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Sample records for gd2wo43 matrix prepared

  1. Review on preparation techniques of particle reinforced metal matrix composites

    Directory of Open Access Journals (Sweden)

    HAO Bin

    2006-02-01

    Full Text Available This paper reviews the investigation status of the techniques for preparation of metal matrix composites and the research outcomes achieved recently. The mechanisms, characteristics, application ranges and levels of development of these preparation techniques are analyzed. The advantages and the disadvantages of each technique are synthetically evaluated. Lastly, the future directions of research and the prospects for the preparation techniques of metal matrix composites are forecasted.

  2. Preparation and Characterization of Sustained Release Matrix ...

    African Journals Online (AJOL)

    Tropical Journal of Pharmaceutical Research October 2015; 14(10): 1749-1754 ... prolonged drug release and improvement in motor activity after spinal injuries. Methods: Matrix .... The friability test was performed using a Roche friabilator ...

  3. Review on preparation techniques of particle reinforced metal matrix composites

    Institute of Scientific and Technical Information of China (English)

    2006-01-01

    This paper reviews the investigation status of the techniques for preparation of metal matrix composites and the research outcomes achieved recently. The mechanisms, characteristics, application ranges and levels of development of these preparatior techniques are analyzed. The advantages and the disadvantages of each technique are synthetically evaluated. Lastly, the future directions of research and the prospects for the preparation techniques of metal matrix composites are forecasted.

  4. Preparation technique of SiCp reinforced Al matrix composite

    Institute of Scientific and Technical Information of China (English)

    HAO Bin; CUI Hua; YU Zhi-yong; TAO Kai; YANG Bin; ZHANG Ji-shan

    2006-01-01

    A new preparation technique-"block dispersal and cast" method is introduced, and three kinds of powd.er mixing methods, vertical, horizontal and inclining styles, are compared. The results demonstrate that the inclining style is the best way to mix powders. The Al and nano SiC powders are pressed into blocks, dipped into molten Al, stirred into mold so that SiC/Al matrix composites can be obtained at last. The microstructure of SiC particle reinforced Al matrix composite prepared by "block dispersal and cast" method have been studied using scanning electron microscopy (SEM). Phase analysis has also been conducted by means of X-ray diffraction (XRD). The results show that nano SiC particles can be dispersed uniformly in Al matrix. Thus, it is feasible to prepare SiC particle reinforced Al matrix composites by this method.

  5. Preparation of biodegradable microspheres and matrix devices containing naltrexone

    OpenAIRE

    DINARVAND, RASSOUL; Moghadam, Shadi H.; Mohammadyari-Fard, Leyla; Atyabi, Fatemeh

    2003-01-01

    In this study, the use of biodegradable polymers for microencapsulation of naltrexone using solvent evaporation technique is investigated. The use of naltrexone microspheres for the preparation of matrix devices is also studied. For this purpose, poly(L-lactide) (PLA) microspheres containing naltrexone prepared by solvent evaporation technique were compressed at temperatures above the Tg of the polymer. The effect of different process parameters, such as drug/polymer ratio and stirring rate d...

  6. Automated acoustic matrix deposition for MALDI sample preparation.

    Science.gov (United States)

    Aerni, Hans-Rudolf; Cornett, Dale S; Caprioli, Richard M

    2006-02-01

    Novel high-throughput sample preparation strategies for MALDI imaging mass spectrometry (IMS) and profiling are presented. An acoustic reagent multispotter was developed to provide improved reproducibility for depositing matrix onto a sample surface, for example, such as a tissue section. The unique design of the acoustic droplet ejector and its optimization for depositing matrix solution are discussed. Since it does not contain a capillary or nozzle for fluid ejection, issues with clogging of these orifices are avoided. Automated matrix deposition provides better control of conditions affecting protein extraction and matrix crystallization with the ability to deposit matrix accurately onto small surface features. For tissue sections, matrix spots of 180-200 microm in diameter were obtained and a procedure is described for generating coordinate files readable by a mass spectrometer to permit automated profile acquisition. Mass spectral quality and reproducibility was found to be better than that obtained with manual pipet spotting. The instrument can also deposit matrix spots in a dense array pattern so that, after analysis in a mass spectrometer, two-dimensional ion images may be constructed. Example ion images from a mouse brain are presented.

  7. Preparation of SiC Fiber Reinforced Nickel Matrix Composite

    Institute of Scientific and Technical Information of China (English)

    Lu Zhang; Nanlin Shi; Jun Gong; Chao Sunt

    2012-01-01

    A method of preparing continuous(Al+Al2O3)-coated SiC fiber reinforced nickel matrix composite was presented,in which the diffusion between SiC fiber and nickel matrix could be prevented.Magnetron sputtering is used to deposit Ni coating on the surface of the(Al+Al2O3)-coated SiC fiber in preparation of the precursor wires.It is shown that the deposited Ni coating combines well with the(Al+Al2O3) coating and has little negative effect on the tensile strength of(Al+Al2O3)-coated SiC fiber.Solid-state diffusion bonding process is employed to prepare the(Al+Al2O3)-coated SiC fiber reinforced nickel matrix with 37% fibers in volume.The solid-state diffusion bonding process is optimized and the optimum parameters are temperature of 870,pressure of 50 MPa and holding time of 2 h.Under this condition,the precursor wires can diffuse well,composite of full density can be formed and the(Al+Al2O3) coating is effective to restrict the reaction between SiC fiber and nickel matrix.

  8. Preparation and characterization of nano-hydroxyapatite within chitosan matrix

    Energy Technology Data Exchange (ETDEWEB)

    Rogina, A., E-mail: arogina@fkit.hr; Ivanković, M.; Ivanković, H.

    2013-12-01

    Nano-composites that show some features of natural bone both in composition and in microstructure have been prepared by in situ precipitation method. Apatite phase has been prepared from cost-effective precursors (calcite and urea phosphate) within chitosan (CS) matrix dissolved in aqueous acetic acid solution. The compositional and morphological properties of composites were studied by means of Fourier transform infrared (FTIR) spectroscopy, X-ray diffraction (XRD) thermogravimetric analysis (TGA) and transmission electron microscopy (TEM). Depending on the reaction conditions (temperature, reaction time, glucose addition and pH control) in addition to hydroxyapatite (HA) as a major phase, octacalcium hydrogen phosphate pentahydrate (OCP) and dicalcium phosphate anhydrate (DCPD) were formed as shown by XRD and FTIR. Crystallite lengths of precipitated HA estimated by Scherrer's equation were between 20 and 30 nm. A fibrous morphology (∼ 400 nm) of HA observed by TEM indicates that HA nucleates on chitosan chains. - Highlights: • Nano-hydroxyapatite (HA) was prepared by in situ precipitation within chitosan hydrogels and colloidal chitosan solution. • pH control was regulated by ammonia and urea degradation. • In situ urea degradation provides homogenous HA formation. • TEM imaging indicates fibrous morphology of HA with crystalline size of 400 nm. • Glucose addition and temperature variation affect inorganic phase formation.

  9. Metal-Matrix Composites Prepared by Paper-Manufacturing Technology

    Science.gov (United States)

    Wenzel, Claudia; Aneziris, Christos G.; Pranke, Katja

    2016-01-01

    In this work, metal-matrix composites were prepared via paper-manufacturing technology using metastable austenitic steel powder of type 16-7-3 (Cr-Mn-Ni in wt pct) and magnesia partially stabilized zirconia reinforcing particles. The influence of the process parameters on the paper web formation and the resulting properties of the MMCs were studied and solids retention of >90 wt pct was achieved. During filtration of the aqueous fiber-filler suspension, the steel particles were incorporated in the fiber network, and steel clusters were formed. Calendering had a positive influence on the porosity, bulk density, and tensile strength of the green paper sheets. Within this contribution, the debinding process for the metal-matrix paper sheets was in focus. A debinding rate of 0.5 K/min to 733 K (460 °C) with a dwell time of 90 minutes was sufficient to completely remove cellulose fibers. The sintered composites attained a tensile strength of up to 177 N/mm2 at a total porosity of 66 pct.

  10. Preparation of Extracellular Matrix Protein Fibers for Brillouin Spectroscopy.

    Science.gov (United States)

    Edginton, Ryan S; Mattana, Sara; Caponi, Silvia; Fioretto, Daniele; Green, Ellen; Winlove, C Peter; Palombo, Francesca

    2016-09-15

    Brillouin spectroscopy is an emerging technique in the biomedical field. It probes the mechanical properties of a sample through the interaction of visible light with thermally induced acoustic waves or phonons propagating at a speed of a few km/sec. Information on the elasticity and structure of the material is obtained in a nondestructive contactless manner, hence opening the way to in vivo applications and potential diagnosis of pathology. This work describes the application of Brillouin spectroscopy to the study of biomechanics in elastin and trypsin-digested type I collagen fibers of the extracellular matrix. Fibrous proteins of the extracellular matrix are the building blocks of biological tissues and investigating their mechanical and physical behavior is key to establishing structure-function relationships in normal tissues and the changes which occur in disease. The procedures of sample preparation followed by measurement of Brillouin spectra using a reflective substrate are presented together with details of the optical system and methods of spectral data analysis.

  11. Hydrodesulfurization catalyst prepared by urea-matrix combustion method

    Institute of Scientific and Technical Information of China (English)

    Dongmei Jiao; Yeyong Ma; Fahai Cao

    2012-01-01

    Co-Mo/γ-Al2O3-TiO2 hydrodesulfurization (HDS) catalyst samples prepared by a urea matrix combustion (UMxC) method,were evaluated in a stainless tubular fixed-bed reactor,with thiophene,benzothiophene and dibenzothiophene in xylene as model feedstocks.The samples were pre-sulfurized using a cyclohexane solution of 3% CS2 and then tested for the HDS reaction.The test results were compared with catalysts prepared by conventional methods involving sequential impregnation (SI) and co-impregnation (CI).The catalysts were characterized using X-ray diffraction (XRD),laser Raman spectroscopy (LRS),high resolution transmission electron microscopy (HRTEM) and N2 physisorption,showing that the UMxC catalyst had higher pore volume and surface area than those prepared by the CI and SI methods.The UMxC method increased metal loading and avoided formation of inert phase,e.g.,β-CoMoO4,for the HDS reaction,suggesting that UMxC method is superior to the conventional impregnation techniques.TiO2 promoter made particles on the catalyst surface closer and alleviated the interaction between molybdenum oxide and the support,and facilitated the formation of well-dispersed Co- and Mo-oxo species on catalyst surface,thus resulting in higher HDS catalytic activity than pure -γ-Al2O3 support without modifiers.Consequently,the addition of TiO2 obviously improved the HDS conversion of dibenzothiophene.

  12. Glass matrix composite material prepared with waste foundry sand

    Directory of Open Access Journals (Sweden)

    ZHANG Zhao-shu

    2006-11-01

    Full Text Available The technology of glass matrix of the composite material manufactured through a sintering process and using waste foundry sand and waste glass as the main raw materials was studied. The effects of technological factors on the performance of this material were studied. The results showed that this composite material is formed with glass as matrix, core particulate as strengthening material, it has the performance of glass and ceramics, and could be used to substitute for stone.

  13. Glass matrix composite material prepared with waste foundry sand

    Institute of Scientific and Technical Information of China (English)

    ZHANG Zhao-shu; XIA Ju-pei; ZHU Xiao-qin; LIU Fan; HE Mao-yun

    2006-01-01

    The technology of glass matrix of the composite material manufactured through a sintering process and using waste foundry sand and waste glass as the main raw materials was studied. The effects of technological factors on the performance of this material were studied. The results showed that this composite material is formed with glass as matrix, core particulate as strengthening material, it has the performance of glass and ceramics, and could be used to substitute for stone.

  14. Evaluation of roll compaction as a preparation method for hydroxypropyl cellulose-based matrix tablets

    Directory of Open Access Journals (Sweden)

    Imjak Jeon

    2011-01-01

    Full Text Available Roll compaction was applied for the preparation of hydroxypropyl cellulose (HPC-based sustained-release matrix tablets. Matrix tablets made via roll compaction exhibited higher dosage uniformity and faster drug release than direct-compacted tablets. HPC viscosity grade, roll pressure, and milling speed affected tablet properties significantly. Roll compaction seems to be an adequate granulation method for the preparation of HPC-based matrix tablets due to the simplicity of the process, less handling difficulty from HPC tackiness as well as easier particle size targeting. Selecting the optimum ratio of plastic excipients and the particle size of starting materials can however be critical issues in this method.

  15. Preparation of Cu-based Bulk Metallic Glass Matrix Composites

    Institute of Scientific and Technical Information of China (English)

    Yufeng SUN; Yuren WANG; Bingchen WEI; Weihuo LI

    2006-01-01

    Cu47Ti34Zr11Ni8 bulk metallic glass (BMG) matrix composites containing in situ formed TiC particles and δ-TiCu dendrite phase were developed by copper mold cast. The thermal stability and microstructure of the composites are investigated. Room temperature compression tests reveal that the composite samples exhibit higher fracture strength and distinct plastic strain of 0.2%~0.5%, comparing with that of the corresponding Cu47Ti34Zr11 Ni8 monolithic BMG.

  16. Preparation of coated valproic acid and sodium valproate sustained-release matrix tablets

    Directory of Open Access Journals (Sweden)

    Phaechamud T

    2010-01-01

    Full Text Available The aim of this research was to investigate the technique for preparation of coated valproic acid and sodium valproate sustained-release matrix tablets. Different diluents were tested and selected as the effective absorbent for oily valproic acid. Effect of the amount of absorbent and hydroxypropylmethylcellulose on drug release from valproic acid-sodium valproate matrix tablets prepared with wet granulation technique was evaluated in pH change system. Colloidal silicon dioxide effectively adsorbed liquid valproic acid during wet granulation and granule preparation. The amounts of colloidal silicon dioxide and hydroxypropylmethylcellulose employed in tablet formulations affected drug release from the tablets. The drug release was prominently sustained for over 12 h using hydroxypropylmethylcellulose-based hydrophilic matrix system. The mechanism of drug release through the matrix polymer was a diffusion control. The drug release profile of the developed matrix tablet was similar to Depakine Chrono; , providing the values of similarity factor (f2 and difference factor (f1 of 85.56 and 2.37, respectively. Eudragit; L 30 D-55 was used as effective subcoating material for core matrix tablets before over coating with hydroxypropylmethylcellulose film with organic base solvent. Drug release profile of coated matrix tablet was almost similar to that of Depakine Chrono; .

  17. Preparation and in vitro evaluation of guar gum based triple-layer matrix tablet of diclofenac sodium

    OpenAIRE

    Chavda, H. V.; M. S. Patel; Patel, C N

    2012-01-01

    The objective of the present study was to design an oral controlled drug delivery system for sparingly soluble diclofenac sodium (DCL) using guar gum as triple-layer matrix tablets. Matrix tablet granules containing 30% (D1), 40% (D2) or 50% (D3) of guar gum were prepared by the conventional wet granulation technique. Matrix tablets of diclofenac sodium were prepared by compressing three layers one by one. Centre layer of sandwich like structure was incorporated with matrix granules containin...

  18. The Optimization of Matrix Preparation Process and Performance Testing for Molten Carbonate Fuel Cell

    Directory of Open Access Journals (Sweden)

    Jian Cheng

    2014-01-01

    Full Text Available A key component in the molten carbonate fuel cell (MCFC is electrolyte matrix, which provides both ionic conduction and gas sealing. The aim of this work is to investigate the effects of selected operating conditions on the performance of the matrix preparation. Slurries were prepared to produce matrices by the technique of tape casting. The characteristics of the slurries and matrices were examined by laser particle size analyzer, scanning electron microscopy, and BET surface area analyzer. The testing results revealed that a slurry composition with 40 wt.% lithium aluminate was the optimal formulation to produce a good matrix with a pore size distribution of 0.1–0.4 μm and porosity of 50 vol.%. Coarse and fine LiAlO2 particles were added in the matrix slurry to enhance the mechanical strength. Several green sheets were heated and pressed to enhance the bulk density to get a dense matrix of MCFC. Finally, a single MCFC was assembled and tested. The testing results showed the matrix with 40% solid loading gave the maximum discharge current of 20 A at 0.56 V.

  19. Sliding wear resistance of metal matrix composite layers prepared by high power laser

    NARCIS (Netherlands)

    Ocelik, Vaclav; Matthews, D; de Hosson, Jeff

    2005-01-01

    Two laser surface engineering techniques, Laser Cladding and Laser Melt Injection (LMI), were used to prepare three different metal matrix composite layers with a thickness of about 1 mm and approximately 25-30% volume fraction of ceramic particles. SiC/Al-8Si, WC/Ti-6Al-4V and TiB2/Ti-6Al-4V layers

  20. Preparation of bioconjugates by solid-phase conjugation to ion exchange matrix-adsorbed carrier proteins

    DEFF Research Database (Denmark)

    Houen, G.; Olsen, D.T.; Hansen, P.R.;

    2003-01-01

    A solid-phase conjugation method utilizing carrier protein bound to an ion exchange matrix was developed. Ovalbumin was adsorbed to an anion exchange matrix using a batch procedure, and the immobilized protein was then derivatized with iodoacetic acid N-hydroxysuccinimid ester. The activated......, and immunization experiments with the eluted conjugates showed that the more substituted conjugates gave rise to the highest titers of glutathione antibodies. Direct immunization with the conjugates adsorbed to the ion exchange matrix was possible and gave rise to high titers of glutathione antibodies. Conjugates...... of ovalbumin and various peptides were prepared in a similar manner and used for production of peptide antisera by direct immunization with the conjugates bound to the ion exchanger. Advantages of the method are its solid-phase nature, allowing fast and efficient reactions and intermediate washings...

  1. Mechanical Properties of TC4 Matrix Composites Prepared by Laser Cladding

    Directory of Open Access Journals (Sweden)

    WANG Lin

    2017-06-01

    Full Text Available In order to improve the penetration performance of TC4, the direct laser deposition technology was used to prepare TC4 composite material. TA15+30% TiC powder, TA15+20%Cr3C2 powder and TA15+15%B4C powder were used as deposited materials for TC4 matrix. The micromorphology, change of hardness of the deposited coating and mechanical properties of the three composites were studied. The experimental results demonstrate that the TC4 matrix with the three kinds of materials can form a complete metallurgical bonding, and the strength of TC4-(TA15+TiC, TC4-(TA15+Cr3C2 and TC4-(TA15+B4C are higher than that of TC4 matrix materials, while the plasticity is slightly worse.

  2. Research on the preparation, biocompatibility and bioactivity of magnesium matrix hydroxyapatite composite material.

    Science.gov (United States)

    Linsheng, Li; Guoxiang, Lin; Lihui, Li

    2016-08-12

    In this paper, magnesium matrix hydroxyapatite composite material was prepared by electrophoretic deposition method. The optimal process parameters of electrophoretic deposition were HA suspension concentration of 0.02 kg/L, aging time of 10 days and voltage of 60 V. Animal experiment and SBF immersion experiment were used to test the biocompatibility and bioactivity of this material respectively. The SD rats were divided into control group and implant group. The implant surrounding tissue was taken to do tissue biopsy, HE dyed and organizational analysis after a certain amount of time in the SD rat body. The biological composite material was soaked in SBF solution under homeothermic condition. After 40 days, the bioactivity of the biological composite material was evaluated by testing the growth ability of apatite on composite material. The experiment results showed that magnesium matrix hydroxyapatite biological composite material was successfully prepared by electrophoretic deposition method. Tissue hyperplasia, connective tissue and new blood vessels appeared in the implant surrounding soft tissue. No infiltration of inflammatory cells of lymphocytes and megakaryocytes around the implant was found. After soaked in SBF solution, a layer bone-like apatite was found on the surface of magnesium matrix hydroxyapatite biological composite material. The magnesium matrix hydroxyapatite biological composite material could promot calcium deposition and induce bone-like apatite formation with no cytotoxicity and good biocompatibility and bioactivity.

  3. Wear Behavior of Aluminium Metal Matrix Composite Prepared from Industrial Waste

    Directory of Open Access Journals (Sweden)

    L. Francis Xavier

    2016-01-01

    Full Text Available With an increase in the population and industrialization, a lot of valuable natural resources are depleted to prepare and manufacture products. However industrialization on the other hand has waste disposal issues, causing dust and environmental pollution. In this work, Aluminium Metal Matrix Composite is prepared by reinforcing 10 wt% and 20 wt% of wet grinder stone dust particles an industrial waste obtained during processing of quarry rocks which are available in nature. In the composite materials design wear is a very important criterion requiring consideration which ensures the materials reliability in applications where they come in contact with the environment and other surfaces. Dry sliding wear test was carried out using pin-on-disc apparatus on the prepared composites. The results reveal that increasing the reinforcement content from 10 wt% to 20 wt% increases the resistance to wear rate.

  4. Specimen Preparation for Metal Matrix Composites with a High Volume Fraction of Reinforcing Particles for EBSD Analysis

    Science.gov (United States)

    Smirnov, A. S.; Belozerov, G. A.; Smirnova, E. O.; Konovalov, A. V.; Shveikin, V. P.; Muizemnek, O. Yu.

    2016-07-01

    The paper deals with a procedure of preparing a specimen surface for the EBSD analysis of a metal matrix composite (MMC) with a high volume fraction of reinforcing particles. Unlike standard procedures of preparing a specimen surface for the EBSD analysis, the proposed procedure is iterative with consecutive application of mechanical and electrochemical polishing. This procedure significantly improves the results of an indexed MMC matrix in comparison with the standard procedure of specimen preparation. The procedure was verified on a MMC with pure aluminum (99.8% Al) as the matrix, SiC particles being used as reinforcing elements. The average size of the SiC particles is 14 μm, and their volume fraction amounts to 50% of the total volume of the composite. It has been experimentally found that, for making the EBSD analysis of a material matrix near reinforcing particles, the difference in height between the particles and the matrix should not exceed 2 µm.

  5. Control of Colloid Surface Chemistry through Matrix Confinement: Facile Preparation of Stable Antibody Functionalized Silver Nanoparticles

    Science.gov (United States)

    Skewis, Lynell R.; Reinhard, Björn M.

    2010-01-01

    Here we describe a simple yet efficient gel matrix assisted preparation method which improves synthetic control over the interface between inorganic nanomaterials and biopolymers and yields stable biofunctionalized silver nanoparticles. Covalent functionalization of the noble metal surface is aided by the confinement of polyethylene glycol acetate functionalized silver nanoparticles in thin slabs of a 1% agarose gel. The gel confined nanoparticles can be transferred between reaction and washing media simply by immersing the gel slab in the solution of interest. The agarose matrix retains nanoparticles but is swiftly penetrated by the antibodies of interest. The antibodies are covalently anchored to the nanoparticles using conventional crosslinking strategies, and the resulting antibody functionalized nanoparticles are recovered from the gel through electroelution. We demonstrate the efficacy of this nanoparticle functionalization approach by labeling specific receptors on cellular surfaces with functionalized silver nanoparticles that are stable under physiological conditions. PMID:20161660

  6. Preparation and properties of Cu matrix composite reinforced by carbon nanotubes

    Institute of Scientific and Technical Information of China (English)

    CHEN Xiao-hua; LI Wen-hua; CHEN Chuan-sheng; XU Long-shan; YANG Zhi; HU Jing

    2005-01-01

    Cu matrix composites reinforced by carbon nanotubes(CNTs) were prepared. The effect of carbon nanotubes on mechanical and tribological properties of the Cu matrix composites were investigated. The chemical method for coating CNTs was reported. The morphology of the fracture surfaces and worn surface were examined by SEM.The results show that Cu/coated-CNTs composites have higher hardness, much better wear resistance and antifriction properties than those of the reference Cu alloy (Cu-10Sn) and Cu/uncoated-CNTs composite sintered under the same conditions. The optimal mechanical properties of the composites occurred at 2. 25% (mass fraction) of CNTs. The excellent wear resistance and anti-friction properties are attributed to the fiber strengthening effect of CNTs and the effect of the spherical wear debris containing carbon nanotubes on the tribo-surface.

  7. Enhanced properties of an AA7075 based metal matrix composite prepared using mechanical alloying

    OpenAIRE

    Nazik, C.; Tarakcioglu, N.; Canakci, A.; Varol, T.; , S. Ozkaya

    2014-01-01

    In this study, firstly, AA7075 metal powder which average particle size 43.9 µm were manufactured by using gas atomization method. Thereafter with mechanical alloying method which powder metallurgy manufacturing methods, 10% B4C particle reinforcements that average particle size of 49.5 µm by participating into AA7075 metal matrix composite powder mixtures were prepared. They were milled for different durations (0-8 hrs) in a high energy planetary ball mill. From these milled powders; 550°C a...

  8. Preparation and Mechanical Properties of Al2O3/Al Laminated Ceramic Matrix Composites

    Institute of Scientific and Technical Information of China (English)

    HUANG Kangming; LI Weixin; XIE Binhuan; RAO Pinggen; PENG Cheng; CHEN Dabo; WU Jianqing

    2011-01-01

    Three series of Al2O3/Al laminated ceramic matrix composites,named SPA,SPV and HP,were fabricated by different methods.SPA and SPV were prepared using Al2O3 slices and Al slurry via screen printing and subsequent heat treatment in air or vacuum.HP samples were made by hot pressing the layered stack of Al foils and Al2O3 slices.SEM and XRD were applied to analyze the microstructure and the interlayer crystal phase.The bending strength,fracture toughness and fracture work of the samples made by the three methods were measured and compared.The results show that the composites have much better toughness and higher fracture work than the Al2O3 slice.Among the samples made by the three methods,the samples made by hot pressing have the optimum mechanical performance.The displacement-load curves and fracture mechanism were analyzed.

  9. Graphene-reinforced aluminum matrix composites prepared by spark plasma sintering

    Institute of Scientific and Technical Information of China (English)

    Wen-ming Tian; Song-mei Li; Bo Wang; Xin Chen; Jian-hua Liu; Mei Yu

    2016-01-01

    Graphene-reinforced 7055 aluminum alloy composites with different contents of graphene were prepared by spark plasma sinter-ing (SPS). The structure and mechanical properties of the composites were investigated. Testing results show that the hardness, compressive strength, and yield strength of the composites are improved with the addition of 1wt% graphene. A clean, strong interface is formed between the metal matrix and graphene via metallurgical bonding on atomic scale. Harmful aluminum carbide (Al4C3) is not formed during SPS processing. Further addition of graphene (above 1wt%) results in the deterioration in mechanical properties of the composites. The agglomeration of graphene plates is exacerbated with increasing graphene content, which is the main reason for this deterioration.

  10. Preparation of Carbon Nanotubes by the Catalysis of Polymer Metal Complex on Porous Al203 Matrix

    Institute of Scientific and Technical Information of China (English)

    SHI YanLi; ZHANG XiaoGang; LI HuLin

    2001-01-01

    @@ At present, synthesis of carbon nanotubes (CNTs) is normally conducted on a vapor-to-solid interface at ca. 500-3500℃ via various vapor phase methods, such as are discharge, laser ablation, catalytic pyrolysis and chemical vapor deposition, etc.1-2 Recently, channel materials (such as channels of alumina and of AlPO4-5 zeolite) 3 have been utilized as solid-state templates to grow CNTs inside the channel. Here we described a novel method to prepare the carbon nanotubes based on the decomposition of C2H2 gas on the Co-Ni catalyst anchored by polymer complex on the porous A12O3 matrix. The degree of graphitization of synthesized CNTs and catalysts are of great interest.

  11. Preparation of Carbon Nanotubes by the Catalysis of Polymer Metal Complex on Porous Al203 Matrix

    Institute of Scientific and Technical Information of China (English)

    SHI; YanLi

    2001-01-01

    At present, synthesis of carbon nanotubes (CNTs) is normally conducted on a vapor-to-solid interface at ca. 500-3500℃ via various vapor phase methods, such as are discharge, laser ablation, catalytic pyrolysis and chemical vapor deposition, etc.1-2 Recently, channel materials (such as channels of alumina and of AlPO4-5 zeolite) 3 have been utilized as solid-state templates to grow CNTs inside the channel. Here we described a novel method to prepare the carbon nanotubes based on the decomposition of C2H2 gas on the Co-Ni catalyst anchored by polymer complex on the porous A12O3 matrix. The degree of graphitization of synthesized CNTs and catalysts are of great interest.  ……

  12. Matrix compatible solid phase microextraction coating, a greener approach to sample preparation in vegetable matrices.

    Science.gov (United States)

    Naccarato, Attilio; Pawliszyn, Janusz

    2016-09-01

    This work proposes the novel PDMS/DVB/PDMS fiber as a greener strategy for analysis by direct immersion solid phase microextraction (SPME) in vegetables. SPME is an established sample preparation approach that has not yet been adequately explored for food analysis in direct immersion mode due to the limitations of the available commercial coatings. The robustness and endurance of this new coating were investigated by direct immersion extractions in raw blended vegetables without any further sample preparation steps. The PDMS/DVB/PDMS coating exhibited superior features related to the capability of the external PDMS layer to protect the commercial coating, and showed improvements in terms of extraction capability and in the cleanability of the coating surface. In addition to having contributed to the recognition of the superior features of this new fiber concept before commercialization, the outcomes of this work serve to confirm advancements in the matrix compatibility of the PDMS-modified fiber, and open new prospects for the development of greener high-throughput analytical methods in food analysis using solid phase microextraction in the near future.

  13. Nanoclay embedded mixed matrix PVDF nanocomposite membrane: Preparation, characterization and biofouling resistance

    Energy Technology Data Exchange (ETDEWEB)

    Rajabi, Hamid [Membrane Research Centre, Department of Chemical Engineering, Razi University, Tagh Bostan, 67149 Kermanshah (Iran, Islamic Republic of); Department of Civil Engineering, Razi University, 67149 Kermanshah (Iran, Islamic Republic of); Ghaemi, Negin, E-mail: negin_ghaemi@kut.ac.ir [Department of Chemical Engineering, Kermanshah University of Technology, 67178 Kermanshah (Iran, Islamic Republic of); Madaeni, Sayed S. [Membrane Research Centre, Department of Chemical Engineering, Razi University, Tagh Bostan, 67149 Kermanshah (Iran, Islamic Republic of); Daraei, Parisa [Department of Chemical Engineering, Kermanshah University of Technology, 67178 Kermanshah (Iran, Islamic Republic of); Khadivi, Mohammad Ali [Friedrich-Alexander University, Erlangen-Nuremberg, Egerland Strasse 3, D-91058 Erlangen (Germany); Falsafi, Monir [Department of Chemistry, Faculty of Science, Razi University, 67149 Kermanshah (Iran, Islamic Republic of)

    2014-09-15

    Highlights: • Nanocomposite membranes were prepared by addition of OMMT to PVDF membrane. • Addition of nanoclay considerably increased the hydrophilicity of PVDF membrane. • Nanocomposite membranes had higher water flux and antifouling properties. • Fouling of membranes blended with nanoclay (<4 wt.%) reduced. - Abstract: In this paper, nanocomposite PVDF/nanoclay membranes were prepared with addition of different concentrations of organically modified montmorillonite (OMMT) into the polymeric casting solution using combination of solution dispersion and phase inversion methods. Membranes were characterized by use of X-ray diffraction (XRD), water contact angle, scanning electron microscopy (SEM) and atomic force microscopy (AFM), and their performances were evaluated in terms of pure water flux and fouling parameters. The surface hydrophilicity of all nanocomposites markedly improved compared to nascent PVDF. In addition, XRD patterns revealed the formation of intercalated layers of mineral clays in PVDF matrix. SEM and AFM images showed that addition of OMMT resulted in nanocomposite membranes with thinner skin layer and higher porosity rather than PVDF membranes. Pure water flux of PVDF/OMMT membranes increased significantly (particularly for fabricated membranes by 4 and 6 wt.% OMMT) compared to that of PVDF membrane. Moreover, nanocomposite membranes showed the elevated antifouling properties, and flux recovery of nascent PVDF membranes increased from 51 to 72% with addition of 2 wt.% OMMT nanoparticles. These nanocomposite membranes also offered a remarkable reusability and durability against biofouling.

  14. One-step preparation of antimicrobial silver nanoparticles in polymer matrix

    Energy Technology Data Exchange (ETDEWEB)

    Lyutakov, O., E-mail: lyutakoo@vscht.cz; Kalachyova, Y. [Institute of Chemical Technology, Department of Solid State Engineering (Czech Republic); Solovyev, A. [Institute of Chemical Process Fundamentals of the ASCR (Czech Republic); Vytykacova, S. [Institute of Chemical Technology, Department of Glass and Ceramics (Czech Republic); Svanda, J.; Siegel, J. [Institute of Chemical Technology, Department of Solid State Engineering (Czech Republic); Ulbrich, P. [Institute of Chemical Technology, Department of Biochemistry and Microbiology (Czech Republic); Svorcik, V. [Institute of Chemical Technology, Department of Solid State Engineering (Czech Republic)

    2015-03-15

    Simple one-step procedure for in situ preparation of silver nanoparticles (AgNPs) in the polymer thin films is described. Nanoparticles (NPs) were prepared by reaction of N-methyl pyrrolidone with silver salt in semi-dry polymer film and characterized by transmission electron microscopy, XPS, and UV–Vis spectroscopy techniques. Direct synthesis of NPs in polymer has several advantages; even though it avoids time-consuming NPs mixing with polymer matrix, uniform silver distribution in polymethylmethacrylate (PMMA) films is achieved without necessity of additional stabilization. The influence of the silver concentration, reaction temperature and time on reaction conversion rate, and the size and size-distribution of the AgNPs was investigated. Polymer films doped with AgNPs were tested for their antibacterial activity on Gram-negative bacteria. Antimicrobial properties of AgNPs/PMMA films were found to be depended on NPs concentration, their size and distribution. Proposed one-step synthesis of functional polymer containing AgNPs is environmentally friendly, experimentally simple and extremely quick. It opens up new possibilities in development of antimicrobial coatings with medical and sanitation applications.

  15. Preparation and Characterization of a Collagen-Liposome-Chondroitin Sulfate Matrix with Potential Application for Inflammatory Disorders Treatment

    Directory of Open Access Journals (Sweden)

    Oana Craciunescu

    2014-01-01

    Full Text Available Smart drug delivery systems with controllable properties play an important role in targeted therapy and tissue regeneration. The aim of our study was the preparation and in vitro evaluation of a collagen (Col matrix embedding a liposomal formulation of chondroitin sulfate (L-CS for the treatment of inflammatory disorders. Structural studies using Oil Red O specific staining for lipids and scanning electron microscopy showed an alveolar network of nanosized Col fibrils decorated with deposits of L-CS at both periphery and inner of the matrix. The porosity and density of Col-L-CS matrix were similar to those of Col matrix, while its mean pore size and biodegradability had significantly higher and lower values (P<0.05, respectively. In vitro cytotoxicity assays showed that the matrix system induced high cell viability and stimulated cell metabolism in L929 fibroblast cell culture. Light and electron micrographs of the cell-matrix construct showed that cells clustered into the porous structure at 72 h of cultivation. In vitro diffusion test indicated that the quantity of released CS was significantly lower (P<0.05 after embedment of L-CS within Col matrix. All these results indicated that the biocompatible and biodegradable Col-L-CS matrix might be a promising delivery system for local treatment of inflamed site.

  16. Matrix-assisted laser desorption/ionization sample preparation optimization for structural characterization of poly(styrene-co-pentafluorostyrene) copolymers

    Energy Technology Data Exchange (ETDEWEB)

    Tisdale, Evgenia; Kennedy, Devin; Wilkins, Charles, E-mail: cwilkins@uark.edu

    2014-01-15

    Graphical abstract: -- Highlights: •We optimized sample preparation for MALDI TOF poly(styrene-copentafluorostyrene) co-polymers. •Influence of matrix choice was investigated. •Influence of matrix/analyte ratio was examined. •Influence of analyte/salt ratio (for Ag+ salt) was studied. -- Abstract: The influence of the sample preparation parameters (the choice of the matrix, matrix:analyte ratio, salt:analyte ratio) was investigated and optimal conditions were established for the MALDI time-of-flight mass spectrometry analysis of the poly(styrene-co-pentafluorostyrene) copolymers. These were synthesized by atom transfer radical polymerization. Use of 2,5-dihydroxybenzoic acid as matrix resulted in spectra with consistently high ion yields for all matrix:analyte:salt ratios tested. The optimized MALDI procedure was successfully applied to the characterization of three copolymers obtained by varying the conditions of polymerization reaction. It was possible to establish the nature of the end groups, calculate molecular weight distributions, and determine the individual length distributions for styrene and pentafluorostyrene monomers, contained in the resulting copolymers. Based on the data obtained, it was concluded that individual styrene chain length distributions are more sensitive to the change in the composition of the catalyst (the addition of small amount of CuBr{sub 2}) than is the pentafluorostyrene component distribution.

  17. A novel sample preparation method of matrix-assisted laser desorption/ionization time of flight mass spectrometry for polystyrene

    Institute of Scientific and Technical Information of China (English)

    Shu Zhang; Zhen Wen Zhao; Lei Xiong; Bin Xin; Wei Hua Hu; Shao Xiang Xiong

    2007-01-01

    A novel sample preparation method of matrix-assisted laser desorption/ionization mass spectrometry for polystyrene was reported.Compared to the conventional dried-droplet method, the efficiency of ionization and signal intensity of mass spectra were improved.The mechanism was also analyzed.

  18. Mixed matrix membranes prepared from high impact polystyrene with dispersed TiO2 nanoparticles for gas separation

    Directory of Open Access Journals (Sweden)

    P. Safaei

    2016-01-01

    Full Text Available The current study presents synthesis and characterization of high impact polystyrene - TiO2 nanoparticles mixed matrix membranes for separation of carbon dioxide from nitrogen. The solution-casting method was used for preparation of membranes. The nano mixed matrix membranes were characterized using scanning electron microscopy to ensure the suitable dispersion of nano particles in high impact polystyrene matrix. The effect of TiO2 nanoparticles loading on membrane performance was investigated. The separation performance of synthesized membranes was investigated in separation of CO2 from CO2/N2 mixture. Effect of feed pressure and TiO2 content on separation of CO2 was studied. The results revealed that increase of feed pressure decreases flux of gases through the mixed matrix membrane. The results also confirmed that the best separation performance can be obtained at TiO2 nanoparticles loading of 7 wt.%.

  19. Preparation and performance study of a novel liquid scintillator with mixed solvent as the matrix

    Science.gov (United States)

    Zheng, Zhanlong; Zhu, Jiayi; Luo, Xuan; Xu, Yewei; Zhang, Qianfeng; Zhang, Xing; Bi, Yutie; Zhang, Lin

    2017-04-01

    A novel liquid scintillator with the mixed solvent as the matrix was prepared for obtaining a good comprehensive performance. In this ternary liquid scintillator, the combination of 20% pseudocumene (PC) and 80% linear-alkyl benzene (LAB) by volume was chosen as the mixed solvent, and 2,5-diphenyloxazole (PPO) and 1,4-bis(2-Methylstyryl) benzene (bis-MSB) were as the primary fluor and wavelength shifter, respectively. The optimum prescription was obtained with regard to the light yield. Some characterizations based on the optimal formulation were conducted. The fluorescence emission spectra and wavelength-dependent optical attenuation length of the sample were measured by the fluorescence spectrophotometer and an UV-Vis spectrometer, respectively. The light yield was characterized by adopting the home-made optical platform device. The decay time was tested by adopting the time-correlated single photon counting (TCSPC) technique featured in high dynamic range of several orders of magnitude in light intensity. The experimental test results showed that the sample had a fairly good comprehensive performance.

  20. Preparation and in vitro evaluation of guar gum based triple-layer matrix tablet of diclofenac sodium.

    Science.gov (United States)

    Chavda, H V; Patel, M S; Patel, C N

    2012-01-01

    The objective of the present study was to design an oral controlled drug delivery system for sparingly soluble diclofenac sodium (DCL) using guar gum as triple-layer matrix tablets. Matrix tablet granules containing 30% (D1), 40% (D2) or 50% (D3) of guar gum were prepared by the conventional wet granulation technique. Matrix tablets of diclofenac sodium were prepared by compressing three layers one by one. Centre layer of sandwich like structure was incorporated with matrix granules containing DCL which was covered on either side by guar gum granule layers containing either 70, 80 or 87% of guar gum as release retardant layers. The tablets were evaluated for hardness, thickness, drug content, and drug release studies. To ascertain the kinetics of drug release, the dissolution profiles were fitted to various mathematical models. The in vitro drug release from proposed system was best explained by the Hopfenberg model indicating that the release of drug from tablets displayed heterogeneous erosion. D3G3, containing 87% of guar gum in guar gum layers and 50% of guar gum in DCL matrix granule layer was found to provide the release rate for prolonged period of time. The results clearly indicate that guar gum could be a potential hydrophilic carrier in the development of oral controlled drug delivery systems.

  1. Preparation and properties of polystyrene encapsulated paraffin wax as possible phase change material in a polypropylene matrix

    Energy Technology Data Exchange (ETDEWEB)

    Mochane, M.J. [Department of Chemistry, University of the Free State (Qwaqwa Campus), Phuthaditjhaba (South Africa); Luyt, A.S., E-mail: LuytAS@qwa.ufs.ac.za [Department of Chemistry, University of the Free State (Qwaqwa Campus), Phuthaditjhaba (South Africa)

    2012-09-20

    Highlights: Black-Right-Pointing-Pointer Polystyrene microcapsules containing about 30 wt% soft paraffin wax were successfully prepared. Black-Right-Pointing-Pointer The presence of microcapsules in polypropylene influenced the morphology and properties of the matrix. Black-Right-Pointing-Pointer The SEBS modifier had little influence on the interaction between polypropylene and microcapsules. - Abstract: The study deals with the preparation and characterization of polystyrene (PS) capsules containing Fischer-Tropsch paraffin wax (PS:wax) as phase change material (PCM) for thermal energy storage embedded in a polypropylene (PP) matrix. Blends of PP/PS:wax were prepared without and with polystyrene-block-poly(ethylene-ran-butylene)-block-polystyrene (SEBS) as a modifier. The influence of PS:wax microcapsules on the morphology, as well as thermal and mechanical properties of the PP was investigated. The scanning electron microscopy (SEM) images of the microencapsulated PCM show that the capsules were grouped in irregular spherical agglomerates of size 16-24 {mu}m. However, after melt-blending with PP smaller, perfectly spherical microcapsules were well dispersed in the PP matrix. There was fairly good interaction between the microcapsules and the matrix, even in the absence of SEBS modification. The FTIR spectrum of the microcapsules is almost exactly the same as that of polystyrene, which indicates that the microcapsules were mostly intact and that the FTIR only detected the polystyrene shell. The amount of wax in the PS:wax microcapsules was determined as 20-30% by weight. An increase in PS:wax content resulted in a decrease in the melting peak temperatures of PP. The thermal stability of the blends decreased with an increase in PS:wax microcapsules content as a consequence of the lower thermal stability of both the wax and PS. There was a drop in storage modulus with increasing PS:wax microcapsules content.

  2. Fabrication and densification enhancement of SiC-particulate-reinforced copper matrix composites prepared via the sinter-forging process

    Institute of Scientific and Technical Information of China (English)

    Mohammadmehdi Shabani; Mohammad Hossein Paydar; Mohammad Mohsen Moshksar

    2014-01-01

    The fabrication of copper (Cu) and copper matrix silicon carbide (Cu/SiCp) particulate composites via the sinter-forging process was investigated. Sintering and sinter-forging processes were performed under an inert Ar atmosphere. The influence of sinter-forging time, tempera-ture, and compressive stress on the relative density and hardness of the prepared samples was systematically investigated and subsequently com-pared with that of the samples prepared by the conventional sintering process. The relative density and hardness of the composites were enhanced when they were prepared by the sinter-forging process. The relative density values of all Cu/SiCp composite samples were observed to decrease with the increase in SiC content.

  3. Preparation and physicochemical characterization of matrix pellets containing APIs with different solubility via extrusion process.

    Science.gov (United States)

    Hegyesi, Diána; Thommes, Markus; Kleinebudde, Peter; Sovány, Tamás; Kása, Péter; Kelemen, András; Pintye-Hódi, Klára; Regdon, Géza

    2017-03-01

    In this study, a multiparticulate matrix system was produced, containing two different active pharmaceutical ingredients (APIs): enalapril-maleate and hydrochlorothiazide. The critical control points of the process were investigated by means of factorial design. Beside the generally used microcrystalline cellulose, ethylcellulose was used as matrix former to achieve modified drug release ensured by diffusion. The matrix pellets were made by extrusion-spheronization using a twin-screw extruder. Some pellet properties (aspect ratio, 10% interval fraction, hardness, deformation process) were determined. The aim of our study was to investigate how the two different APIs with different solubility and particle size influence the process. The amount of the granulation liquid plays a key role in the pellet shaping. A higher liquid feed rate is preferred in the pelletization process.

  4. Preparation of a three-dimensional extracellular matrix by decellularization of rabbit livers

    Directory of Open Access Journals (Sweden)

    Gustavo A. Nari

    2013-03-01

    Full Text Available Introduction: the availability of transplantable livers is not sufficient to fulfill the current demand for grafts, with the search for therapeutic alternatives having generated different lines of research, one of which is the use of decellularized three-dimensional biological matrices and subsequent cell seeding to obtain a functional organ. Objective: to produce a decellularization protocol from rabbit liver to generate a three-dimensional matrix. Methods: a combination of physical, chemical (Triton X-100 and SDS and enzymatic agents to decellularize rabbit livers was used. After 68 h of retrograde perfusion, a decellularized translucent matrix was generated. To evaluate if the decellularization protocol was successful, with the extracellular matrix being preserved, we carried out histological (light microscopy and scanning electron microscopy and biochemical (DNA quantification studies. Results: the decellularization process was verified by macroscopic observation of the organ using macroscopic staining, which revealed a correct conservation of bile and vascular trees. A microscopic observation corroborated these macroscopic results, with the hematoxylin-eosin staining showing no cells or nuclear material and the presence of a portal triad. Wilde's staining demonstrated the conservation of reticulin fibers in the decellularized matrix. In addition, scanning electron microscopy revealed a preserved Glisson's capsule and a decellularized matrix, with the DNA quantification being less than 10 % in the decellularized liver compared to control. Finally, the time taken to develop the decellularization protocol was less than 96 hours. Conclusions: the proposed decellularization protocol was correct, and was verified by an absence of cells. The hepatic matrix had preserved vascular and bile ducts with a suitable three-dimensional architecture permitting further cell seeding.

  5. Preparation of mixed matrix PES-based nanofiltration membrane filled with PANI-co-MWCNT composite nanoparticles

    Energy Technology Data Exchange (ETDEWEB)

    Bagheripour, Ehsan; Moghadassi, Abdolreza; Hosseini, Sayed Mohsen [Faculty of Engineering, Arak University, Arak (Iran, Islamic Republic of)

    2016-04-15

    Mixed matrix polyethersulfone/PANI-co-MWCNTs composite nanoparticle nanofiltration membrane was prepared by casting solution technique. Polyvinylpyrrolidone was also used as membrane pore former in membrane fabrication. The effect of polyaniline-co-multi walled carbon nanotubes composite nanoparticle concentration in the casting solution on membrane structure and performance was investigated. Scanning optical microscopy and scanning electron microscopy, FTIR analysis, porosity, mean pore size, contact angle, water content, NaCl/Na2SO4 rejection, water flux, tensile strength measurements and 3D surface image were also carried out in membrane characterization. SOM images showed nanoparticle agglomeration at high additive loading ratio. SEM images showed the membrane sub-layer porosity and thickness were changed by use of nanoparticles in membrane matrix. The membrane water content, porosity and pore size were increased by increase of nanoparticle concentration, except for 1%wt. Use of PANI-co- MWCNT nanoparticles in the membrane matrix caused a decrease of membrane contact angle from 63.43 to 46.76o. Salt rejection and water flux were improved initially by increase of nanoparticle concentration up to 0.1%wt and then decreased by more additive concentration. In addition, the membranes tensile strength was reduced by increase of PANI-co-MWCNTs composite nanoparticle concentration. 3D surface images showed a smoother surface for mixed matrix membrane filled with 0.1wt% PANI-co-MWCNTs. Modified membrane containing 0.1wt% composite nanoparticles showed better performance compared to others.

  6. Preparation and characterization of silver nanoparticles in methyl cellulose matrix and their antibacterial activity

    Science.gov (United States)

    Kolarova, Katerina; Samec, Daniel; Kvitek, Ondrej; Reznickova, Alena; Rimpelova, Silvie; Svorcik, Vaclav

    2017-06-01

    In this work we present in situ preparation of silver nanoparticles (NPs) by reduction of silver nitrate by methyl cellulose (MC). The aim of this study was to prepare a stable solution of MC-Ag, convert it to solid film, redissolve it and determine how this process influences the form and properties of the prepared NPs. MC was analysed by UV-vis spectrometry, transmission electron microscopy and X-ray photoelectron spectroscopy; it was studied in forms of a solution and as a solid film. We also evaluated the antibacterial activity and material properties of prepared films. Our results indicate that the size and distribution of particles are not negatively influenced by the conversion process. These findings can be used for preparation of antibacterial films or as a way of nanoparticle storage.

  7. Preparation and In-Vitro Evaluation of Sustained Release Matrix Diclofenac Sodium Tablets Using HPMC KM 100 and Gums

    Directory of Open Access Journals (Sweden)

    Zafar Iqbal, Raza Khan, Fazli Nasir, Jamshaid Ali Khan, Lateef Ahmad, Abad Khan, Yaser Shah

    2010-12-01

    Full Text Available Objectives: The impact of hydroxypropylmethyl cellulose(HPMC K 100M alone and in combination with the guar gum,xanthan gum and gum tragacanth on the release of the diclofenac sodium matrix tablets were evaluated.Materials and Methods: The granules were prepared using wet granulation method and compressed into tablets using different ratio of drug and gum ratio. The physical properties of the tablets were within acceptable pharmacopeial limits.The release profiles of the matrix tablets were evaluated in vitro,using USP dissolution apparatus II (paddle method.Results: The formulations containing HPMC K 100M drug ratio1:1.3 and 1:1.6 and formulations containing HPMC, gum and drug with different ratio also sustained the release of diclofenac sodium for 12 hours. The mechanism of drug release from the matrix tablets was studied using Zero order, First order, Higuchi and Korsmeyer’s models using regression coefficient method. The stability of the selected formulations was evaluated at 40˚C and 70% RH for 6 months.Conclusions: HPMC K100M alone and in combination with natural gums as the retarding material retarded the release upto 12 hours and showed little deviation from the theoretical release pattern.

  8. Cu-TiB metal matrix composites prepared by powder metallurgy route

    Directory of Open Access Journals (Sweden)

    Guo Z.

    2015-01-01

    Full Text Available Titanium boride (TiB is characterized by good conductivity, high strength and high melting point. In this work, TiB was used to make Cu-TiB metal matrix composites (MMCs. Amounts of TiB added into Cu matrix were 2wt.%, 5wt.%, 10 wt.% and 15 wt.%. The samples were pressed at pressures of 500MPa, 600MPa, 700MPa and 800MPa and sintered at 820o and 920o, respectively. The properties of the sintered composites such as hardness and impact toughness were studied. Hardness and impact toughness of samples increased with increasing pressures and decreased with increasing contents of TiB. Composite with good mechanical properties and high conductivity was obtained from the sample containing 2wt.%TiB compacted at 800MPa and sintered at 920o. It was shown that 2wt.% TiB is a suitable content to make Cu-TiB MMCs with good mechanical properties and excellent conductivity.

  9. Preparation of organic/inorganic composite membranes using two types of polymer matrix via a sol-gel process

    Energy Technology Data Exchange (ETDEWEB)

    Park, Seung-Hee [School of Chemical Engineering, Hanyang University, 17 Haengdang-dong, Seongdong-gu, Seoul 133-791 (Korea); Polymer Electrolyte Fuel Cell Research Center, Hydrogen and Fuel Cell Department, Korea Institute of Energy Research (KIER), 71-2 Jang-dong, Yuseong-gu, Daejeon 305-343 (Korea); Park, Jin-Soo; Yim, Sung-Dae; Park, Seok-Hee; Kim, Chang-Soo [Polymer Electrolyte Fuel Cell Research Center, Hydrogen and Fuel Cell Department, Korea Institute of Energy Research (KIER), 71-2 Jang-dong, Yuseong-gu, Daejeon 305-343 (Korea); Lee, Young-Moo [School of Chemical Engineering, Hanyang University, 17 Haengdang-dong, Seongdong-gu, Seoul 133-791 (Korea)

    2008-07-01

    Organic/inorganic composite membranes were prepared using two different polymers. BPO{sub 4} particles were introduced into polymers via an in situ sol-gel process. Pre-/post-sulfonated polymers were used to prepare composite membranes as matrix. Pre-sulfonated poly(aryl ether ketone) (SPAEK-6F) copolymer was synthesized via nucleophilic aromatic substitution. Degree of sulfonation was adjusted by the percentage of sulfonated monomer. Post-sulfonated poly(ether ether ketone) (SPEEK) was prepared using concentrated sulfuric acid as sulfonation agent. The membranes were characterized in terms of the ion-exchange capacity (IEC), proton conductivity, water uptake, AFM, SEM and their thermal properties. The SPAEK-6F plain membranes showed higher proton conductivity than that of the SPEEK plain membranes at similar water uptake or IEC due to their structural difference. SEM images of the composite membranes showed that the BPO{sub 4} particles were homogenously dispersed in the polymer matrices and BPO{sub 4} particle size was greatly influenced by polymer matrix. The SPAEK-6F/BPO{sub 4} composite membranes had much smaller BPO{sub 4} particle size than the SPEEK/BPO{sub 4} composite membranes due to well dispersion of BPO{sub 4} sol-like particulates in SPAEK-6F polymer solutions forming more hydrophobic/hydrophilic nanophase than SPEEK polymer solutions. The latter containing a few micrometer-scale BPO{sub 4} particles showed higher proton conductivity than the former containing hundreds nanometer-scale BPO{sub 4} particles at similar water uptake due to the increase in freezable water and effect of particle size. (author)

  10. Preparation of organic/inorganic composite membranes using two types of polymer matrix via a sol-gel process

    Science.gov (United States)

    Park, Seung-Hee; Park, Jin-Soo; Yim, Sung-Dae; Park, Seok-Hee; Lee, Young-Moo; Kim, Chang-Soo

    Organic/inorganic composite membranes were prepared using two different polymers. BPO 4 particles were introduced into polymers via an in situ sol-gel process. Pre-/post-sulfonated polymers were used to prepare composite membranes as matrix. Pre-sulfonated poly(aryl ether ketone) (SPAEK-6F) copolymer was synthesized via nucleophilic aromatic substitution. Degree of sulfonation was adjusted by the percentage of sulfonated monomer. Post-sulfonated poly(ether ether ketone) (SPEEK) was prepared using concentrated sulfuric acid as sulfonation agent. The membranes were characterized in terms of the ion-exchange capacity (IEC), proton conductivity, water uptake, AFM, SEM and their thermal properties. The SPAEK-6F plain membranes showed higher proton conductivity than that of the SPEEK plain membranes at similar water uptake or IEC due to their structural difference. SEM images of the composite membranes showed that the BPO 4 particles were homogenously dispersed in the polymer matrices and BPO 4 particle size was greatly influenced by polymer matrix. The SPAEK-6F/BPO 4 composite membranes had much smaller BPO 4 particle size than the SPEEK/BPO 4 composite membranes due to well dispersion of BPO 4 sol-like particulates in SPAEK-6F polymer solutions forming more hydrophobic/hydrophilic nanophase than SPEEK polymer solutions. The latter containing a few micrometer-scale BPO 4 particles showed higher proton conductivity than the former containing hundreds nanometer-scale BPO 4 particles at similar water uptake due to the increase in freezable water and effect of particle size.

  11. Preparation and properties of unidirectional boron nitride fibre reinforced boron nitride matrix composites via precursor infiltration and pyrolysis route

    Energy Technology Data Exchange (ETDEWEB)

    Li Duan, E-mail: whataboutduan@gmail.com [State Key Laboratory of Advanced Ceramic Fibres and Composites, College of Aerospace and Materials Engineering, National University of Defense Technology, Changsha 410073 (China); Zhang Changrui; Li Bin; Cao Feng; Wang Siqing; Li Junsheng [State Key Laboratory of Advanced Ceramic Fibres and Composites, College of Aerospace and Materials Engineering, National University of Defense Technology, Changsha 410073 (China)

    2011-10-25

    Highlights: {yields} BN fibres degrade little when exposed at elevated temperatures. {yields} Precursor infiltration and pyrolysis route is useful to prepare BNf/BN composites. {yields} Few reports have related to the preparation and properties of BNf/BN composites. {yields} BNf/BN composites have desirable high-temperature mechanical properties. {yields} BNf/BN composites have excellent dielectric properties at 2-18 GHz. - Abstract: The unidirectional boron nitride fibre reinforced boron nitride matrix (BN{sub f}/BN) composites were prepared via the precursor infiltration and pyrolysis (PIP) route, and the structure, composition, mechanical and dielectric properties were studied. The composites have a high content and fine crystallinity of BN. The density is 1.60 g cm{sup -3} with a low open porosity of 4.66%. The composites display good mechanical properties with the average flexural strength, elastic modulus and fracture toughness being 53.8 MPa, 20.8 GPa and 6.88 MPa m{sup 1/2}, respectively. Lots of long fibres pull-out from the fracture surface, suggesting a good fibre/matrix interface. As temperature increases, both of the flexural strength and elastic modulus exhibit a decreasing trend, with the lowest values being 36.2 MPa and 8.6 GPa at 1000 deg. C, respectively. The desirable residual ratios of the flexural strength and elastic modulus at 1000 deg. C are 67.3% and 41.3%, respectively. The composites have excellent dielectric properties, with the average dielectric constant and loss tangent being 3.07 and 0.0044 at 2-18 GHz, respectively.

  12. Preparation of organoclays in matrix elastomer; Preparacao de argilas organofilicas em matriz de elastomero

    Energy Technology Data Exchange (ETDEWEB)

    Gonzales-Fernandes, M.; Valenzuela-Diaz, F.R.; Wiebeck, H., E-mail: mgf@usp.br [Universidade de Sao Paulo (PMT/USP), Sao Paulo, SP (Brazil). Escola Politecnica; Esper, F.J. [Faculdades Metropolitanas Unidas (FISP/FMU), Itapevi, SP (Brazil); Martin-Cortes, G.R. [Centro Universitario Estacio Radial de Sao Paulo (UniRadial), SP (Brazil)

    2014-07-01

    Natural rubber nanocomposite / bentonite modified by sodification chocolate B and treated with quaternary ammonium salt was prepared. The clay in its natural state after sodification and after quaternization was characterized by XRD, IR, and stereoscopic microscope and SEM was measured its ability to swell in many organic solvents. The plates obtained after curing, measures have had their mechanical properties and analyzed by XRD. The nanocomposites showed improvement in their mechanical properties compared to boards without the addition of clay. (author)

  13. A fibrous hypercrosslinked sorbent prepared on PP-ST-DVB matrix via post-crosslinking reaction

    Institute of Scientific and Technical Information of China (English)

    Feng Liu; Si Guo Yuan; Xiao Li Wang; A.P. Polikarpov; A.A. Shunkevich

    2007-01-01

    A fibrous sorbent possessing abundant micropore structure was firstly prepared via post-crosslinking reaction on the PP-ST-DVB original fiber. Its micromorphology and sorptive properties were investigated, and the results. Demonstrated that the novel fibrous hypercrosslinked sorbent has narrow pore-size distribution, small average porous radius (1.90 nm), high specific surface area (362.31 m2/g), and fine sorptive properties for small organic molecules.

  14. Microparticles prepared from biodegradable polyhydroxyalkanoates as matrix for encapsulation of cytostatic drug.

    Science.gov (United States)

    Murueva, A V; Shishatskaya, E I; Kuzmina, A M; Volova, T G; Sinskey, A J

    2013-08-01

    Microparticles made from degradable polyhydroxyalkanoates of different chemical compositions a homopolymer of 3-hydroxybutyric acid, copolymers of 3-hydroxybutyric and 4-hydroxybutyric acids (P3HB/4HB), 3-hydroxybutyric and 3-hydroxyvaleric acids (P3HB/3HV), 3-hydroxybutyric and 3-hydroxyhexanoic acids (P3HB/3HHx) were prepared using the solvent evaporation technique, from double emulsions. The study addresses the influence of the chemical compositions on the size and ξ-potential of microparticles. P3HB microparticles loaded with doxorubicin have been prepared and investigated. Their average diameter and ξ-potential have been found to be dependent upon the level of loading (1, 5, and 10 % of the polymer mass). Investigation of the in vitro drug release behavior showed that the total drug released from the microparticle into the medium increased with mass concentration of the drug. In this study mouse fibroblast NIH 3T3 cells were cultivated on PHA microparticles, and results of using fluorescent DAPI DNA stain, and MTT assay showed that microparticles prepared from PHAs of different chemical compositions did not exhibit cytotoxicity to cells cultured on them and proved to be highly biocompatible. Cell attachment and proliferation on PHA microparticles were similar to those on polystyrene. The cytostatic drug encapsulated in P3HB/3HV microparticles has been proven to be effective against HeLa tumor cells.

  15. Processing and mechanical properties of 2024 aluminum matrix composites containing Tungsten and Tantalum prepared by PM

    Institute of Scientific and Technical Information of China (English)

    LIAN Youyun; YANG Zhimin; YANG Jian; MAO Changhui

    2006-01-01

    The 2024 Al composites containing W, Ta were fabricated by powder metallurgy for their potential use as shielding material.W, Ta powders and gas-atomized 2024 Al aluminum powders were mixed by a ball mixer.The mixtures were consolidated by cold isostatic pressing (CIP) and then hot-extruded into full-density bars.The extruded bars were heat treated in T6 conditions.The microstructure and its relationship with the mechanical properties were investigated by means of scanning electron microscopy (SEM) and X-ray diffraction (XRD).The results show that the particles of nonuniform size and irregular shape randomly disperse in the 2024 aluminum alloy matrix.The tensile tests show that an increase of tensile strength and decrease of elongation to failure of the heat treated composites compared with the extruded composites.

  16. Preparation and characterization of monodisperse large-porous silica microspheres as the matrix for protein separation.

    Science.gov (United States)

    Xia, Hongjun; Wan, Guangping; Zhao, Junlong; Liu, Jiawei; Bai, Quan

    2016-11-04

    High performance liquid chromatography (HPLC) is a kind of efficient separation technology and has been used widely in many fields. Micro-sized porous silica microspheres as the most popular matrix have been used for fast separation and analysis in HPLC. In this paper, the monodisperse large-porous silica microspheres with controllable size and structure were successfully synthesized with polymer microspheres as the templates and characterized. First, the poly(glycidyl methacrylate-co-ethyleneglycol dimethacrylate) microspheres (PGMA-EDMA) were functionalized with tetraethylenepentamine (TEPA) to generate amino groups which act as a catalyst in hydrolysis of tetraethyl orthosilicate (TEOS) to form Si-containing low molecular weight species. Then the low molecular weight species diffused into the functionalized PGMA-EDMA microspheres by induction force of the amino groups to form polymer/silica hybrid microspheres. Finally, the organic polymer templates were removed by calcination, and the large-porous silica microspheres were obtained. The compositions, morphology, size distribution, specific surface area and pore size distribution of the porous silica microspheres were characterized by infrared analyzer, scanning-electron microscopy, dynamic laser scattering, the mercury intrusion method and thermal gravimetric analysis, respectively. The results show that the agglomeration of the hybrid microspheres can be overcome when the templates were functionalized with TEPA as amination reagent, and the yield of 95.7% of the monodisperse large-porous silica microspheres can be achieved with high concentration of polymer templates. The resulting large-porous silica microspheres were modified with octadecyltrichlorosilane (ODS) and the chromatographic evaluation was performed by separating the proteins and the digest of BSA. The baseline separation of seven kinds of protein standards was achieved, and the column delivered a better performance when separating BSA digests

  17. Preparation of carbon nanotube composite material with metal matrix by electroplating

    Institute of Scientific and Technical Information of China (English)

    AN Bai-gang; LI Li-xiang; Li Hong-xi

    2005-01-01

    It is demonstrated that the nickel can be deposited directly on the surface of carbon nanotubes without pre-sensitization by Sn2+ and Pd2+ in a watt bath containing suspended nanotubes by electroplating. The nickel is deposited as spherical nanoparticle on the nanotubes. By increasing reaction time, the carbon nanotube is fully coated with nickel. A probable model, which represents the formation process of carbon nanotube-nickel composites by electroplating, is presented. The results show that this method is efficient and simple for preparing carbon nanotube-metal composite.

  18. Contributions in the Preparation and Processing of Composite Material Type Silumin 3 - Reinforced Matrix with S235JR Steel Mesh

    Directory of Open Access Journals (Sweden)

    Remus Belu-Nica

    2015-07-01

    Full Text Available In the paper are presented concrete data on developing technological batches of metal composite material (MCM type Silumin 3-reinforced matrix with steel mesh S235JR, with the indicating of the parameter and of the distinct stages of work. The samples from prepared batches were cut along and across by water jet abrasive process and were subjected to a destructive testing program and microstructural examination, obtaining results in concordance with the desired quality. The abrasive material used for cut was GMA granite with the average mesh of 80, the particle size ranging between 150-300 µm, density 2300 kg/m3 and melting point 1240°C.

  19. Preparation and Electromechanical Properties of PVDF Matrix Piezoelectric Composites Containing Highly Oriented BaTiO3 Whiskers

    Institute of Scientific and Technical Information of China (English)

    Xuetao LUO; Lifu CHEN; Xiaojun CHEN; Qianjun HUANG

    2004-01-01

    The piezoelectric composites containing highly oriented BaTiO3 whiskers as active phase and PVDF as matrix have been prepared by micro-hole extrusion and orientation in carried fibers. The morphology of oriented BaTiO3 whiskers and microstructure of the composites were observed by SEM. As for its electromechanical properties, it is found that the dielectric constant, piezoelectric constant and remnant of polarization in the BaTiO3 whisker-PVDF composite are considerably higher than that in the BaTiO3 powders-PVDF composite, while the loss factors follow the opposite trend. For the BaTiO3 whisker-PVDF composite, the values of ε, d33 and Pr parallel to the whisker orientation (normal specimen) are much higher than that perpendicular to the whisker orientation (parallel specimen). The significant effects of the connective passages of active phase on electromechanical properties of the piezoelectric composites has also been investigated.

  20. Nanoparticle Thin Films for Gas Sensors Prepared by Matrix Assisted Pulsed Laser Evaporation

    Directory of Open Access Journals (Sweden)

    Roberto Rella

    2009-04-01

    Full Text Available The matrix assisted pulsed laser evaporation (MAPLE technique has been used for the deposition of metal dioxide (TiO2, SnO2 nanoparticle thin films for gas sensor applications. For this purpose, colloidal metal dioxide nanoparticles were diluted in volatile solvents, the solution was frozen at the liquid nitrogen temperature and irradiated with a pulsed excimer laser. The dioxide nanoparticles were deposited on Si and Al2O3 substrates. A rather uniform distribution of TiO2 nanoparticles with an average size of about 10 nm and of SnO2 nanoparticles with an average size of about 3 nm was obtained, as demonstrated by high resolution scanning electron microscopy (SEM-FEG inspections. Gas-sensing devices based on the resistive transduction mechanism were fabricated by depositing the nanoparticle thin films onto suitable rough alumina substrates equipped with interdigitated electrical contacts and heating elements. Electrical characterization measurements were carried out in controlled environment. The results of the gas-sensing tests towards low concentrations of ethanol and acetone vapors are reported. Typical gas sensor parameters (gas responses, response/recovery time, sensitivity, and low detection limit towards ethanol and acetone are presented.

  1. Preparation and characterization of magnetic levan particles as matrix for trypsin immobilization

    Energy Technology Data Exchange (ETDEWEB)

    Maciel, J.C. [Programa de Pos-Graduacao em Ciencias Biologicas, Universidade Federal de Pernambuco, Cidade Universitaria, 50670-901 Recife, PE (Brazil); Andrad, P.L. [Programa de Pos-Graduacao em Ciencia de Materiais, Universidade Federal de Pernambuco, Cidade Universitaria, 50679-901 Recife, PE (Brazil); Neri, D.F.M., E-mail: davidfmneri@yahoo.com.br [Universidade Federal do Vale do Sao Francisco, 56304-205 Petrolina, PE (Brazil); Carvalho, L.B. [Departamento de Bioquimica, Universidade Federal de Pernambuco, Cidade Universitaria, 50679-901 Recife, PE (Brazil); Cardoso, C.A. [Departamento de Fisica, Universidade Federal de Sao Carlos, 13565-905 Sao Carlos, PE (Brazil); Calazans, G.M.T. [Departamento de Antibioticos, Universidade Federal de Pernambuco, Cidade Universitaria, 50670-901 Recife, PE (Brazil); Albino Aguiar, J. [Departamento de Fisica, Universidade Federal de Pernambuco, Cidade Universitaria, 50679-901 Recife, PE (Brazil); Silva, M.P.C. [Departamento de Bioquimica, Universidade Federal de Pernambuco, Cidade Universitaria, 50679-901 Recife, PE (Brazil)

    2012-04-15

    Magnetic levan was synthesized by co-precipitating D-fructofuranosyl homopolysaccharide with a solution containing Fe{sup 2+} and Fe{sup 3+} in alkaline conditions at 100 Degree-Sign C. The magnetic levan particles were characterized by scanning electron microscopy (SEM), magnetization measurements, X-ray diffractometry (XRD) and infrared spectroscopy (IR). Afterwards, magnetic levan particles were functionalized by NaIO{sub 4} oxidation and used as matrices for trypsin covalent immobilization. Magnetite and magnetic levan particles were both heterogeneous in shape and levan-magnetite presented bigger sizes compared to magnetite according to SEM images. Magnetic levan particles exhibited a magnetization 10 times lower as compared to magnetite ones, probably, due to the coating layer. XRD diffractogram showed that magnetite is the dominant phase in the magnetic levan. Infrared spectroscopy showed characteristics absorption bands of levan and magnetite (O-H, C-O-C and Fe-O bonds). The immobilized trypsin derivative was reused 10 times and lost 16% of its initial specific activity only. Therefore, these magnetic levan particles can be proposed as an alternative matrices for enzyme immobilization. - Highlights: Black-Right-Pointing-Pointer The magnetic levan particles presented larger size variation than magnetite particles due to the changes produced by coating. Black-Right-Pointing-Pointer The utilization of magnetic levan particles showed to be efficacious for immobilization of enzymes as trypsin. Black-Right-Pointing-Pointer Magnetic particles can be planned as other matrix for immobilization of biomolecule in various division processes in biotechnology.

  2. Cultivation of corneal endothelial cells on a pericellular matrix prepared from human decidua-derived mesenchymal cells.

    Directory of Open Access Journals (Sweden)

    Ryohei Numata

    Full Text Available The barrier and pump functions of the corneal endothelium are essential for the maintenance of corneal transparency. Although corneal transplantation is the only current therapy for treating corneal endothelial dysfunction, the potential of tissue-engineering techniques to provide highly efficient and less invasive therapy in comparison to corneal transplantation has been highly anticipated. However, culturing human corneal endothelial cells (HCECs is technically difficult, and there is no established culture protocol. The aim of this study was to investigate the feasibility of using a pericellular matrix prepared from human decidua-derived mesenchymal cells (PCM-DM as an animal-free substrate for HCEC culture for future clinical applications. PCM-DM enhanced the adhesion of monkey CECs (MCECs via integrin, promoted cell proliferation, and suppressed apoptosis. The HCECs cultured on the PCM-DM showed a hexagonal morphology and a staining profile characteristic of Na⁺/K⁺-ATPase and ZO-1 at the plasma membrane in vivo, whereas the control HCECs showed a fibroblastic phenotype. The cell density of the cultured HCECs on the PCM-DM was significantly higher than that of the control cells. These results indicate that PCM-DM provides a feasible xeno-free matrix substrate and that it offers a viable in vitro expansion protocol for HCECs while maintaining cellular functions for use as a subsequent clinical intervention for tissue-engineered based therapy of corneal endothelial dysfunction.

  3. Preparation and optimization of sustained release matrix tablets of metoprolol succinate and taro gum using response surface methodology

    Directory of Open Access Journals (Sweden)

    M. Soumya

    2014-01-01

    Full Text Available In the present study, an effort was made to formulate and evaluate matrix tablets of tarogum utilizing metaprolol succinate as the model drug. 3 2 full optimization procedure was adopted where two factors are studied at three levels. The amount of taro gum (X1 and polyvinylpyrrolidone (PVP K30 (X2 were selected as independent variables. The time required for 90% of drug release was selected as the dependent variable. Tablets were prepared by direct compression and were evaluated for various post compression parameters such as tablet hardness, friability, weight variation, drug content and in vitro dissolution. The results were found to be within the acceptable limits. The release exponent (n lies between 0.416 and 0.584 indicating drug release from the matrix tablets may be fickian or non-fickian (anomalous depending upon the concentration of natural polymer. T90 was 10.70, 11.20, 12.05, 12.66 h for B6, B7, B8 and B9 batches respectively showing overriding potential of taro gum, but still the effect of PVP K 30 is noteworthy. PVP K 30 has an indirect effect on all the factors by increasing tensile strength and making the tablet firm and intact.

  4. Cultivation of corneal endothelial cells on a pericellular matrix prepared from human decidua-derived mesenchymal cells.

    Science.gov (United States)

    Numata, Ryohei; Okumura, Naoki; Nakahara, Makiko; Ueno, Morio; Kinoshita, Shigeru; Kanematsu, Daisuke; Kanemura, Yonehiro; Sasai, Yoshiki; Koizumi, Noriko

    2014-01-01

    The barrier and pump functions of the corneal endothelium are essential for the maintenance of corneal transparency. Although corneal transplantation is the only current therapy for treating corneal endothelial dysfunction, the potential of tissue-engineering techniques to provide highly efficient and less invasive therapy in comparison to corneal transplantation has been highly anticipated. However, culturing human corneal endothelial cells (HCECs) is technically difficult, and there is no established culture protocol. The aim of this study was to investigate the feasibility of using a pericellular matrix prepared from human decidua-derived mesenchymal cells (PCM-DM) as an animal-free substrate for HCEC culture for future clinical applications. PCM-DM enhanced the adhesion of monkey CECs (MCECs) via integrin, promoted cell proliferation, and suppressed apoptosis. The HCECs cultured on the PCM-DM showed a hexagonal morphology and a staining profile characteristic of Na⁺/K⁺-ATPase and ZO-1 at the plasma membrane in vivo, whereas the control HCECs showed a fibroblastic phenotype. The cell density of the cultured HCECs on the PCM-DM was significantly higher than that of the control cells. These results indicate that PCM-DM provides a feasible xeno-free matrix substrate and that it offers a viable in vitro expansion protocol for HCECs while maintaining cellular functions for use as a subsequent clinical intervention for tissue-engineered based therapy of corneal endothelial dysfunction.

  5. ELECTRICALLY CONDUCTIVE COMPOSITE PREPARED BY ELECTROCHEMICAL POLYMERIZATION OF PYRROLE IN POLY- (p- PHENYLENE TEREPHTHALAMIDE ) MATRIX

    Institute of Scientific and Technical Information of China (English)

    BI Xiantong; PEI Qibing; HAN Baozhen; BAO Jingshen

    1991-01-01

    The preparation of PPy/PPTA conductive composite films by electrochemical method is presented.The first step is to cast a thin layer of poly (p-phenylene-terephthalamide)(PPTA)on a slice of Pt working electrode. The second step is to electrochemically polymerize pyrrole on the PPTA/Pt working electrode. Both of the electrical conductivity and the mechanical properties of the PPy/PPTA composite film are better than those of the pure PPy film, and the film has excellent flexibility at low temperature, even in liquid nitrogen.The SEM picture of the cross-section of PPy/PPTA composite film showed that the two components were well mixed.Cyclic voltammograms of PPy/PPTA film in aqueous solution showed that the conductive films could be reduced and reoxidized.

  6. Properties of lipophilic matrix tablets containing phenylpropanolamine hydrochloride prepared by hot-melt extrusion.

    Science.gov (United States)

    Liu, J; Zhang, F; McGinity, J W

    2001-09-01

    The objective of the present study was to investigate the influence of formulation factors on the physical properties of hot-melt extruded granules and compressed tablets containing wax as a thermal binder/retarding agent, and to compare the properties of granules and tablets with those prepared by a high-shear melt granulation (MG) method. Powder blends containing phenylpropanolamine hydrochloride, Precirol and various excipients were extruded in a single-screw extruder at open-end discharge conditions. The extrudates were then passed through a 14-mesh screen to form granules. The extrusion conditions and the optimum amount of wax to function as the thermal binder were dependent on the properties of the filler excipients. At the same wax level, drug release from tablets decreased in the order of using microcrystalline cellulose (MCC), lactose and Emcompress as the filler excipient. The observed differences in the dissolution properties of the tablets were due to the differences in the solubility, swellability and density of the filler excipients. Replacing Precirol with Sterotex K, a higher melting point wax, resulted in slightly increased dissolution rates, when the extrusion was performed at the same temperature conditions. Hot-melt extruded granules were observed to be less spherical than high-shear melt granules and showed lower values of bulk/tap densities. However, tablets containing MCC or lactose granules prepared by hot-melt extrusion (HME) exhibited higher hardness values. Slower drug release rates were found for tablets containing MCC by HME compared with MG. Analysis of the hot-melt extruded granules showed better drug content uniformity among granules of different size ranges compared with high-shear melt granules, resulting in a more reproducible drug release from the corresponding tablets.

  7. Influence of double promotion on HDS catalysts prepared by urea-matrix combustion synthesis

    Energy Technology Data Exchange (ETDEWEB)

    Gonzalez-Cortes, Sergio L. [Laboratorio de Cinetica y Catalisis, Departamento de Quimica, Facultad de Ciencias, Universidad de Los Andes, Merida 5101 (Venezuela); Xiao, Tian-Cun; Lin, Tsung-Wu; Green, Malcolm L.H. [Wolfson Catalysis Centre, Inorganic Chemistry Laboratory, University of Oxford, South Parks Road, Oxford OX1 3QR (United Kingdom)

    2006-04-11

    The stringent environmental regulations in the US, Japan and Europe are requiring significant improvement in the quality of transportation fuels. A new strategy based on urea-matrix combustion method for the synthesis of alumina-supported molybdate-based mixed oxides (i.e., bimetallic and trimetallic oxides) has been applied. This permits to control the alumina-mixed oxide interaction and therefore the HDS catalytic behaviour. The oxidic and sulfurized states of the HDS catalysts were characterized by X-ray diffraction (XRD), laser Raman spectroscopy (LRS), temperature-programmed reduction (TPR) and high resolution transmission electron microscopy (HRTEM). Catalyst performance was evaluated using a tubular fixed-bed reactor and the hydrodesulfurization of thiophene under normal pressure as model reaction. It has been found that Ni-promoted alumina-supported MoO{sub 3} catalyst precursor presented a non well-ordered structure of Ni-Mo phase supported on alumina surface. However, when cobalt was added to Ni-Mo precursor the {beta}-isomorph stability was significantly improved and the formation of alumina-supported {beta}-Co{sub 0.5}Ni{sub 0.5}MoO{sub 4} was observed. The activation treatments markedly affect the catalyst structure and hence the HDS catalytic performance. The catalyst series pretreated in H{sub 2}S-H{sub 2} was 2-3 times more active than those C{sub 4}H{sub 4}S-H{sub 2}-pretreated catalysts and ca. 2-10 times more active than the pre-reduced samples. A significantly greater HDS activity of H{sub 2}S-H{sub 2}-pretreated Co{sub 0.5}Mg{sub 0.5}MoS{sub x}/{gamma}-Al{sub 2}O{sub 3} catalyst was observed, which is attributed to the fact that both promoters are into the same network interacting directly with the molybdenum. This feature hinders not only the segregation of cobalt sulfide, but also the formation of long MoS{sub 2} slabs. (author)

  8. Hydroxypropylcellulose controlled release tablet matrix prepared by wet granulation: effect of powder properties and polymer composition

    Directory of Open Access Journals (Sweden)

    Antonio Zenon Antunes Teixeira

    2009-02-01

    Full Text Available The aim of this study was to attain 100% drug release of caffeine after 24 h from hydroxypropylcellulose (HPC tablet matrices and to investigate the effect of co-excipient. Physical properties of the powders were evaluated and suggested for a wet granulation process. The tablet containing caffeine was formulated by different weight ratios of hydrophilic polymers. The results of polymer evaluation confirmed that the increase of HPC level with the same drug content significantly decreased the rate of drug release. The presence of co-polymer excipients carboxymethylcellulose (CMC and polyvinylpyrrolidone (PVP in the tablet matrix was also investigated. The release rate was also controlled by low levels of CMC (O objetivo deste estudo é desenvolver a liberação 100% da droga cafeína em 24 horas em comprimidos matrizes e investigar o uso de hidroxipropilcelulose (HPC mais os efeitos de co-excipiente. As propriedades físicas dos pós foram avaliadas assim como seu uso no processo de granulação úmida. O comprimido contendo a cafeína foi formulado por diferentes relações de peso dos polímeros hidrofílicos. Os resultados da avaliação do polímero confirmaram que o aumento do nível de HPC com o mesmo índice da droga diminuiu significativamente a taxa de liberação da droga. A presença do co-polímero excipiente carboximetilcelulose (CMC e do polivinilpirrolidona (PVP na matriz do comprimido foi também investigado. A taxa de liberação foi controlada principalmente por baixos níveis de CMC (< 10% enquanto PVP não mostrou efeito diferente considerável. A melhor taxa de liberação de cafeína 100% em 24 horas foi obtida quando 10% da lactose monoidrato foi adicionado na formulação.

  9. Preparation and structural stability of ordered nanocomposites: opal matrix - lead titanates

    Science.gov (United States)

    Samoylovich, M. I.; Mkrtchyan, A. R.; Belyanin, A. F.; Bagdasaryan, S. A.; Kiziridi, A. A.

    2016-06-01

    The conditions for the formation of nanocomposites based on the basis of lattice packings of SiO2 nanospheres (opal matrices) with included crystallites of lead titanates (PbTiO3 and PbTi3O7) in interspherical nanospacing are considered. For the formation of nanocomposites are used sample opal matrices with dimensions of single-domain regions ≥0,1 mm.3 The diameter of SiO2 nanospheres was ∼260 nm. Obtained nanocomposites volume >2 cm3 in filling >20% of interspherical nanospacing PbTiO3, PbTi3O7 crystallites were size of 16-36 nm. Using X-ray diffraction and Raman spectroscopy are studied composition and structural stability when heated nanocomposites to 550°C, which allowed the identification of a local phase transition with change of the space group. The dependence of the composition of synthesized materials on the conditions of their preparation is submitted.

  10. Preparation and evaluation of novel metronidazole sustained release and floating matrix tablets.

    Science.gov (United States)

    Asnaashari, Solmaz; Khoei, Nazaninossadat Seyed; Zarrintan, Mohammad Hosein; Adibkia, Khosro; Javadzadeh, Yousef

    2011-08-01

    In the present study, metronidazole was used for preparing floating dosage forms that are designed to retain in the stomach for a long time and have developed as a drug delivery system for better eradication of Helicobacter Pylori in peptic ulcer diseases. For this means, various formulations were designed using multi-factorial design. HPMC, psyllium and carbopol in different concentrations were used as floating agents, and sodium bicarbonate was added as a gas-forming agent. Hardness, friability, drug loading, floating ability and release profiles as well as kinetics of release were assessed. Formulations containing HPMC as filler showed prolonged lag times for buoyancy. Adding psyllium to these formulations had reduced relative lag times. Overall, selected formulations were able to float immediately and showed buoyancy for at least 8?h. Meanwhile, sustained profiles of drug release were also obtained. Kinetically, among the 10 assessed models, the release pattern of metronidazole from the tablets fitted best to Power law, Weibull and Higuchi models in respect overall to mean percentage error values of 3.8, 4.73 and 5.77, respectively, for calcium carbonate-based tablets and, 2.95, 6.39 and 3.9, respectively, for calcium silicate-based tablets. In general, these systems can float in the gastric condition and control the drug release from the tablets.

  11. Solid Matrix Transformation and Tracer Addition using Molten Ammonium Bifluoride Salt as a Sample Preparation Method for Laser Ablation Inductively Coupled Plasma Mass Spectrometry

    Energy Technology Data Exchange (ETDEWEB)

    Grate, Jay W.; Gonzalez, Jhanis J.; O' Hara, Matthew J.; Kellogg, Cynthia M.; Morrison, Samuel S.; Koppenaal, David W.; Chan, George C.; Mao, Xianglei; Zorba, Vassilia; Russo, Richard

    2017-09-08

    Laser ablation (LA) is a means of sample introduction to inductively coupled plasma (ICP) mass spectrometry (MS) that avoids acid dissolution and chemical separation steps conventionally associated with solid sample analysis. At the same time, certain features of LA-ICP-MS are often mentioned in critical reviews including solid matrix variability and its influence on the ablation process, matrix dependent elemental fractionation, lack of matrix matched standards for external calibration, and limitations to internal calibration because it is challenging to add and distribute spikes into solid samples. In this paper we introduce the concept of a synergistic minimal sample preparation method that is used in combination with LA-ICP-MS as a means to overcome these limitations. The aim of this minimal sample preparation procedure is to reactively transform the original matrix to a more consistent matrix for LA-based analysis, thus reducing the effects of matrix variability, while enabling the addition of tracers. In conjunction with ICP-MS, we call this MTR-LA-ICP-MS, where MTR is derived from matrix transformation including the option to add tracers

  12. Preparation and In Vitro-In Vivo Evaluation of Sustained-Release Matrix Pellets of Capsaicin to Enhance the Oral Bioavailability.

    Science.gov (United States)

    Zhang, Ya; Huang, Zhimin; Omari-Siaw, E; Lu, Shuang; Zhu, Yuan; Jiang, Dongmei; Wang, Miaomiao; Yu, Jiangnan; Xu, Ximing; Zhang, Weiming

    2016-04-01

    Capsaicin has multiple pharmacological activities including antioxidant, anticancer, and anti-inflammatory activities. However, its clinical application is limited due to its poor aqueous solubility, gastric irritation, and low oral bioavailability. This research was aimed at preparing sustained-release matrix pellets of capsaicin to enhance its oral bioavailability. The pellets comprised of a core of solid-dispersed capsaicin mixed with microcrystalline cellulose (MCC) and hydroxypropyl cellulose (HPMC) and subsequently coating with ethyl cellulose (EC) were obtained by using the technology of extrusion/spheronization. The physicochemical properties of the pellets were evaluated through scanning electron microscopy (SEM), differential scanning calorimetry (DSC), and X-ray diffractometry (XRD). Besides, the in vitro release, in vivo absorption, and in vitro-in vivo correlation were also assessed. More importantly, the relative bioavailability of the sustained-release matrix pellets was studied in fasted rabbits after oral administration using free capsaicin and solid dispersion as references. The oral bioavailability of the matrix pellets and sustained-release matrix pellets of capsaicin was improved approximately 1.98-fold and 5.34-fold, respectively, compared with the free capsaicin. A good level A IVIVC (in vitro-in vivo correlation) was established between the in vitro dissolution and the in vivo absorption of sustained-release matrix pellets. All the results affirmed the remarkable improvement in the oral bioavailability of capsaicin owing to the successful preparation of its sustained-release matrix pellets.

  13. Photo-induced anisotropy in ZnO/PVA nanocomposites prepared by modified electrochemical method in PMA matrix

    Science.gov (United States)

    Yanchuk, O. M.; Ebothé, J.; El-Naggar, A. M.; Albassam, A.; Tsurkova, L. V.; Marchuk, O. V.; Lakshminarayana, G.; Tkaczyk, S.; Kityk, I. V.; Fedorchuk, A. O.; Vykhryst, O. M.; Urubkov, I. V.

    2017-02-01

    Substantial photo-induced optical anisotropy was discovered in ZnO/PVA nanocomposites under the influence of external bicolor laser illumination. Zinc oxide nanoparticles were synthesized by electrolysis of a sodium chloride aqueous medium including poly-methacrylic acid (PMA) in a cell system having a soluble zinc anode. The structural analysis of the ZnO powder samples has been carried out by X-Ray Diffractometry (XRD) and Scanning Electron Microscopy (SEM). The polyvinyl alcohol (PVA) embedded ZnO films obtained from the powder samples possess larger grain sizes than those in powder form. The films were prepared from the same polymer matrix but elaborated with two different PVA contents which are respectively 15% and 30%. The photoinduced anisotropy was identified by using two bicolor Er: glass laser beams incident at different angles. Substantial influence of the technological processes on the embedded nanoparticle sizes and related birefringence was explored. The process of laser induced anisotropy shows an occurrence of birefringence saturation.

  14. Independent assessment of matrix-assisted laser desorption/ionization mass spectrometry (MALDI-MS) sample preparation quality: A novel statistical approach for quality scoring.

    Science.gov (United States)

    Kooijman, Pieter C; Kok, Sander J; Weusten, Jos J A M; Honing, Maarten

    2016-05-05

    Preparation of samples according to an optimized method is crucial for accurate determination of polymer sample characteristics by Matrix-Assisted Laser Desorption Ionization (MALDI) analysis. Sample preparation conditions such as matrix choice, cationization agent, deposition technique or even the deposition volume should be chosen to suit the sample of interest. Many sample preparation protocols have been developed and employed, yet finding the optimal sample preparation protocol remains a challenge. Because an objective comparison between the results of diverse protocols is not possible, "gut-feeling" or "good enough" is often decisive in the search for an optimum. This implies that sub-optimal protocols are used, leading to a loss of mass spectral information quality. To address this problem a novel analytical strategy based on MALDI imaging and statistical data processing was developed in which eight parameters were formulated to objectively quantify the quality of sample deposition and optimal MALDI matrix composition and finally sum up to an overall quality score of the sample deposition. These parameters can be established in a fully automated way using commercially available mass spectrometry imaging instruments without any hardware adjustments. With the newly developed analytical strategy the highest quality MALDI spots were selected, resulting in more reproducible and more valuable spectra for PEG in a variety of matrices. Moreover, our method enables an objective comparison of sample preparation protocols for any analyte and opens up new fields of investigation by presenting MALDI performance data in a clear and concise way.

  15. Preparation and rebinding properties of protein-imprinted polysiloxane using mesoporous calcium silicate grafted non-woven polypropylene as matrix.

    Science.gov (United States)

    Kan, Bohong; Feng, Lingzhi; Zhao, Kongyin; Wei, Junfu; Zhu, Dunwan; Zhang, Linhua; Ren, Qian

    2016-03-01

    Calcium silicate particle containing mesoporous SiO2 (CaSiO3@SiO2) was grafted on the surface of non-woven polypropylene. The PP non-woven grafted calcium silicate containing mesoporous SiO2 (PP-g-CaSiO3@SiO2) was used as the matrix to prepare bovine serum albumin (BSA) molecularly imprinted polysiloxane (MIP) by using silanes as the functional monomers and BSA as the template. PP non-woven grafted BSA-imprinted polysiloxane (PP-g-CaSiO3@SiO2 MIP) was characterized by scanning electron microscope (SEM), Fourier transform infrared spectometry (FTIR) and drilling string compensator (DSC). Influence factors on the rebinding capacity of the MIP were investigated, such as grafting degree, the pH in treating CaSiO3 and the type and proportion of silanes. The rebinding properties of BSA on PP-g-CaSiO3@SiO2 and MIP were investigated under different conditions. The results indicated that the rebinding capacity of MIP for BSA reached 56.32 mg/g, which was 2.65 times of NIP. The non-woven polypropylene grafted BSA-imprinted polysiloxane could recognize the template protein and the selectivity factor (β) was above 2.4 when using ovalbumin, hemoglobin and γ-globulin as control proteins. The PP-g-CaSiO3@SiO2 MIP has favorable reusability. Copyright © 2015 John Wiley & Sons, Ltd.

  16. Compression and evaluation of extended release matrix pellets prepared by the extrusion/spheronization process into disintegrating tablets

    Directory of Open Access Journals (Sweden)

    Raveendra Pai

    2012-03-01

    Full Text Available In this study, a novel approach for compression of matrix pellets into disintegrating tablets has been studied in an attempt to overcome the issues pertaining to rupture of polymer coat during compression of reservoir-type pellets. Extended release matrix pellets were prepared by the extrusion/spheronization technique using commercially available aqueous dispersions of ethyl cellulose, acrylic polymers and sodium alginate at 10%, 20% and 30%w/w levels. Sertraline hydrochloride was used as the model drug and an in vitro release profile of 12 h was targeted. Tablets containing matrix pellets were prepared by the direct compression process. Acceptance Value, a pharmacopeial test, was applied to study the uniformity of drug distribution. Effect of compression force (2-6 kN, extrusion screen aperture size, diluent blend composition and pellet percentage on drug release and acceptance value were studied. As polymer is uniformly distributed within each pellet, the drug release pattern from uncompressed pellets was comparable to compressed tablets. Surface morphological changes due to calcium chloride treatment were observed using Scanning electron microscopy. The pellet segregated from the surface of the tablet was found to be flattened in the direction of applied compression force with minor deformities. In conclusion, matrix pellets can constitute an alternative approach to reservoir-type pellets in obtaining disintegrating tablets for extended delivery of drugs.Nesse trabalho, estudou-se nova abordagem para a compressão de matrizes de péletes em comprimidos desintegrantes, com o intuito de resolver os problemas relativos à ruptura do polímero de revestimento durante a compressão dos péletes do tipo reservatório. Matrizes de péletes de liberação estendida foram preparadas pela técnica de extrusão/esferonização, utilizando dispersões aquosas comercialmente disponíveis de etil celulose, polímeros acrílicos e alginato de sódio a 10

  17. Microstructure and properties of mechanical alloying particles reinforced aluminum matrix composites prepared by semisolid stirring pouring method

    Directory of Open Access Journals (Sweden)

    Yao-qiang Si

    2016-05-01

    Full Text Available Aluminum matrix composites reinforced with mechanical alloying particles (SiCp were fabricated by the semisolid stirring pouring method. The influence of mechanical alloying particles and Mg on the microstructure and mechanical properties of the composites was investigated by means of optical microscopy (OM, X-ray diffraction scanning (XRD, electron microscopy (SEM and energy dispersive spectroscopy (EDS. Results show that the addition of Mg converts the agglomerate mechanical alloying particles in ZL101 matrix composites into dispersed distribution in ZL101-Mg matrix composites, large matrix grains into fine equiaxed matrix grains, and eutectic phase into fine particles. So the mechanical properties of ZL101-Mg matrix composites are better than those of ZL101 matrix composites. The mechanical properties of ZL101/ZL101-Mg matrix composites are gradually increased with the increase of the volume fraction of mechanical alloying particles. When the volume fraction of mechanical alloying particles is 3%, the Vickers hardness and ultimate tensile strength of the ZL101/ZL101-Mg matrix composites reach their maximum values.

  18. 灌注法制备肺脱细胞基质%Pulmonary perfusion for preparation of the acellular matrix

    Institute of Scientific and Technical Information of China (English)

    龚正

    2015-01-01

    背景:对组织器官进行脱细胞,细胞外基质在经过去除细胞和可溶性蛋白处理之后,可维持正常的器官外形及组织结构基质成分.目的:利用灌注法制备肺脱细胞基质.方法:将 40 只 Wistar 大鼠随机均分为 2 组,常规麻醉处理后打开胸腔,获得完整的肺组织,实验组利用Langendorff灌注模型构建大鼠全肺脱细胞基质支架,对照组不予以特殊处理.动态观察和记录实验组肺脏颜色和形态变化,分别从 2 组大鼠肺脏不同部位获取小块组织,利用电子显微镜进行组织学观察,观察两组的Weigert弹力纤维联合Von Gieson结缔组织染色和苏木精-伊红染色情况.结果与结论:经1%脱氧胆酸钠溶液灌注后,实验组大鼠肺脏颜色逐渐发生改变,表现为从内至外呈分段分叶状逐渐变为白色半透明状,并可观察到清晰肺叶结构,最终肺脏呈现出均一的白色半透明状.经 Weigert 弹力纤维联合Von Gieson结缔组织染色和苏木精-伊红染色发现,对照组新鲜肺组织切片中含有大量细胞,其中包括毛细血管和成纤维细胞及内皮细胞等,细胞呈整齐排列状,具有完整的肺泡结构,弹性纤维结构清晰,胶原纤维也呈整齐排列状,结构较为紧凑;实验组肺组织细胞基本已消失,仍具有完整的肺泡形态结构,但呈较为疏松的状态且裂隙增大,弹性纤维保存良好,胶原纤维呈较疏松排列状.表明利用灌注法课可有效构建大鼠全肺组织基质支架.%BACKGROUND:The extracelular matrix with removal of cels and soluble proteins can maintain the normal shape of organs and matrix components. OBJECTIVE:To prepare the acelular matrix of lung tissue using perfusion method. METHODS:Forty Wistar rats were randomly divided into two groups: under routine anesthesia, the chest was open to obtain complete lung tissue for construction of rat lung acelular matrix scaffold using Langendorff perfusion model in experimental group

  19. 一种高温固化环氧基体树脂的研制%The Preparation of a Kind of High Temperature Curing Epoxy Matrix Resin

    Institute of Scientific and Technical Information of China (English)

    冯浩; 王德志; 曲春艳; 李洪峰

    2011-01-01

    A kind of high temperature curing epoxy matrix resin was prepared by technologies of prepolymerization, synthesis of b-stage resin and mechanical blending. The effect of quantity of CTBN on the toughness and thermal stability of matrix resin was discussed. The results showed that the epoxy matrix resin prepared by the method of prepolymerization obtained higher heat resistance and toughness, the glass-transition temperature reached 189℃ and the impact resistance reached 26.12 Kj/ m2 when the quantity of CTBN was 5 phr. The prepared matrix resin had better viscosity-temperature property and it could meet the requirement of the forming process and comprehensive properties of epoxy matrix composites.%采用预聚合、B阶树脂合成及机械共混工艺制备了一种高温固化环氧基体树脂,探讨了增韧剂-端羧基液体橡胶(CTBN)用量对基体树脂韧性和耐热性的影响.试验结果表明:当CTBN的用量为5phr,且与环氧树脂采用预聚合方式制得的基体树脂获得了较高的耐热性和韧性,玻璃化转变温度为189℃,冲击强度达到了26.12k J/m2;制得的基体树脂具有较好的黏温特性和力学性能,满足环氧基复合材料的成型工艺和综合性能要求.

  20. Effect of the glassy carbon structure on the aspect ratio of micropoints of matrix field-emission cathodes prepared by thermochemical etching

    Science.gov (United States)

    Pleshkova, L. S.; Shesterkin, V. I.

    2016-11-01

    The application of thermochemical etching technology makes it possible to reveal and investigate the structure of SU-2000 glassy carbon using electron microscopy. The glassy carbon structure at the microscopic and nanoscopic levels is inhomogeneous and consists of pockets with an irregular cross section separated by partitions. This structure sets the limits on the aspect ratio of geometrical sizes and micropoint packing density in the matrix prepared by thermochemical etching.

  1. Preparation and characterization of new photoluminescent nano-powder based on Eu3+:La2Ti2O7 and dispersed into silica matrix for latent fingerprint detection

    Science.gov (United States)

    Saif, M.; Alsayed, N.; Mbarek, A.; El-Kemary, M.; Abdel-Mottaleb, M. S. A.

    2016-12-01

    Pure lanthanum titanate doped with europium metal ions (La2Ti2O7:Eu3+) and dispersed in silica matrix phosphor powder was prepared by sol-gel process followed by thermal treatment. The prepared nanophosphors were characterized by powder X-ray Diffraction (XRD), Fourier Transform Infrared (FT-IR), Transmission Electron Microscope (TEM), Energy Dispersive Spectroscopy (EDX), and Photoluminescence Spectroscopy (PL). The effects of silica, thermal treatment, Eu3+ ion, and surfactant (CTAB) concentrations on the crystal, morphology, and photoluminescence properties were investigated. The present work found that dispersion of La2Ti2O7:Eu3+ into silica matrix significantly altered the morphology of La2Ti2O7:Eu3+ from high crystalline micro-plate like shape into amorphous aggregated Nano-spherical shape. The high separated spherical shape with intense red PL emission and long lifetime was obtained from 10 mol% Eu3+:La2Ti2O7:Eu3+, dispersed into silica matrix, and prepared in the presence of CTAB. The high PL Nano-phosphor has been successfully used in developing latent fingerprint from various forensic relevant materials.

  2. Effect of the surface preparation techniques on the EBSD analysis of a friction stir welded AA1100-B{sub 4}C metal matrix composite

    Energy Technology Data Exchange (ETDEWEB)

    Guo, J., E-mail: junfeng.guo@cnrc-nrc.gc.ca [University of Quebec at Chicoutimi, Chicoutimi (QC), G7H 2B1 (Canada); Aluminium Technology Centre, National Research Council Canada, Chicoutimi (QC), G7H 8C3 (Canada); Amira, S.; Gougeon, P. [Aluminium Technology Centre, National Research Council Canada, Chicoutimi (QC), G7H 8C3 (Canada); Chen, X.-G. [University of Quebec at Chicoutimi, Chicoutimi (QC), G7H 2B1 (Canada)

    2011-09-15

    Aluminum based metal matrix composites (MMCs) have been used in various automobile, aerospace and military industries. Yet characterization of the microstructure in these materials remains a challenge. In the present work, the grain structure in the matrix of B{sub 4}C particulate reinforced MMCs and their friction stir welds is characterized by using optical metallography and the electron backscatter diffraction (EBSD) technique. Optical metallography can partially reveal the grain structure in the matrix of AA1100-16 vol.% B{sub 4}C composite. The EBSD technique has been successfully applied to characterize the grain structure in the AA1100-16 vol.% B{sub 4}C friction stir welds, which provides a powerful tool to follow the microstructural evolution of MMC materials during friction stir welding (FSW). Both mechanical polishing and ion beam polishing are used for the EBSD sample preparation. The effect of the sample preparation on the EBSD data acquisition quality is studied. Some typical examples, such as the identification of grains and subgrains, grain size distribution, deformation fields and the texture components are given. - Highlights: {yields} EBSD has been used to characterize the grain structure of Al-B{sub 4}C MMCs. {yields} Mechanical and ion beam polishing are compared for EBSD sample preparation of MMCs. {yields} EBSD shows great advantages over optical microscopy for microtexture analysis of MMCs.

  3. Classification and Preparation of Ocean Engineering Metal Matrix Composite%海洋工程金属基复合材料的分类与制备

    Institute of Scientific and Technical Information of China (English)

    贺毅强

    2011-01-01

    介绍了海洋环境的特点,综述了海洋工程金属基复合材料的发展现状,介绍了海洋工程金属基复合材料的分类与特点,着重介绍了铁基、铝基、钛基及铜基复合材料;综述了金属基复合材料制备技术的发展历程;概述了液态法、扩散粘结法、形变法、沉积法、多层喷射沉积法以及原位合成法等工艺;展望了海洋工程金属基复合材料的产业化发展趋势,提出了海洋工程金属材料朝金属基复合材料的方向发展,而采用防腐蚀涂层和镀层将进一步提高复合材料的耐腐蚀性.%The characteristic of ocean environment was introduced. The current status of ocean engineering metal matrix composite was introduced, and Ferrum matrix, aluminium matrix, titanium matrix and copper matrix composite were recommended specially. The preparation technology development of ocean engineering metal matrix composite was summarized. Specially liquid method, diffusion bonding, deforming method, deposition method, multi-layer spray deposition and in-situ composition were presented. Industrialization and development tendency were summarized. And it is considered that ocean engineering metals develop to the direction of ocean engineering metal matrix composite, and the corrosion resistance of the composite can be improved by anti-corrosion coating and film.

  4. Preparation

    Directory of Open Access Journals (Sweden)

    M.M. Dardir

    2014-03-01

    Full Text Available Some hexanamide-mono and di-linoleniate esters were prepared by the reaction of linolenic acid and hexanamide (derived from the reaction of hexanoic acid and diethanolamine. The chemical structure for the newly prepared hexanamide-mono and di-linoleniate esters were elucidated using elemental analysis, (FTIR, H 1NMR and chemical ionization mass spectra (CI/Ms spectroscopic techniques. The results of the spectroscopic analysis indicated that they were prepared through the right method and they have high purity. The new prepared esters have high biodegradability and lower toxicity (environmentally friendly so they were evaluated as a synthetic-based mud (ester-based mud for oil-well drilling fluids. The evaluation included study of the rheological properties, filtration and thermal properties of the ester based-muds formulated with the newly prepared esters compared to the reference commercial synthetic-based mud.

  5. Effects of MgO Nano Particles on Microstructural and Mechanical Properties of Aluminum Matrix Composite prepared via Powder Metallurgy Route

    Science.gov (United States)

    Baghchesara, Mohammad Amin; Abdizadeh, Hossein; Baharvandi, Hamid Reza

    The objective of the present investigation was to evaluate the microstructural and mechanical properties of Al/nano MgO composite prepared via powder metallurgy method. Pure atomized aluminum powder with an average particle size of 1μm and MgO particulate with an average particle size between 60 to 80 nm were used. Composites containing 1.5, 2.5 and 5 percent of volume fraction of MgO were prepared by powder metallurgy method. The specimens were pressed by Cold Isostatic Press machine (CIP), subsequently were sintered at 575, 600 and 625°C. After sintering and preparing the samples, mechanical properties were measured. The results of microstructure, compression and hardness tests indicated that addition of MgO particulates to aluminum matrix composites improves the mechanical properties.

  6. Wax-matrix tablet for time-dependent colon-specific delivery system of sophora flavescens Aiton: preparation and in vivo evaluation.

    Science.gov (United States)

    Zou, Meijuan; Wang, Yue; Xu, Caihong; Cheng, Gang; Ren, Jungang; Wu, Gaolei

    2009-02-01

    A wax-matrix time-dependent colon-specific tablet (WM-TDCS) was studied. Wax-matrix tablet core consisting of semi-synthetic glycerides, as a wax polymeric expanding agent, carboxymethyl starch sodium (CMS-Na), and NaCl was prepared, and Sophora flavescens Aiton (ASF, extracts of traditional Chinese medicine) was used as model drug. The wax-matrix ASF tablets core was coated with Eudragit NE 30 D as the inner coating materials and with Opadry OY-P-7171 as the outer coating materials. The in vitro release behaviors of the coated tablets were examined and then in vivo absorption kinetics of the coated tablets in dogs was further investigated. The volume of the tablet core was markedly increased at 37 degrees C because of the expand effect of polymer semi-synthetic glycerides and CMS-Na. The drug release from WM-TDCS was more stable than TDCS in vitro and in vivo. The lag time of ASF release was also controlled by the thickness of the inner coating layer. In vivo evaluation demonstrated that in vivo lag time of absorption was in a good agreement with in vitro lag time of release. ASF wax-matrix tablets coated with Eudragit NE 30 D and Opadry OY-P-7171 using the regular coating technique could be designed to achieve a lag time of 3 h in the small intestinal tract.

  7. Controlled release of 5-fluorouracil or mitomycin-c from polymer matrix: Preparation by radiation polymerization and in vivo evaluation of the anticancer drug/polymer composites

    Science.gov (United States)

    Li, Ximing; Shen, Weiming; Liu, Chengjie; Nishimoto, Sei-Ichi; Kagiya, Tsutomu

    Polymer tablets containing anticancer drugs such as 5-fluorouracil (5-FU) and mitomycin-C (MMC) have been prepared to evaluate the drug-release characteristics in vitro and the effect on local control of mouse solid tumors in vivo. Radiation-induced polymerization of hydrophilic monomers (2-hydroxyethyl methacrylate and related monomers) at low temperature (-80°C) was performed to immobilize 5-FU or MMC in the polymer matrix. The drug was dispersed as microcrystallines within the polymer matrix. The rate of drug release in vitro in buffer solution (pH7.0, 37°C) increased with increase in hydrophilicity of polymer matrix. Appropriate amount of crosslinks within the polymer matrix, as formed by ethylene glycol dimethacrylate (2G) added in the polymerization system, was effective to control the rate of drug release. The drug release became faster upon the addition of increasing amount of water in the radiation-induced polymerization. The tablet consisting of drug/polymer was buried surgically near solid tumors of striate muscle sarcoma (S180) transplanted to Kunming mice and the therapeutic effect of slow releasing drugs was evaluated in vivo by reference to intraperitoneal (i.p.) injection of the corresponding drugs. The slow releasing drugs led to high chemotherapeutic gain for local control of solid tumors with remarkable reduction of toxic side effect of the drugs.

  8. Thermal diffusion of {sup 57}Co into rhodium matrix as a second step in preparing Moessbauer sources

    Energy Technology Data Exchange (ETDEWEB)

    Cieszykowska, Izabela; ZoLtowska, MaLgorzata [Institute of Atomic Energy Polatom, Radioisotope Centre, 05-400 Otwock-Swierk (Poland); Zachariasz, Piotr [Institute of Atomic Energy Polatom, Moessbauer Spectroscopy Lab, 05-400 Otwock-Swierk (Poland); Piasecki, Andrzej; Janiak, Tomasz [Institute of Atomic Energy Polatom, Radioisotope Centre, 05-400 Otwock-Swierk (Poland); Mielcarski, MieczysLaw, E-mail: m.mielcarski@polatom.pl [Institute of Atomic Energy Polatom, Radioisotope Centre, 05-400 Otwock-Swierk (Poland)

    2011-09-15

    Thermal diffusion of {sup 57}Co into rhodium matrix was studied. The diffusion degree was evaluated by Moessbauer spectroscopy with the use of {alpha}-Fe absorber. The influence of different annealing conditions was investigated. For a set of sources examined, smooth and rounded Lorentzian lines were observed. The main spectra parameters are fairly acceptable with respect to the typical obtainable values for {alpha}-Fe absorbers in Moessbauer spectroscopy. The results obtained confirm that the deposited {sup 57}Co diffused almost completely into rhodium matrix without substantial loss of the activity deposited.

  9. In situ liquid-liquid extraction as a sample preparation method for matrix-assisted laser desorption/ionization MS analysis of polypeptide mixtures

    DEFF Research Database (Denmark)

    Kjellström, Sven; Jensen, Ole Nørregaard

    2003-01-01

    A novel liquid-liquid extraction (LLE) procedure was investigated for preparation of peptide and protein samples for matrix-assisted laser desorption/ionization mass spectrometry (MALDI MS). LLE using ethyl acetate as the water-immiscible organic solvent enabled segregation of hydrophobic...... matrix to the organic solvent enhanced the efficiency of the LLE-MALDI MS method for analysis of hydrophobic peptides and proteins. LLE-MALDI MS enabled the detection of the hydrophobic membrane protein bacteriorhodopsin as a component in a simple protein mixture. Peptide mixtures containing...... phosphorylated, glycosylated, or acylated peptides were successfully separated and analyzed by the in situ LLE-MALDI MS technique and demonstrate the potential of this method for enhanced separation and structural analysis of posttranslationally modified peptides in proteomics research....

  10. Simplified sample preparation method for protein identification by matrix-assisted laser desorption/ionization mass spectrometry: in-gel digestion on the probe surface

    DEFF Research Database (Denmark)

    Stensballe, A; Jensen, Ole Nørregaard

    2001-01-01

    Identification and detailed characterization of complex mixtures of proteins separated by polyacrylamide gel electrophoresis (PAGE) require optimized and robust methods for interfacing electrophoretic techniques to mass spectrometry. Peptide mapping by matrix-assisted laser desorption/ionization-......Identification and detailed characterization of complex mixtures of proteins separated by polyacrylamide gel electrophoresis (PAGE) require optimized and robust methods for interfacing electrophoretic techniques to mass spectrometry. Peptide mapping by matrix-assisted laser desorption...... for protein identification similar to that obtained by the traditional protocols for in-gel digestion and MALDI peptide mass mapping of human proteins, i.e. approximately 60%. The overall performance of the novel on-probe digestion method is comparable with that of the standard in-gel sample preparation...

  11. Preparation of polypropylene/montmorillonite nanocomposites by intercalative polymerization: Effect of in situ polymer matrix functionalization on the stability of the nanocomposite structure

    Institute of Scientific and Technical Information of China (English)

    YANG KeFang; HUANG YingJuan; DONG JinYong

    2007-01-01

    The copolymerization of propylene and 5-hexenyl-9-borabicyclo[3.3.1]nonane (5-hexenyl-9-BBN) has been conducted with an MgCl2/TiCl4 catalyst intercalated in an organically modified montmorillonite (OMMT) with triethylaluminum (AlEt3) cocatalyst and diphenyldimethoxysilane (DDS) external donor. This polymerization process simultaneously results in both the exfoliation of MMT layers to realize the preparation of polypropylene (PP)/MMT nanocomposites and the implantation of reactive borane groups in the formed PP matrix. The polymer-borne borane groups have been able to undergo an efficient hydrolysis process under very mild reaction conditions (40℃, 3 h, in THF), introducing hydroxy groups into PP without sacrificing the polymerization-formed nanocomposite structure (the exfoliation of MMT). The resultant hydroxyl-functionalized PP/MMT nanocomposites exhibit enhanced structural stability against processing compared with those based on unfunctionalized PP matrix.

  12. Investigation on microstructural and mechanical properties of B4C–aluminum matrix composites prepared by microwave sintering

    Directory of Open Access Journals (Sweden)

    Ehsan Ghasali

    2015-10-01

    Full Text Available B4C reinforced aluminum composites were fabricated by microwave heating of the mixture of B4C (10, 15 and 20 wt% and aluminum powders at 650, 750, 850 and 950 °C. The effect of different amounts of B4C on the microstructure and mechanical properties of aluminum matrix was examined. The maximum bending (238 ± 10 MPa and compressive strength (330 ± 10 MPa values were measured for composites sintered at 950 and 750 °C, respectively. The maximum hardness (112 Vickers was measured for Al–20 wt% B4C composite sintered at 850 °C. XRD investigations showed the decomposition of boron carbide and also the formation of Al3BC by heating the composites at 850 °C. SEM micrographs showed uniform distribution of reinforcement particles in Al matrix.

  13. Nanoscale multilayered and porous carbide interphases prepared by pressure-pulsed reactive chemical vapor deposition for ceramic matrix composites

    Energy Technology Data Exchange (ETDEWEB)

    Jacques, S., E-mail: jacques@lcts.u-bordeaux1.fr [LCTS, University of Bordeaux 1, CNRS, Herakles-Safran, CEA, 3 allee de la Boetie, F-33600 Pessac (France); Jouanny, I.; Ledain, O.; Maillé, L.; Weisbecker, P. [LCTS, University of Bordeaux 1, CNRS, Herakles-Safran, CEA, 3 allee de la Boetie, F-33600 Pessac (France)

    2013-06-15

    In Ceramic Matrix Composites (CMCs) reinforced by continuous fibers, a good toughness is achieved by adding a thin film called “interphase” between the fiber and the brittle matrix, which acts as a mechanical fuse by deflecting the matrix cracks. Pyrocarbon (PyC), with or without carbide sub-layers, is typically the material of choice to fulfill this role. The aim of this work was to study PyC-free nanoscale multilayered carbide coatings as interphases for CMCs. Nanoscale multilayered (SiC–TiC){sub n} interphases were deposited by pressure-Pulsed Chemical Vapor Deposition (P-CVD) on single filament Hi-Nicalon fibers and embedded in a SiC matrix sheath. The thicknesses of the carbide interphase sub-layers could be made as low as a few nanometers as evidenced by scanning and transmission electron microscopy. By using the P-ReactiveCVD method (P-RCVD), in which the TiC growth involves consumption of SiC, it was not only possible to obtain multilayered (SiC–TiC){sub n} films but also TiC films with a porous multilayered microstructure as a result of the Kirkendall effect. The porosity in the TiC sequences was found to be enhanced when some PyC was added to SiC prior to total RCVD consumption. Because the porosity volume fraction was still not high enough, the role of mechanical fuse of the interphases could not be evidenced from the tensile curves, which remained fully linear even when chemical attack of the fiber surface was avoided.

  14. Preparation of sustained release matrix pellets by melt agglomeration in the fluidized bed: influence of formulation variables and modelling of agglomerate growth.

    Science.gov (United States)

    Pauli-Bruns, Anette; Knop, Klaus; Lippold, Bernhard C

    2010-03-01

    The one-step preparation of sustained release matrix pellets, using a melting procedure in a fluidized bed apparatus, was tested in a 2(3) full factorial design of experiments, using microcrystalline wax as lipophilic binder, theophylline as model drug and talc as additional matrix forming agent. The three influence parameters were (A) size of binder particles, (B) fraction of theophylline in solid particles and (C) fraction of microcrystalline wax in formulation. The response variables were agglomerate size and size distribution, dissolution time, agglomerate crush resistance, sphericity, yield and porosity. Nearly spherical pellets comprising a smooth, closed surface could be obtained with the used method, exhibiting the hollow core typical for the immersion and layering mechanism. The reproducibility was very good concerning all responses. The size of agglomerates is proportional to the size of the binder particles, which serve as cores for pellet formation in the molten state in the fluidized bed. Additionally, the agglomerate size is influenced by the volume of the solid particles in relation to the binder particles, with more solid particles leading to larger agglomerates and vice versa. Dissolution times vary in a very wide range, resulting from the interplay between amount of drug in relation to the meltable matrix substance microcrystalline wax and the non-meltable matrix substance talc. The change of binder particle size does not lead to a structural change of the matrix; both dissolution times and porosity are not significantly altered. Agglomerate crush resistance is low due to the hollow core of the pellets. However, it is significantly increased if the volume fraction of microcrystalline wax in the matrix is high, which means that the matrix is mechanically better stabilized. A theoretical model has been established to quantitatively explain agglomerate growth and very good accordance of the full particle size distributions between predicted and

  15. Preparation Methods for Aluminum Matrix Composite%铝基复合材料的制备方法

    Institute of Scientific and Technical Information of China (English)

    倪增磊; 王爱琴; 田可庆

    2011-01-01

    The pressureless infiltration process for the preparation of high volume fraction SiC/Al composite, vacuum canning hot-extrusion process and spray deposition technology process for the preparation of high-silicon aluminum composite were reviewed. The development trends for the preparation of aluminum composite material were looked forward.%综述了无压浸渗法制备高体积分数SiC/Al复合材料,以及粉末真空包套热挤压和喷射沉积工艺制备高硅含量铝基复合材料的方法,同时展望了制备铝基复合材料的发展趋势.

  16. Physicochemical properties and mechanism of drug release from ethyl cellulose matrix tablets prepared by direct compression and hot-melt extrusion.

    Science.gov (United States)

    Crowley, Michael M; Schroeder, Britta; Fredersdorf, Anke; Obara, Sakae; Talarico, Mark; Kucera, Shawn; McGinity, James W

    2004-01-28

    The objective of this research project was to determine the physicochemical properties and investigate the drug release mechanism from ethyl cellulose (EC) matrix tablets prepared by either direct compression or hot-melt extrusion (HME) of binary mixtures of water soluble drug (guaifenesin) and the polymer. Ethyl cellulose was separated into "fine" or "coarse" particle size fractions corresponding to 325-80 and 80-30 mesh particles, respectively. Tablets containing 30% guaifenesin were prepared at 10, 30, or 50 kN compaction forces and extruded at processing temperatures of 80-90 and 90-110 degrees C. The drug dissolution and release kinetics were determined and the tablet pore characteristics, tortuosity, thermal properties and surface morphologies were studied using helium pycnometry, mercury porosimetry, differential scanning calorimetry and scanning electron microscopy. The tortuosity was measured directly by a novel technique that allows for the calculation of diffusion coefficients in three experiments. The Higuchi diffusion model, Percolation Theory and Polymer Free Volume Theory were applied to the dissolution data to explain the release properties of drug from the matrix systems. The release rate was shown to be dependent on the ethyl cellulose particle size, compaction force and extrusion temperature.

  17. A new consideration on reinforcement distribution in the different planes of nanostructured metal matrix composite sheets prepared by accumulative roll bonding (ARB)

    Energy Technology Data Exchange (ETDEWEB)

    Yazdani, Ali [Department of Materials Science and Engineering, School of Engineering, Shiraz University, Zand Blvd., 7134851154 Shiraz (Iran, Islamic Republic of); Salahinejad, E., E-mail: erfan.salahinejad@gmail.com [Department of Materials Science and Engineering, School of Engineering, Shiraz University, Zand Blvd., 7134851154 Shiraz (Iran, Islamic Republic of); Moradgholi, J.; Hosseini, M. [Department of Materials Science and Engineering, School of Engineering, Shiraz University, Zand Blvd., 7134851154 Shiraz (Iran, Islamic Republic of)

    2011-09-29

    Highlights: > Al-B{sub 4}C composites can be successfully prepared by accumulative roll bonding (ARB). > TEM reveals the development of nanostructures in Al-B{sub 4}C composites processed by ARB. > The reinforcement distribution in the RD-ND planes is more uniform than the TD-ND planes. - Abstract: Recently, a number of novel methods based on accumulative roll bonding (ARB) have been introduced to produce particulate metal matrix composites. Nonetheless, the microstructure uniformity from the reinforcement distribution viewpoint in the different planes of ARBed composite sheets has not been focused up to date. This paper aims to compare the evolution of the B{sub 4}C particles distribution in nanostructured Al-10 vol.% B{sub 4}C composites prepared by ARB in the rolling direction-normal direction (RD-ND) and transverse direction-normal direction (TD-ND) planes. From optical microscopic evaluations quantified by the radial distribution function analysis, it is realized that the homogeneity in the RD-ND planes is in excess of the TD-ND planes. In addition, transmission electron microscopy reveals the development of nanostructures in the Al matrix after seven ARB passes.

  18. Storage stability of low-fat sodium reduced fresh merguez sausage prepared with olive oil in konjac gel matrix.

    Science.gov (United States)

    Triki, Mehdi; Herrero, Ana M; Jiménez-Colmenero, Francisco; Ruiz-Capillas, Claudia

    2013-08-01

    This paper evaluates the nutritional values and stability during refrigerated storage of fresh beef merguez sausage as affected by a reformulation process which modified the fat content both by reducing fat (replacing beef fat with konjac gel) and incorporating olive oil (replacing beef fat with olive oil stabilized in a konjac matrix) and by reducing sodium content, replacing sodium chloride with a salt mixture (containing potassium chloride, calcium chloride and magnesium chloride). A preservative (sodium metabisulphite) was also used to extend the shelf-life of the product. The fat was reduced by 32 to 80% and sodium by over 36%. The reformulation did not negatively affect the sensory evaluation. Low microbiota growth rate and biogenic amines were attributed mainly to the presence of sodium metabisulphite. This preservative could be used in the reformulation to enhance safety and/or extend the shelf-life of this type of product.

  19. Preparation of porous styrenics-based monolithic layers for thin layer chromatography coupled with matrix-assisted laser-desorption/ionization time-of-flight mass spectrometric detection.

    Science.gov (United States)

    Lv, Yongqin; Lin, Zhixing; Tan, Tianwei; Svec, Frantisek

    2013-11-01

    Monolithic 50 μm thin poly(4-methylstyrene-co-chloromethylstyrene-co-divinylbenzene) layers attached to 6.0 cm × 3.3 cm glass plates have been prepared, using a thermally initiated polymerization process. These layers had a well-defined porous structure with a globular morphology demonstrated with SEM images and exhibited superhydrophobic properties characterized with a water contact angle of 157°. They were then used for thin-layer chromatography of peptides and proteins fluorescently labeled with fluorescamine. The spots of individual separated compounds were visualized using UV light, and their identities were confirmed with a matrix-assisted laser desorption/ionization time of flight mass spectrometry. The presence of chloromethylstyrene units in the polymer enabled hypercrosslinking via a Friedel-Crafts alkylation reaction, and led to monoliths with much larger surface areas, which were suitable for separations of small dye molecules.

  20. Frontally eluted components procedure with thin layer chromatography as a mode of sample preparation for high performance liquid chromatography quantitation of acetaminophen in biological matrix.

    Science.gov (United States)

    Klimek-Turek, A; Sikora, M; Rybicki, M; Dzido, T H

    2016-03-04

    A new concept of using thin-layer chromatography to sample preparation for the quantitative determination of solute/s followed by instrumental techniques is presented Thin-layer chromatography (TLC) is used to completely separate acetaminophen and its internal standard from other components (matrix) and to form a single spot/zone containing them at the solvent front position (after the final stage of the thin-layer chromatogram development). The location of the analytes and internal standard in the solvent front zone allows their easy extraction followed by quantitation by HPLC. The exctraction procedure of the solute/s and internal standard can proceed from whole solute frontal zone or its part without lowering in accuracy of quantitative analysis. Copyright © 2016 Elsevier B.V. All rights reserved.

  1. Preparation and properties of gel membrane containing porous PVDF-HFP matrix and cross-linked PEG for lithium ion conduction

    Institute of Scientific and Technical Information of China (English)

    Mei ZHANG; Aiqing ZHANG; Zhenyu CUI; Baoku ZHU; Gaigc HAN; Youyi XU

    2008-01-01

    Lithium ion conducting membranes are the key materials for lithium batteries. The lithium ion conducting gel polymer electrolyte membrane (Li-GPEM) based on porous poly(vinylidene fluoride-co-hexafluoropropylene) (PVDF-HFP) matrix and cross-linked PEG network is pre-pared by a typical phase inversion process. By immersing the porous PVDF-HFP membrane in liquid electrolyte con-taining poly(ethylene glycol) diacrylate (PEGDA) and an initiator to absorb the liquid electrolyte at 25℃, and then thermally cross-linking at 60℃, the Li-GPEM is fabricated successfully. The measurements on its weight loss, mech-anical and electrochemical properties reveal that the obtained Li-GPEM has better overall performance than the liquid and blend gel systems used as conductive media in lithium batteries. The ionic conductivity of the fabricated Li-GPEM can reach as high as 2.25 × 10-3S/cm at 25℃.

  2. Preparation, microstructure and oxidation resistance of SiCN ceramic matrix composites with glass-like carbon interface

    Directory of Open Access Journals (Sweden)

    Yi Xia

    2009-02-01

    Full Text Available Glass-like carbon (GC interface was successfully introduced into carbon fiber-reinforced SiCN ceramic matrix composite (C/GC/SiCN by polymer infiltration and pyrolysis using phenolic resin as precursor. In order to highlight the Oxidation resistance of GC interface, the Oxidation behavior of GC, carbon fiber (Cf containing approximately 0.3 μm GC coating and C/GC/SiCN was investigated by means of weight changes and residual strength ratio before and after oxidizing, and the results were also compared with that of Cf containing Pyrocarbon (PyC coating and C/PyC/SiCN composite. Scanning electron microscopy displays homogeneous, adherent GC coating on Cf. Weight loss rate of Cf containing GC coating is lower than that of Cf containing PyC coating. The residual stress ratio of C/GC/SiCN was higher than that of C/PyC/SiCN. The results indicate that GC interface can improve anti-oxidation of Cf-reinforced composite than PyC interface.

  3. Crosslinkable mixed matrix membranes with surface modified molecular sieves for natural gas purification: I. Preparation and experimental results

    KAUST Repository

    Ward, Jason K.

    2011-07-01

    Dense film mixed matrix membranes (MMMs) comprised of SSZ-13 dispersed in a crosslinkable polyimide (PDMC) were fabricated and evaluated for carbon dioxide/methane separations. MMMs containing 25% (w/w) as-received (AR) SSZ-13 exhibited a carbon dioxide permeability of 153 Barrers with a carbon dioxide/methane ideal selectivity of 34.7 at 65. psia and 35 °C. This represents a permeability enhancement of 129% and a decline in selectivity of 4.7% over neat PDMC (PCO2=66.9 Barrers, αCO2/CH4=36.4). A sieve surface modification procedure was developed with the aim of improving SSZ-13/PDMC MMM transport properties. MMMs containing 25% (w/w) surface modified (SM) SSZ-13 exhibited a carbon dioxide permeability of 148 Barrers and carbon dioxide/methane selectivity of 38.9 at 65. psia and 35 °C, representing enhancements in both permeability and selectivity of 121% and 6.9%, respectively. Mixed gas permeation analyses of MMMs containing SM-SSZ-13 using a 10% carbon dioxide/90% methane mixture shows that permeability and selectivity enhancements of 47% and 13%, respectively, over neat PDMC are possible at 700. psia and 35 °C. © 2011 Elsevier B.V.

  4. Near-infrared spectroscopic analysis of the breaking force of extended-release matrix tablets prepared by roller-compaction: influence of plasticizer levels and sintering temperature.

    Science.gov (United States)

    Dave, Vivek S; Fahmy, Raafat M; Hoag, Stephen W

    2015-06-01

    The aim of this study was to investigate the feasibility of near-infrared (NIR) spectroscopy for the determination of the influence of sintering temperature and plasticizer levels on the breaking force of extended-release matrix tablets prepared via roller-compaction. Six formulations using theophylline as a model drug, Eudragit® RL PO or Eudragit® RS PO as a matrix former and three levels of TEC (triethyl citrate) as a plasticizer were prepared. The powder blend was roller compacted using a fixed roll-gap of 1.5 mm, feed screw speed to roller speed ratio of 5:1 and roll pressure of 4 MPa. The granules, after removing fines, were compacted into tablets on a Stokes B2 rotary tablet press at a compression force of 7 kN. The tablets were thermally treated at different temperatures (Room Temperature, 50, 75 and 100 °C) for 5 h. These tablets were scanned in reflectance mode in the wavelength range of 400-2500 nm and were evaluated for breaking force. Tablet breaking force significantly increased with increasing plasticizer levels and with increases in the sintering temperature. An increase in tablet hardness produced an upward shift (increase in absorbance) in the NIR spectra. The principle component analysis (PCA) of the spectra was able to distinguish samples with different plasticizer levels and sintering temperatures. In addition, a 9-factor partial least squares (PLS) regression model for tablets containing Eudragit® RL PO had an r(2) of 0.9797, a standard error of calibration of 0.6255 and a standard error of cross validation (SECV) of 0.7594. Similar analysis of tablets containing Eudragit® RS PO showed an r(2) of 0.9831, a standard error of calibration of 0.9711 and an SECV of 1.192.

  5. Characterization of silica particles prepared via urease-catalyzed urea hydrolysis and activity of urease in sol-gel silica matrix

    Energy Technology Data Exchange (ETDEWEB)

    Kato, Katsuya, E-mail: katsuya-kato@aist.go.jp [National Institute of Advanced Industrial Science and Technology (AIST), 2266-98 Anagahora, Shimoshidami, Moriyama-ku, Nagoya 463-8560 (Japan); Nishida, Masakazu [National Institute of Advanced Industrial Science and Technology (AIST), 2266-98 Anagahora, Shimoshidami, Moriyama-ku, Nagoya 463-8560 (Japan); Ito, Kimiyasu; Tomita, Masahiro [Division of Chemistry for Materials, Graduate School of Engineering, Mie University, 1577 Kurimamachiya-cho, Tsu, Mie 514-8570 (Japan)

    2012-12-01

    Highlights: Black-Right-Pointing-Pointer Silica precipitation occurred via urease-catalytic reactions. Black-Right-Pointing-Pointer Higher urease activity for silica synthesis enables mesostructure of silica-urease composites. Black-Right-Pointing-Pointer Urease encapsulating in silica matrix retained high activity. - Abstract: Urease templated precipitation of silica synthesized by sol-gel chemistry produces a composite material allowing high urease activity. This study investigates the structural properties of the composite material that allow for the retention of the urease hydrolysis activity. Scanning (SEM) and transmission (TEM) electron microscopy reveal that the composite has a mesoporous structure composed of closely packed spherical structures {approx}20-50 nm in diameter. Brunauer-Emmett-Teller (BET) analysis revealed that the surface area and pore volume of the composite prepared under the conditions of 50 mM urea and 25 Degree-Sign C is relatively high (324 m{sup 2}/g and 1.0 cm{sup 3}/g). These values are equivalent to those of usual mesoporous silica materials synthesized from the self-assembly of triblock copolymers as organic templates. In addition, after encapsulating in a sol-gel silica matrix, urease retained high activity ({approx}90% of the activity compared with native urease). Our results suggest a new method for synthesizing mesoporous silica materials with highly tunable pore sizes and shapes under mild conditions.

  6. The corrosion behaviour of the aluminum alloy 7075/SiCp metal matrix composite prepared by spray deposition

    Energy Technology Data Exchange (ETDEWEB)

    Cheng, Y.L.; Chen, Z.H.; Wu, H.L.; Wang, H.M. [College of Materials Science and Engineering, Hunan University, Changsha (China)

    2007-04-15

    Aluminum alloy 7075 and 7075/SiCp (MMC) were prepared by multi-layer spray deposition method and the corrosion behaviour of them were studied by electrochemical measurements to study the effect of the addition of silicon carbide on the corrosion behaviour of the MMC. The electrochemical noise result shows that the amplitude of the potential noise of the composite is lower than that of the spray deposited 7075 alloy. The potentiodynamic polarization curves results show that both the cathodic oxygen reduction current density and the anodic dissolution current density of the 7075/SiCp MMC are less than those of the 7075 alloy. Thus, the addition of SiC particles increases the corrosion resistance of the MMC. This may be due to that the microstructure of the spray deposited MMC is compact and SiC particles are nonmetallic material, the addition of it minimizes the real corrosion area of the alloy. (Abstract Copyright [2007], Wiley Periodicals, Inc.)

  7. Effects of spray-drying on w/o/w multiple emulsions prepared from a stearic acid matrix

    Directory of Open Access Journals (Sweden)

    Mlalila N

    2014-12-01

    Full Text Available Nichrous Mlalila,1 Hulda Swai,2 Lonji Kalombo,2 Askwar Hilonga3 1School of Life Sciences and Bioengineering, Nelson Mandela African Institution of Science and Technology, Arusha, Tanzania; 2Materials Science and Manufacturing, Council for Scientific and Industrial Research, Pretoria, South Africa; 3Department of Materials Science and Engineering, Nelson Mandela African Institution of Science and Technology, Arusha, Tanzania Abstract: The goal of this study was to explore the effects of spray-drying on w/o/w double emulsions of methyltestosterone (MT loaded in a stearic acid matrix. MT-loaded nanoparticles were formulated by a water-in-oil-in-water emulsion technique using 50, 75, and 100 mg of stearic acid, 2% and 3% w/v polyvinyl alcohol, 5% w/v lactose, and 0.2% w/v chitosan. The emulsions were immediately spray-dried based on an optimized model of inlet temperature and pump rate, and characterized for optimized responses with regard to particle size, polydispersity index, and zeta potential, for both emulsion and powder samples. Dynamic light scattering analysis shown that the nanoparticles increased in size with increasing concentrations of polyvinyl alcohol and stearic acid. Scanning electron microscopy indicated that the MT-loaded nanoparticles were spherical in shape, had a smooth surface, and were in an amorphous state, which was confirmed by differential scanning calorimetry. These MT-loaded nanoparticles are a promising candidate carrier for the delivery of MT; however, further studies are needed in order to establish the stability of the system and the cargo release profile under normal conditions of use. Keywords: double emulsions, nanoparticles, pump rate, spray-drying, testosterone

  8. Microstructure and property of sub-micro WC-10%Co particulate reinforced Cu matrix composites prepared by selective laser sintering

    Institute of Scientific and Technical Information of China (English)

    GU Dong-dong; SHEN Yi-fu; DAI Peng; YANG Ming-chuan

    2006-01-01

    The WC-10%Co particulate reinforced Cu matrix composite material with a WC-Co:Cu mass ratio of 20:80 was successfully fabricated by selective laser sintering(SLS) process. The following optimal processing parameters were used: laser power of 700 W, scan speed of 0.06 m/s, scan line spacing of 0.15 mm, and powder layer thickness of 0.3 mm. The microstructure,composition, and phase of the laser processed material were investigated by scanning electron microscopy(SEM), X-ray diffraction(XRD), and energy dispersive X-ray(EDX) spectroscopy. The results show that the bonding mechanism of this process is liquid phase sintering. The Cu and Co act as the binder phase, while the WC acts as the reinforcing phase. The non-equilibrium effects induced by laser melting, such as high degrees of undercooling and high solidification rate, result in the formation of a metastable phase CoC0.25. The WC reinforcing particulates typically have three kinds of morphology. They are agglomerated and undissolved, incompletely separated and partially dissolved, separated and dissolved, which indicates that particle rearrangement acts as the dominant sintering mechanism for the larger WC, while dissolution-precipitation prevails for the smaller WC particles.Microhardness tester was used to determine the Vickers hardness across the cross-section of the laser sintered sample, with the average value being HV0.1268.5. However, the hardness varied considerably, which might be attributed to the WC segregation and the high solidification rate experienced by the molten pool.

  9. DEVELOPMENT OF NEW TYPE ALUMINIUM OXIDE MATRIX CATALYST FOR PREPARATION OF SULFUR%新型氧化铝基制硫催化剂的研制

    Institute of Scientific and Technical Information of China (English)

    商剑峰; 刘爱华; 罗保军; 刘剑利

    2012-01-01

    The paper described the development, characterization and activity valuation of LS -02 new type aluminium oxide matrix catalyst for preparation of sulfur. The LS -02 catalyst was prepared by rotation shaping process and aluminium oxide as main raw material. Compared with LS -300 catalyst, the LS -02 catalyst possessed higher specific surface area, larger pore volume, more reasonable distribution of pore size and higher Claus and hydrolyzation reactivity. Comprehensive properties of the LS -02 catalyst reached foreign similar catalyst.%介绍了LS-02新型氧化铝制硫催化剂的研制、表征及活性评价。该催化剂以氧化铝为主要原料,采用转动成型工艺制备。该催化剂较LS-300催化剂具有更高的比表面积、更大的孔体积、更合理的孔分布及更高的克劳斯活性和水解活性,综合性能达到国外同类催化剂水平。

  10. Preparation of TiO2 photocatalyst with the matrix of palm wood (Arenga pinnata) waste in the photodegradation of batik wastewater

    Science.gov (United States)

    Kresnadipayana, Dian; Wahyuni, Endang Tri; Juari Santosa, Sri; Mudasir

    2017-01-01

    The study aimed to the preparation of TiO2 photocatalyst with the matrix from palm wood waste whose has lignin and cellulose content. TiO2 photocatalyst with the matrix from the wastewater of palm wood waste (TiO2/pww) was used as photocatalyst in photodegradation of batik wastewater. TiO2 solid was dissolved in ethanol and aquadest, added with the powder of wood palm waste and stirred with a magnetic stirrer for 16 hours. Then separation was carried out using buchner and filtrate and residue were obtained. The filtrate was disposed and the residue was calcined with various temperatures for 3 hours. The temperatures in this research were 100 °C (TiO2/pww-100); 200°C (TiO2/pww-200); 300°C (TiO2/pww-300). Analysis and characterization of TiO2/wwp were conducted using X-ray diffraction (XRD) and spectrophotometer Fourier Transform Infra Red (FTIR) methods. Photocalalytic TiO2/wwp use the batch system in a reactor with UV light 40 watts, 220 volts and length wave 360 nm the plate magnetic stirrer. Liquid waste batik adds TiO2/wwp with time variation. At XRD analysis showed that the preparation of TiO2/pww could be done on the heating TiO2/pww temperature of 100°C and 200°C. At the temperature of 300°C, it was indicated that the lignocelluloses in palm wood waste were burned, meaning that few lignocelluloses remained. The result of FTIR analysis showed clearly that at the temperature of 300°C, a few spectrum of lignocelluloses remained in palm wood waste, while at a temperature of 100°C and 200°C, spectra of lignocelluloses of palm wood waste remained. The result of photocatalysis test indicated that TiO2/pww could reduce 40%, 72%, 81% and 64% COD for TiO2 (control), TiO2/pww-100, TiO2/pww-200 and TiO2/pww-300, respectively.

  11. Improved sample preparation to determine acrylamide in difficult matrixes such as chocolate powder, cocoa, and coffee by liquid chromatography tandem mass spectroscopy.

    Science.gov (United States)

    Delatour, Thierry; Périsset, Adrienne; Goldmann, Till; Riediker, Sonja; Stadler, Richard H

    2004-07-28

    An improved sample preparation (extraction and cleanup) is presented that enables the quantification of low levels of acrylamide in difficult matrixes, including soluble chocolate powder, cocoa, coffee, and coffee surrogate. Final analysis is done by isotope-dilution liquid chromatography-electrospray ionization tandem mass spectrometry (LC-MS/MS) using d3-acrylamide as internal standard. Sample pretreatment essentially encompasses (a) protein precipitation with Carrez I and II solutions, (b) extraction of the analyte into ethyl acetate, and (c) solid-phase extraction on a Multimode cartridge. The stability of acrylamide in final extracts and in certain commercial foods and beverages is also reported. This approach provided good performance in terms of linearity, accuracy and precision. Full validation was conducted in soluble chocolate powder, achieving a decision limit (CCalpha) and detection capability (CCbeta) of 9.2 and 12.5 microg/kg, respectively. The method was extended to the analysis of acrylamide in various foodstuffs such as mashed potatoes, crisp bread, and butter biscuit and cookies. Furthermore, the accuracy of the method is demonstrated by the results obtained in three inter-laboratory proficiency tests.

  12. Preparation and performance of ZnO nanowires modified carbon fibers reinforced NiFe{sub 2}O{sub 4} ceramic matrix composite

    Energy Technology Data Exchange (ETDEWEB)

    Zhang, Lei, E-mail: jwlzl77@163.com; Jiao, Wanli

    2013-12-25

    Highlights: •Unlike existing chemical modification, the liquid growth remains fiber’s strength. •ZnO nanowires array are grown on carbon fibers with controllable morphology. •ZnO nanowires array modified carbon fibers can reinforce the strength of ceramic matrix composite. •This research will provide a means to produce multifunctional composites. -- Abstract: The surface of carbon fibers was modified by ZnO nanowires using the liquid growth method. NiFe{sub 2}O{sub 4} ceramic matrix composites reinforced by the modified carbon fibers were prepared by a high-temperature solid-state reaction method at 1300 °C for 5 h in N{sub 2} atmosphere. The influences of modified carbon fibers on the mechanical performances of NiFe{sub 2}O{sub 4} composites were investigated. The crystal structure of modified carbon fibers and the morphology of modified carbon fibers surface and the NiFe{sub 2}O{sub 4} composites fracture cross-section were observed by meaning of X-ray diffraction (XRD) and scanning electron microscope (SEM), respectively. The results showed that hexagonal wurtzite ZnO nanowires array grew from the surface of carbon fibers vertically, with nanowires diameters ranging from 170 nm to 380 nm and lengths up to 2.8 μm. Unlike existing chemical modification and high temperature oxidation method, the liquid growth allowed morphology control and maintained the single fiber tensile strength substantially unchanged under certain growth procedures. Compared to pure NiFe{sub 2}O{sub 4} ceramic and bare carbon fibers reinforced NiFe{sub 2}O{sub 4} composite, the bending strength of NiFe{sub 2}O{sub 4} composite reinforced with ZnO nanowires surface modified carbon fibers was shown to increase by up to 70% and 45%, respectively. The development of an interphase offering control over the morphology will provide a means to produce multifunctional composites.

  13. Efficient upconversion polymer-inorganic nanocomposite thin film emitters prepared by the double beam matrix assisted pulsed laser evaporation (DB-MAPLE)

    Science.gov (United States)

    Darwish, Abdalla M.; Burkett, Allan; Blackwell, Ashley; Taylor, Keylantra; Walker, Vernell; Sarkisov, Sergey; Koplitz, Brent

    2014-09-01

    We report on fabrication and investigation of optical and morphological properties of highly efficient (a quantum yield of 1%) upconversion polymer-inorganic nanocomposite thin film emitters prepared by the new technique of double beam matrix assisted pulsed laser evaporation (DB-MAPLE). Polymer poly(methyl methacrylate) (PMMA) host was evaporated on a silicon substrate using a 1064-nm pulsed laser beam using a target made of frozen (to the temperature of liquid nitrogen) solution of PMMA in chlorobenzene. Concurrently, the second 532-nm pulsed beam from the same laser was used to impregnate the polymer host with the inorganic nanoparticulate made of the rare earth upconversion compounds NaYF4: Yb3+, Er3+, NaYF4: Yb3+, Ho3+, and NaYF4: Yb3+, Tm3+. The compounds were initially synthesized using the wet process, baked, and compressed in solid pellet targets. The proposed DB-MAPLE method has the advantage of making highly homogeneous nanocomposite films with precise control of the doping rate due to the optimized overlapping of the plumes produced by the ablation of the organic and inorganic target with the infrared and visible laser beams respectively. X-ray diffraction, electron and atomic force microscopy, and optical fluorescence spectroscopy indicated that the inorganic nanoparticulate preserved its crystalline structure and upconversion properties (strong emission in green, red, and blue bands upon illumination with 980-nm laser diode) after being transferred from the target in the polymer nanocomposite film. The produced films can be used in applications varying from the efficiency enhancement of the photovoltaic cells, optical sensors and biomarkers to anti-counterfeit labels.

  14. First steps towards a generic sample preparation scheme for inorganic engineered nanoparticles in a complex matrix for detection, characterization, and quantification by asymmetric flow-field flow fractionation coupled to multi-angle light scattering and ICP-MS

    DEFF Research Database (Denmark)

    Wagner, Stephan; Legros, Samuel; Löschner, Katrin

    2015-01-01

    The applicability of a multi-step generic procedure to systematically develop sample preparation methods for the detection, characterization, and quantification of inorganic engineered nanoparticles (ENPs) in a complex matrix was successfully demonstrated. The research focused on the optimization...... content by asymmetric flow-field flow fractionation coupled to a multi-angle light scattering detector and an inductively coupled plasma mass spectrometer. Following the proposed generic procedure SiO2-ENPs were separated from a tomato soup. Two potential sample preparation methods were tested these being...

  15. Preparation and electrochemical characterization of polyvinylchloride/ FeTiO{sub 3}-co-Fe{sub 3}O{sub 4} nanoparticles mixed matrix ion exchange membranes: Investigation of concentration and pH effects

    Energy Technology Data Exchange (ETDEWEB)

    Hosseini, Sayedmohsen; Hamidi, Alireza; Moghadassi, Abdolreza; Parvizian, Fahime [Faculty of Engineering, Arak University, Arak (Iran, Islamic Republic of); Madaeni, Sayed Siavash [Faculty of Engineering, Razi University, Kermanshah (Iran, Islamic Republic of)

    2015-09-15

    Polyvinyl chloride based/FeTiO{sub 3}-co-Fe{sub 3}O{sub 4} nanoparticles mixed matrix heterogeneous cation exchange membranes were prepared by solution casting technique. The effect of using filler additives in casting solution and also electrolyte concentration and pH on electrochemical properties of membrane was studied. Membrane potential, transport number and selectivity were improved by using FeTiO{sub 3}/Fe{sub 3}O{sub 4} nanoparticles in membrane matrix. Utilizing FeTiO{sub 3}/ Fe{sub 3}O{sub 4} nanoparticles in membrane matrix also led to improvement of membrane ionic flux from 2.95*10{sup -5} to 4.15*10{sup -5} (mol/m{sup 2}·s) obviously. Similar trend was also found for membrane electrical conductivity. Moreover, the transport number, selectivity and membrane electrical conductivity were enhanced by increase of electrolyte concentration. Prepared membranes exhibited higher transport number/selectivity at pH 7 compared to other pH values. Obtained results showed that the membrane electrical resistance decreased initially by increase of electrolyte pH sharply and then began to increase. Membranes exhibited lower selectivity for bivalent ions compared to monovalent type. Modified membranes containing FeTiO{sub 3}/Fe{sub 3}O{sub 4} nanoparticles showed more appropriate electrochemical properties compared to other prepared membranes.

  16. Graphite supported preparation (GSP) of α-cyano-4-hydroxycinnamic acid (CHCA) for matrix-assisted laser desorption/ionization mass spectrometry (MALDI-MS) for peptides and proteins.

    Science.gov (United States)

    Gorka, Jan; Bahr, Ute; Karas, Michael

    2012-11-01

    Graphite as MALDI matrix or in combination with other substances has been reported in recent years. Here, we demonstrate that graphite can be used as target coating supporting the crystallization of the α-cyano-4-hydroxycinnamic acid matrix. A conventional dried-droplet preparation of matrix and analyte solution on a graphite-coated metal target leads to a thin, uniform layer of cubic crystals with about 1 μm edge length. Commercially available graphite powder of 1-2 μm particle size is gently wiped over the target using a cotton Q-tip, leading to an ultra-thin, not-visible film. This surface modification considerably improves analysis of peptides and proteins for MALDI MS using conventional dried-droplet preparation. Compared with untreated targets, the signal intensities of standard peptides are up to eight times higher when using the graphite supported crystallization. The relative standard deviation in peak area of angiotensin II for sample amounts between 1 and 50 fmol is reduced to about 15 % compared with 45 % for untreated sample holders. For a quantification of 1 fmol of the peptide using an internal standard the coefficient of variation is reduced to 3.5 % from 8 %. The new graphite supported preparation (GSP) protocol is very simple and does not require any technical nor manual skills. All standard solvents for peptides and proteins can be used.

  17. Preparation and in vitro Drug Release of Betahistine Dihydrochloride Sustained-release Matrix Tablets%盐酸倍他司汀缓释骨架片的制备及体外释药特性研究

    Institute of Scientific and Technical Information of China (English)

    李凯; 陈鹰; 柴俊; 熊运; 熊姣

    2014-01-01

    目的::制备盐酸倍他司汀缓释骨架片。方法:采用亲水性高分子材料HPMC为骨架,制备盐酸倍他司汀缓释片,并用单因素试验考察其释药特征。正交试验优化处方工艺。结果:以60% HPMC K15M为骨架材料,磷酸氢钙为填充剂,用10%PVP的90%乙醇溶液为黏合剂,湿法制粒压片为最佳工艺,片重为500 mg。药物体外释放接近Higuchi模型,能实现药物12 h内缓慢释放。结论:本品制备工艺简便,具有缓解特性。%Objective: To prepare betahistine dihydrochloride sustained-release matrix tablets. Methods: The tablets were pre-pared with water soluble HPMC matrix, and the release behaviors were investigated by single factor study. The formula and preparation procedures were optimized by orthogonal design. Results:The optimal technology was as follows:using 60% HPMC K15M as the ma-trix material, calcium hydrogen phosphate as the filler, 10% PVP in 90% alcohol as the bonding agent;wet granulation compression technique was used to prepare the tablets with the tablet weight of 500mg. The in vitro drug release fits a Higuchi equation and the drug can be sustained-released within 12 h. Conclusion:The preparation technology is simple and the tablets have sustainol release behav-ior.

  18. Preparation and luminescence properties of europium complex with a-naphthylacetic acid incorporated in silica matrix by sol-gel method

    Institute of Scientific and Technical Information of China (English)

    陈野; 蔡伟民; 孙晓君; 崔丹; 于英宁

    2004-01-01

    Europium ternary complex of Eu (NNA)3(NNA=o-naphthylacetic acid) was embedded in silica matrix at different ratios by sol-gel method. The luminescence properties of silica composites were studied by comparing them with those of corresponding pure complex by means of excitation, emission spectra and lifetimes. The fluorescence lifetime was prolonged when the pure complex was incorporated in silica matrix. The relative fluorescence intensity and fluorescence lifetimes increased simultaneously with the increase of Eu(NNA)3.

  19. Preparation of explosive nanoparticles in a porous chromium(III) oxide matrix: a first attempt to control the reactivity of explosives

    Energy Technology Data Exchange (ETDEWEB)

    Comet, M; Siegert, B; Pichot, V; Gibot, P; Spitzer, D [Laboratoire ISL/CNRS ' Nanomateriaux pour les Systemes Sous Sollicitations Extremes' (NS3E), FRE 3026, French-German Research Institute of Saint-Louis (ISL), 5 rue du General Cassagnou, 68301 Saint-Louis (France)], E-mail: comet@isl.tm.fr

    2008-07-16

    This paper reports the first attempt to control the combustion and the detonation properties of a high explosive through its structure. A porous chromium(III) oxide matrix produced by the combustion of ammonium dichromate was infiltrated by hexahydro-1,3,5-trinitro-1,3,5-triazine (RDX). The structure of the Cr{sub 2}O{sub 3} matrix was studied by both scanning and transmission electron microscopy (SEM, TEM); the Cr{sub 2}O{sub 3}/RDX nanocomposites were characterized by nitrogen adsorption. A mathematical model based on these techniques was used to demonstrate that the Cr{sub 2}O{sub 3} matrix encloses and stabilizes RDX particles at the nanoscale. The decomposition process of the nanocomposites was investigated by atomic force microscopy (AFM). The reactivity and sensitivity of the nanocomposites were studied by impact and friction tests, differential scanning calorimetry (DSC), time-resolved cinematography and detonation experiments, and were correlated with their structure. The size of RDX nanoparticles and their distribution in the Cr{sub 2}O{sub 3} matrix have an important influence on their reactivity. The reactive properties of nanostructured RDX differ significantly from those of classical micron-sized RDX. For instance, the melting point disappears and the decomposition temperature is significantly lowered. The quantization of the explosive particles in the Cr{sub 2}O{sub 3} matrix decreases the sensitivity to mechanical stress and allows controlling the decomposition mode-i.e. combustion versus detonation.

  20. Preparation of explosive nanoparticles in a porous chromium(III) oxide matrix: a first attempt to control the reactivity of explosives

    Science.gov (United States)

    Comet, M.; Siegert, B.; Pichot, V.; Gibot, P.; Spitzer, D.

    2008-07-01

    This paper reports the first attempt to control the combustion and the detonation properties of a high explosive through its structure. A porous chromium(III) oxide matrix produced by the combustion of ammonium dichromate was infiltrated by hexahydro-1,3,5-trinitro-1,3,5-triazine (RDX). The structure of the Cr2O3 matrix was studied by both scanning and transmission electron microscopy (SEM, TEM); the Cr2O3/RDX nanocomposites were characterized by nitrogen adsorption. A mathematical model based on these techniques was used to demonstrate that the Cr2O3 matrix encloses and stabilizes RDX particles at the nanoscale. The decomposition process of the nanocomposites was investigated by atomic force microscopy (AFM). The reactivity and sensitivity of the nanocomposites were studied by impact and friction tests, differential scanning calorimetry (DSC), time-resolved cinematography and detonation experiments, and were correlated with their structure. The size of RDX nanoparticles and their distribution in the Cr2O3 matrix have an important influence on their reactivity. The reactive properties of nanostructured RDX differ significantly from those of classical micron-sized RDX. For instance, the melting point disappears and the decomposition temperature is significantly lowered. The quantization of the explosive particles in the Cr2O3 matrix decreases the sensitivity to mechanical stress and allows controlling the decomposition mode—i.e. combustion versus detonation.

  1. Matrix theory

    CERN Document Server

    Franklin, Joel N

    2003-01-01

    Mathematically rigorous introduction covers vector and matrix norms, the condition-number of a matrix, positive and irreducible matrices, much more. Only elementary algebra and calculus required. Includes problem-solving exercises. 1968 edition.

  2. Preparation of diclofenac potassium sustained-release matrix pellets by extrusion-spheronization technique%挤出-滚圆法制备凝胶骨架型双氯芬酸钾缓释微丸

    Institute of Scientific and Technical Information of China (English)

    金庆平

    2014-01-01

    目的 采用挤出滚圆法制备出稳定性良好的双氯芬酸钾缓释微丸.方法 通过挤出滚圆法制备双氯芬酸钾缓释微丸.以制剂体外释放度及加速试验中制剂稳定性为指标,筛选了骨架剂的种类和卡波姆974P用量等影响因素.结果 以卡波姆974P为凝胶型骨架剂,载药量为25%(w)时,制备微丸的释放度符合日本药典标准(0.5h释放20 ~45% (w),2h释放40~70% (w),8h释放70%(w)以上).结论 成功地制备了双氯芬酸钾凝胶骨架型缓释微丸,该制备工艺重现性好,具有理想的缓释效果,加速试验稳定性良好.%Objective To investigate the preparation and storage stability of the diclofenac potassium matrix sustained release pellets by extrusion-spheronization.Methods The diclofenac potassium pellets was prepared by extrusion-spheronization process.The release properties and storage stability of the preparation were investigated to screen the best vehicle and some of the influence factors such as dosage of Carbopol 974P were also be selected.Results The release profiles of diclofenac potassium sustained-release matrix pellets followed Ritger-Peppas equation and the stability of the preparation was satisfactory.Conclusions The preparation technology is reliable and the quality is controllable.

  3. Study of polymeric nanocomposites prepared by inserting graphene and / or Ag, Au and ZnO nanoparticles in a TEGDA polymer matrix, by means of the use of dielectric spectroscopy

    Directory of Open Access Journals (Sweden)

    Valeria Alzari

    2016-03-01

    Full Text Available Polymeric nanocomposites were prepared by inserting graphene and/or Ag, Au and ZnO nanoparticles in a TEGDA (tetraethyleneglycol diacrylate polymer matrix. The polymeric films were characterized in terms of their dielectric properties by electrochemical impedance spectroscopy. The impedance data were fitted by generalized relaxation functions in order to determine conductivity, dielectric response and molecular relaxation time of the nanocomposite films. In particular, a stretched exponential function, Kohlrausch-Williams-Watts function (KWW, was used to investigate polymer/graphene/metal nanocomposites.

  4. [INFLUENCE OF HYPERICUM PERFORATUM L. HERB POLYPHENOLS PREPARATION WITH MINERALS ON THE STATE OF PERIODONTAL CONNECTIVE TISSUE MATRIX OF RATS IN CONDITION OF PERIODONTITIS MODELING].

    Science.gov (United States)

    Kosenko, K N; Nikolaeva, A V; Tkachenko, E K; Novosel'skaia, N G

    2014-01-01

    In experiments on 22 white 1.5-month-old rats-males there were studied influence of Hypericum perforatum L. and minerales from Dyovit® on periodont's tissues under periodontits modelling. Examined preparation normalizes level of glicosaminoglicanes in gum, but did not completely show protective effects relative to collagen's fraction. In periodont's bone preparation decreases resorbrtion; increases activity of AlP and in the same time normalizes activity of AcP.

  5. On the Role of Processing Parameters in Producing Recycled Aluminum AA6061 Based Metal Matrix Composite (MMC-AlR) Prepared Using Hot Press Forging (HPF) Process

    Science.gov (United States)

    Ahmad, Azlan; Lajis, Mohd Amri

    2017-01-01

    Solid-state recycling, which involves the direct recycling of scrap metal into bulk material using severe plastic deformation, has emerged as a potential alternative to the conventional remelting and recycling techniques. Hot press forging has been identified as a sustainable direct recycling technique that has fewer steps and maintains excellent material performance. An experimental investigation was conducted to explore the hardness and density of a recycled aluminum-based metal matrix composite by varying operating temperature and holding time. A mixture of recycled aluminum, AA6061, and aluminum oxide were simultaneously heated to 430, 480, and 530 °C and forged for 60, 90, and 120 min. We found a positive increase in microhardness and density for all composites. The hardness increased approximately 33.85%, while density improved by about 15.25% whenever the temperature or the holding time were increased. Based on qualitative analysis, the composite endures substantial plastic deformation due to the presence of hardness properties due to the aluminum oxide embedded in the aluminum matrix. These increases were significantly affected by the operating temperature; the holding time also had a subordinate role in enhancing the metal matrix composite properties. Furthermore, in an effort to curb the shortage of primary resources, this study reviewed the promising performance of secondary resources produced by using recycled aluminum and aluminum oxide as the base matrix and reinforcement constituent, respectively. This study is an outline for machining practitioners and the manufacturing industry to help increase industry sustainability with the aim of preserving the Earth for our community in the future. PMID:28925963

  6. 无压浸渗制备Al/SiCp陶瓷基复合材料研究%Study on Pressureless Infiltration Preparation of Al/SiCp Ceramic Matrix Composites

    Institute of Scientific and Technical Information of China (English)

    徐跃; 高霖; 崔崇; 钱凤

    2011-01-01

    The present paper studied the effects of Mg、Si and infiltration time on the preparation and microstructure of Al/SiCp ceramic matrix composites prepared by pressureless infiltration.Increasing fluidity of aluminum alloy liquid, improving the infiltration ability between aluminum alloy and SiC and avoiding the formation of bad Al4C3 on interface were important factors in assuring the scientific preparation of composites.Result indicated that two hours holding of infiltration and aluminum alloy containing 10(wt)% Mg and 15(wt)% Si could infiltrate fully with higher density,which was better technology parameters in preparing Al/SiCp ceramic matrix composites.%采用无压浸渗法,研究Mg、Si、浸渗时间时Al/SiCp陶瓷基复合材料制备及组织的影响.增加铝合金液的流动性,提高铝液同SiC之间的浸润性,防止有害ALC3界面形成,是保证复合材料科学制备的重要因素.研究结果表明,2h保温时间、10%Mg和15%Si铝合金液的实验参数制备的Al/SiCp复合材料浸渗充分,组织致密化程度高,是无压浸渗制备复合材料较好的参数.

  7. Culture conditions and sample preparation methods affect spectrum quality and reproducibility during profiling of Staphylococcus aureus with matrix-assisted laser desorption/ionization time-of-flight mass spectrometry.

    Science.gov (United States)

    Goldstein, J E; Zhang, L; Borror, C M; Rago, J V; Sandrin, T R

    2013-08-01

    Matrix-assisted laser desorption/ionization time-of-flight mass spectrometry (MALDI-TOF MS) has emerged as a promising tool to rapidly characterize Staphylococcus aureus. Different protocols have been employed, but effects of experimental factors, such as culture condition and sample preparation, on spectrum quality and reproducibility have not been rigorously examined. We applied MALDI-TOF MS to characterize a model system consisting of five methicillin-sensitive (MSSA) and five methicillin-resistant S. aureus isolates (MRSA) under two culture conditions (agar and broth) and using two sample preparation methods [intact cell method and protein extraction method (PEM)]. The effects of these treatments on spectrum quality and reproducibility were quantified. PEM facilitated increases in the number of peaks and mass range width. Broth cultures further improved spectrum quality in terms of increasing the number of peaks. In addition, PEM increased reproducibility in samples prepared using identical culture conditions. MALDI imaging data suggested that the improvement in reproducibility may result from a more homogeneous distribution of sample associated with the broth/PEM treatment. Broth/PEM treatment also yielded the highest rate (96%) of correct classification for MRSA. Taken together, these results suggest that broth/PEM maximizes the performance of MALDI-TOF MS to characterize S. aureus. Two culture conditions (agar or broth) and two sample preparation methods (intact cell or protein extraction) were evaluated for their effects on profiling of Staphylococcus aureus using matrix-assisted laser desorption/ionization time-of-flight mass spectrometry (MALDI-TOF MS). Results indicated that MALDI-enabled profiling of S. aureus is most effective when cultures are grown in broth and processed using a protein extraction-based approach. These findings should enhance future efforts to maximize the performance of this approach to characterize strains of S. aureus. © 2013

  8. Matrix Factorization and Matrix Concentration

    OpenAIRE

    Mackey, Lester

    2012-01-01

    Motivated by the constrained factorization problems of sparse principal components analysis (PCA) for gene expression modeling, low-rank matrix completion for recommender systems, and robust matrix factorization for video surveillance, this dissertation explores the modeling, methodology, and theory of matrix factorization.We begin by exposing the theoretical and empirical shortcomings of standard deflation techniques for sparse PCA and developing alternative methodology more suitable for def...

  9. Rheocasting Al Matrix Composites

    Science.gov (United States)

    Girot, F. A.; Albingre, L.; Quenisset, J. M.; Naslain, R.

    1987-11-01

    Aluminum alloy matrix composites reinforced by SiC short fibers (or whiskers) can be prepared by rheocasting, a process which consists of the incorporation and homogeneous distribution of the reinforcement by stirring within a semi-solid alloy. Using this technique, composites containing fiber volume fractions in the range of 8-15%, have been obtained for various fibers lengths (i.e., 1 mm, 3 mm and 6 mm for SiC fibers). This paper attempts to delineate the best compocasting conditions for aluminum matrix composites reinforced by short SiC (e.g Nicalon) or SiC whiskers (e.g., Tokamax) and characterize the resulting microstructures.

  10. Preparation of [(68)Ga]PSMA-11 for PET-CT imaging using a manual synthesis module and organic matrix based (68)Ge/(68)Ga generator.

    Science.gov (United States)

    Nanabala, Raviteja; Anees, Muhammed K; Sasikumar, Arun; Joy, Ajith; Pillai, M R A

    2016-08-01

    [(68)Ga]PSMA-11 is a relatively recently introduced radiopharmaceutical for PET-CT imaging of prostate cancer patients. The availability of (68)Ge/(68)Ga generator and PSMA-11 ligand from commercial sources is facilitating the production of the radiopharmaceutical in-house. This paper describes our experience on the preparation of ~200 batches of [(68)Ga]PSMA-11 for conducting PET-CT imaging in patients suspected/suffering from prostate cancer. The radiosynthesis of [(68)Ga]PSMA-11 was done in a hospital based nuclear medicine department using (68)Ge/(68)Ga generator and a manual synthesis module, both supplied by Isotope Technologies Garching (ITG), Germany. The production involved the reaction of 5μg (5.3nmol) of PSMA-11 ligand in 1 ml of 0.25M sodium acetate buffer with 4ml of (68)GaCl3 in 0.05M HCl for 5min at 105°C; followed by purification in a C18 cartridge and collection through a 0.22μm pore size filter. The radiochemical yields obtained were consistently high, 93.19%±3.76%, and there was hardly any batch failure. The radiochemical purity of the product was >99% and the product was stable for over 2h; however it was used in patients immediately after preparation. About 200 batches of [(68)Ga]PSMA-11 were prepared during the period and more than 300 patients received the tracer during the 14months of study. No adverse reaction was observed in any of the patients and the image qualities were consistent with literature reports. [(68)Ga]PSMA-11 with high radiochemical and radionuclidic purity is conveniently prepared by using a (68)Ge/(68)Ga generator and manual synthesis module. The radiochemical yields are very high; and activity sufficient for 3-4 patients can be prepared in a single batch; multiple batches can be done on the same day and when needed after a gap of 1.5-2h. Copyright © 2016 Elsevier Inc. All rights reserved.

  11. Preparation of an apatite-based matrix for the confinement of iodine 129; Mise au point d`une matrice apatitique pour le confinement de l`iode 129

    Energy Technology Data Exchange (ETDEWEB)

    Audubert, F.

    1995-11-08

    The aim of this thesis is the study of the conditioning of iodine 129 from the reprocessing of nuclear wastes. Because of its long half life (1.57 10{sup 7} years), the conditioning of iodine 129 requires a matrix stable during several thousands of years. The study of natural minerals allows the selection of mineral phases having a good long term behaviour. In the first part the policy of nuclear wastes management, and in particular of iodine, is recalled. A naturalistic approach is used to define the best conditioning material and the remarkable properties of apatite in this way are described. In the second part, the preparation and physical-chemical characterization of iodo-apatites are described. A demonstration is made that iodine can penetrate inside vanadate or lead phospho-vanadate apatite-based compounds. The third part deals with the preparation of the conditioning material. The sintering reaction under pressure allows the preparation of composite ceramics including iodo-apatite. A multi-layer coating process is defined: coating of PbI{sub 2} with a Pb{sub 3}(VO{sub 4}){sub 1.6}(PO{sub 4}){sub 0.4} layer and a Ca{sub 10}(PO{sub 4}){sub 6}F{sub 2} layer. Sintering is performed at 700 deg. celsius under a 25 MPa pressure. (J.S.). 131 refs.

  12. Matrix calculus

    CERN Document Server

    Bodewig, E

    1959-01-01

    Matrix Calculus, Second Revised and Enlarged Edition focuses on systematic calculation with the building blocks of a matrix and rows and columns, shunning the use of individual elements. The publication first offers information on vectors, matrices, further applications, measures of the magnitude of a matrix, and forms. The text then examines eigenvalues and exact solutions, including the characteristic equation, eigenrows, extremum properties of the eigenvalues, bounds for the eigenvalues, elementary divisors, and bounds for the determinant. The text ponders on approximate solutions, as well

  13. Preparation of Iron Matrix Composite Reinforced by In-situ Al203 Particles%自生氧化铝颗粒增强铁基复合材料的制备

    Institute of Scientific and Technical Information of China (English)

    周玉成; 魏世忠; 王利敏; 徐流杰

    2011-01-01

    Ethanol was used as reaction media, the ammonia was slowly dropped, constantly stirring into aluminum nitrate ethanol solution to neutralize. By washing with ethanol, filtering and drying, some aluminum hydroxide was obtained. Aluminum hydroxide powder and iron powder, in a certain proportion, were fully mixed. By pressing and sintering, iron matrix composite reinforced with in-situ A12O3 particle was prepared.%采用乙醇作为反应介质,将氨水滴入硝酸铝乙醇溶液中进行中和反应,经洗涤、过滤和烘干后得到氢氧化铝超细粉.将制得的超细氢氧化铝粉与铁粉按一定比例充分混合,经压制、烧结制得氧化铝颗粒增强铁基复合材料.

  14. 壳聚糖锌离子固定化亲和层析填料的制备与性质%Preparation and Properties of Chitosan Immobilized Zinc Ion Affinity Chromatography Matrix

    Institute of Scientific and Technical Information of China (English)

    包海生; 高秀峰; 郑雪妮; 李永生

    2012-01-01

    Purpose:Chitosan immobilized zinc ion affinity chromatography matrixes were prepared,and its properties were studied. Methods: Immobilized metal affinity chromatography (IMAC ) matrixes were successfully prepared with cross-linked chitosan prepared by reverse phase suspension polymerization, and 3-Chloro-l ,2-epoxypropane as activated agent, ethylenediamine as chelating ligand and Zn2* as center ions. Its effective grain size and uniformity coefficient,moisture content,rate of lostmass, amino content,skeletaldensity,bulk density and porosity were characterized. Time,concentration of ZnCl2solution,temperature,pH of Zn * immobilized conditions were optimized to determine the amount of Zn immobilized. After purifying with salting out, aldehyde dehydrogenase containing a histidine-tag was used to examine the affinity of chitosan immobilized Zn + affinity chromatography matrix. Results;the effective grain size,uniformity coefficient,moisture content,rate of lostmass, amino content, skeletaldensity, bulk density and porosity of the prepared matrix is 105pirn, 1. 46,58. 03% , 85.43% ,9.20 mmol/g, 1.2178 g/ml, 0.8432 g/ml and 36.40% respectively. The optimum conditions of Zn2 + immobilized were;time 3h,ZnCl2concentration 0.1 mol / L,temperature 28T ,pH 5.5. And the amount of Zn2 + immobilized is 3.35 mmol/g under these optimum conditions. The affinity of chitosan immobilized zinc ion affinity chromatography matrix for aldehyde dehydrogenase is 4. 14 IU/g(dry weight). Conclusions; The high-efficiency chitosan immobilized zinc ion affinity chromatography matrixes were prepared, and it can be used for quickly separating and purifying the recombinant protein containing a His-tag.%目的:制备了壳聚糖Zn2+固定化亲和层析填料,并对其性能进行了研究.方法:采用反相悬浮法制备了交联壳聚糖;再以环氧氯丙烷为活化剂,乙二胺为螯合配基,制备了固定化亲和层析填料;表征了其有效粒径以及均匀系数、含水量、失

  15. PREPARATION AND CHARACTERIZATION OF CO-PROCESSED EXCIPIENT-PREGELATINIZED CASSAVA STARCH PROPIONATE AS A MATRIX IN THE GASTRORETENTIVE DOSAGE FORM

    Directory of Open Access Journals (Sweden)

    Junaedi

    2011-11-01

    Full Text Available The gastroretentive dosage form is designed to prolong the gastric residence time of the drug delivery system whichalso results in the development of an appropriate excipient. The purpose of this study is to develop and characterize coprocessedexcipient made from carrageenan (kappa-iota = 1:1 and pregelatinized cassava starch propionate (PCSP inratios of 1:1, 1:2, and 1:3. PCSP was prepared with propionic anhydride in an aqueous medium. The product was mixedwith carrageenan (kappa-iota = 1:1, as well as characterized physicochemical and functional properties. The coprocessedexcipient was then used as a mucoadhesive granule and floating tablet. The USP Basket was selected toperform the dissolution test of the granules in HCl buffer (pH 1.2 and distilled water for 8 hours each. Mucoadhesiveproperties were evaluated using bioadhesive through a vitro test and wash-off test. As for the floating tablet, the USPPaddle was selected to perform the dissolution test of the tablets in 0.1 N HCl for 10 hours. The floating lag time andfloating time were tested in 0.1 N HCl for 24 hours. The result of these studies indicated that co-processed excipientcarrageenan-PCSP can retard dosage form in gastric and drug controlled release, thus making it a suitable material forthe gastroretentive dosage form.

  16. PREPARATION AND BIOCOMPATIBILITY OF PORCINE SKELETAL MUSCLE ACELLULAR MATRIX FOR ADIPOSE TISSUE ENGINEERING%骨骼肌无细胞基质的制备及其生物相容性研究

    Institute of Scientific and Technical Information of China (English)

    田春祥; 范雪娇; 陈晓禾; 邓力; 秦廷武; 罗静聪; 李秀群; 吕青

    2012-01-01

    Objective Extracellular matrix is one of the focus researches of the adipose tissue engineering. To investigate the appropriate method to prepare the porcine skeletal muscle acellular matrix and to evaluate the biocompatibility of the matrix. Methods The fresh skeletal muscle tissues were harvested from healthy adult porcine and were sliced into 2-3 mm thick sheets, which were treated by hypotonic-detergent method to remove the cells from the tissue. The matrix was then examined by histology, immunohistochemistry, and scanning electron microscopy. The toxic effects of the matrix were tested by MTT. Human adipose-derived stem cells (hADSCs) were isolated from adipose tissue donated by patients with breast cancer, and identified by morphology, flow cytometry, and differentiation ability. Then, hADSCs of passage 3 were seeded into the skeletal muscle acellular matrix, and cultured in the medium. The cellular behavior was assessed by calcein-AM (CA) and propidium iodide (PI) staining at 1st, 3rd, 5th, and 7th days after culturing. Results Histology, immunohistochemistry, and scanning electron microscopy showed that the muscle fibers were removed completely with the basement membrane structure; a large number of collagenous matrix presented as regular network, porous-like structure. The cytotoxicity score of the matrix was grade 1, which meant that the matrix had good cytocompatibil ity. The CA and PI staining showed the seeded hADSCs had the potential of spread and proliferation on the matrix. Conclusion Porcine skeletal muscle acellular matrix has good biocompatibility and a potential to be used as an ideal biomaterial scaffold for adipose tissue engineering.%目的 细胞外基质是脂肪组织工程材料的研究热点之一.通过探讨骨骼肌无细胞基质的制作方法及生物相容性,为其在脂肪组织工程中的应用奠定基础. 方法 取健康成年小香猪新鲜骨骼肌组织,横切成厚2~3mm的组织块,采用低渗-去垢剂法脱细胞

  17. Matrix Thermalization

    CERN Document Server

    Craps, Ben; Nguyen, Kévin

    2016-01-01

    Matrix quantum mechanics offers an attractive environment for discussing gravitational holography, in which both sides of the holographic duality are well-defined. Similarly to higher-dimensional implementations of holography, collapsing shell solutions in the gravitational bulk correspond in this setting to thermalization processes in the dual quantum mechanical theory. We construct an explicit, fully nonlinear supergravity solution describing a generic collapsing dilaton shell, specify the holographic renormalization prescriptions necessary for computing the relevant boundary observables, and apply them to evaluating thermalizing two-point correlation functions in the dual matrix theory.

  18. Preparation of magnetic graphene/mesoporous silica composites with phenyl-functionalized pore-walls as the restricted access matrix solid phase extraction adsorbent for the rapid extraction of parabens from water-based skin toners.

    Science.gov (United States)

    Feng, Jianan; He, Xinying; Liu, Xiaodan; Sun, Xueni; Li, Yan

    2016-09-23

    In this work, phenyl-functionalized magnetic graphene/mesoporous silica composites (MG-mSiO2-Ph) were prepared and applied as restricted access matrix solid phase extraction (RAM-SPE) adsorbents to determine the parabens in commercially available retail cosmetics. MG-mSiO2-Ph composites were synthesized by a surfactant-mediated co-condensation reaction in which mesoporous silica with phenyl-functionalized pore-walls was coated on a magnetic graphene sheet. The obtained nano-composites were proven to be of sufficient quality for an ideal RAM-SPE adsorbent with a large specific surface area of 369m(2)g(-1), uniform mesopores of 2.8nm, and special phenyl-functionalized pore-walls. Parabens, such as methyl paraben, ethyl paraben and propyl paraben, were extracted from water-based skin toners using one step of the RAM-SPE and were then analysed by a HPLC-DAD system. The SPE conditions were optimized by studying the parameters, such as the adsorbent amount, elution solvent type, adsorption time and desorption time, that influence the extraction efficiency. For each analyte, there were good linearities of approximately 0.10-120μgmL(-1) with determination coefficients (R(2))>0.995. The sensitivity was as low as 0.01-0.025μgmL(-1) for the LOD, and the percent recoveries were 98.37-105.84%. The intra-day and inter-day RSDs were 1.44-6.11% (n=6) and 3.12-11.70% (n=6), respectively. The results indicated that this method with novel RAM-SPE adsorbents is sensitive and convenient. The results also offered an attractive alternative for the extraction and determination of paraben preservatives in a complex matrix, such as cosmetics. Copyright © 2016 Elsevier B.V. All rights reserved.

  19. 异种(猪)无细胞真皮基质的制备及体外生物相容性%Preparation and in vitro biocompatibility of xenogenic(porcine)acellular dermal matrix

    Institute of Scientific and Technical Information of China (English)

    马绍英; 李宝明; 董丽; 王旭昇; 李宝兴; 赵亚平; 康悦

    2009-01-01

    背景:人同种无细胞真皮基质作为一种永久性真皮支架,已成功应用于烧伤创面修复及美容医学等领域,但由于来源有限,限制了其应用.目的;研制异种(猪)无细胞真皮基质,并对其体外生物相容性进行评价.设计、时间及地点:体外细胞学对比观察实验,于2007-08/2008-06在中国辐射防护研究院生物材料与制药技术研究所实验室完成.材料:实验猪由中国辐射防护研究院实验动物中心提供;人成纤维细胞来自武警山西总队医院健康儿童包皮环切术切除的包皮组织.方法:无菌条件下获取健康小白猪猪皮,用高渗盐溶液-去污剂、胰酶消化及超声清洗的方法,制备猪无细胞真皮基质.体外培养人成纤维细胞,用猪无细胞真皮基质浸提液法及人成纤维细胞和猪无细胞真皮基质直接贴附法,评价猪无细胞真皮基质体外生物相容性.主要观察指标:①猪无细胞真皮基质的组织学形态.②猪无细胞真皮基质的体外生物相容性.结果:制备的猪无细胞真皮基质,完全去除了表皮和真皮中的细胞成分,保留了胶原基质.猪无细胞真皮基质浸提液对人成纤维细胞增殖无明显影响.人成纤维细胞可以在猪无细胞真皮基质上贴附、增殖.结论:此种方法制备的无细胞真皮基质完全去除了表皮和真皮中的细胞成分,有较好的体外生物相容性.%BACKGROUND: Human allogenic acellular dermal matrix, as a kind of permanent dermal scaffold, has widely used in the fields of burn wound reparation and aesthetic medicine. However, it is limited due to insufficient resources. OBJECTIVE: To prepare porcine acellular dermal matrix (PADM) dermal matrix, in addition, to estimate its in vitro biocompatibility. DESIGN, TIME AND SETTING: An in vitro cytology contrast experiment. The Experiment was performed at the laboratory of Biomaterials and Pharmacy Technology Institute, China Institute for Radiation Protection

  20. 应用两步接枝法制备新型改性聚丙烯滤嘴材料%A novel filtration of cigarette smoke prepared by two steps grafting of AA and AMPS monomer onto PP matrix

    Institute of Scientific and Technical Information of China (English)

    王海涛; 魏俊富; 王翱; 陈远; 赵禹; 杨闯

    2013-01-01

    In order to improve the poor adsorption for cigarette smoke and tar of polypropylene (PP) fiber, AA and AMPS were grafted onto PP fiber matrix by two steps plasma irradiation grafting for preparation a novel composite filtration of cigarette smoke PP-g-(AA + AMPS). The factors influenced the grafting degree were discussed, such as the irradiation time, concentration of monomer and the concentration of inhibitor. Attenuated total reflection-Fourier transform infrared spectroscopy (ATR-FT-IR) and scanning electron microscopy (SEM) were used to characterize the chemical and morphological changes of the original and grafted PP fiber matrix, the results indicated that AMPS was grafted onto the surface of PP fiber matrix. The results indicated that the filtration efficiency of PP fiber was improved significant after graft modification, the total particulate matter in mainstream cigarette smoke reduces 30. 5%, and the concentration of tar and nicotine are decrease 43. 2% and 31. 7% , respectively.%为了解决烟用聚丙烯(PP)滤嘴材料对烟气吸附性能差、降焦性能低等问题,采用等离子体辐射引发的方法,在烟用聚丙烯纤维基体上分两步接枝丙烯酸(AA)和2-丙烯酰胺-2-甲基丙磺酸(AMPS)单体,制备了聚丙烯高吸附滤嘴.讨论了单体浓度、辐照时间、阻聚剂浓度对聚丙烯纤维接枝率的影响.利用衰减全反射红外光谱和扫描电子显微镜对接枝后的聚丙烯纤维基体的表面化学组成和形貌结构进行表征,结果表明,AMPS单体被成功接枝到PP纤维上.当改性后聚丙烯纤维的接枝率为22.8%时,改性后聚丙烯纤维滤嘴对烟气的过滤效果比改性前明显提高,烟气中的总粒相物比未改性滤嘴降低了30.5%,焦油及烟碱含量分别降低43.2%和31.7%.

  1. Matrix groups for undergraduates

    CERN Document Server

    Tapp, Kristopher

    2016-01-01

    Matrix groups touch an enormous spectrum of the mathematical arena. This textbook brings them into the undergraduate curriculum. It makes an excellent one-semester course for students familiar with linear and abstract algebra and prepares them for a graduate course on Lie groups. Matrix Groups for Undergraduates is concrete and example-driven, with geometric motivation and rigorous proofs. The story begins and ends with the rotations of a globe. In between, the author combines rigor and intuition to describe the basic objects of Lie theory: Lie algebras, matrix exponentiation, Lie brackets, maximal tori, homogeneous spaces, and roots. This second edition includes two new chapters that allow for an easier transition to the general theory of Lie groups. From reviews of the First Edition: This book could be used as an excellent textbook for a one semester course at university and it will prepare students for a graduate course on Lie groups, Lie algebras, etc. … The book combines an intuitive style of writing w...

  2. Matrix inequalities

    CERN Document Server

    Zhan, Xingzhi

    2002-01-01

    The main purpose of this monograph is to report on recent developments in the field of matrix inequalities, with emphasis on useful techniques and ingenious ideas. Among other results this book contains the affirmative solutions of eight conjectures. Many theorems unify or sharpen previous inequalities. The author's aim is to streamline the ideas in the literature. The book can be read by research workers, graduate students and advanced undergraduates.

  3. 浸渗时间对无压浸渗制备Al/SiCp陶瓷基合材料的影响%Infiltration Time Effect of Pressureless Infiltration Preparation of Al/SiCp Ceramic Matrix Composites

    Institute of Scientific and Technical Information of China (English)

    徐跃; 高霖; 崔崇; 钱凤

    2011-01-01

    Microstructure, density and rigidity of Al/SiCp ceramic matrix composites prepared by pressureless infiltration, were investigated in this paper. The result indicates that the infiltration in due course of time made Si and Mg diffusion and interface reaction conducted fully,which increased interface wetting property and decreased interface loose and pore,and advanced the a-luminium alloys infiltration. Holding one hour at proper temperature got full infitration, but poor density and low rigidity, while holding three hours got pulverization so two hours shall be a proper parameter.%本文采用无压浸渗法,研究浸渗时间对Al/SiCp陶瓷基复合材料组织、致密度、硬度的影响.浸渗保温时间1h,能浸透,但致密度差,硬度低.保温时间3h,发生粉化现象.结果表明浸渗保温时间2h是无压浸渗较好的工艺参数.

  4. Mg对无压渗透制备Al/SiCp陶瓷基复合材料的影响%Effect of Mg on Pressureless Infiltration Preparation of Al/SiCp Ceramic Matrix Composites

    Institute of Scientific and Technical Information of China (English)

    徐跃; 高霖; 崔崇; 钱凤

    2011-01-01

    Influence of Mg on preparation and microstructure of SiCp/Al ceramic matrix composites with SiC volume fraction 40% -70% fabricated by pressureless infiltration is discussed in this paper. Result indicated that addition of Mg in aluminium infiltration liquid could improve infiltration ability evidently. Because magnesium diffused and enriched interface of Al and SiC. Interface reaction made Al2O3 film broken to reduce interface strain, that increased liquidity of aluminium alloy liquid. Reaction of Mg and framework air caused negative press that advanced pressureless infiltration process voluntarily.%本文采用无压浸渗法,研究了Mg对Al/SiC.(SiC体积分数为40%-70%)陶瓷基复合材料制备及组织影响.结果表明,Al浸渗液中添加Mg可以显著提高铝液的浸润性,因为Mg扩散并富集于Al/SiCp界面,通过界面反应促使Al2O3膜的破裂降低界面张力,增加了铝合金液的流动性,而且Mg与骨架孔隙内的气氛反应形成负压,促进无压浸渗的自发进行.

  5. Preparation and characterization of a magneto-polymeric nanocomposite: Fe{sub 3}O{sub 4} nanoparticles in a grafted, cross-linked and plasticized poly(vinyl chloride) matrix

    Energy Technology Data Exchange (ETDEWEB)

    Rodriguez-Fernandez, Oliverio S. [Centro de Investigacion en Quimica Aplicada, Boulevard Enrique Reyna Hermosillo No. 140, Saltillo, Coahuila Mexico, C.P. 25253 (Mexico)], E-mail: oliverio@ciqa.mx; Rodriguez-Calzadiaz, C.A.; Yanez-Flores, Isaura G.; Montemayor, Sagrario M. [Centro de Investigacion en Quimica Aplicada, Boulevard Enrique Reyna Hermosillo No. 140, Saltillo, Coahuila Mexico, C.P. 25253 (Mexico)

    2008-07-15

    In this work two kind of materials: (1) grafted, cross-linked and plasticized poly(vinyl chloride) (PVC) 'plastic films' and (2) magnetic plastic films 'magneto-polymeric nanocomposites' were prepared. Precursor solutions or 'plastisols' used to obtain the plastic films were obtained by mixing PVC (emulsion grade) as polymeric matrix, di(2-ethylhexyl)phthalate (DOP) as plasticizer, a thermal stabilizer based in Ca/Zn salts, and a cross-linking agent, 3-mercaptopropyltrimethoxysilane (MTMS) or 3-aminopropyltriethoxysilane (ATES), at several concentrations. Flexible films were obtained from the plastisols using static casting. The stress-strain behavior and the gel content (determined by Soxhlet extraction with boiling THF) of the flexible films were measured in order to evaluate the effect of the cross-linking agent and their content on the degree of cross-linking. The magneto-polymeric nanocomposites were obtained by mixing the optimum composition of the plastisols (analyzed previously) with magnetite (Fe{sub 3}O{sub 4})-based ferrofluid and DOP. Later, flexible films were obtained by static casting of the plastisol/ferrofluid systems. The magnetic films were characterized by the above-mentioned techniques and X-ray diffraction, vibrating sample magnetometry and thermogravimetrical analy0009s.

  6. Design and Preparation of Ceramic Matrix in Metal Ceramic Heater%金属陶瓷发热体中陶瓷基体的设计和制备

    Institute of Scientific and Technical Information of China (English)

    邓腾飞; 贾倩

    2016-01-01

    以碳化硅、工业氢氧化铝、苏州土、钾长石、氧化钙为主要原料,设计了B系列配方。采用半干压成型和注凝成型两种不同的方法来制备金属陶瓷发热体基体,并确定最佳配方及制备工艺参数。以期在降低成本的同时,使其用途更加广泛。实验制备出了陶瓷基体并成功得到经二次烧成后内部镶嵌钨丝的样品。通过XRD和SEM等现代测试技术对材料的性能和微观结构进行了表征,相组成分析结果表明,样品的主晶相为碳化硅和方石英。显微结构分析表明,样品中生成了碳化硅晶粒且热导率与氧化铝陶瓷相比大大提高。%In this paper, using the SiC powder, industrial Al(OH)3, Suzhou kaolin, potash feldspar and CaO as the main raw materials, the metal ceramic heating body was prepared, and its optimum formulation and preparation process parameters were determined. In order to reduce the costs and make it more applicable, the properties and microstructure of the materials were characterized by XRD, SEM and other modern test techniques. The ceramic matrix was prepared by experiment. And the samples inlaid with tungsten wire were obtained successfully by double ifring. The phase composition analysis indicated that the main phases of samples were silicon carbide and cristobalite. The study results of microstructure showed that silicon carbide is gained in the samples. Compared with the alumina ceramics, the thermal conductivity of samples isgreatly improved.

  7. Matrix analysis

    CERN Document Server

    Bhatia, Rajendra

    1997-01-01

    A good part of matrix theory is functional analytic in spirit. This statement can be turned around. There are many problems in operator theory, where most of the complexities and subtleties are present in the finite-dimensional case. My purpose in writing this book is to present a systematic treatment of methods that are useful in the study of such problems. This book is intended for use as a text for upper division and gradu­ ate courses. Courses based on parts of the material have been given by me at the Indian Statistical Institute and at the University of Toronto (in collaboration with Chandler Davis). The book should also be useful as a reference for research workers in linear algebra, operator theory, mathe­ matical physics and numerical analysis. A possible subtitle of this book could be Matrix Inequalities. A reader who works through the book should expect to become proficient in the art of deriving such inequalities. Other authors have compared this art to that of cutting diamonds. One first has to...

  8. The Preparation and Properties of Continuous Carbon Fiber Reinforced Aluminum Matrix Composite%碳纤维增强铝基复合材料的制备及其拉伸性能

    Institute of Scientific and Technical Information of China (English)

    王德庆; 石子源; 高宏

    2000-01-01

    The tensile test specimen of the continuous carbon fiber reinforced aluminum matrix com- posites were prepared by using squeeze casting under three different solidification conditions. The tensile test was also conducted. The tensile strength and elastic modulus of the composite are in- creased with the increase in the carbon fiber content. The tensile strength of the composite with 48 Vol.% carbon fiber is 50% higher than that of the matrix material. However, the plasticities of the composite are decreased dramatically with the increase in the carbon content. When the carbon fiber content is small, the solodification conditions have greater effect on tensile strength but smaller on elastic modulus of the composite, while large amount of carbon fibers are added, solidification condi- tions affect elastic modulus more and tensile strength less.%利用挤压铸造方法,采用三种不同的凝固条件,制备了连续长碳纤维增强铝基复合材料的拉伸试样,并对其拉伸性能进行了试验.试验结果表明,该复合材料的抗拉强度和弹性模量皆随碳纤维的体积含量增加而增加.含48%碳纤维的复合材料比基体材料的拉伸强度高50%以上.但塑性指标随碳纤维含量的增加而显著降低.当连续碳纤维的体积含量较小时,凝固条件对该复合材料的抗拉强度影响较大,对弹性模量的影响较小;当碳纤维的体积含量较大时,凝固条件对该复合材料的抗拉强度影响较小,而对弹性模量的影响较大.

  9. Matrix pentagons

    CERN Document Server

    Belitsky, A V

    2016-01-01

    The Operator Product Expansion for null polygonal Wilson loop in planar maximally supersymmetric Yang-Mills theory runs systematically in terms of multiparticle pentagon transitions which encode the physics of excitations propagating on the color flux tube ending on the sides of the four-dimensional contour. Their dynamics was unravelled in the past several years and culminated in a complete description of pentagons as an exact function of the 't Hooft coupling. In this paper we provide a solution for the last building block in this program, the SU(4) matrix structure arising from internal symmetry indices of scalars and fermions. This is achieved by a recursive solution of the Mirror and Watson equations obeyed by the so-called singlet pentagons and fixing the form of the twisted component in their tensor decomposition. The non-singlet, or charged, pentagons are deduced from these by a limiting procedure.

  10. Preparation of solvent-free epoxy-imide matrix resin with high temperature resistance%无溶剂耐高温环氧-酰亚胺基体树脂的制备

    Institute of Scientific and Technical Information of China (English)

    虞鑫海; 黄莉茜

    2015-01-01

    采用多官能环氧树脂、活性聚酰亚胺、环氧树脂活性稀释剂、固化剂和促进剂,制备了无溶剂耐高温环氧-酰亚胺基体树脂(ECPIM),并研究了其黏度、凝胶化时间、表观活化能、拉伸剪切强度、电容、介电损耗、接触角、表面能、吸水率等.结果表明:ECPIM具有良好的固化反应活性,优异的黏接强度,240 ℃时的拉伸剪切强度高达24.2 MPa;频率为20 Hz~1 MHz时,ECPIM的电容值均较稳定,且介电损耗较低,介电性能优异;ECPIM具有较低的表面能(65.8 mJ/m2)和吸水率(1.12%).%A kind of solvent-free epoxy-imide matrix resin(ECPIM) with high temperature resistance was prepared with multifunctional epoxy resin, reactive polyimide resin, epoxy reactive diluents, curing agent and accelerator as raw materials. The properties including viscosity, gel time, apparent activation energy, tensile shear strength, capacitance value, dielectric loss, contact angle, surface energy, water absorption, etc. were further studied. The results show that the ECPIM has excellent curing activity and bonding strength. The tensile shear strength of ECPIM reaches 24.2 MPa at 240℃.The ECPIM has stable capacitance value and low dielectric loss when the frequency is 20 Hz-1 MHz. The ECPIM has low surface energy of 65.8 mJ/m2 and water absorption of 1.12%.

  11. 新型激光微孔化猪脱细胞真皮基质的制备及应用%Preparation and application of novel laser micropore porcine acellular dermal matrix

    Institute of Scientific and Technical Information of China (English)

    罗旭; 万丽; 李安乐; 徐建军; 夏卫东; 李玉莉; 邓春林; 王平; 林才

    2012-01-01

    目的 介绍一种新型微孔化猪脱细胞真皮基质并验证其安全性、可行性.方法 取新鲜健康小白猪断层真皮,采用高渗盐-胰蛋白酶法脱细胞,经超声波充分震荡洗涤,获得猪脱细胞真皮基质,经特定激光微孔技术,在脱细胞真皮基质上贯穿打孔即获得新型激光微孔化猪脱细胞真皮基质.将24只SD大鼠均切除背部全层皮肤至深筋膜,造成大小2.0 cm×2.0 cm创面,随机分为实验组和对照组,每组各12只,同步I期行自体中厚皮片与真皮材料复合移植于大鼠全层皮肤缺失创面,实验组采用移植真皮材料为激光微孔化猪脱细胞真皮基质(LPADM),对照组采用移植真皮材料为普通的猪皮脱细胞真皮基质(ADM),组织学检查、电镜观察两组真皮材料的物理性状、结构完整性、细胞残留及移植后皮片活性、血管化和移植后动物安全性变化.结果 制备的真皮基质材料LPADM和ADM均呈瓷白色,有光泽,柔软而有弹性;组织学检查未见上皮细胞、内皮细胞残留,结构完整性好;电镜检查胶原纤维排列整齐,保持较好的结构完整性.实验组术后7 d LPADM组织学检查显示移植真皮血管化充分,术后14 d复合移植皮片均存活;对照组术后7 d移植皮片色暗淡,多有起泡,并逐渐失活坏死,ADM组织学检查未见新生血管形成,术后14 d复合移植皮片干性坏死.两组实验动物均无异常死亡或感染,亦未见皮肤过敏反应,体重无减轻.结论 以特定激光微孔化等技术制备的新型猪脱细胞真皮基质动物移植实验中血管化充分、复合皮片愈合良好,获得满意的实验效果.%Objective To prepare a new type of micropore porcine acellular dermal matrix with the aid of laser (PLADM ), and validate the safety and practicability of the PLADM. Methods LPADM was prepared by a specific laser micropore technology with the punch worked in cycles and suspended in the midair on the harvested split

  12. Riemann Zeta Matrix Function

    OpenAIRE

    Kargın, Levent; Kurt, Veli

    2015-01-01

    In this study, obtaining the matrix analog of the Euler's reflection formula for the classical gamma function we expand the domain of the gamma matrix function and give a infinite product expansion of sinπxP.  Furthermore we define Riemann zeta matrix function and evaluate some other matrix integrals. We prove a functional equation for Riemann zeta matrix function.

  13. 十字型微通道制备粒径均一的纤维素层析介质%Preparation of cellulose-based chromatography matrix with uniform size by cross-flow microchannel chip

    Institute of Scientific and Technical Information of China (English)

    童芳丽; 林东强; 刘川; 贠军贤; 姚善泾

    2013-01-01

    为了满足层析介质对粒径单分散的要求,利用十字型微通道的聚焦效应,形成粒径均一的纤维素微液滴,经固化成纤维素微球,再偶联配基制成了纤维素层析介质.以离子液体1-乙基-3-甲基咪唑甲基磷酸直接溶解微晶纤维素为水相,葵花籽油为油相,考察了微通道内微液滴的形成条件,优化了纤维素浓度、分散剂浓度、油水两相流速等因素,得到粒径约100 μm的纤维素微液滴,CV值小于0.2.微液滴固化再生,得到球形度良好的纤维素微球,湿真密度1.019 g.ml-1,孔度94.6%,体均粒径105.5 μm;进一步偶联DEAE配基,制得了离子交换层析介质,离子交换容量为123.3 μmol·g-1,牛血清白蛋白的饱和吸附容量Qm达到220 mg·g-1,有效扩散系数De为1.8×10-11m2·s-1,体现出较好的蛋白质吸附性能.%To prepare the cellulose-based chromatography matrix with uniform size, a cross-flow microchannel chip was used to control the droplet size of cellulose solution and then the microdroplets were solidified to obtain the monodisperse cellulose beads. In the present work, ionic liquid, [EMIM] MP, was used to dissolve the microcrystalline cellulose as water phase and sunflower oil was used as oil phase. The effects of cellulose concentration, surfactant addition, flow rates of oil phase and water phase were investigated. The optimized preparation condition was 2% cellulose solution as water phase, flow rate of water phase of 6 μl · min-1 and flow rate of oil phase of 200 μl · min-1. The microdroplets of cellulose solution thus obtained could be about 100 μm with the variation coefficient less than 0. 2. After solidification and regeneration, cellulose beads were obtained with good sphericity. Wet density of beads was 1. 019 g · ml-1 , porosity was 94. 6%, and mean size was about 105.5 μm. The cellulose beads were coupled with DEAE ligand and used as weak anion-exchange resin. The ion exchange capacity was 123. 3 μmol

  14. Tissue-engineered acellular matrix material:preparation and application in articular cartilage repair%脱细胞基质材料制备方法及在骨关节软骨损伤修复中的应用

    Institute of Scientific and Technical Information of China (English)

    赵玉果; 李明明

    2016-01-01

      结果与结论:①脱细胞基质组织工程材料交联后呈现为深蓝色,疏松多孔,直径为5 mm,硬度适中,具备一定的弹性;②苏木精-伊红染色不含有细胞碎屑及蓝染的核物质,不存在残留的细胞外基质;③甲苯胺蓝染色为蓝色材料支架孔隙率为90%,溶胀率为(1314±337)%;④脱细胞基质组织组材料1,3,5,7,9 d的A值显著高于纤维样组织组(P OBJECTIVE:To investigate the effect of tissue-engineered acelular matrix in articular cartilage repair. METHODS:Totaly 30 New Zealand rabbits were randomly alottedto fibroid tissue andacelular matrix groups (n=15 per group), and then articular cartilage defect models,4mmin diameter,were established at the white rabbitfemoral condyle. Acelular cartilage matrix scaffold was prepared using bovine knee cartilage, and model rats in the acelular matrix group were repaired with acelular cartilage matrix scaffold and the others in the fibroid tissue group repaired with fibroid tissues. Finaly, repair effects between two groups were compared. RESULTS AND CONCLUSION:The dark blue and porous tissue-engineered acelular matrix material could be found, with a diameter of 5mm and moderate hardness, and exhibited certain flexibility after cross-linking. Hematoxylin-eosin staining showed that cel debris,blue-stainednuclear materials and residual extracelular matrix disappeared. Toluidine blue staining found that the porosity of the blue scaffold was 90%, and the sweling ratio was (1314±337)%. The absorbance value in the acelular matrix group was significantly higher than that in the fibroid tissue group at 1, 3, 5, 7 and 9 days (P< 0.05). In the fibroid tissue group,defectsfiled withnewborn fibrous scars were overt. By contrast, in the acelularmatrix group, the white tissuescovered the defect regionwith smooth surface,and the woundwas basicaly healed,withanunclearboundaryafter 12weeks. Moreover, blue-stained, smal flattened cels appeared

  15. Rapid Identification of Bacteria Directly from Positive Blood Cultures by Use of a Serum Separator Tube, Smudge Plate Preparation, and Matrix-Assisted Laser Desorption Ionization-Time of Flight Mass Spectrometry.

    Science.gov (United States)

    Chen, Yan; Porter, Vanessa; Mubareka, Samira; Kotowich, Leona; Simor, Andrew E

    2015-10-01

    We analyzed the matrix-assisted laser desorption ionization-time of flight mass spectrometry (MALDI-TOF MS) of smudge plate growth for bacterial identification from 400 blood cultures. Ninety-seven percent of Gram-negative bacilli and 85% of Gram-positive organisms were correctly identified within 4 h; only eight isolates (2.0%) were misidentified. This method provided rapid and accurate microbial identification from positive blood cultures.

  16. The Matrix Cookbook

    DEFF Research Database (Denmark)

    Petersen, Kaare Brandt; Pedersen, Michael Syskind

    Matrix identities, relations and approximations. A desktop reference for quick overview of mathematics of matrices.......Matrix identities, relations and approximations. A desktop reference for quick overview of mathematics of matrices....

  17. Matrix with Prescribed Eigenvectors

    Science.gov (United States)

    Ahmad, Faiz

    2011-01-01

    It is a routine matter for undergraduates to find eigenvalues and eigenvectors of a given matrix. But the converse problem of finding a matrix with prescribed eigenvalues and eigenvectors is rarely discussed in elementary texts on linear algebra. This problem is related to the "spectral" decomposition of a matrix and has important technical…

  18. TiB2-TiC Ceramics Matrix Composites Prepared by in-situ Technique%原位合成TiB2-TiC陶瓷基复合材料

    Institute of Scientific and Technical Information of China (English)

    唐建新; 曾照强; 胡晓清; 苗赫濯

    2001-01-01

    分析了TiB2-TiC陶瓷基复合材料的原位生成机理,利用普通的热压烧结设备,以TiH2-B4C为原料原位合成了高性能的TiB2-TiC陶瓷基复合材料。TEM和X射线衍射的研究结果表明:原位合成的复合材料中TiB2为长柱状的显微形貌,从而提高了材料的断裂韧性。%The principle of in-situ formation of TiB2-TiC ceramics matrix composites was analyzed in this paper. The TiB2-TiC ceramics matrix composites of high performance were fabricated by hot pressing from TiH2-B4C. The results show that the TiB2 in microstructure presents long column morphologies which improve fracture toughness of the composite.

  19. Enhanced Resource Descriptions Help Learning Matrix Users.

    Science.gov (United States)

    Roempler, Kimberly S.

    2003-01-01

    Describes the Learning Matrix digital library which focuses on improving the preparation of math and science teachers by supporting faculty who teach introductory math and science courses in two- and four-year colleges. Suggests it is a valuable resource for school library media specialists to support new science and math teachers. (LRW)

  20. The Synthesis of 1-(4-Triethoxysilylphenyl-4,4,4-trifluoro-1,3-butanedione, a Novel Trialkoxysilane Monomer for the Preparation of Functionalized Sol-gel Matrix Materials

    Directory of Open Access Journals (Sweden)

    John C. DiCesare

    2008-10-01

    Full Text Available The title compound, 1-(4-triethoxysilylphenyl-4,4,4-trifluoro-1,3-butanedione, was synthesized in a three-step sequence starting from 2-(4-bromophenylpropene. Containing both a trialkoxysilyl and a substituted 1,3-butanedione functional grouping within its structure, this new silane is a viable starting material for the preparation of functionalized sol-gel materials.

  1. Crosslinked collagen/chitosan matrix for artificial livers

    NARCIS (Netherlands)

    Wang, X.H.; Li, D.P.; Wang, W.J.; Feng, Q.L.; Cui, F.Z.; Xu, Y.X.; Song, X.H.; van der Werf, Mark

    2003-01-01

    Matrices composed of collagen and chitosan may create an appropriate environment for the regeneration of livers. In this study, we have prepared, characterized and evaluated a new collagen/chitosan matrix (CCM). The CCM was made by using crosslinking agent

  2. 关于TiC/7075铝基复合材料的制备工艺研究%Preparation Techniques of TiC/7075 Aluminum Matrix Composites

    Institute of Scientific and Technical Information of China (English)

    吴晓飞; 鲁玉梅

    2012-01-01

    采用原位反应近液相线铸造方法制备含有少量原位TiC颗粒的7075铝基复合材料,通过电子显微镜分析研究TiC/7075铝基复合材料的组织形貌。研究了固溶和时效处理工艺对制备的TiC/7075铝基复合材料显微组织的影响。%The 7075 aluminum matrix com posite with a small amount of in situ TiC particales is made by in-situ-reaction near-liquidus casting and the microstructure of the TiC/7075 composite is analyzed and studied with electronic microscopes.The effects of solid solution and aging on the microstructure are studied.

  3. Can matrix solid phase dispersion (MSPD) be more simplified? Application of solventless MSPD sample preparation method for GC-MS and GC-FID analysis of plant essential oil components.

    Science.gov (United States)

    Wianowska, Dorota; Dawidowicz, Andrzej L

    2016-05-01

    This paper proposes and shows the analytical capabilities of a new variant of matrix solid phase dispersion (MSPD) with the solventless blending step in the chromatographic analysis of plant volatiles. The obtained results prove that the use of a solvent is redundant as the sorption ability of the octadecyl brush is sufficient for quantitative retention of volatiles from 9 plants differing in their essential oil composition. The extraction efficiency of the proposed simplified MSPD method is equivalent to the efficiency of the commonly applied variant of MSPD with the organic dispersing liquid and pressurized liquid extraction, which is a much more complex, technically advanced and highly efficient technique of plant extraction. The equivalency of these methods is confirmed by the variance analysis. The proposed solventless MSPD method is precise, accurate, and reproducible. The recovery of essential oil components estimated by the MSPD method exceeds 98%, which is satisfactory for analytical purposes.

  4. Comparing the identification of Clostridium spp. by two Matrix-Assisted Laser Desorption Ionization-Time of Flight (MALDI-TOF) mass spectrometry platforms to 16S rRNA PCR sequencing as a reference standard: a detailed analysis of age of culture and sample preparation.

    Science.gov (United States)

    Chean, Roy; Kotsanas, Despina; Francis, Michelle J; Palombo, Enzo A; Jadhav, Snehal R; Awad, Milena M; Lyras, Dena; Korman, Tony M; Jenkin, Grant A

    2014-12-01

    We compared the identification of Clostridium species using mass spectrometry by two different Matrix-Assisted Laser Desorption Ionization Time-of-Flight Mass Spectrometry (MALDI-TOF MS) platforms (Bruker MS and Vitek MS) against 16S rRNA sequencing as the reference standard. We then examined the impact of different sample preparations and (on one of those platforms) age of bacterial colonial growth on the performance of the MALDI-TOF MS systems. We identified 10 different species amongst the 52 isolates by 16S rRNA sequencing, with Clostridium perfringens the most prevalent (n=30). Spectrometric analysis using Vitek MS correctly speciated 47/52 (90.4%) isolates and was not affected by the sample preparation used. Performance of the Bruker MS was dependent on sample preparation with correct speciation obtained for 36 of 52 (69.2%) isolates tested using the Direct Transfer [DT] protocol, but all 52 (100%) isolates were correctly speciated using either an Extended Direct Transfer [EDT] or a Full Formic Extraction [EX] protocol. We then examined the effect of bacterial colonial growth age on the performance of Bruker MS and found substantial agreement in speciation using DT (Kappa=0.62, 95% CI: 0.46-0.75), almost perfect agreement for EDT (Kappa=0.94, 95% CI: 0.86-1.00) and exact agreement for EX (Kappa=1.00) between different days. Copyright © 2014 Elsevier Ltd. All rights reserved.

  5. Parallelism in matrix computations

    CERN Document Server

    Gallopoulos, Efstratios; Sameh, Ahmed H

    2016-01-01

    This book is primarily intended as a research monograph that could also be used in graduate courses for the design of parallel algorithms in matrix computations. It assumes general but not extensive knowledge of numerical linear algebra, parallel architectures, and parallel programming paradigms. The book consists of four parts: (I) Basics; (II) Dense and Special Matrix Computations; (III) Sparse Matrix Computations; and (IV) Matrix functions and characteristics. Part I deals with parallel programming paradigms and fundamental kernels, including reordering schemes for sparse matrices. Part II is devoted to dense matrix computations such as parallel algorithms for solving linear systems, linear least squares, the symmetric algebraic eigenvalue problem, and the singular-value decomposition. It also deals with the development of parallel algorithms for special linear systems such as banded ,Vandermonde ,Toeplitz ,and block Toeplitz systems. Part III addresses sparse matrix computations: (a) the development of pa...

  6. Ubiquitination of specific mitochondrial matrix proteins

    Energy Technology Data Exchange (ETDEWEB)

    Lehmann, Gilad [The Janet and David Polak Tumor and Vascular Biology Research Center and the Technion Integrated Cancer Center (TICC), The Rappaport Faculty of Medicine and Research Institute, Haifa, 31096 (Israel); Ziv, Tamar [The Smoler Proteomics Center, Faculty of Biology – Technion-Israel Institute of Technology, Haifa, 32000 (Israel); Braten, Ori [The Janet and David Polak Tumor and Vascular Biology Research Center and the Technion Integrated Cancer Center (TICC), The Rappaport Faculty of Medicine and Research Institute, Haifa, 31096 (Israel); Admon, Arie [The Smoler Proteomics Center, Faculty of Biology – Technion-Israel Institute of Technology, Haifa, 32000 (Israel); Udasin, Ronald G. [The Janet and David Polak Tumor and Vascular Biology Research Center and the Technion Integrated Cancer Center (TICC), The Rappaport Faculty of Medicine and Research Institute, Haifa, 31096 (Israel); Ciechanover, Aaron, E-mail: aaroncie@tx.technion.ac.il [The Janet and David Polak Tumor and Vascular Biology Research Center and the Technion Integrated Cancer Center (TICC), The Rappaport Faculty of Medicine and Research Institute, Haifa, 31096 (Israel)

    2016-06-17

    Several protein quality control systems in bacteria and/or mitochondrial matrix from lower eukaryotes are absent in higher eukaryotes. These are transfer-messenger RNA (tmRNA), The N-end rule ATP-dependent protease ClpAP, and two more ATP-dependent proteases, HslUV and ClpXP (in yeast). The lost proteases resemble the 26S proteasome and the role of tmRNA and the N-end rule in eukaryotic cytosol is performed by the ubiquitin proteasome system (UPS). Therefore, we hypothesized that the UPS might have substituted these systems – at least partially – in the mitochondrial matrix of higher eukaryotes. Using three independent experimental approaches, we demonstrated the presence of ubiquitinated proteins in the matrix of isolated yeast mitochondria. First, we show that isolated mitochondria contain ubiquitin (Ub) conjugates, which remained intact after trypsin digestion. Second, we demonstrate that the mitochondrial soluble fraction contains Ub-conjugates, several of which were identified by mass spectrometry and are localized to the matrix. Third, using immunoaffinity enrichment by specific antibodies recognizing digested ubiquitinated peptides, we identified a group of Ub-modified matrix proteins. The modification was further substantiated by separation on SDS-PAGE and immunoblots. Last, we attempted to identify the ubiquitin ligase(s) involved, and identified Dma1p as a trypsin-resistant protein in our mitochondrial preparations. Taken together, these data suggest a yet undefined role for the UPS in regulation of the mitochondrial matrix proteins. -- Highlights: •Mitochondrial matrix contains ubiquitinated proteins. •Ubiquitination occurs most probably in the matrix. •Dma1p is a ubiquitin ligase present in mitochondrial preparations.

  7. Decellularized bone matrix grafts for calvaria regeneration

    Science.gov (United States)

    Lee, Dong Joon; Diachina, Shannon; Lee, Yan Ting; Zhao, Lixing; Zou, Rui; Tang, Na; Han, Han; Chen, Xin; Ko, Ching-Chang

    2016-01-01

    Decellularization is a promising new method to prepare natural matrices for tissue regeneration. Successful decellularization has been reported using various tissues including skin, tendon, and cartilage, though studies using hard tissue such as bone are lacking. In this study, we aimed to define the optimal experimental parameters to decellularize natural bone matrix using 0.5% sodium dodecyl sulfate and 0.1% NH4OH. Then, the effects of decellularized bone matrix on rat mesenchymal stem cell proliferation, osteogenic gene expression, and osteogenic differentiations in a two-dimensional culture system were investigated. Decellularized bone was also evaluated with regard to cytotoxicity, biochemical, and mechanical characteristics in vitro. Evidence of complete decellularization was shown through hematoxylin and eosin staining and DNA measurements. Decellularized bone matrix displayed a cytocompatible property, conserved structure, mechanical strength, and mineral content comparable to natural bone. To study new bone formation, implantation of decellularized bone matrix particles seeded with rat mesenchymal stem cells was conducted using an orthotopic in vivo model. After 3 months post-implantation into a critical-sized defect in rat calvaria, new bone was formed around decellularized bone matrix particles and also merged with new bone between decellularized bone matrix particles. New bone formation was analyzed with micro computed tomography, mineral apposition rate, and histomorphometry. Decellularized bone matrix stimulated mesenchymal stem cell proliferation and osteogenic differentiation in vitro and in vivo, achieving effective bone regeneration and thereby serving as a promising biological bone graft. PMID:28228929

  8. Decellularized bone matrix grafts for calvaria regeneration

    Directory of Open Access Journals (Sweden)

    Dong Joon Lee

    2016-12-01

    Full Text Available Decellularization is a promising new method to prepare natural matrices for tissue regeneration. Successful decellularization has been reported using various tissues including skin, tendon, and cartilage, though studies using hard tissue such as bone are lacking. In this study, we aimed to define the optimal experimental parameters to decellularize natural bone matrix using 0.5% sodium dodecyl sulfate and 0.1% NH4OH. Then, the effects of decellularized bone matrix on rat mesenchymal stem cell proliferation, osteogenic gene expression, and osteogenic differentiations in a two-dimensional culture system were investigated. Decellularized bone was also evaluated with regard to cytotoxicity, biochemical, and mechanical characteristics in vitro. Evidence of complete decellularization was shown through hematoxylin and eosin staining and DNA measurements. Decellularized bone matrix displayed a cytocompatible property, conserved structure, mechanical strength, and mineral content comparable to natural bone. To study new bone formation, implantation of decellularized bone matrix particles seeded with rat mesenchymal stem cells was conducted using an orthotopic in vivo model. After 3 months post-implantation into a critical-sized defect in rat calvaria, new bone was formed around decellularized bone matrix particles and also merged with new bone between decellularized bone matrix particles. New bone formation was analyzed with micro computed tomography, mineral apposition rate, and histomorphometry. Decellularized bone matrix stimulated mesenchymal stem cell proliferation and osteogenic differentiation in vitro and in vivo, achieving effective bone regeneration and thereby serving as a promising biological bone graft.

  9. Mixed matrix membranes : a new platform for enzymatic reactions

    NARCIS (Netherlands)

    de Sousa André, Joao Miguel

    2009-01-01

    Glucose oxidase (GOx) was covalently bound onto Eupergit® C particles embedded in mixed matrix hollow fiber membranes prepared using polyethylene vinyl alcohol (EVAL) as the polymeric macroporous matrix. The Eupergit ® C particles were chemically modified with ethylenediamine and activated with

  10. Phosphine in various matrixes

    Institute of Scientific and Technical Information of China (English)

    2003-01-01

    Matrix-bound phosphine was determined in the Jiaozhou Bay coastal sediment, in prawn-pond bottom soil, in the eutrophic lake Wulongtan, in the sewage sludge and in paddy soil as well. Results showed that matrix-bound phosphine levels in freshwater and coastal sediment, as well as in sewage sludge, are significantly higher than that in paddy soil. The correlation between matrix bound phosphine concentrations and organic phosphorus contents in sediment samples is discussed.

  11. Formulation and Characterization of Matrix and Triple-Layer matrix tablets for Controlled Delivery of Metoprolol tartrate

    OpenAIRE

    Izhar Ahmed Syed; Lakshmi Narsu Mangamoori; Yamsani Madhusudan Rao

    2011-01-01

    In the present study matrix and triple layer matrix tablets of metoprolol tartrate were formulated by using xanthan gum as the matrix forming agent and Sodium Carboxy Methyl Cellulose (Na CMC) as barrier layers. The prepared tablets were analysed for their hardness, friability, drug content and in-vitro drug release studies. Marked differences in dissolution characteristics of (M3) and (M3L3) were observed and showed a significant difference statistically. Mean dissolution time (MDT) for M3 a...

  12. Preparo de Itens de Ensaio de Proficiência em Matriz Queijo para a Pesquisa de Salmonella spp. | Preparation of Proficienc Test Items for Salmonella spp. Detection in Cheese Matrix

    Directory of Open Access Journals (Sweden)

    Juliana de Castro Beltrão da Costa

    2015-08-01

    Full Text Available A participação de laboratórios analíticos em ensaio de proficiência permite a verificação da confiabilidade dos resultados gerados nas análises de controle da qualidade. O objetivo deste estudo foi produzir um lote de itens de ensaio (IE a ser utilizado em ensaio de proficiência (EP para pesquisa de Salmonella spp. em matriz queijo. Queijo Minas Frescal (QMF Ultrafiltrado foi utilizado como matriz e fortificado com uma cepa de Salmonella Enteritidis. A trealose foi utilizada como crioprotetor e a liofilização como técnica de preservação. O lote foi avaliado quanto a verificação do vácuo, teste da homogeneidade, estudo da estabilidade em longo prazo nas temperaturas de -70oC (referência e -20oC (armazenamento e em curto prazo nas temperaturas de 4, 25 e 35ºC (transporte. O lote apresentou presença de vácuo em 95,6% dos frascos e foi considerado suficientemente homogêneo. Os IE apresentaram estabilidade a -70ºC superior a 360 dias e a -20ºC superior a 160 dias. Os IE demonstraram ser estáveis por até seis dias nas temperaturas de 4 e 25ºC, mas não a 35ºC. Conclui-se que a metodologia utilizada foi satisfatória para produção de IE para o ensaio de pesquisa de Salmonella spp. em matriz queijo. ----------------------------------------------------------------------------------------------- The participation of analytical laboratories in proficiency testing allows the verification of the reliability of results in analysis of quality control. The aim of this study was to produce a batch of test items (TI to be used in a proficiency assay for Salmonella spp. research in a cheese matrix. Ultrafiltered Minas cheese was used as the matrix and spiked with a strain of Salmonella Enteritidis. Trehalose was used as cryoprotectant, and freeze-drying was used as the preservation technique. The batch was evaluated for vacuum verification, homogeneity study, and long-term stability testing at temperatures of -70ºC (reference

  13. Matrix metalloproteinases-2/9-sensitive peptide-conjugated polymer micelles for site-specific release of drugs and enhancing tumor accumulation: preparation and in vitro and in vivo evaluation

    Directory of Open Access Journals (Sweden)

    Zhang X

    2016-04-01

    Full Text Available Xiaoyan Zhang, Xiaofei Wang, Weitong Zhong, Xiaoqing Ren, Xianyi Sha, Xiaoling FangKey Laboratory of Smart Drug Delivery, Ministry of Education and People’s Liberation Army of China, School of Pharmacy, Fudan University, Shanghai, People’s Republic of China Abstract: Since elevated expression of matrix metalloproteinase (MMP-2 and MMP-9 is commonly observed in several malignant tumors, MMPs have been widely reported as key factors in the design of drug delivery systems. Several strategies have been proposed to develop MMPs-responsive nanoparticles to deliver chemotherapeutics to malignant solid tumors. A stimuli-responsive drug delivery system, which could be cleaved by MMPs, was proposed in this study. By inserting an MMP-2/9 cleavable oligopeptide GPVGLIGK-NH2 (GK8 as spacer between α-tocopherol succinate (α-TOS and methoxy-polyethylene glycol molecular weight (MW 2000 Da activated by N-hydroxysuccinimide (mPEG2K-NHS, mPEG2K-GK8-α-TOS (TGK was synthesized as the primary ingredient for MMP-2/9-sensitive micelles composed of D-α-tocopheryl polyethylene glycol 1000 succinate (TPGS and TGK (n:n =40:60, TGK micelles. mPEG2K-α-TOS (T2K was similarly synthesized as nonsensitive control. The TGK micelles showed better stability than nonsensitive micelles composed of TPGS and T2K (n:n =40:60, T2K micelles owing to the inserted peptide. Fluorescence resonance energy transfer results indicated that TGK micelles could be successfully cleaved by MMP-2/9. Effective drug release was demonstrated in the presence of collagenase type IV, a mixture of MMP-2 and MMP-9. Compared with nonsensitive micelles, docetaxel (DTX-loaded TGK micelles showed a fold higher cellular uptake in HT1080 cells. While the half-maximal inhibitory concentration (IC50 of TGK and T2K micelles were similar (P>0.05 in MCF-7 cells (MMP-2/9 underexpression, the IC50 values of the aforementioned micelles were 0.064±0.006 and 0.122±0.009 µg/mL, respectively, in HT1080 cells (MMP

  14. High-temperature wear and oxidation behaviors of TiNi/Ti2Ni matrix composite coatings with TaC addition prepared on Ti6Al4V by laser cladding

    Science.gov (United States)

    Lv, Y. H.; Li, J.; Tao, Y. F.; Hu, L. F.

    2017-04-01

    TiNi/Ti2Ni matrix composite coatings were produced on Ti6Al4V surfaces by laser cladding the mixed powders of Ni-based alloy and different contents of TaC (0, 5, 10, 15, 20, 30 and 40 wt.%). Microstructures of the coatings were investigated. High-temperature wear tests of the substrate and the coatings were carried out at 600 °C in air for 30 min. High-temperature oxidation tests of the substrate and the coatings were performed at 1000 °C in air for 50 h. Wear and oxidation mechanisms were revealed in detail. The results showed that TiNi/Ti2Ni as the matrix and TiC/TiB2/TiB as the reinforcements are the main phases of the coatings. The friction coefficients of the substrate and the coatings with different contents of TaC were 0.431 (the substrate), 0.554 (0 wt.%), 0.486 (5 wt.%), 0.457 (10 wt.%), 0.458 (15 wt.%), 0.507 (20 wt.%), 0.462 (30 wt.%) and 0.488 (40 wt.%). The wear rates of the coatings were decreased by almost 83%-98% than that of the substrate and presented a decreasing tendency with increasing TaC content. The wear mechanism of the substrate was a combination of serious oxidation, micro-cutting and brittle debonding. For the coatings, oxidation and slight scratching were predominant during wear, accompanied by slight brittle debonding in partial zones. With the increase in content of TaC, the oxidation film better shielded the coatings from destruction due to the effective friction-reducing role of Ta2O5. The oxidation rates of the substrate and the coatings with different contents of TaC at 1000 °C were 12.170 (the substrate), 5.886 (0 wt.%), 4.937 (5 wt.%), 4.517 (10 wt.%), 4.394 (15 wt.%), 3.951 (20 wt.%), 4.239 (30 wt.%) and 3.530 (40 wt.%) mg2 cm-4 h-1, respectively. The oxidation film formed outside the coating without adding TaC was composed of TiO2, NiO, Cr2O3, Al2O3 and SiO2. When TaC was added, Ta2O5 and TaC were also detected, which effectively improved the oxidation resistance of the coatings. The addition of TaC contributed to the

  15. Scandia doped tungsten matrix for impregnated cathode

    Institute of Scientific and Technical Information of China (English)

    WANG Jinshu; WANG Yanchun; LIU Wei; LI Hongyi; ZHOU Meiling

    2008-01-01

    As a matrix for Sc-type impregnated cathode,scandia doped tungsten with a uniform ldistribution of SC2O3 was obtained by powder metallurgy combined with the liquid-solid doping method.The microstructure and composition of the powder and the anti-ion bombardment behavior of scandium in the matrix were studied by means of SEM,EDS,XRD,and in-situ AES methods.Tungsten powder covered with scandium oxide,an ideal scandium oxide-doped tungsten powder for the preparation of Sc-type impregnated cathode,was obtained using the liquid-solid doping method.Compared with the matrix prepared with the mechanically mixed powder of tungsten and scandium oxide,SC2O3-W matrix prepared with this kind of powder had smaller grain size and uniform distribution of scandium.Sc on the surface of Sc2O3 doped tungsten mauix had good high temperature stability and good anti-ion bombardment capability.

  16. Patience of matrix games

    DEFF Research Database (Denmark)

    Hansen, Kristoffer Arnsfelt; Ibsen-Jensen, Rasmus; Podolskii, Vladimir V.;

    2013-01-01

    For matrix games we study how small nonzero probability must be used in optimal strategies. We show that for image win–lose–draw games (i.e. image matrix games) nonzero probabilities smaller than image are never needed. We also construct an explicit image win–lose game such that the unique optimal...

  17. Patience of matrix games

    DEFF Research Database (Denmark)

    Hansen, Kristoffer Arnsfelt; Ibsen-Jensen, Rasmus; Podolskii, Vladimir V.

    2013-01-01

    For matrix games we study how small nonzero probability must be used in optimal strategies. We show that for image win–lose–draw games (i.e. image matrix games) nonzero probabilities smaller than image are never needed. We also construct an explicit image win–lose game such that the unique optimal...

  18. Transfer function matrix

    Science.gov (United States)

    Seraji, H.

    1987-01-01

    Given a multivariable system, it is proved that the numerator matrix N(s) of the transfer function evaluated at any system pole either has unity rank or is a null matrix. It is also shown that N(s) evaluated at any transmission zero of the system has rank deficiency. Examples are given for illustration.

  19. Microstructure and Properties of Al2O3 Matrix Ceramic Coating Prepared by Thermo Chemical Reaction%热化学反应法制备Al2O3基陶瓷涂层的组织与性能

    Institute of Scientific and Technical Information of China (English)

    张媛; 周小飞

    2016-01-01

    The protective Al2O3 matrix ceramic coatings on the surface of 1Cr18Ni9 steel are prepared by thermo chemical reaction.The micro morphology,composition and structure of the combination layers were studied using SEM and EDS microanalysis instrument,and the corrosion resistance of the coating was tested by immersion corrosion experiments.The results show that the coating is dense and uniform,and there are chemical reaction between the ceramic coating and the matrix.And the existence of ceramic coating can effectively improve the corrosion resistance of 1Cr18Ni9 steel in acid and alkali.%采用热化学法在1Cr 18Ni9钢表面制备Al2O3基陶瓷涂层,利用SEM、EDS等微观分析仪器研究了结合层的微观形貌、成分及组织结构,利用浸泡腐蚀实验检测了涂层的耐蚀性.结果表明,涂层致密均匀,与基体发生了化学反应,陶瓷涂层的存在有效的提高了1Cr18Ni9钢的抗酸、碱腐蚀能力.

  20. PREPARATION OF LEUCITE-BASED COMPOSITES

    Directory of Open Access Journals (Sweden)

    Alexandra Kloužková

    2012-12-01

    Full Text Available The aim of this study was to prepare leucite dental composites from two separately synthesized components - tetragonal leucite and glassy matrix. The newly developed procedure is based on the preparation of crystalline tetragonal leucite powder by relatively low temperature synthesis under hydrothermal conditions. Matrix powder was prepared by a classical melting process and subsequent milling of the quenched glass. The dental composites were prepared by mixing of 10 wt. %, 20 wt. % and 30 wt. % of synthesized tetragonal leucite with glass powder followed by pressing and firing. The sintering process was observed by optical microscope and the optimal firing temperature for each composite was determined. Optical and electron microscopy was used to characterise the microstructure of the composites, especially the distribution of the leucite particles in the matrix. Dilatometric measurements proved that the coefficient of thermal expansion of the composites increased up to 44 % in comparison with the basic matrix.

  1. Preparation of SiO2-P (St-EMA) Nanospheres and Its Application in PP Matrix%SiO2-P(St-EMA)纳米微球的制备及在PP中的应用

    Institute of Scientific and Technical Information of China (English)

    陆璐侃; 东为富; 倪忠斌; 陈明清

    2012-01-01

    SiO1-P(St-EMA) nanospheres were prepared by grafted styrene and ethyl methacrylate on the surface of nano-SiO2 with the multistage emulsion polymerization method. The composite material of SiO2-P (St-EMA) nanospheres and polypropylene ( PP) were prepared by the melt-blending process, the mechanical and crystallization properties were investigated. The results demonstrated that SiOa-P( St-EMA) nanoapheres had a structure of sphericity composed of SiO; as core and P( St-EMA) as shell and it improved the dispersion obviously. The impact and tensile strength of SiO2-P( St-EMA)/ PP were improved significantly when the loading of SiOa-P( St-EMA) was as low as 1 % , and the heterogeneous nucleation effect of nano-SiOj increased the crystallization temperature and melting temperature.%采用多步乳液聚合法在纳米SiO2表面接枝苯乙烯(St)和甲基丙烯酸乙酯(EMA),制得具有核壳结构的SiO2-P(St- EMA)纳米微球,并通过熔融共混方法制备该微球和聚丙烯(PP)基复合材料,研究其力学性能和结晶性能.研究结果表明:SiO2-P(St-EMA)纳米微球具有以SiO2为核,P(St-EMA)为壳的核壳结构,可明显改善纳米SiO2的分散性;当SiO2-P(St-EMA)的填充量达到1%时,复合材料的拉伸强度和冲击强度就有明显的提高,并可在PP中起到异相成核作用,提高PP的结晶温度和熔融温度.

  2. Ubiquitination of specific mitochondrial matrix proteins.

    Science.gov (United States)

    Lehmann, Gilad; Ziv, Tamar; Braten, Ori; Admon, Arie; Udasin, Ronald G; Ciechanover, Aaron

    2016-06-17

    Several protein quality control systems in bacteria and/or mitochondrial matrix from lower eukaryotes are absent in higher eukaryotes. These are transfer-messenger RNA (tmRNA), The N-end rule ATP-dependent protease ClpAP, and two more ATP-dependent proteases, HslUV and ClpXP (in yeast). The lost proteases resemble the 26S proteasome and the role of tmRNA and the N-end rule in eukaryotic cytosol is performed by the ubiquitin proteasome system (UPS). Therefore, we hypothesized that the UPS might have substituted these systems - at least partially - in the mitochondrial matrix of higher eukaryotes. Using three independent experimental approaches, we demonstrated the presence of ubiquitinated proteins in the matrix of isolated yeast mitochondria. First, we show that isolated mitochondria contain ubiquitin (Ub) conjugates, which remained intact after trypsin digestion. Second, we demonstrate that the mitochondrial soluble fraction contains Ub-conjugates, several of which were identified by mass spectrometry and are localized to the matrix. Third, using immunoaffinity enrichment by specific antibodies recognizing digested ubiquitinated peptides, we identified a group of Ub-modified matrix proteins. The modification was further substantiated by separation on SDS-PAGE and immunoblots. Last, we attempted to identify the ubiquitin ligase(s) involved, and identified Dma1p as a trypsin-resistant protein in our mitochondrial preparations. Taken together, these data suggest a yet undefined role for the UPS in regulation of the mitochondrial matrix proteins.

  3. Improved Matrix Uncertainty Selector

    CERN Document Server

    Rosenbaum, Mathieu

    2011-01-01

    We consider the regression model with observation error in the design: y=X\\theta* + e, Z=X+N. Here the random vector y in R^n and the random n*p matrix Z are observed, the n*p matrix X is unknown, N is an n*p random noise matrix, e in R^n is a random noise vector, and \\theta* is a vector of unknown parameters to be estimated. We consider the setting where the dimension p can be much larger than the sample size n and \\theta* is sparse. Because of the presence of the noise matrix N, the commonly used Lasso and Dantzig selector are unstable. An alternative procedure called the Matrix Uncertainty (MU) selector has been proposed in Rosenbaum and Tsybakov (2010) in order to account for the noise. The properties of the MU selector have been studied in Rosenbaum and Tsybakov (2010) for sparse \\theta* under the assumption that the noise matrix N is deterministic and its values are small. In this paper, we propose a modification of the MU selector when N is a random matrix with zero-mean entries having the variances th...

  4. Elementary matrix theory

    CERN Document Server

    Eves, Howard

    1980-01-01

    The usefulness of matrix theory as a tool in disciplines ranging from quantum mechanics to psychometrics is widely recognized, and courses in matrix theory are increasingly a standard part of the undergraduate curriculum.This outstanding text offers an unusual introduction to matrix theory at the undergraduate level. Unlike most texts dealing with the topic, which tend to remain on an abstract level, Dr. Eves' book employs a concrete elementary approach, avoiding abstraction until the final chapter. This practical method renders the text especially accessible to students of physics, engineeri

  5. Rheocasting Al matrix composites

    Energy Technology Data Exchange (ETDEWEB)

    Girot, F.A.; Albingre, L.; Quenisset, J.M.; Naslain, R.

    1987-11-01

    A development status account is given for the rheocasting method of Al-alloy matrix/SiC-whisker composites, which involves the incorporation and homogeneous distribution of 8-15 vol pct of whiskers through the stirring of the semisolid matrix melt while retaining sufficient fluidity for casting. Both 1-, 3-, and 6-mm fibers of Nicalon SiC and and SiC whisker reinforcements have been experimentally investigated, with attention to the characterization of the resulting microstructures and the effects of fiber-matrix interactions. A thin silica layer is found at the whisker surface. 7 references.

  6. Mueller matrix differential decomposition.

    Science.gov (United States)

    Ortega-Quijano, Noé; Arce-Diego, José Luis

    2011-05-15

    We present a Mueller matrix decomposition based on the differential formulation of the Mueller calculus. The differential Mueller matrix is obtained from the macroscopic matrix through an eigenanalysis. It is subsequently resolved into the complete set of 16 differential matrices that correspond to the basic types of optical behavior for depolarizing anisotropic media. The method is successfully applied to the polarimetric analysis of several samples. The differential parameters enable one to perform an exhaustive characterization of anisotropy and depolarization. This decomposition is particularly appropriate for studying media in which several polarization effects take place simultaneously. © 2011 Optical Society of America

  7. The S228P mutation prevents in vivo and in vitro IgG4 Fab-arm exchange as demonstrated using a combination of novel quantitative immunoassays and physiological matrix preparation.

    Science.gov (United States)

    Silva, John-Paul; Vetterlein, Olivia; Jose, Joby; Peters, Shirley; Kirby, Hishani

    2015-02-27

    Human immunoglobulin G isotype 4 (IgG4) antibodies (Abs) are potential candidates for immunotherapy when reduced effector functions are desirable. IgG4 Abs are dynamic molecules able to undergo a process known as Fab arm exchange (FAE). This results in functionally monovalent, bispecific antibodies (bsAbs) with unknown specificity and hence, potentially, reduced therapeutic efficacy. IgG4 FAE is suggested to be an important biological mechanism that provides the basis for the anti-inflammatory activity attributed to IgG4 Abs. To date, the mechanism of FAE is not entirely understood and studies measuring FAE in ex vivo matrices have been hampered by the presence and abundance of endogenous IgG4 wild-type (WT) Abs. Using representative humanized WT IgG4 monoclonal Abs, namely, anti-IL-6 and anti-TNF, and a core-hinge stabilized serine 228 to proline (S228P) anti-IL-6 IgG4 mutant, it is demonstrated for the first time how anti-IgG4 affinity chromatography can be used to prepare physiologically relevant matrices for assessing and quantifying FAE. A novel method for quantifying FAE using a single MSD immunoassay is also reported and confirms previous findings that, dependent on the redox conditions, the S228P mutation can prevent IgG4 FAE to undetectable levels both in vitro and in vivo. Together, the findings and novel methodologies will allow researchers to monitor and quantify FAE of their own IgG4 molecules in physiologically relevant matrices.

  8. Pesticide-Exposure Matrix

    Science.gov (United States)

    The "Pesticide-exposure Matrix" was developed to help epidemiologists and other researchers identify the active ingredients to which people were likely exposed when their homes and gardens were treated for pests in past years.

  9. Matrix theory of gravitation

    CERN Document Server

    Koehler, Wolfgang

    2011-01-01

    A new classical theory of gravitation within the framework of general relativity is presented. It is based on a matrix formulation of four-dimensional Riemann-spaces and uses no artificial fields or adjustable parameters. The geometrical stress-energy tensor is derived from a matrix-trace Lagrangian, which is not equivalent to the curvature scalar R. To enable a direct comparison with the Einstein-theory a tetrad formalism is utilized, which shows similarities to teleparallel gravitation theories, but uses complex tetrads. Matrix theory might solve a 27-year-old, fundamental problem of those theories (sec. 4.1). For the standard test cases (PPN scheme, Schwarzschild-solution) no differences to the Einstein-theory are found. However, the matrix theory exhibits novel, interesting vacuum solutions.

  10. Matrix comparison, Part 2

    DEFF Research Database (Denmark)

    Schneider, Jesper Wiborg; Borlund, Pia

    2007-01-01

    The present two-part article introduces matrix comparison as a formal means for evaluation purposes in informetric studies such as cocitation analysis. In the first part, the motivation behind introducing matrix comparison to informetric studies, as well as two important issues influencing...... such comparisons, matrix generation, and the composition of proximity measures, are introduced and discussed. In this second part, the authors introduce and thoroughly demonstrate two related matrix comparison techniques the Mantel test and Procrustes analysis, respectively. These techniques can compare...... important. Alternatively, or as a supplement, Procrustes analysis compares the actual ordination results without investigating the underlying proximity measures, by matching two configurations of the same objects in a multidimensional space. An advantage of the Procrustes analysis though, is the graphical...

  11. A Novel MALDI Matrix for Analyzing Peptides and Proteins: Paraffin Wax Immobilized Matrix

    Institute of Scientific and Technical Information of China (English)

    WEI Yuanlong; MEI Yuan; XU Zhe; WANG Cuihong; GUO Yinlong; DU Yiping; ZHANG Weibing

    2009-01-01

    A new kind of MALDI matrix, termed paraffin wax immobilized matrix, was used to study peptide mixtures and proteins. During the preparation process, the paraffin wax was heated and coated on the stainless-steel target plate, and then 2,5-dihydrobenzoic acid (DHB) was deposited on the paraffin layer and stainless-steel target plate to obtain different kinds of matrix spots. The morphology of matrices on different supports and peptide-matrix co-crystallization were observed by a high resolution digital-video microscopy system. Peptide mixtures and bovine serum albumin (BSA) digests were used to investigate the performance of the immobilized matrices on the paraffin target. The MALDI-FTMS analysis results also showed that the detection sensitivity of matrices immobilized in the paraffin sample support was better than that on other sample supports.

  12. The Matrix Organization Revisited

    DEFF Research Database (Denmark)

    Gattiker, Urs E.; Ulhøi, John Parm

    1999-01-01

    This paper gives a short overview of matrix structure and technology management. It outlines some of the characteristics and also points out that many organizations may actualy be hybrids (i.e. mix several ways of organizing to allocate resorces effectively).......This paper gives a short overview of matrix structure and technology management. It outlines some of the characteristics and also points out that many organizations may actualy be hybrids (i.e. mix several ways of organizing to allocate resorces effectively)....

  13. Optical Coherency Matrix Tomography

    Science.gov (United States)

    2015-10-19

    optics has been studied theoretically11, but has not been demonstrated experimentally heretofore. Even in the simplest case of two binary DoFs6 (e.g...coherency matrix G spanning these DoFs. This optical coherency matrix has not been measured in its entirety to date—even in the simplest case of two...dense coding, etc. CREOL, The College of Optics & Photonics, University of Central Florida, Orlando , Florida 32816, USA. Correspondence and requests

  14. Matrix fractional systems

    Science.gov (United States)

    Tenreiro Machado, J. A.

    2015-08-01

    This paper addresses the matrix representation of dynamical systems in the perspective of fractional calculus. Fractional elements and fractional systems are interpreted under the light of the classical Cole-Cole, Davidson-Cole, and Havriliak-Negami heuristic models. Numerical simulations for an electrical circuit enlighten the results for matrix based models and high fractional orders. The conclusions clarify the distinction between fractional elements and fractional systems.

  15. Hacking the Matrix.

    Science.gov (United States)

    Czerwinski, Michael; Spence, Jason R

    2017-01-05

    Recently in Nature, Gjorevski et al. (2016) describe a fully defined synthetic hydrogel that mimics the extracellular matrix to support in vitro growth of intestinal stem cells and organoids. The hydrogel allows exquisite control over the chemical and physical in vitro niche and enables identification of regulatory properties of the matrix. Copyright © 2017 Elsevier Inc. All rights reserved.

  16. The Matrix Organization Revisited

    DEFF Research Database (Denmark)

    Gattiker, Urs E.; Ulhøi, John Parm

    1999-01-01

    This paper gives a short overview of matrix structure and technology management. It outlines some of the characteristics and also points out that many organizations may actualy be hybrids (i.e. mix several ways of organizing to allocate resorces effectively).......This paper gives a short overview of matrix structure and technology management. It outlines some of the characteristics and also points out that many organizations may actualy be hybrids (i.e. mix several ways of organizing to allocate resorces effectively)....

  17. POLYSACCHARIDE MATRIX TABLET FOR COLON SPECIFIC DRUG DELIVERY

    OpenAIRE

    Amit Kumar Panigrahi et al

    2012-01-01

    The objective of the present study was to prepare a matrix tablet for colon targeting. Natural gaums (guar gum and xanthan gum) were used for the preparation of colon targeted drug delivery system. Different concentrations of guar gum and xanthan gum and their combinations were tried for the purpose. The prepared tablets were evaluated for in-process parameters as well as colon targeting characteristics. The colon targeting properties were evaluated by analysing the formulations for drug rele...

  18. 倒相法制备PVDF-HFP基复合微孔聚合物电解质%PVDF-HFP matrix complex micro-porous polymer electrolyte prepared by phase inversion method

    Institute of Scientific and Technical Information of China (English)

    刘辉; 顾大明; 白继元

    2012-01-01

    To improve the distribution properties of nanoparticles in the polymer electrolyte,micro-porous polymer electrolyte PVDF-HFP-SiO2(OP-10) was prepared with phase inversion method by adopting nano-sized SiO2 as the inorganic filler and OP-10 as dispersant.The morphology,crystal structure and electrochemical properties of the electrolyte were characterized by scanning electron microscope(SEM),X-ray diffraction(XRD),electrochemical impedance spectra(EIS).The results showed that the addition of nano-SiO2 suppressed the crystallinity of polymer electrolyte and enhanced the tensile intensity.The ionic conductivity was improved,the highest ionic conductivity(20 ℃) of the PVDF-HFP-SiO2(OP-10) polymer electrolyte was 4.90×10-3S·cm-1,with a high electrochemical stability window of 5.3 V,and the corresponding cation transference number was 0.83.The distribution of SiO2 and interfacial compatibility of nanometer particles were improved by the addition of OP-10.%为改善纳米粒子在聚合物电解质中的分散效果,采用倒相制膜法,以纳米SiO2为填料,以OP-10为分散剂,制备复合微孔聚偏氟乙烯-六氟丙烯基电解质PVDF-HFP-SiO2(OP-10).用SEM、XRD、交流阻抗法等测试手段对电解质的微观形貌、内部结构和电化学相关性能等进行表征,结果表明:SiO2的加入降低了聚合物电解质膜的结晶度,增强了电解质的拉伸强度,提高了PVDF-HFP-SiO2(OP-10)聚合物电解质的电导率,在20℃时,可达到4.90×10-3S.cm-1,电化学稳定窗口为5.3 V,电解质的离子迁移数为0.83.分散剂OP-10的加入改善了纳米SiO2与基质的界面相容性,改善了SiO2在基质中的分散度.

  19. Study on Wear Resistance of WC Particulate Reinforced Steel Matrix Composite Prepared by Mechanical Alloying and Spark-plasma Sintering%MA-SPS法制备WC颗粒增强钢基复合材料的耐磨性研究

    Institute of Scientific and Technical Information of China (English)

    谢金乐; 刘允中; 吴汇江; 肖文华

    2011-01-01

    采用机械合金化和放电等离子体法(MA-SPS)制备了WC颗粒增强钢基复合材料,对复合材料的组织形貌、耐磨性及耐磨机理进行研究.结果表明:该方法改善了复合材料的组织形貌,晶粒比较细小且均匀;同时显著提高了材料的硬度和耐磨性,随WC含量的增加,复合材料的致密度、硬度和耐磨性增加,最高硬度达70 HRC,相比基体材料的耐磨性提高了8倍;该材料的主要磨损机制为粘着磨损和磨粒磨损.%WC participate reinforced steel matrix composite was prepared by MA-SPS (mechanical alloying and spark plasma sintering). The morphology, wear resistance and wear mechanism of the composite were studied. The results indicate that the method significantly improves the morphology. The size and distribution of the grain is very small and uniform, respectively. With the increase of WC content, the relative density, hardness and wear resistance of the composite increase. The maximum hardness is up to 70 HRC and the highest wear resistance of the composite is 8 times higher than that of the steel matrix. The main wear mechanism is adhesive wear and abrasive wear.

  20. Matrix Information Geometry

    CERN Document Server

    Bhatia, Rajendra

    2013-01-01

    This book is an outcome of the Indo-French Workshop on Matrix Information Geometries (MIG): Applications in Sensor and Cognitive Systems Engineering, which was held in Ecole Polytechnique and Thales Research and Technology Center, Palaiseau, France, in February 23-25, 2011. The workshop was generously funded by the Indo-French Centre for the Promotion of Advanced Research (IFCPAR).  During the event, 22 renowned invited french or indian speakers gave lectures on their areas of expertise within the field of matrix analysis or processing. From these talks, a total of 17 original contribution or state-of-the-art chapters have been assembled in this volume. All articles were thoroughly peer-reviewed and improved, according to the suggestions of the international referees. The 17 contributions presented  are organized in three parts: (1) State-of-the-art surveys & original matrix theory work, (2) Advanced matrix theory for radar processing, and (3) Matrix-based signal processing applications.  

  1. Ceramic Matrix Composites .

    Directory of Open Access Journals (Sweden)

    J. Mukerji

    1993-10-01

    Full Text Available The present state of the knowledge of ceramic-matrix composites have been reviewed. The fracture toughness of present structural ceramics are not enough to permit design of high performance machines with ceramic parts. They also fail by catastrophic brittle fracture. It is generally believed that further improvement of fracture toughness is only possible by making composites of ceramics with ceramic fibre, particulate or platelets. Only ceramic-matrix composites capable of working above 1000 degree centigrade has been dealt with keeping reinforced plastics and metal-reinforced ceramics outside the purview. The author has discussed the basic mechanisms of toughening and fabrication of composites and the difficulties involved. Properties of available fibres and whiskers have been given. The best results obtained so far have been indicated. The limitations of improvement in properties of ceramic-matrix composites have been discussed.

  2. Matrix interdiction problem

    Energy Technology Data Exchange (ETDEWEB)

    Pan, Feng [Los Alamos National Laboratory; Kasiviswanathan, Shiva [Los Alamos National Laboratory

    2010-01-01

    In the matrix interdiction problem, a real-valued matrix and an integer k is given. The objective is to remove k columns such that the sum over all rows of the maximum entry in each row is minimized. This combinatorial problem is closely related to bipartite network interdiction problem which can be applied to prioritize the border checkpoints in order to minimize the probability that an adversary can successfully cross the border. After introducing the matrix interdiction problem, we will prove the problem is NP-hard, and even NP-hard to approximate with an additive n{gamma} factor for a fixed constant {gamma}. We also present an algorithm for this problem that achieves a factor of (n-k) mUltiplicative approximation ratio.

  3. Extracellular matrix structure.

    Science.gov (United States)

    Theocharis, Achilleas D; Skandalis, Spyros S; Gialeli, Chrysostomi; Karamanos, Nikos K

    2016-02-01

    Extracellular matrix (ECM) is a non-cellular three-dimensional macromolecular network composed of collagens, proteoglycans/glycosaminoglycans, elastin, fibronectin, laminins, and several other glycoproteins. Matrix components bind each other as well as cell adhesion receptors forming a complex network into which cells reside in all tissues and organs. Cell surface receptors transduce signals into cells from ECM, which regulate diverse cellular functions, such as survival, growth, migration, and differentiation, and are vital for maintaining normal homeostasis. ECM is a highly dynamic structural network that continuously undergoes remodeling mediated by several matrix-degrading enzymes during normal and pathological conditions. Deregulation of ECM composition and structure is associated with the development and progression of several pathologic conditions. This article emphasizes in the complex ECM structure as to provide a better understanding of its dynamic structural and functional multipotency. Where relevant, the implication of the various families of ECM macromolecules in health and disease is also presented.

  4. Finite Temperature Matrix Theory

    CERN Document Server

    Meana, M L; Peñalba, J P; Meana, Marco Laucelli; Peñalba, Jesús Puente

    1998-01-01

    We present the way the Lorentz invariant canonical partition function for Matrix Theory as a light-cone formulation of M-theory can be computed. We explicitly show how when the eleventh dimension is decompactified, the N=1 eleven dimensional SUGRA partition function appears. From this particular analysis we also clarify the question about the discernibility problem when making statistics with supergravitons (the N! problem) in Matrix black hole configurations. We also provide a high temperature expansion which captures some structure of the canonical partition function when interactions amongst D-particles are on. The connection with the semi-classical computations thermalizing the open superstrings attached to a D-particle is also clarified through a Born-Oppenheimer approximation. Some ideas about how Matrix Theory would describe the complementary degrees of freedom of the massless content of eleven dimensional SUGRA are also discussed.

  5. Matrixed business support comparison study.

    Energy Technology Data Exchange (ETDEWEB)

    Parsons, Josh D.

    2004-11-01

    The Matrixed Business Support Comparison Study reviewed the current matrixed Chief Financial Officer (CFO) division staff models at Sandia National Laboratories. There were two primary drivers of this analysis: (1) the increasing number of financial staff matrixed to mission customers and (2) the desire to further understand the matrix process and the opportunities and challenges it creates.

  6. IIB Matrix Model

    CERN Document Server

    Aoki, H; Kawai, H; Kitazawa, Y; Tada, T; Tsuchiya, A

    1999-01-01

    We review our proposal for a constructive definition of superstring, type IIB matrix model. The IIB matrix model is a manifestly covariant model for space-time and matter which possesses N=2 supersymmetry in ten dimensions. We refine our arguments to reproduce string perturbation theory based on the loop equations. We emphasize that the space-time is dynamically determined from the eigenvalue distributions of the matrices. We also explain how matter, gauge fields and gravitation appear as fluctuations around dynamically determined space-time.

  7. Little IIB Matrix Model

    CERN Document Server

    Kitazawa, Y; Saito, O; Kitazawa, Yoshihisa; Mizoguchi, Shun'ya; Saito, Osamu

    2006-01-01

    We study the zero-dimensional reduced model of D=6 pure super Yang-Mills theory and argue that the large N limit describes the (2,0) Little String Theory. The one-loop effective action shows that the force exerted between two diagonal blocks of matrices behaves as 1/r^4, implying a six-dimensional spacetime. We also observe that it is due to non-gravitational interactions. We construct wave functions and vertex operators which realize the D=6, (2,0) tensor representation. We also comment on other "little" analogues of the IIB matrix model and Matrix Theory with less supercharges.

  8. Elementary matrix algebra

    CERN Document Server

    Hohn, Franz E

    2012-01-01

    This complete and coherent exposition, complemented by numerous illustrative examples, offers readers a text that can teach by itself. Fully rigorous in its treatment, it offers a mathematically sound sequencing of topics. The work starts with the most basic laws of matrix algebra and progresses to the sweep-out process for obtaining the complete solution of any given system of linear equations - homogeneous or nonhomogeneous - and the role of matrix algebra in the presentation of useful geometric ideas, techniques, and terminology.Other subjects include the complete treatment of the structur

  9. Reduced Google matrix

    CERN Document Server

    Frahm, K M

    2016-01-01

    Using parallels with the quantum scattering theory, developed for processes in nuclear and mesoscopic physics and quantum chaos, we construct a reduced Google matrix $G_R$ which describes the properties and interactions of a certain subset of selected nodes belonging to a much larger directed network. The matrix $G_R$ takes into account effective interactions between subset nodes by all their indirect links via the whole network. We argue that this approach gives new possibilities to analyze effective interactions in a group of nodes embedded in a large directed networks. Possible efficient numerical methods for the practical computation of $G_R$ are also described.

  10. Density matrix perturbation theory.

    Science.gov (United States)

    Niklasson, Anders M N; Challacombe, Matt

    2004-05-14

    An orbital-free quantum perturbation theory is proposed. It gives the response of the density matrix upon variation of the Hamiltonian by quadratically convergent recursions based on perturbed projections. The technique allows treatment of embedded quantum subsystems with a computational cost scaling linearly with the size of the perturbed region, O(N(pert.)), and as O(1) with the total system size. The method allows efficient high order perturbation expansions, as demonstrated with an example involving a 10th order expansion. Density matrix analogs of Wigner's 2n+1 rule are also presented.

  11. Complex matrix model duality

    Energy Technology Data Exchange (ETDEWEB)

    Brown, T.W.

    2010-11-15

    The same complex matrix model calculates both tachyon scattering for the c=1 non-critical string at the self-dual radius and certain correlation functions of half-BPS operators in N=4 super- Yang-Mills. It is dual to another complex matrix model where the couplings of the first model are encoded in the Kontsevich-like variables of the second. The duality between the theories is mirrored by the duality of their Feynman diagrams. Analogously to the Hermitian Kontsevich- Penner model, the correlation functions of the second model can be written as sums over discrete points in subspaces of the moduli space of punctured Riemann surfaces. (orig.)

  12. Transverse fracture and fiber/matrix interface characteristics of hybrid ceramic matrix composites

    Science.gov (United States)

    Haug, Stephen Berry

    Ceramic Matrix Composites (CMCs) represent an attractive class of engineering materials for use in high temperature, high wear and corrosive environments. Much effort has been made to ascertain and improve the strength and fracture characteristics of these materials. Approaches that have received a significant amount of attention include enhancing a ceramic material's mechanical properties through the use of continuous fiber reinforcement; fine, randomly dispersed discontinuous fiber (or whisker) reinforcement; and a hybrid combination of both continuous and discontinuous fibers. This dissertation addresses two important aspects of determining and improving the strength and toughness of CMCs and is comprised of three research papers that have been prepared for journal publication. The first paper, "Transverse Fracture Toughness of Unidirectional Continuous Fiber and Hybrid Ceramic Matrix Composites" provides the results of three-point chevron-notched-beam fracture toughness testing and demonstrates a significant improvement in transverse fracture toughness can be obtained through the use of hybrid fiber reinforcements. The second paper, "A Tensile Testing Method for Ceramic Matrix Composites" presents a novel approach to testing small brittle material specimens using conventional testing equipment with minimal specialized fixture components. The third paper, "Fiber/Matrix Interface Properties of Hybrid Ceramic Matrix Composites", presents a method of determining the characteristics of the fiber/matrix interface of a continuous fiber reinforced CMC and a related hybrid CMC reinforced by both continuous fibers and finely dispersed whiskers using a multiple fiber pullout technique.

  13. Dynamic Matrix Rank

    DEFF Research Database (Denmark)

    Frandsen, Gudmund Skovbjerg; Frandsen, Peter Frands

    2009-01-01

    We consider maintaining information about the rank of a matrix under changes of the entries. For n×n matrices, we show an upper bound of O(n1.575) arithmetic operations and a lower bound of Ω(n) arithmetic operations per element change. The upper bound is valid when changing up to O(n0.575) entri...... closed fields. The upper bound for element updates uses fast rectangular matrix multiplication, and the lower bound involves further development of an earlier technique for proving lower bounds for dynamic computation of rational functions.......We consider maintaining information about the rank of a matrix under changes of the entries. For n×n matrices, we show an upper bound of O(n1.575) arithmetic operations and a lower bound of Ω(n) arithmetic operations per element change. The upper bound is valid when changing up to O(n0.575) entries...... in a single column of the matrix. We also give an algorithm that maintains the rank using O(n2) arithmetic operations per rank one update. These bounds appear to be the first nontrivial bounds for the problem. The upper bounds are valid for arbitrary fields, whereas the lower bound is valid for algebraically...

  14. Empirical codon substitution matrix

    Directory of Open Access Journals (Sweden)

    Gonnet Gaston H

    2005-06-01

    Full Text Available Abstract Background Codon substitution probabilities are used in many types of molecular evolution studies such as determining Ka/Ks ratios, creating ancestral DNA sequences or aligning coding DNA. Until the recent dramatic increase in genomic data enabled construction of empirical matrices, researchers relied on parameterized models of codon evolution. Here we present the first empirical codon substitution matrix entirely built from alignments of coding sequences from vertebrate DNA and thus provide an alternative to parameterized models of codon evolution. Results A set of 17,502 alignments of orthologous sequences from five vertebrate genomes yielded 8.3 million aligned codons from which the number of substitutions between codons were counted. From this data, both a probability matrix and a matrix of similarity scores were computed. They are 64 × 64 matrices describing the substitutions between all codons. Substitutions from sense codons to stop codons are not considered, resulting in block diagonal matrices consisting of 61 × 61 entries for the sense codons and 3 × 3 entries for the stop codons. Conclusion The amount of genomic data currently available allowed for the construction of an empirical codon substitution matrix. However, more sequence data is still needed to construct matrices from different subsets of DNA, specific to kingdoms, evolutionary distance or different amount of synonymous change. Codon mutation matrices have advantages for alignments up to medium evolutionary distances and for usages that require DNA such as ancestral reconstruction of DNA sequences and the calculation of Ka/Ks ratios.

  15. Matrix Embedded Organic Synthesis

    Science.gov (United States)

    Kamakolanu, U. G.; Freund, F. T.

    2016-05-01

    In the matrix of minerals such as olivine, a redox reaction of the low-z elements occurs. Oxygen is oxidized to the peroxy state while the low-Z-elements become chemically reduced. We assign them a formula [CxHyOzNiSj]n- and call them proto-organics.

  16. CO2 Removal from Biogas Using Carbon Nanotubes Mixed Matrix Membranes

    OpenAIRE

    Tutuk Djoko Kusworo; Ahmad Fauzi Ismail; Budiyono; I Nyoman Widiasa; Seno Johari; Sunarso

    2010-01-01

    A new type of mixed matrix membrane consisting of polyethersulfone (PES) and carbon nanotubes (CNTs) is prepared for biogas purification application. PES mixed matrix membrane with and without modification of carbon nanotubes were prepared by a dry/wet phase inversion technique using a pneumatically membrane casting machine system. The modified carbon nanotubes were prepared by treating the carbon nanotubes with chemical modification using acid treatment to allow PES chains to be grafted on c...

  17. Matricial bridges for "Matrix algebras converge to the sphere"

    CERN Document Server

    Rieffel, Marc A

    2015-01-01

    In the high-energy quantum-physics literature one finds statements such as "matrix algebras converge to the sphere". Earlier I provided a general setting for understanding such statements, in which the matrix algebras are viewed as quantum metric spaces, and convergence is with respect to a quantum Gromov-Hausdorff-type distance. In the present paper, as preparation of discussing similar statements for convergence of "vector bundles" over matrix algebras to vector bundles over spaces, we introduce and study suitable matrix-norms for matrix algebras and spaces. Very recently Latremoliere introduced an improved quantum Gromov-Hausdorff-type distance between quantum metric spaces. We use it throughout this paper. To facilitate the calculations we introduce and develop a general notion of "bridges with conditional expectations".

  18. Solution preparation

    Energy Technology Data Exchange (ETDEWEB)

    Seitz, M.G.

    1982-01-01

    Reviewed in this statement are methods of preparing solutions to be used in laboratory experiments to examine technical issues related to the safe disposal of nuclear waste from power generation. Each approach currently used to prepare solutions has advantages and any one approach may be preferred over the others in particular situations, depending upon the goals of the experimental program. These advantages are highlighted herein for three approaches to solution preparation that are currently used most in studies of nuclear waste disposal. Discussion of the disadvantages of each approach is presented to help a user select a preparation method for his particular studies. Also presented in this statement are general observations regarding solution preparation. These observations are used as examples of the types of concerns that need to be addressed regarding solution preparation. As shown by these examples, prior to experimentation or chemical analyses, laboratory techniques based on scientific knowledge of solutions can be applied to solutions, often resulting in great improvement in the usefulness of results.

  19. CNTs Modified and Enhanced Cu Matrix Composites

    Directory of Open Access Journals (Sweden)

    ZHANG Wen-zhong

    2016-12-01

    Full Text Available The composite powders of 2%-CNTs were prepared by wet ball milling and hydrogen annealing treatment-cold pressing sintering was used to consolidate the ball milled composite powders with different modifications of the CNTs. The results show that the length of the CNTs is shortened, ports are open, and amorphous carbon content is increased by ball milling. And after a mixed acid purification, the impurity on the surface of the CNTs is completely removed,and a large number of oxygen-containing reactive groups are introduced; the most of CNTs can be embedded in the Cu matrix and the CNTs have a close bonding with the Cu matrix, forming the lamellar composite structure, then, ultrafine-grained composite powders can be obtained by hydrogen annealing treatment. Shortening and purification of the CNTs are both good for dispersion and bonding of CNTs in the Cu matrix, and the tensile strength and hardness of the composites after shortening and purification reaches the highest, and is 296MPa and 139.8HV respectively, compared to the matrix, up to 123.6% in tensile strength and 42.9% in hardness, attributed to the fine grain strengthening and load transferring.

  20. Matrix string theory

    Science.gov (United States)

    Dijkgraaf, Robbert; Verlinde, Erik; Verlinde, Herman

    1997-02-01

    Via compactification on a circle, the matrix mode] of M-theory proposed by Banks et a]. suggests a concrete identification between the large N limit of two-dimensional N = 8 supersymmetric Yang-Mills theory and type IIA string theory. In this paper we collect evidence that supports this identification. We explicitly identify the perturbative string states and their interactions, and describe the appearance of D-particle and D-membrane states.

  1. Matrix string theory

    Energy Technology Data Exchange (ETDEWEB)

    Dijkgraaf, R. [Amsterdam Univ. (Netherlands). Dept. of Mathematics; Verlinde, E. [TH-Division, CERN, CH-1211 Geneva 23 (Switzerland)]|[Institute for Theoretical Physics, Universtity of Utrecht, 3508 TA Utrecht (Netherlands); Verlinde, H. [Institute for Theoretical Physics, University of Amsterdam, 1018 XE Amsterdam (Netherlands)

    1997-09-01

    Via compactification on a circle, the matrix model of M-theory proposed by Banks et al. suggests a concrete identification between the large N limit of two-dimensional N=8 supersymmetric Yang-Mills theory and type IIA string theory. In this paper we collect evidence that supports this identification. We explicitly identify the perturbative string states and their interactions, and describe the appearance of D-particle and D-membrane states. (orig.).

  2. Matrix String Theory

    CERN Document Server

    Dijkgraaf, R; Verlinde, Herman L

    1997-01-01

    Via compactification on a circle, the matrix model of M-theory proposed by Banks et al suggests a concrete identification between the large N limit of two-dimensional N=8 supersymmetric Yang-Mills theory and type IIA string theory. In this paper we collect evidence that supports this identification. We explicitly identify the perturbative string states and their interactions, and describe the appearance of D-particle and D-membrane states.

  3. Holomorphic matrix integrals

    CERN Document Server

    Felder, G; Felder, Giovanni; Riser, Roman

    2004-01-01

    We study a class of holomorphic matrix models. The integrals are taken over middle dimensional cycles in the space of complex square matrices. As the size of the matrices tends to infinity, the distribution of eigenvalues is given by a measure with support on a collection of arcs in the complex planes. We show that the arcs are level sets of the imaginary part of a hyperelliptic integral connecting branch points.

  4. Metal matrix Composites

    Directory of Open Access Journals (Sweden)

    Pradeep K. Rohatgi

    1993-10-01

    Full Text Available This paper reviews the world wide upsurge in metal matrix composite research and development activities with particular emphasis on cast metal-matrix particulate composites. Extensive applications of cast aluminium alloy MMCs in day-to-day use in transportation as well as durable good industries are expected to advance rapidly in the next decade. The potential for extensive application of cast composites is very large in India, especially in the areas of transportation, energy and electromechanical machinery; the extensive use of composites can lead to large savings in materials and energy, and in several instances, reduce environmental pollution. It is important that engineering education and short-term courses be organized to bring MMCs to the attention of students and engineering industry leaders. India already has excellent infrastructure for development of composites, and has a long track record of world class research in cast metal matrix particulate composites. It is now necessary to catalyze prototype and regular production of selected composite components, and get them used in different sectors, especially railways, cars, trucks, buses, scooters and other electromechanical machinery. This will require suitable policies backed up by funding to bring together the first rate talent in cast composites which already exists in India, to form viable development groups followed by setting up of production plants involving the process engineering capability already available within the country. On the longer term, cast composites should be developed for use in energy generation equipment, electronic packaging aerospace systems, and smart structures.

  5. Weierstrass preparation and algebraic invariants

    CERN Document Server

    Harbater, David; Krashen, Daniel

    2011-01-01

    We prove a form of the Weierstrass Preparation Theorem for normal algebraic curves over complete discrete valuation rings. While the more traditional algebraic form of Weierstrass Preparation applies just to the projective line over a base, our version allows more general curves. This result is then used to obtain applications concerning the values of u-invariants, and on the period-index problem for division algebras, over fraction fields of complete two-dimensional rings. Our approach uses patching methods and matrix factorization results that can be viewed as analogs of Cartan's Lemma.

  6. Matrix Theory of Small Oscillations

    Science.gov (United States)

    Chavda, L. K.

    1978-01-01

    A complete matrix formulation of the theory of small oscillations is presented. Simple analytic solutions involving matrix functions are found which clearly exhibit the transients, the damping factors, the Breit-Wigner form for resonances, etc. (BB)

  7. Matrix Completions and Chordal Graphs

    Institute of Scientific and Technical Information of China (English)

    Kenneth John HARRISON

    2003-01-01

    In a matrix-completion problem the aim is to specifiy the missing entries of a matrix inorder to produce a matrix with particular properties. In this paper we survey results concerning matrix-completion problems where we look for completions of various types for partial matrices supported ona given pattern. We see that thc existence of completions of the required type often depends on thechordal properties of graphs associated with the pattern.

  8. THE GENERALIZED POLARIZATION SCATTERING MATRIX

    Science.gov (United States)

    the Least Square Best Estimate of the Generalized Polarization matrix from a set of measurements is then developed. It is shown that the Faraday...matrix data. It is then shown that the Least Square Best Estimate of the orientation angle of a symmetric target is also determinable from Faraday rotation contaminated short pulse monostatic polarization matrix data.

  9. Preparation of monoclonal antibodies to nuclear matrix proteins of tissues surrounding esophagus cancer and its preliminary identification%食管癌旁组织核基质蛋白单克隆抗体的制备及初步鉴定

    Institute of Scientific and Technical Information of China (English)

    张新梅; 林汉良; 刘乐和; 张昌卿; 钟叔平; 曾金云; 郑克立

    2000-01-01

    目的 制备抗食管癌旁组织核基质蛋白的特异性单抗。方法 SDS-PAGE分析正常食管组织、食管癌旁组织及 食管癌组织核基质蛋白间的差异。用食管癌旁组织核基质蛋白做免疫原免疫Balb/c小鼠,利用杂交瘤技术制备了5株能稳定 分泌单克隆抗体的杂交瘤细胞株,并对9-1-2/D、9-1-7/D 2株细胞作了初步鉴定。结果 免疫组化分析发现9-1-2/D单抗与食管 癌及正常食管组织均有反应,而9-1-7/D单抗只与食管癌组织反应,与正常食管组织无反应。Western Blotting分析显示: 9-1-2/D单抗与电泳图谱上正常食管组织核基质和食管癌旁组织核基质52 kD的蛋白反应,而与食管癌组织核基质55 kD的蛋 白反应。9-1-7/D单抗只与电泳图谱上食管癌旁组织及癌组织核基质46 kD的蛋白反应,与正常食管组织核基质无反应。结论 本实验为食管癌的早期诊断作了初步有意义的探讨。%Objective To prepare anti-nuclear matrix proteins of tissues surrounding esophagus cancer monoclonal anti- bodies. Methods Differences among nuclear matrix proteins (NMPS) of normal esophagus tissues, esophagus cancer tissues and tissues adjacent to cancer were identified by SDS-PAGE. Balb/c mouse were hyperimmunized with NMPS of tissues adja- cent to esophagus cancer. Five mouse lymphocyte hybridoma cell lines were established and preliminary identification of cell lines 9-1-2/D, 9-1-7/D were made. Results Immunohistochemical analysis showed monoclonal antibody 9-1-2/D reacted both with esophagus cancer and normal esophageal tissues; monoclonal antibody 9-1-7/D reacted only with nucleoli of esophagus cancer cells. Western Blotting analysis showed monoclonal antibody 9-1-2/D reacted with 52 kD NMPS of normal esophagus tissues and tissues adjacent to esophagus cancer and reacted with 55 kD NMP of esophagus cancer tissue. Monoclonal anti- body 9-1-7/D reacted only with 46 kD protein of esophagus cancer

  10. Carbon Fiber Reinforced Glass Matrix Composites for Space Based Applications.

    Science.gov (United States)

    1987-08-31

    composite plates were prepared using standard i, c-pressing procedures. The plates were cut into tensile specimens which were then subsequently notched...reinforced HMU composites were prepared using the matrix compositions and hot-pressing parameters shown in Table VI-1. The compositions are identical...shown in Figure VI-6. Traces of a- cristobalite are present in all three composites, with a noticeably larger amount present in the Nb20 5 composite. All

  11. The cellulose resource matrix.

    Science.gov (United States)

    Keijsers, Edwin R P; Yılmaz, Gülden; van Dam, Jan E G

    2013-03-01

    The emerging biobased economy is causing shifts from mineral fossil oil based resources towards renewable resources. Because of market mechanisms, current and new industries utilising renewable commodities, will attempt to secure their supply of resources. Cellulose is among these commodities, where large scale competition can be expected and already is observed for the traditional industries such as the paper industry. Cellulose and lignocellulosic raw materials (like wood and non-wood fibre crops) are being utilised in many industrial sectors. Due to the initiated transition towards biobased economy, these raw materials are intensively investigated also for new applications such as 2nd generation biofuels and 'green' chemicals and materials production (Clark, 2007; Lange, 2007; Petrus & Noordermeer, 2006; Ragauskas et al., 2006; Regalbuto, 2009). As lignocellulosic raw materials are available in variable quantities and qualities, unnecessary competition can be avoided via the choice of suitable raw materials for a target application. For example, utilisation of cellulose as carbohydrate source for ethanol production (Kabir Kazi et al., 2010) avoids the discussed competition with easier digestible carbohydrates (sugars, starch) deprived from the food supply chain. Also for cellulose use as a biopolymer several different competing markets can be distinguished. It is clear that these applications and markets will be influenced by large volume shifts. The world will have to reckon with the increase of competition and feedstock shortage (land use/biodiversity) (van Dam, de Klerk-Engels, Struik, & Rabbinge, 2005). It is of interest - in the context of sustainable development of the bioeconomy - to categorize the already available and emerging lignocellulosic resources in a matrix structure. When composing such "cellulose resource matrix" attention should be given to the quality aspects as well as to the available quantities and practical possibilities of processing the

  12. Matrix string partition function

    CERN Document Server

    Kostov, Ivan K; Kostov, Ivan K.; Vanhove, Pierre

    1998-01-01

    We evaluate quasiclassically the Ramond partition function of Euclidean D=10 U(N) super Yang-Mills theory reduced to a two-dimensional torus. The result can be interpreted in terms of free strings wrapping the space-time torus, as expected from the point of view of Matrix string theory. We demonstrate that, when extrapolated to the ultraviolet limit (small area of the torus), the quasiclassical expressions reproduce exactly the recently obtained expression for the partition of the completely reduced SYM theory, including the overall numerical factor. This is an evidence that our quasiclassical calculation might be exact.

  13. Matrix vector analysis

    CERN Document Server

    Eisenman, Richard L

    2005-01-01

    This outstanding text and reference applies matrix ideas to vector methods, using physical ideas to illustrate and motivate mathematical concepts but employing a mathematical continuity of development rather than a physical approach. The author, who taught at the U.S. Air Force Academy, dispenses with the artificial barrier between vectors and matrices--and more generally, between pure and applied mathematics.Motivated examples introduce each idea, with interpretations of physical, algebraic, and geometric contexts, in addition to generalizations to theorems that reflect the essential structur

  14. Random matrix theory

    CERN Document Server

    Deift, Percy

    2009-01-01

    This book features a unified derivation of the mathematical theory of the three classical types of invariant random matrix ensembles-orthogonal, unitary, and symplectic. The authors follow the approach of Tracy and Widom, but the exposition here contains a substantial amount of additional material, in particular, facts from functional analysis and the theory of Pfaffians. The main result in the book is a proof of universality for orthogonal and symplectic ensembles corresponding to generalized Gaussian type weights following the authors' prior work. New, quantitative error estimates are derive

  15. Supported Molecular Matrix Electrophoresis.

    Science.gov (United States)

    Matsuno, Yu-Ki; Kameyama, Akihiko

    2015-01-01

    Mucins are difficult to separate using conventional gel electrophoresis methods such as SDS-PAGE and agarose gel electrophoresis, owing to their large size and heterogeneity. On the other hand, cellulose acetate membrane electrophoresis can separate these molecules, but is not compatible with glycan analysis. Here, we describe a novel membrane electrophoresis technique, termed "supported molecular matrix electrophoresis" (SMME), in which a porous polyvinylidene difluoride (PVDF) membrane filter is used to achieve separation. This description includes the separation, visualization, and glycan analysis of mucins with the SMME technique.

  16. Matrix algebra for linear models

    CERN Document Server

    Gruber, Marvin H J

    2013-01-01

    Matrix methods have evolved from a tool for expressing statistical problems to an indispensable part of the development, understanding, and use of various types of complex statistical analyses. This evolution has made matrix methods a vital part of statistical education. Traditionally, matrix methods are taught in courses on everything from regression analysis to stochastic processes, thus creating a fractured view of the topic. Matrix Algebra for Linear Models offers readers a unique, unified view of matrix analysis theory (where and when necessary), methods, and their applications. Written f

  17. Difluoromethane preparation

    NARCIS (Netherlands)

    Wiersma, A.; Sandt, E.J.A.; Van Bekkum, H.; Makkee, M.; Moulijn, J.A.

    1996-01-01

    Abstract of NL 9401574 (A) The invention relates to a method for preparing difluoromethane, wherein dichlorodifluoromethane or monochlorodifluoromethane is brought into contact with hydrogen in the presence of palladium on activated carbon, wherein the loading of the palladium on the activated c

  18. Formulation and Characterization of Matrix and Triple-Layer matrix tablets for Controlled Delivery of Metoprolol tartrate

    Directory of Open Access Journals (Sweden)

    Izhar Ahmed Syed

    2011-01-01

    Full Text Available In the present study matrix and triple layer matrix tablets of metoprolol tartrate were formulated by using xanthan gum as the matrix forming agent and Sodium Carboxy Methyl Cellulose (Na CMC as barrier layers. The prepared tablets were analysed for their hardness, friability, drug content and in-vitro drug release studies. Marked differences in dissolution characteristics of (M3 and (M3L3 were observed and showed a significant difference statistically. Mean dissolution time (MDT for M3 and M3L3 were found to be 4.02h and 12.75h, while dissolution efficiency (DE8% decreased, indicating that the release of metoprolol tartrate is slower from triple layer matrix tablets. The finding of the study indicated that the matrix tablets prolonged the release, but predominantly in a first order kinetics. Layering with Na CMC granules on the matrix core, provided linear drug release with zero order kinetics. The triple layer matrix tablets (M3L3 shows precise controlled release of the drug than that of plain matrix tablets. FT-IR and DSC studies confirmed that there was no chemical interaction between drug and excipients used in the formulation.

  19. Extracellular Matrix Proteins

    Directory of Open Access Journals (Sweden)

    Linda Christian Carrijo-Carvalho

    2012-01-01

    Full Text Available Lipocalin family members have been implicated in development, regeneration, and pathological processes, but their roles are unclear. Interestingly, these proteins are found abundant in the venom of the Lonomia obliqua caterpillar. Lipocalins are β-barrel proteins, which have three conserved motifs in their amino acid sequence. One of these motifs was shown to be a sequence signature involved in cell modulation. The aim of this study is to investigate the effects of a synthetic peptide comprising the lipocalin sequence motif in fibroblasts. This peptide suppressed caspase 3 activity and upregulated Bcl-2 and Ki-67, but did not interfere with GPCR calcium mobilization. Fibroblast responses also involved increased expression of proinflammatory mediators. Increase of extracellular matrix proteins, such as collagen, fibronectin, and tenascin, was observed. Increase in collagen content was also observed in vivo. Results indicate that modulation effects displayed by lipocalins through this sequence motif involve cell survival, extracellular matrix remodeling, and cytokine signaling. Such effects can be related to the lipocalin roles in disease, development, and tissue repair.

  20. SALTSTONE MATRIX CHARACTERIZATION AND STADIUM SIMULATION RESULTS

    Energy Technology Data Exchange (ETDEWEB)

    Langton, C.

    2009-07-30

    SIMCO Technologies, Inc. was contracted to evaluate the durability of the saltstone matrix material and to measure saltstone transport properties. This information will be used to: (1) Parameterize the STADIUM{reg_sign} service life code, (2) Predict the leach rate (degradation rate) for the saltstone matrix over 10,000 years using the STADIUM{reg_sign} concrete service life code, and (3) Validate the modeled results by conducting leaching (water immersion) tests. Saltstone durability for this evaluation is limited to changes in the matrix itself and does not include changes in the chemical speciation of the contaminants in the saltstone. This report summarized results obtained to date which include: characterization data for saltstone cured up to 365 days and characterization of saltstone cured for 137 days and immersed in water for 31 days. Chemicals for preparing simulated non-radioactive salt solution were obtained from chemical suppliers. The saltstone slurry was mixed according to directions provided by SRNL. However SIMCO Technologies Inc. personnel made a mistake in the premix proportions. The formulation SIMCO personnel used to prepare saltstone premix was not the reference mix proportions: 45 wt% slag, 45 wt% fly ash, and 10 wt% cement. SIMCO Technologies Inc. personnel used the following proportions: 21 wt% slag, 65 wt% fly ash, and 14 wt% cement. The mistake was acknowledged and new mixes have been prepared and are curing. The results presented in this report are assumed to be conservative since the excessive fly ash was used in the SIMCO saltstone. The SIMCO mixes are low in slag which is very reactive in the caustic salt solution. The impact is that the results presented in this report are expected to be conservative since the samples prepared were deficient in slag and contained excess fly ash. The hydraulic reactivity of slag is about four times that of fly ash so the amount of hydrated binder formed per unit volume in the SIMCO saltstone samples is

  1. Crosslinked collagen/chitosan matrix for artificial livers

    NARCIS (Netherlands)

    Wang, X.H.; Li, D.P.; Wang, W.J.; Feng, Q.L.; Cui, F.Z.; Xu, Y.X.; Song, X.H.; Werf, van der Mark

    2003-01-01

    Matrices composed of collagen and chitosan may create an appropriate environment for the regeneration of livers. In this study, we have prepared, characterized and evaluated a new collagen/chitosan matrix (CCM). The CCM was made by using crosslinking agent 1-ethyl-3-(3-dimethylaminopropyl)-carbodiim

  2. Mixed-matrix membrane adsorbers for protein separation

    NARCIS (Netherlands)

    Avramescu, Maria-Elena; Borneman, Zandrie; Wessling, Matthias

    2003-01-01

    The separation of two similarly sized proteins, bovine serum albumin (BSA) and bovine hemoglobin (Hb) was carried out using a new type of ion-exchange mixed-matrix adsorber membranes. The adsorber membranes were prepared by incorporation of various types of Lewatit ion-exchange resins into an ethyle

  3. Cross-linked leucaena seed gum matrix: an affinity chromatography tool for galactose-specific lectins.

    Science.gov (United States)

    Seshagirirao, Kottapalli; Leelavathi, Chaganti; Sasidhar, Vemula

    2005-05-31

    A cross-linked leucaena (Leucaena leucocephala) seed gum (CLLSG) matrix was prepared for the isolation of galactose-specific lectins by affinity chromatography. The matrix was evaluated for affinity with a known galactose-specific lectin from the seeds of snake gourd (Trichosanthes anguina). The matrix preparation was simple and inexpensive when compared to commercial galactose-specific matrices (i.e. about 1.5 US dollars/100 ml of matrix). The current method is also useful for the demonstration of the affinity chromatography technique in laboratories. Since leucaena seeds are abundant and inexpensive, and the matrix preparation is easy, CLLSG appears to be a promising tool for the separation of galactose-specific lectins.

  4. CO2 Removal from Biogas Using Carbon Nanotubes Mixed Matrix Membranes

    Directory of Open Access Journals (Sweden)

    Tutuk Djoko Kusworo

    2010-07-01

    Full Text Available A new type of mixed matrix membrane consisting of polyethersulfone (PES and carbon nanotubes (CNTs is prepared for biogas purification application. PES mixed matrix membrane with and without modification of carbon nanotubes were prepared by a dry/wet phase inversion technique using a pneumatically membrane casting machine system. The modified carbon nanotubes were prepared by treating the carbon nanotubes with chemical modification using acid treatment to allow PES chains to be grafted on carbon nanotubes surface. The results from the FESEM, DSC and FTIR analysis confirmed that chemical modification on carbon nanotubes surface had taken place. Meanwhile, the nanogaps in the interface of polymer and carbon nanotubes were appeared in the PES mixed matrix membrane with unmodified of carbon nanotubes. The modified carbon nanotubes mixed matrix membrane increases the mechanical properties and the permeability of all gases. For PES-modified carbon nanotubes mixed matrix membrane the maximum selectivity achieved for CO2/CH4 is 23.54

  5. Experimental investigations on mechanical behavior of aluminium metal matrix composites

    Science.gov (United States)

    Rajesh, A. M.; Kaleemulla, Mohammed

    2016-09-01

    Today we are widely using aluminium based metal matrix composite for structural, aerospace, marine and automobile applications for its light weight, high strength and low production cost. The purpose of designing metal matrix composite is to add the desirable attributes of metals and ceramics to the base metal. In this study we developed aluminium metal matrix hybrid composite by reinforced Aluminium7075 alloy with silicon carbide (SiC) and aluminium oxide (alumina) by method of stir casting. This technique is less expensive and very effective. The Hardness test and Wear test were performed on the specimens which are prepared by stir casting techniques. The result reveals that the addition of silicon carbide and alumina particles in aluminium matrix improves the mechanical properties.

  6. Mixed Matrix Silicone and Fluorosilicone/Zeolite 4A Membranes for Ethanol Dehydration by Pervaporation

    Science.gov (United States)

    The ability of homogeneous and mixed matrix membranes prepared using standard silicone rubber, poly(dimethylsiloxane) (PDMS), and fluorosilicone rubber, poly(trifluoropropylmethylsiloxane) (PTFPMS), to dehydrate ethanol by pervaporation was evaluated. Although PDMS is generally c...

  7. Matrix Quantization of Turbulence

    CERN Document Server

    Floratos, Emmanuel

    2011-01-01

    Based on our recent work on Quantum Nambu Mechanics $\\cite{af2}$, we provide an explicit quantization of the Lorenz chaotic attractor through the introduction of Non-commutative phase space coordinates as Hermitian $ N \\times N $ matrices in $ R^{3}$. For the volume preserving part, they satisfy the commutation relations induced by one of the two Nambu Hamiltonians, the second one generating a unique time evolution. Dissipation is incorporated quantum mechanically in a self-consistent way having the correct classical limit without the introduction of external degrees of freedom. Due to its volume phase space contraction it violates the quantum commutation relations. We demonstrate that the Heisenberg-Nambu evolution equations for the Matrix Lorenz system develop fast decoherence to N independent Lorenz attractors. On the other hand there is a weak dissipation regime, where the quantum mechanical properties of the volume preserving non-dissipative sector survive for long times.

  8. Matrix Graph Grammars

    CERN Document Server

    Velasco, Pedro Pablo Perez

    2008-01-01

    This book objective is to develop an algebraization of graph grammars. Equivalently, we study graph dynamics. From the point of view of a computer scientist, graph grammars are a natural generalization of Chomsky grammars for which a purely algebraic approach does not exist up to now. A Chomsky (or string) grammar is, roughly speaking, a precise description of a formal language (which in essence is a set of strings). On a more discrete mathematical style, it can be said that graph grammars -- Matrix Graph Grammars in particular -- study dynamics of graphs. Ideally, this algebraization would enforce our understanding of grammars in general, providing new analysis techniques and generalizations of concepts, problems and results known so far.

  9. Matrix anticirculant calculus

    Science.gov (United States)

    Dimiev, Stancho; Stoev, Peter; Stoilova, Stanislava

    2013-12-01

    The notion of anticirculant is ordinary of interest for specialists of general algebra (to see for instance [1]). In this paper we develop some aspects of anticirculants in real function theory. Denoting by X≔x0+jx1+⋯+jmxm, xk∈R, m+1 = 2n, and jk is the k-th degree of the matrix j = (0100...00010...00001...0..................-1000...0), we study the functional anticirculants f(X)≔f0(x0,x1,...,xm)+jf1(x0,x1,...,xm)+⋯+jm-1fm-1(x0,x1,...,xm)+jmfm(x0,x1,...,xm), where fk(x0,x1,...,xm) are smooth functions of 2n real variables. A continuation for complex function theory will appear.

  10. Light cone matrix product

    Energy Technology Data Exchange (ETDEWEB)

    Hastings, Matthew B [Los Alamos National Laboratory

    2009-01-01

    We show how to combine the light-cone and matrix product algorithms to simulate quantum systems far from equilibrium for long times. For the case of the XXZ spin chain at {Delta} = 0.5, we simulate to a time of {approx} 22.5. While part of the long simulation time is due to the use of the light-cone method, we also describe a modification of the infinite time-evolving bond decimation algorithm with improved numerical stability, and we describe how to incorporate symmetry into this algorithm. While statistical sampling error means that we are not yet able to make a definite statement, the behavior of the simulation at long times indicates the appearance of either 'revivals' in the order parameter as predicted by Hastings and Levitov (e-print arXiv:0806.4283) or of a distinct shoulder in the decay of the order parameter.

  11. Matrix membranes and integrability

    Energy Technology Data Exchange (ETDEWEB)

    Zachos, C. [Argonne National Lab., IL (United States); Fairlie, D. [University of Durham (United Kingdom). Dept. of Mathematical Sciences; Curtright, T. [University of Miami, Coral Gables, FL (United States). Dept. of Physics

    1997-06-01

    This is a pedagogical digest of results reported in Curtright, Fairlie, {ampersand} Zachos 1997, and an explicit implementation of Euler`s construction for the solution of the Poisson Bracket dual Nahm equation. But it does not cover 9 and 10-dimensional systems, and subsequent progress on them Fairlie 1997. Cubic interactions are considered in 3 and 7 space dimensions, respectively, for bosonic membranes in Poisson Bracket form. Their symmetries and vacuum configurations are explored. Their associated first order equations are transformed to Nahm`s equations, and are hence seen to be integrable, for the 3-dimensional case, by virtue of the explicit Lax pair provided. Most constructions introduced also apply to matrix commutator or Moyal Bracket analogs.

  12. Thermoreversible copolymer gels for extracellular matrix.

    Science.gov (United States)

    Vernon, B; Kim, S W; Bae, Y H

    2000-07-01

    To improve the properties of a reversible synthetic extracellular matrix based on a thermally reversible polymer, copolymers of N-isopropylacrylamide and acrylic acid were prepared in benzene with varying contents of acrylic acid (0 to 3%) and the thermal properties were evaluated. The poly(N-isopropylacrylamide) and copolymers made with acrylic acid had molecular weights from 0.8 to 1.7 x10(6) D. Differential scanning calorimetry (DSC) showed the high-molecular-weight acrylic acid copolymers had similar onset temperatures to the homopolymers, but the peak width was considerably increased with increasing acrylic acid content. DSC and cloud point measurements showed that polymers with 0 to 3% acrylic acid exhibit a lower critical solution temperature (LCST) transition between 30 degrees and 37 degrees C. In swelling studies, the homopolymer showed significant syneresis at temperatures above 31 degrees C. Copolymers with 1 and 1.5% showed syneresis beginning at 32 degrees and 37 degrees C, respectively. At 37 degrees C the copolymers with 1.5-3% acrylic acid showed little or no syneresis. Due to the high water content and a transition near physiologic conditions (below 37 degrees C), the polymers with 1.5-2.0% acrylic acid exhibited properties that would be useful in the development of a refillable synthetic extracellular matrix. Such a matrix could be applied to several cell types, including islets of Langerhans, for a biohybrid artificial pancreas.

  13. Inter-Grade and Inter-Batch Variability of Sodium Alginate Used in Alginate-Based Matrix Tablets

    OpenAIRE

    Fu, Shao; Buckner, Ira S.; Block, Lawrence H.

    2014-01-01

    The purpose of this study is to characterize the inter-grade and inter-batch variability of sodium alginate used in the formulation of matrix tablets. Four different grades and three batches of one grade of sodium alginate were used to prepare matrix tablets. Swelling, erosion, and drug release tests of sodium alginate matrix tablets were conducted in a USP dissolution apparatus. Substantial differences in swelling and erosion behavior of sodium alginate matrix tablets were evident among diff...

  14. Spherical membranes in Matrix theory

    CERN Document Server

    Kabat, D; Kabat, Daniel; Taylor, Washington

    1998-01-01

    We consider membranes of spherical topology in uncompactified Matrix theory. In general for large membranes Matrix theory reproduces the classical membrane dynamics up to 1/N corrections; for certain simple membrane configurations, the equations of motion agree exactly at finite N. We derive a general formula for the one-loop Matrix potential between two finite-sized objects at large separations. Applied to a graviton interacting with a round spherical membrane, we show that the Matrix potential agrees with the naive supergravity potential for large N, but differs at subleading orders in N. The result is quite general: we prove a pair of theorems showing that for large N, after removing the effects of gravitational radiation, the one-loop potential between classical Matrix configurations agrees with the long-distance potential expected from supergravity. As a spherical membrane shrinks, it eventually becomes a black hole. This provides a natural framework to study Schwarzschild black holes in Matrix theory.

  15. Linearized supergravity from Matrix theory

    CERN Document Server

    Kabat, D; Kabat, Daniel; Taylor, Washington

    1998-01-01

    We show that the linearized supergravity potential between two objects arising from the exchange of quanta with zero longitudinal momentum is reproduced to all orders in 1/r by terms in the one-loop Matrix theory potential. The essential ingredient in the proof is the identification of the Matrix theory quantities corresponding to moments of the stress tensor and membrane current. We also point out that finite-N Matrix theory violates the Equivalence Principle.

  16. Lectures on Matrix Field Theory

    Science.gov (United States)

    Ydri, Badis

    The subject of matrix field theory involves matrix models, noncommutative geometry, fuzzy physics and noncommutative field theory and their interplay. In these lectures, a lot of emphasis is placed on the matrix formulation of noncommutative and fuzzy spaces, and on the non-perturbative treatment of the corresponding field theories. In particular, the phase structure of noncommutative $\\phi^4$ theory is treated in great detail, and an introduction to noncommutative gauge theory is given.

  17. Matrix elements of unstable states

    CERN Document Server

    Bernard, V; Meißner, U -G; Rusetsky, A

    2012-01-01

    Using the language of non-relativistic effective Lagrangians, we formulate a systematic framework for the calculation of resonance matrix elements in lattice QCD. The generalization of the L\\"uscher-Lellouch formula for these matrix elements is derived. We further discuss in detail the procedure of the analytic continuation of the resonance matrix elements into the complex energy plane and investigate the infinite-volume limit.

  18. Enhancing an R-matrix

    CERN Document Server

    MacKaay, M A

    1996-01-01

    In order to construct a representation of the tangle category one needs an enhanced R-matrix. In this paper we define a sufficient and necessary condition for enhancement that can be checked easily for any R-matrix. If the R-matrix can be enhanced, we also show how to construct the additional data that define the enhancement. As a direct consequence we find a sufficient condition for the construction of a knot invariant.

  19. How Prepared is Prepared Enough?

    Science.gov (United States)

    Porter-Levy; Macleod; Rickert

    1996-10-01

    A 17-year-old female was in the final stage in treatment of right unilateral cleft lip and palate. She had undergone a number of previous surgeries. Hearing and speech were good on evaluation, and her social and family situation were deemed excellent. After preparatory orthodontics she underwent a Lefort I maxillary advancement. Surgery was successful and she was admitted into postoperative recovery. However, the lack of adequate preoperative preparation caused traumatic reaction from the patient and her parents: anxiety over appearance, crying, refusal of oral fluids and oral care, refusal of analgesia, and refusal to mobilize. The patience and persistence of hospital staff slowly overcame all adversities and the patient moved on to full and successful recovery, but this case prompted changes in preoperative procedures and involvement of patients and their families in postoperative meal selection, planing, and preparation.

  20. Matrix Models and Gravitational Corrections

    CERN Document Server

    Dijkgraaf, R; Temurhan, M; Dijkgraaf, Robbert; Sinkovics, Annamaria; Temurhan, Mine

    2002-01-01

    We provide evidence of the relation between supersymmetric gauge theories and matrix models beyond the planar limit. We compute gravitational R^2 couplings in gauge theories perturbatively, by summing genus one matrix model diagrams. These diagrams give the leading 1/N^2 corrections in the large N limit of the matrix model and can be related to twist field correlators in a collective conformal field theory. In the case of softly broken SU(N) N=2 super Yang-Mills theories, we find that these exact solutions of the matrix models agree with results obtained by topological field theory methods.

  1. A matrix model for WZW

    Energy Technology Data Exchange (ETDEWEB)

    Dorey, Nick [Department of Applied Mathematics and Theoretical Physics, University of Cambridge,Wilberforce Road, Cambridge, CB3 OWA (United Kingdom); Tong, David [Department of Applied Mathematics and Theoretical Physics, University of Cambridge,Wilberforce Road, Cambridge, CB3 OWA (United Kingdom); Department of Theoretical Physics, TIFR,Homi Bhabha Road, Mumbai 400 005 (India); Stanford Institute for Theoretical Physics,Via Pueblo, Stanford, CA 94305 (United States); Turner, Carl [Department of Applied Mathematics and Theoretical Physics, University of Cambridge,Wilberforce Road, Cambridge, CB3 OWA (United Kingdom)

    2016-08-01

    We study a U(N) gauged matrix quantum mechanics which, in the large N limit, is closely related to the chiral WZW conformal field theory. This manifests itself in two ways. First, we construct the left-moving Kac-Moody algebra from matrix degrees of freedom. Secondly, we compute the partition function of the matrix model in terms of Schur and Kostka polynomials and show that, in the large N limit, it coincides with the partition function of the WZW model. This same matrix model was recently shown to describe non-Abelian quantum Hall states and the relationship to the WZW model can be understood in this framework.

  2. A Matrix Model for WZW

    CERN Document Server

    Dorey, Nick; Turner, Carl

    2016-01-01

    We study a U(N) gauged matrix quantum mechanics which, in the large N limit, is closely related to the chiral WZW conformal field theory. This manifests itself in two ways. First, we construct the left-moving Kac-Moody algebra from matrix degrees of freedom. Secondly, we compute the partition function of the matrix model in terms of Schur and Kostka polynomials and show that, in the large $N$ limit, it coincides with the partition function of the WZW model. This same matrix model was recently shown to describe non-Abelian quantum Hall states and the relationship to the WZW model can be understood in this framework.

  3. Extended Matrix Variate Hypergeometric Functions and Matrix Variate Distributions

    Directory of Open Access Journals (Sweden)

    Daya K. Nagar

    2015-01-01

    Full Text Available Hypergeometric functions of matrix arguments occur frequently in multivariate statistical analysis. In this paper, we define and study extended forms of Gauss and confluent hypergeometric functions of matrix arguments and show that they occur naturally in statistical distribution theory.

  4. The Effect of Functionalization Carbon Nanotubes (CNTs) on the Performance of PES-CNTs Mixed Matrix Membrane

    OpenAIRE

    Ahmad Mustafa; Tutuk Djoko Kusworo; Abdullah Busairi; Ahmad Fauzi Ismail

    2010-01-01

    A new type of mixed matrix membrane consisting of functionalized carbon nanotubes (CNTs) and polyethersulfone (PES) is prepared for biogas purification. PES mixed matrix membrane with and without modification of carbon nanotubes were prepared by a dry/wet phase inversion technique using a pneumatically flat sheet membrane casting machine system. The modified carbon nanotubes were prepared by treating the carbon nanotubes with chemical modification using Dynasylan Ameo (DA) silane agent to all...

  5. Matrix Product Operators, Matrix Product States, and ab initio Density Matrix Renormalization Group algorithms

    CERN Document Server

    Chan, Garnet Kin-Lic; Nakatani, Naoki; Li, Zhendong; White, Steven R

    2016-01-01

    Current descriptions of the ab initio DMRG algorithm use two superficially different languages: an older language of the renormalization group and renormalized operators, and a more recent language of matrix product states and matrix product operators. The same algorithm can appear dramatically different when written in the two different vocabularies. In this work, we carefully describe the translation between the two languages in several contexts. First, we describe how to efficiently implement the ab-initio DMRG sweep using a matrix product operator based code, and the equivalence to the original renormalized operator implementation. Next we describe how to implement the general matrix product operator/matrix product state algebra within a pure renormalized operator-based DMRG code. Finally, we discuss two improvements of the ab initio DMRG sweep algorithm motivated by matrix product operator language: Hamiltonian compression, and a sum over operators representation that allows for perfect computational par...

  6. Ceramic matrix composite article and process of fabricating a ceramic matrix composite article

    Science.gov (United States)

    Cairo, Ronald Robert; DiMascio, Paul Stephen; Parolini, Jason Robert

    2016-01-12

    A ceramic matrix composite article and a process of fabricating a ceramic matrix composite are disclosed. The ceramic matrix composite article includes a matrix distribution pattern formed by a manifold and ceramic matrix composite plies laid up on the matrix distribution pattern, includes the manifold, or a combination thereof. The manifold includes one or more matrix distribution channels operably connected to a delivery interface, the delivery interface configured for providing matrix material to one or more of the ceramic matrix composite plies. The process includes providing the manifold, forming the matrix distribution pattern by transporting the matrix material through the manifold, and contacting the ceramic matrix composite plies with the matrix material.

  7. Formulation Development and Optimization of Matrix Tablet of Tramadol Hydrochloride.

    Science.gov (United States)

    Deb, Pulak; Singha, Jubaraj; Chanda, Indranil; Chakraborty, Prithviraj

    2017-01-01

    The aim of the present investigation is to formulate and optimize oral sustained release matrix tablet of highly water soluble drug Tramadol HCl and to evaluate the effect of varying concentration of hydrophilic and hydrophobic polymer on drug release, based on a survey done on the recent patents of Tramadol HCl (US7374781, CA 2479252) and sustained release matrix tablets. The tablets were prepared by double granulation process, by melt granulation and wet granulation technique using Carnauba wax (CW) and HPMC K100 as release retardant. Pre and post compression factors were evaluated and all the parameters were found within the limit. The drug release data were subjected to different models in order to evaluate release kinetics and mechanism of drug release. The prepared formulations showed drug release in the range 100±2% in 6hrs, 7hrs, 8hrs and 9hrs and upto 12 hrs respectively. The optimized tablet having 25% CW and 20% HPMC showed sustained drug release pattern. Hydrophilic matrix of HPMC alone could not control the Tramadol release effectively for 12 h whereas when combined with CW could slow down the release of drug and can be successfully employed for formulating sustained-release matrix tablets. Similarity factor, f2 shows the test and reference profile are identical. Double granulation technique with CW and HPMC K100 proved as a better technique for sustaining the drug release from the matrix tablet. Copyright© Bentham Science Publishers; For any queries, please email at epub@benthamscience.org.

  8. Matrix Theory of pp Waves

    CERN Document Server

    Michelson, J

    2004-01-01

    The Matrix Theory that has been proposed for various pp wave backgrounds is discussed. Particular emphasis is on the existence of novel nontrivial supersymmetric solutions of the Matrix Theory. These correspond to branes of various shapes (ellipsoidal, paraboloidal, and possibly hyperboloidal) that are unexpected from previous studies of branes in pp wave geometries.

  9. How to Study a Matrix

    Science.gov (United States)

    Jairam, Dharmananda; Kiewra, Kenneth A.; Kauffman, Douglas F.; Zhao, Ruomeng

    2012-01-01

    This study investigated how best to study a matrix. Fifty-three participants studied a matrix topically (1 column at a time), categorically (1 row at a time), or in a unified way (all at once). Results revealed that categorical and unified study produced higher: (a) performance on relationship and fact tests, (b) study material satisfaction, and…

  10. Machining of Metal Matrix Composites

    CERN Document Server

    2012-01-01

    Machining of Metal Matrix Composites provides the fundamentals and recent advances in the study of machining of metal matrix composites (MMCs). Each chapter is written by an international expert in this important field of research. Machining of Metal Matrix Composites gives the reader information on machining of MMCs with a special emphasis on aluminium matrix composites. Chapter 1 provides the mechanics and modelling of chip formation for traditional machining processes. Chapter 2 is dedicated to surface integrity when machining MMCs. Chapter 3 describes the machinability aspects of MMCs. Chapter 4 contains information on traditional machining processes and Chapter 5 is dedicated to the grinding of MMCs. Chapter 6 describes the dry cutting of MMCs with SiC particulate reinforcement. Finally, Chapter 7 is dedicated to computational methods and optimization in the machining of MMCs. Machining of Metal Matrix Composites can serve as a useful reference for academics, manufacturing and materials researchers, manu...

  11. Matrix Model Approach to Cosmology

    CERN Document Server

    Chaney, A; Stern, A

    2015-01-01

    We perform a systematic search for rotationally invariant cosmological solutions to matrix models, or more specifically the bosonic sector of Lorentzian IKKT-type matrix models, in dimensions $d$ less than ten, specifically $d=3$ and $d=5$. After taking a continuum (or commutative) limit they yield $d-1$ dimensional space-time surfaces, with an attached Poisson structure, which can be associated with closed, open or static cosmologies. For $d=3$, we obtain recursion relations from which it is possible to generate rotationally invariant matrix solutions which yield open universes in the continuum limit. Specific examples of matrix solutions have also been found which are associated with closed and static two-dimensional space-times in the continuum limit. The solutions provide for a matrix resolution of cosmological singularities. The commutative limit reveals other desirable features, such as a solution describing a smooth transition from an initial inflation to a noninflationary era. Many of the $d=3$ soluti...

  12. Matrix convolution operators on groups

    CERN Document Server

    Chu, Cho-Ho

    2008-01-01

    In the last decade, convolution operators of matrix functions have received unusual attention due to their diverse applications. This monograph presents some new developments in the spectral theory of these operators. The setting is the Lp spaces of matrix-valued functions on locally compact groups. The focus is on the spectra and eigenspaces of convolution operators on these spaces, defined by matrix-valued measures. Among various spectral results, the L2-spectrum of such an operator is completely determined and as an application, the spectrum of a discrete Laplacian on a homogeneous graph is computed using this result. The contractivity properties of matrix convolution semigroups are studied and applications to harmonic functions on Lie groups and Riemannian symmetric spaces are discussed. An interesting feature is the presence of Jordan algebraic structures in matrix-harmonic functions.

  13. Manufacturing Titanium Metal Matrix Composites by Consolidating Matrix Coated Fibres

    Institute of Scientific and Technical Information of China (English)

    Hua-Xin PENG

    2005-01-01

    Titanium metal matrix composites (TiMMCs) reinforced by continuous silicon carbide fibres are being developed for aerospace applications. TiMMCs manufactured by the consolidation of matrix-coated fibre (MCF) method offer optimum properties because of the resulting uniform fibre distribution, minimum fibre damage and fibre volume fraction control. In this paper, the consolidation of Ti-6Al-4V matrix-coated SiC fibres during vacuum hot pressing has been investigated. Experiments were carried out on multi-ply MCFs under vacuum hot pressing (VHP). In contrast to most of existing studies, the fibre arrangement has been carefully controlled either in square or hexagonal arraysthroughout the consolidated sample. This has enabled the dynamic consolidation behaviour of MCFs to be demonstrated by eliminating the fibre re-arrangement during the VHP process. The microstructural evolution of the matrix coating was reported and the deformation mechanisms involved were discussed.

  14. Reproducible Matrix Deposition for MALDI MSI Based on Open-Source Software and Hardware.

    Science.gov (United States)

    Stoeckli, Markus; Staab, Dieter

    2015-06-01

    The new open-source software and hardware matrix deposition device named iMatrixSpray was optimized and specified for homogeneity, reproducibility, and sensitivity in MS imaging experiments. The results confirm the design claims, with the device delivering uniform coatings with a constant quality from experiment to experiment. The robustness in combination with the open design allows developing and sharing of matrix deposition and sample preparation protocols between labs. This tool therefore enables researchers to enter the field of MALDI MSI without previous experience in matrix coating.

  15. FABRICATION AND EVALUATION OF GLIPIZIDE ABELMOSCHUS ESCULENTUS FRUIT MUCILAGE POVIDONE CONTROLLED RELEASE MATRIX TABLETS

    Directory of Open Access Journals (Sweden)

    Hindustan Abdul Ahad

    2011-02-01

    Full Text Available The present investigation was aimed to prepare matrix type controlled release tablets of Glipizide with Abelmoschus esculentus fruit mucilage and Povidone. The polymers were studied for its functionality as a matrix forming property to sustain the Glipizide release from the dosage form. Physicochemical properties of dried powdered mucilage of Abelmoschus esculentus fruit mucilage and Povidone blend were studied. Various formulations of Glipizide Abelmoschus esculentus fruit mucilage and Povidone were prepared. The prepared tablets were found to have better pharmacopoeial parameters with low standard deviation values. The swelling behavior and release rate characteristics were studied. The in-vitro dissolution study proved that the dried Abelmoschus esculentus fruit mucilage and Povidone in combination can be used as a matrix forming polymers for making controlled release matrix tablets.

  16. Effect of aligned carbon nanotubes on electrical conductivity behaviour in polycarbonate matrix

    Indian Academy of Sciences (India)

    M M Larijani; E J Khamse; Z Asadollahi; M Asadi

    2012-06-01

    This article reports effects of alignment of embedded carbon nanotubes in a polycarbonate polymer matrix under magnetic, direct and alternating current electric fields on the electrical properties of the resulting nanocomposites. Composites consisting of different quantities of carbon nanotubes in a polycarbonate matrix have been prepared using a solution casting technique. The effects of field strength and nanotube concentration on the resulted network structure and conductivity of the composites were studied by in situ optical microscopy, transmission electron microscopy and four-point probe technique. The results showed that the composites prepared in the presence of field had better conductivity than those of as-prepared composites. It was also concluded that the application of alternating current electric field and magnetic field in this system led to the formation of relatively continuing networks while direct current electric field only prevented agglomeration of the carbon nanotubes in the polycarbonate matrix and created relatively uniform distribution of nanotubes in the matrix.

  17. Rhenium Nanochemistry for Catalyst Preparation

    Directory of Open Access Journals (Sweden)

    Vadim G. Kessler

    2012-08-01

    Full Text Available The review presents synthetic approaches to modern rhenium-based catalysts. Creation of an active center is considered as a process of obtaining a nanoparticle or a molecule, immobilized within a matrix of the substrate. Selective chemical routes to preparation of particles of rhenium alloys, rhenium oxides and the molecules of alkyltrioxorhenium, and their insertion into porous structure of zeolites, ordered mesoporous MCM matrices, anodic mesoporous alumina, and porous transition metal oxides are considered. Structure-property relationships are traced for these catalysts in relation to such processes as alkylation and isomerization, olefin metathesis, selective oxidation of olefins, methanol to formaldehyde conversion, etc.

  18. Nanometeric hydroxyapatite in situ formed in demineralized bone matrix by electrochemical technique

    Institute of Scientific and Technical Information of China (English)

    CHEN Ji-da; WANG Yuan-ling; CAI Hao-xi; CAO Yin

    2001-01-01

    @@ To prepare biomimic bone materials, some thick meshes of demineralized bone matrix (DBM), which are the interest work of collagen fibrils, have been prepared in normal way, and calcium phosphate of nanometeric apatite-li.ke was introduced into these mesh works with aqueous calcium and phosphate salt solution by means of the electrochemical technique at room temperature.

  19. New pole placement algorithm - Polynomial matrix approach

    Science.gov (United States)

    Shafai, B.; Keel, L. H.

    1990-01-01

    A simple and direct pole-placement algorithm is introduced for dynamical systems having a block companion matrix A. The algorithm utilizes well-established properties of matrix polynomials. Pole placement is achieved by appropriately assigning coefficient matrices of the corresponding matrix polynomial. This involves only matrix additions and multiplications without requiring matrix inversion. A numerical example is given for the purpose of illustration.

  20. High temperature polymer matrix composites

    Science.gov (United States)

    Serafini, Tito T. (Editor)

    1987-01-01

    These are the proceedings of the High Temperature Polymer Matrix Composites Conference held at the NASA Lewis Research Center on March 16 to 18, 1983. The purpose of the conference is to provide scientists and engineers working in the field of high temperature polymer matrix composites an opportunity to review, exchange, and assess the latest developments in this rapidly expanding area of materials technology. Technical papers are presented in the following areas: (1) matrix development; (2) adhesive development; (3) Characterization; (4) environmental effects; and (5) applications.

  1. Matrix Elements for Hylleraas CI

    Science.gov (United States)

    Harris, Frank E.

    The limitation to at most a single interelectron distance in individual configurations of a Hylleraas-type multiconfiguration wave function restricts significantly the types of integrals occurring in matrix elements for energy calculations, but even then if the formulation is not handled efficiently the angular parts of these integrals escalate to create expressions of great complexity. This presentation reviews ways in which the angular-momentum calculus can be employed to systematize and simplify the matrix element formulas, particularly those for the kinetic-energy matrix elements.

  2. Matrix product operators, matrix product states, and ab initio density matrix renormalization group algorithms

    Science.gov (United States)

    Chan, Garnet Kin-Lic; Keselman, Anna; Nakatani, Naoki; Li, Zhendong; White, Steven R.

    2016-07-01

    Current descriptions of the ab initio density matrix renormalization group (DMRG) algorithm use two superficially different languages: an older language of the renormalization group and renormalized operators, and a more recent language of matrix product states and matrix product operators. The same algorithm can appear dramatically different when written in the two different vocabularies. In this work, we carefully describe the translation between the two languages in several contexts. First, we describe how to efficiently implement the ab initio DMRG sweep using a matrix product operator based code, and the equivalence to the original renormalized operator implementation. Next we describe how to implement the general matrix product operator/matrix product state algebra within a pure renormalized operator-based DMRG code. Finally, we discuss two improvements of the ab initio DMRG sweep algorithm motivated by matrix product operator language: Hamiltonian compression, and a sum over operators representation that allows for perfect computational parallelism. The connections and correspondences described here serve to link the future developments with the past and are important in the efficient implementation of continuing advances in ab initio DMRG and related algorithms.

  3. Matrix product operators, matrix product states, and ab initio density matrix renormalization group algorithms.

    Science.gov (United States)

    Chan, Garnet Kin-Lic; Keselman, Anna; Nakatani, Naoki; Li, Zhendong; White, Steven R

    2016-07-01

    Current descriptions of the ab initio density matrix renormalization group (DMRG) algorithm use two superficially different languages: an older language of the renormalization group and renormalized operators, and a more recent language of matrix product states and matrix product operators. The same algorithm can appear dramatically different when written in the two different vocabularies. In this work, we carefully describe the translation between the two languages in several contexts. First, we describe how to efficiently implement the ab initio DMRG sweep using a matrix product operator based code, and the equivalence to the original renormalized operator implementation. Next we describe how to implement the general matrix product operator/matrix product state algebra within a pure renormalized operator-based DMRG code. Finally, we discuss two improvements of the ab initio DMRG sweep algorithm motivated by matrix product operator language: Hamiltonian compression, and a sum over operators representation that allows for perfect computational parallelism. The connections and correspondences described here serve to link the future developments with the past and are important in the efficient implementation of continuing advances in ab initio DMRG and related algorithms.

  4. Automated MALDI Matrix Coating System for Multiple Tissue Samples for Imaging Mass Spectrometry

    Science.gov (United States)

    Mounfield, William P.; Garrett, Timothy J.

    2012-03-01

    Uniform matrix deposition on tissue samples for matrix-assisted laser desorption/ionization (MALDI) is key for reproducible analyte ion signals. Current methods often result in nonhomogenous matrix deposition, and take time and effort to produce acceptable ion signals. Here we describe a fully-automated method for matrix deposition using an enclosed spray chamber and spray nozzle for matrix solution delivery. A commercial air-atomizing spray nozzle was modified and combined with solenoid controlled valves and a Programmable Logic Controller (PLC) to control and deliver the matrix solution. A spray chamber was employed to contain the nozzle, sample, and atomized matrix solution stream, and to prevent any interference from outside conditions as well as allow complete control of the sample environment. A gravity cup was filled with MALDI matrix solutions, including DHB in chloroform/methanol (50:50) at concentrations up to 60 mg/mL. Various samples (including rat brain tissue sections) were prepared using two deposition methods (spray chamber, inkjet). A linear ion trap equipped with an intermediate-pressure MALDI source was used for analyses. Optical microscopic examination showed a uniform coating of matrix crystals across the sample. Overall, the mass spectral images gathered from tissues coated using the spray chamber system were of better quality and more reproducible than from tissue specimens prepared by the inkjet deposition method.

  5. GoM Diet Matrix

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — This data set was taken from CRD 08-18 at the NEFSC. Specifically, the Gulf of Maine diet matrix was developed for the EMAX exercise described in that center...

  6. Linear connections on matrix geometries

    CERN Document Server

    Madore, J; Mourad, J; Madore, John; Masson, Thierry; Mourad, Jihad

    1994-01-01

    A general definition of a linear connection in noncommutative geometry has been recently proposed. Two examples are given of linear connections in noncommutative geometries which are based on matrix algebras. They both possess a unique metric connection.

  7. Matrix Quantum Mechanics from Qubits

    CERN Document Server

    Hartnoll, Sean A; Mazenc, Edward A

    2016-01-01

    We introduce a transverse field Ising model with order N^2 spins interacting via a nonlocal quartic interaction. The model has an O(N,Z), hyperoctahedral, symmetry. We show that the large N partition function admits a saddle point in which the symmetry is enhanced to O(N). We further demonstrate that this `matrix saddle' correctly computes large N observables at weak and strong coupling. The matrix saddle undergoes a continuous quantum phase transition at intermediate couplings. At the transition the matrix eigenvalue distribution becomes disconnected. The critical excitations are described by large N matrix quantum mechanics. At the critical point, the low energy excitations are waves propagating in an emergent 1+1 dimensional spacetime.

  8. The R-matrix theory

    Energy Technology Data Exchange (ETDEWEB)

    Descouvemont, P; Baye, D [Physique Nucleaire Theorique et Physique Mathematique, C.P. 229, Universite Libre de Bruxelles (ULB), B 1050 Brussels (Belgium)], E-mail: pdesc@ulb.ac.be, E-mail: dbaye@ulb.ac.be

    2010-03-15

    The different facets of the R-matrix method are presented pedagogically in a general framework. Two variants have been developed over the years: (i) The 'calculable' R-matrix method is a calculational tool to derive scattering properties from the Schroedinger equation in a large variety of physical problems. It was developed rather independently in atomic and nuclear physics with too little mutual influence. (ii) The 'phenomenological' R-matrix method is a technique to parametrize various types of cross sections. It was mainly (or uniquely) used in nuclear physics. Both directions are explained by starting from the simple problem of scattering by a potential. They are illustrated by simple examples in nuclear and atomic physics. In addition to elastic scattering, the R-matrix formalism is applied to inelastic and radiative-capture reactions. We also present more recent and more ambitious applications of the theory in nuclear physics.

  9. Matrix analysis of electrical machinery

    CERN Document Server

    Hancock, N N

    2013-01-01

    Matrix Analysis of Electrical Machinery, Second Edition is a 14-chapter edition that covers the systematic analysis of electrical machinery performance. This edition discusses the principles of various mathematical operations and their application to electrical machinery performance calculations. The introductory chapters deal with the matrix representation of algebraic equations and their application to static electrical networks. The following chapters describe the fundamentals of different transformers and rotating machines and present torque analysis in terms of the currents based on the p

  10. Random Matrix Theory of Dynamical Cross Correlations in Financial Data

    Science.gov (United States)

    Nakayama, Y.; Iyetomi, H.

    A new method taking advantage of the random matrix theory is proposed to extract genuine dynamical correlations between price fluctuations of different stocks. One-day returns of 557 Japanese major stocks for the 11-year period from 1996 to 2006 are used for this study. We carry out the discrete Fourier transform of the returns to construct a correlation matrix at each frequency. Also we prepare series of random numbers which are mutually uncorrelated and hence serve as a reference. Comparison of the eigenvalues of the empirical correlation matrix with the reference results of the random one enables us to distinguish between information and noise involved in complicated behavior of the stock returns. It is thus demonstrated that there exist collective motions of the stock prices with periods well over days. Finally we indicate a possible application of the present finding to the risk evaluation of portfolios.

  11. Possibility of Quantum Teleportation and the Reduced Density Matrix

    Institute of Scientific and Technical Information of China (English)

    朱红波; 曾谨言

    2001-01-01

    It is shown that only the maximally entangled two-particle (spin 1/2) states whose one-particle reduced density matrix is p (i) = (1/2)I2 can realize the teleportation of an arbitrary one-particle spin state. Based on this,to teleport an arbitrary k-particle spin state, one must prepare an N-particle entangled state whose k-particle (k < N) reduced density matrix has the structure 2-kI2k (I2k being the 2k × 2k identity matrix). The N-particle Greenberger-Horne-Zeilinger states cannot realize the teleportation of an arbitrary k-particle (N>k≥2) state,except for special states with only two components.

  12. Novel Phosphate—sensitive Fluorescent Composite Matrix

    Institute of Scientific and Technical Information of China (English)

    XIEZeng-hong; LINXu-cong; CHENGuo-nan

    2003-01-01

    Via several techniques to modify sensitive matrix for inhabiting the leakage of fluoreseent indicator,a new stable scnsing material for monitoring phosphates has been prepared and applied to the measurement of phosphates in artificial seawater.It is based on the reaction of PO43- with Al(Ⅲ)-Morin that leads to the fluorescence quenching of the composite matrix.At pH value 4.0and the salinity value 25.0,the response time of output signal having reached the steady state is less than 300 seconds.Its calibration graph is gained in the range of H2PO4- mass concentration from 1.50 to 7.00μg/mL with the limit of detection (3σ/K)0.02μg/mL.When it was used to measure phosphates in artificial seawater,the recovery ranged from 96.78% to 102.09%.Being stored under the proper condition,the membranes maintain sensitive for 90-120days,and are able to be used for 50-80times with indicator supplement.

  13. Matrix isolation studies with Fourier transform IR

    Energy Technology Data Exchange (ETDEWEB)

    Green, David W.; Reedy, Gerald T.

    1977-01-01

    The combination of Fourier transform infrared (FT-IR) spectroscopy with the matrix-isolation techniques has advantages compared with the use of more conventional grating spectroscopy. Furthermore, the recent commercial availability of Fourier transform spectrometers has made FT-IR a practical alternative. Some advantages of the FT-IR spectrometer over the grating spectrometer are the result of the computerized data system that is a necessary part of the FT-IR spectrometer; other advantages are a consequence of the difference in optical arrangements and these represent the inherent advantages of the FT-IR method. In most applications with the matrix-isolation technique, the use of FT-IR spectroscopy results in either an improved signal-to-noise ratio or a shorter time for data collection compared with grating infrared spectroscopy. Fourier transform infrared spectroscopy has been used in the laboratory to study several molecular species in low-temperature matrices. Some species have been produced by high-temperature vaporization from Knudsen cells and others by sputtering. By sputtering, Ar and Kr matrices have been prepared which contain U atoms, UO, UO/sub 2/, UO/sub 3/, PuO, PuO/sub 2/, UN, or UN/sub 2/, depending upon the composition of the gas used to sputter as well as the identity of the metallic cathode. Infrared spectra of matrices containing these compounds are presented and discussed. (JRD)

  14. SVD row or column symmetric matrix

    Institute of Scientific and Technical Information of China (English)

    2000-01-01

    A new architecture for row or column symmetric matrix called extended matrix is defined, and a precise correspondence of the singular values and singular vectors between the extended matrix and its original (namely, the mother matrix) is derived. As an illustration of potential, we show that, for a class of extended matrices, the singular value decomposition using the mother matrix rather than the extended matrix per se can save the CPU time and memory without loss of numerical precision.

  15. Citric Acid Capped Iron Oxide Nanoparticles as an Effective MALDI Matrix for Polymers

    Science.gov (United States)

    Liang, Qiaoli; Sherwood, Jennifer; Macher, Thomas; Wilson, Joseph M.; Bao, Yuping; Cassady, Carolyn J.

    2016-12-01

    A new matrix-assisted laser desorption ionization (MALDI) mass spectrometry matrix is proposed for molecular mass determination of polymers. This matrix contains an iron oxide nanoparticle (NP) core with citric acid (CA) molecules covalently bound to the surface. With the assistance of additives, the particulate nature of NPs allows the matrix to mix uniformly with polar or nonpolar polymer layers and promotes ionization, which may simplify matrix selection and sample preparation procedures. Several distinctively different polymer classes (polyethyleneglycol (PEG), polywax/polyethylene, perfluoropolyether, and polydimethylsiloxane) are effectively detected by the water or methanol dispersed NPCA matrix with NaCl, NaOH, LiOH, or AgNO3 as additives. Furtheremore, successful quantitative measurements of PEG1000 using polypropylene glycol 1000 as an internal standard are demonstrated.

  16. Minimal Realizations of Supersymmetry for Matrix Hamiltonians

    CERN Document Server

    Andrianov, Alexandr A

    2014-01-01

    The notions of weak and strong minimizability of a matrix intertwining operator are introduced. Criterion of strong minimizability of a matrix intertwining operator is revealed. Criterion and sufficient condition of existence of a constant symmetry matrix for a matrix Hamiltonian are presented. A method of constructing of a matrix Hamiltonian with a given constant symmetry matrix in terms of a set of arbitrary scalar functions and eigen- and associated vectors of this matrix is offered. Examples of constructing of $2\\times2$ matrix Hamiltonians with given symmetry matrices for the cases of different structure of Jordan form of these matrices are elucidated.

  17. Platelet-rich fibrin matrix for facial plastic surgery.

    Science.gov (United States)

    Sclafani, Anthony P; Saman, Masoud

    2012-05-01

    Platelets are known primarily for their role in hemostasis, but there is increasing interest in the effect of platelets on wound healing. Platelet isolates such as platelet-rich plasma have been advocated to enhance and accelerate wound healing. This article describes the use of a novel preparation, platelet-rich fibrin matrix (PRFM), for facial plastic surgery applications such as volume augmentation, fat transfer supplementation, and as an adjunct to open surgical procedures.

  18. Plastic timber with wheat straw and polymer matrix

    OpenAIRE

    García-Velázquez, Ángel; Amado-Moreno, María Guadalupe; Campbell-Ramírez, Héctor Enrique; Brito-Páez, Reyna Arcelia; Toscano-Palomar, Lydia

    2013-01-01

    The objective of the research was to develop plastic timber with wheat straw and polymer matrix. In the Mexicali Valley in Baja California, Mexico, the agricultural activities and the maquiladora industry are the main source of income in the region.  However, agricultural activities generate wastes that contribute heavily to pollution of Mexicali and its valley. The burning of agricultural waste is a traditional practice in the Valley, and is done in order to prepare the soil for the next cro...

  19. Sparse Planar Array Synthesis Using Matrix Enhancement and Matrix Pencil

    Directory of Open Access Journals (Sweden)

    Mei-yan Zheng

    2013-01-01

    Full Text Available The matrix enhancement and matrix pencil (MEMP plays important roles in modern signal processing applications. In this paper, MEMP is applied to attack the problem of two-dimensional sparse array synthesis. Firstly, the desired array radiation pattern, as the original pattern for approximating, is sampled to form an enhanced matrix. After performing the singular value decomposition (SVD and discarding the insignificant singular values according to the prior approximate error, the minimum number of elements can be obtained. Secondly, in order to obtain the eigenvalues, the generalized eigen-decomposition is employed on the approximate matrix, which is the optimal low-rank approximation of the enhanced matrix corresponding to sparse planar array, and then the ESPRIT algorithm is utilized to pair the eigenvalues related to each dimension of the planar array. Finally, element positions and excitations of the sparse planar array are calculated according to the correct pairing of eigenvalues. Simulation results are presented to illustrate the effectiveness of the proposed approach.

  20. The Astrobiology Matrix and the "Drake Matrix" in Education

    Science.gov (United States)

    Mizser, A.; Kereszturi, A.

    2003-01-01

    We organized astrobiology lectures in the Eotvos Lorand University of Sciences and the Polaris Observatory in 2002. We present here the "Drake matrix" for the comparison of the astrobiological potential of different bodies [1], and astrobiology matrix for the visualization of the interdisciplinary connections between different fields of astrobiology. Conclusion: In Hungary it is difficult to integrate astrobiology in the education system but the great advantage is that it can connect different scientific fields and improve the view of students. We would like to get in contact with persons and organizations who already have experience in the education of astrobiology.

  1. A survey of matrix theory and matrix inequalities

    CERN Document Server

    Marcus, Marvin

    2010-01-01

    Written for advanced undergraduate students, this highly regarded book presents an enormous amount of information in a concise and accessible format. Beginning with the assumption that the reader has never seen a matrix before, the authors go on to provide a survey of a substantial part of the field, including many areas of modern research interest.Part One of the book covers not only the standard ideas of matrix theory, but ones, as the authors state, ""that reflect our own prejudices,"" among them Kronecker products, compound and induced matrices, quadratic relations, permanents, incidence

  2. Matrix factorizations and elliptic fibrations

    Science.gov (United States)

    Omer, Harun

    2016-09-01

    I use matrix factorizations to describe branes at simple singularities of elliptic fibrations. Each node of the corresponding Dynkin diagrams of the ADE-type singularities is associated with one indecomposable matrix factorization which can be deformed into one or more factorizations of lower rank. Branes with internal fluxes arise naturally as bound states of the indecomposable factorizations. Describing branes in such a way avoids the need to resolve singularities. This paper looks at gauge group breaking from E8 fibers down to SU (5) fibers due to the relevance of such fibrations for local F-theory GUT models. A purpose of this paper is to understand how the deformations of the singularity are understood in terms of its matrix factorizations. By systematically factorizing the elliptic fiber equation, this paper discusses geometries which are relevant for building semi-realistic local models. In the process it becomes evident that breaking patterns which are identical at the level of the Kodaira type of the fibers can be inequivalent at the level of matrix factorizations. Therefore the matrix factorization picture supplements information which the conventional less detailed descriptions lack.

  3. Octonionic matrix representation and electromagnetism

    Energy Technology Data Exchange (ETDEWEB)

    Chanyal, B. C. [Kumaun University, S. S. J. Campus, Almora (India)

    2014-12-15

    Keeping in mind the important role of octonion algebra, we have obtained the electromagnetic field equations of dyons with an octonionic 8 x 8 matrix representation. In this paper, we consider the eight - dimensional octonionic space as a combination of two (external and internal) four-dimensional spaces for the existence of magnetic monopoles (dyons) in a higher-dimensional formalism. As such, we describe the octonion wave equations in terms of eight components from the 8 x 8 matrix representation. The octonion forms of the generalized potential, fields and current source of dyons in terms of 8 x 8 matrix are discussed in a consistent manner. Thus, we have obtained the generalized Dirac-Maxwell equations of dyons from an 8x8 matrix representation of the octonion wave equations in a compact and consistent manner. The generalized Dirac-Maxwell equations are fully symmetric Maxwell equations and allow for the possibility of magnetic charges and currents, analogous to electric charges and currents. Accordingly, we have obtained the octonionic Dirac wave equations in an external field from the matrix representation of the octonion-valued potentials of dyons.

  4. Matrix factorizations and elliptic fibrations

    Directory of Open Access Journals (Sweden)

    Harun Omer

    2016-09-01

    Full Text Available I use matrix factorizations to describe branes at simple singularities of elliptic fibrations. Each node of the corresponding Dynkin diagrams of the ADE-type singularities is associated with one indecomposable matrix factorization which can be deformed into one or more factorizations of lower rank. Branes with internal fluxes arise naturally as bound states of the indecomposable factorizations. Describing branes in such a way avoids the need to resolve singularities. This paper looks at gauge group breaking from E8 fibers down to SU(5 fibers due to the relevance of such fibrations for local F-theory GUT models. A purpose of this paper is to understand how the deformations of the singularity are understood in terms of its matrix factorizations. By systematically factorizing the elliptic fiber equation, this paper discusses geometries which are relevant for building semi-realistic local models. In the process it becomes evident that breaking patterns which are identical at the level of the Kodaira type of the fibers can be inequivalent at the level of matrix factorizations. Therefore the matrix factorization picture supplements information which the conventional less detailed descriptions lack.

  5. An Epichlorohydrin-Crosslinked Semi-Interpenetrating GG-PEO Network as a Xerogel Matrix for Sustained Release of Sulpiride

    National Research Council Canada - National Science Library

    Hoosain, Famida G; Choonara, Yahya E; Kumar, Pradeep; Tomar, Lomas K; Tyagi, Charu; du Toit, Lisa C; Pillay, Viness

    2014-01-01

    The current study involved the development of a novel sustained release crosslinked semi-IPN xerogel matrix tablet prepared by chemical crosslinking of poly(ethylene) oxide (PEO) and gellan gum (GG...

  6. Preparation and Luminescence Properties of Ternary Europium Complexes In-Situ Synthesized in Silica/Polymer Hybrid Matrix by a Two-Step Sol-Gel Process%两步溶胶-凝胶法于SiO2/聚合物杂化基质中原位合成铕的三元配合物及其发光性质

    Institute of Scientific and Technical Information of China (English)

    符连社; 张洪杰; 王淑彬; 孟庆国; 杨魁跃; 倪嘉缵

    1999-01-01

    采用两步溶胶-凝胶过程制备了含铕的三元配合物的凝胶.荧光激发光谱证实于SiO2基质中原位合成了铕的配合物.含铕配合物的杂化材料发出铕的特征荧光,与相应的纯配合物溶于乙醇相比,铕离子具有较长的荧光寿命.%The gels containing ternary europium complexes have been prepared by a two-step sol-gel method.Europium complexes are in-situ synthesized in sol-gel derived silica/poly(hydroxyethyl methacrylate) matrix,and confirmed by the luminescence excitation spectrum.The hybrid materials that contain europium complexes exhibit the characteristic emission bands of Eu3+ and present longer fluorescence lifetimes than the corresponding complexes powder dissolved in ethanol solution.

  7. On Geometry and Matrix Models

    CERN Document Server

    Dijkgraaf, R; Dijkgraaf, Robbert; Vafa, Cumrun

    2002-01-01

    We point out two extensions of the relation between matrix models, topological strings and N=1 supersymmetric gauge theories. First, we note that by considering double scaling limits of unitary matrix models one can obtain large N duals of the local Calabi-Yau geometries that engineer N=2 gauge theories. In particular, a double scaling limit of the Gross-Witten one-plaquette lattice model gives the SU(2) Seiberg-Witten solution, including its induced gravitational corrections. Secondly, we point out that the effective superpotential terms for N=1 ADE quiver gauge theories is similarly computed by large multi-matrix models, that have been considered in the context of ADE minimal models on random surfaces. The associated spectral curves are multiple branched covers obtained as Virasoro and W-constraints of the partition function.

  8. On geometry and matrix models

    Science.gov (United States)

    Dijkgraaf, Robbert; Vafa, Cumrun

    2002-11-01

    We point out two extensions of the relation between matrix models, topological strings and N=1 supersymmetric gauge theories. First, we note that by considering double scaling limits of unitary matrix models one can obtain large- N duals of the local Calabi-Yau geometries that engineer N=2 gauge theories. In particular, a double scaling limit of the Gross-Witten one-plaquette lattice model gives the SU(2) Seiberg-Witten solution, including its induced gravitational corrections. Secondly, we point out that the effective superpotential terms for N=1 ADE quiver gauge theories is similarly computed by large- N multi-matrix models, that have been considered in the context of ADE minimal models on random surfaces. The associated spectral curves are multiple branched covers obtained as Virasoro and W-constraints of the partition function.

  9. On geometry and matrix models

    Energy Technology Data Exchange (ETDEWEB)

    Dijkgraaf, Robbert E-mail: rhd@science.uva.nl; Vafa, Cumrun

    2002-11-11

    We point out two extensions of the relation between matrix models, topological strings and N=1 supersymmetric gauge theories. First, we note that by considering double scaling limits of unitary matrix models one can obtain large-N duals of the local Calabi-Yau geometries that engineer N=2 gauge theories. In particular, a double scaling limit of the Gross-Witten one-plaquette lattice model gives the SU(2) Seiberg-Witten solution, including its induced gravitational corrections. Secondly, we point out that the effective superpotential terms for N=1 ADE quiver gauge theories is similarly computed by large-N multi-matrix models, that have been considered in the context of ADE minimal models on random surfaces. The associated spectral curves are multiple branched covers obtained as Virasoro and W-constraints of the partition function.

  10. Lectures on matrix field theory

    CERN Document Server

    Ydri, Badis

    2017-01-01

    These lecture notes provide a systematic introduction to matrix models of quantum field theories with non-commutative and fuzzy geometries. The book initially focuses on the matrix formulation of non-commutative and fuzzy spaces, followed by a description of the non-perturbative treatment of the corresponding field theories. As an example, the phase structure of non-commutative phi-four theory is treated in great detail, with a separate chapter on the multitrace approach. The last chapter offers a general introduction to non-commutative gauge theories, while two appendices round out the text. Primarily written as a self-study guide for postgraduate students – with the aim of pedagogically introducing them to key analytical and numerical tools, as well as useful physical models in applications – these lecture notes will also benefit experienced researchers by providing a reference guide to the fundamentals of non-commutative field theory with an emphasis on matrix models and fuzzy geometries.

  11. Noncommutative spaces from matrix models

    Science.gov (United States)

    Lu, Lei

    Noncommutative (NC) spaces commonly arise as solutions to matrix model equations of motion. They are natural generalizations of the ordinary commutative spacetime. Such spaces may provide insights into physics close to the Planck scale, where quantum gravity becomes relevant. Although there has been much research in the literature, aspects of these NC spaces need further investigation. In this dissertation, we focus on properties of NC spaces in several different contexts. In particular, we study exact NC spaces which result from solutions to matrix model equations of motion. These spaces are associated with finite-dimensional Lie-algebras. More specifically, they are two-dimensional fuzzy spaces that arise from a three-dimensional Yang-Mills type matrix model, four-dimensional tensor-product fuzzy spaces from a tensorial matrix model, and Snyder algebra from a five-dimensional tensorial matrix model. In the first part of this dissertation, we study two-dimensional NC solutions to matrix equations of motion of extended IKKT-type matrix models in three-space-time dimensions. Perturbations around the NC solutions lead to NC field theories living on a two-dimensional space-time. The commutative limit of the solutions are smooth manifolds which can be associated with closed, open and static two-dimensional cosmologies. One particular solution is a Lorentzian fuzzy sphere, which leads to essentially a fuzzy sphere in the Minkowski space-time. In the commutative limit, this solution leads to an induced metric that does not have a fixed signature, and have a non-constant negative scalar curvature, along with singularities at two fixed latitudes. The singularities are absent in the matrix solution which provides a toy model for resolving the singularities of General relativity. We also discussed the two-dimensional fuzzy de Sitter space-time, which has irreducible representations of su(1,1) Lie-algebra in terms of principal, complementary and discrete series. Field

  12. Supersymmetry in random matrix theory

    Energy Technology Data Exchange (ETDEWEB)

    Kieburg, Mario

    2010-05-04

    I study the applications of supersymmetry in random matrix theory. I generalize the supersymmetry method and develop three new approaches to calculate eigenvalue correlation functions. These correlation functions are averages over ratios of characteristic polynomials. In the first part of this thesis, I derive a relation between integrals over anti-commuting variables (Grassmann variables) and differential operators with respect to commuting variables. With this relation I rederive Cauchy- like integral theorems. As a new application I trace the supermatrix Bessel function back to a product of two ordinary matrix Bessel functions. In the second part, I apply the generalized Hubbard-Stratonovich transformation to arbitrary rotation invariant ensembles of real symmetric and Hermitian self-dual matrices. This extends the approach for unitarily rotation invariant matrix ensembles. For the k-point correlation functions I derive supersymmetric integral expressions in a unifying way. I prove the equivalence between the generalized Hubbard-Stratonovich transformation and the superbosonization formula. Moreover, I develop an alternative mapping from ordinary space to superspace. After comparing the results of this approach with the other two supersymmetry methods, I obtain explicit functional expressions for the probability densities in superspace. If the probability density of the matrix ensemble factorizes, then the generating functions exhibit determinantal and Pfaffian structures. For some matrix ensembles this was already shown with help of other approaches. I show that these structures appear by a purely algebraic manipulation. In this new approach I use structures naturally appearing in superspace. I derive determinantal and Pfaffian structures for three types of integrals without actually mapping onto superspace. These three types of integrals are quite general and, thus, they are applicable to a broad class of matrix ensembles. (orig.)

  13. Polychoric/Tetrachoric Matrix or Pearson Matrix? A methodological study

    Directory of Open Access Journals (Sweden)

    Dominguez Lara, Sergio Alexis

    2014-04-01

    Full Text Available The use of product-moment correlation of Pearson is common in most studies in factor analysis in psychology, but it is known that this statistic is only applicable when the variables related are in interval scale and normally distributed, and when are used in ordinal data may to produce a distorted correlation matrix . Thus is a suitable option using polychoric/tetrachoric matrices in item-level factor analysis when the items are in level measurement nominal or ordinal. The aim of this study was to show the differences in the KMO, Bartlett`s Test and Determinant of the Matrix, percentage of variance explained and factor loadings in depression trait scale of Depression Inventory Trait - State and the Neuroticism dimension of the short form of the Eysenck Personality Questionnaire -Revised, regarding the use of matrices polychoric/tetrachoric matrices and Pearson. These instruments was analyzed with different extraction methods (Maximum Likelihood, Minimum Rank Factor Analysis, Unweighted Least Squares and Principal Components, keeping constant the rotation method Promin were analyzed. Were observed differences regarding sample adequacy measures, as well as with respect to the explained variance and the factor loadings, for solutions having as polychoric/tetrachoric matrix. So it can be concluded that the polychoric / tetrachoric matrix give better results than Pearson matrices when it comes to item-level factor analysis using different methods.

  14. Symmetries and Interactions in Matrix String Theory

    NARCIS (Netherlands)

    Hacquebord, F.H.

    1999-01-01

    This PhD-thesis reviews matrix string theory and recent developments therein. The emphasis is put on symmetries, interactions and scattering processes in the matrix model. We start with an introduction to matrix string theory and a review of the orbifold model that flows out of matrix string theory

  15. Minimal realizations of supersymmetry for matrix Hamiltonians

    Energy Technology Data Exchange (ETDEWEB)

    Andrianov, Alexander A., E-mail: andrianov@icc.ub.edu; Sokolov, Andrey V., E-mail: avs_avs@rambler.ru

    2015-02-06

    The notions of weak and strong minimizability of a matrix intertwining operator are introduced. Criterion of strong minimizability of a matrix intertwining operator is revealed. Criterion and sufficient condition of existence of a constant symmetry matrix for a matrix Hamiltonian are presented. A method of constructing of a matrix Hamiltonian with a given constant symmetry matrix in terms of a set of arbitrary scalar functions and eigen- and associated vectors of this matrix is offered. Examples of constructing of 2×2 matrix Hamiltonians with given symmetry matrices for the cases of different structure of Jordan form of these matrices are elucidated. - Highlights: • Weak and strong minimization of a matrix intertwining operator. • Criterion of strong minimizability from the right of a matrix intertwining operator. • Conditions of existence of a constant symmetry matrix for a matrix Hamiltonian. • Method of constructing of a matrix Hamiltonian with a given constant symmetry matrix. • Examples of constructing of 2×2 matrix Hamiltonians with a given symmetry matrix.

  16. Properties of the matrix A-XY

    NARCIS (Netherlands)

    Steerneman, A.G.M.; van Perlo -ten Kleij, Frederieke

    2005-01-01

    The main topic of this paper is the matrix V = A - XY*, where A is a nonsingular complex k x k matrix and X and Y are k x p complex matrices of full column rank. Because properties of the matrix V can be derived from those of the matrix Q = I - XY*, we will consider in particular the case where A =

  17. Symmetries and Interactions in Matrix String Theory

    NARCIS (Netherlands)

    Hacquebord, F.H.

    1999-01-01

    This PhD-thesis reviews matrix string theory and recent developments therein. The emphasis is put on symmetries, interactions and scattering processes in the matrix model. We start with an introduction to matrix string theory and a review of the orbifold model that flows out of matrix string theory

  18. Towards Google matrix of brain

    Energy Technology Data Exchange (ETDEWEB)

    Shepelyansky, D.L., E-mail: dima@irsamc.ups-tlse.f [Laboratoire de Physique Theorique (IRSAMC), Universite de Toulouse, UPS, F-31062 Toulouse (France); LPT - IRSAMC, CNRS, F-31062 Toulouse (France); Zhirov, O.V. [Budker Institute of Nuclear Physics, 630090 Novosibirsk (Russian Federation)

    2010-07-12

    We apply the approach of the Google matrix, used in computer science and World Wide Web, to description of properties of neuronal networks. The Google matrix G is constructed on the basis of neuronal network of a brain model discussed in PNAS 105 (2008) 3593. We show that the spectrum of eigenvalues of G has a gapless structure with long living relaxation modes. The PageRank of the network becomes delocalized for certain values of the Google damping factor {alpha}. The properties of other eigenstates are also analyzed. We discuss further parallels and similarities between the World Wide Web and neuronal networks.

  19. Preparing for Surgery

    Science.gov (United States)

    ... Events Advocacy For Patients About ACOG Preparing for Surgery Home For Patients Search FAQs Preparing for Surgery ... Surgery FAQ080, August 2011 PDF Format Preparing for Surgery Gynecologic Problems What is the difference between outpatient ...

  20. Preparing for Surgery

    Science.gov (United States)

    ... Events Advocacy For Patients About ACOG Preparing for Surgery Home For Patients Search FAQs Preparing for Surgery ... Surgery FAQ080, August 2011 PDF Format Preparing for Surgery Gynecologic Problems What is the difference between outpatient ...

  1. Preparation of zeolite covered cellulose fibers

    Energy Technology Data Exchange (ETDEWEB)

    Mintova, S.; Valtchev, V. [Institute of Applied Mineralogy, Sofia (Bulgaria)

    1995-12-01

    Membrane separation has proved to be an important technology in chemical industry. That is why the design of different type of zeolite containing membranes has received much attention during the last decade. Zeolite containing filters and membranes were prepared by embedding zeolite crystals with adhesive substances in the cellulose matrix. This communication discussed the preparation of zeolite containing cellulose materials by in situ crystallization. Discussed axe: (1) the effect of the vegetal fiber structure and chemical composition (2) the effect of the type of the zeolite coating; (3) the effect of the mechanical and chemical treatment of the fibers on the process of the fiber zeolite coating.

  2. Random matrix theory and multivariate statistics

    OpenAIRE

    Diaz-Garcia, Jose A.; Jáimez, Ramon Gutiérrez

    2009-01-01

    Some tools and ideas are interchanged between random matrix theory and multivariate statistics. In the context of the random matrix theory, classes of spherical and generalised Wishart random matrix ensemble, containing as particular cases the classical random matrix ensembles, are proposed. Some properties of these classes of ensemble are analysed. In addition, the random matrix ensemble approach is extended and a unified theory proposed for the study of distributions for real normed divisio...

  3. Matrix theory selected topics and useful results

    CERN Document Server

    Mehta, Madan Lal

    1989-01-01

    Matrices and operations on matrices ; determinants ; elementary operations on matrices (continued) ; eigenvalues and eigenvectors, diagonalization of normal matrices ; functions of a matrix ; positive definiteness, various polar forms of a matrix ; special matrices ; matrices with quaternion elements ; inequalities ; generalised inverse of a matrix ; domain of values of a matrix, location and dispersion of eigenvalues ; symmetric functions ; integration over matrix variables ; permanents of doubly stochastic matrices ; infinite matrices ; Alexander matrices, knot polynomials, torsion numbers.

  4. Sign Patterns That Allow the Given Matrix

    Institute of Scientific and Technical Information of China (English)

    邵燕灵; 孙良

    2003-01-01

    Let P be a property referring to a real matrix. For a sign pattern A, if there exists a real matrix B in the qualitative class of A such that B has property P, then we say A allows P. Three cases that A allows an M-matrix, an inverse M-matrix and a P0-matrix are considered. The complete characterizations are obtained.

  5. Osteoblast Differentiation and Bone Matrix Formation In Vivo and In Vitro.

    Science.gov (United States)

    Blair, Harry C; Larrouture, Quitterie C; Li, Yanan; Lin, Hang; Beer-Stoltz, Donna; Liu, Li; Tuan, Rocky S; Robinson, Lisa J; Schlesinger, Paul H; Nelson, Deborah J

    2017-06-01

    We review the characteristics of osteoblast differentiation and bone matrix synthesis. Bone in air breathing vertebrates is a specialized tissue that developmentally replaces simpler solid tissues, usually cartilage. Bone is a living organ bounded by a layer of osteoblasts that, because of transport and compartmentalization requirements, produce bone matrix exclusively as an organized tight epithelium. With matrix growth, osteoblasts are reorganized and incorporated into the matrix as living cells, osteocytes, which communicate with each other and surface epithelium by cell processes within canaliculi in the matrix. The osteoblasts secrete the organic matrix, which are dense collagen layers that alternate parallel and orthogonal to the axis of stress loading. Into this matrix is deposited extremely dense hydroxyapatite-based mineral driven by both active and passive transport and pH control. As the matrix matures, hydroxyapatite microcrystals are organized into a sophisticated composite in the collagen layer by nucleation in the protein lattice. Recent studies on differentiating osteoblast precursors revealed a sophisticated proton export network driving mineralization, a gene expression program organized with the compartmentalization of the osteoblast epithelium that produces the mature bone matrix composite, despite varying serum calcium and phosphate. Key issues not well defined include how new osteoblasts are incorporated in the epithelial layer, replacing those incorporated in the accumulating matrix. Development of bone in vitro is the subject of numerous projects using various matrices and mesenchymal stem cell-derived preparations in bioreactors. These preparations reflect the structure of bone to variable extents, and include cells at many different stages of differentiation. Major challenges are production of bone matrix approaching the in vivo density and support for trabecular bone formation. In vitro differentiation is limited by the organization and

  6. Unravelling the nuclear matrix proteome

    DEFF Research Database (Denmark)

    Albrethsen, Jakob; Knol, Jaco C; Jimenez, Connie R

    2009-01-01

    The nuclear matrix (NM) model posits the presence of a protein/RNA scaffold that spans the mammalian nucleus. The NM proteins are involved in basic nuclear function and are a promising source of protein biomarkers for cancer. Importantly, the NM proteome is operationally defined as the proteins...

  7. Parallel Sparse Matrix - Vector Product

    DEFF Research Database (Denmark)

    Alexandersen, Joe; Lazarov, Boyan Stefanov; Dammann, Bernd

    This technical report contains a case study of a sparse matrix-vector product routine, implemented for parallel execution on a compute cluster with both pure MPI and hybrid MPI-OpenMP solutions. C++ classes for sparse data types were developed and the report shows how these class can be used...

  8. Matrix Treatment of Ray Optics.

    Science.gov (United States)

    Quon, W. Steve

    1996-01-01

    Describes a method to combine two learning experiences--optical physics and matrix mathematics--in a straightforward laboratory experiment that allows engineering/physics students to integrate a variety of learning insights and technical skills, including using lasers, studying refraction through thin lenses, applying concepts of matrix…

  9. Sparse Matrix Vector Processing Formats

    NARCIS (Netherlands)

    Stathis, P.T.

    2004-01-01

    In this dissertation we have identified vector processing shortcomings related to the efficient storing and processing of sparse matrices. To alleviate existent problems we propose two storage formats denoted as Block Based Compression Storage (BBCS) format and Hierarchical Sparse Matrix (HiSM) stor

  10. The COMPADRE Plant Matrix Database

    DEFF Research Database (Denmark)

    2014-01-01

    COMPADRE contains demographic information on hundreds of plant species. The data in COMPADRE are in the form of matrix population models and our goal is to make these publicly available to facilitate their use for research and teaching purposes. COMPADRE is an open-access database. We only request...

  11. Hyper-systolic matrix multiplication

    NARCIS (Netherlands)

    Lippert, Th.; Petkov, N.; Palazzari, P.; Schilling, K.

    2001-01-01

    A novel parallel algorithm for matrix multiplication is presented. It is based on a 1-D hyper-systolic processor abstraction. The procedure can be implemented on all types of parallel systems. (C) 2001 Elsevier Science B,V. All rights reserved.

  12. Student Transfer Matrix, Fall 1996.

    Science.gov (United States)

    Oklahoma State Regents for Higher Education, Oklahoma City.

    The Student Transfer Matrix provides data on the numbers of students transferring from Oklahoma public and private institutions of higher education to other Oklahoma institutions, using data from receiving institutions. Among the highlights are: the number of students who transferred to four-year and two-year institutions remained steady at 57.8…

  13. Regularization in Matrix Relevance Learning

    NARCIS (Netherlands)

    Schneider, Petra; Bunte, Kerstin; Stiekema, Han; Hammer, Barbara; Villmann, Thomas; Biehl, Michael

    2010-01-01

    A In this paper, we present a regularization technique to extend recently proposed matrix learning schemes in learning vector quantization (LVQ). These learning algorithms extend the concept of adaptive distance measures in LVQ to the use of relevance matrices. In general, metric learning can displa

  14. Perturbation semigroup of matrix algebras

    OpenAIRE

    Neumann, N.; Suijlekom, W.D. van

    2016-01-01

    In this article we analyze the structure of the semigroup of inner perturbations in noncommutative geometry. This perturbation semigroup is associated to a unital associative *-algebra and extends the group of unitary elements of this *-algebra. We compute the perturbation semigroup for all matrix algebras.

  15. Bilateral matrix-exponential distributions

    DEFF Research Database (Denmark)

    Bladt, Mogens; Esparza, Luz Judith R; Nielsen, Bo Friis

    2012-01-01

    In this article we define the classes of bilateral and multivariate bilateral matrix-exponential distributions. These distributions have support on the entire real space and have rational moment-generating functions. These distributions extend the class of bilateral phasetype distributions of [1]...

  16. Multivariate Modelling via Matrix Subordination

    DEFF Research Database (Denmark)

    Nicolato, Elisa

    stochastic volatility via time-change is quite ineffective when applied to the multivariate setting. In this work we propose a new class of models, which is obtained by conditioning a multivariate Brownian Motion to a so-called matrix subordinator. The obtained model-class encompasses the vast majority...

  17. Neonatal disorders of germinal matrix

    NARCIS (Netherlands)

    Raets, M M A; Dudink, J; Govaert, P

    2015-01-01

    The germinal matrix (GM) is a richly vascularized, transient layer near the ventricles. It produces neurons and glial cells, and is present in the foetal brain between 8 and 36 weeks of gestation. At 25 weeks, it reaches its maximum volume and subsequently withers. The GM is vulnerable to haemorrhag

  18. Adams Operations on Matrix Factorizations

    OpenAIRE

    Brown, Michael K.; Miller, Claudia; Thompson, Peder; Walker, Mark E.

    2016-01-01

    We define Adams operations on matrix factorizations, and we show these operations enjoy analogues of several key properties of the Adams operations on perfect complexes with support developed by Gillet-Soul\\'e in their paper "Intersection Theory Using Adams Operations". As an application, we give a proof of a conjecture of Dao-Kurano concerning the vanishing of Hochster's theta invariant.

  19. Parallel Sparse Matrix - Vector Product

    DEFF Research Database (Denmark)

    Alexandersen, Joe; Lazarov, Boyan Stefanov; Dammann, Bernd

    This technical report contains a case study of a sparse matrix-vector product routine, implemented for parallel execution on a compute cluster with both pure MPI and hybrid MPI-OpenMP solutions. C++ classes for sparse data types were developed and the report shows how these class can be used...

  20. The COMPADRE Plant Matrix Database

    DEFF Research Database (Denmark)

    2014-01-01

    COMPADRE contains demographic information on hundreds of plant species. The data in COMPADRE are in the form of matrix population models and our goal is to make these publicly available to facilitate their use for research and teaching purposes. COMPADRE is an open-access database. We only request...

  1. Multivariate Matrix-Exponential Distributions

    DEFF Research Database (Denmark)

    Bladt, Mogens; Nielsen, Bo Friis

    2010-01-01

    -exponential distributions. We prove a characterization that states that a distribution is an MVME distribution if and only if all non-negative, non-null linear combinations of the coordinates have a univariate matrix-exponential distribution. This theorem is analog to a well-known characterization theorem...

  2. Preparation of Rodent Testis Co-Cultures

    OpenAIRE

    Wegner, Susanna; Hong, Sungwoo; Yu, Xiaozhong; Faustman, Elaine M.

    2013-01-01

    Male reproductive development is a complex process that is sensitive to disruption by a range of toxicants. There is a great need for in vitro models that can evaluate potential male reproductive toxicants. The current unit presents a protocol for preparation of a three-dimensional in vitro model of male reproductive development that reduces the number of animals required for evaluation of toxicants. A Matrigel overlay provides a three-dimensional extracellular matrix that improves cell attac...

  3. The HDTV digital audio matrix

    Science.gov (United States)

    Mason, A. J.

    Multichannel sound systems are being studied as part of the Eureka 95 and Radio-communication Bureau TG10-1 investigations into high definition television. One emerging sound system has five channels; three at the front and two at the back. This raises some compatibility issues. The listener might have only, say, two loudspeakers or the material to be broadcast may have fewer than five channels. The problem is how best to produce a set of signals to be broadcast, which is suitable for all listeners, from those that are available. To investigate this area, a device has been designed and built which has six input channels and six output channels. Each output signal is a linear combination of the input signals. The inputs and outputs are in AES/EBU digital audio format using BBC-designed AESIC chips. The matrix operation, to produce the six outputs from the six inputs, is performed by a Motorola DSP56001. The user interface and 'housekeeping' is managed by a T222 transputer. The operator of the matrix uses a VDU to enter sets of coefficients and a rotary switch to select which set to use. A set of analog controls is also available and is used to control operations other than the simple compatibility matrixing. The matrix has been very useful for simple tasks: mixing a stereo signal into mono, creating a stereo signal from a mono signal, applying a fixed gain or attenuation to a signal, exchanging the A and B channels of an AES/EBU bitstream, and so on. These are readily achieved using simple sets of coefficients. Additions to the user interface software have led to several more sophisticated applications which still consist of a matrix operation. Different multichannel panning laws have been evaluated. The analog controls adjust the panning; the audio signals are processed digitally using a matrix operation. A digital SoundField microphone decoder has also been implemented. digital audio matrix is such that it can be applied to a wide variety of signal processing

  4. A DIRECT ALGORITHM FOR DISTINGUISHING NONSINGULAR M-MATRIX AND H-MATRIX

    Institute of Scientific and Technical Information of China (English)

    Li Yaotang; Zhu Yan

    2005-01-01

    A direct algorithm is proposed by which one can distinguish whether a matrix is an M-matrix (or H-matrix) or not quickly and effectively. Numerical examples show that it is effective and convincible to distinguish M-matrix (or H-matrix) by using the algorithm.

  5. Gum copal and gum damar: Novel matrix forming materials for sustained drug delivery

    OpenAIRE

    Morkhade D; Fulzele S; Satturwar P; Joshi S

    2006-01-01

    This study concerns the evaluation of natural gum copal and gum damar as novel sustained release matrix forming materials in tablet formulation. Along with the physicochemical properties, gum copal and gum damar were characterized for molecular weight, polydispersity index and glass transition temperature. Matrix tablets were prepared by wet granulation technique using isopropyl alcohol as a granulating agent. Diclofenac sodium was used as a model drug. Tablet weight (250 mg) and diameter (9 ...

  6. A Study of Groundwater Matrix Effects for the Destruction of Trichloroethylene Using Fe/Pd Nanoaggregates

    Energy Technology Data Exchange (ETDEWEB)

    meyer, D E [Univ of KY, dept of chemical and materials engineering; Hampson, Steve [Univ of KY Center for Applied Energy Research - Ky Research Consortium of Energy and Environment; ormsbee, Lindelle [Univ of KY Center for Applied Energy Research - Ky Research Consortium of Energy and Environment; Bhattacharyya, Dibakar [univ of KY, Dept of Chemical and Materials Engineering

    2008-06-01

    Fe nanoaggregates have been prepared using the sodium borohydride reduction method and post-coated with Pd using aqueous phase electro-depostition. The Fe/Pd particles have been used to examine dechlorination of TCE with regard to matrix effects using materials representative of examine dechlorination of TCE with regard to matrix effects using materials representative of a potential zero-valent metal remediation site surrounding the Paducah Gaseous Diffusion Plant in Paducah, KY.

  7. Texture and residual strain in SiC/Ti-6-2-4-2 titanium matrix composites

    Energy Technology Data Exchange (ETDEWEB)

    Rangaswamy, P.; Bennett, K.; Bourke, M.A.M.; Dreele, R. von; Roberts, J.A. [Los Alamos National Lab., NM (United States). Manuel Lujan Jr. Neutron Scattering Center; Jayaraman, N. [Univ. of Cincinnati, OH (United States). Dept. of Materials Science and Engineering

    1997-11-01

    Residual strain and texture variations were measured in two Titanium matrix composites reinforced with Silicon Carbide fibers (Ti/SiC) having the same composition but fabricated by dramatically different processing routes. In both specimens the Titanium matrix comprised an {alpha}/{beta} alloy (Ti-6242) containing approximately 35% by volume of continuous SiC fibers. In one case the matrix was produced by a plasma spray (PS) route and the other by a wire drawing (WD) process. The resulting textures in the matrix differ significantly, from approximately random for the PS matrix to 6.25X random in the WD matrix. No significant differences in matrix residual strains between the composites prepared by the two procedures were noted. Plane-specific elastic moduli, measured in load tests on the unreinforced matrices also showed little difference.

  8. Optimization of matrix tablets controlled drug release using Elman dynamic neural networks and decision trees.

    Science.gov (United States)

    Petrović, Jelena; Ibrić, Svetlana; Betz, Gabriele; Đurić, Zorica

    2012-05-30

    The main objective of the study was to develop artificial intelligence methods for optimization of drug release from matrix tablets regardless of the matrix type. Static and dynamic artificial neural networks of the same topology were developed to model dissolution profiles of different matrix tablets types (hydrophilic/lipid) using formulation composition, compression force used for tableting and tablets porosity and tensile strength as input data. Potential application of decision trees in discovering knowledge from experimental data was also investigated. Polyethylene oxide polymer and glyceryl palmitostearate were used as matrix forming materials for hydrophilic and lipid matrix tablets, respectively whereas selected model drugs were diclofenac sodium and caffeine. Matrix tablets were prepared by direct compression method and tested for in vitro dissolution profiles. Optimization of static and dynamic neural networks used for modeling of drug release was performed using Monte Carlo simulations or genetic algorithms optimizer. Decision trees were constructed following discretization of data. Calculated difference (f(1)) and similarity (f(2)) factors for predicted and experimentally obtained dissolution profiles of test matrix tablets formulations indicate that Elman dynamic neural networks as well as decision trees are capable of accurate predictions of both hydrophilic and lipid matrix tablets dissolution profiles. Elman neural networks were compared to most frequently used static network, Multi-layered perceptron, and superiority of Elman networks have been demonstrated. Developed methods allow simple, yet very precise way of drug release predictions for both hydrophilic and lipid matrix tablets having controlled drug release.

  9. Spine fusion using cell matrix composites enriched in bone marrow-derived cells.

    Science.gov (United States)

    Muschler, George F; Nitto, Hironori; Matsukura, Yoichi; Boehm, Cynthia; Valdevit, Antonio; Kambic, Helen; Davros, William; Powell, Kimerly; Easley, Kirk

    2003-02-01

    Bone marrow-derived cells including osteoblastic progenitors can be concentrated rapidly from bone marrow aspirates using the surface of selected implantable matrices for selective cell attachment. Concentration of cells in this way to produce an enriched cellular composite graft improves graft efficacy. The current study was designed to test the hypothesis that the biologic milieu of a bone marrow clot will significantly improve the efficacy of such a graft. An established posterior spinal fusion model and cancellous bone matrix was used to compare an enriched cellular composite bone graft alone, bone matrix plus bone marrow clot, and an enriched bone matrix composite graft plus bone marrow clot. Union score, quantitative computed tomography, and mechanical testing were used to define outcome. The union score for the enriched bone matrix plus bone marrow clot composite was superior to the enriched bone matrix alone and the bone matrix plus bone marrow clot. The enriched bone matrix plus bone marrow clot composite also was superior to the enriched bone matrix alone in fusion volume and in fusion area. These data confirm that the addition of a bone marrow clot to an enriched cell-matrix composite graft results in significant improvement in graft performance. Enriched composite grafts prepared using this strategy provide a rapid, simple, safe, and inexpensive method for intraoperative concentration and delivery of bone marrow-derived cells and connective tissue progenitors that may improve the outcome of bone grafting.

  10. DEVELOPMENT OF LIGNIN EPOXIDE—A POTENTIAL MATRIX OF RESIN MATRIX COMPOSITE

    Institute of Scientific and Technical Information of China (English)

    2000-01-01

    To develop new kinds of matrix resin of composite and utilize lignosulfonate in large scale and high value, a kind of lignosulfonate was modified into epoxide in this paper. Two kinds of phenolized lignosulfonic acid and two kinds of lignin epoxides were prepared. The lignin epoxides and a kind of bisphenol-A epoxy resin were mixed respectively with a kind of liquid anhydride (MNA) to be measured by DSC technology. Both of these two kinds of epoxides can be cured by MNA, and curing exotherm of the liquid one is more than that of the solid one. Samples of the phenolized lignosulfonic acid and the epoxides were all analyzed by IR spectroscopy to find relations between them. It is suggested that the phenolation decide the type and the yield of the lignin epoxides.

  11. Grewia polysaccharide as a pharmaceutical excipient in matrix tablets

    Directory of Open Access Journals (Sweden)

    Elijah I. Nep

    2011-03-01

    Full Text Available Matrix-based tablets using different concentrations of grewia gum, and the model drug ibuprofen, were prepared using a wet granulation technique. Similar formulations were also prepared using HPMC, guar gum or ethyl cellulose as the polymer matrix. In addition to tablet properties, swelling and erosion of tablets and kinetics of drug release were also investigated. In vitro drug release studies, in phosphate buffer (pH 7.2 using USP type II apparatus, revealed that grewia gum at concentrations of 16%, 32% and 48% can sustain therelease of ibuprofen tablets for up to 24 hours. Release profiles were similar to those tablets containing ethyl cellulose as the matrix former. Swelling and erosion of grewia gum matrices occurred simultaneously, and ibuprofen release was by anomalous diffusion in accordance with the Korsmeyer-Peppas model. There was evidence suggesting synergism between grewia gum and guar gum in sustaining the release of ibuprofen from tablets when used in the ratio 2:1. Grewia gum may therefore prove a useful excipient, when used on its own, or in combination with other polymers, to modify drug release.

  12. Preparation and Characterization of Magnetic Chitosan Microcapsules

    Directory of Open Access Journals (Sweden)

    Xiaopeng Xiong

    2013-01-01

    Full Text Available By dispersing aqueous precipitant in liquid paraffin to prepare a W/O emulsion then adding chitosan (CS solution, CS microcapsules have been successfully prepared. It is a facile way to prepare polymer microcapsules by using aqueous precipitant or nonsolvent as template, which avoids the removal of template and would free from the necessity to cross-link the microcapsule as usual methods to directly form dense shell. The hollow feature of the obtained materials is revealed. The diameter of the microcapsules ranges from several μm to over 100 μm. Magnetic CS microcapsules have been prepared in this way when Fe3+ and Fe2+ were mixed with CS to prepare a mixture starting solution. The appearance and microstructure of the composite microcapsules were studied. The results indicate that the formed Fe3O4 nanoparticles are embedded in the CS matrix evenly due to strong interaction between the Fe3O4 nanoparticles and the CS molecules. The Fe3O4 content and the magnetic properties of the composite microcapsule were measured. The composite microcapsules were calcined in air at 700°C to prepare pure inorganic hollow microspheres. It is general to prepare hollow polymeric or composite particles by using this method.

  13. NewIn-situ synthesis method of magnesium matrix composites reinforced with TiC particulates

    Directory of Open Access Journals (Sweden)

    Zhang Xiuqing

    2006-12-01

    Full Text Available Magnesium matrix composites reinforced with TiC particulates was prepared using a new in-situ synthesis method of remelting and dilution technique. And measurements were performed on the composites. The results of x ray diffraction (XRD analysis confirmed that TiC particulates were synthesized during the sintering process, and they retained in magnesium matrix composites after the remelting and dilution processing. From the microstructure characterization and electron probe microanalysis (EPMA, we could see that fine TiC particulates distributed uniformly in the matrix material.

  14. TECHNOLOGY AND ANALYSIS DEVELOPMENT OF STOMATOLOGICAL MATRIX SYSTEM OF MULTIFUNCTIONAL ACTION DELIVERY

    Directory of Open Access Journals (Sweden)

    T. F. Marinina

    2014-01-01

    Full Text Available Timeliness of double-layer matrix system (of stomatological medicated films with antiinflammatory, local anesthetic, regenerative, anti-edematous action was shown. One layer of the system includes lidocaine hydrochloride and kalanchoe sap, another contains furacilin and urea. The best possible polymer carriers of preparations under study which provide their sufficient release from matrix system. Signified antimicrobic activity of double-layer system and osmotic activity were established. Double-layer matrix systems offered may be used in stomatology with for treatment and preventive measures of different diseases of parodontium tissues

  15. Preparation and properties of gluten/calcium carbonate composites

    Institute of Scientific and Technical Information of China (English)

    Min Zuo; Zheng Zheng Lai; Yi Hu Song; Qiang Zheng

    2008-01-01

    Environment friendly thermosetting composites were prepared by blending wheat gluten (WG) as matrix, calcium carbonate (CaCO3) as filler and glycerol as plasticizer followed by compression molding the mixture at 120 ℃ to crosslink the WG matrix. Morphology observation showed that the CaCO3 particles were finely dispersed in matrix. Incorporation of CaCO3 up to 10 wt% into the composites caused Young's modulus and tensile strength to increase markedly. On the other hand, the moisture absorption and elongation at break decreased slightly.

  16. The Constrained Solutions of Two Matrix Equations

    Institute of Scientific and Technical Information of China (English)

    An Ping LIAO; Zhong Zhi BAI

    2002-01-01

    We study the symmetric positive semidefinite solution of the matrix equation AX1AT +BX2BT = C, where A is a given real m × n matrix, B is a given real m × p matrix, and C is a givenreal m × m matrix, with m, n, p positive integers; and the bisymmetric positive semidefinite solutionof the matrix equation DTXD = C, where D is a given real n × m matrix, C is a given real m × mmatrix, with m, n positive integers. By making use of the generalized singular value decomposition, wederive general analytic formulae, and present necessary and sufficient conditions for guaranteeing theexistence of these solutions.

  17. Automated MALDI matrix deposition method with inkjet printing for imaging mass spectrometry.

    Science.gov (United States)

    Baluya, Dodge L; Garrett, Timothy J; Yost, Richard A

    2007-09-01

    Careful matrix deposition on tissue samples for matrix-assisted laser desorption/ionization (MALDI) is critical for producing reproducible analyte ion signals. Traditional methods for matrix deposition are often considered an art rather than a science, with significant sample-to-sample variability. Here we report an automated method for matrix deposition, employing a desktop inkjet printer (printer tray, designed to hold CDs and DVDs, was modified to hold microscope slides. Empty ink cartridges were filled with MALDI matrix solutions, including DHB in methanol/water (70:30) at concentrations up to 40 mg/mL. Various samples (including rat brain tissue sections and standards of small drug molecules) were prepared using three deposition methods (electrospray, airbrush, inkjet). A linear ion trap equipped with an intermediate-pressure MALDI source was used for analyses. Optical microscopic examination showed that matrix crystals were formed evenly across the sample. There was minimal background signal after storing the matrix in the cartridges over a 6-month period. Overall, the mass spectral images gathered from inkjet-printed tissue specimens were of better quality and more reproducible than from specimens prepared by the electrospray and airbrush methods.

  18. Tricolor white emitting phosphor co-doped with Eu, Dy in SiO2 matrix

    Institute of Scientific and Technical Information of China (English)

    HU XiaoYun; FAN Jun; ZHANG DeKai; MA YiPing; BAI JinTao; REN ZhaoYu; HOU Xun

    2008-01-01

    A Eu, Dy co-doped SiO2 matrix, white emitting phosphor was prepared by the sol-gel technique. Strong red, green and blue emissions located at 618 nm, 573 nm and 400-550 nm were observed under UV laser excitation at room temperature. Such techniques as FT-IR and TGA-DSC were used to measure the microstructure of the luminescent material. The influence of the preparation techniques on the lu-minescence property of the Eu, Dy co-doped SiO2 matrix, such as anneal temperature, anneal time, dried atmosphere and the components of the matrix, was systematically studied, and the luminescence mechanism was interpreted. The red emission is the strongest when annealed at 750℃. However, blue emission appears when annealed at 700℃ and is the intensest at 900℃. For the samples dried in vac-uum, Eu3+ is more easily deoxidized to Eu2+ at lower temperatures, because the samples dried in the air compared with that dried in vacuum need higher temperature to form network structures. Only the SA and SAB matrix annealed at 850℃ had blue emission in the four matrices (SA, SAB, SB, S) xerogel and the emission in the SAB matrix was stronger than that in the SA matrix. This may be due to the eutectic phase formed by the oxide boron, alkaline oxide and alumina in the SAB matrix, which constructs network structures and stabilizes the emission center and enhances the blue emission.

  19. Scrambling with matrix black holes

    Science.gov (United States)

    Brady, Lucas; Sahakian, Vatche

    2013-08-01

    If black holes are not to be dreaded sinks of information but rather fully described by unitary evolution, they must scramble in-falling data and eventually leak it through Hawking radiation. Sekino and Susskind have conjectured that black holes are fast scramblers; they generate entanglement at a remarkably efficient rate, with the characteristic time scaling logarithmically with the entropy. In this work, we focus on Matrix theory—M-theory in the light-cone frame—and directly probe the conjecture. We develop a concrete test bed for quantum gravity using the fermionic variables of Matrix theory and show that the problem becomes that of chains of qubits with an intricate network of interactions. We demonstrate that the black hole system evolves much like a Brownian quantum circuit, with strong indications that it is indeed a fast scrambler. We also analyze the Berenstein-Maldacena-Nastase model and reach the same tentative conclusion.

  20. Link Prediction via Matrix Completion

    CERN Document Server

    Pech, Ratha; Pan, Liming; Cheng, Hong; Zhou, Tao

    2016-01-01

    Inspired by practical importance of social networks, economic networks, biological networks and so on, studies on large and complex networks have attracted a surge of attentions in the recent years. Link prediction is a fundamental issue to understand the mechanisms by which new links are added to the networks. We introduce the method of robust principal component analysis (robust PCA) into link prediction, and estimate the missing entries of the adjacency matrix. On one hand, our algorithm is based on the sparsity and low rank property of the matrix, on the other hand, it also performs very well when the network is dense. This is because a relatively dense real network is also sparse in comparison to the complete graph. According to extensive experiments on real networks from disparate fields, when the target network is connected and sufficiently dense, whatever it is weighted or unweighted, our method is demonstrated to be very effective and with prediction accuracy being considerably improved comparing wit...

  1. Standardisation of ceramic matrix composites

    Directory of Open Access Journals (Sweden)

    Gomez Philippe

    2015-01-01

    Full Text Available The standardisation on ceramic matrix composite (CMCs test methods occurred in the 1980's as these materials began to display interesting properties for aeronautical applications. Since the French Office of standardisation B43C has participated in establishing more than 40 standards and guides dealing with their thermal mechanical properties, their reinforcement and their fibre/matrix interface. As their maturity has been demonstrated through several technological development programmes (plugs, flaps, blades …, the air framers and engine manufacturers are now thinking of develop industrial parts which require a certification from airworthiness authorities. Now the standardisation of CMCs has to turn toward documents completing the certification requirement for civil and military applications. The news standards will allow being more confident with CMCs in taking into account their specificity.

  2. Density matrix quantum Monte Carlo

    CERN Document Server

    Blunt, N S; Spencer, J S; Foulkes, W M C

    2013-01-01

    This paper describes a quantum Monte Carlo method capable of sampling the full density matrix of a many-particle system, thus granting access to arbitrary reduced density matrices and allowing expectation values of complicated non-local operators to be evaluated easily. The direct sampling of the density matrix also raises the possibility of calculating previously inaccessible entanglement measures. The algorithm closely resembles the recently introduced full configuration interaction quantum Monte Carlo method, but works all the way from infinite to zero temperature. We explain the theory underlying the method, describe the algorithm, and introduce an importance-sampling procedure to improve the stochastic efficiency. To demonstrate the potential of our approach, the energy and staggered magnetization of the isotropic antiferromagnetic Heisenberg model on small lattices and the concurrence of one-dimensional spin rings are compared to exact or well-established results. Finally, the nature of the sign problem...

  3. Matrix dynamics of fuzzy spheres

    CERN Document Server

    Jatkar, D P; Wadia, S R; Yogendran, K P; Jatkar, Dileep P.; Mandal, Gautam; Wadia, Spenta R.

    2002-01-01

    We study the dynamics of fuzzy two-spheres in a matrix model which represents string theory in the presence of RR flux. We analyze the stability of known static solutions of such a theory which contain commuting matrices and SU(2) representations. We find that irreducible as well as reducible representations are stable. Since the latter are of higher energy, this stability poses a puzzle. We resolve this puzzle by noting that reducible representations have marginal directions corresponding to non-spherical deformations. We obtain new static solutions by turning on these marginal deformations. These solutions now have instability or tachyonic directions. We discuss condensation of these tachyons which correspond to classical trajectories interpolating from multiple, small fuzzy spheres to a single, large sphere. We briefly discuss spatially independent configurations of a D3/D5 system described by the same matrix model which now possesses a supergravity dual.

  4. Matrix metalloproteinases in lung biology

    Directory of Open Access Journals (Sweden)

    Parks William C

    2000-12-01

    Full Text Available Abstract Despite much information on their catalytic properties and gene regulation, we actually know very little of what matrix metalloproteinases (MMPs do in tissues. The catalytic activity of these enzymes has been implicated to function in normal lung biology by participating in branching morphogenesis, homeostasis, and repair, among other events. Overexpression of MMPs, however, has also been blamed for much of the tissue destruction associated with lung inflammation and disease. Beyond their role in the turnover and degradation of extracellular matrix proteins, MMPs also process, activate, and deactivate a variety of soluble factors, and seldom is it readily apparent by presence alone if a specific proteinase in an inflammatory setting is contributing to a reparative or disease process. An important goal of MMP research will be to identify the actual substrates upon which specific enzymes act. This information, in turn, will lead to a clearer understanding of how these extracellular proteinases function in lung development, repair, and disease.

  5. Vibrational Density Matrix Renormalization Group.

    Science.gov (United States)

    Baiardi, Alberto; Stein, Christopher J; Barone, Vincenzo; Reiher, Markus

    2017-08-08

    Variational approaches for the calculation of vibrational wave functions and energies are a natural route to obtain highly accurate results with controllable errors. Here, we demonstrate how the density matrix renormalization group (DMRG) can be exploited to optimize vibrational wave functions (vDMRG) expressed as matrix product states. We study the convergence of these calculations with respect to the size of the local basis of each mode, the number of renormalized block states, and the number of DMRG sweeps required. We demonstrate the high accuracy achieved by vDMRG for small molecules that were intensively studied in the literature. We then proceed to show that the complete fingerprint region of the sarcosyn-glycin dipeptide can be calculated with vDMRG.

  6. Matrix Factorization for Evolution Data

    Directory of Open Access Journals (Sweden)

    Xiao-Yu Huang

    2014-01-01

    Full Text Available We study a matrix factorization problem, that is, to find two factor matrices U and V such that R≈UT×V, where R is a matrix composed of the values of the objects O1,O2,…,On at consecutive time points T1,T2,…,Tt. We first present MAFED, a constrained optimization model for this problem, which straightforwardly performs factorization on R. Then based on the interplay of the data in U, V, and R, a probabilistic graphical model using the same optimization objects is constructed, in which structural dependencies of the data in these matrices are revealed. Finally, we present a fitting algorithm to solve the proposed MAFED model, which produces the desired factorization. Empirical studies on real-world datasets demonstrate that our approach outperforms the state-of-the-art comparison algorithms.

  7. Organ-specific chemotactic factors present in lung extracellular matrix.

    Science.gov (United States)

    Cerra, R F; Nathanson, S D

    1989-05-01

    The preferential colonization of a distant organ by a circulating tumor cell (organ specific metastasis) may be regulated by chemotactic factors present within the extracellular matrix of the host organ. Organ-specific extracellular matrix was prepared from murine kidney and lung by high salt extraction and DNAase/RNAase digestion. A soluble protein fraction (S2) from each of the matricies was obtained by 4 M guanidine extraction and was tested for organ-specific chemotactic activity in a modified Boyden chamber. The lung colonizing B16-F10 and B16-BL6 tumor cell lines demonstrated organ-specific motility only toward the lung extract. The low metastasizing B16 parental line and liver colonizing B16-L4b line showed no preference for either lung or kidney. The lung activity resolves into five fractions by gel filtration chromatography, with the highest activity eluting at Mr approximately 71,000. Chemotactic factors present in lung extracellular matrix may regulate the preferential colonization of an organ by stimulating the migration of tumor cells in a specific manner. These factors may be released during the degradation of the extracellular matrix.

  8. On Skew Triangular Matrix Rings

    Institute of Scientific and Technical Information of China (English)

    Wang Wei-liang; Wang Yao; Ren Yan-li

    2016-01-01

    Letαbe a nonzero endomorphism of a ring R, n be a positive integer and Tn(R,α) be the skew triangular matrix ring. We show that some properties related to nilpotent elements of R are inherited by Tn(R,α). Meanwhile, we determine the strongly prime radical, generalized prime radical and Behrens radical of the ring R[x;α]/(xn), where R[x;α] is the skew polynomial ring.

  9. Staggered chiral random matrix theory

    CERN Document Server

    Osborn, James C

    2010-01-01

    We present a random matrix theory (RMT) for the staggered lattice QCD Dirac operator. The staggered RMT is equivalent to the zero-momentum limit of the staggered chiral Lagrangian and includes all taste breaking terms at their leading order. This is an extension of previous work which only included some of the taste breaking terms. We will also present some results for the taste breaking contributions to the partition function and the Dirac eigenvalues.

  10. Model Reduction via Reducibility Matrix

    Institute of Scientific and Technical Information of China (English)

    Musa Abdalla; Othman Alsmadi

    2006-01-01

    In this work, a new model reduction technique is introduced. The proposed technique is derived using the matrix reducibility concept. The eigenvalues of the reduced model are preserved; that is, the reduced model eigenvalues are a subset of the full order model eigenvalues. This preservation of the eigenvalues makes the mathematical model closer to the physical model. Finally, the outcomes of this method are fully illustrated using simulations of two numeric examples.

  11. Myocardial structure and matrix metalloproteinases.

    Science.gov (United States)

    Aggeli, C; Pietri, P; Felekos, I; Rautopoulos, L; Toutouzas, K; Tsiamis, E; Stefanadis, C

    2012-01-01

    Metalloproteinases (MMPs) are enzymes which enhance proteolysis of extracellular matrix proteins. The pathophysiologic and prognostic role of MMPs has been demonstrated in numerous studies. The present review covers a wide a range of topics with regards to MMPs structural and functional properties, as well as their role in myocardial remodeling in several cardiovascular diseases. Moreover, the clinical and therapeutic implications from their assessment are highlighted.

  12. Coherence matrix of plasmonic beams

    DEFF Research Database (Denmark)

    Novitsky, Andrey; Lavrinenko, Andrei

    2013-01-01

    We consider monochromatic electromagnetic beams of surface plasmon-polaritons created at interfaces between dielectric media and metals. We theoretically study non-coherent superpositions of elementary surface waves and discuss their spectral degree of polarization, Stokes parameters, and the for...... of the spectral coherence matrix. We compare the polarization properties of the surface plasmonspolaritons as three-dimensional and two-dimensional fields concluding that the latter is superior....

  13. Random matrix improved subspace clustering

    KAUST Repository

    Couillet, Romain

    2017-03-06

    This article introduces a spectral method for statistical subspace clustering. The method is built upon standard kernel spectral clustering techniques, however carefully tuned by theoretical understanding arising from random matrix findings. We show in particular that our method provides high clustering performance while standard kernel choices provably fail. An application to user grouping based on vector channel observations in the context of massive MIMO wireless communication networks is provided.

  14. MALDI Matrix Research for Biopolymers

    Science.gov (United States)

    Fukuyama, Yuko

    2015-01-01

    Matrices are necessary materials for ionizing analytes in matrix-assisted laser desorption/ionization-mass spectrometry (MALDI-MS). The choice of a matrix appropriate for each analyte controls the analyses. Thus, in some cases, development or improvement of matrices can become a tool for solving problems. This paper reviews MALDI matrix research that the author has conducted in the recent decade. It describes glycopeptide, carbohydrate, or phosphopeptide analyses using 2,5-dihydroxybenzoic acid (2,5-DHB), 1,1,3,3-tetramethylguanidinium (TMG) salts of p-coumaric acid (CA) (G3CA), 3-aminoquinoline (3-AQ)/α-cyano-4-hydroxycinnamic acid (CHCA) (3-AQ/CHCA) or 3-AQ/CA and gengeral peptide, peptide containing disulfide bonds or hydrophobic peptide analyses using butylamine salt of CHCA (CHCAB), 1,5-diaminonaphthalene (1,5-DAN), octyl 2,5-dihydroxybenzoate (alkylated dihydroxybenzoate, ADHB), or 1-(2,4,6-trihydroxyphenyl)octan-1-one (alkylated trihydroxyacetophenone, ATHAP). PMID:26819908

  15. Topics in Matrix Sampling Algorithms

    CERN Document Server

    Boutsidis, Christos

    2011-01-01

    We study three fundamental problems of Linear Algebra, lying in the heart of various Machine Learning applications, namely: 1)"Low-rank Column-based Matrix Approximation". We are given a matrix A and a target rank k. The goal is to select a subset of columns of A and, by using only these columns, compute a rank k approximation to A that is as good as the rank k approximation that would have been obtained by using all the columns; 2) "Coreset Construction in Least-Squares Regression". We are given a matrix A and a vector b. Consider the (over-constrained) least-squares problem of minimizing ||Ax-b||, over all vectors x in D. The domain D represents the constraints on the solution and can be arbitrary. The goal is to select a subset of the rows of A and b and, by using only these rows, find a solution vector that is as good as the solution vector that would have been obtained by using all the rows; 3) "Feature Selection in K-means Clustering". We are given a set of points described with respect to a large numbe...

  16. Integrable matrix theory: Level statistics.

    Science.gov (United States)

    Scaramazza, Jasen A; Shastry, B Sriram; Yuzbashyan, Emil A

    2016-09-01

    We study level statistics in ensembles of integrable N×N matrices linear in a real parameter x. The matrix H(x) is considered integrable if it has a prescribed number n>1 of linearly independent commuting partners H^{i}(x) (integrals of motion) [H(x),H^{i}(x)]=0, [H^{i}(x),H^{j}(x)]=0, for all x. In a recent work [Phys. Rev. E 93, 052114 (2016)2470-004510.1103/PhysRevE.93.052114], we developed a basis-independent construction of H(x) for any n from which we derived the probability density function, thereby determining how to choose a typical integrable matrix from the ensemble. Here, we find that typical integrable matrices have Poisson statistics in the N→∞ limit provided n scales at least as logN; otherwise, they exhibit level repulsion. Exceptions to the Poisson case occur at isolated coupling values x=x_{0} or when correlations are introduced between typically independent matrix parameters. However, level statistics cross over to Poisson at O(N^{-0.5}) deviations from these exceptions, indicating that non-Poissonian statistics characterize only subsets of measure zero in the parameter space. Furthermore, we present strong numerical evidence that ensembles of integrable matrices are stationary and ergodic with respect to nearest-neighbor level statistics.

  17. Integrable matrix theory: Level statistics

    Science.gov (United States)

    Scaramazza, Jasen A.; Shastry, B. Sriram; Yuzbashyan, Emil A.

    2016-09-01

    We study level statistics in ensembles of integrable N ×N matrices linear in a real parameter x . The matrix H (x ) is considered integrable if it has a prescribed number n >1 of linearly independent commuting partners Hi(x ) (integrals of motion) "]Hi(x ) ,Hj(x ) ]">H (x ) ,Hi(x ) =0 , for all x . In a recent work [Phys. Rev. E 93, 052114 (2016), 10.1103/PhysRevE.93.052114], we developed a basis-independent construction of H (x ) for any n from which we derived the probability density function, thereby determining how to choose a typical integrable matrix from the ensemble. Here, we find that typical integrable matrices have Poisson statistics in the N →∞ limit provided n scales at least as logN ; otherwise, they exhibit level repulsion. Exceptions to the Poisson case occur at isolated coupling values x =x0 or when correlations are introduced between typically independent matrix parameters. However, level statistics cross over to Poisson at O (N-0.5) deviations from these exceptions, indicating that non-Poissonian statistics characterize only subsets of measure zero in the parameter space. Furthermore, we present strong numerical evidence that ensembles of integrable matrices are stationary and ergodic with respect to nearest-neighbor level statistics.

  18. Screening Test of Greenhouse Seeding Exercise Matrix for Tissue Culture Seeding of Dendrobium Officinale Kimura et Migo

    Directory of Open Access Journals (Sweden)

    Zhou Yuan

    2015-01-01

    Full Text Available The Dendrobium officinale Kimura et Migo has a high demand on planting matrix, while its tissue culture seeding has much more demands on planting matrix. To find out a seeding exercise matrix to enhance the survival rate of tissue culture seeding of Dendrobium officinale Kimura et Migo more efficiently, this article carries out a screening test of greenhouse seeding exercise matrix material for tissue culture seeding of Dendrobium officinale Kimura et Migo. The test adopts full random test design, mainly for screening test of five matrix materials, namely pine bark, camphor tree bark, fern root, peanut shell and longan bark. Compare the impact of prepared seeding exercise matrix on the survival rate and growth trend (including plant height, growth rate and bud growth rate. The test result shows that: The seeding exercise matrix prepared by fern root is the most efficient, and the survival rate, plant height, growth rate and bud growth rate have achieved 100%, 4.5cm, 43.67% and 54.33% respectively. The main reason may be that the seeding exercise matrix C prepared by fern root is fairly loose and has a great water permeability, which is conducive to the growth of Dendrobium officinale Kimura et Migo.

  19. Matrix Superpotential Linear in Variable Parameter

    CERN Document Server

    Karadzhov, Yuri

    2011-01-01

    The paper presents the classification of matrix valued superpotentials corresponding to shape invariant systems of Schr\\"odinger equations. All inequivalent irreducible matrix superpotentials realized by matrices of arbitrary dimension with linear dependence on variable parameter are presented explicitly.

  20. Cubic Matrix, Nambu Mechanics and Beyond

    OpenAIRE

    Kawamura, Y

    2002-01-01

    We propose a generalization of cubic matrix mechanics by introducing a canonical triplet and study its relation to Nambu mechanics. The generalized cubic matrix mechanics we consider can be interpreted as a “quantum” generalization of Nambu mechanics.

  1. "On some definitions in matrix algebra"

    OpenAIRE

    Magnus, Jan R.; Karim M. Abadir

    2007-01-01

    Many definitions in matrix algebra are not standardized. This notediscusses some of thepitfalls associated with undesirable orwrong definitions, anddealswith central conceptslikesymmetry, orthogonality, square root, Hermitian and quadratic forms, and matrix derivatives.

  2. L’Hospital rule for matrix functions

    Directory of Open Access Journals (Sweden)

    Z.M. Kishka

    2013-07-01

    Full Text Available In this paper, the L’Hospital rule for evaluating limits of complex matrix functions is introduced. We present some specific examples on certain matrix functions showing the applicability of our approach.

  3. Synthesis and characterization of optically transparent epoxy matrix nanocomposites

    Energy Technology Data Exchange (ETDEWEB)

    Esposito Corcione, C., E-mail: carola.corcione@unile.it [Dipartimento di Ingegneria dell' Innovazione Via Monteroni 73100, Lecce (Italy); Manera, M.G. [IMM-CNR Istituto per la microelettronica e microsistemi - sezione di Lecce, c/o campus universitario, via per Monteroni, 73100 Lecce (Italy); Maffezzoli, A. [Dipartimento di Ingegneria dell' Innovazione Via Monteroni 73100, Lecce (Italy); Rella, R. [IMM-CNR Istituto per la microelettronica e microsistemi - sezione di Lecce, c/o campus universitario, via per Monteroni, 73100 Lecce (Italy)

    2009-08-01

    In this work optically transparent nanocomposites were prepared and characterized from an optical and morphological point of view. An organically modified boehmite was added at different concentrations in a diglycidyl ether of bisphenol A (DGEBA) epoxy matrix, hardened with a polyether diamine. Nanocomposites were characterized structurally by X-ray diffraction (XRD), optically by UV-Vis-NIR spectrophotometry and their morphology was investigated by Atomic Force Microscopy (AFM). Morphological investigation reveals the presence of boehmite particles dispersed in the epoxy matrix in different dimensions ranging from ten to hundreds of nanometers; some aggregation in the particles is the tendency noticed in the AFM images. The acquisition of multiple AFM images in different areas of the sample was used for a statistical analysis of the volumetric distribution of boehmite aggregates. The obtained result, (3.6 {+-} 0.3)%vol, is well comparable to thermogravimetric analysis.

  4. Matrix theory from generalized inverses to Jordan form

    CERN Document Server

    Piziak, Robert

    2007-01-01

    Each chapter ends with a list of references for further reading. Undoubtedly, these will be useful for anyone who wishes to pursue the topics deeper. … the book has many MATLAB examples and problems presented at appropriate places. … the book will become a widely used classroom text for a second course on linear algebra. It can be used profitably by graduate and advanced level undergraduate students. It can also serve as an intermediate course for more advanced texts in matrix theory. This is a lucidly written book by two authors who have made many contributions to linear and multilinear algebra.-K.C. Sivakumar, IMAGE, No. 47, Fall 2011Always mathematically constructive, this book helps readers delve into elementary linear algebra ideas at a deeper level and prepare for further study in matrix theory and abstract algebra.-L'enseignement Mathématique, January-June 2007, Vol. 53, No. 1-2.

  5. Synthesis and Preparation of Polysulfone Hollow Fiber Chelating Membrane Modified with Thiourea

    Institute of Scientific and Technical Information of China (English)

    WANG Bing; HUANG Lei; XIAO Feng

    2006-01-01

    Several kinds of chloromethyl polysulfones (CMPF) with different chlorinity and reactive groups were synthesized by Friedel-crafts reaction, which could be utilized as reactively matrix membrane materials. The CMPF hollow matrix membranes were prepared with phase inversion by utilization of CMPF/additive/DMAC casting solution and CMPF as membrane materials. It was found that the effects of additive content, bore liquid and dry spinning distance on the structure of CMPF hollow fiber matrix membrane were different. A high qualified polysulfone hollow fiber chelating membrane modified with thiourea as chelating groups was prepared using CMPF as membrane matrix materials,through the reaction between thiourea and CMPF hollow fiber matrix membrane to afford the methyl iso-thiourium polysulfone. The experimental results showed that thermal drawing could increase the mechanical properties of matrix membrane, and the thermal treatment could increase the homogeneity and stability of the structure of polysulfone hollow fiber chelating membrane modified with thiourea.

  6. Alternative sample preparation methods for MALDI-MS

    Energy Technology Data Exchange (ETDEWEB)

    Hurst, G.B.; Buchanan, M.V. [Oak Ridge National Lab., TN (United States); Czartoski, T.J. [Kenyon College, Gambier, OH (United States)

    1994-12-31

    Since the introduction of matrix-assisted laser desorption and ionization (MALDI), sample preparation has been a limiting step in the applicability of this important technique for mass spectrometric analysis of biomolecules. A number of variations on the original sample preparation method for have been described. The {open_quotes}standard{close_quotes} method of MALDI sample preparation requires mixing a solution containing the analyte and a large excess of matrix, and allowing a small volume of this solution to dry on a probe tip before insertion into the mass spectrometer. The resulting sample can fairly inhomogeneous. As a result, the process of aiming the desorption laser at a favorable spot on the dried sample can be tedious and time-consuming. The authors are evaluating several approaches to MALDI sample preparation, with the goal of developing a faster and more reproducible method.

  7. SINE TRANSFORM MATRIX FOR SOLVING TOEPLITZ MATRIX PROBLEMS

    Institute of Scientific and Technical Information of China (English)

    Li-zhi Cheng

    2001-01-01

    In recent papers, some authors studied the solutions of symmetricpositive definite(SPD) Toeplitz systems Tn x = b by the conjugate gradient method(CG) with different sine trans- forms based preconditioners. In this paper, we first discuss the properties of eigenvalues for the main known circulant, skew circulant and sine transform based preconditioners. A counter example shows that E.Boman's preconditioner is only positive semi-definite for the banded Toeplitz matrix. To use preconditioner effectively, then we propose a modified Boman's preconditioner and a new Cesaro sum type sine transform based preconditioner. Finally, the results of numerical experimentation with these two preconditioners are pre- sented.

  8. Random Matrix theory approach to Quantum mechanics

    OpenAIRE

    Chaitanya, K. V. S. Shiv

    2015-01-01

    In this paper, we give random matrix theory approach to the quantum mechanics using the quantum Hamilton-Jacobi formalism. We show that the bound state problems in quantum mechanics are analogous to solving Gaussian unitary ensemble of random matrix theory. This study helps in identify the potential appear in the joint probability distribution function in the random matrix theory as a super potential. This approach allows to extend the random matrix theory to the newly discovered exceptional ...

  9. Analytic matrix elements with shifted correlated Gaussians

    DEFF Research Database (Denmark)

    Fedorov, D. V.

    2017-01-01

    Matrix elements between shifted correlated Gaussians of various potentials with several form-factors are calculated analytically. Analytic matrix elements are of importance for the correlated Gaussian method in quantum few-body physics.......Matrix elements between shifted correlated Gaussians of various potentials with several form-factors are calculated analytically. Analytic matrix elements are of importance for the correlated Gaussian method in quantum few-body physics....

  10. Orthogonal Matrix-Valued Wavelet Packets

    Institute of Scientific and Technical Information of China (English)

    Qingjiang Chen; Cuiling Wang; Zhengxing Cheng

    2007-01-01

    In this paper,we introduce matrix-valued multiresolution analysis and matrixvalued wavelet packets. A procedure for the construction of the orthogonal matrix-valued wavelet packets is presented. The properties of the matrix-valued wavelet packets are investigated. In particular,a new orthonormal basis of L2(R,Cs×s) is obtained from the matrix-valued wavelet packets.

  11. Continued Fraction Algorithm for Matrix Exponentials

    Institute of Scientific and Technical Information of China (English)

    2001-01-01

    A recursive rational algorithm for matrix exponentials was obtained by making use of the generalized inverse of a matrix in this paper. On the basis of the n-th convergence of Thiele-type continued fraction expansion, a new type of the generalized inverse matrix-valued Padé approximant (GMPA) for matrix exponentials was defined and its remainder formula was proved. The results of this paper were illustrated by some examples.

  12. Neutrophil activator of matrix metalloproteinase-2 (NAM).

    Science.gov (United States)

    Rollo, Ellen E; Hymowitz, Michelle; Schmidt, Cathleen E; Montana, Steve; Foda, Hussein; Zucker, Stanley

    2006-01-01

    We have isolated a novel soluble factor(s), neutrophil activator of matrix metalloproteinases (NAM), secreted by unstimulated normal human peripheral blood neutrophils that causes the activation of cell secreted promatrix metalloproteinase-2 (proMMP-2). Partially purified preparations of NAM have been isolated from the conditioned media of neutrophils employing gelatin-Sepharose chromatography and differential membrane filter centrifugation. NAM activity, as assessed by exposing primary human umbilical vein endothelial cells (HUVEC) or HT1080 cells to NAM followed by gelatin zymography, was seen within one hour. Tissue inhibitor of metalloproteinase-2 (TIMP-2) and hydroxamic acid derived inhibitors of MMPs (CT1746 and BB94) abrogated the activation of proMMP-2 by NAM, while inhibitors of serine and cysteine proteases showed no effect. NAM also produced an increase in TIMP-2 binding to HUVEC and HT1080 cell surfaces that was inhibited by TIMP-2, CT1746, and BB94. Time-dependent increases in MT1-MMP protein and mRNA were seen following the addition of NAM to cells. These data support a role for NAM in cancer dissemination.

  13. Positivity of Matrices with Generalized Matrix Functions

    Institute of Scientific and Technical Information of China (English)

    Fuzhen ZHANG

    2012-01-01

    Using an elementary fact on matrices we show by a unified approach the positivity of a partitioned positive semidefinite matrix with each square block replaced by a compound matrix,an elementary symmetric function or a generalized matrix function.In addition,we present a refined version of the Thompson determinant compression theorem.

  14. Matrix algebra for higher order moments

    NARCIS (Netherlands)

    Meijer, Erik

    2005-01-01

    A large part of statistics is devoted to the estimation of models from the sample covariance matrix. The development of the statistical theory and estimators has been greatly facilitated by the introduction of special matrices, such as the commutation matrix and the duplication matrix, and the corre

  15. Matrix Sampling of Test Items. ERIC Digest.

    Science.gov (United States)

    Childs, Ruth A.; Jaciw, Andrew P.

    This Digest describes matrix sampling of test items as an approach to achieving broad coverage while minimizing testing time per student. Matrix sampling involves developing a complete set of items judged to cover the curriculum, then dividing the items into subsets and administering one subset to each student. Matrix sampling, by limiting the…

  16. An inversion algorithm for general tridiagonal matrix

    Institute of Scientific and Technical Information of China (English)

    Rui-sheng RAN; Ting-zhu HUANG; Xing-ping LIU; Tong-xiang GU

    2009-01-01

    An algorithm for the inverse of a general tridiagonal matrix is presented. For a tridiagonal matrix having the Doolittle factorization, an inversion algorithm is established.The algorithm is then generalized to deal with a general tridiagonal matrix without any restriction. Comparison with other methods is provided, indicating low computational complexity of the proposed algorithm, and its applicability to general tridiagonal matrices.

  17. Confocal Microscopy Imaging of the Biofilm Matrix

    DEFF Research Database (Denmark)

    Schlafer, Sebastian; Meyer, Rikke Louise

    2016-01-01

    The extracellular matrix is an integral part of microbial biofilms and an important field of research. Confocal laser scanning microscopy is a valuable tool for the study of biofilms, and in particular of the biofilm matrix, as it allows real-time visualization of fully hydrated, living specimens...... the concentration of solutes and the diffusive properties of the biofilm matrix....

  18. Stabilization of modified polyamide matrix

    Energy Technology Data Exchange (ETDEWEB)

    Marchini, Leonardo G.; Parra, Duclerc F.; Lugao, Ademar B., E-mail: dfparra@ipen.b [Instituto de Pesquisas Energeticas e Nucleares (IPEN/CNEN-SP), Sao Paulo, SP (Brazil)

    2011-07-01

    Films of PA 6 (polyamide) doped with europium luminescent complexes have been develop and studied for applications in advanced technologies. Development of optical marker for process monitoring is the focus of the present study. Based in doped luminescent polyamide samples were prepared for polymer processing use. Films were prepared by dissolution of PA 6 in acid moiety with addition of europium complex. Stability evaluation was done in samples submitted to irradiation with 10 and 100 kGy of ionizing source. The luminescent polymer matrices were characterized using the techniques of infrared, thermogravimetry, differential scanning calorimetry and photoluminescent properties by electron emission spectroscopy. (author)

  19. Preparation and In Vitro, In Vivo Evaluation of Clarithromycin Microcapsules

    OpenAIRE

    Hu, LianDong; Liu, Wei; Li, Li; Zhao, Jiqiang; Yang, Xun

    2011-01-01

    PURPOSE: To develop and validate a method to prepare clarithromycin (CLM) microcapsules to mask the bitter taste and provide effective treatment, and evaluate the quality of microcapsules in detail, especially the in vitro and in vivo pharmacokinetics behavior. METHODS: CLM microcapsules were prepared using ethyl cellulose as matrix material by an emulsion solvent diffusion method. The physicochemical property, in vitro release study, sensory test and stability test were evaluated. Self-made ...

  20. Teaching Tip: When a Matrix and Its Inverse Are Stochastic

    Science.gov (United States)

    Ding, J.; Rhee, N. H.

    2013-01-01

    A stochastic matrix is a square matrix with nonnegative entries and row sums 1. The simplest example is a permutation matrix, whose rows permute the rows of an identity matrix. A permutation matrix and its inverse are both stochastic. We prove the converse, that is, if a matrix and its inverse are both stochastic, then it is a permutation matrix.

  1. In Vitro – In Vivo Evaluation of Sustained – Release Lithium Carbonate Matrix Tablets: Influence of Hydrophilic Matrix Materials

    Directory of Open Access Journals (Sweden)

    J Emami

    2004-04-01

    Full Text Available Background: Conventional Lithium carbonate (LC tablets produce rapid and relatively high peak blood levels resulting in adverse effects. These drawbacks can be overcome by designing a suitable sustained or controlled-release LC preparation. Methods: Sustained-release matrix tablets were therefore developed using different types and ratios of polymers including carbomer (CP, Na carboxymethylcellulose (Na CMC and hydroxypropylmethylcellulose (HPMC, to assess the release profiles and in vivo performance of the formulations. The tablets were prepared by either direct compression (DC or wet granulation (WG. In the DC method, 69% (450 mg LC, 5, 10 or 15% CP or Na CMC (of total tablet weight, lactose and /or Avicel (to maintain constant tablet weight were mixed and directly compressed. In the WG method, 450 mg LC and 10, 20, or 30% HPMC were granulated with Eudragit S100 solution, dried, and then compressed to formulate the tablets. In vitro and in vivo, newly formulated sustained-release LC tablets were compared with sustained-release commercial tablets (Eskalith and Priadel. In vivo studies were conducted in nine healthy subjects in a cross-over design, with a 3x3 Latin square sequence, and pharmacokinetic parameters were estimated using classical methods. Results: The matrix tablets containing 15% CP exhibited suitable release kinetics and uniform absorption characteristics comparable to that of Eskalith. In vivo, this formulation produced a smooth and extended absorption phase very much similar to that of Eskalith with the identical elimination half-life and extent of absorption. Conclusion: The matrix tablets containing 15% CP reduces the incidence of side effects often associated with high serum concentration of Lithium and blood level variations. Direct correlation between the dissolution profiles and the relative bioavailability of the formulations could be observed. Keywords: Lithium carbonate, Matrix tablets, Sustained-release, In vitro

  2. Preparing for Multiple Births

    Science.gov (United States)

    ... Video Games, and the Internet Preparing for Multiple Births KidsHealth > For Parents > Preparing for Multiple Births Print ... a combination of both. The Risks of Multiple Births The most common risk involved with multiple births ...

  3. Diffusive dynamics on paper matrix

    Science.gov (United States)

    Chaudhury, Kaustav; Kar, Shantimoy; Chakraborty, Suman

    2016-11-01

    Writing with ink on a paper and the rapid diagnostics of diseases using paper cartridge, despite their remarkable diversities from application perspective, both involve the motion of a liquid from a source on a porous hydrophilic substrate. Here we bring out a generalization in the pertinent dynamics by appealing to the concerned ensemble-averaged transport with reference to the underlying molecular picture. Our results reveal that notwithstanding the associated complexities and diversities, the resultant liquid transport characteristics on a paper matrix, in a wide variety of applications, resemble universal diffusive dynamics. Agreement with experimental results from diversified applications is generic and validates our unified theory.

  4. Integrable matrix theory: Level statistics

    OpenAIRE

    2016-01-01

    We study level statistics in ensembles of integrable $N\\times N$ matrices linear in a real parameter $x$. The matrix $H(x)$ is considered integrable if it has a prescribed number $n>1$ of linearly independent commuting partners $H^i(x)$ (integrals of motion) $\\left[H(x),H^i(x)\\right] = 0$, $\\left[H^i(x), H^j(x)\\right]$ = 0, for all $x$. In a recent work, we developed a basis-independent construction of $H(x)$ for any $n$ from which we derived the probability density function, thereby determin...

  5. Matrix Completion from Noisy Entries

    CERN Document Server

    Keshavan, Raghunandan H; Oh, Sewoong

    2009-01-01

    Given a matrix M of low-rank, we consider the problem of reconstructing it from noisy observations of a small, random subset of its entries. The problem arises in a variety of applications, from collaborative filtering (the `Netflix problem') to structure-from-motion and positioning. We study a low complexity algorithm introduced by Keshavan et al.(2009), based on a combination of spectral techniques and manifold optimization, that we call here OptSpace. We prove performance guarantees that are order-optimal in a number of circumstances.

  6. Random matrix theory within superstatistics.

    Science.gov (United States)

    Abul-Magd, A Y

    2005-12-01

    We propose a generalization of the random matrix theory following the basic prescription of the recently suggested concept of superstatistics. Spectral characteristics of systems with mixed regular-chaotic dynamics are expressed as weighted averages of the corresponding quantities in the standard theory assuming that the mean level spacing itself is a stochastic variable. We illustrate the method by calculating the level density, the nearest-neighbor-spacing distributions, and the two-level correlation functions for systems in transition from order to chaos. The calculated spacing distribution fits the resonance statistics of random binary networks obtained in a recent numerical experiment.

  7. Neonatal disorders of germinal matrix.

    Science.gov (United States)

    Raets, M M A; Dudink, J; Govaert, P

    2015-11-01

    The germinal matrix (GM) is a richly vascularized, transient layer near the ventricles. It produces neurons and glial cells, and is present in the foetal brain between 8 and 36 weeks of gestation. At 25 weeks, it reaches its maximum volume and subsequently withers. The GM is vulnerable to haemorrhage in preterm infants. This selective vulnerability is explained by limited astrocyte end-feet coverage of microvessels, reduced expression of fibronectin and immature tight junctions. Focal lesions in the neonatal period include haemorrhage, germinolysis and stroke. Such lesions in transient layers interrupt normal brain maturation and induce neurodevelopmental sequelae.

  8. Random Matrix Theory and Econophysics

    Science.gov (United States)

    Rosenow, Bernd

    2000-03-01

    Random Matrix Theory (RMT) [1] is used in many branches of physics as a ``zero information hypothesis''. It describes generic behavior of different classes of systems, while deviations from its universal predictions allow to identify system specific properties. We use methods of RMT to analyze the cross-correlation matrix C of stock price changes [2] of the largest 1000 US companies. In addition to its scientific interest, the study of correlations between the returns of different stocks is also of practical relevance in quantifying the risk of a given stock portfolio. We find [3,4] that the statistics of most of the eigenvalues of the spectrum of C agree with the predictions of RMT, while there are deviations for some of the largest eigenvalues. We interpret these deviations as a system specific property, e.g. containing genuine information about correlations in the stock market. We demonstrate that C shares universal properties with the Gaussian orthogonal ensemble of random matrices. Furthermore, we analyze the eigenvectors of C through their inverse participation ratio and find eigenvectors with large ratios at both edges of the eigenvalue spectrum - a situation reminiscent of localization theory results. This work was done in collaboration with V. Plerou, P. Gopikrishnan, T. Guhr, L.A.N. Amaral, and H.E Stanley and is related to recent work of Laloux et al.. 1. T. Guhr, A. Müller Groeling, and H.A. Weidenmüller, ``Random Matrix Theories in Quantum Physics: Common Concepts'', Phys. Rep. 299, 190 (1998). 2. See, e.g. R.N. Mantegna and H.E. Stanley, Econophysics: Correlations and Complexity in Finance (Cambridge University Press, Cambridge, England, 1999). 3. V. Plerou, P. Gopikrishnan, B. Rosenow, L.A.N. Amaral, and H.E. Stanley, ``Universal and Nonuniversal Properties of Cross Correlations in Financial Time Series'', Phys. Rev. Lett. 83, 1471 (1999). 4. V. Plerou, P. Gopikrishnan, T. Guhr, B. Rosenow, L.A.N. Amaral, and H.E. Stanley, ``Random Matrix Theory

  9. Linear algebra and matrix analysis for statistics

    CERN Document Server

    Banerjee, Sudipto

    2014-01-01

    Matrices, Vectors, and Their OperationsBasic definitions and notations Matrix addition and scalar-matrix multiplication Matrix multiplication Partitioned matricesThe ""trace"" of a square matrix Some special matricesSystems of Linear EquationsIntroduction Gaussian elimination Gauss-Jordan elimination Elementary matrices Homogeneous linear systems The inverse of a matrixMore on Linear EquationsThe LU decompositionCrout's Algorithm LU decomposition with row interchanges The LDU and Cholesky factorizations Inverse of partitioned matrices The LDU decomposition for partitioned matricesThe Sherman-W

  10. MatrixPlot: visualizing sequence constraints

    DEFF Research Database (Denmark)

    Gorodkin, Jan; Stærfeldt, Hans Henrik; Lund, Ole

    1999-01-01

    MatrixPlot: visualizing sequence constraints. Sub-title Abstract Summary : MatrixPlot is a program for making high-quality matrix plots, such as mutual information plots of sequence alignments and distance matrices of sequences with known three-dimensional coordinates. The user can add information...... about the sequences (e.g. a sequence logo profile) along the edges of the plot, as well as zoom in on any region in the plot. Availability : MatrixPlot can be obtained on request, and can also be accessed online at http://www. cbs.dtu.dk/services/MatrixPlot. Contact : gorodkin@cbs.dtu.dk...

  11. The q-Laguerre matrix polynomials.

    Science.gov (United States)

    Salem, Ahmed

    2016-01-01

    The Laguerre polynomials have been extended to Laguerre matrix polynomials by means of studying certain second-order matrix differential equation. In this paper, certain second-order matrix q-difference equation is investigated and solved. Its solution gives a generalized of the q-Laguerre polynomials in matrix variable. Four generating functions of this matrix polynomials are investigated. Two slightly different explicit forms are introduced. Three-term recurrence relation, Rodrigues-type formula and the q-orthogonality property are given.

  12. Singular Value Decomposition for Unitary Symmetric Matrix

    Institute of Scientific and Technical Information of China (English)

    ZOUHongxing; WANGDianjun; DAIQionghai; LIYanda

    2003-01-01

    A special architecture called unitary sym-metric matrix which embodies orthogonal, Givens, House-holder, permutation, and row (or column) symmetric ma-trices as its special cases, is proposed, and a precise corre-spondence of singular values and singular vectors between the unitary symmetric matrix and its mother matrix is de-rived. As an illustration of potential, it is shown that, for a class of unitary symmetric matrices, the singular value decomposition (SVD) using the mother matrix rather than the unitary symmetric matrix per se can save dramatically the CPU time and memory without loss of any numerical precision.

  13. MatrixPlot: visualizing sequence constraints

    DEFF Research Database (Denmark)

    Gorodkin, Jan; Stærfeldt, Hans Henrik; Lund, Ole

    1999-01-01

    MatrixPlot: visualizing sequence constraints. Sub-title Abstract Summary : MatrixPlot is a program for making high-quality matrix plots, such as mutual information plots of sequence alignments and distance matrices of sequences with known three-dimensional coordinates. The user can add information...... about the sequences (e.g. a sequence logo profile) along the edges of the plot, as well as zoom in on any region in the plot. Availability : MatrixPlot can be obtained on request, and can also be accessed online at http://www. cbs.dtu.dk/services/MatrixPlot. Contact : gorodkin@cbs.dtu.dk...

  14. Determination of palladium by graphite furnace atomic absorption spectroscopy without matrix matching.

    Science.gov (United States)

    Jia, X; Wang, T; Wu, J

    2001-05-30

    A graphite furnace atomic absorption spectroscopy method for the analysis of the palladium (Pd) content in bulk pharmaceutical drug substances and their intermediates prepared in aqueous solutions is extended to samples prepared in acetonitrile (ACN) and ACN-water mixtures as well to samples prepared in dimethyl sulfoxide (DMSO) and DMSO-water mixtures. The Pd content in samples solubilized in these solvents can be accurately determined with calibration established with standards prepared in aqueous solutions without matrix matching or using the method of standard additions. The validity of this method is demonstrated by spike recovery studies and by the agreement with results for the same samples prepared in these solvents, in concentrated nitric acid, and prepared by a microwave digestion system.

  15. Thesis Preparation Manual

    OpenAIRE

    1999-01-01

    "This Thesis Preparation Manual has been written to provide you with format and procedure guidance for preparing and processing your thesis at the Naval Postgraduate School. It covers both unclassified and classified theses. All theses and thesis technical reports must be prepared in accordance with these guidelines. Please note that this manual is not written in the thesis format." form the Foreword

  16. Sparse Matrix Inversion with Scaled Lasso

    CERN Document Server

    Sun, Tingni

    2012-01-01

    We propose a new method of learning a sparse nonnegative-definite target matrix. Our primary example of the target matrix is the inverse of a population covariance matrix or correlation matrix. The algorithm first estimates each column of the matrix by scaled Lasso, a joint estimation of regression coefficients and noise level, and then adjusts the matrix estimator to be symmetric. The procedure is efficient in the sense that the penalty level of the scaled Lasso for each column is completely determined by the data via convex minimization, without using cross-validation. We prove that this method guarantees the fastest proven rate of convergence in the spectrum norm under conditions of weaker form than those in the existing analyses of other $\\ell_1$ algorithms, and has faster guaranteed rate of convergence when the ratio of the $\\ell_1$ and spectrum norms of the target inverse matrix diverges to infinity. A simulation study also demonstrates the competitive performance of the proposed estimator.

  17. Interpolation of rational matrix functions

    CERN Document Server

    Ball, Joseph A; Rodman, Leiba

    1990-01-01

    This book aims to present the theory of interpolation for rational matrix functions as a recently matured independent mathematical subject with its own problems, methods and applications. The authors decided to start working on this book during the regional CBMS conference in Lincoln, Nebraska organized by F. Gilfeather and D. Larson. The principal lecturer, J. William Helton, presented ten lectures on operator and systems theory and the interplay between them. The conference was very stimulating and helped us to decide that the time was ripe for a book on interpolation for matrix valued functions (both rational and non-rational). When the work started and the first partial draft of the book was ready it became clear that the topic is vast and that the rational case by itself with its applications is already enough material for an interesting book. In the process of writing the book, methods for the rational case were developed and refined. As a result we are now able to present the rational case as an indepe...

  18. Solid-matrix luminescence analysis

    Energy Technology Data Exchange (ETDEWEB)

    Hurtubise, R.J.

    1993-01-15

    Several interactions with lumiphors adsorbed on filter paper were elucidated from experiments with moisture, modulus and heavy-atom salts. The data were interpreted using static and dynamic quenching models, heavy-atom theory, and a theory related to the modulus of paper. With cyclodextrin-salt matrices, it was shown that 10% [alpha]-cyclodextrin/NaCl was very effective for obtaining strong room-temperature fluorescence and moderate room-temperature phosphorescence from adsorbed stereoisomeric tetrols. Extensive photophysical information was obtained for the four tetrols on 10% [alpha]-cyclodextrin/NaCl. The photophysical information acquired was used to develop a method for characterizing two of the tetrols. Work with model compounds adsorbed on deuterated sodium acetate showed that C-H vibrations in the undeuterated sodium acetate were not responsible for the deactivation of the excited triplet state in the model phosphors investigated. A considerable amount of solution luminescence and solid-matrix luminescence data were compared. The most important finding was that in several cases the room-temperature solid-matrix luminescence quantum yields were greater than the solution low-temperature quantum yield values.

  19. Study the Effect of Different Reinforcements on the Damping Properties of the Polymer Matrix Composite

    Directory of Open Access Journals (Sweden)

    Mustafa Ziyara Shamukh

    2016-09-01

    Full Text Available In this research, damping properties for composite materials were evaluated using logarithmic decrement method to study the effect of reinforcements on the damping ratio of the epoxy matrix. Three stages of composites were prepared in this research. The first stage included preparing binary blends of epoxy (EP and different weight percentages of polysulfide rubber (PSR (0%, 2.5%, 5%, 7.5% and 10%. It was found that the weight percentage 5% of polysulfide was the best percentage, which gives the best mechanical properties for the blend matrix. The advantage of this blend matrix is that; it mediates between the brittle properties of epoxy and the flexible properties of a blend matrix with the highest percentage of PSR. The second stage included reinforcing the best blend matrix of epoxy-polysulfide (the blend matrix with the best percentage of polysulfide resulted from the previous stage, by different volume percentages of short fibers (Carbon& Glass separately and randomly. The volume percentages of fibers were (2.5%, 5%, 7.5%, and 10%. The third stage included reinforcing the blend composites with highest percentages of carbon and glass fiber, by different weight percentages of nano-particles (Red mud& Fly ash separately. The weight percentages of particles were (0.5%, 1%, 1.5%, and 2%. The experimental results showed that blending polysulfide rubber with epoxy increased the damping ratio. As for reinforcement materials, they decreased the damping ratio, where glass fiber composites have significantly higher damping ratio than other composites.

  20. Preparation and evaluation of controlled release tablets of carvedilol

    Directory of Open Access Journals (Sweden)

    Varahala Setti M

    2009-01-01

    Full Text Available The objective of the present investigation is to design and evaluate controlled release tablets of carvedilol, employing synthetic polymers like polyethylene oxides, of different molecular weights as release retarding materials and to select the optimized formulation based on the pharmacokinetics of carvedilol. Matrix tablets each containing 80 mg of carvedilol were formulated employing PEO N60 K, PEO 301, and PEO 303 as release-retarding polymers and β Cyclodextrin and HP β cyclodextrin as release modulators from the matrix. Carvedilol release from the formulated tablets was very slow. Hence the release was modulated with the use of cyclodextrins. The dissolution from the matrix tablets was spread over more than 24 hours and depended on the type of polymer, its concentration and the type of cyclodextrin used. All the matrix tablets prepared using polyethylene oxides showed very good controlled release over more than 24 hours. The matrix tablets prepared using HP β cyclodextrin showed a higher dissolution rate and gave a dissolution profile that was comparable to the theoretical sustained release needed for once-a-day administration of carvedilol. The drug release mechanism from the matrix tablets was found to be quasi Fickian mechanism.

  1. A new soft dielectric silicone elastomer matrix with high mechanical integrity and low losses

    DEFF Research Database (Denmark)

    Madsen, Frederikke Bahrt; Yu, Liyun; Daugaard, Anders Egede

    2015-01-01

    in Young's modulus, however, is often accompanied by the loss of mechanical stability and thereby the lifetime of the DE. A new soft elastomer matrix, with no loss of mechanical stability and high dielectric permittivity, was prepared through the use of alkyl chloride-functional siloxane copolymers...

  2. The effect of hydrophilic and hydrophobic polymers on release profiles of diclofenac sodium from matrix tablets

    Directory of Open Access Journals (Sweden)

    Md Imamul Islam

    2013-01-01

    Conclusion: The present study demonstrated that Diclofenac could be successfully prepared using an appropriate amount of Methocel K15 MCR® and CA in the form of matrix tablets with similar dissolution profile of patent product Voltaren SR® . The type of polymers used was found to induce a profound effect on release rate and mechanism.

  3. International perspectives on coal preparation

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    1997-12-31

    The report consists of the vugraphs from the presentations which covered the following topics: Summaries of the US Department of Energy`s coal preparation research programs; Preparation trends in Russia; South African coal preparation developments; Trends in hard coal preparation in Germany; Application of coal preparation technology to oil sands extraction; Developments in coal preparation in China; and Coal preparation in Australia.

  4. Matrix assisted ionization: new aromatic and nonaromatic matrix compounds producing multiply charged lipid, peptide, and protein ions in the positive and negative mode observed directly from surfaces.

    Science.gov (United States)

    Li, Jing; Inutan, Ellen D; Wang, Beixi; Lietz, Christopher B; Green, Daniel R; Manly, Cory D; Richards, Alicia L; Marshall, Darrell D; Lingenfelter, Steven; Ren, Yue; Trimpin, Sarah

    2012-10-01

    Matrix assisted inlet ionization (MAII) is a method in which a matrix:analyte mixture produces mass spectra nearly identical to electrospray ionization without the application of a voltage or the use of a laser as is required in laserspray ionization (LSI), a subset of MAII. In MAII, the sample is introduced by, for example, tapping particles of dried matrix:analyte into the inlet of the mass spectrometer and, therefore, permits the study of conditions pertinent to the formation of multiply charged ions without the need of absorption at a laser wavelength. Crucial for the production of highly charged ions are desolvation conditions to remove matrix molecules from charged matrix:analyte clusters. Important factors affecting desolvation include heat, vacuum, collisions with gases and surfaces, and even radio frequency fields. Other parameters affecting multiply charged ion production is sample preparation, including pH and solvent composition. Here, findings from over 100 compounds found to produce multiply charged analyte ions using MAII with the inlet tube set at 450 °C are presented. Of the compounds tested, many have -OH or -NH(2) functionality, but several have neither (e.g., anthracene), nor aromaticity or conjugation. Binary matrices are shown to be applicable for LSI and solvent-free sample preparation can be applied to solubility restricted compounds, and matrix compounds too volatile to allow drying from common solvents. Our findings suggest that the physical properties of the matrix such as its morphology after evaporation of the solvent, its propensity to evaporate/sublime, and its acidity are more important than its structure and functional groups.

  5. On the Matrix Formulation of Kaiser's Varimax Criterion.

    Science.gov (United States)

    Neudecker, H.

    1981-01-01

    A full-fledged matrix derivation of Sherin's matrix formulation of Kaiser's varimax criterion is provided. Matrix differential calculus is used in conjunction with the Hadamard (or Schur) matrix product. Two results on Hadamard products are presented. (Author/JKS)

  6. Physical and Hydrodynamic Properties of Spherical Cellulose—Titanium Dioxide Composite Matrix for Expanded Bed Adsorption

    Institute of Scientific and Technical Information of China (English)

    雷引林; 林东强; 姚善泾; 刘坐镇; 朱自强

    2003-01-01

    Expanded bed adsorption (EBA) has been widely used in industrial downstream bioprocessing,Solid matrix is the principal pillar supporting the successful application of EBA.A novel spherical ceelulose-titanium dioxide composite matrix was prepared through the method of water-in-oil suspension thermal regeneration.Its typical physical properties were wet density 1.18g.cm-3,,diameters in the range of 100-300μm ,porosity 85.5%,and water content 72.3%.Expansion characteristics and liquid mixing performance of the matrix in expanded bed were investigated using water and 10% (by mass )glycerol solution as mobile phases,The results indicate that the custom-assembled matrix has a stable flow hydrodynamics and exhibits the same degree of liquid-phase mixing or column efficiency as the commercially available Streamline adsorbent.

  7. Tropomyosin is localized in the nuclear matrix and chromosome scaffold of physarum polycephalum

    Institute of Scientific and Technical Information of China (English)

    ZENGXIANLU; XIAOGUANGWANG; 等

    1999-01-01

    The nuclei and chromosomes were isolated from plasmodia of Physarum polycephalum.The nuclear matrix and chromosome scaffold were obtained after the DNA and most of the proteins were extracted with DNase I and 2 M NaCl.SD-PAGE analyses revealed that the nuclear matrix and chromosome scaffold contained a 37 kD polypeptide which is equivalent to tropomyosin in molecular weight.Immunofluorescence observations upon slide preparations labeled with anti-tropomyosin antibody showed that the nuclear matrix and chromosome scaffold emanated bright fluorescence,suggesting the presence of the antigen in them.Immunodotting results confirmed the presence of tropomyosin in the nuclear matrix and chromosome scaffold.Immunoelectron microscopic observations further demonstrated that tropomyosin was dispersively distributed in the interphase nuclei and metaphase chromosomes.

  8. Quantitative sandwich ELISA for determination of traces of hazelnut (Corylus avellana) protein in complex food matrixes.

    Science.gov (United States)

    Holzhauser, T; Vieths, S

    1999-10-01

    A hazelnut-specific sandwich-type ELISA based on polyclonal antisera was developed for detection of hidden hazelnut protein residues in complex food matrixes. In the absence of a food matrix, extractable protein from different native and toasted hazelnuts was detected at rates of 94 +/- 13 and 96 +/- 7% applying standards prepared from native and toasted hazelnuts, respectively. From complex food matrixes, 0.001-10% of hazelnut was recovered between 67 and 132%, in average by 106 +/- 17%. Depending on the food matrix, hazelnut protein could be detected down to the ppb (ng/g) level. Intraassay precision was hazelnut >/= 0.001% and interassay precision was hazelnut >/= 0.01%. In 12 of 28 commercial food products without labeling or declaration of hazelnut components, between 2 and 421 ppm of hazelnut protein was detected, demonstrating a remarkable presence of potentially allergenic hazelnut protein "hidden" in commercial food products.

  9. Chitosan-g-polyaniline: a creatine amidinohydrolase immobilization matrix for creatine biosensor

    Directory of Open Access Journals (Sweden)

    2009-09-01

    Full Text Available A novel matrix composed of chitosan-graft-polyaniline (CHIT-g-PANI was electrochemically prepared to investigate the immobilization of creatine amidinohydrolase (CAH. CAH enzyme was covalently immobilized with the CHIT-g-PANI matrix using glutaraldehyde as a linker. The resulting CAH/CHIT-g-PANI biomatrix was characterized with Fourier transform infrared spectroscopy (FTIR, atomic force microscopy (AFM, contact angle measurement and cyclic voltammetry (CV taking CHIT-g-PANI as a reference. The influence of various parameters on CAH enzyme activity within the matrix was investigated including pH, temperature, and time. The Michaelis-Menten constant and apparent activities for the CAH enzyme were calculated to be 0.51 mM and 83.59 mg/cm2, respectively; indicating CHIT-g-PANI matrix has a high affinity to immobilize CAH enzyme.

  10. Characterization and formation mechanism of water-insoluble DNA-matrix induced by UV irradiation.

    Science.gov (United States)

    Yamada, M; Satoh, S; Nomizu, M; Ohkawa, K; Yamamoto, H; Nishi, N

    2001-01-01

    We have prepared water-insoluble and nuclease resistant DNA-matrixes by UV irradiation. The UV-irradiated DNA-matrix could effectively accumulate and condense harmful DNA-intercalating compounds, such as acridine orange (AO) and ethidium bromide (EB), from diluted aqueous solutions. The binding constant of AO and EB for UV-irradiated DNA were determined to be 1.0 (+/- 0.2) x 10(5) M-1 and 6.8 (+/- 0.3) x 10(4) M-1, respectively; values consisted with reported results for non-irradiated DNA. In addition, the agarose gel electrophoresis and AFM measurements indicate that DNA matrix forms an intermolecular cross-linking structure with the radical reaction. The UV-irradiated DNA-matrixes have potential uses as a biomaterial filter for the removal of harmful DNA intercalating compounds.

  11. Alteration of nuclear matrix-intermediate filament system and differential expression of nuclear matrix proteins during human hepatocarcinoma cell differentiation

    Institute of Scientific and Technical Information of China (English)

    Jian Tang; Jing-Wen Niu; Dong-Hui Xu; Zhi-Xing Li; Qi-Fu Li; Jin-An Chen

    2007-01-01

    AIM:To investigate the association between the configurational and compositional changes of nuclear matrix and the differentiation of carcinoma cells.METHODS: Cells cultured with or without 5 × 10-3mmol/L of hexamethylene bisacetamide (HMBA) on Nickel grids were treated by selective extraction and prepared for whole mount observation under electron microscopy. The samples were examined under transmission electron microscope. Nuclear matrix proteins were selectively extracted and subjected to subcellular proteomics study. The protein expression patterns were analyzed by PDQuest software. Spots of differentially expressed nuclear matrix proteins were excised and subjected to in situ digestion with trypsin.The peptides were analyzed by matrix-assisted laserdesorption/ionization time of flight mass spectrometry (MALDI-TOF-MS). Data were submitted for database searching using Mascot tool (www. Matrixscience.com).RESULTS: The nuclear matrix (NM) and intermediate filament (IF) in SMMC-7721 hepatocarcinoma cells were found relatively sparse and arranged irregularly.The nuclear lamina was non-uniform, and two kinds of filaments were not tightly connected. After induction for differentiation by HMBA, the NM-IF filaments were concentrated and distributed uniformly. The heterogeneous population of filaments, including highly branched utrathin filaments could also be seen in the regular meshwork. The connection between the two kinds of filaments and the relatively thin, condensed and sharply demarcated lamina composed of intermediatesized filaments was relatively fastened. Meanwhile, 21NM proteins changed remarkably during SMMC-7721cell differentiation. Four proteins, I.e. Mutant Pyst1,hypothetical protein, nucleophosmin1, and LBP were downregulated, whereas four other proteins, eIF6, p44subunit, β-tubulin, and SIN3B were upregulated with the last one, SR2/ASF found only in the differentiated SMMC-7721 cells.CONCLUSION: The induced differentiation of SMMC-7721cells by HMBA is

  12. Distributed-memory matrix computations

    DEFF Research Database (Denmark)

    Balle, Susanne Mølleskov

    1995-01-01

    in these algorithms is that many scientific applications rely heavily on the performance of the involved dense linear algebra building blocks. Even though we consider the distributed-memory as well as the shared-memory programming paradigm, the major part of the thesis is dedicated to distributed-memory architectures....... We emphasize distributed-memory massively parallel computers - such as the Connection Machines model CM-200 and model CM-5/CM-5E - available to us at UNI-C and at Thinking Machines Corporation. The CM-200 was at the time this project started one of the few existing massively parallel computers...... performance can we expect to achieve? Why? 2.Solving systems of linear equations using a Strassen-type matrix-inversion algorithm. A good way to solve systems of linear equations on massively parallel computers? 3.Aspects of computing the singular value decomposition on the Connec-tion Machine CM-5/CM-5E...

  13. The Biblical Matrix of Economics

    Directory of Open Access Journals (Sweden)

    Grigore PIROŞCĂ

    2012-05-01

    Full Text Available The rationale of this paper is a prime pattern of history of economic thought in the previous ages of classic ancient times of Greek and Roman civilizations using a methodological matrix able to capture the mainstream ideas from social, political and religious events within the pages of Bible. The economic perspective of these events follows the evolution of the seeds of economic thinking within the Fertile Crescent, focused on the Biblical patriarchic heroes’ actions, but also on the empires which their civilization interacted to. The paper aims to discover the path followed by the economic doctrines from the Bible in order to find a match with economic actuality of present days.

  14. Density matrix theory and applications

    CERN Document Server

    Blum, Karl

    2012-01-01

    Written in a clear pedagogic style, this book deals with the application of density matrix theory to atomic and molecular physics. The aim is to precisely characterize sates by a vector and to construct general formulas and proofs of general theorems. The basic concepts and quantum mechanical fundamentals (reduced density matrices, entanglement, quantum correlations) are discussed in a comprehensive way. The discussion leads up to applications like coherence and orientation effects in atoms and molecules, decoherence and relaxation processes. This third edition has been updated and extended throughout and contains a completely new chapter exploring nonseparability and entanglement in two-particle spin-1/2 systems. The text discusses recent studies in atomic and molecular reactions. A new chapter explores nonseparability and entanglement in two-particle spin-1/2 systems.

  15. Inter-grade and inter-batch variability of sodium alginate used in alginate-based matrix tablets.

    Science.gov (United States)

    Fu, Shao; Buckner, Ira S; Block, Lawrence H

    2014-10-01

    The purpose of this study is to characterize the inter-grade and inter-batch variability of sodium alginate used in the formulation of matrix tablets. Four different grades and three batches of one grade of sodium alginate were used to prepare matrix tablets. Swelling, erosion, and drug release tests of sodium alginate matrix tablets were conducted in a USP dissolution apparatus. Substantial differences in swelling and erosion behavior of sodium alginate matrix tablets were evident among different viscosity grades. Even different batches of the same grade exhibit substantial differences in the swelling and erosion behavior of their matrix tablets. The erosion behavior of sodium alginate matrix tablets can be partly explained by their rheological properties (both apparent viscosity and viscoelasticity) in solution. Sodium alginate with higher apparent viscosity and viscoelasticity in solution show slower erosion rate and higher swelling rate. Compacts prepared from grades or batches with higher viscosity and higher viscoelasticity show slower drug release. For grades or batches with similar apparent viscosities, apparent viscosities of sodium alginate solution at low concentration alone are not sufficient to predict the functionality of sodium alginate in matrix tablets. Viscoelastic properties of sodium alginate solutions at one high concentration corresponding to the polymer gel state, may be suitable indicia of the extended release behavior of sodium alginate matrix tablets.

  16. Progress in various crosslinking modification for acellular matrix

    Institute of Scientific and Technical Information of China (English)

    Yang Haitang; Tan Qiang; Zhao Heng

    2014-01-01

    Objective To review the current crosslinking strategies for acelluar matrix scaffold,laying the foundation for subsequent experiment.Data sources Data were mainly obtained from recent papers published in PubMed or indexed by Web of Science,with keyword like crosslinking.Results Various crosslinking strategies,including chemical,physical and biological methods,have been introduced to facilitate the performance of fresh acellular matrix.Chemical crosslinking reagents,involved in synthetic and naturally derived agents,need to be eliminated before implantation in case of their potential biotoxicity,although several crosslinking agents with less toxicity and specific characteristics have been developed.Physical crosslinking methods present to be safe,additive-free and relatively controllable for rapid surface functionalization with no consideration of remaining radioactivity.Biological crosslinking strategies have attracted great interest,and have been demonstrated to enhance collagen-based crosslinking since their preparations do not need toxic or potentially biologically contaminated substances and can be carried out under physiological conditions.Conclusions Kinds of crosslinking methods with its potential advantages have been developed to modify raw acelluar matrix,of which the performance are promising after being crosslinked by several crosslinking treatments.Further preclinical and clinical evaluations should be taken to vertify their safety and efficacy for the tissues and organs substitutes in tissue and regenerative medicine.

  17. Osteogenic Matrix Cell Sheets Facilitate Osteogenesis in Irradiated Rat Bone

    Directory of Open Access Journals (Sweden)

    Yoshinobu Uchihara

    2015-01-01

    Full Text Available Reconstruction of large bone defects after resection of malignant musculoskeletal tumors is a significant challenge in orthopedic surgery. Extracorporeal autogenous irradiated bone grafting is a treatment option for bone reconstruction. However, nonunion often occurs because the osteogenic capacity is lost by irradiation. In the present study, we established an autogenous irradiated bone graft model in the rat femur to assess whether osteogenic matrix cell sheets improve osteogenesis of the irradiated bone. Osteogenic matrix cell sheets were prepared from bone marrow-derived stromal cells and co-transplanted with irradiated bone. X-ray images at 4 weeks after transplantation showed bridging callus formation around the irradiated bone. Micro-computed tomography images at 12 weeks postoperatively showed abundant callus formation in the whole circumference of the irradiated bone. Histology showed bone union between the irradiated bone and host femur. Mechanical testing showed that the failure force at the irradiated bone site was significantly higher than in the control group. Our study indicates that osteogenic matrix cell sheet transplantation might be a powerful method to facilitate osteogenesis in irradiated bones, which may become a treatment option for reconstruction of bone defects after resection of malignant musculoskeletal tumors.

  18. Release behaviour of clozapine matrix pellets based on percolation theory.

    Science.gov (United States)

    Aguilar-de-Leyva, Angela; Sharkawi, Tahmer; Bataille, Bernard; Baylac, Gilles; Caraballo, Isidoro

    2011-02-14

    The release behaviour of clozapine matrix pellets was studied in order to investigate if it is possible to explain it applying the concepts of percolation theory, previously used in the understanding of the release process of inert and hydrophilic matrix tablets. Thirteen batches of pellets with different proportions of clozapine/microcrystalline cellulose (MCC)/hydroxypropylmethyl cellulose (HPMC) and different clozapine particle size fractions were prepared by extrusion-spheronisation and the release profiles were studied. It has been observed that the distance to the excipient (HPMC) percolation threshold is important to control the release rate. Furthermore, the drug percolation threshold has a big influence in these systems. Batches very close to the drug percolation threshold, show a clear effect of the drug particle size in the release rate. However, this effect is much less evident when there is a bigger distance to the drug percolation threshold, so the release behaviour of clozapine matrix pellets is possible to be explained based on the percolation theory.

  19. FORMULATION DEVELOPMENT OF ISOXSUPRINE HYDROCHLORIDE MODIFIED RELEASE MATRIX TABLETS

    Directory of Open Access Journals (Sweden)

    Ketan Patel

    2012-01-01

    Full Text Available The objective of the present investigation was to study the effect of critical formulation parameters affecting release of isoxsuprine hydrochloride from matrix tablets using combination of polyethylene oxide (PEO and dicalcium phosphate (DCP. The powder blend consisting of drug and excipients was analyzed for angle of repose, Carr’s index and Hausner’s ratio. The tablets were prepared by direct compression method. To assess the compressional behavior of the drug-excipient blend, the tablets were analyzed for friability and crushing strength. The in vitro drug release study was carried out in distilled water. The powder blend exhibited satisfactorily flow as measured by angle of repose, Carr’s index and Hausner’s ratio. The formulation ingredients showed satisfactory tableting properties (friability <1%, crushing strength ≥ 4 kgf. The drug release was modified on addition of PEO and DCP. Addition of 5 to 25% DCP in the formulation of matrix tablets caused apparent difference in the drug dissolution in distilled water. However, the difference was insignificant as analyzed by analysis of variance (ANOVA and similarity factor ( f2. The drug release from the tablets was best explained by Weibull model. Unified Weibull model was evolved to predict drug release from the formulated batches. The findings of this investigation can be extended to industry to cut down the cost of formulation and to by-pass the existing patents employing hydrophilic matrixing agents, at least for selective drugs.

  20. Incorporation of Nanohybrid Films of Silica into Recycled Polystyrene Matrix

    Directory of Open Access Journals (Sweden)

    Genoveva Hernández-Padrón

    2015-01-01

    Full Text Available An alternative for the reutilization of polystyrene waste containers consisting in creating a hybrid material made of SiO2 nanoparticles embedded in a matrix of recycled polystyrene (PSR has been developed. Recycled polystyrene functionalized (PSRF was used to influence the morphological and antifog properties by the sol-gel synthesis of nanohybrid silica. To this end, silica nanoparticles were produced from alkoxide precursors in the presence of recycled polystyrene. The functionalization of this polymeric matrix was with the purpose of uniting in situ carboxyl and silanol groups during the sol-gel process. In this way, opaque or transparent solid substrates can be obtained, with each of these endowed with optical conditions that depend on the amount of reactants employed to prepare each nanohybrid specimen. The nanohybrids were labelled as SiO2/PSR (HPSR and SiO2/PSRF (HPSRF and their properties were then compared to those of commercial polystyrene (PS. All the prepared samples were used for coating glass substrates. The hydrophobicity of the resultant coatings was determined through contact angle measurement. The nanohybrid materials were characterized by FT-IR and 1H-NMR techniques. Additionally, TGA and SEM were employed to determine their thermal and textural properties.

  1. Introduction to matrix analysis and applications

    CERN Document Server

    Hiai, Fumio

    2014-01-01

    Matrices can be studied in different ways. They are a linear algebraic structure and have a topological/analytical aspect (for example, the normed space of matrices) and they also carry an order structure that is induced by positive semidefinite matrices. The interplay of these closely related structures is an essential feature of matrix analysis. This book explains these aspects of matrix analysis from a functional analysis point of view. After an introduction to matrices and functional analysis, it covers more advanced topics such as matrix monotone functions, matrix means, majorization and entropies. Several applications to quantum information are also included. Introduction to Matrix Analysis and Applications is appropriate for an advanced graduate course on matrix analysis, particularly aimed at studying quantum information. It can also be used as a reference for researchers in quantum information, statistics, engineering and economics.

  2. Optimized Projection Matrix for Compressive Sensing

    Directory of Open Access Journals (Sweden)

    Jianping Xu

    2010-01-01

    Full Text Available Compressive sensing (CS is mainly concerned with low-coherence pairs, since the number of samples needed to recover the signal is proportional to the mutual coherence between projection matrix and sparsifying matrix. Until now, papers on CS always assume the projection matrix to be a random matrix. In this paper, aiming at minimizing the mutual coherence, a method is proposed to optimize the projection matrix. This method is based on equiangular tight frame (ETF design because an ETF has minimum coherence. It is impossible to solve the problem exactly because of the complexity. Therefore, an alternating minimization type method is used to find a feasible solution. The optimally designed projection matrix can further reduce the necessary number of samples for recovery or improve the recovery accuracy. The proposed method demonstrates better performance than conventional optimization methods, which brings benefits to both basis pursuit and orthogonal matching pursuit.

  3. Eigenvalues properties of terms correspondences matrix

    Science.gov (United States)

    Bondarchuk, Dmitry; Timofeeva, Galina

    2016-12-01

    Vector model representations of text documents are widely used in the intelligent search. In this approach a collection of documents is represented in the form of the term-document matrix, reflecting the frequency of terms. In the latent semantic analysis the dimension of the vector space is reduced by the singular value decomposition of the term-document matrix. Authors use a matrix of terms correspondences, reflecting the relationship between the terms, to allocate a semantic core and to obtain more simple presentation of the documents. With this approach, reducing the number of terms is based on the orthogonal decomposition of the matrix of terms correspondences. Properties of singular values of the term-document matrix and eigenvalues of the matrix of terms correspondences are studied in the case when documents differ substantially in length.

  4. Matrix multiplication on the Intel Touchstone Delta

    Energy Technology Data Exchange (ETDEWEB)

    Huss-Lederman, S.; Jacobson, E.M.; Tsao, A. [Supercomputing Research Center, Bowie, MD (United States); Zhang, G. [CONVEX Computer Corp., Richardson, TX (United States)

    1993-12-31

    Matrix multiplication is a key primitive in block matrix algorithms such as those found in LAPACK. We present results from our study of matrix multiplication algorithms on the Intel Touchstone Delta, a distributed memory message-passing architecture with a two-dimensional mesh topology. We obtain an implementation that uses communication primitives highly suited to the Delta and exploits the single node assembly-coded matrix multiplication. Our algorithm is completely general, able to deal with arbitrary mesh aspect ratios and matrix dimensions, and has achieved parallel efficiency of 86% with overall peak performance in excess of 8 Gflops on 256 nodes for an 8800 {times} 8800 matrix. We describe our algorithm design and implementation, and present performance results that demonstrate scalability and robust behavior over varying mesh topologies.

  5. Gum copal and gum damar: Novel matrix forming materials for sustained drug delivery

    Directory of Open Access Journals (Sweden)

    Morkhade D

    2006-01-01

    Full Text Available This study concerns the evaluation of natural gum copal and gum damar as novel sustained release matrix forming materials in tablet formulation. Along with the physicochemical properties, gum copal and gum damar were characterized for molecular weight, polydispersity index and glass transition temperature. Matrix tablets were prepared by wet granulation technique using isopropyl alcohol as a granulating agent. Diclofenac sodium was used as a model drug. Tablet weight (250 mg and diameter (9 mm was kept constant. Tablets were evaluated for pharmacotechnical properties, drug content uniformity and in vitro drug release kinetics. Effect of gum concentration (10, 20 and 30% w/w with respect to total tablet weight on in vitro drug release profile was examined. Both the gums produced matrix tablets with good strength and acceptable pharmacotechnical properties. Matrix tablets with 30% w/w gum copal and gum damar showed sustained drug delivery beyond 10 h. Drug release from gum copal matrix tablets followed zero order kinetics while gum damar (10 and 20% w/w was found suitable to formulate the insoluble plastic matrix that releases the drug by diffusion. It is concluded that both gums possess substantial matrix forming property that could be used for sustained drug delivery.

  6. Modelling of polypropylene fibre-matrix composites using finite element analysis

    Directory of Open Access Journals (Sweden)

    2009-01-01

    Full Text Available Polypropylene (PP fibre-matrix composites previously prepared and studied experimentally were modelled using finite element analysis (FEA in this work. FEA confirmed that fibre content and composition controlled stress distribution in all-PP composites. The stress concentration at the fibre-matrix interface became greater with less fibre content. Variations in fibre composition were more significant in higher stress regions of the composites. When fibre modulus increased, the stress concentration at the fibres decreased and the shear stress at the fibre-matrix interface became more intense. The ratio between matrix modulus and fibre modulus was important, as was the interfacial stress in reducing premature interfacial failure and increasing mechanical properties. The model demonstrated that with low fibre concentration, there were insufficient fibres to distribute the applied stress. Under these conditions the matrix yielded when the applied stress reached the matrix yield stress, resulting in increased fibre axial stress. When the fibre content was high, there was matrix depletion and stress transfer was inefficient. The predictions of the FEA model were consistent with experimental and published data.

  7. Riemann--Hilbert problems, matrix orthogonal polynomials and discrete matrix equations with singularity confinement

    CERN Document Server

    Cassatella-Contra, Giovanni A

    2011-01-01

    In this paper matrix orthogonal polynomials in the real line are described in terms of a Riemann--Hilbert problem. This approach provides an easy derivation of discrete equations for the corresponding matrix recursion coefficients. The discrete equation is explicitly derived in the matrix Freud case, associated with matrix quartic potentials. It is shown that, when the initial condition and the measure are simultaneously triangularizable, this matrix discrete equation possesses the singularity confinement property, independently if the solution under consideration is given by recursion coefficients to quartic Freud matrix orthogonal polynomials or not.

  8. Micromechanical Evaluation of Ceramic Matrix Composites

    Science.gov (United States)

    1991-02-01

    Materials Sciences Corporation AD-A236 756 M.hM. 9 1 0513 IEIN HIfINU IIl- DTIC JUN 06 1991 MICROMECHANICAL EVALUATION OF S 0 CERAMIC MATRIX COMPOSITES C...Classification) \\() Micromechanical Evaluation of Ceramic Matrix Composites ) 12. PERSONAL AUTHOR(S) C-F. Yen, Z. Hashin, C. Laird, B.W. Rosen, Z. Wang 13a. TYPE...and strengthen the ceramic composites. In this task, various possibilities of crack propagation in unidirectional ceramic matrix composites under

  9. String Interactions in c=1 Matrix Model

    CERN Document Server

    De Boer, J; Verlinde, E; Yee, J T; Boer, Jan de; Sinkovics, Annamaria; Verlinde, Erik; Yee, Jung-Tay

    2004-01-01

    We study string interactions in the fermionic formulation of the c=1 matrix model. We give a precise nonperturbative description of the rolling tachyon state in the matrix model, and discuss S-matrix elements of the c=1 string. As a first step to study string interactions, we compute the interaction of two decaying D0-branes in terms of free fermions. This computation is compared with the string theory cylinder diagram using the rolling tachyon ZZ boundary states.

  10. Imposing causality on a matrix model

    Energy Technology Data Exchange (ETDEWEB)

    Benedetti, Dario [Perimeter Institute for Theoretical Physics, 31 Caroline St. N, N2L 2Y5, Waterloo ON (Canada)], E-mail: dbenedetti@perimeterinstitute.ca; Henson, Joe [Perimeter Institute for Theoretical Physics, 31 Caroline St. N, N2L 2Y5, Waterloo ON (Canada)

    2009-07-13

    We introduce a new matrix model that describes Causal Dynamical Triangulations (CDT) in two dimensions. In order to do so, we introduce a new, simpler definition of 2D CDT and show it to be equivalent to the old one. The model makes use of ideas from dually weighted matrix models, combined with multi-matrix models, and can be studied by the method of character expansion.

  11. Polyamide/nano mixed matrix membranes for pervaporation dehydration Ethylene glycols

    Directory of Open Access Journals (Sweden)

    Omid Sabzevari

    2015-06-01

    Full Text Available In this study, nano silica was successfully incorporated into the polyamide solution to prepare polyamide/nano silica mixed matrix membranes (MMMs. The prepared MMMs were characterized by scanning electron microscopy (SEM. The prepared MMMs were used to separate mixtures of Ethylene glycols/water at 25 C in the pervaporation (PV process. The different nano silica loadings in polyamide polymer, such as 0.5, 1 and 2 wt%, have been tried and nano silica with 0.5 wt% loading shows the best PV performance. As a result, the 0.5 wt% nano silica in polyamide membrane leads to increases in permeation, but, decrease in the separation factor. Separation factor decreases significantly at higher loadings of nano silica due to the agglomeration of nano-particles in the polyamide matrix.

  12. [Aesthetic surgery, psychic preparation].

    Science.gov (United States)

    Feiss, R

    2003-10-01

    The aesthetic surgery impacts the psychological picture of the body. The candidate must be prepared to this change in appearance. If not, the surgeon must suggest the psychological preparation, evaluating the risk of dissatisfaction, in order to allow the surgical and narcissistic success of his operation. The author, a psychiatric, beneficiary in a strong experience of a surgical assistance, develops the interest of such a preparation upon a period of about 15 years (1988-2002).

  13. Query Through Heterogeneous Ontologies Using Association Matrix

    Institute of Scientific and Technical Information of China (English)

    KANG Da-zhou; XU Bao-wen; LU Jian-jiang; WANG Peng; LI Yan-hui

    2004-01-01

    This paper introduces the definition and calculation of the association matrix between ontologies.It uses the association matrix to describe the relations between concepts in different ontologies and uses concept vectors to represent queries; then computes the vectors with the association matrix in order to rewrite queries.This paper proposes a simple method of querying through heterogeneous Ontology using association matrix.This method is based on the correctness of approximate information filtering theory; and it is simple to be implemented and expected to run quite fast.

  14. Multiscale Modeling of Ceramic Matrix Composites

    Science.gov (United States)

    Bednarcyk, Brett A.; Mital, Subodh K.; Pineda, Evan J.; Arnold, Steven M.

    2015-01-01

    Results of multiscale modeling simulations of the nonlinear response of SiC/SiC ceramic matrix composites are reported, wherein the microstructure of the ceramic matrix is captured. This micro scale architecture, which contains free Si material as well as the SiC ceramic, is responsible for residual stresses that play an important role in the subsequent thermo-mechanical behavior of the SiC/SiC composite. Using the novel Multiscale Generalized Method of Cells recursive micromechanics theory, the microstructure of the matrix, as well as the microstructure of the composite (fiber and matrix) can be captured.

  15. Risk matrix model for rotating equipment

    Directory of Open Access Journals (Sweden)

    Wassan Rano Khan

    2014-07-01

    Full Text Available Different industries have various residual risk levels for their rotating equipment. Accordingly the occurrence rate of the failures and associated failure consequences categories are different. Thus, a generalized risk matrix model is developed in this study which can fit various available risk matrix standards. This generalized risk matrix will be helpful to develop new risk matrix, to fit the required risk assessment scenario for rotating equipment. Power generation system was taken as case study. It was observed that eight subsystems were under risk. Only vibration monitor system was under high risk category, while remaining seven subsystems were under serious and medium risk categories.

  16. Basic matrix algebra and transistor circuits

    CERN Document Server

    Zelinger, G

    1963-01-01

    Basic Matrix Algebra and Transistor Circuits deals with mastering the techniques of matrix algebra for application in transistors. This book attempts to unify fundamental subjects, such as matrix algebra, four-terminal network theory, transistor equivalent circuits, and pertinent design matters. Part I of this book focuses on basic matrix algebra of four-terminal networks, with descriptions of the different systems of matrices. This part also discusses both simple and complex network configurations and their associated transmission. This discussion is followed by the alternative methods of de

  17. New recursive algorithm for matrix inversion

    Institute of Scientific and Technical Information of China (English)

    Cao Jianshu; Wang Xuegang

    2008-01-01

    To reduce the computational complexity of matrix inversion, which is the majority of processing in many practical applications, two numerically efficient recursive algorithms (called algorithms Ⅰ and Ⅱ, respectively)are presented. Algorithm Ⅰ is used to calculate the inverse of such a matrix, whose leading principal minors are all nonzero. Algorithm Ⅱ, whereby, the inverse of an arbitrary nonsingular matrix can be evaluated is derived via improving the algorithm Ⅰ. The implementation, for algorithm Ⅱ or Ⅰ, involves matrix-vector multiplications and vector outer products. These operations are computationally fast and highly parallelizable. MATLAB simulations show that both recursive algorithms are valid.

  18. A random matrix theory of decoherence

    Science.gov (United States)

    Gorin, T.; Pineda, C.; Kohler, H.; Seligman, T. H.

    2008-11-01

    Random matrix theory is used to represent generic loss of coherence of a fixed central system coupled to a quantum-chaotic environment, represented by a random matrix ensemble, via random interactions. We study the average density matrix arising from the ensemble induced, in contrast to previous studies where the average values of purity, concurrence and entropy were considered; we further discuss when one or the other approach is relevant. The two approaches agree in the limit of large environments. Analytic results for the average density matrix and its purity are presented in linear response approximation. The two-qubit system is analysed, mainly numerically, in more detail.

  19. Partitioned R-matrix theory for molecules

    Energy Technology Data Exchange (ETDEWEB)

    Tennyson, Jonathan [Department of Physics and Astronomy, University College London, Gower St., London WC1E 6BT (United Kingdom)

    2004-03-14

    R-matrix calculations usually require all the eigenvalues and eigenvectors of the inner region Hamiltonian matrix. For molecular problems, particularly when large configuration interaction expansions are used for the target, the Hamiltonian matrix is often too large to be completely diagonalized. Berrington and Ballance (2002 J. Phys. B: At. Mol. Opt. Phys. 35 2275) proposed a partitioned R-matrix theory which only required a proportion of the solutions of the Hamiltonian matrix. This theory was implemented and tested in the atomic R-matrix code. The theory is adapted to the needs of R-matrix calculations on low-energy electron-molecule collisions. A number of alternative procedures are tested. The best is shown to give reliable results with explicit inclusion of only a fraction of the solutions. It is shown that with this revised theory the number of solutions required does not depend on the complexity of the target wavefunction even though this strongly influences the size of the final Hamiltonian matrix. This method will be implemented as part of the UK molecular R-matrix program suite.

  20. A random matrix theory of decoherence

    Energy Technology Data Exchange (ETDEWEB)

    Gorin, T [Departamento de FIsica, Universidad de Guadalajara, Blvd Marcelino GarcIa Barragan y Calzada OlImpica, Guadalajara CP 44840, JalIsco (Mexico); Pineda, C [Institut fuer Physik und Astronomie, University of Potsdam, 14476 Potsdam (Germany); Kohler, H [Fachbereich Physik, Universitaet Duisburg-Essen, D-47057 Duisburg (Germany); Seligman, T H [Instituto de Ciencias FIsicas, Universidad Nacional Autonoma de Mexico (Mexico)], E-mail: thomas.gorin@red.cucei.udg.mx, E-mail: carlospgmat03@gmail.com

    2008-11-15

    Random matrix theory is used to represent generic loss of coherence of a fixed central system coupled to a quantum-chaotic environment, represented by a random matrix ensemble, via random interactions. We study the average density matrix arising from the ensemble induced, in contrast to previous studies where the average values of purity, concurrence and entropy were considered; we further discuss when one or the other approach is relevant. The two approaches agree in the limit of large environments. Analytic results for the average density matrix and its purity are presented in linear response approximation. The two-qubit system is analysed, mainly numerically, in more detail.

  1. Developed Matrix inequalities via Positive Multilinear Mappings

    OpenAIRE

    Dehghani, Mahdi; Kian, Mohsen; Seo, Yuki

    2015-01-01

    Utilizing the notion of positive multilinear mappings, we give some matrix inequalities. In particular, Choi--Davis--Jensen and Kantorovich type inequalities including positive multilinear mappings are presented.

  2. Matrix Krylov subspace methods for image restoration

    Directory of Open Access Journals (Sweden)

    khalide jbilou

    2015-09-01

    Full Text Available In the present paper, we consider some matrix Krylov subspace methods for solving ill-posed linear matrix equations and in those problems coming from the restoration of blurred and noisy images. Applying the well known Tikhonov regularization procedure leads to a Sylvester matrix equation depending the Tikhonov regularized parameter. We apply the matrix versions of the well known Krylov subspace methods, namely the Least Squared (LSQR and the conjugate gradient (CG methods to get approximate solutions representing the restored images. Some numerical tests are presented to show the effectiveness of the proposed methods.

  3. A Generalization of the Alias Matrix

    DEFF Research Database (Denmark)

    Kulahci, Murat; Bisgaard, S.

    2006-01-01

    The investigation of aliases or biases is important for the interpretation of the results from factorial experiments. For two-level fractional factorials this can be facilitated through their group structure. For more general arrays the alias matrix can be used. This tool is traditionally based...... on the assumption that the error structure is that associated with ordinary least squares. For situations where that is not the case, we provide in this article a generalization of the alias matrix applicable under the generalized least squares assumptions. We also show that for the special case of split plot error...... structure, the generalized alias matrix simplifies to the ordinary alias matrix....

  4. Faster Algorithms for Rectangular Matrix Multiplication

    CERN Document Server

    Gall, François Le

    2012-01-01

    Let {\\alpha} be the maximal value such that the product of an n x n^{\\alpha} matrix by an n^{\\alpha} x n matrix can be computed with n^{2+o(1)} arithmetic operations. In this paper we show that \\alpha>0.30298, which improves the previous record \\alpha>0.29462 by Coppersmith (Journal of Complexity, 1997). More generally, we construct a new algorithm for multiplying an n x n^k matrix by an n^k x n matrix, for any value k\

  5. Titanium Matrix Composite Pressure Vessel Project

    Data.gov (United States)

    National Aeronautics and Space Administration — For over 15 years, FMW Composite Systems has developed Metal Matrix Composite manufacturing methodologies for fabricating silicon-carbide-fiber-reinforced titanium...

  6. Preparation of rodent testis co-cultures.

    Science.gov (United States)

    Wegner, Susanna; Hong, Sungwoo; Yu, Xiaozhong; Faustman, Elaine M

    2013-02-01

    Male reproductive development is a complex process that is sensitive to disruption by a range of toxicants. There is a great need for in vitro models that can evaluate potential male reproductive toxicants. The current unit presents a protocol for preparation of a three-dimensional in vitro model of male reproductive development that reduces the number of animals required for evaluation of toxicants. A Matrigel overlay provides a three-dimensional extracellular matrix that improves cell attachment, viability, and communication, and makes the model more reflective of in vivo environments. © 2013 by John Wiley & Sons, Inc.

  7. Preparation and Properties of Polyaniline Composite Films

    Institute of Scientific and Technical Information of China (English)

    ZHANG Qing-hua

    2002-01-01

    Polyaniline (PAn) was synthesized by chemical oxidation polymerization. The conductive polymer doped by camphor sulfonic acid (CSA) and a matrix polymer,polyamide- 66, polyamide - 1010 or polyamide- 11, were dissolved in m-cresol and the blend solution was cast in a glass and dried for preparing polyaniline composite films.Conductivity was from 10 -6 to 10 0Ω-1·cm-1 with different weight fraction of PAn-CSA. The crystallizttion of the films was studied by means of differential scanning calorimeter (DSC). The treatment of the composite films in different pH value solution would result in decrease of conductivity, especially in an alkaline solution.

  8. Preparation of Reference Material for Radioactive Soil in the First Mixture

    Institute of Scientific and Technical Information of China (English)

    XU; Li-jun; YE; Hong-sheng; DIAO; Li-jun; ZHANG; Wei-dong; XIA; Wen; LIN; Min; CHEN; Ke-sheng; CHEN; Yi-zhen; LI; Ming

    2015-01-01

    After the samples were prepared by mixing the soil and radioactive solution,the next step is mixing with the order of kg soil matrix.There are two alternative methods of preparing the step:First,use the scroll-type ball mill to achieve uniform mixing in the process of milling;

  9. Materials Preparation Center

    Data.gov (United States)

    Federal Laboratory Consortium — MPC is recognized throughout the worldwide research community for its unique capabilities in purification, preparation, and characterization of: rare earth metals,...

  10. Materials Preparation Center

    Data.gov (United States)

    Federal Laboratory Consortium — MPC is recognized throughout the worldwide research community for its unique capabilities in purification, preparation, and characterization of: rare earth metals,...

  11. Reduction of multipartite qubit density matrixes to bipartite qubit density matrixes and criteria of partial separability of multipartite qubit density matrixes

    OpenAIRE

    Zhong, Zai-Zhe

    2004-01-01

    The partial separability of multipartite qubit density matrixes is strictly defined. We give a reduction way from N-partite qubit density matrixes to bipartite qubit density matrixes, and prove a necessary condition that a N-partite qubit density matrix to be partially separable is its reduced density matrix to satisfy PPT condition.

  12. Reduction of multipartite qubit density matrixes to bipartite qubit density matrixes and criteria of partial separability of multipartite qubit density matrixes

    OpenAIRE

    Zhong, Zai-Zhe

    2004-01-01

    The partial separability of multipartite qubit density matrixes is strictly defined. We give a reduction way from N-partite qubit density matrixes to bipartite qubit density matrixes, and prove a necessary condition that a N-partite qubit density matrix to be partially separable is its reduced density matrix to satisfy PPT condition.

  13. 金属基掺杂水滑石自修复型溶胶-凝胶膜层制备及机理研究%Preparation of metal matrix-containing hydrotalcite sol-gel self-healing coating and its corrosion resistance

    Institute of Scientific and Technical Information of China (English)

    李龙芹; 王韶音; 李青

    2013-01-01

    设计并实现了一种自修复溶胶-凝胶膜层。利用膜层中添加的水滑石颗粒的阴离子交换作用实现了自修复功能,并对其修复机理进行设想和论证。长期浸泡测试结果表明,膜层中水滑石颗粒的最佳添加量为10%(质量分数)。通过 X 射线衍射和扫描电子显微镜观察验证设想。此种膜层的自修复功能是通过膜层中添加的水滑石颗粒的阴离子交换作用实现的。%In this work,hydrotalcite (HT)powder was prepared by the classical co-precipitation method using magnesium and aluminum nitrates as precursors.Different weight percentages (5%,10% and 15wt%)of hydrotalcite were added to sols.The sol-gel coatings were deposited by spin-coating method on AZ91D magnesi-um alloy substrate.Scanning electronmicroscopy (SEM)revealed the distribution of the agglomerates.The cor-rosion performance was evaluated by electrochemical impedance spectroscopy (EIS).The results showed a marked improvement of the corrosion resistance on the sol-gel/magnesium system when hydrotalcite was added to the sol-gel coating.And the healing effects may be due to the anion exchange capacity of hydrotalcite.

  14. The 5‘—flanking cis—acting elements of the human ε—globin gene associates with the nuclear matrix and binds to the nuclear matrix proteins

    Institute of Scientific and Technical Information of China (English)

    YANZHIJIANG; RUOLANQIAN

    1998-01-01

    The nuclear matrix attachment regions(MARs) and the binding nuclear matrix proteins in the 5'-flanking cisacting elements of the human ε-globin gene have been examined.Using in vitro DNA-matrix binding assay,it has been shown that the positive stage-specific regulatory element (ε-PREII,-446bp- -419bp) upstream of this gene could specifically associate with the nuclear matrix from K562 cells,indicating that ε-PREII may be an erythroidspecific facultative MAR.In gel mobility shift assay and Southwestern blotting assay,an erythroid-specific nuclear matrix protein (ε-NMPk) in K562 cells has been revealed to bind to this positive regulatory element (ε-PREII).Furthermore,we demonstrated that the silencer (-392bp- -177bp) upstream of the human ε-globin gene could associate with the nuclear matrices from K562,HEL and Raji cells.In addition,the nuclear matrix proteins prepared from these three cell lines could also bind to this silencer,suggesting that this silencer element might be a constitutive nuclear matrix attachment region(constitutive MAR).Our results demonstrated that the nuclear matrix and nuclear matrix proteins might play an important role in the regulation of the human ε-globin gene expression.

  15. TRASYS form factor matrix normalization

    Science.gov (United States)

    Tsuyuki, Glenn T.

    1992-01-01

    A method has been developed for adjusting a TRASYS enclosure form factor matrix to unity. This approach is not limited to closed geometries, and in fact, it is primarily intended for use with open geometries. The purpose of this approach is to prevent optimistic form factors to space. In this method, nodal form factor sums are calculated within 0.05 of unity using TRASYS, although deviations as large as 0.10 may be acceptable, and then, a process is employed to distribute the difference amongst the nodes. A specific example has been analyzed with this method, and a comparison was performed with a standard approach for calculating radiation conductors. In this comparison, hot and cold case temperatures were determined. Exterior nodes exhibited temperature differences as large as 7 C and 3 C for the hot and cold cases, respectively when compared with the standard approach, while interior nodes demonstrated temperature differences from 0 C to 5 C. These results indicate that temperature predictions can be artificially biased if the form factor computation error is lumped into the individual form factors to space.

  16. Direct Model Checking Matrix Algorithm

    Institute of Scientific and Technical Information of China (English)

    Zhi-Hong Tao; Hans Kleine Büning; Li-Fu Wang

    2006-01-01

    During the last decade, Model Checking has proven its efficacy and power in circuit design, network protocol analysis and bug hunting. Recent research on automatic verification has shown that no single model-checking technique has the edge over all others in all application areas. So, it is very difficult to determine which technique is the most suitable for a given model. It is thus sensible to apply different techniques to the same model. However, this is a very tedious and time-consuming task, for each algorithm uses its own description language. Applying Model Checking in software design and verification has been proved very difficult. Software architectures (SA) are engineering artifacts that provide high-level and abstract descriptions of complex software systems. In this paper a Direct Model Checking (DMC) method based on Kripke Structure and Matrix Algorithm is provided. Combined and integrated with domain specific software architecture description languages (ADLs), DMC can be used for computing consistency and other critical properties.

  17. Allylhydridopolycarbosilane (AHPCS) as matrix resin for C/SiC ceramic matrix composites

    Energy Technology Data Exchange (ETDEWEB)

    Sreeja, R. [Ceramic Matrix Products Division, Propellants and Special Chemicals Group, PCM Entity, Vikram Sarabhai Space Center, Thiruvananthapuram 695022 (India); Swaminathan, B., E-mail: swami1423@gmail.co [Ceramic Matrix Products Division, Propellants and Special Chemicals Group, PCM Entity, Vikram Sarabhai Space Center, Thiruvananthapuram 695022 (India); Painuly, Anil; Sebastian, T.V.; Packirisamy, S. [Ceramic Matrix Products Division, Propellants and Special Chemicals Group, PCM Entity, Vikram Sarabhai Space Center, Thiruvananthapuram 695022 (India)

    2010-04-15

    In present study, partially allyl-substituted hydridopolycarbosilane (5 mol% allyl) [AHPCS] has been characterized by spectral techniques and thermal analysis. The DSC studies show that, the polymer is self-cross-linking at lower temperatures without any incorporation of cross-linking agents. The spectral and thermal characterizations carried out at different processing stages indicate the possibility of extensive structural rearrangement accompanied by the loss of hydrogen and other reactions of C and Si containing species resulting in the conversion of the branched chain segment into a 3D SiC network structure. AHPCS gave ceramic residue of 72% and 70% at 900 and 1500 deg. C respectively in argon atmosphere. XRD pattern of 1500 deg. C heat-treated AHPCS, indicates the formation of silicon carbide with the particle size of 3-4 nm. AHPCS was used as matrix resin for the preparation of C/SiC composite without any interfacial coating over the T-300 carbon fabric reinforcement. Flexural strength value of 74-86 MPa for C/SiC specimen with density of 1.7 g/cm{sup 3} was obtained after four infiltration and pyrolysis cycles.

  18. Effect of polymers on in-vitro performance of eplerenone sustained release matrix tablets

    Directory of Open Access Journals (Sweden)

    Sunil Reddy

    2012-01-01

    Full Text Available Objectives: The intention of the present study was to design and assess oral sustained drug delivery systems for Eplerenone, using Cellulose and natural polymers as release modifiers in the form of matrix tablets. Material and methods: Matrix tablets containing cellulose polymers like HPMC K4M, HPMC K15M, NaCMC and natural polymers like Guar Gum, Xanthan Gum, and Karaya Gum were prepared by wet granulation technique using PVP K60 as a tablet binder. Results: The optimized formulation (F1 contains 1: 0.70 ratio (D: HPMC K4M and (F4 contains 1:1 ratio (D: Guar gum respectively. The in-vitro release kinetic studies of prepared matrix tablets with both the polymers were studied. The kinetic treatment illustrate that the optimized formulation (F1 and F4 followed zero order kinetics with release exponent (n 0.87. Drug content in the tablets and amount of drug released were estimated by reported HPLC method. The FT-IR and DSC studies did not show any interaction of drug with the excipients used in the formulation. Conclusion: The results clearly indicated that Eplerenone could be successfully prepared using an appropriate ratio of cellulose polymers like HPMC K4M, and natural gums like Guar gum in the form of matrix tablets

  19. FINITE RIODAN MATRIX AND RIODAN GROUP

    Institute of Scientific and Technical Information of China (English)

    2000-01-01

    Riodan Matrix is a lower triangular matrix of in finite order with certainly restricted conditions.In this paper,the author defines two kinds of finite Riodan matrices which are not limited to lower triangular.Properties of group theory of the two kinds matrices are considered.Applications of the finite Riodan matrices are researched.

  20. The Matrix exponential, Dynamic Systems and Control

    DEFF Research Database (Denmark)

    Poulsen, Niels Kjølstad

    2004-01-01

    The matrix exponential can be found in various connections in analysis and control of dynamic systems. In this short note we are going to list a few examples. The matrix exponential usably pops up in connection to the sampling process, whatever it is in a deterministic or a stochastic setting...

  1. Exploratory matrix factorization for PET image analysis.

    Science.gov (United States)

    Kodewitz, A; Keck, I R; Tomé, A M; Lang, E W

    2010-01-01

    Features are extracted from PET images employing exploratory matrix factorization techniques such as nonnegative matrix factorization (NMF). Appropriate features are fed into classifiers such as a support vector machine or a random forest tree classifier. An automatic feature extraction and classification is achieved with high classification rate which is robust and reliable and can help in an early diagnosis of Alzheimer's disease.

  2. Matrix perturbations: bounding and computing eigenvalues

    NARCIS (Netherlands)

    Reis da Silva, R.J.

    2011-01-01

    Despite the somewhat negative connotation of the word, not every perturbation is a bad perturbation. In fact, while disturbing the matrix entries, many perturbations still preserve useful properties such as the orthonormality of the basis of eigenvectors or the Hermicity of the original matrix. In t

  3. Matrix subordinators and related Upsilon transformations

    DEFF Research Database (Denmark)

    Barndorff-Nielsen, Ole Eiler; Pérez-Abreu, V.

    2008-01-01

    A class of upsilon transformations of Lévy measures for matrix subordinators is introduced. Some regularizing properties of these transformations are derived, such as absolute continuity and complete monotonicity. The class of Lévy measures with completely monotone matrix densities is characterized....... Examples of infinitely divisible nonnegative definite random matrices are constructed using an upsilon transformation....

  4. New Matrix Loop Algebra and Its Application

    Institute of Scientific and Technical Information of China (English)

    DONG Huan-He; XU Yue-Cai

    2008-01-01

    A new matrix Lie algebra and its corresponding Loop algebra are constructed firstly, as its appfication, the multi-component TC equation hierarchy is obtained, then by use of trace identity the Hamiltonian structure of the above system is presented. Finally, the integrable couplings of the obtained system is worked out by the expanding matrix Loop algebra.

  5. The Matrix exponential, Dynamic Systems and Control

    DEFF Research Database (Denmark)

    Poulsen, Niels Kjølstad

    2004-01-01

    The matrix exponential can be found in various connections in analysis and control of dynamic systems. In this short note we are going to list a few examples. The matrix exponential usably pops up in connection to the sampling process, whatever it is in a deterministic or a stochastic setting...

  6. Differential analysis of matrix convex functions II

    DEFF Research Database (Denmark)

    Hansen, Frank; Tomiyama, Jun

    2009-01-01

    We continue the analysis in [F. Hansen, and J. Tomiyama, Differential analysis of matrix convex functions. Linear Algebra Appl., 420:102--116, 2007] of matrix convex functions of a fixed order defined in a real interval by differential methods as opposed to the characterization in terms of divide...

  7. The Cartan Matrix of a Centralizer Algebra

    Indian Academy of Sciences (India)

    Umesh V Dubey; Amritanshu Prasad; Pooja Singla

    2012-02-01

    The centralizer algebra of a matrix consists of those matrices that commute with it. We investigate the basic representation-theoretic invariants of centralizer algebras, namely their radicals, projective indecomposable modules, injective indecomposable modules, simple modules and Cartan matrices. With the help of our Cartan matrix calculations we determine their global dimensions. Many of these algebras are of infinite global dimension.

  8. Finding nonoverlapping substructures of a sparse matrix

    Energy Technology Data Exchange (ETDEWEB)

    Pinar, Ali; Vassilevska, Virginia

    2004-08-09

    Many applications of scientific computing rely on computations on sparse matrices, thus the design of efficient implementations of sparse matrix kernels is crucial for the overall efficiency of these applications. Due to the high compute-to-memory ratio and irregular memory access patterns, the performance of sparse matrix kernels is often far away from the peak performance on a modern processor. Alternative data structures have been proposed, which split the original matrix A into A{sub d} and A{sub s}, so that A{sub d} contains all dense blocks of a specified size in the matrix, and A{sub s} contains the remaining entries. This enables the use of dense matrix kernels on the entries of A{sub d} producing better memory performance. In this work, we study the problem of finding a maximum number of non overlapping rectangular dense blocks in a sparse matrix, which has not been studied in the sparse matrix community. We show that the maximum non overlapping dense blocks problem is NP-complete by using a reduction from the maximum independent set problem on cubic planar graphs. We also propose a 2/3-approximation algorithm for 2 times 2 blocks that runs in linear time in the number of nonzeros in the matrix. We discuss alternatives to rectangular blocks such as diagonal blocks and cross blocks and present complexity analysis and approximation algorithms.

  9. Matrix model description of baryonic deformations

    Energy Technology Data Exchange (ETDEWEB)

    Bena, Iosif; Murayama, Hitoshi; Roiban, Radu; Tatar, Radu

    2003-03-13

    We investigate supersymmetric QCD with N{sub c} + 1 flavors using an extension of the recently proposed relation between gauge theories and matrix models.The impressive agreement between the two sides provides a beautiful confirmation of the extension of the gauge theory-matrix model relation to this case.

  10. Fragmentation of extracellular matrix by hypochlorous acid

    DEFF Research Database (Denmark)

    Woods, Alan A; Davies, Michael Jonathan

    2003-01-01

    The interaction of extracellular matrix with cells regulates their adhesion, migration and proliferation, and it is believed that damage to vascular matrix components is a factor in the development of atherosclerosis. Evidence has been provided for a role for the haem enzyme MPO (myeloperoxidase)...

  11. Modeling and Simulation of Matrix Converter

    DEFF Research Database (Denmark)

    Liu, Fu-rong; Klumpner, Christian; Blaabjerg, Frede

    2005-01-01

    This paper discusses the modeling and simulation of matrix converter. Two models of matrix converter are presented: one is based on indirect space vector modulation and the other is based on power balance equation. The basis of these two models is• given and the process on modeling is introduced...

  12. Infinite Matrix Products and the Representation of the Matrix Gamma Function

    Directory of Open Access Journals (Sweden)

    J.-C. Cortés

    2015-01-01

    Full Text Available We introduce infinite matrix products including some of their main properties and convergence results. We apply them in order to extend to the matrix scenario the definition of the scalar gamma function given by an infinite product due to Weierstrass. A limit representation of the matrix gamma function is also provided.

  13. Update of the stability of drugs cytostatic drugs by applying the methodology of the matrix of risk for the manufacture of sterile drugs

    Directory of Open Access Journals (Sweden)

    Ángela Usarralde-Pérez

    2016-07-01

    Full Text Available Objective: To establish limits of validity to opened or reconstituted vials and cytostatic mixtures according to their physico- chemical stability and the level of risk and preparation requirements. The level of risk and preparation requirements were assigned by the risk matrix the Guide of Good Practice of Preparation of Drugs in Hospital Pharmacy Services. Method: A table of stabilities of cytostatic drugs was developed. Physicochemical stability data were obtained from data sheets and literature reviews. The level of risk was assigned by the matrix of risk depending on the requirements of each preparation. When the physico-chemical stability was equal to or higher than indicated by the matrix, it is assumed the terms of validity of the matrix; otherwise, validity periods coincided with the peak period of physicochemical stability. Results: 61 drugs were reviewed. It was assumed the chemical term of validity in 45.9% of opened/reconstituted vials and 50.8% of cytostatic mixtures, and indicated by the risk in the rest array, respectively. According to the matrix, the level of risk was medium in most of cytostatic drugs. Only one preparation was high risk. No preparation obtained low-risk. Conclusions: To assign the term of validity of opened/reconstituted vials and cytostatic mixtures not only it is necessary to consider physical and chemical stability. The level of risk and preparation requirements are also important, allowing more adequate validity periods

  14. Block Hadamard measurement matrix with arbitrary dimension in compressed sensing

    Science.gov (United States)

    Liu, Shaoqiang; Yan, Xiaoyan; Fan, Xiaoping; Li, Fei; Xu, Wen

    2017-01-01

    As Hadamard measurement matrix cannot be used for compressing signals with dimension of a non-integral power-of-2, this paper proposes a construction method of block Hadamard measurement matrix with arbitrary dimension. According to the dimension N of signals to be measured, firstly, construct a set of Hadamard sub matrixes with different dimensions and make the sum of these dimensions equals to N. Then, arrange the Hadamard sub matrixes in a certain order to form a block diagonal matrix. Finally, take the former M rows of the block diagonal matrix as the measurement matrix. The proposed measurement matrix which retains the orthogonality of Hadamard matrix and sparsity of block diagonal matrix has highly sparse structure, simple hardware implements and general applicability. Simulation results show that the performance of our measurement matrix is better than Gaussian matrix, Logistic chaotic matrix, and Toeplitz matrix.

  15. Perturbative analysis of gauged matrix models

    Science.gov (United States)

    Dijkgraaf, Robbert; Gukov, Sergei; Kazakov, Vladimir A.; Vafa, Cumrun

    2003-08-01

    We analyze perturbative aspects of gauged matrix models, including those where classically the gauge symmetry is partially broken. Ghost fields play a crucial role in the Feynman rules for these vacua. We use this formalism to elucidate the fact that nonperturbative aspects of N=1 gauge theories can be computed systematically using perturbative techniques of matrix models, even if we do not possess an exact solution for the matrix model. As examples we show how the Seiberg-Witten solution for N=2 gauge theory, the Montonen-Olive modular invariance for N=1*, and the superpotential for the Leigh-Strassler deformation of N=4 can be systematically computed in perturbation theory of the matrix model or gauge theory (even though in some of these cases an exact answer can also be obtained by summing up planar diagrams of matrix models).

  16. Perturbative Analysis of Gauged Matrix Models

    CERN Document Server

    Dijkgraaf, R; Kazakov, V A; Vafa, C; Dijkgraaf, Robbert; Gukov, Sergei; Kazakov, Vladimir A.; Vafa, Cumrun

    2003-01-01

    We analyze perturbative aspects of gauged matrix models, including those where classically the gauge symmetry is partially broken. Ghost fields play a crucial role in the Feynman rules for these vacua. We use this formalism to elucidate the fact that non-perturbative aspects of N=1 gauge theories can be computed systematically using perturbative techniques of matrix models, even if we do not possess an exact solution for the matrix model. As examples we show how the Seiberg-Witten solution for N=2 gauge theory, the Montonen-Olive modular invariance for N=1*, and the superpotential for the Leigh-Strassler deformation of N=4 can be systematically computed in perturbation theory of the matrix model/gauge theory (even though in some of these cases the exact answer can also be obtained by summing up planar diagrams of matrix models).

  17. Matrix Coherence and the Nystrom Method

    CERN Document Server

    Talwalkar, Ameet

    2010-01-01

    The Nystrom method is an efficient technique to speed up large-scale learning applications by generating low-rank approximations. Crucial to the performance of this technique is the assumption that a matrix can be well approximated by working exclusively with a subset of its columns. In this work we relate this assumption to the concept of matrix coherence and connect matrix coherence to the performance of the Nystrom method. Making use of related work in the compressed sensing and the matrix completion literature, we derive novel coherence-based bounds for the Nystrom method in the low-rank setting. We then present empirical results that corroborate these theoretical bounds. Finally, we present more general empirical results for the full-rank setting that convincingly demonstrate the ability of matrix coherence to measure the degree to which information can be extracted from a subset of columns.

  18. Extracellular matrix component signaling in cancer

    DEFF Research Database (Denmark)

    Multhaupt, Hinke A. B.; Leitinger, Birgit; Gullberg, Donald

    2016-01-01

    Cell responses to the extracellular matrix depend on specific signaling events. These are important from early development, through differentiation and tissue homeostasis, immune surveillance, and disease pathogenesis. Signaling not only regulates cell adhesion cytoskeletal organization and motil...... as well as matrix constitution and protein crosslinking. Here we summarize roles of the three major matrix receptor types, with emphasis on how they function in tumor progression. [on SciFinder(R)]......Cell responses to the extracellular matrix depend on specific signaling events. These are important from early development, through differentiation and tissue homeostasis, immune surveillance, and disease pathogenesis. Signaling not only regulates cell adhesion cytoskeletal organization...... and motility but also provides survival and proliferation cues. The major classes of cell surface receptors for matrix macromols. are the integrins, discoidin domain receptors, and transmembrane proteoglycans such as syndecans and CD44. Cells respond not only to specific ligands, such as collagen, fibronectin...

  19. Spectral clustering based on matrix perturbation theory

    Institute of Scientific and Technical Information of China (English)

    TIAN Zheng; LI XiaoBin; JU YanWei

    2007-01-01

    This paper exposes some intrinsic characteristics of the spectral clustering method by using the tools from the matrix perturbation theory. We construct a weight matrix of a graph and study its eigenvalues and eigenvectors. It shows that the number of clusters is equal to the number of eigenvalues that are larger than 1, and the number of points in each of the clusters can be approximated by the associated eigenvalue. It also shows that the eigenvector of the weight matrix can be used directly to perform clustering; that is, the directional angle between the two-row vectors of the matrix derived from the eigenvectors is a suitable distance measure for clustering. As a result, an unsupervised spectral clustering algorithm based on weight matrix (USCAWM) is developed. The experimental results on a number of artificial and real-world data sets show the correctness of the theoretical analysis.

  20. Confocal microscopy imaging of the biofilm matrix.

    Science.gov (United States)

    Schlafer, Sebastian; Meyer, Rikke L

    2017-07-01

    The extracellular matrix is an integral part of microbial biofilms and an important field of research. Confocal laser scanning microscopy is a valuable tool for the study of biofilms, and in particular of the biofilm matrix, as it allows real-time visualization of fully hydrated, living specimens. Confocal microscopes are held by many research groups, and a number of methods for qualitative and quantitative imaging of the matrix have emerged in recent years. This review provides an overview and a critical discussion of techniques used to visualize different matrix compounds, to determine the concentration of solutes and the diffusive properties of the biofilm matrix. Copyright © 2016 Elsevier B.V. All rights reserved.