens, Ohio 45701 (United States); Cummings, Marvin; Shirato, Nozomi; Stripe, Benjamin; Preissner, Curt; Freeland, John W. [Advanced Photon Source, Argonne National Laboratory, 9700 South Cass Avenue, Argonne, Illinois 60439 (United States); Rosenmann, Daniel [Center for Nanoscale Materials, Argonne National Laboratory, 9700 South Cass Avenue, Argonne, Illinois 60439 (United States); Kersell, Heath; Hla, Saw-Wai [Nanoscale and Quantum Phenomena Institute, Physics & Astronomy Department, Ohio University, Athens, Ohio 45701 (United States); Center for Nanoscale Materials, Argonne National Laboratory, 9700 South Cass Avenue, Argonne, Illinois 60439 (United States); Rose, Volker, E-mail: vrose@anl.gov [Advanced Photon Source, Argonne National Laboratory, 9700 South Cass Avenue, Argonne, Illinois 60439 (United States); Center for Nanoscale Materials, Argonne National Laboratory, 9700 South Cass Avenue, Argonne, Illinois 60439 (United States)

2016-01-28

High-speed beam choppers are a crucial part of time-resolved x-ray studies as well as a necessary component to enable elemental contrast in synchrotron x-ray scanning tunneling microscopy (SX-STM). However, many chopper systems are not capable of operation in vacuum, which restricts their application to x-ray studies with high photon energies, where air absorption does not present a significant problem. To overcome this limitation, we present a fully ultra-high vacuum (UHV) compatible chopper system capable of operating at variable chopping frequencies up to 4 kHz. The lightweight aluminum chopper disk is coated with Ti and Au films to provide the required beam attenuation for soft and hard x-rays with photon energies up to about 12 keV. The chopper is used for lock-in detection of x-ray enhanced signals in SX-STM.

CCD [charge-coupled device] sensors in synchrotron x-ray detectors

International Nuclear Information System (INIS)

Strauss, M.G.; Naday, I.; Sherman, I.S.; Kraimer, M.R.; Westbrook, E.M.; Zaluzec, N.J.

1987-01-01

The intense photon flux from advanced synchrotron light sources, such as the 7-GeV synchrotron being designed at Argonne, require integrating-type detectors. Charge-coupled devices (CCDs) are well suited as synchrotron x-ray detectors. When irradiated indirectly via a phosphor followed by reducing optics, diffraction patterns of 100 cm 2 can be imaged on a 2 cm 2 CCD. With a conversion efficiency of ∼1 CCD electron/x-ray photon, a peak saturation capacity of >10 6 x rays can be obtained. A programmable CCD controller operating at a clock frequency of 20 MHz has been developed. The readout rate is 5 x 10 6 pixels/s and the shift rate in the parallel registers is 10 6 lines/s. The test detector was evaluated in two experiments. In protein crystallography diffraction patterns have been obtained from a lysozyme crystal using a conventional rotating anode x-ray generator. Based on these results we expect to obtain at a synchrotron diffraction images at the rate of ∼1 frame/s or a complete 3-dimensional data set from a single crystal in ∼2 min. 16 refs., 16 figs., 2 tabs

X-ray diffraction microtomography using synchrotron radiation

CERN Document Server

Barroso, R C; Jesus, E F O; Oliveira, L F

2001-01-01

The X-ray diffraction computed tomography technique is based on the interference phenomena of the coherent scatter. For low-momentum transfer, it is most probable that the scattering interaction will be coherent. A selective discrimination of a given element in a scanned specimen can be realized by fixing the Bragg angle which produces an interference peak and then, to carry out the computed tomography in the standard mode. The image reconstructed exalts the presence of this element with respect to other ones in a sample. This work reports the feasibility of a non-destructive synchrotron radiation X-ray diffraction imaging technique. This research was performed at the X-ray Diffraction beam line of the National Synchrotron Light Laboratory (LNLS) in Brazil. The coherent scattering properties of different tissue and bone substitute materials were evaluated. Furthermore, diffraction patterns of some polycrystalline solids were studied due to industrial and environmental human exposure to these metals. The obtai...

Submicron hard X-ray fluorescence imaging of synthetic elements.

Science.gov (United States)

Jensen, Mark P; Aryal, Baikuntha P; Gorman-Lewis, Drew; Paunesku, Tatjana; Lai, Barry; Vogt, Stefan; Woloschak, Gayle E

2012-04-13

Synchrotron-based X-ray fluorescence microscopy (XFM) using hard X-rays focused into sub-micron spots is a powerful technique for elemental quantification and mapping, as well as microspectroscopic measurements such as μ-XANES (X-ray absorption near edge structure). We have used XFM to image and simultaneously quantify the transuranic element plutonium at the L(3) or L(2)-edge as well as Th and lighter biologically essential elements in individual rat pheochromocytoma (PC12) cells after exposure to the long-lived plutonium isotope (242)Pu. Elemental maps demonstrate that plutonium localizes principally in the cytoplasm of the cells and avoids the cell nucleus, which is marked by the highest concentrations of phosphorus and zinc, under the conditions of our experiments. The minimum detection limit under typical acquisition conditions with an incident X-ray energy of 18 keV for an average 202 μm(2) cell is 1.4 fg Pu or 2.9×10(-20) moles Pu μm(-2), which is similar to the detection limit of K-edge XFM of transition metals at 10 keV. Copper electron microscopy grids were used to avoid interference from gold X-ray emissions, but traces of strontium present in naturally occurring calcium can still interfere with plutonium detection using its L(α) X-ray emission. Copyright © 2012 Elsevier B.V. All rights reserved.

Magnetic X-Ray Scattering with Synchrotron Radiation

DEFF Research Database (Denmark)

Moncton, D. E.; Gibbs, D.; Bohr, Jakob

1986-01-01

With the availability of high-brilliance synchrotron radiation from multiple wigglers, magnetic X-ray scattering has become a powerful new probe of magnetic structure and phase transitions. Similar to the well-established magnetic neutron scattering technique, magnetic X-ray scattering methods have...... many complementary advantages. A brief review is presented of the history of magnetic X-ray scattering as well as recent results obtained in studies of the rare-earth magnet holmium with emphasis on instrumentational aspects. In particular, the development of a simple polarization analyzer...... to distinguish charge and magnetic scattering is described....

Center for X-ray Optics, 1988

International Nuclear Information System (INIS)

1989-04-01

This report briefly reviews the following topics: soft-x-ray imaging; reflective optics for hard x-rays; coherent XUV sources; spectroscopy with x-rays; detectors for coronary artery imaging; synchrotron-radiation optics; and support for the advanced light source

Discovery of Diffuse Hard X-ray Emission associated with Jupiter

Science.gov (United States)

Ezoe, Y.; Miyoshi, Y.; Ishikawa, K.; Ohashi, T.; Terada, N.; Uchiyama, Y.; Negoro, H.

2009-12-01

Our discovery of diffuse hard (1-5 keV) X-ray emission around Jupiter is reported. Recent Chandra and XMM-Newton observations revealed several types of X-rays in the vicinity of Jupiter such as auroral and disk emission from Jupiter and faint diffuse X-rays from the Io Plasma Torus (see Bhardwaj et al. 2007 for review). To investigate possible diffuse hard X-ray emission around Jupiter with the highest sensitivity, we conducted data analysis of Suzaku XIS observations of Jupiter on Feb 2006. After removing satellite and planetary orbital motions, we detected a significant diffuse X-ray emission extending to ~6 x 3 arcmin with the 1-5 keV X-ray luminosity of ~3e15 erg/s. The emitting region very well coincided with the Jupiter's radiation belts. The 1-5 keV X-ray spectrum was represented by a simple power law model with a photon index of 1.4. Such a flat continuum strongly suggests non-thermal origin. Although such an emission can be originated from multiple background point sources, its possibility is quite low. We hence examined three mechanisms, assuming that the emission is truly diffuse: bremsstrahlung by keV electrons, synchrotron emission by TeV electrons, and inverse Compton scattering of solar photons by MeV electrons. The former two can be rejected because of the X-ray spectral shape and implausible existence of TeV electrons around Jupiter, respectively. The last possibility was found to be possible because tens MeV electrons, which have been confirmed in inner radiation belts (Bolton et al. 2002), can kick solar photons to the keV energy range and provide a simple power-law continuum. We estimated an average electron density from the X-ray luminosity assuming the oblate spheroid shaped emitting region with 8 x 8 x 4 Jovian radii. The necessary density was 0.02 1/cm3 for 50 MeV electrons. Hence, our results may suggest a new particle acceleration phenomenon around Jupiter.

Cryogenic radiometry in the hard X-ray range

International Nuclear Information System (INIS)

Gerlach, M.; Krumrey, M.; Cibik, L.; Muller, P.; Rabus, H.; Ulm, G.

2008-01-01

For many applications in radiometry, spectroscopy or astrophysics, absolute measurement of radiant power with low uncertainty is essential. Cryogenic electrical substitution radiometers (ESRs) are regarded as the highest-accuracy primary standard detector in radiometry, from the infrared to the ultraviolet region; in combination with tuneable monochromatized synchrotron radiation from electron storage rings, their range of operation has been extended to the soft x-ray region. ESRs are absolute thermal detectors, based on the equivalence of electrical power and radiant power that can be traced back to electrical SI units and be measured with low uncertainties. Their core piece is a cavity absorber, which is typically made of copper to achieve a short response time suitable for use with synchrotron radiation. At higher photon energies, the use of copper prevents the operation of ESRs due to increasing transmittance. A new absorber design for hard x-rays has been developed at the laboratory of the Physikalisch-Technische Bundesanstalt (PTB) at the electron storage ring BESSY II. The Monte Carlo simulation code Geant4 was applied to optimize its absorptance for photon energies of up to 60 keV, resulting in a cavity absorber with a gold base and a cylindrical shell made of copper, in combination with a thermal sensitivity of around 150 mK μW -1 and a time constant of less than 3 min, which is short compared with the lifetime of many hours for the storage ring current. The measurement of the radiant power of monochromatized synchrotron radiation was achieved with relative standard uncertainties of less than 0.2%, covering the entire photon energy range of three beamlines from 50 eV to 60 keV. Monochromatized synchrotron radiation of high spectral purity was used to calibrate silicon photodiodes against the ESR for photon energies up to 60 keV with relative standard uncertainties below 0.3%. (authors)

Cryogenic radiometry in the hard X-ray range

Energy Technology Data Exchange (ETDEWEB)

Gerlach, M.; Krumrey, M.; Cibik, L.; Muller, P.; Rabus, H.; Ulm, G. [Physikalisch-Technische Bundesanstalt, Braunschweig and Berlin, Berlin (Germany)

2008-10-15

For many applications in radiometry, spectroscopy or astrophysics, absolute measurement of radiant power with low uncertainty is essential. Cryogenic electrical substitution radiometers (ESRs) are regarded as the highest-accuracy primary standard detector in radiometry, from the infrared to the ultraviolet region; in combination with tuneable monochromatized synchrotron radiation from electron storage rings, their range of operation has been extended to the soft x-ray region. ESRs are absolute thermal detectors, based on the equivalence of electrical power and radiant power that can be traced back to electrical SI units and be measured with low uncertainties. Their core piece is a cavity absorber, which is typically made of copper to achieve a short response time suitable for use with synchrotron radiation. At higher photon energies, the use of copper prevents the operation of ESRs due to increasing transmittance. A new absorber design for hard x-rays has been developed at the laboratory of the Physikalisch-Technische Bundesanstalt (PTB) at the electron storage ring BESSY II. The Monte Carlo simulation code Geant4 was applied to optimize its absorptance for photon energies of up to 60 keV, resulting in a cavity absorber with a gold base and a cylindrical shell made of copper, in combination with a thermal sensitivity of around 150 mK {mu}W{sup -1} and a time constant of less than 3 min, which is short compared with the lifetime of many hours for the storage ring current. The measurement of the radiant power of monochromatized synchrotron radiation was achieved with relative standard uncertainties of less than 0.2%, covering the entire photon energy range of three beamlines from 50 eV to 60 keV. Monochromatized synchrotron radiation of high spectral purity was used to calibrate silicon photodiodes against the ESR for photon energies up to 60 keV with relative standard uncertainties below 0.3%. (authors)

Cryogenic radiometry in the hard x-ray range

Science.gov (United States)

Gerlach, M.; Krumrey, M.; Cibik, L.; Müller, P.; Rabus, H.; Ulm, G.

2008-10-01

For many applications in radiometry, spectroscopy or astrophysics, absolute measurement of radiant power with low uncertainty is essential. Cryogenic electrical substitution radiometers (ESRs) are regarded as the highest-accuracy primary standard detector in radiometry, from the infrared to the ultraviolet region; in combination with tuneable monochromatized synchrotron radiation from electron storage rings, their range of operation has been extended to the soft x-ray region. ESRs are absolute thermal detectors, based on the equivalence of electrical power and radiant power that can be traced back to electrical SI units and be measured with low uncertainties. Their core piece is a cavity absorber, which is typically made of copper to achieve a short response time suitable for use with synchrotron radiation. At higher photon energies, the use of copper prevents the operation of ESRs due to increasing transmittance. A new absorber design for hard x-rays has been developed at the laboratory of the Physikalisch-Technische Bundesanstalt (PTB) at the electron storage ring BESSY II. The Monte Carlo simulation code Geant4 was applied to optimize its absorptance for photon energies of up to 60 keV, resulting in a cavity absorber with a gold base and a cylindrical shell made of copper, in combination with a thermal sensitivity of around 150 mK µW-1 and a time constant of less than 3 min, which is short compared with the lifetime of many hours for the storage ring current. The measurement of the radiant power of monochromatized synchrotron radiation was achieved with relative standard uncertainties of less than 0.2%, covering the entire photon energy range of three beamlines from 50 eV to 60 keV. Monochromatized synchrotron radiation of high spectral purity was used to calibrate silicon photodiodes against the ESR for photon energies up to 60 keV with relative standard uncertainties below 0.3%.

Achromatic nested Kirkpatrick–Baez mirror optics for hard X-ray nanofocusing

International Nuclear Information System (INIS)

Liu, Wenjun; Ice, Gene E.; Assoufid, Lahsen; Liu, Chian; Shi, Bing; Khachatryan, Ruben; Qian, Jun; Zschack, Paul; Tischler, Jonathan Z.; Choi, J.-Y.

2011-01-01

A nested Kirkpatrick–Baez mirror pair has been designed, fabricated and tested for achromatic nanofocusing synchrotron hard X-rays. The prototype system achieved a FWHM focal spot of about 150 nm in both horizontal and vertical directions. The first test of nanoscale-focusing Kirkpatrick–Baez (KB) mirrors in the nested (or Montel) configuration used at a hard X-ray synchrotron beamline is reported. The two mirrors are both 40 mm long and coated with Pt to produce a focal length of 60 mm at 3 mrad incident angle, and collect up to a 120 µm by 120 µm incident X-ray beam with maximum angular acceptance of 2 mrad and a broad bandwidth of energies up to 30 keV. In an initial test a focal spot of about 150 nm in both horizontal and vertical directions was achieved with either polychromatic or monochromatic beam. The nested mirror geometry, with two mirrors mounted side-by-side and perpendicular to each other, is significantly more compact and provides higher demagnification than the traditional sequential KB mirror arrangement. Ultimately, nested mirrors can focus larger divergence to improve the diffraction limit of achromatic optics. A major challenge with the fabrication of the required mirrors is the need for near-perfect mirror surfaces near the edge of at least one of the mirrors. Special polishing procedures and surface profile coating were used to preserve the mirror surface quality at the reflecting edge. Further developments aimed at achieving diffraction-limited focusing below 50 nm are underway

Synchrotron x-ray reflectivity study of oxidation/passivation of copper and silicon

International Nuclear Information System (INIS)

Chu, Y.; Nagy, Z.; Parkhutik, V.; You, H.

1999-01-01

Synchrotron x-ray-scattering technique studies of copper and silicon electrochemical interfaces are reported. These two examples illustrate the application of synchrotron x-ray techniques for oxidation, passivation, and dissolution of metals and semiconductors

Synchrotron x-ray reflectivity study of oxidation/passivation of copper and silicon.

Energy Technology Data Exchange (ETDEWEB)

Chu, Y.; Nagy, Z.; Parkhutik, V.; You, H.

1999-07-21

Synchrotron x-ray-scattering technique studies of copper and silicon electrochemical interfaces are reported. These two examples illustrate the application of synchrotron x-ray techniques for oxidation, passivation, and dissolution of metals and semiconductors.

Polarization and dipole effects in hard X-ray photoelectron spectroscopy

Energy Technology Data Exchange (ETDEWEB)

Novak, M. [Universite Libre de Bruxelles, Service de Metrologie Nucleaire (CP 165/84), 50 av. F. D. Roosevelt, B-1050 Brussels (Belgium); Pauly, N., E-mail: nipauly@ulb.ac.be [Universite Libre de Bruxelles, Service de Metrologie Nucleaire (CP 165/84), 50 av. F. D. Roosevelt, B-1050 Brussels (Belgium); Dubus, A. [Universite Libre de Bruxelles, Service de Metrologie Nucleaire (CP 165/84), 50 av. F. D. Roosevelt, B-1050 Brussels (Belgium)

2012-03-15

Highlights: Black-Right-Pointing-Pointer X-rays are unpolarized or linearly polarized. Black-Right-Pointing-Pointer A difference of polarization implies a variation in path travelled by the photoelectrons. Black-Right-Pointing-Pointer We show the influence of the polarization on the partial intensity distributions. Black-Right-Pointing-Pointer We also point out the influence of the dipole approximation. Black-Right-Pointing-Pointer We use Monte Carlo simulations. - Abstract: Hard X-ray photoelectron spectroscopy (HXPS) using X-rays in the 1.5-15 keV energy range generated by synchrotron sources becomes an increasingly important analysis technique due to its potential for bulk sensitive measurements. However, besides their high energy, another characteristic of photons generated by synchrotron sources is their linear polarization while X-rays from Al K{alpha} or Mg K{alpha} for instance are unpolarized. This difference implies a possible variation in total path travelled by the photoelectrons generated by the X-rays inside the medium and consequently a modification of the resulting spectrum shape. We show the influence of the polarization on the partial intensity distributions, namely the number of electrons escaping after n inelastic scattering events, for photoelectron with energies of 0.5, 1, 2, 3, 4 and 5 keV and originating from Si 1s{sub 1/2}, Cu 1s{sub 1/2}, Cu 2p{sub 3/2}, Au 4d{sub 3/2} and Au 4f{sub 7/2} subshells. Moreover, we point out the influence of the dipole approximation leading to an underestimation of the partial intensity distributions due to the neglect of the forward-backward asymmetry of the angular photoelectron distribution.

Sub-100 nm hard X-ray microbeam generation with Fresnel zone plate optics

CERN Document Server

Takano, H; Takeuchi, A

2003-01-01

A hard X-ray focusing test of a Fresnel zone plate has been performed with a synchrotron radiation source at the undulator beamline 20XU of SPring-8. Fresnel zone plate with a radius of 150 mu m, and an outermost zone width of 100 nm was used for the X-ray focusing device. The 248-m-long beamline provides fully coherent illumination for the focusing device. The focused beam evaluated by the knife-edge-scan method and scanning microscope test using test charts. Nearly diffraction- limited focusing with a size of 120 nm was achieved for the first-order diffraction at 10 keV X-ray. Evaluation for the third order diffraction was also performed at 8 keV X-ray, and a focal size of 50 m has been obtained. (author)

Synchrotron X-ray PIV Technique for Measurement of Blood Flow Velocity

International Nuclear Information System (INIS)

Kim, Guk Bae; Lee, Sang Joon; Je, Jung Ho

2007-01-01

Synchrotron X-ray micro-imaging method has been used to observe internal structures of various organisms, industrial devices, and so on. However, it is not suitable to see internal flows inside a structure because tracers typically employed in conventional optical flow visualization methods cannot be detectable with the X-ray micro-imaging method. On the other hand, a PIV (particle image velocimetry) method which has recently been accepted as a reliable quantitative flow visualization technique can extract lots of flow information by applying digital image processing techniques However, it is not applicable to opaque fluids such as blood. In this study, we combined the PIV method and the synchrotron X-ray micro-imaging technique to compose a new X-ray PIV technique. Using the X-ray PIV technique, we investigated the optical characteristics of blood for a coherent synchrotron X-ray beam and quantitatively visualized real blood flows inside an opaque tube without any contrast media. The velocity field information acquired would be helpful for investigating hemorheologic characteristics of the blood flow

DOE/DMS workshop on future synchrotron VUV and x-ray beam Lines

International Nuclear Information System (INIS)

Green, P.H.

1992-03-01

This document contains an overview of the participating DOE Laboratory beam line interests and the projected science to be addressed on these beam lines, both at new and existing synchrotron facilities. The scientific programs associated with present and planned synchrotron research by DOE Laboratories are discussed in chapters titled ''VUV and Soft X-Ray Research'' and ''Hard X-Ray Research.'' This research encompasses a broad range of the nation's scientific and technical research needs from fundamental to applied, in areas including environmental, biological, and physical sciences; new materials; and energy-related technologies. The projected cost of this proposed construction has been provided in tabular form using a uniform format so that anticipated DOE and outside funding agency contributions for construction and for research and development can be determined. The cost figures are, of course, subject to uncertainties of detailed design requirements and the availability of facility-designed generic components and outside vendors. The report also contains a compendium (as submitted by the beam line proposers) of the design capabilities, the anticipated costs, and the scientific programs of projected beam line construction at the four synchrotron facilities. A summary of the projected cost of these beam lines to be requested of DOE is compiled

A synchrotron radiation facility for x-ray astronomy

DEFF Research Database (Denmark)

Hall, C.J.; Lewis, R.A.; Christensen, Finn Erland

1997-01-01

A proposal for an x-ray optics test facility based at a synchrotron radiation source is presented. The facility would incorporate a clean preparation area, and a large evacuable test area. The advantages of using a synchrotron as the source of the test radiation are discussed. These include the a...

NuSTAR Hard X-Ray Observation of the Gamma-Ray Binary Candidate HESS J1832–093

DEFF Research Database (Denmark)

Mori, Kaya; Gotthelf, E. V.; Hailey, Charles J.

2017-01-01

−093, is detected up to ~30 keV and is well-described by an absorbed power-law model with a best-fit photon index . A re-analysis of archival Chandra and XMM-Newton data finds that the long-term X-ray flux increase of XMMU J183245−0921539 is (90% C.L.), much less than previously reported. A search for a pulsar spin...... of XMMU J183245−0921539 are most consistent with a non-accreting binary generating synchrotron X-rays from particle acceleration in the shock formed as a result of the pulsar and stellar wind collision. We also report on three nearby hard X-ray sources, one of which may be associated with diffuse emission...

Hard X-ray imaging with a slat collimated telescope

International Nuclear Information System (INIS)

Lu Zhuguo; Kotov, Yu.D.; Suslov, A.Yu.

1995-01-01

Imaging experiments with a slat collimated hard X-ray telescope are described in this paper demonstrating the feasibility of the direct demodulation imaging method used in hard X-ray scanning modulation experiments. On 25 September 1993 an X-ray raster scan observation of Cyg X-1 was performed in a balloon flight with the hard X-ray telescope HAPI-4. An experiment to image radioactive X-ray sources was performed in the laboratory before. In both experiments the expected X-ray images were obtained, confirming the imaging capability of this method. (orig.)

A multiple CCD X-ray detector and its first operation with synchrotron radiation X-ray beam

CERN Document Server

Suzuki, M; Kumasaka, T; Sato, K; Toyokawa, H; Aries, I F; Jerram, P A; Ueki, T

1999-01-01

A 4x4 array structure of 16 identical CCD X-ray detector modules, called the multiple CCD X-ray detector system (MCCDX), was submitted to its first synchrotron radiation experiment at the protein crystallography station of the RIKEN beamline (BL45XU) at the SPring-8 facility. An X-ray diffraction pattern of cholesterol powder was specifically taken in order to investigate the overall system performance.

Synchrotron-based X-ray microscopic studies for bioeffects of nanomaterials.

Science.gov (United States)

Zhu, Ying; Cai, Xiaoqing; Li, Jiang; Zhong, Zengtao; Huang, Qing; Fan, Chunhai

2014-04-01

There have been increasing interests in studying biological effects of nanomaterials, which are nevertheless faced up with many challenges due to the nanoscale dimensions and unique chemical properties of nanomaterials. Synchrotron-based X-ray microscopy, an advanced imaging technology with high spatial resolution and excellent elemental specificity, provides a new platform for studying interactions between nanomaterials and living systems. In this article, we review the recent progress of X-ray microscopic studies on bioeffects of nanomaterials in several living systems including cells, model organisms, animals and plants. We aim to provide an overview of the state of the art, and the advantages of using synchrotron-based X-ray microscopy for characterizing in vitro and in vivo behaviors and biodistribution of nanomaterials. We also expect that the use of a combination of new synchrotron techniques should offer unprecedented opportunities for better understanding complex interactions at the nano-biological interface and accounting for unique bioeffects of nanomaterials. Synchrotron-based X-ray microscopy is a non-destructive imaging technique that enables high resolution spatial mapping of metals with elemental level detection methods. This review summarizes the current use and perspectives of this novel technique in studying the biology and tissue interactions of nanomaterials. Copyright © 2014 Elsevier Inc. All rights reserved.

Broadband Correlations Provide Evidence for Synchrotron Self-Compton X-rays from the Black Hole Binary GX 339-4

International Nuclear Information System (INIS)

Coriat, M.; Corbel, S.; Buxton, M. M.; Baylin, C. D.

2009-01-01

GX 339-4 has been one of the key sources for unravelling the accretion ejection coupling in accreting stellar mass black holes. After a long period of quiescence between 1999 and 2002, GX 339-4 underwent a series of 4 outbursts that have been intensively observed by many ground based observatories (radio/infrared/optical) and satellites (X-rays). Here, we present some specific results of these broad band observational campaigns, focusing on the optical-infrared/X-ray flux correlations over the four outbursts. Thanks to our extensive data-set, we found a strong OIR/X-ray correlation over four decades with the presence of a break in the correlation index. These results seem to favour a synchrotron self-Compton origin for the X-ray emission in GX 339-4 during the hard state and could also provide an indirect detection of the break frequency in the synchrotron spectrum of the compact jets.

Parallel beam microradiography of dental hard tissue using synchrotron radiation and X-ray image magnification

International Nuclear Information System (INIS)

Takagi, S.; Chow, L.C.; Brown, W.E.; Dobbyn, R.C.; Kuriyama, M.

1984-01-01

A novel technique utilizing a highly parallel beam of monochromatic synchrotron radiation combined with X-ray image magnification has been used to obtain microradiographs of caries lesions in relatively thick tooth sections. Preliminary results reveal structural features not previously reported. This technique holds the promise of allowing one to follow the structural changes accompanying the formation, destruction and chemical repair of mineralized tissue in real time. (orig.)

Sub-micron Hard X-ray Fluorescence Imaging of Synthetic Elements

Science.gov (United States)

Jensen, Mark P.; Aryal, Baikuntha P.; Gorman-Lewis, Drew; Paunesku, Tatjana; Lai, Barry; Vogt, Stefan; Woloschak, Gayle E.

2013-01-01

Synchrotron-based X-ray fluorescence microscopy (SXFM) using hard X-rays focused into sub-micron spots is a powerful technique for elemental quantification and mapping, as well as microspectroscopic measurement such as μ-XANES (X-ray absorption near edge structure). We have used SXFM to image and simultaneously quantify the transuranic element plutonium at the L3 or L2 edge as well as lighter biologically essential elements in individual rat pheochromocytoma (PC12) cells after exposure to the long-lived plutonium isotope 242Pu. Elemental maps reveal that plutonium localizes principally in the cytoplasm of the cells and avoids the cell nucleus, which is marked by the highest concentrations of phosphorus and zinc, under the conditions of our experiments. The minimum detection limit under typical acquisition conditions for an average 202 μm2 cell is 1.4 fg Pu/cell or 2.9 × 10−20 moles Pu/μm2, which is similar to the detection limit of K-edge SXFM of transition metals at 10 keV. Copper electron microscopy grids were used to avoid interference from gold X-ray emissions, but traces of strontium present in naturally occurring calcium can still interfere with plutonium detection using its Lα X-ray emission. PMID:22444530

Application of synchrotron radiation to X-ray interferometry

Energy Technology Data Exchange (ETDEWEB)

Hart, M [King' s Coll., London (UK). Wheatstone Physics Lab.

1980-05-01

X-ray interferometry has been attempted with synchrotron radiation at Hamburg and at Orsay. Experiments will start this year at the Storage Ring Source at Daresbury. This review covers work which has already been completed and outlines the likely trends in phase sensitive X-ray polarimetry, high resolution spectroscopy (including real and imaginary-part EXAFS) and novel experiments with many-beam-case interferometers.

Fast synchrotron X-ray tomography study of the rod packing structures

Energy Technology Data Exchange (ETDEWEB)

Zhang Xiaodan; Xia Chengjie; Sun Haohua; Wang Yujie [Department of Physics, Shanghai Jiao Tong University, 800 Dong Chuan Road, Shanghai 200240 (China)

2013-06-18

We present a fast synchrotron X-ray tomography study of the packing structures of rods under tapping. Utilizing the high flux of the X-rays generated from the third-generation synchrotron source, we can complete a tomography scan within several seconds, after which the three-dimensional (3D) packing structure can be obtained for the subsequent structural analysis. Due to the high-energy nature of the X-ray beam, special image processing steps including image phase-retrieval has been implemented. Overall, this study suggests the possibility of acquiring statistically significant static packing structures within a reasonable time scale using high-intensity X-ray sources.

The Ferrara hard X-ray facility for testing/calibrating hard X-ray focusing telescopes

Science.gov (United States)

Loffredo, Gianluca; Frontera, Filippo; Pellicciotta, Damiano; Pisa, Alessandro; Carassiti, Vito; Chiozzi, Stefano; Evangelisti, Federico; Landi, Luca; Melchiorri, Michele; Squerzanti, Stefano

2005-12-01

We will report on the current configuration of the X-ray facility of the University of Ferrara recently used to perform reflectivity tests of mosaic crystals and to calibrate the experiment JEM X aboard Integral. The facility is now located in the technological campus of the University of Ferrara in a new building (named LARIX laboratory= LARge Italian X-ray facility) that includes a tunnel 100 m long with, on the sides, two large experimental rooms. The facility is being improved for determining the optical axis of mosaic crystals in Laue configuration, for calibrating Laue lenses and hard X-ray mirror prototypes.

Computer simulation for synchrotron radiation based X-ray fluorescent microtomography

International Nuclear Information System (INIS)

Deng Biao; Yu Xiaohan; Xu Hongjie

2007-01-01

Synchrotron radiation based fluorescent microtomography (SR-XFMT) is a nondestructive technique for detecting elemental composition and distribution inside a specimen with high spatial resolution and sensitivity, and will be an optional experimental technique at SSRF hard X-ray micro-focusing beamline now under construction. In this paper, the principles and developments of SR-XFMT are briefly introduced. Computer simulation of SR-XFMT experiment is performed. The image of the simulated sample is reconstructed using Filtered Back Projection (FBP), Algebraic Reconstruction Techniques (ART) and modified FBP with absorption correction. The qualities of the reconstructed images are analyzed and compared. The validity of these reconstruction techniques is discussed. (authors)

Characterization of Polycrystalline Materials Using Synchrotron X-ray Imaging and Diffraction Techniques

DEFF Research Database (Denmark)

Ludwig, Wolfgang; King, A.; Herbig, M.

2010-01-01

The combination of synchrotron radiation x-ray imaging and diffraction techniques offers new possibilities for in-situ observation of deformation and damage mechanisms in the bulk of polycrystalline materials. Minute changes in electron density (i.e., cracks, porosities) can be detected using...... propagation based phase contrast imaging, a 3-D imaging mode exploiting the coherence properties of third generation synchrotron beams. Furthermore, for some classes of polycrystalline materials, one may use a 3-D variant of x-ray diffraction imaging, termed x-ray diffraction contrast tomography. X-ray...

X-ray electromagnetic application technology

International Nuclear Information System (INIS)

2011-01-01

The investigating committee aimed at research on electromagnetic fields in functional devices and X-ray fibers for efficient coherent X-ray generation and their material science, high-precision manufacturing, particularly for X-ray electromagnetic application technology from January 2006 to December 2008. In this report, we describe our research results, in particular, on the topics of synchrotron radiation and free-electron laser, Saga Synchrotron Project, X-ray waveguides and waveguide-based lens-less hard-X-ray imaging, X-ray nanofocusing for capillaries and zone plates, dispersion characteristics in photonics crystal consisting of periodic atoms for nanometer waveguides, electromagnetic characteristics of grid structures for scattering fields of nano-meter electromagnetic waves and X-rays, FDTD parallel computing of fundamental scattering and attenuation characteristics of X-ray for medical imaging diagnosis, orthogonal relations of electromagnetic fields including evanescent field in dispersive medium. (author)

A new miniature microchannel plate X-ray detector for synchrotron radiation

International Nuclear Information System (INIS)

Rosemeier, R.G.; Green, R.E. Jr.

1982-01-01

A state-of-the-art microchannel plate detector has been developed which allows real time X-ray imaging of X-ray diffraction as well as radiographic phenomenon. Advantages of the device include a 50 mm X-ray input, length less than 4'', and a weight of less than 1 lb. Since the use of synchrotron radiation is greatly facilitated by the capability of remote viewing of X-ray diffraction or radiographic images in real time, a prototype electro-optical system has been designed which couples the X-ray microchannel plate detector with a solid state television camera. Advantages of the miniature, lightweight, X-ray synchrotron camera include a large 50 mm X-ray input window, an output signal that is available in both analog format for display on a television monitor and in digital format for computer processing, and a completely modular design which allows all the components to be exchanged for other components optimally suited for the desired applications. (orig.)

Investigation of hepatic fibrosis with synchrotron X-ray diffraction enhanced imaging

International Nuclear Information System (INIS)

Li Hui; Beijing Univ., Health Science Center, Beijing; Wang Xueyan; Zhao Tao; Hu Chunhong; Lu Weiyuan; Luo Shuqian; Wang Tailing; Wang Baoen; Zhao Xinyan; Zhu Peiping; Huang Wanxia; Yuan Qingxi; Wang Junyue

2008-01-01

In this paper, imaging investigation of hepatic fibrosis in rats induced by human albumin with hard X-ray diffraction enhanced imaging (DEI) is reported. The experiments were performed at 4W1A beamline of Beijing Synchrotron Radiation Facility (BSRF). The results show that great differences can be observed in DEI images between the normal and diseased rats in different stages of liver fibrosis. The difference can also be revealed by the profile curve and texture measurements on regions of interest. The results show that DEI may be a potential way for diagnosis of hepatic fibrosis. (authors)

A MODEL FOR THE CORRELATION OF HARD X-RAY INDEX WITH EDDINGTON RATIO IN BLACK HOLE X-RAY BINARIES

International Nuclear Information System (INIS)

Qiao, Erlin; Liu, B. F.

2013-01-01

Observations show that there is a positive correlation between the Eddington ratio λ and hard X-ray index Γ for λ ∼> 0.01, and there is an anti-correlation between λ and Γ for λ ∼ bol /L Edd ). In this work, we theoretically investigate the correlation between Γ and λ within the framework of a disk-corona model. We improve the model by taking into account all cooling processes, including synchrotron and self-Compton radiations in the corona, Comptonization of the soft photons from the underlying accretion disk, and the bremsstrahlung radiations. Presuming that the coronal flow above the disk can reach up to the 0.1 Eddington rate at the outer region, we calculate the structure of the two-phase accretion flows and the emergent spectra for accretion rates from 0.003 to 0.1. We find that at accretion rates larger than bsim0.01 Eddington rate, a fraction of coronal gas condenses into the disk and an inner disk can be sustained by condensation. In this case, the X-ray emission is dominated by the scattering of the soft photon from the underlying disk in the corona. The emission from the inner disk and corona can produce the positive correlation between λ and Γ. While at accretion rates lower than bsim0.01 Eddington accretion rate, the inner disk vanishes completely by evaporation, and the accretion is dominated by advection-dominated accretion flows (ADAFs), in which the X-ray emission is produced by the Comptonization of the synchrotron and bremsstrahlung photons of ADAF itself. The emission from ADAFs can produce the anti-correlation between λ and Γ. We show that our model can roughly explain the observed evolution of Γ 3-25keV with L 0.5-25keV /L Edd for the black hole X-ray transient H1743–322 in the decay of 2003 from the thermal-dominated state to low/hard state.

Nanofocusing parabolic refractive x-ray lenses

International Nuclear Information System (INIS)

Schroer, C.G.; Kuhlmann, M.; Hunger, U.T.; Guenzler, T.F.; Kurapova, O.; Feste, S.; Frehse, F.; Lengeler, B.; Drakopoulos, M.; Somogyi, A.; Simionovici, A.S.; Snigirev, A.; Snigireva, I.; Schug, C.; Schroeder, W.H.

2003-01-01

Parabolic refractive x-ray lenses with short focal distance can generate intensive hard x-ray microbeams with lateral extensions in the 100 nm range even at a short distance from a synchrotron radiation source. We have fabricated planar parabolic lenses made of silicon that have a focal distance in the range of a few millimeters at hard x-ray energies. In a crossed geometry, two lenses were used to generate a microbeam with a lateral size of 380 nm by 210 nm at 25 keV in a distance of 42 m from the synchrotron radiation source. Using diamond as the lens material, microbeams with a lateral size down to 20 nm and below are conceivable in the energy range from 10 to 100 keV

Light source for synchrotron radiation x-ray topography study at Beijing Synchrotron Radiation Laboratory (BSRL)

International Nuclear Information System (INIS)

Zhao Jiyong; Jiang Jianhua; Tian Yulian

1992-01-01

Characteristics of the synchrotron radiation source for X-ray topography study at Beijing Synchrotron Radiation Laboratory (BSRL) is described, local geometrical resolution of topographies is discussed, and the diffracting intensities of white beam topography is given

An x-ray microprobe using focussing optics with a synchrotron radiation source

International Nuclear Information System (INIS)

Thompson, A.C.; Underwood, J.H.; Wu, Y.; Giauque, R.D.

1989-01-01

An x-ray microprobe can be used to produce maps of the concentration of elements in a sample. Synchrotron radiation provides x-ray beams with enough intensity and collimation to make possible elemental images with femtogram sensitivity. The use of focussing x-ray mirrors made from synthetic multilayers with a synchrotron x-ray beam allows beam spot sizes of less than 10 μm /times/ 10 μm to be produced. Since minimal sample preparation is required and a vacuum environment is not necessary, there will be a wide variety of applications for such microprobes. 8 refs., 6 figs

Hard X-ray studies on the Castor tokamak

International Nuclear Information System (INIS)

Mlynar, J.

1990-04-01

The electron runaway processes in tokamaks are discussed with regard to hard X radiation measurements. The origin and confinement of runaway electrons, their bremsstrahlung spectra and the influence of lower hybrid current drive on the distribution of high-energy electrons are analyzed for the case of the Castor tokamak. The hard X-ray spectrometer designed for the Castor tokamak is also described and preliminary qualitative results of hard X-ray measurements are presented. The first series of integral measurements made it possible to map the azimuthal dependence of the hard X radiation

Hard-x-ray phase-imaging microscopy using the self-imaging phenomenon of a transmission grating

International Nuclear Information System (INIS)

Yashiro, Wataru; Harasse, Sebastien; Momose, Atsushi; Takeuchi, Akihisa; Suzuki, Yoshio

2010-01-01

We report on a hard-x-ray imaging microscope consisting of a lens, a sample, and a transmission grating. After the theoretical framework of self-imaging phenomenon by the grating in the system is presented, equations for the electric field on the image plane are derived for ideal and real lenses and an equation for the intensity on the image plane for partially coherent illumination is derived. The equations are simple and similar to those applying to a projection microscope consisting of a transmission grating except that there is no defocusing effect, regardless of whether the grating is in front of or behind the lens. This means that x-ray phase-imaging microscopy can be done without the defocusing effect. It is also shown that, by resolving the self-image on the image plane, high-sensitive x-ray phase-imaging microscopy can be attained without degradation in the spatial resolution due to diffraction by the grating. Experimental results obtained using partially coherent illumination from a synchrotron x-ray source confirm that hard-x-ray phase-imaging microscopy can be quantitatively performed with high sensitivity and without the spatial resolution degradation.

Black hole and neutron star soft X-ray transients: a hard X-ray view of their outbursts

International Nuclear Information System (INIS)

Yu, W.

2004-01-01

The RXTE public observations of the outbursts of black hole soft X-ray transients XTE J1550-564, XTE J1859+226, 4U 1630-47, XTE J1118+480, XTE J1650-500, and the neutron star soft X-ray transients 4U 1608-52, Aquila X-1, including a variable 'persistent' neutron star low mass X-ray binary 4U 1705-44, are summarized in this paper. The hard X-ray view of those outbursts, which is quite different from that of the soft X-ray band, suggests that there are several types of outbursts which result in different hard X-ray outburst profile - the outburst profiles are energy dependent. One type is the low/hard state outbursts, the other type is the outburst showing transitions from the low/hard state to the high/soft state, or to the intermediate or to the very high state. The later has an initial low/hard state, introducing the phenomena that the hard X-ray precedes the soft X-ray in the outburst rise. Such outbursts in XTE J1550-564, Aql X-1 and 4U 1705-44 support a two-accretion-flow model which involves one Keplerian disk flow and one sub-Keplerian flow for the initial outburst rise

Stabilization of synchrotron radiation x-ray beam by MOSTAB

CERN Document Server

Kudo, T P; Tanida, H; Furukawa, Y; Hirono, T; Ishikawa, T; Nishino, Y

2003-01-01

Monochromator stabilization (MOSTAB) is a feedback control system to stabilize an x-ray beam of synchrotron radiation. It applies a feedback voltage to a piezo electric transducer attached to a double-crystal monochromator. We developed MOSTAB modules and examined their performances using SPring-8 beamlines. The x-ray beam position stabilization using MOSTAB was realized simultaneously with the x-ray beam intensity stabilization. As an example of its application, we performed EXAFS measurement with MOSTAB. (author)

X-ray beam splitting design for concurrent imaging at hard X-ray FELs and synchrotron facilities

Energy Technology Data Exchange (ETDEWEB)

Oberta, P., E-mail: peter.oberta@rigaku.com [Institute of Physics, Academy of Sciences of the Czech Republic, v.v.i., Na Slovance 2, Praha 8, CZ-18221 (Czech Republic); Rigaku, Novodvorská 994, Praha 4, CZ-14221 (Czech Republic); Mokso, R. [Swiss Light Source, Paul Scherrer Institut, Villigen, CH-5232 Villigen (Switzerland)

2013-11-21

A new configuration of diffractive–refractive optics for beam splitting is investigated. The set-up can be applied to perform imaging with two beams simultaneously. It brings advantages toward dynamic studies using image guided diffraction or fluorescence spectroscopy. The optimal energy range of operation for the beam-splitter is between 7 keV and 24 keV, reaching best efficiency at an energy of 10 keV. Due to the long focusing distances (several tens of meters) created by the diffractive–refractive optics and the higher refraction efficiency in the softer energy range, the presented set-ups are ideal for hard X-ray FEL sources.

Three-dimensional monochromatic x-ray computed tomography using synchrotron radiation

Science.gov (United States)

Saito, Tsuneo; Kudo, Hiroyuki; Takeda, Tohoru; Itai, Yuji; Tokumori, Kenji; Toyofuku, Fukai; Hyodo, Kazuyuki; Ando, Masami; Nishimura, Katsuyuki; Uyama, Chikao

1998-08-01

We describe a technique of 3D computed tomography (3D CT) using monochromatic x rays generated by synchrotron radiation, which performs a direct reconstruction of a 3D volume image of an object from its cone-beam projections. For the development, we propose a practical scanning orbit of the x-ray source to obtain complete 3D information on an object, and its corresponding 3D image reconstruction algorithm. The validity and usefulness of the proposed scanning orbit and reconstruction algorithm were confirmed by computer simulation studies. Based on these investigations, we have developed a prototype 3D monochromatic x-ray CT using synchrotron radiation, which provides exact 3D reconstruction and material-selective imaging by using the K-edge energy subtraction technique.

Imaging characters of the lung cancer phantoms under the simulative clinical condition performed with hard X-ray in-line holography

International Nuclear Information System (INIS)

Zhang, J; Chen, Y; Li, G; Jiang, X

2013-01-01

The simulative lung cancer tissues under the approximate clinical condition were imaged using in-line holography method with 35 keV synchrotron radiation hard X-ray. The millimeter scale simulative cancer phantoms showed adequate contrast to lung tissues in our experiment. It demonstrates that in-line holography method with synchrotron radiation hard X-ray promises to be a potential sensitive method for the early detection of lung cancer. The image contrast, standard deviation (SD) and normalized standard deviation (NSD) of different areas were calculated. It shows that the traditional method of contrast calculation does not always give a convincible result in image judgment; a standard deviation map of image taken with a proper distance of sample to detector (DSD) will correspond well to the projecting image and supply effective assistance in diagnostic judgment.

Thermal management of next-generation contact-cooled synchrotron x-ray mirrors

Energy Technology Data Exchange (ETDEWEB)

Khounsary, A.

1999-10-29

In the past decade, several third-generation synchrotrons x-ray sources have been constructed and commissioned around the world. Many of the major problems in the development and design of the optical components capable of handling the extremely high heat loads of the generated x-ray beams have been resolved. It is expected, however, that in the next few years even more powerful x-ray beams will be produced at these facilities, for example, by increasing the particle beam current. In this paper, the design of a next generation of synchrotron x-ray mirrors is discussed. The author shows that the design of contact-cooled mirrors capable of handing x-ray beam heat fluxes in excess of 500 W/mm{sup 2} - or more than three times the present level - is well within reach, and the limiting factor is the thermal stress rather then thermally induced slope error.

NuSTAR Hard X-ray Survey of the Galactic Center Region. I. Hard X-ray Morphology and Spectroscopy of the Diffuse Emission

DEFF Research Database (Denmark)

Mori, Kaya; Hailey, Charles J.; Krivonos, Roman

2015-01-01

We present the first sub-arcminute images of the Galactic Center above 10 keV, obtained with NuSTAR. NuSTAR resolves the hard X-ray source IGR J17456-2901 into non-thermal X-ray filaments, molecular clouds, point sources, and a previously unknown central component of hard X-ray emission (CHXE). Nu...

X-ray phase contrast imaging: From synchrotrons to conventional sources

International Nuclear Information System (INIS)

Olivo, A.; Castelli, E.

2014-01-01

Phase-based approaches can revolutionize X-ray imaging and remove its main limitation: poor image contrast arising from low attenuation differences. They exploit the unit decrement of the real part of the refractive index, typically 1000 times larger than the imaginary part driving attenuation. This increases the contrast of all details, and enables the detection of features classically considered 'X-ray invisible'. Following pioneering experiments dating back to the mid-sixties, X-ray phase contrast imaging 'exploded' in the mid-nineties, when third generation synchrotron sources became more widely available. Applications were proposed in fields as diverse as material science, palaeontology, biology, food science, cultural heritage preservation, and many others. Among these applications, medicine has been constantly considered the most important; among medical applications, mammography is arguably the one that attracted most attention. Applications to mammography were pioneered by the SYRMEP (SYnchrotron Radiation for MEdical Physics) group in Trieste, which was already active in the area through a combination of innovative ways to do imaging at synchrotrons and development of novel X-ray detectors. This pioneering phase led to the only clinical experience of phase contrast mammography on human patients, and spawned a number of ideas as to how these advances could be translated into clinical practice.

Extragalactic Hard X-ray Surveys: From INTEGRAL to Simbol-X

Science.gov (United States)

Paltani, S.; Dwelly, T.; Walter, R.; McHardy, I. M.; Courvoisier, T. J.-L.

2009-05-01

We present some results of the deepest extragalactic survey performed by the INTEGRAL satellite. The fraction of very absorbed AGN is quite large. The sharp decrease in the absorption fraction with X-ray luminosity observed at lower-energy X-rays is not observed. The current lack of truly Compton-thick objects, with an upper limit of 14% to the size of this population, is just compatible with recent modeling of the cosmic X-ray background. We also study the prospects for a future hard X-ray serendipitous survey with Simbol-X. We show that Simbol-X will easily detect a large number of serendipitous AGN, allowing us to study the evolution of AGN up to redshifts about 2, opening the door to the cosmological study of hard X-ray selected AGN, which is barely possible with existing satellites like Swift and INTEGRAL.

High-energy synchrotron X-ray radiography of shock-compressed materials

Science.gov (United States)

Rutherford, Michael E.; Chapman, David J.; Collinson, Mark A.; Jones, David R.; Music, Jasmina; Stafford, Samuel J. P.; Tear, Gareth R.; White, Thomas G.; Winters, John B. R.; Drakopoulos, Michael; Eakins, Daniel E.

2015-06-01

This presentation will discuss the development and application of a high-energy (50 to 250 keV) synchrotron X-ray imaging method to study shock-compressed, high-Z samples at Beamline I12 at the Diamond Light Source synchrotron (Rutherford-Appleton Laboratory, UK). Shock waves are driven into materials using a portable, single-stage gas gun designed by the Institute of Shock Physics. Following plate impact, material deformation is probed in-situ by white-beam X-ray radiography and complimentary velocimetry diagnostics. The high energies, large beam size (13 x 13 mm), and appreciable sample volumes (~ 1 cm3) viable for study at Beamline I12 compliment existing in-house pulsed X-ray capabilities and studies at the Dynamic Compression Sector. The authors gratefully acknowledge the ongoing support of Imperial College London, EPSRC, STFC and the Diamond Light Source, and AWE Plc.

Multi-spacecraft observations of solar hard X-ray bursts

International Nuclear Information System (INIS)

Kane, S.R.

1981-01-01

The role of multi-spacecraft observations in solar flare research is examined from the point of view of solar hard X-ray bursts and their implications with respect to models of the impulsive phase. Multi-spacecraft measurements provide a stereoscopic view of the flare region, and hence represent the only direct method of measuring directivity of X-rays. In absence of hard X-ray imaging instruments with high spatial and temporal resolution, multi-spacecraft measurements provide the only means of determining the radial (vertical) structure of the hard X-ray source. This potential of the multi-spacecraft observations is illustrated with an analysis of the presently available observations of solar hard X-ray bursts made simultaneously by two or more of the following spacecraft: International Sun Earth Explorer-3 (ISEE-3), Pioneer Venus Orbiter (PVO), Helios-B and High Energy Astrophysical Observatory-A (HEAO-A). In particular, some conclusions have been drawn about the spatial structure and directivity of 50-100 keV X-rays from impulsive flares. Desirable features of future multi-spacecraft missions are briefly discussed followed by a short description of the hard X-ray experiment on the International Solar Polar Mission which has been planned specifically for multi-spacecraft observations of the Sun. (orig.)

Toward a fourth-generation X-ray source

International Nuclear Information System (INIS)

Monction, D. E.

1999-01-01

The field of synchrotron radiation research has grown rapidly over the last 25 years due to both the push of the accelerator and magnet technology that produces the x-ray beams and the pull of the extraordinary scientific research that is possible with them. Three successive generations of synchrotrons radiation facilities have resulted in beam brilliances 11 to 12 orders of magnitude greater than the standard laboratory x-ray tube. However, greater advances can be easily imagined given the fact that x-ray beams from present-day facilities do not exhibit the coherence or time structure so familiar with the optical laser. Theoretical work over the last ten years or so has pointed to the possibility of generating hard x-ray beams with laser-like characteristics. The concept is based on self-amplified spontaneous emission (SASE) in flee-electron lasers. A major facility of this type based upon a superconducting linac could produce a cost-effective facility that spans wave-lengths from the ultraviolet to the hard x-ray regime, simultaneously servicing large numbers experimenters from a wide range of disciplines. As with each past generation of synchrotrons facilities, immense new scientific opportunities would result from fourth-generation sources.

Fast photoconductor CdTe detectors for synchrotron x-ray studies

International Nuclear Information System (INIS)

Yoo, Sung Shik; Faurie, J.P.; Huang Qiang; Rodricks, B.

1993-09-01

The Advanced Photon Source will be that brightest source of synchrotron x-rays when it becomes operational in 1996. During normal operation, the ring will be filled with 20 bunches of positrons with an interbunch spacing of 177 ns and a bunch width of 119 ps. To perform experiments with x-rays generated by positrons on these time scales one needs extremely high speed detectors. To achieve the necessary high speed, we are developing MBE-grown CdTe-base photoconductive position sensitive array detectors. The arrays fabricated have 64 pixels with a gap of 100 μm between pixels. The high speed response of the devices was tested using a short pulse laser. X-ray static measurements were performed using an x-ray tube and synchrotron radiation to study the device's response to flux and wavelength changes. This paper presents the response of the devices to some of these tests and discusses different physics aspects to be considered when designing high speed detectors

Applications of synchrotron X-rays in microelectronics industry research

International Nuclear Information System (INIS)

Jordan-Sweet, Jean L.; Detavernier, Christophe; Lavoie, Christian; Mooney, Patricia M.; Toney, Michael F.

2005-01-01

The high flux and density of X-rays produced at synchrotrons provide the microelectronics industry with a powerful probe of the structure and behavior of a wide array of solid materials that are being developed for use in devices of the future. They also are of great use in determining why currently-used materials and processes sometimes fail. This paper describes the X20 X-ray beamline facility operated by IBM at the National Synchrotron Light Source, and presents a series of three industry challenges and results that illustrate the variety of techniques used and problems addressed. The value of this research ranges from solving short-term, technically specific problems to increasing our academic understanding of materials in general. Techniques discussed include high-resolution diffraction, time-resolved diffraction, texture measurements, and grazing-incidence diffraction

Characteristics of hard X-ray double sources in impulsive solar flares

Science.gov (United States)

Sakao, T.; Kosugi, T.; Masuda, S.; Yaji, K.; Inda-Koide, M.; Makishima, K.

1996-01-01

Imaging observations of solar flare hard X-ray sources with the Hard X-ray Telescope (HXT) aboard the Yohkoh satellite have revealed that hard X-ray emissions (greater than 30 ke V) originate most frequently from double sources. The double sources are located on both sides of the magnetic neutral line, suggesting that the bulk of hard X-rays is emitted from footpoints of flaring magnetic loops. We also found that hard X-rays from the double sources are emitted simultaneously within a fraction of second and that the weaker source tends to be located in the stronger magnetic field region, showing a softer spectrum. Physcial implications on the observed characteristics of the hard X-ray double sources are discussed.

Microfocussing of synchrotron X-rays using X-ray refractive lens ...

Indian Academy of Sciences (India)

2014-07-02

Jul 2, 2014 ... together. The first refractive lenses for hard X-rays were fabricated and tested by Snigirev et al [3]. ... using silicon and diamond refractive lens materials [4]. Many groups ... PMMA has lower radiation resistance com- pared to ...

Fracture mechanics by three-dimensional crack-tip synchrotron X-ray microscopy.

Science.gov (United States)

Withers, P J

2015-03-06

To better understand the relationship between the nucleation and growth of defects and the local stresses and phase changes that cause them, we need both imaging and stress mapping. Here, we explore how this can be achieved by bringing together synchrotron X-ray diffraction and tomographic imaging. Conventionally, these are undertaken on separate synchrotron beamlines; however, instruments capable of both imaging and diffraction are beginning to emerge, such as ID15 at the European Synchrotron Radiation Facility and JEEP at the Diamond Light Source. This review explores the concept of three-dimensional crack-tip X-ray microscopy, bringing them together to probe the crack-tip behaviour under realistic environmental and loading conditions and to extract quantitative fracture mechanics information about the local crack-tip environment. X-ray diffraction provides information about the crack-tip stress field, phase transformations, plastic zone and crack-face tractions and forces. Time-lapse CT, besides providing information about the three-dimensional nature of the crack and its local growth rate, can also provide information as to the activation of extrinsic toughening mechanisms such as crack deflection, crack-tip zone shielding, crack bridging and crack closure. It is shown how crack-tip microscopy allows a quantitative measure of the crack-tip driving force via the stress intensity factor or the crack-tip opening displacement. Finally, further opportunities for synchrotron X-ray microscopy are explored.

Hard x-ray to low energy gamma ray spectrum of the Crab Nebula

International Nuclear Information System (INIS)

Jung, G.V.

1986-01-01

The spectrum of the Crab Nebula has been determined in the energy range 10 keV to 5 MeV from the data of the UCSD/MIT Hard-X-ray and Low Energy Gamma Ray Experiment on the first High Energy Astronomy Observatory, HEAO-1. The x-ray to γ-ray portion of the continuous emission from the Crab is indicative of the electron spectrum, its transport through the nebula, and the physical conditions near the shocked interface between the nebular region and the wind which is the physical link between the nebula and the pulsar, NP0532. The power-law dependence of the spectrum found in the lower-energy decade of this observation (10 to 100 keV) is not continued without modification to higher energies. Evidence for this has been accumulating from previous observations in the γ-ray ranges of 1-10 MeV and above 35 MeV. The observations on which this dissertation is based further characterize the spectral change in the 100 keV to 1 MeV region. These observations provide a crucial connection between the x-ray and γ-ray spectrum of the non-pulsed emission of the Crab Nebula. The continuity of this spectrum suggests that the emission mechanism responsible for the non-pulsed γ-rays observed above 35 MeV is of the same origin as the emission at lower energies, i.e. that of synchrotron radiation in the magnetic field of the nebula

Hard X-ray Microscopy with sub 30 nm Spatial Resolution

International Nuclear Information System (INIS)

Tang, M.-T.; Song, Y.-F.; Yin, G.-C.; Chen, J.-H.; Chen, Y.-M.; Liang, Keng S.; Chen, F.-R.; Duewer, F.; Yun Wenbing

2007-01-01

A transmission X-ray microscope (TXM) has been installed at the BL01B beamline at National Synchrotron Radiation Research Center in Taiwan. This state-of-the-art TXM operational in a range 8-11 keV provides 2D images and 3D tomography with spatial resolution 60 nm, and with the Zernike-phase contrast mode for imaging light materials such as biological specimens. A spatial resolution of the TXM better than 30 nm, apparently the best result in hard X-ray microscopy, has been achieved by employing the third diffraction order of the objective zone plate. The TXM has been applied in diverse research fields, including analysis of failure mechanisms in microelectronic devices, tomographic structures of naturally grown photonic specimens, and the internal structure of fault zone gouges from an earthquake core. Here we discuss the scope and prospects of the project, and the progress of the TXM in NSRRC

Development of compact synchrotron light source LUNA for x-ray lithography

International Nuclear Information System (INIS)

Takahashi, M.; Mandai, S.; Hoshi, Y.; Kohno, Y.

1992-01-01

A compact synchrotron light source LUNA has been developed by Ishikawajima-Harima Heavy Industries Co., Ltd. (IHI), especially for x-ray lithography. It consists of a 45-MeV linac as an electron injector and an 800-MeV synchrotron. The peak wavelength of synchrotron radiation is around 10 A. The installation of LUNA was completed in April 1989 at the Tsuchiura Facility of IHI. The synchrotron radiation was first observed in December 1989. A stored beam current of 50 mA at 800 MeV and a lifetime over 1 h have been achieved. At present, experiments are still continuing to increase the stored current and the lifetime. X-ray lithography testing is scheduled to begin in a clean room in this facility. This paper describes the outline of LUNA and the present status

X-ray and synchrotron methods in studies of cultural heritage sites

Energy Technology Data Exchange (ETDEWEB)

Koval’chuk, M. V.; Yatsishina, E. B.; Blagov, A. E.; Tereshchenko, E. Yu., E-mail: elenatereschenko@yandex.ru; Prosekov, P. A.; Dyakova, Yu. A. [National Research Centre “Kurchatov Institute” (Russian Federation)

2016-09-15

X-ray and synchrotron methods that are most widely used in studies of cultural heritage objects (including archaeological sites)—X-ray diffraction analysis, X-ray spectroscopy, and visualization techniques— have been considered. The reported examples show high efficiency and informativeness of natural science studies when solving most diverse problems of archaeology, history, the study of art, museology, etc.

X-ray and synchrotron methods in studies of cultural heritage sites

International Nuclear Information System (INIS)

Koval’chuk, M. V.; Yatsishina, E. B.; Blagov, A. E.; Tereshchenko, E. Yu.; Prosekov, P. A.; Dyakova, Yu. A.

2016-01-01

X-ray and synchrotron methods that are most widely used in studies of cultural heritage objects (including archaeological sites)—X-ray diffraction analysis, X-ray spectroscopy, and visualization techniques— have been considered. The reported examples show high efficiency and informativeness of natural science studies when solving most diverse problems of archaeology, history, the study of art, museology, etc.

A hard X-ray nanoprobe beamline for nanoscale microscopy

Energy Technology Data Exchange (ETDEWEB)

Winarski, Robert P., E-mail: winarski@anl.gov; Holt, Martin V. [Argonne National Laboratory, 9700 South Cass Avenue, Argonne, IL 60441 (United States); Rose, Volker [Argonne National Laboratory, 9700 South Cass Avenue, Argonne, IL 60441 (United States); Fuesz, Peter; Carbaugh, Dean; Benson, Christa; Shu, Deming; Kline, David; Stephenson, G. Brian; McNulty, Ian [Argonne National Laboratory, 9700 South Cass Avenue, Argonne, IL 60441 (United States); Maser, Jörg [Argonne National Laboratory, 9700 South Cass Avenue, Argonne, IL 60441 (United States)

2012-11-01

The Hard X-ray Nanoprobe Beamline is a precision platform for scanning probe and full-field microscopy with 3–30 keV X-rays. A combination of high-stability X-ray optics and precision motion sensing and control enables detailed studies of the internal features of samples with resolutions approaching 30 nm. The Hard X-ray Nanoprobe Beamline (or Nanoprobe Beamline) is an X-ray microscopy facility incorporating diffraction, fluorescence and full-field imaging capabilities designed and operated by the Center for Nanoscale Materials and the Advanced Photon Source at Sector 26 of the Advanced Photon Source at Argonne National Laboratory. This facility was constructed to probe the nanoscale structure of biological, environmental and material sciences samples. The beamline provides intense focused X-rays to the Hard X-ray Nanoprobe (or Nanoprobe) which incorporates Fresnel zone plate optics and a precision laser sensing and control system. The beamline operates over X-ray energies from 3 to 30 keV, enabling studies of most elements in the periodic table, with a particular emphasis on imaging transition metals.

Possibilities and Challenges of Scanning Hard X-ray Spectro-microscopy Techniques in Material Sciences

Directory of Open Access Journals (Sweden)

Andrea Somogyi

2015-06-01

Full Text Available Scanning hard X-ray spectro-microscopic imaging opens unprecedented possibilities in the study of inhomogeneous samples at different length-scales. It gives insight into the spatial variation of the major and minor components, impurities and dopants of the sample, and their chemical and electronic states at micro- and nano-meter scales. Measuring, modelling and understanding novel properties of laterally confined structures are now attainable. The large penetration depth of hard X-rays (several keV to several 10 keV beam energy makes the study of layered and buried structures possible also in in situ and in operando conditions. The combination of different X-ray analytical techniques complementary to scanning spectro-microscopy, such as X-ray diffraction, X-ray excited optical luminescence, secondary ion mass spectrometry (SIMS and nano-SIMS, provides access to optical characteristics and strain and stress distributions. Complex sample environments (temperature, pressure, controlled atmosphere/vacuum, chemical environment are also possible and were demonstrated, and allow as well the combination with other analysis techniques (Raman spectroscopy, infrared imaging, mechanical tensile devices, etc. on precisely the very same area of the sample. The use of the coherence properties of X-rays from synchrotron sources is triggering emerging experimental imaging approaches with nanometer lateral resolution. New fast analytical possibilities pave the way towards statistically significant studies at multi- length-scales and three dimensional tomographic investigations. This paper gives an overview of these techniques and their recent achievements in the field of material sciences.

A synchrotron-based X-ray exposure station for radiation biology experiments

International Nuclear Information System (INIS)

Thompson, A.C.; Blakely, E.A.; Bjornstad, K.A.; Chang, P.Y.; Rosen, C.J.; Schwarz, R.I.

2007-01-01

Synchrotron X-ray sources enable radiation biology experiments that are difficult with conventional sources. A synchrotron source can easily deliver a monochromatic, tunable energy, highly collimated X-ray beam of well-calibrated intensity. An exposure station at beamline 10.3.1 of the Advanced Light Source (ALS) has been developed which delivers a variable energy (5-20 keV) X-ray fan beam with very sharp edges (10-90% in less than 3 μm). A series of experiments have been done with a four-well slide where a stripe (100 μm widex18 mm long) of cells in each well has been irradiated and the dose varied from well to well. With this facility we have begun a series of experiments to study cells adjacent to irradiated cells and how they respond to the damage of their neighbors. Initial results have demonstrated the advantages of using synchrotron radiation for these experiments

A synchrotron-based X-ray exposure station for radiation biology experiments

Energy Technology Data Exchange (ETDEWEB)

Thompson, A.C. [Division of Life Sciences, Lawrence Berkeley National Laboratory, Bld. 50A-6120, Berkeley, CA 94720 (United States)], E-mail: acthompson@lbl.gov; Blakely, E.A.; Bjornstad, K.A. [Division of Life Sciences, Lawrence Berkeley National Laboratory, Bld. 50A-6120, Berkeley, CA 94720 (United States); Chang, P.Y. [Division of Life Sciences, Lawrence Berkeley National Laboratory, Bld. 50A-6120, Berkeley, CA 94720 (United States); SRI International, Menlo Park, CA (United States); Rosen, C.J.; Schwarz, R.I. [Division of Life Sciences, Lawrence Berkeley National Laboratory, Bld. 50A-6120, Berkeley, CA 94720 (United States)

2007-11-11

Synchrotron X-ray sources enable radiation biology experiments that are difficult with conventional sources. A synchrotron source can easily deliver a monochromatic, tunable energy, highly collimated X-ray beam of well-calibrated intensity. An exposure station at beamline 10.3.1 of the Advanced Light Source (ALS) has been developed which delivers a variable energy (5-20 keV) X-ray fan beam with very sharp edges (10-90% in less than 3 {mu}m). A series of experiments have been done with a four-well slide where a stripe (100 {mu}m widex18 mm long) of cells in each well has been irradiated and the dose varied from well to well. With this facility we have begun a series of experiments to study cells adjacent to irradiated cells and how they respond to the damage of their neighbors. Initial results have demonstrated the advantages of using synchrotron radiation for these experiments.

Nanofocusing Parabolic Refractive X-Ray Lenses

International Nuclear Information System (INIS)

Schroer, C.G.; Kuhlmann, M.; Hunger, U.T.; Guenzler, T.F.; Kurapova, O.; Feste, S.; Lengeler, B.; Drakopoulos, M.; Somogyi, A.; Simionovici, A. S.; Snigirev, A.; Snigireva, I.

2004-01-01

Parabolic refractive x-ray lenses with short focal distance can generate intensive hard x-ray microbeams with lateral extensions in the 100nm range even at short distance from a synchrotron radiation source. We have fabricated planar parabolic lenses made of silicon that have a focal distance in the range of a few millimeters at hard x-ray energies. In a crossed geometry, two lenses were used to generate a microbeam with a lateral size of 330nm by 110nm at 25keV in a distance of 41.8m from the synchrotron radiation source. First microdiffraction and fluorescence microtomography experiments were carried out with these lenses. Using diamond as lens material, microbeams with lateral size down to 20nm and below are conceivable in the energy range from 10 to 100keV

Detectability of rotation-powered pulsars in future hard X-ray surveys

International Nuclear Information System (INIS)

Wang Wei

2009-01-01

Recent INTEGRAL/IBIS hard X-ray surveys have detected about 10 young pulsars. We show hard X-ray properties of these 10 young pulsars, which have a luminosity of 10 33 -10 37 erg s -1 and a photon index of 1.6-2.1 in the energy range of 20-100 keV. The correlation between X-ray luminosity and spin-down power of L X ∝ L sd 1.31 suggests that the hard X-ray emission in rotation-powered pulsars is dominated by the pulsar wind nebula (PWN) component. Assuming spectral properties are similar in 20-100 keV and 2-10 keV for both the pulsar and PWN components, the hard X-ray luminosity and flux of 39 known young X-ray pulsars and 8 millisecond pulsars are obtained, and a correlation of L X ∝ L sd 1.5 is derived. About 20 known young X-ray pulsars and 1 millisecond pulsars could be detected with future INTEGRAL and HXMT surveys. We also carry out Monte Carlo simulations of hard X-ray pulsars in the Galaxy and the Gould Belt, assuming values for the pulsar birth rate, initial position, proper motion velocity, period, and magnetic field distribution and evolution based on observational statistics and the L X - L sd relations: L X ∝ L sd 1.31 and L X ∝ L sd 1.5 . More than 40 young pulsars (mostly in the Galactic plane) could be detected after ten years of INTEGRAL surveys and the launch of HXMT. So, the young pulsars would be a significant part of the hard X-ray source population in the sky, and will contribute to unidentified hard X-ray sources in present and future hard X-ray surveys by INTEGRAL and HXMT.

X-ray optics, a vital aspect of work with synchrotron radiation

International Nuclear Information System (INIS)

Bilderback, D.H.

1986-01-01

The kind of optical components that have been developed over the centuries to make use of visible light won't work for x-rays. New ways must be found to manipulate the much shorter-wavelength x-ray beams to produce effects similar to those achieved with such familiar devices as mirrors, lenses, prisms, and gratings. This is the province of the field of x-ray optics. One challenge is to design optical elements that can focus, disperse, or reflect beams in the x-ray region of the electromagnetic spectrum, where wavelengths are about a thousand times shorter than those in the region of visible light. A second problem is encountered in using the intense, high-energy x-radiation from a synchrotron: how to make the desired beam accessible to a user who is conducting an experiment in a shielded enclosure many meters away from the synchrotron storage ring. Depending on the application, one might want to pick out a single wavelength from the broad spectrum available from the synchrotron, or isolate a narrow band of wavelengths. Then the beam must be collimated. When samples to be exposed are of millimeter dimension or smaller, it may be desirable to increase the intensity by focusing the x-ray beam horizontally and vertically. All these manipulations are analogous to those done with visible light, but the shape and form of the optical components can be quite different

Synchrotron x-ray imaging of acoustic cavitation bubbles induced by acoustic excitation

International Nuclear Information System (INIS)

Jung, Sung Yong; Park, Han Wook; Park, Sung Ho; Lee, Sang Joon

2017-01-01

The cavitation induced by acoustic excitation has been widely applied in various biomedical applications because cavitation bubbles can enhance the exchanges of mass and energy. In order to minimize the hazardous effects of the induced cavitation, it is essential to understand the spatial distribution of cavitation bubbles. The spatial distribution of cavitation bubbles visualized by the synchrotron x-ray imaging technique is compared to that obtained with a conventional x-ray tube. Cavitation bubbles with high density in the region close to the tip of the probe are visualized using the synchrotron x-ray imaging technique, however, the spatial distribution of cavitation bubbles in the whole ultrasound field is not detected. In this study, the effects of the ultrasound power of acoustic excitation and working medium on the shape and density of the induced cavitation bubbles are examined. As a result, the synchrotron x-ray imaging technique is useful for visualizing spatial distributions of cavitation bubbles, and it could be used for optimizing the operation conditions of acoustic cavitation. (paper)

Hard X-ray Photoelectric Polarimeter

Data.gov (United States)

National Aeronautics and Space Administration — Our objective is to determine the gas mixtures and pressures that would enable a sensitive, hard X-ray polarimeter using existing flight components with the goal of...

X-ray stress measurement by use of synchrotron radiation source

International Nuclear Information System (INIS)

Yoshioka, Yasuo; Matsui, Hisaaki; Moro-oka, Toshimasa; Hasegawa, Ken-ichi; Nakajima, Tetsuo.

1986-01-01

In the field of X-ray stress measurement of polycrystalline materials, a diffraction plane at higher Bragg angle has to be selected in order to obtain the precise value of stress. However, the stress measurement on an optional (hkl) plane desired is not always possible because the X-ray beam exited from a metal target has a dispersive wave length. Recently, we have been able to use the synchrotron radiation source (SR) as an excellent X-ray source. In Japan, the facility of synchrotron radiation (Photon Factory, PF) was constructed in the National Laboratory for High Energy Physics (KEK) at Tsukuba academic city. The use of this SR enables the stress measurements on many (hkl) planes with high accuracy in the higher Bragg angle region by providing an X-ray beam having an optional wave length. We have started the X-ray stress analysis by use of the synchrotron radiation source. This paper reports the system of measurement and some results of preliminaly experiments. Since a monochromatic X-ray beam is required for the stress measurement, we used a beam line which consists of a double crystal monochrometer and a focusing mirror. X-rays between 4 KeV (λ = 0.31 nm) and 10 KeV (λ = 0.12 nm) are available with this optical system. We adopted a constant Bragg angle of 2θ = 154 deg for all the diffraction planes. A PSPC having a carbon fiber anode is made and used as a detector with the use of a fast digital signal processor. We could observe the diffraction profiles from (200), (211), (220), (310) and (321) crystal plane of alpha iron, respectively, and the residual stresses in these planes except the (200) plane were measured with high accuracy in a short time. Such feature especially suits the stress analysis of the material which has preferred orientation or stress gradient. (author)

The over-the-limb hard X-ray events

Science.gov (United States)

Hudson, H. S.

Over-the-limb hard X-ray events offer a uniquely direct view of the hard X-ray emission from the solar corona during a major flare. Limb occultation at angles greater than about 10 deg (an arbitrary definition of this class of events) excludes any confusion with brighter chromospheric sources. Published observations of seven over-the-limb events, beginning with the prototype flare of March 30, 1969, are reviewed. The hard X-ray spectra appear to fall into two classes: hard events, with power-law index of about 2.0; and soft events, with power-law index about 5.4. This tendency towards bimodality is only significant at the 90-percent confidence level due to the smallness of the number of events observed to date. If borne out by future data, the bimodality would suggest the existence of two different acceleration mechanisms.

Hard X-Ray PHA System on the HT-7 Tokamak

International Nuclear Information System (INIS)

Lin Shiyao; Shi Yuejiang; Wan Baonian; Chen Zhongyong; Hu Liqun

2006-01-01

A new hard X-ray pulse-height analysis (PHA) system has been established on HT-7 tokamak for long pulse steady-state operation. This PHA system consists of hard X-ray diagnostics and multi-channel analysers (MCA). The hard X-ray diagnostics consists of a vertical X-ray detector array (CdTe) and a horizontal X-ray detector array (NaI). The hard X-ray diagnostics can provide the profile of power deposition and the distribution function of fast electron during radio frequency (RF) current drive. The MCA system is the electronic part of the PHA system, which has been modularized and linked to PC through LAN. Each module of MCA can connect with 8 X-ray detectors. The embedded Ethernet adapter in the MCA module makes the data communication between PC and MCA very convenient. A computer can control several modules of MCA through certain software and a hub. The RAM in MCA can store 1024 or more spectra for each detector and therefore the PHA system can be applied in the long pulse discharge of several minutes

NuSTAR HARD X-RAY SURVEY OF THE GALACTIC CENTER REGION. I. HARD X-RAY MORPHOLOGY AND SPECTROSCOPY OF THE DIFFUSE EMISSION

Energy Technology Data Exchange (ETDEWEB)

Mori, Kaya; Hailey, Charles J.; Perez, Kerstin; Nynka, Melania; Zhang, Shuo; Canipe, Alicia M. [Columbia Astrophysics Laboratory, Columbia University, New York, NY 10027 (United States); Krivonos, Roman; Tomsick, John A.; Barrière, Nicolas; Boggs, Steven E.; Craig, William W. [Space Sciences Laboratory, University of California, Berkeley, CA 94720 (United States); Hong, Jaesub [Harvard-Smithsonian Center for Astrophysics, Cambridge, MA 02138 (United States); Ponti, Gabriele [Max-Planck-Institut f. extraterrestrische Physik, HEG, Garching (Germany); Bauer, Franz [Instituto de Astrofísica, Facultad de Física, Pontificia Universidad Católica de Chile, 306, Santiago 22 (Chile); Alexander, David M. [Department of Physics, Durham University, Durham DH1 3LE (United Kingdom); Baganoff, Frederick K. [Kavli Institute for Astrophysics and Space Research, Massachusets Institute of Technology, Cambridge, MA 02139 (United States); Barret, Didier [Université de Toulouse, UPS-OMP, IRAP, Toulouse (France); Christensen, Finn E. [DTU Space—National Space Institute, Technical University of Denmark, Elektrovej 327, DK-2800 Lyngby (Denmark); Forster, Karl [Cahill Center for Astronomy and Astrophysics, California Institute of Technology, Pasadena, CA 91125 (United States); Giommi, Paolo, E-mail: kaya@astro.columbia.edu [ASI Science Data Center, Via del Politecnico snc I-00133, Roma (Italy); and others

2015-12-01

We present the first sub-arcminute images of the Galactic Center above 10 keV, obtained with NuSTAR. NuSTAR resolves the hard X-ray source IGR J17456–2901 into non-thermal X-ray filaments, molecular clouds, point sources, and a previously unknown central component of hard X-ray emission (CHXE). NuSTAR detects four non-thermal X-ray filaments, extending the detection of their power-law spectra with Γ ∼ 1.3–2.3 up to ∼50 keV. A morphological and spectral study of the filaments suggests that their origin may be heterogeneous, where previous studies suggested a common origin in young pulsar wind nebulae (PWNe). NuSTAR detects non-thermal X-ray continuum emission spatially correlated with the 6.4 keV Fe Kα fluorescence line emission associated with two Sgr A molecular clouds: MC1 and the Bridge. Broadband X-ray spectral analysis with a Monte-Carlo based X-ray reflection model self-consistently determined their intrinsic column density (∼10{sup 23} cm{sup −2}), primary X-ray spectra (power-laws with Γ ∼ 2) and set a lower limit of the X-ray luminosity of Sgr A* flare illuminating the Sgr A clouds to L{sub X} ≳ 10{sup 38} erg s{sup −1}. Above ∼20 keV, hard X-ray emission in the central 10 pc region around Sgr A* consists of the candidate PWN G359.95–0.04 and the CHXE, possibly resulting from an unresolved population of massive CVs with white dwarf masses M{sub WD} ∼ 0.9 M{sub ⊙}. Spectral energy distribution analysis suggests that G359.95–0.04 is likely the hard X-ray counterpart of the ultra-high gamma-ray source HESS J1745–290, strongly favoring a leptonic origin of the GC TeV emission.

Prepulse dependence in hard x-ray generation from microdroplets

International Nuclear Information System (INIS)

Anand, M.; Kahaly, S.; Kumar, G. Ravindra; Sandhu, A. S.; Gibbon, P.; Krishnamurthy, M.

2006-01-01

We report on experiments which show that liquid microdroplets are very efficient in hard x-ray generation. We make a comparative study of hard x-ray emission from 15 μm methanol microdroplets and a plain slab target of similar atomic composition at similar laser intensities. The hard X-ray yield from droplet plasmas is about 35 times more than that obtained from solid plasmas. A prepulse that is about 10ns and at least 2% in intensity of the main pulse is essential for hard x-ray generation from the droplets at about 1015 W cm-2. A hot electron temperature of 36 keV is measured from the droplets at 8 x 1014 W cm-2; three times higher intensity is needed to obtain similar hot electron temperature from solid plasmas that have similar atomic composition. We use 1D-PIC simulation to obtain qualitative correlation to the experimental observations

Synchrotron X-ray imaging applied to solar photovoltaic silicon

International Nuclear Information System (INIS)

Lafford, T A; Villanova, J; Plassat, N; Dubois, S; Camel, D

2013-01-01

Photovoltaic (PV) cell performance is dictated by the material of the cell, its quality and purity, the type, quantity, size and distribution of defects, as well as surface treatments, deposited layers and contacts. A synchrotron offers unique opportunities for a variety of complementary X-ray techniques, given the brilliance, spectrum, energy tunability and potential for (sub-) micron-sized beams. Material properties are revealed within in the bulk and at surfaces and interfaces. X-ray Diffraction Imaging (X-ray Topography), Rocking Curve Imaging and Section Topography reveal defects such as dislocations, inclusions, misorientations and strain in the bulk and at surfaces. Simultaneous measurement of micro-X-Ray Fluorescence (μ-XRF) and micro-X-ray Beam Induced Current (μ-XBIC) gives direct correlation between impurities and PV performance. Together with techniques such as microscopy and Light Beam Induced Current (LBIC) measurements, the correlation between structural properties and photovoltaic performance can be deduced, as well as the relative influence of parameters such as defect type, size, spatial distribution and density (e.g [1]). Measurements may be applied at different stages of solar cell processing in order to follow the evolution of the material and its properties through the manufacturing process. Various grades of silicon are under study, including electronic and metallurgical grades in mono-crystalline, multi-crystalline and mono-like forms. This paper aims to introduce synchrotron imaging to non-specialists, giving example results on selected solar photovoltaic silicon samples.

Ring artifact reduction in synchrotron X-ray tomography through helical acquisition

NARCIS (Netherlands)

D.M. Pelt (Daniël); D.Y. Parkinson (Dilworth)

2017-01-01

textabstractIn synchrotron X-ray tomography, systematic defects in certain detector elements can result in arc-shaped artifacts in the final reconstructed image of the scanned sample. These ring artifacts are commonly found in many applications of synchrotron tomography, and can make

Application of X-ray synchrotron microscopy instrumentation in biology

International Nuclear Information System (INIS)

Gasperini, F. M.; Pereira, G. R.; Granjeiro, J. M.; Calasans-Maia, M. D.; Rossi, A. M.; Perez, C. A.; Lopes, R. T.; Lima, I.

2011-01-01

X-ray micro-fluorescence imaging technique has been used as a significant tool in order to investigate minerals contents in some kinds of materials. The aim of this study was to evaluate the elemental distribution of calcium and zinc in bone substitute materials (nano-hydroxyapatite spheres) and cortical bones through X-Ray Micro-fluorescence analysis with the increment of Synchrotron Radiation in order to evaluate the characteristics of the newly formed bone and its interface, the preexisting bone and biomaterials by the arrangement of collagen fibers and its birefringence. The elemental mapping was carried out at Brazilian Synchrotron Light Laboratory, Campinas - Sao Paulo, Brazil working at D09-XRF beam line. Based on this study, the results suggest that hydroxyapatite-based biomaterials are biocompatible, promote osteo-conduction and favored bone repair. (authors)

Hard X-ray diffraction enhanced imaging only using two crystals

Institute of Scientific and Technical Information of China (English)

LI Gang; WANG Nan; WU Ziyu

2004-01-01

Different configurations for the monochromator crystals and the analyzer crystals have been used in hard X-ray diffraction enhanced imaging (DEI) methods to overcome the complex task to adjust each of them to the ideal position. Here we present a very compact DEI configuration, and preliminary results of experiments performed at the Beijing Synchrotron Radiation Facility (BSRF) using only two crystals: the first one acting as monochromator and the second one as analyzer in the Bragg geometry. Refraction contrast images characterized by high contrast and spatial resolution are obtained and compared with absorption images. Differences among these images will be outlined and discussed emphasizing the potential capabilities of this very simple layout that guarantees a high transmission efficiency.

Investigation of the hard x-ray background in backlit pinhole imagers

Energy Technology Data Exchange (ETDEWEB)

Fein, J. R., E-mail: jrfein@umich.edu; Holloway, J. P. [Department of Nuclear Engineering and Radiological Sciences, University of Michigan, Ann Arbor, Michigan 48109-2143 (United States); Peebles, J. L. [Center for Energy Research, University of California, San Diego, La Jolla, California 92093 (United States); Keiter, P. A.; Klein, S. R.; Kuranz, C. C.; Manuel, M. J.-E.; Drake, R. P. [Department of Atmospheric, Oceanic and Space Sciences, University of Michigan, Ann Arbor, Michigan 48109-2143 (United States)

2014-11-15

Hard x-rays from laser-produced hot electrons (>10 keV) in backlit pinhole imagers can give rise to a background signal that decreases signal dynamic range in radiographs. Consequently, significant uncertainties are introduced to the measured optical depth of imaged plasmas. Past experiments have demonstrated that hard x-rays are produced when hot electrons interact with the high-Z pinhole substrate used to collimate the softer He-α x-ray source. Results are presented from recent experiments performed on the OMEGA-60 laser to further study the production of hard x-rays in the pinhole substrate and how these x-rays contribute to the background signal in radiographs. Radiographic image plates measured hard x-rays from pinhole imagers with Mo, Sn, and Ta pinhole substrates. The variation in background signal between pinhole substrates provides evidence that much of this background comes from x-rays produced in the pinhole substrate itself. A Monte Carlo electron transport code was used to model x-ray production from hot electrons interacting in the pinhole substrate, as well as to model measurements of x-rays from the irradiated side of the targets, recorded by a bremsstrahlung x-ray spectrometer. Inconsistencies in inferred hot electron distributions between the different pinhole substrate materials demonstrate that additional sources of hot electrons beyond those modeled may produce hard x-rays in the pinhole substrate.

Hard X-ray observation of HER X-1

Energy Technology Data Exchange (ETDEWEB)

Ubertini, P.; Bazzano, A.; La Padula, C.; Polcaro, V.F.; Vialetto, G. (Consiglio Nazionale delle Ricerche, Frascati (Italy). Lab. di Astrofisica Spaziale); Manchanda, R.K. (Tata Inst. of Fundamental Research, Bombay (India))

1981-01-01

A hard X-rays (15-170 KeV) measurement of the spectrum of Her X-1, during a mid turn-on is presented. The presence of an emission line at about 53 KeV during the mid-on state is confirmed by the present measure.

Hard X-ray submicrometer tomography of human brain tissue at Diamond Light Source

Science.gov (United States)

Khimchenko, A.; Bikis, C.; Schulz, G.; Zdora, M.-C.; Zanette, I.; Vila-Comamala, J.; Schweighauser, G.; Hench, J.; Hieber, S. E.; Deyhle, H.; Thalmann, P.; Müller, B.

2017-06-01

There is a lack of the necessary methodology for three-dimensional (3D) investigation of soft tissues with cellular resolution without staining or tissue transformation. Synchrotron radiation based hard X-ray in-line phase contrast tomography using single-distance phase reconstruction (SDPR) provides high spatial resolution and density contrast for the visualization of individual cells using a standard specimen preparation and data reconstruction. In this study, we demonstrate the 3D characterization of a formalin-fixed paraffin-embedded (FFPE) human cerebellum specimen by SDPR at the Diamond-Manchester Imaging Branchline I13-2 (Diamond Light Source, UK) at pixel sizes down to 0.45 μm. The approach enables visualization of cerebellar layers (Stratum moleculare and Stratum granulosum), the 3D characterization of individual cells (Purkinje, stellate and granule cells) and can even resolve some subcellular structures (nucleus and nucleolus of Purkinje cells). The tomographic results are qualitatively compared to hematoxylin and eosin (H&E) stained histological sections. We demonstrate the potential benefits of hard X-ray microtomography for the investigations of biological tissues in comparison to conventional histology.

Hard X-ray submicrometer tomography of human brain tissue at Diamond Light Source

International Nuclear Information System (INIS)

Khimchenko, A; Bikis, C; Schulz, G; Hieber, S E; Deyhle, H; Thalmann, P; Müller, B; Zdora, M-C; Zanette, I; Vila-Comamala, J; Schweighauser, G; Hench, J

2017-01-01

There is a lack of the necessary methodology for three-dimensional (3D) investigation of soft tissues with cellular resolution without staining or tissue transformation. Synchrotron radiation based hard X-ray in-line phase contrast tomography using single-distance phase reconstruction (SDPR) provides high spatial resolution and density contrast for the visualization of individual cells using a standard specimen preparation and data reconstruction. In this study, we demonstrate the 3D characterization of a formalin-fixed paraffin-embedded (FFPE) human cerebellum specimen by SDPR at the Diamond-Manchester Imaging Branchline I13-2 (Diamond Light Source, UK) at pixel sizes down to 0.45 μm. The approach enables visualization of cerebellar layers ( Stratum moleculare and Stratum granulosum ), the 3D characterization of individual cells (Purkinje, stellate and granule cells) and can even resolve some subcellular structures (nucleus and nucleolus of Purkinje cells). The tomographic results are qualitatively compared to hematoxylin and eosin (H and E) stained histological sections. We demonstrate the potential benefits of hard X-ray microtomography for the investigations of biological tissues in comparison to conventional histology. (paper)

A free-electron laser fourth-generation X-ray source

International Nuclear Information System (INIS)

Moncton, D. E.

1999-01-01

The field of synchrotrons radiation research has grown rapidly over the last 25 years due to both the push of the accelerator and magnet technology that produces the x-ray beams and the pull of the extraordinary scientific research those beams make possible. Three successive generations of synchrotrons radiation facilities have resulted in beam brilliances 11 to 12 orders of magnitude greater than the standard laboratory x-ray tube. However, greater advances can be easily imagined given the fact that x-ray beams from present-day facilities do not exhibit the coherence or time structure so familiar with the.optical laser. Theoretical work over the last ten years or so has pointed to the possibility of generating hard x-ray beams with laser-like characteristics. The concept is based on self-amplified spontaneous emission in free electron lasers. The use of a superconducting linac could produce a major, cost-effective facility that spans wavelengths from the ultraviolet to the hard x-ray regime, simultaneously servicing large numbers experimenters from a wide range of disciplines. As with each past generation of synchrotron facilities, immense new scientific opportunities from fourth-generation sources

Hard X-ray observation of HER X-1

International Nuclear Information System (INIS)

Ubertini, P.; Bazzano, A.; La Padula, C.; Polcaro, V.F.; Vialetto, G.

1981-01-01

A hard X-rays (15-170 KeV) measurement of the spectrum of Her X-1, during a mid turn-on is presented. The presence of an emission line at about 53 KeV during the mid-on state is confirmed by the present measure. (orig.)

Current status of the hard x-ray nanoprobe beamline at the SSRF

Science.gov (United States)

Li, Aiguo; Jiang, Hui; Wang, Hua; Zhang, Zhaohong; He, Yan; Zhao, Gaofeng; Shu, Deming

2017-09-01

The hard X-ray nanoprobe beamline (HXN) designed at the Shanghai Synchrotron Radiation facility (SSRF) will be of capability to realize a focal spot size of 10 nm for hard X-rays to satisfy requirements in biology, environmental, material sciences and etc.. The beamline includes two modes of operation, high energy resolution mode and high flux mode respectively. High flux mode utilizes the multilayer KB system to obtain high-flux diffraction-limited focusing of 10nm. An ultra-high-precision figure fabrication for diffraction-limited focusing is required to meet the Rayleigh Criterion. An idea to overcome this problem is to introduce a phase compensator upstream of the KB system to compensate the wavefront errors in the beamline. At wavelength speckle-based method will be used to measure the wavefront error in the beamline and feedback to the phase compensator. Vibration measurements have been carried out at the secondary source and endstation hutch. The flexure hinge mechanisms and high-precision actuators ensure the KB system and sample manipulator working with high stability. The building of HXN has been designed and is under construction at present.

Nanoscopium: a Scanning Hard X-ray Nanoprobe Beamline at Synchrotron Soleil

Science.gov (United States)

Somogyi, A.; Polack, F.; Moreno, T.

2010-06-01

Nanoscopium is the single scanning hard X-ray nano-probe beamline planned at SOLEIL. This ˜155 m long beamline will fully exploit the high brilliance and coherence characteristics of the X-ray beam both for diffraction limited focusing and for contrast formation. It will offer the most advanced imaging techniques in multimodal mode and will be a research tool for a wide user community working in the fields of earth-, environmental-, and life-sciences. The different μ-μnano-probe techniques offered by the beamline will permit elemental mapping at trace (ppm) levels (scanning XRF), speciation mapping (XANES), phase gradient mapping (scanning differential phase contrast), and density-contrast based imaging of internal structures (coherent diffraction imaging) in the 30 nm to 1 μm spatial resolution range, also in "in situ conditions". Nanoscopium will cover the 5-20 keV energy range. The stability of the nanobeam will be ensured by horizontally reflecting beamline optics (a sagitally and a tangentially pre-focusing mirror, horizontally reflecting monochromators) in front of the overfilled secondary source. Trade-off between high energy resolution (ΔE/E˜10-4) and high flux (1011 ph/s with ΔE/E˜10-2) will be achieved by two interchangeable monochromators (a double crystal and a double multilayer one). KB mirror and FZP lenses will be used as focusing devices. The beamline is in the design and construction phase. It is foreseen to be open for users at the beginning of 2013.

Backscatter, anisotropy, and polarization of solar hard X-rays

International Nuclear Information System (INIS)

Bai, T.; Ramaty, R.

1978-01-01

Hard X-rays incident upon the photosphere with energies > or approx. =15 keV have high probabilities of backscatter due to Compton collisions with electrons. This effect has a strong influence on the spectrum, intensity, and polarization of solar hard X-rays - especially for anisotropic models in which the primary X-rays are emitted predominantly toward the photosphere. We have carried out a detailed study of X-ray backscatter, and we have investigated the interrelated problems of anisotropy, polarization, center-to-limb variation of the X-ray spectrum, and Compton backscatter in a coherent fashion. The results of this study are compared with observational data. Because of the large contribution from backscatter, for an anisotropic primary X-ray source which is due to bremsstrahlung of accelerated electrons moving predominantly down toward the photosphere, the observed X-ray flux around 30 keV does not depend significantly on the position of flare on the Sun. For such an anisotropic source, the X-ray spectrum observed in the 15-50 keV range becomes steeper with the increasing heliocentric angle of the flare. These results are compatible with the data. The degree of polarization of the sum of the primary and reflected X-rays with energies between about 15 and 30 keV can be very large for anisotropic primary X-ray sources, but it is less than about 4% for isotropic sources. We also discuss the characteristics of the brightness distribution of the X-ray albedo patch created by the Compton backscatter. The height and anisotropy of the primary hard X-ray source might be inferred from the study of the albedo patch

Synchrotron X-ray adaptative monochromator: study and realization of a prototype

International Nuclear Information System (INIS)

Dezoret, D.

1995-01-01

This work presents a study of a prototype of a synchrotron X-ray monochromator. The spectral qualities of this optic are sensitive to the heat loads which are particularly important on third synchrotron generation like ESRF. Indeed, powers generated by synchrotron beams can reach few kilowatts and power densities about a few tens watts per square millimeters. The mechanical deformations of the optical elements of the beamlines issue issue of the heat load can damage their spectral efficiencies. In order to compensate the deformations, wa have been studying the transposition of the adaptive astronomical optics technology to the x-ray field. First, we have considered the modifications of the spectral characteristics of a crystal induced by x-rays. We have established the specifications required to a technological realisation. Then, thermomechanical and technological studies have been required to transpose the astronomical technology to an x-ray technology. After these studies, we have begun the realisation of a prototype. This monochromator is composed by a crystal of silicon (111) bonded on a piezo-electric structure. The mechanical control is a loop system composed by a infrared light, a Shack-Hartmann CDD and wave front analyser. This system has to compensate the deformations of the crystal in the 5 kcV to 60 kcV energy range with a power density of 1 watt per square millimeters. (authors)

Simulations of X-ray synchrotron beams using the EGS4 code system in medical applications

International Nuclear Information System (INIS)

Orion, I.; Henn, A.; Sagi, I.; Dilmanian, F.A.; Pena, L.; Rosenfeld, A.B.

2001-01-01

X-ray synchrotron beams are commonly used in biological and medical research. The availability of intense, polarized low-energy photons from the synchrotron beams provides a high dose transfer to biological materials. The EGS4 code system, which includes the photoelectron angular distribution, electron motion inside a magnetic field, and the LSCAT package, found to be the appropriate Monte Carlo code for synchrotron-produced X-ray simulations. The LSCAT package was developed in 1995 for the EGS4 code to contain the routines to simulate the linear polarization, the bound Compton, and the incoherent scattering functions. Three medical applications were demonstrated using the EGS4 Monte Carlo code as a proficient simulation code system for the synchrotron low-energy X-ray source. (orig.)

X-ray microscopy using collimated and focussed synchrotron radiation

International Nuclear Information System (INIS)

Jones, K.W.; Kwiatek, W.M.; Gordon, B.M.

1987-01-01

X-ray microscopy is a field that has developed rapidly in recent years. Two different approaches have been used. Zone plates have been employed to produce focused beams with sizes as low as 0.07 μm for x-ray energies below 1 keV. Images of biological materials and elemental maps for major and minor low Z have been produced using above and below absorption edge differences. At higher energies collimators and focusing mirrors have been used to make small diameter beams for excitation of characteristic K- or L-x rays of all elements in the periodic table. The practicality of a single instrument combining all the features of these two approaches is unclear. The use of high-energy x rays for x-ray microscopy has intrinsic value for characterization of thick samples and determination of trace amounts of most elements. A summary of work done on the X-26 beam line at the National Synchrotron Light Source (NSLS) with collimated and focused x rays with energies above 4 keV is given here. 6 refs., 5 figs., 1 tab

A hard X-ray laboratory for monochromator characterisation

Energy Technology Data Exchange (ETDEWEB)

Hamelin, B [Institut Max von Laue - Paul Langevin (ILL), 38 - Grenoble (France)

1997-04-01

Since their installation at ILL during the 1970`s the ILL {gamma}-ray diffractometers have been intensively used in the development of neutron monochromators. However, the ageing of the sources and new developments in hard X-ray diffractometry lead to a decision at the end of 1995 to replace the existing {gamma}-ray laboratory with a hard X-ray laboratory, based on a 420 keV generator, making available in the long term several beam-lines for rapid characterisation of monochromator crystals. The facility is now installed and its characteristics and advantages are outlined. (author). 2 refs.

Absorption and Phase Contrast X-Ray Imaging in Paleontology Using Laboratory and Synchrotron Sources

Energy Technology Data Exchange (ETDEWEB)

Bidola, Pidassa; Stockmar, Marco; Achterhold, Klaus; Pfeiffer, Franz; Pacheco, Mirian L.A.F.; Soriano, Carmen; Beckmann, Felix; Herzen, Julia

2015-10-01

X-ray micro-computed tomography (CT) is commonly used for imaging of samples in biomedical or materials science research. Owing to the ability to visualize a sample in a nondestructive way, X-ray CT is perfectly suited to inspect fossilized specimens, which are mostly unique or rare. In certain regions of the world where important sedimentation events occurred in the Precambrian geological time, several fossilized animals are studied to understand questions related to their origin, environment, and life evolution. This article demonstrates the advantages of applying absorption and phase-contrast CT on the enigmatic fossil Corumbella werneri, one of the oldest known animals capable of building hard parts, originally discovered in Corumba (Brazil). Different tomographic setups were tested to visualize the fossilized inner structures: a commercial laboratory-based CT device, two synchrotron-based imaging setups using conventional absorption and propagation-based phase contrast, and a commercial X-ray microscope with a lens-coupled detector system, dedicated for radiography and tomography. Based on our results we discuss the strengths and weaknesses of the different imaging setups for paleontological studies.

Time-resolved soft x-ray absorption setup using multi-bunch operation modes at synchrotrons

International Nuclear Information System (INIS)

Stebel, L.; Sigalotti, P.; Ressel, B.; Cautero, G.; Malvestuto, M.; Capogrosso, V.; Bondino, F.; Magnano, E.; Parmigiani, F.

2011-01-01

Here, we report on a novel experimental apparatus for performing time-resolved soft x-ray absorption spectroscopy in the sub-ns time scale using non-hybrid multi-bunch mode synchrotron radiation. The present setup is based on a variable repetition rate Ti:sapphire laser (pump pulse) synchronized with the ∼500 MHz x-ray synchrotron radiation bunches and on a detection system that discriminates and singles out the significant x-ray photon pulses by means of a custom made photon counting unit. The whole setup has been validated by measuring the time evolution of the L 3 absorption edge during the melting and the solidification of a Ge single crystal irradiated by an intense ultrafast laser pulse. These results pave the way for performing synchrotron time-resolved experiments in the sub-ns time domain with variable repetition rate exploiting the full flux of the synchrotron radiation.

Soft X-ray microscopy and lithography with synchrotron radiation

International Nuclear Information System (INIS)

Gudat, W.

1977-12-01

Considerable progress in the technique microscopy with soft X-ray radiation has been achieved in particular through the application of synchrotron radiation. Various methods which are currently being studied theoretically or already being used practically will be described briefly. Attention is focussed on the method of contact microscopy. Various biological specimens have been investigated by this method with a resolution as good as 100 A. X-ray lithography which in the technical procedure is very similar to contact microscopy gives promise for the fabrication of high quality submicron structures in electronic device production. Important factors limiting the resolution and determining the performance of contact microscopy and X-ray lithography will be discussed. (orig.) [de

The Hard X-ray Sky: Recent Observational Progress

International Nuclear Information System (INIS)

Gehrels, Neil; Cannizzo, John K.

2009-01-01

The last fifty years have witnessed the birth, development, and maturation to full potential of hard X-ray astrophysics. The primary force driving the history of the field has been the development of space-based instrumentation optimized for getting the maximum science out of observations of high-energy photons from astrophysical sources. Hard X-ray telescopes are leading research in areas such as galactic diffuse emission, galactic transients, and active galactic nuclei.

Report of the second workshop on synchrotron radiation sources for x-ray lithography

International Nuclear Information System (INIS)

Barton, M.Q.; Craft, B.; Williams, G.P.

1986-01-01

The reported workshop is part of an effort to implement a US-based x-ray lithography program. Presentations include designs for three storage rings (one superconducting and two conventional) and an overview of a complete lithography program. The background of the effort described, the need for synchrotron radiation, and the international competition in the area are discussed briefly. The technical feasibility of x-ray lithography is discussed, and synchrotron performance specifications and construction options are given, as well as a near-term plan. It is recommended that a prototype synchrotron source be built as soon as possible, and that a research and development plan on critical technologies which could improve cost effectiveness of the synchrotron source be established. It is further recommended that a small number of second generation prototype synchrotrons be distributed to IC manufacturing centers to expedite commercialization

Quantitative Phase Imaging Using Hard X Rays

International Nuclear Information System (INIS)

Nugent, K.A.; Gureyev, T.E.; Cookson, D.J.; Paganin, D.; Barnea, Z.

1996-01-01

The quantitative imaging of a phase object using 16keV xrays is reported. The theoretical basis of the techniques is presented along with its implementation using a synchrotron x-ray source. We find that our phase image is in quantitative agreement with independent measurements of the object. copyright 1996 The American Physical Society

UV-Visible Absorption Spectroscopy Enhanced X-ray Crystallography at Synchrotron and X-ray Free Electron Laser Sources.

Science.gov (United States)

Cohen, Aina E; Doukov, Tzanko; Soltis, Michael S

2016-01-01

This review describes the use of single crystal UV-Visible Absorption micro-Spectrophotometry (UV-Vis AS) to enhance the design and execution of X-ray crystallography experiments for structural investigations of reaction intermediates of redox active and photosensitive proteins. Considerations for UV-Vis AS measurements at the synchrotron and associated instrumentation are described. UV-Vis AS is useful to verify the intermediate state of an enzyme and to monitor the progression of reactions within crystals. Radiation induced redox changes within protein crystals may be monitored to devise effective diffraction data collection strategies. An overview of the specific effects of radiation damage on macromolecular crystals is presented along with data collection strategies that minimize these effects by combining data from multiple crystals used at the synchrotron and with the X-ray free electron laser.

Preliminary study on X-ray phase contrast imaging using synchrotron radiation facility

International Nuclear Information System (INIS)

Xiong Zhuang; Wang Jianhua; Yu Yongqiang; Jiang Shiping; Chen Yang; Tian Yulian

2006-01-01

Objective: To study the methodology of X-ray phase contrast imaging using synchrotron radiation, and evaluate the quality of phase contrast images. Methods: Several experiments to obtain phase contrast images and absorption contrast images of various biological samples were conducted in Beijing Synchrotron Radiation Facility (BSRF), and then these images were interpreted to find out the difference between the two kinds of imaging methods. Results: Satisfactory phase contrast images of these various samples were obtained, and the quality of these images was superior to that obtained with absorption contrast imaging. The phase contrast formation is based on the phenomenon of fresnel diffraction which transforms phase shifts into intensity variations upon a simple act of free-space propagation, so it requires highly coherent X-rays and appropriate distance between sample and detector. This method of imaging is very useful in imaging of low-absorption objects or objects with little absorption variation, and its resolution is far higher than that of the conventional X-ray imaging. The photographs obtained showed very fine inner microstructure of the biological samples, and the smallest microstructure to be distinguished is within 30-40 μm. There is no doubt that phase contrast imaging has a practical applicability in medicine. Moreover, it improves greatly the efficiency and the resolution of the existing X-ray diagnostic techniques. Conclusions: X-ray phase contrast imaging can be performed with synchrotron radiation source and has some advantages over the conventional absorption contrast imaging. (authors)

Exploring the Hard and Soft X-ray Emission of Magnetic Cataclysmic Variables

Science.gov (United States)

de Martino, D.; Anzolin, G.; Bonnet-Bidaud, J.-M.; Falanga, M.; Matt, G.; Mouchet, M.; Mukai, K.; Masetti, N.

2009-05-01

A non-negligible fraction of galactic hard (>20 keV) X-ray sources were identified as CVs of the magnetic Intermediate Polar type in INTEGRAL, SWIFT and RXTE surveys, that suggests a still hidden but potentially important population of faint hard X-ray sources. Simbol-X has the unique potential to simultaneously characterize their variable and complex soft and hard X-ray emission thus allowing to understand their putative role in galactic populations of X-ray sources.

Hard-X-ray photoelectron spectroscopy of NaxCoO2.yH2O

International Nuclear Information System (INIS)

Chainani, A.; Yokoya, T.; Takata, Y.; Tamasaku, K.; Taguchi, M.; Shimojima, T.; Kamakura, N.; Horiba, K.; Tsuda, S.; Shin, S.; Miwa, D.; Nishino, Y.; Ishikawa, T.; Yabashi, M.; Kobayashi, K.; Namatame, H.; Taniguchi, M.; Takada, K.; Sasaki, T.; Sakurai, H.; Takayama-Muromachi, E.

2005-01-01

We study the bulk electronic structure of Na x CoO 2 .yH 2 O using Hard X-ray (HX, hν = 5.95KeV) synchrotron photoelectron spectroscopy (PES). The Co 2p core level spectra show well-separated Co 3+ and Co 4+ ions. Cluster calculations suggest low spin Co 3+ and Co 4+ character, and a moderate on-site Coulomb correlation energy U dd ∼3-5.5eV. Photon-dependent valence band PES identifies Co 3d and O 2p derived states, in near agreement with band structure calculations. We discuss the importance of HX-PES for studying correlated transition metal oxides

X-ray studies on electrochemical systems. Synchrotron methods for energy materials

Energy Technology Data Exchange (ETDEWEB)

Braun, Artur [Empa. Eidgenoessische Materialpruefungs- und Forschungsanstalt, Duebendorf (Switzerland)

2017-07-01

This book is your graduate level entrance into battery, fuel cell and solar cell research at synchrotron X-ray sources. Materials scientists find numerous examples for the combination of electrochemical experiments with simple and with highly complex X-ray scattering and spectroscopy methods. Physicists and chemists can link applied electrochemistry with fundamental concepts of condensed matter physics, physical chemistry and surface science.

Data and videos for ultrafast synchrotron X-ray imaging studies of metal solidification under ultrasound

Directory of Open Access Journals (Sweden)

Bing Wang

2018-04-01

Full Text Available The data presented in this article are related to the paper entitled ‘Ultrafast synchrotron X-ray imaging studies of microstructure fragmentation in solidification under ultrasound’ [Wang et al., Acta Mater. 144 (2018 505-515]. This data article provides further supporting information and analytical methods, including the data from both experimental and numerical simulation, as well as the Matlab code for processing the X-ray images. Six videos constructed from the processed synchrotron X-ray images are also provided.

Time-resolved x-ray diffraction measurement of C60 under high pressure and temperature using synchrotron radiation

International Nuclear Information System (INIS)

Horikawa, T; Suito, K; Kobayashi, M; Onodera, A

2002-01-01

C 60 has been studied by means of time-resolved x-ray diffraction measurements using synchrotron radiation. Diffraction patterns were recorded at intervals of 1-10 min for samples under high pressure (12.5 and 14.3 GPa) and high temperature (up to 800 deg. C) for, at the longest, 3 h. Time, pressure, and temperature dependences of the C 60 structure are presented and the relevance to the hardness of materials derived from C 60 is discussed

Synchrotron x-ray sources and new opportunities in the soil and environmental sciences

International Nuclear Information System (INIS)

Schulze, D.; Anderson, S.; Mattigod, S.

1990-07-01

This report contains the following papers: characteristics of the advanced photon source and comparison with existing synchrotron facilities; x-ray absorption spectroscopy: EXAFS and XANES -- A versatile tool to study the atomic and electronic structure of materials; applications of x-ray spectroscopy and anomalous scattering experiments in the soil and environmental sciences; X-ray fluorescence microprobe and microtomography

Development of Compton X-ray spectrometer for high energy resolution single-shot high-flux hard X-ray spectroscopy

Energy Technology Data Exchange (ETDEWEB)

Kojima, Sadaoki, E-mail: kojima-s@ile.osaka-u.ac.jp, E-mail: sfujioka@ile.osaka-u.ac.jp; Ikenouchi, Takahito; Arikawa, Yasunobu; Sakata, Shohei; Zhang, Zhe; Abe, Yuki; Nakai, Mitsuo; Nishimura, Hiroaki; Shiraga, Hiroyuki; Fujioka, Shinsuke, E-mail: kojima-s@ile.osaka-u.ac.jp, E-mail: sfujioka@ile.osaka-u.ac.jp; Azechi, Hiroshi [Institute of Laser Engineering, Osaka University, 2-6 Yamada-oka, Suita, Osaka 565-0871 (Japan); Ozaki, Tetsuo [National Institute for Fusion Science, 322-6 Oroshi, Toki, Gifu 509-5292 (Japan); Miyamoto, Shuji; Yamaguchi, Masashi; Takemoto, Akinori [Laboratory of Advanced Science and Technology for Industry, University of Hyogo, 3-1-2 Kouto, Kamigori-cho, Ako-gun, Hyogo 678-1205 (Japan)

2016-04-15

Hard X-ray spectroscopy is an essential diagnostics used to understand physical processes that take place in high energy density plasmas produced by intense laser-plasma interactions. A bundle of hard X-ray detectors, of which the responses have different energy thresholds, is used as a conventional single-shot spectrometer for high-flux (>10{sup 13} photons/shot) hard X-rays. However, high energy resolution (Δhv/hv < 0.1) is not achievable with a differential energy threshold (DET) X-ray spectrometer because its energy resolution is limited by energy differences between the response thresholds. Experimental demonstration of a Compton X-ray spectrometer has already been performed for obtaining higher energy resolution than that of DET spectrometers. In this paper, we describe design details of the Compton X-ray spectrometer, especially dependence of energy resolution and absolute response on photon-electron converter design and its background reduction scheme, and also its application to the laser-plasma interaction experiment. The developed spectrometer was used for spectroscopy of bremsstrahlung X-rays generated by intense laser-plasma interactions using a 200 μm thickness SiO{sub 2} converter. The X-ray spectrum obtained with the Compton X-ray spectrometer is consistent with that obtained with a DET X-ray spectrometer, furthermore higher certainly of a spectral intensity is obtained with the Compton X-ray spectrometer than that with the DET X-ray spectrometer in the photon energy range above 5 MeV.

Hard x-ray telescope mission

DEFF Research Database (Denmark)

Gorenstein, P.; Worrall, D.; Joensen, K.D.

1996-01-01

The Hard X-Ray Telescope was selected for study as a possible new intermediate size mission for the early 21st century. Its principal attributes are: (1) multiwavelength observing with a system of focussing telescopes that collectively observe from the UV to over 1 MeV, (2) much higher sensitivity...

Effect of Cobalt Fillers on Polyurethane Segmentations Investigated by Synchrotron Small Angle X-Ray Scattering

Directory of Open Access Journals (Sweden)

Krit Koyvanich

2013-01-01

Full Text Available The segmentation between rigid and rubbery chains in polyurethanes (PUs influences polymeric properties and implementations. Several models have successfully been proposed to visualize the configuration between the hard segment (HS and soft segment (SS. For particulate PU composites, the arrangement of HS and SS is more complicated because the fillers tend to disrupt the chain formation and segmentation. In this work, the effect of ferromagnetic cobalt (Co powders (average diameter 2 μm on PU synthesized from a reaction between polyether polyol (soft segment and diphenylmethane-4,4′-diisocyanate (hard segment was studied with varying loadings (0, 20, 40, and 60 wt.%. The 300 μm thick PU/Co samples were tape-casted and then received heat treatment at 80°C for 180 min. From synchrotron small angle X-ray scattering (SAXS, the plot of the X-ray scattering intensity (I against the scattering vector (q exhibited a typical single peak of PU whose intensity was reduced by the increase in the Co loading. Characteristic SAXS peaks in the case of 0-20 wt.% Co agreed well with the scattering by globular hard segment domains according to Zernike-Prins and Percus-Yevick models. The higher Co loadings led to larger deviations from all theoretical models.

Soft x-ray lasers

International Nuclear Information System (INIS)

Matthews, D.L.; Rosen, M.D.

1988-01-01

One of the elusive dreams of laser physicists has been the development of an x-ray laser. After 25 years of waiting, the x-ray laser has at last entered the scientific scene, although those now in operation are still laboratory prototypes. They produce soft x rays down to about five nanometers. X-ray lasers retain the usual characteristics of their optical counterparts: a very tight beam, spatial and temporal coherence, and extreme brightness. Present x-ray lasers are nearly 100 times brighter that the next most powerful x-ray source in the world: the electron synchrotron. Although Lawrence Livermore National Laboratory (LLNL) is widely known for its hard-x-ray laser program which has potential applications in the Strategic Defense Initiative, the soft x-ray lasers have no direct military applications. These lasers, and the scientific tools that result from their development, may one day have a place in the design and diagnosis of both laser fusion and hard x-ray lasers. The soft x-ray lasers now in operation at the LLNL have shown great promise but are still in the primitive state. Once x-ray lasers become reliable, efficient, and economical, they will have several important applications. Chief among them might be the creation of holograms of microscopic biological structures too small to be investigated with visible light. 5 figs

Recent applications of hard x-ray photoelectron spectroscopy

Energy Technology Data Exchange (ETDEWEB)

Weiland, Conan; Woicik, Joseph C., E-mail: Joseph.Woicik@NIST.gov [National Institute of Standards and Technology, Gaithersburg, Maryland 20899 (United States); Rumaiz, Abdul K. [National Synchrotron Light Source II, Brookhaven National Laboratory, Upton, New York 11973 (United States); Pianetta, Piero [SLAC National Accelerator Laboratory, Menlo Park, California 94025 (United States)

2016-05-15

Recent applications of hard x-ray photoelectron spectroscopy (HAXPES) demonstrate its many capabilities in addition to several of its limitations. Examples are given, including measurement of buried interfaces and materials under in situ or in operando conditions, as well as measurements under x-ray standing-wave and resonant excitation. Physical considerations that differentiate HAXPES from photoemission measurements utilizing soft x-ray and ultraviolet photon sources are also presented.

VLBI OBSERVATION OF MICROQUASAR CYG X-3 DURING AN X-RAY STATE TRANSITION FROM SOFT TO HARD IN THE 2007 MAY-JUNE FLARE

Energy Technology Data Exchange (ETDEWEB)

Kim, Jeong-Sook; Kim, Sang Joon [School of Space Science, Kyunghee University, Seocheon-dong, Giheung-si, Gyeonggi-do 446-701 (Korea, Republic of); Kim, Soon-Wook [Korea Astronomy and Space Science Institute, 776 Daedeokdaero, Yuseong, Daejeon 305-348 (Korea, Republic of); Kurayama, Tomoharu [Graduate School of Science and Engineering, Kagoshima University, 1-21-35 Korimoto, Kagoshima, Kagoshima 890-0065 (Japan); Honma, Mareki [National Astronomical Observatory of Japan, 2-21-1 Osawa, Mitaka, Tokyo 181-8588 (Japan); Sasao, Tetsuo, E-mail: evony@kasi.re.kr, E-mail: skim@kasi.re.kr [Yaeyama Star Club, Ookawa, Ishigaki, Okinawa 904-0022 (Japan)

2013-07-20

We present a radio observation of microquasar Cyg X-3 during an X-ray state transition from ultrasoft to hard state in the 2007 May-June flare using the VLBI Exploration of Radio Astrometry at 22 GHz. During the transition, a short-lived mini-flare of {approx}< 3 hr was detected prior to the major flare. In such a transition, a jet ejection is believed to occur, but there have been no direct observations to support it. An analysis of Gaussian fits to the observed visibility amplitudes shows a time variation of the source axis, or a structural change, during the mini-flare. Our model fits, together with other multiwavelength observations in the radio, soft, and hard X-rays, and the shock-in-jet models for other flaring activities at GHz wavebands, suggest a high possibility of synchrotron flares during the mini-flare, indicative of a predominant contribution from jet activity. Therefore, the mini-flare with an associated structural change is indicative of a jet ejection event in the state transition from ultrasoft to hard state.

Synchrotron radiation and free-electron lasers principles of coherent X-ray generation

CERN Document Server

Kim, Kwang-Je; Lindberg, Ryan

2017-01-01

Learn about the latest advances in high-brightness X-ray physics and technology with this authoritative text. Drawing upon the most recent theoretical developments, pre-eminent leaders in the field guide readers through the fundamental principles and techniques of high-brightness X-ray generation from both synchrotron and free-electron laser sources. A wide range of topics is covered, including high-brightness synchrotron radiation from undulators, self-amplified spontaneous emission, seeded high-gain amplifiers with harmonic generation, ultra-short pulses, tapering for higher power, free-electron laser oscillators, and X-ray oscillator and amplifier configuration. Novel mathematical approaches and numerous figures accompanied by intuitive explanations enable easy understanding of key concepts, whilst practical considerations of performance-improving techniques and discussion of recent experimental results provide the tools and knowledge needed to address current research problems in the field. This is a comp...

Image alignment for tomography reconstruction from synchrotron X-ray microscopic images.

Directory of Open Access Journals (Sweden)

Chang-Chieh Cheng

Full Text Available A synchrotron X-ray microscope is a powerful imaging apparatus for taking high-resolution and high-contrast X-ray images of nanoscale objects. A sufficient number of X-ray projection images from different angles is required for constructing 3D volume images of an object. Because a synchrotron light source is immobile, a rotational object holder is required for tomography. At a resolution of 10 nm per pixel, the vibration of the holder caused by rotating the object cannot be disregarded if tomographic images are to be reconstructed accurately. This paper presents a computer method to compensate for the vibration of the rotational holder by aligning neighboring X-ray images. This alignment process involves two steps. The first step is to match the "projected feature points" in the sequence of images. The matched projected feature points in the x-θ plane should form a set of sine-shaped loci. The second step is to fit the loci to a set of sine waves to compute the parameters required for alignment. The experimental results show that the proposed method outperforms two previously proposed methods, Xradia and SPIDER. The developed software system can be downloaded from the URL, http://www.cs.nctu.edu.tw/~chengchc/SCTA or http://goo.gl/s4AMx.

Image alignment for tomography reconstruction from synchrotron X-ray microscopic images.

Science.gov (United States)

Cheng, Chang-Chieh; Chien, Chia-Chi; Chen, Hsiang-Hsin; Hwu, Yeukuang; Ching, Yu-Tai

2014-01-01

A synchrotron X-ray microscope is a powerful imaging apparatus for taking high-resolution and high-contrast X-ray images of nanoscale objects. A sufficient number of X-ray projection images from different angles is required for constructing 3D volume images of an object. Because a synchrotron light source is immobile, a rotational object holder is required for tomography. At a resolution of 10 nm per pixel, the vibration of the holder caused by rotating the object cannot be disregarded if tomographic images are to be reconstructed accurately. This paper presents a computer method to compensate for the vibration of the rotational holder by aligning neighboring X-ray images. This alignment process involves two steps. The first step is to match the "projected feature points" in the sequence of images. The matched projected feature points in the x-θ plane should form a set of sine-shaped loci. The second step is to fit the loci to a set of sine waves to compute the parameters required for alignment. The experimental results show that the proposed method outperforms two previously proposed methods, Xradia and SPIDER. The developed software system can be downloaded from the URL, http://www.cs.nctu.edu.tw/~chengchc/SCTA or http://goo.gl/s4AMx.

Assessment of a synchrotron X-ray method for quantitative analysis of calcium hydroxide

International Nuclear Information System (INIS)

Williams, P. Jason; Biernacki, Joseph J.; Bai Jianming; Rawn, Claudia J.

2003-01-01

Thermogravimetric analysis (TGA) and quantitative X-ray diffraction (QXRD) are widely used to determine the calcium hydroxide (CH) content in cementitious systems containing blends of Portland cement, fly ash, blast furnace slag, silica fume and other pozzolanic and hydraulic materials. These techniques, however, are destructive to cement samples and subject to various forms of error. While precise weight losses can be measured by TGA, extracting information from samples with multiple overlapping thermal events is difficult. And, however, while QXRD can offer easier deconvolution, the accuracy for components below about 5 wt.% is typically poor when a laboratory X-ray source is used. Furthermore, the destructive nature of both techniques prevents using them to study the in situ hydration of a single contiguous sample for kinetic analysis. In an attempt to overcome these problems, the present research evaluated the use of synchrotron X-rays for quantitative analysis of CH. A synchrotron X-ray source was used to develop calibration data for quantification of the amount of CH in mixtures with fly ash. These data were compared to conventional laboratory XRD data for like samples. While both methods were found to offer good quantification, synchrotron XRD (SXRD) provided a broader range of detectability and higher accuracy than laboratory diffraction and removed the subjectivity as compared to TGA analysis. Further, the sealed glass capillaries used with the synchrotron source provided a nondestructive closed, in situ environment for tracking hydrating specimens from zero to any desired age

Effective high voltage at X-ray tube in hard X-ray chest imaging

International Nuclear Information System (INIS)

Klein, J.

1987-01-01

The FRG standard TGL 36 661 (March 1980) for synoptical chest pictures of large size in adults specifies the 120 kV voltage at the X-ray tube together with maximal, 100% use of the capacity of the tube (hard picture, short exposure time). By means of circular recording and by measuring the high voltage at the X-ray tube it was quantitatively shown that the effective voltage during exposure is (according to the exposure time and the attenuation phase of the generator) always lower than the set-up voltage of 120 kV. This phenomenon is the more marked the shorter the actual exposure time in comparison with the attenuation phase of the generator. The typical characteristic of a hard X-ray chest picture is thus not given only by the setting-up of voltage. The impact of the reduction in voltage is thus quantitatively shown also from the aspect of the radiation burden for the patient. (author). 7 figs., 8 refs

Synchrotron X-ray adaptative monochromator: study and realization of a prototype; Monochromateur adaptatif pour rayonnement X synchrotron: etude et realisation d`un prototype

Energy Technology Data Exchange (ETDEWEB)

Dezoret, D.

1995-12-12

This work presents a study of a prototype of a synchrotron X-ray monochromator. The spectral qualities of this optic are sensitive to the heat loads which are particularly important on third synchrotron generation like ESRF. Indeed, powers generated by synchrotron beams can reach few kilowatts and power densities about a few tens watts per square millimeters. The mechanical deformations of the optical elements of the beamlines issue issue of the heat load can damage their spectral efficiencies. In order to compensate the deformations, wa have been studying the transposition of the adaptive astronomical optics technology to the x-ray field. First, we have considered the modifications of the spectral characteristics of a crystal induced by x-rays. We have established the specifications required to a technological realisation. Then, thermomechanical and technological studies have been required to transpose the astronomical technology to an x-ray technology. After these studies, we have begun the realisation of a prototype. This monochromator is composed by a crystal of silicon (111) bonded on a piezo-electric structure. The mechanical control is a loop system composed by a infrared light, a Shack-Hartmann CDD and wave front analyser. This system has to compensate the deformations of the crystal in the 5 kcV to 60 kcV energy range with a power density of 1 watt per square millimeters. (authors).

Noninvasive 3D Structural Analysis of Arthropod by Synchrotron X-Ray Phase Contrast Tomography

International Nuclear Information System (INIS)

Yao, S.; Zong, Y.; Fan, J.; Sun, Z.; Jiang, H.

2015-01-01

X-ray imaging techniques significantly advanced our understanding of materials and biology, among which phase contrast X-ray microscopy has obvious advantages in imaging biological specimens which have low contrast by conventional absorption contrast microscopy. In this paper, three-dimensional microstructure of arthropod with high contrast has been demonstrated by synchrotron X-ray in-line phase contrast tomography. The external morphology and internal structures of an earthworm were analyzed based upon tomographic reconstructions with and without phase retrieval. We also identified and characterized various fine structural details such as the musculature system, the digestive system, the nervous system, and the circulatory system. This work exhibited the high efficiency, high precision, and wide potential applications of synchrotron X-ray phase contrast tomography in nondestructive investigation of low-density materials and biology.

Hard X-ray Vela supernova observation on rocket experiment WRX-R

Science.gov (United States)

Stehlikova, V.; Urban, M.; Nentvich, O.; Daniel, V.; Sieger, L.; Tutt, J.

2017-07-01

This paper presents a hard X-ray telescope for the Vela nebula observation during a sounding rocket flight. The Water Recovery X-ray Rocket (WRX-R) experiment is organised by the Pennsylvania State University (PSU), USA with a primary payload of a soft X-ray spectroscope. The Czech team developed a hard X-ray Lobster-eye telescope as a secondary payload. The Czech experiment’s astrophysical object of study is the Vela pulsar in the centre of the Vela nebula.

Use of a synchrotron radiation x-ray microprobe for elemental analysis at the National Synchrotron Light Source

International Nuclear Information System (INIS)

Gordon, B.M.

1980-01-01

The National Synchrotron Light Source (NSLS) is a facility consisting of a 700 MeV and a 2.5 GeV electron storage ring and dedicated to providing synchrotron radiation in the energy range from the vacuum ultraviolet to high energy x rays. Some of the properties of synchrotron radiation that contribute to its usefulness for x-ray fluorescence are: a continuous, tunable energy spectrum, strong collimation in the horizontal plane, high polarization in the storage ring plane, and relatively low energy deposition. The highest priority is for the development of an x-ray microprobe beam line capable of trace analysis in the parts per million range with spatial resolution as low as one micrometer. An eventual capability for bulk sample analysis is also planned with sensitivities in the more favorable cases beings low as 50 parts per billion in dry biological tissue. The microprobe technique has application to a variety of fields including the geological, medical, materials and environmental sciences. Examples of investigations include multielemental trace analysis across grain boundaries for the study of diffusion and cooling processes in geological and materials sciences samples; in leukocytes and other types of individual cells for studying the relationship between trace element concentrations and disease or nutrition; and in individual particles in air pollution samples

Possibilities for x-ray holography using synchrotron radiation

International Nuclear Information System (INIS)

Howells, M.R.

1983-11-01

Since the theoretical and experimental demonstrations of the effectiveness of soft x-rays in imaging biological material there has been considerable study given to the prospects for further development of the presently existing techniques. This has been motivated to a large extent by advances in source technology, particularly the use of undulators on electron storage rings and recent improvements in short wavelength lasers. The present author has carried out theoretical evaluations of the possibilities of holographic imaging and has also recorded a number of holograms using the U15 soft x-ray beamline at the National Synchrotron Light Source (NSLS) 750 MeV storage ring at Brookhaven. Some of these have been successfully reconstructed using He:Cd laser light. In this paper we first review the physical processes which generate information containing wavefronts when soft x-rays interact with matter. We then briefly describe the holographic method which has been highly developed using visible light lasers and identify holographic geometries which are promising for x-ray applications. We discuss some of the practical and theoretical limitations involved in making holographic images and then give the results of our own experiments

Model independent method to deconvolve hard X-ray spectra

Energy Technology Data Exchange (ETDEWEB)

Polcaro, V.F.; Bazzano, A.; Ubertini, P.; La Padula, C. (Consiglio Nazionale delle Ricerche, Frascati (Italy). Lab. di Astrofisica Spaziale); Manchanda, R.K. (Tata Inst. of Fundamental Research, Bombay (India))

1984-07-01

A general purpose method to deconvolve the energy spectra detected by means of the use of a hard X-ray telescope is described. The procedure does not assume any form of input spectrum and the observed energy loss spectrum is directly deconvolved into the incident photon spectrum, the form of which can be determined independently of physical interpretation of the data. Deconvolution of the hard X-ray spectrum of Her X-1, detected during the HXR 81M experiment, by the method independent method is presented.

Ultraprecision motion control technique for high-resolution x-ray instrumentation

Energy Technology Data Exchange (ETDEWEB)

Shu, D.; Toellner, T. S.; Alp, E. E.

2000-07-17

With the availability of third-generation hard x-ray synchrotron radiation sources, such as the Advanced Photon Source (APS) at Argonne National Laboratory, x-ray inelastic scattering and x-ray nuclear resonant scattering provide powerful means for investigating the vibrational dynamics of a variety of materials and condensed matter systems. Novel high-resolution hard x-ray optics with meV energy resolution requires a compact positioning mechanism with 20--50-nrad angular resolution and stability. In this paper, the authors technical approach to this design challenge is presented. Sensitivity and stability test results are also discussed.

Modelling the flaring activity of the high-z, hard X-ray-selected blazar IGR J22517+2217: Flaring activity of IGR J22517+2217

International Nuclear Information System (INIS)

Lanzuisi, G.; De Rosa, A.; Ghisellini, G.; Panessa, F.

2012-01-01

We present new Suzaku and Fermi data and re-analysed archival hard X-ray data from the INTErnational Gamma-Ray Astrophysics Laboratory (INTEGRAL) and Swift–Burst Alert Telescope (BAT) surveys to investigate the physical properties of the luminous, high-redshift, hard X-ray-selected blazar IGR J22517+2217, through the modelling of its broad-band spectral energy distribution (SED) in two different activity states. Through analysis of new Suzaku data and flux-selected data from archival hard X-ray observations, we build the source SED in two different states, one for the newly discovered flare that occurred in 2005 and one for the following quiescent period. Both SEDs are strongly dominated by the high-energy hump peaked at 10 20 –10 22 Hz, which is at least two orders of magnitude higher than the low-energy (synchrotron) one at 10 11 –10 14 Hz and varies by a factor of 10 between the two states. In both states the high-energy hump is modelled as inverse Compton emission between relativistic electrons and seed photons produced externally to the jet, while the synchrotron self-Compton component is found to be negligible. In our model the observed variability can be accounted for by a variation of the total number of emitting electrons and by a dissipation region radius changing from inside to outside the broad-line region as the luminosity increases. In its flaring activity, IGR J22517+2217 is revealed as one of the most powerful jets among the population of extreme, hard X-ray-selected, high-redshift blazars observed so far.

K-Edge Subtraction Angiography with Synchrotron X-Rays

CERN Document Server

Giacomini, J C

1996-01-01

The purpose of this project was to utilize dual energy, monochromatic X-rays produced from synchrotrons radiation in order to obtain noninvasive medical imaging. The application of synchrotrons radiation to medical imaging is based on the principle of iodine dichromography, first described by Bertil Jacobson of the Karolinska Institute in 1953. Medical imaging using synchrotrons radiation and K-edge dichromography was pioneered at Stanford University under the leadership of Dr. Ed Rubenstein, and the late Nobel Laureate in Physics, Dr. Robert Hofstadter. With progressive refinements in hardware, clinical-quality images were obtained of human coronary arteries utilizing peripheral injections of iodinated contrast agent. These images even now are far superior to those being presented by investigators using MRI as an imaging tool for coronary arteries. However, new supplies and instruments in the cardiac catheterization laboratory have served to transform coronary angiography into an outpatient procedure, with r...

Great microwave bursts and hard X-rays from solar flares

International Nuclear Information System (INIS)

Wiehl, H.J.; Batchelor, D.A.; Crannell, C.J.; Dennis, B.R.; Price, P.N.

1983-06-01

The microwave and hard X-ray charateristics of 13 solar flares that produced microwave fluxes greater than 500 Solar Flux Units were analyzed. These Great Microwave Bursts were observed in the frequency range from 3 to 35 GHz at Berne, and simultaneous hard X-ray observations were made in the energy range from 30 to 500 keV with the Hard X-Ray Burst Spectrometer on the Solar Maximum Mission spacecraft. The principal aim of this analysis is to determine whether or not the same distribution of energetic electrons can explain both emissions. Correlations were found between respective temporal characteristics and, for the first time, between microwave and hard X-ray spectral characteristics. A single-temperature and a multi-temperature model from the literature were tested for consistency with the coincident X-ray and microwave spectra at microwave burst maximum. Four events are inconsistent with both of the models tested, and neither of the models attempts to explain the high-frequency part of the microwave spectrum. A model in which the emissions above and below the peak frequency originate in two different parts of a diverging magnetic loop is proposed. With this model the entire microwave spectrum of all but one of the events is explained

The Relationship Between Solar Radio and Hard X-Ray Emission

Science.gov (United States)

White, S. M.; Benz, A. O.; Christe, S.; Farnik, F.; Kundu, M. R.; Mann, G.; Ning, Z.; Raulin, J.-P.; Silva-Valio, A. V. R.; Saint-Hilaire, P.;

Synchrotron X-ray fluorescence analysis in environmental and earth sciences

Directory of Open Access Journals (Sweden)

Adams F.

2010-12-01

Full Text Available Compared to other microscopic analytical tools X-ray microscopy techniques have the advantage that the large penetration depth of X-rays in matter allows one to investigate the interior of an object without destructive sample preparation. In combination with X-ray fluorescence tomography, analytical information from inside of a specimen can be obtained. Different X-ray analytical techniques can be used to produce contrast, X-ray absorption, fluorescence, and diffraction, to yield chemical, elemental, and structural information about the sample. Scanning microscopy on the basis of various lens systems in synchrotron radiation sources provides a routine spatial resolution of now about 100 nanometer but in the foreseeable future a 10–20 nanometer spatial resolution can be expected. X-ray absorption spectrometry can also provide chemical (speciation information on the sample. All this makes X-ray microscopy attractive to many fields of science. In this paper the techniques are briefly reviewed and a number of applications in the earth, planetary and cosmos sciences are illustrated with state-of-the art examples, while applications in the environmental sciences and biology are also briefly discussed.

Nanometer Linear Focusing of Hard X Rays by a Multilayer Laue Lens

International Nuclear Information System (INIS)

Kang, H.C.; Stephenson, G.B.; Maser, J.; Liu, C.; Conley, R.; Macrander, A.T.; Vogt, S.

2006-01-01

We report on a type of linear zone plate for nanometer-scale focusing of hard x rays, a multilayer Laue lens (MLL), produced by sectioning a multilayer and illuminating it in Laue diffraction geometry. Because of its large optical depth, a MLL spans the diffraction regimes applicable to a thin Fresnel zone plate and a crystal. Coupled wave theory calculations indicate that focusing to 5 nm or smaller with high efficiency should be possible. Partial MLL structures with outermost zone widths as small as 10 nm have been fabricated and tested with 19.5 keV synchrotron radiation. Focal sizes as small as 30 nm with efficiencies up to 44% are measured

Measurement of spherical compound refractive X-ray lens at ANKA synchrotron radiation source

International Nuclear Information System (INIS)

Dudchik, Yu.I.; Simon, R.; Baumbach, T.

2007-01-01

Parameters of compound refractive X-ray lens were measured at ANKA synchrotron radiation source. The lens consists of 224 spherical concave epoxy microlenses formed inside glass capillary. The curvature radius of individual microlens is equal to 100 microns. Measured were: X-ray focal spot, lens focal length and gain in intensity. The energy of X-ray beam was equal to 12 keV and 14 keV. It is shown that when X-ray lens is used, the gain in intensity of the X-ray beam in some cases may exceed value of 100. Tested lens is suitable to focus X-rays into, at least, 2-microns in size spot. (authors)

Hard x- and gamma-rays from supernova 1987A

International Nuclear Information System (INIS)

Kumagai, S.; Shigeyama, T.; Nomoto, K.; Nishmura, J.; Itoh, M.

1988-01-01

The x-ray light curve and spectrum from SN 1987A due to Compton degradation of γ-rays from the 56 Co decay are calculated and compared with the Ginga and Kvant observations. If mixing of 56 Co into outer layers has taken place, the x-rays emerge much earlier than in the case without mixing and the resulting hard x-rays are in reasonable agreement with observations

A gas microstrip wide angle X-ray detector for application in synchrotron radiation experiments

CERN Document Server

Bateman, J E; Derbyshire, G E; Duxbury, D M; Lipp, J; Mir, J A; Simmons, J E; Spill, E J; Stephenson, R; Dobson, B R; Farrow, R C; Helsby, W I; Mutikainen, R; Suni, I

2002-01-01

The Gas Microstrip Detector has counting rate capabilities several orders of magnitude higher than conventional wire proportional counters while providing the same (or better) energy resolution for X-rays. In addition the geometric flexibility provided by the lithographic process combined with the self-supporting properties of the substrate offers many exciting possibilities for X-ray detectors, particularly for the demanding experiments carried out on Synchrotron Radiation Sources. Using experience obtained in designing detectors for Particle Physics we have developed a detector for Wide Angle X-ray Scattering studies. The detector has a fan geometry which makes possible a gas detector with high detection efficiency, sub-millimetre spatial resolution and good energy resolution over a wide range of X-ray energy. The detector is described together with results of experiments carried out at the Daresbury Laboratory Synchrotron Radiation Source.

Application of X-rays and Synchrotron X Rays to Residual Stress Evaluation Near Surfaces

International Nuclear Information System (INIS)

Pyzalla, Anke

1999-01-01

A nondestructive residual stress analysis can be performed using diffraction methods. The easiest accessible radiation is characteristic X radiation that has a penetration depth of ∼10 microm suitable for the determination of the residual stresses in near-surface layers. Special techniques have been developed, e.g., with respect to in situ analyses of the stress state in oxide layers and the residual stress analysis in coarse grained zones of steel welds or annealed Ni-base alloys. Depending on the size of the gauge volume, neutron diffraction can provide information at depths of tens of millimetres of steel and many tens of millimetres of Al. An alternative to the use of the characteristic synchrotron radiation is the use of a high-energy polychromatic beam in an energy dispersive arrangement, which gives access to higher penetration depths at still gauge volumes as small as 100 microm x 100 microm x 1 mm in steel rods of 15-mm diameter. The combination of neutrons with conventional X rays and monochromatic and polychromatic synchrotron radiation allows for a comprehensive investigation of the phase composition, the texture, and the residual stresses

Progress in Cell Marking for Synchrotron X-ray Computed Tomography

Science.gov (United States)

Hall, Christopher; Sturm, Erica; Schultke, Elisabeth; Arfelli, Fulvia; Menk, Ralf-Hendrik; Astolfo, Alberto; Juurlink, Bernhard H. J.

2010-07-01

Recently there has been an increase in research activity into finding ways of marking cells in live animals for pre-clinical trials. Development of certain drugs and other therapies crucially depend on tracking particular cells or cell types in living systems. Therefore cell marking techniques are required which will enable longitudinal studies, where individuals can be examined several times over the course of a therapy or study. The benefits of being able to study both disease and therapy progression in individuals, rather than cohorts are clear. The need for high contrast 3-D imaging, without harming or altering the biological system requires a non-invasive yet penetrating imaging technique. The technique will also have to provide an appropriate spatial and contrast resolution. X-ray computed tomography offers rapid acquisition of 3-D images and is set to become one of the principal imaging techniques in this area. Work by our group over the last few years has shown that marking cells with gold nano-particles (GNP) is an effective means of visualising marked cells in-vivo using x-ray CT. Here we report the latest results from these studies. Synchrotron X-ray CT images of brain lesions in rats taken using the SYRMEP facility at the Elettra synchrotron in 2009 have been compared with histological examination of the tissues. Some deductions are drawn about the visibility of the gold loaded cells in both light microscopy and x-ray imaging.

Beryllium window flange for synchrotron radiation X-ray beamline fabricated by hot isostatic press method

International Nuclear Information System (INIS)

Asaoka, Seiji; Maezawa, Hideki; Nishida, Kiyotoshi; Sakamoto, Naoki.

1995-01-01

The synchrotron radiation experimental facilities in National Laboratory for High Energy Physics are the experimental facilities for joint utilization, that possess the positron storage ring of 2.5 GeV exclusively used for synchrotron radiation. Synchrotron radiation is led through a mainstay beam channel to the laboratory, and in the beam line of X-ray, it is used for experiment through the taking-out window made of beryllium. At this time, the function of the taking-out window is to shut off between the ultrahigh vacuum in the mainstay beam channel and the atmosphere, and to cut the low energy component of synchrotron radiation spectra. The experiment using X-ray is carried out mostly in the atmosphere. The design of the efficient cooling water channel which is compatible with the flange construction is important under the high thermal load of synchrotron radiation. The beryllium window flange for synchrotron radiation X-ray was made by HIP method, and the ultrahigh vacuum test, the high pressure water flow test and the actual machine test were carried out by heat cycle. The properties required for the window material, the requirement of the construction, the new development of HIP method, and the experiments for evaluating the manufactured beryllium window are described. (K.I.)

Hard X-ray spectrum of Her X-1

International Nuclear Information System (INIS)

Ubertini, P.; Bazzano, A.; La Padula, C.D.; Polcaro, V.F.

1981-01-01

The results of a balloon borne hard X-ray observation of Her X-1 is presented. The experiment, released from the base of Hyderabad (India) the 19th April 1980, was a collaboration between the Istituto di Astrofisica Spaziale (Italy) and the TIFR (India). The data obtained are compatible with a thermal emission at low energy with a strong emission line overimposed on the continuum around 50-60 keV

A CCD-based area detector for X-ray crystallography using synchrotron and laboratory sources

International Nuclear Information System (INIS)

Phillips, W.C.; Li Youli; Stanton, M.; Xie Yuanhui; O'Mara, D.; Kalata, K.

1993-01-01

The design and characteristics of a CCD-based area detector suitable for X-ray crystallographic studies using both synchrotron and laboratory sources are described. The active area is 75 mm in diameter, the FWHM of the point response function is 0.20 mm, and for Bragg peaks the dynamic range is 900 and the DQE ∼0.3. The 1320x1035-pixel Kodak CCD is read out into an 8 Mbyte memory system in 0.14 s and digitized to 12 bits. X-ray crystallographic data collected at the NSLS synchrotron from cubic insulin crystals are presented. (orig.)

Synchrotron radiation sources: their properties and applications for VUV and X-ray spectroscopy

International Nuclear Information System (INIS)

Koch, E.E.

1976-09-01

Synchrotron radiation from accelerators and storage rings offers far reaching possibilities for many fields of basic and applied physics. The properties of synchrotron radiation, existing and planned synchrotron radiation facilities, as well as instrumental aspects are discussed. In order to illustrate the usefulness of the synchrotron radiation sources a few highlights from atomic, molelucar, and solid state spectroscopy are presented and examples from x-ray experiments and from the field of applied physics are given. (orig.) [de

Glancing angle synchrotron X-ray diffraction

Energy Technology Data Exchange (ETDEWEB)

Cernik, R J [Daresbury Lab., Warrington, WA (United States)

1996-09-01

This paper describes in basic detail some of the techniques that can be used to study thin films and surfaces. These are all in the X-ray region and cover reflectivity, diffraction form polycrystalline films, textured films and single crystal films. Other effects such as fluorescence and diffuse scattering are mentioned but not discussed in detail. Two examples of the reflectivity from multilayers and the diffraction from iron oxide films are discussed. The advantages of the synchrotron for these studies is stressed and the experimental geometries that can be employed are described i detail. A brief bibliography is provided at the end to accompany this part of the 1996 Frascati school.

Glancing angle synchrotron X-ray diffraction

International Nuclear Information System (INIS)

Cernik, R.J.

1996-01-01

This paper describes in basic detail some of the techniques that can be used to study thin films and surfaces. These are all in the X-ray region and cover reflectivity, diffraction form polycrystalline films, textured films and single crystal films. Other effects such as fluorescence and diffuse scattering are mentioned but not discussed in detail. Two examples of the reflectivity from multilayers and the diffraction from iron oxide films are discussed. The advantages of the synchrotron for these studies is stressed and the experimental geometries that can be employed are described i detail. A brief bibliography is provided at the end to accompany this part of the 1996 Frascati school

A SUZAKU SEARCH FOR NONTHERMAL EMISSION AT HARD X-RAY ENERGIES IN THE COMA CLUSTER

International Nuclear Information System (INIS)

Wik, Daniel R.; Sarazin, Craig L.; Finoguenov, Alexis; Matsushita, Kyoko; Nakazawa, Kazuhiro; Clarke, Tracy E.

2009-01-01

The brightest cluster radio halo known resides in the Coma cluster of galaxies. The relativistic electrons producing this diffuse synchrotron emission should also produce inverse Compton emission that becomes competitive with thermal emission from the intracluster medium (ICM) at hard X-ray energies. Thus far, claimed detections of this emission in Coma are controversial. We present a Suzaku HXD-PIN observation of the Coma cluster in order to nail down its nonthermal hard X-ray content. The contribution of thermal emission to the HXD-PIN spectrum is constrained by simultaneously fitting thermal and nonthermal models to it and a spatially equivalent spectrum derived from an XMM-Newton mosaic of the Coma field. We fail to find statistically significant evidence for nonthermal emission in the spectra which are better described by only a single- or multitemperature model for the ICM. Including systematic uncertainties, we derive a 90% upper limit on the flux of nonthermal emission of 6.0 x 10 -12 erg s -1 cm -2 (20-80 keV, for Γ = 2.0), which implies a lower limit on the cluster-averaged magnetic field of B>0.15 μG. Our flux upper limit is 2.5 times lower than the detected nonthermal flux from RXTE and BeppoSAX. However, if the nonthermal hard X-ray emission in Coma is more spatially extended than the observed radio halo, the Suzaku HXD-PIN may miss some fraction of the emission. A detailed investigation indicates that ∼50%-67% of the emission might go undetected, which could make our limit consistent with that of Rephaeli and Gruber and Fusco-Femiano et al. The thermal interpretation of the hard Coma spectrum is consistent with recent analyses of INTEGRAL and Swift data.

Development and application of cryogenic radiometry with hard X-rays; Entwicklung und Anwendung der Kryoradiometrie mit harter Roentgenstrahlung

Energy Technology Data Exchange (ETDEWEB)

Gerlach, Martin

2008-06-06

To establish cryogenic radiometry with hard X-ray radiation for photon energies of up to 60 keV, a novel type of cavity absorber had to be developed for the cryogenic radiometer SYRES I, which is deployed by the Physikalisch-Technische Bundesanstalt (PTB) as primary standard detector at the electron storage ring BESSY II. This new type of cavity absorber allows for the complete absorption of hard X-ray radiation in combination with an appropriate sensitivity and an adequate time constant for the measurement of synchrotron radiation at BESSY II. As the process of fabrication of different types of absorbers is very time-consuming, the interaction of hard X-ray radiation with different absorber materials and geometries was studied intensively by using the Monte Carlo simulation code Geant4. The accuracy of the simulations was verified comparing them to scattering experiments performed at a wavelength shifter beamline at BESSY II with a calibrated energy dispersive detector. It was shown that Geant4 describes the photo-effect, including fluorescence as well as Compton- and Rayleigh scattering, with high accuracy. The simulations and experiments resulted in a cavity absorber with a gold base 550 {mu}m in thickness and a cylindrical shell made of copper 90 {mu}m in thickness to reduce losses caused by fluorescence and scattered radiation. Monochromatized synchrotron radiation of high spectral purity was then used to calibrate semiconductor photodiodes, which can be used as compact and inexpensive secondary standard detectors, against a cryogenic radiometer, covering the entire photon energy range of three beamlines from 50 eV to 60 keV with relative uncertainties of less than 0.5 %. Furthermore the spatial homogeneity of the spectral responsivity, the transmittance and the linearity of the photodiodes was investigated. Through a direct comparison of the free-air ionization chamber PK100, a primary detector standard of PTB used in dosimetry, and the cryogenic radiometer

Conical geometry for sagittal focusing as applied to X rays from synchrotrons

International Nuclear Information System (INIS)

Ice, G.E.; Sparks, C.J.

1993-06-01

The authors describe a method for simultaneously focusing and monochromatization of X rays from a fan of radiation having up to 15 mrad divergence in one dimension. This geometry is well suited to synchrotron radiation sources at magnifications of one-fifth to two and is efficient for X-ray energies between 3 and 40 keV (0.48 and 6.4 fJ). The method uses crystals bent to part of a cone for sagittal focusing and allows for the collection of a larger divergence with less mixing of the horizontal into the vertical divergence than is possible with X-ray mirrors. They describe the geometry required to achieve the highest efficiency when a conical crystal follows a flat crystal in a nondispersive two-crystal monochromator. At a magnification of one-third, the geometry is identical to a cylindrical focusing design described previously. A simple theoretical calculation is shown to agree well with ray-tracing results. Minimum aberrations are observed at magnifications near one. Applications of the conical focusing geometry to existing and future synchrotron radiation facilities are discussed

W/SiC X-ray multilayers optimized for use above 100 keV

DEFF Research Database (Denmark)

Windt, D.L.; Dongey, S.; Hailey, C.J.

2002-01-01

-derived optical constants, which we determined from reflectance-vs-incidence angle measurements also made using synchrotron radiation, in the range E=120 - 180 keV. We describe our experimental investigation in detail, compare the new W/SiC multilayers with both W/Si and W/B4C films that have been studied......We have developed a new depth-graded multilayer system comprising W and SiC layers, suitable for use as hard X-ray reflective coatings operating in the energy range 100 - 200 keV. Grazing incidence X-ray reflectance at E=8 keV was used to characterize the interface widths, as well as the temporal...... and thermal stability in both periodic and depth-graded W/SiC structures, while synchrotron radiation was used to measure the hard X-ray reflectance of a depth-graded multilayer designed specifically for use in the range Esimilar to150 - 170 keV. We have modeled the hard X-ray reflectance using newly...

W/SiC x-ray multilayers optimized for use above 100 keV

DEFF Research Database (Denmark)

Windt, D.L.; Donguy, S.; Hailey, C.J.

2003-01-01

optical constants, which we determined from reflectance versus incidence angle measurements also made using synchrotron radiation, in the range E = 120-180 keV. We describe our experimental investigation in detail, compare the new W/SiC multilayers with both W/Si and W/B4C films that have been studied......We have developed a new depth-graded multilayer system comprising W and SiC layers, suitable for use as hard x-ray reflective coatings operating in the energy range 100-200 keV. Grazing-incidence x-ray reflectance at E = 8 keV was used to characterize the interface widths, as well as the temporal...... and thermal stability in both periodic and depth-graded W/SiC structures, whereas synchrotron radiation was used to measure the hard x-ray reflectance of a depth-graded multilayer designed specifically for use in, the range Esimilar to150-170 keV. We have modeled the hard x-ray reflectance using newly derived...

Time-resolved x-ray diffraction measurement of C{sub 60} under high pressure and temperature using synchrotron radiation

Energy Technology Data Exchange (ETDEWEB)

Horikawa, T [Graduate School of Engineering Science, Osaka University, Toyonaka, Osaka 560-8531 (Japan); Suito, K [Graduate School of Engineering Science, Osaka University, Toyonaka, Osaka 560-8531 (Japan); Kobayashi, M [Graduate School of Engineering Science, Osaka University, Toyonaka, Osaka 560-8531 (Japan); Onodera, A [Graduate School of Engineering Science, Osaka University, Toyonaka, Osaka 560-8531 (Japan)

2002-11-11

C{sub 60} has been studied by means of time-resolved x-ray diffraction measurements using synchrotron radiation. Diffraction patterns were recorded at intervals of 1-10 min for samples under high pressure (12.5 and 14.3 GPa) and high temperature (up to 800 deg. C) for, at the longest, 3 h. Time, pressure, and temperature dependences of the C{sub 60} structure are presented and the relevance to the hardness of materials derived from C{sub 60} is discussed.

Energy-dispersive X-ray diffraction beamline at Indus-2 synchrotron ...

Indian Academy of Sciences (India)

An energy-dispersive X-ray diffraction beamline has been designed, developed and commissioned at BL-11 bending magnet port of the Indian synchrotron source, Indus-2. The performance of this beamline has been benchmarked by measuring diffraction patterns from various elemental metals and standard inorganic ...

The 105-Month Swift-BAT All-Sky Hard X-Ray Survey

Science.gov (United States)

Oh, Kyuseok; Koss, Michael; Markwardt, Craig B.; Schawinski, Kevin; Baumgartner, Wayne H.; Barthelmy, Scott D.; Cenko, S. Bradley; Gehrels, Neil; Mushotzky, Richard; Petulante, Abigail;

Hard X-ray balloon observations of compact galactic and extragalactic X-ray sources

International Nuclear Information System (INIS)

Staubert, R.; Kendziorra, E.; Pietsch, W.; Proctor, R.J.; Reppin, C.; Steinle, H.; Truemper, J.; Voges, W.

1981-01-01

A balloon program in hard X-ray astronomy (20-200 keV) is jointly pursued by the Astronomisches Institut der Universitaet Tuebingen (AIT) and the Max Planck-Institut fuer Extraterrestrische Physik in Garching (MPE). Since 1973 nine succussful balloon flights have been performed from Texas and Australia. Here results on Centaurus A and on several galactic binary X-ray sources are summarized. In particular the high energy photon spectrum of Hercules X-1 and the evidence for the cyclotron line feature which was discovered by us in 1976 is reviewed. (orig.)

Measurement of X-ray mass attenuation coefficient of nickel around the K-edge using synchrotron radiation based X-ray absorption study

International Nuclear Information System (INIS)

Roy, Bunty Rani; Rajput, Parasmani; Jha, S.N.; Nageswara Rao, A.S.

2015-01-01

The work presents the X-ray absorption fine structure (XAFS) technique for measuring the X-ray mass attenuation coefficient of nickel metal foil in the X-ray energy range of 8271.2–8849.4 eV using scanning XAFS beam line (BL-09) at Indus-2 synchrotron radiation source facility, Raja Ramanna Centre for Advanced Technology (RRCAT) at Indore, India. The result represents the X-ray mass attenuation coefficient data for 0.02 mm thick Ni metal foil in the XAFS region of Ni K-edge. However, the results are compared to theoretical values using X-COM. There is a maximum deviation which is found exactly near the K-edge jump and decreases as we move away from the absorption edge. Oscillatory structure appears just above the observed absorption edge i.e., 8348.7 eV and is confined to around 250 eV above the edge. - Highlights: • Mass attenuation coefficient measurements of nickel using synchrotron radiation. • The measurements were taken exactly near the Ni K-edge at an energy step of 1 eV. • A maximum deviation is found near the K-edge

Design and Tests of the Hard X-ray Polarimeter X-Calibur

Directory of Open Access Journals (Sweden)

M. Beilicke

2014-12-01

Full Text Available X-ray polarimetry promises to give qualitatively new information bout high-energy astrophysical sources, such as binary black hole  systems, micro-quasars, active galactic nuclei, and gamma-ray bursts. We designed, built and tested ahard X-ray polarimeter, X-Calibur, to be used in the focal plane of the InFOCuS grazing incidence hard X-ray telescope.X-Calibur combines a low-Z Compton scatterer with a CZT detector assembly to measure the polarization of 20−60 keV X-rays making use of the fact that polarized photons Compton scatter preferentially perpendicular to the electric field orientation; in principal, a similar space-borne experiment could be operated in the 5−100 keV regime. X-Calibur achieves a high detection efficiency of order unity.

Hard X-ray intensity reduction during lower hybrid current drive experiments

International Nuclear Information System (INIS)

Mlynar, J.; Stoeckel, J.; Magula, P.

1993-01-01

A strong hard X-ray intensity reduction during a standard LHCD at the CASTOR tokamak was studied. From discussion it followed that the magnetic fluctuations level decrease is likely to be responsible for this effect beside the loop voltage decrease. To verify this idea, the connection between the magnetic fluctuation level and the hard X-ray intensity was studied in a nonstandard LHCD regime with a zero loop voltage reduction. These measurements strongly supported the concept that magnetic fluctuations level substantially influences the runaway electrons cross-field transport. Though, more data and a good code for modelling the anomalous transport and hard X-rays production would be of high value. Similar measurements especially for higher RF power should be carried out soon. Besides, the reduction of hard X-rays was observed in the experiments with edge plasma polarization lately; therefore, the magnetic fluctuations level in these experiments should be studied soon. (author) 6 figs., 6 refs

Measuring Cavitation with Synchrotron X-Rays

Science.gov (United States)

Duke, Daniel; Kastengren, Alan; Powell, Chris; X-Ray Fuel Spray Group, Energy Systems Division Team

2012-11-01

Cavitation plays an important role in the formation of sprays from small nozzles such as those found in fuel injection systems. A sharp-edged inlet from the sac into the nozzle of a diesel fuel injector is shown to inititate a strong sheet-like cavitation along the boundary layer of the nozzle throat, which is difficult to measure and can lead to acoustic damage. To investigate this phenomenon, a diagnostic technique capable of mapping the density field of the nozzle through regions of intense cavitation is required. Available visible-light techniques are limited to qualitative observations of the outer extent of cavitation zones. However, brilliant X-rays from a synchrotron source have negligible refraction and are capable of penetrating the full extent of cavitation zones. We present the early results of a novel application of line-of-sight, time-resolved X-ray radiography on a cavitating model nozzle. Experiments were conducted at Sector 7-BM of the Advanced Photon Source. Density and vapor distribution are measured from the quantitative absorption of monochromatic X-rays. The density field can then be tomographically reconstructed from the projections. The density is then validated against a range of compressible and incompressible numerical simulations. This research was performed at the 7-BM beamline of the Advanced Photon Source. We acknowledge the support of the U.S. Department of Energy under Contract No. DE-AC02-06CH11357 and the DOE Vehicle Technologies Program (DOE-EERE).

Calcified-tissue investigations using synchrotron x-ray microscopy

International Nuclear Information System (INIS)

Jones, K.W.; Spanne, P.; Schidlovsky, G.; Dejun, X.; Bockman, R.S.; Hammond, P.B.; Bornschein, R.L.; Hoeltzel, D.A.

1990-10-01

Synchrotron x-ray microscopy (SXRM) in both emission and absorption modes has been used to examine elemental distributions in specimens of rat tibia, human deciduous teeth, and an orthopedic implant phantom. The work was performed with a spatial resolution of 8 μm for the emission work and 25 μm for the absorption work. The results illustrate the usefulness of SXRM for measurements of different types of calcified tissue. 3 figs

Guiding hard x rays with glass polycapillary fiber

International Nuclear Information System (INIS)

Xiao, Q.F.; Ponomarev, I.Y.; Kolomitsev, A.I.; Gibson, D.M.; Dilmanian, F.A.; Nachaliel, E.

1993-01-01

X rays can be guided through a polycapillary fiber by multiple total reflections from the smooth channel walls of the fiber. Using monochromatic Synchrotron Radiation at energies of 22 and 44 keV, we measured the efficiency of transmission of x rays through polycapillary fibers with channel diameters of about 13 μm. Efficiencies of 57.3% and 54.5% for 22 keV and 44 keV x rays, respectively, were obtained with a 120-mm-long straight polycapillary fiber aligned with the incident beam. These values are close to the open fraction of the fiber, which is about 60%. In addition, transmission efficiency was measured as a function of the tilt angle between the incident beam and the axis of the fiber. We also measured the transmission efficiency as a function of the deflection angle for a 114-mm-long curved polycapillary fiber. The measurements are compared with a ray-tracing simulation

Utilization of synchrotron radiation in analytical chemistry. Soft X-ray emission and absorption spectroscopy

International Nuclear Information System (INIS)

Muramatsu, Yasuji

2015-01-01

Synchrotron soft X-ray spectroscopy includes three major types of spectroscopy such as X-ray absorption spectroscopy (XAS), X-ray emission spectroscopy (XES), and X-ray photoelectron spectroscopy (XPS). This paper takes up XAS and XES of soft X-rays, and briefly describes the principle. XAS is roughly classified into XANES (X-ray absorption near-edge structure) and EXAFS (extended X-ray absorption fine structure), and XANES is mainly used in the analysis based on XAS of soft X-rays. As the examples of the latest soft X-ray analyses, the following are introduced: (1) bandgap of boron implantation diamond and the local structure of boron, (2) catalytic sites in solid fuel cell carbon electrode, and (3) soft X-ray analysis under atmospheric pressure. (A.O.)

Hard X-ray bursts and DD microfusion neutrons from complex ...

Indian Academy of Sciences (India)

explosive destruction of micrograins is accompanied by X-ray radiation (during hydrody- ... makes it possible to produce lasing in hard X-rays due to the effects of multiple scattering ... portant, information on the X-ray random media, including some indirect diagnostics. In ... stages of ionization in the total flux of particles.

Bulk sensitive hard x-ray photoemission electron microscopy

Energy Technology Data Exchange (ETDEWEB)

Patt, M., E-mail: m.patt@fz-juelich.de; Wiemann, C. [Peter Grünberg Institute (PGI-6) and JARA-FIT, Research Center Jülich, D-52425 Jülich (Germany); Weber, N.; Escher, M.; Merkel, M. [Focus GmbH, Neukirchner Str. 2, D-65510 Hünstetten (Germany); Gloskovskii, A.; Drube, W. [DESY Photon Science, Deutsches Elektronen-Synchrotron, D-22603 Hamburg (Germany); Schneider, C. M. [Peter Grünberg Institute (PGI-6) and JARA-FIT, Research Center Jülich, D-52425 Jülich (Germany); Fakultät f. Physik and Center for Nanointegration Duisburg-Essen (CeNIDE), Universität Duisburg-Essen, D-47048 Duisburg (Germany)

2014-11-15

Hard x-ray photoelectron spectroscopy (HAXPES) has now matured into a well-established technique as a bulk sensitive probe of the electronic structure due to the larger escape depth of the highly energetic electrons. In order to enable HAXPES studies with high lateral resolution, we have set up a dedicated energy-filtered hard x-ray photoemission electron microscope (HAXPEEM) working with electron kinetic energies up to 10 keV. It is based on the NanoESCA design and also preserves the performance of the instrument in the low and medium energy range. In this way, spectromicroscopy can be performed from threshold to hard x-ray photoemission. The high potential of the HAXPEEM approach for the investigation of buried layers and structures has been shown already on a layered and structured SrTiO{sub 3} sample. Here, we present results of experiments with test structures to elaborate the imaging and spectroscopic performance of the instrument and show the capabilities of the method to image bulk properties. Additionally, we introduce a method to determine the effective attenuation length of photoelectrons in a direct photoemission experiment.

Apparatus development for high-pressure X-ray diffraction using synchrotron radiation

International Nuclear Information System (INIS)

Martinez, L.G.; Orlando, M.T.D.; Rossi, J.L.; Passamai Junior, J.L.; Melo, F.C.L.; Ferreira, F.F.

2006-01-01

Some phenomena in the field of condensed matter physics can be studied when the matter is submitted to extreme conditions of pressure, magnetic fields or temperatures. Once submitted to these conditions it is generally necessary to measure the properties of the matter in situ. The existence of a synchrotron light laboratory in Brazil opens up the chance of studying materials in extreme conditions by techniques like X-ray diffraction and absorption. However, when compared to high-energy synchrotrons accelerators, the Brazilian source offers a narrower energy range and lower flux. These facts impose limitation to perform diffraction experiments by energy dispersion and, consequently, the use of pressure cells with denser anvils like diamond. However, for a lower-pressure range, preliminary studies showed the viability of measurements in an angular dispersion configuration. This allows the use of silicon carbide anvils B 4C . In this work it is described the development of a hydrostatic pressure cell suitable for X-rays diffraction measurements in the Brazilian Synchrotron Light Laboratory using materials and technologies developed by the institutions and researchers involved in this project (IPEN, UFES, CTA and LNLS). This development can provide the scientific community with the possibility of performing X-ray diffraction measurements under hydrostatic pressure, initially up to 2 GPa, with possibilities of increasing the maximum pressure to higher values, with or without application of magnetic fields and high or low temperatures. (author)

In-Situ Synchrotron X-ray Study of the Phase and Texture Evolution of Ceria and Superconductor Films Deposited by Chemical Solution Method

DEFF Research Database (Denmark)

Yue, Zhao; Grivel, Jean-Claude; He, Dong

2012-01-01

In situ synchrotron x-ray diffraction is used to study the phase and texture formation of ceria based films and superconductor films deposited by the chemical solution method on technical substrates. Combined analysis using in situ synchrotron x-ray diffraction, thermogravimetry/differential ther......In situ synchrotron x-ray diffraction is used to study the phase and texture formation of ceria based films and superconductor films deposited by the chemical solution method on technical substrates. Combined analysis using in situ synchrotron x-ray diffraction, thermogravimetry...

Combined X-ray fluorescence and absorption computed tomography using a synchrotron beam

International Nuclear Information System (INIS)

Hall, C

2013-01-01

X-ray computed tomography (CT) and fluorescence X-ray computed tomography (FXCT) using synchrotron sources are both useful tools in biomedical imaging research. Synchrotron CT (SRCT) in its various forms is considered an important technique for biomedical imaging since the phase coherence of SR beams can be exploited to obtain images with high contrast resolution. Using a synchrotron as the source for FXCT ensures a fluorescence signal that is optimally detectable by exploiting the beam monochromaticity and polarisation. The ability to combine these techniques so that SRCT and FXCT images are collected simultaneously, would bring distinct benefits to certain biomedical experiments. Simultaneous image acquisition would alleviate some of the registration difficulties which comes from collecting separate data, and it would provide increased information about the sample: functional X-ray images from the FXCT, with the morphological information from the SRCT. A method is presented for generating simultaneous SRCT and FXCT images. Proof of principle modelling has been used to show that it is possible to recover a fluorescence image of a point-like source from an SRCT apparatus by suitably modulating the illuminating planar X-ray beam. The projection image can be successfully used for reconstruction by removing the static modulation from the sinogram in the normal flat and dark field processing. Detection of the modulated fluorescence signal using an energy resolving detector allows the position of a fluorescent marker to be obtained using inverse reconstruction techniques. A discussion is made of particular reconstruction methods which might be applied by utilising both the CT and FXCT data.

Iron overload of human colon adenocarcinoma cells studied by synchrotron-based X-ray techniques

NARCIS (Netherlands)

Mihucz, Victor G.; Meirer, Florian; Polgári, Zsófia; Réti, Andrea; Pepponi, Giancarlo; Ingerle, Dieter; Szoboszlai, Norbert; Streli, Christina

2016-01-01

Fast- and slow-proliferating human adenocarcinoma colorectal cells, HT-29 and HCA-7, respectively, overloaded with transferrin (Tf), Fe(III) citrate, Fe(III) chloride and Fe(II) sulfate were studied by synchrotron radiation total-reflection X-ray spectrometry (TXRF), TXRF-X-ray absorption near edge

Characterization of a next-generation piezo bimorph X-ray mirror for synchrotron beamlines

Energy Technology Data Exchange (ETDEWEB)

Alcock, Simon G., E-mail: simon.alcock@diamond.ac.uk; Nistea, Ioana; Sutter, John P.; Sawhney, Kawal [Diamond Light Source, Harwell Science and Innovation Campus, Didcot, Oxfordshire OX11 0DE (United Kingdom); Fermé, Jean-Jacques; Thellièr, Christophe; Peverini, Luca [Thales-SESO, 305 rue Louis Armand, Pôle d’Activités d’Aix les Milles, Aix-en-Provence (France)

2015-01-01

A next-generation bimorph mirror with piezos bonded to the side faces of a monolithic substrate was created. When replacing a first-generation bimorph mirror suffering from the junction effect, the new type of mirror significantly improved the size and shape of the reflected synchrotron X-ray beam. No evidence of the junction effect was observed even after eight months of continuous beamline usage. Piezo bimorph mirrors are versatile active optics used on many synchrotron beamlines. However, many bimorphs suffer from the ‘junction effect’: a periodic deformation of the optical surface which causes major aberrations to the reflected X-ray beam. This effect is linked to the construction of such mirrors, where piezo ceramics are glued directly below the thin optical substrate. In order to address this problem, a next-generation bimorph with piezos bonded to the side faces of a monolithic substrate was developed at Thales-SESO and optimized at Diamond Light Source. Using metrology feedback from the Diamond-NOM, the optical slope error was reduced to ∼0.5 µrad r.m.s. for a range of ellipses. To maximize usability, a novel holder was built to accommodate the substrate in any orientation. When replacing a first-generation bimorph on a synchrotron beamline, the new mirror significantly improved the size and shape of the reflected X-ray beam. Most importantly, there was no evidence of the junction effect even after eight months of continuous beamline usage. It is hoped that this new design will reinvigorate the use of active bimorph optics at synchrotron and free-electron laser facilities to manipulate and correct X-ray wavefronts.

Characterization of a next-generation piezo bimorph X-ray mirror for synchrotron beamlines

International Nuclear Information System (INIS)

Alcock, Simon G.; Nistea, Ioana; Sutter, John P.; Sawhney, Kawal; Fermé, Jean-Jacques; Thellièr, Christophe; Peverini, Luca

2015-01-01

A next-generation bimorph mirror with piezos bonded to the side faces of a monolithic substrate was created. When replacing a first-generation bimorph mirror suffering from the junction effect, the new type of mirror significantly improved the size and shape of the reflected synchrotron X-ray beam. No evidence of the junction effect was observed even after eight months of continuous beamline usage. Piezo bimorph mirrors are versatile active optics used on many synchrotron beamlines. However, many bimorphs suffer from the ‘junction effect’: a periodic deformation of the optical surface which causes major aberrations to the reflected X-ray beam. This effect is linked to the construction of such mirrors, where piezo ceramics are glued directly below the thin optical substrate. In order to address this problem, a next-generation bimorph with piezos bonded to the side faces of a monolithic substrate was developed at Thales-SESO and optimized at Diamond Light Source. Using metrology feedback from the Diamond-NOM, the optical slope error was reduced to ∼0.5 µrad r.m.s. for a range of ellipses. To maximize usability, a novel holder was built to accommodate the substrate in any orientation. When replacing a first-generation bimorph on a synchrotron beamline, the new mirror significantly improved the size and shape of the reflected X-ray beam. Most importantly, there was no evidence of the junction effect even after eight months of continuous beamline usage. It is hoped that this new design will reinvigorate the use of active bimorph optics at synchrotron and free-electron laser facilities to manipulate and correct X-ray wavefronts

Recurrent pulse trains in the solar hard X-ray flare of 1980 June 7

International Nuclear Information System (INIS)

Kiplinger, A.L.; Dennis, B.R.; Frost, K.J.; Orwig, L.E.

1983-01-01

This study presents a detailed examination of the solar hard X-ray and γ-ray flare of 1980 June 7 as seen by the Hard X-Ray Burst Spectrometer on SMM. The hard X-ray profile is most unusual in that it is characterized by an initial pulse train of seven intense hard X-ray spikes. However, the event is unique among the 6300 events observed by HXRBS in that the temporal signature of this pulse train recurs twice during the flare. Such signatures of temporal stability in impulsive solar flares have not been observed before. Examinations of the hard X-ray data in conjunction with radio and γ-ray observations show that the 28--480 keV X-ray emission is simultaneous with the 17 GHz microwave fluxes within 128 ms and that the 3.5--6.5 MeV prompt γ-ray line emission is coincident with secondary maxima of the microwave and X-ray fluxes. Studies of the temporal and spectral properties of the pulses indicate that the pulses are not produced by purely reversible processes, and that if the source is oscillatory, it is not a high quality oscillator. Although the absence of spatially resolved hard X-ray observations leaves other possibilities open, a parameterization of the event as a set of seven sequentially firing loops is presented that offers many satisfying explanations of the observations

Design of grazing-incidence multilayer supermirrors for hard-X-ray reflectors

DEFF Research Database (Denmark)

Joensen, K. D.; Voutov, P.; Szentgyorgyi, A.

1995-01-01

Extremely broadband grazing-incidence multilayers for hard-X-ray reflection can be obtained by a gradual change of the layer thicknesses down through the structure. Existing approaches for designing similar neutron optics, called supermirrors, are shown to provide respectable performance when...... applied to X-ray multilayers. However, none of these approaches consider the effects of imperfect layer interfaces and absorption in the overlying layers. Adaptations of neutron designs that take these effects into account are presented, and a thorough analysis of two specific applications (a single hard......-X-ray reflector and a hard-X-ray telescope) shows that an improved performance can be obtained. A multilayer whose bilayer thicknesses are given by a power law expression is found to provide the best solution; however, it is only slightly better than some of the adapted neutron designs...

Synthesis of nanoparticles through x-ray radiolysis using synchrotron radiation

Science.gov (United States)

Yamaguchi, A.; Okada, I.; Fukuoka, T.; Ishihara, M.; Sakurai, I.; Utsumi, Y.

2016-09-01

The synthesis and deposition of nanoparticles consisting of Cu and Au in a CuSO4 solution with some kinds of alcohol and electroplating solution containing gold (I) trisodium disulphite under synchrotron X-ray radiation was investigated. The functional group of alcohol plays an important in nucleation, growth and aggregation process of copper and cupric oxide particles. We found that the laboratory X-ray source also enables us to synthesize the NPs from the metallic solution. As increasing X-ray exposure time, the full length at half width of particle size distribution is broader and higher-order nanostructure containing NPs clusters is formed. The surface-enhanced Raman scattering (SERS) of 4, 4'-bipyridine (4bpy) in aqueous solution was measured using higher-order nanostructure immobilized on silicon substrates under systematically-varied X-ray exposure. This demonstration provide a clue to develop a three-dimensional printing and sensor for environmental analyses and molecular detection through simple SERS measurements.

SYNCHROTRON X-RAY OBSERVATIONS OF A MONOLAYER TEMPLATE FOR MINERALIZATION

International Nuclear Information System (INIS)

Dimasi, E.; Gower, L.B.

2000-01-01

Mineral nucleation at a Langmuir film interface has been studied by synchrotron x-ray scattering. Diluted calcium bicarbonate solutions were used as subphases for arachidic and stearic acid monolayers, compressed in a Langmuir trough. Self-assembly of the monolayer template is observed directly, and subsequent crystal growth monitored in-situ

Heat transfer issues in high-heat-load synchrotron x-ray beams

International Nuclear Information System (INIS)

Khounsary, A.M.; Mills, D.M.

1994-09-01

In this paper, a short description of the synchrotron radiation x-ray sources and the associated power loads is given, followed by a brief description of typical synchrotron components and their heat load. It is emphasized that the design goals for most of these components is to limit (a) temperature, (b) stresses, or (c) strains in the system. Each design calls for a different geometry, material selection, and cooling scheme. Cooling schemes that have been utilized so far are primarily single phase and include simple macrochannel cooling, microchannel cooling, contact cooling, pin-post cooling, porous-flow cooling, jet cooling, etc. Water, liquid metals, and various cryogenic coolants have been used. Because the trend in x-ray beam development is towards brighter (i.e., more powerful) beams and assuming that no radical changes in the design of x-ray generating machines occurs in the next few years, it is fair to state that the utilization of various effective cooling schemes and, in particular, two-phase flow (e.g., subcooled boiling) warrants further investigation. This, however, requires a thorough examination of stability and reliability of two-phase flows for high-heat-flux components operating in ultrahigh vacuum with stringent reliability requirements

A Hard X-Ray Power-Law Spectral Cutoff in Centaurus X-4

DEFF Research Database (Denmark)

Chakrabarty, Deepto; Tomsick, John A.; Grefenstette, Brian W.

2015-01-01

The low-mass X-ray binary Cen X-4 is the brightest and closest (<1.2 kpc) quiescent neutron star transient. Previous 0.5-10 keV X-ray observations of Cen X-4 in quiescence identified two spectral components: soft thermal emission from the neutron star atmosphere and a hard power-law tail of unkno...... behavior with PSR J1023+0038, IGR J18245-2452, and XSS J12270-4859, which have shown transitions between LMXB and radio pulsar modes at a similar X-ray luminosity....

Analytical research using synchrotron radiation based techniques

International Nuclear Information System (INIS)

Jha, Shambhu Nath

2015-01-01

There are many Synchrotron Radiation (SR) based techniques such as X-ray Absorption Spectroscopy (XAS), X-ray Fluorescence Analysis (XRF), SR-Fourier-transform Infrared (SRFTIR), Hard X-ray Photoelectron Spectroscopy (HAXPS) etc. which are increasingly being employed worldwide in analytical research. With advent of modern synchrotron sources these analytical techniques have been further revitalized and paved ways for new techniques such as microprobe XRF and XAS, FTIR microscopy, Hard X-ray Photoelectron Spectroscopy (HAXPS) etc. The talk will cover mainly two techniques illustrating its capability in analytical research namely XRF and XAS. XRF spectroscopy: XRF spectroscopy is an analytical technique which involves the detection of emitted characteristic X-rays following excitation of the elements within the sample. While electron, particle (protons or alpha particles), or X-ray beams can be employed as the exciting source for this analysis, the use of X-ray beams from a synchrotron source has been instrumental in the advancement of the technique in the area of microprobe XRF imaging and trace level compositional characterisation of any sample. Synchrotron radiation induced X-ray emission spectroscopy, has become competitive with the earlier microprobe and nanoprobe techniques following the advancements in manipulating and detecting these X-rays. There are two important features that contribute to the superb elemental sensitivities of microprobe SR induced XRF: (i) the absence of the continuum (Bremsstrahlung) background radiation that is a feature of spectra obtained from charged particle beams, and (ii) the increased X-ray flux on the sample associated with the use of tunable third generation synchrotron facilities. Detection sensitivities have been reported in the ppb range, with values of 10 -17 g - 10 -14 g (depending on the particular element and matrix). Keeping in mind its demand, a microprobe XRF beamline has been setup by RRCAT at Indus-2 synchrotron

Ultra high-speed x-ray imaging of laser-driven shock compression using synchrotron light

Science.gov (United States)

Olbinado, Margie P.; Cantelli, Valentina; Mathon, Olivier; Pascarelli, Sakura; Grenzer, Joerg; Pelka, Alexander; Roedel, Melanie; Prencipe, Irene; Laso Garcia, Alejandro; Helbig, Uwe; Kraus, Dominik; Schramm, Ulrich; Cowan, Tom; Scheel, Mario; Pradel, Pierre; De Resseguier, Thibaut; Rack, Alexander

2018-02-01

A high-power, nanosecond pulsed laser impacting the surface of a material can generate an ablation plasma that drives a shock wave into it; while in situ x-ray imaging can provide a time-resolved probe of the shock-induced material behaviour on macroscopic length scales. Here, we report on an investigation into laser-driven shock compression of a polyurethane foam and a graphite rod by means of single-pulse synchrotron x-ray phase-contrast imaging with MHz frame rate. A 6 J, 10 ns pulsed laser was used to generate shock compression. Physical processes governing the laser-induced dynamic response such as elastic compression, compaction, pore collapse, fracture, and fragmentation have been imaged; and the advantage of exploiting the partial spatial coherence of a synchrotron source for studying low-density, carbon-based materials is emphasized. The successful combination of a high-energy laser and ultra high-speed x-ray imaging using synchrotron light demonstrates the potentiality of accessing complementary information from scientific studies of laser-driven shock compression.

A model independent method to deconvolve hard X-ray spectra

International Nuclear Information System (INIS)

Polcaro, V.F.; Bazzano, A.; Ubertini, P.; La Padula, C.

1984-01-01

A general purpose method to deconvolve the energy spectra detected by means of the use of a hard X-ray telescope is described. The procedure does not assume any form of input spectrum and the observed energy loss spectrum is directly deconvolved into the incident photon spectrum, the form of which can be determined independently of physical interpretation of the data. Deconvolution of the hard X-ray spectrum of Her X-1, detected during the HXR 81M experiment, by the method independent method is presented. (orig.)

The 105-Month Swift-BAT All-sky Hard X-Ray Survey

Science.gov (United States)

Oh, Kyuseok; Koss, Michael; Markwardt, Craig B.; Schawinski, Kevin; Baumgartner, Wayne H.; Barthelmy, Scott D.; Cenko, S. Bradley; Gehrels, Neil; Mushotzky, Richard; Petulante, Abigail; Ricci, Claudio; Lien, Amy; Trakhtenbrot, Benny

2018-03-01

We present a catalog of hard X-ray sources detected in the first 105 months of observations with the Burst Alert Telescope (BAT) coded-mask imager on board the Swift observatory. The 105-month Swift-BAT survey is a uniform hard X-ray all-sky survey with a sensitivity of 8.40× {10}-12 {erg} {{{s}}}-1 {cm}}-2 over 90% of the sky and 7.24× {10}-12 {erg} {{{s}}}-1 {cm}}-2 over 50% of the sky in the 14–195 keV band. The Swift-BAT 105-month catalog provides 1632 (422 new detections) hard X-ray sources in the 14–195 keV band above the 4.8σ significance level. Adding to the previously known hard X-ray sources, 34% (144/422) of the new detections are identified as Seyfert active galactic nuclei (AGNs) in nearby galaxies (zBAT catalog, we release eight-channel spectra and monthly sampled light curves for each object in the online journal and at the Swift-BAT 105-month website.

Synchrotron X-ray diffraction analysis for quantitative defect evaluation in GaP/Si nanolayers

Energy Technology Data Exchange (ETDEWEB)

Nguyen Thanh, T.; Robert, C. [Université Européenne de Bretagne, INSA, FOTON, UMR 6082, F-35708 RENNES (France); Létoublon, A., E-mail: Antoine.letoublon@insa-rennes.fr [Université Européenne de Bretagne, INSA, FOTON, UMR 6082, F-35708 RENNES (France); Cornet, C. [Université Européenne de Bretagne, INSA, FOTON, UMR 6082, F-35708 RENNES (France); Quinci, T. [Université Européenne de Bretagne, INSA, FOTON, UMR 6082, F-35708 RENNES (France); CEA LCP, INES, 50 av. du Lac Léman, Savoie Technolac, 73375 Le Bourget du Lac (France); Giudicelli, E.; Almosni, S. [Université Européenne de Bretagne, INSA, FOTON, UMR 6082, F-35708 RENNES (France); Boudet, N. [CRG-D2AM, ESRF and Inst. Néel, CNRS-UJF, 25 Av des Martyrs, 38042 Grenoble (France); Ponchet, A. [CEMES, CNRS, Université de Toulouse, 29 rue J. Marvig BP 94347, 31055 Toulouse Cedex 4 (France); Kuyyalil, J. [Université Européenne de Bretagne, INSA, FOTON, UMR 6082, F-35708 RENNES (France); Danila, M. [National Institute for Research and Development in Microtechnologies (IMT), 126A Erou Iancu Nicolae Street, 077190, Bucharest (Romania); Durand, O.; Bertru, N.; Le Corre, A. [Université Européenne de Bretagne, INSA, FOTON, UMR 6082, F-35708 RENNES (France)

2013-08-31

In the context of III–V monolithic integration on silicon, synchrotron X-ray diffraction has been employed in this study using a bi-dimensional large area hybrid pixel detector (XPAD third generation) to characterize defects in the GaP layers. Despite a very coherent interface (low plastic relaxation) of GaP/Si, 2 types of defect are detected. Micro-twins contributions are evidenced and quantitatively evaluated from additional reflections analysis. Antiphase domains are evidenced using the Williamson-Hall-like plot method applied to transverse scans extracted directly from single XPAD images taken on specular GaP reflections. - Highlights: ► Antiphase domain evidence and characterization in GaP/Si using X-ray diffraction ► Microtwin evidence and characterization ► Synchrotron diffraction ► Large area X-ray hybrid pixel detector.

NuSTAR Hard X-Ray Survey of the Galactic Center Region. II. X-Ray Point Sources

DEFF Research Database (Denmark)

Hong, JaeSub; Mori, Kaya; Hailey, Charles J.

2016-01-01

persistent luminous X-ray binaries (XBs) and the likely run-away pulsar called the Cannonball. New source-detection significance maps reveal a cluster of hard (>10 keV) X-ray sources near the Sgr. A diffuse complex with no clear soft X-ray counterparts. The severe extinction observed in the Chandra spectra...

Synchrotron-Based X Ray and FTIR Micro-Spectroscopy for the Cultural Heritage Science at the ID21 Beamline, ESRF

International Nuclear Information System (INIS)

Cotte, M.; Radepont, M.; Pouyet, E.; Salome, M.; Susini, J.

2016-01-01

Synchrotron-based techniques are increasingly used for the study of Cultural Heritage (CH) materials. These analyses rely on light-matter interactions and can be carried out directly onto the artworks. They also benefit from the synchrotron assets and in particular from the gain in terms of lateral resolution when comparing with laboratory equipment. Thanks to the synchrotron beam high brightness and low divergence, X rays can be focused down to less than 1μm, making possible the selective analysis of various compounds in complex structures. The ID21 beamline, at the ESRF, is devoted to such high resolution microscopy, using both X ray and infrared beams. Almost all kinds of CH materials can be studied, from hard matter, such as metals, glasses, pigments, to soft matters such as varnishes, tissues, wood, paper, textile, wax… Usually, samples are prepared as transversal cross-sections in order to highlight the internal structure of the matter (corrosion patina on metals, multilayer structures in paintings…). 2D elemental mapping are generated by micro-X ray fluorescence, with low detection limit. Chemical information can be obtained both by X ray absorption spectroscopy (micro-XANES) and by infrared spectroscopy (micro-FTIR). Studies usually aim at understanding degradation mechanisms (corrosion, colour variation, formation of crust), or at identifying artistic processes (choice of pigments and binders for paintings, optical effects in glasses…). The X ray energy range at ID21 is 2-9keV, giving access to all the K-edges from P to Cu. It covers S and Cl, which are frequently implied in degradation processes, and the 3d transition metals, which enter in the composition of many artworks (being in pigments, inks, glasses or metal). The FTIR-microscope provides complementary molecular information, and is used more particularly for the analysis of organic and hybrid components. The two microscopes are independent and can be operated simultaneously. Various hardware

Hard X-ray Flux from Low-Mass Stars in the Cygnus OB2 Association

Science.gov (United States)

Caramazza, M.; Drake, J. J.; Micela, G.; Flaccomio, E.

2009-05-01

We investigate the X-ray emission in the 20-40 keV band expected from the flaring low-mass stellar population in Cygnus OB2 assuming that the observed soft X-ray emission is due to a superposition of flares and that the ratio of hard X-ray to soft X-ray emission is described by a scaling found for solar flares by Isola and co-workers. We estimate a low-mass stellar hard X-ray flux in the 20-40 keV band in the range ~7×1031-7×1033 erg/s and speculate the limit of this values. Hard X-ray emission could lie at a level not much below the current observed flux upper limits for Cygnus OB2. Simbol-X, with its broad energy band (10-100 keV) and its sensitivity should be able to detect this emission and would provide insights into the hard X-ray production of flares on pre-main sequence stars.

Development of fast parallel multi-technique scanning X-ray imaging at Synchrotron Soleil

Science.gov (United States)

Medjoubi, K.; Leclercq, N.; Langlois, F.; Buteau, A.; Lé, S.; Poirier, S.; Mercère, P.; Kewish, C. M.; Somogyi, A.

2013-10-01

A fast multimodal scanning X-ray imaging scheme is prototyped at Soleil Synchrotron. It permits the simultaneous acquisition of complementary information on the sample structure, composition and chemistry by measuring transmission, differential phase contrast, small-angle scattering, and X-ray fluorescence by dedicated detectors with ms dwell time per pixel. The results of the proof of principle experiments are presented in this paper.

Hard-x-ray phase-difference microscopy with a low-brilliance laboratory x-ray source

International Nuclear Information System (INIS)

Kuwabara, Hiroaki; Yashiro, Wataru; Harasse, Sebastien; Momose, Atsushi; Mizutani, Haruo

2011-01-01

We have developed a hard-X-ray phase-imaging microscopy method using a low-brilliance X-ray source. The microscope consists of a sample, a Fresnel zone plate, a transmission grating, and a source grating creating an array of mutually incoherent X-ray sources. The microscope generates an image exhibiting twin features of the sample with opposite signs separated by a distance, which is processed to generate a phase image. The method is quantitative even for non-weak-phase objects that are difficult to be quantitatively examined by the widely used Zernike phase-contrast microscopy, and it has potentially broad applications in the material and biological science fields. (author)

A cryogenic electrical substitution radiometer for hard X-rays

International Nuclear Information System (INIS)

Gerlach, M.; Krumrey, M.; Cibik, L.; Mueller, P.; Ulm, G.

2007-01-01

Cryogenic electrical substitution radiometers (ESR) are well established in radiometry to determine radiant power with low uncertainties from the infrared to the soft X-ray region. The absorbers are made of copper to achieve a small time constant. At higher photon energies, the use of copper prevents the operation of ESR due to increasing transmittance. A new absorber design for hard X-rays has been developed at the laboratory of the Physikalisch-Technische Bundesanstalt (PTB) at BESSY II. In the first place, extensive simulations were performed for a variety of materials and absorber geometries using the Monte Carlo simulation code Geant4. The accuracy of the simulations was verified comparing them to scattering experiments performed at a 7 T wavelength shifter beamline at BESSY II. It was shown that Geant4 describes the photo-effect, including fluorescence as well as Compton- and Rayleigh scattering, with high accuracy. The simulations and experiments resulted in an absorber with a gold base 500 μm in thickness, inclined by 30 deg., and a cylindrical shell made of copper 80 μm in thickness to reduce losses caused mainly by fluorescence. The absorber was manufactured at PTB by means of electroforming and was implemented into an existing ESR. Monochromatized synchrotron radiation of high spectral purity was used to calibrate silicon photodiodes against the ESR for photon energies up to 60 keV with relative uncertainties below 1%

A cryogenic electrical substitution radiometer for hard X-rays

Energy Technology Data Exchange (ETDEWEB)

Gerlach, M. [Physikalisch-Technische Bundesanstalt, Abbestr. 2-12, 10587 Berlin (Germany)], E-mail: Martin.Gerlach@ptb.de; Krumrey, M.; Cibik, L.; Mueller, P.; Ulm, G. [Physikalisch-Technische Bundesanstalt, Abbestr. 2-12, 10587 Berlin (Germany)

2007-09-21

Cryogenic electrical substitution radiometers (ESR) are well established in radiometry to determine radiant power with low uncertainties from the infrared to the soft X-ray region. The absorbers are made of copper to achieve a small time constant. At higher photon energies, the use of copper prevents the operation of ESR due to increasing transmittance. A new absorber design for hard X-rays has been developed at the laboratory of the Physikalisch-Technische Bundesanstalt (PTB) at BESSY II. In the first place, extensive simulations were performed for a variety of materials and absorber geometries using the Monte Carlo simulation code Geant4. The accuracy of the simulations was verified comparing them to scattering experiments performed at a 7 T wavelength shifter beamline at BESSY II. It was shown that Geant4 describes the photo-effect, including fluorescence as well as Compton- and Rayleigh scattering, with high accuracy. The simulations and experiments resulted in an absorber with a gold base 500 {mu}m in thickness, inclined by 30 deg., and a cylindrical shell made of copper 80 {mu}m in thickness to reduce losses caused mainly by fluorescence. The absorber was manufactured at PTB by means of electroforming and was implemented into an existing ESR. Monochromatized synchrotron radiation of high spectral purity was used to calibrate silicon photodiodes against the ESR for photon energies up to 60 keV with relative uncertainties below 1%.

A cryogenic electrical substitution radiometer for hard X-rays

Science.gov (United States)

Gerlach, M.; Krumrey, M.; Cibik, L.; Müller, P.; Ulm, G.

2007-09-01

Cryogenic electrical substitution radiometers (ESR) are well established in radiometry to determine radiant power with low uncertainties from the infrared to the soft X-ray region. The absorbers are made of copper to achieve a small time constant. At higher photon energies, the use of copper prevents the operation of ESR due to increasing transmittance. A new absorber design for hard X-rays has been developed at the laboratory of the Physikalisch-Technische Bundesanstalt (PTB) at BESSY II. In the first place, extensive simulations were performed for a variety of materials and absorber geometries using the Monte Carlo simulation code Geant4. The accuracy of the simulations was verified comparing them to scattering experiments performed at a 7 T wavelength shifter beamline at BESSY II. It was shown that Geant4 describes the photo-effect, including fluorescence as well as Compton- and Rayleigh scattering, with high accuracy. The simulations and experiments resulted in an absorber with a gold base 500 μm in thickness, inclined by 30°, and a cylindrical shell made of copper 80 μm in thickness to reduce losses caused mainly by fluorescence. The absorber was manufactured at PTB by means of electroforming and was implemented into an existing ESR. Monochromatized synchrotron radiation of high spectral purity was used to calibrate silicon photodiodes against the ESR for photon energies up to 60 keV with relative uncertainties below 1%.

High resolution X-ray detector for synchrotron-based microtomography

CERN Document Server

Stampanoni, M; Wyss, P; Abela, R; Patterson, B; Hunt, S; Vermeulen, D; Rueegsegger, P

2002-01-01

Synchrotron-based microtomographic devices are powerful, non-destructive, high-resolution research tools. Highly brilliant and coherent X-rays extend the traditional absorption imaging techniques and enable edge-enhanced and phase-sensitive measurements. At the Materials Science Beamline MS of the Swiss Light Source (SLS), the X-ray microtomographic device is now operative. A high performance detector based on a scintillating screen optically coupled to a CCD camera has been developed and tested. Different configurations are available, covering a field of view ranging from 715x715 mu m sup 2 to 7.15x7.15 mm sup 2 with magnifications from 4x to 40x. With the highest magnification 480 lp/mm had been achieved at 10% modulation transfer function which corresponds to a spatial resolution of 1.04 mu m. A low-noise fast-readout CCD camera transfers 2048x2048 pixels within 100-250 ms at a dynamic range of 12-14 bit to the file server. A user-friendly graphical interface gives access to the main parameters needed for ...

Frontiers in X-Ray Science

International Nuclear Information System (INIS)

Young, Linda

2011-01-01

The year 2010 marked the fiftieth anniversary of the optical laser and the first anniversary of the world's first hard x-ray free-electron laser, the Linac Coherent Light Source (LCLS) at SLAC. This exciting, new accelerator-based source of x-rays provides peak brilliances roughly a billion times greater than currently available from synchrotron sources such as the Advanced Photon Source at Argonne, and thus explores a qualitatively different parameter space. This talk will describe the first experiments at the LCLS aimed at understanding the nature of high intensity x-ray interactions, related applications in ultrafast imaging on the atomic scale and sketch nascent plans for the extension of both linac and storage-ring based photon sources.

Imaging escape gated MPWC for hard X-ray astronomy

Energy Technology Data Exchange (ETDEWEB)

Ubertini, P.; Bazzano, A.; Boccaccini, L.; La Padula, C.; Mastropietro, M.; Patriarca, R.; Polcaro, V.F.; Barbareschi, L.; Perotti, F.; Villa, G.

1983-11-15

A scientific forward step in the hard X-ray and soft gamma-ray astronomy will only be possible with the use of a new generation of space borne instruments. Their main characteristics have to be the two-dimensional imaging capability over a large collecting area and the fine spectral resolution in order to discriminate between the weak signal coming from cosmic sources to be detected and the strong background induced by cosmic rays, in the space environment, on the detector. To reach this goal we have developed a new hard X-ray position sensitive proportional counter operating with the escape gate technique in the range 15-150 keV, to be used together with a pseudo-random coded mask in order to obtain sky images. The detector is a high pressure (5 bar) xenon-argon-isobutane filled chamber with a spatial resolution of 30x2 mm and a spectral resolution of 5% at 60 keV on the sensitive area of 3000 cm/sup 2/.

Characterization of a next-generation piezo bimorph X-ray mirror for synchrotron beamlines.

Science.gov (United States)

Alcock, Simon G; Nistea, Ioana; Sutter, John P; Sawhney, Kawal; Fermé, Jean Jacques; Thellièr, Christophe; Peverini, Luca

2015-01-01

Piezo bimorph mirrors are versatile active optics used on many synchrotron beamlines. However, many bimorphs suffer from the `junction effect': a periodic deformation of the optical surface which causes major aberrations to the reflected X-ray beam. This effect is linked to the construction of such mirrors, where piezo ceramics are glued directly below the thin optical substrate. In order to address this problem, a next-generation bimorph with piezos bonded to the side faces of a monolithic substrate was developed at Thales-SESO and optimized at Diamond Light Source. Using metrology feedback from the Diamond-NOM, the optical slope error was reduced to ∼ 0.5 µrad r.m.s. for a range of ellipses. To maximize usability, a novel holder was built to accommodate the substrate in any orientation. When replacing a first-generation bimorph on a synchrotron beamline, the new mirror significantly improved the size and shape of the reflected X-ray beam. Most importantly, there was no evidence of the junction effect even after eight months of continuous beamline usage. It is hoped that this new design will reinvigorate the use of active bimorph optics at synchrotron and free-electron laser facilities to manipulate and correct X-ray wavefronts.

Accelerated Synchrotron X-ray Diffraction Data Analysis on a Heterogeneous High Performance Computing System

Energy Technology Data Exchange (ETDEWEB)

Qin, J; Bauer, M A, E-mail: qin.jinhui@gmail.com, E-mail: bauer@uwo.ca [Computer Science Department, University of Western Ontario, London, ON N6A 5B7 (Canada)

2010-11-01

The analysis of synchrotron X-ray Diffraction (XRD) data has been used by scientists and engineers to understand and predict properties of materials. However, the large volume of XRD image data and the intensive computations involved in the data analysis makes it hard for researchers to quickly reach any conclusions about the images from an experiment when using conventional XRD data analysis software. Synchrotron time is valuable and delays in XRD data analysis can impact decisions about subsequent experiments or about materials that they are investigating. In order to improve the data analysis performance, ideally to achieve near real time data analysis during an XRD experiment, we designed and implemented software for accelerated XRD data analysis. The software has been developed for a heterogeneous high performance computing (HPC) system, comprised of IBM PowerXCell 8i processors and Intel quad-core Xeon processors. This paper describes the software and reports on the improved performance. The results indicate that it is possible for XRD data to be analyzed at the rate it is being produced.

Accelerated Synchrotron X-ray Diffraction Data Analysis on a Heterogeneous High Performance Computing System

International Nuclear Information System (INIS)

Qin, J; Bauer, M A

2010-01-01

The analysis of synchrotron X-ray Diffraction (XRD) data has been used by scientists and engineers to understand and predict properties of materials. However, the large volume of XRD image data and the intensive computations involved in the data analysis makes it hard for researchers to quickly reach any conclusions about the images from an experiment when using conventional XRD data analysis software. Synchrotron time is valuable and delays in XRD data analysis can impact decisions about subsequent experiments or about materials that they are investigating. In order to improve the data analysis performance, ideally to achieve near real time data analysis during an XRD experiment, we designed and implemented software for accelerated XRD data analysis. The software has been developed for a heterogeneous high performance computing (HPC) system, comprised of IBM PowerXCell 8i processors and Intel quad-core Xeon processors. This paper describes the software and reports on the improved performance. The results indicate that it is possible for XRD data to be analyzed at the rate it is being produced.

Observation of hard X-rays line emission from Her X-1

Energy Technology Data Exchange (ETDEWEB)

Polcaro, V.F.; Bazzano, A.; la Padula, C.; Ubertini, P.; Vialetto, G.; Manchanda, R.K.; Damle, S.V.

1982-04-01

We present the results of a hard X-ray measurement of the binary source Her X-1, carried out with a balloon borne X-ray telescope consisting of two Multiwire Proportional Counters, having 900 cm/sup 2/ sensitive area each and spectral resolution of 15% and 24% FWHM respectively at 60 keV. The source was observed during the 'Mid-on' state. Our data confirm the previously reported high energy emission line overimposed on the low energy thermal spectrum.

Hard X-ray quantum optics in thin films nanostructures

Energy Technology Data Exchange (ETDEWEB)

Haber, Johann Friedrich Albert

2017-05-15

This thesis describes quantum optical experiments with X-rays with the aim of reaching the strong-coupling regime of light and matter. We make use of the interaction which arises between resonant matter and X-rays in specially designed thin-film nanostructures which form X-ray cavities. Here, the resonant matter are Tantalum atoms and the Iron isotope {sup 57}Fe. Both limit the number of modes available to the resonant atoms for interaction, and enhances the interaction strength. Thus we have managed to observe a number of phenomena well-known in quantum optics, which are the building blocks for sophisticated applications in e.g. metrology. Among these are the strong coupling of light and matter and the concurrent exchange of virtual photons, often called Rabi oscillations. Furthermore we have designed and tested a type of cavity hitherto unused in X-ray optics. Finally, we develop a new method for synchrotron Moessbauer spectroscopy, which not only promises to yield high-resolution spectra, but also enables the retrieval of the phase of the scattered light. The results open new avenues for quantum optical experiments with X-rays, particularly with regards to the ongoing development of high-brilliance X-ray free-electron lasers.

Hard X-ray quantum optics in thin films nanostructures

International Nuclear Information System (INIS)

Haber, Johann Friedrich Albert

2017-05-01

This thesis describes quantum optical experiments with X-rays with the aim of reaching the strong-coupling regime of light and matter. We make use of the interaction which arises between resonant matter and X-rays in specially designed thin-film nanostructures which form X-ray cavities. Here, the resonant matter are Tantalum atoms and the Iron isotope "5"7Fe. Both limit the number of modes available to the resonant atoms for interaction, and enhances the interaction strength. Thus we have managed to observe a number of phenomena well-known in quantum optics, which are the building blocks for sophisticated applications in e.g. metrology. Among these are the strong coupling of light and matter and the concurrent exchange of virtual photons, often called Rabi oscillations. Furthermore we have designed and tested a type of cavity hitherto unused in X-ray optics. Finally, we develop a new method for synchrotron Moessbauer spectroscopy, which not only promises to yield high-resolution spectra, but also enables the retrieval of the phase of the scattered light. The results open new avenues for quantum optical experiments with X-rays, particularly with regards to the ongoing development of high-brilliance X-ray free-electron lasers.

Weak hard X-ray emission from broad absorption line quasars: evidence for intrinsic X-ray weakness

International Nuclear Information System (INIS)

Luo, B.; Brandt, W. N.; Scott, A. E.; Alexander, D. M.; Gandhi, P.; Stern, D.; Teng, S. H.; Arévalo, P.; Bauer, F. E.; Boggs, S. E.; Craig, W. W.; Christensen, F. E.; Comastri, A.; Farrah, D.; Hailey, C. J.; Harrison, F. A.; Koss, M.; Ogle, P.; Puccetti, S.; Saez, C.

2014-01-01

We report NuSTAR observations of a sample of six X-ray weak broad absorption line (BAL) quasars. These targets, at z = 0.148-1.223, are among the optically brightest and most luminous BAL quasars known at z < 1.3. However, their rest-frame ≈2 keV luminosities are 14 to >330 times weaker than expected for typical quasars. Our results from a pilot NuSTAR study of two low-redshift BAL quasars, a Chandra stacking analysis of a sample of high-redshift BAL quasars, and a NuSTAR spectral analysis of the local BAL quasar Mrk 231 have already suggested the existence of intrinsically X-ray weak BAL quasars, i.e., quasars not emitting X-rays at the level expected from their optical/UV emission. The aim of the current program is to extend the search for such extraordinary objects. Three of the six new targets are weakly detected by NuSTAR with ≲ 45 counts in the 3-24 keV band, and the other three are not detected. The hard X-ray (8-24 keV) weakness observed by NuSTAR requires Compton-thick absorption if these objects have nominal underlying X-ray emission. However, a soft stacked effective photon index (Γ eff ≈ 1.8) for this sample disfavors Compton-thick absorption in general. The uniform hard X-ray weakness observed by NuSTAR for this and the pilot samples selected with <10 keV weakness also suggests that the X-ray weakness is intrinsic in at least some of the targets. We conclude that the NuSTAR observations have likely discovered a significant population (≳ 33%) of intrinsically X-ray weak objects among the BAL quasars with significantly weak <10 keV emission. We suggest that intrinsically X-ray weak quasars might be preferentially observed as BAL quasars.

CORRELATION OF HARD X-RAY AND WHITE LIGHT EMISSION IN SOLAR FLARES

Energy Technology Data Exchange (ETDEWEB)

Kuhar, Matej; Krucker, Säm; Battaglia, Marina; Kleint, Lucia; Casadei, Diego [University of Applied Sciences and Arts Northwestern Switzerland, Bahnhofstrasse 6, 5210 Windisch (Switzerland); Oliveros, Juan Carlos Martinez; Hudson, Hugh S. [Space Sciences Laboratory, University of California, Berkeley, CA 94720-7450 (United States)

2016-01-01

A statistical study of the correlation between hard X-ray and white light emission in solar flares is performed in order to search for a link between flare-accelerated electrons and white light formation. We analyze 43 flares spanning GOES classes M and X using observations from the Reuven Ramaty High Energy Solar Spectroscopic Imager and Helioseismic and Magnetic Imager. We calculate X-ray fluxes at 30 keV and white light fluxes at 6173 Å summed over the hard X-ray flare ribbons with an integration time of 45 s around the peak hard-X ray time. We find a good correlation between hard X-ray fluxes and excess white light fluxes, with a highest correlation coefficient of 0.68 for photons with energy of 30 keV. Assuming the thick target model, a similar correlation is found between the deposited power by flare-accelerated electrons and the white light fluxes. The correlation coefficient is found to be largest for energy deposition by electrons above ∼50 keV. At higher electron energies the correlation decreases gradually while a rapid decrease is seen if the energy provided by low-energy electrons is added. This suggests that flare-accelerated electrons of energy ∼50 keV are the main source for white light production.

Beer analysis by synchrotron radiation total reflection X-ray fluorescence (SR-TXRF)

International Nuclear Information System (INIS)

Moreira, Silvana; Vives, Ana Elisa S. de; Nascimento Filho, Virgilio F.; Zucchi, Orgheda L.D.A.

2005-01-01

In this work the concentrations of P, S, Cl, K, Ca, Mn, Fe, Zn and Br in twenty-nine brands of national and international beers were determined by Synchrotron Radiation Total Reflection X-Ray Fluorescence analysis (SR-TXRF). The results were compared with the limits established by the Brazilian Legislation and the nutritive values established by National Agricultural Library (NAL). The measurements were performed at the X-ray Fluorescence Beamline at Synchrotron Light Source Laboratory, in Campinas, Sao Paulo, Brazil, using a polychromatic beam for excitation. A small volume of 5 μL of sample beers containing just an internal standard, used to correct geometry effects, were analyzed without any pre-treatment. The measuring time was 100 s and the detection limits obtained varied from 1μg.L -1 for Mn and Fe to 15μg.L -1 for P. (author)

Performance of the IBM synchrotron X-ray source for lithography

International Nuclear Information System (INIS)

Archie, C.

1993-01-01

The compact superconducting synchrotron X-ray source at the IBM Advanced Lithography Facility in East Fishkill, New York has been in service to customers since the start of 1992. It availability during scheduled time is greater than 90%, with recent months frequently surpassing 95%. Data on the long-term behavior of the X-ray source properties and subsystem performance are now available. The full system continues to meet all specifications and even to surpass them in key areas. Measured electron beam properties such as beam size, short- and long-term positional stability, and beam life are presented. Lifetimes greater than 20 hours for typical stored beams have significantly simplified operations and increased availability compared to projections. This paper also describes some unique features of this X-ray source and goes beyond a discussion of downtime to describe the efforts behind the scenes to maintain and operate it

Diamond monochromator for high heat flux synchrotron x-ray beams

International Nuclear Information System (INIS)

Khounsary, A.M.; Smither, R.K.; Davey, S.; Purohit, A.

1992-12-01

Single crystal silicon has been the material of choice for x-ray monochromators for the past several decades. However, the need for suitable monochromators to handle the high heat load of the next generation synchrotron x-ray beams on the one hand and the rapid and on-going advances in synthetic diamond technology on the other make a compelling case for the consideration of a diamond mollochromator system. In this Paper, we consider various aspects, advantage and disadvantages, and promises and pitfalls of such a system and evaluate the comparative an monochromator subjected to the high heat load of the most powerful x-ray beam that will become available in the next few years. The results of experiments performed to evaluate the diffraction properties of a currently available synthetic single crystal diamond are also presented. Fabrication of diamond-based monochromator is within present technical means

Bonded Multilayer Laue Lens for focusing hard X-rays

International Nuclear Information System (INIS)

Liu Chian; Conley, R.; Qian, J.; Kewish, C.M.; Macrander, A.T.; Maser, J.; Kang, H.C.; Yan, H.; Stephenson, G.B.

2007-01-01

We have fabricated partial Multilayer Laue Lens (MLL) linear zone plate structures with thousands of alternating WSi 2 and Si layers and various outermost zone widths according to the Fresnel zone plate formula. Using partial MLL structures, we were able to focus hard X-rays to line foci with a width of 30 nm and below. Here, we describe challenges and approaches used to bond these multilayers to achieve line and point focusing. Bonding was done by coating two multilayers with AuSn and heating in a vacuum oven at 280-300 o C. X-ray reflectivity measurements confirmed that there was no change in the multilayers after heating to 350 o C. A bonded MLL was polished to a 5-25 μm wedge without cracking. SEM image analyses found well-positioned multilayers after bonding. These results demonstrate the feasibility of a bonded full MLL for focusing hard X-rays

Chemical crystallography with pulsed neutrons and synchrotron x-rays

International Nuclear Information System (INIS)

Carrondo, M.A.; Jeffrey, G.A.

1988-01-01

Solid-state chemists and physicists, crystallographers and molecular biologists who are using or who plan to use the special properties of pulsed neutron spallation and synchrotron X-ray sources will find this book invaluable. Those scientists who have not yet gained experience in working with such sources will find the basic physics of the radiations, their production and their scattering properties explained, together with descriptions of the different types of diffraction experiments which use them

Fabrication of nested elliptical KB mirrors using profile coating for synchrotron radiation X-ray focusing

International Nuclear Information System (INIS)

Liu Chian; Ice, G.E.; Liu, W.; Assoufid, L.; Qian, J.; Shi, B.; Khachatryan, R.; Wieczorek, M.; Zschack, P.; Tischler, J.Z.

2012-01-01

This paper describes fabrication methods used to demonstrate the advantages of nested or Montel optics for micro/nanofocusing of synchrotron X-ray beams. A standard Kirkpatrick-Baez (KB) mirror system uses two separated elliptical mirrors at glancing angles to the X-ray beam and sequentially arranged at 90° to each other to focus X-rays successively in the vertical and horizontal directions. A nested KB mirror system has the two mirrors positioned perpendicular and side-by-side to each other. Compared to a standard KB mirror system, Montel optics can focus a larger divergence and the mirrors can have a shorter focal length. As a result, nested mirrors can be fabricated with improved demagnification factor and ultimately smaller focal spot, than with a standard KB arrangement. The nested system is also more compact with an increased working distance, and is more stable, with reduced complexity of mirror stages. However, although Montel optics is commercially available for laboratory X-ray sources, due to technical difficulties they have not been used to microfocus synchrotron radiation X-rays, where ultra-precise mirror surfaces are essential. The main challenge in adapting nested optics for synchrotron microfocusing is to fabricate mirrors with a precise elliptical surface profile at the very edge where the two mirrors meet and where X-rays scatter. For example, in our application to achieve a sub-micron focus with high efficiency, a surface figure root-mean-square (rms) error on the order of 1 nm is required in the useable area along the X-ray footprint with a ∼0.1 mm-diameter cross section. In this paper we describe promising ways to fabricate precise nested KB mirrors using our profile coating technique and inexpensive flat Si substrates.

Synchrotron X-radiation research

International Nuclear Information System (INIS)

Kabler, M.N.; Nagel, D.J.; Skelton, E.F.

1990-05-01

The Naval Research Laboratory (NRL) has been involved in the exploitation of X rays since the 1920s. The report gives a brief description of the generation and characteristics of synchrotron radiation, and review highlights of current research. Research examples include soft-X-ray optics, semiconductor surface passivation, surface electron dynamics, space-charge dynamics on silicon, photochemistry on GaAs, local atomic structure, crystal structures from X-ray diffraction. The report then discusses emerging research opportunities

Synchrotron radiation spectroscopy including X-ray absorption spectroscopy and industrial applications

International Nuclear Information System (INIS)

Oshima, Masaharu

2016-01-01

Recent trends of synchrotron radiation spectroscopy, especially X-ray absorption spectroscopy for industrial applications are introduced based on our latest results for energy efficient devices such as magnetic RAM, LSI and organic FET, power generation devices such as fuel cells, and energy storage devices such as Li ion batteries. Furthermore, future prospects of spectroscopy with higher energy resolution, higher spatial resolution, higher temporal resolution and operando spectroscopy taking advantage of much brighter synchrotron radiation beam at low emittance SR rings are discussed from the view point of practical applications. (author)

The Elusive Soft Emission from Hard X-ray Symbiotic System RT Cru

Science.gov (United States)

Karovska, Margarita

2014-09-01

RT Cru is a fascinating member of a new class of hard X-ray emitting symbiotic binaries showing X-ray emission extending to over 50keV. While its hard X-ray emission has been studied in detail, the soft component of the spectrum, including flares, remains elusive, since previous observations have focused on the high-energy regime. We propose Chandra HRC-S/LETG observations to determine the spatial, spectral, and temporal characteristics of the source of the soft X-ray emission with a goal to establish the origin of the soft component, and determine whether and how it is tied to the hard component. Determining the origin of the soft emission is a crucial piece of the puzzle to understanding the geometry, energetics, and the environment of WD accretion in this class of symbiotic systems.

Hard x-ray monochromator with milli-electron volt bandwidth for high-resolution diffraction studies of diamond crystals

Energy Technology Data Exchange (ETDEWEB)

Stoupin, Stanislav; Shvyd' ko, Yuri; Shu Deming; Khachatryan, Ruben; Xiao, Xianghui; DeCarlo, Francesco; Goetze, Kurt; Roberts, Timothy; Roehrig, Christian; Deriy, Alexey [Advanced Photon Source, Argonne National Laboratory, Illinois 60439 (United States)

2012-02-15

We report on design and performance of a high-resolution x-ray monochromator with a spectral bandwidth of {Delta}E{sub X}{approx_equal} 1.5 meV, which operates at x-ray energies in the vicinity of the backscattering (Bragg) energy E{sub H} = 13.903 keV of the (008) reflection in diamond. The monochromator is utilized for high-energy-resolution diffraction characterization of diamond crystals as elements of advanced x-ray crystal optics for synchrotrons and x-ray free-electron lasers. The monochromator and the related controls are made portable such that they can be installed and operated at any appropriate synchrotron beamline equipped with a pre-monochromator.

Model experiment of in vivo synchrotron X-ray diffraction of human kidney stones

Energy Technology Data Exchange (ETDEWEB)

Ancharov, A.I. [Institute of Solid State Chemistry and Mechanochemistry SB RAS, Novosibirsk (Russian Federation)]. E-mail: ancharov@mail.ru; Potapov, S.S. [Institute of Mineralogy UB RAS, Miass (Russian Federation); Moiseenko, T.N. [The State Regional Clinical Hospital, Novosibirsk (Russian Federation); Feofilov, I.V. [The State Regional Clinical Hospital, Novosibirsk (Russian Federation); Nizovskii, A.I. [Boreskov Institute of Catalysis SB RAS, Novosibirsk (Russian Federation)

2007-05-21

The diffraction of synchrotron radiation (SR) was used to explore the phase composition of kidney stones placed into a specific object phantom, which imitated the human body. As an imitation of the patient breath, the kidney stone was moved vertically and rotated to an angle of 15{sup o} during the recording of the X-ray pattern. It was shown that rotation and displacement did not distort the X-ray pattern.

Model experiment of in vivo synchrotron X-ray diffraction of human kidney stones

International Nuclear Information System (INIS)

Ancharov, A.I.; Potapov, S.S.; Moiseenko, T.N.; Feofilov, I.V.; Nizovskii, A.I.

2007-01-01

The diffraction of synchrotron radiation (SR) was used to explore the phase composition of kidney stones placed into a specific object phantom, which imitated the human body. As an imitation of the patient breath, the kidney stone was moved vertically and rotated to an angle of 15 o during the recording of the X-ray pattern. It was shown that rotation and displacement did not distort the X-ray pattern

Solar flare hard and soft x ray relationship determined from SMM HXRBS and BCS data

Science.gov (United States)

Toot, G. David

1989-01-01

The exact nature of the solar flare process is still somewhat a mystery. A key element to understanding flares if the relationship between the hard x rays emitted by the most energetic portions of the flare and the soft x rays from other areas and times. This relationship was studied by comparing hard x ray light curved from the Hard X-Ray Burst Spectrometer (HXRBS) with the soft x ray light curve and its derivation from the Bent Crystal Spectrometer (BCS) which is part of the X-Ray Polychrometer (XRP), these instruments being on the Solar Maximum Mission spacecraft (SMM). Data sample was taken from flares observed with the above instruments during 1980, the peak of the previous maximum of solar activity. Flares were chosen based on complete coverage of the event by several instruments. The HXRBS data covers the x ray spectrum from about 25 keV to about 440 keV in 15 spectral channels, while the BCS data used covers a region of the Spectrum around 3 angstroms including emission from the Ca XIX ion. Both sets of data were summed over their spectral ranges and plotted against time at a maximum time resolution of around 3 seconds. The most popular theory of flares holds that a beam of electrons produces the hard x rays by bremsstrahlung while the soft x rays are the thermal response to this energy deposition. The question is whether the rate of change of soft x ray emission might reflect the variability of the electron beam and hence the variability of the hard x rays. To address this, we took the time derivative of the soft x ray light curve and compared it to the hard flares, 12 of them showed very closed agreement between the soft x ray derivative and the hard x ray light curve. The other five did not show this behavior but were similar to each other in general soft x ray behavior. Efforts to determine basic differences between the two kinds of flares continue. In addition the behavior of soft x ray temperature of flares was examined.

X-ray magnetic circular dichroism and hard X-ray photoelectron spectroscopy of tetragonal Mn72Ge28 epitaxial thin film

Science.gov (United States)

Kim, Jinhyeok; Mizuguchi, Masaki; Inami, Nobuhito; Ueno, Tetsuro; Ueda, Shigenori; Takanashi, Koki

2018-04-01

An epitaxially grown Mn72Ge28 film with a tetragonal crystal structure was fabricated. It was clarified that the film had a perpendicular magnetization and a high perpendicular magnetic anisotropy energy of 14.3 Merg/cm3. The electronic structure was investigated by X-ray magnetic circular dichroism and hard X-ray photoelectron spectroscopy. The obtained X-ray magnetic circular dichroism spectrum revealed that the Mn orbital magnetic moment governed the magnetocrystalline anisotropy of the Mn72Ge28 film. A doublet structure was observed for the Mn 2p3/2 peak of hard X-ray photoelectron spectrum, indicating the spin exchange interaction between the 2p core-hole and 3d valence electrons.

Line focus x-ray tubes-a new concept to produce high brilliance x-rays.

Science.gov (United States)

Bartzsch, Stefan; Oelfke, Uwe

2017-10-27

Currently hard coherent x-ray radiation at high photon fluxes can only be produced with large and expensive radiation sources, such as 3[Formula: see text] generation synchrotrons. Especially in medicine, this limitation prevents various promising developments in imaging and therapy from being translated into clinical practice. Here we present a new concept of highly brilliant x-ray sources, line focus x-ray tubes (LFXTs), which may serve as a powerful and cheap alternative to synchrotrons and a range of other existing technologies. LFXTs employ an extremely thin focal spot and a rapidly rotating target for the electron beam which causes a change in the physical mechanism of target heating, allowing higher electron beam intensities at the focal spot. Monte Carlo simulations and numeric solutions of the heat equation are used to predict the characteristics of the LFXT. In terms of photon flux and coherence length, the performance of the line focus x-ray tube compares with inverse Compton scattering sources. Dose rates of up to 180 Gy [Formula: see text] can be reached in 50 cm distance from the focal spot. The results demonstrate that the line focus tube can serve as a powerful compact source for phase contrast imaging and microbeam radiation therapy. The production of a prototype seems technically feasible.

High spectral resolution measurements of a solar flare hard X-ray burst

International Nuclear Information System (INIS)

Lin, R.P.; Schwartz, R.A.; NASA, Goddard Space Flight Center, Greenbelt, MD)

1987-01-01

Observations are reported of an intense solar flare hard X-ray burst on June 27, 1980, made with a balloon-borne array of liquid nitrogen-cooled Ge detector which provided unprecedented spectral resolution (no more than 1 keV FWHM). The hard X-ray spectra throughout the impulsive phase burst fitted well to a double power-law form, and emission from an isothermal 0.1-1 billion K plasma can be specifically excluded. The temporal variations of the spectrum indicate that the hard X-ray burst is made up of two superposed components: individual spikes lasting about 3-15 sec, which have a hard spectrum and a break energy of 30-65 keV; and a slowly varying component characterized by a soft spectrum with a constant low-energy slope and a break energy which increases from 25 kev to at least 100 keV through the event. The double power-law shape indicates that DC electric field acceleration, similar to that occurring in the earth's auroral zone, may be the source of the energetic electrons which produce the hard X-ray emission. 39 references

Study of moire fringes using synchrotron X-rays

International Nuclear Information System (INIS)

Yoshimura, Jun-ichi

1992-01-01

It has recently been shown that X-ray moire fringes are not exactly the projection of the intensity distribution of the wave field on the exit surface of the crystal, but do oscillate along the beam path behind the crystal. Such nonprojectiveness of moire fringes is inexplicable by the conventional understanding of moire fringes, and therefore is of interest from a fundamental viewpoint as well as practical one. In this paper the phenomena of the nonprojectiveness are described on the basis of the latest experimental data obtained by synchrotron radiation. (author)

Synchrotron radiation X-ray tomographic microscopy (SRXTM) of brachiopod shell interiors for taxonomy: Preliminary report

OpenAIRE

Motchurova-Dekova Neda; Harper David A.T.

2010-01-01

Synchrotron radiation X-ray tomographic microscopy (SRXTM) is a non-destructive technique for the investigation and visualization of the internal features of solid opaque objects, which allows reconstruction of a complete three-dimensional image of internal structures by recording of the differences in the effects on the passage of waves of energy reacting with those structures. Contrary to X-rays, produced in a conventional X-ray tube, the intense synchrot...

In situ 3D characterization of high temperature fatigue damage mechanisms in a cast aluminum alloy using synchrotron X-ray tomography

International Nuclear Information System (INIS)

Dezecot, Sebastien; Buffiere, Jean-Yves; Koster, Alain; Maurel, Vincent; Szmytka, Fabien; Charkaluk, Eric; Dahdah, Nora; El Bartali, Ahmed; Limodin, Nathalie; Witz, Jean-Francois

2016-01-01

Fatigue tests were performed at 250 °C on a cast AlSi7Cu3Mg aluminum alloy and monitored with Synchrotron in situ X-ray tomography in order to understand the micro-mechanisms of crack initiation and propagation. The analysis of the 3D images reveals that internal shrinkage pores are responsible for the main crack initiation. Crack propagation is mainly due to the complex and highly interconnected network of hard particles of the eutectic regions.

Development and characterization of a laser-based hard x-ray source

International Nuclear Information System (INIS)

Tillman, C.

1996-11-01

A laser-produced plasma was generated by focusing 100 fs laser pulses, with an energy of 150 mJ, onto metal targets. The laser intensity was expected to reach 10 17 W/cm -2 . Radiation was emitted from the created plasma, with photon energies up to the MeV region. The laser-based X-ray source was optimized, with the purpose of making it a realistic source of hard X-rays (>10 keV). Dedicated equipment was developed for efficient generation and utilization of the hard X-rays. The X-ray source was characterized with respect to its spatial extent and the X-ray yield. Measurements were made of the spectral distribution, by the use of single-photon-counting detectors in different geometries, crystal spectrometers and dose measurements in combination with absorption filters. Ablation of the target material in the laser produced plasma was investigated. Imaging applications have been demonstrated, including ultrafast (picosecond) X-ray imaging, magnification imaging of up to x80, differential imaging in the spectral domain, and imaging of various biological and technical objects. The biological response of ultra-intense X-ray pulses was assessed in cell-culture exposures. The results indicate that the biological response from ultra-intense X-ray exposures is similar to the response with conventional X-ray tubes. 82 refs., 14 figs

Development and characterization of a laser-based hard x-ray source

Energy Technology Data Exchange (ETDEWEB)

Tillman, C.

1996-11-01

A laser-produced plasma was generated by focusing 100 fs laser pulses, with an energy of 150 mJ, onto metal targets. The laser intensity was expected to reach 10{sup 17} W/cm{sup -2}. Radiation was emitted from the created plasma, with photon energies up to the MeV region. The laser-based X-ray source was optimized, with the purpose of making it a realistic source of hard X-rays (>10 keV). Dedicated equipment was developed for efficient generation and utilization of the hard X-rays. The X-ray source was characterized with respect to its spatial extent and the X-ray yield. Measurements were made of the spectral distribution, by the use of single-photon-counting detectors in different geometries, crystal spectrometers and dose measurements in combination with absorption filters. Ablation of the target material in the laser produced plasma was investigated. Imaging applications have been demonstrated, including ultrafast (picosecond) X-ray imaging, magnification imaging of up to x80, differential imaging in the spectral domain, and imaging of various biological and technical objects. The biological response of ultra-intense X-ray pulses was assessed in cell-culture exposures. The results indicate that the biological response from ultra-intense X-ray exposures is similar to the response with conventional X-ray tubes. 82 refs., 14 figs.

Bragg concentrators for hard (> 10 keV) X-ray astronomy: Status report

Energy Technology Data Exchange (ETDEWEB)

Pareschi, G.; Pasqualini, G. [Ferrara, Univ. (Italy). Dipt. di Fisica; Frontera, F. [CNR, Bologna (Italy). Istituto di TESRE]|[Ferrara, Univ. (Italy). Dipt. di Fisica

1997-09-01

The use of focusing telescopes in hard X-ray (E > 10 keV) astronomy will provide better flux sensitivity and imaging performances with respect to the direct-viewing detectors, utilized until now. They present recent results obtained from their group regarding the possible use of Bragg-diffraction technique to design hard X-ray focusing telescopes.

Bragg concentrators for hard (> 10 keV) X-ray astronomy: Status report

International Nuclear Information System (INIS)

Pareschi, G.; Pasqualini, G.; Frontera, F.; Ferrara, Univ.

1997-01-01

The use of focusing telescopes in hard X-ray (E > 10 keV) astronomy will provide better flux sensitivity and imaging performances with respect to the direct-viewing detectors, utilized until now. They present recent results obtained from their group regarding the possible use of Bragg-diffraction technique to design hard X-ray focusing telescopes

Spectral and temporal properties of the X-ray pulsar SMC X-1 at hard X-rays

Science.gov (United States)

Kunz, M.; Gruber, D. E.; Kendziorra, E .; Kretschmar, P.; Maisack, M.; Mony, B.; Staubert, R.; Doebereiner, S.; Englhauser, J.; Pietsch, W.

1993-01-01

The binary X-ray pulsar SMC X- 1 has been observed at hard X-rays with the High Energy X-Ray Experiment (HEXE) on nine occasions between Nov. 1987 and March 1989. A thin thermal bremsstrahlung fit to the phase averaged spectrum yields a plasma temperature (14.4 +/- 1.3) keV and a luminosity above (1.1 +/- 0.1) x 10 exp 38 erg/s in the 20-80 keV band. Pulse period values have been established for three observations, confirming the remarkably stable spin-up trend of SMC X-1. In one of the three observations the pulse profile was seen to deviate from a dominant double pulsation, while at the same time the pulsed fraction was unusually large. For one observation we determined for the first time the pulsed fraction in narrow energy bands. It increases with photon energy from about 20 percent up to over 60 percent in the energy range from 20 to 80 keV.

NSLS [National Synchrotron Light Source] X-19A beamline performance for x-ray absorption measurements

International Nuclear Information System (INIS)

Yang, C.Y.; Penner-Hahn, J.E.; Stefan, P.M.

1989-01-01

Characterization of the X-19A beamline at the National Synchrotron Light Source (NSLS) is described. The beamline is designed for high resolution x-ray absorption spectroscopy over a wide energy range. All of the beamline optical components are compatible with ultrahigh vacuum (UHV) operation. This permits measurements to be made in a window-less mode, thereby facilitating lower energy (<4 KeV) studies. To upgrade the beamline performance, several possible improvements in instrumentation and practice are discussed to increase photon statistics with an optimum energy resolution, while decreasing the harmonic contamination and noise level. A special effort has been made to improve the stability and UHV compatibility of the monochromator system. Initial x-ray absorption results demonstrate the capabilities of this beamline for x-ray absorption studies of low Z elements (e.g. S) in highly dilute systems. The future use of this beamline for carrying out various x-ray absorption experiments is presented. 10 refs., 4 figs

Hard X-ray-induced optical luminescence via biomolecule-directed metal clusters†

Science.gov (United States)

Pratx, Guillem; Sun, Conroy; Sakamoto, Masanori; Ahmad, Moiz; Volotskova, Olga; Ong, Qunxiang; Teranishi, Toshiharu; Harada, Yoshie

2014-01-01

Here, we demonstrate that biomolecule-directed metal clusters are applicable in the study of hard X-ray excited optical luminescence, promising a new direction in the development of novel X-ray-activated imaging probes. PMID:24463467

Hard X-ray variability of V404 Cygni during the 2015 outburst

Science.gov (United States)

Sánchez-Fernández, C.; Kajava, J. J. E.; Motta, S. E.; Kuulkers, E.

2017-06-01

Aims: Hard X-ray spectra of black hole binaries (BHB) are produced by Comptonization of soft seed photons by hot electrons near the black hole. The slope of the resulting energy spectra is governed by two main parameters: the electron temperature (Te) and optical depth (τ) of the emitting plasma. Given the extreme brightness of V404 Cyg during the 2015 outburst, we aim to constrain the source spectral properties using an unprecedented time resolution in hard X-rays, and to monitor the evolution of Te and τ over the outburst. Methods: We have extracted and analysed 602 X-ray spectra of V404 Cyg obtained by the IBIS/ISGRI instrument on-board INTEGRAL during the 2015 June outburst, using effective integration times ranging between 8 and 176 000 s. We fitted the resulting spectra in the 20-200 keV energy range. Results: We find that while the light curve and soft X-ray spectra of V404 Cyg are remarkably different from those of other BHBs, the spectral evolution of V404 Cyg in hard X-rays and the relations between the spectral parameters are consistent with those observed in other BHBs. We identify a hard branch in which the Te is anti-correlated with the hard X-ray flux, and a soft flaring branch in which the relation reverses. In addition, we find that during long X-ray plateaus detected at intermediate fluxes, the thermal Comptonization models fail to describe the spectra. However, the statistics improve if we allow NH to vary freely in the fits to these spectra. Conclusions: We conclude that the hard branch in V404 Cyg is analogous to the canonical hard state of BHBs. V404 Cyg never seems to enter the canonical soft state, although the soft flaring branch bears resemblance to the BHB intermediate state and ultra-luminous state. The X-ray plateaus are likely the result of absorption by a Compton-thick outflow (NH ≳ 1024 cm-2) which reduces the observed flux by a factor of about 10. Variable covering of the central source by this Compton-thick material may be the

Differential phase contrast setup for a non coherent beamline at HASYLAB using hard X-ray grating interferometer

Energy Technology Data Exchange (ETDEWEB)

Herzen, Julia; Beckmann, Felix; Haibel, Astrid; Schreyer, Andreas [GKSS Research Centre, Geesthacht (Germany); Donath, Tilman; David, Christian; Gruenzweig, Christian [Paul Scherrer Institute, Villigen PSI (Switzerland); Pfeiffer, Franz [Paul Scherrer Institute, Villigen PSI (Switzerland); EPF Lausanne, Lausanne (Switzerland)

2009-07-01

Phase-contrast imaging is a common technique to visualize soft tissue with much higher contrast than the conventional absorption-contrast imaging. Differential phase contrast (DPC), developed at PSI, Switzerland, makes use of a hard x-ray grating interferometer and allows for phase-contrast imaging with high brilliance synchrotron sources as well as with conventional x-ray tubes. It is recently reported also to provide dark field information that is very sensitive to micro structures like porosity within the materials. Here we present the plans to adopt the DPC technique to the HARWI-II materials science beamline, operated by GKSS Research Centre, in cooperation with DESY, Hamburg. This will offer an amount of new applications especially in the field of materials science like for example characterizing new light weight materials like magnesium and studying its corrosion as implant material.

Beer analysis by synchrotron radiation total reflection X-ray fluorescence (SR-TXRF)

Energy Technology Data Exchange (ETDEWEB)

Moreira, Silvana [Universidade Estadual de Campinas, SP (Brazil). Faculdade de Engenharia Civil, Arquitetura e Urbanismo. Dept. de Recursos Hidricos]. E-mail: silvana@fec.unicamp.br; Vives, Ana Elisa S. de [Universidade Metodista de Piracicaba (UNIMEP), Santa Barbara D' Oeste, SP (Brazil). Faculdade de Engenharia, Arquitetura e Urbanismo]. E-mail: aesvives@unimep.br; Nascimento Filho, Virgilio F. [Centro de Energia Nuclear na Agricultura (CENA), Piracicaba, SP (Brazil). Lab. de Instrumentacao Nuclear]. E-mail: virgilio@cena.usp.br; Zucchi, Orgheda L.D.A. [Sao Paulo Univ., Ribeirao Preto, SP (Brazil). Faculdade de Ciencias Farmaceuticas de Ribeirao Preto]. E-mail: olzucchi@fcfrp.usp.br

2005-07-01

In this work the concentrations of P, S, Cl, K, Ca, Mn, Fe, Zn and Br in twenty-nine brands of national and international beers were determined by Synchrotron Radiation Total Reflection X-Ray Fluorescence analysis (SR-TXRF). The results were compared with the limits established by the Brazilian Legislation and the nutritive values established by National Agricultural Library (NAL). The measurements were performed at the X-ray Fluorescence Beamline at Synchrotron Light Source Laboratory, in Campinas, Sao Paulo, Brazil, using a polychromatic beam for excitation. A small volume of 5 {mu}L of sample beers containing just an internal standard, used to correct geometry effects, were analyzed without any pre-treatment. The measuring time was 100 s and the detection limits obtained varied from 1{mu}g.L{sup -1} for Mn and Fe to 15{mu}g.L{sup -1} for P. (author)

Application of thermoluminescence dosimeter on the measurement of hard X-ray pulse energy spectrum

International Nuclear Information System (INIS)

Song Zhaohui; Wang Baohui; Wang Kuilu; Hei Dongwei; Sun Fengrong; Li Gang

2003-01-01

This paper introduces the application of thermoluminescence dosimeter (TLD) which composed by TLD-3500 reader and GR-100 M chips on the measurement of hard X-ray pulse energy spectrum. The idea using Filter Fluorescence Method (FFM) and TLD to measure hard X-ray pulse energy spectrum (from 10 keV to 100 keV) is discussed in details. Considering all the factors of the measuring surrounding, the measurement system of hard X-ray pulse has been devised. The calibration technique of absolute energy response of TLD is established. This method has been applied successfully on the radiation parameters measurement of the huge pulse radiation device-high-power pulser I. Hard X-ray pulse energy spectrum data of the pulser are acquired

The advantages of soft X-rays and cryogenic spectrometers for measuring chemical speciation by X-ray spectroscopy

Energy Technology Data Exchange (ETDEWEB)

Drury, Owen B. [Lawrence Livermore National Laboratory, Advanced Detector Group, 7000 East Ave., L-270, Livermore, CA 94550 (United States); UC Davis, Biophysics Graduate Group, 1 Shields Ave, CA 95616 (United States); LBNL, Advanced Biological and Environmental X-ray Facility, 1 Cyclotron Road, MS 6-2100, Berkeley, CA 92720 (United States); Friedrich, Stephan [Lawrence Livermore National Laboratory, Advanced Detector Group, 7000 East Ave., L-270, Livermore, CA 94550 (United States) and LBNL, Advanced Biological and Environmental X-ray Facility, 1 Cyclotron Road, MS 6-2100, Berkeley, CA 92720 (United States)]. E-mail: friedrich1@llnl.gov; George, Simon J. [LBNL, Advanced Biological and Environmental X-ray Facility, 1 Cyclotron Road, MS 6-2100, Berkeley, CA 92720 (United States); Cramer, Stephen P. [UC Davis, Biophysics Graduate Group, 1 Shields Ave, CA 95616 (United States); LBNL, Advanced Biological and Environmental X-ray Facility, 1 Cyclotron Road, MS 6-2100, Berkeley, CA 92720 (United States)

2006-04-15

We have built a 36-pixel high-resolution superconducting tunnel junction (STJ) soft X-ray spectrometer for chemical analysis of dilute metals by fluorescence-detected X-ray absorption spectroscopy (XAS) at the Advanced Light Source synchrotron. Soft X-ray absorption edges are preferred over traditional hard X-ray spectroscopy at the K-edges, since they have narrower natural linewidths and exhibit stronger chemical shifts. STJ detectors are preferred in the soft X-ray band over traditional Ge or grating spectrometers, since they have sufficient energy resolution to resolve transition metal L and M lines from light element K emission, and sufficient detection efficiency to measure the weak lines of dilute specimens within an acceptable time. We demonstrate the capabilities of our STJ spectrometer for chemical analysis with soft XAS measurements of molybdenum speciation on the Mo M{sub 4,5}-edges.

Integrated image presentation of transmission and fluorescent X-ray CT using synchrotron radiation

Energy Technology Data Exchange (ETDEWEB)

Zeniya, T.; Takeda, T. E-mail: ttakeda@md.tsukuba.ac.jp; Yu, Q.; Hasegawa, Y.; Hyodo, K.; Yuasa, T.; Hiranaka, Y.; Itai, Y.; Akatsuka, T

2001-07-21

We have developed a computed tomography (CT) system with synchrotron radiation (SR) to detect fluorescent X-rays and transmitted X-rays simultaneously. Both SR transmission X-ray CT (SR-TXCT) and SR fluorescent X-ray CT (SR-FXCT) can describe cross-sectional images with high spatial and contrast resolutions as compared to conventional CT. TXCT gives morphological information and FXCT gives functional information of organs. So, superposed display system for SR-FXCT and SR-TXCT images has been developed for clinical diagnosis with higher reliability. Preliminary experiment with brain phantom was carried out and the superposition of both images was performed. The superposed SR-CT image gave us both functional and morphological information easily with high reliability, thus demonstrating the usefulness of this system.

Integrated image presentation of transmission and fluorescent X-ray CT using synchrotron radiation

Science.gov (United States)

Zeniya, T.; Takeda, T.; Yu, Q.; Hasegawa, Y.; Hyodo, K.; Yuasa, T.; Hiranaka, Y.; Itai, Y.; Akatsuka, T.

2001-07-01

We have developed a computed tomography (CT) system with synchrotron radiation (SR) to detect fluorescent X-rays and transmitted X-rays simultaneously. Both SR transmission X-ray CT (SR-TXCT) and SR fluorescent X-ray CT (SR-FXCT) can describe cross-sectional images with high spatial and contrast resolutions as compared to conventional CT. TXCT gives morphological information and FXCT gives functional information of organs. So, superposed display system for SR-FXCT and SR-TXCT images has been developed for clinical diagnosis with higher reliability. Preliminary experiment with brain phantom was carried out and the superposition of both images was performed. The superposed SR-CT image gave us both functional and morphological information easily with high reliability, thus demonstrating the usefulness of this system.

Prospects for compact high-intensity laser synchrotron x-ray and gamma sources

International Nuclear Information System (INIS)

Pogorelsky, I.V.

1996-11-01

A laser interacting with a relativistic electron beam behaves like a virtual wiggler of an extremely short period equal to half of the laser wavelength. This approach opens a route to relatively compact, high-brightness x-ray sources alternative or complementary to conventional synchrotron light sources. Although not new, the laser synchrotron source (LSS) concept is still waiting for a convincing demonstration. Available at the BNL Accelerator Test Facility (ATF), a high-brightness electron beam and the high-power CO 2 laser may be used as prototype LSS brick stones. In a feasible demonstration experiment, 10-GW, 100-ps CO 2 laser beam will be brought to a head-on collision with a 10-ps, 0.5-nC, 50 MeV electron bunch. Flashes of collimated 4.7 keV (2.6 angstrom) x-rays of 10-ps pulse duration, with a flux of ∼ 10 19 photons/sec, will be produced via linear Compton backscattering. The x-ray spectrum is tunable proportionally to the e-beam energy. A rational short-term extension of the proposed experiment would be further enhancement of the x-ray flux to the 10 22 photons/sec level, after the ongoing ATF CO 2 laser upgrade to 5 TW peak power and electron bunch shortening to 3 ps is realized. In the future, exploiting the promising approach of a high-gradient laser wake field accelerator, a compact ''table-top'' LSS of monochromatic gamma radiation may become feasible

Prospects for compact high-intensity laser synchrotron x-ray and gamma sources

International Nuclear Information System (INIS)

Pogorelsky, I.V.

1997-01-01

A laser interacting with a relativistic electron beam behaves like a virtual wiggler of an extremely short period equal to half of the laser wavelength. This approach opens a route to relatively compact, high- brightness x-ray sources alternative or complementary to conventional synchrotron light sources. Although not new, the laser synchrotron source (LSS) concept is still waiting for a convincing demonstration. Available at the BNL Accelerator Test Facility (ATF), a high- brightness electron beam and the high-power C0 2 laser may be used as prototype LSS brick stones. In a feasible demonstration experiment, 10 GW, 100 ps C0 2 laser beam will be brought to a head-on collision with a 10 ps, 0.5 nC, 50 MeV electron bunch. Flashes of collimated 4.7 keV (2.6 A) x-rays of 10-ps pulse duration, with a flux of ∼10 19 photons/sec, will be produced via linear Compton backscattering. The x-ray spectra is tunable proportionally to the e- beam energy. A rational short-term extension of the proposed experiment would be further enhancement of the x-ray flux to the 10 22 photon/sec level, after the ongoing ATF C0 2 laser upgrade to 5 TW peak power and electron bunch shortening to 3 ps is realized. In the future, exploiting the promising approach of a high-gradient laser wake field accelerator, a compact ''table- top'' LSS of monochromatic gamma radiation may become feasible

The Correlation between Hard X-Ray Peak Flux and Soft X-Ray Peak Flux in the Outburst Rise of Low-Mass X-Ray Binaries

NARCIS (Netherlands)

Yu, W.; van der Klis, M.; Fender, R.P.

2004-01-01

We have analyzed Rossi X-Ray Timing Explorer pointed observations of the outbursts of black hole and neutron star soft X-ray transients in which an initial low/hard state, or ``island'' state, followed by a transition to a softer state was observed. In three sources-the black hole transient XTE

A hard x-ray prototype production exposure station at NSLS

International Nuclear Information System (INIS)

Johnson, E.D.; Milne, J.C.

1997-07-01

Exposures conducted at the NSLS R and D beamline (X-27B) for High Aspect Ratio Precision Manufacture have proven sufficiently successful that the authors are constructing a dedicated hard x-ray exposure beamline. The new beamline (X-14B) provides an exposure field ∼ 120 mm wide, three times larger than that of X-27B. The scanner is based on the hydraulic system from the X-27B program. It is optimized for planar exposures and takes advantage of the full 525 mm stroke available. Exposures of multiple substrates and masks will be possible, with the fixturing supporting mounting of substrate holders from other groups (ALS, APS, CAMD, and UW). The function of this beamline is to establish a hard x-ray exposure station where manufacturing scale protocols can be developed and ultimately exploited for production runs

Hard X-ray/soft gamma-ray telescope designs for future astrophysics missions

DEFF Research Database (Denmark)

Ferreira, Desiree Della Monica; Christensen, Finn Erland; Pivovaroff, Michael J.

2013-01-01

We present several concept designs of hard X-ray/soft λ-ray focusing telescopes for future astrophysics missions. The designs are based on depth graded multilayer coatings. These have been successfully employed on the NuSTAR mission for energies up to 80 keV. Recent advances in demonstrating...

A Hard X-Ray Study of the Normal Star-Forming Galaxy M83 with NuSTAR

DEFF Research Database (Denmark)

Yukita, M.; Hornschemeier, A. E.; Lehmer, B. D.

2016-01-01

We present the results from sensitive, multi-epoch NuSTAR observations of the late-type star-forming galaxy M83 (d = 4.6 Mpc). This is the first investigation to spatially resolve the hard (E > 10 keV) X-ray emission of this galaxy. The nuclear region and similar to 20 off-nuclear point sources......, including a previously discovered ultraluminous X-ray source, are detected in our NuSTAR observations. The X-ray hardnesses and luminosities of the majority of the point sources are consistent with hard X-ray sources resolved in the starburst galaxy NGC 253. We infer that the hard X-ray emission is most...

Deducing Electron Properties from Hard X-Ray Observations

Science.gov (United States)

Kontar, E. P.; Brown, J. C.; Emslie, A. G.; Hajdas, W.; Holman, G. D.; Hurford, G. J.; Kasparova, J.; Mallik, P. C. V.; Massone, A. M.; McConnell, M. L.;

X-ray detectors for diffraction studies and their use with synchrotron radiation

International Nuclear Information System (INIS)

Milch, J.

1976-02-01

All techniques for X-ray diffraction studies on biological materials exhibit certain limitations. The characteristics of several X-ray detection systems, namely film, multiwire proportional counter and image intensified TV, are discussed and compared for application to specific biological studies. For the high count-rate situation existing at a synchrotron, it is shown that film is a good choice, but that the image intensified TV exhibits significant advantages. The details of such a system now being used at Princeton with a low intensity source are given and current results presented

Synchrotron X-ray Investigations of Mineral-Microbe-Metal Interactions

International Nuclear Information System (INIS)

Kemner, Kenneth M.; O'Loughlin, Edward J.; Kelly, Shelly D.; Boyanov, Maxim I.

2005-01-01

Interactions between microbes and minerals can play an important role in metal transformations (i.e. changes to an element's valence state, coordination chemistry, or both), which can ultimately affect that element's mobility. Mineralogy affects microbial metabolism and ecology in a system; microbes, in turn, can affect the system's mineralogy. Increasingly, synchrotron-based X-ray experiments are in routine use for determining an element's valence state and coordination chemistry, as well as for examining the role of microbes in metal transformations.

Measured reflectance of graded multilayer mirrors designed for astronomical hard X-ray telescopes

DEFF Research Database (Denmark)

Christensen, Finn Erland; Craig, W.W.; Windt, D.L.

2000-01-01

Future astronomical X-ray telescopes, including the balloon-borne High-Energy Focusing Telescope (HEFT) and the Constellation-X Hard X-ray Telescope (Con-X HXT) plan to incorporate depth-graded multilayer coatings in order to extend sensitivity into the hard X-ray (10 less than or similar to E less......-graded W/Si multilayers optimized for broadband performance up to 69.5 keV (WK-edge). These designs are ideal for both the HEFT and Con-X HXT applications. We compare the measurements to model calculations to demonstrate that the reflectivity can be well described by the intended power law distribution...

An imaging escape gated MPWC for hard X-ray astronomy

International Nuclear Information System (INIS)

Ubertini, P.; Bazzano, A.; Boccaccini, L.; La Padula, C.; Mastropietro, M.; Patriarca, R.; Polcaro, V.F.; Barbareschi, L.; Perotti, F.; Villa, G.; Butler, R.C.; Di Cocco, G.; Spada, G.; Charalambous, P.; Dean, A.J.; Stephen, J.B.

1983-01-01

A scientific forward step in the hard X-ray and soft gamma-ray astronomy will only be possible with the use of a new generation of space borne instruments. Their main characteristics have to be the two-dimensional imaging capability over a large collecting area and the fine spectral resolution in order to discriminate between the weak signal coming from cosmic sources to be detected and the strong background induced by cosmic rays, in the space environment, on the detector. To reach this goal we have developed a new hard X-ray position sensitive proportional counter operating with the escape gate technique in the range 15-150 keV, to be used together with a pseudo-random coded mask in order to obtain sky images. The detector is a high pressure (5 bar) xenon-argon-isobutane filled chamber with a spatial resolution of 30x2 mm and a spectral resolution of 5% at 60 keV on the sensitive area of 3000 cm 2 . (orig.)

Crab Nebula Variations in Hard X-rays

Science.gov (United States)

Wilson-Hodge, Colleen A.

2012-01-01

The Crab Nebula was surprisingly variable from 2001-2010, with less variability before 2001 and since mid-2010. We presented evidence for spectral softening from RXTE, Swift/BAT, and Fermi GBM during the mid-2008-2010 flux decline. We see no clear connections between the hard X-ray variations and the GeV flares

Search for Nonthermal X-Rays from Supernova Remnant Shells

Science.gov (United States)

Petre, R.; Keohane, J.; Hwang, U.; Allen, G.; Gotthelf, E.

The demonstration by ASCA that the nonthermal X-ray emission from the rim of SN1006 is synchrotron emission from TeV electrons, produced in the same environment responsible for cosmic ray protons and nuclei (Koyama et al. 1995, Nature 378, 255), has stimulated a search for nonthermal X-rays from other remnants. Nonthermal emission has subsequently been found to arise in the shells of at least two other remnants, Cas A and IC 443. In Cas A, a hard tail is detected using ASCA, XTE, and OSSE to energies exceeding 100 keV; the shape of the spectrum rules out all mechanisms except synchrotron radiation. In IC 443, the previously known hard emission has been shown using ASCA to be isolated to a small region along the rim of the remnant, where the shock is interacting most strongly with a molecular cloud. Nonthermal X-ray emission is thought to arise here by enhanced cosmic ray production associated with the shock/cloud interaction (Keohane et al. 1997, ApJ in press). We describe the properties of the nonthermal emission in SN1006, Cas A, and IC 443, and discuss the status of our search for nonthermal emission associated with the shocks of other Galactic and LMC SNR's.

Thermal, structural, and fabrication aspects of diamond windows for high power synchrotron x-ray beamlines

International Nuclear Information System (INIS)

Khounsary, A.M.; Phillips, W.

1992-01-01

Recent advances in chemical vapor deposition (CVD) technology have made it possible to produce thin free-standing diamond foils that can be used as the window material in high heat load, synchrotron beamlines. Numerical simulations suggest that these windows can offer an attractive and at times the only altemative to beryllium windows for use in third generation x-ray synchrotron radiation beamlines. Utilization, design, and fabrication aspects of diamond windows for high heat load x-ray beamlines are discussed, as are the microstructure characteristics bearing on diamond's performance in this role. Analytic and numerical results are also presented to provide a basis for the design and testing of such windows

Metals determination in wood treated by synchrotron radiation X-ray fluorescence analysis

International Nuclear Information System (INIS)

Vives, Ana Elisa Sirito de; Medeiros, Jean Gabriel da Silva; Tomazello Filho, Mario

2005-01-01

The paper describes the use of X-Ray fluorescence analysis for distribution and quantification of metals in the hardwood (Eucalyptus sp) and softwood (Pinus sp) treated with CCA (copper-chromium-arsenic). The sapwood/heartwood for hardwood sample and the growth-rings for softwood sample were analyzed. The samples were scanned in 320 mm steps in the vertical direction. For excitation of the elements a white beam synchrotron radiation of ∼ 320 x 180 mm was employed and for the X-ray detection a Si(Li) semiconductor detector. The elements K, Ca, Cr, Mn, Cu, Zn and As were determined. Fundamental parameters were used to quantify the elements concentrations. (author)

Metals determination in wood treated by synchrotron radiation X-ray fluorescence analysis

Energy Technology Data Exchange (ETDEWEB)

Vives, Ana Elisa Sirito de [Universidade Metodista de Piracicaba (UNIMEP), Santa Barbara D' Oeste, SP (Brazil). Faculdade de Engenharia, Arquitetura e Urbanismo]. E-mail: aesvives@unimep.br; Silva, Richard Maximiliano da Cunha [Centro de Energia Nuclear na Agricultura, Piracicaba, SP (Brazil)]. E-mail: maxcunha@cena.usp.br; Medeiros, Jean Gabriel da Silva; Tomazello Filho, Mario [Sao Paulo Univ., Piracicaba, SP (Brazil). Escola Superior de Agricultura Luiz de Queiroz]. E-mail: jeangm@esalq.usp.br; mtomazel@esalq.usp.br; Moreira, Silvana [Universidade Estadual de Campinas, SP (Brazil). Faculdade de Engenharia Civil, Arquitetura e Urbanismo]. E-mail: Silvana@fec.unicamp.br; Zucchi, Orgheda Luiza Araujo Domingues [Sao Paulo Univ., Ribeirao Preto, SP (Brazil). Faculdade de Ciencias Farmaceuticas]. E-mail: olzucchi@fcfrp.usp.br; Barroso, Regina Cely [Universidade do Estado, Rio de Janeiro, RJ (Brazil)]. E-mail: cely@uerj.br

2005-07-01

The paper describes the use of X-Ray fluorescence analysis for distribution and quantification of metals in the hardwood (Eucalyptus sp) and softwood (Pinus sp) treated with CCA (copper-chromium-arsenic). The sapwood/heartwood for hardwood sample and the growth-rings for softwood sample were analyzed. The samples were scanned in 320 mm steps in the vertical direction. For excitation of the elements a white beam synchrotron radiation of {approx} 320 x 180 mm was employed and for the X-ray detection a Si(Li) semiconductor detector. The elements K, Ca, Cr, Mn, Cu, Zn and As were determined. Fundamental parameters were used to quantify the elements concentrations. (author)

Synchrotron X-ray CT of rose peduncles. Evaluation of tissue damage by radiation

International Nuclear Information System (INIS)

Herppich, Werner B.; Zabler, Simon; Dawson, Martin; Choinka, Gerard; Manke, Ingo

2015-01-01

''Bent-neck'' syndrome, an important postharvest problem of cut roses, is probably caused by water supply limitations and/or the structural weakness of vascular bundles of the peduncle tissue. For this reason, advanced knowledge about the microstructures of rose peduncles and their cultivar specific variations may lead to a better understanding of the underlying mechanisms. Synchrotron X-ray computed tomography (SXCT), especially phase-based CT, is a highly suitable technique to nondestructively investigate plants' micro anatomy. SXCT with monochromatic X-ray beams of 30, 40 and 50 keV photon energy was used to evaluate the three-dimensional inner structures of the peduncles of 3 rose cultivars that differ greatly in their bent-neck susceptibility. Results indicated that this technique achieves sufficiently high spatial resolution to investigate complex tissues. However, further investigations with chlorophyll fluorescence analysis (CFA) and optical microscope imagery reveal different kinds of heavy damage of the irradiated regions induced by synchrotron X-rays; in a cultivar-specific manner, partial destruction of cell walls occurred a few hours after X-ray irradiation. Furthermore, a delayed inhibition of photosynthesis accompanied by the degradation of chlorophyll was obvious from CFA within hours and days after the end of CT measurements. Although SXCT is certainly well suited for three-dimensional anatomical analysis of rose peduncles, the applied technique is not nondestructive.

Synchrotron X-ray CT of rose peduncles. Evaluation of tissue damage by radiation

Energy Technology Data Exchange (ETDEWEB)

Herppich, Werner B. [Leibniz-Institut fuer Agrartechnik Potsdam-Bornim e.V., Potsdam (Germany). Abt. Technik im Gartenbau; Matsushima, Uzuki [Iwate Univ., Morioka (Japan). Faculty of Agriculture; Graf, Wolfgang [Association for Technology and Structures in Agriculture (KTBL), Darmstadt (Germany); Zabler, Simon [Fraunhofer-Institut fuer Integrierte Schaltungen (IIS), Wuerzburg (Germany). Project group NanoCT Systems (NCTS); Dawson, Martin [Salford Univ., Greater Manchester (United Kingdom); Choinka, Gerard; Manke, Ingo [Helmholtz Center Berlin for Materials and Energy (HZB), Berlin (Germany)

2015-02-01

''Bent-neck'' syndrome, an important postharvest problem of cut roses, is probably caused by water supply limitations and/or the structural weakness of vascular bundles of the peduncle tissue. For this reason, advanced knowledge about the microstructures of rose peduncles and their cultivar specific variations may lead to a better understanding of the underlying mechanisms. Synchrotron X-ray computed tomography (SXCT), especially phase-based CT, is a highly suitable technique to nondestructively investigate plants' micro anatomy. SXCT with monochromatic X-ray beams of 30, 40 and 50 keV photon energy was used to evaluate the three-dimensional inner structures of the peduncles of 3 rose cultivars that differ greatly in their bent-neck susceptibility. Results indicated that this technique achieves sufficiently high spatial resolution to investigate complex tissues. However, further investigations with chlorophyll fluorescence analysis (CFA) and optical microscope imagery reveal different kinds of heavy damage of the irradiated regions induced by synchrotron X-rays; in a cultivar-specific manner, partial destruction of cell walls occurred a few hours after X-ray irradiation. Furthermore, a delayed inhibition of photosynthesis accompanied by the degradation of chlorophyll was obvious from CFA within hours and days after the end of CT measurements. Although SXCT is certainly well suited for three-dimensional anatomical analysis of rose peduncles, the applied technique is not nondestructive.

THE 22 MONTH SWIFT-BAT ALL-SKY HARD X-RAY SURVEY

International Nuclear Information System (INIS)

Tueller, J.; Baumgartner, W. H.; Markwardt, C. B.; Skinner, G. K.; Mushotzky, R. F.; Barthelmy, S.; Cummings, J.; Gehrels, N.; Holland, S.; Ajello, M.; Beardmore, A.; Evans, P.; Godet, O.; Brandt, W. N.; Burrows, D.; Grupe, D.; Chincarini, G.; Campana, S.; Cusumano, G.; Fenimore, E.

2010-01-01

We present the catalog of sources detected in the first 22 months of data from the hard X-ray survey (14-195 keV) conducted with the Burst Alert Telescope (BAT) coded mask imager on the Swift satellite. The catalog contains 461 sources detected above the 4.8σ level with BAT. High angular resolution X-ray data for every source from Swift-XRT or archival data have allowed associations to be made with known counterparts in other wavelength bands for over 97% of the detections, including the discovery of ∼30 galaxies previously unknown as active galactic nuclei and several new Galactic sources. A total of 266 of the sources are associated with Seyfert galaxies (median redshift z ∼ 0.03) or blazars, with the majority of the remaining sources associated with X-ray binaries in our Galaxy. This ongoing survey is the first uniform all-sky hard X-ray survey since HEAO-1 in 1977. Since the publication of the nine-month BAT survey we have increased the number of energy channels from four to eight and have substantially increased the number of sources with accurate average spectra. The BAT 22 month catalog is the product of the most sensitive all-sky survey in the hard X-ray band, with a detection sensitivity (4.8σ) of 2.2 x 10 -11 erg cm -2 s -1 (1 mCrab) over most of the sky in the 14-195 keV band.

Adaptive Lobster-Eye Hard X-Ray Telescope, Phase I

Data.gov (United States)

National Aeronautics and Space Administration — To address NASA needs for hard X-ray telescopes for starlight detection and wavefront analysis, Physical Optics Corporation (POC) proposes to develop an Adjustable...

The hard X-ray spectrum of Cyg X-1 during the transition in November 1975

International Nuclear Information System (INIS)

Sommer, M.; Maurus, H.; Urbach, R.

1976-01-01

Some observations are reported of the hard X-ray spectrum of Cyg X-1 during a transition to the high state in November 1975, made with a balloon-borne X-ray detector. The range covered was 25 to 150 keV. The data obtained appeared to confirm the characteristic spectral time variation, and suggested a single power law spectrum from 3 to 80 keV, with an increasing spectral index during the upward transition to the high state. A power spectrum is expected if it is assumed that the universe Compton effect is the basic mechanism that produces the hard X-ray tail of Cyg X-1. Spectral time variation may be caused by a varying intensity of an inner soft photon source within a stable hot cloud. (U.K.)

X-ray Free-electron Lasers

Energy Technology Data Exchange (ETDEWEB)

Feldhaus, J.; /DESY; Arthur, J.; Hastings, J.B.; /SLAC

2007-02-23

In a free-electron laser (FEL) the lasing medium is a high-energy beam of electrons flying with relativistic speed through a periodic magnetic field. The interaction between the synchrotron radiation that is produced and the electrons in the beam induces a periodic bunching of the electrons, greatly increasing the intensity of radiation produced at a particular wavelength. Depending only on a phase match between the electron energy and the magnetic period, the wavelength of the FEL radiation can be continuously tuned within a wide spectral range. The FEL concept can be adapted to produce radiation wavelengths from millimeters to Angstroms, and can in principle produce hard x-ray beams with unprecedented peak brightness, exceeding that of the brightest synchrotron source by ten orders of magnitude or more. This paper focuses on short-wavelength FELs. It reviews the physics and characteristic properties of single-pass FELs, as well as current technical developments aiming for fully coherent x-ray radiation pulses with pulse durations in the 100 fs to 100 as range. First experimental results at wavelengths around 100 nm and examples of scientific applications planned on the new, emerging x-ray FEL facilities are presented.

Tabletop synchrotron and its unique features

CERN Document Server

Yamada, H

2002-01-01

Two synchrotrons, AURORA and MIRRORCLE, were built in Ritsumeikan University. MIRRORCLE-20 is the smallest normal conduction synchrotron (15 cm orbit radius and 1.2 m outer diameter) in the world. It uses 2/3 resonance method for electron beam incidence but is not optimized for X-ray generation. MIRRORCLE-6 shall be optimized for X-ray generation. X-ray generated by MIRRORCLE shows very flat white light, rich in hard X-ray, pulse with width changeable from a few mu s to a few ms , wide radiation angle of 25 mrad at MIRRORCLE-20 and 80 mrad at MIRRORCLE-8 and high coherence. The feature such as pulsed light and high coherence is expected to new application which photon radiation cannot practice. Imaging experiments by MIRRORCLE were carried out by Cu plate, Al plate, Teflon and acryl plate. We took a photograph of insect, electric lamp, connector, and cyclotron. New X-ray generation mechanism, X-ray strength, development of tabletop synchrotron and features of X-ray beam are explained. (S.Y.)

Tabletop synchrotron and its unique features

International Nuclear Information System (INIS)

Yamada, Hironari

2002-01-01

Two synchrotrons, AURORA and MIRRORCLE, were built in Ritsumeikan University. MIRRORCLE-20 is the smallest normal conduction synchrotron (15 cm orbit radius and 1.2 m outer diameter) in the world. It uses 2/3 resonance method for electron beam incidence but is not optimized for X-ray generation. MIRRORCLE-6 shall be optimized for X-ray generation. X-ray generated by MIRRORCLE shows very flat white light, rich in hard X-ray, pulse with width changeable from a few μs to a few ms , wide radiation angle of 25 mrad at MIRRORCLE-20 and 80 mrad at MIRRORCLE-8 and high coherence. The feature such as pulsed light and high coherence is expected to new application which photon radiation cannot practice. Imaging experiments by MIRRORCLE were carried out by Cu plate, Al plate, Teflon and acryl plate. We took a photograph of insect, electric lamp, connector, and cyclotron. New X-ray generation mechanism, X-ray strength, development of tabletop synchrotron and features of X-ray beam are explained. (S.Y.)

Performances of synchrotron radiation microbeam focused by monolithic half focusing polycapillary X-ray lens

International Nuclear Information System (INIS)

Sun Tianxi; Liu Zhiguo; He Bo; Wei Shiqiang; Xie Yaning; Liu Tao; Hu Tiandou; Ding Xunliang

2007-01-01

A monolithic half focusing polycapillary X-ray lens (MHFPXRL) composed of 289,000 capillaries is used to produce a synchrotron radiation microbeam. The energy dependence of the output focal distance, focal spot size, transmission efficiency, vertical beam position, and gain in flux density of this microbeam is studied in detail. There is a slight change in the output focal distance of the MHFPXRL when the X-ray energies change

Hard X-ray sources from miniature plasma focus devices

International Nuclear Information System (INIS)

Raspa, V.; Silva, P.; Moreno, J.; Zambra, M.; Soto, L.

2004-01-01

As first stage of a program to design a repetitive pulsed radiation generator for industrial applications, two miniature plasma foci have been designed and constructed at the Chilean commission of nuclear energy. The devices operate at an energy level of the order of tens of joules (PF-50 J, 160 nF capacitor bank, 20-35 kV, 32-100 J, ∼ 150 ns time to peak current) and hundred of joules (PF-400 J, 880 nF, 20-35 kV, 176-539 J, ∼ 300 ns time to peak current). Hard X-rays are being studied in these devices operating with hydrogen. Images of metallic plates with different thickness were obtained on commercial radiographic film, Agfa Curix ST-G2, in order to characterize the energy of the hard X-ray outside of the discharge chamber of PF-400 J. An effective energy of the order of 90 keV was measured under those conditions. X ray images of different metallic objects also have been obtained. (authors)

Hard X-ray sources from miniature plasma focus devices

Energy Technology Data Exchange (ETDEWEB)

Raspa, V. [Buenos Aires Univ., PLADEMA, CONICET and INFIP (Argentina); Silva, P.; Moreno, J.; Zambra, M.; Soto, L. [Comision Chilena de Energia Nuclear, Santiago (Chile)

2004-07-01

As first stage of a program to design a repetitive pulsed radiation generator for industrial applications, two miniature plasma foci have been designed and constructed at the Chilean commission of nuclear energy. The devices operate at an energy level of the order of tens of joules (PF-50 J, 160 nF capacitor bank, 20-35 kV, 32-100 J, {approx} 150 ns time to peak current) and hundred of joules (PF-400 J, 880 nF, 20-35 kV, 176-539 J, {approx} 300 ns time to peak current). Hard X-rays are being studied in these devices operating with hydrogen. Images of metallic plates with different thickness were obtained on commercial radiographic film, Agfa Curix ST-G2, in order to characterize the energy of the hard X-ray outside of the discharge chamber of PF-400 J. An effective energy of the order of 90 keV was measured under those conditions. X ray images of different metallic objects also have been obtained. (authors)

Comparison of three types of XPAD3.2/CdTe single chip hybrids for hard X-ray applications in material science and biomedical imaging

Energy Technology Data Exchange (ETDEWEB)

Buton, C., E-mail: clement.buton@synchrotron-soleil.fr [Synchrotron SOLEIL, L´Orme des Merisiers, Saint-Aubin — BP 48 91192, Gif-sur-Yvette Cedex (France); Dawiec, A. [Synchrotron SOLEIL, L´Orme des Merisiers, Saint-Aubin — BP 48 91192, Gif-sur-Yvette Cedex (France); Graber-Bolis, J.; Arnaud, K. [CPPM, Aix-Marseille Université, CNRS/IN2P3, Marseille (France); Bérar, J.F.; Blanc, N.; Boudet, N. [Université Grenoble Alpes, Institut NÉEL, F-38042 Grenoble (France); CNRS, Institut NÉEL, F-38042 Grenoble (France); Clémens, J.C.; Debarbieux, F. [CPPM, Aix-Marseille Université, CNRS/IN2P3, Marseille (France); Delpierre, P.; Dinkespiler, B. [imXPAD SAS — Espace Mistral, Athélia IV, 297 avenue du Mistral, 13600 La Ciotat (France); Gastaldi, T. [CPPM, Aix-Marseille Université, CNRS/IN2P3, Marseille (France); Hustache, S. [Synchrotron SOLEIL, L´Orme des Merisiers, Saint-Aubin — BP 48 91192, Gif-sur-Yvette Cedex (France); Morel, C.; Pangaud, P. [CPPM, Aix-Marseille Université, CNRS/IN2P3, Marseille (France); Perez-Ponce, H. [imXPAD SAS — Espace Mistral, Athélia IV, 297 avenue du Mistral, 13600 La Ciotat (France); Vigeolas, E. [CPPM, Aix-Marseille Université, CNRS/IN2P3, Marseille (France)

2014-09-11

The CHIPSPECT consortium aims at building a large multi-modules CdTe based photon counting detector for hard X-ray applications. For this purpose, we tested nine XPAD3.2 single chip hybrids in various configurations (i.e. Ohmic vs. Schottky contacts or electrons vs. holes collection mode) in order to select the most performing and best suited configuration for our experimental requirements. Measurements have been done using both X-ray synchrotron beams and {sup 241}Am source. Preliminary results on the image quality, calibration, stability, homogeneity and linearity of the different types of detectors are presented.

The nature of ancient Egyptian copper-containing carbon inks is revealed by synchrotron radiation based X-ray microscopy

OpenAIRE

Christiansen , Thomas; Cotte , Marine; Loredo-Portales , René; Lindelof , Poul ,; Mortensen , Kell; Ryholt , Kim; Larsen , Sine

2017-01-01

International audience; For the first time it is shown that carbon black inks on ancient Egyptian papyri from different time periods and geographical regions contain copper. The inks have been investigated using synchrotron-based micro X-ray fluorescence (XRF) and micro X-ray absorption near-edge structure spectroscopy (XANES) at the European Synchrotron Radiation Facility (ESRF). The composition of the copper-containing carbon inks showed no significant differences that could be related to t...

Short Hard Gamma Ray Bursts And Their Afterglows

CERN Document Server

Dado, Shlomo

2009-01-01

Long duration gamma ray bursts (GRBs) and X-ray flashes (XRFs) are produced by highly- relativistic jets ejected in core-collapse supernova explosions. The origin of short hard gamma-ray bursts (SHBs) has not been established. They may be produced by highly relativistic jets ejected in various processes: mergers of compact stellar objects; large-mass accretion episodes onto compact stars in close binaries or onto intermediate-mass black holes in dense stellar regions; phase transition of compact stars. Natural environments of such events are the dense cores of globular clusters, superstar clusters and young supernova remnants. We have used the cannonball model of GRBs to analyze all Swift SHBs with a well-sampled X-ray afterglow. We show that their prompt gamma-ray emission can be explained by inverse Compton scattering (ICS) of the progenitor's glory light, and their extended soft emission component by ICS of high density light or synchrotron radiation (SR) in a high density interstellar medium within the cl...

X-ray and synchrotron studies of porous silicon

Energy Technology Data Exchange (ETDEWEB)

Sivkov, V. N., E-mail: svn@dm.komisc.ru [Russian Academy of Sciences, Komi Scientific Center, Ural Branch (Russian Federation); Lomov, A. A. [Russian Academy of Sciences, Physical-Technological Institute (Russian Federation); Vasil' ev, A. L. [Russian Academy of Sciences, Shubnikov Institute of Crystallography (Russian Federation); Nekipelov, S. V. [Komi State Pedagogical Institute (Russian Federation); Petrova, O. V. [Russian Academy of Sciences, Komi Scientific Center, Ural Branch (Russian Federation)

2013-08-15

The results of comprehensive studies of layers of porous silicon of different conductivity types, grown by anodizing standard Si(111) substrates in an electrolyte based on fluoric acid and ethanol with the addition of 5% of iodine and kept in air for a long time, are discussed. Measurements are performed by scanning electron microscopy, high-resolution X-ray diffraction, and ultrasoft X-ray spectroscopy using synchrotron radiation. The structural parameters of the layers (thickness, strain, and porosity) and atomic and chemical composition of the porous-silicon surface are determined. It is found that an oxide layer 1.5-2.3-nm thick is formed on the surface of the silicon skeleton. The near-edge fine structure of the Si 2p absorption spectrum of this layer corresponds to the fine structure of the 2p spectrum of well coordinated SiO{sub 2}. In this case, the fine structure in the Si 2p-edge absorption region of the silicon skeleton is identical to that of the 2p absorption spectrum of crystalline silicon.

Applications of synchrotron-based X-ray fluorescence technique in materials science-possibilities at INDUS-2

International Nuclear Information System (INIS)

Tiwari, Manoj K.

2016-01-01

X-ray fluorescence (XRF) spectroscopy has seen remarkable progress over the last few decades. Numerous applications in basic and applied sciences demonstrate its importance. Various advantages of XRF technique have motivated us to construct a microfocus XRF beamline (BL-16) on Indus-2 national synchrotron radiation facility. The BL-16 beamline offers a wide range of usages - both from research laboratories and industries; and for researchers working in diverse fields. Apart from the fields of pure sciences like physics and chemistry, the beamline provides an attractive platform to exercise material science applications, interdisciplinary applied sciences like medical, forensic and environmental studies etc. In addition to micro-XRF characterization, BL-16 beamline allows a user to perform studies using other advanced synchrotron based experimental methodologies, viz; grazing incidence X-ray fluorescence (GIXRF) analysis, chemical speciation, near-edge absorption spectroscopy and X-ray reflectivity studies of thin layered materials etc. The combined XRR-GIXRF analysis feature of the BL-16 beamline offers a novel capability to perform GIXRF assisted depth resolved X-ray studies to investigate chemical state and electronic structure of the thin nano-structured materials. The design aspects and various salient features of the BL-16 beamline X-ray reflectometer will be presented along with the measured performance. (author)

The hard x-ray imager onboard IXO

Science.gov (United States)

Nakazawa, Kazuhiro; Takahashi, Tadayuki; Limousin, Olivier; Kokubun, Motohide; Watanabe, Shin; Laurent, Philippe; Arnaud, Monique; Tajima, Hiroyasu

2010-07-01

The Hard X-ray Imager (HXI) is one of the instruments onboard International X-ray Observatory (IXO), to be launched into orbit in 2020s. It covers the energy band of 10-40 keV, providing imaging-spectroscopy with a field of view of 8 x 8 arcmin2. The HXI is attached beneath the Wide Field Imager (WFI) covering 0.1-15 keV. Combined with the super-mirror coating on the mirror assembly, this configuration provides observation of X-ray source in wide energy band (0.1-40.0 keV) simultaneously, which is especially important for varying sources. The HXI sensor part consists of the semiconductor imaging spectrometer, using Si in the medium energy detector and CdTe in the high energy detector as its material, and an active shield covering its back to reduce background in orbit. The HXI technology is based on those of the Japanese-lead new generation X-ray observatory ASTRO-H, and partly from those developed for Simbol-X. Therefore, the technological development is in good progress. In the IXO mission, HXI will provide a major assets to identify the nature of the object by penetrating into thick absorbing materials and determined the inherent spectral shape in the energy band well above the structure around Fe-K lines and edges.

NuSTAR hard X-ray observations of the Jovian magnetosphere during Juno perijove and apojove intervals

Science.gov (United States)

Dunn, W.; Mori, K.; Hailey, C. J.; Branduardi-Raymont, G.; Grefenstette, B.; Jackman, C. M.; Hord, B. J.; Ray, L. C.

2017-12-01

The Nuclear Spectroscopic Telescope Array (NuSTAR) is the first focusing hard X-ray telescope operating in the 3-79 keV band with sub-arcminute angular resolution (18" FWHM). For the first time, NuSTAR provides sufficient sensitivity to detect/resolve hard X-ray emission from Jupiter above 10 keV, since the in-situ Ulysses observation failed to detect X-ray emission in the 27-48 keV band [Hurley et al. 1993]. The initial, exploratory NuSTAR observation of Jupiter was performed in February 2015 with 100 ksec exposure. NuSTAR detected hard X-ray emission (E > 10 keV) from the south polar region at a marginally significance of 3 sigma level [Mori et al. 2016, AAS meeting poster]. This hard X-ray emission is likely an extension of the non-thermal bremsstrahlung component detected up to 7 keV by XMM-Newton [Branduardi-Raymont et al. 2007]. The Ulysses non-detection suggests there should be a spectral cutoff between 7 and 27 keV. Most intriguingly, the NuSTAR detection of hard X-ray emission from the south aurora is in contrast to the 2003 XMM-Newton observations where soft X-ray emission below 8 keV was seen from both the north and south poles [Gladstone et al. 2002]. Given the marginal, but tantalizing, hard X-ray detection of the southern Jovian aurora, a series of NuSTAR observations with total exposure of nearly half a million seconds were approved in the NuSTAR GO and DDT program. These NuSTAR observations coincided with one Juno apojove (in June 2017) and three perijoves (in May, July and September 2017), also joining the multi-wavelength campaigns of observing Jupiter coordinating with Chandra and XMM-Newton X-ray telescope (below 10 keV) and HST. We will present NuSTAR imaging, spectral and timing analysis of Jupiter. NuSTAR imaging analysis will map hard X-ray emission in comparison with soft X-ray and UV images. In addition to investigating any distinctions between the soft and hard X-ray morphology of the Jovian aurorae, we will probe whether hard X-ray

Hard x-ray nanoprobe of beamline P06 at PETRA III

Energy Technology Data Exchange (ETDEWEB)

Schroer, C. G., E-mail: christian.schroer@desy.de [Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, D-22607 Hamburg (Germany); Department Physik, Universität Hamburg, Luruper Chaussee 149, D-22761 Hamburg (Germany); Baumbach, C. [Institute of Optics and Photonics of Condensed Matter, Technische Universität Chemnitz, D-09126 Chemnitz (Germany); Döhrmann, R.; Kahnt, M.; Reinhardt, J.; Scholz, M.; Schropp, A.; Seyrich, M.; Wittwer, F.; Falkenberg, G. [Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, D-22607 Hamburg (Germany); Klare, S.; Hoppe, R.; Patommel, J.; Ritter, S.; Samberg, D.; Seiboth, F. [Institut für Strukturphysik, Technische Universität Dresden, D-01062 Dresden (Germany)

2016-07-27

The hard x-ray scanning microscope at beamline P06 of PETRA III at DESY in Hamburg serves a large user community, from physics, chemistry, and nanotechnology to the bio-medical, materials, environmental, and geosciences. It has been in user operation since 2012, and is mainly based on nanofocusing refractive x-ray lenses. Using refractive optics, nearly gaussian-limited nanobeams in the range from 50 to 100 nm can be generated in the hard x-ray energy range from 8 to 30 keV. The degree of coherence can be traded off against the flux in the nanobeam by a two-stage focusing scheme. We give a brief overview on published results from this instrument and describe its most important components and parameters.

Report of the workshop on transferring X-ray Lithography Synchrotron (XLS) technology to industry

Energy Technology Data Exchange (ETDEWEB)

Marcuse, W.

1987-01-01

This paper reports on plans to develop an x-ray synchrotron for use in lithography. The primary concern of the present paper is technology transfer from national laboratories to private industry. (JDH)

New hard X-ray sources at 380 declination

International Nuclear Information System (INIS)

Ubertini, P.; Bazzano, A.; La Padula, C.; Polcaro, V.F.

1981-01-01

We report the detection of three new hard X-rays sources emitting in the range 15-150 KeV. Their observation was carried out by means of a balloon borne payload, consisting of two large area high spectral resolution Multiwire Spectroscopic Proportional Counters. (orig.)

On the origin of X-ray spectra in luminous blazars

International Nuclear Information System (INIS)

Sikora, Marek; Janiak, Mateusz; Moderski, Rafał; Nalewajko, Krzysztof; Madejski, Greg M.

2013-01-01

Gamma-ray luminosities of some quasar-associated blazars imply jet powers reaching values comparable to the accretion power even if assuming very strong Doppler boosting and very high efficiency of gamma-ray production. With much lower radiative efficiencies of protons than of electrons, and the recent reports of very strong coupling of electrons with shock-heated protons indicated by particle-in-cell simulations, the leptonic models seem to be strongly favored over the hadronic ones. However, the electron-proton coupling combined with the external-radiation-Compton (ERC) models of gamma-ray production in leptonic models predict extremely hard X-ray spectra, with energy indices α x ∼ 0. This is inconsistent with the observed 2-10 keV slopes of blazars, which cluster around α x ∼ 0.6. This problem can be resolved by assuming that electrons can be efficiently cooled down radiatively to non-relativistic energies, or that blazar spectra are entirely dominated by the synchrotron self-Compton (SSC) component up to at least 10 keV. Here, we show that the required cooling can be sufficiently efficient only at distances r < 0.03 pc. SSC spectra, on the other hand, can be produced roughly co-spatially with the observed synchrotron and ERC components, which are most likely located roughly at a parsec scale. We show that the dominant SSC component can also be produced much further than the dominant synchrotron and ERC components, at distances of ≳ 10 pc. Hence, depending on the spatial distribution of the energy dissipation along the jet, one may expect to see γ-ray/optical events with either correlated or uncorrelated X-rays. In all cases the number of e + e – pairs per proton is predicted to be very low. The direct verification of the proposed SSC scenario, and particularly the question of the co-spatiality of the SSC component with other spectral components, requires sensitive observations in the hard X-ray band. This is now possible with the deployment of the Nu

Combined use of infrared and hard X-ray microprobes for spectroscopy-based neuroanatomy

Science.gov (United States)

Surowka, A. D.; Ziomber, A.; Czyzycki, M.; Migliori, A.; Pieklo, L.; Kasper, K.; Szczerbowska-Boruchowska, M.

2018-05-01

Understanding the pathological triggers that affect the structural and physiological integrity of biochemical milieu of neurons is crucial to extend our knowledge on brain disorders, that are in many circumstances hardly treatable. Over recently, by using sophisticated hyperspectral micro-imaging modalities, it has been placed within our reach to get an insight into high fidelity histological details along with corresponding biochemical information in a label-free fashion, without using any additional chemical fixatives. However, in order to push forwards extensive application of these methods in the clinical arena, it is viable to make further iterations in novel data analysis protocols in order to boost their sensitivity. Therefore, in our study we proposed a new combined approach utilizing both benchtop Fourier transform infrared (FTIR) and synchrotron X-ray fluorescence (SR-XRF) micro-spectroscopies coupled with multivariate data clustering using the K-means algorithm for combined molecular and elemental micro-imaging, so that these complimentary analytical tools could be used for delineating between various brain structures based on their biochemical composition. By utilizing mid-IR transmission FTIR experiments, the biochemical composition in terms of lipids, proteins and phosphodiesters became accessible. In turn, the SR-XRF experiment was carried out at the advanced IAEA X-ray spectrometry station at Elettra Sincrotrone Trieste. By measuring in vacuum and by using the primary exciting X-ray beam, monochromatized to 10.5 keV, we took advantage of accessing the characteristic X-ray lines of a variety of elements ranging from carbon to zinc. Herein, we can report that the developed methodology has high specificity for label-free discriminating between lipid- and protein-rich brain tissue areas.

Synchrotron x-ray methods in studies of thin organic film structure

International Nuclear Information System (INIS)

Gentle, I.

2002-01-01

Full text: In recent years, the study of the structures of organic films as thin as a single monolayer has been revolutionized by methods that take advantage of the characteristics of synchrotron radiation. In particular, the methods of grazing incidence X-ray diffraction (GIXD) and X-ray reflectivity have led to a number of valuable insights into structural aspects of thin films at molecular resolution. Our group has been studying films formed at the air/water interface as insoluble monolayers and subsequently transferred to solid substrates using either the vertical (Langmuir-Blodgett) or horizontal (Langmuir-Schaeffer) methods. The main aim of these experiments is to exert control over film structure in the direction parallel to the substrate surface. This is highly desirable in order to design devices that exploit the optical and electrooptical properties of functional materials, but is difficult to do. By varying the chemical structure of the film materials and controlling deposition conditions a degree of control is possible, but only using synchrotron methods can it be easily verified. We have also developed a novel method of rapidly collecting data from GIXD measurements by the application of area detection (imaging plates), which has made possible measurements of dynamic processes such as in-situ annealing. Such measurements are not possible using traditional scanning methods. One area of current interest is films composed of porphyrins as functional materials, either alone or as mixed films with fatty acids. We have been investigating ways of assembling porphyrins in such a way as to overcome the tendency to aggregate, and to produce patterning and ordered structures in the plane of the interface. Examples will be given of how film composition and deposition method affects the final structure, and of how X-ray methods can be used to elucidate both the structures and the mechanisms. Copyright (2002) Australian X-ray Analytical Association Inc

Possibility of coherent hard x-ray production by pumping with synchrotron radiation and low energy photons. Period covered: November 17, 1976--August 16, 1977

International Nuclear Information System (INIS)

Csonka, P.L.

1977-01-01

Coherent x-rays in the keV range could be produced by pumping a suitable gas with synchrotron radiation in combination with low energy photon beams in the presence of appropriately arranged mirrors. With a wiggler magnet placed in the low beta section of the PEP machine to be constructed at Stanford, 1020 eV coherent photons could be produced from Ne. Appropriate synchrotron radiation will produce a highly ionized cool gas. Low energy photons modify the outer electron structure of ions to enhance lasing: they modify the lifetime of the inverted state, counterbalance unwanted collisionally induced transitions, reduce Stark line broadening

Using x-ray microprobes for environmental research

International Nuclear Information System (INIS)

Cai, Z.; Jastrow, J.; Kemner, K. M.; Lai, B.; Lee, H.-R.; Legnini, D. G.; Miller, R. M.; Pratt, S. T.; Rodrigues, W.; Yun, W.

1998-01-01

Understanding the fate of environmental contaminants is of fundamental importance in the development and evaluation of effective remediation strategies. Among the factors influencing the transport of these contaminants are the chemical speciation of the sample and the chemical and physical attributes of the surrounding medium. Characterization of the spatial distribution and chemical speciation at micron and submicron resolution is essential for studying the microscopic physical, geological, chemical, and biological interfaces that play a crucial role in determining contaminant fate and mobility. Hard X-ray spectroscopy and imaging are powerful techniques for the element-specific investigation of complex environmental samples at the needed micron and submicron resolution. An important advantage of these techniques results from the large penetration depth of hard X-rays in water. This minimizes the requirements for sample preparation and allows the detailed study of hydrated samples. This paper discusses some current problems in environmental science that can be addressed by using synchrotron-based X-ray imaging and spectroscopy. These concepts are illustrated by the results of recent X-ray microscopy studies at the Advanced Photon Source

Hard X-ray Optics Technology Development for Astronomy at the Marshall Space Flight Center

Science.gov (United States)

Gubarev, Mikhail; Ramsey, Brian; Kilaru, Kiranmayee

2009-01-01

Grazing-incidence telescopes based on Wolter 1 geometry have delivered impressive advances in astrophysics at soft-x-ray wavelengths, while the hard xray region remains relatively unexplored at fine angular resolution and high sensitivities. The ability to perform ground-breaking science in the hard-x-ray energy range had been the motivation for technology developments aimed at fabricating low-cost, light-weight, high-quality x-ray mirrors. Grazing-incidence x-ray optics for high-energy astrophysical applications is being developed at MSFC using the electroform-nickel replication process.

The application of thermoluminescence dosimeter on the measurement of hard X-ray pulse energy spectrum

International Nuclear Information System (INIS)

Song Zhaohui; Wang Baohui; Wang Kuilu; Hei Dongwei; Sun Fengrong; Li Gang

2001-01-01

This paper introduce the application of thermoluminescence dosimeter (TLD) which composed by TLD-3500 Reader and TLD-100M chips on the measurement of hard X-ray pulse energy spectrum. The idea, using Filter Fluorescence Method (FFM) and TLD to measure hard X-ray pulse energy spectrum (from 10 keV to 100 keV), is discussed in details. Considering all the factors of the measuring surroundings, the measurement system of hard X-ray pulse has been devised. The calibration technique of absolute energy response of TLD is established. This method has been applied successfully on the radiation parameters measurement of the huge pulse radiation device -high-power pulser I. Hard X-ray pulse energy spectrum data of the pulser are acquired

Versatile, reprogrammable area pixel array detector for time-resolved synchrotron x-ray applications

Energy Technology Data Exchange (ETDEWEB)

Gruner, Sol [Cornell Univ., Ithaca, NY (United States)

2010-05-01

The final technical report for DOE grant DE-SC0004079 is presented. The goal of the grant was to perform research, development and application of novel imaging x-ray detectors so as to effectively utilize the high intensity and brightness of the national synchrotron radiation facilities to enable previously unfeasible time-resolved x-ray research. The report summarizes the development of the resultant imaging x-ray detectors. Two types of detector platforms were developed: The first is a detector platform (called a Mixed-Mode Pixel Array Detector, or MM-PAD) that can image continuously at over a thousand images per second while maintaining high efficiency for wide dynamic range signals ranging from 1 to hundreds of millions of x-rays per pixel per image. Research on an even higher dynamic range variant is also described. The second detector platform (called the Keck Pixel Array Detector) is capable of acquiring a burst of x-ray images at a rate of millions of images per second.

INTEGRAL SPI Observations of Cygnus X-1 in the Soft State: What about the Jet Contribution in Hard X-Rays?

Science.gov (United States)

Jourdain, E.; Roques, J. P.; Chauvin, M.

2014-07-01

During the first 7 yr of the INTEGRAL mission (2003-2009), Cyg X-1 has essentially been detected in its hard state (HS), with some incursions in intermediate HSs. This long, spectrally stable period allowed in particular the measurement of the polarization of the high-energy component that has long been observed above 200 keV in this peculiar object. This result strongly suggests that here we see the contribution of the jet, known to emit a strong synchrotron radio emission. In 2010 June, Cyg X-1 underwent a completed transition toward a soft state (SS). It gave us the unique opportunity to study in detail the corona emission in this spectral state, and to investigate in particular the behavior of the jet contribution. Indeed, during the SS, the hard X-ray emission decreases drastically, with its maximum energy shifted toward lower energy and its flux divided by a factor of ~5-10. Interestingly, the radio emission follows a similar drop, supporting the correlation between the jet emission and the hard component, even though the flux is too low to quantify the polarization characteristics. Based on observations with INTEGRAL, an ESA project with instruments and science data center funded by ESA member states (especially the PI countries: Denmark, France, Germany, Italy, Spain, and Switzerland), the Czech Republic and Poland with the participation of Russia and USA.

Solar Coronal Events with Extended Hard X-ray and Gamma-ray Emission

Science.gov (United States)

Hudson, H. S.

2017-12-01

A characteristic pattern of solar hard X-ray emission, first identified in SOL1969-03-31 by Frost & Dennis (1971) now has been linked to prolonged high-energy gamma-ray emission detected by the Fermi/LAT experiment, for example in SOL2014-09-01. The distinctive features of these events include flat hard X-ray spectra extending well above 100 keV, a characteristic pattern of time development, low-frequency gyrosynchrotron peaks, CME association, and gamma-rays identifiable with pion decay originating in GeV ions. The identification of these events with otherwise known solar structures nevertheless remains elusive, in spite of the wealth of imagery available from AIA. The quandary is that these events have a clear association with CMEs in the high corona, and yet the gamma-ray production implicates the photosphere itself. The vanishingly small loss cone in the nominal acceleration region makes this extremely difficult. I propose direct inward advection of a part of the SEP particle population, as created on closed field structures, as a possible resolution of this puzzle, and note that this requires retracting magnetic structures on long time scales following the flare itself.

Synchrotron x-ray diffraction studies of the structural properties of electrode materials in operating battery cells

International Nuclear Information System (INIS)

Thurston, T.R.; Jisrawi, N.M.; Mukerjee, S.; Yang, X.Q.; McBreen, J.; Daroux, M.L.; Xing, X.K.

1996-01-01

Hard x rays from a synchrotron source were utilized in diffraction experiments which probed the bulk of electrode materials while they were operating in situ in battery cells. Two technologically relevant electrode materials were examined; an AB 2 -type anode in a nickel endash metal endash hydride cell and a LiMn 2 O 4 cathode in a Li-ion open-quote open-quote rocking chair close-quote close-quote cell. Structural features such as lattice expansions and contractions, phase transitions, and the formation of multiple phases were easily observed as either hydrogen or lithium was electrochemically intercalated in and out of the electrode materials. The relevance of this technique for future studies of battery electrode materials is discussed. copyright 1996 American Institute of Physics

From Storage Rings to Free Electron Lasers for Hard X-Rays

International Nuclear Information System (INIS)

Nuhn, H

2004-01-01

The intensity of X-ray sources has increased at a rapid rate since the late 1960s by 10 orders of magnitude and more through the use of synchrotron radiation produced by bending magnets, wigglers and undulators. Three generations of radiation sources have been identified depending on amplitude and quality of the radiation provided. While user facilities of the third generation were being constructed a new concept of radiation generating devices was being developed that offers an even larger increase in peak and average brightness than had been achieved till then. The new concept of the X-ray Free Electron Laser based on the principle of Self-Amplified Spontaneous Emission will be the basis of fourth generation X-ray source user facilities of this century. The paper will start with a brief history of the development of x-ray sources, discuss some of the differences between storage ring and free electron laser based approaches, and close with an update of the present development of x-ray free electron laser user facilities

From Storage Rings to Free Electron Lasers for Hard X-Rays

Energy Technology Data Exchange (ETDEWEB)

Nuhn, H

2004-01-09

The intensity of X-ray sources has increased at a rapid rate since the late 1960s by 10 orders of magnitude and more through the use of synchrotron radiation produced by bending magnets, wigglers and undulators. Three generations of radiation sources have been identified depending on amplitude and quality of the radiation provided. While user facilities of the third generation were being constructed a new concept of radiation generating devices was being developed that offers an even larger increase in peak and average brightness than had been achieved till then. The new concept of the X-ray Free Electron Laser based on the principle of Self-Amplified Spontaneous Emission will be the basis of fourth generation X-ray source user facilities of this century. The paper will start with a brief history of the development of x-ray sources, discuss some of the differences between storage ring and free electron laser based approaches, and close with an update of the present development of x-ray free electron laser user facilities.

From storage rings to free electron lasers for hard x-rays

International Nuclear Information System (INIS)

Nuhn, Heinz-Dieter

2004-01-01

The intensity of x-ray sources has increased at a rapid rate since the late 1960s by ten orders of magnitude and more through the use of synchrotron radiation produced by bending magnets, wigglers and undulators. Three generations of radiation sources have been identified depending on amplitude and quality of the radiation provided. While user facilities of the third generation were being constructed, a new concept of radiation generating devices was being developed that offers an even larger increase in peak and average brightness than had been achieved till then. The new concept of the x-ray free electron laser based on the principle of self-amplified spontaneous emission will be the basis of fourth generation x-ray source user facilities of this century. The paper will start with a brief history of the development of x-ray sources, it will then discuss some of the differences between storage ring and free electron laser based approaches, and will close with an update of the present development of x-ray free electron laser user facilities

Optics for protein microcrystallography using synchrotron and laboratory X-ray sources

International Nuclear Information System (INIS)

Varghese, J.N.; Van Donkelaar, A.; Balaic, D.X.; Barnea, Z.

2000-01-01

Full text: For protein crystallography, a highly-intense focused beam overcomes a serious constraint in current biological research: the inability of many protein molecules to form crystals larger than a few tens of microns in size. High structure-resolution X-ray diffraction analysis of microcrystals is currently only being studied at synchrotron X-ray sources. We shall examine how this is being carried out, and also report the development of a novel tapered glass monocapillary toroidal-mirror optic, which achieves a high-intensity, low-divergence focused beam from a rotating-anode Xray generator. We have used this optic, which demonstrates an ∼28x intensity gain at the beam focus to solve the structure of a plant exoglucanse/inhibtor complex microcrystal to 2.8 Angstroms, with volume equivalent to a 30-micron-edge cube

X-ray diffraction on nanoparticles chromium and nickel oxides obtained by gelatin using synchrotron radiation

International Nuclear Information System (INIS)

Menezes, Alan Silva de; Medeiros, Angela Maria de Lemos; Miranda, Marcus Aurelio Ribeiro; Almeida, Juliana Marcela Abraao; Remedios, Claudio Marcio Rocha; Silva, Lindomar R.D. da; Gouveia, S.T.; Sasaki, Jose Marcos; Jardim, P.M.

2003-01-01

Full text: Cr 2 O 3 nanoparticles has many applications like green pigments, wear resistance, and coating materials for thermal protection. Several methods to produce chromium oxide nanoparticles have already been studied, gas condensation, laser induced pyrolysis, microwave plasma, sol-gel and gamma radiation methods. Many applications for this kind of material can be provide concerning the particle size. For instance, particle size approximately of 200 nm are preferable as pigment due to its opacity and below 50 nm can be used as transparent pigment. In this work we have demonstrated that chromium and nickel oxide nanoparticles can be prepared by gelatin method. X-Ray diffraction (XRD) show that mean particle size for chromium oxide of 15-150 nm and nickel oxide of 90 nm were obtained for several temperature of sintering. The X-Ray powder diffraction pattern were performed using Synchrotron Radiation X-Ray source at XRD1 beamline in National Laboratory of Light Synchrotron (LNLS). (author)

Effects of synchrotron radiation spectrum energy on polymethyl methacrylate photosensitivity to deep x-ray lithography

International Nuclear Information System (INIS)

Mekaru, Harutaka; Utsumi, Yuichi; Hattori, Tadashi

2003-01-01

Since X-ray lithography requires a high photon flux to achieve deep resist exposure, a synchrotron radiation beam, which is not monochromatized, is generally used as a light source. If the synchrotron radiation beam is monochromatized, photon flux will decrease rapidly. Because of this reason, the wavelength dependence of the resist sensitivity has not been investigated for deep X-ray lithography. Measuring the spectrum of a white beam with a Si solid-state detector (SSD) is difficult because a white beam has a high intensity and an SSD has a high sensitivity. We were able to measure the spectrum and the photocurrent of a white beam from a beam line used for deep X-ray lithography by keeping the ring current below 0.05 mA. We evaluated the characteristics of the output beam based on the measured spectrum and photocurrent, and used them to investigate the relationship between the total exposure energy and the dose-processing depth with polymethyl methacrylate (PMMA). We found that it is possible to guess the processing depth of PMMA from the total exposure energy in deep X-ray lithography. (author)

Hard X ray lines from neutron stars

Energy Technology Data Exchange (ETDEWEB)

Polcaro, V.F.; Bazzano, A.; La Padula, C.; Ubertini, P.

1982-01-01

Experimental evidence is presented and evaluated concerning the features of the hard X-ray spectra detected in a number of cosmic X-ray sources which contain a neutron star. The strong emission line at cyclotron resonance detected in the spectrum of Her XI at an energy of 58 keV is evaluated and the implications of this finding are discussed. Also examined is the presence of spectral features in the energy range 20-80 keV found in the spectra of gamma-ray bursts, which have been interpreted as cyclotron resonance from interstellar-gas-accreting neutron stars. The less understood finding of a variable emission line at approximately 70 keV in the spectrum of the Crab Pulsar is considered. It is determined that several features varying with time are present in the spectra of cosmic X-ray sources associated with neutron stars. If these features are due to cyclotron resonance, it is suggested that they provide a direct measurement of neutron star magnetic fields on the order of 10 to the 11th-10 to the 13th Gauss. However, the physical condition of the emitting region and its geometry are still quite obscure.

Mechanical design of thin-film diamond crystal mounting apparatus for coherence preservation hard x-ray optics

International Nuclear Information System (INIS)

Shu, Deming; Shvyd’ko, Yuri V.; Stoupin, Stanislav; Kim, Kwang-Je

2016-01-01

A new thin-film diamond crystal mounting apparatus has been designed at the Advanced Photon Source (APS) for coherence preservation hard x-ray optics with optimized thermal contact and minimized crystal strain. This novel mechanical design can be applied to new development in the field of: x-ray optics cavities for hard x-ray free-electron laser oscillators (XFELOs), self-seeding monochromators for hard x-ray free-electron laser (XFEL) with high average thermal loading, high heat load diamond crystal monochromators and beam-sharing/beam-split-and-delay devices for XFEL facilities and future upgraded high-brightness coherent x-ray source in the MBA lattice configuration at the APS.

Mechanical design of thin-film diamond crystal mounting apparatus for coherence preservation hard x-ray optics

Energy Technology Data Exchange (ETDEWEB)

Shu, Deming, E-mail: shu@aps.anl.gov; Shvyd’ko, Yuri V.; Stoupin, Stanislav; Kim, Kwang-Je [Advanced Photon Source, Argonne National Laboratory, Argonne, IL 60439, U.S.A (United States)

2016-07-27

A new thin-film diamond crystal mounting apparatus has been designed at the Advanced Photon Source (APS) for coherence preservation hard x-ray optics with optimized thermal contact and minimized crystal strain. This novel mechanical design can be applied to new development in the field of: x-ray optics cavities for hard x-ray free-electron laser oscillators (XFELOs), self-seeding monochromators for hard x-ray free-electron laser (XFEL) with high average thermal loading, high heat load diamond crystal monochromators and beam-sharing/beam-split-and-delay devices for XFEL facilities and future upgraded high-brightness coherent x-ray source in the MBA lattice configuration at the APS.

Theoretical modeling of Comptonized X-ray spectra of super-Eddington accretion flow: Origin of hard excess in ultraluminous X-ray sources

Science.gov (United States)

Kitaki, Takaaki; Mineshige, Shin; Ohsuga, Ken; Kawashima, Tomohisa

2017-12-01

X-ray continuum spectra of super-Eddington accretion flow are studied by means of Monte Carlo radiative transfer simulations based on the radiation hydrodynamic simulation data, in which both thermal- and bulk-Compton scatterings are taken into account. We compare the calculated spectra of accretion flow around black holes with masses of MBH = 10, 102, 103, and 104 M⊙ for a fixed mass injection rate (from the computational boundary at 103 rs) of 103 LEdd/c2 (with rs, LEdd, and c being the Schwarzschild radius, the Eddington luminosity, and the speed of light, respectively). The soft X-ray spectra exhibit mass dependence in accordance with the standard-disk relation; the maximum surface temperature is scaled as T ∝ M_{ BH}^{ -1/4}. The spectra in the hard X-ray band, by contrast with soft X-ray, look to be quite similar among different models, if we normalize the radiation luminosity by MBH. This reflects that the hard component is created by thermal- and bulk-Compton scatterings of soft photons originating from an accretion flow in the overheated and/or funnel regions, the temperatures of which have no dependence on mass. The hard X-ray spectra can be reproduced by a Wien spectrum with the temperature of T ˜ 3 keV accompanied by a hard excess at photon energy above several keV. The excess spectrum can be fitted well with a power law with a photon index of Γ ˜ 3. This feature is in good agreement with that of the recent NuSTAR observations of ULXs (ultra-luminous X-ray sources).

X-ray emission from BL Lac objects: Comparison to the synchrotron self-Compton models

International Nuclear Information System (INIS)

Schwartz, D.A.; Madejski, G.; Ku, W.H.-M.

1982-01-01

As one part of our joint study of the X-ray properties of BL Lac objects, the authors compare the measured X-ray flux densities with those predicted using the synchrotron self-Compton (SSC) formalism (Jones et al. 1974). Naive application of the formalism predicts X-ray fluxes from 10 -3 to 10 5 those observed. They therefore ask what we can learn by simply assuming the SSC mechanism, and looking for ways to reconcile the observed and measured X-ray fluxes. This paper reports investigation of beaming factors due to relativistic ejection of a radiation source which is isotropic in its own rest frame. The authors conclude that large Lorentz factors, GAMMA approximately > 10, do not apply to BL Lac objects as a class. (Auth.)

Advanced Nanoscale Characterization of Cement Based Materials Using X-Ray Synchrotron Radiation: A Review

KAUST Repository

Chae, Sejung R.; Moon, Juhyuk; Yoon, Seyoon; Bae, Sungchul; Levitz, Pierre; Winarski, Robert; Monteiro, Paulo J. M.

2013-01-01

We report various synchrotron radiation laboratory based techniques used to characterize cement based materials in nanometer scale. High resolution X-ray transmission imaging combined with a rotational axis allows for rendering of samples in three

Elemental Composition of Mars Return Samples Using X-Ray Fluorescence Imaging at the National Synchrotron Light Source II

Science.gov (United States)

Thieme, J.; Hurowitz, J. A.; Schoonen, M. A.; Fogelqvist, E.; Gregerson, J.; Farley, K. A.; Sherman, S.; Hill, J.

2018-04-01

NSLS-II at BNL provides a unique and critical capability to perform assessments of the elemental composition and the chemical state of Mars returned samples using synchrotron radiation X-ray fluorescence imaging and X-ray absorption spectroscopy.

Hard x ray imaging and the relative contribution of thermal and nonthermal emission in flares

International Nuclear Information System (INIS)

Holman, G.D.

1986-01-01

The question of whether the impulsive 25 to 100 keV x ray emission from solar flares is thermal or nonthermal has been a long-standing controversy. Both thermal and nonthermal (beam) models have been developed and applied to the hard x ray data. It now seems likely that both thermal and nonthermal emission have been observed at hard x ray energies. The Hinotori classification scheme, for example, is an attempt to associate the thermal-nonthermal characteristics of flare hard x ray emission with other flare properties. From a theoretical point of view, it is difficult to generate energetic, nonthermal electrons without dumping an equal or greater amount of energy into plasma heating. On the other hand, any impulsive heating process will invariably generate at least some nonthermal particles. Hence, strictly speaking, although thermal or nonthermal emission may dominate the hard x ray emission in a given energy range for a given flare, there is no such thing as a purely thermal or nonthermal flare mechanism

Relationship between type III-V radio and hard X-ray bursts

International Nuclear Information System (INIS)

Stewart, R.T.

1978-01-01

Type III-V radio bursts are found to be closely associated with impulsive hard X-ray bursts. Probably 0.1% to 1% of the fast electrons in the X-ray source region escape to heights >0.1 solar radii in the corona and excite the type III-V burst. (Auth.)

Characterizing X-Ray and Radio Emission in the Black Hole X-Ray Binary V404 Cygni During Quiescence

Science.gov (United States)

Rana, Vikram; Loh, Alan; Corbel, Stephane; Tomsick, John A.; Chakrabarty, Deepto; Walton, Dominic J.; Barret, Didier; Boggs, Steven E.; Christensen, Finn E.; Craig, William;

The synchrotron radiation

International Nuclear Information System (INIS)

Chevallier, P.

1994-01-01

Synchrotron Radiation is a fantastic source of electromagnetic radiation the energy spectrum of which spreads continuously from the far infrared to hard X-rays. For this reason a wide part of the scientific community, fundamentalists as well as industry, is concerned by its use. We shall describe here the main properties of this light source and give two examples of application in the field of characterization of materials: EXAFS (Extended X-Ray Absorption Fine Structure) and X-ray fluorescence. (author). 8 figs., 21 refs

MICROANALYSIS OF MATERIALS USING SYNCHROTRON RADIATION.

Energy Technology Data Exchange (ETDEWEB)

JONES,K.W.; FENG,H.

2000-12-01

High intensity synchrotron radiation produces photons with wavelengths that extend from the infrared to hard x rays with energies of hundreds of keV with uniquely high photon intensities that can be used to determine the composition and properties of materials using a variety of techniques. Most of these techniques represent extensions of earlier work performed with ordinary tube-type x-ray sources. The properties of the synchrotron source such as the continuous range of energy, high degree of photon polarization, pulsed beams, and photon flux many orders of magnitude higher than from x-ray tubes have made possible major advances in the possible chemical applications. We describe here ways that materials analyses can be made using the high intensity beams for measurements with small beam sizes and/or high detection sensitivity. The relevant characteristics of synchrotron x-ray sources are briefly summarized to give an idea of the x-ray parameters to be exploited. The experimental techniques considered include x-ray fluorescence, absorption, and diffraction. Examples of typical experimental apparatus used in these experiments are considered together with descriptions of actual applications.

Determination of electronic and atomic properties of surface, bulk and buried interfaces: Simultaneous combination of hard X-ray photoelectron spectroscopy and X-ray diffraction

Energy Technology Data Exchange (ETDEWEB)

Rubio-Zuazo, J., E-mail: rubio@esrf.fr [SpLine, Spanish CRG BM25 Beamline at the ESRF, ESRF, B.P. 220, F-38043 Grenoble (France); Instituto de Ciencia de Materiales de Madrid, ICMM, CSIC, Cantoblanco, E-28049 Madrid (Spain); Castro, G.R. [SpLine, Spanish CRG BM25 Beamline at the ESRF, ESRF, B.P. 220, F-38043 Grenoble (France); Instituto de Ciencia de Materiales de Madrid, ICMM, CSIC, Cantoblanco, E-28049 Madrid (Spain)

2013-10-15

Highlights: •We have developed a novel and exceptional tool for non-destructive characterization of bulk and buried interfaces that combine XRD and HAXPES. •We studied the correlation between the atomic, electronic and transport properties of oxygen deficient manganite thin films. •The diffraction data showed a cooperative tilt of the MnO{sub 6} block along the out-of-plane direction. •We shown the absence of the conventional basal plane rotation for the oxygen deficient samples. -- Abstract: Hard X-ray photoelectron spectroscopy (HAXPES) is a powerful novel emerging technique for bulk compositional, chemical and electronic properties determination in a non-destructive way. It benefits from the exceptionally large escape depth of high kinetic energy photoelectrons enabling the study of bulk and buried interfaces up to several tens of nanometres depth. Its advantage over conventional XPS is based on the long mean free path of high kinetic energetic photoelectrons. Using the advantage of tuneable X-ray radiation provided by synchrotron sources the photoelectron kinetic energy, i.e. the information depth can be changed and consequently electronic and compositional depth profiles can be obtained. The combination of HAXPES with an atomic structure sensitive technique, as X-ray diffraction, opens a new research field with great potential for many systems in which their electronic properties are intimately linked to their crystallographic structure. At SpLine, the Spanish CRG Beamline at the European Synchrotron Radiation Facility (ESRF) we have developed a novel and exceptional set-up that combine grazing incidence X-ray diffraction (GIXRD) and HAXPES. Both techniques can be operated simultaneously on the same sample and using the same excitation source. The set-up includes a heavy 2S+3D diffractometer and UHV chamber equipped with an electrostatic analyzer. The UHV chamber has also MBE evaporation sources, an ion gun, a LEED optic, a sample heating and cooling

Achieving few-femtosecond time-sorting at hard X-ray free-electron lasers

Science.gov (United States)

Harmand, M.; Coffee, R.; Bionta, M. R.; Chollet, M.; French, D.; Zhu, D.; Fritz, D. M.; Lemke, H. T.; Medvedev, N.; Ziaja, B.; Toleikis, S.; Cammarata, M.

2013-03-01

Recently, few-femtosecond pulses have become available at hard X-ray free-electron lasers. Coupled with the available sub-10 fs optical pulses, investigations into few-femtosecond dynamics are not far off. However, achieving sufficient synchronization between optical lasers and X-ray pulses continues to be challenging. We report a `measure-and-sort' approach, which achieves sub-10 fs root-mean-squared (r.m.s.) error measurement at hard X-ray FELs, far beyond the 100-200 fs r.m.s. jitter limitations. This timing diagnostic, now routinely available at the Linac Coherent Light Source (LCLS), is based on ultrafast free-carrier generation in optically transparent materials. Correlation between two independent measurements enables unambiguous demonstration of ~6 fs r.m.s. error in reporting the optical/X-ray delay, with single shot error suggesting the possibility of reaching few-femtosecond resolution.

Effects of synchrotron x-rays on PVD deposited and ion implanted α-Si

International Nuclear Information System (INIS)

Yu, K.M.; Wang, L.; Walukiewicz, W.; Muto, S.; McCormick, S.; Abelson, J.R.

1997-01-01

The authors have studied the effects of intense X-ray irradiation on the structure of amorphous Si films. The films were obtained by either physical vapor deposition or by implantation of high energy ions into crystalline Si. They were exposed to different total doses of synchrotron X-rays. From the EXAFS and EXELFS measurements they find that an exposure to X-rays increases the Si coordination number. Also in the PVD films a prolonged X-ray exposure enlarges, by about 2%, the Si-Si bond length. Raman spectroscopy shows that Si amorphized with high energy ions contains small residual amounts of crystalline material. Irradiation of such films with X-rays annihilates those crystallites resulting in homogeneously amorphous layer with a close to four-fold coordination of Si atoms. This rearrangement of the local structure has a pronounced effect on the crystallization process of the amorphous films. Thermal annealing of X-ray irradiated ion amorphized films leads to nearly defect free solid phase epitaxy at 500 C. Also they observe a delay in the onset of the crystallization process in X-ray irradiated PVD films. They associate this with a reduced concentration of nucleation centers in the x-ray treated materials

Short term variation of Cyg X-1 in the hard x-ray region

International Nuclear Information System (INIS)

Doi, Kosei

1978-01-01

Cyg X-1 is a peculiar celestial body considered to be a close binary system of a black hole and a blue super-giant star. It is presently known that the time fluctuation of Cyg X-1 is considerably complex, ranging from seconds to days or months. Of these variation, attention has been paid to the short time variation in relation to the black hole theory. Observations of fluctuations in the order of second have been limited to soft X-ray (20 keV or more) so far, because great technical difficulties are involved due to the low intensity of hard X-ray. The present investigation is based on the fluctuations in the order of second in hard X-ray, and was conducted by employing an unprecedented large area X-ray telescope. The text describes on the brief history of the short time fluctuation, explains the experimental plan, X-ray detecting system, flight of a balloon and the analyses and discussions of fluctuation factor by variation function method, and gives the analysis data and conclusion. The observations resulted in the fact that the fluctuations in the order of second were small at 20 to 30 keV, but become large when energy is higher or lower than this value. The most natural explanation available for this result may be that it is essentially spectrum fluctuation, being inverse correlation in higher and lower energies. Physical meaning of such spectrum fluctuation is considered in connection with precipitating disk model around a black hole. (Wakatsuki, Y.)

Short term variation of Cyg X-1 in the hard x-ray region

Energy Technology Data Exchange (ETDEWEB)

Doi, Kosei [Tokyo Univ. (Japan). Inst. of Space and Aeronautical Science

1978-08-01

Cyg X-1 is a peculiar celestial body considered to be a close binary system of a black hole and a blue super-giant star. It is presently known that the time fluctuation of Cyg X-1 is considerably complex, ranging from seconds to days or months. Of these variation, attention has been paid to the short time variation in relation to the black hole theory. Observations of fluctuations in the order of second have been limited to soft X-ray (20 keV or more) so far, because great technical difficulties are involved due to the low intensity of hard X-ray. The present investigation is based on the fluctuations in the order of second in hard X-ray, and was conducted by employing an unprecedented large area X-ray telescope. The text describes on the brief history of the short time fluctuation, explains the experimental plan, X-ray detecting system, flight of a balloon and the analyses and discussions of fluctuation factor by variation function method, and gives the analysis data and conclusion. The observations resulted in the fact that the fluctuations in the order of second were small at 20 to 30 keV, but become large when energy is higher or lower than this value. The most natural explanation available for this result may be that it is essentially spectrum fluctuation, being inverse correlation in higher and lower energies. Physical meaning of such spectrum fluctuation is considered in connection with precipitating disk model around a black hole.

Variable magnification with Kirkpatrick-Baez optics for synchrotron x-ray microscopy

OpenAIRE

Jach, T.; Bakulin, A. S.; Durbin, S. M.; Pedulla, J.; Macrander, A.

2006-01-01

We describe the distinction between the operation of a short focal length x-ray microscope forming a real image with a laboratory source (convergent illumination) and with a highly collimated intense beam from a synchrotron light source (Kohler illumination). We demonstrate the distinction with a Kirkpatrick-Baez microscope consisting of short focal length multilayer mirrors operating at an energy of 8 keV. In add...

CAT-ACT—A new highly versatile x-ray spectroscopy beamline for catalysis and radionuclide science at the KIT synchrotron light facility ANKA

Science.gov (United States)

Zimina, A.; Dardenne, K.; Denecke, M. A.; Doronkin, D. E.; Huttel, E.; Lichtenberg, H.; Mangold, S.; Pruessmann, T.; Rothe, J.; Spangenberg, Th.; Steininger, R.; Vitova, T.; Geckeis, H.; Grunwaldt, J.-D.

2017-11-01

CAT-ACT—the hard X-ray beamline for CATalysis and ACTinide/radionuclide research at the KIT synchrotron radiation facility ANKA—is dedicated to X-ray spectroscopy, including "flux hungry" photon-in/photon-out and correlative techniques and combines state-of-the-art optics with a unique infrastructure for radionuclide and catalysis research. Measurements can be performed at photon energies varying between 3.4 keV and 55 keV, thus encompassing the actinide M- and L-edge or potassium K-edge up to the K-edges of the lanthanide series such as cerium. Well-established X-ray absorption fine structure spectroscopy in transmission and fluorescence detection modes is available in combination with high energy-resolution X-ray emission spectroscopy or X-ray diffraction techniques. The modular beamline design with two alternately operated in-line experimental stations enables sufficient flexibility to adapt sample environments and detection systems to many scientific challenges. The ACT experimental station focuses on various aspects of nuclear waste disposal within the mission of the Helmholtz association to contribute to the solution of one of the greatest scientific and social challenges of our time—the safe disposal of heat producing, highly radioactive waste forms from nuclear energy production. It augments present capabilities at the INE-Beamline by increasing the flux and extending the energy range into the hard X-ray regime. The CAT experimental station focuses on catalytic materials, e.g., for energy-related and exhaust gas catalysis. Characterization of catalytically active materials under realistic reaction conditions and the development of in situ and operando cells for sample environments close to industrial reactors are essential aspects at CAT.

Probing deformation substructure by synchrotron X-ray diffraction and dislocation dynamics modelling.

Science.gov (United States)

Korsunsky, Alexander M; Hofmann, Felix; Song, Xu; Eve, Sophie; Collins, Steve P

2010-09-01

Materials characterization at the nano-scale is motivated by the desire to resolve the structural aspects and deformation behavior at length scales relevant to those mechanisms that define the novel and unusual properties of nano-structured materials. A range of novel techniques has recently become accessible with the help of synchrotron X-ray beams that can be focused down to spot sizes of less than a few microns on the sample. The unique combination of tunability (energy selection), parallelism and brightness of synchrotron X-ray beams allows their use for high resolution diffraction (determination of crystal structure and transformations, analysis of dislocation sub-structures, orientation and texture analysis, strain mapping); small angle X-ray scattering (analysis of nano-scale voids and defects; orientation analysis) and imaging (radiography and tomography). After a brief review of the state-of-the-art capabilities for monochromatic and white beam synchrotron diffraction, we consider the usefulness of these techniques for the task of bridging the gap between experiment and modeling. Namely, we discuss how the experiments can be configured to provide information relevant to the validation and improvement of modeling approaches, and also how the results of various simulations can be post-processed to improve the possibility of (more or less) direct comparison with experiments. Using the example of some recent experiments carried out on beamline 116 at Diamond Light Source near Oxford, we discuss how such experimental results can be interpreted in view and in conjunction with numerical deformation models, particularly those incorporating dislocation effects, e.g., finite-element based pseudo-continuum strain gradient formulations, and discrete dislocation simulations. Post-processing of FE and discrete dislocation simulations is described, illustrating the kind of information that can be extracted from comparisons between modeling and experimental data.

Parabolic refractive X-ray lenses: a breakthrough in X-ray optics

CERN Document Server

Lengeler, B; Benner, B; Guenzler, T F; Kuhlmann, M; Tümmler, J; Simionovici, A S; Drakopoulos, M; Snigirev, A; Snigireva, I

2001-01-01

Refractive X-ray lenses, considered for a long time as unfeasible, have been realized with a rotational parabolic profile at our institute: The main features of the new lenses are: they focus in two directions and are free of spherical aberration. By varying the number of individual lenses in the stack the focal length can be chosen in a typical range from 0.5 to 2 m for photon energies between about 6 and 60 keV. The aperture of the lens is about 1 mm matching the angular divergence of undulator beams at 3d generation synchrotron radiation sources. They cope without problems with the heat load from the white beam of an undulator. Finally, they are easy to align and to operate. Refractive X-ray lenses can be used with hard X-rays in the same way as glass lenses can be used for visible light, if it is take into account that the numerical aperture is small (of the order 10 sup - sup 4). Being high-quality optical elements, the refractive X-ray lenses can be used for generating a focal spot in the mu m range wit...

Energy Dependence of Synchrotron X-Ray Rims in Tycho's Supernova Remnant

Science.gov (United States)

Tran, Aaron; Williams, Brian J.; Petre, Robert; Ressler, Sean M.; Reynolds, Stephen P.

2015-01-01

Several young supernova remnants exhibit thin X-ray bright rims of synchrotron radiation at their forward shocks. Thin rims require strong magnetic field amplification beyond simple shock compression if rim widths are only limited by electron energy losses. But, magnetic field damping behind the shock could produce similarly thin rims with less extreme field amplification. Variation of rim width with energy may thus discriminate between competing influences on rim widths. We measured rim widths around Tycho's supernova remnant in 5 energy bands using an archival 750 ks Chandra observation. Rims narrow with increasing energy and are well described by either loss-limited or damped scenarios, so X-ray rim width-energy dependence does not uniquely specify a model. But, radio counterparts to thin rims are not loss-limited and better reflect magnetic field structure. Joint radio and X-ray modeling favors magnetic damping in Tycho's SNR with damping lengths approximately 1-5% of remnant radius and magnetic field strengths approximately 50-400 micron G assuming Bohm diffusion. X-ray rim widths are approximately 1% of remnant radius, somewhat smaller than inferred damping lengths. Electron energy losses are important in all models of X-ray rims, suggesting that the distinction between loss-limited and damped models is blurred in soft X-rays. All loss-limited and damping models require magnetic fields approximately greater than 20 micron G, arming the necessity of magnetic field amplification beyond simple compression.

Impact of a Vertically Polarized Undulator on LCLS Hard X-ray Experiments

Energy Technology Data Exchange (ETDEWEB)

Fritz, David [SLAC National Accelerator Lab., Menlo Park, CA (United States)

2014-11-14

The LCLS-II project will install two variable gap, horizontally polarized undulators into the LCLS undulator hall. One undulator is designed to produce soft x-rays spanning an energy range of 200-1250 eV (SXU) while the other is designed for the hard spectral range of 1-25 keV (HXU). The hard x-ray LCLS instruments (X-ray Pump- Probe [XPP], X-ray correlation Spectroscopy [XCS], Coherent X-ray Imaging [CXI], Matter in Extreme Conditions [MEC]) will be repurposed to operate on the HXU line while two new soft x-ray beamlines will be created for the SXU line. An alternate HXU undulator design is being considered that could provide advantages over the present design choice. In particular, the project team is collaborating with Argonne National Laboratory to develop a vertically polarized undulator (VPU). A 1-m prototype VPU device was successfully constructed this year and a full size prototype is in process. A decision to alter the project baseline, which is the construction of a horizontally polarized device, must be made in the coming weeks to not impact the present project schedule. Please note that a change to the soft x-ray undulator is not under discussion at the moment.

Hard x-ray measurements of the hot-electron rings in EBT-S

International Nuclear Information System (INIS)

Hillis, D.L.

1982-06-01

A thorough understanding of the hot electron rings in ELMO Bumpy Torus-Scale (EBT-S) is essential to the bumpy torus concept of plasma production, since the rings provide bulk plasma stability. The hot electrons are produced via electron cyclotron resonant heating using a 28-GHz cw gyrotron, which has operated up to power levels of 200 kW. The parameters of the energetic electron rings are studied via hard x-ray measurement techniques and with diamagnetic pickup coils. The hard x-ray measurements have used collimated NaI(Tl) detectors to determine the electron temperature T/sub e/ and electron density n/sub e/ for the hot electron annulus. Typical values of T/sub e/ are 400 to 500 keV and of n/sub e/ 2 to 5 x 10 11 cm -3 . The total stored energy of a single energetic electron ring as measured by diamagnetic pickup loops approaches approx. 40 J and is in good agreement with that deduced from hard x-ray measurements. By combining the experimental measurements from hard x-rays and the diamagnetic loops, an estimate can be obtained for the volume of a single hot electron ring. The ring volume is determined to be approx. 2.2 litres, and this volume remains approximately constant over the T-mode operating regime. Finally, the power in the electrons scattered out of the ring is measured indirectly by measuring the x-ray radiation produced when those electrons strike the chamber walls. The variation of this radiation with increasing microwave power levels is found to be consistent with classical scattering estimates

Nanoscale X-Ray Microscopic Imaging of Mammalian Mineralized Tissue

OpenAIRE

Andrews, Joy C.; Almeida, Eduardo; van der Meulen, Marjolein C.H.; Alwood, Joshua S.; Lee, Chialing; Liu, Yijin; Chen, Jie; Meirer, Florian; Feser, Michael; Gelb, Jeff; Rudati, Juana; Tkachuk, Andrei; Yun, Wenbing; Pianetta, Piero

2010-01-01

A novel hard transmission X-ray microscope (TXM) at the Stanford Synchrotron Radiation Light-source operating from 5 to 15 keV X-ray energy with 14 to 30 µm2 field of view has been used for high-resolution (30–40 nm) imaging and density quantification of mineralized tissue. TXM is uniquely suited for imaging of internal cellular structures and networks in mammalian mineralized tissues using relatively thick (50 µm), untreated samples that preserve tissue micro- and nanostructure. To test this...

Extended hard-X-ray emission in the inner few parsecs of the Galaxy

DEFF Research Database (Denmark)

Perez, Kerstin; Hailey, Charles J.; Bauer, Franz E.

2015-01-01

of objects emitting soft X-rays (less than 10 kiloelectronvolts) within the surrounding hundreds of parsecs, as well as the population responsible for unresolved X-ray emission extending along the Galactic plane, is dominated by accreting white dwarf systems. Observations of diffuse hard-X-ray (more than 10...... kiloelectronvolts) emission in the inner 10 parsecs, however, have been hampered by the limited spatial resolution of previous instruments. Here we report the presence of a distinct hard-X-ray component within the central 4 × 8 parsecs, as revealed by subarcminute-resolution images in the 20-40 kiloelectronvolt...... outflows interacting with the surrounding radiation field, dense molecular material or magnetic fields. However, all these interpretations pose significant challenges to our understanding of stellar evolution, binary formation, and cosmic-ray production in the Galactic Centre....

Full Multilayer Laue Lens for Focusing Hard X-rays

International Nuclear Information System (INIS)

Liu Chian; Shi, B.; Qian, J.; Conley, R.; Yan, H.; Wieczorek, M.; Macrander, A. T.; Maser, J.; Stephenson, G. B.

2010-01-01

Multilayer Laue Lenses (MLLs) were developed by us using dynamic diffraction effects to efficiently focus hard x-rays to very small spots. Using a partial MLL we were able to focus 19.5-keV hard x-rays to a line focus of 16 nm with an efficiency of 31%. A full MLL is a complete linear MLL structure. It can be fabricated by bonding two partial MLL wafers, or by growing the full structure using magnetron sputtering without bonding. A 40-μm full MLL, with a total of 5166 layers of WSi 2 and Si, has been successfully grown by sputter deposition. The layer thicknesses gradually vary from 4 nm to ∼400 nm and then back to 4 nm. Two coating runs were used to grow the full structure, one for each half. It took over 56 h for each run. A 100-μm nearly-full MLL was constructed by bonding. Each 50-μm half-structure has 1788 WSi 2 and Si layers with 12-nm to ∼32-nm thicknesses and ∼32-μm total thickness, followed by a thick WSi 2 layer of ∼17 μm, and an AuSn layer of ∼1 μm. Both full MLL structures survived dicing and polishing. The primary results demonstrate the feasibility and potential of a full MLL with a doubled numerical aperture and large beam acceptance for hard x-rays.

X-Ray Absorption with Transmission X-Ray Microscopes

NARCIS (Netherlands)

de Groot, F.M.F.

2016-01-01

In this section we focus on the use of transmission X-ray microscopy (TXM) to measure the XAS spectra. In the last decade a range of soft X-ray and hard X-ray TXM microscopes have been developed, allowing the measurement of XAS spectra with 10–100 nm resolution. In the hard X-ray range the TXM

MODELING THE THERMAL DIFFUSE SOFT AND HARD X-RAY EMISSION IN M17

International Nuclear Information System (INIS)

Velázquez, P. F.; Rodríguez-González, A.; Esquivel, A.; Rosado, M.; Reyes-Iturbide, J.

2013-01-01

We present numerical models of very young wind driven superbubbles. The parameters chosen for the simulations correspond to the particular case of the M17 nebula, but are appropriate for any young superbubble in which the wind sources have not completely dispersed their parental cloud. From the simulations, we computed the diffuse emission in the soft ([0.5-1.5] keV) and hard ([1.5-5] keV) X-ray bands. The total luminosity in our simulations agrees with the observations of Hyodo et al., about two orders of magnitude below the prediction of the standard model of Weaver et al.. The difference with respect to the standard (adiabatic) model is the inclusion of radiative cooling, which is still important in such young bubbles. We show that for this type of object the diffuse hard X-ray luminosity is significant compared to that of soft X-rays, contributing as much as 10% of the total luminosity, in contrast with more evolved bubbles where the hard X-ray emission is indeed negligible, being at least four orders of magnitude lower than the soft X-ray emission.

Hard X-ray brightening of Ginga 1843+009 seen by INTEGRAL

DEFF Research Database (Denmark)

Leyder, J.-C.; Chenevez, Jérôme; Fiocchi, M.T.

2005-01-01

The transient X-ray pulsar, Ginga 1843+009, appears to be undergoing a hard X-ray outburst brighter than the one reported in May 2003 (ATEL #159). The source has been observed during ISWT observations of the Scutum Arm region with INTEGRAL and was first detected when the source was in the field o...

In situ synchrotron X-ray diffraction study on epitaxial-growth dynamics of III–V semiconductors

Science.gov (United States)

Takahasi, Masamitu

2018-05-01

The application of in situ synchrotron X-ray diffraction (XRD) to the molecular-beam epitaxial (MBE) growth of III–V semiconductors is overviewed along with backgrounds of the diffraction theory and instrumentation. X-rays are sensitive not only to the surface of growing films but also to buried interfacial structures because of their large penetration depth. Moreover, a spatial coherence length up to µm order makes X-rays widely applicable to the characterization of low-dimensional structures, such as quantum dots and wires. In situ XRD studies during growth were performed using an X-ray diffractometer, which was combined with an MBE chamber. X-ray reciprocal space mapping at a speed matching a typical growth rate was achieved using intense X-rays available from a synchrotron light source and an area detector. The importance of measuring the three-dimensional distribution of XRD intensity in a reciprocal space map is demonstrated for the MBE growth of two-, one-, and zero-dimensional structures. A large amount of information about the growth process of two-dimensional InGaAs/GaAs(001) epitaxial films has been provided by three-dimensional X-ray reciprocal mappings, including the anisotropic strain relaxation, the compositional inhomogeneity, and the evolution of surface and interfacial roughness. For one-dimensional GaAs nanowires grown in a Au-catalyzed vapor-liquid–solid mode, the relationship between the diameter of the nanowires and the formation of polytypes has been suggested on the basis of in situ XRD measurements. In situ three-dimensional X-ray reciprocal space mapping is also shown to be useful for determining the lateral and vertical sizes of self-assembled InAs/GaAs(001) quantum dots as well as their internal strain distributions during growth.

National Synchrotron Light Source users manual: Guide to the VUV and x-ray beam lines

International Nuclear Information System (INIS)

Gmuer, N.F.; White-DePace, S.M.

1987-08-01

The success of the National Synchrotron Light Source in the years to come will be based, in large part, on the size of the users community and the diversity of the scientific disciplines represented by these users. In order to promote this philosophy, this National Synchrotron Light Source (NSLS) Users Manual: Guide to the VUV and X-Ray Beam Lines, has been published. This manual serves a number of purposes. In an effort to attract new research, it will present to the scientific community-at-large the current and projected architecture and capabilities of the various VUV and x-ray beam lines and storage rings. We anticipate that this publication will be updated periodically in order to keep pace with the constant changes at the NSLS

High-pressure phases of uranium monophosphide studied by synchrotron x-ray diffraction

DEFF Research Database (Denmark)

Olsen, J. Staun; Gerward, Leif; Benedict, U.

1988-01-01

X-ray diffraction studies have been performed on UP powder for pressures up to 51 GPa using synchrotron radiation and a diamond-anvil cell. At ambient pressure UP has the rocksalt structure. The bulk modulus has been determined to B0=102(4) GPa and its pressure derivative to B0’=4.0(8). The cubic...

Applications of synchrotron x-ray diffraction topography to fractography

International Nuclear Information System (INIS)

Bilello, J.C.

1983-01-01

Fractographs have been taken using a variety of probes each of which produces different types of information. Methods which have been used to examine fracture surfaces include: (a) optical microscopy, particularly interference contrast methods, (b) scanning electron microscopy (SEM), (c) SEM with electron channelling, (d) SEM with selected-area electron channelling, (e) Berg-Barrett (B-B) topography, and now (f) synchrotron x-radiation fractography (SXRF). This review concentrated on the role that x-ray methods can play in such studies. In particular, the ability to nondestructively assess the subsurface microstructure associated with the fracture to depths of the order of 5 to 10 μm becomes an important attribute for observations of a large class of semi-brittle metals, semiconductors and ceramics