WorldWideScience

Sample records for fast ferrite icrf

  1. ICRF antenna matching systems with ferrite tuners for the Alcator C-Mod tokamak

    Energy Technology Data Exchange (ETDEWEB)

    Lin, Y., E-mail: ylin@psfc.mit.edu; Binus, A.; Wukitch, S.J.; Koert, P.; Murray, R.; Pfeiffer, A.

    2015-11-15

    Highlights: • We have developed a fast ferrite tuner (FFT) based antenna matching system. • The FFT system works well on the ICRF antennas on the Alcator C-Mod tokamak. • The FFT system maintains <1% RF power reflection for most plasma discharges. • The FFT system can deal with plasma transients. • The FFT system can handle high RF power operation. - Abstract: Real-time fast ferrite tuning (FFT) has been successfully implemented on the ICRF antennas on Alcator C-Mod. The former prototypical FFT system on the E-port 2-strap antenna has been upgraded using new ferrite tuners. A new FFT system with two ferrite tuners and one fixed-length stub has been installed on the transmission line of the D-port 2-strap antenna. These two systems are able to achieve and maintain the reflected power to the transmitters to less than 1% in real time under almost all plasma conditions and help ensure reliable high power operation of the antennas. The loading insensitivity feature vs. plasma conditions of the innovative field-aligned (FA) 4-strap antenna on the J-port allows us to significantly improve the matching by installing a carefully designed stub on each of the two transmission lines. The reduction of the RF voltages in the transmission lines has enabled the J-port FA antenna to deliver 3.7 MW RF power to plasmas out of 4 MW source power. The matching on the J-port antenna can be further improved by adding a single ferrite tuner under real-time control on each transmission line and this scheme will be implemented in the near future.

  2. ICRF antenna matching system with ferrite tuners for the Alcator C-Mod tokamak

    Science.gov (United States)

    Lin, Y.; Binus, A.; Wukitch, S. J.; Koert, P.; Murray, R.; Pfeiffer, A.

    2015-12-01

    Real-time fast ferrite tuning (FFT) has been successfully implemented on the ICRF antennas on Alcator C-Mod. The former prototypical FFT system on the E-port 2-strap antenna has been upgraded using new ferrite tuners that have been designed specifically for the operational parameters of the Alcator C-Mod ICRF system (˜ 80 MHz). Another similar FFT system, with two ferrite tuners and one fixed-length stub, has been installed on the transmission line of the D-port 2-strap antenna. These two systems share a Linux-server-based real-time controller. These FFT systems are able to achieve and maintain the reflected power to the transmitters to less than 1% in real time during the plasma discharges under almost all plasma conditions, and help ensure reliable high power operation of the antennas. The innovative field-aligned (FA) 4-strap antenna on J-port has been found to have an interesting feature of loading insensitivity vs. plasma conditions. This feature allows us to significantly improve the matching for the FA J-port antenna by installing carefully designed stubs on the two transmission lines. The reduction of the RF voltages in the transmission lines has enabled the FA J-port antenna to deliver 3.7 MW RF power to plasmas out of the 4 MW source power in high performance I-mode plasmas.

  3. Fast ion generation and bulk plasma heating with three-ion ICRF scenarios

    Energy Technology Data Exchange (ETDEWEB)

    Kazakov, Ye. O., E-mail: yevgen.kazakov@rma.ac.be; Van Eester, D.; Ongena, J.; Lerche, E.; Messiaen, A. [Laboratory for Plasma Physics, LPP-ERM/KMS, EUROfusion Consortium Member, Brussels (Belgium); Dumont, R. [CEA, IRFM, F-13108 Saint-Paul-lez-Durance (France)

    2015-12-10

    Launching electromagnetic waves in the ion cyclotron range of frequencies (ICRF) is an efficient method of plasma heating, actively employed in most of fusion machines. ICRF has a number of important supplementary applications, including the generation of high-energy ions. In this paper, we discuss a new set of three-ion ICRF scenarios and the prospect of their use as a dedicated tool for fast ion generation in tokamaks and stellarators. A distinct feature of these scenarios is a strong absorption efficiency possible at very low concentrations of resonant minority ions (∼ 1% or even below). Such concentration levels are typical for impurities contaminating fusion plasmas. An alternative ICRF scenario for maximizing the efficiency of bulk D-T ion heating is suggested for JET and ITER tokamaks, which is based on three-ion ICRF heating of intrinsic Beryllium impurities.

  4. Fast ion generation and bulk plasma heating with three-ion ICRF scenarios

    Science.gov (United States)

    Kazakov, Ye. O.; Van Eester, D.; Dumont, R.; Ongena, J.; Lerche, E.; Messiaen, A.

    2015-12-01

    Launching electromagnetic waves in the ion cyclotron range of frequencies (ICRF) is an efficient method of plasma heating, actively employed in most of fusion machines. ICRF has a number of important supplementary applications, including the generation of high-energy ions. In this paper, we discuss a new set of three-ion ICRF scenarios and the prospect of their use as a dedicated tool for fast ion generation in tokamaks and stellarators. A distinct feature of these scenarios is a strong absorption efficiency possible at very low concentrations of resonant minority ions (˜ 1% or even below). Such concentration levels are typical for impurities contaminating fusion plasmas. An alternative ICRF scenario for maximizing the efficiency of bulk D-T ion heating is suggested for JET and ITER tokamaks, which is based on three-ion ICRF heating of intrinsic Beryllium impurities.

  5. ICRF fast wave current drive and mode conversion current drive in EAST tokamak

    Science.gov (United States)

    Yin, L.; Yang, C.; Gong, X. Y.; Lu, X. Q.; Du, D.; Chen, Y.

    2017-10-01

    Fast wave in the ion-cyclotron resonance frequency (ICRF) range is a promising candidate for non-inductive current drive (CD), which is essential for long pulse and high performance operation of tokamaks. A numerical study on the ICRF fast wave current drive (FWCD) and mode-conversion current drive (MCCD) in the Experimental Advanced Superconducting Tokamak (EAST) is carried out by means of the coupled full wave and Ehst-Karney parameterization methods. The results show that FWCD efficiency is notable in two frequency regimes, i.e., f ≥ 85 MHz and f = 50-65 MHz, where ion cyclotron absorption is effectively avoided, and the maximum on-axis driven current per unit power can reach 120 kA/MW. The sensitivity of the CD efficiency to the minority ion concentration is confirmed, owing to fast wave mode conversion, and the peak MCCD efficiency is reached for 22% minority-ion concentration. The effects of the wave-launch position and the toroidal wavenumber on the efficiency of current drive are also investigated.

  6. Measurement of fast minority /sub 3/He/sup + +/ energy distribution during ICRF heating

    Science.gov (United States)

    Post, D.E. Jr.; Grisham, L.R.; Medley, S.S.

    A method and means for measuring the fast /sub 3/He/sup + +/ distribution during /sub 3/He/sup + +/ minority Ion Cyclotron Resonance Frequency (ICRF) heating is disclosed. The present invention involves the use of 10 to 100 keV beams of neutral helium atoms to neutralize the fast /sub 3/He/sup + +/ ions in a heated plasma by double charge exchange (/sub 3/He/sup + +/ + /sub 4/He/sup 0/ ..-->.. /sub 3/He/sup 0/ + /sub 4/He/sup + +/). The neutralized fast /sub 3/He/sup 0/ atoms then escape from the hot plasma confined by a magnetic field and are detected by conventional neutral particle analyzing means. This technique permits the effectiveness of the coupling of the ion cyclotron waves to the /sub 3/He/sup + +/ minority ions to be accurately measured. The present invention is particularly adapted for use in evaluating the effectiveness of the intermediate coupling between the RF heating and the /sub 3/He/sup + +/ in an energetic toroidal plasma.

  7. Feedback controlled hybrid fast ferrite tuners

    Energy Technology Data Exchange (ETDEWEB)

    Remsen, D.B.; Phelps, D.A.; deGrassie, J.S.; Cary, W.P.; Pinsker, R.I.; Moeller, C.P. [General Atomics, San Diego, CA (United States); Arnold, W.; Martin, S.; Pivit, E. [ANT-Bosch, Backnang (Germany)

    1993-09-01

    A low power ANT-Bosch fast ferrite tuner (FFT) was successfully tested into (1) the lumped circuit equivalent of an antenna strap with dynamic plasma loading, and (2) a plasma loaded antenna strap in DIII-D. When the FFT accessible mismatch range was phase-shifted to encompass the plasma-induced variation in reflection coefficient, the 50 {Omega} source was matched (to within the desired 1.4 : 1 voltage standing wave ratio). The time required to achieve this match (i.e., the response time) was typically a few hundred milliseconds, mostly due to a relatively slow network analyzer-computer system. The response time for the active components of the FFT was 10 to 20 msec, or much faster than the present state-of-the-art for dynamic stub tuners. Future FFT tests are planned, that will utilize the DIII-D computer (capable of submillisecond feedback control), as well as several upgrades to the active control circuit, to produce a FFT feedback control system with a response time approaching 1 msec.

  8. A new type of MHD activity in JET ICRF-only discharges with high fast-ion energy contents

    Energy Technology Data Exchange (ETDEWEB)

    Mantsinen, M.J. [JET Joint Undertaking, Abingdon, Oxfordshire (United Kingdom); Helsinki University of Technology, Association Euratom-Tekes (Finland); Sharapov, S.; Alper, B.; Gondhalekar, A.; McDonald, D.C. [JET Joint Undertaking, Abingdon, Oxfordshire (United Kingdom)

    2000-12-01

    The question of sawtooth stabilization at very high fast-ion energy contents has been addressed in discharges carried out in the JET tokamak with ion cyclotron resonance frequency (ICRF) heating and varying plasma density, controlled by deuterium gas puffs. In these experiments dramatic differences in the sawtooth behaviour have been observed. When the plasma density n{sub e} decreases below a certain threshold, the sawtooth frequency and the crash duration time increase by a factor of five. Since the fast-ion energy content increases with decreasing n{sub e} due to the inverse proportionality of the fast-ion slowing-down time on n{sub e}, the threshold in n{sub e} corresponds to a threshold in the fast-ion energy content. In the present experiments, this threshold is reached when the fast-ion energy contribution to the total plasma diamagnetic energy content becomes larger than 45%. The sawtooth activity with short sawtooth free period is accompanied by MHD activity, with a toroidal mode number n = 1 at frequencies between 55 and 65 kHz. This activity is interpreted as an energetic particle fishbone mode that is resonant with the ICRF-driven fast ions. The experimental results appear to be consistent with the stability diagram for sawtooth and fishbone modes (White 1989 Theory of Tokamak Plasmas (Amsterdam: North-Holland)), exploring the part of the diagram with a very large fast-ion population. (author)

  9. A new type of MHD activity in JET ICRF-only discharges with high fast-ion energy contents

    Energy Technology Data Exchange (ETDEWEB)

    Mantsinen, M.; Sharapov, S.; Alper, B. [and others

    2000-12-01

    The question of sawtooth stabilisation at very high fast ion energy contents has been addressed in discharges carried out in the JET tokamak with ion cyclotron resonance frequency (ICRF) heating and varying plasma density, controlled by deuterium gas puffs. In these experiments dramatic differences in the sawtooth behaviour have been observed. When the plasma density n{sub e} decreases below a certain threshold, the sawtooth frequency and the crash duration time increase by a factor of five. Since the fast-ion energy content increases with decreasing n{sub e} due to the inverse proportionality of the fast-ion slowing-down time on n{sub e}, the threshold in n{sub e} corresponds to a threshold in the fast ion energy content. In the present experiments, this threshold is reached when the fast ion energy contribution to the total plasma diamagnetic energy content becomes larger than 45%. The sawtooth activity with short sawtooth free period is accompanied by MHD activity, with a toroidal mode number n = 1 at frequencies between 55-65 kHz. This activity is interpreted as an energetic particle fishbone mode that is resonant with the ICRF-driven fast ions. The experimental results appear to be consistent with the stability diagram for sawtooth and fishbone modes [White, Theory of Tokamak Plasmas (North-Holland, Amsterdam, 1989)], exploring the part of the diagram with a very large fast ion population. (author)

  10. A new type of MHD activity in JET ICRF-only discharges with high fast-ion energy contents

    Science.gov (United States)

    Mantsinen, M. J.; Sharapov, S.; Alper, B.; Gondhalekar, A.; McDonald, D. C.

    2000-12-01

    The question of sawtooth stabilization at very high fast-ion energy contents has been addressed in discharges carried out in the JET tokamak with ion cyclotron resonance frequency (ICRF) heating and varying plasma density, controlled by deuterium gas puffs. In these experiments dramatic differences in the sawtooth behaviour have been observed. When the plasma density ne decreases below a certain threshold, the sawtooth frequency and the crash duration time increase by a factor of five. Since the fast-ion energy content increases with decreasing ne due to the inverse proportionality of the fast-ion slowing-down time on ne, the threshold in ne corresponds to a threshold in the fast-ion energy content. In the present experiments, this threshold is reached when the fast-ion energy contribution to the total plasma diamagnetic energy content becomes larger than 45%. The sawtooth activity with short sawtooth free period is accompanied by MHD activity, with a toroidal mode number n = 1 at frequencies between 55 and 65 kHz. This activity is interpreted as an energetic particle fishbone mode that is resonant with the ICRF-driven fast ions. The experimental results appear to be consistent with the stability diagram for sawtooth and fishbone modes (White 1989 Theory of Tokamak Plasmas (Amsterdam: North-Holland)), exploring the part of the diagram with a very large fast-ion population.

  11. Spatial distribution of {gamma} emissivity and fast ions during ({sup 3}He)D ICRF heating experiments on JET

    Energy Technology Data Exchange (ETDEWEB)

    Start, D.F.H. [Commission of the European Communities, Abingdon (United Kingdom). JET Joint Undertaking; Righi, E. [Imperial Coll. of Science and Technology, London (United Kingdom); Warrick, C. [UKAEA Culham Lab., Abingdon (United Kingdom)

    1994-07-01

    A model is presented that can simulate the {gamma} emissivity in the poloidal cross-section during ({sup 3}He)D ICRF heated discharges in JET plasmas, by merging information obtained from the fast ion distribution and from nuclear reactions producing the observed {gamma} emissivity (production of {gamma} photons during {sup 3}He-{sup 9}Be reactions). This technique can play an important role in the identification of plasma instabilities that affect the redistribution of the fast ions in the plasma, like the TAE modes and the ripple in the tokamak magnetic field. 9 refs., 4 figs., 1 tab.

  12. The technology of ICRF systems

    Energy Technology Data Exchange (ETDEWEB)

    Baity, F.W.; Barber, G.C.; Bigelow, T.S. [and others

    1995-12-31

    The technology of ICRF systems has made substantial gains in the past few years. The total power levels have increased from the 5-MW level to greater than 20 MW; the pulse lengths have increased from the 100-msec level to 30 seconds. Recently, fast wave current drive (FWCD) has been demonstrated using phased arrays of ICRF antennas. In order to achieve such large gains, substantial changes and improvements were needed in the level of design analysis, fabrication techniques, and system controls.

  13. Ferritic steels for sodium-cooled fast reactors: Design principles and challenges

    Science.gov (United States)

    Raj, Baldev; Vijayalakshmi, M.

    2010-09-01

    An overview of the current status of development of ferritic steels for emerging fast reactor technologies is presented in this paper. The creep-resistant 9-12Cr ferritic/martensitic steels are classically known for steam generator applications. The excellent void swelling resistance of ferritic steels enabled the identification of their potential for core component applications of fast reactors. Since then, an extensive knowledge base has been generated by identifying the empirical correlations between chemistry of the steels, heat treatment, structure, and properties, in addition to their in-reactor behavior. A few concerns have also been identified which pertain to high-temperature irradiation creep, embrittlement, Type IV cracking in creep-loaded weldments, and hard zone formation in dissimilar joints. The origin of these problems and the methodologies to overcome the limitations are highlighted. Finally, the suitability of the ferritic steels is re-evaluated in the emerging scenario of the fast reactor technology, with a target of achieving better breeding ratio and improved thermal efficiency.

  14. Modelling of advanced three-ion ICRF heating and fast ion generation scheme for tokamaks and stellarators

    Science.gov (United States)

    Faustin, J. M.; Graves, J. P.; Cooper, W. A.; Lanthaler, S.; Villard, L.; Pfefferlé, D.; Geiger, J.; Kazakov, Ye O.; Van Eester, D.

    2017-08-01

    Absorption of ion-cyclotron range of frequencies waves at the fundamental resonance is an efficient source of plasma heating and fast ion generation in tokamaks and stellarators. This heating method is planned to be exploited as a fast ion source in the Wendelstein 7-X stellarator. The work presented here assesses the possibility of using the newly developed three-ion species scheme (Kazakov et al (2015) Nucl. Fusion 55 032001) in tokamak and stellarator plasmas, which could offer the capability of generating more energetic ions than the traditional minority heating scheme with moderate input power. Using the SCENIC code, it is found that fast ions in the MeV range of energy can be produced in JET-like plasmas. The RF-induced particle pinch is seen to strongly impact the fast ion pressure profile in particular. Our results show that in typical high-density W7-X plasmas, the three-ion species scheme generates more energetic ions than the more traditional minority heating scheme, which makes three-ion scenario promising for fast-ion confinement studies in W7-X.

  15. ODS Ferritic/martensitic alloys for Sodium Fast Reactor fuel pin cladding

    Science.gov (United States)

    Dubuisson, Philippe; Carlan, Yann de; Garat, Véronique; Blat, Martine

    2012-09-01

    The development of ODS materials for the cladding for Sodium Fast Reactors is a key issue to achieve the objectives required for the GEN IV reactors. CEA, AREVA and EDF have launched in 2007 an important program to determine the optimal fabrication parameters, and to measure and understand the microstructure and properties before, under and after irradiation of such cladding materials. The aim of this paper is to present the French program and the major results obtained recently at CEA on Fe-9/14/18Cr1WTiY2O3 ferritic/martensitic ODS materials. The first step of the program was to consolidate Fe-9/14/18Cr ODS materials as plates and bars to study the microstructure and the mechanical properties of the new alloys. The second step consists in producing tubes at a geometry representative of the cladding of new Sodium Fast Reactors. The optimization of the fabrication route at the laboratory scale is conducted and different tubes were produced. Their microstructure depends on the martensitic (Fe-9Cr) or ferritic (Fe-14Cr) structure. To join the plug to the tube, the reference process is the welding resistance. A specific approach is developed to model the process and support the development of the welds performed within the "SOPRANO" facility. The development at CEA of Fe-9/14/18Cr new ODS materials for the cladding for GENIV Sodium Fast Reactors is in progress. The first microstructural and mechanical characterizations are very encouraging and the full assessment and qualification of this new alloys and products will pass through the irradiation of specimens, tubes, fuel pins and subassemblies up to high doses.

  16. Localized bulk electron heating with ICRF mode conversion in the JET tokamak

    DEFF Research Database (Denmark)

    Mantsinen, M.J.; Mayoral, M.-L.; Eester, D. Van

    2004-01-01

    Ion cyclotron resonance frequencies (ICRF) mode conversion has been developed for localized on-axis and off-axis bulk electron heating on the JET tokamak. The fast magnetosonic waves launched from the low-field side ICRF antennas are mode-converted to short-wavelength waves on the high-field side...

  17. SMALL VOLUME LONG PULSE X RAY PREIONISED XeCl LASER WITH DOUBLE DISCHARGE AND FAST FERRITE MAGNETIC SWITCH

    OpenAIRE

    J. Hueber; Kobhio, M.; Fontaine, B.; Delaporte, Ph.; Sentis, M.; Forestier, B.

    1991-01-01

    Experimental results obtained with a high efficiency small volume long pulse X-Ray preionised XeCl laser with double discharge and very fast ferrite magnetic switch are presented and compared with the results given by a new XeCl laser numerical self consistant model. The model takes into account most recent kinetic data and time variation of discharge impedence and switch inductance. There is a good agreement between experiment and model on electrical and laser parameters for typical conditions.

  18. ICRF-3: Roadmap to the next generation ICRF

    Science.gov (United States)

    Jacobs, C.; Arias, F.; Boboltz, D.; Boehm, J.; Bolotin, S.; Bourda, G.; Charlot, P.; de Witt, A.; Fey, A.; Gaume, R.; Gordon, D.; Heinkelmann, R.; Lambert, S.; Ma, C.; Malkin, Z.; Nothnagel, A.; Seitz, M.; Skurikhina, E.; Souchay, J.; Titov, O.

    2014-12-01

    We propose a 3rd generation radio-based International Celestial Reference Frame (ICRF- 3) to improve upon the highly successful ICRF-2. Our goals are to improve the precision as well as the spatial and frequency coverages relative to the ICRF-2 by 2018. This date is driven by the desire to create radio frames early enough to test the Gaia optical frame during its construction. Several specific actions are underway. A collaboration has been started to improve S/X-band precision of the ˜2200 VLBA Calibrator Survey sources which are typically 5 times less precise than the rest of the ICRF-2. S/X-band southern precision improvements are planned from observations with southern antennas such as the AuScope and HartRAO, S. Africa. We seek to improve radio frequency coverage with X/Ka and K-band work. An X/Ka frame of 631 sources now has full sky coverage from the addition of a 2nd southern station in Argentina which should strengthen the southern hemisphere in general. A K-band collaboration has formed with similar coverage and southern hemisphere precision goals. On the analysis front, special attention will be given to combination techniques both of VLBI catalogs and of multiple data types (e.g. VLBI+GPS). Finally, work is underway to identify and pinpoint sources bright enough in both radio and optical to allow for a robust frame tie between VLBI and Gaia optical frames.

  19. Patent Analysis of Ferritic/Martensitic Steels for the Fuel Cladding in Sodium-cooled Fast Reactor

    Energy Technology Data Exchange (ETDEWEB)

    Baek, Jong Hyuk; Kim, Sung Ho; Kim, Tae Kyu; Kim, Woo Gon; Jang, Jin Sung; Kim, Dae Whan; Han, Chang Hee; Lee, Chan Bock

    2007-09-15

    The Korean, Japanese, U.S. and European patents related to the ferritic/martensitic steels were systematically surveyed to evaluate their patent status, which would be applicable to the fuel cladding materials for the Sodium-cooled Fast Reactor (SFR). From the surveys, totally 38 patents were finally selected for the quantitative and qualitative analysis. Among them, 28 patents (74%) were processed by Japanese companies and Sumitomo Metal industries Ltd. was top-ranked in the number (9) of priority patents. On the basis of these surveys, most patents could be applicable to the fuel cladding materials for SFR and, especially, some useful patents as the cladding were registered by the Russian and the Korean.

  20. Patent Analysis of Ferritic/Martensitic Steels for the Fuel Cladding in Sodium-cooled Fast Reactor

    Energy Technology Data Exchange (ETDEWEB)

    Baek, Jong Hyuk; Kim, Sung Ho; Kim, Tae Kyu; Kim, Woo Gon; Jang, Jin Sung; Kim, Dae Whan; Han, Chang Hee; Lee, Chan Bock

    2007-09-15

    The Korean, Japanese, U.S. and European patents related to the ferritic/martensitic steels were systematically surveyed to evaluate their patent status, which would be applicable to the fuel cladding materials for the Sodium-cooled Fast Reactor (SFR). From the surveys, totally 38 patents were finally selected for the quantitative and qualitative analysis. Among them, 28 patents (74%) were processed by Japanese companies and Sumitomo Metal industries Ltd. was top-ranked in the number (9) of priority patents. On the basis of these surveys, most patents could be applicable to the fuel cladding materials for SFR and, especially, some useful patents as the cladding were registered by the Russian and the Korean.

  1. A method to determine arc position in ICRF systems

    Energy Technology Data Exchange (ETDEWEB)

    D’Inca, R., E-mail: rodolphe.dinca@ipp.mpg.de [Max-Planck-Institut für Plasmaphysik, EURATOM Association, Garching (Germany); Polozhiy, K.; Eckert, B.; Siegel, G. [Max-Planck-Institut für Plasmaphysik, EURATOM Association, Garching (Germany); Noterdaeme, J.-M. [Max-Planck-Institut für Plasmaphysik, EURATOM Association, Garching (Germany); EESA Department, Gent University (Belgium)

    2013-10-15

    Highlights: ► We show that the voltage noise characteristic of an arc in an ICRF system is due to the propagation and reflections of an electromagnetic pulse emitted by this arc. ► A simplified RF model of an arc in a testbed representative of an ICRF system is developed to see the effect of its location on the voltage noise it emits. ► The model is compared with the results on the testbed for arcs occurring at two locations: one can be determined precisely, the other with a decreased accuracy. -- Abstract: The study of arcs on ICRF systems has mainly focused on the development of fast detectors to detect a breakdown, independently from its position, before they can damage the components [1]. However, the ability to localize an arc is also an important factor: arcs can be the sign of a defect and if they occur at the same location, they give a good indication of the position of this defect without having to use intrusive diagnostics like optical fibers. We present here a method to find the position of arcs based on the analysis of their high-frequency noise. Arcs are indeed fast transient which excite frequencies in the MHz range. The SHAD system reacts on the integral value of this noise signal to detect the development of arcs. But a further investigation of this signal shows detailed features like splittings and chirpings of the frequency peaks which give more information on the source of the breakdown: at its birth, the arc emits a short electromagnetic pulse of several nanoseconds that propagates inside the ICRF system; this pulse is reflected by components like the antenna, the stub tuners or the generators back to the arc thereby changing its boundary conditions. This resonance between the arc and the ICRF system can be measured and the time of propagation of the pulse gives useful data on the position of the breakdown. We have carried out tests on the Manipulator eXPeriment (a testbed to artificially create arcs in a representative ICRF system) and

  2. First ICRF heating experiment in the large helical device

    Energy Technology Data Exchange (ETDEWEB)

    Mutoh, T.; Kumazawa, R.; Seki, T. [National Inst. for Fusion Science, Toki, Gifu (Japan)] [and others

    1999-07-01

    Initial ICRF heating experiment in the LHD was carried out in 1998. One pair of the movable loop antennas was used and the coupling resistance was around one ohm for the low density ECH plasma. The loading characteristics were consistent with the fast wave excitation. By applying the ICRF heating of 300 kW to the ECH target plasma, the diamagnetic energy was increased from 13 kJ to 26 kJ. The heating performance was decided by hydrogen mixture rate on puffing gas. Efficient electron heating was observed at the higher hydrogen gas ratio. These results can be explained by the one dimensional wave analysis calculation on slab plasma model. (J.P.N.)

  3. Benchmarking ICRF simulations for ITER

    Energy Technology Data Exchange (ETDEWEB)

    R. V. Budny, L. Berry, R. Bilato, P. Bonoli, M. Brambilla, R.J. Dumont, A. Fukuyama, R. Harvey, E.F. Jaeger, E. Lerche, C.K. Phillips, V. Vdovin, J. Wright, and members of the ITPA-IOS

    2010-09-28

    Abstract Benchmarking of full-wave solvers for ICRF simulations is performed using plasma profiles and equilibria obtained from integrated self-consistent modeling predictions of four ITER plasmas. One is for a high performance baseline (5.3 T, 15 MA) DT H-mode plasma. The others are for half-field, half-current plasmas of interest for the pre-activation phase with bulk plasma ion species being either hydrogen or He4. The predicted profiles are used by seven groups to predict the ICRF electromagnetic fields and heating profiles. Approximate agreement is achieved for the predicted heating power partitions for the DT and He4 cases. Profiles of the heating powers and electromagnetic fields are compared.

  4. Overview of the ICRF Program on C-Mod

    Science.gov (United States)

    Porkolab, M.; Basse, N.; Bonoli, P. T.; Edlund, E.; Lin, L.; Lin, Y.; Parisot, A.; Snipes, J.; Wright, J. C.; Wukitch, S. J.; Schilling, G.

    2004-11-01

    Recent ICRF experiments have focused upon mode conversion, antenna performance and coupling, and wave particle interactions. Fast wave mode conversion into the ion Bernstein (IBW) and/or ion cyclotron (ICW) waves in multi-ion species plasmas should be important for plasma heating, current drive and flow drive. The recently upgraded Phase Contrast Imaging diagnostic (PCI) has allowed simultaneous observation of both the IBW and ICW in a D(^3He) plasma and prove unambiguously the existence of both modes. These results provide a means to verify predictions of full wave codes and to optimize such processes for plasma control. Recent improvements in the antenna designs have allowed 1 sec, 5 MW pulses. ICRF loading studies have shown that loading variations are related to changes in the density pedestal height rather than the evanescent distance. With increased ICRF power, the first monster sawteeth and fundamental and second harmonic Alfven cascades were observed. The sawtooth period was found to be dependent on antenna phasing for minority absorption.

  5. Development of Advanced 9Cr Ferritic-Martensitic Steels and Austenitic Stainless Steels for Sodium-Cooled Fast Reactor

    Energy Technology Data Exchange (ETDEWEB)

    Sham, Sam [ORNL; Tan, Lizhen [ORNL; Yamamoto, Yukinori [ORNL

    2013-01-01

    Ferritic-martensitic (FM) steel Grade 92, with or without thermomechanical treatment (TMT), and austenitic stainless steels HT-UPS (high-temperature ultrafine precipitate strengthening) and NF709 were selected as potential candidate structural materials in the U.S. Sodium-cooled Fast Reactor (SFR) program. The objective is to develop advanced steels with improved properties as compared with reference materials such as Grade 91 and Type 316H steels that are currently in nuclear design codes. Composition modification and/or processing optimization (e.g., TMT and cold-work) were performed to improve properties such as resistance to thermal aging, creep, creep-fatigue, fracture, and sodium corrosion. Testings to characterize these properties for the advanced steels were conducted by the Idaho National Laboratory, the Argonne National Laboratory and the Oak Ridge National Laboratory under the U.S. SFR program. This paper focuses on the resistance to thermal aging and creep of the advanced steels. The advanced steels exhibited up to two orders of magnitude increase in creep life compared to the reference materials. Preliminary results on the weldment performance of the advanced steels are also presented. The superior performance of the advanced steels would improve reactor design flexibility, safety margins and economics.

  6. High CW power, phase and amplitude modulatorrealized with fast ferrite phase-shifters

    CERN Document Server

    Valuch, D

    2004-01-01

    Superconducting cavity resonators are suffering from detuning effects caused by high internal electromagnetic fields (Lorentz force detuning). For classical resonators working with continuous wave signals, this detuning is static and compensated by the slow mechanical tuning system. However, pulsing of superconducting cavities, an operational mode only recently considered, results in dynamic detuning effects. New ways to handle this effect have to be found and worked out. A way to supply several superconducting cavities in the particle accelerator by one large transmitter while keeping the possibility of controlling the field in each individual cavity is shown. By introducing a fast phase and amplitude modulator into each cavity feeder line, the individual deviations of each cavity with respect to the average can be compensated in order to equalize their behaviour for the main control loop, which will compensate the global detuning of all cavities. Several types of phase and amplitude modulators suitable for ...

  7. ICRF wave field measurements in the presence of scrape off layer turbulence on the ASDEX Upgrade tokamak (invited)

    Science.gov (United States)

    Ochoukov, R.; Bobkov, V.; Faugel, H.; Fünfgelder, H.; Jacquot, J.; Noterdaeme, J.-M.; Suárez López, G.

    2016-11-01

    A new array of B-dot probes was installed on ASDEX Upgrade. The purpose of the new diagnostic is to study Ion Cyclotron Range-off Frequencies (ICRF) wave field distributions in the evanescent scrape-off layer (SOL) plasma region on the low field side of ASDEX Upgrade. The vacuum measurements (no gas, BT = 0 T) reveal ICRF wave field measurements consistent with the profiles expected from the newly installed 3-strap ICRF antennas outside the antenna box: the shape of the toroidal distribution of both the amplitude and the phase is the same for the case of only the central straps being active, as for the case of only the side straps being active. These profiles become strongly modified during plasma operations. The modifications can be separated into two types: "Inter-edge localized mode (ELM)" and "During-ELM" periods. The phase distribution of the ICRF wave fields remains well-defined during the Inter-ELM period; however, it becomes more spread out over the entire 360° range during ELMs. The observed modulations cannot be explained by the observed changes in the ICRF power, as monitored in the transmission line. However, they are consistent with ICRF coupling changes introduced by plasma filaments: the plasma density perturbations due to the filaments are high enough to change the nature of the fast ICRF wave field from evanescent to propagating. The coverage of the present diagnostic is being expanded to include both the low field side and the high field side probes. Additionally, a manipulator probe head is being developed to measure ICRF wave field radial profiles across the SOL region.

  8. Integrity assessment of the ferritic / austenitic dissimilar weld joint between intermediate heat exchanger and steam generator in fast reactor

    Energy Technology Data Exchange (ETDEWEB)

    Jayakumar, T.; Laha, K.; Chandravathi, K. S.; Parameswaran, P.; Goyal, S.; Kumar, J. G.; Mathew, M. D. [Metallurgy and Materials Group, Indira Gandhi Centre for Atomic Research, Kalpakkam- 603 102 (India)

    2012-07-01

    Integrity of the modified 9Cr-1Mo / alloy 800 dissimilar joint welded with Inconel 182 electrodes has been assessed under creep condition based on the detailed analysis of microstructure and stress distribution across the joint by finite element analysis. A hardness peak at the ferritic / austenitic weld interface and a hardness trough at the inter-critical heat affected zone (HAZ) in ferritic base metal developed. Un-tempered martensite was found at the ferritic / austenitic weld interface to impart high hardness in it; whereas annealing of martensitic structure of modified 9Cr-1Mo steel by inter-critical heating during welding thermal cycle resulted in hardness tough in the inter-critical HAZ. Creep tests were carried out on the joint and ferritic steel base metal at 823 K over a stress range of 160-320 MPa. The joint possessed lower creep rupture strength than its ferritic steel base metal. Failure of the joint at relatively lower stresses occurred at the ferritic / austenitic weld interface; whereas it occurred at inter-critical region of HAZ at moderate stresses. Cavity nucleation associated with the weld interface particles led to premature failure of the joint. Finite element analysis of stress distribution across the weld joint considering the micro-mechanical strength inhomogeneity across it revealed higher von-Mises and principal stresses at the weld interface. These stresses induced preferential creep cavitation at the weld interface. Role of precipitate in enhancing creep cavitation at the weld interface has been elucidated based on the FE analysis of stress distribution across it. (authors)

  9. Plasma-surface interactions with ICRF antennas and lower hybrid grills in Tore Supra

    Science.gov (United States)

    Harris, J. H.; Hutter, T.; Hogan, J. T.; Basiuk, V.; Beaumont, B.; Becoulet, A.; Bremond, S.; Carter, M. D.; Goniche, M.; Goulding, R. H.; Guilhem, D.; Haste, G. R.; Hoffman, D. J.; Litaudon, X.; Nguyen, F.

    1997-02-01

    The edge plasma interactions of the actively cooled radio-frequency heating launchers in Tore Supra ion-cyclotron range of frequencies (ICRF) antennas and lower-hybrid (LH) grills are studied using infrared video imaging. On the two-strap ICRF antennas, operated in fast-wave electron heating or current drive mode, hot spots with temperatures of 500-900°C are observed by the end of 2 s power pulses of 2 MW per antenna. The steady-state temperature distribution is determined principally by the relative phase of the two antenna straps: dipole (heating) phasing results in significantly less antenna heating than does 90° (current drive) phasing. Transient heat fluxes of 1-20 MW/m 2 are measured on the lateral protection bumpers at ICRF turn-on; these fluxes are primarily a function of plasma and radio frequency (rf) control. The remarkable feature of the lower hybrid edge interaction is the production of beams of heat flux in front of the grills; these beams propagate along the helical magnetic field lines and can deliver fluxes of 5-10 MW/m 2 over areas of several cm 2 to plasma-facing components. Both the ICRF and LH phenomena appear to result from the acceleration of particles by the near fields of the launchers. Modeling of the heat flux deposition on components and its relation to sputtering processes is presented.

  10. Mode conversion in three ion species ICRF heating scenario

    Science.gov (United States)

    Lin, Y.; Edlund, E.; Ennever, P.; Porkolab, M.; Wright, J.; Wukitch, S.

    2016-10-01

    Three-ion species ICRF heating has been studied on Alcator C-Mod and on JET. It has been shown to heat the plasma and generate energetic particles. In a typical three-ion scenario, the plasma consists of 60-70% D, 30-40% H and a trace level (1% or less) of 3He. This species mixture creates two hybrid resonances (D-3He and 3He-H) in the plasma, in the vicinity of the 3He IC resonance (on both sides). The fast wave can undergo mode conversion (MC) to ion Bernstein waves and ion cyclotron waves at the two hybrid resonances. A phase contrast imaging (PCI) system has been used to measure the RF waves in the three-ion heating experiment. The experimentally measured MC locations and the separating distance between the two MC regions help to determine the concentration of the three species. The PCI signal amplitudes for the RF waves are found to be sensitive to RF and plasma parameters, including PRF, Te, ne and also the species mix concentration. The parameter dependences found in the experiment will be compared with ICRF code simulations. Supported by USDoE Awards DE-FC02-99ER54512 and DE-FG02-94-ER54235.

  11. 3D electromagnetic theory of ICRF multi PORT multi loop antenna

    Energy Technology Data Exchange (ETDEWEB)

    Vdovin, V.L.; Kamenskij, I.V.

    1997-01-01

    In this report the theory of three dimensional antenna in Ion Cyclotron Resonance Frequency (ICRF) is developed for a plasma with circular magnetic surfaces. The multi loop antenna is located in ITER several ports. Circular plasma and antenna geometry provides new important tools to account for: (1) right loading antenna impedance matrix calculation urgently needed for a matching of RF generator with an antenna; (2) right calculation of an antenna toroidal and poloidal excited spectra because the DIFFRACTION, refraction and REFLECTION effects for the Fast Waves (FW) are in FIRST time are included self consistently in 3D ICRF antenna - plasma treatment; (3) right calculation of RF power deposition profiles because self consistently found 3D antenna - plasma FW excited spectra in non slab plasma model are important ones in a weakly dissipated plasma for Fast Waves (even for ITER parameters). (J.P.N.)

  12. ICRF antenna modeling and simulation. Final report, March 1, 1993--May 31, 1996

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    1996-08-30

    SAIC has undergone a three year research and development program in support of the DOE Office of Fusion Energy`s (OFE) program in Ion Cyclotron Range of Frequencies (ICRF) heating of present, next generation, and future plasma fusion devices. The effort entailed advancing theoretical models and numerical simulation technology of ICRF physics and engineering issues associated predominately with, but not limited to, tokamak Ion Cyclotron Heating (ICH) and fast wave current drive (FWCD). Ion cyclotron heating and current drive is a central element in all current and planned large fusion experiments. In recent years, the variety of uses for ICRF systems has expanded, and includes the following: (1) Heating sufficient to drive plasma to ignition. (a) Second-harmonic T heating. (b) He{sup 3} minority heating. (2) Second-harmonic He{sup 4} heating in H plasma (for non-activated phase). (3) Detailed equilibrium profile control minority heating. (a) Ion minority (He{sup 3}) CD (for profile control on inside of plasma). (b) Ion minority (He{sup 3}) CD (for profile control on outside of plasma). (4) Ion-ion hybrid regime majority ion heating. (5) Electron current drive. (6) Mode conversion to drive current. (7) Deuterium minority heating. (8) Sawtooth instability stabilization. (9) Alpha particle parameter enhancement. (10) The generation of minority tails by ICRF to simulate D-T plasma particle physics in a deuterium plasma. Optimization of ICRF antenna performance for either heating or current drive depends critically on the complex balance and interplay between the plasma physics and the electromechanical system requirements. For example, ITER IC rf designs call for an IC. system frequency range from 20 MHz to 100 MHz. Additionally, antenna designs and operational modes that minimize impurity production and induced sheath formation may degrade current drive efficiency. Such effects have been observed in experiments involving it versus zero antenna phasing.

  13. Overview of Results from the Upgraded ICRF System on Alcator C-Mod

    Science.gov (United States)

    Schilling, G.; Wukitch, S. J.; Bonoli, P. T.; Boivin, R. L.; Fiore, C.; Goetz, J. A.; Hubbard, A.; Hutchinson, I. H.; Lee, W. D.; Marmar, E.; Mazurenko, A.; Nelson-Melby, E.; Porkolab, M.; Rice, J.; Hosea, J.; Perkins, F. W.; Phillips, C. K.; Taylor, G.; White, R.; Wilson, J. R.

    2000-10-01

    Alcator C-Mod's ICRF program has added to existing physics studies and generated new physics results. Simulations of mode conversion physics using the full-wave code TORIC are in good agreement with experimental measurements of electron power deposition profiles. Phase contrast imaging has detected density fluctuations associated with the propagation of the launched fast wave and also ion Bernstein waves in the plasma core. During experiments to measure toroidal rotation, a core transport barrier was observed in addition to the edge H-mode barrier with the minority ion resonance on the high-field side of the axis. Initial operation of the PPPL 4-strap ICRF antenna was hindered by impurity generation problems and antenna arcing which were largely eliminated by improvements made in January 2000. Subsequently, more than 3 MW of power have been launched into plasma. A closed-box configuration for this antenna will be tested.

  14. Vienna Contribution to the ICRF3

    Science.gov (United States)

    Mayer, David; Krásná, Hana; Böhm, Johannes

    2016-12-01

    The current realization of the ICRS, the ICRF2, was published in 2009. New stations were implemented, and the amount of data from the southern hemisphere increased dramatically. The demands on the accuracy of the celestial reference frame are higher than ever, with the GAIA mission providing a catalog in the visible spectrum with comparable accuracy. These advances in VLBI and new demands on accuracy entail the necessity of a new version of the celestial reference frame which will be called ICRF3. We will report on the progress and plans of the Vienna group to estimate such a reference frame. Differences in our solution (especially in declination) compared to other groups are discussed. Furthermore, we examine issues which arise during the estimation process such as a declination bias (a maximal offset of about 150 μas in declination).

  15. Fast synthesis of rare-earth (Pr{sup 3+}, Sm{sup 3+}, Eu{sup 3+} and Gd{sup 3+}) doped bismuth ferrite powders with enhanced magnetic properties

    Energy Technology Data Exchange (ETDEWEB)

    Iorgu, A.I. [Department of Chemical Thermodynamics, “Ilie Murgulescu” Institute of Physical Chemistry, 060021 Bucharest (Romania); Department of Inorganic Chemistry, Physical Chemistry and Electrochemistry, University “Politehnica” of Bucharest, 011061 Bucharest (Romania); Maxim, F., E-mail: fmaxim@icf.ro [Department of Chemical Thermodynamics, “Ilie Murgulescu” Institute of Physical Chemistry, 060021 Bucharest (Romania); Matei, C. [Department of Inorganic Chemistry, Physical Chemistry and Electrochemistry, University “Politehnica” of Bucharest, 011061 Bucharest (Romania); Ferreira, Liliana Pires [Centro de Física da Matéria Condensada, Faculdade de Ciências, Universidade de Lisboa, Campo Grande, 1749-016 Lisboa (Portugal); Department of Physics, University of Coimbra, 3004-516 Coimbra (Portugal); Ferreira, P. [Department of Materials and Ceramics Engineering, CICECO, Universidade de Aveiro, 3810-193 Aveiro (Portugal); Cruz, M.M. [Centro de Física da Matéria Condensada, Faculdade de Ciências, Universidade de Lisboa, Campo Grande, 1749-016 Lisboa (Portugal); Departamento de Física, Faculdade de Ciências, Universidade de Lisboa, Campo Grande, 1749-016 Lisboa (Portugal); Berger, D., E-mail: danaberger01@yahoo.com [Department of Inorganic Chemistry, Physical Chemistry and Electrochemistry, University “Politehnica” of Bucharest, 011061 Bucharest (Romania)

    2015-04-25

    Highlights: • Synthesis of rare earth doped bismuth ferrite powders by combustion method. • SEM and TEM were used to investigate the morphology and size of particles. • Effect of Bi substitution with Pr, Sm, Eu and Gd on magnetic properties of powders. - Abstract: Rare-earth (Pr{sup 3+}, Sm{sup 3+}, Eu{sup 3+} and Gd{sup 3+}) doped bismuth ferrite powders were synthesized for the first time by solution combustion method, which is a fast soft chemistry route for obtaining oxide powders. The materials were investigated by X-ray diffraction, Raman spectroscopy, as well as scanning and transmission electron microscopy. A distortion from rhombohedral R3c symmetry, specific to pure bismuth ferrite, to orthorhombic symmetry was observed for all doped samples. The SEM analysis of pure and doped bismuth ferrite powders showed the formation of sintered grains, with faceted cuboids-shaped particles with different size and lower average dimension in the case of doped samples. Magnetic properties were analyzed using SQUID magnetometry, M–H hysteresis loops being measured at 10 K and 300 K. All studied pure and doped bismuth ferrite samples presented high susceptibility values for high magnetic fields indicating strong antiferromagnetic interactions, whereas the behavior at low magnetic field demonstrates the existence of ferromagnetic coupling. Compared to BiFeO{sub 3}, Bi{sub 0.9}RE{sub 0.1}FeO{sub 3} (RE = Pr, Sm, Eu and Gd) powders exhibit higher susceptibility, remanence and coercivity values, Bi{sub 0.9}Eu{sub 0.1}FeO{sub 3} sample displaying the highest remanence and coercivity at room temperature.

  16. Ferrite Solutions for Electromagnetic Shock Lines

    Energy Technology Data Exchange (ETDEWEB)

    Coleman, Phillip D. [Sandia National Lab. (SNL-NM), Albuquerque, NM (United States); Dudley, Mark [Sandia National Lab. (SNL-NM), Albuquerque, NM (United States); Primm, Paul [Sandia National Lab. (SNL-NM), Albuquerque, NM (United States)

    2014-09-01

    The goal of this work is to develop tools and test procedures for identifying ferrites suitable for use in shock line applications. Electromagnetic shocklines have been used to provide fast rising voltage pulses for many applications. In these applications a slow rising pulse is injected into the line where currents drive the ferrites into saturation leading to a fast rising output pulse. A shockline’s unique capabilities could be applied to new detonator configurations. A properly conditioned voltage pulse is critical for fire set applications. A carefully designed shockline could provide a passive solution to generating a fast rising voltage pulse for the fire set. Traditional circuits use ferrites operating in a linear regime. Shock lines push the ferrites well into the nonlinear regime where very few tools and data currently exist. Ferrite material is key to the operation of these shock lines, and tools for identifying suitable ferrites are critical. This report describes an experimental setup to that allows testing of ferrite samples and comparison to models with the goal of identifying optimal ferrites for shockline use.

  17. 15-MeV proton emission from ICRF-heated plasmas

    Energy Technology Data Exchange (ETDEWEB)

    Jarvis, O.N.; Conroy, S.W.; Hone, M.; Sadler, G.J.; Van Belle, P. [Commission of the European Communities, Luxembourg (Luxembourg)

    1994-07-01

    {sup 3} He-d fusion reaction protons emitted from ICRF-heated discharges were recorded with a silicon diode detector installed in the JET tokamak. The detection rates demonstrated that sawtooth crashes eject fast particles from the inner region of the plasma. The energy spectra of the fusion product protons using H minority provided evidence for the second harmonic acceleration of deuterons at sub-MW levels of RF power and those with {sup 3} He minority did not possess the expected twin-lobed shape predicted by kinematics calculations. (authors). 5 refs., 6 figs.

  18. Recent ICRF results on Alcator C-Mod

    Science.gov (United States)

    Wukitch, S. J.; Boivin, R. L.; Bonoli, P. T.; Fiore, C.; Greenwald, M.; Goetz, J. A.; Hosea, J.; Hubbard, A.; Hutchinson, I. H.; Irby, J.; Lee, W. D.; Marmar, E.; Mazurenko, A.; Nelson-Melby, E.; Phillips, C. K.; Porkolab, M.; Rice, J.; Schilling, G.; Wilson, J. R.; Wolfe, S. M.

    2001-10-01

    Internal transport barrier (ITB) modes have been observed with intense, off-axis ICRF heating in Alcator C-Mod. This barrier mode is routinely produced in enhanced Dα H-mode, 4.5 T, 0.8 MA discharges (H cyclotron position is r/a˜0.5 to the high field side). From TRANSP analysis, the χeff is significantly reduced inside r/a˜0.4 where the density peaking is observed. With the barrier formation, the toroidal plasma rotation near the axis reversed from co-current (+50 km/sec) to counter current direction (-20 km/sec). In an effort to maintain the barrier, experiments utilizing a third antenna, operated at 70 MHz, allowed central ICRF heating of the ITB mode. Initial experiments with up to 1.2 MW confirmed the energy transport barrier and allowed significant increase in the ion temperatures. With the central heating, the ITB was sustained and the density and impurity peaking were arrested. Furthermore, the central rotation was observed to rotate in the co-current direction with the central heating. We have also had success in detecting electron density fluctuations at the RF frequency with a heterodyned phase contrast imaging diagnostic. The fast wave was observed with peaked density profiles and the measured wave number was in reasonable agreement with the cold plasma dispersion relationship. The mode-converted ion Bernstein wave (IBW) has also been observed in H (3He,D) plasmas The measured wave number is in good agreement with the hot plasma dispersion relationship and indicates the wave is a backward wave as expected from the dispersion relationship, Simulations, utilizing the full wave code TORIC have been critical to this analysis. TORIC has recently been upgraded to allow for higher poloidal mode number resolution. The predicted electron absorbed power more accurately reflects the measured values. Recent success in commissioning a 4-strap (J-port) antenna has allowed the maximum injected power to reach 2.5 MW from this antenna. To obtain this power, some

  19. Three dimensional modelling of ICRF launchers for fusion devices

    Science.gov (United States)

    Carter, M. D.; Rasmussen, D. A.; Ryan, P. M.; Hanson, G. R.; Stallings, D. C.; Batchelor, D. B.; Bigelow, T. S.; England, A. C.; Hoffman, D. J.; Murakami, M.; Wang, C. Y.; Wilgen, J. B.; Rogers, J. H.; Wilson, J. R.; Majeski, R.; Schilling, G.

    1996-02-01

    The three dimensional (3-D) nature of antennas for fusion applications in the ion cyclotron range of frequencies (ICRF) requires accurate modelling to design and analyse new antennas. In this article, analysis and design tools for radiofrequency (RF) antennas are successfully benchmarked with experiment, and the 3-D physics of the launched waves is explored. The systematic analysis combines measured density profiles from a reflectometer system, transmission line circuit modelling, detailed 3-D magnetostatics modelling and a new 3-D electromagnetic antenna model including plasma. This analysis gives very good agreement with measured loading data from the Tokamak Fusion Test Reactor (TFTR) Bay-M antenna, thus demonstrating the validity of the analysis for the design of new RF antennas. The 3-D modelling is contrasted with 2-D models, and significant deficiencies are found in the latter. The 2-D models are in error by as much as a factor of 2 in real and reactive loading, even after they are corrected for the most obvious 3-D effects. Three dimensional effects play the most significant role at low parallel wavenumbers, where the launched power spectrum can be quite different from the predictions of 2-D models. Three dimensional effects should not be ignored for many RF designs, especially those intended for fast wave current drive

  20. Influence of the plasma on ICRF antenna voltage limits

    Science.gov (United States)

    Bobkov, V.; Noterdaeme, J.-M.; Wesner, F.; Wilhelm, R.; ASDEX Upgrade Team

    2003-03-01

    An ion cyclotron range of frequencies (ICRF) probe [F.W. Baity, G.C. Barber, V. Bobkov, R.H. Goulding, J.-M. Noterdaeme, D.W. Swain, in: 14th Topical Conference on Radiofrequency Power in Plasmas, Oxnard 2001, AIP Conference Proceedings 595, AIP, Melville, NY, 2001, p. 510] has been implemented to study voltage stand-off of the ICRF antennas on ASDEX Upgrade (AUG). The probe was operated at first in a test stand where features of high RF voltage operation in vacuum and plasma created by an ion source of the Hall type [Plasma Sources Sci. Technol. 8 (1999) R1] were studied. Vacuum arcs as well as ignition of high voltage glow discharge are candidate processes to explain voltage limits of the ICRF antennas. The setup on AUG was used to expose high RF voltages in real conditions of the tokamak scrape-off layer which are faced by the ICRF antennas. It is found that high voltage breakdown on the ICRF antenna is often correlated with ELM activity. The maximal RF voltage increased from shot to shot, i.e. the conditioning effect is observed. For the good-conditioned ICRF probe it was shown experimentally that the voltage limit can be increased while the rectified current is suppressed at the same time.

  1. Power Compensation for ICRF Heating in EAST

    Science.gov (United States)

    Chen, Gen; Qin, Chengming; Mao, Yuzhou; Zhao, Yanping; Yuan, Shuai; Zhang, Xinjun

    2016-08-01

    The source system covering a working frequency range of 24 MHz to 70 MHz with a total maximum output power of 12 MW has already been fabricated for Ion Cyclotron Range of Frequency (ICRF) heating in EAST from 2012. There are two continuous wave (CW) antennas consisting of four launching elements each fed by a separate 1.5 MW transmitter. Due to the strong mutual coupling among the launching elements, the injection power for launching elements should be imbalance to keep the k‖ (parallel wave number) spectrum of the launcher symmetric for ICRF heating. Cross power induced by the mutual coupling will also induce many significant issues, such as an uncontrollable phase of currents in launching elements, high voltage standing wave ratio (VSWR), and impedance mismatching. It is necessary to develop a power compensation system for antennas to keep the power balance between the feed points. The power balance system consists of two significant parts: a decoupler and phase control. The decoupler helps to achieve ports isolation to make the differential phase controllable and compensate partly cross power. After that, the differential phase of 0 or π will keep the power balance of two feed points completely. The first power compensation system consisting of four decouplers was assembled and tested for the port B antenna at the working frequency of 35 MHz. With the application of the power compensation system, the power balance, phase feedback control, and voltage standing wave ratio (VSWR) had obviously been improved in the 2015 EAST campaign. supported by the National Magnetic Confinement Fusion Science Program of China (No. 2015GB101001) and National Natural Science Foundation of China (Nos. 11575237, 11375235, 11375236)

  2. The Fine-scale Structure of the Radial Electric Field in the Scrape-Off-Layer during ICRF Heating in Alcator C-Mod

    Science.gov (United States)

    Terry, J. L.; Cziegler, I.; Wukitch, S. J.; Lin, Y.; Zweben, S. J.

    2011-10-01

    By observing the radial structure in the poloidal dynamics of the SOL turbulence, we find a fine-scale radial structure in the broadband turbulence poloidal phase velocities (Vθ) with the application of ICRF power (PRF > 0.6 MW). The radial profiles are very different from typical profiles in Ohmic plasmas. Since Vθ(r) in the SOL is dominated by VExB, this structure implies a fine-scale Er profile is formed in the presence of the ICRF. The existence of such spatial structure is not predicted to be a result of the ICRF since the radial size-scale is much smaller than the fast-wave perpendicular wavelength (~10 cm). Such an Er profile may help to explain the increased impurity content observed with ICRF heating and will be important for SOL flows and transport. Using 2D Gas-Puff-Imaging we find that, in the ~3 cm region outside the separatrix, the dominant propagation direction for Vθ reverses up to 3 times. This is found beyond the region where the antenna near-fields are present; the fast wave is propagating there. While the mechanism is still unknown, it must be consistent with the following: the structure is dependent on which antenna is energized; it changes with q95 and is present when the RF frequency is 78 or 50 MHz. Supported by USDoE awards DE-FC02-99ER54512 and DE-AC02-09CH11466.

  3. Development and test of decoupler for ICRF antenna in EAST

    Energy Technology Data Exchange (ETDEWEB)

    Chen, Gen, E-mail: chengen@ipp.ac.cn; Mao, Yuzhou; Zhao, Yanping; Yuan, Shuai; Zhang, Xinjun; Qing, Chengming

    2016-06-15

    Highlights: • The mechanism of decoupler for ICRF antenna is proposed. • Three candidate assembly positions for the decouper can be used. • The performance relies on the ohmic dissipation and the assembly position of decoupler. - Abstract: Ion Cyclotron Range of Frequency (ICRF) heating has been adopted in EAST tokamak as one of main auxiliary heating methods. The ICRF antenna usually consists of multiple launching elements because of limited port and space of tokamak device. Mutual coupling between straps has been observed in previous EAST ICRF current drive experiments. Due to adverse effects of such mutual coupling, many issues induced by cross power cannot be ignored, such as power imbalance in feed lines, high voltage standing wave ratio (VSWR), and etc. To restrain such mutual coupling, A device named decoupler was developed and tested in EAST ICRF system. According to the admittance matrix of load, three assembly positions (oscillation position, optimum position, and smooth position) along transmission line for the decoupler were taken into account and tested. The test results showed that ohmic dissipation in decoupler could not be neglected, which partly influenced the decoupling performance. The oscillation position and optimum position could restrain such adverse effects of ohmic dissipation and showed good decoupling performance. However, they cannot ensure the steady operation during H-mod due to the load variation. Finally, the smooth position has been adopted for EAST I port antenna because of steady decoupling performance comprised with engineering error and load resilience, which sincerely enhance the capability of system operation.

  4. ICRF heating of deuterium-tritium plasmas in TFTR

    Energy Technology Data Exchange (ETDEWEB)

    Taylor, G.; Murakami, M.; Adler, H.

    1995-03-01

    The first experiments to heat D-T plasmas in the ion cyclotron range of frequencies (ICRF) have been performed on the Tokamak Fusion Test Reactor (TFTR). These experiments have two major objectives: to study the RF physics of ICRF-heated D-T plasmas and to enhance the performance of D-T discharges. Experiments have been conducted at 43 MHz with out-of-phase current strap excitation to explore n{sub T}/n{sub e} concentrations up to approximately 40%. In these experiments n{sub T}/n{sub e} was limited by D recycling from the carbon walls. The location of the T resonance was varied by changing the toroidal magnetic field, and the RF power was modulated (f{sub mod}=5-10 Hz) to elucidate competing heating mechanisms. Up to 5.8 MW of ICRF heating has been coupled into D-T plasmas. The addition of 5.5 MW of ICRF heating to a D-T supershot resulted in an increase in central ion temperature from 26 to 36 keV and an increase in central electron temperature from 8 to 10.5 keV. Up to 80% of the absorbed ICRF power was coupled directly to ions, in good agreement with computer code predictions. These results extrapolate to efficient T heating in future devices such as ITER.

  5. EDITORIAL: Special section on the physics and technology of plasma heating by ICRF power

    Science.gov (United States)

    Noterdaeme, Jean-Marie; Van Eester, Dirk

    2006-07-01

    This special section brings together much of what is currently at the forefront of ion cyclotron resonance frequency (ICRF) research. Which theories are people working on? Where is progress being made? What results are being obtained? The present Nuclear Fusion section on ICRF is not—and was explicitly meant not to be—an overview or review of ICRF systems, research achievements or theories. It is more a snapshot of the leading edge of the investigations. It is based, in part, on presentations to the 16th Topical Conference on RF Power in Plasmas, Park City, Utah, USA, April 2005. The forefront of ICRF research currently being actively pursued covers a wide range of topics: theoretical, experimental and technological. As can be expected, most of the papers in this section have direct relevance to ITER. Elements that will be important in ITER, and that are being addressed and developed in the papers, are the presence of fast particles with their influence on wave propagation and damping, the non-linear mechanisms in the edge—in particular close to the wave launcher—and steady-state aspects. Specific ITER components as well as RF scenarios are studied. Continued efforts to improve the analytical description of wave damping and absorption and the availability of gradually more powerful computers led to significant progress in incorporating the effect of particles with non-thermal velocity distributions—the presence of which has already become significant in present-day machines due to massive RF and/or NBI heating which forces the particles away from thermo-dynamical equilibrium (Brambilla et al, Jaeger et al). The exact role that RF-created and fusion-born fast particles will play is still a matter of lively debate. As shown in the papers by Choi et al and Pinsker et al, the presence of energetic particles is a significant factor in the wave absorption, even at high harmonics. Accounting for the actual magnetic topology allows the capture of RF induced

  6. A new electromagnetic code for ICRF antenna in EAST

    CERN Document Server

    Yang, Hua; Dong, Sa; Zhang, Xin-Jun; Zhao, Yan-Ping; Shang, Lei

    2015-01-01

    The demand for an effective tool to help in the design of ion cyclotron radio frequency (ICRF) antenna system for fusion experiment has driven the development of predictive codes. A new electromagnetic code based on the method of moments (MOM) is described in the paper. The code computes the electromagnetic field by the solution of the electric field integral equation. The structure of ICRF antennas are discretized with triangular mesh. By using the new code, the scattering parameter and the surface current are given and compared with the result by commercial code CST. Moreover, the power spectra are studied with different toroidal phases for heating and current drive. Good agreement of simulation results between the new code and CST are obtained. The code has been validated against CST for EAST ICRF antenna.

  7. Microwave reflectometry for ICRF coupling studies on TFTR

    Science.gov (United States)

    Wilgen, J. B.; Hanson, G. R.; Bigelow, T. S.; Batchelor, D. B.; Collazo, I.; Hoffman, D. J.; Murakami, M.; Rasmussen, D. A.; Stallings, D. C.; Raftopoulos, S.; Wilson, J. R.

    1994-10-01

    A dual-frequency differential-phase reflectometer has been developed for use in ICRF power coupling studies on TFTR. This system has been optimized for measurements of the electron density profile in the edge-gradient region, where density fluctuations are large. Initial proof-of-principle measurements demonstrate that this is an effective way to measure the electron density profile in the plasma-edge region. A new reflectometer launcher is presently being installed on the center axis of the bay-K ICRF antenna on TFTR, along with the associated waveguide transmission line. This will allow direct measurement of the edge-density profile within the high-power-density environment of the ICRF antenna where density profile modification might be expected.

  8. Microwave reflectometry for ICRF coupling studies on TFTR

    Energy Technology Data Exchange (ETDEWEB)

    Wilgen, J.B.; Hanson, G.R.; Bigelow, T.S.; Batchelor, D.B.; Collazo, I.; Hoffman, D.J.; Murakami, M.; Rasmussen, D.A.; Stallings, D.C. (Oak Ridge National Laboratory, Oak Ridge, Tennessee 37831-8072 (United States)); Raftopoulos, S.; Wilson, J.R. (Plasma Physics Laboratory, Princeton University, P.O. Box 451, Princeton, New Jersey 08543 (United States))

    1994-10-15

    A dual-frequency differential-phase reflectometer has been developed for use in ICRF power coupling studies on TFTR. This system has been optimized for measurements of the electron density profile in the edge-gradient region, where density fluctuations are large. Initial proof-of-principle measurements demonstrate that this is an effective way to measure the electron density profile in the plasma-edge region. A new reflectometer launcher is presently being installed on the center axis of the bay-K ICRF antenna on TFTR, along with the associated waveguide transmission line. This will allow direct measurement of the edge-density profile within the high-power-density environment of the ICRF antenna where density profile modification might be expected.

  9. Microwave reflectometry for ICRF coupling studies on TFTR

    Energy Technology Data Exchange (ETDEWEB)

    Wilgen, J.B.; Bigelow, T.S.; Batchelor, D.B.; Hoffman, D.J.; Murakami, M.; Rasmussen, D.A.; Stallings, D.C. [Oak Ridge National Lab., TN (United States); Hanson, G.R. [Oak Ridge Associated Universities, Inc., TN (United States); Collazo, I. [Georgia Inst. of Tech., Atlanta, GA (United States); Raftopoulos, S.; Wilson, J.R. [Princeton Univ., NJ (United States). Plasma Physics Lab.

    1993-06-01

    A dual-frequency differential-phase reflectometer has been developed for use in ICRF power coupling studies on TFTR. This system has been optimized for measurements of the electron density profile in the edge-gradient region, where density fluctuations are large. Initial proof-of-principle measurements demonstrate that this is an effective way to measure the electron density profile in the plasma-edge region. A new reflectometer launcher is presently being installed on the center axis of the bay-K ICRF antenna on TFTR, along with the associated waveguide transmission line. This will allow direct measurement of the edge-density profile within the high-power-density environment of the ICRF antenna where density modification might be expected.

  10. Benchmarking ICRF Full-wave Solvers for ITER

    Energy Technology Data Exchange (ETDEWEB)

    R. V. Budny, L. Berry, R. Bilato, P. Bonoli, M. Brambilla, R. J. Dumont, A. Fukuyama, R. Harvey, E. F. Jaeger, K. Indireshkumar, E. Lerche, D. McCune, C. K. Phillips, V. Vdovin, J. Wright, and members of the ITPA-IOS

    2011-01-06

    Abstract Benchmarking of full-wave solvers for ICRF simulations is performed using plasma profiles and equilibria obtained from integrated self-consistent modeling predictions of four ITER plasmas. One is for a high performance baseline (5.3 T, 15 MA) DT H-mode. The others are for half-field, half-current plasmas of interest for the pre-activation phase with bulk plasma ion species being either hydrogen or He4. The predicted profiles are used by six full-wave solver groups to simulate the ICRF electromagnetic fields and heating, and by three of these groups to simulate the current-drive. Approximate agreement is achieved for the predicted heating power for the DT and He4 cases. Factor of two disagreements are found for the cases with second harmonic He3 heating in bulk H cases. Approximate agreement is achieved simulating the ICRF current drive.

  11. Investigations of the boundary conditions of acicular ferrite formation in fast-quenched welded materials. Final report; Untersuchungen der Randbedingungen fuer die Bildung von 'acicular ferrite' in Schweissguetern bei schneller Abkuehlung. Schlussbericht

    Energy Technology Data Exchange (ETDEWEB)

    Dilthey, U.; Biesenbach, M.

    2000-06-19

    The authors investigated the boundary conditions in which a fine-grained ferritic needle structure with sufficient low-temperature toughness is obtained in conditions of extreme heating and cooling. Alloy compositions and welding boundary conditions were investigated for laser welding, electron beam welding in a vacuum and electron beam welding at atmospheric pressure. [German] Im Rahmen dieser Arbeit soll untersucht werden, welche Randbedingungen erfuellt sein muessen, damit sich unter extremen Aufheiz- und Abkuehlbedingungen, wie sie bei den Strahlschweissverfahren vorliegen, ein feinkoerniges nadelferritisches Gefuege mit ausreichend hoher Tieftemperaturzaehigkeit bildet. Diesbezueglich ist fuer die Strahlschweissverfahren Laserstrahlschweissen, Elektronenstrahlschweissen im Vakuum und Elektronenstrahlschweissen unter Atmosphaerendruck zu ermitteln, welche Legierungszusammensetzungen diese Voraussetzungen erfuellen und wie sie unter realen Schweissbedingungen verwirklicht werden koennen. (orig.)

  12. Design and Analysis of the Alcator C-Mod Two-Strap ICRF Antenna

    Science.gov (United States)

    Takase, Y.; Golovator, S. N.; Porkolab, M.; Bajwa, K.; Becker, H.; Caldwell, D.

    1992-01-01

    ICRF fast wave heating with up to 8 MW of rf power at 80 MHz is planned on the Alcator C-MOD tokamak (R=0.665 m, a=0.21 m, κ=1.8, B≤9 T, I≤3 MA). During the initial tokamak operation, a movable single-strap antenna will be used to ensure operational flexibility. The second ICRF antenna, which is currently under construction, has two current straps which can be driven out-of-phase to improve the heating efficiency and minimize impurity generation. The current straps are mechanically isolated from the 4` feedthroughs. The Faraday shield consists of a single layer of circular cross section rods which are slanted at 10° to horizontal to approximately align with the field line over a wide range of operating conditions. The antenna box is protected by TiC coated TZM (Molybdenum alloy) tiles arranged in a ``picture-frame'' fashion. These tiles can be replaced with tiles made of a lower Z material. Because of its larger size, the two-strap antenna must be assembled inside the vacuum chamber and attached to the wall of the vacuum vessel to support against larger disruption loads. The rf thermal loads are significantly lower for the same total power (2 MW per antenna), which allows a longer pulse (10 sec) operation.

  13. Bulk ion heating with ICRF waves in tokamaks

    Energy Technology Data Exchange (ETDEWEB)

    Mantsinen, M. J., E-mail: mervi.mantsinen@bsc.es [Catalan Institution for Research and Advanced Studies, Barcelona (Spain); Barcelona Supercomputing Center, Barcelona (Spain); Bilato, R.; Bobkov, V. V.; Kappatou, A.; McDermott, R. M.; Odstrčil, T.; Tardini, G.; Bernert, M.; Dux, R.; Maraschek, M.; Noterdaeme, J.-M.; Ryter, F.; Stober, J. [Max-Planck-Institut für Plasmaphysik, Garching (Germany); Nocente, M. [Dipartimento di Fisica “G. Occhialini”, Università degli Studi di Milano-Bicocca, Milano (Italy); Istituto di Fisica del Plasma “P. Caldirola”, CNR, Milano (Italy); Hellsten, T. [Dept. of Fusion Plasma Physics, EES, KTH, Stockholm (Sweden); Mantica, P.; Tardocchi, M. [Istituto di Fisica del Plasma “P. Caldirola”, CNR, Milano (Italy); Nielsen, S. K.; Rasmussen, J.; Stejner, M. [Technical University of Denmark, Department of Physics, Lyngby (Denmark); and others

    2015-12-10

    Heating with ICRF waves is a well-established method on present-day tokamaks and one of the heating systems foreseen for ITER. However, further work is still needed to test and optimize its performance in fusion devices with metallic high-Z plasma facing components (PFCs) in preparation of ITER and DEMO operation. This is of particular importance for the bulk ion heating capabilities of ICRF waves. Efficient bulk ion heating with the standard ITER ICRF scheme, i.e. the second harmonic heating of tritium with or without {sup 3}He minority, was demonstrated in experiments carried out in deuterium-tritium plasmas on JET and TFTR and is confirmed by ICRF modelling. This paper focuses on recent experiments with {sup 3}He minority heating for bulk ion heating on the ASDEX Upgrade (AUG) tokamak with ITER-relevant all-tungsten PFCs. An increase of 80% in the central ion temperature T{sub i} from 3 to 5.5 keV was achieved when 3 MW of ICRF power tuned to the central {sup 3}He ion cyclotron resonance was added to 4.5 MW of deuterium NBI. The radial gradient of the T{sub i} profile reached locally values up to about 50 keV/m and the normalized logarithmic ion temperature gradients R/LT{sub i} of about 20, which are unusually large for AUG plasmas. The large changes in the T{sub i} profiles were accompanied by significant changes in measured plasma toroidal rotation, plasma impurity profiles and MHD activity, which indicate concomitant changes in plasma properties with the application of ICRF waves. When the {sup 3}He concentration was increased above the optimum range for bulk ion heating, a weaker peaking of the ion temperature profile was observed, in line with theoretical expectations.

  14. Using radio stars to link ICRF and GCRF reference frames

    CERN Document Server

    Malkin, Zinovy

    2016-01-01

    One of the possible strategies for linking the optical Gaia Celestial Reference Frame (GCRF) to the VLBI-based International Celestial Reference Frame (ICRF) is using radio stars in a manner similar to that used for linking HIPPARCOS Celestial Reference System (HCRF) to ICRF. A reachable precision of the orientation angles between GCRF and ICRF frames was estimated through Monte Carlo simulation. Supposing the radio stars position uncertainty obtained by VLBI in the range of 0.1 to 4 mas, and Gaia position uncertainty in the range of 0.055 to 0.4 mas, depending in the first place on the brightness of radio star in radio and optics and number of VLBI observations, the orientation angles uncertainty will be 0.02 to 0.66 mas for 46 radio stars used, and 0.01 to 0.39 mas for 138 radio stars used. Properly organized VLBI observing program on radio stars observations can allow to tie GCRF to ICRF with the accuracy better than 0.1 mas.

  15. Bulk Ion Heating with ICRF Waves in Tokamaks

    DEFF Research Database (Denmark)

    Mantsinen, M. J.; Bilato, R.; Bobkov, V. V.

    2015-01-01

    Heating with ICRF waves is a well-established method on present-day tokamaks and one of the heating systems foreseen for ITER. However, further work is still needed to test and optimize its performance in fusion devices with metallic high-Z plasma facing components (PFCs) in preparation of ITER a...

  16. MW-scale ICRF plasma heating using IGBT switches in a multi-pulse scheme

    Science.gov (United States)

    Be'ery, I.; Kogan, K.; Seemann, O.

    2015-06-01

    Solid-state silicon switches are cheap and reliable option for 1-10 MHz RF power sources, required for plasma ion cyclotron RF heating (ICRF). The large `on' resistance of MOSFET and similar devices limits their power delivery to a few tens of kW per switch. Low resistivity devices, such as IGBT, suffer from large `off' switching time, which limits their useful frequency range and increases the power dissipated in the switch. Here we demonstrate more than 0.8 MW circulated RF power at 2 MHz using only three high voltage IGBT switches. The circuit uses the fast `on' switching capability of the IGBTs to generate high-Q pulse train. This operation mode also simplifies the measurement of RF coupling between the antenna and the plasma.

  17. Ferrites and ceramic composites

    CERN Document Server

    Jotania, Rajshree B

    2013-01-01

    The Ferrite term is used to refer to all magnetic oxides containing iron as major metallic component. Ferrites are very attractive materials because they simultaneously show high resistivity and high saturation magnetization, and attract now considerable attention, because of the interesting physics involved. Typical ferrite material possesses excellent chemical stability, high corrosion resistivity, magneto-crystalline anisotropy, magneto-striction, and magneto-optical properties. Ferrites belong to the group of ferrimagnetic oxides, and include rare-earth garnets and ortho-ferrites. Several

  18. The ICRF-3: Status, plans, and progress on the next generation International Celestial Reference Frame

    CERN Document Server

    Malkin, Z; Arias, F; Boboltz, D; Boehm, J; Bolotin, S; Bourda, G; Charlot, P; De Witt, A; Fey, A; Gaume, R; Heinkelmann, R; Lambert, S; Ma, C; Nothnagel, A; Seitz, M; Gordon, D; Skurikhina, E; Souchay, J; Titov, O

    2015-01-01

    The goal of this presentation is to report the latest progress in creation of the next generation of VLBI-based International Celestial Reference Frame, ICRF3. Two main directions of ICRF3 development are improvement of the S/X-band frame and extension of the ICRF to higher frequencies. Another important task of this work is the preparation for comparison of ICRF3 with the new generation optical frame GCRF expected by the end of the decade as a result of the Gaia mission.

  19. Dual-mode latching ferrite devices

    Science.gov (United States)

    Xu, Y.; Jiang, Z.

    1986-05-01

    A primary consideration with microwave ferrite control devices is related to the switching speed. In order to achieve fast switching with the considered devices, an operation in the latching mode is required. A description is given of a new class of ferrite latching devices, taking into account latching quadrupole devices and their modifications. It is pointed out that the advantages of the new devices include fast switching, high electrical performance, and simple construction. According to the utilization of external or internal magnetic return paths, there are two modes of operation in latching ferrite devices. Attention is given to constructions and calculations, the design of a model for each of the two modes of operation, polarization insensitive phase shifters (PIPS) with external magnetic return paths, and PIPS with internal magnetic return paths.

  20. Effects of corrosion and precipitates on mechanical properties in the ferritic/martensitic steel cladding under ultra-long cycle fast reactor environment at 650 .deg. C

    Energy Technology Data Exchange (ETDEWEB)

    Kim, Tae Yong; Lee, Jeong Hyeon; Kim, Ji Hyun [UNIST, Ulsan (Korea, Republic of); Shin, Sang Hun [KAERI, Daejeon (Korea, Republic of)

    2016-05-15

    This changes chemical compositions of inter-surface and effects on behavior of precipitations. NaCrO{sub 2} which is ternary sodium compound occurs intergranular corrosion resulting in thickness reduction. This change can cause a degradation of mechanical strength of structure material of UCFR. Therefore, we should consider longterm compatibility with sodium and study about life prediction. The research about ferritic/martensitic steel on effects of long term exposure in liquid sodium at 650 .deg. C, 20ppm oxygen includes weight loss of test material (Gr. 92) by corrosion and mechanism about nucleation and growth of precipitates like Laves-phase in bulk. There are many changes such as segregation of component to nucleate precipitates, affecting into microstructural evolution of the steel. Therefore, the thermochemical reaction research to predict behavior about precipitates should be performed. In a specific procedure, the micro-structure and the surface phenomenon of ferritic/martensitic steels (Gr. 92) that are exposed to liquid sodium at 650 .deg. C, 20 ppm oxygen and aged in high pure Argon gas environment to express bulk have been investigated by using scanning electron microscope (SEM) and transmission electron microscope (TEM). At 10 ppm oxygen designed oxygen value for UCFR, there is 107μm thickness reduction for 30 years. Thus, if there is no degradation of mechanical strength caused by aging effect, the tolerance of load of initial cladding should be higher than real load at least 23.6 %. Compared to specimens exposed to Ar-gas environment, Specimen which solutions are leaded into sodium has degradation of strength by reduction of solution hardening.

  1. Heat loads on JET plasma facing components from ICRF and LH wave absorption in the SOL

    Science.gov (United States)

    Jacquet, P.; Colas, L.; Mayoral, M.-L.; Arnoux, G.; Bobkov, V.; Brix, M.; Coad, P.; Czarnecka, A.; Dodt, D.; Durodie, F.; Ekedahl, A.; Frigione, D.; Fursdon, M.; Gauthier, E.; Goniche, M.; Graham, M.; Joffrin, E.; Korotkov, A.; Lerche, E.; Mailloux, J.; Monakhov, I.; Noble, C.; Ongena, J.; Petrzilka, V.; Portafaix, C.; Rimini, F.; Sirinelli, A.; Riccardo, V.; Vizvary, Z.; Widdowson, A.; Zastrow, K.-D.; EFDA Contributors, JET

    2011-10-01

    In JET, lower hybrid (LH) and ion cyclotron resonance frequency (ICRF) wave absorption in the scrape-off layer can lead to enhanced heat fluxes on some plasma facing components (PFCs). Experiments have been carried out to characterize these heat loads in order to: (i) prepare JET operation with the Be wall which has a reduced power handling capability as compared with the carbon wall and (ii) better understand the physics driving these wave absorption phenomena and propose solutions for next generation systems to reduce them. When using ICRF, hot spots are observed on the antenna structures and on limiters close to the powered antennas and are explained by acceleration of ions in RF-rectified sheath potentials. High temperatures up to 800 °C can be reached on locations where a deposit has built up on tile surfaces. Modelling which takes into account the fast thermal response of surface layers can reproduce well the surface temperature measurements via infrared (IR) imaging, and allow evaluation of the heat fluxes local to active ICRF antennas. The flux scales linearly with the density at the antenna radius and with the antenna voltage. Strap phasing corresponding to wave spectra with lower kpar values can lead to a significant increase in hot spot intensity in agreement with antenna modelling that predicts, in that case, an increase in RF sheath rectification. LH absorption in front of the antenna through electron Landau damping of the wave with high Npar components generates hot spots precisely located on PFCs magnetically connected to the launcher. Analysis of the LH hot spot surface temperature from IR measurements allows a quantification of the power flux along the field lines: in the worst case scenario it is in the range 15-30 MW m-2. The main driving parameter is the LH power density along the horizontal rows of the launcher, the heat fluxes scaling roughly with the square of the LH power density. The local electron density in front of the grill increases

  2. Potential of ion cyclotron resonance frequency current drive via fast waves in DEMO

    Science.gov (United States)

    Kazakov, Ye O.; Van Eester, D.; Wauters, T.; Lerche, E.; Ongena, J.

    2015-02-01

    For the continuous operation of future tokamak-reactors like DEMO, non-inductively driven toroidal plasma current is needed. Bootstrap current, due to the pressure gradient, and current driven by auxiliary heating systems are currently considered as the two main options. This paper addresses the current drive (CD) potential of the ion cyclotron resonance frequency (ICRF) heating system in DEMO-like plasmas. Fast wave CD scenarios are evaluated for both the standard midplane launch and an alternative case of exciting the waves from the top of the machine. Optimal ICRF frequencies and parallel wave numbers are identified to maximize the CD efficiency. Limitations of the high frequency ICRF CD operation are discussed. A simplified analytical method to estimate the fast wave CD efficiency is presented, complemented with the discussion of its dependencies on plasma parameters. The calculated CD efficiency for the ICRF system is shown to be similar to those for the negative neutral beam injection and electron cyclotron resonance heating.

  3. Recent results from the TFTR ICRF DT Program

    Energy Technology Data Exchange (ETDEWEB)

    Rogers, J.H.; Darrow, D.; Majeski, R. [and others

    1995-03-01

    The first experiments to be performed with ICRF heating of DT plasmas are reported. ICRF heating of minority ions, tritium (second harmonic resonance), as well as direct electron heating are being performed during the DT phase of TFTR. RF power modulation and Fourier transform techniques are used to attempt to elucidate the competition between tritium second harmonic, direct electron, and {sup 3}He fundamental heating in DT plasmas. A significant fraction of the RF power has been found to couple to the tritium ions via second harmonic heating. Relevant RF coupling physics is investigated using {sup 3}He minority heating (43 MHz), H minority heating (64 MHz), and mode conversion (43 MHz, comparable densities of {sup 3}He and {sup 4}He) at a toroidal field of 4.5T.

  4. Effects of alloying and processing modifications on precipitation and strength in 9%Cr ferritic/martensitic steels for fast reactor cladding

    Science.gov (United States)

    Tippey, Kristin E.

    P92 was modified with respect to alloying and processing in the attempt to enhance high-temperature microstructural stability and mechanical properties. Alloying effects were modeled in ThermoCalcRTM and analyzed with reference to literature. ThermoCalcRTM modeling was conducted to design two low-carbon P92-like low-carbon alloys with austenite stabilized by alternative alloying; full conversion to austenite allows for a fully martensitic structure. Goals included avoidance of Z-phase, decrease of M23C6 phase fraction and maintained or increased MX phase fraction. Fine carbonitride precipitation was optimized by selecting alloying compositions such that all V and Nb could be solutionized at temperatures outside the delta-ferrite phase field. A low-carbon alloy (LC) and a low-carbon-zero-niobium alloy (0Nb) were identified and fabricated. This low-carbon approach stems from the increased creep resistance reported in several low-carbon alloys, presumably from reduced M23C6 precipitation and maintained MX precipitation [1], although these low-carbon alloys also contained additional tungsten (W) and cobalt (Co) compared to the base P92 alloy. The synergistic effect of Co and W on the microstructure and mechanical properties are difficult to deconvolute. Higher solutionizing temperatures allow more V and Nb into solution and increase prior austenite grain size; however, at sufficiently high temperatures delta-ferrite forms. Optimal solutionizing temperatures to maximize V and Nb in solution, while avoiding the onset of the delta ferrite phase field, were analyzed in ThermoCalcRTM. Optical microscopy showed ThermoCalc RTM predicted higher delta-ferrite onset temperatures of 20 °C in P92 alloys to nearly 50 °C in the designed alloys of the critical temperature. Identifying the balance where maximum fine precipitation is achieved and delta-ferrite avoided is a key factor in the design of an acceptable P92-like alloy for Generation IV reactor cladding. Processing was

  5. Observation of Central Toroidal Rotation Induced by ICRF on EAST

    Science.gov (United States)

    Pan, Xiayun; Wang, Fudi; Zhang, Xinjun; Lyu, Bo; Chen, Jun; Li, Yingying; Fu, Jia; Shi, Yuejiang; Yu, Yi; Ye, Minyou; Wan, Baonian

    2016-02-01

    Core plasma rotation of both L-mode and H-mode discharges with ion cyclotron range of frequency (ICRF) minority heating (MH) scheme was measured with a tangential X-ray imaging crystal spectrometer on EAST (Experimental Advanced Superconducting Tokamak). Co-current central impurity toroidal rotation change was observed in ICRF-heated L- and H-mode plasmas. Rotation increment as high as 30 km/s was generated at ∼1.7 MW ICRF power. Scaling results showed similar trend as the Rice scaling but with significant scattering, especially in L-mode plasmas. We varied the plasma current, toroidal field and magnetic configuration individually to study their effect on L-mode plasma rotation, while keeping the other major plasma parameters and heating unchanged during the scanning. It was found that larger plasma current could induce plasma rotation more efficiently. A scan of the toroidal magnetic field indicated that the largest rotation was obtained for on-axis ICRF heating. A comparison between lower-single-null (LSN) and double-null (DN) configurations showed that LSN discharges rendered a larger rotation change for the same power input and plasma parameters. supported by the National Magnetic Confinement Fusion Science Program of China (Nos. 2013GB112004 and 2015GB103002), National Natural Science Foundation of China (Nos. 11175208, 11305212, 11375235, 11405212 and 11261140328), the Innovative Program of Development Foundation of Hefei Center for Physical Science and Technology (2014FXCX003) and Brain Korea 21 Program for Leading Universities & Students (BK21 PLUS)

  6. Characterization of local heat fluxes around ICRF antennas on JET

    Energy Technology Data Exchange (ETDEWEB)

    Campergue, A.-L. [Ecole Nationale des Ponts et Chaussées, F77455 Marne-la-Vallée (France); Jacquet, P.; Monakhov, I.; Arnoux, G.; Brix, M.; Sirinelli, A. [Euratom/CCFE Association, Culham Science Centre, Abingdon, OX14 3DB (United Kingdom); Bobkov, V. [Max-Planck-Institut für Plasmaphysik, EURATOM-Assoziation, Garching (Germany); Milanesio, D. [Politecnico di Torino, Department of Electronics, Torino (Italy); Colas, L. [CEA, IRFM, F-13108 Saint-Paul-Lez-Durance (France); Collaboration: JET-EFDA Contributors

    2014-02-12

    When using Ion Cyclotron Range of Frequency (ICRF) heating, enhanced power deposition on Plasma-Facing Components (PFCs) close to the antennas can occur. Experiments have recently been carried out on JET with the new ITER-Like-Wall (ILW) to characterize the heat fluxes on the protection of the JET ICRF antennas, using Infra-Red (IR) thermography measurement. The measured heat flux patterns along the poloidal limiters surrounding powered antennas were compared to predictions from a simple RF sheath rectification model. The RF electric field, parallel to the static magnetic field in front of the antenna, was evaluated using the TOPICA code, integrating a 3D flattened model of the JET A2 antennas. The poloidal density variation in front of the limiters was obtained from the mapping of the Li-beam or edge reflectometry measurements using the flux surface geometry provided by EFIT equilibrium reconstruction. In many cases, this simple model can well explain the position of the maximum heat flux on the different protection limiters and the heat-flux magnitude, confirming that the parallel RF electric field and the electron plasma density in front of the antenna are the main driving parameters for ICRF-induced local heat fluxes.

  7. FAST

    DEFF Research Database (Denmark)

    Zuidmeer-Jongejan, Laurian; Fernandez-Rivas, Montserrat; Poulsen, Lars K.

    2012-01-01

    ABSTRACT: The FAST project (Food Allergy Specific Immunotherapy) aims at the development of safe and effective treatment of food allergies, targeting prevalent, persistent and severe allergy to fish and peach. Classical allergen-specific immunotherapy (SIT), using subcutaneous injections with aqu......ABSTRACT: The FAST project (Food Allergy Specific Immunotherapy) aims at the development of safe and effective treatment of food allergies, targeting prevalent, persistent and severe allergy to fish and peach. Classical allergen-specific immunotherapy (SIT), using subcutaneous injections...... with aqueous food extracts may be effective but has proven to be accompanied by too many anaphylactic side-effects. FAST aims to develop a safe alternative by replacing food extracts with hypoallergenic recombinant major allergens as the active ingredients of SIT. Both severe fish and peach allergy are caused...... in depth serological and cellular immune analyses will be performed, allowing identification of novel biomarkers for monitoring treatment efficacy. FAST aims at improving the quality of life of food allergic patients by providing a safe and effective treatment that will significantly lower their threshold...

  8. Effect of energetic ion loss on ICRF heating efficiency and energy confinement time in heliotrons

    Energy Technology Data Exchange (ETDEWEB)

    Murakami, S.; Nakajima, N.; Okamoto, M. [National Inst. for Fusion Science, Toki, Gifu (Japan); Nuehrenberg, J.

    1999-06-01

    ICRF heating efficiency and the global energy confinement time during ICRF heating are investigated including the effect of energetic ion loss in heliotrons. The approximate formula of ICRF heating efficiency is derived using the results based on Monte Carlo simulations. The global energy confinement time including energetic ion effect can be expressed in terms of ICRF heating power, plasma density, and magnetic field strength in heliotrons. Our results in the CHS plasma show the systematic decrement of the global energy confinement time due to the energetic ion loss from the assumed energy confinement scaling law, which is consistent with the experimental observations. Also we apply our model to the ICRF minority heating in the LHD plasma in two cases of typical magnetic configurations. The clear increment of the global energy confinement time due to the stored energy of energetic tail ions is obtained in the `orbit improved` configuration, while the decrement is observed in the `standard` configuration. (author)

  9. VizieR Online Data Catalog: The epoch ICRF (Xu+, 2013)

    Science.gov (United States)

    Xu, M. H.; Wang, G. L.; Zhao, M.

    2014-04-01

    The epoch International Celestial Reference Frame (epoch ICRF) is proposed as a new concept in order to consider the effect of apparent proper motion of the position of a radio source due to acceleration of the spatial origin of the ICRF, the centre of mass of the Solar system. This apparent proper motion has a magnitude of approximately 5.8-microarcsec (μas) per year, and for the 30-year very long baseline interferometry (VLBI) observational history these position variations will exceed 100μas. We show that the dipole structure of the apparent proper motions leads to global rotation in the ICRF2 and the main term, the shift of direction of the origin of right ascension, reaches 25μas per century. The 'epoch ICRF' is constructed using epoch positions at J2000.0 and apparent proper motions of radio sources, which are reported here for 295 ICRF2-defining sources. (1 data file).

  10. Survey of the TS-ECE Discrepancy and recent investigations in ICRF heated plasmas at Alcator C-Mod

    Directory of Open Access Journals (Sweden)

    Reinke M. L.

    2012-09-01

    Full Text Available This paper reports on a new investigation of the long-standing, unresolved discrepancy between Thomson Scattering (TS and Electron Cyclotron Emission (ECE measurements of electron temperature in high temperature tokamak plasmas. At the Alcator C-Mod tokamak, ion cyclotron range of frequency (ICRF heating is used to produce high temperature conditions where the TS- ECE discrepancy, as observed in the past at JET and TFTR, should appear. Plasmas with Te(0 up to 8 keV are obtained using three different heating scenarios: Ion Cyclotron Resonance Heating (ICRH, ICRF mode conversion heating and a combination of the two heating methods. This is done in order to explore the hypothesis that ICRH-generated fast ions may be related to the discrepancy. In all high temperature cases at C-Mod, we find no evidence for the type of discrepancy reported at JET and TFTR. Here we present the C-Mod results along with a summary of past work on the TS-ECE discrepancy.

  11. Monte Carlo simulation of ICRF discharge initiation in ITER

    Science.gov (United States)

    Tripský, M.; Wauters, T.; Lyssoivan, A.; Křivská, A.; Louche, F.; Van Schoor, M.; Noterdaeme, J.-M.

    2015-12-01

    Discharges produced and sustained by ion cyclotron range of frequency (ICRF) waves in absence of plasma current will be used on ITER for (ion cyclotron-) wall conditioning (ICWC). The here presented simulations aim at ensuring that the ITER ICRH&CD system can be safely employed for ICWC and at finding optimal parameters to initiate the plasma. The 1D Monte Carlo code RFdinity1D3V was developed to simulate ICRF discharge initiation. The code traces the electron motion along one toroidal magnetic field line, accelerated by the RF field in front of the ICRF antenna. Electron collisions in the calculations are handled by a Monte Carlo procedure taking into account their energies and the related electron collision cross sections for collisions with H2, H2+ and H+. The code also includes Coulomb collisions between electrons and ions (e - e, e - H2+ , e - H+). We study the electron multiplication rate as a function of the RF discharge parameters (i) antenna input power (0.1-5MW), and (ii) the neutral pressure (H2) for two antenna phasing (monopole [0000]-phasing and small dipole [0π0π]-phasing). Furthermore, we investigate the electron multiplication rate dependency on the distance from the antenna straps. This radial dependency results from the decreasing electric amplitude and field smoothening with increasing distance from the antenna straps. The numerical plasma breakdown definition used in the code corresponds to the moment when a critical electron density nec for the low hybrid resonance (ω = ωLHR) is reached. This numerical definition was previously found in qualitative agreement with experimental breakdown times obtained from the literature and from experiments on the ASDEX Upgrade and TEXTOR.

  12. ICRF array module development and optimization for high power density

    Energy Technology Data Exchange (ETDEWEB)

    Ryan, P.M.; Swain, D.W.

    1997-02-01

    This report describes the analysis and optimization of the proposed International Thermonuclear Experimental Reactor (ITER) Antenna Array for the ion cyclotron range of frequencies (ICRF). The objectives of this effort were to: (1) minimize the applied radiofrequency rf voltages occurring in vacuum by proper layout and shape of components, limit the component`s surface/volumes where the rf voltage is high; (2) study the effects of magnetic insulation, as applied to the current design; (3) provide electrical characteristics of the antenna for the development and analysis of tuning, arc detection/suppression, and systems for discriminating between arcs and edge-localized modes (ELMs); (4) maintain close interface with mechanical design.

  13. SciDAC Center for Simulation of Wave-Plasma Interactions - Iterated Finite-Orbit Monte Carlo Simulations with Full-Wave Fields for Modeling Tokamak ICRF Wave Heating Experiments - Final Report

    Energy Technology Data Exchange (ETDEWEB)

    Choi, Myunghee [Retired; Chan, Vincent S. [General Atomics

    2014-02-28

    This final report describes the work performed under U.S. Department of Energy Cooperative Agreement DE-FC02-08ER54954 for the period April 1, 2011 through March 31, 2013. The goal of this project was to perform iterated finite-orbit Monte Carlo simulations with full-wall fields for modeling tokamak ICRF wave heating experiments. In year 1, the finite-orbit Monte-Carlo code ORBIT-RF and its iteration algorithms with the full-wave code AORSA were improved to enable systematical study of the factors responsible for the discrepancy in the simulated and the measured fast-ion FIDA signals in the DIII-D and NSTX ICRF fast-wave (FW) experiments. In year 2, ORBIT-RF was coupled to the TORIC full-wave code for a comparative study of ORBIT-RF/TORIC and ORBIT-RF/AORSA results in FW experiments.

  14. International Celestial Reference Frame (ICRF): mantenimiento y extensión

    Science.gov (United States)

    Ma, C.; Arias, E. F.; Eubanks, T.; Fey, A. L.; Gontier, A.-M.; Jacobs, C. S.; Sovers, O. J.; Archinal, B. A.; Charlot, P.

    A partir de enero de 1998 el sistema de referencia celeste convencional está representado por el International Celestial Reference System (ICRS) y materializado a través de las coordenadas VLBI del conjunto de radiofuentes extragalácticas que conforman el International Celestial Reference Frame (ICRF). La primera realización del ICRF, fue elaborada en 1995 por un grupo de expertos designado por la IAU, la que encomendó al International Earth Rotation Service el mantenimiento del ICRS, del ICRF y del vínculo con marcos de referencia en otras frecuencias. Una primera extensión del ICRF se realizó entre abril y junio de 1999, con el objetivo primario de proveer posiciones de radiofuentes extragalácticas observadas a partir de julio de 1995 y de mejorar las posiciones de las fuentes ``candidatas" con la inclusión de observaciones adicionales. Objetivos secundarios fueron monitorear a las radiofuentes para verificar que siguen siendo adecuadas para realizar al ICRF y mejorar las técnicas de análisis de datos. Como resultado del nuevo análisis se obtuvo una solución a partir de la cual se construyó la primera extensión del ICRF, denominada ICRF - Ext.1. Ella representa al ICRS, sus fuentes de definición se mantienen con las mismas posiciones y errores que en la primera realización del ICRF; las demás radiofuentes tienen coordenadas mejor determinadas que en ICRF; el marco de referencia se densificó con el agregado de 59 nuevas radiofuentes.

  15. ICRF heating in JET during initial operations with the ITER-like wall

    Energy Technology Data Exchange (ETDEWEB)

    Jacquet, P.; Brix, M.; Graham, M.; Mayoral, M.-L.; Meigs, A.; Monakhov, I.; Sirinelli, A. [Euratom/CCFE Fusion Association, Culham Science Centre, Abingdon, OX14 3DB (United Kingdom); Bobkov, V.; Drewelow, P.; Pütterich, T. [Max-Planck-Institut für Plasmaphysik, EURATOM-Assoziation, Garching (Germany); Brezinsek, S. [IEK-4, Forschungszentrum Jülich, Association EURATOM-FZJ (Germany); Campergue, A-L. [Ecole Nationale des Ponts et Chaussées, F77455 Marne-la-Vallée (France); Colas, L. [CEA, IRFM, F-13108 Saint-Paul-Lez-Durance (France); Czarnecka, A. [Association Euratom-IPPLM, Hery 23, 01-497 Warsaw (Poland); Klepper, C. C. [Oak Ridge National Laboratory, Oak Ridge, TN 37831-6169 (United States); Lerche, E.; Van-Eester, D. [Association EURATOM-Belgian State, ERM-KMS, Brussels (Belgium); Milanesio, D. [Politecnico di Torino, Department of Electronics, Torino (Italy); Mlynar, J. [Association EURATOM-IPP.CR, Za Slovankou 3, 182 21 Praha 8 (Czech Republic); Collaboration: JET-EFDA Contributors

    2014-02-12

    In 2011/12, JET started operation with its new ITER-Like Wall (ILW) made of a tungsten (W) divertor and a beryllium (Be) main chamber wall. The impact of the new wall material on the JET Ion Cyclotron Resonance Frequency (ICRF) operation was assessed and also the properties of JET plasmas heated with ICRF were studied. No substantial change of the antenna coupling resistance was observed with the ILW as compared with the carbon wall. Heat-fluxes on the protecting limiters close the antennas quantified using Infra-Red (IR) thermography (maximum 4.5 MW/m{sup 2} in current drive phasing) are within the wall power load handling capabilities. A simple RF sheath rectification model using the antenna near-fields calculated with the TOPICA code can well reproduce the heat-flux pattern around the antennas. ICRF heating results in larger tungsten and nickel (Ni) contents in the plasma and in a larger core radiation when compared to Neutral Beam Injection (NBI) heating. Some experimental facts indicate that main-chamber W components could be an important impurity source: the divertor W influx deduced from spectroscopy is comparable when using RF or NBI at same power and comparable divertor conditions; the W content is also increased in ICRF-heated limiter plasmas; and Be evaporation in the main chamber results in a strong and long lasting reduction of the impurity level. The ICRF specific high-Z impurity content decreased when operating at higher plasma density and when increasing the hydrogen concentration from 5% to 20%. Despite the higher plasma bulk radiation, ICRF exhibited overall good plasma heating efficiency; The ICRF power can be deposited at plasma centre and the radiation is mainly from the outer part of the plasma. Application of ICRF heating in H-mode plasmas started, and the beneficial effect of ICRF central electron heating to prevent W accumulation in the plasma core could be observed.

  16. Detailed Modeling of Grounding Solutions for the ITER ICRF Antenna

    Science.gov (United States)

    Kyrytsya, V.; Dumortier, P.; Messiaen, A.; Louche, F.; Durodié, F.

    2011-12-01

    The excitation of non-TEM modes around the ITER ICRF antenna plug can considerably increase the level of RF voltages and currents on the ITER plug. First study of these modes and a solution to avoid them in the ITER ion cyclotron range of frequencies were reported in [1]. In this work a detailed analysis of electrical properties of the ITER ICRF antenna with the plug was studied for different grounding solutions with CST Microwave Studio® [2]. Conclusions of an earlier work [ 1 ] were confirmed on the detailed model of the antenna with the plug. Different grounding contacts (capacitive, galvanic and mixed capacitive-galvanic) as well as their distribution inside the plug gap were analyzed. It was shown that capacitive and mixed capacitive-galvanic grounding are less effective because they demand high values of the capacitance and are more sensitive to the frequency and antenna spectrum. In particular a galvanic grounding realized by the contacts put around the perimeter of the plug gap at lm behind the front face of the antenna is the most suitable solution from the electromagnetic point of view. An optimization of the layout and arrangement of the contacts in order to assess and optimize the current distribution on them is under way. Measurements on a scaled mock-up of the complete antenna and the plug are under way for modeling results confirmation.

  17. Modern Ferrite Technology

    CERN Document Server

    Goldman, Alex

    2006-01-01

    Modern Ferrite Technology, 2nd Ed. offers the readers an expert overview of the latest ferrite advances as well as their applications in electronic components. This volume develops the interplay among material properties, component specification and device requirements using ferrites. Throughout, emphasis is placed on practical technological concerns as opposed to mathematical and physical aspects of the subject. The book traces the origin of the magnetic effect in ferrites from the level of the simplest particle and then increases the scope to include larger hierarchies. From the desired magnetic properties, the author deduces the physical and chemical material parameters, taking into consideration major chemistry, impurity levels, ceramic microstructures and grain boundary effects. He then discusses the processing conditions and associated conditions required for implementation. In addition to conventional ceramic techniques, he describes non-conventional methods such as co-precipitation, co-spray roasting ...

  18. Removal of Particles by ICRF Cleaning in HT-7 Superconducting Tokamak

    Institute of Scientific and Technical Information of China (English)

    2001-01-01

    The ICRF (Ion Cyclotron Range Frequency) cleaning technique has been used as aroutine wall cleaning method in the HT-7 superconducting tokamak. In a wide range of toroidalfield, thc removal rate of residual gas by ICRF cleaning was about twenty times higher than that ofglow discharge cleaning (GDC). At different gas pressure and RF power levels, the ICRF cleaningis studied carcfully. A good impurity clcaning effect and a very high hydrogen removal rate wereobtained. The removal rate of hydrogen by 5 kW ICRF cleaning achieved was 1.6 × 10-5 Torr.1/s.And the relationships among pressure P, outgassing rate Q, atomic layers L absorbed on surfaceand the cleaning mode were discussed briefly.

  19. Initial operation of high power ICRF system for long pulse in EAST

    Energy Technology Data Exchange (ETDEWEB)

    Qin, C. M., E-mail: chmq@ipp.ac.cn; Zhao, Y. P.; Zhang, X. J.; Wan, B. N.; Gong, X. Z.; Mao, Y. Z.; Yuan, S.; Chen, G. [Institute of Plasma Physics, Chinese Academy of Sciences, Hefei 230031 (China)

    2015-12-10

    The ICRF heating system on EAST upgraded by active cooling aims for long pulse operation. In this paper, the main technical features of the ICRF system are described. One of a major challenges for long pulse operation is RF-edge interactions induced impurity production and heat loading. In EAST, ICRF antenna protections and Faraday screen bars damaged due to LH electron beam are found. Preliminary results for the analysis of the interaction between LHCD and ICRF antenna are discussed. Increase of metal impurities in the plasma during RF pulse and in a larger core radiation are also shown. These RF-edge interactions at EAST and some preliminary results for the optimizing RF performance will be presented.

  20. Field-aligned-impedance-transforming ICRF antenna in the LHD

    Energy Technology Data Exchange (ETDEWEB)

    Saito, K., E-mail: saito@nifs.ac.jp; Seki, T.; Kasahara, H.; Seki, R.; Kamio, S.; Nomura, G.; Mutoh, T.

    2015-10-15

    Newly developed ion cyclotron range of frequencies (ICRF) antennas were fabricated and installed in the Large Helical Device (LHD). The antennas, called field-aligned-impedance-transforming (FAIT) antennas, were designed based on former handshake form (HAS) antennas for high power and steady-state operation. The FAIT antennas demonstrated higher loading resistance and lower temperature on ceramic feed-through than HAS antennas. Antenna impedance and injected power were measured precisely using a directional coupler installed between the impedance matching device and antenna. It was shown that an injection power of 1.8 MW or a power density of 15 MW/m{sup 2} would be possible for short-pulse discharges. The mutual coupling between two FAIT antennas is small enough, since any current phase is possible without adjusting the impedance matching device. Although the FAIT antennas are aligned in a poloidal direction, a high heating efficiency of 85% was achieved with the proper minority concentration ratio.

  1. Impedance calculation for ferrite inserts

    Energy Technology Data Exchange (ETDEWEB)

    Breitzmann, S.C.; Lee, S.Y.; /Indiana U.; Ng, K.Y.; /Fermilab

    2005-01-01

    Passive ferrite inserts were used to compensate the space charge impedance in high intensity space charge dominated accelerators. They study the narrowband longitudinal impedance of these ferrite inserts. they find that the shunt impedance and the quality factor for ferrite inserts are inversely proportional to the imaginary part of the permeability of ferrite materials. They also provide a recipe for attaining a truly passive space charge impedance compensation and avoiding narrowband microwave instabilities.

  2. Morphology of Proeutectoid Ferrite

    Science.gov (United States)

    Yin, Jiaqing; Hillert, Mats; Borgenstam, Annika

    2017-03-01

    The morphology of grain boundary nucleated ferrite particles in iron alloys with 0.3 mass pct carbon has been classified according to the presence of facets. Several kinds of particles extend into both grains of austenite and have facets to both. It is proposed that they all belong to a continuous series of shapes. Ferrite plates can nucleate directly on the grain boundary but can also develop from edges on many kinds of particles. Feathery structures of parallel plates on both sides of a grain boundary can thus form. In sections, parallel to their main growth direction, plates have been seen to extend the whole way from the nucleation site at the grain boundary and to the growth front. This happens in the whole temperature range studied from 973 K to 673 K (700 °C to 400 °C). The plates thus grow continuously and not by subunits stopping at limited length and continuing the growth by new ones nucleating. Sometimes, the plates have ridges and in oblique sections they could be mistaken for the start of new plates. No morphological signs were observed indicating a transition between Widmanstätten ferrite and bainitic ferrite. It is proposed that there is only one kind of acicular ferrite.

  3. Ferrite logic reliability study

    Science.gov (United States)

    Baer, J. A.; Clark, C. B.

    1973-01-01

    Development and use of digital circuits called all-magnetic logic are reported. In these circuits the magnetic elements and their windings comprise the active circuit devices in the logic portion of a system. The ferrite logic device belongs to the all-magnetic class of logic circuits. The FLO device is novel in that it makes use of a dual or bimaterial ferrite composition in one physical ceramic body. This bimaterial feature, coupled with its potential for relatively high speed operation, makes it attractive for high reliability applications. (Maximum speed of operation approximately 50 kHz.)

  4. Density convection near radiating ICRF antennas and its effect on the coupling of lower hybrid waves

    Energy Technology Data Exchange (ETDEWEB)

    Ekedahl, A.; Colas, L.; Beaumont, B.; Bibet, Ph.; Bremond, S.; Kazarian, F. [Association Euratom-CEA Cadarache, 13 - Saint-Paul-lez-Durance (France). Dept. de Recherches sur la Fusion Controlee; Mayoral, M.L.; Mailloux, J. [Euratom/UKAEA Fusion Association, Culham Science Centre, Abingdon, OX (United Kingdom); Noterdaeme, J.M. [Max-Planck-Institut fuer Plasmaphysik, Euratom Association, Garching (Germany)]|[Gent University, EESA Dept. (Belgium); Tuccillo, A.A. [Associazione Euratom-ENEA sulla Fusione, CR Frascati, Rome (Italy)

    2003-07-01

    Combined operation of lower hybrid (LH) and Ion Cyclotron Resonance Frequency (ICRF) waves can result in a degradation of the LH wave coupling, as observed both in the Tore-Supra and Jet tokamaks. The reflection coefficient on the part of the LH launcher magnetically connected to the powered ICRF antenna increases, suggesting a local decrease in the electron density in the connecting flux tubes. This has been confirmed by Langmuir probe measurements on the LH launchers in the latest Tore-Supra experiments. Moreover, recent experiments in Jet indicate that the LH coupling degradation depends on the ICRF power and its launched k{sub /} spectrum. The 2D density distribution around the Tore-Supra ICRF antennas has been modelled with the CELLS-code, balancing parallel losses with diffusive transport and sheath induced ExB convection, obtained from RF field mapping using the ICANT-code. The calculations are in qualitative agreement with the experimental observations, i.e. density depletion is obtained, localised mainly in the antenna shadow, and dependent on ICRF power and antenna spectrum. (authors)

  5. Trends of W behavior in ICRF assisted discharges in ASDEX Upgrade

    Science.gov (United States)

    Czarnecka, A.; Bobkov, V.; Dux, R.; Pütterich, T.; Sertoli, M.

    2015-08-01

    During Ion Cyclotron Range of Frequencies (ICRF) operation with metallic plasma facing components, plasma wall interaction processes are modified, which needs to be understood in order to reduce the ICRF-related rise in impurity concentration and maximize ICRF coupling. This contribution is focused on gathering and analyzing a database on W-behavior during ICRF spanning a multi-parameter space. The gas puff dependence is investigated in selected pulses that feature the injection of deuterium (D2) main gas, with impurity gas nitrogen (N2), argon (Ar) and krypton (Kr). CW was found to decrease with the total gas injection rate, which was also correlated with the changes of electron density in the location of the CW measurements. Although the addition of N2, Ar and Kr impacted on the increase in sputtering, to achieve a similar CW level with mixed puffing, one needs to inject considerably more gas. Moreover, CW is shown to change after implementation of boron coatings on the ICRF antenna limiters.

  6. Effect on the tritium breeding ratio for a distributed ICRF antenna in a DEMO reactor

    Energy Technology Data Exchange (ETDEWEB)

    Garcia, A., E-mail: albert.garcia.hp@gmail.com [Max-Planck-Institut für Plasmaphysik (IPP), Garching (Germany); Karlsruhe Institute of Technology (KIT), Karlsruhe (Germany); Polytechnic University of Catalonia (UPC), Barcelona (Spain); Department of Applied Physics, Ghent University, Ghent (Belgium); Noterdaeme, J.-M. [Max-Planck-Institut für Plasmaphysik (IPP), Garching (Germany); Department of Applied Physics, Ghent University, Ghent (Belgium); Fischer, U. [Karlsruhe Institute of Technology (KIT), Karlsruhe (Germany); Dies, J. [Polytechnic University of Catalonia (UPC), Barcelona (Spain)

    2015-12-10

    The paper reports results of MCNP-5 calculations to assess the effect on the Tritium Breeding Ratio (TBR) when integrating a distributed Ion Cyclotron Range of Frequencies (ICRF) antenna in the blanket of DEMO fusion power reactor. The calculations consider different parameters such as the ICRF covering ratio and the type of breeding blanket including the Helium Cooled Pebble Bed (HCPB) and the Helium Cooled Lithium Lead (HCLL) concepts. For an antenna with a full toroidal circumference of 360°, located poloidally at 40° with a poloidal extension of 1 m, the reduction of the TBR is −0.349% for the HCPB blanket and −0.532% for the HCLL blanket. The distributed ICRF antenna is thus shown to have only a marginal effect on the TBR of the DEMO reactor.

  7. Effect on the tritium breeding ratio for a distributed ICRF antenna in a DEMO reactor

    Science.gov (United States)

    Garcia, A.; Noterdaeme, J.-M.; Fischer, U.; Dies, J.

    2015-12-01

    The paper reports results of MCNP-5 calculations to assess the effect on the Tritium Breeding Ratio (TBR) when integrating a distributed Ion Cyclotron Range of Frequencies (ICRF) antenna in the blanket of DEMO fusion power reactor. The calculations consider different parameters such as the ICRF covering ratio and the type of breeding blanket including the Helium Cooled Pebble Bed (HCPB) and the Helium Cooled Lithium Lead (HCLL) concepts. For an antenna with a full toroidal circumference of 360°, located poloidally at 40° with a poloidal extension of 1 m, the reduction of the TBR is -0.349% for the HCPB blanket and -0.532% for the HCLL blanket. The distributed ICRF antenna is thus shown to have only a marginal effect on the TBR of the DEMO reactor.

  8. Progress in controlling ICRF-edge interactions in ASDEX upgrade

    Energy Technology Data Exchange (ETDEWEB)

    Bobkov, Vl., E-mail: bobkov@ipp.mpg.de; Ochoukov, R.; Bilato, R.; Braun, F.; Carralero, D.; Dux, R.; Faugel, H.; Fünfgelder, H.; Jacquot, J.; Lunt, T.; Potzel, S.; Pütterich, Th. [Max-Planck-Institut für Plasmaphysik, Boltzmannstr.2, D-85748 (Germany); Jacquet, Ph.; Monakhov, I. [CCFE, Culham Science Centre, Abingdon, OX14 3DB (United Kingdom); Zhang, W.; Noterdaeme, J.-M.; Stepanov, I. [Max-Planck-Institut für Plasmaphysik, Boltzmannstr.2, D-85748 (Germany); Department of Applied Physics, Gent University, 9000 Gent (Belgium); Colas, L.; Meyer, O. [CEA, IRFM, F-13108 Saint-Paul-lez-Durance (France); Czarnecka, A. [Institute of Plasma Physics and Laser Microfusion, Hery 23 Str., 01-497 Warsaw (Poland); and others

    2015-12-10

    RF measurements during variation of the strap voltage balance of the original 2-strap ICRF antenna in ASDEX Upgrade at constant power are consistent with electromagnetic calculations by HFSS and TOPICA, more so for the latter. RF image current compensation is observed at the antenna limiters in the experiment at a local strap voltage of about half of the value of the remote strap, albeit with a non-negligible uncertainty in phasing. The RF-specific tungsten (W) source at the broad-limiter 2-strap antenna correlates strongly with the RF voltage at the local strap at the locations not connected to opposite side of the antenna along magnetic field lines. The trends of the observed increase of the RF loading with injection of local gas are well described by a combined EMC3-Eirene – FELICE calculations, with the most efficient improvement confirmed for the outer-midplane valves, but underestimated by about 1/3. The corresponding deuterium density tailoring is also likely responsible for the decrease of local W sources observed in the experiment.

  9. Commissioning of the ITER-like ICRF antenna for JET

    Energy Technology Data Exchange (ETDEWEB)

    Durodie, F. [ERM-KMS, Association EURATOM-Belgian State, Brussels (Belgium); Dumortier, P. [ERM-KMS, Association EURATOM-Belgian State, Brussels (Belgium); Huygen, S. [ERM-KMS, Association EURATOM-Belgian State, Brussels (Belgium); Jachmich, S. [ERM-KMS, Association EURATOM-Belgian State, Brussels (Belgium); Lerche, E. [ERM-KMS, Association EURATOM-Belgian State, Brussels (Belgium); Messiaen, A. [ERM-KMS, Association EURATOM-Belgian State, Brussels (Belgium); Ongena, J [ERM-KMS, Association EURATOM-Belgian State, Brussels, Belgium; Van Eester, D. [Laboratory for Plasma Physics-ERM/KMS (LPP-ERM/KMS), Brussels (Belgium); Vervier, M. [ERM-KMS, Association EURATOM-Belgian State, Brussels (Belgium); Vrancken, M. [ERM-KMS, Association EURATOM-Belgian State, Brussels (Belgium); Nightingale, M. [EURATOM / UKAEA, Abingdon (United Kingdom); Blackman, T. [EURATOM / UKAEA, Abingdon (United Kingdom); Edwards, P. [EURATOM / UKAEA, Abingdon (United Kingdom); Fanthome, J. [EURATOM / UKAEA, Abingdon (United Kingdom); Graham, M. [EURATOM / UKAEA, Abingdon (United Kingdom); Jacquet, P. [EURATOM / UKAEA, Abingdon (United Kingdom); Kaye, A. [EURATOM / UKAEA, Abingdon (United Kingdom); Mayoral, M. -L. [EURATOM / UKAEA, Abingdon (United Kingdom); Monakhov, I. [EURATOM / UKAEA, Abingdon (United Kingdom); Nicholls, K. [EURATOM / UKAEA, Abingdon (United Kingdom); Stork, D. [EURATOM / UKAEA, Abingdon (United Kingdom); Walden, A. [EURATOM / UKAEA, Abingdon (United Kingdom); Whitehurst, A. [EURATOM / UKAEA, Abingdon (United Kingdom); Zastrow, K. -D. [EURATOM / UKAEA, Abingdon (United Kingdom); Argouarch, A. [CEA-Cadarache, St. Paul lex Durance (France); Berger-By, G. [CEA-Cadarache, St. Paul lex Durance (France); Loarer, T. [CEA-Cadarache, St. Paul lex Durance (France); Rimini, F. [CEA-Cadarache, St. Paul lex Durance (France); Castano-Giraldo, C. [University of Illinois, Urbana-Champaign, IL (United States); Caughman, John B. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Goulding, Richard Howell [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Cocilovo, V. [Association Euratom-ENEA sulla Fusione (Italy); Frigione, D. [Association Euratom-ENEA sulla Fusione (Italy); Sozzi, C. [Association Euratom-ENEA sulla Fusione (Italy); Hobrik, J. [Max-Planck-Institut fuer Plasmaphysik, EURATOM Association, Garching (Germany); Lamalle, Philippe [ITER Joint Work Site, Cadarache (France); Nave, M. F. F. [Association EURATOM/IST, Lisbon (Portugal); Tsalas, M. [Association EURATOM-Hellas, Attica (Greece)

    2009-06-01

    The new JET ion cyclotron resonance frequency (ICRF) ITER-like antenna (ILA), which was assembled during 2006, was commissioned on the JET RF testbed prior to installation on the JET torus. The 4 resonant double loops (RDL) of the ILA were tested at high power at 42 MHz up to 42 kV for 5 s in 10 min intervals. Low power matching studies using a saltwater load placed in front of the ILA have allowed testing and optimizing proposed matching algorithms on single RDLs, paired RDLs and finally on the full array. The upper limit of the frequency range of the ILA appears to be limited to 47 49 MHz due to the effect on the electrical lengths of the connection between the capacitors and the conjugate T point. Capacitor position scans have allowed obtaining the necessary data to confirm the RF model of the RDL which is necessary for the scattering matrix arc detection. The latter is deemed necessary in order to detect arcs at the low impedance conjugate T of the circuit. The antenna was installed onto JET during August 2007 and commissioning on plasma started May 2008. At present the commissioning of the ILA on JET is ongoing in a series of dedicated experimental campaigns.

  10. Optical Spectra of Candidate International Celestial Reference Frame (ICRF) Flat-spectrum Radio Sources. III.

    Science.gov (United States)

    Titov, O.; Pursimo, T.; Johnston, Helen M.; Stanford, Laura M.; Hunstead, Richard W.; Jauncey, David L.; Zenere, Katrina A.

    2017-04-01

    In extending our spectroscopic program, which targets sources drawn from the International Celestial Reference Frame (ICRF) Catalog, we have obtained spectra for ˜160 compact, flat-spectrum radio sources and determined redshifts for 112 quasars and radio galaxies. A further 14 sources with featureless spectra have been classified as BL Lac objects. Spectra were obtained at three telescopes: the 3.58 m European Southern Observatory New Technology Telescope, and the two 8.2 m Gemini telescopes in Hawaii and Chile. While most of the sources are powerful quasars, a significant fraction of radio galaxies is also included from the list of non-defining ICRF radio sources.

  11. Magnesium ferrite nanoparticles: a rapid gas sensor for alcohol

    Science.gov (United States)

    Godbole, Rhushikesh; Rao, Pratibha; Bhagwat, Sunita

    2017-02-01

    Highly porous spinel MgFe2O4 nanoparticles with a high specific surface area have been successfully synthesized by a sintering free auto-combustion technique and characterized for their structural and surface morphological properties using XRD, BET, TEM and SEM techniques. Their sensing properties to alcohol vapors viz. ethanol and methanol were investigated. The site occupation of metal ions was investigated by VSM. The as-synthesized sample shows the formation of sponge-like porous material which is necessary for gas adsorption. The gas sensing characteristics were obtained by measuring the gas response as a function of operating temperature, concentration of the gas, and the response-recovery time. The response of magnesium ferrite to ethanol and methanol vapors was compared and it was revealed that magnesium ferrite is more sensitive and selective to ethanol vapor. The sensor operates at a substantially low vapor concentration of about 1 ppm of alcohol vapors, exhibits fantastic response reproducibility, long term reliability and a very fast response and recovery property. Thus the present study explored the possibility of making rapidly responding alcohol vapor sensor based on magnesium ferrite. The sensing mechanism has been discussed in co-relation with magnetic and morphological properties. The role of occupancy of Mg2+ ions in magnesium ferrite on its gas sensing properties has also been studied and is found to influence the response of magnesium ferrite ethanol sensor.

  12. ICRF antennas optimized for operation with a high-Z metallic wall in ASDEX Upgrade

    Energy Technology Data Exchange (ETDEWEB)

    Zammuto, I. [Euratom Association, Max Planck-Institut fuer Plasmaphysik, Boltzmannstrasse 2, D-85748 Garching (Germany)], E-mail: i.zammuto@libero.it; Krivska, A. [Euratom Association, Institute of Plasma Physics ASCR, Prague (Czech Republic); Telecommunication Engineering Department, Czech Technical University of Prague, Prague (Czech Republic); Bobkov, V.; Braun, F.; Bilato, R. [Euratom Association, Max Planck-Institut fuer Plasmaphysik, Boltzmannstrasse 2, D-85748 Garching (Germany); Noterdaeme, J.-M. [Euratom Association, Max Planck-Institut fuer Plasmaphysik, Boltzmannstrasse 2, D-85748 Garching (Germany); EESA Department, University of Gent, Gent (Belgium)

    2009-06-15

    High-Z materials are considered the best candidates for plasma facing components (PFCs) in future fusion devices, while ion cyclotron range of frequencies (ICRF) heating is a method of choice because of its flexibility, cost effectiveness, and plug-to-power efficiency. But high-Z materials and ICRF have been a difficult combination. ASDEX Upgrade (AUG) is pioneering the use of a tungsten (W) wall and in the next years it will prove (or disprove) the appropriateness of this combination for the future. This paper describes the optimization procedure for and the main features of a new proposed ICRF antenna for AUG specifically designed to improve the compatibility of ICRF with a high-Z metallic wall. The optimization criteria for a new design are based on a reduction of the parasitic parallel electric field responsible of the impurity production. The evolutionary design of the 2-strap antenna is compared with a redesigned 4-strap antenna embedded in the wall. Moreover, options and constraints on how to integrate a wider antenna in the present configuration of ASDEX Upgrade and its integration on the stabilizing wall are discussed.

  13. Estimation of sheath potentials in front of ASDEX upgrade ICRF antenna with SSWICH asymptotic code

    Science.gov (United States)

    Křivská, A.; Bobkov, V.; Colas, L.; Jacquot, J.; Milanesio, D.; Ochoukov, R.

    2015-12-01

    Multi-megawatt Ion Cyclotron Range of Frequencies (ICRF) heating became problematic in ASDEX Upgrade (AUG) tokamak after coating of ICRF antenna limiters and other plasma facing components by tungsten. Strong impurity influx was indeed produced at levels of injected power markedly lower than in the previous experiments. It is assumed that the impurity production is mainly driven by parallel component of Radio-Frequency (RF) antenna electric near-field E// that is rectified in sheaths. In this contribution we estimate poloidal distribution of sheath Direct Current (DC) potential in front of the ICRF antenna and simulate its relative variations over the parametric scans performed during experiments, trying to reproduce some of the experimental observations. In addition, relative comparison between two types of AUG ICRF antenna configurations, used for experiments in 2014, has been performed. For this purpose we use the Torino Polytechnic Ion Cyclotron Antenna (TOPICA) code and asymptotic version of the Self-consistent Sheaths and Waves for Ion Cyclotron Heating (SSWICH) code. Further, we investigate correlation between amplitudes of the calculated oscillating sheath voltages and the E// fields computed at the lateral side of the antenna box, in relation with a heuristic antenna design strategy at IPP Garching to mitigate RF sheaths.

  14. Expanding the operating space of ICRF on JET with a view to ITER

    DEFF Research Database (Denmark)

    Lamalle, P.U.; Mantsinen, M.J.; Noterdaeme, J.M.

    2006-01-01

    This paper reports on ITER-relevant ion cyclotron resonance frequency (ICRF) physics investigated on JET in 2003 and early 2004. Minority heating of helium three in hydrogen plasmas-(He-3)H-was systematically explored by varying the 3 He concentration and the toroidal phasing of the antenna array...

  15. Estimation of sheath potentials in front of ASDEX upgrade ICRF antenna with SSWICH asymptotic code

    Energy Technology Data Exchange (ETDEWEB)

    Křivská, A., E-mail: alena.krivska@rma.ac.be [LPP-ERM/KMS, Royal Military Academy, 30 Avenue de la Renaissance B-1000, Brussels (Belgium); Bobkov, V.; Jacquot, J.; Ochoukov, R. [Max-Planck-Institut für Plasmaphysik, D-85748 Garching (Germany); Colas, L. [CEA, IRFM, F-13108 Saint-Paul-Lez-Durance (France); Milanesio, D. [Politecnico di Torino, Corso Duca degli Abruzzi 24, I-10129 Torino (Italy)

    2015-12-10

    Multi-megawatt Ion Cyclotron Range of Frequencies (ICRF) heating became problematic in ASDEX Upgrade (AUG) tokamak after coating of ICRF antenna limiters and other plasma facing components by tungsten. Strong impurity influx was indeed produced at levels of injected power markedly lower than in the previous experiments. It is assumed that the impurity production is mainly driven by parallel component of Radio-Frequency (RF) antenna electric near-field E// that is rectified in sheaths. In this contribution we estimate poloidal distribution of sheath Direct Current (DC) potential in front of the ICRF antenna and simulate its relative variations over the parametric scans performed during experiments, trying to reproduce some of the experimental observations. In addition, relative comparison between two types of AUG ICRF antenna configurations, used for experiments in 2014, has been performed. For this purpose we use the Torino Polytechnic Ion Cyclotron Antenna (TOPICA) code and asymptotic version of the Self-consistent Sheaths and Waves for Ion Cyclotron Heating (SSWICH) code. Further, we investigate correlation between amplitudes of the calculated oscillating sheath voltages and the E// fields computed at the lateral side of the antenna box, in relation with a heuristic antenna design strategy at IPP Garching to mitigate RF sheaths.

  16. The behavior of neutron emissions during ICRF minority heating of plasma at EAST

    Science.gov (United States)

    Zhong, Guoqiang; Cao, Hongrui; Hu, Liqun; Zhou, Ruijie; Xiao, Min; Li, Kai; Pu, Neng; Huang, Juan; Liu, Guangzhu; Lin, Shiyao; Lyu, Bo; Liu, Haiqing; Zhang, Xinjun; EAST Team

    2016-07-01

    Ion cyclotron radio frequency (ICRF) wave heating is a primary method to heat ions in the Experimental Advanced Superconducting Tokamak (EAST). Through neutron diagnostics, effective ion heating was observed in hydrogenminority heating (MH) scenarios. At present, investigation of deuterium-deuterium (DD) fusion neutrons is mostly based on time-resolved flux monitor and spectrometer measurements. When the ICRF was applied, the neutron intensity became one order higher. The H/H  +  D ratio was in the range of 5-10%, corresponding to the hydrogen MH dominated scenario, and a strong high energy tail was not displayed on the neutron spectrum that was measured by a liquid scintillator. Moreover, ion temperature in the plasma center (T i) was inversely calculated by the use of neutron source strength (S n) and the plasma density based on classical fusion reaction equations. This result indicates that T i increases by approximately 30% in L-mode plasma, and by more than 50% in H-mode plasma during ICRF heating, which shows good agreement with x-ray crystal spectrometer (XCS) diagnostics. Finally, the DD neutron source strength scaling law, with regard to plasma current (I P) and ICRF coupling power (P RF) on the typical minority heating condition, was obtained by statistical analysis.

  17. Implementation of the new multichannel X-mode edge density profile reflectometer for the ICRF antenna on ASDEX Upgrade

    Science.gov (United States)

    Aguiam, D. E.; Silva, A.; Bobkov, V.; Carvalho, P. J.; Carvalho, P. F.; Cavazzana, R.; Conway, G. D.; D'Arcangelo, O.; Fattorini, L.; Faugel, H.; Fernandes, A.; Fünfgelder, H.; Gonçalves, B.; Guimarais, L.; De Masi, G.; Meneses, L.; Noterdaeme, J. M.; Pereira, R. C.; Rocchi, G.; Santos, J. M.; Tuccillo, A. A.; Tudisco, O.

    2016-11-01

    A new multichannel frequency modulated continuous-wave reflectometry diagnostic has been successfully installed and commissioned on ASDEX Upgrade to measure the plasma edge electron density profile evolution in front of the Ion Cyclotron Range of Frequencies (ICRF) antenna. The design of the new three-strap ICRF antenna integrates ten pairs (sending and receiving) of microwave reflectometry antennas. The multichannel reflectometer can use three of these to measure the edge electron density profiles up to 2 × 1019 m-3, at different poloidal locations, allowing the direct study of the local plasma layers in front of the ICRF antenna. ICRF power coupling, operational effects, and poloidal variations of the plasma density profile can be consistently studied for the first time. In this work the diagnostic hardware architecture is described and the obtained density profile measurements were used to track outer radial plasma position and plasma shape.

  18. Evaluation of the topoisomerase II-inactive bisdioxopiperazine ICRF-161 as a protectant against doxorubicin-induced cardiomyopathy

    DEFF Research Database (Denmark)

    Martin, E.; Thougaard, A.V.; Grauslund, M.

    2009-01-01

    of topoisomerase II, resulting in the risk of additional myelosuppression in patients receiving ICRF-187 as a cardioprotectant in combination with doxorubicin. The development of a topoisomerase II-inactive iron chelating compound thus appeared attractive. In the present paper we evaluate the topoisomerase II......-inactive 3 carbon linker bisdioxopiperazine analog ICRF-161 as a cardioprotectant. We demonstrate that this compound does chelate iron and protects against doxorubicin-induced LDH release from primary rat cardiomyocytes in vitro, similarly to ICRF-187. The compound does not target topoisomerase II in vitro...... was not capable of protecting against the cardiotoxic effects of doxorubicin. Modulation of the activity of the beta isoform of the topoisomerase II enzyme by ICRF-187 has recently been proposed as the mechanism behind its cardioprotection. This concept is thus supported by the present study in that iron...

  19. Implementation of the new multichannel X-mode edge density profile reflectometer for the ICRF antenna on ASDEX Upgrade

    Energy Technology Data Exchange (ETDEWEB)

    Aguiam, D. E., E-mail: daguiam@ipfn.tecnico.ulisboa.pt; Silva, A.; Carvalho, P. J.; Carvalho, P. F.; Fernandes, A.; Gonçalves, B.; Guimarais, L.; Meneses, L.; Pereira, R. C.; Santos, J. M. [Instituto de Plasmas e Fusão Nuclear, Instituto Superior Técnico, Universidade de Lisboa, 1049-001 Lisboa (Portugal); Bobkov, V.; Conway, G. D.; Faugel, H.; Fünfgelder, H. [Max-Planck-Institut für Plasmaphysik, Boltzmannstr. 2, D-85748 Garching (Germany); Cavazzana, R.; De Masi, G. [Consorzio RFX (CNR, ENEA, INFN, Universitá di Padova, Acciaierie Venete SpA), Corso Stati Uniti 4, 35127 Padova (Italy); D’Arcangelo, O.; Rocchi, G.; Tuccillo, A. A. [ENEA, Dipartimento FSN, C. R. Frascati, Via E. Fermi 45, 00044 Frascati, Roma (Italy); and others

    2016-11-15

    A new multichannel frequency modulated continuous-wave reflectometry diagnostic has been successfully installed and commissioned on ASDEX Upgrade to measure the plasma edge electron density profile evolution in front of the Ion Cyclotron Range of Frequencies (ICRF) antenna. The design of the new three-strap ICRF antenna integrates ten pairs (sending and receiving) of microwave reflectometry antennas. The multichannel reflectometer can use three of these to measure the edge electron density profiles up to 2 × 10{sup 19} m{sup −3}, at different poloidal locations, allowing the direct study of the local plasma layers in front of the ICRF antenna. ICRF power coupling, operational effects, and poloidal variations of the plasma density profile can be consistently studied for the first time. In this work the diagnostic hardware architecture is described and the obtained density profile measurements were used to track outer radial plasma position and plasma shape.

  20. Development of two-step softening heat-treatment in ODS ferritic steel claddings with recrystallized grain structure

    Energy Technology Data Exchange (ETDEWEB)

    Narita, Takeshi; Ukai, Shigeharu; Kaito, Takeji; Ohtsuka, Satoshi [Japan Nuclear Cycle Development Inst., Oarai, Ibaraki (Japan). Oarai Engineering Center; Kobayashi, Toshimi [Sumitomo Metal Technology, Inc., Tokyo (Japan)

    2003-03-01

    Oxide dispersion-strengthened (ODS) ferritic steels have been developed as prospective cladding materials for attaining higher burnup and higher coolant outlet temperature in advanced fast reactors. In the cladding manufacturing process, two-step softening heat-treatment was developed as an effective method for application to the recrystalizing heat-treatment, which made possible the improvement of formability, ductility and the disappearance of strength anisotropy in the ODS ferritic steel claddings. A mass production process is predicted and cost reduction is concomitantly expected for manufacturing ODS ferritic steel claddings with an adequate strength level at 700degC for commercialized fast reactors. (author)

  1. Characterization of SOL plasma flows and potentials in ICRF-heated plasmas in Alcator C-mod

    Science.gov (United States)

    Hong, R.; Wukitch, S. J.; Lin, Y.; Terry, J. L.; Cziegler, I.; Reinke, M. L.; Tynan, G. R.

    2017-10-01

    Gas-puff imaging techniques are employed to determine the far SOL region radial electric field and the plasma potential in ICRF heated discharges in the Alcator C-Mod tokamak. The two-dimensional velocity fields of the turbulent structures, which are advected by RF-induced {E}× {B} flows, are obtained via the time-delay estimation (TDE) techniques. Both the magnitude and radial extension of the radial electric field E r are observed to increase with the toroidal magnetic field strength B φ and the ICRF power. In particular, the RF-induced E r extends from the vicinity of the ICRF antenna to the separatrix when {B}\\varphi =7.9 {{T}} and {P}{ICRF}≳ 1 {MW}. In addition, low-Z impurity seeding near the antenna is found to substantially reduce the sheath potential associated with ICRF power. The TDE techniques have also been used to revisit and estimate ICRF-induced potentials in different antenna configurations: (1) conventional toroidally aligned (TA) antenna versus field-aligned (FA) antenna; (2) FA monopole versus FA dipole. It shows that FA and TA antennas produce similar magnitude of plasma potentials, and the FA monopole induced greater potential than the FA dipole phasing. The TDE estimations of RF-induced plasma potentials are consistent with previous results based on the poloidal phase velocity.

  2. Gaia Data Release 1. Reference frame and optical properties of ICRF sources

    Science.gov (United States)

    Mignard, F.; Klioner, S.; Lindegren, L.; Bastian, U.; Bombrun, A.; Hernández, J.; Hobbs, D.; Lammers, U.; Michalik, D.; Ramos-Lerate, M.; Biermann, M.; Butkevich, A.; Comoretto, G.; Joliet, E.; Holl, B.; Hutton, A.; Parsons, P.; Steidelmüller, H.; Andrei, A.; Bourda, G.; Charlot, P.

    2016-11-01

    Context. As part of the data processing for Gaia Data Release 1 (Gaia DR1) a special astrometric solution was computed, the so-called auxiliary quasar solution. This gives positions for selected extragalactic objects, including radio sources in the second realisation of the International Celestial Reference Frame (ICRF2) that have optical counterparts bright enough to be observed with Gaia. A subset of these positions was used to align the positional reference frame of Gaia DR1 with the ICRF2. Although the auxiliary quasar solution was important for internal validation and calibration purposes, the resulting positions are in general not published in Gaia DR1. Aims: We describe the properties of the Gaia auxiliary quasar solution for a subset of sources matched to ICRF2, and compare their optical and radio positions at the sub-mas level. Methods: Descriptive statistics are used to characterise the optical data for the ICRF sources and the optical-radio differences. The most discrepant cases are examined using online resources to find possible alternative explanations than a physical optical-radio offset of the quasars. Results: In the auxiliary quasar solution 2191 sources have good optical positions matched to ICRF2 sources with high probability. Their formal standard errors are better than 0.76 milliarcsec (mas) for 50% of the sources and better than 3.35 mas for 90%. Optical magnitudes are obtained in Gaia's unfiltered photometric G band. The Gaia results for these sources are given as a separate table in Gaia DR1. The comparison with the radio positions of the defining sources shows no systematic differences larger than a few tenths of a mas. The fraction of questionable solutions, not readily accounted for by the statistics, is less than 6%. Normalised differences have extended tails requiring case-by-case investigations for around 100 sources, but we have not seen any difference indisputably linked to an optical-radio offset in the sources. Conclusions: With

  3. Development of new ferritic / martensitic steels for fuel cladding in fast neutron reactors; Developpement de nouvelles nuances d'aciers ferritiques / martensitiques pour le gainage d'elements combustibles des Reacteurs a Neutrons Rapides au sodium

    Energy Technology Data Exchange (ETDEWEB)

    Ratti, M.

    2009-11-15

    Many studies are directed toward the development of ferritic / martensitic ODS materials for applications in Gen IV programs. In this study, the mechanisms of formation of nano-phases (Y, Ti, O) and the influence of titanium on the precipitation refinement have been analyzed by small angle neutron scattering, X-ray diffraction and neutron diffraction. The obtained results allow developing new materials reinforced by nitrides (NDS which stands for Nitride Dispersion Strengthened). A first CEA patent is now being registered on these NDS materials processed by mechanical alloying. However, microstructural and mechanical characterizations are necessary to improve these new alloys. At last, a tensile and creep database has been acquired on an ODS Fe-18Cr material between room temperature and 650 C. These tests allow a qualitative description of the ODS mechanical behaviour. (author)

  4. Plasma heating and generation of energetic ions with novel three-ion ICRF scenarios on Alcator C-Mod and JET tokamak facilities

    Science.gov (United States)

    Kazakov, Yevgen

    2016-10-01

    This talk will report the first experimental results of novel three-ion ICRF scenarios (two or more majority ion species and one minority) for plasma heating and generating energetic ions in fusion facilities. The key feature of these scenarios is strong absorption of RF power possible at lower concentrations of minority ions than in two-ion plasmas. Effective plasma heating by injecting a small amount of 3He ions into H-D plasma mixtures with nH /ne 70 % has been successfully demonstrated in Alcator C-Mod and JET tokamaks. In C-Mod, efficient plasma heating was observed for 3He concentrations from 0.4-2%. During the discharges, a strong increase in Alfvén eigenmode activity was found to coincide with the addition of 3He to the H-D plasmas. Even lower 3He concentrations ( 0.2 %) were utilized in recent JET experiments. The potential of the D-(3He) -H scenario for plasma heating and generating MeV-range ions in JET plasmas was confirmed by a set of independent measurements, including stabilization of sawteeth, characteristic γ-ray emission, fast-ion loss detector. Furthermore, toroidal Alfvén eigenmodes with a range of toroidal mode numbers n were detected, which is another indication for the presence of significant population of high-energy 3He ions in a plasma. The discussed mechanism of resonant wave-particle interaction opens up various unexplored opportunities for ICRF system, including new scenarios for plasma heating. Three-ion ICRF scenarios are also relevant for the experimental programme of ITER. The possibility of using intrinsic 9Be impurities as the minority (instead of 3He) was suggested for heating bulk ions in D-T plasmas of JET and ITER, as well as heating trace amounts of 3He and 4He ions in H majority plasmas of ITER. The latest results and simulation comparisons will be presented. On behalf of Alcator C-Mod Team (MIT-PSFC, US) and JET Contributors (Culham, UK). Work supported by the US DOE (C-Mod DE-FC02-99ER54512 and SciDAC DE-FC02-01ER54648

  5. Microwave applications of soft ferrites

    CERN Document Server

    Pardavi-Horvath, M P

    2000-01-01

    Signal processing requires broadband, low-loss, low-cost microwave devices (circulators, isolators, phase shifters, absorbers). Soft ferrites (garnets, spinels, hexaferrites), applied in planar microwave devices, are reviewed from the point of view of device requirements. Magnetic properties, specific to operation in high-frequency electromagnetic fields, are discussed. Recent developments in thick film ferrite technology and device design are reviewed. Magnetic losses related to planar shape and inhomogeneous internal fields are analyzed.

  6. High beta and second region stability analysis and ICRF edge modeling

    Energy Technology Data Exchange (ETDEWEB)

    1989-01-01

    This report describes the tasks accomplished under Department of Energy contract [number sign]DE-FG02-86ER53236 in modeling the edge plasma-antenna interaction that occurs during Ion Cyclotron Range of Frequency (ICRF) heating. This work has resulted in the development of several codes which determine kinetic and fluid modifications to the edge plasma. When used in combination, these code predict the level of impurity generation observed in experiments on the experiments on the Princeton Large Torus. In addition, these models suggest improvements to the design of ICRF antennas. Also described is progress made on high beta and second region analysis. Code development for a comprehensive infernal mode analysis code is nearing completion. A method has been developed for parameterizing the second region of stability and is applied to circular cross section tokamas. Various studies for high beta experimental devices such as PBX-M and DIII-D have been carried out and are reported on.

  7. The ICRF-3: Proposed Roadmap to the Next Generation International Celestial Reference Frame

    Science.gov (United States)

    Jacobs, Christopher S.; Arias, F.; Boehm, J.; Bolotin, S.; Bourda, G.; Charlot, P.; de Witt, A.; Fey, A.; Gaume, R.; Gordon, D.; Heinkelmann, R.; Kurdubov, S.; Lambert, S.; Ma, C.; Malkin, Z.; Nothnagel, A.; Seitz, M.; Skurikhina, E.; Souchay, J.; Titov, O.; Boboltz, D.

    2014-10-01

    ICRF-3 seeks to improve upon the highly successful ICRF-2. Our goals are to improve the precision, spatial and frequency coverage relative to the ICRF-2 by 2018. This date is driven by the desire to create radio frames that are ready for comparison with the Gaia optical frame. Several specific actions are underway. A collaboration has started to improve at S/X-band precision of the VLBA Calibrator Survey's ~2200 sources which are typically 5 times less precise than the rest of the ICRF-2. S/X-band southern precision improvements are underway with observations using southern antennas such as the AuScope and HartRAO, S. Africa. We also seek to improve radio frequency coverage with X/Ka and K-band work. An X/Ka frame of 654 sources now has full sky coverage from the addition of a 2nd southern station in Argentina which should strengthen the southern hemisphere in general. A K-band collaboration has formed with similar coverage and southern precision goals. On the analysis front, special attention is being given to combination techniques both of VLBI frames and of multiple data types. Consistency of the CRF with the TRF and EOP is another area of concern. Comparison of celestial frame solutions from various groups is underway in order to identify and correct systematic errors. Finally, work is underway to identify and pinpoint sources bright enough in both radio and optical to allow for a robust frame tie between VLBI and Gaia optical frames.

  8. High-power and steady-state operation of ICRF heating in the large helical device

    Energy Technology Data Exchange (ETDEWEB)

    Mutoh, T., E-mail: mutoh@nifs.ac.jp; Seki, T.; Saito, K.; Kasahara, H.; Seki, R.; Kamio, S.; Kumazawa, R.; Kubo, S.; Shimozuma, T.; Yoshimura, Y.; Igami, H.; Takahashi, H.; Ii, T.; Makino, R.; Nagaoka, K.; Nomura, G. [National Institute for Fusion Science, 322-6, Oroshi-cho, Toki, Gifu, 509-5292 (Japan); Shinya, T. [The University of Tokyo, Kashiwa 2777-8561 (Japan)

    2015-12-10

    Recent progress in an ion cyclotron range of frequencies (ICRF) heating system and experiment results in a Large Helical Device (LHD) are reported. Three kinds of ICRF antenna pairs were installed in the LHD, and the operation power regimes were extended up to 4.5 MW; also, the steady-state operation was extended for more than 45 min in LHD at a MW power level. We studied ICRF heating physics in heliotron configuration using a Hand Shake type (HAS) antenna, Field Aligned Impedance Transforming (FAIT) antenna, and Poloidal Array (PA) antenna, and established the optimum minority-ion heating scenario in an LHD. The FAIT antenna having a novel impedance transformer inside the vacuum chamber could reduce the VSWR and successfully injected a higher power to plasma. We tested the PA antennas completely removing the Faraday-shield pipes to avoid breakdown and to increase the plasma coupling. The heating performance was almost the same as other antennas; however, the heating efficiency was degraded when the gap between the antenna and plasma surface was large. Using these three kinds of antennas, ICRF heating could contribute to raising the plasma beta with the second- and third-harmonic cyclotron heating mode, and also to raising the ion temperature as discharge cleaning tools. In 2014, steady-state operation plasma with a line-averaged electron density of 1.2 × 10{sup 19} m{sup −3}, ion and electron temperature of 2 keV, and plasma sustainment time of 48 min was achieved with ICH and ECH heating power of 1.2 MW for majority helium with minority hydrogen. In 2015, the higher-power steady-state operation with a heating power of up to 3 MW was tested with higher density of 3 × 10{sup 19} m{sup −3}.

  9. On the role of ion heating in ICRF-heated discharges in Tore Supra

    Energy Technology Data Exchange (ETDEWEB)

    Eriksson, L.G.; Hoang, G.; Bergeaud, V

    2000-09-01

    The effect of bulk ion heating in Tore Supra has been investigated by studying discharges with varying concentrations of minority ions during ICRF hydrogen minority heating in Deuterium/{sup 4}He plasmas. As expected, the level of bulk ion heating is found to increase with the minority concentration. Higher levels of ion heating are shown to be accompanied by two significant effects: an improved energy confinement and a strong influence on the plasma rotation. (author)

  10. [Flow cytometric analysis of ICRF-193 influence on cell passage through mitosis].

    Science.gov (United States)

    Shatrova, A N; Aksenov, N D; Zenin, V V

    2002-01-01

    Studying the effect of topoisomerase II (topo II) inhibitors on cell passage through mitosis seems to be important for understanding the role of this enzyme during chromosome condensation and segregation. A flow cytometric assay (Zenin et al., 2001) allowed to determine the mitotic index, and to discriminate between not only cells in G2 and M phases (including metaphase and anaphase cells), but also cells in pseudo-G1 with 4c DNA content. It is shown that topo II catalytic inhibitor ICRF-193 blocks G2-M transition in a lymphoblastoid cell line GM-130. Addition of caffeine to cells abrogated a block of their entering mitosis but not the inhibitor action. Cells entered mitosis, which was proven by the presence of chromosomes in the examined specimen, and, bypassing anaphase, appeared in pseudo-G1 with 4c DNA content. We have found that in the presence of ICRF-193 cells, GM-130 and Hep-2 lines, previously blocked by nocodazole when in mitosis and then washed, pass through metaphase, enter anaphase and leave it to pass to pseudo-G1 with the 4c DNA content. Thus, by inhibiting topo II activity ICRF-193 causes abnormal mitotic transition.

  11. Analysis of crowbar action of high voltage DC power supply in the LHD ICRF system

    Energy Technology Data Exchange (ETDEWEB)

    Li Xiaodong [Southwestern Institute of Physics, Chengdu, Sichuan (China); Mutoh, T.; Kumazawa, R.; Watari, T.; Seki, T.; Shimpo, F.; Nomura, G.; Saito, K.

    1999-04-01

    Ion Cyclotron Range of Frequency (ICRF) heating will be applied to the Large Helical Device (LHD) at the 2nd experimental campaign in 1998. The LHD ICRF system is characterised by its high power (up to 12 MW at final stage) and steady state operation for more than 30 minutes. One of the main R and D items was a high power and steady state transmitter. The RF transmitter system having a wide frequency range from 25 to 95 MHz was designed and fabricated. This report describes the analysis of the DC power supply that contains the crowbar circuit protecting the tetrode from the arcing inside the tube. The DC power supply of the transmitter is fed from the commercial AC electric line which also supply the power to the LHD helical and poloidal coil power supplies. The voltage drop of the commercial line when the ICRF crowbar action happened is the serious problem for all experimental system. This paper analyses the crowbar effect on the commercial line with and without leakage transformer between the step-up transformer of transmitter and the commercial line. (author)

  12. HIS-TORIC: extending core ICRF wave simulation to include realistic SOL plasmas

    Science.gov (United States)

    Shiraiwa, S.; Wright, J. C.; Lee, J. P.; Bonoli, P. T.

    2017-08-01

    This paper presents a novel approach to incorporating an arbitrarily shaped edge scrape-off-layer (SOL) plasma and an ion cyclotron range of frequency (ICRF) antenna structure into existing core ICRF wave simulation models. We partition the entire computation domain into two sub-domains: a core and an edge region. Simulations in each domain are performed separately with appropriate numerical solvers. For the core, the TORIC ICRF solver (Brambilla 1999 Plasma Phys. Control. Fusion 41 1) was modified to impose an essential (Dirichlet) boundary condition at its interface with the edge domain. In the edge, a finite element method is used to solve a cold collisional plasma model. The domains are then joined together using the continuity boundary condition for the tangential electric and magnetic fields at their interfaces (Hybrid Integration of SOL to TORIC: HIS-TORIC). The model developed here was tested using an ICRH H minority heating scenario on the Alcator C-Mod tokamak (Hutchinson et al 1994 Phys. Plasmas 1 1511). The simulated pattern of core wave propagation agrees well with a standard TORIC simulation. This approach opens the possibility of using a realistic diverted SOL plasma and a complicated 3D RF antenna together with a rigorous hot core plasma model, while requiring only minimal modification to existing RF codes.

  13. Gaia Data Release 1: The reference frame and the optical properties of ICRF sources

    CERN Document Server

    Mignard, F; Lindegren, L; Bastian, U; Bombrun, A; Hernandez, J; Hobbs, D; Lammers, U; Michalik, D; Ramos-Lerate, M; Biermann, M; Butkevich, A; Comoretto, G; Joliet, E; Holl, B; Hutton, A; Parsons, P; Steidelmueller, H; Andrei, A; Bourda, G; Charlot, P

    2016-01-01

    As part of the data processing for Gaia Data Release~1 (Gaia DR1) a special astrometric solution was computed, the so-called auxiliary quasar solution. This gives positions for selected extragalactic objects, including radio sources in the second realisation of the International Celestial Reference Frame (ICRF2) that have optical counterparts bright enough to be observed with Gaia. A subset of these positions was used to align the positional reference frame of Gaia DR1 with the ICRF2. We describe the properties of the Gaia auxiliary quasar solution for a subset of sources matched to ICRF2, and compare their optical and radio positions at the sub-mas level. Their formal standard errors are better than 0.76~milliarcsec (mas) for 50% of the sources and better than 3.35~mas for 90%. Optical magnitudes are obtained in Gaia's unfiltered photometric G band. The comparison with the radio positions of the defining sources shows no systematic differences larger than a few tenths of a mas. The fraction of questionable s...

  14. Modeling and simulation support for ICRF heating of fusion plasmas. Annual report, 1990

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    1990-03-15

    Recent experimental, theoretical and computational results have shown the need and usefulness of a combined approach to the design, analysis and evaluation of ICH antenna configurations. The work at the University of Wisconsin (UW) in particular has shown that much needed information on the vacuum operation of ICH antennas can be obtained by a modest experimental and computational effort. These model experiments at UW and SAIC simulations have shown dramatically the potential for positive impact upon the ICRF program. Results of the UW-SAIC joint ICRF antenna analysis effort have been presented at several international meetings and numerous meetings in the United States. The PPPL bay M antenna has been modeled using the ARGUS code. The results of this effort are shown in Appendix C. SAIC has recently begun a collaboration with the ICRF antenna design and analysis group at ORNL. At present there are two separate projects underway. The first is associated with the simulation of and determination of the effect of adding slots in the antenna septum and side walls. The second project concerns the modeling and simulation of the ORNL folded waveguide (FWG) concept.

  15. Ferrite attenuator modulation improves antenna performance

    Science.gov (United States)

    Hooks, J. C.; Larson, S. G.; Shorkley, F. H.; Williams, B. T.

    1970-01-01

    Ferrite attenuator inserted into appropriate waveguide reduces the gain of the antenna element which is causing interference. Modulating the ferrite attenuator to change the antenna gain at the receive frequency permits ground tracking until the antenna is no longer needed.

  16. Full-wave and Fokker Planck analysis of ICRF heating experiments in the Alcator C-Mod tokamak

    Energy Technology Data Exchange (ETDEWEB)

    Bonoli, P.T.; Golovato, S.; Porkolab, M.; Takase, Y. [MIT Plasma Fusion Center, Cambridge, MA (United States)

    1996-12-31

    The Alcator C-Mod device is a high field, high density, shaped tokamak with parameters a = 0.22 m, R{sub 0} = 0.67 m, B{sub 0} {le} 9.0 T, {kappa} {le} 1.8, {delta} {le} 0.8, and 1.0 x 10{sup 20} m{sup -3} n{sub e} (0) {le} 1.0 x 10{sup 21} m{sup -3}. Four megawatt of ICRF power is available at 80 MHz. The wide operating range in magnetic field makes several heating schemes possible: (i) Second harmonic heating of hydrogen (f{sub 0} = 2f{sub CH}) at 2.6 T in (D-H); (ii) Fundamental heating of (H) (f{sub 0} = f{sub CH}) at 5.3T in a D-(H) plasma; and (iii) Fundamental heating of ({sup 3}He) (f{sub 0} = f{sub C{sup 3}He}) at 7.9 T in a D-({sup 3}He) plasma. The most successful heating regime to date has been (H)-minority heating at 5.3 T. Pellet enhanced performance (PEP) modes have also been achieved in C-Mod in D-(H) at 5.3 T and in D-({sup 3}He) at 7.9 T, with a combination of intense ICRF heating and Li-pellet injection. A variety of numerical models are used to analyze these heating schemes. A 1-D full-wave code (FELICE) is used to study {open_quotes}single pass{close_quotes} damping of the ICRF wavefront and damping of mode-converted ion Bernstein waves. A toroidal full-wave code (FISIC) is used to study interference and focussing effects of the ICRF waves as well as damping of the ICRF power upon multiple passes of the ICRF wavefront. A combined bounce averaged Fokker Planck and toroidal full-wave code (FPPRF) is used to study the ion tail formation, orbit losses, and the power partition of the ICRF tail to the background electrons and ions. Full-wave and Fokker Planck analyses confirm the strong single pass absorption of the ICRF power in D-(H) at 5.3 T. Analysis of PEP-mode plasmas in D-({sup 3}He) indicates improved wave focussing and {sup 3}He-cyclotron absorption of the ICRF waves relative to L-mode. A dramatic increase in the transfer of {sup 3}He tail power to the background deuterium is also found for PEP-mode plasmas.

  17. Articles comprising ferritic stainless steels

    Energy Technology Data Exchange (ETDEWEB)

    Rakowski, James M.

    2016-06-28

    An article of manufacture comprises a ferritic stainless steel that includes a near-surface region depleted of silicon relative to a remainder of the ferritic stainless steel. The article has a reduced tendency to form an electrically resistive silica layer including silicon derived from the steel when the article is subjected to high temperature oxidizing conditions. The ferritic stainless steel is selected from the group comprising AISI Type 430 stainless steel, AISI Type 439 stainless steel, AISI Type 441 stainless steel, AISI Type 444 stainless steel, and E-BRITE.RTM. alloy, also known as UNS 44627 stainless steel. In certain embodiments, the article of manufacture is a fuel cell interconnect for a solid oxide fuel cell.

  18. High power ferrite microwave switch

    Science.gov (United States)

    Bardash, I.; Roschak, N. K.

    1975-01-01

    A high power ferrite microwave switch was developed along with associated electronic driver circuits for operation in a spaceborne high power microwave transmitter in geostationary orbit. Three units were built and tested in a space environment to demonstrate conformance to the required performance characteristics. Each unit consisted of an input magic-tee hybrid, two non-reciprocal latching ferrite phase shifters, an out short-slot 3 db quadrature coupler, a dual driver electronic circuit, and input logic interface circuitry. The basic mode of operation of the high power ferrite microwave switch is identical to that of a four-port, differential phase shift, switchable circulator. By appropriately designing the phase shifters and electronic driver circuits to operate in the flux-transfer magnetization mode, power and temperature insensitive operation was achieved. A list of the realized characteristics of the developed units is given.

  19. The use of ferrites at microwave frequencies

    CERN Document Server

    Thourel, Léo

    1964-01-01

    The Use of Ferrites at Microwave Frequencies describes the applications of ferrites at microwave frequencies and the apparatus involved. Topics covered range from the properties of ferrites to gyromagnetic and non-reciprocal effects, ferrite isolators, circulators, and modulators. The use of ferrites in variable frequency filter cavities is also discussed. Mathematical explanations are reduced to the strict minimum and only the results of calculations are indicated. This book consists of seven chapters and opens with a review of the theory of magnetism, touching on subjects such as the BOHR m

  20. The influence of ICRF-159 and levamisole on the incidence of metastases following local irradiation of a solid tumor

    Energy Technology Data Exchange (ETDEWEB)

    Baker, D.; Constable, W.; Elkon, D.; Rinehart, L.

    1981-11-15

    Courses of irradiation consisting of 6000 rad in ten equal fractions over 12 days delivered to KHT sarcomas in mice controlled 55% of the local tumors but 83% of the mice died from metastases. Three strategies to reduce the risk of metastatic spread were tested. The fractionation scheme was changed to deliver the same total dose using a large initial fraction followed by seven equal portions with the same overall time. ICRF-159 was used with the intention of partially synchronizing the tumor growth fraction in a radiosensitive state of the growth cycle and of promoting normalization of the tumor vasculature. Levamisole was used to stimulate the immune system. The combination of ICRF-159 with the eight-fraction radiation course proved to be effective for both increasing local control and decreasing the incidence of metastases. The addition of levamisole did not improve the results obtained with a combination of ICRF-159 and irradiation.

  1. Influence of ICRF-159 and levamisole on the incidence of metastases following local irradiation of a solid tumor

    Energy Technology Data Exchange (ETDEWEB)

    Baker, D.; Constable, W.; Elkon, D.; Rinehart, L.

    1981-11-15

    Courses of irradiation consisting of 6000 rad in ten equal fractions over 12 days delivered to KHT sarcomas in mice controlled 55% of the local tumors but 83% of the mice died from metastases. Three strategies to reduce the risk of metastatic spread were tested. The fractionation scheme was changed to deliver the same total dose using a large initial fraction followed by seven equal portions with the same overall time. ICRF-159 was used with the intention of partially synchronizing the tumor growth fraction in a radiosensitive state of the growth cycle and of promoting normalization of the tumor vasculature. Levamisole was used to stimulate the immune system. The combination of ICRF-159 with the eight-fraction radiation course proved to be effective for both increasing local control and decreasing the incidence of metastases. The addition of levamisole did not improve the results obtained with a combination of ICRF-159 and irradiation.

  2. VizieR Online Data Catalog: Radio fluxes of 195 ICRF2-Gaia transfer sources (Le Bail+, 2016)

    Science.gov (United States)

    Le Bail, K.; Gipson, J. M.; Gordon, D.; MacMillan, D. S.; Behrend, D.; Thomas, C. C.; Bolotin, S.; Himwich, W. E.; Baver, K. D.; Corey, B. E.; Titus, M.; Bourda, G.; Charlot, P.; Collioud, A.

    2016-07-01

    The second realization of the International Celestial Reference Frame (ICRF2) is based on Very Long Baseline Interferometry (VLBI) data at radio frequencies in X band and S band. The European Space Agency's Gaia mission, launched on 2013 December 19, started routine scientific operations in 2014 July. By scanning the whole sky, it is expected to observe ~500000 Quasi Stellar Objects in the optical domain. This means that, in the future, two extragalactic celestial reference frames, at two different frequency domains, will coexist. It will thus be important to align them very accurately. In 2012, the Laboratoire d'Astrophysique de Bordeaux (LAB) selected 195 sources from ICRF2 that will be observed by Gaia and should be suitable for aligning the radio and optical frames: they are called ICRF2-Gaia transfer sources. The LAB submitted a proposal to the International VLBI Service (IVS) to regularly observe these ICRF2-Gaia transfer sources at the same rate as Gaia observes them in the optical realm, e.g., roughly once a month. Of the 195 sources, all but one have been successfully observed in the 12 months prior to 2015 September 01. Table1 lists the 195 ICRF2-Gaia transfer sources. Beginning in 2003 June, the Goddard VLBI group developed a program to purposefully monitor when sources were observed and to increase the observations of "under-observed" sources. In 2013 March, we added all 195 ICRF2-Gaia transfer sources to the IVS source monitoring program with an observation target of 12 successful sessions per year. (1 data file).

  3. Irradiation creep of various ferritic alloys irradiated at ˜400°C in the PFR and FFTF reactors

    Science.gov (United States)

    Toloczko, M. B.; Garner, F. A.; Eiholzer, C. R.

    1998-10-01

    Irradiation creep of three ferritic alloys at ˜400 ∘C has been studied. Specimens were in the form of pressurized tubes. In a joint US/UK creep study, two identical sets of creep specimens constructed from one heat of HT9 were irradiated in fast reactors, one in the Prototypic Fast Reactor (PFR) and the other in the Fast Flux Test Facility (FFTF). The specimens in PFR were irradiated to a dose of ˜50 dpa, whereas the specimens in FFTF were irradiated to a dose of 165 dpa. The observed swelling and creep behavior were very different in the two reactors. Creep specimens constructed from D57, a developmental alloy ferritic alloy, were also irradiated in PFR to a dose of ˜50 dpa. Creep behavior typical of previous studies on ferritic alloys was observed. Finally, creep specimens constructed from MA957, a Y 2O 3 dispersion-hardened ferritic alloy, were irradiated in FFTF to a dose of ˜110 dpa. This alloy exhibited a large amount of densification, and the creep behavior was different than observed in more conventional ferritic or ferritic-martensitic alloys.

  4. 先进快堆外套管材料铁素体/马氏体钢研究进展%Development of ferritic/martensitic steels used as advanced duct material for fast reactor

    Institute of Scientific and Technical Information of China (English)

    冯伟; 黄晨; 杜爱兵; 李正操; 柴茂盛

    2011-01-01

    This paper introduced the operation requirement and selection of duct materials for fast reactors at home and abroad. Irradiation effects on the microstructure and mechanical properties of F/M steels were discussed. R&D plan of F/M steels for domestic duct material of fast reactor was also introduced. F/M steels have excellent irradiation resistance to void swelling, and T92 which is the third generation F/M steels and has good high-temperature strength is chosen as the primary candidate domestic duct material of fast reactor.%介绍了快堆外套管材料的使用要求以及国内外快堆外套管材料的选用情况,论述了快堆中中子辐照对铁素体/马氏体钢的微观结构和力学性能的影响,并介绍了国产快堆外套管材料铁索体/马氏体钢的研发计划.铁索体/马氏体钢具有优异的抗辐照肿胀性能,T92钢作为第三代铁索体/马氏体钢同时具有良好的高温强度,被作为国产快堆外套管的首要候选材料.

  5. A STUDY OF FERRITE CAVITY.

    Energy Technology Data Exchange (ETDEWEB)

    ZHAO, Y.

    2002-04-19

    This note addresses the general concerns for the design of a ferrite cavity. The parameters are specified for the RCMS, for which the frequency ramp is in the range of 1.27 MHz to 6.44 MHz, or a ratio of 1:5.

  6. Study of ICRF wave propagation and plasma coupling efficiency in a linear magnetic mirror device

    Energy Technology Data Exchange (ETDEWEB)

    Peng, S.Y.

    1991-07-01

    Ion Cyclotron Range of Frequency (ICRF) wave propagation in an inhomogeneous axial magnetic field in a cylindrical plasma-vacuum system has historically been inadequately modelled. Previous works either sacrifice the cylindrical geometry in favor of a simpler slab geometry, concentrate on the resonance region, use a single mode to represent the entire field structure, or examine only radial propagation. This thesis performs both analytical and computational studies to model the ICRF wave-plasma coupling and propagation problem. Experimental analysis is also conducted to compare experimental results with theoretical predictions. Both theoretical as well as experimental analysis are undertaken as part of the thesis. The theoretical studies simulate the propagation of ICRF waves in an axially inhomogeneous magnetic field and in cylindrical geometry. Two theoretical analysis are undertaken - an analytical study and a computational study. The analytical study treats the inhomogeneous magnetic field by transforming the (r,z) coordinate into another coordinate system ({rho},{xi}) that allows the solution of the fields with much simpler boundaries. The plasma fields are then Fourier transformed into two coupled convolution-integral equations which are then differenced and solved for both the perpendicular mode number {alpha} as well as the complete EM fields. The computational study involves a multiple eigenmode computational analysis of the fields that exist within the plasma-vacuum system. The inhomogeneous axial field is treated by dividing the geometry into a series of transverse axial slices and using a constant dielectric tensor in each individual slice. The slices are then connected by longitudinal boundary conditions.

  7. Modeling of EAST ICRF antenna performance using the full-wave code TORIC

    Energy Technology Data Exchange (ETDEWEB)

    Edlund, E. M., E-mail: eedlund@pppl.gov [Princeton Plasma Physics Laboratory, Princeton, NJ (United States); Bonoli, P. T.; Porkolab, M.; Wukitch, S. J. [MIT Plasma Science and Fusion Center, Cambridge, MA (United States)

    2015-12-10

    Access to advanced operating regimes in the EAST tokamak will require a combination of electron-cyclotron resonance heating (ECRH), neutral beam injection (NBI) and ion cyclotron range frequency heating (ICRF), with the addition of lower-hybrid current drive (LHCD) for current profile control. Prior experiments at the EAST tokamak facility have shown relatively weak response of the plasma temperature to application of ICRF heating, with typical coupled power about 2 MW out of 12 MW source. The launched spectrum, at n{sub φ} = 34 for 0-π -0-π phasing and 27 MHz, is largely inaccessible at line-averaged densities of approximately 2 × 10{sup 19} m{sup −3}. However, with variable antenna phasing and frequency, this system has considerable latitude to explore different heating schemes. To develop an ICRF actuator control model, we have used the full-wave code TORIC to explore the physics of ICRF wave propagation in EAST. The results presented from this study use a spectrum analysis using a superposition of n{sub φ} spanning −50 to +50. The low density regime typical of EAST plasmas results in a perpendicular wavelength comparable to the minor radius which results in global cavity resonance effects and eigenmode formation when the single-pass absorption is low. This behavior indicates that improved performance can be attained by lowering the peak of the k{sub ||} spectrum by using π/3 phasing of the 4-strap antenna. Based on prior studies conducted at Alcator C-Mod, this phasing is also expected to have the advantage of nearly divergence-free box currents, which should result in reduced levels of impurity production. Significant enhancements of the loading resistance may be achieved by using low k{sub ||} phasing and a combination of magnetic field and frequency to vary the location of the resonance and mode conversion regions. TORIC calculations indicate that the significant power may be channeled to the electrons and deuterium majority. We expect that

  8. Neutron Flux Measurements in an ICRF Mode Conversion Regime Heating Plasmas on HT-7

    Institute of Scientific and Technical Information of China (English)

    LI Xiao-Ling; WAN Bao-Nian; ZHONG Guo-Qiang; HU Li-Qun; LIN Shi-Yao; ZHANG Xin-Jun; ZANG Qing

    2011-01-01

    Ion cyclotron resonance heating experiments using antenna, in the high Reid side (HFS) have been carried out on HT-7 in different target plasmas. Unlike a standard-mode conversion heating scheme with dominant electron heating, anomalous ion heating and DD neutron fluxes higher than those estimated from thermal ions were observed in the present experiments with the ion-ion hybrid resonant layer near the center of plasma. The features of ion cyclotron range frequency (ICRF) antenna in HFS and experiments suggest that this is most probably due to the nonlinear 3/2 harmonic deuterium heating by the mode-converted ion Bernstein wave, which could produce a high energy tail on ion energy distribution.%Ion cyclotron resonance heating experiments using antenna in the high field side (HFS) have been carried out on HT-7 in different target plasmas.Unlike a standard-mode conversion heating scheme with dominant electron heating,anomalous ion heating and DD neutron fluxes higher than those estimated from thermal ions were observed in the present experiments with the ion-ion hybrid resonant layer near the center of plasma.The features of ion cyclotron range frequency (ICRF) antenna in HFS and experiments suggest that this is most probably due to the nonlinear 3/2 harmonic deuterium heating by the mode-converted ion Bernstein wave,which could produce a high energy tail on ion energy distribution.Neutron diagnostics have been applied in ion cyclotron range frequency (ICRF) plasmas on HT-7 for measurements of the fusion reaction product,which give a direct measure of the ICRF heating.The neutron emission is recorded by a 3He proportional counter,whose sensitive size is φ30 mm × 300 mm,gas pressure is 49.34 kPa and the responsibility to thermal neutrons is 133 cps/n.cm-2.s-1.It exploits large reaction cross sections and is therefore embedded in polythene moderators to thermalize the incident neutrons.

  9. Ferrites – what is new?

    Indian Academy of Sciences (India)

    R Ranganathan; Anindita Ray

    2002-05-01

    Ferrites, combining insulating and ferrimagnetic properties, have long been used in technology. The aim of this paper is to focus on new features in these materials. In the classical theory of ferrimagnets, Neel had predicted the unusual thermal variation of the spontaneous magnetization, such as, the disappearance of the magnetization at a temperature which was not the Curie temperature but at a point where there was compensation of the spontaneous magnetization of the two sublattices. We show experimentally that temperature (K) in spinel oxide is different under the ZFC and FC magnetization method. To our knowledge, only limited attempt has been made to study K as very few systems exhibit such behavior. In general, some of the ferrites have specific semiconducting properties, e.g., a very low carrier mobility. We discuss the anomalies of the magneto-resistance in ferrites that occur at order–disorder and order–order magnetic phase transition along with our ac and dc conductivity data near the spin compensation temperature. Another notable feature of the ferrites is that, upon irradiation of heavy ions, one can tune the magnetic ordering on bulk sample without destructive effects, i.e., irradiation-induced magnetization. It is interesting to note that spinel ferrite (nano) particle is an ideal small particle magnetic system as the crystal chemistry issue can be controlled, unlike pure metal particle systems where the crystal chemistry issues are basically fixed. In relevance to this, we will also discuss the future prospects, namely, the effect of irradiation on small particle magnetism, as, so far, only a limited attempt has been made in this field.

  10. Development of a monolithic ferrite memory array

    Science.gov (United States)

    Heckler, C. H., Jr.; Bhiwandker, N. C.

    1972-01-01

    The results of the development and testing of ferrite monolithic memory arrays are presented. This development required the synthesis of ferrite materials having special magnetic and physical characteristics and the development of special processes; (1) for making flexible sheets (laminae) of the ferrite composition, (2) for embedding conductors in ferrite, and (3) bonding ferrite laminae together to form a monolithic structure. Major problems encountered in each of these areas and their solutions are discussed. Twenty-two full-size arrays were fabricated and fired during the development of these processes. The majority of these arrays were tested for their memory characteristics as well as for their physical characteristics and the results are presented. The arrays produced during this program meet the essential goals and demonstrate the feasibility of fabricating monolithic ferrite memory arrays by the processes developed.

  11. Impact of localized gas injection on ICRF coupling and SOL parameters in JET-ILW H-mode plasmas

    Energy Technology Data Exchange (ETDEWEB)

    Lerche, E., E-mail: elerche@jet.efda.org [LPP-ERM-KMS, TEC Partner, 1000 Brussels (Belgium); CCFE, Culham Science Centre, Abingdon OX14 3DB (United Kingdom); Goniche, M. [CEA, IRFM, F-13108 Saint-Paul-Lez-Durance (France); Jacquet, P. [CCFE, Culham Science Centre, Abingdon OX14 3DB (United Kingdom); Van Eester, D. [LPP-ERM-KMS, TEC Partner, 1000 Brussels (Belgium); Bobkov, V. [Max-Planck-Institut für Plasmaphysik, Garching (Germany); Colas, L. [CCFE, Culham Science Centre, Abingdon OX14 3DB (United Kingdom); Czarnecka, A. [IPPLM, 01-497 Warsaw (Poland); Brezinsek, S. [Forschungszentrum Jülich, Institute of Energy Research, Jülich (Germany); Brix, M. [CCFE, Culham Science Centre, Abingdon OX14 3DB (United Kingdom); Crombe, K. [LPP-ERM-KMS, TEC Partner, 1000 Brussels (Belgium); Graham, M. [CCFE, Culham Science Centre, Abingdon OX14 3DB (United Kingdom); Groth, M. [Aalto University, 02015 Espoo (Finland); Monakhov, I. [CCFE, Culham Science Centre, Abingdon OX14 3DB (United Kingdom); Mathurin, T. [École des Mines de Paris, 75006 Paris (France); Matthews, G. [CCFE, Culham Science Centre, Abingdon OX14 3DB (United Kingdom); Meneses, L. [Instituto de Plasma e Fusão Nuclear, Instituto Superior Técnico, Lisbon (Portugal); Noble, C. [CCFE, Culham Science Centre, Abingdon OX14 3DB (United Kingdom); Petrzilka, V. [Institute of Plasma Physics, Prague (Czech Republic); Rimini, F.; Shaw, A. [CCFE, Culham Science Centre, Abingdon OX14 3DB (United Kingdom)

    2015-08-15

    Recent JET-ILW [1,2] experiments reiterated the importance of tuning the plasma fuelling in order to optimize ion cyclotron resonance frequency (ICRF) heating in high power H-mode discharges. By fuelling the plasma from gas injection modules (GIMs) located in the mid-plane and on the top of the machine instead of adopting the more standardly used divertor GIMs, a considerable increase of the ICRF antenna coupling resistances was achieved with moderate gas injection rates (<1.5 × 10{sup 22} e/s). This effect is explained by an increase of the scrape-off-layer density in front of the antennas when mid-plane and top fuelling is used. By distributing the gas injection to optimize the coupling of all ICRF antenna arrays simultaneously, a substantial increase in the ICRF power capability and reliability was attained. Although similar core/pedestal plasma properties were observed for the different injection cases, the experiments indicate that the RF-induced impurity sources are reduced when switching from divertor to main chamber gas injection.

  12. An option of ICRF ion heating scenario in Large Helical Device

    Energy Technology Data Exchange (ETDEWEB)

    Vdovin, V.; Watari, T.; Fukuyama, A.

    1997-07-01

    Specific behavior of confining magnetic field in Large Helical Device suppresses tokamak-like ion heating scheme for ion cyclotron plasma heating with outside ICRF antenna. Respectively, the basic ICRF scenario with D(H) plasma will heat the electrons, as have been shown in stellarator CHS experiments. To overcome this difficulty, we propose to use in LHD high magnetic field side antenna operating in `heavy` minority heating scenarios H(D) or H(He-3), where brackets indicate minority ions. We show analytically that predominantly heated in this scenario will be the minority ions, subsequently transferring their energy to bulk proton ions. Another proposed scenario operates with `light` ion minority scheme like D(H), but with addition of third isotope ion component like C{sup 13}, Ne{sup 21}, Li{sup 7}, etc.. These third isotope ions eliminate degeneration of second harmonic frequency with fundamental frequency of minority ion(H) or second harmonics of deuterium ions. Isotopic ions will be heated due to a mode converted Ion Bernstein Waves close to second harmonic ion cyclotron layer ({omega}=2{omega}{sub ci}). (author)

  13. Design of a New Type of Stub Tuner in ICRF Experiment

    Institute of Scientific and Technical Information of China (English)

    秦成明; 赵燕平; 毛玉周; 丁家义; 王鹏; 潘亚平; 李国超

    2003-01-01

    In the Ion Cyclotron Range of Frequency (ICRF) heating experiment, impedancematching is of great practical significance, because wide variations in antenna loading are observedwithin the discharge, in tokamaks operating in H-mode. A sudden decrease in antenna loadingaccompanying the L-mode to H-mode transition typically occurs on a timescale of a few millisec-onds, as does the increase in loading at the H- to L-mode transition. Therefore, it is necessary tomatch dynamically in the transmission line between the generator output and the antenna inputconnections [1]. A new type of stub tuner being developed utilizes the difference in radio-frequencywavelengths between gas and liquid due to different relative dielectric constants. The impedancematchiug can be adjusted in realtime in an attempt to track the variations in the antenna loading.Since there are no mechanically moving parts in the short ends of stub, the change can be moreconveuient and safe, moreover, it can withstand higher voltage without breakdown. This systemdevice will be applied in the HT-7 superconductor Tokamak ICRF experiment.

  14. Electric field and radial transport during ICRF heating in the edge plasma of JET

    Energy Technology Data Exchange (ETDEWEB)

    Tagle, J.A.; Brinkschulte, H.; Bures, M.; De Kock, L. (Commission of the European Communities, Abingdon (UK). JET Joint Undertaking); Laux, M. (Akademie der Wissenschaften der DDR, Berlin. Zentralinstitut fuer Elektronenphysik (United Kingdom)); Clement, S. (Centro de Investigaciones Energeticas, Medioambientales y Tecnologicas, Madrid (Spain)); Erents, S.K. (UKAEA Culham Lab., Abingdon (United Kingdom))

    1990-04-01

    The plasma boundary in front of and outside the JET ICRF antenna Faraday screen has been studied using Langmuir probes. Plasma densities of n{sub e} {approx equal}10{sup 15}-10{sup 16} m{sup -3} and electron temperatures Tc {approx equal} 20-80 eV have been measured at the Faraday screen. Both n{sub e} and T{sub e} scale almost linearly with total input power (P{sub RF} up to 12 MW). DC electric fields up to 20 V/cm, with a large poloidal component perpendicular to the magnetic field lines were generated during ICRF heating. The total electric field intensity depends on the minority gas (H or {sup 3}He) and is also linearly dependent on the applied RF power. Spatially resolved measurements of the plasma space potential up to 50-100 V at the limiter flux surface were measured. The relevance of these fields to the transport in the scrape off layer (SOL), to the local particle balance at the boundary and to the impurity production during RF heating is discussed. (orig.).

  15. Status of R&D activity for ITER ICRF power source system

    Energy Technology Data Exchange (ETDEWEB)

    Mukherjee, Aparajita, E-mail: aparajita.mukherjee@iter-india.org [ITER-India, Institute for Plasma Research, Bhat, Gandhinagar–382428 (India); Trivedi, Rajesh; Singh, Raghuraj; Rajnish, Kumar; Machchhar, Harsha; Ajesh, P.; Suthar, Gajendra; Soni, Dipal; Patel, Manoj; Mohan, Kartik; Hari, J.V.S.; Anand, Rohit; Verma, Sriprakash; Agarwal, Rohit; Jha, Akhil [ITER-India, Institute for Plasma Research, Bhat, Gandhinagar–382428 (India); Kazarian, Fabienne; Beaumont, Bertrand [ITER Organization, CS 90 046, 13067 Sain-Paul-Les-Durance (France)

    2015-10-15

    Highlights: • R&D program to establish high power RF technology for ITER ICRF source is described. • R&D RF source is being developed using Diacrode & Tetrode technologies. • Test rig (3 MW/3600 s/35–65 MHz) simulating plasma load is developed. - Abstract: India is in-charge for the procurement of ITER Ion Cyclotron Resonance Frequency (ICRF) sources (1 Prototype + 8 series units) along with auxiliary power supplies and Local Control Unit. As there is no unique amplifier chain able to meet the output power specifications as per ITER requirement (2.5 MW per source at 35–65 MHz/CW/VSWR 2.0), two parallel three-stage amplifier chains along with a combiner circuit on the output side is considered. This kind of RF source will be unique in terms of its stringent specifications and building a first of its kind is always a challenge. An R&D phase has been initiated for establishing the technology considering single amplifier chain experimentation (1.5 MW/35–65 MHz/3600 s/VSWR 2.0) prior to Prototype and series production. This paper presents the status of R&D activity to resolve technological challenges involved and various infrastructures developed at ITER-India lab to support such operation.

  16. Magnetic Field Emissions for Ferrite and Non-Ferrite Geometries for Wireless Power Transfer to Vehicles

    DEFF Research Database (Denmark)

    Batra, Tushar; Schaltz, Erik

    2014-01-01

    . For geometries without ferrite, these zones can be defined only on basis of distance from coils. The simulation results indicate that magnetic field profile in the surroundings is influenced for ferrite based geometries and the three zones tend to overlap. This overlapping is studied via Comsol simulations...... profile of magnetic field emissions (with and without ferrite) for wireless power transfer to vehicles....

  17. Trapped electron effects on ICRF Current Drive Predictions in TFTR

    Science.gov (United States)

    Wright, John C.; Phillips, Cynthia K.; Bonoli, Paul T.

    1996-11-01

    Most 2D RF modeling codes use a parameterization^1 of current drive efficiencies to calculate fast wave driven currents. Because this parameterization is derived from a ray--tracing model, there are difficulties in applying it to a spectrum of waves. In addition, one cannot account for multiple resonances and coherency effects between the electrons and the waves. These difficulties may be avoided by a direct calculation of the quasilinear diffusion coefficient in an inhomogenous geometry coupled with a full wave code for the field polarizations. Current profiles are then calculated using the adjoint formulation^2, with the magnetic equilibrium specified consistently in both the adjoint routine and the full wave code. This approach has been implemented in the FISIC code^3. Results are benchmarked by comparing a power deposition calculation from conductivity to one from the quasilinear expression. It is shown that the two expressions agree. We quantify differences seen based upon aspect ratio and elongation. The largest discrepancies are seen in the regime of small aspect ratio, and little loss in accuracy for moderate aspect ratios ~>3. This work supported by DoE contract No. DE--AC02--76--CH03073. ^1 D. A. Ehst and C. F. F. Karney, Nucl. Fusion 31, 1933 (1991). ^2 C. F. F. Karney, Computer Physics Reports 4, 183 (1986). ^3 M. Brambilla and T. Krücken, Nucl. Fusion 28, 1813 (1988).

  18. Sonochemical Synthesis of Cobalt Ferrite Nanoparticles

    Directory of Open Access Journals (Sweden)

    Partha P. Goswami

    2013-01-01

    Full Text Available Cobalt ferrite being a hard magnetic material with high coercivity and moderate magnetization has found wide-spread applications. In this paper, we have reported the sonochemical synthesis of cobalt ferrite nanoparticles using metal acetate precursors. The ferrite synthesis occurs in three steps (hydrolysis of acetates, oxidation of hydroxides, and in situ microcalcination of metal oxides that are facilitated by physical and chemical effects of cavitation bubbles. The physical and magnetic properties of the ferrite nano-particles thus synthesized have been found to be comparable with those reported in the literature using other synthesis techniques.

  19. Biological synthesis of cobalt ferrite nanoparticles

    Directory of Open Access Journals (Sweden)

    Anal K. Jha

    2012-01-01

    Full Text Available A low-cost green and reproducible yeast (Saccharomyces cerevisiae mediated biosynthesis of cobalt ferrite nanoparticles is reported. The synthesis is performed at close to room temperature in the laboratory. X-ray, Fourier transform infrared spectroscopy and high resolution transmission electron microscopy analyses are performed to ascertain the formation of cobalt ferrite nanoparticles. Individual nanoparticles, as well as a very few aggregate having the size of 3-15 nm, were found. The vibrating sample magnetometer measurement showed superparamagnetic behavior in cobalt ferrite nanoparticles. The mechanism involved in the biosynthesis of cobalt ferrite nanoparticles has also been discussed.

  20. Modeling of austenite to ferrite transformation

    Indian Academy of Sciences (India)

    Mohsen Kazeminezhad

    2012-06-01

    In this research, an algorithm based on the -state Potts model is presented for modeling the austenite to ferrite transformation. In the algorithm, it is possible to exactly track boundary migration of the phase formed during transformation. In the algorithm, effects of changes in chemical free energy, strain free energy and interfacial energies of austenite–austenite, ferrite–ferrite and austenite–ferrite during transformation are considered. From the algorithm, the kinetics of transformation and mean ferrite grain size for different cooling rates are calculated. It is found that there is a good agreement between the calculated and experimental results.

  1. Microwave dielectric properties of nanostructured nickel ferrite

    Indian Academy of Sciences (India)

    John Jacob; M Abdul Khadar; Anil Lonappan; K T Mathew

    2008-11-01

    Nickel ferrite is one of the important ferrites used in microwave devices. In the present work, we have synthesized nanoparticles of nickel ferrite using chemical precipitation technique. The crystal structure and grain size of the particles are studied using XRD. The microwave dielectric properties of nanostructured nickel ferrite samples of three different average grain sizes and those of two sintered samples were studied. The parameters like dielectric constant, dielectric loss and heating coefficient of the nanoparticles samples are studied in the frequency range from 2.4 to 4 GHz. The values of these parameters are compared with those of sintered pellets of the same samples. All these parameters show size dependent variations.

  2. Microwave Ferrites for Cryogenic Applications

    OpenAIRE

    G. Dionne

    1997-01-01

    Recent advances in microwave ferrite device technology have seen the introduction of superconductivity that virtually eliminates insertion losses due to electrical conduction in microstrip circuits. The conventional ferrimagnetic spinel and garnet compositions, however, are not generally optimized for temperatures in the vicinity of 77 K and may require chemical redesign in order to realize the full potential of these devices. For microwave transmission, absorption losses may be reduced by a ...

  3. Progress in ferrite phase shifters

    Science.gov (United States)

    Boyd, C. R., Jr.

    1983-10-01

    Advances in the technology of reciprocal ferrite phase shifters are outlined. Nonlatching rotary-field phase shifters have been produced with enhanced phase accuracy and modest control power. A significant quantity of dual-mode latching units has been built at 35 GHz, with good results. Both types of phase shifter can be adapted to perform other functions in addition to phase shifting. Examples of phase shifters that perform duplexing and polarization switching functions are given.

  4. Spin canting in ferrite nanoparticles

    Energy Technology Data Exchange (ETDEWEB)

    Marx, J., E-mail: jmarx@physik.uni-kl.de; Huang, H.; Salih, K. S. M.; Thiel, W. R.; Schünemann, V. [University of Kaiserslautern, Department of Physics (Germany)

    2016-12-15

    Recently, an easily scalable process for the production of small (3 −7 nm) monodisperse superparamagnetic ferrite nanoparticles MeFe{sub 2}O{sub 4} (Me = Zn, Mn, Co) from iron metal and octanoic acid has been reported (Salih et al., Chem. Mater. 25 1430–1435 2013). Here we present a Mössbauer spectroscopic study of these ferrite nanoparticles in external magnetic fields of up to B = 5 T at liquid helium temperatures. Our analysis shows that all three systems show a comparable inversion degree and the cationic distribution for the tetrahedral A and the octahedral B sites has been determined to (Zn{sub 0.19}Fe{sub 0.81}){sup A}[Zn{sub 0.81}Fe{sub 1.19}] {sup B}O{sub 4}, (Mn{sub 0.15}Fe{sub 0.85}){sup A}[Mn{sub 0.85}Fe{sub 1.15}] {sup B}O{sub 4} and (Co{sub 0.27}Fe{sub 0.73}){sup A}[Co{sub 0.73}Fe{sub 1.27}] {sup B}O{sub 4}. Spin canting occurs presumably in the B-sites and spin canting angles of 33°, 51° and 59° have been determined for the zinc, the manganese, and the cobalt ferrite nanoparticles.

  5. Enlargement of Tuning Range in a Ferrite-Tuned Cavity Through Superposed Orthogonal and Parallel Magnetic Bias

    CERN Document Server

    Vollinger, C

    2013-01-01

    Conventional ferrite-tuned cavities operate either with bias fields that are orthogonal or parallel to the magnetic RF-field. For a cavity that tunes rapidly over an overall frequency range around 100-400 MHz with high Q, we use ferrite garnets exposed to an innovative new biasing method consisting of a superposition of perpendicular and parallel magnetic fields. This method leads to a significant enlargement of the high-Q cavity tuning range by defining an operation point close to the magnetic saturation and thus improving ferrite material behaviour. A further advantage of this technique is the fast tuning speed resulting from the fact that tuning is carried out either with pure parallel biasing, or together with a very small change of operating point from perpendicular bias. In this paper, several scaled test models of ferrite-filled resonators are shown; measurements on the set-ups are compared and discussed.

  6. Alloying design of oxide dispersion strengthened ferritic steel for long life FBRs core materials

    Science.gov (United States)

    Ukai, S.; Harada, M.; Okada, H.; Inoue, M.; Nomura, S.; Shikakura, S.; Asabe, K.; Nishida, T.; Fujiwara, M.

    1993-09-01

    Oxide dispersion strengthened (ODS) ferritic steels with excellent swelling resistance and superior high temperature strength are prospective cladding materials for advanced fast breeder reactors. The addition of Ti in 13Cr-3W ODS ferritic steels improved the high temperature strength remarkably by the formation of uniformly distributed ultra-fine oxide particles. ODS ferritic steels have a bamboo-like grain structure and a strong deformation texture. The decrease of creep rupture strength in the bi-axial direction compared to the uni-axial direction is attributed mainly to this unique bamboo grain structure. Nearly equivalent creep rupture strength for both bi-axial and uni-axial direction was successfully attained by introducing the α to γ transformation in ODS martensitic steel.

  7. Formation of austenite in high Cr ferritic/martensitic steels by high fluence neutron irradiation

    Science.gov (United States)

    Lu, Z.; Faulkner, R. G.; Morgan, T. S.

    2008-12-01

    High Cr ferritic/martensitic steels are leading candidates for structural components of future fusion reactors and new generation fission reactors due to their excellent swelling resistance and thermal properties. A commercial grade 12%CrMoVNb ferritic/martensitic stainless steel in the form of parent plate and off-normal weld materials was fast neutron irradiated up to 33 dpa (1.1 × 10 -6 dpa/s) at 400 °C and 28 dpa (1.7 × 10 -6 dpa/s) at 465 °C, respectively. TEM investigation shows that the fully martensitic weld metal transformed to a duplex austenite/ferrite structure due to high fluence neutron irradiation, the austenite was heavily voided (˜15 vol.%) and the ferrite was relatively void-free; whilst no austenite phases were detected in plate steel. Thermodynamic and phase equilibria software MTDATA has been employed for the first time to investigate neutron irradiation-induced phase transformations. The neutron irradiation effect is introduced by adding additional Gibbs free energy into the system. This additional energy is produced by high energy neutron irradiation and can be estimated from the increased dislocation loop density caused by irradiation. Modelling results show that neutron irradiation reduces the ferrite/austenite transformation temperature, especially for high Ni weld metal. The calculated results exhibit good agreement with experimental observation.

  8. Formation of austenite in high Cr ferritic/martensitic steels by high fluence neutron irradiation

    Energy Technology Data Exchange (ETDEWEB)

    Lu, Z. [IPTME, Loughborough University, Loughborough LE11 3U (United Kingdom)], E-mail: zheng.lu@lboro.ac.uk; Faulkner, R.G.; Morgan, T.S. [IPTME, Loughborough University, Loughborough LE11 3U (United Kingdom)

    2008-12-01

    High Cr ferritic/martensitic steels are leading candidates for structural components of future fusion reactors and new generation fission reactors due to their excellent swelling resistance and thermal properties. A commercial grade 12%CrMoVNb ferritic/martensitic stainless steel in the form of parent plate and off-normal weld materials was fast neutron irradiated up to 33 dpa (1.1 x 10{sup -6} dpa/s) at 400 deg. C and 28 dpa (1.7 x 10{sup -6} dpa/s) at 465 deg. C, respectively. TEM investigation shows that the fully martensitic weld metal transformed to a duplex austenite/ferrite structure due to high fluence neutron irradiation, the austenite was heavily voided ({approx}15 vol.%) and the ferrite was relatively void-free; whilst no austenite phases were detected in plate steel. Thermodynamic and phase equilibria software MTDATA has been employed for the first time to investigate neutron irradiation-induced phase transformations. The neutron irradiation effect is introduced by adding additional Gibbs free energy into the system. This additional energy is produced by high energy neutron irradiation and can be estimated from the increased dislocation loop density caused by irradiation. Modelling results show that neutron irradiation reduces the ferrite/austenite transformation temperature, especially for high Ni weld metal. The calculated results exhibit good agreement with experimental observation.

  9. Optimization and testing results of Zr-bearing ferritic steels

    Energy Technology Data Exchange (ETDEWEB)

    Tan, Lizhen [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Yang, Ying [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Tyburska-Puschel, Beata [Univ. of Wisconsin, Madison, WI (United States); Sridharan, K. [Univ. of Wisconsin, Madison, WI (United States)

    2014-09-01

    The mission of the Nuclear Energy Enabling Technologies (NEET) program is to develop crosscutting technologies for nuclear energy applications. Advanced structural materials with superior performance at elevated temperatures are always desired for nuclear reactors, which can improve reactor economics, safety margins, and design flexibility. They benefit not only new reactors, including advanced light water reactors (LWRs) and fast reactors such as sodium-cooled fast reactor (SFR) that is primarily designed for management of high-level wastes, but also life extension of the existing fleet when component exchange is needed. Developing and utilizing the modern materials science tools (experimental, theoretical, and computational tools) is an important path to more efficient alloy development and process optimization. Ferritic-martensitic (FM) steels are important structural materials for nuclear reactors due to their advantages over other applicable materials like austenitic stainless steels, notably their resistance to void swelling, low thermal expansion coefficients, and higher thermal conductivity. However, traditional FM steels exhibit a noticeable yield strength reduction at elevated temperatures above ~500°C, which limits their applications in advanced nuclear reactors which target operating temperatures at 650°C or higher. Although oxide-dispersion-strengthened (ODS) ferritic steels have shown excellent high-temperature performance, their extremely high cost, limited size and fabricability of products, as well as the great difficulty with welding and joining, have limited or precluded their commercial applications. Zirconium has shown many benefits to Fe-base alloys such as grain refinement, improved phase stability, and reduced radiation-induced segregation. The ultimate goal of this project is, with the aid of computational modeling tools, to accelerate the development of a new generation of Zr-bearing ferritic alloys to be fabricated using conventional

  10. Microwave Measurements of Ferrite Polymer Composite Materials

    Directory of Open Access Journals (Sweden)

    Rastislav Dosoudil

    2004-01-01

    Full Text Available The article focuses on the microwave measurements performed on the nickel-zinc sintered ferrite with the chemical formula Ni0.3Zn0.7Fe2O4 produced by the ceramic technique and composite materials based on this ferrite and a non-magnetic polymer (polyvinyl chloride matrix. The prepared composite samples had the same particle size distribution 0-250um but different ferrite particle concentrations between 23 vol% and 80 vol%. The apparatus for measurement of the signal proportional to the absolute value of scattering parameter S11 (reflexion coefficient is described and the dependence of measured reflected signal on a bias magnetic field has been studied. By means of experiments, the resonances to be connected with the geometry of microwave experimental set-up were distinguished from ferromagnetic resonance arising in ferrite particles of composite structure. The role of local interaction fields of ferrite particles in composite material has been discussed.

  11. The ICRF-3: Status, Plans, and Multi-wavelength Progress on the next generation Celestial Reference Frame.

    Science.gov (United States)

    Jacobs, Christopher

    2015-08-01

    ICRF-3 seeks to improve upon the highly successful ICRF-2. Our goals are to improve the precision, spatial and frequency coverage relative to the ICRF-2 by 2018. This date is driven by the desire to create radio frames that are ready for comparison with the Gaia optical frame.Several specific actions are underway. A collaboration to improve at S/X-band precision of the Very Long Baseline Array (VLBA) Calibrator Survey's ~2200 sources, which are typically 5 times less precise than the rest of the ICRF-2, is bearing fruit and is projected to yield a factor of 3 improvement in precision. S/X-band southern hemisphere precision improvements are underway with observations using southern antennas such as the AuScope, Warkworth, and HartRAO, South Africa.We also seek to improve radio frequency coverage with X/Ka-band and K-band work. An X/Ka frame of 660 sources now has full sky coverage from the addition of a 2nd southern station in Argentina which is strengthening the southern hemisphere in general. The X/Ka-band frame's precision is now comparable to the ICRF-2 for the 530 sources in common. A K-band collaboration has formed with similar coverage and southern precision goals. By the time of this meeting, we expect K-band to complete full sky coverage with south polar cap observations and to improve spatial density north of -30 deg declination with VLBA observations.On the analysis front, special attention is being given to combination techniques both of Very Long Baseline Interferometry (VLBI) frames and of multiple data types. Consistency of the Celestial Reference Frame (CRF) with the Terrestrial Reference Frame (TRF) and Earth Oreintation Parameters (EOP) is another area of concern. Comparison of celestial frame solutions from various groups is underway in order to identify and correct systematic errors. We will discuss evidence emerging for 100 µas zonal errors in the ICRF2 in the declination range from 0 to -30 deg.Finally, work is underway to identify and

  12. Two frequency ICRF heating of D-T plasmas on TFTR

    Energy Technology Data Exchange (ETDEWEB)

    Rogers, J.H.; Majeski, R.; Wilson, J.R.; Hosea, J.C.; Schilling, G.; Stevens, J. [Princeton Univ., NJ (United States). Plasma Physics Lab.; Ho, Y.L. [Science Applications International Corp., San Diego, CA (United States); Raman, S. [Michigan Univ., Ann Arbor, MI (United States); Rasmussen, D.A. [Oak Ridge National Lab., TN (United States)

    1993-11-01

    Modifications have been made to allow two of the ICRF antennas (bays L and M) on TFTR to operate at either of two frequencies, 43 MHz or 64 MHz. This was accomplished by lengthening the resonant loops feeding the antennas (2{lambda} at 43 MHz, 3{lambda} at 64 MHz) and replacing the conventional quarter wave impedance transformers with a tapered impedance design. The other two antennas (bays K and N) will operate at a fixed frequency, 43 MHz. The two frequency operation allows a combination of {sup 3}He-minority (or T second harmonic) and H-minority heating at full toroidal field on TFIR. Multiple frequency operation may also be useful in direct electron heating and current drive experiments. Other modifications have been made which are expected to permit arbitrary phasing between the current straps on bays M and L. The system design of the antenna, resonant loops and impedance matching system as well as preliminary TFTR results are discussed.

  13. Observation of Electron Energy Pinch in HT-7 ICRF Heated Plasmas

    Science.gov (United States)

    Ding, Siye; Wan, Baonian; Wang, Lu; Ti, Ang; Zhang, Xinjun; Liu, Zixi; Qian, Jinping; Zhong, Guoqiang; Duan, Yanmin

    2014-09-01

    Inward energy transport (pinch phenomenon) in the electron channel is observed in HT-7 plasmas using off-axis ion cyclotron resonance frequency (ICRF) heating. Experimental results and power balance transport analysis by TRANSP code are presented in this article. With the aids of GLF23 and Chang-Hinton transport models, which predict energy diffusivity in experimental conditions, the estimated electron pinch velocity is obtained by experimental data and is found reasonably comparable to the results in the previous study, such as Song on Tore Supra. Density scanning shows that the energy convective velocity in the electron channel has a close relation to density scale length, which is qualitatively in agreement with Wang's theoretical prediction. The parametric dependence of electron energy convective velocity on plasma current is still ambiguous and is worthy of future research on EAST.

  14. Making ICRF power compatible with a high-Z wall in ASDEX Upgrade

    Science.gov (United States)

    Bobkov, V.; Aguiam, D.; Bilato, R.; Brezinsek, S.; Colas, L.; Faugel, H.; Fünfgelder, H.; Herrmann, A.; Jacquot, J.; Kallenbach, A.; Milanesio, D.; Maggiora, R.; Neu, R.; Noterdaeme, J.-M.; Ochoukov, R.; Potzel, S.; Pütterich, T.; Silva, A.; Tierens, W.; Tuccilo, A.; Tudisco, O.; Wang, Y.; Yang, Q.; Zhang, W.; ASDEX Upgrade Team; the EUROfusion MST1 Team

    2017-01-01

    A comparison of the ASDEX Upgrade 3-strap ICRF antenna data with the linear electro-magnetic TOPICA calculations is presented. The comparison substantiates a reduction of the local electric field at the radially protruding plasma-facing elements of the antenna as a relevant approach for minimizing tungsten (W) sputtering in conditions when the slow wave is strongly evanescent. The measured reaction of the time-averaged RF current at the antenna limiters to the antenna feeding variations is less sensitive than predicted by the calculations. This is likely to have been caused by temporal and spatial fluctuations in the 3D plasma density distribution affected by local non-linear interactions. The 3-strap antenna with the W-coated limiters produces drastically less W sputtering compared to the W-coated 2-strap antennas. This is consistent with the non-linear asymptotic SSWICH-SW calculations for RF sheaths.

  15. Delta ferrite in the weld metal of reduced activation ferritic martensitic steel

    Science.gov (United States)

    Sam, Shiju; Das, C. R.; Ramasubbu, V.; Albert, S. K.; Bhaduri, A. K.; Jayakumar, T.; Rajendra Kumar, E.

    2014-12-01

    Formation of delta(δ)-ferrite in the weld metal, during autogenous bead-on-plate welding of Reduced Activation Ferritic Martensitic (RAFM) steel using Gas Tungsten Arc Welding (GTAW) process, has been studied. Composition of the alloy is such that delta-ferrite is not expected in the alloy; but examination of the weld metal revealed presence of delta-ferrite in the weld metal. Volume fraction of delta-ferrite is found to be higher in the weld interface than in the rest of the fusion zone. Decrease in the volume fraction of delta-ferrite, with an increase in preheat temperature or with an increase in heat input, is observed. Results indicate that the cooling rate experienced during welding affects the volume fraction of delta-ferrite retained in the weld metal and variation in the delta-ferrite content with cooling rate is explained with variation in the time that the weld metal spends in various temperature regimes in which delta-ferrite is stable for the alloy during its cooling from the liquid metal to the ambient temperature. This manuscript will discuss the effect of welding parameters on formation of delta-ferrite and its retention in the weld metal of RAFM steel.

  16. Theoretical study for ICRF sustained LHD type p-{sup 11}B reactor

    Energy Technology Data Exchange (ETDEWEB)

    Watanabe, Tsuguhiro (ed.)

    2003-04-01

    This is a summary of the workshop on 'Theoretical Study for ICRF Sustained LHD Type p-{sup 11}B Reactor' held in National Institute for Fusion Science (NIFS) on July 25, 2002. In the workshop, study of LHD type D-{sup 3}He reactor is also reported. A review concerning the advanced nuclear fusion fuels is also attached. This review was reported at the workshop of last year. The development of the p-{sup 11}B reactor research which uses the LHD magnetic field configuration has been briefly summarized in section 1. In section 2, an integrated report on advanced nuclear fusion fuels is given. Ignition conditions in a D-{sup 3}He helical reactor are summarized in section 3. 0-dimensional particle and power balance equations are solved numerically assuming the ISS95 confinement law including a confinement factor ({gamma}{sub HH}). It is shown that high average beta plasma confinement, a large confinement factor ({gamma}{sub HH} > 3) and the hot ion mode (T{sub i}/T{sub e} > 1.4) are necessary to achieve the ignition of the D-{sup 3}He helical reactor. Characteristics of ICRF sustained p-{sup 11}B reactor are analyzed in section 4. The nuclear fusion reaction rate < {sigma}{upsilon} > is derived assuming a quasilinear plateau distribution function (QPDF) for protons, and an ignition condition of p-{sup 11}B reactor is shown to be possible. The 3 of the presented papers are indexed individually. (J.P.N.)

  17. OPTICAL SPECTRA OF CANDIDATE INTERNATIONAL CELESTIAL REFERENCE FRAME (ICRF) FLAT-SPECTRUM RADIO SOURCES

    Energy Technology Data Exchange (ETDEWEB)

    Titov, O.; Stanford, Laura M. [Geoscience Australia, P.O. Box 378, Canberra, ACT 2601 (Australia); Johnston, Helen M.; Hunstead, Richard W. [Sydney Institute for Astronomy, School of Physics, University of Sydney, NSW 2006 (Australia); Pursimo, T. [Nordic Optical Telescope, Nordic Optical Telescope Apartado 474E-38700 Santa Cruz de La Palma, Santa Cruz de Tenerife (Spain); Jauncey, David L. [CSIRO Astronomy and Space Science, ATNF and Research School of Astronomy and Astrophysics, Australian National University, Canberra, ACT 2611 (Australia); Maslennikov, K. [Central Astronomical Observatory at Pulkovo, Pulkovskoye Shosse, 65/1, 196140, St. Petersburg (Russian Federation); Boldycheva, A., E-mail: oleg.titov@ga.gov.au [Ioffe Physical Technical Institute, 26 Polytekhnicheskaya, St. Petersburg, 194021 (Russian Federation)

    2013-07-01

    Continuing our program of spectroscopic observations of International Celestial Reference Frame (ICRF) sources, we present redshifts for 120 quasars and radio galaxies. Data were obtained with five telescopes: the 3.58 m European Southern Observatory New Technology Telescope, the two 8.2 m Gemini telescopes, the 2.5 m Nordic Optical Telescope (NOT), and the 6.0 m Big Azimuthal Telescope of the Special Astrophysical Observatory in Russia. The targets were selected from the International VLBI Service for Geodesy and Astrometry candidate International Celestial Reference Catalog which forms part of an observational very long baseline interferometry (VLBI) program to strengthen the celestial reference frame. We obtained spectra of the potential optical counterparts of more than 150 compact flat-spectrum radio sources, and measured redshifts of 120 emission-line objects, together with 19 BL Lac objects. These identifications add significantly to the precise radio-optical frame tie to be undertaken by Gaia, due to be launched in 2013, and to the existing data available for analyzing source proper motions over the celestial sphere. We show that the distribution of redshifts for ICRF sources is consistent with the much larger sample drawn from Faint Images of the Radio Sky at Twenty cm (FIRST) and Sloan Digital Sky Survey, implying that the ultra-compact VLBI sources are not distinguished from the overall radio-loud quasar population. In addition, we obtained NOT spectra for five radio sources from the FIRST and NRAO VLA Sky Survey catalogs, selected on the basis of their red colors, which yielded three quasars with z > 4.

  18. Effect on the Tritium Breeding Ratio due to a distributed ICRF antenna in a DEMO reactor

    Energy Technology Data Exchange (ETDEWEB)

    Garcia, A., E-mail: albert.garcia.hp@gmail.com [Max-Planck-Institut für Plasmaphysik (IPP), Garching (Germany); Karlsruhe Institute of Technology (KIT), Karlsruhe (Germany); Polytechnic University of Catalonia (UPC), Barcelona (Spain); Department of Applied Physics, Ghent University, Ghent (Belgium); Noterdaeme, J.-M. [Max-Planck-Institut für Plasmaphysik (IPP), Garching (Germany); Department of Applied Physics, Ghent University, Ghent (Belgium); Fischer, U. [Karlsruhe Institute of Technology (KIT), Karlsruhe (Germany); Dies, J. [Polytechnic University of Catalonia (UPC), Barcelona (Spain)

    2016-11-15

    This thesis reports results of MCNP-5 calculations, with the nuclear data library FENDL-2.1, to assess the effect on the Tritium Breeding Ratio (TBR) due to a distributed Ion Cyclotron Range of Frequencies (ICRF) antenna integrated in the blanket of a DEMO fusion power reactor. A preliminary design of the antenna with a reference configuration of the DEMO reactor was used together with a parametric analysis for different parameters that strongly affect the TBR. These are the type of breeding blanket (Helium Cooled Pebble Bed, Helium Cooled Lithium Lead and Water Cooled Lithium Lead), the covering ratio of the straps of the antenna (the ratio between the surface of all the straps and the projected surface of the antenna slot: 0.49, 0.72 and 0.94), the antenna radial thickness (20 cm and 40 cm), the thickness of the straps (2 cm, 4 cm and a double layer of 0.2 cm plus 2.5 cm with the composition of the First Wall), and finally the poloidal position of the antenna (0°, which is the equatorial port, 40° and 90°, which is the upper port). For an antenna with a full toroidal circumference of 360°, located poloidaly at 40° with a poloidal extension of 1 m and a total First Wall surface of 67 m{sup 2}, the reduction of the TBR is −0.35% for a HCPB blanket concept, −0.53% for a HCLL blanket concept and −0.51% for a WCLL blanket concept. In all cases covered by the parametric analysis, the loss of TBR remains below 0.61%. Such a distributed ICRF antenna has thus only a marginal effect on the TBR for a DEMO reactor.

  19. Measurement and simulation of ICRF wave intensity with a recalibrated phase contrast imaging diagnostic on Alcator C-Mod

    Energy Technology Data Exchange (ETDEWEB)

    Tsujii, N., E-mail: tsujii@k.u-tokyo.ac.jp [The University of Tokyo, Kashiwa (Japan); Porkolab, M.; Bonoli, P. T.; Edlund, E. M.; Ennever, P. C.; Lin, Y.; Wright, J. C.; Wukitch, S. J. [MIT Plasma Science and Fusion Center, Cambridge, Massachusetts (United States); Jaeger, E. F. [XCEL Engineering, Oak Ridge, Tennessee (United States); Green, D. L. [Oak Ridge National Laboratory, Oak Ridge, Tennessee (United States); Harvey, R. W. [CompX, Del Mar, California (United States)

    2015-12-10

    Waves in the ion cyclotron range of frequencies (ICRF) are one of the major tools to heat fusion plasmas. Full-wave simulations are essential to predict the wave propagation and absorption quantitatively, and it is important that these codes be validated against actual experimental measurements. In this work, the absolute intensity of the ICRF waves previously measured with a phase contrast imaging diagnostic was recalibrated and compared once more with full-wave predictions. In the earlier work, significant discrepancies were found between the measured and the simulated mode converted wave intensity [N. Tsujii et al., Phys. Plasmas 19, 082508]. With the new calibration of the detector array, the measured mode converted wave intensity is now in much better agreement with the full-wave predictions. The agreement is especially good for comparisons performed close to the antenna.

  20. High beta and second region stability analysis and ICRF edge modeling. Progress report, March 15, 1988--May 14, 1989

    Energy Technology Data Exchange (ETDEWEB)

    1989-12-31

    This report describes the tasks accomplished under Department of Energy contract {number_sign}DE-FG02-86ER53236 in modeling the edge plasma-antenna interaction that occurs during Ion Cyclotron Range of Frequency (ICRF) heating. This work has resulted in the development of several codes which determine kinetic and fluid modifications to the edge plasma. When used in combination, these code predict the level of impurity generation observed in experiments on the experiments on the Princeton Large Torus. In addition, these models suggest improvements to the design of ICRF antennas. Also described is progress made on high beta and second region analysis. Code development for a comprehensive infernal mode analysis code is nearing completion. A method has been developed for parameterizing the second region of stability and is applied to circular cross section tokamas. Various studies for high beta experimental devices such as PBX-M and DIII-D have been carried out and are reported on.

  1. Tailoring magnetic and dielectric properties of rubber ferrite composites containing mixed ferrites

    Indian Academy of Sciences (India)

    M R Anantharaman; K A Malini; S Sindhu; E M Mohammed; S K Date; S D Kulkarni; P A Joy; Philip Kurian

    2001-12-01

    Rubber ferrite composites containing various mixed ferrites were prepared for different compositions and various loadings. The magnetic and dielectric properties of the fillers as well as the ferrite filled matrixes were evaluated separately. The results are correlated. Simple equations are proposed to predetermine the magnetic and dielectric properties. The validity of these equations is verified and they are found to be in good agreement. These equations are useful in tailoring the magnetic and dielectric properties of these composites with predetermined properties.

  2. Spinel ferrite thin-film synthesis by spin-spray ferrite plating

    Energy Technology Data Exchange (ETDEWEB)

    Hai, Tran Hoang; Van, Ha Thi Bich; Phong, Tran Canh; Abe, Masanori

    2003-04-01

    By spin-spray ferrite plating with optimizing conditions in the oxidizing and reaction solutions, we can synthesize polycrystalline ferrite film of spinel type (Fe, M){sub 3}O{sub 4}, where M=Fe, Co, Ni, Zn, etc., in low temperatures (<100 deg. C). By this method we can synthesize Co, Co-Ni ferrite for perpendicular magnetic recording media with high coercivity H{sub c} in the plane perpendicular to the film.

  3. Effects of outer top gas injection on ICRF coupling in ASDEX Upgrade: towards modelling of ITER gas injection

    Science.gov (United States)

    Zhang, W.; Bobkov, V.; Noterdaeme, J.-M.; Tierens, W.; Bilato, R.; Carralero, D.; Coster, D.; Jacquot, J.; Jacquet, P.; Lunt, T.; Pitts, R. A.; Rohde, V.; Siegl, G.; Fuenfgelder, H.; Aguiam, D.; Silva, A.; Colas, L.; Ceccuzzi, S.; the ASDEX Upgrade Team

    2017-07-01

    The influence of outer top gas injection on the scrape-off layer (SOL) density and ion cyclotron range of frequency (ICRF) coupling has been studied in ASDEX Upgrade (AUG) L-mode plasmas for the first time. The three-dimensional (3D) edge plasma fluid and neutral transport code EMC3-EIRENE is used to simulate the SOL plasma density, and the 3D wave code RAPLICASOL is used to compute the ICRF coupling resistance with the calculated density. Improvements have been made in the EMC3-EIRENE simulations by fitting transport parameters separately for each gas puffing case. It is found that the calculated local density profiles and coupling resistances are in good agreement with the experimental ones. The results indicate that the SOL density increase depends sensitively on the spreading of the injected outer top gas. If more gas enters into the main chamber through the paths near the top of vessel, the SOL density increase will be more toroidally uniform; if more gas chooses the paths closer to the mid-plane, then the SOL density increase will be more local and more significant. Among the various local gas puffing methods, the mid-plane gas valve close to the antenna is still the best option in terms of improving ICRF coupling. Differences between the outer top gas puffing in AUG and the outer top gas puffing in ITER are briefly summarized. Instructive suggestions for ITER and future plans for ITER gas injection simulations are discussed.

  4. Structural analysis of emerging ferrite: Doped nickel zinc ferrite

    Energy Technology Data Exchange (ETDEWEB)

    Kumar, Rajinder; Kumar, Hitanshu; Singh, Ragini Raj; Barman, P. B., E-mail: pb.barman@juit.ac.in [Nanotechnology Lab, Department of Physics & Materials Science, Jaypee University of Information Technology, Waknaghat, Solan (H.P)-173234 (India)

    2015-08-28

    Ni{sub 0.6-x}Zn{sub 0.4}Co{sub x}Fe{sub 2}O{sub 4} (x = 0, 0.033, 0.264) nanoparticles were synthesized by sol-gel method and annealed at 900°C. Structural properties of all prepared samples were examined with X-ray diffraction (XRD). The partial formation of hematite (α-Fe{sub 2}O{sub 3}) secondary phase with spinel phase cubic structure of undoped and cobalt doped nickel zinc ferrite was found by XRD peaks. The variation in crystallite size and other structural parameters with cobalt doping has been calculated for most prominent peak (113) of XRD and has been explained on the basis of cations ionic radii difference.

  5. Manganese ferrite thin films Part II: Properties

    NARCIS (Netherlands)

    Hulscher, W.S.

    1972-01-01

    Some properties of evaporated manganese ferrite thin films are investigated, e.g. resistivity, magnetization reversal, Curie temperature, Faraday rotation and optical absorption. The properties are partly related to the partial oxygen pressure present during a preceding annealing process.

  6. ALL-FERRITE RHIC INJECTION KICKER

    Energy Technology Data Exchange (ETDEWEB)

    HAHN,H.; FISCHER,W.; PTITSYN,V.I.; TUOZZOLO,J.E.

    2001-06-18

    Ion beams are transferred from the AGS into RHIC in boxcar fashion as single bunches. The nominal design assumes 60 bunches per ring but increasing the number of bunches to gain luminosity is possible, thereby requiring injection kickers with a shorter rise time. The original injection system consists of traveling-wave dielectric loaded kicker magnets and a Blumlein pulser with a rise time adequate for the present operation. Voltage breakdown in the dielectric kickers suggested the use of all-ferrite magnets. In order to minimize the conversion cost, the design of the all-ferrite kicker uses the same components as the dielectric loaded units. The all-ferrite kickers showed in bench measured good breakdown properties and a current rise time of < 50 ns. A prototype kicker has been installed in the blue ring and was tested with beam. Beam measurements indicate suitability of all-ferrite kicker magnets for upgraded operation.

  7. Ferrite HOM Absorber for the RHIC ERL

    Energy Technology Data Exchange (ETDEWEB)

    Hahn,H.; Choi, E.M.; Hammons, L.

    2008-10-01

    A superconducting Energy Recovery Linac is under construction at Brookhaven National Laboratory to serve as test bed for RHIC upgrades. The damping of higher-order modes in the superconducting five-cell cavity for the Energy-Recovery linac at RHIC is performed exclusively by two ferrite absorbers. The ferrite properties have been measured in ferrite-loaded pill box cavities resulting in the permeability values given by a first-order Debye model for the tiled absorber structure and an equivalent permeability value for computer simulations with solid ring dampers. Measured and simulated results for the higher-order modes in the prototype copper cavity are discussed. First room-temperature measurements of the finished niobium cavity are presented which confirm the effective damping of higher-order modes in the ERL. by the ferrite absorbers.

  8. Ferrite Nanoparticles in Pharmacological Modulation of Angiogenesis

    Science.gov (United States)

    Deshmukh, Aparna; Radha, S.; Khan, Y.; Tilak, Priya

    2011-07-01

    Nanoparticles are being explored in the targeted drug delivery of pharmacological agents : angiogenesis being one such novel application which involves formation of new blood vessels or branching of existing ones. The present study involves the use of ferrite nanoparticles for precise therapeutic modulation of angiogenesis. The ferrite nanoparticles synthesized by co-precipitation of ferrous and ferric salts by a suitable base, were found to be 10-20 nm from X-ray diffraction and TEM measurements. The magnetization measurements showed superparamagnetic behavior of the uncoated nanoparticles. These ferrite nanoparticles were found to be bio-compatible with lymphocytes and neural cell lines from the biochemical assays. The chick chorioallantoic membrane(CAM) from the shell of fertile white Leghorn eggs was chosen as a model to study angiogenic activity. An enhancement in the angiogenic activity in the CAM due to addition of uncoated ferrite nanoparticles was observed.

  9. Development and application of ferrite materials for low temperature co-fired ceramic technology

    Science.gov (United States)

    Zhang, Huai-Wu; Li, Jie; Su, Hua; Zhou, Ting-Chuan; Long, Yang; Zheng, Zong-Liang

    2013-11-01

    Development and application of ferrite materials for low temperature co-fired ceramic (LTCC) technology are discussed, specifically addressing several typical ferrite materials such as M-type barium ferrite, NiCuZn ferrite, YIG ferrite, and lithium ferrite. In order to permit co-firing with a silver internal electrode in LTCC process, the sintering temperature of ferrite materials should be less than 950 °C. These ferrite materials are research focuses and are applied in many ways in electronics.

  10. Polymer bonded ferrite materials as EMC components

    Energy Technology Data Exchange (ETDEWEB)

    Toepfer, J. [Fachhochschule Jena, FB Werkstofftechnik, Carl-Zeiss-Promenade 2, 07745 Jena (Germany); Hermsdorfer Institut fuer Technische Keramik e.V., M.-Curie-Str. 17, 07629 Hermsdorf (Germany); Pawlowski, B. [Hermsdorfer Institut fuer Technische Keramik e.V., M.-Curie-Str. 17, 07629 Hermsdorf (Germany); Graebner, F. [IMG Nordhausen, An der Salza 8a, 99734 Nordhausen (Germany)

    2003-07-01

    Polymer bonded ferrites composed of a mixture of Mn-Zn ferrites or Ni-Zn ferrites in a polymer binder (PE, PA) were prepared and tested as electromagnetic-wave absorbing materials. Test samples and cases were prepared by hot or injection molding. Permeability spectra show loss contributions in the frequency range 100-1000 MHz. Absorption measurements of injection molded polymer-ferrite cases display a 3-5 dB better attenuation characteristics compared to graphite-loaded polyamide housings. (Abstract Copyright [2003], Wiley Periodicals, Inc.) [German] Polymer-gebundene Ferritwerkstoffe auf der Basis von Ferrit (Mn-Zn oder Ni-Zn Ferrite) - Thermoplast Mischungen wurden praepariert und hinsichtlich ihrer Eignung zur Absorption elektromagnetischer Strahlung untersucht. Es wurden sowohl Testproben wie auch komplette Gehaeusekomponenten durch Heisspressen oder Spritzgiessen hergestellt. Die Permeabilitaetsspektren weisen verlustbehaftete Komponenten im Frequenzbereich von 100-1000 MHz auf. Schirmdaempfungsmessungen an spritzgegossenen Gehaeuseteilen zeigen eine um 3-5 dB bessere Daempfung im Vergleich zu Graphit-gefuellten Polyamid-Gehaeusen. (Abstract Copyright [2003], Wiley Periodicals, Inc.)

  11. Influence of the blanket shield modules geometry on the operation of the ITER ICRF antenna

    Energy Technology Data Exchange (ETDEWEB)

    Louche, F., E-mail: fabrice.louche@rma.ac.be [Laboratory for Plasma Physics, Royal Military Academy, 30, Avenue de la Renaissance, 1000 Brussels (Belgium); Dumortier, P.; Durodié, F.; Messiaen, A. [Laboratory for Plasma Physics, Royal Military Academy, 30, Avenue de la Renaissance, 1000 Brussels (Belgium)

    2013-10-15

    Highlights: ► The ITER ICRF antenna and its surrounding blanket shield modules have been modeled with the 3D electromagnetic software Microwave Studio. ► Unexpected resonances are detected in the ITER relevant range of frequencies. ► These resonances are caused by the geometry of the modules, and in particular by the cavity at the back, between the module rear face and the port plug outer face, present in the considered model. ► Simplified modeling and transmission line computations validate this interpretation. ► The resonance is strongly dependent on the detailed geometry of the modules, but large voids should be avoided. -- Abstract: Three-dimensional electromagnetic simulations of the ITER ICRF antenna have been recently performed with the commercial code CST Microwave Studio{sup ®} (MWS) [1]. A detailed model imported from the CATIA{sup ®} file has been considered: it includes the 24 straps array (CY3.1 geometry [2]) and the surrounding blanket shield modules. The transient solver in MWS has detected the presence of a very localized peak in the input impedance matrix at a frequency of approximately 51 MHz in vacuum conditions. The presence of such a resonance in the ITER operating range of frequency is of concern and should be understood as previous analysis reported in [3] concluded that TEM and non-TEM modes are not expected in this frequency band as long as the antenna is grounded to the port at 1 m back from the antenna front face. By using a simplified model of the geometry we demonstrate that the resonance is a consequence of the considered geometry of the blanket shield modules and in particular of the cavity at the back of the modules made of the module attachment and the port plug outer face. We show that the presence of such a cavity locally increases the coaxial line impedance and allows for a TEM mode in the band. This physical analysis is supported by a transmission line model where the system made of the antenna and its surrounding

  12. Maximization of ICRF power by SOL density tailoring with local gas injection

    Science.gov (United States)

    Jacquet, P.; Goniche, M.; Bobkov, V.; Lerche, E.; Pinsker, R. I.; Pitts, R. A.; Zhang, W.; Colas, L.; Hosea, J.; Moriyama, S.; Wang, S.-J.; Wukitch, S.; Zhang, X.; Bilato, R.; Bufferand, H.; Guimarais, L.; Faugel, H.; Hanson, G. R.; Kocan, M.; Monakhov, I.; Noterdaeme, J.-M.; Petrzilka, V.; Shaw, A.; Stepanov, I.; Sips, A. C. C.; Van Eester, D.; Wauters, T.; JET contributors, the; the ASDEX Upgrade Team; the DIII-D Team; ITPA ‘Integrated Operation Scenarios' members, the; experts

    2016-04-01

    Experiments have been performed under the coordination of the International Tokamak Physics Activity (ITPA) on several tokamaks, including ASDEX Upgrade (AUG), JET and DIII-D, to characterize the increased Ion cyclotron range of frequency (ICRF) antenna loading achieved by optimizing the position of gas injection relative to the RF antennas. On DIII-D, AUG and JET (with the ITER-Like Wall) a 50% increase in the antenna loading was observed when injecting deuterium in ELMy H-mode plasmas using mid-plane inlets close to the powered antennas instead of divertor injection and, with smaller improvement when using gas inlets located at the top of the machine. The gas injection rate required for such improvements (~0.7  ×  1022 el s-1 in AUG, ~1.0  ×  1022 el s-1 in JET) is compatible with the use of this technique to optimize ICRF heating during the development of plasma scenarios and no degradation of confinement was observed when using the mid-plane or top inlets compared with divertor valves. An increase in the scrape-off layer (SOL) density was measured when switching gas injection from divertor to outer mid-plane or top. On JET and DIII-D, the measured SOL density increase when using main chamber puffing is consistent with the antenna coupling resistance increase provided that the distance between the measurement lines of sight and the injection location is taken into account. Optimized gas injection was also found to be beneficial for reducing tungsten (W) sputtering at the AUG antenna limiters, and also to reduce slightly the W and nickel (Ni) content in JET plasmas. Modeling the specific effects of divertor/top/mid-plane injection on the outer mid-plane density was carried out using both the EDGE2D-EIRENE and EMC3-EIRENE plasma boundary code packages; simulations indeed indicate that outer mid-plane gas injection maximizes the density in the mid-plane close to the injection point with qualitative agreement with the AUG SOL density measurements

  13. Irradiation creep of various ferritic alloys irradiated {approximately}400 C in the PFR and FFTF reactors

    Energy Technology Data Exchange (ETDEWEB)

    Toloczko, M.B. [Washington State Univ., WA (United States); Garner, F.A. [Pacific Northwest National Lab., Richland, WA (United States); Eiholzer, C.R. [Westinghouse Hanford Co., WA (United States)

    1998-03-01

    Three ferritic alloys were irradiated in two fast reactors to doses of 50 dpa or more at temperatures near 400 C. One martensitic alloy, HT9, was irradiated in both the FFTF and PFR reactors. PFR is the Prototype Fast Reactor in Dourneay, Scotland, and FFTF is the Fast Flux Test Facility in Richland, WA. D57 is a developmental alloy that was irradiated in PFR only, and MA957 is a Y{sub 2}O{sub 3} dispersion-hardened ferritic alloy that was irradiated only in FFTF. These alloys exhibited little or no void swelling at {approximately}400 C. Depending on the alloy starting condition, these steels develop a variety of non-creep strains early in the irradiation that are associated with phase changes. Each of these alloys creeps at a rate that is significantly lower than that of austenitic steels irradiated in the same experiments. The creep compliance for ferritic alloys in general appears to be {approximately}0.5 {times} 10{sup {minus}6} MPa{sup {minus}1} dpa{sup {minus}1}, independent of both composition and starting state. The addition of Y{sub 2}O{sub 3} as a dispersoid does not appear to change the creep behavior.

  14. A Global Astrometric Solution for Pan-STARRS referenced to ICRF2

    CERN Document Server

    Berghea, C T; Frouard, J; Hennessy, G S; Dorland, B N; Veillette, D R; Dudik, R P; Magnier, E A; Burgett, W S; Chambers, K C; Denneau, L; Flewelling, H; Kaiser, N; Tonry, J L; Wainscoat, R J; Sesar, B

    2016-01-01

    We describe development and application of a Global Astrometric Solution (GAS) to the problem of Pan-STARRS1 (PS1) astrometry. Current PS1 astrometry is based on differential astrometric measurements using 2MASS reference stars, thus PS1 astrometry inherits the errors of the 2MASS catalog. The GAS, based on a single, least squares adjustment to approximately 750k grid stars using over 3000 extragalactic objects as reference objects, avoids this catalog-to-catalog propagation of errors to a great extent. The GAS uses a relatively small number of Quasi-Stellar Objects (QSOs, or distant AGN) with very accurate (<1 mas) radio positions, referenced to the ICRF2. These QSOs provide a hard constraint in the global least squares adjustment. Solving such a system provides absolute astrometry for all the stars simultaneously. The concept is much cleaner than conventional astrometry but is not easy to perform for large catalogs. In this paper we describe our method and its application to Pan-STARRS1 data. We show tha...

  15. Development of plasma sources for ICRF heating experiment in KMAX mirror device

    Science.gov (United States)

    Sun, Xuan; Liu, Ming; Yi, Hongshen; Lin, Munan; Shi, Peiyun

    2016-10-01

    KMAX, Keda Mirror with AXisymmeticity, is a tandem mirror machine with a length of 10 meters and diameters of 1.2 meters in the central cell and 0.3 meters in the mirror throat. In the past experiments, the plasma was generated by helicon wave launched from the west end. We obtained the blue core mode in argon discharge, however, it cannot provide sufficient plasma for hydrogen discharge, which is at least 1012 cm-3 required for effective ICRF heating. Several attempts have thus been tried or under design to increase the central cell's plasma density: (1) a washer gun with aperture of 1cm has been successfully tested, and a plasma density of 1013 cm-3 was achieved in the west cell near the gun, however, the plasma is only 1011 cm-3 in the central cell possible due to the mirror trapping and/or neutral quenching effect (2) a larger washer gun with aperture of 2.5 cm and a higher power capacitor bank are being assembled in order to generate more plasmas. In addition, how to mitigate the neutrals is under consideration (3) A hot cathode is been designed and will be tested in combination with plasma gun or alone. Preliminary results from those plasma sources will be presented and discussed.

  16. RF optimisation of the port plug layout and performance assessment of the ITER ICRF antenna

    Energy Technology Data Exchange (ETDEWEB)

    Vrancken, M., E-mail: Mark.Vrancken@ccfe.ac.uk [ERM-KMS, Association EURATOM-Belgian State, Brussels (Belgium); Durodié, F. [ERM-KMS, Association EURATOM-Belgian State, Brussels (Belgium); Bamber, R.; Dalton, N. [EURATOM/CCFE Association, Culham Science Centre, Abingdon OX14 3DB (United Kingdom); Dumortier, P. [ERM-KMS, Association EURATOM-Belgian State, Brussels (Belgium); Graham, M.; Horvat, A.; Hancock, D.; Lockley, D. [EURATOM/CCFE Association, Culham Science Centre, Abingdon OX14 3DB (United Kingdom); Louche, F. [ERM-KMS, Association EURATOM-Belgian State, Brussels (Belgium); Maggiora, R. [Associazione EURATOM-ENEA, Politecnico di Torino, Torino (Italy); Messiaen, A. [ERM-KMS, Association EURATOM-Belgian State, Brussels (Belgium); Milanesio, D. [Associazione EURATOM-ENEA, Politecnico di Torino, Torino (Italy); Nightingale, M.P.S.; Shannon, M.; Tigwell, P. [EURATOM/CCFE Association, Culham Science Centre, Abingdon OX14 3DB (United Kingdom); Van Schoor, M. [ERM-KMS, Association EURATOM-Belgian State, Brussels (Belgium); Wilson, D. [EURATOM/CCFE Association, Culham Science Centre, Abingdon OX14 3DB (United Kingdom); Winkler, K. [IPP-MPI, EURATOM-Assoziation, Garching (Germany); Team, Cycle [ERM-KMS, Association EURATOM-Belgian State, Brussels (Belgium); EURATOM/CCFE Association, Culham Science Centre, Abingdon OX14 3DB (United Kingdom); Associazione EURATOM-ENEA, Politecnico di Torino, Torino (Italy); IPP-MPI, EURATOM-Assoziation, Garching (Germany); Association EURATOM-CEA, DSM/IRFM, Cadarache (France)

    2013-10-15

    The ITER Ion Cyclotron Range of Frequencies (ICRF) antenna's capacity to couple power to plasma is determined by the plasma Scrape-Off Layer (SOL) profile, shaping of the front strap array, layout of the Port Plug (PP) and detailed design of its RF components. The first two factors are taken into account by the Torino Polytechnic Ion Cyclotron Antenna (TOPICA) calculated strap array Scattering/Impedance 24-port (S{sub 24×24}−/Z{sub 24×24}−) matrices, while this paper deals with the optimisation of the PP layout and components. The RF modeling techniques are explained and used to maximise the coupled power under a set of constraints on RF quantities inside the PP. The total PP RF surface conductive and volumetric dielectric losses are calculated. The resulting S-parameters at the rear RF PP flanges are evaluated as input for the design of the pre-match, decoupling and matching network outside the PP. A discussion of the effect of errors on the PP excitation on the coupled power is also included.

  17. A Diagnostic for Electric Field Measurements in the Near/Far-Field Regions of ICRF Antenna

    Science.gov (United States)

    Martin, E. H.; Caughman, J. B. O.; Isler, R. C.

    2015-11-01

    The physics mechanisms of wave heating and current drive processes in the bulk hot plasma are generally well identified. However, details of the wave-plasma interaction with a material surface in the cold plasma edge are still not fully understood. The driver behind this interaction is the time-periodic wave electric field and is referred to as the near/far-field depending on the location with respect to the antenna. Various models have been formulated to capture the near/far-field physics but have not been tested experimentally. Thus, a diagnostic capable of measuring the electric field with temporal and 3D-spatial resolution is critical for confidence in the codes used to design next generation ICRF antennas. This research is focused on the development of a laser based spectroscopic technique, Doppler-free saturation spectroscopy (DFSS), and its implementation to study near/far-field physics. Using DFSS the spectra line profile of various electronic transitions are measured and fit to a quantum mechanical model incorporating both magnetic and dynamic electric field operators. The electric field direction and magnitude are extracted from the fit. The experimental setup and planned experiments will be discussed. Additionally, initial measurements of fitted Hδ spectrum under the influence of known electric and magnetic fields will be presented.

  18. Nanodisperse Nickel Ferrite: Methods of Production, Structure and Magnetic Properties

    National Research Council Canada - National Science Library

    N Zaporina; J Grabis; M Maiorov; A Krumina; G Heidemane; D Bocharov

    2012-01-01

      Nanodisperse Nickel Ferrite: Methods of Production, Structure and Magnetic Properties The nickel ferrite nanoparticles were prepared using combustion synthesis and plasma chemical synthesis based on evaporation of coarse-grained...

  19. Measuring Permeability and Q-factor of Ferrite Toroids

    Institute of Scientific and Technical Information of China (English)

    XuZhe; WangChunxiao; ZhangWenzhi

    2003-01-01

    In the process of design RF cavity of CSRe, we use ferrite as the loading material of cavity. The characteristic of ferrite directly affects whether the cavity can obtain the target designed, so the measurement of ferrite material appears most important obviously.

  20. Characteristics of Strain-Induced Ferrite in Low Carbon Steel

    Institute of Scientific and Technical Information of China (English)

    LI Wei-juan; LIU Cui-qin; WANG Guo-dong; LIU Xiang-hua

    2003-01-01

    The strain-induced ferrite formed under different conditions was observed with SEM and optical microscope. The nucleation sites of strain-induced ferrite include grain boundary, grain inside, deformed band and annealing twin boundary. The shapes of the ferrite accordingly are equiaxed irregular polygonal, strip-shaped and acicular.

  1. Synthesis of ferrite and nickel ferrite nanoparticles using radio-frequency thermal plasma torch

    Science.gov (United States)

    Son, S.; Taheri, M.; Carpenter, E.; Harris, V. G.; McHenry, M. E.

    2002-05-01

    Nanocrystalline (NC) ferrite powders have been synthesized using a 50 kW-3 MHz rf thermal plasma torch for high-frequency soft magnet applications. A mixed powder of Ni and Fe (Ni:Fe=1:2), a NiFe permalloy powder with additional Fe powder (Ni:Fe=1:2), and a NiFe permalloy powder (Ni:Fe=1:1) were used as precursors for synthesis. Airflow into the reactor chamber was the source of oxygen for oxide formation. XRD patterns clearly show that the precursor powders were transformed into NC ferrite particles with an average particle size of 20-30 nm. SEM and TEM studies indicated that NC ferrite particles had well-defined polygonal growth forms with some exhibiting (111) faceting and many with truncated octahedral and truncated cubic shapes. The Ni content in the ferrite particles was observed to increase in going from mixed Ni and Fe to mixed permalloy and iron and finally to only permalloy starting precursor. The plasma-torch synthesized ferrite materials using exclusively the NiFe permalloy precursor had 40%-48% Ni content in the Ni-ferrite particle, differing from the NiFe2O4 ideal stoichiometry. EXAFS was used to probe the cation coordination in low Ni magnetite species. The coercivity and Neel temperature of the high Ni content ferrite sample were 58 Oe and ˜590 °C, respectively.

  2. Ferrite LTCC based phased array antennas

    KAUST Repository

    Ghaffar, Farhan A.

    2016-11-02

    Two phased array antennas realized in multilayer ferrite LTCC technology are presented in this paper. The use of embedded bias windings in these designs allows the negation of external magnets which are conventionally employed with bulk ferrite medium. This reduces the required magnetostatic field strength by 90% as compared to the traditional designs. The phase shifters are implemented using the SIW technology. One of the designs is operated in the half mode waveguide topology while the other design is based on standard full mode waveguide operation. The two phase shifter designs are integrated with two element patch antenna array and slotted SIW array respectively. The array designs demonstrate a beam steering of 30° and ±19° respectively for a current excitation of 200 mA. The designs, due to their small factor can be easily integrated in modern communication systems which is not possible in the case of bulk ferrite based designs.

  3. Micromagnetic simulations of spinel ferrite particles

    Energy Technology Data Exchange (ETDEWEB)

    Dantas, Christine C., E-mail: ccdantas@iae.cta.b [Divisao de Materiais (AMR), Instituto de Aeronautica e Espaco (IAE), Departamento de Ciencia e Tecnologia Aeroespacial - DCTA (Brazil); Gama, Adriana M., E-mail: adriana-gama@uol.com.b [Divisao de Materiais (AMR), Instituto de Aeronautica e Espaco (IAE), Departamento de Ciencia e Tecnologia Aeroespacial - DCTA (Brazil)

    2010-10-15

    This paper presents the results of simulations of the magnetization field ac response (at 2-12 GHz) of various submicron ferrite particles (cylindrical dots). The ferrites in the present simulations have the spinel structure, expressed here by M{sub 1}-{sub n}Zn{sub n}Fe{sub 2}O{sub 4} (where M stands for a divalent metal), and the parameters chosen were the following: (a) for n=0: M={l_brace}Fe, Mn, Co, Ni, Mg, Cu {r_brace}; (b) for n=0.1: M = {l_brace}Fe, Mg{r_brace} (mixed ferrites). These runs represent full 3D micromagnetic (one-particle) ferrite simulations. We find evidences of confined spin waves in all simulations, as well as a complex behavior nearby the main resonance peak in the case of the M = {l_brace}Mg, Cu{r_brace} ferrites. A comparison of the n=0 and n=0.1 cases for fixed M reveals a significant change in the spectra in M = Mg ferrites, but only a minor change in the M=Fe case. An additional larger scale simulation of a 3 by 3 particle array was performed using similar conditions of the Fe{sub 3}O{sub 4} (magnetite; n=0, M = Fe) one-particle simulation. We find that the main resonance peak of the Fe{sub 3}O{sub 4} one-particle simulation is disfigured in the corresponding 3 by 3 particle simulation, indicating the extent to which dipolar interactions are able to affect the main resonance peak in that magnetic compound.

  4. TEM observation of sintered permanent magnetic strontium ferrite

    Institute of Scientific and Technical Information of China (English)

    YU Hongya; LIU Zhengyi; ZENG Dechang

    2006-01-01

    Sintered permanent magnetic strontium ferrites were studied using transmission electron microscopy to investigate the microstructure morphology and its correlation with the magnetic properties. The present study shows that the microstructure of sintered permanent magnetic strontium ferrites is an important parameter in determining their magnetic properties. The microstructure morphology in low-performance ferrite magnet is obviously different from high-performance one. Themagnetic properties of sintered permanent strontium ferrite depend strongly on the orientation degree of strong magnetic crystals. The presence of ferric oxidephase in ferrite magnet can deteriorate the magnetic properties. Moreover, proper quantities of crystal defects are beneficial to high coercive force due to the fixing of magnetic domain.

  5. Simulation of non-linear coaxial line using ferrite beads

    Energy Technology Data Exchange (ETDEWEB)

    Furuya, S.; Matsumoto, H.; Tachi, K.; Takano, S.; Irisawa, J. [Nagaoka Univ. of Technology, Niigata (Japan)

    2002-06-01

    A ferrite sharpener is a non-linear coaxial line using ferrite beads, which produces high-voltage, high-dV/dt pulses. We have been examining the characteristics of ferrite sharpeners experimentally, varying various parameters. Also we have made the simulation of the ferrite sharpener and compared the predictions with the experimental results in detail to analyze the characteristics of the sharpener. In this report, calculating the magnetization M of the ferrite bead, we divide the bead into n sections radially instead of adopting M at the average radius in the previous report. (author)

  6. Cation distributions on rapidly solidified cobalt ferrite

    Science.gov (United States)

    De Guire, Mark R.; Kalonji, Gretchen; O'Handley, Robert C.

    1990-01-01

    The cation distributions in two rapidly solidified cobalt ferrites have been determined using Moessbauer spectroscopy at 4.2 K in an 8-T magnetic field. The samples were obtained by gas atomization of a Co0-Fe2O3-P2O5 melt. The degree of cation disorder in both cases was greater than is obtainable by cooling unmelted cobalt ferrite. The more rapidly cooled sample exhibited a smaller departure from the equilibrium cation distribution than did the more slowly cooled sample. This result is explained on the basis of two competing effects of rapid solidification: high cooling rate of the solid, and large undercooling.

  7. Cation distributions on rapidly solidified cobalt ferrite

    Science.gov (United States)

    De Guire, Mark R.; Kalonji, Gretchen; O'Handley, Robert C.

    1990-01-01

    The cation distributions in two rapidly solidified cobalt ferrites have been determined using Moessbauer spectroscopy at 4.2 K in an 8-T magnetic field. The samples were obtained by gas atomization of a Co0-Fe2O3-P2O5 melt. The degree of cation disorder in both cases was greater than is obtainable by cooling unmelted cobalt ferrite. The more rapidly cooled sample exhibited a smaller departure from the equilibrium cation distribution than did the more slowly cooled sample. This result is explained on the basis of two competing effects of rapid solidification: high cooling rate of the solid, and large undercooling.

  8. Confirmation of a new concept of ICRF antenna by modelling and experiments

    Energy Technology Data Exchange (ETDEWEB)

    Messiaen, Andre, E-mail: a.messiaen@fz-juelich.de; Dumortier, Pierre; Louche, Fabrice; Vervier, Michel

    2015-10-15

    The new ICRF antenna concept proposed in Milanesio and Maggiora (2014) has been confirmed. In the ANTITER II code a layer of low loss dielectric replaces the artificial dielectric covering the back-plate of the antenna box. This allows producing any surface impedance Z{sub S} at the dielectric boundary. The W7-X antenna is taken as a reference example. High Q resonances are obtained for discrete values of Z{sub S} at a given frequency. They correspond to TE{sub n,0} cavity modes of the antenna box, partially filled with dielectric. These resonances can occur when the wave of the considered mode is propagating into the dielectric and evanescent in the vacuum part. The conclusions of the modelling have been experimentally verified on an antenna box partially filled with a dielectric; excited either by a strap or a side loop and loaded by a salted water dummy load. The high Q resonances are damped by the dummy load at the aperture of the antenna box but also by the losses in the dielectric. The loading also shifts their resonance frequencies. Therefore: (i) resonance tracking is mandatory either by acting on the dielectric (or equivalent one) or on the generator frequency, (ii) very low loss dielectric or equivalent artificial one is needed to avoid the dissipation of a significant part of the power in it. The strap is not needed to excite the resonance: appropriate side loops can be used and designed to be close to matching for the average loading condition.

  9. Scattering characteristics of conducting cylinder coated with nonuniform magnetized ferrite

    Institute of Scientific and Technical Information of China (English)

    Hu Bin-Jie; Edward Yung Kai-Ning; Zhang Jun; Toutain Serge

    2005-01-01

    An analytical technique, referred to as the scattering matrix method (SMM), is developed to analyse the scattering of a planar wave from a conducting cylinder coated with nonuniform magnetized ferrite. The SMM solution for the nonuniform ferrite coating can be reduced to the expressions for the scattering and penetrated coefficients in four particular cases: nonuniform magnetized ferrite cylinder, uniform magnetized ferrite-coated conducting cylinder, uniform ferrite cylinder as well as homogeneous dielectric-coated conducting cylinder. The resonant condition for the nonuniform ferrite coating is obtained. The distinctive differences in scattering between the nonuniform ferrite coating and the nonuniform dielectric coating are demonstrated. The effects of applied magnetic fields and wave frequencies on the scattering characteristics for two types of the linear profiles are revealed.

  10. Co-containing spinel ferrite thin-film perpendicular magnetic recording media with Mn-Zn ferrite backlayer

    OpenAIRE

    Yamamoto, Setsuo; Kuniki, Hirofumi; Kurisu, Hiroki; Matsuura, Mitsuru

    2003-01-01

    Co-containing ferrite thin-film/Mn-Zn ferrite thin-film double-layered perpendicular media were prepared using reactive ECR sputtering and magnetron sputtering methods, and their magnetic and structural properties and recording characteristics were studied. The Mn-Zn ferrite thin-film backlayer had saturation magnetization of 3.5 kG and coercivity of 60 Oe. Reproduced voltage for the Co-containing ferrite thin-film/Mn-Zn ferrite thin-film double-layered medium was about twice of that for the ...

  11. Validation of the electrical design of the W7-X ICRF antenna on a reduced-scale mock-up

    Energy Technology Data Exchange (ETDEWEB)

    Dumortier, Pierre, E-mail: pierre.dumortier@rma.ac.be; Křivská, Alena; Messiaen, André; Vervier, Michel; Louche, Fabrice; Ongena, Jozef

    2015-10-15

    Highlights: • The electrical design of the W7X ICRF antenna is validated on a reduced-scale mock-up. • High dieletric constant materials are needed for the dummy load to mimic the plasma load. • Salted water and a mix of ferroelectric BaTiO{sub 3} and salted water are used as loads. • A comparison is made between experimental measurements and numerical simulations by 3 codes: Antiter II, CST MWS and Topica. • The best agreement is obtained with the BaTiO{sub 3} mix load for all phasings. • The dependence of the coupled power estimate on the dielectric load properties is given. - Abstract: A scaled mock-up (1/4) of the proposed W7-X ICRF antenna has been constructed and placed in front of dielectric dummy loads. It allows comparing measured and predicted coupling performances and hence validating the electrical design of the antenna. High dielectric constant materials are needed for the dummy load to mimic the plasma. Salted water and a mix of the ferroelectric BaTiO{sub 3} and salted water are used. The measurements are compared with the expectations of 3 codes: ANTITER II, MWS and TOPICA. The best agreement is obtained with the BaTiO{sub 3} load for all phasings.

  12. Development of Scientific Simulation 3D Full Wave ICRF Code for Stellarators and Heating/CD Scenarios Development

    Energy Technology Data Exchange (ETDEWEB)

    Vdovin V.L.

    2005-08-15

    In this report we describe theory and 3D full wave code description for the wave excitation, propagation and absorption in 3-dimensional (3D) stellarator equilibrium high beta plasma in ion cyclotron frequency range (ICRF). This theory forms a basis for a 3D code creation, urgently needed for the ICRF heating scenarios development for the operated LHD, constructed W7-X, NCSX and projected CSX3 stellarators, as well for re evaluation of ICRF scenarios in operated tokamaks and in the ITER . The theory solves the 3D Maxwell-Vlasov antenna-plasma-conducting shell boundary value problem in the non-orthogonal flux coordinates ({Psi}, {theta}, {var_phi}), {Psi} being magnetic flux function, {theta} and {var_phi} being the poloidal and toroidal angles, respectively. All basic physics, like wave refraction, reflection and diffraction are self consistently included, along with the fundamental ion and ion minority cyclotron resonances, two ion hybrid resonance, electron Landau and TTMP absorption. Antenna reactive impedance and loading resistance are also calculated and urgently needed for an antenna -generator matching. This is accomplished in a real confining magnetic field being varying in a plasma major radius direction, in toroidal and poloidal directions, through making use of the hot dense plasma wave induced currents with account to the finite Larmor radius effects. We expand the solution in Fourier series over the toroidal ({var_phi}) and poloidal ({theta}) angles and solve resulting ordinary differential equations in a radial like {Psi}-coordinate by finite difference method. The constructed discretization scheme is divergent-free one, thus retaining the basic properties of original equations. The Fourier expansion over the angle coordinates has given to us the possibility to correctly construct the ''parallel'' wave number k{sub //}, and thereby to correctly describe the ICRF waves absorption by a hot plasma. The toroidal harmonics are tightly

  13. Effect of ferrite addition above the base ferrite on the coupling factor of wireless power transfer for vehicle applications

    DEFF Research Database (Denmark)

    Batra, Tushar; Schaltz, Erik; Ahn, Seungyoung

    2015-01-01

    Power transfer capability of wireless power transfer systems is highly dependent on the magnetic design of the primary and secondary inductors and is measured quantitatively by the coupling factor. The inductors are designed by placing the coil over a ferrite base to increase the coupling factor...... and reduce magnetic emissions to the surroundings. Effect of adding extra ferrite above the base ferrite at different physical locations on the self-inductance, mutual inductance and coupling factor is under investigation in this paper. The addition can increase or decrease the mutual inductance depending...... on the placement of ferrite. Also, the addition of ferrite increases the self-inductance of the coils and there is a probability for an overall decrease in the coupling factor. Correct placement of ferrite on the other hand can increase the coupling factor relatively higher than the base ferrite as it is closer...

  14. Temperature stabilization of microwave ferrite devices

    Science.gov (United States)

    Kaminsky, R.; Wendt, E. J.

    1978-01-01

    Thin-film heating element for strip-line circulator is sandwiched between insulation and copper laminations. Disks conform to shape of circulator ferrite disks and are installed between copper-clad epoxy ground planes. Heater design eliminates external cartridges and reduces weight by approximately one-third.

  15. Adding calcium improves lithium ferrite core

    Science.gov (United States)

    Lessoff, H.

    1969-01-01

    Adding calcium increases uniformity of grain growth over a wide range of sintering temperatures and reduces porosity within the grain. Ferrite cores containing calcium have square hysteresis loops and high curie temperatures, making them useful in coincident current memories of digital electronic computers.

  16. Transmission through Ferrite Samples at Submillimeter Frequencies

    Science.gov (United States)

    1986-05-01

    y Y In all the equations given above, c and 1’e are, in general, complex. Measurements are generally made on the power transmitted which is ITaI ? in...Frequency (cm-’) using measurements of2T 1 given eby Figure 8. Power transmission coeffi- equation( 2),Tp1 = ITaI ~cient for 100-m-thick ferrite slab

  17. Spinel cobalt ferrite by complexometric synthesis

    NARCIS (Netherlands)

    Pham Duc Thang, P.D.T.; Rijnders, Augustinus J.H.M.; Blank, David H.A.

    2005-01-01

    Magnetic fine particles of cobalt ferrite (CoFe2O4) have been synthesized using complexometric method in which ethylene diamine tetra acetic acid C10H16N2O8 (EDTA) acts as a complexing agent. The crystallographic structure, microstructure and magnetic properties of the synthesized powder were

  18. Synthesis of lithium ferrites from polymetallic carboxylates

    Directory of Open Access Journals (Sweden)

    STEFANIA STOLERIU

    2008-10-01

    Full Text Available Lithium ferrite was prepared by the thermal decomposition of three polynuclear complex compounds containing as ligands the anions of malic, tartaric and gluconic acid: (NH42[Fe2.5Li0.5(C4H4O53(OH4(H2O2]×4H2O (I, (NH46[Fe2.5Li0.5(C4H4O63(OH8]×2H2O (II and (NH42[Fe2.5Li0.5(C6H11O73(OH7] (III. The polynuclear complex precursors were characterized by chemical analysis, IR and UV–Vis spectra, magnetic measurements and thermal analysis. The obtained lithium ferrites were characterized by XRD, scanning electron microscopy, IR spectra and magnetic measurements. The single α-Li0.5Fe2.5O4 phase was obtained by thermal decomposition of the tartarate complex annealed at 700 °C for 1 h. The magnetization value ≈ 50 emu g-1 is lower than that obtained for the bulk lithium ferrite due to the nanostructural character of the ferrite. The particle size was smaller than 100 nm.

  19. Ferrite Quantification Methodologies for Duplex Stainless Steel

    Directory of Open Access Journals (Sweden)

    Arnaldo Forgas Júnior

    2016-07-01

    Full Text Available In order to quantify ferrite content, three techniques, XRD, ferritoscope and optical metallography, were applied to a duplex stainless steel UNS S31803 solution-treated for 30 min at 1,000, 1,100 and 1,200 °C, and then compared to equilibrium of phases predicted by ThermoCalc® simulation. As expected, the microstructure is composed only by austenite and ferrite phases, and ferrite content increases as the solution treatment temperature increases. The microstructure presents preferred grains orientation along the rolling directions even for a sample solution treated for 30 min at 1,200 °C. For all solution treatment temperatures, the ferrite volume fractions obtained by XRD measurements were higher than those achieved by the other two techniques and ThermoCalc® simulation, probably due to texturing effect of previous rolling process. Values obtained by quantitative metallography look more assertive as it is a direct measurement method but the ferritoscope technique should be considered mainly for in loco measurement.

  20. Barium Ferrite Films Grown by Laser Ablation

    NARCIS (Netherlands)

    Lisfi, A.; Lodder, J.C.; Haan, de P.; Smithers, M.A.; Roesthuis, F.J.G.

    1998-01-01

    Pulsed laser ablation (PLA) has been used to grow barium ferrite films on Al2O3 single crystal substrates. When deposition occurs in an oxidising atmosphere at high temperatures, the films are single BaFe12O19 phase, very well oriented with (001) texture, and exhibit a large perpendicular magnetic a

  1. Extending the boundaries of mechanical properties of Ti-Nb low-carbon steel via combination of ultrafast cooling and deformation during austenite-to-ferrite transformation

    Science.gov (United States)

    Deng, Xiangtao; Fu, Tianliang; Wang, Zhaodong; Liu, Guohuai; Wang, Guodong; Misra, R. D. K.

    2017-01-01

    We underscore here a novel approach to extend the boundaries of mechanical properties of Ti-Nb low-carbon steel via combination of ultrafast cooling and deformation during austenite-to-ferrite transformation. The proposed approach yields a refined microstructure and high density nano-sized precipitates, with consequent increase in strength. Steels subjected to ultra-fast cooling during austenite-to-ferrite transformation led to 145 MPa increase in yield strength, while the small deformation after ultra-fast cooling process led to increase in strength of 275 MPa. The ultra-fast cooling refined the ferrite and pearlite constituents and enabled uniform dispersion, while the deformation after ultra-fast cooling promoted precipitation and broke the lamellar pearlite to spherical cementite and long thin strips of FexC. The contribution of nano-sized precipitates to yield strength was estimated to be 247.9 MPa and 358.3 MPa for ultrafast cooling and deformation plus ultrafast cooling processes. The nano precipitates carbides were identified to be (Ti, Nb)C and had a NaCl-type crystal structure, and obeyed the Baker-Nutting orientation relationship with the ferrite matrix.

  2. Differential cytotoxicity of copper ferrite nanoparticles in different human cells.

    Science.gov (United States)

    Ahmad, Javed; Alhadlaq, Hisham A; Alshamsan, Aws; Siddiqui, Maqsood A; Saquib, Quaiser; Khan, Shams T; Wahab, Rizwan; Al-Khedhairy, Abdulaziz A; Musarrat, Javed; Akhtar, Mohd Javed; Ahamed, Maqusood

    2016-10-01

    Copper ferrite nanoparticles (NPs) have the potential to be applied in biomedical fields such as cell labeling and hyperthermia. However, there is a lack of information concerning the toxicity of copper ferrite NPs. We explored the cytotoxic potential of copper ferrite NPs in human lung (A549) and liver (HepG2) cells. Copper ferrite NPs were crystalline and almost spherically shaped with an average diameter of 35 nm. Copper ferrite NPs induced dose-dependent cytotoxicity in both types of cells, evident by 3-(4,5-dimethylthiazol-2-yl)-2,5-diphenyltetrazoliumbromide and neutral red uptake assays. However, we observed a quite different susceptibility in the two kinds of cells regarding toxicity of copper ferrite NPs. Particularly, A549 cells showed higher susceptibility against copper ferrite NP exposure than those of HepG2 cells. Loss of mitochondrial membrane potential due to copper ferrite NP exposure was observed. The mRNA level as well as activity of caspase-3 enzyme was higher in cells exposed to copper ferrite NPs. Cellular redox status was disturbed as indicated by induction of reactive oxygen species (oxidant) generation and depletion of the glutathione (antioxidant) level. Moreover, cytotoxicity induced by copper ferrite NPs was efficiently prevented by N-acetylcysteine treatment, which suggests that reactive oxygen species generation might be one of the possible mechanisms of cytotoxicity caused by copper ferrite NPs. To the best of our knowledge, this is the first report showing the cytotoxic potential of copper ferrite NPs in human cells. This study warrants further investigation to explore the mechanisms of differential toxicity of copper ferrite NPs in different types of cells. Copyright © 2016 John Wiley & Sons, Ltd.

  3. Cr-W-V bainitic/ferritic steel with improved strength and toughness and method of making

    Science.gov (United States)

    Klueh, Ronald L.; Maziasz, Philip J.

    1994-01-01

    A high strength, high toughness Cr-W-V ferritic steel composition suitable for fast induced-radioactivity (FIRD) decay after irradiation in a fusion reactor comprises 2.5-3.5 wt % Cr, 2. This invention was made with Government support under contract DE-AC05-840R21400 awarded by the U.S. Department of Energy to Martin Marietta Energy Systems, Inc. and the Government has certain rights in this invention.

  4. Microstructure of pre-sintered permanent magnetic strontium ferrite powder

    Institute of Scientific and Technical Information of China (English)

    YU Hongya; LIU Zhengyi; ZENG Dechang

    2006-01-01

    The microstructure and characteristics of pre-sintered strontium ferrite powderwere investigated by X-ray diffraction, scanning electron microscopy and transmission electron microscopy. The present study shows that the pre-sintered strontium ferrite powder is provided with a certain particle size distribution, which results in high-density magnets. The strontium ferrite particle has a laminar hexagonal structure with a size similar to ferrite single domain. Ferric oxidephase due to an incomplete solid phase reaction in the first sintering is discovered, which will deteriorate the magnetic properties of ferrite magnet. In addition, the waste ferrite magnets with needle shape arranging along C axis in good order into the powders are found, which have no negative effects on finished product quality.

  5. Ferrite-Piezoelectric Layered Composites: Synthesis and Magnetoelectric Characterization

    Science.gov (United States)

    Hayes, R. W.; Srinivasan, G.

    2004-10-01

    The observation of strong magnetoelectric effects is reported in thick film bilayers and multilayers of ferrite-lead titanate zirconate (PZT). The ferrites used in our studies included pure and zinc substituted cobalt-, nickel- and lithium ferrites. Samples were prepared by sintering 10-40 mm thick films obtained by tape-casting. Measurements of ME voltage coefficients at 10-1000 Hz indicated a giant ME effect in nickel ferrite-PZT, but a relatively weak coupling in other ferrite-PZT systems. Evidence was found for enhancement in ME coefficients when Zn was substituted in ferrites. The Zn-assisted increase was attributed to low anisotropy and high permeability that resulted in favorable magneto-mechanical coupling in the composites. G. Srinivasan, E. T. Rasmussen, and R. Hayes, Phys. Rev. B 67, 014418 (2003) Supported by NSF and ARO grants.

  6. Elevated-Temperature Ferritic and Martensitic Steels and Their Application to Future Nuclear Reactors

    Energy Technology Data Exchange (ETDEWEB)

    Klueh, RL

    2005-01-31

    In the 1970s, high-chromium (9-12% Cr) ferritic/martensitic steels became candidates for elevated-temperature applications in the core of fast reactors. Steels developed for conventional power plants, such as Sandvik HT9, a nominally Fe-12Cr-1Mo-0.5W-0.5Ni-0.25V-0.2C steel (composition in wt %), were considered in the United States, Europe, and Japan. Now, a new generation of fission reactors is in the planning stage, and ferritic, bainitic, and martensitic steels are again candidates for in-core and out-of-core applications. Since the 1970s, advances have been made in developing steels with 2-12% Cr for conventional power plants that are significant improvements over steels originally considered. This paper will review the development of the new steels to illustrate the advantages they offer for the new reactor concepts. Elevated-temperature mechanical properties will be emphasized. Effects of alloying additions on long-time thermal exposure with and without stress (creep) will be examined. Information on neutron radiation effects will be discussed as it applies to ferritic and martensitic steels.

  7. Irradiation creep of various ferritic alloys irradiated at {approximately}400{degrees}C in the PFR and FFTF reactors

    Energy Technology Data Exchange (ETDEWEB)

    Toloczko, M.B.; Garner, F.A. [Pacific Northwest National Lab., Richland, WA (United States); Eiholzer, C.R. [Westinghouse Hanford Company, Richland, WA (United States)

    1997-04-01

    Three ferritic alloys were irradiated in two fast reactors to doses of 50 dpa or more at temperatures near 400{degrees}C. One martensitic alloy, HT9, was irradiated in both the FFTF and PFR reactors. PFR is the Prototype Fast Reactor in Dourneay, Scotland, and FFTF is the Fast Flux Test Facility in Richland, WA. D57 is a developmental alloy that was irradiated in PFR only, and MA957 is a Y{sub 2}O{sub 3} dispersion-hardened ferritic alloy that was irradiated only in FFTF. These alloys exhibited little or no void swelling at {approximately}400{degrees}C. Depending on the alloy starting condition, these steels develop a variety of non-creep strains early in the irradiation that are associated with phase changes. Each of these alloys creeps at a rate that is significantly lower than that of austenitic steels irradiated in the same experiments. The creep compliance for ferritic alloys in general appears to be {approximately}0.5 x 10{sup {minus}6} MPa{sup {minus}1} dpa{sup {minus}1}, independent of both composition and starting state. The addition of Y{sub 2}O{sub 3} as a dispersoid does not appear to change the creep behavior.

  8. An investigation of co-fired varistor-ferrite materials

    OpenAIRE

    Rafferty, Aran; Gun'ko, Yurii; Raghavendra, Ramesh

    2004-01-01

    The purpose of this work was to co-fire crack-free varistor-ferrite ceramic multilayers fabricated via a dry pressing route. Multilayers were sintered using a standard industrial grade varistor sintering regime. Sinter shrinkages of both varistor and ferrite materials were measured using dilatometry and showed that the varistor shrunk significantly more than the ferrite material. X-ray diffraction analysis indicated that no significant phase changes occurred in the materials under in...

  9. The Development of Low Activation Ferritic Steels for Fusion Application

    OpenAIRE

    Kohyama, A; Hishinuma, A.; Kohno, Y; Shiba, K; Sagara, A.

    1997-01-01

    The development of low-activation ferritic/martensitic steels is a key to the achievement of nuclear fusion as a safe, environmentally attractive and economically competitive energy source. The Japanese and the European Fusion Materials programs have put low-activation ferritic and martensitic steels R & D at the highest priority for a demonstration reactor (DEMO) and the beyond. An international collaborative test program on low-activation ferritic/martensitic steels for fusion is in progres...

  10. HYDROTHERMAL SYNTHESIS OF NANO-METER MICROPOROUS ZINC FERRITE

    Institute of Scientific and Technical Information of China (English)

    Xiaoling Hu; Ping Guan; Xin Yan

    2004-01-01

    Nano-meter microporous zinc ferrite was prepared by a hydrothermal method, using triethylamine as a template. Adsorption curves showed that the product had a microporous structure. The effects of precursor pH, reaction temperature and reaction time on the preparation were studied, yielding optimal conditions: pH=11,448 K, 360 min. The morphology of zinc ferrite as observed by TEM, showed that zinc ferrite was well-crystallized and well-dispersed with little conglomeration.

  11. Annealing-induced Grain Refinement in a Nanostructured Ferritic Steel

    Institute of Scientific and Technical Information of China (English)

    Limin Wang; Zhenbo Wangt; Sheng Guo; Ke Lu

    2012-01-01

    A nanostructured surface layer with a mean ferrite grain size of -8 nm was produced on a Fe-gCr steel by means of surface mechanical attrition treatment. Upon annealing, ferrite grains coarsen with increasing temperature and their sizes increase to -40 nm at 973 K. Further increasing annealing temperature leads to an obvious reduction of ferrite grain sizes, to -14 nm at 1173 K. The annealing-induced grain refinement is analyzed in terms of phase transformations in the nanostructured steel.

  12. Tunable dielectric properties of ferrite-dielectric based metamaterial.

    Science.gov (United States)

    Bi, K; Huang, K; Zeng, L Y; Zhou, M H; Wang, Q M; Wang, Y G; Lei, M

    2015-01-01

    A ferrite-dielectric metamaterial composed of dielectric and ferrite cuboids has been investigated by experiments and simulations. By interacting with the electromagnetic wave, the Mie resonance can take place in the dielectric cuboids and the ferromagnetic precession will appear in the ferrite cuboids. The magnetic field distributions show the electric Mie resonance of the dielectric cuboids can be influenced by the ferromagnetic precession of ferrite cuboids when a certain magnetic field is applied. The effective permittivity of the metamaterial can be tuned by modifying the applied magnetic field. A good agreement between experimental and simulated results is demonstrated, which confirms that these metamaterials can be used for tunable microwave devices.

  13. Ferrite microwave electronics Citations from the NTIS data base

    Science.gov (United States)

    Reed, W. E.

    1980-07-01

    Research reports on single crystals, thin films, dielectrics, semiconductor devices, integrated circuits, phase shifters, and waveguide components are cited. Studies on the microwave properties of ferrites are included.

  14. Ferritic-austenitic cast steel - selected problems

    Directory of Open Access Journals (Sweden)

    Z. Stradomski

    2011-07-01

    Full Text Available The author has been involved in the problems occurring in the manufacture of ferritic-austenitic cast steel castings for many years. The author’s remarks and investigation results reported in this article will enable potential manufacturers to determine their own technical capabilities and structural determinants related to the chemical composition of material, which are crucial to the good quality of a casting. Particular emphasis should be laid on the role of enhanced carbon content, the presence of copper, the precipitates of the ζ phase, and the nature of solidification structure in the tendency of duplex-type cast steel to cracking. It seems that in view of the pro-ecological activities undertaken, including flue gas desulphurization in coal-fired power plants, efforts should be made in steel foundries to introduce selected grades of ferritic-austenitic cast steel to production.

  15. Simulations of gas puff effects on edge density and ICRF coupling in ASDEX upgrade using EMC3-Eirene

    Energy Technology Data Exchange (ETDEWEB)

    Zhang, W., E-mail: wei.zhang@ipp.mpg.de [Applied Physics Department, University of Ghent, Ghent (Belgium); Max-Planck-Institut für Plasmaphysik, Garching (Germany); Institute of Plasma Physics, Chinese Academy of Sciences, Hefei (China); Lunt, T.; Bobkov, V.; Coster, D.; Brida, D. [Max-Planck-Institut für Plasmaphysik, Garching (Germany); Noterdaeme, J.-M. [Applied Physics Department, University of Ghent, Ghent (Belgium); Max-Planck-Institut für Plasmaphysik, Garching (Germany); Jacquet, P. [CCFE, Culham Science Centre, Abingdon (United Kingdom); Feng, Y. [Max-Planck-Institut für Plasmaphysik, Greifswald (Germany)

    2015-12-10

    Simulations were carried out with the 3D plasma transport code EMC3-EIRENE, to study the deuterium gas (D{sub 2}) puff effects on edge density and the coupling of Ion Cyclotron Range of Frequency (ICRF) power in ASDEX Upgrade. Firstly we simulated an inter-ELM phase of an H-mode discharge with a moderate (1.2 × 10{sup 22} electrons/s) lower divertor gas puff. Then we changed the gas source positions to the mid-plane or top of machine while keeping other conditions the same. Cases with different mid-plane or top gas valves are investigated. Our simulations indicate that compared to lower divertor gas puffing, the mid-plane gas puff can enhance the local density in front of the antennas most effectively, while a rather global (toroidally uniform) but significantly smaller enhancement is found for top gas puffing. Our results show quantitative agreement with the experiments.

  16. Tensile properties and deformation mechanisms of a 14Cr ODS ferritic steel

    Science.gov (United States)

    Steckmeyer, A.; Praud, M.; Fournier, B.; Malaplate, J.; Garnier, J.; Béchade, J. L.; Tournié, I.; Tancray, A.; Bougault, A.; Bonnaillie, P.

    2010-10-01

    The search for a new cladding material is part of the research studies carried out at CEA to develop a sodium-cooled fast reactor meeting the expectations of the Generation IV International Forum. In this study, the tensile properties of a ferritic oxide dispersion strengthened steel produced by hot extrusion at CEA have been evaluated. They prove the studied alloy to be as resistant as and more ductile than the other nano-reinforced alloys of literature. The effects of the strain rate and temperature on the total plastic strain of the material remind of diffusion phenomena. Intergranular damage and intergranular decohesion are clearly highlighted.

  17. High Efficiency ELID Grinding of Garnet Ferrite

    Institute of Scientific and Technical Information of China (English)

    2002-01-01

    Hard and brittle materials such as ferrite, optical glass and ceramics have been widely used in many fields because of their good characteristics and still gain more attentions. However, it is difficult to machine and get good surface quality. Some parts made of these materials have large machining allowances and need to be produced with large batch, but the machining efficiency is very low with usual grinding method. So it is of great importance to research the high efficiency grinding technology of hard ...

  18. Preparation and Characterization of Manganese Ferrite Aluminates

    Directory of Open Access Journals (Sweden)

    R. L. Dhiman

    2008-01-01

    Full Text Available Aluminum doped manganese ferrites MnAlxFe2−xO4 with 0.0≤x≤1.0 have been prepared by the double ceramic route. The formation of mixed spinel phase has been confirmed by X-ray diffraction analysis. The unit cell parameter `aO' is found to decrease linearly with aluminum concentration due to smaller ionic radius of aluminum. The cation distributions were estimated from X-ray diffraction intensities of various planes. The theoretical lattice parameter, X-ray density, oxygen positional parameter, ionic radii, jump length, and bonds and edges lengths of the tetrahedral (A and octahedral (B sites were determined. 57Fe Mössbauer spectra recorded at room temperature were fitted with two sextets corresponding to Fe3+ ions at A- and B-sites. In the present ferrite system, the area ratio of Fe3+ ions at the A- and B-sites determined from the spectral analysis of Mössbauer spectra gives evidence that Al3+ ions replace iron ions at B-sites. This change in the site preference reflects an abrupt change in magnetic hyperfine fields at A- and B-sites as aluminum concentration increases, which has been explained on the basis of supertransferred hyperfine field. On the basis of estimated cation distribution, it is concluded that aluminum doped manganese ferrites exhibit a 55% normal spinel structure.

  19. The Formation Process of Silico-Ferrite of Calcium (SFC) from Binary Calcium Ferrite

    Science.gov (United States)

    Ding, Xiang; Guo, Xing-Min

    2014-08-01

    Silico-ferrite of calcium (SFC) is a significant equilibrium crystalline phase in the Fe2O3-CaO-SiO2 (FCS) ternary system and a key bonding phase in the sintering process of fine iron ore. In this work, the formation process of SFC from binary calcium ferrite has been determined by X-ray diffraction and field-emission scanning electron microscopy. Experiments were carried out under air at 1473 K (1200 °C) by adding SiO2 and Fe2O3 into CaO·Fe2O3 (CF). It was found that the formation of SFC is dominated by solid-state reactions in the FCS ternary system, in which Fe2O3 reacts with CaO·Fe2O3 to form the binary calcium ferrite phase. The chemical composition of binary calcium ferrite is Ca2.5Fe15.5O25 and approximately Ca2Fe12O20 (CaO·3Fe2O3). Then Si4+ and Ca2+ ions take the place of Fe3+ ion in preference located on the octahedral layers which belongs to (0 0 18) plane of binary calcium ferrite. The crystal structure of binary calcium ferrite gradually transforms from orthorhombic to triclinic, and the grain is refined with the addition of silica due to the smaller radius of Si4+ ion. A solid solution SFC forms completely when the content of SiO2 reaches approximately 3.37 wt pct at 1473 K (1200 °C).

  20. Active and fast particle driven Alfvén eigenmodes in Alcator C-Moda)

    Science.gov (United States)

    Snipes, J. A.; Basse, N.; Boswell, C.; Edlund, E.; Fasoli, A.; Gorelenkov, N. N.; Granetz, R. S.; Lin, L.; Lin, Y.; Parker, R.; Porkolab, M.; Sears, J.; Sharapov, S.; Tang, V.; Wukitch, S.

    2005-05-01

    Alfvén eigenmodes (AEs) are studied to assess their stability in high density reactor relevant regimes where Ti≈Te and as a diagnostic tool. Stable AEs are excited with active magnetohydrodynamics antennas in the range of the expected AE frequency. Toroidal Alfvén eigenmode (TAE) damping rates between 0.5%<γ/ω<4.5% have been observed in diverted and limited Ohmic plasmas. Unstable AEs are excited with a fast ion tail driven by H minority ion cyclotron radio frequency (ICRF) heating with electron densities in the range of n¯e=0.5-2×1020m-3. Energetic particle modes or TAEs have been observed to decrease in frequency and mode number with time up to a large sawtooth collapse, indicating the role fast particles play in stabilizing sawteeth. In the current rise phase, unstable modes with frequencies that increase rapidly with time are observed with magnetic pick-up coils at the wall and phase contrast imaging density fluctuation measurements in the core. Modeling of these modes constrains the calculated safety factor profile to be very flat or with slightly reversed shear. AEs are found to be more stable for an inboard than for central or outboard ICRF resonances in qualitative agreement with modeling.

  1. Stabilization of sawteeth with third harmonic deuterium ICRF-accelerated beam in JET plasmas

    Energy Technology Data Exchange (ETDEWEB)

    Girardo, Jean-Baptiste [EUROfusion Consortium, JET, Culham Science Centre, Abingdon OX14 3DB (United Kingdom); CEA, IRFM, F-13108 Saint-Paul-lez-Durance (France); Sharapov, Sergei; Fitzgerald, Michael; Hawkes, Nick; Kiptily, Vasily; Lupelli, Ivan [CCFE, Culham Science Centre, Abingdon OX14 3DB (United Kingdom); Boom, Jurrian [Max-Planck-Institut für Plasmaphysik, 85748 Garching (Germany); Dumont, Rémi; Garbet, Xavier; Sarazin, Yanick; Schneider, Mireille [CEA, IRFM, F-13108 Saint-Paul-lez-Durance (France); Eriksson, Jacob [Department of Physics and Astronomy, Uppsala University, 751 20 Uppsala (Sweden); Mantsinen, Mervi [Catalan Institution for Research and Advanced Studies, 08010 Barcelona (Spain); Barcelona Supercomputing Center, 08034 Barcelona (Spain)

    2016-01-15

    Sawtooth stabilisation by fast ions is investigated in deuterium (D) and D-helium 3 (He3) plasmas of JET heated by deuterium Neutral Beam Injection combined in synergy with Ion Cyclotron Resonance Heating (ICRH) applied on-axis at 3rd beam cyclotron harmonic. A very significant increase in the sawtooth period is observed, caused by the ICRH-acceleration of the beam ions born at 100 keV to the MeV energy range. Four representative sawteeth from four different discharges are compared with Porcelli's model. In two discharges, the sawtooth crash appears to be triggered by core-localized Toroidal Alfvén Eigenmodes inside the q = 1 surface (also called “tornado” modes) which expel the fast ions from within the q = 1 surface, over time scales comparable with the sawtooth period. Two other discharges did not exhibit fast ion-driven instabilities in the plasma core, and no degradation of fast ion confinement was found in both modelling and direct measurements of fast ion profile with the neutron camera. The developed sawtooth scenario without fast ion-driven instabilities in the plasma core is of high interest for the burning plasmas. Possible causes of the sawtooth crashes on JET are discussed.

  2. Photoelectrochemical properties of ferrites with the spinel structure

    NARCIS (Netherlands)

    Haart, L.G.J. De; Blasse, G.

    1985-01-01

    The photoelectrochemical properties of the ferrites ZnFe2O4, MgFe2O4 and Li0.5O4 with the spinel structure are reported. The ferrites seem reasonable candidates for photoanodes in a photoelectrochemical cell, because of their 2.2 eV bandgap. The results show, however, that the visible absorptivity,

  3. A model for ferrite-loaded transversely biased coaxial resonators

    DEFF Research Database (Denmark)

    Acar, Öncel; Zhurbenko, Vitaliy; Johansen, Tom Keinicke

    2013-01-01

    This work describes a simple model for shortened coaxial cavity resonators with transversely biased ferrite elements. The ferrite allows the resonance frequency to be tuned, and the presented model provides a method of approximately calculating these frequencies to generate the tuning curve...

  4. Fundamental study of a one-step ambient temperature ferrite ...

    African Journals Online (AJOL)

    Fundamental study of a one-step ambient temperature ferrite process for treatment ... The approach involves the controlled oxidation of ferrous-containing AMD water at ... The resulting oxidation product is the ferrite (M13+2M22+O4) magnetite ...

  5. Structural investigation of an extended milled ferrite powder

    Energy Technology Data Exchange (ETDEWEB)

    Moisin, A.M.; Macrin, M. (Institutul de Cercetari Electronice, Bucharest (Romania))

    1980-01-01

    An investigation of the structural modifications introduced by the extended milling and annealing processes in the barium ferrite powder during its preparation is presented. X-ray diffraction measuements on a barium ferrite powder in various milling and annealing conditions have been carried out and the results concerning the phase compositions, lattice constants and crystallite sizes are discussed.

  6. Defects, phase transformations and magnetic properties of lithium ferrite

    Energy Technology Data Exchange (ETDEWEB)

    Mishra, R.K.

    1977-03-01

    Achieving suitable magnetic properties in ceramic ferrites through thermomechanical treatments rather than through varying the processing and fabrication parameters alone has been investigated. Ferrimagnetic lithium ferrite and some other spinel structure materials were chosen for this investigation. Extensive characterization of phase transformations and lattice defects was done.

  7. Harmonic Ratcheting for Ferrite Tuned RF Acceleration of Charged Particles

    Science.gov (United States)

    Cook, Nathan; Brennan, Mike

    2013-04-01

    One of the most persistent difficulties in the design of RF cavities for acceleration of charged particles is the rapid and efficient acceleration of particles over a large range of frequencies. From medical synchrotrons to accelerator driven systems, there is a strong need for fast acceleration of protons and light ions over hundreds of MeV. Conventionally, this is a costly undertaking, requiring specially designed ferrite loaded cavities to be tuned over a large range of frequencies. Ferromagnetic materials allow for the precise adjustment of cavity resonant frequency, but rapid changes in the frequency as well as operation outside material specific frequency ranges result in significant Q-loss to the cavity. This leads to a considerable increase in power required and is thus undesirable for regular operation. We introduce an acceleration scheme known as harmonic ratcheting which can be used to reduce the cavity frequency range needed for accelerating an ion beam in a synchrotron. In particular, this scheme addresses the need for high rep. rate machines for applications such as radiation therapy in which low beam intensity is needed. We demonstrate with simulations the type of ramps achievable using this technique and consider its advantages over h=1 acceleration schemes.

  8. Development of New Heats of Advanced Ferritic/Martensitic Alloys

    Energy Technology Data Exchange (ETDEWEB)

    Maloy, Stuart Andrew [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Pestovich, Kimberly Shay [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Anderoglu, Osman [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Aydogan, Eda [Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

    2017-06-23

    The Fuel Cycle Research and Development program is investigating methods of transmuting minor actinides in various fuel cycle options. To achieve this goal, new fuels and cladding materials must be developed and tested to high burnup levels (e.g. >20%) requiring cladding to withstand very high doses (greater than 200 dpa) while in contact with the coolant and the fuel. To develop and qualify materials to a total fluence greater than 200 dpa requires development of advanced alloys and irradiations in fast reactors to test these alloys. Recent results from testing numerous ferritic/martensitic steels at low temperatures suggest that improvements in low temperature radiation tolerance can be achieved through carefully controlling the nitrogen content in these alloys. Thus, four new heats of HT-9 were produced with controlled nitrogen content: two by Metalwerks and two by Sophisticated Alloys. Initial results on these new alloys are presented including microstructural analysis and hardness testing. Future testing will include irradiation testing with ions and in reactor.

  9. Modeling non-saturated ferrite-based devices: Application to twin toroid ferrite phase shifters

    Science.gov (United States)

    Le Gouellec, A.; Vérissimo, G.; Laur, V.; Queffelec, P.; Albert, I.; Girard, T.

    2016-08-01

    This article describes a new set of tools developed to improve the conception and modeling of non-saturated ferrite-based devices such as twin toroid phase shifters. These new simulation tools benefit from a generalized permeability tensor model able to describe the permeability tensor of a ferrite sample whatever its magnetization state. This model is coupled to a homemade 3D multi-scale magnetostatic analysis program, which describes the evolution of the magnetization through the definition of a hysteresis loop in every mesh cell. These computed spectra are then integrated into 3D electromagnetic simulation software that retains the spatial variations of the ferrite properties by using freshly developed macro programming functions. This new approach allows the designers to accurately model complex ferrite devices such as twin toroid phase shifters. In particular, we demonstrated a good agreement between simulated and measured phase shifts as a function of applied current values with a predicted maximum phase shift of 0.96 times the measured value.

  10. Substrate integrated ferrite phase shifters and active frequency selective surfaces

    CERN Document Server

    Cahill, B M

    2002-01-01

    There are two distinct parts to this thesis; the first investigates the use of ferrite tiles in the construction of printed phase shifting transmission lines, culminating in the design of two compact electromagnetic controlled beam steered patch and slot antenna arrays. The second part investigates the use of active frequency selective surfaces (AFSS), which are later used to cover a uPVC constructed enclosure. Field intensity measurements are taken from within the enclosure to determine the dynamic screening effectiveness. Trans Tech G-350 Ferrite is investigated to determine its application in printed microstrip and stripline phase shifting transmission lines. 50-Ohm transmission lines are constructed using the ferrite tile and interfaced to Rogers RT Duroid 5870 substrate. Scattering parameter measurements are made under the application of variable magnetic fields to the ferrite. Later, two types of planar microwave beam steering antennas are constructed. The first uses the ferrites integrated into the Dur...

  11. Electrical transport behavior of nonstoichiometric magnesium-zinc ferrite

    Energy Technology Data Exchange (ETDEWEB)

    Ghatak, S. [Department of Physics, National Institute of Technology, Deemed University, Mahatma Gandhi Avenue, Durgapur 713209, West Bengal (India); Sinha, M. [Department of Physics, University of Burdwan, Golapbag, Burdwan 713104, West Bengal (India); Meikap, A.K., E-mail: meikapnitd@yahoo.com [Department of Physics, National Institute of Technology, Deemed University, Mahatma Gandhi Avenue, Durgapur 713209, West Bengal (India); Pradhan, S.K. [Department of Physics, University of Burdwan, Golapbag, Burdwan 713104, West Bengal (India)

    2010-08-15

    This paper presents the direct current conductivity, alternate current conductivity and dielectric properties of nonstoichiometric magnesium-zinc ferrite below room temperature. The frequency exponent (s) of conductivity shows an anomalous temperature dependency. The magnitude of the temperature exponent (n) of dielectric permittivity strongly depends on frequency and its value decreases with increasing frequency. The grain boundary contribution is dominating over the grain contribution in conduction process and the temperature dependence of resistance due to grain and grain boundary contribution exhibits two activation regions. The ferrite shows positive alternating current magnetoconductivity. The solid state processing technique was used for the preparation of nanocrystalline ferrite powder from oxides of magnesium, zinc and iron. The X-ray diffraction methods were used in determining the structure and composition of obtained ferrite, while multimeter, impedance analyzer, liquid nitrogen cryostat and electromagnet were used in the study of conducting and dielectric properties of ferrite.

  12. Corrosion behavior of magnetic ferrite coating prepared by plasma spraying

    Energy Technology Data Exchange (ETDEWEB)

    Liu, Yi; Wei, Shicheng, E-mail: wsc33333@163.com; Tong, Hui; Tian, Haoliang; Liu, Ming; Xu, Binshi

    2014-12-15

    Graphical abstract: The saturation magnetization (M{sub s}) of the ferrite coating is 34.417 emu/g while the M{sub s} value of the ferrite powder is 71.916 emu/g. It can be seen that plasma spray process causes deterioration of the room temperature soft magnetic properties. - Highlights: • Spinel ferrite coatings have been prepared by plasma spraying. • The coating consists of nanocrystalline grains. • The saturation magnetization of the ferrite coating is 34.417 emu/g. • Corrosion behavior of the ferrite coating was examined in NaCl solution. - Abstract: In this study, spray dried spinel ferrite powders were deposited on the surface of mild steel substrate through plasma spraying. The structure and morphological studies on the ferrite coatings were carried out using X-ray diffraction, scanning electron microscope and Raman spectroscopy. It was showed that spray dried process was an effective method to prepare thermal spraying powders. The coating showed spinel structure with a second phase of LaFeO{sub 3}. The magnetic property of the ferrite samples were measured by vibrating sample magnetometer. The saturation magnetization (M{sub s}) of the ferrite coating was 34.417 emu/g. The corrosion behavior of coating samples was examined by electrochemical impedance spectroscopy. EIS diagrams showed three corrosion processes as the coating immersed in 3.5 wt.% NaCl solution. The results suggested that plasma spraying was a promising technology for the production of magnetic ferrite coatings.

  13. Assessment of the integrity of ferritic-austenitic dissimilar weld joints of different grades of Cr-Mo ferritic steels

    Energy Technology Data Exchange (ETDEWEB)

    Laha, K.; Chandravathi, K.S.; Parameswaran, P.; Goyal, Sunil; Mathew, M.D. [Indira Gandhi Centre for Atomic Research, Kalpakkam (India). Metallurgy and Materials Group

    2010-07-01

    Integrity of the 2.25 Cr-1Mo / Alloy 800, 9Cr-1Mo / Alloy 800 and 9Cr-1Mo-VNb / Alloy 800 ferritic-austenitic dissimilar joints, fusion welded employing Inconel 182 electrode, has been assessed under creep conditions at 823 K. The dissimilar weld joints displayed lower creep rupture strength than their respective ferritic steel base metals. The strength reduction was more for 2.25Cr-1Mo steel joint and least for 9Cr-1Mo steel joint. The failure location in the joints was found to shift from the ferritic steel base metal to the intercritical region of heat-affected zone (HAZ) in ferritic steel (type IV cracking) with decrease in stress. At still lower stresses the failure occurred at the ferritic / austenitic weld interface. Localized creep deformation and cavitation in the soft intercritical HAZ induced type IV failure whereas creep cavitation at the weld interface particles induced ferritic / austenitic interface cracking due to high creep strength mismatch across it. Micromechanisms of type IV failure and interface cracking in the ferritic / austenitic joints and different susceptibility to failure for different grades of ferritic steels are discussed based on microstructural investigation, mechanical testing and finite element analysis. (Note from indexer: paper contains many typographical errors.)

  14. Cobalt ferrite nanoparticles under high pressure

    Energy Technology Data Exchange (ETDEWEB)

    Saccone, F. D.; Ferrari, S.; Grinblat, F.; Bilovol, V. [Instituto de Tecnologías y Ciencias de la Ingeniería, “Ing. H. Fernández Long,” Av. Paseo Colón 850 (1063), Buenos Aires (Argentina); Errandonea, D., E-mail: daniel.errandonea@uv.es [Departamento de Fisica Aplicada, Institut Universitari de Ciència dels Materials, Universitat de Valencia, c/ Doctor Moliner 50, E-46100 Burjassot, Valencia (Spain); Agouram, S. [Departamento de Física Aplicada y Electromagnetismo, Universitat de València, 46100 Burjassot, Valencia (Spain)

    2015-08-21

    We report by the first time a high pressure X-ray diffraction and Raman spectroscopy study of cobalt ferrite (CoFe{sub 2}O{sub 4}) nanoparticles carried out at room temperature up to 17 GPa. In contrast with previous studies of nanoparticles, which proposed the transition pressure to be reduced from 20–27 GPa to 7.5–12.5 GPa (depending on particle size), we found that cobalt ferrite nanoparticles remain in the spinel structure up to the highest pressure covered by our experiments. In addition, we report the pressure dependence of the unit-cell parameter and Raman modes of the studied sample. We found that under quasi-hydrostatic conditions, the bulk modulus of the nanoparticles (B{sub 0} = 204 GPa) is considerably larger than the value previously reported for bulk CoFe{sub 2}O{sub 4} (B{sub 0} = 172 GPa). In addition, when the pressure medium becomes non-hydrostatic and deviatoric stresses affect the experiments, there is a noticeable decrease of the compressibility of the studied sample (B{sub 0} = 284 GPa). After decompression, the cobalt ferrite lattice parameter does not revert to its initial value, evidencing a unit cell contraction after pressure was removed. Finally, Raman spectroscopy provides information on the pressure dependence of all Raman-active modes and evidences that cation inversion is enhanced by pressure under non-hydrostatic conditions, being this effect not fully reversible.

  15. Magnetic resonance in superparamagnetic zinc ferrite

    Indian Academy of Sciences (India)

    Jitendra Pal Singh; Gagan Dixit; R C Srivastava; Hemant Kumar; H M Agrawal; Prem Chand

    2013-08-01

    In the present work, we have synthesized zinc ferrite nanoparticles by nitrate method. Presence of almost zero value of coercivity and remanence in the hysteresis of these samples shows the superparamagnetic nature at room temperature. Electron paramagnetic resonance spectroscopy performed on these samples in the temperature range 120–300 K indicates the systematic variation of the line-shapes of the spectra with temperature. Both gvalue and peak-to-peak linewidth decrease with increase in temperature. The variation of g-values and peak-topeak linewidth with temperature has been fitted with existing models and we observed different values of activation energies of the spins for both the samples.

  16. CASS Ferrite and Grain Structure Relationship

    Energy Technology Data Exchange (ETDEWEB)

    Ruud, Clayton O. [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Ramuhalli, Pradeep [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Meyer, Ryan M. [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Diaz, Aaron A. [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Anderson, Michael T. [Pacific Northwest National Lab. (PNNL), Richland, WA (United States)

    2016-07-13

    This document summarizes the results of research conducted at Pacific Northwest National Laboratory (PNNL) to determine whether, based on experimental measurements, a correlation existed between grain structure in cast austenitic stainless steel (CASS) piping and ferrite content of the casting alloy. The motivation for this research lies in the fact that ultrasonic testing (UT) is strongly influenced by CASS grain structure; knowledge of this grain structure may help improve the ability to interpret UT responses, thereby improving the overall reliability of UT inspections of CASS components.

  17. Atomically flat ultrathin cobalt ferrite islands.

    Science.gov (United States)

    Martín-García, Laura; Quesada, Adrián; Munuera, Carmen; Fernández, Jose F; García-Hernández, Mar; Foerster, Michael; Aballe, Lucía; de la Figuera, Juan

    2015-10-21

    A route for fabricating structurally perfect cobalt ferrite magnetic nanostructures is demonstrated. Ultrathin islands of up to 100 μm(2) with atomically flat surfaces and free from antiphase boundaries are developed. The extremely low defect concentration leads to a robust magnetic order, even for thicknesses below 1 nm, and exceptionally large magnetic domains. This approach allows the evaluation of the influence of specific extrinsic effects on domain wall pinning. © 2015 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

  18. Influence of rapid heating process on the microstructure and tensile properties of high-strength ferrite-martensite dual-phase steel

    Institute of Scientific and Technical Information of China (English)

    Pei Li; Jun Li; Qing-ge Meng; Wen-bin Hu; Chun-fu Kuang

    2015-01-01

    Three low-carbon dual-phase (DP) steels with almost constant martensite contents of 20vol%were produced by intercritical an-nealing at different heating rates and soaking temperatures. Microstructures prepared at low temperature (1043 K, FH1) with fast-heating (300 K/s) show banded ferrite/martensite structure, whereas those soaked at high temperature (1103 K, FH2) with fast heating reveal blocky martensite uniformly distributed in the fine-grained ferrite matrix. Their mechanical properties were tested under tensile conditions and compared to a slow-heated (5 K/s) reference material (SH0). The tensile tests indicate that for a given martensite volume fraction, the yield strength and total elongation values are noticeably affected by the refinement of ferrite grains and the martensite morphology. Metallographic observations reveal the formation of microvoids at the ferrite/martensite interface in the SH0 and FH2 samples, whereas microvoids nucleate via the fracture of banded martensite particles in the FH1 specimen. In addition, analyses of the work-hardening behaviors of the DP micro-structures using the differential Crussard–Jaoul technique demonstrate two stages of work hardening for all samples.

  19. Cast Stainless Steel Ferrite and Grain Structure

    Energy Technology Data Exchange (ETDEWEB)

    Ruud, Clayton O.; Ramuhalli, Pradeep; Meyer, Ryan M.; Mathews, Royce; Diaz, Aaron A.; Anderson, Michael T.

    2012-09-01

    In-service inspection requirements dictate that piping welds in the primary pressure boundary of light-water reactors be subject to a volumetric examination based on the rules contained within the American Society of Mechanical Engineers Boiler and Pressure Vessel Code, Section XI. The purpose of the inspection is the reliable detection and accurate sizing of service-induced degradation and/or material flaws introduced during fabrication. The volumetric inspection is usually carried out using ultrasonic testing (UT) methods. However, the varied metallurgical macrostructures and microstructures of cast austenitic stainless steel piping and fittings, including statically cast stainless steel and centrifugally cast stainless steel (CCSS), introduce significant variations in the propagation and attenuation of ultrasonic energy. These variations complicate interpretation of the UT responses and may compromise the reliability of UT inspection. A review of the literature indicated that a correlation may exist between the microstructure and the delta ferrite content of the casting alloy. This paper discusses the results of a recent study where the goal was to determine if a correlation existed between measured and/or calculated ferrite content and grain structure in CCSS pipe.

  20. Use of Specific Properties of Zinc Ferrite in Innovative Technologies

    Directory of Open Access Journals (Sweden)

    Kmita A.

    2016-12-01

    Full Text Available Zinc ferrite ZnFe2O4 both in the micro and nano scale is widely used in various fields. The article discusses the structure of this compound and its properties in the nanoscale, which is clearly different from those which the ferrite shows in the microscale. The properties of dust generated electric arc furnace, which can contain up to 40% zinc, substantially in the form of ZnFe2O4 are disscused here. Specific properties (electric, magnetic, thermal of zinc ferrite nanoparticles determine the very wide possibilities of their use, inter alia as catalysts, absorbents, gas sensors, and a tool to combat cancer.

  1. Dysprosium Modification of Cobalt Ferrite Ionic Magnetic Fluids

    Institute of Scientific and Technical Information of China (English)

    JIANG Rong-li; LIU Yong-chao; GENG Quan-rong; ZHAO Wen-tao

    2005-01-01

    Dysprosium composite cobalt ferrite ionic magnetic fluids were prepared by precipitation in the presence of Tri-sodium citrate. Influence of dysprosium modification on magnetic property is studied. The result shows that magnetic response toward exterior magnetic field can be improved by adding Dy3+. Studies also show that the increase of reaction temperature may improve the modification effect of dysprosium. By adding dysprosium ions, the average diameter of the magnetic nanoparticles will be decreased evidently. It is clear that the particles appear as balls, Cobalt ferrite with sizes of 12-15 nm, rare earth composite cobalt ferrite with sizes of 6-8 nm.

  2. Preparation and characterization of rice husk/ferrite composites

    Institute of Scientific and Technical Information of China (English)

    2010-01-01

    A novel ferrite composite using rice husk as substrate has been prepared via high temperature treatment under nitrogen atmosphere.The rice husk substrate consists of porous activated carbon and silica,where spinel ferrite particles with average diameter of 59 nm are distributed.The surface area of the composite is greater than 170 m~2 g~(-1) and the bulk density is less than 0.6 g cm~(-3).Inert atmosphere is indispensable for the synthesis of pure ferrite composites,while different preparation temperatur...

  3. Nickel hydroxide/cobalt-ferrite magnetic nanocatalyst for alcohol oxidation.

    Science.gov (United States)

    Bhat, Pooja B; Inam, Fawad; Bhat, Badekai Ramachandra

    2014-08-11

    A magnetically separable, active nickel hydroxide (Brønsted base) coated nanocobalt ferrite catalyst has been developed for oxidation of alcohols. High surface area was achieved by tuning the particle size with surfactant. The surface area of 120.94 m2 g(-1) has been achieved for the coated nanocobalt ferrite. Improved catalytic activity and selectivity were obtained by synergistic effect of transition metal hydroxide (basic hydroxide) on nanocobalt ferrite. The nanocatalyst oxidizes primary and secondary alcohols efficiently (87%) to corresponding carbonyls in good yields.

  4. Modeling of Incubation Time for Austenite to Ferrite Phase Transformation

    Institute of Scientific and Technical Information of China (English)

    ZHOU Xiao-guang; LIU Zhen-yu; WU Di; WANG Wei; JIAO Si-hai

    2006-01-01

    On the basis of the classical nucleation theory, a new model of incubation time for austenite to ferrite transformation has been developed, in which the effect of deformation on austenite has been taken into consideration. To prove the precision of modeling, ferrite transformation starting temperature (Ar3) has been calculated using the Scheil′s additivity rule, and the Ar3 values were measured using a Gleeble 1500 thermomechanical simulator. The Ar3 values provided by the modeling method coincide with the measured ones, indicating that the model is precise in predicting the incubation time for austenite to ferrite transformation in hot deformed steels.

  5. Ultra-fine ferrite grains obtained in the TSDR process

    Institute of Scientific and Technical Information of China (English)

    Ling Zhang; Wangyue Yang; Chunxia Xue; Zuqing Sun

    2008-01-01

    By careful design of rolling schedule, ultra-fine (~2 μm) ferrite grains in a low carbon high niobium (0.09wt%Nb) micro-alloying steel with average austenite grain sizes above 800 μm can be achieved in the simulated thin slab direct rolling process. The 5-pass deformation was divided into two stages: the refinement of austenite through complete recrystallization and the refinement of ferrite through dynamic strain-induced transformation. The effects of Nb in solution and strain-induced NbCN precipitates on the fer-rite transformation were also extensively discussed.

  6. Ferric Oxide from Hematite Used in Microwave Ferrite Material

    Institute of Scientific and Technical Information of China (English)

    2000-01-01

    Ferric Oxide is an essential and raw material in the production of ferrite materials. At present, ferric oxide used by many domestic factories is mainly produced by chemical method. In this paper, we use ferric oxide refined from hematite and applied in the microwave ferrite material production test. Compared with the normal ferric oxide, we get the same or similar results. It shows that ferric oxide from hematite and applied in the microwave ferrite material production test. Compared with the normal ferric oxide, we get the same or similar results. It shows that ferric oxide from hematite has a bright application prospect.

  7. Edge measurements during ICRF (ion cyclotron range of frequency) heating on the PLT (Princeton Large Torus) tokamak

    Energy Technology Data Exchange (ETDEWEB)

    Lehrman, I.S.; Colestock, P.L.; McNeill, D.H.; Greene, G.J.; Bernabei, S.; Hosea, J.C.; Ono, M.; Shohet, J.L.; Wilson, J.R.

    1989-04-01

    Edge measurements have been conducted on the PLT tokamak under a variety of operating conditions in order to ascertain the relevant processes at work in coupling rf power to plasmas. The edge density is found to increase significantly with the application of ICRF, and electron heating occurs in the vicinity of the Faraday shield surrounding the antenna. Spectroscopic measurements indicate that the energized antenna is a significant particle source. The relative increase of metallic impurities was found to be /approximately/2.7 times larger than the corresponding increase in deuterium. In addition, the relative increase of deuterium and impurities was /approximately/3--4 times greater at the energized antenna than at other locations around the torus. Model calculations show that for deuterium released from the Faraday shield, the D/sub ..cap alpha../ emission is localized radially to a region within 4 cm of the antenna. A correlation was found between the edge density and the D/sub ..cap alpha../ intensity that justifies its use as a measure of the particle source rate. 26 refs., 14 figs.

  8. Microstructural Features During Strain Induced Ferrite Transformation in 08 and 20Mn Steels

    Institute of Scientific and Technical Information of China (English)

    2001-01-01

    The microstructure evolution during strain induced ferrite transformation was followed in thermal-simulation tests of clean 08 and 20Mn steels. The influences of carbon equivalence and initial austenite grain size on ferrite grain refinement and the volume fraction of ferrite during straining were inspected. The results revealed that the accelerating effect of ferrite transformation by strain was increased as the carbon equivalence decreased. However, finer ferrite grains were obtained at higher carbon content. At strain of ~1.5 ferrite grains less than 3m and 2m can be obtained in 08 and 20Mn steels respectively. Whereas the ferrite grain refinement in 08 steel was due to both effects of strain induced transformation and ferrite dynamic recrystallization, that in 20Mn was mainly due to strain induced transformation. Heavy strain can produce fine ferrite grains in coarse austenite grained 08 steel, but it would lead to band microstructure in coarse austenite grained 20Mn.

  9. Performance Variation of Ferrite Magnet PMBLDC Motor with Temperature

    DEFF Research Database (Denmark)

    Fasil, Muhammed; Mijatovic, Nenad; Jensen, Bogi Bech

    2015-01-01

    a different approach when deciding their operating point. In this work, laboratory measured BH curves of a ferrite magnet are used for estimating the possibility of demagnetization in a segmented axial torus (SAT) permanent magnet brushless DC (PMBLDC) motor. The BH characteristics for different temperatures...... have been used to study the performance variation of the ferrite magnet SAT PMBLDC motor with temperature. A detailed analysis is carried out to ensure that, the designed ferrite magnet motor is capable of delivering the specified torque throughout the operating speed, without any irreversible...... demagnetization of magnets. It has been shown that the ferrite magnet PMBLDC motor operation is influenced by the magnet temperature and the maximum motor speed for a given load torque decreases as the magnet temperature drops....

  10. New sintering process adjusts magnetic value of ferrite cores

    Science.gov (United States)

    Vinal, A. W.

    1964-01-01

    A two-phase sintering technique based on time and temperature permits reversible control of the coercive threshold of sintered ferrite cores. Threshold coercivity may be controlled over a substantial range of values by selective control of the cooling rate.

  11. Ferrite core coupled slapper detonator apparatus and method

    Science.gov (United States)

    Boberg, Ralph E.; Lee, Ronald S.; Weingart, Richard C.

    1989-01-01

    Method and apparatus are provided for coupling a temporally short electric power pulse from a thick flat-conductor power cable into a thin flat-conductor slapper detonator circuit. A first planar and generally circular loop is formed from an end portion of the power cable. A second planar and generally circular loop, of similar diameter, is formed from all or part of the slapper detonator circuit. The two loops are placed together, within a ferrite housing that provides a ferrite path that magnetically couples the two loops. Slapper detonator parts may be incorporated within the ferrite housing. The ferrite housing may be made vacuum and water-tight, with the addition of a hermetic ceramic seal, and provided with an enclosure for protecting the power cable and parts related thereto.

  12. Mössbauer and magnetization studies of nanosize chromium ferrite

    African Journals Online (AJOL)

    user

    Synthesized chromium ferrite powders were in good phase and .... This could be because in smaller particles sample defect density is very high due to more broken .... nanosize particles using co-precipitation technique followed by ball milling, ...

  13. Tunable dielectric properties of ferrite-dielectric based metamaterial.

    Directory of Open Access Journals (Sweden)

    K Bi

    Full Text Available A ferrite-dielectric metamaterial composed of dielectric and ferrite cuboids has been investigated by experiments and simulations. By interacting with the electromagnetic wave, the Mie resonance can take place in the dielectric cuboids and the ferromagnetic precession will appear in the ferrite cuboids. The magnetic field distributions show the electric Mie resonance of the dielectric cuboids can be influenced by the ferromagnetic precession of ferrite cuboids when a certain magnetic field is applied. The effective permittivity of the metamaterial can be tuned by modifying the applied magnetic field. A good agreement between experimental and simulated results is demonstrated, which confirms that these metamaterials can be used for tunable microwave devices.

  14. Ferrite-filled cavities for compact planar resonators

    Science.gov (United States)

    Keatley, P. S.; Durrant, C. J.; Berry, S. J.; Sirotkin, E.; Hibbins, A. P.; Hicken, R. J.

    2014-01-01

    Sub-wavelength metallic planar cavities, closed at one end, have been constructed by wrapping aluminium foil around teflon or ferrite slabs. Finite cavity width perturbs the fundamental cavity mode frequency of ferrite-filled cavities due to different permeability inside and outside of the cavity, in contrast to teflon-filled cavities, while the cavity length required to achieve a specific resonance frequency is significantly reduced for a ferrite-filled cavity. Ferrite-filled cavities may be excited by an in-plane alternating magnetic field and may be advantageous for high-frequency (HF) and ultra HF tagging and radio frequency identification of metallic objects within security, manufacturing, and shipping environments.

  15. Application of Ferrite Nanomaterial in RF On-Chip Inductors

    Directory of Open Access Journals (Sweden)

    Hua-Lin Cai

    2013-01-01

    Full Text Available Several kinds of ferrite-integrated on-chip inductors are presented. Ferrite nanomaterial applied in RF on-chip inductors is prepared and analyzed to show the properties of high permeability, high ferromagnetic resonance frequency, high resistivity, and low loss, which has the potential that will improve the performance of RF on-chip inductors. Simulations of different coil and ferrite nanomaterial parameters, inductor structures, and surrounding structures are also conducted to achieve the trend of gains of inductance and quality factor of on-chip inductors. By integrating the prepared ferrite magnetic nanomaterial to the on-chip inductors with different structures, the measurement performances show an obvious improvement even in GHz frequency range. In addition, the studies of CMOS compatible process to integrate the nanomaterial promote the widespread application of magnetic nanomaterial in RF on-chip inductors.

  16. Cadmium substituted high permeability lithium ferrite

    Indian Academy of Sciences (India)

    S S Bellad; S C Watawe; A M Shaikh; B K Chougule

    2000-04-01

    Polycrystalline Li0.5–/2 Cd Fe2.5–/2O4 ferrites where = 0, 0.1, 0.2, 0.3, 0.4, 0.5 and 0.6 were prepared by a double sintering ceramic technique and characterized by X-ray diffraction and scanning electron microscopy (SEM). The lattice parameter is found to increase monotonically with the cadmium content. It is explained in terms of the sizes of component ions. The grain size of the samples increases up to = 0.3 and then it decreases for higher values of . A similar trend is observed in the variation of Ms with Cd2+ content. The initial permeability () is however found to increase continuously with . The increase in is attributed to decrease of anisotropy constant K1 and higher grain size of the samples.

  17. Synthesis and characterization of nanocrystalline zinc ferrite

    DEFF Research Database (Denmark)

    Jiang, J.S.; Yang, X.L.; Gao, L.

    1999-01-01

    Nanocrystalline zinc ferrite powders with a partially inverted spinel structure were synthesized by high-energy ball milling in a closed container at ambient temperature from a mixture of alpha-Fe2O3 and ZnO crystalline powders in equimolar ratio. From low-temperature and in-field Mossbauer...... measurements it is revealed that ZnFe2O4 particles prepared are in superparamagnetic state at ambient temperature. A doublet with an average quadrupole splitting of 0.8 nm/s is observed for the as-milled sample at 295 K, which is much larger than that for bulk ZnFe2O4 prepared by traditional ceramic method...... and that for ultrafine ZnFe2O4 particles prepared by the co-precipitation method. This indicates larger structural defects in the nanometer-sized ZnFe2O4 particles prepared by high-energy ball milling....

  18. Structural properties of Cd–Co ferrites

    Indian Academy of Sciences (India)

    S P Dalawai; T J Shinde; A B Gadkari; P N Vasambekar

    2013-10-01

    Ferrite samples with composition, CdCo1−Fe2O4 ( = 0.80, 0.85, 0.90, 0.95 and 1.0), were prepared by standard ceramic method and characterized by XRD, IR and SEM techniques. X-ray analysis confirms the formation of single phase cubic spinel structure. Lattice constant and grain size of the samples increase with increase in cadmium content. Bond length (A–O) and ionic radii (A) on -sites increase, whereas bond length (B–O) and ionic radii (B) on -site decrease. The crystallite sites of the samples lie in the range of 29.1–42.8 nm. IR study shows two absorption bands around 400 cm-1 and 600 cm-1 corresponding to tetrahedral and octahedral sites, respectively.

  19. New ferritic steels for advanced steam plants

    Energy Technology Data Exchange (ETDEWEB)

    Mayer, K.H; Koenig, H. [GEC ALSTHOM Energie GmbH, Nuremberg (Germany)

    1998-12-31

    During the last 15-20 years ferritic-martensitic 9-12 % chromium steels have been developed under international research programmes which permit inlet steam temperatures up to approx. 625 deg C and pressures up to about 300 bars, thus leading to improvements in thermal efficiency of around 8 % and a CO{sub 2} reduction of about 20 % versus conventional steam parameters. These new steels are already being applied in 13 European and 34 Japanese power stations with inlet steam temperature up to 610 deg C. This presentation will give an account of the content, scope and results of the research programmes and of the experience gained during the production of components which have been manufactured from the new steels. (orig.) 13 refs.

  20. Ethanol sensor based on nanocrystallite cadmium ferrite

    Energy Technology Data Exchange (ETDEWEB)

    Gadkari, Ashok B., E-mail: ashokgadkari88@yahoo.com [Department of Physics, GKG College, Kolhapur-416012 (India); Shinde, Tukaram J. [Department of Physics, KRP Kanya Mahavidyalaya, Islampur-415409 (India); Vasambekar, Pramod N. [Department of Electronics, Shivaji University Kolhapur-416004 (India)

    2015-06-24

    The cadmium ferrite was synthesized by oxalate co-precipitation method. The crystal structure and surface morphology were examined by X-ray diffraction and SEM techniques, respectively. The nanocrystallite CdFe{sub 2}O{sub 4} sensor was tested for LPG, Cl{sub 2} and C{sub 2}H{sub 5}OH. The sensitivity was measured at various operating temperatures in the range of 100-400°C. The sensor shows highest sensitivity and selectivity to C{sub 2}H{sub 5}OH at 350°C. The response and recovery time was measured at operating temperature of 350°C. The sensor exhibits a lower response and recovery time for LPG and Cl{sub 2} as compared to ethanol.

  1. Joining Techniques for Ferritic ODS Alloys

    Energy Technology Data Exchange (ETDEWEB)

    V.G. Krishnardula; V.G. Krishnardula; D.E. Clark; T.C. Totemeier

    2005-06-01

    This report presents results of research on advanced joining techniques for ferritic oxide-dispersion strengthened alloys MA956 and PM2000. The joining techniques studied were resistance pressure welding (also known as pressure forge welding), transient liquid phase bonding, and diffusion bonding. All techniques were shown to produce sound joints in fine-grained, unrecrystallized alloys. Post-bond heat treatment to produce a coarse-grained, recrystallized microstructure resulted in grain growth across the bondline for transient liquid phase and diffusion bonds, giving microstructures essentially identical to that of the parent alloy in the recrystallized condition. The effects of bond orientation, boron interlayer thickness, and bonding parameters are discussed for transient liquid phase and diffusion bonding. The report concludes with a brief discussion of ODS joining techniques and their applicability to GEN IV reactor systems.

  2. Propagation along azimuthally magnetized ferrite-loaded circular waveguides

    Science.gov (United States)

    Mueller, R. S.; Rosenbaum, F. J.

    1977-01-01

    The paper describes the modal dispersion characteristics of electromagnetic waves traveling along the azimuthally magnetized ferrite-loaded coaxial transmission line and the ferrite-loaded wire. The modal dispersion curves are used to determine the pass and stop bands of normal propagation. Boundary-value problems were solved with Bolle-Heller functions. The dispersion characteristics of transverse electric modes are presented as plots of the normalized propagation constant vs the normalized frequency.

  3. Residual ferrite formation in 12CrODS steels

    OpenAIRE

    Ukai, S.; Kudo, Y.; Wu, X; N. Oono; Hayashi, S.(University of Tokyo, Tokyo, Japan); Ohtsuka, S; T. Kaito

    2014-01-01

    Increasing Cr content from 9 to 12 mass% leads to superior corrosion and high-temperature oxidation resistances, and usually changes microstructure from martensite to a ferrite. To make transformable martensitic type of 12CrODS steels that have superior processing capability by using alpha/gamma phase transformation, alloy design was conducted through varying nickel content. The structure of 12CrODS steels was successfully modified from full ferrite to a transformable martensite-base matrix c...

  4. Processing of Ultralow Carbon Pipeline Steels with Acicular Ferrite

    Institute of Scientific and Technical Information of China (English)

    Furen XIAO; Mingchun ZHAO; Yiyin SHAN; Bo LIAO; Ke YANG

    2004-01-01

    Acicular ferrite microstructure was achieved for an ultralow carbon pipeline steel through the improved thermomechanical control process (TMCP), which was based on the transformation process of deformed austenite of steel.Compared with commercial pipeline steels, the experimental ultralow carbon pipeline steel possessed the satisfied strength and toughness behaviors under the current improved TMCP, although it contained only approximately 0.025% C, which should mainly be attributed to the microstructural characteristics of acicular ferrite.

  5. DARHT-II Injector Transients and the Ferrite Damper

    Energy Technology Data Exchange (ETDEWEB)

    Waldron, Will; Reginato, Lou; Chow, Ken; Houck, Tim; Henestroza, Enrique; Yu, Simon; Kang, Michael; Briggs, Richard

    2006-08-04

    This report summarizes the transient response of the DARHT-II Injector and the design of the ferrite damper. Initial commissioning of the injector revealed a rise time excited 7.8 MHz oscillation on the diode voltage and stalk current leading to a 7.8 MHz modulation of the beam current, position, and energy. Commissioning also revealed that the use of the crowbar to decrease the voltage fall time excited a spectrum of radio frequency modes which caused concern that there might be significant transient RF electric field stresses imposed on the high voltage column insulators. Based on the experience of damping the induction cell RF modes with ferrite, the concept of a ferrite damper was developed to address the crowbar-excited oscillations as well as the rise-time-excited 7.8 MHz oscillations. After the Project decided to discontinue the use of the crowbar, further development of the concept focused exclusively on damping the oscillations excited by the rise time. The design was completed and the ferrite damper was installed in the DARHT-II Injector in February 2006. The organization of this report is as follows. The suite of injector diagnostics are described in Section 2. The data and modeling of the injector transients excited on the rise-time and also by the crowbar are discussed in Section 3; the objective is a concise summary of the present state of understanding. The design of the ferrite damper, and the small scale circuit simulations used to evaluate the ferrite material options and select the key design parameters like the cross sectional area and the optimum gap width, are presented in Section 4. The details of the mechanical design and the installation of the ferrite damper are covered in Section 5. A brief summary of the performance of the ferrite damper following its installation in the injector is presented in Section 6.

  6. Formation of nanoscale titanium carbides in ferrite: an atomic study

    Science.gov (United States)

    Lv, Yanan; Hodgson, Peter; Kong, Lingxue; Gao, Weimin

    2016-03-01

    The formation and evolution of nanoscale titanium carbide in ferrite during the early isothermal annealing process were investigated via molecular dynamics simulation. The atomic interactions of titanium and carbon atoms during the initial formation process explained the atoms aggregation and carbides formation. It was found that the aggregation and dissociation of titanium carbide occurred simultaneously, and the composition of carbide clusters varied in a wide range. A mechanism for the formation of titanium carbide clusters in ferrite was disclosed.

  7. Ferrite bead effect on Class-D amplifier audio quality

    OpenAIRE

    Haddad, Kevin El; Mrad, Roberto; Morel, Florent; Pillonnet, Gael; Vollaire, Christian; Nagari, Angelo

    2014-01-01

    International audience; This paper studies the effect of ferrite beads on the audio quality of Class-D audio amplifiers. This latter is a switch-ing circuit which creates high frequency harmonics. Generally, a filter is used at the amplifier output for the sake of electro-magnetic compatibility (EMC). So often, in integrated solutions, this filter contains ferrite beads which are magnetic components and present nonlinear behavior. Time domain measurements and their equivalence in frequency do...

  8. Tuning the magnetism of ferrite nanoparticles

    Energy Technology Data Exchange (ETDEWEB)

    Viñas, S. Liébana [Faculty of Physics and CENIDE, University Duisburg-Essen, Duisburg 47048 (Germany); Departamento de Física Aplicada, Universidade de Vigo, Vigo 36310 (Spain); Simeonidis, K. [Department of Physics, Aristotle University of Thessaloniki, Thessaloniki 54124 (Greece); Li, Z.-A.; Ma, Z. [Faculty of Physics and CENIDE, University Duisburg-Essen, Duisburg 47048 (Germany); Myrovali, E.; Makridis, A.; Sakellari, D. [Department of Physics, Aristotle University of Thessaloniki, Thessaloniki 54124 (Greece); Angelakeris, M., E-mail: agelaker@auth.gr [Department of Physics, Aristotle University of Thessaloniki, Thessaloniki 54124 (Greece); Wiedwald, U.; Spasova, M. [Faculty of Physics and CENIDE, University Duisburg-Essen, Duisburg 47048 (Germany); Farle, M., E-mail: michael.farle@uni-due.de [Faculty of Physics and CENIDE, University Duisburg-Essen, Duisburg 47048 (Germany)

    2016-10-01

    The importance of magnetic interactions within an individual nanoparticle or between adjacent ones is crucial not only for the macroscopic collective magnetic behavior but for the AC magnetic heating efficiency as well. On this concept, single-(MFe{sub 2}O{sub 4} where M=Fe, Co, Mn) and core–shell ferrite nanoparticles consisting of a magnetically softer (MnFe{sub 2}O{sub 4}) or magnetically harder (CoFe{sub 2}O{sub 4}) core and a magnetite (Fe{sub 3}O{sub 4}) shell with an overall size in the 10 nm range were synthesized and studied for their magnetic particle hyperthermia efficiency. Magnetic measurements indicate that the coating of the hard magnetic phase (CoFe{sub 2}O{sub 4}) by Fe{sub 3}O{sub 4} provides a significant enhancement of hysteresis losses over the corresponding single-phase counterpart response, and thus results in a multiplication of the magnetic hyperthermia efficiency opening a novel pathway for high-performance, magnetic hyperthermia agents. At the same time, the existence of a biocompatible Fe{sub 3}O{sub 4} outer shell, toxicologically renders these systems similar to iron-oxide ones with significantly milder side-effects. - Highlights: • Magnetic hyperthermia is studied for 10 nm single and core/shell ferrite nanoparticles. • Maximum heating rate is observed for Fe{sub 3}O{sub 4}-coated CoFe{sub 2}O{sub 4} nanoparticles. • The increase is attributed to the interaction of phases with different anisotropy. • The presence of biocompatible Fe{sub 3}O{sub 4} shell potentially minimizes toxic side-effects.

  9. Electric properties of Co substituted Ni-Zn ferrites

    Energy Technology Data Exchange (ETDEWEB)

    Ghodake, J.S. [Department of Physics, Solapur University, Solapur 413255, MS (India); Kambale, R.C., E-mail: rckambale@hotmail.co [Department of Physics, Shivaji University, Kolhapur 416004 (India); Salvi, S.V. [Department of Physics, Birla college, Kalyan, Mumbai, MS (India); Sawant, S.R. [Department of Electronics, Shivaji University, Kolhapur 416004 (India); Suryavanshi, S.S., E-mail: sssuryavanshi@rediffmail.co [Department of Physics, Solapur University, Solapur 413255, MS (India)

    2009-11-03

    Nanocrystalline Ni-Co-Zn ferrites have been synthesized by chemical co precipitation method, using oxalate precursors. The phase formation of the sintered ferrite was confirmed by X-ray diffraction study. The lattice parameter 'a' increases with the addition of Co{sup 2+} content in the Ni-Zn ferrites. The electrical resistivity (rho) of mixed Ni-Zn ferrites has been studied as a function of varying Co{sup 2+} compositions. The resistivity was found to increase with the addition Co content in the Ni-Zn ferrite matrix. The variation of dc resistivity as a function of temperature is almost linear up to the Curie temperature and thereafter a break occurs indicating a change of magnetic ordering from ferrimagnetism to paramagnetism. The values of activation energy in paramagnetic region are found to be greater than those in ferrimagnetic region, which suggests that the process of conduction is affected by the change in magnetic ordering. The dielectric properties were studied as a function of frequency by using an LCR precision meter bridge. It was observed that the dielectric constant (epsilon') and dielectric loss tangent (tan delta) decreases with the substitution of Co{sup 2+} content in the Ni-Zn ferrites.

  10. Coating of zinc ferrite particles with a conducting polymer, polyaniline.

    Science.gov (United States)

    Stejskal, Jaroslav; Trchová, Miroslava; Brodinová, Jitka; Kalenda, Petr; Fedorova, Svetlana V; Prokes, Jan; Zemek, Josef

    2006-06-01

    Particles of zinc ferrite, ZnOFe2O3, were coated with polyaniline (PANI) phosphate during the in situ polymerization of aniline in an aqueous solution of phosphoric acid. The PANI-ferrite composites were characterized by FTIR spectroscopy. X-ray photoelectron spectroscopy was used to determine the degree of coating with a conducting polymer. Even a low content of PANI, 1.4 wt%, resulted in the 45% coating of the particles' surface. On the other hand, even at high PANI content, the coating of ferrite surface did not exceeded 90%. This is explained by the clustering of hydrophobic aniline oligomers at the hydrophilic ferrite surface and the consequent irregular PANI coating. The conductivity increased from 2 x 10(-9) to 6.5 S cm(-1) with increasing fraction of PANI phosphate in the composite. The percolation threshold was located at 3-4 vol% of the conducting component. In the absence of any acid, a conducting product, 1.4 x 10(-2) Scm(-1), was also obtained. As the concentration of phosphoric acid increased to 3 M, the conductivity of the composites reached 1.8 S cm(-1) at 10-14 wt% of PANI. The ferrite alone can act as an oxidant for aniline; a product having a conductivity 0.11 S cm(-1) was obtained after a one-month immersion of ferrite in an acidic solution of aniline.

  11. Dielectric properties of Al-substituted Co ferrite nanoparticles

    Indian Academy of Sciences (India)

    A T Raghavender; K M Jadhav

    2009-12-01

    A series of polycrystalline spinel ferrites with composition, CoFe2–AlO4 (0 ≤ ≤ 1), have been synthesized by sol–gel method. The effect of Al-substitution on structural and dielectric properties is reported in this paper. X-ray diffraction analysis revealed the nanocrystalline nature in the prepared ferrite samples. The particle size, , decreases with increase in Al-content. The lattice parameter, and X-ray density, x, decreased with increase in Al-content. The dielectric properties for all the samples have been studied as a function of frequency in the range 100 Hz–10 MHz. Dielectric properties such as dielectric constant, ′, dielectric loss, ″ and dielectric loss tangent, tan , have been studied for nanocrystalline ferrite samples as a function of frequency. The dielectric constant and dielectric loss obtained for the nanocrystalline ferrites proposed by this technique possess lower value than that of the ferrites prepared by other methods for the same composition. The low dielectric behaviour makes ferrite materials useful in high frequency applications.

  12. Intragranular ferrite morphologies in medium carbon vanadium-microalloyed steel

    Directory of Open Access Journals (Sweden)

    Fadel A.

    2013-01-01

    Full Text Available The aim of this work was to determine TTT diagram of medium carbon V-N micro-alloyed steel with emphasis on the development of intragranular ferrite morphologies. The isothermal treatment was carried out at 350, 400, 450, 500, 550 and 600°C. These treatments were interrupted at different times in order to analyze the evolution of the microstructure. Metallographic evaluation was done using optical and scanning electron microscopy (SEM. The results show that at high temperatures (≥ 500°C polygonal intragranulary nucleated ferrite idiomorphs, combined with grain boundary ferrite and pearlite were produced and followed by an incomplete transformation phenomenon. At intermediate temperatures (450, 500°C an interloced acicular ferrite (AF microstructure is produced, and at low temperatures (400, 350°C the sheave of parallel acicular ferrite plates, similar to bainitic sheaves but intragranularly nucleated were observed. In addition to sheaf type acicular ferrite, the grain boundary nucleated bainitic sheaves are observed. [Projekat Ministartsva nauke Republike Srbije, br. OI174004

  13. Synthesis and characterization of biocompatible hydroxyapatite coated ferrite

    Indian Academy of Sciences (India)

    S Deb; J Giri; S Dasgupta; D Datta; D Bahadur

    2003-12-01

    Ferrite particles coated with biocompatible phases can be used for hyperthermia treatment of cancer. We have synthesized substituted calcium hexaferrite, which is not stable on its own but is stabilized with small substitution of La. Hexaferrite of chemical composition (CaO)0.75(La2O3)0.20(Fe2O3)6 was prepared using citrate gel method. Hydroxyapatite was prepared by precipitating it from aqueous solution of Ca(NO3)2 and (NH4)2HPO4 maintaining pH above 11. Four different methods were used for coating of hydroxyapatite on ferrite particles. SEM with EDX and X-ray diffraction analysis shows clear evidence of coating of hydroxy-apatite on ferrite particles. These coated ferrite particles exhibited coercive field up to 2 kOe, which could be made useful for hysteresis heating in hyperthermia. Studies by culturing BHK-21 cells and WBC over the samples show evidence of biocompatibility. SEM micrographs and cell counts give clear indication of cell growth on the surface of the sample. Finally coated ferrite particle was implanted in Kasaulli mouse to test its biocompatibility. The magnetic properties and biocompatibility studies show that these hydroxyapatite coated ferrites could be useful for hyperthermia.

  14. Effect of heat treatment and irradiation temperature on impact behavior of irradiated reduced-activation ferritic steels

    Energy Technology Data Exchange (ETDEWEB)

    Klueh, R.L.; Alexander, D.J. [Oak Ridge National Lab., TN (United States)

    1998-03-01

    Charpy tests were conducted on eight normalized-and-tempered reduced-activation ferritic steels irradiated in two different normalized conditions. Irradiation was conducted in the Fast Flux Test Facility at 393 C to {approx}14 dpa on steels with 2.25, 5, 9, and 12% Cr (0.1% C) with varying amounts of W, V, and Ta. The different normalization treatments involved changing the cooling rate after austenitization. The faster cooling rate produced 100% bainite in the 2.25 Cr steels, compared to duplex structures of bainite and polygonal ferrite for the slower cooling rate. For both cooling rates, martensite formed in the 5 and 9% Cr steels, and martensite with {approx}25% {delta}-ferrite formed in the 12% Cr steel. Irradiation caused an increase in the ductile-brittle transition temperature (DBTT) and a decrease in the upper-shelf energy. The difference in microstructure in the low-chromium steels due to the different heat treatments had little effect on properties. For the high-chromium martensitic steels, only the 5 Cr steel was affected by heat treatment. When the results at 393 C were compared with previous results at 365 C, all but a 5 Cr and a 9 Cr steel showed the expected decrease in the shift in DBTT with increasing temperature.

  15. Mechanical Properties and Microstructure of Dissimilar Friction Stir Welds of 11Cr-Ferritic/Martensitic Steel to 316 Stainless Steel

    Science.gov (United States)

    Sato, Yutaka S.; Kokawa, Hiroyuki; Fujii, Hiromichi T.; Yano, Yasuhide; Sekio, Yoshihiro

    2015-12-01

    Dissimilar joints between ferritic and austenitic steels are of interest for selected applications in next generation fast reactors. In this study, dissimilar friction-stir welding of an 11 pct Cr ferritic/martensitic steel to a 316 austenitic stainless steel was attempted and the mechanical properties and microstructure of the resulting welds were examined. Friction-stir welding produces a stir zone without macroscopic weld-defects, but the two dissimilar steels are not intermixed. The two dissimilar steels are interleaved along a sharp zigzagging interface in the stir zone. During small-sized tensile testing of the stir zone, this sharp interface did not act as a fracture site. Furthermore, the microstructure of the stir zone was refined in both the ferritic/martensitic steel and the 316 stainless steel resulting in improved mechanical properties over the adjacent base material regions. This study demonstrates that friction-stir welding can produce welds between dissimilar steels that contain no macroscopic weld-defects and display suitable mechanical properties.

  16. A Study on Sodium Effects on the Mechanical Properties of Ferritic-Martensitic Steels

    Energy Technology Data Exchange (ETDEWEB)

    Shin, Sang Hun; Kim, Ji Hyun [Ulsan National Institute of Science and Technology, Ulsan (Korea, Republic of); Kim, Jun Hwan [Korea Atomic Energy Research Institute, Daejeon (Korea, Republic of)

    2014-05-15

    A sodium-cooled fast reactor (SFR) that uses fast neutrons as a fission process is considered one of the most probable candidates in next generation reactors. As an SFR core experiences high temperatures (650 .deg. C) and neutron doses (200 dpa), ferritic-martensitic steel, especially HT9 steel containing 12% Cr, is being considered due to its superior dimensional stability against high-energy neutron irradiation. After irradiation to 35 dpa at 420 .deg. C, at the Fast Flux Test Facility (FFTF), swelling of the reduced-activation 9Cr-2WV and 9Cr-2WVTa steels and the conventional 9Cr-1Mo-VNb and 12Cr-1Mo-VW steels was estimated by transmission electron microscopy (TEM) to be 0.2%, 0.33%, 0.85%, and 0.007%, respectively. The irradiation creep coefficient for neutron-irradiated steels is 2 Χ 10{sup -7} Mpa{sup -1} dpa{sup -1} for HT9 at 440-500 .deg. C with 14 dpa (EBR-II), and 1.5 Χ 10{sup -7} Mpa{sup -1} dpa{sup -1} is a good estimate for such ferritic/martensitic steels. In this study, ASTM A192 Gr. 92 steels were exposed to liquid sodium at 650 .deg. C for 1583 h and 3095 h and evaluation of the microstructure as well as the mechanical properties using ring hoop tensile tests and ring hoop creep tests were conducted. The objective of this study is to evaluate the microstructure and mechanical properties of ferritic-martensitic steel (ASTM A192 Gr. 92) that has been exposed to a high-temperature sodium environment. In order to investigate the effect of the aging process on the precipitates and the mechanical properties of Gr. 92 steel, specimens were exposed to 650 .deg. C liquid sodium and aged in a 650 .deg. C argon environment for a given time. V-rich MX-type carbonitride and M{sub 23}C{sub 6} were found in the as-received specimen. In the specimens which were exposed to sodium, mainly Cr{sub 23}C{sub 6} was observed while the Laves phase was mainly observed in the specimen that was aged in an argon environment. The maximum load of Gr. 92 steel that was

  17. Frequency-dependent magnetic susceptibility of magnetite and cobalt ferrite nanoparticles embedded in PAA hydrogel.

    Science.gov (United States)

    van Berkum, Susanne; Dee, Joris T; Philipse, Albert P; Erné, Ben H

    2013-05-14

    Chemically responsive hydrogels with embedded magnetic nanoparticles are of interest for biosensors that magnetically detect chemical changes. A crucial point is the irreversible linkage of nanoparticles to the hydrogel network, preventing loss of nanoparticles upon repeated swelling and shrinking of the gel. Here, acrylic acid monomers are adsorbed onto ferrite nanoparticles, which subsequently participate in polymerization during synthesis of poly(acrylic acid)-based hydrogels (PAA). To demonstrate the fixation of the nanoparticles to the polymer, our original approach is to measure low-field AC magnetic susceptibility spectra in the 0.1 Hz to 1 MHz range. In the hydrogel, the magnetization dynamics of small iron oxide nanoparticles are comparable to those of the particles dispersed in a liquid, due to fast Néel relaxation inside the particles; this renders the ferrogel useful for chemical sensing at frequencies of several kHz. However, ferrogels holding thermally blocked iron oxide or cobalt ferrite nanoparticles show significant decrease of the magnetic susceptibility resulting from a frozen magnetic structure. This confirms that the nanoparticles are unable to rotate thermally inside the hydrogel, in agreement with their irreversible fixation to the polymer network.

  18. Frequency-Dependent Magnetic Susceptibility of Magnetite and Cobalt Ferrite Nanoparticles Embedded in PAA Hydrogel

    Directory of Open Access Journals (Sweden)

    Ben H. Erné

    2013-05-01

    Full Text Available Chemically responsive hydrogels with embedded magnetic nanoparticles are of interest for biosensors that magnetically detect chemical changes. A crucial point is the irreversible linkage of nanoparticles to the hydrogel network, preventing loss of nanoparticles upon repeated swelling and shrinking of the gel. Here, acrylic acid monomers are adsorbed onto ferrite nanoparticles, which subsequently participate in polymerization during synthesis of poly(acrylic acid-based hydrogels (PAA. To demonstrate the fixation of the nanoparticles to the polymer, our original approach is to measure low-field AC magnetic susceptibility spectra in the 0.1 Hz to 1 MHz range. In the hydrogel, the magnetization dynamics of small iron oxide nanoparticles are comparable to those of the particles dispersed in a liquid, due to fast Néel relaxation inside the particles; this renders the ferrogel useful for chemical sensing at frequencies of several kHz. However, ferrogels holding thermally blocked iron oxide or cobalt ferrite nanoparticles show significant decrease of the magnetic susceptibility resulting from a frozen magnetic structure. This confirms that the nanoparticles are unable to rotate thermally inside the hydrogel, in agreement with their irreversible fixation to the polymer network.

  19. Frequency-Dependent Magnetic Susceptibility of Magnetite and Cobalt Ferrite Nanoparticles Embedded in PAA Hydrogel

    Science.gov (United States)

    van Berkum, Susanne; Dee, Joris T.; Philipse, Albert P.; Erné, Ben H.

    2013-01-01

    Chemically responsive hydrogels with embedded magnetic nanoparticles are of interest for biosensors that magnetically detect chemical changes. A crucial point is the irreversible linkage of nanoparticles to the hydrogel network, preventing loss of nanoparticles upon repeated swelling and shrinking of the gel. Here, acrylic acid monomers are adsorbed onto ferrite nanoparticles, which subsequently participate in polymerization during synthesis of poly(acrylic acid)-based hydrogels (PAA). To demonstrate the fixation of the nanoparticles to the polymer, our original approach is to measure low-field AC magnetic susceptibility spectra in the 0.1 Hz to 1 MHz range. In the hydrogel, the magnetization dynamics of small iron oxide nanoparticles are comparable to those of the particles dispersed in a liquid, due to fast Néel relaxation inside the particles; this renders the ferrogel useful for chemical sensing at frequencies of several kHz. However, ferrogels holding thermally blocked iron oxide or cobalt ferrite nanoparticles show significant decrease of the magnetic susceptibility resulting from a frozen magnetic structure. This confirms that the nanoparticles are unable to rotate thermally inside the hydrogel, in agreement with their irreversible fixation to the polymer network. PMID:23673482

  20. Analysis of ferrite heating of the LHC injection kickers and proposals for future reduction of temperature

    CERN Document Server

    Barnes, M J; Garrel, N; Goddard, B; Mertens, V; Weterings, W

    2012-01-01

    The two LHC injection kicker magnet (MKI) systems must produce a kick of 1.3 T.m with a flat top duration variable up to 7860 ns, and rise and fall times of less than 900 ns and 3000 ns, respectively. A beam screen is placed in the aperture of the magnets: the screen consists of a ceramic tube with conductors on the inner wall. The conductors provide a path for the image current of the high intensity LHC beam and screen the ferrite against wake fields. The conductors initially used gave adequately low beam coupling impedance however screen conductor discharges occurred during pulsing of the magnet; hence an alternative design with fewer screen conductors was implemented to meet the often conflicting requirements for low beam coupling impedance, fast magnetic field rise-time and good high voltage behaviour. During 2011 the LHC was operated with high intensity beam, coasting for many hours at a time, resulting in heating of the ferrite yoke of the MKIs. This paper presents an analysis of thermal measurement dat...

  1. Kinetics of niobium carbide precipitation in ferrite; Cinetiques de precipitation du carbure de niobium dans la ferrite

    Energy Technology Data Exchange (ETDEWEB)

    Gendt, D

    2001-07-01

    The aim of this study is to develop a NbC precipitation modelling in ferrite. This theoretical study is motivated by the fact it considers a ternary system and focus on the concurrence of two different diffusion mechanisms. An experimental study with TEP, SANS and Vickers micro-hardening measurements allows a description of the NbC precipitation kinetics. The mean radius of the precipitates is characterized by TEM observations. To focus on the nucleation stage, we use the Tomographic Atom Probe that analyses, at an atomistic scale, the position of the solute atoms in the matrix. A first model based on the classical nucleation theory and the diffusion-limited growth describes the precipitation of spherical precipitates. To solve the set of equations, we use a numerical algorithm that furnishes an evaluation of the precipitated fraction, the mean radius and the whole size distribution of the particles. The parameters that are the interface energy, the solubility product and the diffusion coefficients are fitted with the data available in the literature and our experimental results. It allows a satisfactory agreement as regards to the simplicity of the model. Monte Carlo simulations are used to describe the evolution of a ternary alloy Fe-Nb-C on a cubic centred rigid lattice with vacancy and interstitial mechanisms. This is realized with an atomistic description of the atoms jumps and their related frequencies. The model parameters are fitted with phase diagrams and diffusion coefficients. For the sake of simplicity, we consider that the precipitation of NbC is totally coherent and we neglect any elastic strain effect. We can observe different kinetic paths: for low supersaturations, we find an expected precipitation of NbC but for higher supersaturations, the very fast diffusivity of carbon atoms conducts to the nucleation of iron carbide particles. We establish that the occurrence of this second phenomenon depends on the vacancy arrival kinetics and can be related

  2. Synthesis, characterization and potential application of MnZn ferrite and MnZn ferrite @ Au nanoparticles.

    Science.gov (United States)

    Wang, Xin; Wang, Lingyan; Lim, I-Im S; Bao, Kun; Mott, Derrick; Park, Hye-Young; Luo, Jin; Hao, Shunli; Zhong, Chuan-Jian

    2009-05-01

    The ability to tune the magnetic properties of magnetic nanoparticles by manipulating the composition or surface properties of the nanoparticles is important for exploiting the application of the nanomaterials. This report describes preliminary findings of an investigation of the viability of synthesizing MnZn ferrite and core @ shell MnZn ferrite @ Au nanoparticles as potentially magnetization-tunable nanomaterials. The synthesis of the core-shell magnetic nanoparticles involved a simple combination of seed formation of the MnZn ferrite magnetic nanoparticles and surface coating of the seeds with gold shells. Water-soluble MnZn ferrite nanoparticles of 20-40 nm diameters and MnZn ferrite @ Au nanoparticles of 30-60 nm have been obtained. The MnZn ferrite @ Au nanoparticles have been demonstrated to be viable in magnetic separation of nanoparticles via interparticle antibody-specific binding reactivity between antibodies on the gold shells of the core-shell magnetic particles and proteins on gold nanoparticles. These findings have significant implications to the design of the core @ shell magnetic nanomaterials with core composition tuned magnetization for bioassay application.

  3. Analytical modeling of demagnetizing effect in magnetoelectric ferrite/PZT/ferrite trilayers taking into account a mechanical coupling

    Science.gov (United States)

    Loyau, V.; Aubert, A.; LoBue, M.; Mazaleyrat, F.

    2017-03-01

    In this paper, we investigate the demagnetizing effect in ferrite/PZT/ferrite magnetoelectric (ME) trilayer composites consisting of commercial PZT discs bonded by epoxy layers to Ni-Co-Zn ferrite discs made by a reactive Spark Plasma Sintering (SPS) technique. ME voltage coefficients (transversal mode) were measured on ferrite/PZT/ferrite trilayer ME samples with different thicknesses or phase volume ratio in order to highlight the influence of the magnetic field penetration governed by these geometrical parameters. Experimental ME coefficients and voltages were compared to analytical calculations using a quasi-static model. Theoretical demagnetizing factors of two magnetic discs that interact together in parallel magnetic structures were derived from an analytical calculation based on a superposition method. These factors were introduced in ME voltage calculations which take account of the demagnetizing effect. To fit the experimental results, a mechanical coupling factor was also introduced in the theoretical formula. This reflects the differential strain that exists in the ferrite and PZT layers due to shear effects near the edge of the ME samples and within the bonding epoxy layers. From this study, an optimization in magnitude of the ME voltage is obtained. Lastly, an analytical calculation of demagnetizing effect was conducted for layered ME composites containing higher numbers of alternated layers (n ≥ 5). The advantage of such a structure is then discussed.

  4. Interaction between fast ions and ion cyclotron heating in a tokamak plasma; Interaction des ions rapides avec les ondes a la frequence cyclotronique ionique dans un plasma de tokamak

    Energy Technology Data Exchange (ETDEWEB)

    Bergeaud, V

    2001-11-01

    In an ignited fusion reactor, the plasma temperature is sustained by the fusion reactions. However, before this regime is reached, it is necessary to bring an additional power to the plasma. One of the methods that enables the coupling of power is the use of an electromagnetic wave in the ion cyclotron range of frequencies (ICRF). This thesis deals with the interaction between ICRF heating and the fast ions. The thesis contains a theoretical study of the influence of ICRF heating on the ion distribution function. A particular emphasis is put on the importance of the toroidal spectrum of the modes of propagation of the wave in the tokamak. It is necessary to take into account all these modes in order to correctly assess the strength of the wave particle interaction, especially for high energy particles (of the order of hundreds of keV). The classical treatment of the wave particle interaction is based on the hypothesis that the cyclotron phase of the particle and the wave phase are de-correlated between successive resonant interactions. One is therefore led to consider ICRF heating as a diffusive process. This hypothesis is reconsidered in this thesis and it is shown that strong correlations exist in a large part of the velocity space. For this study, a numerical code that computes the full trajectory of particles interacting with a complete electromagnetic field has been developed. The thesis also deals with the problem of fast ion losses due to the breaking of the toroidal symmetry of the confinement magnetic field (called the ripple modulation). Between two toroidal coils, local magnetic wells exist, and particles can be trapped there. When trapped they undergo a vertical drift that makes them quit the plasma rapidly. The ripple modulation also causes an enhancement of the radial diffusion, thereby increasing the losses. A Monte Carlo model describing these mechanisms is presented. This model is validated thanks to a comparison with an experimental database from

  5. Interaction of fast ions with ion cyclotron electromagnetic waves in tokamak plasma; Interaction des ions rapides avec les ondes a la frequence cyclotronique ionique dans un plasma de tokamak

    Energy Technology Data Exchange (ETDEWEB)

    Bergeaud, V

    2000-12-01

    In an ignited fusion reactor, the plasma temperature is sustained by the fusion reactions. However, before this regime is reached, it is necessary to bring an additional power to the plasma. One of the methods that enables the coupling of power is the use of an electromagnetic wave in the ion cyclotron range of frequencies (ICRF). This thesis deals with the interaction between ICRF heating and the fast ions. The thesis contains a theoretical study of the influence of ICRF heating on the ion distribution function. A particular emphasis is put on the importance of the toroidal spectrum of the modes of propagation of the wave in the tokamak. It is necessary to take into account all these modes in order to correctly assess the strength of the wave particle interaction, especially for high energy particles (of the order of hundreds of keV). The classical treatment of the wave particle interaction is based on the hypothesis that the cyclotron phase of the particle and the wave phase are de-correlated between successive resonant interactions. One is therefore led to consider ICRF heating as a diffusive process. This hypothesis is reconsidered in this thesis and it is shown that strong correlations exist in a large part of the velocity space. For this study, a numerical code that computes the full trajectory of particles interacting with a complete electromagnetic field has been developed. The thesis also deals with the problem of fast ion losses due to the breaking of the toroidal symmetry of the confinement magnetic field (called the ripple modulation). Between two toroidal coils, local magnetic wells exist, and particles can be trapped there. When trapped they undergo a vertical drift that makes them quit the plasma rapidly. The ripple modulation also causes an enhancement of the radial diffusion, thereby increasing the losses. A Monte Carlo model describing these mechanisms is presented. This model is validated thanks to a comparison with an experimental database from

  6. Physical facets of ultrasonic cavitational synthesis of zinc ferrite particles.

    Science.gov (United States)

    Reddy, Bhaskar Rao; Sivasankar, Thirugnanasambandam; Sivakumar, Manickam; Moholkar, Vijayanand S

    2010-02-01

    This paper addresses the physical features of the ultrasonic cavitational synthesis of zinc ferrite particles and tries to establish the relationship between cavitation physics and sonochemistry of the zinc ferrite synthesis. A dual approach of coupling experimental results with simulations of radial motion of cavitation bubbles has been adopted. The precursors for the zinc ferrite, viz. ZnO and Fe(3)O(4) are produced in situ by the hydrolysis of Zn and Fe(II) acetates stimulated by (*)OH radicals produced from the transient collapse of the cavitation bubbles. Experiments performed under different conditions create significant variation in the production of (*)OH radicals, and hence, the rate of acetate hydrolysis. Correlation of the results of experiments and simulations sheds light on the important facets of the physical mechanism of ultrasonic cavitational zinc ferrite synthesis. It is revealed that too much or too little rate of acetate hydrolysis results in smaller particle size of zinc ferrite. The first effect of a higher rate of hydrolysis leads to excessively large growth of particles, due to which they become susceptible to the disruptive action of cavitation bubbles. Whereas, the second effect of too small rate of hydrolysis of Zn and Fe(II) acetates restricts the growth of particles. It has been observed that the initial reactant concentration does not influence the mean particle size or the size distribution of zinc ferrite particles. The present investigation clearly confirms that the rate-controlling step of zinc ferrite synthesis through ultrasonic cavitational route is the rate of formation of (*)OH radicals from cavitation bubbles.

  7. Scattering from the Quasi-Optical Ferrite Circulator Using a Coupled Integral Equation/FEM Solution

    Science.gov (United States)

    Epp, L. W.; Hoppe, D. J.; Chinn, G. C.; Lee, J.

    1994-01-01

    Ferrite materials are used in microwave devices that exploit the property of Faraday rotation to give non-reciprocal behavior. Examples of common waveguide components that use ferrite materials include circulators, isolators and gyrators.

  8. Unraveling the Effect of Thermomechanical Treatment on the Dissolution of Delta Ferrite in Austenitic Stainless Steels

    Science.gov (United States)

    Rezayat, Mohammad; Mirzadeh, Hamed; Namdar, Masih; Parsa, Mohammad Habibi

    2016-02-01

    Considering the detrimental effects of delta ferrite stringers in austenitic stainless steels and the industrial considerations regarding energy consumption, investigating, and optimizing the kinetics of delta ferrite removal is of vital importance. In the current study, a model alloy prone to the formation of austenite/delta ferrite dual phase microstructure was subjected to thermomechanical treatment using the wedge rolling test aiming to dissolve delta ferrite. The effect of introducing lattice defects and occurrence of dynamic recrystallization (DRX) were investigated. It was revealed that pipe diffusion is responsible for delta ferrite removal during thermomechanical process, whereas when the DRX is dominant, the kinetics of delta ferrite dissolution tends toward that of the static homogenization treatment for delta ferrite removal that is based on the lattice diffusion of Cr and Ni in austenite. It was concluded that the optimum condition for dissolution of delta ferrite can be defined by the highest rolling temperature and strain in which DRX is not pronounced.

  9. Low temperature sintering of MgCuZn ferrite and its electrical and magnetic properties

    Indian Academy of Sciences (India)

    S R Murthy

    2001-08-01

    The low temperature sintering of MgCuZn ferrite was investigated using the usual ceramic method. The effect of Cu substitution on the properties of MgZn ferrites was also investigated and it was found that the densification of MgCuZn ferrite is dependent upon Cu concentration. The sintered ferrite with a density of 4.93 g/cm3 and electrical resistivity > 1011-cm was obtained for the ferrite with 12 mol% Cu at relatively low sintering temperature (910°C). The magnetic properties of the ferrites also improved by the Cu substitution. The chip inductors made of the ferrite fired at 910 C with 12 mol% Cu exhibited higher d.c. resistance. From these studies it is concluded that the good quality chip inductor can be obtained using the MgCuZn ferrites.

  10. Synthesis of Novel Ferrite Based Recyclable Catalyst Used to Clean Dye and Emerging Contaminates from Water

    Science.gov (United States)

    Herein, we describe synthesis of novel palladium, copper, cobalt and vanadium ferrites. The ferrites were synthesized by combustion method using polyvinyl alcohol. The particles phases were confirmed using X-ray diffraction and sizes were determined using particle size analyzer. ...

  11. Synthesis of Novel Ferrite Based Recyclable Catalyst Used to Clean Dye and Emerging Contaminates from Water

    Science.gov (United States)

    Herein, we describe synthesis of novel palladium, copper, cobalt and vanadium ferrites. The ferrites were synthesized by combustion method using polyvinyl alcohol. The particles phases were confirmed using X-ray diffraction and sizes were determined using particle size analyzer. ...

  12. Performance of ferrite fillers on electrical behavior of polymer nanocomposite electrolyte

    Science.gov (United States)

    Pandey, Kamlesh; Mauli Dwivedi, Mrigank; Singh, Markandey; Agrawal, S. L.

    2011-04-01

    Dispersal of nanofillers in polymer electrolytes have shown to improve the ionic properties of Polyethylene oxide (PEO)-based polymer electrolytes in recent times. The effects of different nanoferrite fillers (i.e., Al-Zn ferrite, Mg-Zn ferrite, and Zn ferrite) on the electrical transport properties have been studied here on the composite polymer electrolyte system. The interaction of salt/filler with electrolyte has been investigated by XRD studies. SEM image and infrared spectral studies give an indication of nanocomposite formation. In conductivity studies, all electrolyte systems are seen to follow universal power law. Composition dependence (with ferrite filler) gives the maximum conductivity in [93PEO-7NH4SCN]: X ferrite (where X = 2% in Al-Zn ferrite, 1% Mg-Zn ferrite, and 1% Zn ferrite) system.

  13. Sodium fast reactor evaluation: Core materials

    Science.gov (United States)

    Cheon, Jin Sik; Lee, Chan Bock; Lee, Byoung Oon; Raison, J. P.; Mizuno, T.; Delage, F.; Carmack, J.

    2009-07-01

    In the framework of the Generation IV Sodium Fast Reactor (SFR) Program the Advanced Fuel Project has conducted an evaluation of the available fuel systems supporting future sodium cooled fast reactors. In this paper the status of available and developmental materials for SFR core cladding and duct applications is reviewed. To satisfy the Generation IV SFR fuel requirements, an advanced cladding needs to be developed. The candidate cladding materials are austenitic steels, ferritic/martensitic (F/M) steels, and oxide dispersion strengthened (ODS) steels. A large amount of irradiation testing is required, and the compatibility of cladding with TRU-loaded fuel at high temperatures and high burnup must be investigated. The more promising F/M steels (compared to HT9) might be able to meet the dose requirements of over 200 dpa for ducts in the GEN-IV SFR systems.

  14. Oxide dispersion strengthened ferritic steels: a basic research joint program in France

    Science.gov (United States)

    Boutard, J.-L.; Badjeck, V.; Barguet, L.; Barouh, C.; Bhattacharya, A.; Colignon, Y.; Hatzoglou, C.; Loyer-Prost, M.; Rouffié, A. L.; Sallez, N.; Salmon-Legagneur, H.; Schuler, T.

    2014-12-01

    AREVA, CEA, CNRS, EDF and Mécachrome are funding a joint program of basic research on Oxide Dispersion Strengthened Steels (ODISSEE), in support to the development of oxide dispersion strengthened 9-14% Cr ferritic-martensitic steels for the fuel element cladding of future Sodium-cooled fast neutron reactors. The selected objectives and the results obtained so far will be presented concerning (i) physical-chemical characterisation of the nano-clusters as a function of ball-milling process, metallurgical conditions and irradiation, (ii) meso-scale understanding of failure mechanisms under dynamic loading and creep, and, (iii) kinetic modelling of nano-clusters nucleation and α/α‧ unmixing.

  15. Functionalized bismuth ferrite harmonic nanoparticles for cancer cells labeling and imaging

    Energy Technology Data Exchange (ETDEWEB)

    Passemard, Solène; Staedler, Davide; Sonego, Giona [Ecole Polytechnique Fédérale de Lausanne, Institute of Chemical Sciences and Engineering (Switzerland); Magouroux, Thibaud [Université de Genève, GAP-Biophotonics (Switzerland); Schneiter, Guillaume Stéphane [Ecole Polytechnique Fédérale de Lausanne, Institute of Chemical Sciences and Engineering (Switzerland); Juillerat-Jeanneret, Lucienne [University Institute of Pathology, CHUV-UNIL (Switzerland); Bonacina, Luigi [Université de Genève, GAP-Biophotonics (Switzerland); Gerber-Lemaire, Sandrine, E-mail: Sandrine.Gerber@epfl.ch [Ecole Polytechnique Fédérale de Lausanne, Institute of Chemical Sciences and Engineering (Switzerland)

    2015-10-15

    Bismuth ferrite (BFO) harmonic nanoparticles (NPs) display high nonlinear optical efficiency and excellent biocompatibility profile which make them attractive for the development of diagnostic applications as contrast agents. In this study, we present a general method for the functionalization of this material with chemical ligands targeting cancer molecular biomarkers. In particular, a conjugation protocol based on click reaction between alkynyl-containing targeting ligands and poly(ethylene glycol)-coated BFO NPs (67.7 nm) displaying surface reactive azido groups was developed. Copper-free click reaction allowed fast and efficient conjugation of a covalent inhibitor of prolyl-specific endopeptidases to coated BFO NPs. The ability of these functionalized nanomaterials (134.2 nm) to act as imaging probes for cancer cells was demonstrated by the selective labeling of human lung cancer cells.

  16. Beam Coupling Impedances of Traveling-Wave Ferrite-Free Extraction Kickers

    Science.gov (United States)

    Kurennoy, Sergey

    2002-04-01

    Fast traveling-wave extraction kickers contain no ferrite and consist of two long metallic parallel plates supported by insulators inside a beam pipe. A beam is deflected by both the electric and magnetic fields of a TEM wave created by a pulse propagating along the strips in the direction opposite to the beam. Computations of the beam coupling impedances for such structures are difficult because of their length. In the paper, the beam coupling impedances of such transmission-line kickers are calculated by combining analytical and numerical methods: the wake potentials computed in short models are extended analytically to obtain the wakes for the long kickers, and then the corresponding beam impedances are derived. As one can expect, at very low frequencies the results are in agreement with simple analytical expressions available for the coupling impedances of striplines in beam position monitors.

  17. Plasma spot welding of ferritic stainless steels

    Directory of Open Access Journals (Sweden)

    Lešnjak, A.

    2002-06-01

    Full Text Available Plasma spot welding of ferritic stainless steels is studied. The study was focused on welding parameters, plasma and shielding gases and the optimum welding equipment. Plasma-spot welded overlap joints on a 0.8 mm thick ferritic stainless steel sheet were subjected to a visual examination and mechanical testing in terms of tension-shear strength. Several macro specimens were prepared. Plasma spot welding is suitable to use the same gas as shielding gas and as plasma gas, i.e., a 98 % Ar/2 % H 2 gas mixture. Tension-shear strength of plasma-spot welded joints was compared to that of resistance-spot welded joints. It was found that the resistance welded joints withstand a somewhat stronger load than the plasma welded joints due to a larger weld spot diameter of the former. Strength of both types of welded joints is approximately the same.

    El artículo describe el proceso de soldeo de aceros inoxidables ferríticos por puntos con plasma. La investigación se centró en el establecimiento de los parámetros óptimos de la soldadura, la definición del gas de plasma y de protección más adecuado, así como del equipo óptimo para la realización de la soldadura. Las uniones de láminas de aceros inoxidables ferríticos de 0,8 mm de espesor, soldadas a solape por puntos con plasma, se inspeccionaron visualmente y se ensayaron mecánicamente mediante el ensayo de cizalladura por tracción. Se realizaron macro pulidos. Los resultados de la investigación demostraron que la solución más adecuada para el soldeo por puntos con plasma es elegir el mismo gas de plasma que de protección. Es decir, una mezcla de 98 % de argón y 2 % de hidrógeno. La resistencia a la cizalladura por tracción de las uniones soldadas por puntos con plasma fue comparada con la resistencia de las uniones soldadas por resistencia por puntos. Se llegó a la conclusión de que las uniones soldadas por resistencia soportan una carga algo mayor que la uniones

  18. 2-dimensional mapping of ICRF-induced scrape-off layer modifications with a retarding field analyser on ASDEX-Upgrade

    Science.gov (United States)

    Colas, L.; Bobkov, V.; Carralero, D.; Kočan, M.; Müller, H. W.; Manz, P.; Kubič, M.; Gunn, J. P.; Herrmann, A.; Rohde, V.; ASDEX-Upgrade Team

    2014-02-01

    Using a reciprocating Retarding Field Analyser (RFA), Scrape-Off Layer (SOL) modifications were investigated on ASDEX-Upgrade during heating with waves in the Ion Cyclotron Range of Frequencies (ICRF), suspected for enhanced impurity production in this all-metal machine. Two quantities involved in the sputtering were measured: the current Islit on a saturated slit plate, proportional to the parallel ion flux and the mean parallel energy t of collected ions, averaged over many RF cycles. Combining multiple RFA reciprocations over a scan of q95 provided 2D poloidal/radial resolution. In the outer SOL a localized RF-perturbed zone was evidenced on the RFA side magnetically connected to an active ICRF antenna. A flat 2D Islit pattern surrounded by steep gradients was observed, correlatively with t exceeding 150eV. The centre of the zone is connected radially slightly behind the leading edge of antenna side limiters, with a radial extension up to ±2cm. The zone is broadest and t is largest near the bottom of the active antenna. This is interpreted as a zone of local plasma biasing via sheath rectification, creating density convection around it. The Islit pattern is qualitatively consistent with simple considerations about E×B particle convection.

  19. LETTER: Study of combined NBI and ICRF enhancement of the D-3He fusion yield with a Fokker-Planck code

    Science.gov (United States)

    Azoulay, M.; George, M. A.; Burger, A.; Collins, W. E.; Silberman, E.

    A two-dimensional bounce averaged Fokker-Planck code is used to study the fusion yield and the wave absorption by residual hydrogen ions in higher harmonic ICRF heating of D (120 keV) and 3He (80 keV) beams in the JT-60U tokamak. Both for the fourth harmonic resonance of 3He (ω = 4ωc3He(0), which is accompanied by the third harmonic resonance of hydrogen (ω = 3ωcH) at the low field side, and for the third harmonic resonance of 3He (ω = 4ωcD(0) = 3ωc3He(0)) = 2ωcH(0)), a few per cent of hydrogen ions are found to absorb a large fraction of the ICRF power and to degrade the fusion output power. In the latter case, D beam acceleration due to the fourth harmonic resonance in the 3He(D) regime can enhance the fusion yield more effectively. A discussion is given of the effect of D beam acceleration due to the fifth harmonic resonance (ω = 5ωcD) at the high field side in the case of ω = 4ωc3He(0) and of the optimization of the fusion yield in the case of lower electron density and higher electron temperature

  20. Microwave left-handed composite material made of slim ferrite rods and metallic wires

    Institute of Scientific and Technical Information of China (English)

    Xu Fang; Bai Yang; Qiao Li-Jie; Zhao Hong-Jie; Zhou Ji

    2009-01-01

    This paper reports on experimental study of the microwave properties of a composite material consisting of ferrite and copper wires.It finds that the slim ferrite rods can modify the magnetic field distribution through their anisotropy,so that the ferrite's negative influence on the copper wires'plasma will be reduced.Left-handed properties are observed even in the specimen with close stuck ferrite rods and copper wires.

  1. Nucleation and three-dimensional morphology of intragranular ferrite in a vanadium microalloyed steel

    Institute of Scientific and Technical Information of China (English)

    2005-01-01

    The formation of intragranular ferrite at inclusions was analyzed by SEM-EDX in a vanadium microalloyed steel with an excess amount of sulfur. The precipitation of MnS at aluminum oxides may result in Mn depletion, which, in turn, promotes the formation of intragranular ferrite. The morphology of intragranular ferrite changed with undercooling. At higher temperatures intragranular ferrite is nearly equiaxed whereas it is plate-like at lower temperatures.

  2. Plasma discharge in ferritic first wall vacuum vessel of the Hitachi Tokamak HT-2

    Energy Technology Data Exchange (ETDEWEB)

    Abe, Mitsushi; Nakayama, Takeshi; Asano, Katsuhiko; Otsuka, Michio [Hitachi Ltd., Tokyo (Japan)

    1997-11-01

    A tokamak discharge with ferritic material first wall was tried successfully. The Hitachi Tokamak HT-2 had a stainless steel SUS304 vacuum vessel and modified to have a ferritic plate first wall for experiments to investigate the possibility of ferritic material usage in magnetic fusion devices. The achieved vacuum pressure and times used for discharge cleaning was roughly identical with the stainless steel first wall or the original HT-2. We concluded that ferritic material vacuum vessel is possible for tokamaks. (author)

  3. 77 FR 60478 - Control of Ferrite Content in Stainless Steel Weld Metal

    Science.gov (United States)

    2012-10-03

    ... COMMISSION Control of Ferrite Content in Stainless Steel Weld Metal AGENCY: Nuclear Regulatory Commission... Ferrite Content in Stainless Steel Weld Metal.'' This guide describes a method that the NRC staff considers acceptable for controlling ferrite content in stainless steel weld metal. Revision 4 updates...

  4. Kinetics modeling of delta-ferrite formation and retainment during casting of supermartensitic stainless steel

    DEFF Research Database (Denmark)

    Nießen, Frank; Tiedje, Niels Skat; Hald, John

    2017-01-01

    -ferrite originates from the incomplete transformation to austenite. The kinetics model predicted the measured amount of δ-ferrite and the partitioning of Cr and Ni reasonably well. Further, it showed that slower cooling for the investigated alloy leads to less retained δ-ferrite, which is in excellent agreement...

  5. Ferrite-based magnetic nanofluids used in hyperthermia applications

    Energy Technology Data Exchange (ETDEWEB)

    Sharifi, Ibrahim [Electroceramics Group, Department of Materials Science and Engineering, Shiraz University of Technology, Shiraz (Iran, Islamic Republic of); Shokrollahi, H., E-mail: Shokrollahi@sutech.ac.ir [Electroceramics Group, Department of Materials Science and Engineering, Shiraz University of Technology, Shiraz (Iran, Islamic Republic of); Amiri, S. [Electroceramics Group, Department of Materials Science and Engineering, Shiraz University of Technology, Shiraz (Iran, Islamic Republic of)

    2012-03-15

    Magnetic ferrofluids (magnetic nanofluids) have received special attention due to their various biomedical applications such as drug delivery and hyperthermia treatment for cancer. The biological applications impose some special requirements. For example, the well-known iron oxide ferrofluids become undesirable because their iron atoms are poorly distinguishable from those of hemoglobin. A conceivable solution is to use mixed-ferrites (MFe{sub 2}O{sub 4} where M=Co, Mn, Ni, Zn) to have a range of magnetic properties. These ferrites have attracted special attention because they save time, and because of their low inherent toxicity, ease of synthesis, physical and chemical stabilities and suitable magnetic properties. Based on the importance of ferrite particles in ferrofluids for hyperthermia treatment, this paper gives a summary on the physical concepts of ferrofluids, hyperthermia principal, magnetic properties and synthesis methods of nanosized ferrites. - Highlights: Black-Right-Pointing-Pointer This paper gives a suitable summary and literature survey on the ferrofluids. Black-Right-Pointing-Pointer Ferrofluids have an important role in biomedicine and our life. Black-Right-Pointing-Pointer Ferrofluids include a magnetic core, surfactant and a liquid medium. Black-Right-Pointing-Pointer Nano-ferrites' cores are good candidates for hyperthermia purposes. Black-Right-Pointing-Pointer They present a suitable heat generation for hyperthermia.

  6. Strong and moldable cellulose magnets with high ferrite nanoparticle content.

    Science.gov (United States)

    Galland, Sylvain; Andersson, Richard L; Ström, Valter; Olsson, Richard T; Berglund, Lars A

    2014-11-26

    A major limitation in the development of highly functional hybrid nanocomposites is brittleness and low tensile strength at high inorganic nanoparticle content. Herein, cellulose nanofibers were extracted from wood and individually decorated with cobalt-ferrite nanoparticles and then for the first time molded at low temperature (ferrite and cellulose material. A nanocomposite with 70 wt % ferrite, 20 wt % cellulose nanofibers, and 10 wt % epoxy showed a modulus of 12.6 GPa, a tensile strength of 97 MPa, and a strain at failure of ca. 4%. Magnetic characterization was performed in a vibrating sample magnetometer, which showed that the coercivity was unaffected and that the saturation magnetization was in proportion with the ferrite content. The used ferrite, CoFe2O4, is a magnetically hard material, demonstrated by that the composite material behaved as a traditional permanent magnet. The presented processing route is easily adaptable to prepare millimeter-thick and moldable magnetic objects. This suggests that the processing method has the potential to be scaled-up for industrial use for the preparation of a new subcategory of magnetic, low-cost, and moldable objects based on cellulose nanofibers.

  7. Quantum mechanical method for estimating ionicity of spinel ferrites

    Energy Technology Data Exchange (ETDEWEB)

    Ji, D.H. [Hebei Advanced Thin Films Laboratory, Department of Physics, Hebei Normal University, Shijiazhuang City 050024 (China); Tang, G.D., E-mail: tanggd@mail.hebtu.edu.cn [Hebei Advanced Thin Films Laboratory, Department of Physics, Hebei Normal University, Shijiazhuang City 050024 (China); Li, Z.Z.; Hou, X.; Han, Q.J.; Qi, W.H.; Liu, S.R.; Bian, R.R. [Hebei Advanced Thin Films Laboratory, Department of Physics, Hebei Normal University, Shijiazhuang City 050024 (China)

    2013-01-15

    The ionicity (0.879) of cubic spinel ferrite Fe{sub 3}O{sub 4} has been determined, using both experimental magnetization and density of state calculations from the density functional theory. Furthermore, a quantum mechanical estimation method for the ionicity of spinel ferrites is proposed by comparing the results from Phillips' ionicity. On the basis of this, ionicities of the spinel ferrites MFe{sub 2}O{sub 4} (M=Mn, Fe, Co, Ni, Cu) are calculated. As an application, the ion distribution at (A) and [B] sites of (A)[B]{sub 2}O{sub 4} spinel ferrites MFe{sub 2}O{sub 4} (M=Fe, Co, Ni, Cu) are calculated using current ionicity values. - Highlights: Black-Right-Pointing-Pointer The ionicity of Fe{sub 3}O{sub 4} was determined as 0.879 by the density functional theory. Black-Right-Pointing-Pointer The ionicities of spinel ferrites were estimated by a quantum mechanical method. Black-Right-Pointing-Pointer A quantum mechanical method estimating ionicity is suitable for II-VI compounds. Black-Right-Pointing-Pointer The ion distributions of MFe{sub 2}O{sub 4} are calculated by current ionicities values.

  8. The development of low activation ferritic steels for fusion application

    Energy Technology Data Exchange (ETDEWEB)

    Kohyama, A. [Kyoto Univ., Uji (Japan). Inst. of Advanced Energy; Hishinuma, A.; Kohno, Y.; Shiba, K.; Sagara, A.

    1997-03-01

    The development of low-activation ferritic/martensitic steels is a key to the achievement of nuclear fusion as a safe, environmentally attractive and economically competitive energy source. The Japanese and the European Fusion Materials programs have put low-activation ferritic and martensitic steels R and D at the highest priority for a demonstration reactor (DEMO) and the beyond. An international collaborative test program on low-activation ferritic/martensitic steels for fusion is in progress as an activity of the International Energy Agency (IEA) fusion materials working group to verify the feasibility of using ferritic/martensitic steels for fusion by an extensive test program covering the most relevant technical issues for the qualification of a material for a nuclear application. The development of a comprehensive data base on the representative industrially processed reduced-activation steels of type 8-9Cr-2WVTa is underway for providing designers a preliminary set of material data for the mechanical design of components, e.g. for DEMO relevant blanket modules. The current design status of FFHR and SSTR utilizing low-activation ferritic steels is reviewed and future prospects are defined. (author)

  9. The development of ferritic steels for DEMO blanket

    Energy Technology Data Exchange (ETDEWEB)

    Kohyama, A. [Kyoto Univ. (Japan). Inst. of Advanced Energy; Hishinuma, A.; Shiba, K. [Tokai Establishment, JAERI, Tokai, Ibaraki (Japan); Kohno, Y. [Department of Materials Science, University of Tokyo, Hongo, Tokyo 113 (Japan); Sagara, A. [National Institute for Fusion Science, Toki, Gifu (Japan)

    1998-09-01

    The development of low-activation ferritic/martensitic steels is a key to the achievement of nuclear fusion as a safe, environmentally attractive and economically competitive energy source. The Japanese and the European Fusion Materials programs have put low-activation ferritic and martensitic steels R and D at the highest priority for a demonstration reactor (DEMO) and the beyond. An international collaborative test program on low-activation ferritic/martensitic steels for fusion is in progress as an activity of the International Energy Agency (IEA) fusion materials working group to verify the feasibility of using ferritic/martensitic steels for fusion by an extensive test program covering the most relevant technical issues for the qualification of a material for a nuclear application. The development of a comprehensive data base on the representative industrially processed reduced-activation steels of type 8-9Cr-2WVTa is underway for providing designers a preliminary set of material data for the mechanical design of components, e.g. for DEMO relevant blanket modules. The current design status of FFHR and SSTR utilizing low-activation ferritic steels is reviewed and future prospects are defined. (orig.) 12 refs.

  10. Direct formation of ferrite films in wet process

    Science.gov (United States)

    Abe, M.; Tanno, Y.; Tamaura, Y.

    1985-04-01

    We have prepared a polycrystalline Co-ferrite film by the electroless ferrite-plating technique of our invention [J. Appl. Phys. 55, 2614 (1984)] in an aqueous solution at 70 °C on substrates of organic compounds (polyethylene terephthalate, polymethyl methacrylate, polycarbonate, Teflon), a stainless steel, and a polyester fiber. We used no intermediate layer, which we needed previously to enhance the adhesion of the ferrite film to the surface. By exposing the organic substrates to an rf-excited air plasma, the wettability of the surface improved, which enhanced the adhesion of the film to the substrate. Here we have measured the adhesion by a cross-cut test. The plasma forms hydrophilic groups such as -OH and -COOH, which improve the wettability. The OH group adsorbs the metal ions in the reaction solution, initiating the ferrite film formation. The glass shows a strong adhesion to the film even when it is not exposed to the plasma, because the glass has the OH group on the surface inherently. The stainless steel does not enhance the adhesion by the plasma treatment because the plasma forms no OH group on the metal surface. The adhesion power higher than ˜10 kg/cm2 has been obtained between the Co-ferrite film and the glass (not plasma treated), the polyethylene terephthalate (plasma treated) and the Teflon (plasma treated).

  11. Dielectric behaviour of erbium substituted Mn–Zn ferrites

    Indian Academy of Sciences (India)

    D Ravinder; K Vijaya Kumar

    2001-10-01

    Dielectric properties such as dielectric constant (') and dielectric loss tangent (tan ⋹ ) of mixed Mn–Zn–Er ferrites having the compositional formula Mn0.58Zn0.37Fe2.05–ErO4 (where = 0.2, 0.4, 0.6, 0.8 and 1.0) were measured at room temperature in the frequency range 1–13 MHz using a HP 4192A impedance analyser. Plots of dielectric constant (') vs frequency show a normal dielectric behaviour of spinel ferrites. The frequency dependence of dielectric loss tangent (tan ) was found to be abnormal, giving a peak at certain frequency for all mixed Mn–Zn–Er ferrites. A qualitative explanation is given for the composition and frequency dependence of the dielectric constant and dielectric loss tangent. Plots of dielectric constant vs temperature have shown a transition near the Curie temperature for all the samples of Mn–Zn–Er ferrites. However, Mn0.58Zn0.37Er1.0Fe1.05O4 does not show a transition. On the basis of these results an explanation for the dielectric mechanism in Mn–Zn–Er ferrites is suggested.

  12. Ferritic Alloys with Extreme Creep Resistance via Coherent Hierarchical Precipitates

    Science.gov (United States)

    Song, Gian; Sun, Zhiqian; Li, Lin; Xu, Xiandong; Rawlings, Michael; Liebscher, Christian H.; Clausen, Bjørn; Poplawsky, Jonathan; Leonard, Donovan N.; Huang, Shenyan; Teng, Zhenke; Liu, Chain T.; Asta, Mark D.; Gao, Yanfei; Dunand, David C.; Ghosh, Gautam; Chen, Mingwei; Fine, Morris E.; Liaw, Peter K.

    2015-01-01

    There have been numerous efforts to develop creep-resistant materials strengthened by incoherent particles at high temperatures and stresses in response to future energy needs for steam turbines in thermal-power plants. However, the microstructural instability of the incoherent-particle-strengthened ferritic steels limits their application to temperatures below 900 K. Here, we report a novel ferritic alloy with the excellent creep resistance enhanced by coherent hierarchical precipitates, using the integrated experimental (transmission-electron microscopy/scanning-transmission-electron microscopy, in-situ neutron diffraction, and atom-probe tomography) and theoretical (crystal-plasticity finite-element modeling) approaches. This alloy is strengthened by nano-scaled L21-Ni2TiAl (Heusler phase)-based precipitates, which themselves contain coherent nano-scaled B2 zones. These coherent hierarchical precipitates are uniformly distributed within the Fe matrix. Our hierarchical structure material exhibits the superior creep resistance at 973 K in terms of the minimal creep rate, which is four orders of magnitude lower than that of conventional ferritic steels. These results provide a new alloy-design strategy using the novel concept of hierarchical precipitates and the fundamental science for developing creep-resistant ferritic alloys. The present research will broaden the applications of ferritic alloys to higher temperatures. PMID:26548303

  13. Virtual Prototyping and Development of Rotary Field Ferrite Phase Shifter

    Directory of Open Access Journals (Sweden)

    Meenakshi Aggarwal

    2016-03-01

    Full Text Available Review of the virtual prototyping and physical development of the rotary field ferrite phase shifter is presented. A description of the basic principle of operation of the rotary field ferrite phase shifter has been given along with the key aspects about the design and virtual prototyping of various parts of the phase shifter viz ferrite rod, yoke, polarisers and matching section using HFSS and 3-D Maxwell softwares. Calibrated simulation performance of the phase shifters is presented and it shows good agreement with physical measurement results. Three prototypes and one hundred production capable phase shifter modules were fabricated, functionally tested and RF characterised. This is an indigenous development of the physical prototypes of rotary field class of ferrite phase shifters of C-band. This class of ferrite phase shifters finds application in phased array radars, such as battery level radar and weapon locating radar, because of its high phase accuracy and high power handling capability.Defence Science Journal, Vol. 66, No. 2, March 2016, pp. 156-161, DOI: http://dx.doi.org/10.14429/dsj.66.9309

  14. A biosensor system using nickel ferrite nanoparticles

    Science.gov (United States)

    Singh, Prachi; Rathore, Deepshikha

    2016-05-01

    NiFe2O4 ferrite nanoparticles were synthesized by chemical co-precipitation method and the structural characteristics were investigated using X-ray diffraction technique, where single cubic phase formation of nanoparticles was confirmed. The average particle size of NiFe2O4 was found to be 4.9 nm. Nanoscale magnetic materials are an important source of labels for biosensing due to their strong magnetic properties which are not found in biological systems. This property of the material was exploited and the fabrication of the NiFe2O4 nanoparticle based biosensor was done in the form of a capacitor system, with NiFe2O4 as the dielectric material. The biosensor system was tested towards different biological materials with the help of electrochemical workstation and the same was analysed through Cole-Cole plot of NiFe2O4. The performance of the sensor was determined based on its sensitivity, response time and recovery time.

  15. Influence of Substituion on Barium Ferrite Properties

    Directory of Open Access Journals (Sweden)

    Vladimir Jancarik

    2004-01-01

    Full Text Available BaFe12-2x(Ni, ZnxSnxO19 M - type compounds processed by citrate precursor method with substitution level 0.0 ferrite powder specimens were measured. A large change of the coercitity Hc from 330kA/m (x=0.0 to ~70kA/m (x=0.6 was reached as a function of the substitution x. These changes are caused by rearrangement of the Fe3+ ions within the crystalline lattice. Sn4+ ions replace Fe3+ ions on 2b slightly 2a+4f1 sites, while Ni2+ ions occupy 4f2 and 12k sites and Zn2+ ions strongly prefer 4f1 sites.

  16. Magnetocaloric phenomena in Mg-ferrite nanoparticles

    Energy Technology Data Exchange (ETDEWEB)

    Burianova, S; Holec, P; Plocek, J [Charles University, Faculty of Science, Department of Inorganic chemistry, Prague (Czech Republic); Poltierova-Vejpravova, J, E-mail: burianovasimona@email.c, E-mail: jana@mag.mff.cuni.c

    2010-01-01

    A comparative study of magnetocaloric effect (MCE) in superparamagnetic (SPM) regime is reported in two different types of magnesium ferrite nanostructures. The samples were prepared either by microemulsion method as MgFe{sub 2}O{sub 4} nanoparticles encapsulated in amorphous SiO{sub 2}, or as matrix-less nanoparticles using hydrothermal synthesis in supercritical water conditions. The particle diameter in all prepared samples was obtained from XRD measurements and TEM analysis. All samples show a SPM behavior above the blocking temperature, T{sub B}. The entropy change, {Delta}S was finally derived from the measurements of magnetization, M(H,T) curves at defined temperature intervals. We observed, that all samples show a broad peak of {Delta}S in the temperature range that is fairly above the T{sub B}. The values of the {Delta}S also depend on the particle size, and they are of about two orders lower than those reported in the famous giant magnetocaloric materials.

  17. Tuning the magnetism of ferrite nanoparticles

    Science.gov (United States)

    Viñas, S. Liébana; Simeonidis, K.; Li, Z.-A.; Ma, Z.; Myrovali, E.; Makridis, A.; Sakellari, D.; Angelakeris, M.; Wiedwald, U.; Spasova, M.; Farle, M.

    2016-10-01

    The importance of magnetic interactions within an individual nanoparticle or between adjacent ones is crucial not only for the macroscopic collective magnetic behavior but for the AC magnetic heating efficiency as well. On this concept, single-(MFe2O4 where M=Fe, Co, Mn) and core-shell ferrite nanoparticles consisting of a magnetically softer (MnFe2O4) or magnetically harder (CoFe2O4) core and a magnetite (Fe3O4) shell with an overall size in the 10 nm range were synthesized and studied for their magnetic particle hyperthermia efficiency. Magnetic measurements indicate that the coating of the hard magnetic phase (CoFe2O4) by Fe3O4 provides a significant enhancement of hysteresis losses over the corresponding single-phase counterpart response, and thus results in a multiplication of the magnetic hyperthermia efficiency opening a novel pathway for high-performance, magnetic hyperthermia agents. At the same time, the existence of a biocompatible Fe3O4 outer shell, toxicologically renders these systems similar to iron-oxide ones with significantly milder side-effects.

  18. Spinel cobalt ferrite by complexometric synthesis

    Energy Technology Data Exchange (ETDEWEB)

    Thang, Pham D. [Inorganic Materials Science, Faculty of Science and Technology, MESA Institute for Nanotechnology, University of Twente, P.O. Box 217, 7500 AE Enschede (Netherlands)]. E-mail: t.d.pham@tnw.utwente.nl; Rijnders, Guus [Inorganic Materials Science, Faculty of Science and Technology, MESA Institute for Nanotechnology, University of Twente, P.O. Box 217, 7500 AE Enschede (Netherlands); Blank, Dave H.A. [Inorganic Materials Science, Faculty of Science and Technology, MESA Institute for Nanotechnology, University of Twente, P.O. Box 217, 7500 AE Enschede (Netherlands)

    2005-09-15

    Magnetic fine particles of cobalt ferrite (CoFe{sub 2}O{sub 4}) have been synthesized using complexometric method in which ethylene diamine tetra acetic acid C{sub 10}H{sub 16}N{sub 2}O{sub 8} (EDTA) acts as a complexing agent. The crystallographic structure, microstructure and magnetic properties of the synthesized powder were characterized by using X-ray diffraction (XRD), particle size analysis and vibrating sample magnetometry (VSM). The material crystallized in cubic spinel structure with lattice parameter of about 8.38 A. Depending on the calcining temperature, the particle size of the powders varies in the range of hundreds of nanometers to tens of micrometers. A desired relative density above 95% of the theoretical value is obtained for the bulk sample after sintering. The calcined powders and sintered sample exhibit saturation magnetizations around 80 Am{sup 2}/kg which is expected for inverse CoFe{sub 2}O{sub 4}. With increasing calcining temperature the coercivity of these samples decreases. This simple synthesis route leads to a reproducible and stoichiometric material.

  19. Chemical looping coal gasification with calcium ferrite and barium ferrite via solid--solid reactions

    Energy Technology Data Exchange (ETDEWEB)

    Siriwardane, Ranjani [U.S. Department of Energy/NETL; Riley, Jarrett [Oak Ridge Inst. for Science and Education (ORISE), Oak Ridge, TN (United States); Tian, Hanjing [West Virginia Univ., Morgantown, WV (United States); Richards, George [U.S. Department of Energy/NETL

    2016-01-01

    Coal gasification to produce synthesis gas by chemical looping was investigated with two oxygen carriers, barium ferrite (BaFe2O4) and calcium ferrite (CaFe2O4). Thermo-gravimetric analysis (TGA) and fixed-bed flow reactor data indicated that a solid–solid interaction occurred between oxygen carriers and coal to produce synthesis gas. Both thermodynamic analysis and experimental data indicated that BaFe2O4 and CaFe2O4 have high reactivity with coal but have a low reactivity with synthesis gas, which makes them very attractive for the coal gasification process. Adding steam increased the production of hydrogen (H2) and carbon monoxide (CO), but carbon dioxide (CO2) remained low because these oxygen carriers have minimal reactivity with H2 and CO. Therefore, the combined steam–oxygen carrier produced the highest quantity of synthesis gas. It appeared that neither the water–gas shift reaction nor the water splitting reaction promoted additional H2 formation with the oxygen carriers when steam was present. Wyodak coal, which is a sub-bituminous coal, had the best gasification yield with oxygen carrier–steam while Illinois #6 coal had the lowest. The rate of gasification and selectivity for synthesis gas production was significantly higher when these oxygen carriers were present during steam gasification of coal. The rates and synthesis gas yields during the temperature ramps of coal–steam with oxygen carriers were better than with gaseous oxygen.

  20. An analysis of JET fast-wave heating and current drive experiments directly related to ITER

    Energy Technology Data Exchange (ETDEWEB)

    Bhatnagar, V.P.; Eriksson, L.; Gormezano, C.; Jacquinot, J.; Kaye, A.; Start, D.F.H. [Commission of the European Communities, Abingdon (United Kingdom). JET Joint Undertaking

    1994-07-01

    The ITER fast-wave system is required to serve a variety of purposes, in particular, plasma heating to ignition, current profile and burn control and eventually, in conjunction with other schemes, a central non-inductive current drive (CD) for the steady-state operation of ITER. The ICRF heating and current drive data that has been obtained in JET are analyzed in terms of dimensionless parameters, with a view to ascertaining its direct relevance to key ITER requirements. The analysis is then used to identify areas both in physics and technological aspects of ion-cyclotron resonance heating (ICRH) and CD that require further experimentation in ITER-relevant devices such as JET to establish the required data base. (authors). 12 refs., 8 figs.

  1. The nature of temper brittleness of high-chromium ferrite

    Energy Technology Data Exchange (ETDEWEB)

    Sarrak, V.I.; Suvorova, S.O.; Golovin, I.S.; Mishin, V.M.; Kislyuk, I.V. [Central Scientific-Research Institute for Ferrous Metallurgy, Moscow (Russian Federation)

    1995-03-01

    The reasons for development of {open_quotes}475{degrees}C brittleness{close_quotes} of high-chromium ferritic steels are considered from the standpoint of fracture mechanics. It is shown that the general rise in the curve of temperature-dependent local flow stress has the decisive influence on the position of the ductile-to-brittle transformation temperature and the increase in it as the result of a hold at temperatures of development of brittleness. The established effect is related to the change in the parameters determining dislocation mobility, that is, the activation energy of dislocation movement in high-chromium ferrite and the resistance to microplastic deformation, both caused by processes of separation into layers of high-chromium ferrite and decomposition of the interstitial solid solution.

  2. Antimicrobial Lemongrass Essential Oil-Copper Ferrite Cellulose Acetate Nanocapsules.

    Science.gov (United States)

    Liakos, Ioannis L; Abdellatif, Mohamed H; Innocenti, Claudia; Scarpellini, Alice; Carzino, Riccardo; Brunetti, Virgilio; Marras, Sergio; Brescia, Rosaria; Drago, Filippo; Pompa, Pier Paolo

    2016-04-20

    Cellulose acetate (CA) nanoparticles were combined with two antimicrobial agents, namely lemongrass (LG) essential oil and Cu-ferrite nanoparticles. The preparation method of CA nanocapsules (NCs), with the two antimicrobial agents, was based on the nanoprecipitation method using the solvent/anti-solvent technique. Several physical and chemical analyses were performed to characterize the resulting NCs and to study their formation mechanism. The size of the combined antimicrobial NCs was found to be ca. 220 nm. The presence of Cu-ferrites enhanced the attachment of LG essential oil into the CA matrix. The magnetic properties of the combined construct were weak, due to the shielding of Cu-ferrites from the polymeric matrix, making them available for drug delivery applications where spontaneous magnetization effects should be avoided. The antimicrobial properties of the NCs were significantly enhanced with respect to CA/LG only. This work opens novel routes for the development of organic/inorganic nanoparticles with exceptional antimicrobial activities.

  3. Ferrite core non-linearity in coils for magnetic neurostimulation.

    Science.gov (United States)

    RamRakhyani, Anil Kumar; Lazzi, Gianluca

    2014-10-01

    The need to correctly predict the voltage across terminals of mm-sized coils, with ferrite core, to be employed for magnetic stimulation of the peripheral neural system is the motivation for this work. In such applications, which rely on a capacitive discharge on the coil to realise a transient voltage curve of duration and strength suitable for neural stimulation, the correct modelling of the non-linearity of the ferrite core is critical. A demonstration of how a finite-difference model of the considered coils, which include a model of the current-controlled inductance in the coil, can be used to correctly predict the time-domain voltage waveforms across the terminals of a test coil is presented. Five coils of different dimensions, loaded with ferrite cores, have been fabricated and tested: the measured magnitude and width of the induced pulse are within 10% of simulated values.

  4. Impedimetric detection of alcohol vapours using nanostructured zinc ferrite.

    Science.gov (United States)

    Kannan, Padmanathan Karthick; Saraswathi, Ramiah

    2014-11-01

    A comparative study on the sensing characteristics of nanostructured zinc ferrite to three primary alcohols viz. methanol, ethanol and propanol has been carried out. The zinc ferrite has been prepared by a combustion method and characterized by XRD, FTIR, AFM and SEM. Impedance studies in the alcohol concentration range varying from 100 to 1000 ppm show definite variations in response to both the nature of the alcohol and its concentration. The nanostructured zinc ferrite shows the highest sensor response to methanol and least to propanol. Equivalent circuit modelling and calibration have been made for all the three alcohol sensors. The material shows a better selectivity to the alcohols compared to formaldehyde, ammonia and acetone vapours.

  5. Transition metal-substituted cobalt ferrite nanoparticles for biomedical applications.

    Science.gov (United States)

    Sanpo, Noppakun; Berndt, Christopher C; Wen, Cuie; Wang, James

    2013-03-01

    Transition metals of copper, zinc, chromium and nickel were substituted into cobalt ferrite nanoparticles via a sol-gel route using citric acid as a chelating agent. The microstructure and elemental composition were characterized using scanning electron microscopy combined with energy-dispersive X-ray spectroscopy. Phase analysis of transition metal-substituted cobalt ferrite nanoparticles was performed via X-ray diffraction. Surface wettability was measured using the water contact angle technique. The surface roughness of all nanoparticles was measured using profilometry. Moreover, thermogravimetric analysis and differential scanning calorimetry were performed to determine the temperature at which the decomposition and oxidation of the chelating agents took place. Results indicated that the substitution of transition metals influences strongly the microstructure, crystal structure and antibacterial property of the cobalt ferrite nanoparticles.

  6. Abnormal austenite-ferrite transformation behavior in pure iron

    Institute of Scientific and Technical Information of China (English)

    LIU Yongchang; F.Sommer; E.J. Mittemeijer

    2004-01-01

    The austenite → ferrite transformation is the most important reaction route in the manufacture of Fe-based materials. Here the austenite (γ) → ferrite (α)transformation of pure iron was systematically explored by high-resolution dilatometry. Abnormal transformation kinetics, multi-peak discontinuous reaction, was recognized in pure iron according to the variation of the ferrite-formation rate. The occurrence the one or the other type of γ→α trans formation strongly depends on the grain size: the transformation type changes from abnormal to normal (single-peak continuous reaction) with decreasing grain size. The inherent reason for the occurrence of abnormal transformation could be attributed to the repeated nucleation in front of the moving γ/α interface induced by the accumulation of elastic and plastic accommodation energy.

  7. Synthesis and magnetic properties of a novel ferrite organogel

    Science.gov (United States)

    Li, Sichu; John, Vijay T.; Irvin, Glen C.; Rachakonda, Suguna H.; McPherson, Gary L.; O'Connor, Charles J.

    1999-04-01

    A novel magnetic organogel that can be considered a precursor example of a magnetoresponsive gel is reported. The gel is formed by the bridging of ferrite containing anionic bis(2-ethlhexyl) sodium sulfosuccinate reverse micelles with 2,6-dihydroxynaphthalene (2,6-DHN). The addition of 2,6-DHN leads to a room temperature quotes "freezing in" of the liquid solution to a clear organogel. Ferrite particles in the size range 10-15 nm are doped into the gel network and are thus suspended in the optically clear gel media. The magnetic properties of the gel were measured using a superconducting quantum interference device magnetometer. The results reveal that the gel exhibits superparamagnetic behavior with a blocking temperature of 6 K (at an applied field of 1000 G), and a coercivity of 850 G at 2 K. The ferrites introduced into the gel serve the function of magnetic "seeds" via which magnetic properties are acquired by the gel.

  8. Geometry effect on the magnetic properties of manganese zinc ferrite

    Energy Technology Data Exchange (ETDEWEB)

    Landgraf, F.J.G.; Lazaro-Colan, V. [Polytechnic School - EPUSP, Av.Prof. Luciano Gualberto 380, Sao Paulo 05508-900 (Brazil); Leicht, J. [Institute for Technological Research of Sao Paulo, Almeida Prado 532, Sao Paulo 05508-901 (Brazil)], E-mail: leichtj@ipt.br; Janasi, S.R. [Institute for Technological Research of Sao Paulo, Almeida Prado 532, Sao Paulo 05508-901 (Brazil); Lopes, M.F. [IMAG Industria e Comercio de Componentes Eletronicos Ltda, Embaixador 74, Ribeirao Pires 09410-650 (Brazil)

    2008-10-15

    The geometry effect on the bulk magnetic properties of MnZn ferrite toroidal cores produced by the ceramic method was investigated. The MnZn ferrite powder was pressed at two different toroidal sizes and sintered, under controlled atmosphere at different temperatures. The MnZn ferrites cores were characterized according to their magnetic losses, electrical resistivity, initial permeability and Curie temperature. The total loss (200 mT, 100 kHz) in the small cores S (aspect ratio (AR)=2.84) is lower compared with the total loss in the large cores L (AR=0.79). These results show an agreement with the geometry effect observed on electrical steels.

  9. Modeling the Permittivity of Ferrite-Dielectric Composites

    Directory of Open Access Journals (Sweden)

    V.A. Astakhov

    2016-10-01

    Full Text Available The paper presents the model of ferrite-dielectric (ferroelectric composites with semiconductive powder fillers. Such media have the potential for designing systems with controlled frequency dispersion. Experimentally observed significant increase of effective dielectric permittivity in Mn-Zn ferrite composites with the semiconductor pellet is explained on the basis of the capacitance effect. Composites based on Ni-Zn ferrite, which have significantly higher electrical resistance, do not exhibit such phenomena and their behavior is described in the framework of the traditional models of effective medium approximation. There is proposed an analytical solution for the dielectric constant of the composite, based on consideration of the impedances of equivalent circuit involving initial materials (matrix and filler.

  10. Some properties of the circular waveguide with azimuthally magnetized ferrite

    Science.gov (United States)

    Ivanov, Kamen P.; Georgiev, Georgi N.

    1990-05-01

    A comprehensive analysis of normal rotationally symmetric TE modes in a circular waveguide, filled with ferrite, magnetized azimuthally to remanence by a coaxial switching conductor of finite radius, is presented. The characteristic equation of the structure, derived in terms of Kummer and Tricomi confluent hypergeometric functions of complex parameter and variable, is solved numerically, using specially compiled tables of wave functions. Families of theoretically calculated nonreciprocal phase characteristics of the gyrotropic waveguide are shown in normalized form for the two latched states of remanent magnetization, a variety of ferrite parameters, and different values of switching conductor to waveguide radius ratio. The influence of structure geometry and parameters of anisotropic ferrite on normalized differential phase shift and cutoff frequency spectrum of the TE01 mode is discussed.

  11. XANES evidence of arsenate removal from water with magnetic ferrite.

    Science.gov (United States)

    Tu, Yao-Jen; You, Chen-Feng; Chang, Chien-Kuei; Wang, Shan-Li

    2013-05-15

    Arsenic (As) in groundwater and surface water is a worldwide problem possessing a serious threat to public health. In this study, a magnetic ferrite, was synthesized and investigated for its As(V) removal efficiency. The adsorption of As(V) by magnetic ferrite exhibited an L-shaped nonlinear isotherm, suggesting limiting binding sites on the adsorbent surface. The As K-edge X-Ray Absorption Near-Edge Structure (XANES) revealed that the adsorbed As(V) on ferrite was not reduced to more toxic As(III) by Fe(2+) in the ferrite structure. The maximum As adsorption capacity of ferrite was 14 mg/g at pH 3 and decreased with increasing pH due to enhanced electrostatic repulsion between As(V) and the adsorbent surface. Desorption of As(V) using six different acid and salt solutions showed that the desorption rate decreased in an order of H3PO4 > Na3PO4 > H2SO4 > Na2SO4 > HCl > HNO3. These results suggest that magnetic ferrite without surface modification is an effective adsorbent for removing As(V) from water, which was confirmed by the effective removal of As(V) from contaminated groundwater using this material. The used material can then be recovered using a magnet because of its paramagnetism; the adsorbed As(V) on the material can be recovered using H3PO4 or Na3PO4 solutions.

  12. INTRAGRANULAR FERRITE FORMED IN ASSOCIATION WITH INCLUSIONS IN A VANADIUM MICROALLOYED STEEL

    Institute of Scientific and Technical Information of China (English)

    K.M. Wu; M. Enomoto

    2004-01-01

    Intragranular ferrite was formed at inclusions in a vanadium microalloyed steel with excess amount of sulfur. The chemical composition of inclusions in the steel was analyzed by SEM-EDS. The inclusions were mainly composed of MnS and aluminum oxides. The precipitation of MnS at aluminum oxides might result in Mn depletion, which, in turn, promotes the formation of intragranular ferrite. Optical and SEM observations and threedimensional (3D) reconstruction demonstrated that intragranular ferrite was formed at inclusions. The morphology of intragranular ferrite changed with undercooling. At higher temperatures intragranular ferrite was nearly equiaxed whereas it was plate-like or lath-like at lower temperatures.

  13. Cobalt ferrite based magnetostrictive materials for magnetic stress sensor and actuator applications

    Science.gov (United States)

    Jiles, David C. (Inventor); Paulsen, Jason A. (Inventor); Snyder, John E. (Inventor); Lo, Chester C. H. (Inventor); Ring, Andrew P. (Inventor); Bormann, Keith A. (Inventor)

    2008-01-01

    Magnetostrictive material based on cobalt ferrite is described. The cobalt ferrite is substituted with transition metals (such manganese (Mn), chromium (Cr), zinc (Zn) and copper (Cu) or mixtures thereof) by substituting the transition metals for iron or cobalt to form substituted cobalt ferrite that provides mechanical properties that make the substituted cobalt ferrite material effective for use as sensors and actuators. The substitution of transition metals lowers the Curie temperature of the material (as compared to cobalt ferrite) while maintaining a suitable magnetostriction for stress sensing applications.

  14. Electrical and optical properties of gadolinium doped bismuth ferrite nanoparticles

    Energy Technology Data Exchange (ETDEWEB)

    Mukherjee, A., E-mail: soumen.basu@phy.nitdgp.ac.in; Banerjee, M., E-mail: soumen.basu@phy.nitdgp.ac.in; Basu, S., E-mail: soumen.basu@phy.nitdgp.ac.in [Department of Physics, National Institute of Technology, Durgapur-713209 (India); Pal, M. [CSIR-Central Mechanical Engineering Research Institute, Durgapur-713209 (India)

    2014-04-24

    Multiferroic bismuth ferrite (BFO) and gadolinium (Gd) doped bismuth ferrite had been synthesized by a sol-gel method. Particle size had been estimated by Transmission electron microscopy (TEM) and found to decrease with Gd doping. We studied the temperature and frequency dependence of impedance and electric modulus and calculated the grain and grain boundary resistance and capacitance of the investigated samples. We observed that electrical activation energy increases for all the doped samples. Optical band gap also increases for the doped samples which can be used in photocatalytic application of BFO.

  15. Gas atomization of cobalt ferrite-phosphate melts

    Science.gov (United States)

    De Guire, Mark R.; O'Handley, R. C.; Kalonji, G.

    1989-01-01

    XRD, Moessbauer spectroscopy, and EDXS have been used to characterize a rapidly-solidified (Co,Fe)3O4 spinel generated in a cobalt-iron-phosphate glass matrix by gas atomization of melts. Of the two compositions tested, that containing 20 mol pct P2O5 exhibited randomly-oriented ferrite crystallization whose growth appears to have been diffusion-controlled. Unlike the ferrite, in which the iron has both tetrahedral and octahedral coordination, the iron in the glassy matrix was primarily of distorted-octahedral coordination. Calculations indicate that the cooling rates obtained with oxide melts vary strongly with droplet size, but less strongly with melt temperature.

  16. Permanent magnetic ferrite based power-tunable metamaterials

    Science.gov (United States)

    Zhang, Guanqiao; Lan, Chuwen; Gao, Rui; Zhou, Ji

    2017-08-01

    Power-tunable metamaterials based on barium permanent magnetic ferrite have been proposed and fabricated in this research. Scattering parameter measurements confirm a shift in resonant frequency in correlation to changes in incident electromagnetic power within microwave frequency band. The tunable phenomenon represented by a blue-shift in transmission spectra in the metamaterials array can be attributed to a decrease in saturation magnetization resulting from FMR-induced temperature elevation upon resonant conditions. This power-dependent behavior offers a simple and practical route towards dynamically fine-tunable ferrite metamaterials.

  17. Magnetodielectric effect of Mn-Zn ferrite at resonant frequency

    Science.gov (United States)

    Pengfei, Pan; Ning, Zhang

    2016-10-01

    The dielectric properties and the magnetodielectric effect in Mn-Zn ferrite at resonant frequency have been studied in this paper. Dimensional-resonance-induced abnormal dielectric spectrum was observed at f≈1 MHz. The relatively large magnetodielectric ratio of 4500% in a magnetic field of 3.5 kOe was achieved from the Mn-Zn ferrite sample with the initial permeability of 15 K at resonant frequency at room temperature. Theoretical analysis suggests that the large MD effect at resonant frequency is attributed to the enhanced magnetostriction effect.

  18. Cobalt Ferrite Nanocrystallites for Sustainable Hydrogen Production Application

    Directory of Open Access Journals (Sweden)

    Rajendra S. Gaikwad

    2011-01-01

    Full Text Available Cobalt ferrite, CoFe2O4, nanocrystalline films were deposited using electrostatic spray method and explored in sustainable hydrogen production application. Reflection planes in X-ray diffraction pattern confirm CoFe2O4 phase. The surface scanning microscopy photoimages reveal an agglomeration of closely-packed CoFe2O4 nanoflakes. Concentrated solar-panel, a two-step water splitting process, measurement technique was preferred for measuring the hydrogen generation rate. For about 5 hr sustainable, 440 mL/hr, hydrogen production activity was achieved, confirming the efficient use of cobalt ferrite nanocrystallites film in hydrogen production application.

  19. Gas atomization of cobalt ferrite-phosphate melts

    Science.gov (United States)

    De Guire, Mark R.; O'Handley, R. C.; Kalonji, G.

    1989-01-01

    XRD, Moessbauer spectroscopy, and EDXS have been used to characterize a rapidly-solidified (Co,Fe)3O4 spinel generated in a cobalt-iron-phosphate glass matrix by gas atomization of melts. Of the two compositions tested, that containing 20 mol pct P2O5 exhibited randomly-oriented ferrite crystallization whose growth appears to have been diffusion-controlled. Unlike the ferrite, in which the iron has both tetrahedral and octahedral coordination, the iron in the glassy matrix was primarily of distorted-octahedral coordination. Calculations indicate that the cooling rates obtained with oxide melts vary strongly with droplet size, but less strongly with melt temperature.

  20. Enhanced durability and reactivity for zinc ferrite desulfurization sorbent

    Energy Technology Data Exchange (ETDEWEB)

    Jha, M.C.; Berggren, M.H.

    1988-11-14

    AMAX Research Development Center (AMAX R D) has been investigating methods for enhancing the reactivity and durability of the zinc ferrite desulfurization sorbent. Zinc ferrite sorbents are intended for use in desulfurization of hot coal gas in integrated gasification combined cycle (IGCC) or molten carbonate fuel cell (MCFC) applications. For the present program, the reactivity of the sorbent may be defined as its sulfur sorption capacity at the breakthrough point and at saturation in a bench-scale, fixed-bed reactor. Durability may be defined as the ability of the sorbent to maintain important physical characteristics such As size, strength, and specific surface area during 10 cycles of sulfidation and oxidation.

  1. Preparation of Rare-Earth Composite Ferrite Magnetic Fluid

    Institute of Scientific and Technical Information of China (English)

    蒋荣立; 刘永超; 刘守坤; 鞠明礼

    2004-01-01

    Water-based rare-earth ferrite (RexFe3-xO4)magnetic fluids were prepared by chemical co-precipitation method. The result shows that saturation magnetic intensity of ferrite magnetic fluids can be improved by adding Dy3+ and the saturation magnetic intensity will reach the highest if n(Fe)∶n(Dy3+)=30∶1. The modification and formation mechanism of RexFe3-xO4 particles is discussed in detail. The physicochemical properties are investigated by the Gouy magnetic balance, IR, TEM, XRD, and EDX, etc.

  2. Superparamagnetic response of zinc ferrite incrusted nanoparticles

    Energy Technology Data Exchange (ETDEWEB)

    Lopez-Maldonado, K.L., E-mail: liliana.lopez.maldonado@gmail.com [Instituto de Ingeniería y Tecnología, Universidad Autónoma de Ciudad Juárez, Av. Del Charro 450 norte, 32310 Ciudad Juárez (Mexico); Presa, P. de la, E-mail: pmpresa@ucm.es [Instituto de Magnetismo Aplicado (UCM-ADIF-CSIC), PO Box 155, 28230 Las Rozas (Spain); Dpto. Física de Materiales, Univ. Complutense de Madrid, Madrid (Spain); Betancourt, I., E-mail: israelb@unam.mx [Departamento de Materiales Metálicos y Cerámicos, Instituto de Investigaciones en Materiales, Universidad Nacional Autónoma de México, México, D.F. 04510 (Mexico); Farias Mancilla, J.R., E-mail: rurik.farias@uacj.mx [Instituto de Ingeniería y Tecnología, Universidad Autónoma de Ciudad Juárez, Av. Del Charro 450 norte, 32310 Ciudad Juárez (Mexico); Matutes Aquino, J.A., E-mail: jose.matutes@cimav.edu.mx [Centro de Investigación en Materiales Avanzados, Miguel de Cervantes 120, 31109 Chihuahua (Mexico); Hernando, A., E-mail: antonio.hernando@externos.adif.es [Instituto de Magnetismo Aplicado (UCM-ADIF-CSIC), PO Box 155, 28230 Las Rozas (Spain); Dpto. Física de Materiales, Univ. Complutense de Madrid, Madrid (Spain); and others

    2015-07-15

    Highlights: • Incrusted nanoparticles are found at the surface of ZnFe{sub 2}O{sub 4} microparticles. • Magnetic contribution of nano and microparticles are analyzed by different models. • Langevin model is used to calculate the nanoparticles-superparamagnetic diameter. • Susceptibility and Langevin analysis and calculations agree with experimental data. - Abstract: Zinc ferrite is synthesized via mechano-activation, followed by thermal treatment. Spinel ZnFe{sub 2}O{sub 4} single phase is confirmed by X-ray diffraction. SEM micrographs show large particles with average particle size 〈D{sub part}〉 = 1 μm, with particles in intimate contact. However, TEM micrographs show incrusted nanocrystallites at the particles surface, with average nanocrystallite size calculated as 〈D{sub inc}〉 ≈ 5 nm. The blocking temperature at 118 K in the ZFC–FC curves indicates the presence of a superparamagnetic response which is attributable to the incrusted nanocrystallites. Moreover, the hysteresis loops show the coexistence of superpara- and paramagnetic responses. The former is observable at the low field region; meanwhile, the second one is responsible of the lack of saturation at high field region. This last behavior is related to a paramagnetic contribution coming from well-ordered crystalline microdomains. The hysteresis loops are analyzed by means of two different models. The first one is the susceptibility model used to examine separately the para- and superparamagnetic contributions. The fittings with the theoretical model confirm the presence of the above mentioned magnetic contributions. Finally, using the Langevin-based model, the average superparamagnetic diameter 〈D{sub SPM}〉 is calculated. The obtained value 〈D{sub SPM}〉 = 4.7 nm (∼5 nm) is consistent with the average nanocrystallite size observed by TEM.

  3. Recent advances in nanosized Mn-Zn ferrite magnetic fluid hyperthermia for cancer treatment.

    Science.gov (United States)

    Lin, Mei; Huang, Junxing; Sha, Min

    2014-01-01

    This paper reviews the recent research and development of nanosized manganese zinc (Mn-Zn) ferrite magnetic fluid hyperthermia (MFH) for cancer treatment. Mn-Zn ferrite MFH, which has a targeted positioning function that only the temperature of tumor tissue with magnetic nanoparticles can rise, while normal tissue without magnetic nanoparticles is not subject to thermal damage, is a promising therapy for cancer. We introduce briefly the composition and properties of magnetic fluid, the concept of MFH, and features of Mn-Zn ferrite magnetic nanoparticles for MFH such as thermal bystander effect, universality, high specific absorption rate, the targeting effect of small size, uniformity of hyperthermia temperature, and automatic temperature control and constant temperature effect. Next, preparation methods of Mn-Zn ferrite magnetic fluid are discussed, and biocompatibility and biosecurity of Mn-Zn ferrite magnetic fluid are analyzed. Then the applications of nanosized Mn-Zn ferrite MFH in cancer are highlighted, including nanosized Mn-Zn ferrite MFH alone, nanosized Mn-Zn ferrite MFH combined with As2O3 chemotherapy, and nanosized Mn-Zn ferrite MFH combined with radiotherapy. Finally, the combination application of nanosized Mn-Zn ferrite MFH and gene-therapy is conceived, and the challenges and perspectives for the future of nanosized Mn-Zn ferrite MFH for oncotherapy are discussed.

  4. Comparison of Ferrite Refinement Mechanisms by Different Processing Schedules in 08 and 20Mn Steels

    Institute of Scientific and Technical Information of China (English)

    2001-01-01

    The influence of deforming temperature on ferrite refinement was analyzed by comparing the microstructures obtained by deformation at above Ar3, in two-phase region of (+) and at below A1 in clean 08 and 20Mn steels. The results indicate that ferrite refinement through strain induced transformation by deformation at above Ar3 is more effe ctive than that by deformation simply through ferrite dynamic recrysta llization. The main problem of ferrite refinement by deformation at be low Ar3 is the inhomogeneity of microstructure which is controlled by the orientations and sizes of ferrite grains and the distribution of s econd phases. Ferrite dynamic recrystallization after strain induced t ransformation can further effectively refine ferrite.

  5. Design Guidelines for Ferrite Absorbers Submitted to RF-induced Heating

    CERN Document Server

    Bertarelli, A

    2013-01-01

    The use of ferrite absorbers is one of the most effective means of damping potentially harmful high order RF modes, which may lead to beam instabilities and excessive power losses in accelerator devices. However, the power deposited on ferrite absorbers themselves maylead to ferrite exceeding its Curie temperature, losing its damping properties. An evaluation of the ferrite capability to dissipate deposited heat is hence of paramount importance for the safe design of particle accelerator devices. In this paper, figures of merit are proposed to assess the maximum specific power allowed on a generic ferrite tile, before it reaches its Curie temperature. Due to its inherent brittleness, sufficient contact pressure between ferrite and its housing, allowing heat transmission by conduction, can hardly be applied. A semi-analytical study is thus performed, assuming that ferrite is evacuating heat solely through radiation. The described method is then exemplified in the case of the BPM-embedded tertiary collimator (T...

  6. Barium Ferrite Films Grown By Pulsed Laser Ablation

    NARCIS (Netherlands)

    Lisfi, A.; Lodder, J.C.; Haan, de P.; Roesthuis, F.J.G.

    1998-01-01

    Abstract available only. It is known that barium ferrite (BaFe12019) can grow with perpendicular anisotropy on A1203 a single crystal substrate,' but also on an amorphous substrate by using a ZnO buffer.2 Because of its large magnetic anisotropy which can easily overcome the shape anisotropy of the

  7. Millimetre-wave isolator based on Al substituted Ba ferrite

    Science.gov (United States)

    Ustinov, A. B.; Vinnik, D. A.; Belyavskii, P. Yu; Gudkova, S. A.; Zakharchuk, I.; Lähderanta, E.

    2016-11-01

    A mm-wave isolator is fabricated and studied. The operating frequency of the devices is 78.5 GHz. A bandwidth at the level of -3 dB equals 1.6 GHz. The device used a flux grown single-crystal aluminum substituted barium ferrite.

  8. Study of DNA interaction with cobalt ferrite nanoparticles.

    Science.gov (United States)

    Pershina, A G; Sazonov, A E; Novikov, D V; Knyazev, A S; Izaak, T I; Itin, V I; Naiden, E P; Magaeva, A A; Terechova, O G

    2011-03-01

    Interaction of cobalt ferrite nanopowder and nucleic acid was investigated. Superparamagnetic cobalt ferrite nanoparticles (6-12 nm) were prepared by mechanochemical synthesis. Structure of the nanopowder was characterized using X-ray diffraction. It was shown that cobalt ferrite nanoparticles were associated with ssDNA and dsDNA in Tris-buffer resulting in bionanocomposite formation with mass weight relation nanoparticles: DNA 1:(0.083 +/- 0.003) and 1:(0.075 +/- 0.003) respectively. The mechanism of interaction between a DNA and cobalt ferrite nanoparticles was considered basing on the whole set of obtained data: FTIR-spectroscopy, analyzing desorption of DNA from the surface of the particles while changing the chemical content of the medium, and on the modeling interaction of specific biomolecule fragments with surface of a inorganic material. It was supposed that the linkage was based on coordination interaction of the phosphate groups and oxygen atoms heterocyclic bases of DNA with metal ions on the particle surface. These data can be used to design specific magnetic DNA-nanoparticles hybrid structures.

  9. A novel high power X-band ferrite phase shifter.

    Science.gov (United States)

    Deng, G J; Huang, W H; Li, J W; Ba, T; Guo, L T; Jiang, Y

    2017-01-01

    A novel high power X-band ferrite phase shifter (PS) employing the structure of several waveguides connected in parallel is proposed. Each of the waveguides is a phase shift unit utilizing a dual-toroid structure. First, the phase shift unit is designed, manufactured, and tested. The results indicate that the power capacity reaches 115 kW. At this power, the maximum magnetic field strength of ferrite is 7.9 kA/m, beyond which the nonlinear effect of ferrite will occur. On this basis, the PS that consists of four units connected in parallel is designed. According to the threshold of ferrite, the power capacity of the PS can theoretically reach 430 kW. Limited by the maximum output power of the microwave source, the preliminary high-power test results demonstrate that the PS can operate properly at 270 kW. The PS exhibits an insertion loss of 0.82 dB and a maximum differential phase shift of approximately 300° at 9.3 GHz. The return loss of the PS is more than 16 dB from 9.0 to 9.5 GHz.

  10. The structural and magnetic properties of dual phase cobalt ferrite.

    Science.gov (United States)

    Gore, Shyam K; Jadhav, Santosh S; Jadhav, Vijaykumar V; Patange, S M; Naushad, Mu; Mane, Rajaram S; Kim, Kwang Ho

    2017-05-31

    The bismuth (Bi(3+))-doped cobalt ferrite nanostructures with dual phase, i.e. cubic spinel with space group Fd3m and perovskite with space group R3c, have been successfully engineered via self-ignited sol-gel combustion route. To obtain information about the phase analysis and structural parameters, like lattice constant, Rietveld refinement process is applied. The replacement of divalent Co(2+) by trivalent Bi(3+) cations have been confirmed from energy dispersive analysis of the ferrite samples. The micro-structural evolution of cobalt ferrite powders at room temperature under various Bi(3+) doping levels have been identified from the digital photoimages recorded using scanning electron microscopy. The hyperfine interactions, like isomer shift, quadrupole splitting and magnetic hyperfine fields, and cation distribution are confirmed from the Mossbauer spectra. Saturation magnetization is increased with Bi(3+)-addition up to x = 0.15 and then is decreased when x = 0.2. The coercivity is increased from 1457 to 2277 G with increasing Bi(3+)-doping level. The saturation magnetization, coercivity and remanent ratio for x = 0.15 sample is found to be the highest, indicating the potential of Bi(3+)-doping in enhancing the magnetic properties of cobalt ferrite.

  11. High coercivity in nanostructured Co-ferrite thin films

    Indian Academy of Sciences (India)

    J H Yin; B H Liu; J Ding; Y C Wang

    2006-11-01

    Three methods including sol–gel, rf sputtering and pulsed laser deposition (PLD) have been used for the fabrication of high coercivity Co-ferrite thin films with a nanocrystalline structure. The PLD method is demonstrated to be a possible tool to achieve Co-ferrite films with high coercivity and small grain size at low deposition temperature. High coercivity, over 10 kOe, has been successfully achieved in Co-ferrite films with a thickness of ∼ 100 nm deposited using PLD with a substrate temperature at 550°C. The Co-ferrite films prepared by PLD at over 300°C on different substrates including amorphous glass, quartz and silicon exhibits an obvious (111) textured structure and possesses perpendicular anisotropy. Our study has also shown that the high coercivity is related with a large residual strain, which may induce an additional magnetic anisotropy (stress anisotropy) and at the same time serve as pinning centres, which can restrict the domain wall movement and therefore, increase the coercivity.

  12. Electromagnetic properties of manganese-zinc ferrite with lithium substitution

    Energy Technology Data Exchange (ETDEWEB)

    De Fazio, E. [LAFMACEL, Facultad de Ingenieria, Universidad de Buenos Aires, Paseo Colon 850 (1063), Buenos Aires (Argentina); Bercoff, P.G., E-mail: bercoff@famaf.unc.edu.ar [FAMAF, Universidad Nacional de Cordoba, IFEG-Conicet, Ciudad Universitaria, 5000 Cordoba (Argentina); Jacobo, S.E. [LAFMACEL, Facultad de Ingenieria, Universidad de Buenos Aires, Paseo Colon 850 (1063), Buenos Aires (Argentina)

    2011-11-15

    Polycrystalline manganese-zinc ferrite with lithium substitution of composition Li{sub 0.5x}Mn{sub 0.4}Zn{sub 0.6-x}Fe{sub 2+0.5x}O{sub 4} (0.0{<=}x{<=}0.4) was prepared by the usual ceramic method. X-ray diffraction analysis confirmed that the samples have a spinel structure and are of single phase for some values of Li content. Lithium doping considerably modifies saturation magnetization since its value increases from 57.5 emu/g for x=0.0 to 82.9 emu/g for x=0.4. Lithium inclusion increases the real permeability (over 1 MHz) while the natural resonance frequency shifts to lower values as the fraction of Li increases. These ferrites show good electromagnetic properties as absorbers in the microwave range of 1 MHz - 1 GHz. - Highlights: > Li-doped manganese-zinc ferrites were successfully prepared by the usual ceramic method. > Lithium doping enhances saturation magnetization and increases real permeability (over 1 MHz). > Natural resonance frequency shifts to lower values as fraction of Li increases. > These ferrites show good electromagnetic properties as absorbers in the microwave range of 1 MHz-1 GHz.

  13. Magnetoelastic coupling in epitaxial cobalt ferrite/barium titanate heterostructures

    Energy Technology Data Exchange (ETDEWEB)

    Gräfe, Joachim; Welke, Martin [Wilhelm-Ostwald-Institut für Physikalische und Theoretische Chemie, Universität Leipzig, Linnéstraße 2, 04103 Leipzig (Germany); Bern, Francis; Ziese, Michael [Institut für Experimentelle Physik II, Universität Leipzig, Linnéstraße 5, 04103 Leipzig (Germany); Denecke, Reinhard, E-mail: denecke@uni-leipzig.de [Wilhelm-Ostwald-Institut für Physikalische und Theoretische Chemie, Universität Leipzig, Linnéstraße 2, 04103 Leipzig (Germany)

    2013-08-15

    Ultra-thin cobalt ferrite films have been synthesised on ferroelectric barium titanate crystals. The cobalt ferrite films exhibit a magnetic response to strain induced by structural changes in the barium titanate substrate, suggesting a pathway to multiferroic coupling. These structural changes are achieved by heating through the phase transition temperatures of barium titanate. In addition the ferromagnetic signal of the substrate itself is taken into account, addressing the influence of impurities or defects in the substrate. The cobalt ferrite/barium titanate heterostructure is a suitable oxidic platform for future magnetoelectric applications with an established ferroelectric substrate and widely tuneable magnetic properties by changing the transition metal in the ferrite film. - Highlights: ► Ultra-thin CoFe{sub 2}O{sub 4} films grown on ferroelectric BaTiO{sub 3} crystals by PLD. ► Magnetic response to structural changes of BaTiO{sub 3} at transition temperatures. ► Significant magneto-elastic coupling of in-plane magnetisation in SQUID experiments. ► Clear distinction between contribution by BaTiO{sub 3} substrate and by CoFe{sub 2}O{sub 4} film.

  14. Structural and magnetic properties of ball milled copper ferrite

    DEFF Research Database (Denmark)

    Goya, G.F.; Rechenberg, H.R.; Jiang, Jianzhong

    1998-01-01

    The structural and magnetic evolution in copper ferrite (CuFe2O4) caused by high-energy ball milling are investigated by x-ray diffraction, Mössbauer spectroscopy, and magnetization measurements. Initially, the milling process reduces the average grain size of CuFe2O4 to about 6 nm and induces ca...

  15. Magnetoabsorption and magnetic hysteresis in Ni ferrite nanoparticles

    Directory of Open Access Journals (Sweden)

    Torres C.

    2013-01-01

    Full Text Available Nickel ferrite nanoparticles were prepared by a modified sol-gel technique employing coconut oil, and then annealed at different temperatures in 400-1200 °C range. This route of preparation has revealed to be one efficient and cheap technique to obtain high quality nickel ferrite nanosized powder. Sample particles sizes obtained with XRD data and Scherrer’s formula lie in 13 nm to 138 nm, with increased size with annealing temperature. Hysteresis loops have been obtained at room temperature with an inductive method. Magnetic field induced microwave absorption in nanoscale ferrites is a recent an active area of research, in order to characterize and explore potential novel applications. In the present work microwave magnetoabsorption data of the annealed nickel ferrite nanoparticles are presented. These data have been obtained with a system based on a network analyzer that operates in the frequency range 0 - 8.5 GHz. At fields up to 400 mT we can observe a peak according to ferromagnetic resonance theory. Sample annealed at higher temperature exhibits different absorption, coercivity and saturation magnetization figures, revealing its multidomain character.

  16. Bismuth Ferrite for Active Control of Surface Plasmon Polariton Modes

    DEFF Research Database (Denmark)

    Babicheva, Viktoriia; Zhukovsky, Sergei; Lavrinenko, Andrei

    2014-01-01

    We propose and investigate several layouts of m etal-insulator-metal waveguide with active core which can be utilized for dynamic switching in photonic integrated circuits. The active material, bismuth ferrite (BiFeO3), is sandwiched between metal plates and changes i ts refractive index through ...

  17. Tailoring the magnetic properties of cobalt-ferrite nanoclusters

    Energy Technology Data Exchange (ETDEWEB)

    Vega, A. Estrada de la; Garza-Navarro, M. A., E-mail: marco.garzanr@uanl.edu.mx; Durán-Guerrero, J. G.; Moreno Cortez, I. E.; Lucio-Porto, R.; González-González, V. [Universidad Autónoma de Nuevo León, Facultad de Ingeniería Mecánica y Eléctrica (Mexico)

    2016-01-15

    In this contribution, we report on the tuning of magnetic properties of cobalt-ferrite nanoclusters. The cobalt-ferrite nanoclusters were synthesized from a two-step approach that consists of the synthesis of cobalt-ferrite nanoparticles in organic media, followed by their dispersion into aqueous dissolution to form an oil-in-water emulsion. These emulsions were prepared at three different concentrations of the cationic surfactant cetyltrimethylammonium bromide (CTAB), in order to control the size and clustering density of the nanoparticles in the nanoclusters. The synthesized samples were characterized by transmission electron microscopy and their related techniques, such as bright-field and Z-contrast imaging, electron diffraction and energy-dispersive X-ray spectrometry; as well as static magnetic measures. The experimental evidence indicates that the size, morphology, and nanoparticles clustering density in the nanoclusters is highly dependent of the cobalt-ferrite:CTAB molar ratio that is used in their synthesis. In addition, due to the clustering of the nanoparticles into the nanoclusters, their magnetic moments are blocked to relax cooperatively. Hence, the magnetic response of the nanoclusters can be tailored by controlling the size and nanoparticles clustering density.

  18. Deuterium Retention and Physical Sputtering of Low Activation Ferritic Steel

    Institute of Scientific and Technical Information of China (English)

    T. Hino; K. Yamaguchi; Y. Yamauchi; Y. Hirohata; K. Tsuzuki; Y.Kusama

    2005-01-01

    Low activation materials have to be developed toward fusion demonstration reactors. Ferritic steel, vanadium alloy and SiC/SiC composite are candidate materials of the first wall,vacuum vessel and blanket components, respectively. Although changes of mechanical-thermal properties owing to neutron irradiation have been investigated so far, there is little data for the plasma material interactions, such as fuel hydrogen retention and erosion. In the present study,deuterium retention and physical sputtering of low activation ferritic steel, F82H, were investigated by using deuterium ion irradiation apparatus.After a ferritic steel sample was irradiated by 1.7 kev D+ ions, the weight loss was measured to obtain the physical sputtering yield. The sputtering yield was 0.04, comparable to that of stainless steel. In order to obtain the retained amount of deuterium, technique of thermal desorption spectroscopy (TDS) was employed to the irradiated sample. The retained deuterium desorbed at temperature ranging from 450 K to 700 K, in the forms of DHO, D2, D2O and hydrocarbons. Hence, the deuterium retained can be reduced by baking with a relatively low temperature. The fluence dependence of retained amount of deuterium was measured by changing the ion fluence. In the ferritic steel without mechanical polish, the retained amount was large even when the fluence was low. In such a case, a large amount of deuterium was trapped in the surface oxide layer containing O and C. When the fluence was large, the thickness of surface oxide layer was reduced by the ion sputtering, and then the retained amount in the oxide layer decreased. In the case of a high fluence, the retained amount of deuterium became comparable to that of ferritic steel with mechanical polish or SS 316 L, and one order of magnitude smaller than that of graphite. When the ferritic steel is used, it is required to remove the surface oxide layer for reduction of fuel hydrogen retention.Ferritic steel sample was

  19. RF design and tests on a broadband, high-power coaxial quadrature hybrid applicable to ITER ICRF transmission line system for load-resilient operations

    Energy Technology Data Exchange (ETDEWEB)

    Kim, Hae Jin, E-mail: haejin@nfri.re.kr [National Fusion Research Institute, Daejeon (Korea, Republic of); Wang, Son Jong; Park, Byoung Ho; Kwak, Jong-Gu [National Fusion Research Institute, Daejeon (Korea, Republic of); Hillairet, Julien [CEA/IRFM, Saint-lez-Durance (France); Choi, Jin Joo [Kwangwoon University, Seoul (Korea, Republic of)

    2015-10-15

    Highlights: • Amplitude balanced 3 dB coaxial hybrid splitter has been designed and rf tested. • The proposed hybrid is applicable to ITER ICRF transmission line for load resilience. • Two-section, broadband coaxial hybrid can be tunable by changing dielectric insulator. - Abstract: RF design and network analyzer tests of broadband, amplitude-balanced coaxial hybrid junctions are presented. We have designed two 3 dB hybrid splitters with 9 and 12 in. coaxial transmission lines applicable to ITER ICRF for load-resilient operations using ANSYS HFSS. Amplitude-balanced broadband responses were obtained with the combination of impedance reductions of longitudinal and transverse branches in unequal proportion, length change of 50 Ω lines and diameter change of high impedance lines connected transversely to the T-section of the hybrid splitter, respectively. We have fabricated and RF tested the 9 in. coaxial hybrid coupler. We obtained an excellent coupling flatness of −3.2 ± 0.2 dB, phase difference of 4 degrees and return loss of 16 dB in 40–55 MHz. The measured data of 9 in. hybrid splitter is highly consistent with HFSS simulations. We found that the proposed 3 dB hybrid splitter can be tunable with amplitude-balanced, broadband response by changing dielectric insulators to keep the inner and outer conductors of coaxial line apart. The proposed 3 dB hybrid splitter can be utilized for load-resilient operations in a wide range of antenna load variations due to mode transitions or edge localized modes (ELMs) in fusion plasmas.

  20. Development of an extensive database of mechanical properties for Reduced Activation Ferritic/Martensitic Steels

    Energy Technology Data Exchange (ETDEWEB)

    Tanigawa, H.; Shiba, K.; Ando, M.; Wakai, E.; Jitsukawa, S. [Japan Atomic Energy Agency, Tokai-mura, Naga-gun, Ibaraki-ken (Japan); Hirose, T. [Blanket Engineering Group, Japan Atomic Energy Agency, Naka, Ibaraki (Japan); Kasada, R.; Kimura, A.; Kohyama, A. [Kyoto Univ., lnstitute of Advanced Energy (Japan); Kohno, Y. [Muroran Institute of Technology, Muroran, Hokkaido (Japan); Klueh, R.L. [0ak Ridge Noational Laboratory, TN (United States); Sokolov, M.; Stoller, R.; Zinklek, S. [0ak Ridge Noational Laboratory, Materials Science and Technology Div., TN (United States); Yamamoto, T.; Odette, G. [UCSB, Dept. of Chemical Engineering UCSB, Santa-Barbara (United States); Kurtz, R.J. [Pacifie Northwest National Laboratory, Richland WA (United States)

    2007-07-01

    Full text of publication follows: Reduced activation ferritic/martensitic steels (RAFMs) are recognized as the primary candidate structural materials for fusion blanket systems, as they have been developed based on massive industrial experience of ferritic/martensitic steel replacing Mo and Nb of high chromium heat resistant martensitic steels (such as modified 9Cr-1Mo) with W and Ta, respectively. F82H (8Cr-2W-0.2V-0.04Ta-0.1C) and JLF-1 (9Cr-2W-0.2V-0.08Ta-0.1C) are RAFMs, which have been developed and studied in Japan and the various effects of irradiation were reported. F82H is designed with emphasis on high temperature property and weldablility, and was provided and evaluated in various countries as a part of the IEA fusion materials development collaboration. The Japan/US collaboration program also has been conducted with the emphasis on heavy irradiation effects of F82H, JLF-1 and ORNL9Cr2WVTa over the past two decades using Fast Flux Testing Facility (FFTF) of PNNL and High Flux Isotope Reactor (HFIR) of ORNL, and the irradiation condition of the irradiation capsules of those reactors were precisely controlled by the well matured capsule designing and instrumentation. Now, among the existing database for RAFMs the most extensive one is that for F82H. The objective of this paper is to review the database status of RAFMs, mainly on F82H, to identify the key issues for the future development of database. Tensile, fracture toughness, creep and fatigue properties and microstructural studies before and after irradiation are summarized. (authors)

  1. Effect of rare earth substitution in cobalt ferrite bulk materials

    Energy Technology Data Exchange (ETDEWEB)

    Bulai, G., E-mail: georgiana.bulai@uaic.ro [Faculty of Physics, Alexandru Ioan Cuza University of Iasi, Bd. Carol I, nr. 11, 700506 Iasi (Romania); Diamandescu, L. [National Institute of Material Physics, P.O. Box MG-7, 07125 Bucharest (Romania); Dumitru, I.; Gurlui, S. [Faculty of Physics, Alexandru Ioan Cuza University of Iasi, Bd. Carol I, nr. 11, 700506 Iasi (Romania); Feder, M. [National Institute of Material Physics, P.O. Box MG-7, 07125 Bucharest (Romania); Caltun, O.F. [Faculty of Physics, Alexandru Ioan Cuza University of Iasi, Bd. Carol I, nr. 11, 700506 Iasi (Romania)

    2015-09-15

    The study was focused on the influence of small amounts of rare earth (RE=La, Ce, Sm, Gd, Dy, Ho, Er, Yb) addition on the microstructure, phase content and magnetic properties of cobalt ferrite bulk materials. The X-Ray diffraction measurements confirmed the formation of the spinel structure but also the presence of secondary phases of RE oxides or orthoferrite in small percentages (up to 3%). Density measurements obtained by Archimedes method revealed a ~1 g cm{sup −3} decrease for the RE doped cobalt ferrite samples compared with stoichiometric one. Both the Mössbauer and Fourier Transform Infrared Spectrocopy analysis results confirmed the formation of the spinel phase. The saturation magnetization and coercive field values of the doped samples obtained by Vibrating Sample Magnetometry were close to those of the pure cobalt ferrite. For magnetostrictive property studies the samples were analyzed using the strain gauge method. Higher maximum magnetostriction coefficients were found for the Ho, Ce, Sm and Yb doped cobalt ferrite bulk materials as related to the stoichiometric CoFe{sub 2}O{sub 4} sample. Moreover, improved strain derivative was observed for these samples but at higher magnetic fields due to the low increase of the coercive field values for doped samples. - Highlights: • Substitution by a large number of rare earth elements was investigated. • First reported results on magnetostriction measurements of RE doped cobalt ferrite. • The doped samples presented an increased porosity and a decreased grain size. • Increased magnetostrctive response was observed for several doped samples.

  2. Dependence of microwave absorption properties on ferrite volume fraction in MnZn ferrite/rubber radar absorbing materials

    Energy Technology Data Exchange (ETDEWEB)

    Gama, Adriana M., E-mail: adrianaamg@iae.cta.br [Divisao de Materiais (AMR), Instituto de Aeronautica e Espaco (IAE), Departamento de Ciencia e Tecnologia Aeroespacial - DCTA (Brazil); Rezende, Mirabel C., E-mail: mirabelmcr@iae.cta.br [Divisao de Materiais (AMR), Instituto de Aeronautica e Espaco (IAE), Departamento de Ciencia e Tecnologia Aeroespacial - DCTA (Brazil); Dantas, Christine C., E-mail: christineccd@iae.cta.br [Divisao de Materiais (AMR), Instituto de Aeronautica e Espaco (IAE), Departamento de Ciencia e Tecnologia Aeroespacial - DCTA (Brazil)

    2011-11-15

    We report the analysis of measurements of the complex magnetic permeability ({mu}{sub r}) and dielectric permittivity ({epsilon}{sub r}) spectra of a rubber radar absorbing material (RAM) with various MnZn ferrite volume fractions. The transmission/reflection measurements were carried out in a vector network analyzer. Optimum conditions for the maximum microwave absorption were determined by substituting the complex permeability and permittivity in the impedance matching equation. Both the MnZn ferrite content and the RAM thickness effects on the microwave absorption properties, in the frequency range of 2-18 GHz, were evaluated. The results show that the complex permeability and permittivity spectra of the RAM increase directly with the ferrite volume fraction. Reflection loss calculations by the impedance matching degree (reflection coefficient) show the dependence of this parameter on both thickness and composition of RAM. - Highlights: > Permeability and permittivity spectra of a MnZn ferrite RAM (2-18 GHz) are given. > Higher MnZn volume fraction favors increase of RAM/'s permeability and permittivity. > Minimum RL as a function of frequency, thickness and MnZn volume fraction given. > Higher thicknesses imply better absorption; optimum band shifts to lower frequencies. > For higher volume fractions, smaller thickness might offer better absorption (>10 GHz).

  3. Accelerated development of Zr-containing new generation ferritic steels for advanced nuclear reactors

    Energy Technology Data Exchange (ETDEWEB)

    Tan, Lizhen [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Yang, Ying [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Sridharan, K. [Univ. of Wisconsin, Madison, WI (United States)

    2015-12-01

    The mission of the Nuclear Energy Enabling Technologies (NEET) program is to develop crosscutting technologies for nuclear energy applications. Advanced structural materials with superior performance at elevated temperatures are always desired for nuclear reactors, which can improve reactor economics, safety margins, and design flexibility. They benefit not only new reactors, including advanced light water reactors (LWRs) and fast reactors such as the sodium-cooled fast reactor (SFR) that is primarily designed for management of high-level wastes, but also life extension of the existing fleet when component exchange is needed. Developing and utilizing the modern materials science tools (experimental, theoretical, and computational tools) is an important path to more efficient alloy development and process optimization. The ultimate goal of this project is, with the aid of computational modeling tools, to accelerate the development of Zr-bearing ferritic alloys that can be fabricated using conventional steelmaking methods. The new alloys are expected to have superior high-temperature creep performance and excellent radiation resistance as compared to Grade 91. The designed alloys were fabricated using arc-melting and drop-casting, followed by hot rolling and conventional heat treatments. Comprehensive experimental studies have been conducted on the developed alloys to evaluate their hardness, tensile properties, creep resistance, Charpy impact toughness, and aging resistance, as well as resistance to proton and heavy ion (Fe2+) irradiation.

  4. HOT ROLLING OF A FERRITIC STAINLESS STEEL IN A STECKEL MILL: THERMOMECHANICAL AND MICROSTRUCTURAL CARACTERIZATION AND MATHEMATICAL MODELLING OF THE EVOLUTION OF RECRYSTALLIZED VOLUME FRACTION OF FERRITE

    Directory of Open Access Journals (Sweden)

    Willy Schuwarten Júnior

    2013-10-01

    Full Text Available A thermomechanical and a microstructure caracterization and a mathematical model of the evolution of the recrystallized volume fraction of ferrite in hot rolling in a Steckel mill have been carried out here. The proposed model is able to reasonably predict the observed in hot rolling, that is, there is 100% recrystallization of ferrite after roughing and partial recrystallization only after finishing

  5. A Comparison of Creep Rupture Strength of Ferritic/Austenitic Dissimilar Weld Joints of Different Grades of Cr-Mo Ferritic Steels

    Science.gov (United States)

    Laha, K.; Chandravathi, K. S.; Parameswaran, P.; Goyal, Sunil; Mathew, M. D.

    2012-04-01

    Evaluations of creep rupture properties of dissimilar weld joints of 2.25Cr-1Mo, 9Cr-1Mo, and 9Cr-1MoVNb steels with Alloy 800 at 823 K were carried out. The joints were fabricated by a fusion welding process employing an INCONEL 182 weld electrode. All the joints displayed lower creep rupture strength than their respective ferritic steel base metals, and the strength reduction was greater in the 2.25Cr-1Mo steel joint and less in the 9Cr-1Mo steel joint. Failure location in the joints was found to shift from the ferritic steel base metal to the intercritical region of the heat-affected zone (HAZ) of the ferritic steel (type IV cracking) with the decrease in stress. At still lower stresses, the failure in the joints occurred at the ferritic/austenitic weld interface. The stress-life variation of the joints showed two-slope behavior and the slope change coincided with the occurrence of ferritic/austenitic weld interface cracking. Preferential creep cavitation in the soft intercritical HAZ induced type IV failure, whereas creep cavitation at the interfacial particles induced ferritic/austenitic weld interface cracking. Micromechanisms of the type IV failure and the ferritic/austenitic interface cracking in the dissimilar weld joint of the ferritic steels and relative cracking susceptibility of the joints are discussed based on microstructural investigation, mechanical testing, and finite element analysis (FEA) of the stress state across the joint.

  6. Simulation of layer - sequence of Ni-Zn ferrite thin films and multilayers for EMC applications >1000 MHz; Untersuchung zur Schichtfolge eines Multilayerschichtsystems NiZn Ferrit / Si bzw. SiO{sub 2} fuer Hoechstfrequenzleiterplatten im Frequenzbereich groesser 1000 MHz

    Energy Technology Data Exchange (ETDEWEB)

    Graebner, F.; Hildenbrand, S. [Institut fuer Maschinen, Antriebe und elektronische Geraetetechnik Nordhausen (Germany); Teichert, G.; Hungsberg, A.; Koledintseva, M. [Materialforschungs-und Pruefanstalt Weimar, Aussenstelle Ilmenau (Germany); Knedlik, Ch.; Romanus, H. [Institut fuer Maschinen, Antriebe und elektronische Geraetetechnik gGmbH, Neue HF-Materialien, An der Salza 8a, 99734 Nordhausen (Germany)

    2003-07-01

    NiZn ferrite multilayer have attracted much attention as materials with unique properties. One of these properties is enhanced microwave absorption. This gives a possibility to product absorption electromagnetic covers (EMC) with ultrathin thickness. The Electromagnetic Compatibility absorption of NiZn Ferrite polycristalline sample is 0,6 dB in the rf- range. (Abstract Copyright [2003], Wiley Periodicals, Inc.) [German] Es ist gelungen mittels des Sputterverfahrens ferritische Multilayerschichten auf HF-Leiterplattenmaterial der Firmen Rogers (USA) und Mauritz (Germany) abzuscheiden. Es wurde eine fast linear anwachsende Reflexionsdaempfung von 0,6 dB ab 1000 MHz bis 77000 MHz gemessen. Die theoretische Betrachtung mit einem numerischen Simulator 2DTLM zum Schichtfolgeaufbau konnte im Experiment in der Striplineanordnung bis 3800 MHZ diskutiert werden. Theoretische Simulationsergebnisse weisen auf gute Daempfungsergebnisse bei einem Schichtaufbau mit Anordnung einer Ferritschicht am Metallabschluss hin. (Abstract Copyright [2003], Wiley Periodicals, Inc.)

  7. Fast wave power flow along SOL field lines in NSTX

    Science.gov (United States)

    Perkins, R. J.; Bell, R. E.; Diallo, A.; Gerhardt, S.; Hosea, J. C.; Jaworski, M. A.; Leblanc, B. P.; Kramer, G. J.; Phillips, C. K.; Roquemore, L.; Taylor, G.; Wilson, J. R.; Ahn, J.-W.; Gray, T. K.; Green, D. L.; McLean, A.; Maingi, R.; Ryan, P. M.; Jaeger, E. F.; Sabbagh, S.

    2012-10-01

    On NSTX, a major loss of high-harmonic fast wave (HHFW) power can occur along open field lines passing in front of the antenna over the width of the scrape-off layer (SOL). Up to 60% of the RF power can be lost and at least partially deposited in bright spirals on the divertor floor and ceiling [1,2]. The flow of HHFW power from the antenna region to the divertor is mostly aligned along the SOL magnetic field [3], which explains the pattern of heat deposition as measured with infrared (IR) cameras. By tracing field lines from the divertor back to the midplane, the IR data can be used to estimate the profile of HHFW power coupled to SOL field lines. We hypothesize that surface waves are being excited in the SOL, and these results should benchmark advanced simulations of the RF power deposition in the SOL (e.g., [4]). Minimizing this loss is critical optimal high-power long-pulse ICRF heating on ITER while guarding against excessive divertor erosion.[4pt] [1] J.C. Hosea et al., AIP Conf Proceedings 1187 (2009) 105. [0pt] [2] G. Taylor et al., Phys. Plasmas 17 (2010) 056114. [0pt] [3] R.J. Perkins et al., to appear in Phys. Rev. Lett. [0pt] [4] D.L. Green et al., Phys. Rev. Lett. 107 (2011) 145001.

  8. Optimization of multiroute synthesis for polyaniline-barium ferrite composites

    Energy Technology Data Exchange (ETDEWEB)

    Ben Ghzaiel, Tayssir, E-mail: tayssir.ben-ghzaiel@satie.ens-cachan.fr [Université de Tunis El Manar Faculté des Sciences de Tunis, UR11ES18 Unité de Recherche de Chimie Minérale Appliquée, 2092, Tunis (Tunisia); SATIE, ENS Cachan, CNRS, Université Paris-Saclay, 61 av du Président Wilson, F-94230, Cachan (France); Dhaoui, Wadia [Université de Tunis El Manar Faculté des Sciences de Tunis, UR11ES18 Unité de Recherche de Chimie Minérale Appliquée, 2092, Tunis (Tunisia); Pasko, Alexander; Mazaleyrat, Frédéric [SATIE, ENS Cachan, CNRS, Université Paris-Saclay, 61 av du Président Wilson, F-94230, Cachan (France)

    2016-08-15

    A comparative study of physicochemical and magnetic properties of Polyaniline-BaFe{sub 12}O{sub 19} composites prepared by Solid-Based Polymerization (SBP) and by Aqueous-Based Polymerization (ABP) is carried out. The composites obtained by the latter method underwent a grinding to study the influence of shear stress. Thus, in a systematic approach, an investigation of stirring effect was done by synthesizing these composites using aqueous-based polymerization but without mechanical stirring. Different mass ratio of BaFe{sub 12}O{sub 19} was used to explore their impact on composites properties. X-ray diffraction, FTIR, SEM, TGA, conductivity and vibrating sample magnetometer measurements were performed. Structural and morphological investigations confirmed the presence of polyaniline and barium hexaferrite phase, which were in interaction in the composites regardless the polymerization route. The powder obtained by solid-based pathway revealed distinct particles with uniform distribution for various compositions (wt. %) of BaFe{sub 12}O{sub 19} in Pani, while the composites obtained by aqueous-based polymerization presented agglomerated nanostructures. Thermogravimetric analysis exhibited an improved thermal stability for Pani-BaFe{sub 12}O{sub 19} obtained by solid-based route. The electric conductivity has displayed decreasing trend of DC conductivity with the increase of BaFe{sub 12}O{sub 19} particles in the polymer matrix. Magnetic studies showed a ferromagnetic behaviour for all composites. The saturation magnetization monotonously increased with the increasing of BaFe{sub 12}O{sub 19} amount. The magnetic properties of the powders were mainly related to the hexaferrite loading which was determined using measured magnetic data. These results revealed that magnetization saturation was dependant of volume fraction of ferrite in the composites which was significantly affected by the reaction medium and mechanical stirring. The powders obtained by solid

  9. Influence of ferrite phase in alite-calcium sulfoaluminate cements

    Science.gov (United States)

    Duvallet, Tristana Yvonne Francoise

    Since the energy crisis in 1970's, research on low energy cements with low CO2- emissions has been increasing. Numerous solutions have been investigated, and the goal of this original research is to create a viable hybrid cement with the components of both Ordinary Portland cement (OPC) and calcium sulfoaluminate cement (CSAC), by forming a material that contains both alite and calcium sulfoaluminate clinker phases. Furthermore, this research focuses on keeping the cost of this material reasonable by reducing aluminum requirements through its substitution with iron. The aim of this work would produce a cement that can use large amounts of red mud, which is a plentiful waste material, in place of bauxite known as an expensive raw material. Modified Bogue equations were established and tested to formulate this novel cement with different amounts of ferrite, from 5% to 45% by weight. This was followed by the production of cement from reagent chemicals, and from industrial by-products as feedstocks (fly ash, red mud and slag). Hydration processes, as well as the mechanical properties, of these clinker compositions were studied, along with the addition of gypsum and the impact of a ferric iron complexing additive triisopropanolamine (TIPA). To summarize this research, the influence of the addition of 5-45% by weight of ferrite phase, was examined with the goal of introducing as much red mud as possible in the process without negatively attenuate the cement properties. Based on this PhD dissertation, the production of high-iron alite-calcium sulfoaluminateferrite cements was proven possible from the two sources of raw materials. The hydration processes and the mechanical properties seemed negatively affected by the addition of ferrite, as this phase was not hydrated entirely, even after 6 months of curing. The usage of TIPA counteracted this decline in strength by improving the ferrite hydration and increasing the optimum amount of gypsum required in each composition

  10. Tunable dual-band negative refractive index in ferrite-based metamaterials.

    Science.gov (United States)

    Bi, Ke; Zhou, Ji; Zhao, Hongjie; Liu, Xiaoming; Lan, Chuwen

    2013-05-06

    A tunable dual-band ferrite-based metamaterial has been investigated by experiments and simulations. The negative permeability is realized around the ferromagnetic resonance (FMR) frequency which can be influenced by the dimension of the ferrites. Due to having two negative permeability frequency regions around the two FMR frequencies, the metamaterials consisting of metallic wires and ferrite rods with different sizes possess two passbands in the transmission spectra. The microwave transmission properties of the ferrite-based metamaterials can be not only tuned by the applied magnetic field, but also adjusted by the dimension of the ferrite rods. A good agreement between experimental and simulated results is demonstrated, which confirms that the tunable dual-band ferrite-based metamaterials can be used for cloaks, antennas and absorbers.

  11. Science Letters:Preparation of high-permeability NiCuZn ferrite

    Institute of Scientific and Technical Information of China (English)

    HU Jun; YAN Mi

    2005-01-01

    Appropriate addition of CuO/V2O5 and the reduction of the granularity of the raw materials particle decrease the sintering temperature ofNiZn ferrite from 1200 ℃ to 930 ℃. Furthermore, the magnetic properties of the NiZn ferrite prepared at low temperature of 930 ℃ is superior to that of the NiZn ferrite prepared by sintering at high temperature of 1200 ℃ because the microstructure of the NiZn ferrite sintered at 930 ℃ is more uniform and compact than that of the NiZn ferrite sintered at 1200 ℃.The high permeability of 1700 and relative loss coefficient tanδ//μi of 9.0×10-6 at 100 kHz was achieved in the (Ni0.17Zn0.63Cu0.20)Fe1.915O4 ferrite.

  12. Bench-Scale Testing of Zinc Ferrite Sorbent for Hot Gas Clean-up

    Institute of Scientific and Technical Information of China (English)

    Meisheng Liang; Hongyan Xu; Kechang Xie

    2007-01-01

    Advanced integrated gasification combined cycle (IGCC) power generation systems require the development of high-temperature, regenerable desulfurization sorbents, which are capable of removing hydrogen sulfide from coal gasifier gas to very low levels. In this paper, zinc ferrites prepared by co-precipitation were identified as a novel coal gas desulfurization sorbent at high temperature. Preparation of zinc ferrite and effects of binders on pore volume, strength and desulfurization efficiency of zinc ferrite desulfurizer were studied. Moreover, the behavior of zinc ferrite sorbent during desulfurization and regeneration under the temperature range of 350-400 ℃ are investigated. Effects of binders on the pore volume, mechanical strength and desulfurization efficiency of zinc ferrite sorbents indicated that the addition of kaolinite to zinc ferrite desulfurizer seems to be superior to other binders under the experimental conditions.

  13. Comments on ferrite phase shifter configurations for the millimeter wave region

    Science.gov (United States)

    Reuss, M. L., Jr.

    1982-09-01

    In the microwave region of the electromagnetic spectrum, electronically controllable ferrite phase shifters have demonstrated their value as components and as control elements for switches and attenuators. As the need for control components operating in the lower millimeter wave region increases, it is a reasonable approach to scale successful microwave ferrite configurations into the lower millimeter wave region (30 GHz to 140 GHz). However, many problems are encountered when attempting to scale efficient microwave ferrite configurations, particularly latching ferrite configurations, into the millimeter wave region. It is the objective of this report to review several ferrite configurations with the intent that consideration of these configurations may stimulate development of practical millimeter wave configurations. Ferrite phase shifter configurations that will be the subject of comment include the toroidal (dual slab), dual mode, Bush-Reggia-Spencer, and single slab configurations. Comments are also presented on a circulator used as a phase shifter.

  14. Delta ferrite-containing austenitic stainless steel resistant to the formation of undesirable phases upon aging

    Science.gov (United States)

    Leitnaker, James M.

    1981-01-01

    Austenitic stainless steel alloys containing delta ferrite, such as are used as weld deposits, are protected against the transformation of delta ferrite to sigma phase during aging by the presence of carbon plus nitrogen in a weight percent 0.015-0.030 times the volume percent ferrite present in the alloy. The formation of chi phase upon aging is controlled by controlling the Mo content.

  15. The influence of the heat treatment on delta ferrite transformation in austenitic stainless steel welds

    Directory of Open Access Journals (Sweden)

    B. Mateša

    2012-04-01

    Full Text Available Shielded metal arc (SMAW welded specimens using austenitic consumable materials with different amount of delta-ferrite are annealed in range 650-750 °C through 2-10 hours. Factorial plan 33 with influenced factors regression analyze of measured delta-ferrite values is used. The transformation i.e. decomposition of delta ferrite during annealing was analyzed regarding on weld cracking resistance using metallographic examination and WRC-1992 diagram.

  16. Negative and near zero refraction metamaterials based on permanent magnetic ferrites

    OpenAIRE

    Bi, Ke; Guo, Yunsheng; ZHOU, JI; Dong, Guoyan; Zhao, Hongjie; Zhao, Qian; Xiao, Zongqi; Liu, Xiaoming; Lan, Chuwen

    2014-01-01

    Ferrite metamaterials based on the negative permeability of ferromagnetic resonance in ferrites are of great interest. However, such metamaterials face a limitation that the ferromagnetic resonance can only take place while an external magnetic field applied. Here, we demonstrate a metamaterial based on permanent magnetic ferrite which exhibits not only negative refraction but also near zero refraction without applied magnetic field. The wedge-shaped and slab-shaped structures of permanent ma...

  17. Ultra-Pure Ferritic Stainless Steels-Grade, Refining Operation, and Application

    Institute of Scientific and Technical Information of China (English)

    YOU Xiang-mi; JIANG Zhou-hua; LI Hua-bing

    2007-01-01

    The grades of ultra-pure ferritic stainless steels, especially the grades used in automobile exhaust system, were reviewed. The dependence of properties on alloying elements, the refining facilities, and the mechanism of the reactions in steel melts were described in detail. Vacuum, strong stirring, and powder injection proved to be effective technologies in the melting of ultra-pure ferritic stainless steels. The application of the ferritic grades was also briefly introduced.

  18. Hydrogen-Induced Delayed Cracking in TRIP-Aided Lean-Alloyed Ferritic-Austenitic Stainless Steels

    Directory of Open Access Journals (Sweden)

    Suvi Papula

    2017-06-01

    Full Text Available Susceptibility of three lean-alloyed ferritic-austenitic stainless steels to hydrogen-induced delayed cracking was examined, concentrating on internal hydrogen contained in the materials after production operations. The aim was to study the role of strain-induced austenite to martensite transformation in the delayed cracking susceptibility. According to the conducted deep drawing tests and constant load tensile testing, the studied materials seem not to be particularly susceptible to delayed cracking. Delayed cracks were only occasionally initiated in two of the materials at high local stress levels. However, if a delayed crack initiated in a highly stressed location, strain-induced martensite transformation decreased the crack arrest tendency of the austenite phase in a duplex microstructure. According to electron microscopy examination and electron backscattering diffraction analysis, the fracture mode was predominantly cleavage, and cracks propagated along the body-centered cubic (BCC phases ferrite and α’-martensite. The BCC crystal structure enables fast diffusion of hydrogen to the crack tip area. No delayed cracking was observed in the stainless steel that had high austenite stability. Thus, it can be concluded that the presence of α’-martensite increases the hydrogen-induced cracking susceptibility.

  19. Preparation of Mn-Zn ferrite nanoparticles and their silica-coated clusters: Magnetic properties and transverse relaxivity

    Science.gov (United States)

    Kaman, Ondřej; Kuličková, Jarmila; Herynek, Vít; Koktan, Jakub; Maryško, Miroslav; Dědourková, Tereza; Knížek, Karel; Jirák, Zdeněk

    2017-04-01

    Hydrothermal synthesis of Mn1-xZnxFe2O4 nanoparticles followed by direct encapsulation of the as-grown material into silica is demonstrated as a fast and facile method for preparation of efficient negative contrast agents based on clusters of ferrite crystallites. At first, the hydrothermal procedure is optimized to achieve strictly single-phase magnetic nanoparticles of Mn-Zn ferrites in the compositional range of x≈0.2-0.6 and with the mean size of crystallites ≈10 nm. The products are characterized by powder X-ray diffraction, X-ray fluorescence spectroscopy, and SQUID magnetometry, and the composition close to x=0.4 is selected for the preparation of silica-coated clusters with the mean diameter of magnetic cores ≈25 nm. Their composite structure is studied by means of transmission electron microscopy combined with detailed image analysis and magnetic measurements in DC fields. The relaxometric studies, performed in the magnetic field of B0=0.5 T, reveal high transverse relaxivity (r2(20 °C)=450 s-1 mmol(Me3O4)-1 L) with a pronounced temperature dependence, which correlates with the observed temperature dependence of magnetization and is ascribed to a mechanism of transverse relaxation similar to the motional averaging regime.

  20. Hydrogen-Induced Delayed Cracking in TRIP-Aided Lean-Alloyed Ferritic-Austenitic Stainless Steels.

    Science.gov (United States)

    Papula, Suvi; Sarikka, Teemu; Anttila, Severi; Talonen, Juho; Virkkunen, Iikka; Hänninen, Hannu

    2017-06-03

    Susceptibility of three lean-alloyed ferritic-austenitic stainless steels to hydrogen-induced delayed cracking was examined, concentrating on internal hydrogen contained in the materials after production operations. The aim was to study the role of strain-induced austenite to martensite transformation in the delayed cracking susceptibility. According to the conducted deep drawing tests and constant load tensile testing, the studied materials seem not to be particularly susceptible to delayed cracking. Delayed cracks were only occasionally initiated in two of the materials at high local stress levels. However, if a delayed crack initiated in a highly stressed location, strain-induced martensite transformation decreased the crack arrest tendency of the austenite phase in a duplex microstructure. According to electron microscopy examination and electron backscattering diffraction analysis, the fracture mode was predominantly cleavage, and cracks propagated along the body-centered cubic (BCC) phases ferrite and α'-martensite. The BCC crystal structure enables fast diffusion of hydrogen to the crack tip area. No delayed cracking was observed in the stainless steel that had high austenite stability. Thus, it can be concluded that the presence of α'-martensite increases the hydrogen-induced cracking susceptibility.

  1. Method for making conductors for ferrite memory arrays. [from pre-formed metal conductors

    Science.gov (United States)

    Heckler, C. H.; Baba, P. D.; Bhiwandker, N. C. (Inventor)

    1974-01-01

    The ferrite memory arrays are made from pre-formed metal conductors for the ferrite arrays. The conductors are made by forming a thin sheet of a metallizing paste of metal alloy powder, drying the paste layer, bisque firing the dried sheet at a first temperature, and then punching the conductors from the fired sheet. During the bisque firing, the conductor sheet shrinks to 58 percent of its pre-fired volume and the alloy particles sinter together. The conductors are embedded in ferrite sheet material and finally fired at a second higher temperature during which firing the conductors shrink approximately the same degree as the ferrite material.

  2. Cofiring behavior of NiCuZn ferrite/PMN ferroelectrics di-layer composites

    Institute of Scientific and Technical Information of China (English)

    MIAO Chun-lin; ZHOU Ji; YUE Zhen-xing; LI Long-tu

    2005-01-01

    The cofiring compatibility between ferrite and relaxor ferroelectrics materials is the key issue in the production of multilayer chip LC filters. The cofiring behavior, interfacial microstructure and diffusion of di-layer composites of NiCuZn ferrite/PMN relaxor ferroelectrics are studied. In order to analyze the matching condition of thermodynamic properties between ferrite and relaxor ferroelectric ceramics, TMA is performed on PMN ferroelectrics and NiCuZn ferrite with certain percentage of Bi2 O3, respectively. EDS results demonstrate that serious element diffusions exist at the interface, which is in accordance with the phase analysis based on XRD patterns.

  3. Deformation Behavior of Ultra-low Carbon Steel in Ferrite Region during Warm Processing

    Institute of Scientific and Technical Information of China (English)

    XU Guang; CHEN Zhenye; LIU Li; YU Shengfu

    2008-01-01

    The hot deformation experiments of ultra-low carbon steel in ferrite range were carried out ina hot simulator in order to research hot deformation behaviors of ultra-low carbon steel in ferrite range at low temperature.The results show that the influences of deformation parameters on flow stress are different to those in austenitic deformation.The deformation characteristic parameters were calculated for ultra-low carbon steel in ferrite region.The flow stress equation for ultra-low carbon steel in ferritic deformation at low temperature was obtained.

  4. Material for magnetostrictive sensors and other applications based on ferrite materials

    Science.gov (United States)

    McCallum, R. William; Snyder, John E.; Dennis, Kevin W.; Schwichtenberg, Carl R.; Jiles, David C.

    2000-07-25

    The present invention provides magnetostrictive compositions that include an oxide ferrite which provides mechanical properties that make the magnetostrictive compositions effective for use as sensors and actuators.

  5. Nanophotonic Modulator with Bismuth Ferrite as Low-loss Switchable Material

    DEFF Research Database (Denmark)

    Babicheva, Viktoriia; Zhukovsky, Sergei; Lavrinenko, Andrei

    2015-01-01

    We propose a nanophotonic waveguide modulator with bismuth ferrite as a tunable material. Due to near-zero losses in bismuth ferrite, modulation with up to 20 dB/μm extinction ratio and 12 μm propagation length is achieved.......We propose a nanophotonic waveguide modulator with bismuth ferrite as a tunable material. Due to near-zero losses in bismuth ferrite, modulation with up to 20 dB/μm extinction ratio and 12 μm propagation length is achieved....

  6. Fabrication and electromagnetic properties of flake ferrite particles based on diatomite

    Energy Technology Data Exchange (ETDEWEB)

    Zhang Deyuan [Bionic and Micro/Nano/Bio Manufacturing Technology Research Center, Beihang University, Beijing 100191 (China); Zhang Wenqiang, E-mail: zwqzwqzwqzwq@126.com [Bionic and Micro/Nano/Bio Manufacturing Technology Research Center, Beihang University, Beijing 100191 (China); Cai Jun, E-mail: jun_cai@buaa.edu.cn [Bionic and Micro/Nano/Bio Manufacturing Technology Research Center, Beihang University, Beijing 100191 (China)

    2011-09-15

    Hexagonal ferrite BaZn{sub 1.1}Co{sub 0.9}Fe{sub 16}O{sub 27} coated surfaces of diatomite flakes of low density were synthesized by a sol-gel method. The phase structures, morphologies, particle size and chemical compositions of the composites were characterized by X-ray diffraction, scanning electron microscope and energy dispersive X-ray spectroscopy. The results show that hexagonal ferrite coated diatomite flakes can be achieved, and that the coating consisted of BaZn{sub 1.1}Co{sub 0.9}Fe{sub 16}O{sub 27} nanoparticles. The vibranting sample magnetometer results reveal that the flake ferrite particles have static magnetic properties. The complex permeability and permittivity of the composites were measured in the frequency range of 1-18 GHz. The microwave absorption properties of these ferrite particles are discussed. The results indicate that the flake ferrites have the potential to be used as a lightweight broad band microwave absorber. - Highlights: > We synthesize the flake ferrite particles using diatomite as a template. > Flake ferrite particles' coating layers are constituted by BaZn{sub 1.1}Co{sub 0.9}Fe{sub 16}O{sub 27} nanoparticles. > Flake ferrite particles have good static magnetic properties. > Flake ferrites are a kind lightweight broad band microwave absorber.

  7. Microstructure characterization and cation distribution of nanocrystalline cobalt ferrite

    Energy Technology Data Exchange (ETDEWEB)

    Abbas, Y.M., E-mail: ymabbas@live.com [Suez Canal University, Faculty of Science, Physics Department, Ismailia (Egypt); Mansour, S.A.; Ibrahim, M.H. [Suez Canal University, Faculty of Science, Physics Department, Ismailia (Egypt); Ali, Shehab E., E-mail: shehab_physics@yahoo.com [Suez Canal University, Faculty of Science, Physics Department, Ismailia (Egypt)

    2011-11-15

    Nanocrystalline cobalt ferrite has been synthesized using two different methods: ceramic and co-precipitation techniques. The nanocrystalline ferrite phase has been formed after 3 h of sintering at 1000 deg. C. The structural and microstructural evolutions of the nanophase have been studied using X-ray powder diffraction and the Rietveld method. The refinement result showed that the type of the cationic distribution over the tetrahedral and octahedral sites in the nanocrystalline lattice is partially an inverse spinel. The transmission electronic microscope analysis confirmed the X-ray results. The magnetic properties of the samples were characterized using a vibrating sample magnetometer. - Highlights: > The refinement result showed that the cationic distribution over the sites in the lattice is partially an inverse spinel. > The transmission electronic microscope analysis confirmed the X-ray results. > The magnetic properties of the samples were characterized using a vibrating sample magnetometer.

  8. Structural and magnetic study of dysprosium substituted cobalt ferrite nanoparticles

    Energy Technology Data Exchange (ETDEWEB)

    Kumar, Hemaunt, E-mail: hvatsal@gmail.com [Department of Physics, Govind Ballabh Pant University of Agr. & Technology, Pantnagar, Uttarakhand 263145 (India); Srivastava, R.C. [Department of Physics, Govind Ballabh Pant University of Agr. & Technology, Pantnagar, Uttarakhand 263145 (India); Pal Singh, Jitendra [Advanced Analysis Centre, Korea Institute of Science and Technology, Seoul 02792 (Korea, Republic of); Negi, P. [Department of Physics, Govind Ballabh Pant University of Agr. & Technology, Pantnagar, Uttarakhand 263145 (India); Agrawal, H.M. [Advanced Analysis Centre, Korea Institute of Science and Technology, Seoul 02792 (Korea, Republic of); Das, D. [UGC-DAE CSR Kolkata Centre, Kolkata 700098 (India); Hwa Chae, Keun [Advanced Analysis Centre, Korea Institute of Science and Technology, Seoul 02792 (Korea, Republic of)

    2016-03-01

    The present work investigates the magnetic behavior of Dy{sup 3+} substituted cobalt ferrite nanoparticles. X-ray diffraction studies reveal presence of cubic spinel phases in these nanoparticles. Raman spectra of these nanoparticles show change in intensity of Raman bands, which reflects cation redistribution in cubic spinel lattice. Saturation magnetization and coercivity decrease with increase of Dy{sup 3+}concentration in these nanoparticles. Room temperature Mössbauer measurements show the cation redistribution in these nanoparticles and corroborates the results obtained from Raman Spectroscopic measurements. Decrease in magnetization of Dy{sup 3+} substituted cobalt ferrite is attributed to the reduction in the magnetic interaction and cation redistribution. - Highlights: • Slight decrease in crystallite size after Dy{sup 3+} doping. • Saturation magnetization and coercivity decrease after Dy{sup 3+} doping. • Mössbauer measurements show the cation redistribution in the samples.

  9. Development of ferrite logic devices for an arithmetic processor

    Science.gov (United States)

    Heckler, C. H., Jr.

    1972-01-01

    A number of fundamentally ultra-reliable, all-magnetic logic circuits are developed using as a basis a single element ferrite structure wired as a logic delay element. By making minor additions or changes to the basic wiring pattern of the delay element other logic functions such as OR, AND, NEGATION, MAJORITY, EXCLUSIVE-OR, and FAN-OUT are developed. These logic functions are then used in the design of a full-adder, a set/reset flip-flop, and an edge detector. As a demonstration of the utility of all the developed devices, an 8-bit, all-magnetic, logic arithmetic unit capable of controlled addition, subtraction, and multiplication is designed. A new basic ferrite logic element and associated complementary logic scheme with the potential of improved performance is also described. Finally, an improved batch process for fabricating joint-free power drive and logic interconnect conductors for this basic class of all-magnetic logic is presented.

  10. Dye removal using modified copper ferrite nanoparticle and RSM analysis.

    Science.gov (United States)

    Mahmoodi, Niyaz Mohammad; Soltani-Gordefaramarzi, Sajjad; Sadeghi-Kiakhani, Moosa

    2013-12-01

    In this paper, copper ferrite nanoparticle (CFN) was synthesized, modified by cetyl trimethylammonium bromide, and characterized. Dye removal ability of the surface modified copper ferrite nanoparticle (SMCFN) from single system was investigated. The physical characteristics of SMCFN were studied using Fourier transform infrared, scanning electron microscopy, and X-ray diffraction. Acid Blue 92, Direct Green 6, Direct Red 23, and Direct Red 80 were used as model compounds. The effect of operational parameters (surfactant concentration, adsorbent dosage, dye concentration, and pH) on dye removal was evaluated. Response surface methodology (RSM) was used for the analysis of the dye removal data. The experimental checking in these optimal conditions confirms good agreements with RSM results. The results showed that the SMCFN being a magnetic adsorbent might be a suitable alternative to remove dyes from colored aqueous solutions.

  11. Microstructure development of welding joints in high Cr ferritic steels

    Energy Technology Data Exchange (ETDEWEB)

    Kubushiro, Keiji; Takahashi, Satoshi; Morishima, Keiko [IHI Corporation (Japan). Research Lab.

    2010-07-01

    Creep failure in high Cr ferritic steels welding joints are Type IV failure. Type IV-failure was ruptured in fine grained region of heat affected zone, microstructure and phase transformation process at welding in fine grained region were very important to clarify. Microstructure difference of heat affected zone was investigated in Gr.91, Gr.92, Gr.122 welding joint. The fraction of 60 degree block boundary, packet boundary, random boundary (including prior gamma boundary) length was compared in three ferritic steels by EBSP(Electron Backscatter Diffraction Pattern) analysis. HAZ was almost fully martensite phase in Gr.122 weld joint. On the other hand, HAZ in Gr.91 welding joint were some equiaxial grain and martensite structure. (orig.)

  12. Study of magnesium ferrite nano particles with excess iron content

    Energy Technology Data Exchange (ETDEWEB)

    Sumangala, T.P., E-mail: sumampoornima@gmail.com [Department of Metallurgical Engineering and Materials Science, Indian Institute of Technology Bombay, Powai, Mumbai 400076 (India); Mahender, C. [Department of Metallurgical Engineering and Materials Science, Indian Institute of Technology Bombay, Powai, Mumbai 400076 (India); Sahu, B.N. [Department of Physics, Indian Institute of Technology Bombay, Powai, Mumbai 400076 (India); Venkataramani, N. [Department of Metallurgical Engineering and Materials Science, Indian Institute of Technology Bombay, Powai, Mumbai 400076 (India); Prasad, Shiva [Department of Physics, Indian Institute of Technology Bombay, Powai, Mumbai 400076 (India)

    2014-09-01

    Stoichiometric and non stoichiometric magnesium ferrite (MgFe{sub 2+δ}O{sub 4}, δ=0.0, 0.1) were synthesized by the sol gel combustion method resulting in nanocrystalline powders with size ranging from 10 to 100 nm. These powders were calcined at various temperatures (300–800 °C). One part of the calcined powder was quenched in liquid nitrogen and the other part furnace cooled. α-Fe{sub 2}O{sub 3} was observed in all calcined samples by XRD and this was also reflected in the magnetization data. Electrical response of MgFe{sub 2.1}O{sub 4+δ} spinel phase to 75 ppm ethanol was found to be greater than that for a stoichiometric magnesium ferrite.

  13. Synthesis and characterization of nano silver ferrite composite

    Science.gov (United States)

    Murthy, Y. L. N.; Kondala Rao, T.; Kasi viswanath, I. V.; Singh, Rajendra

    2010-07-01

    We report the synthesis of nano sized silver ferrite composite having the empirical formula AgFeO 2 by a co-precipitation method. The resulting powders are thin platelets, transparent and a rich ruby red in color in transmission. The X-ray diffraction (XRD) powder data consisted of only nine reflections, and the analysis showed the unit cell to be rhombohedral. The powders showed extensive XRD line broadening and the sizes of the crystals are calculated to be in the range 4-36.5 nm. The morphology of the silver ferrite composite studied using scanning electron microscope showed nano sized particles. The particle size is found to increase with increase in annealing temperature. The magnetic behavior, measured using a vibrating sample magnetometer, indicated a change from paramagnetic to ferromagnetic with increase in particle size.

  14. The role of cobalt ferrite magnetic nanoparticles in medical science.

    Science.gov (United States)

    Amiri, S; Shokrollahi, H

    2013-01-01

    The nanotechnology industry is rapidly growing and promises that the substantial changes that will have significant economic and scientific impacts be applicable to a wide range of areas, such as aerospace engineering, nano-electronics, environmental remediation and medical healthcare. In this area, cobalt ferrite nanoparticles have been regarded as one of the competitive candidates because of their suitable physical, chemical and magnetic properties like the high anisotropy constant, high coercivity and high Curie temperature, moderate saturation magnetization and ease of synthesis. This paper introduces the magnetic properties, synthesis methods and some medical applications, including the hyperthermia, magnetic resonance imaging (MRI), magnetic separation and drug delivery of cobalt ferrite nanoparticles. Copyright © 2012 Elsevier B.V. All rights reserved.

  15. Magnetodielectric effect of Mn–Zn ferrite at resonant frequency

    Energy Technology Data Exchange (ETDEWEB)

    Pengfei, Pan; Ning, Zhang, E-mail: zhangning@njnu.edu.cn

    2016-10-15

    The dielectric properties and the magnetodielectric effect in Mn–Zn ferrite at resonant frequency have been studied in this paper. Dimensional-resonance-induced abnormal dielectric spectrum was observed at f≈1 MHz. The relatively large magnetodielectric ratio of 4500% in a magnetic field of 3.5 kOe was achieved from the Mn–Zn ferrite sample with the initial permeability of 15 K at resonant frequency at room temperature. Theoretical analysis suggests that the large MD effect at resonant frequency is attributed to the enhanced magnetostriction effect. - Highlights: • Dimensional resonance was measured in dielectric spectrum at f≈1 MHz. • The MD ratio of 4500% was induced by H = 3.5 kOe at resonant frequency. • The magnetostriction effect leads to the large MD effect at resonant frequency.

  16. Issues Affecting the Synthetic Scalability of Ternary Metal Ferrite Nanoparticles

    Directory of Open Access Journals (Sweden)

    Lauren Morrow

    2015-01-01

    Full Text Available Ternary Mn-Zn ferrite (MnxZn1-xFe2O4 nanoparticles (NPs have been prepared by the thermal decomposition of an oleate complex, sodium dodecylbenzenesulfonate (SDBS mediated hydrazine decomposition of the chloride salts, and triethylene glycol (TREG mediated thermal decomposition of the metal acetylacetonates. Only the first method was found to facilitate the synthesis of uniform, isolable NPs with the correct Mn : Zn ratio (0.7 : 0.3 as characterized by small angle X-ray scattering (SAXS, transmission electron microscopy (TEM, and inductively coupled plasma-optical emission spectroscopy (ICP-OES. Scaling allowed for retention of the composition and size; however, attempts to prepare Zn-rich ferrites did not result in NP formation. Thermogravimetric analysis (TGA indicated that the incomplete decomposition of the metal-oleate complexes prior to NP nucleation for Zn-rich compositions is the cause.

  17. Stress insensitive multilayer chip inductor with ferrite core

    Energy Technology Data Exchange (ETDEWEB)

    Vishwas, B.; Madhuri, W., E-mail: madhuriw12@gmail.com; Rao, N. Madhusudan; Kaleemulla, S. [School of Advanced Sciences, VIT University, Vellore-632014 (India)

    2015-06-24

    Mg{sub 0.25}Cu{sub 0.25}Zn{sub 0.5}Fe{sub 2}O{sub 4} is synthesized by sol gel auto combustion technique. The obtained ferrite powder is finally sintered in a microwave furnace at 850°C. Multilayer chip inductor (MLCI) of two layers is prepared by screen printing technique. The sintered ferrite is characterized by X-ray diffraction. The frequency response of dielectric constant is studied in the frequency range of 100Hz to 5MHz. Dielectric polarization is discussed in the light of Maxwell-Wagner interfacial polarization. The prepared MLCI is studied for stress sensitivity in the range of 0 to 8 MPa.

  18. A NOVEL HYDROTHERMAL SYNTHESIS METHOD FOR BARIUM FERRITE

    Institute of Scientific and Technical Information of China (English)

    Kang Li; Hongchen Gu; Qun Wei

    2004-01-01

    In the present work, fine barium ferrite powder has been synthesized through a one-step hydrothermal process in an autoclave at [OH-]/[Cl-] ratio of 2:1 in the temperature range from 180 to 260 ℃ using barium chloride (BaCl2), ferrous chloride (FeCl2) and potassium nitrate (KNO3) as the starting materials. Both particle size and saturation magnetization (Ms) increase with increasing hydrothermal reaction temperature, while the intrinsic coercivity (iHc) peaks at 685 Oe at 230 ℃. Morphology progress from the barium ferrite precursor particles to the barium hexaferrite particles has been monitored with increasing hydrothermal reaction time at 230 ℃ in the autoclave.

  19. Development of oxide dispersion strengthened ferritic steels for fusion

    Energy Technology Data Exchange (ETDEWEB)

    Mukhopadhyay, D.K. [Vista Metals, Inc., McKeesport, PA (United States); Froes, F.H. [Univ. of Idaho, ID (United States); Gelles, D.S. [Pacific Northwest National Lab., Richland, WA (United States)

    1998-03-01

    An oxide dispersion strengthened (ODS) ferritic steel with high temperature strength has been developed in line with low activation criteria for application in fusion power systems. The composition Fe-13.5Cr-2W-0.5Ti-0.25Y{sub 2}O{sup 3} was chosen to provide a minimum chromium content to insure fully delta-ferrite stability. High temperature strength has been demonstrated by measuring creep response of the ODS alloy in uniaxial tension at 650 and 900 C in an inert atmosphere chamber. Results of tests at 900 C demonstrate that this alloy has creep properties similar to other alloys of similar design and can be considered for use in high temperature fusion power system designs. The alloy selection process, materials production, microstructural evaluation and creep testing are described.

  20. Effect of deformation in controlled rolling on ferrite nucleation

    Energy Technology Data Exchange (ETDEWEB)

    Khlestov, V.M. [Priazovsky State Technical Univ., Mariupol (Ukraine); Konopleva, E.V.; McQueen, H.J. [Concordia Univ., Mechanical Engineering Dept., Montreal, Quebec (Canada)

    2001-04-01

    Nucleation of ferrite either at austenite grain boundaries or within them on deformation defects has been examined experimentally and analyzed on the basis of the theory of heterogeneous nucleation. Low-carbon low-alloy steels were deformed by controlled rolling schedules to a total reduction of 50 or 68% in finish rolling at 730-800 {sup o}C. Deformation accelerates the kinetics of the {gamma}-{alpha} transformation and strongly activates ferrite nucleation at grain boundaries. Both experimental and theoretical estimations showed that the rate of intragranular nucleation is much less compared to nucleation at grain boundaries. Intragranular nuclei develop notably only in the final stages of transformation in deformed austenite and affect the formation of structure only in the small separated areas. (author)

  1. Development of oxide dispersion strengthened ferritic steels for fusion

    Science.gov (United States)

    Mukhopadhyay, D. K.; Froes, F. H.; Gelles, D. S.

    1998-10-01

    An oxide dispersion strengthened (ODS) ferritic steel with high temperature strength has been developed in line with low activation criteria for application in fusion power systems. The composition Fe-13.5Cr-2W-0.5Ti-0.25Y 2O 3 was chosen to provide a minimum chromium content to insure fully delta-ferrite stability. High temperature strength has been demonstrated by measuring creep response of the ODS alloy in uniaxial tension at 650°C and 900°C in an inert atmosphere chamber. Results of tests at 900°C demonstrate that this alloy has creep properties similar to other alloys of similar design and can be considered for use in high temperature fusion power system designs. The alloy selection process, materials production, microstructural evaluation and creep testing are described.

  2. Preparation of lanthanum ferrite powder at low temperature

    Energy Technology Data Exchange (ETDEWEB)

    Andoulsi, R.; Horchani-Naifer, K.; Ferid, M., E-mail: karima_horchani@yahoo.com [Physical Chemistry Laboratory of Mineral Materials and their Applications, Hammam-Lif (Tunisia)

    2012-01-15

    Single lanthanum ferrite phase was successfully prepared at low processing temperature using the polymerizable complex method. To implement this work, several techniques such as differential scanning calorimetry, X-ray diffraction, Fourier Transform Infrared Spectroscopy, scanning electron microscopy and BET surface area measurements were used. Throw the obtained results, it was shown that steps of preparing the powder precursor and temperature of its calcination are critical parameters for avoiding phase segregation and obtaining pure lanthanum ferrite compound. Thus, a single perovskite phase was obtained at 600 deg C. At this temperature, the powder was found to be fine and homogeneous with an average crystallite size of 13 nm and a specific surface area of 12.5 m{sup 2}.g{sup -1}. (author)

  3. Studies on structural properties of clay magnesium ferrite nano composite

    Energy Technology Data Exchange (ETDEWEB)

    Kaur, Manpreet, E-mail: manpreetchem@pau.edu; Singh, Mandeep [Department of Chemistry, Punjab Agricultural University, Ludhiana-141004 (India); Jeet, Kiran, E-mail: kiranjeet@pau.edu; Kaur, Rajdeep [Electron Microscopy and Nanoscience Laboratory, Punjab Agricultural University, Ludhiana-141004 (India)

    2015-08-28

    Magnesium ferrite-bentonite clay composite was prepared by sol-gel combustion method employing citric acid as complexing agent and fuel. The effect of clay on the structural properties was studied with X-ray diffraction (XRD), Fourier transform infrared (FT-IR) Spectroscopy, Scanning electron microscopy (SEM), SEM- Energy dispersive Spectroscope (EDS) and BET surface area analyzer. Decrease in particle size and density was observed on addition of bentonite clay. The BET surface area of nano composite containing just 5 percent clay was 74.86 m{sup 2}/g. Whereas porosity increased from 40.5 per cent for the pure magnesium ferrite to 81.0 percent in the composite showing that nano-composite has potential application as an adsorbent.

  4. Design and screening of nanoprecipitates-strengthened advanced ferritic alloys

    Energy Technology Data Exchange (ETDEWEB)

    Tan, Lizhen [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Yang, Ying [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Chen, Tianyi [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Sridharan, K. [Univ. of Wisconsin, Madison, WI (United States); He, Li [Univ. of Wisconsin, Madison, WI (United States)

    2016-12-30

    Advanced nuclear reactors as well as the life extension of light water reactors require advanced alloys capable of satisfactory operation up to neutron damage levels approaching 200 displacements per atom (dpa). Extensive studies, including fundamental theories, have demonstrated the superior resistance to radiation-induced swelling in ferritic steels, primarily inherited from their body-centered cubic (bcc) structure. This study aims at developing nanoprecipitates strengthened advanced ferritic alloys for advanced nuclear reactor applications. To be more specific, this study aims at enhancing the amorphization ability of some precipitates, such as Laves phase and other types of intermetallic phases, through smart alloying strategy, and thereby promote the crystalline®amorphous transformation of these precipitates under irradiation.

  5. Dielectric Spectroscopy of Localized Electrical Charges in Ferrite Thin Film

    Science.gov (United States)

    Abdellatif, M. H.; Azab, A. A.; Moustafa, A. M.

    2017-09-01

    A thin film of Gd-doped Mn-Cr ferrite has been prepared by pulsed laser deposition from a bulk sample of the same ferrite prepared by the conventional double sintering ceramic technique. The charge localization and surface conduction in the ferromagnetic thin film were studied. The relaxation of the dielectric dipoles after exposure to an external alternating-current (AC) electric field was investigated. The effect of charge localization on the real and imaginary parts of the dielectric modulus was studied. The charge localization in the thin film was enhanced and thereby the Maxwell-Wagner-type interfacial polarization. The increase in interfacial polarization is a direct result of the enhanced charge localization. The sample was characterized in terms of its AC and direct-current (DC) electrical conductivity, and thermally stimulated discharge current.

  6. 3mm波铁氧体高速开关仿真设计%Simulation design of 3-mm wave ferrite high-speed switch

    Institute of Scientific and Technical Information of China (English)

    尹久红; 何绍强; 闫欢; 蒋运石; 胡艺缤; 丁敬垒

    2016-01-01

    According to the requirementof 3-mm wave radar, the ferrite switch scheme of the corresponding band is proposed. Through analysis on the principle and scheme,simulation and optimization design, processing technology, the ferrite high-speed switch was obtained featureing low insertion loss, fast switching time, low power consumption, high reliability. The ferrite switch has such good working performance in 3-mm band as VSMR of higher than 1.16, insertion lossα+≤0.58dB, isolationα―≥22dB 22dB and response timet≤2μs, which is of conference for the furthersimulation, design and process on the millimeter wave ferrite switch.%针对目前3mm波雷达要求,提出了相应频段的铁氧体开关方案。通过原理与方案分析、仿真优化设计和加工工艺的探索设计制作了一种具有插损低、开关转换时间快、功耗低和可靠性高等优点的3mm铁氧体高速开关。所研制的铁氧体开关在3mm频段内工作性能良好,性能为:输入电压驻波比VSWR≤1.16,正向损耗(插损)α+≤0.58dB,反向损耗(隔离度)α―≥22dB,开关响应时间 t≤2μs,为后续毫米波的仿真研究、加工技术手段提供了一定的方向与参考。

  7. Magnetic and magnetostrictive properties of Cu substituted Co-ferrites

    Energy Technology Data Exchange (ETDEWEB)

    Chandra Sekhar, B. [Vignan' s Institute of Engineering for Women, Visakhapatnam 530046 (India); Rao, G.S.N. [Dr. V.S. Krishna Govt. Degree College, Visakhapatnam (India); Caltun, O.F. [Department of Physics, A.I. Cuza University, Iasi (Romania); Dhana Lakshmi, B. [Department of Physics, Andhra University, Visakhapatnam 530003 (India); Parvatheeswara Rao, B., E-mail: bprao250@yahoo.com [Department of Physics, Andhra University, Visakhapatnam 530003 (India); Subba Rao, P.S.V. [Department of Physics, Andhra University, Visakhapatnam 530003 (India)

    2016-01-15

    Copper substituted cobalt ferrite, Co{sub 1−x}Cu{sub x}Fe{sub 2}O{sub 4} (x=0.00–0.25), nanoparticles were synthesized by sol–gel autocombustion method. X-ray diffraction analysis on the samples was done to confirm the cubic spinel structures and Scherrer equation was used to estimate the mean crystallite size as 40 nm. Using the obtained nanoparticles, fabrication of the sintered pellets was done by standard ceramic technique. Magnetic and magnetostrictive measurements on the samples were made by strain gauge and vibrating sample magnetometer techniques, respectively. Maximum magnetostriction and strain derivative values were deduced from the field dependent magnetostriction curves while the magnetic parameters such as saturation magnetization (51.7–61.9 emu/g) and coercivity (1045–1629 Oe) on the samples were estimated from the obtained magnetic hysteresis loops. Curie temperature values (457–315 °C) were measured by a built in laboratory set-up. Copper substituted cobalt ferrites have shown improved strain derivative values as compared to the pure cobalt ferrite and thus making them suitable for stress sensing applications. The results have been explained on the basis of cationic distributions, strength of exchange interactions and net decreased anisotropic contributions due to the increased presence of Co{sup 2+} ions in B-sites as a result of Cu substitutions. - Highlights: • Sol–gel autocombustion synthesized Co{sub 1–x}Cu{sub x}Fe{sub 2}O{sub 4} were investigated. • Moderate values of magnetostriction and saturation magnetization were obtained. • Cu substitution in Co ferrite enhances strain derivative and reduces Curie temperature. • Obtained results of Co{sub 1−x}Cu{sub x}Fe{sub 2}O{sub 4} find themselves suitable for magnetostrictive sensors.

  8. Synthesis and Properties of Tubular Polyaniline-Barium Ferrite Composite

    Institute of Scientific and Technical Information of China (English)

    Yuan-Xun Li; Ying-Li Liu; Jie Li; Fa-Ming Long; Jian-Hong Kang

    2007-01-01

    The polyanilinebarium ferrite composite was synthesized by in situ polymerization of aniline in the presence of BaFe12O19 nanoparticles. The structure,morphology, and magnetic properties of samples were characterized by powder Xray diffraction (XRD), Fourier transform infrared (FTIR), scanning electron microscopy (SEM) and vibrating sample magnetometer (VSM). The testing results showed that the composite exhibited the ferromagnetic and electric behaviors, which benefit for the application of electromagnetic interfence.

  9. Investigation of effects of inhomogeneous exchange within ferrites

    Energy Technology Data Exchange (ETDEWEB)

    Kuetche, Victor K., E-mail: vkuetche@yahoo.fr [National Advanced School of Engineering, University of Yaounde I, P.O. Box 8390 (Cameroon); Centre d' Excellence en Technologies de l' Information et de la Communication (CETIC), University of Yaounde I, P.O. Box 812 (Cameroon); Department of Physics, Faculty of Science, University of Yaounde I, P.O. Box 812 (Cameroon); The Abdus Salam International Centre for Theoretical Physics (ICTP), Strada Costiera, 11-I-34151 Trieste (Italy); Nguepjouo, Francis T., E-mail: nguepjouofrancis@yahoo.fr [National Advanced School of Engineering, University of Yaounde I, P.O. Box 8390 (Cameroon); Centre d' Excellence en Technologies de l' Information et de la Communication (CETIC), University of Yaounde I, P.O. Box 812 (Cameroon); Department of Physics, Faculty of Science, University of Yaounde I, P.O. Box 812 (Cameroon); Kofane, Timoleon C., E-mail: tckofane@yahoo.com [Centre d' Excellence en Technologies de l' Information et de la Communication (CETIC), University of Yaounde I, P.O. Box 812 (Cameroon); Department of Physics, Faculty of Science, University of Yaounde I, P.O. Box 812 (Cameroon); The Abdus Salam International Centre for Theoretical Physics (ICTP), Strada Costiera, 11-I-34151 Trieste (Italy)

    2015-01-15

    In this paper, we investigate the effects of inhomogeneous exchange on the magnetization dynamics within a ferromagnetic slab of 0.5 mm thickness from the viewpoint of the Landau–Lifshitz–Gilbert phenomenological theory of damping in ferromagnets. As a result, we unearth a new coupled system of magnetization dynamics in which structural analysis reveals the existence of soliton propagation in the above ferrite.

  10. A new approach to spinel ferrites through mean field approximation

    Energy Technology Data Exchange (ETDEWEB)

    Yazdani, A. [Tarbyat Modares University, Tehran P.C 14115-175 (Iran, Islamic Republic of)]. E-mail: yazdania@modares.ac.ir; Jalilian Nosrati, M.R. [Islamic Azad University Central Tehran Branch, Tehran P.C 14168-94351 (Iran, Islamic Republic of); Ghasemi, R. [Islamic Azad University Central Tehran Branch, Tehran P.C 14168-94351 (Iran, Islamic Republic of)

    2006-09-15

    The magnetic behavior and specification of spinel ferrites regarding exchange interactions is being studied. The strength of interactions has been examined through the cation substitution with application of mean field approximation of exchange interaction J{sub ij} . Two correlation and approximation parameters have been defined: correlation length R {sub c} in super-exchange and the magnetic effect of ion on the electron fluctuation J {sub 0}.

  11. Study of fluidized-bed desulfurization with zinc ferrite

    Energy Technology Data Exchange (ETDEWEB)

    Grindley, T

    1991-01-01

    Previous work established the technical feasibility of desulfurizing the hot product gases of coal gasification with fixed beds of a regenerable zinc ferrite sorbent. This process, intended for integration with coal gasifiers and gas turbines, has been tested and studied in considerable detail in a process development unit. Though possessing the advantages of high-sulfur absorption at low-sulfur breakthrough and the lack of sorbent attrition characteristic of a stationary bed, fixed beds also have inherent disadvantages: susceptibility to plugging by particles and a large diluent requirement during regeneration to control the reaction zone temperature. Therefore, METC conducted a scoping laboratory test program to determine the desulfurizing capability of fluid beds of zinc ferrite. Results from this program are presented. The results generally demonstrated that fluid beds of zinc ferrite have the potential to lower the H{sub 2}S level in hot gas from 10,000 to 10 ppmv. To achieve this at a high-sorbent sulfur loading would require two fluid-bed stages. Sorbent attrition appears to be acceptably low. Planned future activities include tests at high pressure with both simulated gas and in a gasifier sidestream.

  12. Thick barium ferrite films use for passive isolators

    Energy Technology Data Exchange (ETDEWEB)

    Capraro, Stephane; Chatelon, Jean Pierre; Rouiller, Thomas; Rousseau, Jean Jacques [DIOM, University of Saint-Etienne, 23 rue Michelon, 42023 Saint-Etienne cedex (France); Berre, Martine Le; Barbier, Daniel [LPM, UMR 5511, INSA Lyon, 7 av. Jean Capelle, 69621 Villeurbanne cedex (France); Joisten, Helene [CEA-LETI, 17 rue des martyrs, 38041 Grenoble cedex (France)

    2004-12-01

    Ferrites have magnetic properties suitable for electronic applications, especially in the microwave range (circulators and isolators). Hexagonal ferrite, such as barium ferrite, are of great interest for microwave device applications because of their large resistivity and high permeability at high frequencies. BaM films are deposited under optimized conditions by RF magnetron sputtering on alumina substrates. In order to crystallize the films that are amorphous after deposition, a post deposition annealing at 800 C is implemented. All samples present a good crystallization, a smooth surface and a good in-depth uniformity. The magnetic properties of BaM films show an optimized coercive force and saturation magnetization of 330 kA/m and 500 mT respectively. These values are close to that of the bulk BaM. Isolators are then realized and measured by a vector network analyzer and a probing system. Results on transmission coefficients show a non reciprocal effect, which reaches 8.3 dB/cm at 50 GHz. This proves that such a component behaves like an isolator in the 50 GHz band. (copyright 2004 WILEY-VCH Verlag GmbH and Co. KGaA, Weinheim) (orig.)

  13. Magnetic and Structural Investigations of Nanocrystalline Cobalt-Ferrite

    Directory of Open Access Journals (Sweden)

    I. Sharifi

    2012-10-01

    Full Text Available Cobalt ferrite is an important magnetic material due to their large magneto-crystalline anisotropy, high cohercivity, moderate saturation magnetization and chemical stability.In this study, cobalt ferrites Nanoparticles have been synthesized by the co-precipitation method and a new microemulsion route. We examined the cation occupancy in the spinel structure based on the “Rietveld with energies” method. The Xray measurements revealed the production of a broad single ferrite cubic phase with the average particle sizes of about 12 nm and 7nm, for co-precipitation and micro-emulsion methods, respectively. The FTIR measurements between 400 and 4000 cm-1 confirmed the intrinsic cation vibrations of the spinelstructure for the two methods. Furthermore, the Vibrating Sample Magnetometer (VSM was carried out at room temperature to study the structural and magnetic properties. The results revealed that by changing the method from co-precipitation to the reverse micelle the material exhibits a softer magnetic behavior in such a way that both saturation magnetization and coercivity decrease from 58 to 29 emu/g and from 286 to 25 Oe, respectively.

  14. Physiological Remediation of Cobalt Ferrite Nanoparticles by Ferritin

    Science.gov (United States)

    Volatron, Jeanne; Kolosnjaj-Tabi, Jelena; Javed, Yasir; Vuong, Quoc Lam; Gossuin, Yves; Neveu, Sophie; Luciani, Nathalie; Hémadi, Miryana; Carn, Florent; Alloyeau, Damien; Gazeau, Florence

    2017-01-01

    Metallic nanoparticles have been increasingly suggested as prospective therapeutic nanoplatforms, yet their long-term fate and cellular processing in the body is poorly understood. Here we examined the role of an endogenous iron storage protein - namely the ferritin - in the remediation of biodegradable cobalt ferrite magnetic nanoparticles. Structural and elemental analysis of ferritins close to exogenous nanoparticles within spleens and livers of mice injected in vivo with cobalt ferrite nanoparticles, suggests the intracellular transfer of degradation-derived cobalt and iron, entrapped within endogenous protein cages. In addition, the capacity of ferritin cages to accommodate and store the degradation products of cobalt ferrite nanoparticles was investigated in vitro in the acidic environment mimicking the physiological conditions that are present within the lysosomes. The magnetic, colloidal and structural follow-up of nanoparticles and proteins in the lysosome-like medium confirmed the efficient remediation of nanoparticle-released cobalt and iron ions by ferritins in solution. Metal transfer into ferritins could represent a quintessential process in which biomolecules and homeostasis regulate the local degradation of nanoparticles and recycle their by-products.

  15. Study of Zn-Cu ferrite nanoparticles for LPG sensing.

    Science.gov (United States)

    Jain, Anuj; Baranwal, Ravi Kant; Bharti, Ajaya; Vakil, Z; Prajapati, C S

    2013-01-01

    Nanostructured zinc-copper mixed ferrite was synthesized using sol-gel method. XRD patterns of different compositions of zinc-copper ferrite, Zn(1-x)Cu(x)Fe2O4 (x = 0.0, 0.25, 0.50, 0.75), revealed single phase inverse spinel ferrite in all the samples synthesized. With increasing copper concentration, the crystallite size was found to be increased from 28 nm to 47 nm. The surface morphology of all the samples studied by the Scanning Electron Microscopy there exhibits porous structure of particles throughout the samples. The pellets of the samples are prepared for LPG sensing characteristics. The sensing is carried out at different operating temperatures (200, 225, and 250°C) with the variation of LPG concentrations (0.2, 0.4, and 0.6 vol%). The maximum sensitivity of 55.33% is observed at 250°C operating for the 0.6 vol% LPG.

  16. Synthesis and Formation Mechanisms of Calcium Ferrite Compounds

    Institute of Scientific and Technical Information of China (English)

    Hesham I. Saleh

    2004-01-01

    Calcium ferrite compounds were prepared using calcium nitrate and iron nitrate with different molar ratios, 1:1, 0.5:1, and 1:0.5,respectively. The reactions of formation were investigated at different temperatures following the differential thermal analysis (DTA) results. Calcium ferrite compounds are CaFeO3, Ca2FeO3.5, Ca2Fe2O5, CaFe2O4, CaFe4O7, Ca7.2Fe0.8Fe30O53,Ca3Fe15O25, Ca4Fe14O25, and Ca4Fe9O17. Other reactive species of calcium nitrate are still present after firing at 450℃.Compounds were characterized using X-ray diffraction (XRD), DTA, TG, magnetic susceptibility, infrared spectra and scanning electron microscope (SEM). It is concluded that the formation mechanism of Ca-ferrite compounds depends mainly on the valency of iron cations which in role depends on its molar ratio and the existing atmosphere.

  17. Physiological Remediation of Cobalt Ferrite Nanoparticles by Ferritin.

    Science.gov (United States)

    Volatron, Jeanne; Kolosnjaj-Tabi, Jelena; Javed, Yasir; Vuong, Quoc Lam; Gossuin, Yves; Neveu, Sophie; Luciani, Nathalie; Hémadi, Miryana; Carn, Florent; Alloyeau, Damien; Gazeau, Florence

    2017-01-09

    Metallic nanoparticles have been increasingly suggested as prospective therapeutic nanoplatforms, yet their long-term fate and cellular processing in the body is poorly understood. Here we examined the role of an endogenous iron storage protein - namely the ferritin - in the remediation of biodegradable cobalt ferrite magnetic nanoparticles. Structural and elemental analysis of ferritins close to exogenous nanoparticles within spleens and livers of mice injected in vivo with cobalt ferrite nanoparticles, suggests the intracellular transfer of degradation-derived cobalt and iron, entrapped within endogenous protein cages. In addition, the capacity of ferritin cages to accommodate and store the degradation products of cobalt ferrite nanoparticles was investigated in vitro in the acidic environment mimicking the physiological conditions that are present within the lysosomes. The magnetic, colloidal and structural follow-up of nanoparticles and proteins in the lysosome-like medium confirmed the efficient remediation of nanoparticle-released cobalt and iron ions by ferritins in solution. Metal transfer into ferritins could represent a quintessential process in which biomolecules and homeostasis regulate the local degradation of nanoparticles and recycle their by-products.

  18. Antimicrobial Lemongrass Essential Oil—Copper Ferrite Cellulose Acetate Nanocapsules

    Directory of Open Access Journals (Sweden)

    Ioannis L. Liakos

    2016-04-01

    Full Text Available Cellulose acetate (CA nanoparticles were combined with two antimicrobial agents, namely lemongrass (LG essential oil and Cu-ferrite nanoparticles. The preparation method of CA nanocapsules (NCs, with the two antimicrobial agents, was based on the nanoprecipitation method using the solvent/anti-solvent technique. Several physical and chemical analyses were performed to characterize the resulting NCs and to study their formation mechanism. The size of the combined antimicrobial NCs was found to be ca. 220 nm. The presence of Cu-ferrites enhanced the attachment of LG essential oil into the CA matrix. The magnetic properties of the combined construct were weak, due to the shielding of Cu-ferrites from the polymeric matrix, making them available for drug delivery applications where spontaneous magnetization effects should be avoided. The antimicrobial properties of the NCs were significantly enhanced with respect to CA/LG only. This work opens novel routes for the development of organic/inorganic nanoparticles with exceptional antimicrobial activities.

  19. IR absorption spectroscopic study of mixed cobalt substituted lithium ferrites

    Science.gov (United States)

    Sawant, V. S.; Bagade, A. A.; Mohite, S. V.; Rajpure, K. Y.

    2014-10-01

    The IR spectra of Li0.5-(x/2)CoxFe2.5-(x/2)O4 ferrite samples (0≤x≤0.6) prepared by solution combustion method have been reported. The influence of Co substitution is verified. XRD studies confirm the spinel phase formation of ferrites. Lattice constant varies linearly from 8.31 Å (x=0) to 8.35 Å (x=0.6) with composition. Evidence of two absorption bands in the IR spectra (below 800 cm-1) reveals the characteristic feature of spinel ferrite. The IR spectra featured additional three absorption bands around 550, 670 and 705 cm-1 for the samples x=0.1 and x=0.6. Absence of bands splitting specifies that Fe ions do not exist in excess form. It is found that high frequency band (ν1), due to tetrahedral (A) group, lies at around 600 cm-1 and low frequency band (ν2), due to octahedral (B) group, around 450 cm-1. The positions of bands are found to be composition dependent. The IR bands due to tetrahedral complexes shift slightly towards high frequency side with composition upto x=0.4 where as that due to octahedral complexes shift towards lower frequency side with x. Based on the data of absorption bands, force constants (kt, ko) and bond lengths (RA, RB) were estimated. Compositional dependence of force constants is explained on the basis of cation-oxygen bond distances of respective sites and cation distribution.

  20. Aging and memory effect in magnetoelectric gallium ferrite single crystals

    Energy Technology Data Exchange (ETDEWEB)

    Singh, Vijay; Mukherjee, Somdutta [Department of Physics, Indian Institute of Technology Kanpur, Kanpur 208016 (India); Mitra, Chiranjib [Department of Physics, Indian Institute of Science Education and Research, Kolkata 741252 (India); Garg, Ashish [Department of Materials Science and Engineering, Indian Institute of Technology Kanpur, Kanpur 208016 (India); Gupta, Rajeev, E-mail: guptaraj@iitk.ac.in [Department of Physics, Indian Institute of Technology Kanpur, Kanpur 208016 (India); Materials Science Programme, Indian Institute of Technology Kanpur, Kanpur 208016 (India)

    2015-02-01

    Here, we present a time and temperature dependent magnetization study to understand the spin dynamics in flux grown single crystals of gallium ferrite (GaFeO{sub 3}), a known magnetoelectric, ferroelectric and ferrimagnet. Results of the magnetic measurements conducted in the field-cooled (FC) and zero-field-cooled (ZFC) protocols in the heating and cooling cycles were reminiscent of a “memory” effect. Subsequent time dependent magnetic relaxation measurements carried out in ZFC mode at 30 K with an intermittent cooling to 20 K in the presence of a small field show that the magnetization in the final wait period tends to follow its initial state which was present before the cooling break taken at 20 K. These observations provide an unambiguous evidence of single crystal gallium ferrite having a spin glass like phase. - Highlights: • Gallium ferrite a room temperature magnetoelectric and ferrimagnetic material. • Spin‐glass like phase at low temperatures below ∼200 K. • Observation of memory and aging effects in GFO.

  1. Defect detection for end surface of ferrite magnetic tile

    Science.gov (United States)

    Tao, Jiayuan; Wang, Yuwei; Wang, Keyi

    2016-09-01

    A visual automatic detection method is proposed for defect detection on end surface of ferrite magnetic tile to tackle the disadvantages generated by human work which has low efficiency and unstable accuracy. Because the defects on end surface of ferrite magnetic tile with dark colors and low contrasts are negative for defect detection, uniform illumination is provided by LED light source and a dedicated optical system is designed to extract defects conveniently. The approach uses comparison of the fitting and actual edge curves to detect defects mainly with most defects located on the edge. Firstly improved adaptive median filter is used as the image preprocessing. Subsequently the appropriate threshold is calculated by Otsu algorithm based on the extreme points in the gray-level histogram to segment the preprocessing image. Then the Sobel operator can be used to extract the edge of end surface precisely. Finally through comparing the ideal fitting and actual edge curves of end surface, to detect the defects with some relevant features. Experimental results show that the proposed scheme could detect defects on the end surface of ferrite magnetic tile efficiency and accurately with 93.33% accuracy rate, 2.30% false acceptance rate and 8.45% correct rejection rate.

  2. Evidence of domain wall pinning in aluminum substituted cobalt ferrites

    Science.gov (United States)

    Maurya, J. C.; Janrao, P. S.; Datar, A. A.; Kanhe, N. S.; Bhoraskar, S. V.; Mathe, V. L.

    2016-08-01

    In the present work spinel structured cobalt ferrites with aluminum substitution having composition CoAlxFe2-xO4 (x=0.0, 0.1, 0.2 and 0.3) have been synthesized using chemical co-precipitation method. Their microstructural, magnetic, magnetostriction and magnetoimpedance properties have been investigated. The piezomagnetic coefficient (dλ/dH) obtained from magnetostriction data is found to enhance with 0.1 Al substitutions in place of iron which decreases with further increase of Al content. It is noticed that 0.3 Al substitutions in place of Fe introduces domain wall pinning as evidenced from magnetostriction, magnetoimpedance and dc magnetization data. It is noted that ferrites so prepared using a simple procedure are magnetostrictive in good measure and with the addition of very small amount of non-magnetic aluminum their magnetostriction has shown saturation at relatively low magnetic fields. Such magnetostrictive ferrites find their applications in magnetic sensors and actuators.

  3. Characteristics of Magnetic Properties of Substituted Hexagonal Ferrites

    Directory of Open Access Journals (Sweden)

    Vladimir Jancarik

    2006-01-01

    Full Text Available The samples of barium hexaferrite BaFe12-2x(Me1Me2xO19 with x from 0.0 to 0.6 were prepared by variousmethods. The cationic preference of mainly divalent Me1 = Zn, Co, Ni, Sn ions and tetravalent Me2 = Ti, Zr, Ir, Sn, Ru ionsand their combinations in substituted Ba ferrites was investigated. The substitutions were performed to reduce the grain sizeand high magnetic uniaxial anisotropy field of the M-type Ba ferrite without affecting the magnetic polarisation. The goal isto reach the properties of ferrite proper for high-density magnetic recording and microwave absorption devices. Magneticproperties were determined as a function of the substitution level x. The specific saturation magnetic polarisation Js–m andremanence Js–rincreased with small x due to the substitution of non-magnetic and less magnetic ions in 4f1 and 4f2 sites. Thesteep decrease of coercivity Hc with increasing x may be caused by the Co2+ preference of 4f2 site and Ti4+or Zr4+ions preference of 2b and slightly in 4f1 sites. The temperature coefficient of the coercivity TKHc was very low (0.01kA.m-1.°C-1for the Co-Zr substitutions and positive for the rest of samples.

  4. Nanocrystalline spinel ferrites by solid state reaction route

    Indian Academy of Sciences (India)

    T K Kundu; S Mishra

    2008-06-01

    Nanostructured NiFe2O4, MnFe2O4 and (NiZn)Fe2O4 were synthesized by aliovalent ion doping using conventional solid-state reaction route. With the doping of Nb2O5, the size of NiFe2O4 is reduced down to 33 nm. Similarly, nanostructured manganese ferrites (MnFe2O4) with diameters in the range of 45–30 nm were synthesized by Ti4+ ion doping. Particle diameters in all the specimens are found to decrease with increasing dopant content. The substitution of Nb5+ or Ti3+ ions essentially breaks up the ferrimagnetically active oxygen polyhedra. This created nanoscale regions of ferrites. Saturation magnetization and coercive field show a strong dependence on the size of the ferrite grains. Superparamagnetic behaviour is observed from the Mössbauer spectra of nanostructured NiFe2O4, if the particle size is reduced to 30 nm. Zero field cooled and field cooled curves from 30 nm sized MnFe2O4 particles showed a peak at B (∼ 125 K), typical of superparamagnetic blocking temperature. These results are explained in terms of core/shell structure of the materials. The d.c. resistivity of the doped specimens decreases by atleast five orders of magnitude compared to pure sample. This is ascribed to the presence of an interfacial amorphous phase between the sites.

  5. Magnetic interactions in Cu-substituted manganese ferrites

    Science.gov (United States)

    Rana, Mazhar U.; Misbah-ul-Islam; Abbas, Tahir

    2003-04-01

    A series of Mn 1- xCu xFe 2O 4, with x=0, 0.25, 0.50, 0.75 and 1.0, spinel ferrites were prepared by standard ceramic method, to study the effect of compositional variation on magnetic susceptibility, saturation magnetization ( Ms), Curie temperature ( Tc) and magnetic moments ( μB). The Curie temperatures have been evaluated by measuring the ac susceptibility using the mutual inductance technique. On increasing Cu contents from 0.0 to 0.50, the saturation magnetization increases while the Curie temperature decreases. On further increase in Cu contents, x>0.50 a decreasing trend in Ms is exhibited while Tc continues to decrease. This effect can be partially related to the low magnetic moments of Cu +2 ions. The dominant interaction in all ferrite samples is A-B interaction which is due to the negative values of the characteristic temperature θ(K) showing that the magnetic ordering is antiferromagnetic. The Y-K angle increases gradually with increasing copper contents and extrapolates to 90° for CuFe 2O 4. From the computation of Y-K angles for Mn 1- xCu xFe 2O 4, it can be concluded that the mixed copper ferrites exhibit a non-collinearity of the Y-K type while MnFe 2O 4 shows a Neel type of ordering.

  6. A Ferrite LTCC-Based Monolithic SIW Phased Antenna Array

    KAUST Repository

    Nafe, Ahmed

    2016-11-17

    In this work, we present a novel configuration for realizing monolithic SIW-based phased antenna arrays using Ferrite LTCC technology. Unlike the current common schemes for realizing SIW phased arrays that rely on surface-mount component (p-i-n diodes, etc) for controlling the phase of the individual antenna elements, here the phase is tuned by biasing of the ferrite filling of the SIW. This approach eliminates the need for mounting of any additional RF components and enables seamless monolithic integration of phase shifters and antennas in SIW technology. As a proof of concept, a two-element slotted SIW-based phased array is designed, fabricated and measured. The prototype exhibits a gain of 4.9 dBi at 13.2 GHz and a maximum E-plane beam-scanning of 28 degrees using external windings for biasing the phase shifters. Moreover, the array can achieve a maximum beam-scanning of 19 degrees when biased with small windings that are embedded in the package. This demonstration marks the first time a fully monolithic SIW-based phased array is realized in Ferrite LTCC technology and paves the way for future larger-size implementations.

  7. Corrosion of an austenite and ferrite stainless steel weld

    Directory of Open Access Journals (Sweden)

    BRANIMIR N. GRGUR

    2011-07-01

    Full Text Available Dissimilar metal connections are prone to frequent failures. These failures are attributed to the difference in the mechanical properties across the weld, the coefficients of thermal expansion of the two types of steels and the resulting creep at the interface. For the weld analyzed in this research, it was shown that corrosion measurements can be used for a proper evaluation of the quality of weld material and for the prediction of whether or not the material, after the applied welding process, can be in service without failures. It was found that the corrosion of the weld analyzed in this research resulted from the simultaneous activity of different types of corrosion. In this study, electrochemical techniques including polarization and metallographic analysis were used to analyze the corrosion of a weld material of ferrite and austenitic stainless steels. Based on surface, chemical and electrochemical analyses, it was concluded that corrosion occurrence was the result of the simultaneous activity of contact corrosion (ferrite and austenitic material conjuction, stress corrosion (originating from deformed ferrite structure and inter-granular corrosion (due to chromium carbide precipitation. The value of corrosion potential of –0.53 V shows that this weld, after the thermal treatment, is not able to repassivate a protective oxide film.

  8. Lattice strain induced magnetism in substituted nanocrystalline cobalt ferrite

    Science.gov (United States)

    Kumar, Rajnish; Kar, Manoranjan

    2016-10-01

    Strontium (Sr) substituted cobalt ferrite i.e. Co1-xSrxFe2O4 (x=0.00, 0.01, 0.015, 0.02, 0.05, 0.1) have been synthesized by the citric acid modified sol-gel method. Crystal structure and phase purity have been studied by the X-ray powder diffraction technique. The Rietveld refinement of XRD pattern using the space group Fd 3 bar m shows monotonically increasing of lattice parameter with the increase in Sr concentration. Magnetic hysteresis loops measurement has been carried out at room temperature using a vibrating sample magnetometer (VSM) over a field range of ±1.5 T. Magnetocrystalline anisotropy constant were calculated by employing the Law of Approach (LA) to the saturation. It is observed that magnetocrystalline anisotropy has anomaly for x=0.01 (Co0.99Sr0.01Fe2O4) sample. Strain mediated modification of magnetic properties in Sr substituted cobalt ferrite has been observed. The saturation magnetization for doping concentration i.e. x=0.01 abruptly increase while for x>0.01 decreases with the increase in Sr concentration. A correlation between lattice strain and magnetic behavior in non-magnetic Sr- substituted nano-crystalline cobalt ferrite has been reported.

  9. Impedance spectroscopic characterization of gadolinium substituted cobalt ferrite ceramics

    Science.gov (United States)

    Rahman, Md. T.; Ramana, C. V.

    2014-10-01

    Gadolinium (Gd) substituted cobalt ferrites (CoFe2-xGdxO4, referred to CFGO) with variable Gd content (x = 0.0-0.4) have been synthesized by solid state ceramic method. The crystal structure and impedance properties of CFGO compounds have been evaluated. X-ray diffraction measurements indicate that CFGO crystallize in the inverse spinel phase. The CFGO compounds exhibit lattice expansion due to substitution of larger Gd ions into the crystal lattice. Impedance spectroscopy analysis was performed under a wide range of frequency (f = 20 Hz-1 MHz) and temperature (T = 303-573 K). Electrical properties of Gd incorporated Co ferrite ceramics are enhanced compared to pure CoFe2O4 due to the lattice distortion. Impedance spectroscopic analysis illustrates the variation of bulk grain and grain-boundary contributions towards the electrical resistance and capacitance of CFGO materials with temperature. A two-layer heterogeneous model consisting of moderately conducting grain interior (ferrite-phase) regions separated by insulating grain boundaries (resistive-phase) accurately account for the observed temperature and frequency dependent electrical characteristic of CFGO ceramics.

  10. Synthesis of Nanocrystalline Barium Ferrite in Ethanol/Water Media

    Institute of Scientific and Technical Information of China (English)

    M.Montazeri-Pour; A.Ataie

    2009-01-01

    Nanocrystalline particles of barium ferrite magnetic material have been prepared by co-precipitation route using aqueous and non-aqueous solutions of iron and barium chlorides with a Fe/Ba molar ratio of 11 and subsequent drying-annealing treatment. Water and ethanol/water mixture with volume ratio of 3:1 were used as solvents in the process. Coprecipitated powders were annealed at various temperatures for 1 h. FTIR (Fourier transform infrared spectroscopy), XRD (X-ray diffraction), DTA/TGA (differential thermal analy-sis/thermogravimetric analysis) and SEM (scanning electron microscopy) techniques were used to evaluate powder particle characteristics. DTA/TGA results confirmed by those obtained from XRD indicated that the formation of barium ferrite occurs in sample synthesized in ethanol/water solution at a relatively low temperature of 631℃. Nano-size particles of barium ferrite with mean particle size of almost 75 and 100 nm were observed in the SEM micrographs of the samples synthesized in ethanol/water solution after annealing at 700 and 800℃ for 1 h, respectively.

  11. Precipitation of Epsilon Copper in Ferrite Antibacterial Stainless Steel

    Institute of Scientific and Technical Information of China (English)

    Zhixia ZHANG; Gang LIN; Zhou XU

    2008-01-01

    The precipitation of epsilon copper at 1023 K ageing in ferrite antibacterial stainless steel was investigated by a combination of electron microscopy and micro-Vickers hardness measurement. The results show that epsilon copper precipitation occurs within 90 s. Complex rnultilayer structure confirmed as twins and stacking faults on {111}ε-Cu planes was observed in the precipitates. The precipitates grow by the lengthwise enlargement of a set of parallel layers, having [111]ε-Cu and [112]ε-Cu preferred growth orientations. The volume fraction of precipitates f formed within 120 min can be predicted by a modified Avrami equation (In 1/1-f= kt+b).Simultaneously, substituent atom clusters with a size of 5-10 nm was found to occur in the solution and cause matrix strain. The precipitate morphology and distribution on the surface of ferrite antibacterial stainlesss teel are associated with surface crystallographic orientation of the matrix. The precipitates are predominantly located within the ferrite grains of orientation. The precipitates located on {111}α-Fe surface planes have sphere or ellipse shape.

  12. Fatigue crack growth behaviors in hot-rolled low carbon steels: A comparison between ferrite-pearlite and ferrite-bainite microstructures

    Energy Technology Data Exchange (ETDEWEB)

    Guan, Mingfei [School of Materials Science and Engineering, University of Science and Technology Beijing, Beijing 100083 (China); Yu, Hao, E-mail: yhzhmr@126.com [School of Materials Science and Engineering, University of Science and Technology Beijing, Beijing 100083 (China)

    2013-01-01

    The roles of microstructure types in fatigue crack growth behaviors in ferrite-pearlite steel and ferrite-bainite steel were investigated. The ferrite-bainite dual-phase microstructure was obtained by intermediate heat treatment, conducted on ferrite-pearlite hot-rolled low carbon steel. This paper presents the results from investigation using constant stress-controlled fatigue tests with in-situ scanning electron microscopy (SEM), fatigue crack growth (FCG) rate tests, and fatigue fractography analysis. Microscopy images arrested by in-situ SEM showed that the fatigue crack propagation in F-P steel could become unstable more ealier compared with that in F-B steel. The fatigue cracks in ferrite-pearlite were more tortuous and could propagate more freely than that in ferrite-bainite microstructures. However, frequent crack branching were observed in ferrite-bainite steel and it indicated that the second hard bainite phase effectively retarded the crack propagation. The variation of FCG rate (da/dN) with stress intensity factor range ({Delta}K) for F-P and F-B steels was discussed within the Paris region. It was shown that FCG rate of F-P steel was higher than that of F-B steel. Moreover, the fatigue fracture surface analysis proved that grain boundaries could also play a role in the resistance of crack propagation.

  13. Long-term R and V-band monitoring of some suitable targets for the link between ICRF and the future Gaia celestial reference frame

    Science.gov (United States)

    Taris, F.; Andrei, A.; Roland, J.; Klotz, A.; Vachier, F.; Souchay, J.

    2016-03-01

    Context. The Gaia astrometric mission of the European Space Agency was launched on December 2013. It will provide a catalog of 500 000 quasars. Some of these targets will be chosen to build an optical reference system that will be linked to the International Celestial Reference Frame (ICRF). The astrometric coordinates of these sources will have roughly the same uncertainty at both optical and radio wavelengths, and it is then mandatory to observe a common set of targets to build the link. In the ICRF, some targets have been chosen because of their pointlikeness. They are quoted as defining sources, and they ensure very good uncertainty about their astrometric coordinates. At optical wavelengths, a comparable uncertainty could be achieved for targets that do not exhibit strong astrophysical phenomena, which is a potential source of photocenter flickering. A signature of these phenomena is a magnitude variation at optical wavelengths. Aims: The goal of this work is to present the time series of 14 targets suitable for the link between the ICRF and the future Gaia Celestial Reference Frame. The observations have been done systematically by robotic telescopes in France and Chile once every two nights since 2011 and in two filters. These time series are analyzed to search for periodic or quasi-periodic phenomena that must be taken into account when computing the uncertainty about the astrometric coordinates. Methods: Two independent methods were used in this work to analyze the time series. We used the CLEAN algorithm to compare the frequency obtained to those given by the Lomb-Scargle method. It avoids misinterpreting the frequency peaks given in the periodograms. Results: For the 14 targets we determine some periods with a confidence level above 90% in each case. Some of the periods found in this work were not previously known. For the others, we did a comparative study of the periods previously studied by others and always confirm their values. All the periods given

  14. Regulation mechanism of EM parameters in natural ferrite and its application in microwave absorbing materials

    Institute of Scientific and Technical Information of China (English)

    ZHENG; Yongchun; WANG; Shijie; FENG; Junming; LI; Chunlai; OUYANG; Ziyuan; LIU; Jianzhong; LI; Xiaobiao

    2006-01-01

    Electromagnetic (EM) parameters (ε', ε″,μ', μ″ ) of several M2+Fe2O4 and Fe2O3 type natural ferrites with different geological occurrences are measured in this paper. The measurement results show that EM parameters of a magmatic-occurring natural ferrite is very different from other types occurring from sedimentary-metamorphic iron deposit, hydrothermal vein iron deposit, outer contact of magmatic iron deposit. It has potential to be used as magnetic absorbent in microwave absorbing materials. After mineral separation and concentration, this magmatic-occurring natural ferrite was processed into type A ferrite absorbent. Type A natural ferrite absorbent is a kind of magnetic material with low dielectric constants, high magnetic conductivity and high EM loss. Its EM parameters areε' = 58.60, ε″ = 10.0, μ' = 1.2-1.5, μ″ = 1.0-1.2, respectively. In order to illuminate the regulation mechanism of EM parameters, we studied the chemical and mineral composition of type A ferrite absorbent. There is high concentration of natural impurities, which regulate the EM parameters of type A ferrite greatly. For comparison, the other types of natural ferrite, single-phase magnetite and two-phase iron minerals (ilmenite and magnetite), have few impurity. Thus regulation mechanism of EM parameters was absent in these ferrites. As a result, the regulation of EM parameters is advantageous to develop type A natural ferrite as excellent absorbent, lowers the reflectivity coefficients and enhances the absorbing efficiency of MAM made from it. Furthermore, the impurities in type A natural ferrite and its effects on EM parameters are very difficult to simulate in the synthesize ferrite. The carbonyl-iron powder is another kind of absorbent that is used extensively in MAM. To compare the absorbing properties of these two absorbent, type A natural ferrite and carbonyl-iron powder were mixed with rubber and processed into microwave absorbing sheets with the same procedures and

  15. Views of TAGSI on the effects of gamma irradiation on the mechanical properties of irradiated ferritic steel reactor pressure vessels

    Energy Technology Data Exchange (ETDEWEB)

    Knott, J.F. [School of Engineering, Metallurgy and Materials, University of Birmingham, Edgbaston, Birmingham B15 2TT (United Kingdom); English, C.A. [Materials and Chemistry Consultancy, Nexia Solutions, 168 Harwell International Business Centre, Didcot, Oxon OX11 0QJ (United Kingdom); Weaver, D.R. [School of Physics, University of Birmingham, Edgbaston, Birmingham B15 2TT (United Kingdom); Lidbury, D.P.G. [Serco Assurance, Walton House, 404 The Quadrant, Birchwood Park, Warrington, Cheshire WA3 6AT (United Kingdom)

    2005-12-01

    The paper reviews and analyses the effects of gamma irradiation dose on the properties of ferritic steels used in reactor pressure vessels (RPVs). It explains factors that affect the embrittlement of a RPV steel induced by combinations of fast neutrons, thermal neutrons, and gamma irradiation. TAGSI were asked to consider the effects of gamma irradiation dose on the properties of steels used in reactor pressure vessels. TAGSI endorsed the use of the MCBEND code to calculate gamma fluxes and energetic gamma ray displacement cross-sections calculated using either Baumann or Alexander methods. TAGSI endorsed the calculation of the materials property changes due to an additional gamma dose using trend curves based on empirical correlation to neutron-induced damage (where k {sub {gamma}}{approx}1{+-}0.25)

  16. Effect of long-term aging degradation on magnetic properties of ferritic 11Cr low- carbon steel

    Energy Technology Data Exchange (ETDEWEB)

    Kim, Chung Seok [Dept. of Metallurgical Material Engineering, Chosun University, Gwangju (Korea, Republic of); Ryu, Kwon Sang [KRISS, Daejeon (Korea, Republic of)

    2016-10-15

    The effect of long-term aging degradation on magnetic properties of ferritic 11Cr low-carbon steel was investigated. Coercivity and hysteresis loss measured from the hysteresis loops decreased with long-term aging time and showed that the relation was well fitted by a second order exponential function. Vickers hardness also decreased with aging time and resulted in mechanical softening. In addition, the microstructural evolution was observed by the scanning electron microscopy, backscattered electron image and X-ray diffraction. The Cr23C6 precipitates along grain boundary grew fast and Laves (Fe{sub 2}W) phase on martensitic lath boundaries in interior grains was developed. The solid solution atoms depleted in matrix and lath subgrains recovered owing to precipitate coarsening with long-term aging degradation. There was a close relation with softening of magnetic and mechanical properties.

  17. Thermal Diffusivity of Reduced Activation Ferritic/Martensitic Steel Determined by the Time Domain Photoacoustic Piezoelectric Technique

    Science.gov (United States)

    Zhao, Binxing; Wang, Yafei; Gao, Chunming; Sun, Qiming; Wang, Pinghuai

    2015-06-01

    The thermal diffusivity of reduced activation ferritic/martensitic steel (CLF-1), which is recognized as the primary candidate structural material for the test blanket module of the international thermal-nuclear experimental reactor, has been studied by the time-domain (TD) photoacoustic piezoelectric (PAPE) technique. The TD PAPE model based on a simplified thermoelastic theory under square-wave modulated laser excitation is presented, relating the TD PAPE signal to the modulation frequency, thermal diffusivity, and other material parameters. Thermal diffusivities of reference samples such as copper and nickel were measured and analyzed, by which the validity of the technique is verified. The thermal diffusivity of the CLF-1 sample was measured to be , which is at a medium level among the ordinary steel materials ( to and has decent heat-dissipation ability. The results show that the TD PAPE technique can provide a fast and economic way for the investigation of the thermophysical properties of fusion reactor structural materials.

  18. Copper ferrite nanoparticle-induced cytotoxicity and oxidative stress in human breast cancer MCF-7 cells.

    Science.gov (United States)

    Ahamed, Maqusood; Akhtar, Mohd Javed; Alhadlaq, Hisham A; Alshamsan, Aws

    2016-06-01

    Copper ferrite (CuFe2O4) nanoparticles (NPs) are important magnetic materials currently under research due to their applicability in nanomedicine. However, information concerning the biological interaction of copper ferrite NPs is largely lacking. In this study, we investigated the cellular response of copper ferrite NPs in human breast cancer (MCF-7) cells. Copper ferrite NPs were prepared by co-precipitation technique with the thermal effect. Prepared NPs were characterized by X-ray diffraction (XRD), field emission transmission electron microscopy (FETEM) and dynamic light scattering (DLS). Characterization data showed that copper ferrite NPs were crystalline, spherical with smooth surfaces and average diameter of 15nm. Biochemical studies showed that copper ferrite NPs induce cell viability reduction and membrane damage in MCF-7 cells and degree of induction was dose- and time-dependent. High SubG1 cell population during cell cycle progression and MMP loss with a concomitant up-regulation of caspase-3 and caspase-9 genes suggested that copper ferrite NP-induced cell death through mitochondrial pathway. Copper ferrite NP was also found to induce oxidative stress in MCF-7 cells as indicated by reactive oxygen species (ROS) generation and glutathione depletion. Cytotoxicity due to copper ferrite NPs exposure was effectively abrogated by N-acetyl-cysteine (ROS scavenger) suggesting that oxidative stress could be the plausible mechanism of copper ferrite NPs toxicity. Further studies are underway to explore the toxicity mechanisms of copper ferrite NPs in different types of human cells. This study warrants further generation of extensive biointeraction data before their application in nanomedicine.

  19. Steady state tests of high voltage ceramic feedthroughs and co-axial transmission line of ICRF heating system for the Large Helical Device

    Energy Technology Data Exchange (ETDEWEB)

    Mutoh, Takashi; Kumazawa, Ryuhei; Seki, Tetsuo; Simpo, Fujio; Nomura, Goro; Ido, Tsuyoshi; Watari, Tetsuo [National Inst. for Fusion Science, Toki, Gifu (Japan); Norterdaeme, J.M.

    1998-06-01

    Steady state ICRF heating technologies have been developed to heat plasma for more than 30 minutes in the LHD. Steady state operation tests of high voltage up to 40 kV{sub OP} for more than 30 minutes were carried out on the RF vacuum feedthroughs and the co-axial transmission line in the test set. Four types of ceramic feedthroughs each having a diameter of 240 mm were tested. The cone-type alumina ceramic and the cylinder-type silicon nitride composite-ceramic feedthroughs produced good performances of 40 kV/30 minutes and 50 kV/10 seconds. The others had vacuum leaks when subjected to a long pulse duration. The temperature of the cone-type alumina ceramic feedthrough was measured during the ICRF operations. By using gas-cooling techniques, the temperature increase of the ceramic was substantially reduced and saturated within 20 minutes. Without gas-cooling, the temperature increased linearly and did not saturated. So, this approach could not be used for steady state. The RF dissipation on the ceramic was calculated using the finite element computer code (ANSYS). It was found that damaged feedthroughs had local high heat spots, which could result in vacuum leaks. A water-cooled co-axial transmission line of 240 mm diameter was designed and tested. The specially designed connector components and Teflon insulator disks were tested. During the test, the insulation gases of nitrogen, sulfur hexafluoride and carbon dioxide were used to compare the capability of insulation for steady state. For the duration of a 10-second pulse, these gases performed well up to 60 kV{sub OP}. However, for steady state operation, carbon dioxide gas could not withstand voltages above 40 kV{sub OP}. The connector components of the transmission line performed without problems below 50 kV{sub OP} and 1 kA{sub OP} for a 30-minute operation. The performance of the feedthroughs and transmission line exceeded the specifications for steady state heating in the LHD. (J.P.N.)

  20. Magnetic ferrites synthesised using the microwave-hydrothermal method

    Energy Technology Data Exchange (ETDEWEB)

    Melo, R.S.; Silva, F.C.; Moura, K.R.M. [Department of Chemistry, Federal University of Maranhão, Campus of Bacanga, São Luís 65080-805 (Brazil); Menezes, A.S. de [Department of Physics, Federal University of Maranhão, Campus of Bacanga, São Luís 65080-805 (Brazil); Sinfrônio, F.S.M., E-mail: kjvida@mac.com [Department of Electrical Engineering, Federal University of Maranhão, Campus of Bacanga, São Luís 65080-805 (Brazil)

    2015-05-01

    Ceramic spinel-based ferrites of Cobalt, Nickel, Copper and Zinc were prepared using the hydrothermal method assisted with microwave. All samples were characterised using EDS, WDXRF, XRD, SEM, FTIR, Raman and VSM techniques. The structural, compositional, phonic and magnetic properties indicate that the evaluated method can produce magnetic materials. The EDS and WDXRF analyses suggest the materialisation of Co{sub 1.0}Fe{sub 2.0}O{sub 4}, Ni{sub 0.9}Fe{sub 2.1}O{sub 4}, Cu{sub 1.1}Fe{sub 1.9}O{sub 4} and Zn{sub 1.1}Fe{sub 1.9}O{sub 4} ferrites. XRD measurements indicate the formation of monophasic Cobalt, Nickel and Zinc cubic inverse-spinel-based structures, whereas Cooper ferrite was structured as body-centred tetragonal distorted inverse-spinel and cubic phase, which was contaminated with monoclinic CuO. The estimated average crystallite sizes using Rietveld refinement were approximately 163 nm (Co{sub 1.0}Fe{sub 2.0}O{sub 4}), 187 nm (Ni{sub 0.9}Fe{sub 2.1}O{sub 4}), 21 nm (Cu{sub 1.1}Fe{sub 1.9}O{sub 4}) and 226 nm (Zn{sub 1.1}Fe{sub 1.9}O{sub 4}). Infrared spectra exhibit characteristic modes at approximately 574–581 cm{sup −1} [ν(Co–O)]{sub Td}, 568–603 cm{sup −1} [ν(N–O)]{sub Td}, 607–661 cm{sup −1} [ν(Cu–O)]{sub Td} and 578–598 cm{sup −1} [ν(Zn–O)]{sub Td}. The Raman spectra for Co{sub 1.0}Fe{sub 2.0}O{sub 4} exhibit vibrational modes at 172 (T{sub 2g}), 304 (E{sub g}) 460 (A{sub 1g}) and 620–680 cm{sup −1} (A{sub 1g}), whereas Ni{sub 0.9}Fe{sub 2.1}O{sub 4} exhibits T{sub 2g} (477 cm{sup −1}) A{sub 1g} (690 cm{sup −1}) modes. Cu{sub 1.1}Fe{sub 1.9}O{sub 4} shows vibrational modes at approximately 148 (F{sub 2g}), 447 (F{sub 2g}), 552 (F{sub 2g}) and 671 cm{sup −1} (A{sub 1g}), and Zn{sub 1.1}Fe{sub 1.9}O{sub 4} has another four distinct modes at approximately 248, 348, 486 and 651, which are assigned to E{sub g}, T{sub 2g} and A{sub 1g} symmetries. Several obtained ferrites exhibit soft magnetisation with

  1. Low-temperature Spin Spray Deposited Ferrite/piezoelectric Thin Film Magnetoelectric Heterostructures with Strong Magnetoelectric Coupling

    Science.gov (United States)

    2014-01-08

    1ITLE AND SUBTITLE 5a CONTRACTNUMBER Low-temperature spin spray deposited ferrite /piezoelectric thin W911NF-09-l-0435 film magnetoelectric...ABSTRACT Low-temperature spin spray deposited ferrite /piezoelectric thin film magnetoelectric heterostructures with strong magnetoelectric coupling...energy dissipation, which can be readily integrated in different integrated circuits. Low-temperature spin spray deposited ferrite /pie Approved

  2. High permeability and low loss of Ni-Zn-Fe ferrite/metal composite cores in high frequency region

    Science.gov (United States)

    Mori, Satoshi; Mitsuoka, Takeshi; Sonehara, Makoto; Sato, Toshiro; Matsushita, Nobuhiro

    2017-05-01

    A Ni-Zn-Fe ferrite was deposited on the surface of Fe-Si and three kinds of Fe-Si-Cr powders as an insulating material using an ultrasonic-enhanced ferrite plating method. All ferrite-coated powders exhibited a high magnetization of about 180 emu/g derived from their soft magnetic metal and ferrite composition. The three different ferrite-coated Fe-Si-Cr cores annealed at 973 K exhibited a constant permeability μ' of 55-60 in the frequency range up to 50 MHz owing to the insulating effect of the ferrite layer. In contrast, the permeability μ' of the ferrite-coated Fe-3.5Si mass % core decreased in the MHz range. The Cr component acted as a passive layer that made it possible to maintain the Ni-Zn-Fe ferrite layer after annealing. The core loss of the ferrite-coated Fe-3.5Si-4.5Cr mass % core was 448 kW/m3 at 100 kHz and 50 mT, which was half of that observed for the Fe-3.5Si-4.5Cr core without ferrite layer. Additionally, the eddy-current loss of the ferrite-coated Fe-3.5Si-4.5Cr core was strongly decreased compared with the non-coated Fe-3.5Si-4.5Cr core owing to the insulating properties of the ferrite layer.

  3. FAST: FAST Analysis of Sequences Toolbox.

    Science.gov (United States)

    Lawrence, Travis J; Kauffman, Kyle T; Amrine, Katherine C H; Carper, Dana L; Lee, Raymond S; Becich, Peter J; Canales, Claudia J; Ardell, David H

    2015-01-01

    FAST (FAST Analysis of Sequences Toolbox) provides simple, powerful open source command-line tools to filter, transform, annotate and analyze biological sequence data. Modeled after the GNU (GNU's Not Unix) Textutils such as grep, cut, and tr, FAST tools such as fasgrep, fascut, and fastr make it easy to rapidly prototype expressive bioinformatic workflows in a compact and generic command vocabulary. Compact combinatorial encoding of data workflows with FAST commands can simplify the documentation and reproducibility of bioinformatic protocols, supporting better transparency in biological data science. Interface self-consistency and conformity with conventions of GNU, Matlab, Perl, BioPerl, R, and GenBank help make FAST easy and rewarding to learn. FAST automates numerical, taxonomic, and text-based sorting, selection and transformation of sequence records and alignment sites based on content, index ranges, descriptive tags, annotated features, and in-line calculated analytics, including composition and codon usage. Automated content- and feature-based extraction of sites and support for molecular population genetic statistics make FAST useful for molecular evolutionary analysis. FAST is portable, easy to install and secure thanks to the relative maturity of its Perl and BioPerl foundations, with stable releases posted to CPAN. Development as well as a publicly accessible Cookbook and Wiki are available on the FAST GitHub repository at https://github.com/tlawrence3/FAST. The default data exchange format in FAST is Multi-FastA (specifically, a restriction of BioPerl FastA format). Sanger and Illumina 1.8+ FastQ formatted files are also supported. FAST makes it easier for non-programmer biologists to interactively investigate and control biological data at the speed of thought.

  4. FAST: FAST Analysis of Sequences Toolbox

    Directory of Open Access Journals (Sweden)

    Travis J. Lawrence

    2015-05-01

    Full Text Available FAST (FAST Analysis of Sequences Toolbox provides simple, powerful open source command-line tools to filter, transform, annotate and analyze biological sequence data. Modeled after the GNU (GNU’s Not Unix Textutils such as grep, cut, and tr, FAST tools such as fasgrep, fascut, and fastr make it easy to rapidly prototype expressive bioinformatic workflows in a compact and generic command vocabulary. Compact combinatorial encoding of data workflows with FAST commands can simplify the documentation and reproducibility of bioinformatic protocols, supporting better transparency in biological data science. Interface self-consistency and conformity with conventions of GNU, Matlab, Perl, BioPerl, R and GenBank help make FAST easy and rewarding to learn. FAST automates numerical, taxonomic, and text-based sorting, selection and transformation of sequence records and alignment sites based on content, index ranges, descriptive tags, annotated features, and in-line calculated analytics, including composition and codon usage. Automated content- and feature-based extraction of sites and support for molecular population genetic statistics makes FAST useful for molecular evolutionary analysis. FAST is portable, easy to install and secure thanks to the relative maturity of its Perl and BioPerl foundations, with stable releases posted to CPAN. Development as well as a publicly accessible Cookbook and Wiki are available on the FAST GitHub repository at https://github.com/tlawrence3/FAST. The default data exchange format in FAST is Multi-FastA (specifically, a restriction of BioPerl FastA format. Sanger and Illumina 1.8+ FastQ formatted files are also supported. FAST makes it easier for non-programmer biologists to interactively investigate and control biological data at the speed of thought.

  5. Effect of O-vacancies on magnetic properties of bismuth ferrite nanoparticles by solution evaporation method

    Energy Technology Data Exchange (ETDEWEB)

    Afzal, A.M., E-mail: Amirafzal461@gmail.com [Department of Physics, GC University, Faisalabad 38000 (Pakistan); Umair, M., E-mail: umairranwerr@gmail.com [Department of Physics, GC University, Faisalabad 38000 (Pakistan); Dastgeer, G., E-mail: dtedastgeer@gmail.com [Department of Physics, University of Agriculture, Faisalabad 38000 (Pakistan); Rizwan, M., E-mail: h.rizwan70@gmail.com [Department of Physics, GC University, Faisalabad 38000 (Pakistan); Yaqoob, M.Z., E-mail: zeeshaan32@gmail.com [Department of Physics, GC University, Faisalabad 38000 (Pakistan); Rashid, R., E-mail: rashid.kanwar22@gmail.com [Department of Physics, University of Agriculture, Faisalabad 38000 (Pakistan); Munir, H.S., E-mail: sadiamunir.cute@gmail.com [Department of Physics, GC University, Faisalabad 38000 (Pakistan)

    2016-02-01

    Bismuth ferrite is a multiferroic material which shows high magnetization and polarization at room temperature. In present work, the effect of Oxygen (O) vacancies on magnetic properties of bismuth ferrite nanoparticles is studied. Bismuth ferrite nanoparticles (BiFeO{sub 3}) were synthesized by solution evaporation method (SEM) at room temperature. The sample was annealed under two different atmospheres such as in air and oxygen, to check the effect of O-vacancies on magnetic properties. The average crystallite size of Bismuth ferrite nanoparticles (NPs) as calculated by X-ray diffraction (XRD) falls in the range of 23–32 nm and 26–39 nm for the case of air and oxygen respectively. The crystallite size of bismuth ferrite nanoparticles increases as the temperature was varied from 450 °C to 650 °C. Further the influence of annealing temperature on the magnetic properties of the bismuth ferrite nanoparticles was also observed. It was concluded that the magnetic properties of Bismuth ferrite nanoparticles are directly interconnected to annealing atmosphere and annealing temperature. The magnetic properties were increased in the case of oxygen annealing, which actually leads in our case to an improvement of the crystallinity. - Highlights: • Bismuth ferrite was synthesized by solution evaporation method. • The effect of different annealing atmosphere on magnetic properties was studied. • The magnetic properties dramatically increased in case of Oxygen annealing. • The influence of crystalline size on magnetic properties was studied. • The magnetization was decreased as the temperature and crystallite size increased.

  6. Layer-by-Layer Self-Assembled Ferrite Multilayer Nanofilms for Microwave Absorption

    Directory of Open Access Journals (Sweden)

    Jiwoong Heo

    2015-01-01

    Full Text Available We demonstrate a simple method for fabricating multilayer thin films containing ferrite (Co0.5Zn0.5Fe2O4 nanoparticles, using layer-by-layer (LbL self-assembly. These films have microwave absorbing properties for possible radar absorbing and stealth applications. To demonstrate incorporation of inorganic ferrite nanoparticles into an electrostatic-interaction-based LbL self-assembly, we fabricated two types of films: (1 a blended three-component LbL film consisting of a sequential poly(acrylic acid/oleic acid-ferrite blend layer and a poly(allylamine hydrochloride layer and (2 a tetralayer LbL film consisting of sequential poly(diallyldimethylammonium chloride, poly(sodium-4-sulfonate, bPEI-ferrite, and poly(sodium-4-sulfonate layers. We compared surface morphologies, thicknesses, and packing density of the two types of ferrite multilayer film. Ferrite nanoparticles (Co0.5Zn0.5Fe2O4 were prepared via a coprecipitation method from an aqueous precursor solution. The structure and composition of the ferrite nanoparticles were characterized by X-ray diffraction, energy dispersive X-ray spectroscopy, transmission electron microscopy, and scanning electron microscopy. X-ray diffraction patterns of ferrite nanoparticles indicated a cubic spinel structure, and energy dispersive X-ray spectroscopy revealed their composition. Thickness growth and surface morphology were measured using a profilometer, atomic force microscope, and scanning electron microscope.

  7. Investigation on the effects of milling atmosphere on synthesis of barium ferrite/magnetite nanocomposite

    NARCIS (Netherlands)

    Molaei, M.J.; Ataie, A.; Raygan, S.; Picken,n S.J.

    2011-01-01

    In this research, barium ferrite /magnetite nanocomposites synthesized via a mechano-chemical route. Graphite was used in order to reduce hematite content of barium ferrite to magnetite to produce a magnetic nanocomposite. The effects of processing conditions on the powder characteristics were inves

  8. Antibacterial activity and characteristics of modified ferrite powder coated with a gemini pyridinium salt molecule.

    Science.gov (United States)

    Shirai, Akihiro; Maeda, Takuya; Ohkita, Motoaki; Nagamune, Hideaki; Kourai, Hiroki

    2007-09-01

    This report describes the synthesis of an antibacterial material consisting of a gemini quaternary ammonium salt (gemini-QUAT) immobilized on ferrite powder, and its antibacterial activity. A gemini-QUAT containing two pyridinium residues per molecule, 4,4'-[1,3-(2,2-dihydroxylmethyl-1,3-dithiapropane)]bis (1-octylpyridinium bromide), was immobilized on ferrite powder by a reaction between the hydroxyl group of the QUAT and trimethoxysilane. Immobilization of the gemini-QUAT on ferrite (F-gemini-QUAT) was confirmed when the dye, bromophenol blue, was released from F-gemini-QUAT-dye after contact between ferrite and the dye. Elemental analysis of the QUAT-ferrite determined the molar amount of QUAT on the ferrite. The antibacterial effect of the ferrite was investigated using a batch treatment system, and this effect was compared with that of another QUAT-ferrite (F-mono-QUAT) binding a mono-QUAT, which possesses one pyridinium residue, prepared by the same immobilization method as F-gemini-QUAT. Results indicated the F-gemini QUAT possessed a higher bactericidal potency and broader antibacterial spectrum compared to F-mono-QUAT. In addition, this study suggested that gemini-QUATs possessed high bactericidal potency without being influenced by immobilization to materials, and the antibacterial activity and characteristics of F-gemini-QUAT could be attributed to the unique structure of the immobilized gemini-QUAT.

  9. Predication of Plastic Flow Characteristics in Ferrite/Pearlite Steel Using a Fern Unit Cell Method

    Institute of Scientific and Technical Information of China (English)

    Hong Li; Jingtao Han; Jing Liu; Lv Zhang

    2004-01-01

    The flow stress of ferrite/pearlite steel under uni-axial tension was simulated with finite element method (FEM) by applying commercial software MARC/MENTAT. Flow stress curves of ferrite/pearlite steels were calculated based on unit cell model. The effects of volume fraction, distribution and the aspect ratio of pearlite on tensile properties have been investigated.

  10. 78 FR 63517 - Control of Ferrite Content in Stainless Steel Weld Metal

    Science.gov (United States)

    2013-10-24

    ... COMMISSION Control of Ferrite Content in Stainless Steel Weld Metal AGENCY: Nuclear Regulatory Commission... revision to Regulatory Guide (RG) 1.31, ``Control of Ferrite Content in Stainless Steel Weld Metal.'' This... content in stainless steel weld metal. It updates the guide to remove references to outdated standards...

  11. Effect of powder compaction on radiation-thermal synthesis of lithium-titanium ferrites

    Science.gov (United States)

    Surzhikov, A. P.; Lysenko, E. N.; Vlasov, V. A.; Malyshev, A. V.; Korobeynikov, M. V.; Mikhailenko, M. A.

    2017-01-01

    Effect of powder compaction on the efficiency of thermal and radiation-thermal synthesis of lithium-substituted ferrites was investigated by X-Ray diffraction and specific magnetization analysis. It was shown that the radiation-thermal heating of compacted powder reagents mixture leads to an increase in efficiency of lithium-titanium ferrites synthesis.

  12. Proeutectoid ferrite transformation in iron alloys. Tetsugokin no shoseki feraito hentai

    Energy Technology Data Exchange (ETDEWEB)

    Enomoto, M. (Ibaraki Univ., Ibaraki (Japan). Faculty of Engineering)

    1994-02-20

    This article is not a comprehensive introduction of proeutectoid ferrite transformation, but is an arrangement of the research trends on ferrite transformation prepared by the author from the basic viewpoint on ferrite transformation centering around topics which he was involved. Concerning proeutectoid ferrite transformation, only the mother phase and the final equilibrium phase concern in it and since data of thermodynamics, crystallography and diffusion are outstandingly better organized than other fields, it is considered to be the transformation suitable for comparing the nucleus forming theory with the measured nucleus forming rate. In this article, with regard to proeutectoid ferrite transformation, nucleus forming from a solid phase to a solid phase is discussed, and it is pointed out that activating energy of formation of ferrite nucleus differs noticeably between the edge and surface of the grain boundary, thereby a big difference is made in its nucleus forming rate. Furthermore, the following items are mentioned; diffusion rate determining growth in a ternary alloy and diffusion via a grain boundary of an alloying element, a study on ferrite growth utilizing the fact that the movement of ledges on the side face of ferrite can be observed in situ, incomplete transformation of alloying elements and synergetic effects, etc. 39 refs., 16 figs.

  13. High Frequency Characteristics Of Ferrite Materials And Applications To Microstrip Circuits

    OpenAIRE

    Moataza A. Hindy

    1999-01-01

    Dispersion behavior of the parameters of microstrip lines printed on ferrite substrate is presented. The characteristic impedance for lines on magnetized ferrite substrates are obtained for partially magnetized substrates in the direction of wave propagation and vertically magnetized substrates with variable DC magnetic field. The obtained results are applied to analyze variable phase shifters, controlled resonators, and impedance matching.

  14. Magnetic properties of cobalt ferrite-silica nanocomposites prepared by a sol-gel autocombustion technique

    DEFF Research Database (Denmark)

    Cannas, C.; Musinu, A.; Piccaluga, G.

    2006-01-01

    The magnetic properties of cobalt ferrite-silica nanocomposites with different concentrations (15, 30, and 50 wt %) and sizes (7, 16, and 28 nm) of ferrite particles have been studied by static magnetization measurements and Mossbauer spectroscopy. The results indicate a superparamagnetic behavio...

  15. Physical and Electromagnetic Properties of Customized Coatings for SNS Injection Ceramic Chambers and Extraction Ferrite Kickers

    CERN Document Server

    Hseuh Hsiao Chaun; He, Ping; Henderson, Stuart; Pai, Chien; Raparia, Deepak; Todd, Robert J; Wang, Lanfa; Wei, Jie; Weiss, Daniel; Yung Lee, Yong

    2005-01-01

    The inner surfaces of the 248 m SNS accumulator ring vacuum chambers are coated with ~100 nm of titanium nitride (TiN) to reduce the secondary electron yield (SEY) of the chamber walls. All the ring inner surfaces are made of stainless or inconel, except those of the injection and extraction kickers. Ceramic vacuum chambers are used for the 8 injection kickers to avoid shielding of a fast-changing kicker field and to reduce eddy current heating. The internal diameter was coated with Cu to reduce the beam coupling impedance and provide passage for beam image current, and a TiN overlayer to reduce SEY. The ferrite surfaces of the 14 extraction kicker modules were coated with TiN to reduce SEY. Customized masks were used to produce coating strips of 1 cm x 5 cm with 1 to 1.5 mm separation among the strips. The masks maximized the coated area to more than 80%, while minimizing the eddy current effect to the kicker rise time. The coating method, as well as the physical and electromagnetic properties of the coating...

  16. Comparison of hydrogen gas embrittlement of austenitic and ferritic stainless steels

    Science.gov (United States)

    Perng, T. P.; Altstetter, C. J.

    1987-01-01

    Hydrogen-induced slow crack growth (SCG) was compared in austenitic and ferritic stainless steels at 0 to 125 °Cand 11 to 216 kPa of hydrogen gas. No SCG was observed for AISI 310, while AISI 301 was more susceptible to hydrogen embrittlement and had higher cracking velocity than AL 29-4-2 under the same test conditions. The kinetics of crack propagation was modeled in terms of the hydrogen transport in these alloys. This is a function of temperature, microstructure, and stress state in the embrittlement region. The relatively high cracking velocity of AISI 301 was shown to be controlled by the fast transport of hydrogen through the stress-induced α' martensite at the crack tip and low escape rate of hydrogen through the γ phase in the surrounding region. Faster accumulation rates of hydrogen in the embrittlement region were expected for AISI 301, which led to higher cracking velocities. The mechanism of hydrogen-induced SCG was discussed based upon the concept of hydrogen-enhanced plasticity.

  17. Effect of processing parameters on the electrochemical performance of graphene/ nickel ferrite (G-NF nanocomposite

    Directory of Open Access Journals (Sweden)

    Elham Kamali Heidari

    2015-06-01

    Full Text Available Fuel cells, secondary batteries and capacitors are among many promising energy storage devices. In particular, supercapacitors have attracted much attention because of their long life cycle and high power density. Graphene/nickel ferrite(G-NF based supercapacitors were successfully fabricated through a one-step facile solvothermal route. Effects of synthesis conditions i.e. solvothermal time and temperature, on the powder particle characteristics were evaluated using x-ray photoelectron spectroscopy (XPS, powder x-ray diffraction (XRD and high-resolution transmission electron microscopy (HRTEM. Fast Fourier transformation (FFT patterns were also recorded on the HRTEM microscope to determine the lattice and crystallinity of the nanocomposites. Structural and chemical studies proved that increasing the solvothermal duration and temperature leads to improved crystallinity of NiFe2O4phase as well as higher degree of reduction of graphene oxide to graphene. The electrochemical measurements showed that solvothermal conditions of 180°C and 10h produces the highest specific capacity of 312 and 196 F g-1 at current densities of 1 and 5 A g-1, respectively calculated from charge-discharge test. This G-NF electrode material, also showed a capacity of 105 F g-1 after 1500 cycles at current density of 10 A g-1 which makes it an outstanding supercapacitor material with promising long cycle electrochemical stability and performance.

  18. Modification in the Microstructure of Mod. 9Cr-1Mo Ferritic Martensitic Steel Exposed to Sodium

    Science.gov (United States)

    Prasanthi, T. N.; Sudha, Cheruvathur; Paul, V. Thomas; Bharasi, N. Sivai; Saroja, S.; Vijayalakshmi, M.

    2014-09-01

    Mod. 9Cr-1Mo is used as the structural material in the steam generator circuit of liquid metal-cooled fast breeder reactors. Microstructural modifications on the surface of this steel are investigated after exposing to flowing sodium at a temperature of 798 K (525 °C) for 16000 hours. Sodium exposure results in the carburization of the ferritic steel up to a depth of ~218 µm from the surface. Electron microprobe analysis revealed the existence of two separate zones with appreciable difference in microchemistry within the carburized layer. Differences in the type, morphology, volume fraction, and microchemistry of the carbides present in the two zones are investigated using analytical transmission electron microscopy. Formation of separate zones within the carburized layer is understood as a combined effect of leaching, diffusion of the alloying elements, and thermal aging. Chromium concentration on the surface in the α-phase suggested possible degradation in the corrosion resistance of the steel. Further, concentration-dependent diffusivities for carbon are determined in the base material and carburized zones using Hall's and den Broeder's methods, respectively. These are given as inputs for simulating the concentration profiles for carbon using numerical computation technique based on finite difference method. Predicted thickness of the carburized zone agrees reasonably well with that of experiment.

  19. Precipitate phases in normalized and tempered ferritic/martensitic steel P92

    Science.gov (United States)

    Shen, Yinzhong; Liu, Huan; Shang, Zhongxia; Xu, Zhiqiang

    2015-10-01

    Ferritic/martensitic steel P92 is a promising candidate for cladding and duct applications in Sodium-Cooled Fast Reactor. The precipitate phases of the P92 steel normalized at 1323 K (1050 °C) for 30 min and tempered at 1038 K (765 °C) for 1 h have been investigated using transmission electron microscopes. Four types of phases consisting of M23C6, MX, M2X and sigma-FeCr were identified in the steel. MX phases consist of Nb-rich M(C,N) carbonitride, Nb-rich MC carbide, V-rich M(C,N) carbonitride, V-rich MC carbide, V-rich MN nitride, and complex MC carbides with Nb-rich MC core and V-rich MC wings. M2X phases consist of Cr-rich M2(C,N) carbonitride, Cr-rich M2C carbide and M2N nitride. Sigma-FeCr has a simple tetragonal lattice and a typical chemical formula of Fe0.45Cr0.45W0.1. M23C6 and MX are the dominant phases, while the sigma-FeCr has the lowest content. The formation of sigma-FeCr and M2X phases in the steel is also discussed.

  20. Electrical permittivity of Ni and NiZn ferrite-polymer composites

    Energy Technology Data Exchange (ETDEWEB)

    Razzitte, A.C. [Laboratorio de Fisicoquimica de Materiales Ceramicos Electronicos (LAFMACEL), Departamento de Quimica, Universidad de Buenos Aires, Paseo Colon 850, Capital Fedcral 1063, Buenos Aires (Argentina)]. E-mail: arazzit@fi.uba.ar; Fano, W.G. [Departamento de Electronica, Facultad.de Ingenieria, Universidad de Buenos Aires, Paseo Colon 850, Capital Fedcral 1063, Buenos Aires (Argentina); Jacobo, S.E. [Laboratorio de Fisicoquimica de Materiales Ceramicos Electronicos (LAFMACEL), Departamento de Quimica, Universidad de Buenos Aires, Paseo Colon 850, Capital Fedcral 1063, Buenos Aires (Argentina)

    2004-12-31

    Electrical properties of polymers, well known for their insulating properties, may be improved by adding various functional fillers. Polymer-ferrite composites have been a subject of recent extensive research. Electric properties of such composites depend on the size, shape and amount of added filler in general. When polymer-ferrite composites are particularly used as electromagnetic wave absorbers and EMI shielding materials, it is very important to explain the variation of permeability and permittivity in the measured frequency ranges. In this paper, acrylic-Ni ferrite composites and acrylic-NiZn ferrite composites were used. The effects of the weight fraction of ferrite on the frequency dispersion characteristics of the complex permittivity are studied.

  1. Negative and near zero refraction metamaterials based on permanent magnetic ferrites.

    Science.gov (United States)

    Bi, Ke; Guo, Yunsheng; Zhou, Ji; Dong, Guoyan; Zhao, Hongjie; Zhao, Qian; Xiao, Zongqi; Liu, Xiaoming; Lan, Chuwen

    2014-02-20

    Ferrite metamaterials based on the negative permeability of ferromagnetic resonance in ferrites are of great interest. However, such metamaterials face a limitation that the ferromagnetic resonance can only take place while an external magnetic field applied. Here, we demonstrate a metamaterial based on permanent magnetic ferrite which exhibits not only negative refraction but also near zero refraction without applied magnetic field. The wedge-shaped and slab-shaped structures of permanent magnetic ferrite-based metamaterials were prepared and the refraction properties were measured in a near-field scanning system. The negative and near zero refractive behaviors are confirmed by the measured spatial electric field maps. This work offers new opportunities for the development of ferrite-based metamaterials.

  2. Level Set-Based Topology Optimization for the Design of an Electromagnetic Cloak With Ferrite Material

    DEFF Research Database (Denmark)

    Otomori, Masaki; Yamada, Takayuki; Andkjær, Jacob Anders;

    2013-01-01

    This paper presents a structural optimization method for the design of an electromagnetic cloak made of ferrite material. Ferrite materials exhibit a frequency-dependent degree of permeability, due to a magnetic resonance phenomenon that can be altered by changing the magnitude of an externally...... applied dc magnetic field. Thus, such ferrite cloaks have the potential to provide novel functions, such as on-off operation in response to on-off application of an external magnetic field. The optimization problems are formulated to minimize the norm of the scattering field from a cylindrical obstacle....... A level set-based topology optimization method incorporating a fictitious interface energy is used to find optimized configurations of the ferrite material. The numerical results demonstrate that the optimization successfully found an appropriate ferrite configuration that functions as an electromagnetic...

  3. Modeling for Formation of Proeutectoid Ferrite in Steel during Continuous Cooling

    Institute of Scientific and Technical Information of China (English)

    YE Jian-song; CHANG Hong-bing; T Y Hsu(XU Zu-yao)

    2004-01-01

    A novel model of the evolution of microstructure during continuous cooling with the formation of proeutectoid ferrite in steel was proposed from a Voronoi construction for the austenite grains, based on the Rappaz′s integral nucleation model and the assumption that the ferrite nucleates at the edges of the original austenite grains and the successive growth of the ferrite grain is radial. The model can be used to calculate the fraction of ferrite as a function of time or temperature during continuous cooling, and to determine the microstructure of ferrite. The calculated results are in agreement with experimental results investigated in 0.38C-0.28Si-0.55Mn-0.92Cr-0.20Mo steel under continuous cooling using a Gleeble 1500 thermomechanical simulator.

  4. Automatic Ferrite Content Measurement based on Image Analysis and Pattern Classification

    Directory of Open Access Journals (Sweden)

    Hafiz Muhammad Tanveer

    2015-05-01

    Full Text Available The existing manual point counting technique for ferrite content measurement is a difficult time consuming method which has limited accuracy due to limited human perception and error induced by points on boundaries of grid spacing. In this paper, we present a novel algorithm, based on image analysis and pattern classification, to evaluate the volume fraction of ferrite in microstructure containing ferrite and austenite. The prime focus of the proposed algorithm is to solve the problem of ferrite content measurement using automatic binary classification approach. Classification of image data into two distinct classes, using optimum threshold finding method, is the key idea behind the new algorithm. Automation of the process to measure the ferrite content and to speed up specimen’s testing procedure is the main feature of the newly developed algorithm. Improved performance index by reducing error sources is reflected from obtained results and validated through the comparison with a well-known method of Ohtsu.

  5. Microstructure and magnetic performance of Ni-substituted high density MnZn ferrite

    Institute of Scientific and Technical Information of China (English)

    YU Zhong; LAN Zhongwen; CHEN Shengming; SUN Yueming; SUN Ke

    2006-01-01

    The effects of NiO on microstructure and magnetic properties of Mn-Zn ferrite with a nominal composition of Zn0.32Mn0.60-xNixFe2.08O4 were investigated. The calcined powder of Mn-Zn ferrite was characterized by X-ray diffraction (XRD), the fracture surface of Mn-Zn ferrite was checked by scanning electronic microscope (SEM), and then the magnetic properties were measured. As a result, the substitution of Ni can cause the crystallattice constant of MnZn ferrite to decline, and the grain size to decrease, therefore improve the magnetic performance of MnZn ferrite whose density exceeds 5.0 g·cm-3.

  6. Tensile and Impact Properties of Shielded Metal Arc Welded AISI 409M Ferritic Stainless Steel Joints

    Institute of Scientific and Technical Information of China (English)

    K.Shanmugam; A.K.Lakshminarayanan; V.Balasubramanian

    2009-01-01

    The present study is concerned with the effect of filler metals such as austenitic stainless steel, ferritic stainless steel and duplex stainless steel on tensile and impact properties of the ferritic stainless steel conforming to AISI 409M grade. Rolled plates of 4 mm thickness were used as the base material for preparing single pass butt welded joints. Tensile and impact properties, microhardness, microstructure and fracture surface morphology of the joints fabricated by austenitic stainless steel, ferritic stainless steel and duplex stainless steel filler metals were evaluated and the results were reported. From this investigation, it is found that the joints fabricated by duplex stainless steel filler metal showed higher tensile strength and hardness compared to the joints fabricated by austenitic and ferritic stainless steel filler metals. Joints fabricated by austenitic stainless steel filler metal exhibited higher ductility and impact toughness compared with the joints fabricated by ferritic stainless steel and duplex stainless steel filler metals.

  7. The recycling of Mn-Zn ferrite wastes through a hydrometallurgical route

    Energy Technology Data Exchange (ETDEWEB)

    Li, Kangkang [School of Metallurgical Science and Engineering, Central South University, Changsha 410083 (China); Peng, Changhong, E-mail: phc416@csu.edu.cn [School of Metallurgical Science and Engineering, Central South University, Changsha 410083 (China); Jiang, Kaiqi [School of Metallurgical Science and Engineering, Central South University, Changsha 410083 (China)

    2011-10-30

    Highlights: {yields} Mn-Zn ferrite wastes were recycled through wet chemical route. {yields} The Mn-Zn ferrite takes advantage over A102 made in Acme Electronics Corporation. {yields} The novel recycling technology attained environmental, social and economic benefits. - Abstract: A novel recycling route using acid leaching, reduction, purification, co-precipitation and traditional ceramic process was applied to process the Mn-Zn ferrite wastes and prepare the corresponding high permeability soft magnetic product. Above 95% of Fe, Mn, Zn in the waste materials could be recycled in the form of Mn-Zn ferrite products through the hydrometallurgical route. The comprehensive properties of Mn-Zn ferrite prepared from wastes by this route have broader frequency characteristics, higher resistivity, lower loss coefficient and temperature coefficient as compared to the A102 product (Acme Electronics Corporation, Taiwan). Moreover, the cost of this recycling technology has economical advantage over the traditional ceramic process, which holds a promising industrial application.

  8. Room temperature magnetism in zinc nano ferrite synthesized by a novel oxalate-ceramic method

    Energy Technology Data Exchange (ETDEWEB)

    Bhatt, Kapil K., E-mail: getdrkapil@yahoo.com [Department of Physics, Wilson College, Chowpatty, Mumbai 400 007 (India); Department of Physics and National Centre for Nanosciences and Nanotechnology, University of Mumbai, Santacruz (E), Mumbai 400 098 (India); Niwate, Yogesh S.; Garje, Shivram S. [Department of Chemistry, University of Mumbai, Santacruz (E), Mumbai 400 098 (India); Kothari, D.C. [Department of Physics and National Centre for Nanosciences and Nanotechnology, University of Mumbai, Santacruz (E), Mumbai 400 098 (India)

    2015-07-01

    Zinc nano-ferrite has been synthesized using a novel oxalate-ceramic method and its magnetic properties are reported in this paper. The hysteresis loop recorded at 300 K exhibits ferrimagnetic behavior. The Neel temperature was found to be 557 K. The AC susceptibility curve also indicates ferrimagnetic behavior. The temperature dependent magnetization curves, obtained in the temperature range of 4–300 K, show spin glass behavior. Using this method of synthesis large quantity of ferrite can be synthesized therefore this method can become useful technique for industrial scale production. - Highlights: • Oxalate-ceramic method is a novel technique to synthesize spinel ferrites. • Zinc ferrite synthesized by this technique are in nanocrystalline form with average crystallite size of 32 nm. • Neel temperature of zinc ferrite is found to be 557 K. • Different magnetic behavior in different temperature regime.

  9. Doxorubicin reduces the iron(III) complexes of the hydrolysis products of the antioxidant cardioprotective agent dexrazoxane (ICRF-187) and produces hydroxyl radicals.

    Science.gov (United States)

    Malisza, K L; Hasinoff, B B

    1995-02-01

    Dexrazoxane (ICRF-187) is very effective in protecting against doxorubicin-induced cardiotoxicity. Dexrazoxane likely acts though its metal ion binding hydrolysis product ADR-925 by reducing doxorubicin-promoted iron-based oxygen-free radical damage. In this study we show that doxorubicin and epirubicin (but not daunorubicin, idarubicin, or mitoxantrone) are able to reduce iron(III)-ADR-925 and under aerobic conditions are able to produce hydroxyl radicals that are detectable by EPR spin trapping. The ability of iron(III)-ADR-925 to produce hydroxyl radicals in the presence of anthraquinones is compared with that of other ferric chelates, including those of the one-ring open hydrolysis intermediates of dexrazoxane, the tetraacid derivative of ADR-925, EDTA, DTPA, and deferoxamine. The anthraquinones that lacked an alpha-ketol side chain (daunorubicin, idarubicin, and mitoxantrone) produced much less hydroxyl radical than those that did (doxorubicin and epirubicin). The model alpha-ketol, dihydroxyacetone, was also able to promote the formation of hydroxyl radicals in the presence of iron(III) chelates. Since dexrazoxane and doxorubicin are administered together, the possibility must be considered that anthracyclines with alpha-ketol side chains may be oxidized by iron(III)-ADR-925, thus changing their antitumor activity.

  10. Oxidative stress mediated apoptosis induced by nickel ferrite nanoparticles in cultured A549 cells.

    Science.gov (United States)

    Ahamed, Maqusood; Akhtar, Mohd Javed; Siddiqui, Maqsood A; Ahmad, Javed; Musarrat, Javed; Al-Khedhairy, Abdulaziz A; AlSalhi, Mohamad S; Alrokayan, Salman A

    2011-05-10

    Due to the interesting magnetic and electrical properties with good chemical and thermal stabilities, nickel ferrite nanoparticles are being utilized in many applications including magnetic resonance imaging, drug delivery and hyperthermia. Recent studies have shown that nickel ferrite nanoparticles produce cytotoxicity in mammalian cells. However, there is very limited information concerning the toxicity of nickel ferrite nanoparticles at the cellular and molecular level. The aim of this study was to investigate the cytotoxicity, oxidative stress and apoptosis induction by well-characterized nickel ferrite nanoparticles (size 26 nm) in human lung epithelial (A549) cells. Nickel ferrite nanoparticles induced dose-dependent cytotoxicity in A549 cells demonstrated by MTT, NRU and LDH assays. Nickel ferrite nanoparticles were also found to induce oxidative stress evidenced by generation of reactive oxygen species (ROS) and depletion of antioxidant glutathione (GSH). Further, co-treatment with the antioxidant L-ascorbic acid mitigated the ROS generation and GSH depletion due to nickel ferrite nanoparticles suggesting the potential mechanism of oxidative stress. Quantitative real-time PCR analysis demonstrated that following the exposure of A549 cells to nickel ferrite nanoparticles, the level of mRNA expressions of cell cycle checkpoint protein p53 and apoptotic proteins (bax, caspase-3 and caspase-9) were significantly up-regulated, whereas the expression of anti-apoptotic proteins (survivin and bcl-2) were down-regulated. Moreover, activities of caspase-3 and caspase-9 enzymes were also significantly higher in nickel ferrite nanoparticles exposed cells. To the best of our knowledge this is the first report showing that nickel ferrite nanoparticles induced apoptosis in A549 cells through ROS generation and oxidative stress via p53, survivin, bax/bcl-2 and caspase pathways.

  11. Numerical Study of Negative-Refractive Index Ferrite Waveguide

    Directory of Open Access Journals (Sweden)

    Mohammed O. Sid-Ahmed

    2012-03-01

    Full Text Available Consider a magnetized ferrite-wire waveguide structure situated between two half free spaces. Ferrites to provide negative permeability and wire array to provide negative permittivity. The structure form left-handed material (LHM with negative refractive index. The transmission of electromagnetic waves through the structure is investigated theoretically. Maxwell's equations are used to determine the electric and magnetic fields of the incident waves at each layer. Snell's law is applied and the boundary conditions are imposed at each layer interface to calculate the reflected and transmitted powers of the structure. Numerical results are illustrated to show the effect of frequency, applied magnetic fields, angle of incidence and LHM thickness on the mentioned powers. The analyzed results show that the transmission is very good when the permeability and permittivity of the structure are both simultaneously negative. The frequency band corresponding to this transmission can be tuned by changing the applied magnetic fields. The obtained results are in agreement with the law of conservation of energy. Consider a magnetized ferrite-wire waveguide structure situated between two half free spaces. Ferrites to provide negative permeability and wire array to provide negative permittivity. The structure form left-handed material (LHM with negative refractive index. The transmission of electromagnetic waves through the structure is investigated theoretically. Maxwell's equations are used to determine the electric and magnetic fields of the incident waves at each layer. Snell's law is applied and the boundary conditions are imposed at each layer interface to calculate the reflected and transmitted powers of the structure. Numerical results are illustrated to show the effect of frequency, applied magnetic fields, angle of incidence and LHM thickness on the mentioned powers. The analyzed results show that the transmission is very good when the permeability and

  12. Assessment of delta ferrite in multipass TIG welds of 40 mm thick SS 316L: A comparative study of ferrite number (FN) prediction and measurements

    Science.gov (United States)

    Buddu, Ramesh Kumar; Raole, P. M.; Sarkar, B.

    2017-04-01

    Austenitic stainless steels are widely used in the fabrication of fusion reactor major systems like vacuum vessel, divertor, cryostat and other structural components development. Multipass welding is used for the development of thick plates for the structural components fabrication. Due to the repeated weld thermal cycles, the microstructure adversely alters owing to the presence of complex phases like austenite, ferrite and delta ferrite and subsequently influences the mechanical properties like tensile and impact toughness of joints. The present paper reports the detail analysis of delta ferrite phase in welded region of 40 mm thick SS316L plates welded by special design multipass narrow groove TIG welding process under three different heat input conditions. The correlation of delta ferrite microstructure of different type structures acicular and vermicular is observed. The chemical composition of weld samples was used to predict the Ferrite Number (FN), which is representative form of delta ferrite in welds, with Schaeffler’s, WRC-1992 diagram and DeLong techniques by calculating the Creq and Nieq ratios and compared with experimental data of FN from Feritescope measurements. The low heat input conditions (1.67 kJ/mm) have produced higher FN (7.28), medium heat input (1.72 kJ/mm) shown FN (7.04) where as high heat input (1.87 kJ/mm) conditions has shown FN (6.68) decreasing trend and FN data is compared with the prediction methods.

  13. Exchange coupling between soft magnetic ferrite and hard ferromagnetic Sm2Fe17N3 in ferrite/Sm2Fe17N3 composites

    Directory of Open Access Journals (Sweden)

    N. Imaoka

    2016-05-01

    Full Text Available In our previous work, we succeeded in fabricating ferrite/Sm2Fe17N3 composite magnets from explosive-consolidating Sm2Fe17N3 powders (2μm size which were coated with a continuous iron ferrite layer (50nm thick in an aqueous solution. The magnetization curves had no inflection, which suggests that the soft magnetic ferrite layer is exchange-coupled with the hard ferromagnetic Sm2Fe17N3 particles. In this paper, we provide evidence of exchange coupling in ferrite/Sm2Fe17N3 composites by the following means: 1 measurements of recoil permeability, 2 detailed microstructural observation and 3 calculations of the reduction in remanence due to the introduction of a ferrite layer in the Sm2Fe17N3 magnets. Our ferrite/Sm2Fe17N3 composite magnets are a novel type of spring magnet in which an insulating soft magnetic phase is exchange-coupled with hard magnetic phase.

  14. Exchange coupling between soft magnetic ferrite and hard ferromagnetic Sm2Fe17N3 in ferrite/Sm2Fe17N3 composites

    Science.gov (United States)

    Imaoka, N.; Kakimoto, E.; Takagi, K.; Ozaki, K.; Tada, M.; Nakagawa, T.; Abe, M.

    2016-05-01

    In our previous work, we succeeded in fabricating ferrite/Sm2Fe17N3 composite magnets from explosive-consolidating Sm2Fe17N3 powders (2μm size) which were coated with a continuous iron ferrite layer (50nm thick) in an aqueous solution. The magnetization curves had no inflection, which suggests that the soft magnetic ferrite layer is exchange-coupled with the hard ferromagnetic Sm2Fe17N3 particles. In this paper, we provide evidence of exchange coupling in ferrite/Sm2Fe17N3 composites by the following means: 1) measurements of recoil permeability, 2) detailed microstructural observation and 3) calculations of the reduction in remanence due to the introduction of a ferrite layer in the Sm2Fe17N3 magnets. Our ferrite/Sm2Fe17N3 composite magnets are a novel type of spring magnet in which an insulating soft magnetic phase is exchange-coupled with hard magnetic phase.

  15. Latest progress of low temperature sintering ferrite powder%发展我国电子元件工业的思路

    Institute of Scientific and Technical Information of China (English)

    李盛涛; 李建英; 张伟强

    2001-01-01

    The progress of low temperature sintering ferrite powder are reviewed on the basis of the major projects under The State 863 Plan and the important theses of The 8th International Conference on Ferrite. NiCuZn ferrite, MgCuZn ferrite and hexagonal crystal system Co2Z ferrite prepared by solid phase reaction are presented. And the achievement of newly developed NicuZu ferrite and hexagonal crystal system Co2Z ferrite prepared by soft chemical technique are reported.(14 refs.)

  16. Synthesis and characterizations of manganese ferrites for hyperthermia applications

    Energy Technology Data Exchange (ETDEWEB)

    Doaga, A.; Cojocariu, A.M. [Faculty of Physics, Alexandru Ioan Cuza University, Bd. Carol I, Nr. 11, 700506 Iasi (Romania); Amin, W.; Heib, F. [Physical Chemistry, Universität des Saarlandes, 66123 Saarbrücken (Germany); Bender, P. [Experimental Physics, Universität des Saarlandes, 66123 Saarbrücken (Germany); Hempelmann, R. [Physical Chemistry, Universität des Saarlandes, 66123 Saarbrücken (Germany); Caltun, O.F., E-mail: caltun@uaic.ro [Faculty of Physics, Alexandru Ioan Cuza University, Bd. Carol I, Nr. 11, 700506 Iasi (Romania)

    2013-12-16

    In the last few years, magnetic nanoparticles have turned out to offer great potential in biomedical applications. This study was focused on Mn{sub x}Fe{sub 1−x}Fe{sub 2}O{sub 4} ferrite particles series with x ranging between 0 and 1. Manganese ferrites nanoparticles were prepared by co-precipitation method that allows a good control of their shape and size. The X-ray analysis indicated a crystallite size of the particles in the nanometers domain increasing with the Mn cation substitution level. Average grain size of the nanoparticles calculated from transmission electron microscopy images of the samples was ranging between 10.5 and 19.0 nm suggesting that the majority of the nanoparticles are monodomain. The hydrodynamic diameter of the water dispersed nanoparticles measured by dynamic light scattering was ranging between 60 and 105 nm proving the tendency of agglomeration. Vibrating sample magnetometer measurement confirmed the superparamagnetic behavior of the powders. The magnetic properties were analyzed considering the proposed cation distribution and Yafet–Kittel angles, while the specific absorption rate (SAR) measurement at 1.95 MHz frequency confirmed the influence of substitution level on magnetic properties and thermal transfer rate. From our results the highest value for specific absorption rate was 148.4 W g{sup −1} for Mn{sub 2}Fe{sub 2}O{sub 4} at an AC field of 4500 A m{sup −1}. - Highlights: • Mn{sub x}Fe{sub 1−x}Fe{sub 2}O{sub 4} nanoparticles (0 ≤ x ≤ 1) were synthesized by coprecipitation method. • The microstructure and average grain size of nanoparticles were determined from XRD and TEM. • The magnetic behavior was characterized using VSM and SAR. • The main results are discussed in terms of cation distribution and microstructure. • The Mn ferrite based ferrofluids can be used in medical application as hyperthermia.

  17. IR absorption spectroscopic study of mixed cobalt substituted lithium ferrites

    Energy Technology Data Exchange (ETDEWEB)

    Sawant, V.S.; Bagade, A.A.; Mohite, S.V.; Rajpure, K.Y., E-mail: rajpure@yahoo.com

    2014-10-15

    The IR spectra of Li{sub 0.5−(x/2)}Co{sub x}Fe{sub 2.5−(x/2)}O{sub 4} ferrite samples (0≤x≤0.6) prepared by solution combustion method have been reported. The influence of Co substitution is verified. XRD studies confirm the spinel phase formation of ferrites. Lattice constant varies linearly from 8.31 Å (x=0) to 8.35 Å (x=0.6) with composition. Evidence of two absorption bands in the IR spectra (below 800 cm{sup −1}) reveals the characteristic feature of spinel ferrite. The IR spectra featured additional three absorption bands around 550, 670 and 705 cm{sup −1} for the samples x=0.1 and x=0.6. Absence of bands splitting specifies that Fe ions do not exist in excess form. It is found that high frequency band (ν{sub 1}), due to tetrahedral (A) group, lies at around 600 cm{sup −1} and low frequency band (ν{sub 2}), due to octahedral (B) group, around 450 cm{sup −1}. The positions of bands are found to be composition dependent. The IR bands due to tetrahedral complexes shift slightly towards high frequency side with composition upto x=0.4 where as that due to octahedral complexes shift towards lower frequency side with x. Based on the data of absorption bands, force constants (k{sub t}, k{sub o}) and bond lengths (R{sub A}, R{sub B}) were estimated. Compositional dependence of force constants is explained on the basis of cation–oxygen bond distances of respective sites and cation distribution.

  18. Dielectric properties of nanocrystalline Co-Mg ferrites

    Energy Technology Data Exchange (ETDEWEB)

    Sharma, Jyoti, E-mail: jyotijoshi.phy2008@gmail.com [Department of Physics, University of Rajasthan, Jaipur (India); Sharma, Neha [Department of Physics, VEC Lakhanpur, Sarguja University, Ambikapur (C.G.) (India); Parashar, Jyoti; Saxena, V.K.; Bhatnagar, D. [Department of Physics, University of Rajasthan, Jaipur (India); Sharma, K.B. [Department of Physics, S. S. Jain Subodh P. G. College, Jaipur (India)

    2015-11-15

    Nanocrystalline powder samples with chemical formula Co{sub x}Mg{sub 1−x}Fe{sub 2}O{sub 4} (x = 0, 0.2, 0.4, 0.6, 0.8 and 1.0) have been synthesized by sol–gel auto combustion method using citric acid as fuel agent. The rietveld refinement study of x-ray diffraction patterns confirmed the spinel single phase formation for all samples. Dielectric constant (ε′), dielectric loss tangent (tan δ) and AC conductivity of Co{sub x}Mg{sub 1−x}Fe{sub 2}O{sub 4} ferrite nanoparticles have been measured at room temperature in the frequency range from 1000 Hz to 120 MHz. The dielectric dispersion observed at lower frequency region is attributed to Maxwell–Wagner two layer model, which is in agreement with Koops phenomenological theory. The observed results have been explained by polarization which is attributed to the electron exchange between Fe{sup 2+} and Fe{sup 3+} ions. The temperature variation of ε′ and tanδ for some particular frequencies were studied. The rapid increase in ε′ and tan δ has been explained using thermally activated electron exchange between Fe{sup 2+} ↔ Fe{sup 3+} and Co{sup 2+} ↔ Co{sup 3+} ions at adjacent octahedral sites. The role of interfacial polarization has been focused to explain the high dispersion in ε′ and tanδ with temperature observed at low frequencies. - Graphical abstract: (a) TEM image of Co{sub 0.4}Mg{sub 0.6}Fe{sub 2}O{sub 4} shows the nano size of the synthesized ferrite particles and (b) Dielectric constant behavior with frequency of Co{sub x}Mg{sub 1−x}Fe{sub 2}O{sub 4} ferrite.

  19. Structural elucidation and magnetic behavior evaluation of rare earth (La, Nd, Gd, Tb, Dy) doped BaCoNi-X hexagonal nano-sized ferrites

    Energy Technology Data Exchange (ETDEWEB)

    Majeed, Abdul, E-mail: abdulmajeed2276@gmail.com [Department of Physics, The Islamia University of Bahawalpur, Bahawalpur 63100 (Pakistan); Khan, Muhammad Azhar, E-mail: azhar.khan@iub.edu.pk [Department of Physics, The Islamia University of Bahawalpur, Bahawalpur 63100 (Pakistan); Raheem, Faseeh ur; Hussain, Altaf; Iqbal, F. [Department of Physics, The Islamia University of Bahawalpur, Bahawalpur 63100 (Pakistan); Murtaza, Ghulam [Centre for Advanced Studies in Physics, Government College University, Lahore 54000 (Pakistan); Akhtar, Majid Niaz [Department of Physics, COMSATS Institute of Information Technology, Lahore 54000 (Pakistan); Shakir, Imran [Deanship of Scientific Research, College of Engineering, King Saud University, PO Box 800, Riyadh 11421 (Saudi Arabia); Warsi, Muhammad Farooq [Department of Chemistry, The Islamia University of Bahawalpur, Bahawalpur 63100 (Pakistan)

    2016-06-15

    Rare-earth (RE=La{sup 3+}, Nd{sup 3+}, Gd{sup 3+}, Tb{sup 3+}, Dy{sup 3+}) doped Ba{sub 2}NiCoRE{sub x}Fe{sub 28−x}O{sub 46} (x=0.25) hexagonal ferrites were synthesized for the first time via micro-emulsion route, which is a fast chemistry route for obtaining nano-sized ferrite powders. These nanomaterials were investigated by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), as well as vibrating sample magnetometer (VSM). The XRD analysis exhibited that all the samples crystallized into single X-type hexagonal phase. The crystalline size calculated by Scherrer's formula was found in the range 7–19 nm. The variations in lattice parameters elucidated the incorporation of rare-earth cations in these nanomaterials. FTIR absorption spectra of these X-type ferrites were investigated in the wave number range 500–2400 cm{sup −1.} Each spectrum exhibited absorption bands in the low wave number range, thereby confirming the X-type hexagonal structure. The enhancement in the coercivity was observed with the doping of rare-earth cations. The saturation magnetization was lowered owing to the redistribution of rare-earth cations on the octahedral site (3b{sub VI}). The higher values of coercivity (664–926 Oe) of these nanomaterials suggest their use in longitudinal recording media. - Graphical abstract: Nano-sized rare-earth (RE=La{sup 3+}, Nd{sup 3+}, Gd{sup 3+}, Tb{sup 3+}, Dy{sup 3+}) doped Ba{sub 2}NiCoRE{sub x}Fe{sub 28−x}O{sub 46} (x=0.25) hexagonal ferrites were synthesized for the first time via micro-emulsion route and the crystallite size was found in the range 7–19 nm. The enhancement in the coercivity was observed with the doping of rare-earth cations. The higher values of coercivity (664–926 Oe) of these nanomaterials suggest their use in longitudinal recording media. - Highlights: • Micro-emulsion route was used to synthesize Ba{sub 2}NiCoRE{sub x}Fe{sub 28−x}O{sub 46} ferrites. • The crystallite size was found

  20. Investigation of surface magnetostatic wave propagation in ferrite superconductor structure

    CERN Document Server

    Semenov, A A; Melkov, A A; Bobyl', A V; Suris, R A; Gal'perin, Y M; Iokhansen, T K

    2001-01-01

    Electrodynamic model describing dispersion properties of surface magnetostatic wave in ferrite/superconductor structure was suggested. On the basis of the model a new method of ascertaining superhigh frequency surface resistance R sub s of superconducting films in magnetic fields was developed. The calculated values agree with the results obtained by the Tauber method, making up R sub s =0.20-1.96 m Ohm. A regulated incursion of wave phase amounting to about 1.5 pi with the change in penetration depth 2.0-0.8 mu m for YBCO film was attained for YIG/YBCO structures

  1. Advanced Microwave Ferrite Research (AMFeR): Phase Three

    Science.gov (United States)

    2008-07-31

    samples are kept in the high magnetic field for 48 hours, and then released and cured at room temperature for another 48 hours. Figure 3. Substrate...material source named target, such Au, Cu , or Ti. The substrate is placed in a vacuum chamber with the target and an inert gas, such as argon, is introduced...Propagation in Ferrite or polarization terms to Ampere’s law (as in the case of Debye Media [5], Lorentz [6] or plasma media [7]). By doing so, we never

  2. Microstructural change on electron irradiated oxide dispersion strengthened ferritic steels

    Science.gov (United States)

    Kinoshita, H.; Akasaka, N.; Takahashi, H.; Shibahara, I.; Onose, S.

    1992-09-01

    Oxide dispersion strengthened (ODS) ferritic steels were irradiated in a high voltage electron microscope (HVEM) to study their response to irradiation. Fe-13Cr with 0.25 wt% Y2O3 as dispersed particles and containing additions of either 0.45% Nb, 0.45% V and 0.67% Zr were irradiated at 673 and 723 K up to 15 dpa. The Y2O3 particles in all specimens were stable under these irradiation conditions. During irradiation, two types of dislocations were formed but observable voids were not formed. Furthermore, plate-like and granular-like precipitates formed in both the irradiated and nonirradiated regions.

  3. Size dependence of magnetorheological properties of cobalt ferrite ferrofluid

    Energy Technology Data Exchange (ETDEWEB)

    Radhika, B.; Sahoo, Rasmita; Srinath, S., E-mail: srinath@uohyd.ac.in [School of Physics, University of Hyderabad, Hyderabad-500040 (India)

    2015-06-24

    Cobalt Ferrite nanoparticles were synthesized using co-precipitation method at reaction temperatures of 40°C and 80°C. X-Ray diffraction studies confirm cubic phase formation. The average crystallite sizes were found to be ∼30nm and ∼48nm for 40°C sample and 80°C sample respectively. Magnetic properties measured using vibrating sample magnetometer show higher coercivety and magnetization for sample prepared at 80°C. Magnetorheological properties of CoFe2O4 ferrofluids were measured and studied.

  4. Room temperature texturing of austenite/ferrite steel by electropulsing

    Science.gov (United States)

    Rahnama, Alireza; Qin, Rongshan

    2017-01-01

    The work reports an experimental observation on crystal rotation in a duplex (austenite + ferrite) steel induced by the electropulsing treatment at ambient temperature, while the temperature rising due to ohmic heating in the treatment was negligible. The results demonstrate that electric current pulses are able to dissolve the initial material’s texture that has been formed in prior thermomechanical processing and to produce an alternative texture. The results were explained in terms of the instability of an interface under perturbation during pulsed electromigation. PMID:28195181

  5. Austenite and ferrite grain size evolution in plain carbon steel

    Energy Technology Data Exchange (ETDEWEB)

    Militzer, M.; Giumelli, A.; Hawbolt, E.B.; Meadowcroft, T.R. [British Columbia Univ., Vancouver, BC (Canada)

    1995-01-01

    Grain size evolution in a 0.17%C, 0.74%Mn plain carbon steel is investigated using a Gleeble 1500 thermomechanical simulator. Austenite grain growth measurements in the temperature range from 900 to 1150{degrees}C have been used to validate the Abbruzzese and Luecke model, which is recommended for simulating grain growth during reheating. For run-out table conditions, the ferrite grain size decreases from 1l{mu}m to 4{mu}m when the cooling rate from the austenite is increased from 1 to 80{degrees}C/s.

  6. Modeling the austenite decomposition into ferrite and bainite

    Science.gov (United States)

    Fazeli, Fateh

    2005-12-01

    Novel advanced high-strength steels such as dual-phase (DP) and transformation induced plasticity (TRIP) steels, are considered as promising materials for new generation of lightweight vehicles. The superior mechanical properties of these steels, compared to classical high strength steels, are associated with their complex microstructures. The desired phase configuration and morphology can only be achieved through well-controlled processing paths with rather tight processing windows. To implement such challenging processing stages into the current industrial facilities a significant amount of development efforts, in terms of mill trials, have to be performed. Alternatively, process models as predictive tools can be employed to aid the process development' and also to design new steel grades. Knowledge-based process models are developed by virtue of the underlying physical phenomena occurring during the industrial processing and are validated with experimental data. The goal of the present work is to develop an integrated microstructure model to adequately describe the kinetics of austenite decomposition into polygonal ferrite and bainite, such that for complex thermal paths simulating those of industrial practice, the final microstructure in advanced high strength steels can reasonably be predicted. This is in particular relevant to hot-rolled DP and TRIP steels, where the intercritical ferrite evolution due to its crucial influence on the onset and kinetics of the subsequent bainite formation, has to be quantified precisely. The calculated fraction, size and spatial carbon distribution of the intercritical austenite are employed as input to characterize adequately the kinetic of the bainite reaction. Pertinent to ferrite formation, a phenomenological, physically-based model was developed on the ground of the mixed-mode approach. The model deals with the growth stage since nucleation site saturation at prior austenite grain boundaries is likely to be attained

  7. Influence of high temperature pre-deformation on the dissolution rate of delta ferrites in martensitic heat-resistant steels

    Science.gov (United States)

    Li, Junru; Liu, Jianjun; Jiang, Bo; Zhang, Chaolei; Liu, Yazheng

    2017-03-01

    The dissolution process of delta ferrites and the influence of high temperature pre-deformation on the dissolution rate of delta ferrites in martensitic heat-resistant steel 10Cr12Ni3Mo2VN were studied by isothermal heating and thermal simulation experiments. The precipitation temperature of delta ferrites in experimental steel is about 1195 °C. M23C6-type carbides incline to precipitate and coarsen at the boundaries of delta ferrites below 930 °C, and can be rapidly dissolved by heating at 1180 °C. The percentage of delta ferrites gradually decreases with heating time. And a Kolmogorov-Johnson-Mehl-Avrami equation was established to describe the dissolution process of delta ferrites at 1180 °C. High temperature pre-deformation can markedly increase the dissolution rate of delta ferrites. Pre-deformation can largely increase the interface area between delta ferrite and matrix and thus increase the unit-time diffusing quantities of alloying elements between delta ferrites and matrix. In addition, high temperature pre-deformation leads to dynamic recrystallization and increases the number of internal grain boundaries in the delta ferrites. This can also greatly increase the diffusing rate of alloying elements. In these cases, the dissolution of delta ferrites can be promoted.

  8. Surface chemistry, friction, and wear of Ni-Zn and Mn-Zn ferrites in contact with metals

    Science.gov (United States)

    Miyoshi, K.; Buckley, D. H.

    1983-01-01

    X-ray photoelectron and Auger electron spectroscopy analysis were used in sliding friction experiments. These experiments were conducted with hot-pressed polycrystalline Ni-Zn and Mn-Zn ferrites, and single-crystal Mn-Zn ferrite in contact with various transition metals at room temperature in both vacuum and argon. The results indicate that Ni2O3 and Fe3O4 were present on the Ni-Zn ferrite surface in addition to the nominal bulk constituents, while MnO2 and Fe3O4 were present on the Mn-Zn ferrite surface in addition to the nominal bulk constituents. The coefficients of friction for the ferrites in contact with metals were related to the relative chemical activity of these metals. The more active the metal, the higher is the coefficient of friction. The coefficients of friction for the ferrites were correlated with the free energy of formation of the lowest metal oxide. The interfacial bond can be regarded as a chemical bond between the metal atoms and the oxygen anions in the ferrite surfaces. The adsorption of oxygen on clean metal and ferrite does strengthen the metal-ferrite contact and increase the friction. The ferrites exhibit local cracking and fracture with sliding under adhesive conditions. All the metals transferred to the surfaces of the ferrites in sliding. Previously announced in STAR as N83-19901

  9. Influence of particle size on the magnetic spectrum of NiCuZn ferrites for electromagnetic shielding applications

    Science.gov (United States)

    Wu, Xiaohan; Yan, Shuoqing; Liu, Weihu; Feng, Zekun; Chen, Yajie; Harris, Vincent G.

    2016-03-01

    The effect of ferrite particle size on the magnetic spectra (1 MHz to 1 GHz) of NiCuZn polycrystalline ferrites doped with Co2O3 and Bi2O3 were systematically investigated. The experiments indicate that the ferrite particle size tailored by grinding time and corresponding sintering temperatures is crucial to achieving high permeability, high Q-factor and low magnetic loss, at 13.56 MHz for electromagnetic shielding applications especially in the near field communication (NFC) field. It is evident that high-performance NiZnCu ferrite materials are strongly tailored by morphology and microstructure. It is conclusive that fine ferrite particles and relatively low sintering temperatures are favorable to lowering magnetic loss and enhancing permeability. This work has built a foundation for improvement of the ferrite slurry used for fabrication of large area tape-casting ferrite sheets.

  10. Mechanism of oxygen releasing of copper ferrite in the formation of the corresponding oxygen-deficient compound

    Institute of Scientific and Technical Information of China (English)

    ZHANG Ping; YU Bo; ZHANG Lei

    2009-01-01

    Copper ferrite is a promising material for hydrogen production through thermochemical water splitting. In this work, the cation distribution of copper ferrite and the corresponding oxygen-deficient compound of spinel structure was analyzed based on the crystal structural chemistry theory. The mechanism of oxygen releasing of CuO, Fe2O3, CuFe2O4 and metal (M=Ni, Mn or Zn) doped copper ferrite in the proc-ess of temperature rising was investigated by differential thermal analysis-thermogravimetry (DTA-TG). By combining the theoretical analysis with experimental results, the mechanism of oxygen releasing of copper ferrite is proposed, which is different from that of other ferrites. For copper ferrite, the oxygen releasing caused by Cu(Ⅱ)→Cu(I) plays a predominant role, while for other ferrites, the oxygen releas-ing resulting from Fe(ⅡI)→Fe(Ⅱ) is dominant.

  11. Mechanism of oxygen releasing of copper ferrite in the formation of the corresponding oxygen-deficient compound

    Institute of Scientific and Technical Information of China (English)

    2009-01-01

    Copper ferrite is a promising material for hydrogen production through thermochemical water splitting.In this work,the cation distribution of copper ferrite and the corresponding oxygen-deficient compound of spinel structure was analyzed based on the crystal structural chemistry theory.The mechanism of oxygen releasing of CuO,Fe2O3,CuFe2O4 and metal(M=Ni,Mn or Zn) doped copper ferrite in the proc-ess of temperature rising was investigated by differential thermal analysis-thermogravimetry(DTA-TG).By combining the theoretical analysis with experimental results,the mechanism of oxygen releasing of copper ferrite is proposed,which is different from that of other ferrites.For copper ferrite,the oxygen releasing caused by Cu(Ⅱ)→Cu(Ⅰ) plays a predominant role,while for other ferrites,the oxygen releas-ing resulting from Fe(Ⅲ)→Fe(Ⅱ) is dominant.

  12. Characterization and Modeling of Grain Boundary Chemistry Evolution in Ferritic Steels under Irradiation

    Energy Technology Data Exchange (ETDEWEB)

    Marquis, Emmanuelle [Univ. of Michigan, Ann Arbor, MI (United States); Wirth, Brian [Univ. of Tennessee, Knoxville, TN (United States); Was, Gary [Univ. of Michigan, Ann Arbor, MI (United States)

    2016-03-28

    Ferritic/martensitic (FM) steels such as HT-9, T-91 and NF12 with chromium concentrations in the range of 9-12 at.% Cr and high Cr ferritic steels (oxide dispersion strengthened steels with 12-18% Cr) are receiving increasing attention for advanced nuclear applications, e.g. cladding and duct materials for sodium fast reactors, pressure vessels in Generation IV reactors and first wall structures in fusion reactors, thanks to their advantages over austenitic alloys. Predicting the behavior of these alloys under radiation is an essential step towards the use of these alloys. Several radiation-induced phenomena need to be taken into account, including phase separation, solute clustering, and radiation-induced segregation or depletion (RIS) to point defect sinks. RIS at grain boundaries has raised significant interest because of its role in irradiation assisted stress corrosion cracking (IASCC) and corrosion of structural materials. Numerous observations of RIS have been reported on austenitic stainless steels where it is generally found that Cr depletes at grain boundaries, consistently with Cr atoms being oversized in the fcc Fe matrix. While FM and ferritic steels are also subject to RIS at grain boundaries, unlike austenitic steels, the behavior of Cr is less clear with significant scatter and no clear dependency on irradiation condition or alloy type. In addition to the lack of conclusive experimental evidence regarding RIS in F-M alloys, there have been relatively few efforts at modeling RIS behavior in these alloys. The need for predictability of materials behavior and mitigation routes for IASCC requires elucidating the origin of the variable Cr behavior. A systematic detailed high-resolution structural and chemical characterization approach was applied to ion-implanted and neutron-irradiated model Fe-Cr alloys containing from 3 to 18 at.% Cr. Atom probe tomography analyses of the microstructures revealed slight Cr clustering and segregation to dislocations and

  13. Microstructural evolution of delta ferrite in SAVE12 steel under heat treatment and short-term creep

    Energy Technology Data Exchange (ETDEWEB)

    Li, Shengzhi, E-mail: lishengzhi@sjtu.edu.cn [School of Materials Science and Engineering, Shanghai Jiao Tong University, Shanghai 200240 (China); Eliniyaz, Zumrat; Zhang, Lanting; Sun, Feng [School of Materials Science and Engineering, Shanghai Jiao Tong University, Shanghai 200240 (China); Shen, Yinzhong [School of Nuclear Science and Engineering, Shanghai Jiao Tong University, Shanghai 200240 (China); Shan, Aidang, E-mail: adshan@sjtu.edu.cn [School of Materials Science and Engineering, Shanghai Jiao Tong University, Shanghai 200240 (China)

    2012-11-15

    This research focused on the formation and microstructural evolution of delta ferrite phase in SAVE12 steel. The formation of delta ferrite was due to the high content of ferrite forming alloy elements such as Cr, W, and Ta. This was interpreted through either JMatPro-4.1 computer program or Cr{sub eq} calculations. Delta ferrite was found in bamboo-like shape and contained large amount of MX phase. It was surrounded by Laves phases before creep or aging treatment. Annealing treatments were performed under temperatures from 1050 Degree-Sign C to 1100 Degree-Sign C and various time periods to study its dissolution kinetics. The result showed that most of the delta ferrite can be dissolved by annealing in single phase austenitic region. Dissolution process of delta ferrite may largely depend on dissolution kinetic factors, rather than on thermodynamic factors. Precipitation behavior during short-term (1100 h) creep was investigated at temperature of 600 Degree-Sign C under a stress of 180 MPa. The results demonstrated that delta ferrite became preferential nucleation sites for Laves phase at the early stage of creep. Laves phase on the boundary around delta ferrite showed relatively slower growth and coarsening rate than that inside delta ferrite. - Highlights: Black-Right-Pointing-Pointer Delta ferrite is systematically studied under heat treatment and short-term creep. Black-Right-Pointing-Pointer Delta ferrite contains large number of MX phase and is surrounded by Laves phases before creep or aging treatment. Black-Right-Pointing-Pointer Formation of delta ferrite is interpreted by theoretical and empirical methods. Black-Right-Pointing-Pointer Most of the delta ferrite is dissolved by annealing in single phase austenitic region. Black-Right-Pointing-Pointer Delta ferrite becomes preferential nucleation sites for Laves phase at the early stage of creep.

  14. Chemical and physical characterizations of spinel ferrite nanoparticles containing Nd and B elements.

    Science.gov (United States)

    Iwamoto, Takashi; Komorida, Yuki; Mito, Masaki; Takahara, Atsushi

    2010-05-15

    We first succeeded in synthesizing ferrite nanoparticles containing Nd and B elements by a chemical route using a polyol process. The lattice constants of the ferrite nanoparticles were equivalent to 8.39Å of the lattice constant for Fe(3)O(4) with the spinel structure in a bulk state independently of the size in diameter and composition (Fe:Nd:B). The size in diameter was actually dominated by the amount of ligands (oleic acid and oleylamine) coating the nanoparticles and easily tuned by changing refluxing-time under reaction. The spinel-structured ferrite nanoparticles containing Nd and B elements showed large coercivity as compared to Fe(3)O(4) nanoparticles with the spinel structure, which were prepared by the same chemical method. By doping Nd and B elements into the spinel structure of ferrite, magnetic anisotropy increased in comparison with Fe(3)O(4) nanoparticles. According to the analysis of magnetization curve using the modified Langevin function, the ferrite nanoparticles displayed the coexistence of superparamagnetic and antiferromagnetic phases. The ferrite nanoparticles containing Nd and B elements exhibited magnetic core/shell structure on the basis of various magnetic properties. The interface effect between the superparamagnetic core and antiferromagnetic shell might enhance the effective magnetic anisotropy of the ferrite nanoparticles containing Nd and B elements.

  15. Effect of Niobium on Isothermal Transformation of Austenite to Ferrite in HSLA Low-Carbon Steel

    Institute of Scientific and Technical Information of China (English)

    CAO Jian-chun; LIU Qing-you; YONG Qi-long; SUN Xin-jun

    2007-01-01

    Using thermomechanical simulation experiment, the kinetics of the isothermal transformation of austenite to ferrite in two HSLA low-carbon steels containing different amounts of niobium was investigated under the conditions of both deformation and undeformation. The results of optical microstructure observation and quantitative metallography analysis showed that the kinetics of the isothermal transformation of austenite to ferrite in lower niobium steel with and without deformation suggests a stage mechanism, wherein there exists a linear relationship between the logarithms of holding time and ferrite volume fraction according to Avrami equation, whereas the isothermal transformation of austenite to ferrite in high niobium steel proceeds via a two stage mechanism according to micrographs, wherein, the nucleation rate of ferrite in the initial stage of transformation is low, and in the second stage,the rate of transformation is high and the transformation of residual austenite to ferrite is rapidly complete. Using carbon extraction replica TEM, niobium carbide precipitation for different holding time was investigated and the results suggested that NbC precipitation and the presence of solute niobium would influence the transformation of austenite to ferrite. The mechanism of the effect of niobium on the isothermal transformation was discussed.

  16. Effect of filler loading of nickel zinc ferrite on the tensile properties of PLA nanocomposites

    Science.gov (United States)

    Shahdan, Dalila; Ahmad, Sahrim Hj

    2013-05-01

    The mechanical strength of magnetic polymer nanocomposite (MPNC) of nickel zinc (NiZn) ferrite nanoparticles incorporated with polylactic acid (PLA) and liquid natural rubber (LNR) as compatibilizer is reported. The matrix was prepared from PLA and LNR in the ratio of 90:10. The MPNC were prepared at constant mixing temperature at 180°C, mixing time of 15 min. and mixing speed of 100 rpm. In order to achieve a good dispersion of NiZn ferrite in the matrix, firstly an ultrasonic treatment had been employed to mix the LNR and NiZn ferrite for 1 hour. The MPNC of PLA/LNR/NiZn ferrite then were prepared via Thermo Haake internal mixer using melt-blending method from different filler loading from 1-5 wt% NiZn ferrite. The result of tensile tests showed that as the filler loading increases the tensile strength also increases until an optimum value of filler loading was reached. The Young's modulus, tensile strength and elongation at break have also increased. The study proves that NiZn ferrite is excellent reinforcement filler in PLA matrix. Scanning electron micrograph (SEM) and energy dispersive X-ray spectroscopy (EDX) were meant to show the homogeneity dispersion of nanoparticles within the matrix and to confirm the elemental composition of NiZn ferrites-PLA/LNR nanocomposites respectively.

  17. Microstructural Dependence of Work Hardening Behavior in Martensite-Ferrite Microalloyed Steels

    Science.gov (United States)

    Anand, N.; Sankaran, S.; Madhavan, R.; Suwas, Satyam; Venugopal, P.

    2015-01-01

    Martensite-ferrite microstructures were produced in four microalloyed steels A (Fe-0.44C-Cr-V), B (Fe-0.26C-Cr-V), C (Fe-0.34C-Cr-Ti-V), and D (Fe-0.23C-Cr-V) by intercritical annealing. SEM analysis reveals that steels A and C contained higher martensite fraction and finer ferrite when compared to steels B and D which contained coarser ferrite grains and lower martensite fraction. A network of martensite phase surrounding the ferrite grains was found in all the steels. Crystallographic texture was very weak in these steels as indicated by EBSD analysis. The steels contained negligible volume fraction of retained austenite (approx. 3-6%). TEM analysis revealed the presence of twinned and lath martensite in these steels along with ferrite. Precipitates (carbides and nitrides) of Ti and V of various shapes with few nanometers size were found, particularly in the microstructures of steel B. Work hardening behavior of these steels at ambient temperature was evaluated through modified Jaoul-Crussard analysis, and it was characterized by two stages due to presence of martensite and ferrite phases in their microstructure. Steel A displayed large work hardening among other steel compositions. Work hardening behavior of the steels at a warm working temperature of 540 °C was characterized by a single stage due to the decomposition of martensite into ferrite and carbides at this temperature as indicated by SEM images of the steels after warm deformation.

  18. Temperature dependence of core loss in cobalt substituted Ni-Zn-Cu ferrites

    Energy Technology Data Exchange (ETDEWEB)

    Lucas, A., E-mail: ant50_lucas@yahoo.f [THALES R and T, Campus Polytechnique, 1 Avenue Augustin Fresnel, 91767 Palaiseau (France); SATIE, ENS de Cachan, 61 Avenue du President Wilson, 94235 Cachan (France); Lebourgeois, R. [THALES R and T, Campus Polytechnique, 1 Avenue Augustin Fresnel, 91767 Palaiseau (France); Mazaleyrat, F. [SATIE, ENS de Cachan, 61 Avenue du President Wilson, 94235 Cachan (France); Laboure, E. [SATIE, ENS de Cachan, 61 Avenue du President Wilson, 94235 Cachan (France); LGEP, SUPELEC, Plateau de Moulon, 11 rue Joliot-Curie, 91192 Gif Sur Yvette (France)

    2011-03-15

    The temperature dependence of core loss in cobalt substituted Ni-Zn-Cu ferrites was investigated. Co{sup 2+} ions are known to lead to a compensation of the magneto-crystalline anisotropy in Ni-Zn ferrites, at a temperature depending on the cobalt content and the Ni/Zn ratio. We observed similar behaviour in Ni-Zn-Cu and it was found that the core loss goes through a minimum around this magneto-crystalline anisotropy compensation. Moreover, the anisotropy induced by the cobalt allowed a strong decrease of core loss, a ferrite having a core loss of 350 mW/cm{sup 3} at 80 {sup o}C was then developed (measured at 1.5 MHz and 25 mT). This result represents an improvement of a factor 4 compared to the state of art Ni-Zn ferrites. - Research highlights: > Low temperature sintering ferrite. > Improvement of the core loss of high frequency ferrites. > Power ferrites working at high temperature.

  19. Synthesis of nonstoichiometric M-type barium ferrite nanobelt by spark plasma sintering method

    Institute of Scientific and Technical Information of China (English)

    ZHAO Wenyu; ZHANG Qingjie; TANG Xinfeng; CHENG Haibin

    2005-01-01

    This study investigated the feasibility of ultrafast crystallization of M-type barium ferrite when the coprecipitation precursors in stoichiometric proportions as BaFe12O19, Fe(OH)3 and BaCO3 nanoparticles, had been heated by spark plasma sintering (SPS) process. The results show that SPS method may realize the ultrafast crystallization of M-type barium ferrite, absolutely prevent the crystallization of intermediate phase α-Fe2O3, and significantly decrease the crystallization temperature of M-type barium ferrite. The sintered samples obtained at 800℃ by sintering the precursors for 10 minutes are a kind of multiphase ferrites composed of major phase M-type barium ferrite and trace amount of BaFe0.24Fe0.76O2.88. It is discovered that M-type barium ferrites in the holes of the sintered samples are in nanobelt microstructure about 100-300 nm in width and several micrometers in length. These M-type barium ferrite nanobelts are non-stoichiometric and may be expressed as BaFe12+Xo19+1.5x (-4.77≤x≤6.50). Their composistions suggest completely random Fe-rich or Ba-rich domains.

  20. Tailoring the temperature characteristics of the magnetic permeability of NiZn ferrites

    Energy Technology Data Exchange (ETDEWEB)

    Tsakaloudi, V., E-mail: vikaki@cperi.certh.g [Center for Research and Technology-Hellas, Chemical Process Engineering Research Institute, Laboratory of Inorganic Materials, P.O. Box 60361, 57001 Thessaloniki (Greece); Zaspalis, V.T. [Center for Research and Technology-Hellas, Chemical Process Engineering Research Institute, Laboratory of Inorganic Materials, P.O. Box 60361, 57001 Thessaloniki (Greece)

    2010-03-15

    The effect of cobalt addition on the temperature characteristics of the magnetic permeability of NiZn ferrites was studied and a comparison to the respective behaviour of cobalt in NiCuZn ferrites was examined. Cobalt-doped NiZn and NiCuZn ferrites were manufactured by the ceramic route and sintered under various atmosphere profiles. The chemical and morphological characteristics were evaluated by X-ray diffraction (XRD), scanning electron microscopy (SEM) and thermogravimetric analysis (TGA). The evaluation of the magnetic performance of the sintered ferrites showed that N{sub 2}-rich atmosphere profiles during the top temperature and cooling time of the sintering process favour the temperature stability of the permeability in the case of NiZn ferrites, while preserving the losses at low levels. Two mechanisms that take place at the same time are proposed: the change of the Fe{sup 2+}/Fe{sup 3+} ratio due to the reduction-promoting atmosphere of N{sub 2} in combination with an increase in magnetocrystalline anisotropy and magnetostriction due to the presence of Co{sup 2+} suggest a useful method to tailor the temperature factor alpha{sub F} of NiZn ferrites. However, the method cannot be applied in NiCuZn ferrites, as the reduction Cu{sup 2+}-Cu{sup +} taking place under N{sub 2}-rich atmospheres enhances secondary re-crystallization phenomena, causing a dramatic increase in losses.