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Sample records for electron microprobe idades

  1. Electron Microprobe

    Data.gov (United States)

    Federal Laboratory Consortium — The JEOL JXA-8600 is a conventional hairpin filament thermal emission electron microprobe that is more than 20 years old. It is capable of performing qualitative and...

  2. Automated electron microprobe

    International Nuclear Information System (INIS)

    Thompson, K.A.; Walker, L.R.

    1986-01-01

    The Plant Laboratory at the Oak Ridge Y-12 Plant has recently obtained a Cameca MBX electron microprobe with a Tracor Northern TN5500 automation system. This allows full stage and spectrometer automation and digital beam control. The capabilities of the system include qualitative and quantitative elemental microanalysis for all elements above and including boron in atomic number, high- and low-magnification imaging and processing, elemental mapping and enhancement, and particle size, shape, and composition analyses. Very low magnification, quantitative elemental mapping using stage control (which is of particular interest) has been accomplished along with automated size, shape, and composition analysis over a large relative area

  3. Beam electron microprobe

    CERN Document Server

    Stoller, D; Muterspaugh, M W; Pollock, R E

    1999-01-01

    A beam profile monitor based on the deflection of a probe electron beam by the electric field of a stored, electron-cooled proton beam is described and first results are presented. Electrons were transported parallel to the proton beam by a uniform longitudinal magnetic field. The probe beam may be slowly scanned across the stored beam to determine its intensity, position, and size. Alternatively, it may be scanned rapidly over a narrow range within the interior of the stored beam for continuous observation of the changing central density during cooling. Examples of a two dimensional charge density profile obtained from a raster scan and of a cooling alignment study illustrate the scope of measurements made possible by this device.

  4. Electron microprobe analysis of tantalum--nitride thin films

    International Nuclear Information System (INIS)

    Stoltz, D.L.; Starkey, J.P.

    1979-06-01

    Quantitative chemical analysis of 500- and 2000-angstrom tantalum--nitride films on glass substrates has been accomplished using an electron microprobe x-ray analyzer. In order to achieve this analysis, modifications to the microprobe were necessary. A description of the calibration procedure, the method of analysis, and the quantitative results are discussed

  5. New electron microprobe for radioactive materials

    International Nuclear Information System (INIS)

    Perrot, M.; Geoffroy, G.; Trotabas, M.

    1989-01-01

    The latest model of CAMECA microprobe SX 50R has just been set up in the high activity laboratory of the Centre d'Etudes Nucleaires de SACLAY. It has been especially designed for the examination of nuclear fuel and irradiated materials. The spectrometers are protected from the radioactivity by an armour plate and the entire equipment has been installed into a special cell in order to protect the operators. The special sample holder allows to examine specimens as large as 80 mm in diameter. One of the interesting uses concerns the quantitative determination of the oxygen content in zircaloy oxidized by steam at high temperature. This analysis was made possible by using the new type of crystals (multilayer)

  6. Cryosystem for cathodoluminescence investigations by means of electron microprobe analysis

    International Nuclear Information System (INIS)

    Schreiber, J.

    1982-01-01

    A cryosystem is presented which has been designed as auxiliary equipment for electron beam microprobes used in cathodoluminescence studies. The sample holder temperature is adjustable down to 66 K with an accuracy of 0.5 K. Finally, experimental results (transmission spectra and cathodoluminescence spectra of N-doped GaP epitaxial layers at 80 K; changes in microscopic cathodoluminescence distribution at small angle grain boundaries at the (0001) plane of CdS during temperature decrease from 300 to 80 K) obtained by means of the described measuring equipment are given for illustration

  7. False colour backscatter electron images and their application during electron microprobe analysis of ores and host rocks

    International Nuclear Information System (INIS)

    Cousens, D.R.; French, D.H.; Ramsden, A.R.

    1989-01-01

    The limited contrast range of conventional black and white imaging does not enable full use to be made of the dynamic range of the video signal obtained from a scanning electron microscope or microprobe. The use of false colour substantially increases the information that can be derived from such images enabling relationships to be displayed that cannot be observed in black and white. This capability is now used extensively in combination with quantitative electron microprobe analysis as a research tool for ore characterization and host rocks studies related to minerals exploration in the CSIRO Div.sion of Exploration Geoscience. Thus the CAMEBAX scanning electron microprobe has been modified to allow digital images acquisition and software (IMAGE) developed which allows false colour backscatter electron (BSE) images to be obtained during the course of routine electron microprobe analysis. 1 fig

  8. Core Community Specifications for Electron Microprobe Operating Systems: Software, Quality Control, and Data Management Issues

    Science.gov (United States)

    Fournelle, John; Carpenter, Paul

    2006-01-01

    Modem electron microprobe systems have become increasingly sophisticated. These systems utilize either UNIX or PC computer systems for measurement, automation, and data reduction. These systems have undergone major improvements in processing, storage, display, and communications, due to increased capabilities of hardware and software. Instrument specifications are typically utilized at the time of purchase and concentrate on hardware performance. The microanalysis community includes analysts, researchers, software developers, and manufacturers, who could benefit from exchange of ideas and the ultimate development of core community specifications (CCS) for hardware and software components of microprobe instrumentation and operating systems.

  9. A photomultiplier-based secondary electron imaging system for a nuclear microprobe

    International Nuclear Information System (INIS)

    Alves, L.C.; Breese, M.B.H.; Silva, M.F. da; Soares, J.C.

    2002-01-01

    The ability to define, or recognise particular regions of interest or surface features is vital to the analysis and interpretation of spatially-resolved images collected with a nuclear microprobe. However, good topographic image contrast is difficult to accomplish using PIXE or RBS images due to their inherent insensitivity to topography, lack of elemental variation or poor statistics. Topographic image contrast is commonly obtained in scanning electron microscopy (SEM) by detecting a large flux of secondary electrons produced by the focused keV electron beam. Similar systems have not been widely used on nuclear microprobes due to ion beam intensity fluctuations, which limit the minimum resolvable contrast and present a major limitation for this technique. This paper describes a secondary electron imaging system which has been developed on the Lisbon microprobe. It is based on a scintillator, a photomultiplier operated in a pulsed mode, a pulse shaping electronic chain and ADC, and requires no changes to the existing data acquisition system. Examples of the images obtained from materials such as patterned SiGe wafers and hydrogen-implanted silicon are given, and compared with SEM or optical images

  10. Color electron microprobe cathodoluminescence of Bishunpur meteorite compared with the traditional optical microscopy method

    Directory of Open Access Journals (Sweden)

    Amanda Araujo Tosi

    Full Text Available Abstract Cathodoluminescence (CL imaging is an outstanding method for sub classification of Unequilibrated Ordinary Chondrites (UOC - petrological type 3. CL can be obtained by several electron beam apparatuses. The traditional method uses an electron gun coupled to an optical microscope (OM. Although many scanning electron microscopes (SEM and electron microprobes (EPMA have been equipped with a cathodoluminescence, this technique was not fully explored. Images obtained by the two methods differ due to a different kind of signal acquisition. While in the CL-OM optical photography true colors are obtained, in the CL-EPMA the results are grayscale monochromatic electronic signals. L-RGB filters were used in the CL-EPMA analysis in order to obtain color data. The aim of this work is to compare cathodoluminescence data obtained from both techniques, optical microscope and electron microprobe, on the Bishunpur meteorite classified as LL 3.1 chondrite. The present study allows concluding that 20 KeV and 7 nA is the best analytical condition at EPMA in order to test the equivalence between CL-EPMA and CL-OM colour results. Moreover, the color index revealed to be a method for aiding the study of the thermal metamorphism, but it is not definitive for the meteorite classification.

  11. $ANBA; a rapid, combined data acquisition and correction program for the SEMQ electron microprobe

    Science.gov (United States)

    McGee, James J.

    1983-01-01

    $ANBA is a program developed for rapid data acquisition and correction on an automated SEMQ electron microprobe. The program provides increased analytical speed and reduced disk read/write operations compared with the manufacturer's software, resulting in a doubling of analytical throughput. In addition, the program provides enhanced analytical features such as averaging, rapid and compact data storage, and on-line plotting. The program is described with design philosophy, flow charts, variable names, a complete program listing, and system requirements. A complete operating example and notes to assist in running the program are included.

  12. Applications of petrography and electron microprobe analysis to the study of Indian stone sculpture

    International Nuclear Information System (INIS)

    Newman, R.

    1992-01-01

    Examples of research on ancient Indian stone artefacts utilizing petrographic examination coupled with qualitative and quantitative electron beam microprobe analysis of specific minerals are described. Types of artefacts discussed include Gandharan schist sculptures, Pala dynasty phyllite and schist objects from eastern India. Hoysala sculptures from Karnataka state (southern India), and sandstone objects from northern India. In spite of the rich history of stone sculpture in the Indian subcontinent, characterization studies to date have been limited in scope, typically involving unprovenanced artefacts. The examples described point to areas in which more extensive research could produce useful information for the provenancing of artefacts. (author)

  13. Positron annihilation microprobe

    Energy Technology Data Exchange (ETDEWEB)

    Canter, K F [Brandeis Univ., Waltham, MA (United States)

    1997-03-01

    Advances in positron annihilation microprobe development are reviewed. The present resolution achievable is 3 {mu}m. The ultimate resolution is expected to be 0.1 {mu}m which will enable the positron microprobe to be a valuable tool in the development of 0.1 {mu}m scale electronic devices in the future. (author)

  14. Electron microprobe investigations of ore minerals of the Altenberg tin deposit (Erzgebirge, GDR). 3

    International Nuclear Information System (INIS)

    Foerster, H.J.; Hunger, H.J.; Grimm, L.

    1987-01-01

    Members of the scheelite-powellite solid solution series filling thin fractures or mantling wolframite were found in association with fluorite within a small polymineralic quartz vein traversing a topaz-protolithionite-quartz greisen. The composition of the mixed-crystal series determined by means of an automated ARL SEMQ energy-dispersive electron microprobe is characterized by a great variability and heterogeneity which has not previously been reported from any specimen nor from this special mode of occurrence yet. With an amount of powellite component between 3.2 and 58 mole percent, the molybdoscheelites from Altenberg show the today known extent of complete miscibility in the natural scheelite-powellite series. Final remarks deal with the possibilities of using the mineral series, together with some other tungsten minerals, as an indicator of the physicochemical conditions of ore formation. (author)

  15. Physical aspects of quantitative particles analysis by X-ray fluorescence and electron microprobe techniques

    International Nuclear Information System (INIS)

    Markowicz, A.

    1986-01-01

    The aim of this work is to present both physical fundamentals and recent advances in quantitative particles analysis by X-ray fluorescence (XRF) and electron microprobe (EPXMA) techniques. A method of correction for the particle-size effect in XRF analysis is described and theoretically evaluated. New atomic number- and absorption correction procedures in EPXMA of individual particles are proposed. The applicability of these two correction methods is evaluated for a wide range of elemental composition, X-ray energy and sample thickness. Also, a theoretical model for composition and thickness dependence of Bremsstrahlung background generated in multielement bulk specimens as well as thin films and particles are presented and experimantally evaluated. Finally, the limitations and further possible improvements in quantitative particles analysis by XFR and EPXMA are discussed. 109 refs. (author)

  16. Trans-Regional technologies and the Lapita problem: characterisation of volcanic glass inclusions by electron microprobe

    International Nuclear Information System (INIS)

    Grave, P.; Nockolds, C.; White, P.

    1997-01-01

    Full text: Analysis of pre-modern pottery of the Pacific has long attempted to formulate measures independent of style for constructing archaeologically meaningful groups. However, the variable character of fabrics and the longevity of production (Lapita and post-Lapita wares from 3000 years ago to the present) have tended to obscure differences due to changes in production practices and resources through time and differences relating to the exchange of ceramics between islands or regions. In this poster we outline a preliminary study that employs an economical and robust technique to distinguish both within- and between-region groups. This is achieved with electron microprobe analysis of small volcanic glass fragments present in wares tempered with volcanic sands, and interpretation based on Principal Components Analysis. The method builds on the chemical groupings for glass from different volcanic complexes in the Pacific established through high energy ion beam (PIXE-PIGME) analysis. The purpose of this study is to characterise a selection of samples of pottery from the Duke of York's peninsula using electron microprobe analysis of very small glass fragments in the sections that ranged in size from around 0.05 mm to 1 mm.. The study involved the identification and elemental characterisation of individual fragments of glass in a section. Principal Component Analysis was used to identify structure latent in the dataset. The results of the study show that clear characterisation is possible to enable the wider application of the technique to Lapita and post Lapita ceramics produced originating in volcanic areas of the Pacific

  17. Determination of trace element mineral/liquid partition coefficients in melilite and diopside by ion and electron microprobe techniques

    Science.gov (United States)

    Kuehner, S. M.; Laughlin, J. R.; Grossman, L.; Johnson, M. L.; Burnett, D. S.

    1989-01-01

    The applicability of ion microprobe (IMP) for quantitative analysis of minor elements (Sr, Y, Zr, La, Sm, and Yb) in the major phases present in natural Ca-, Al-rich inclusions (CAIs) was investigated by comparing IMP results with those of an electron microprobe (EMP). Results on three trace-element-doped glasses indicated that it is not possible to obtain precise quantitative analysis by using IMP if there are large differences in SiO2 content between the standards used to derive the ion yields and the unknowns.

  18. Treatment of dentin with stannous fluoride - SEM and electron microprobe study

    International Nuclear Information System (INIS)

    Ellingsen, J.E.; Roella, G.

    1987-01-01

    The effect of SnF 2 -treatment of dentin surfaces was investigated by means of scanning electron microscopy (SEM) and electron microprobe analysis. Human dentin was treated with aqueous SnF 2 solutions of concentrations varying from 1 to 10%. The treatment periods lasted for 1, 5, 10 or 60 min. Both tin and fluoride were identified on the surfaces. The concentration varied depending on the extensiveness of the treatment. Immersion in 1 M KOH for 15 h removed both tin and fluoride from the surfaces. This reaction was not observed after immersion in H 2 O for the same time period. Examination of the SnF 2 -treated dentin surfaces showed a dense layer of globular particles and in addition some larger particles. The dentinal tubules were totally covered even after the treatment with the lowest concentration of SnF 2 . Deposition of tin- and fluoride-containing globules on dentin surfaces may be of clinical interest. This layer may have importance both for the caries resistance of dentin and for hypersensitivity reactions. (author)

  19. CALCMIN - an EXCEL™ Visual Basic application for calculating mineral structural formulae from electron microprobe analyses

    Science.gov (United States)

    Brandelik, Andreas

    2009-07-01

    CALCMIN, an open source Visual Basic program, was implemented in EXCEL™. The program was primarily developed to support geoscientists in their routine task of calculating structural formulae of minerals on the basis of chemical analysis mainly obtained by electron microprobe (EMP) techniques. Calculation programs for various minerals are already included in the form of sub-routines. These routines are arranged in separate modules containing a minimum of code. The architecture of CALCMIN allows the user to easily develop new calculation routines or modify existing routines with little knowledge of programming techniques. By means of a simple mouse-click, the program automatically generates a rudimentary framework of code using the object model of the Visual Basic Editor (VBE). Within this framework simple commands and functions, which are provided by the program, can be used, for example, to perform various normalization procedures or to output the results of the computations. For the clarity of the code, element symbols are used as variables initialized by the program automatically. CALCMIN does not set any boundaries in complexity of the code used, resulting in a wide range of possible applications. Thus, matrix and optimization methods can be included, for instance, to determine end member contents for subsequent thermodynamic calculations. Diverse input procedures are provided, such as the automated read-in of output files created by the EMP. Furthermore, a subsequent filter routine enables the user to extract specific analyses in order to use them for a corresponding calculation routine. An event-driven, interactive operating mode was selected for easy application of the program. CALCMIN leads the user from the beginning to the end of the calculation process.

  20. Ion microprobes

    International Nuclear Information System (INIS)

    Coles, J.N.; Long, J.V.P.

    1977-01-01

    An ion microprobe is described that has an ion extraction arrangement comprising two separate paths for ions and electrons diverging from a common point. A cone shaped or pyramidal guard electrode surrounds each path the apex angles being equal and coinciding with the said point. The guard electrodes are positioned to lie tangentially to each other and to a planar surface including the said point. An aperture is provided for the two paths at the apexes of both guard electrodes, and electrical connections between the guard electrodes enable the same potential to be applied to both guard electrodes. Means are provided for generating oppositely polarised electric fields within the guard electrodes, together with means for causing a focused ion beam to strike the common point without suffering astigmatism. The means for causing a focused ion beam to strike the said point includes an ion gun for directing an ion beam along one of the paths and means to provide an axial accelerating field there along. Optical viewing means are also provided. Existing designs enable only ions or electrons, but not both, to be extracted at any one time. (U.K.)

  1. Evaluation of the odd-even effect in limits of detection for electron microprobe analysis of natural minerals

    Energy Technology Data Exchange (ETDEWEB)

    Verma, Surendra P., E-mail: spv@cie.unam.mx [Departamento de Sistemas Energeticos, Centro de Investigacion en Energia, Universidad Nacional Autonoma de Mexico, Priv. Xochicalco s/no., Col Centro, A.P. 34, Temixco, Mor. 62580 (Mexico); Pandarinath, Kailasa [Departamento de Sistemas Energeticos, Centro de Investigacion en Energia, Universidad Nacional Autonoma de Mexico, Priv. Xochicalco s/no., Col Centro, A.P. 34, Temixco, Mor. 62580 (Mexico); Velasco-Tapia, Fernando [Facultad de Ciencias de la Tierra, Universidad Autonoma de Nuevo Leon, Carretera Linares-Cerro Prieto km. 8, Linares, N.L. 67700 (Mexico); Rodriguez-Rios, Rodolfo [Facultad de Ingenieria e Instituto de Geologia, Universidad Autonoma de San Luis Potosi, Av. Dr. Manuel Nava No. 8, Zona Universitaria, San Luis Potosi, S.L.P. 78240 (Mexico)

    2009-04-13

    Limit of detection (LOD), being a fundamental quality parameter for analytical techniques, has been recently investigated and a systematic behavior has been observed for most odd-even element pairs for many techniques. However, to the best of our knowledge very few LOD data are available in published literature for electron microprobe analysis; these consist of three papers, two being on rare-earth elements and the third covering a large number of elements of atomic number between 21 and 92. These data confirm the systematic behavior of LODs for many odd-even pairs. To initiate to full this gap, we determined LODs for several major rock-forming chemical elements from Na to Fe with atomic numbers between 11 and 26, during the microprobe analysis of common minerals (olivine, plagioclase, pyroxene, amphibole, quartz, and opaques) in volcanic rocks. The odd-even effect of nuclear stability seems to be present in LOD data for most odd-even pairs investigated. Nevertheless, the experimental strategy concerning the reference materials, calibration procedure, and blank measurements, should be substantially modified to better evaluate the systematic behavior of LOD values in microprobe analysis.

  2. Evaluation of the odd-even effect in limits of detection for electron microprobe analysis of natural minerals

    International Nuclear Information System (INIS)

    Verma, Surendra P.; Pandarinath, Kailasa; Velasco-Tapia, Fernando; Rodriguez-Rios, Rodolfo

    2009-01-01

    Limit of detection (LOD), being a fundamental quality parameter for analytical techniques, has been recently investigated and a systematic behavior has been observed for most odd-even element pairs for many techniques. However, to the best of our knowledge very few LOD data are available in published literature for electron microprobe analysis; these consist of three papers, two being on rare-earth elements and the third covering a large number of elements of atomic number between 21 and 92. These data confirm the systematic behavior of LODs for many odd-even pairs. To initiate to full this gap, we determined LODs for several major rock-forming chemical elements from Na to Fe with atomic numbers between 11 and 26, during the microprobe analysis of common minerals (olivine, plagioclase, pyroxene, amphibole, quartz, and opaques) in volcanic rocks. The odd-even effect of nuclear stability seems to be present in LOD data for most odd-even pairs investigated. Nevertheless, the experimental strategy concerning the reference materials, calibration procedure, and blank measurements, should be substantially modified to better evaluate the systematic behavior of LOD values in microprobe analysis.

  3. Review on the application of electron microprobe chemical dating method in the age research of uranium/pitchblende

    International Nuclear Information System (INIS)

    Ge Xiangkun; Qin Mingkuan; Fan Guang

    2011-01-01

    Different micro dating methods have been developed in recent years, the advantages and disadvantages are simply introduced at first. The recent development of electron microprobe chemical dating method in the age research of uraninite/pitchblende and the used analytical conditions by the precurser are presented in detail by stages. Finally, the application foreground of this method in the age research of uraninite/pitchblende and the possible problems are systematically investigated and discussed. It is believed that this method will play a big role in the age research of uranium minerals, especially in the micro dating research of tiny uranium minerals (φ < 10 μm) and uranium micro-ores of multi-stage. (authors)

  4. San Francisco Estuary Striped Bass Migration History Determined by Electron-microprobe Analysis of Otolith Sr/Ca Ratio

    Energy Technology Data Exchange (ETDEWEB)

    Ostrach, D J; Phillis, C C; Weber, P K; Ingram, B L; Zinkl, J G

    2004-09-17

    Habitat use has been shown to be an important factor in the bioaccumulation of contaminants in striped bass. This study examines migration in striped bass as part of a larger study investigating bioaccumulation and maternal transfer of xenobiotics to progeny in the San Francisco Estuary system. Habitat use, residence time and spawning migration over the life of females (n = 23) was studied. Female striped bass were collected between Knights Landing and Colusa on the Sacramento River during the spawning runs of 1999 and 2001. Otoliths were removed, processed and aged via otolith microstructure. Subsequently, otoliths were analyzed for strontium/calcium (Sr/Ca) ratio using an electron-microprobe to measure salinity exposure and to distinguish freshwater, estuary, and marine habitat use. Salinity exposure during the last year before capture was examined more closely for comparison of habitat use by the maternal parent to contaminant burden transferred to progeny. Results were selectively confirmed by ion microprobe analyses for habitat use. The Sr/Ca data demonstrate a wide range of migratory patterns. Age of initial ocean entry differs among individuals before returning to freshwater, presumably to spawn. Some fish reside in freshwater year-round, while others return to more saline habitats and make periodic migrations to freshwater. Frequency of habitat shifts and residence times differs among fish, as well as over the lifetime of individual fish. While at least one fish spent its final year in freshwater, the majority of spawning fish spent their final year in elevated salinity. However, not all fish migrated to freshwater to spawn in the previous year. Results from this investigation concerning migration history in striped bass can be combined with contaminant and histological developmental analyses to better understand the bioaccumulation of contaminants and the subsequent effects they and habitat use have on fish populations in the San Francisco Estuary system.

  5. Investigation of the Electronic Properties of Cadmium Zinc Telluride (CZT) Detectors using a Nuclear Microprobe

    International Nuclear Information System (INIS)

    BRUNETT, BRUCE A.; DOYLE, BARNEY L.; JAMES, RALPH B.; VIZKELETHY, GYORGY; WALSH, DAVID S.

    1999-01-01

    The electronic transport properties of Cadmium Zinc Telluride (CZT) determine the charge collection efficiency (i.e. the signal quality) of CZT detectors. These properties vary on both macroscopic and microscopic scale and depend on the presence of impurities and defects introduced during the crystal growth. Ion Beam Induced Charge Collection (IBICC) is a proven method to measure the charge collection efficiency. Using an ion microbeam, the charge collection efficiency can be mapped with submicron resolution, and the map of electronic properties (such as drift length) can be calculated from the measurement. A more sophisticated version of IBICC, the Time Resolved IBICC (TRIBICC) allows them to determine the mobility and the life time of the charge carriers by recording and analyzing the transient waveform of the detector signal. Furthermore, lateral IBICC and TRIBICC can provide information how the charge collection efficiency depends on the depth where the charge carriers are generated. This allows one to deduce information on the distribution of the electric field and transport properties of the charge carriers along the detector axis. IBICC and TRIBICC were used at the Sandia microbeam facility to image electronic properties of several CZT detectors. From the lateral TRIBICC measurement the electron and hole drift length profiles were calculated

  6. Highly stable single-crystal LaB6 cathode for conventional electron microprobe instruments

    International Nuclear Information System (INIS)

    Shimizu, R.; Shinike, T.; Ichimura, S.; Kawaii, S.; Tanaka, T.

    1978-01-01

    The performance of single-crystal LaB 6 cathode was examined by measuring the brightness and current stability under the same conditions as for the conventional W hairpin cathode. The LaB 6 cathode was mounted in Vogel-type electron gun assembly of an electron probe microanalyser JAX-3 specifically modified for this purpose. The result shows that the present LaB 6 cathode provides not only high brightness of 2 x 10 5 A/cm 2 str. at 20 kV, but also high-current stability better than 1 x 10 - 3 Ah - 1 in standard operation without any specific aid for current stabilization. Thus an order of magnitude increase in both the brightness and service lifetime can easily be obtained provided that the vacuum of the system is adequate, namely better than 1 x 10 - 5 Torr (1.33 x 10 - 3 Pa). This substantial improvement of the present single-crystal LaB 6 cathode over the conventional W hairpin was also confirmed in a practical way by use in a commercial-type scanning Auger electron microscope, JAMP III

  7. Use of electron microprobe x-ray analysis for determination of low calcium concentrations across leaves deficient in calcium

    Science.gov (United States)

    Barta, D. J.; Tibbitts, T. W.

    1991-01-01

    An electron microprobe with wavelength-dispersive x-ray spectrometry (WDS) was found to be useful for the determination of Ca concentrations in leaf tissue deficient in Ca. WDS effectively detected Ca concentrations as low as 0.2 mg/g dry wt in the presence of high levels of K and Mg (120 and 50 mg/g dry wt, respectively). Leaf specimens were prepared for analysis by quick-freezing in liquid nitrogen and freeze-drying at -20 degrees C to maintain elemental integrity within the tissue. Because dry material was analyzed, sample preparation was simple and samples could be stored for long periods before analysis. A large beam diameter of 50 gm was used to minimize tissue damage under the beam and analyze mineral concentrations within several cells at one time. Beam penetration was between 50 and 55 microns, approximately one-third of the thickness of the leaf. For analysis of concentrations in interveinal areas, analyses directed into the abaxial epidermis were found most useful. However, because of limited beam penetration, analyses of veinal areas would require use of cross sections [correction of crosssections]. Solid mineral standards were used for instrument standardization. To prevent measurement errors resulting from differences between the matrix of the mineral standards and the analyzed tissue, concentrations in leaves were corrected using gelatin standards prepared and analyzed under the same conditions. WDS was found to be useful for documenting that very low Ca levels occur in specific areas of lettuce leaves exhibiting the Ca deficiency injury termed tipburn.

  8. Electron microprobe Th-U-Pb monazite dating and metamorphic evolution of the Acaiaca Granulite Complex, Minas Gerais, Brazil

    Energy Technology Data Exchange (ETDEWEB)

    Medeiros Junior, Edgar Batista; Marques, Rodson Abreu, E-mail: edgarjr@ymail.com, E-mail: rodson.marques@ufes.br [Universidade Federal do Espirito Santo (UFES), Alegre, ES (Brazil). Departamento de Geologia; Jordt-Evangelista, Hanna; Queiroga, Glaucia Nascimento, E-mail: hanna@degeo.ufop.br, E-mail: glauciaqueiroga@yahoo.com.br [Universidade Federal de Ouro Preto (UFOP), Ouro Preto, MG (Brazil). Escola de Minas. Departamento de Geologia; Schulz, Bernhard, E-mail: bernhard.schulz@mineral.tu-freiberg.de [TU Bergakademie - Institute of Mineralogy, Freiberg - Saxony (Germany)

    2016-01-15

    The Acaiaca Complex (AC) is located in southeastern Minas Gerais state, and comprises felsic, mafic, ultramafic, and aluminous granulite as well as lower grade gneisses and mylonite. The complex is distributed over an area of ca. 36 km by 6 km, surrounded by amphibolite facies gneisses of the Mantiqueira Complex (MC). The discrepancy in the metamorphic grade between both complexes led to the present study aiming to understand the metamorphic history of the AC by means of geothermobarometry calculations and electron microprobe Th-U-Pb monazite dating. Estimates of the metamorphic conditions of the granulite based on conventional geothermobarometry and THERMOCALC resulted in temperatures around 800 deg C and pressures between of 5.0 and 9.9 kbar and a retro metamorphic path characterized by near-isobaric cooling. Part of the granulite was affected by anatexis. The melting of felsic granulite resulted in the generation of pegmatites and two aluminous lithotypes. These are: 1) garnet-sillimanite granulite with euhedral plagioclase and cordierite that show straight faces against quartz, and is the crystallization product of an anatectic melt, and 2) garnet-kyanite-cordierite granulite, which is probably the restite of anatexis, as indicated by textures and high magnesium contents. Th-U-Pb monazite geochronology of two granulite samples resulted in a metamorphic age around 2060 Ma, which is similar to the age of the MC registered in the literature. The similar Paleoproterozoic metamorphic ages of both complexes lead to the conclusion that the Acaiaca Complex may be the high grade metamorphic unit geochronological related to the lower grade Mantiqueira Complex. (author)

  9. Electron microprobe analyses of selected samples from deep rock disposal experiment No. 1

    International Nuclear Information System (INIS)

    Hlava, P.F.; Chambers, W.F.

    1976-04-01

    Deep Rock Disposal Experiment No. 1 was designed to provide information about the interaction between a molten, glass-based, nuclear waste simulant and rock material. Selected samples from this experiment were examined by optical microscopy and electron probe microanalysis. Analysis of the homogenized material in the convection cell that was created in the central portion of the melt region shows that an amount of rock equal to about one-half of the original amount of waste simulant was incorporated in the melt during the experiment. Stagnant melt at the sides of the cell formed a glass with large compositional gradients. A white band separated the convected and stagnant materials. The color of the band is attributed to light scattering by small crystallites formed during cooling. Four types of crystallites grew from the melt: two oxides, a Mg--Fe borate, and a silicate. Spinel (MgO, Cr 2 O 3 , FeO (Fe 2 O 3 ), and NiO) was the most common crystallite in the glass. The spinel crystallites found within the convection cell displayed skeletal morphology and oscillatory zoning which indicates growth at varying temperatures as they were carried along by convection. A single cluster of nonskeletal (Fe,Cr) 2 O 3 crystallites was found at the bottom of the melt zone where convection did not occur. Mg--Fe borate crystallites grew in clusters in the central portion of the convection cell after convection ceased. A silicate similar to Fe-rich diopside (CaMgSi 2 O 6 ) with unusual amounts of Ce 2 O 3 and other heavy metal oxides formed as larger crystallites in the stagnant melt at the side of the convection cell and as many very small crystallites in the white band

  10. Microprobe analysis in human pathology

    International Nuclear Information System (INIS)

    Baker, D.; Kupke, K.G.; Ingram, P.; Roggli, V.L.; Shelburne, J.D.

    1985-01-01

    This tutorial paper reviews the literature on the application of microprobe analysis to practical problems in diagnostic human pathology. The goal is to allow the reader ready access to the literature on specific clinical problems. Specimen preparation and commonly encountered artifacts are also considered. It is concluded that energy dispersive x-ray microanalysis and back-scattered electron imaging are at present the most generally useful microprobe techniques for clinical work, and are no longer solely research tools. The findings often have diagnostic, therapeutic, and/or legal implications. 332 references

  11. Complementary microanalysis of Zn, Mn and Fe in the chelicera of spiders and scorpions using scanning MeV-ion and electron microprobes

    International Nuclear Information System (INIS)

    Schofield, R.; Lefevre, H.; Shaffer, M.

    1989-01-01

    Energy-loss scanning transmission ion microscopy (ELSTIM or just STIM), PIXE and electron microprobe techniques are used to investigate certain minor element accumulations in a few spiders and scorpions. STIM and PIXE are used to survey the unsectioned specimens, while electron microprobe techniques are used for higher resolution investigations of several sections of the specimens. Concentration values measured using STIM and PIXE are found to be in satisfactory agreement with those measured using electron probe microanalysis. A garden spider Araneous diadematus is found to contain high concentrations of zinc in a thin layer near the surface of its fangs (reaching 23% of dry weight), and manganese in its marginal teeth (about 5% of dry weight). A wolf spider Alopecosa kochi is found to have similar concentrations of zinc in a layer near the surface of it's fang, and concentrations of manganese reaching 1.5% in a layer beneath the zinc containing layer. A scorpion Centruroides sp. is found to contain high concentrations of iron (reaching 8%) and zinc (reaching 24%) in the tips of teeth on the cheliceral fingers, and manganese (about 5%) in the stinger. The hypothesis that these elements simply harden the cuticle does not appear to explain their segregation patterns. (orig.)

  12. De-MA: a web Database for electron Microprobe Analyses to assist EMP lab manager and users

    Science.gov (United States)

    Allaz, J. M.

    2012-12-01

    Lab managers and users of electron microprobe (EMP) facilities require comprehensive, yet flexible documentation structures, as well as an efficient scheduling mechanism. A single on-line database system for managing reservations, and providing information on standards, quantitative and qualitative setups (element mapping, etc.), and X-ray data has been developed for this purpose. This system is particularly useful in multi-user facilities where experience ranges from beginners to the highly experienced. New users and occasional facility users will find these tools extremely useful in developing and maintaining high quality, reproducible, and efficient analyses. This user-friendly database is available through the web, and uses MySQL as a database and PHP/HTML as script language (dynamic website). The database includes several tables for standards information, X-ray lines, X-ray element mapping, PHA, element setups, and agenda. It is configurable for up to five different EMPs in a single lab, each of them having up to five spectrometers and as many diffraction crystals as required. The installation should be done on a web server supporting PHP/MySQL, although installation on a personal computer is possible using third-party freeware to create a local Apache server, and to enable PHP/MySQL. Since it is web-based, any user outside the EMP lab can access this database anytime through any web browser and on any operating system. The access can be secured using a general password protection (e.g. htaccess). The web interface consists of 6 main menus. (1) "Standards" lists standards defined in the database, and displays detailed information on each (e.g. material type, name, reference, comments, and analyses). Images such as EDS spectra or BSE can be associated with a standard. (2) "Analyses" lists typical setups to use for quantitative analyses, allows calculation of mineral composition based on a mineral formula, or calculation of mineral formula based on a fixed

  13. Characterisation of corrosion processes of using electron micro-probe, scanning probe microscopy and synchrotron-generated x-ray fluorescence imaging

    International Nuclear Information System (INIS)

    Neufeld, A.K.; Cole, I.S.; Furman, S.A.; Isaacs, H.S.

    2002-01-01

    Full text: With recent advances in computerized technology, the study of chemical reactions can now be visualized as they occur in real time and has resulted in analytical techniques with orders of magnitude greater sensitivity and resolution. This ability offers the corrosion scientist a unique opportunity to study the processes relevant to degradation science which could only be theoretically considered. Neufeld el al (1,2) have attempted to explain in great detail the mechanism of corrosion initiation of zinc by using X-ray micro-probe, Scanning Kelvin probe, and more recently by using synchrotron-generated X-rays and X-ray fluorescence imaging. New results are presented from the synchrotron studies where the transport of ions in-situ has been investigated. The synthesis of information from the techniques will also be discussed in its relevance to atmospheric corrosion processes. Copyright (2002) Australian Society for Electron Microscopy Inc

  14. Materials analysis with a nuclear microprobe

    International Nuclear Information System (INIS)

    Maggiore, C.J.

    1980-01-01

    The ability to produce focused beams of a few MeV light ions from Van de Graaff accelerators has resulted in the development of nuclear microprobes. Rutherford backscattering, nuclear reactions, and particle-induced x-ray emission are used to provide spatially resolved information from the near surface region of materials. Rutherford backscattering provides nondestructive depth and mass resolution. Nuclear reactions are sensitive to light elements (Z < 15). Particle-induced x-ray analysis is similar to electron microprobe analysis, but 2 orders of magnitude more sensitive. The focused beams are usually produced with specially designed multiplets of magnetic quadrupoles. The LASL microprobe uses a superconducting solenoid as a final lens. The data are acquired by a computer interfaced to the experiment with CAMAC. The characteristics of the information acquired with a nuclear microprobe are discussed; the means of producing the beams of nuclear particles are described; and the limitations and applications of such systems are given

  15. High current pulsed positron microprobe

    International Nuclear Information System (INIS)

    Howell, R.H.; Stoeffl, W.; Kumar, A.; Sterne, P.A.; Cowan, T.E.; Hartley, J.

    1997-01-01

    We are developing a low energy, microscopically focused, pulsed positron beam for defect analysis by positron lifetime spectroscopy to provide a new defect analysis capability at the 10 10 e + s -l beam at the Lawrence Livermore National Laboratory electron linac. When completed, the pulsed positron microprobe will enable defect specific, 3-dimensional maps of defect concentrations with sub-micron resolution of defect location. By coupling these data with first principles calculations of defect specific positron lifetimes and positron implantation profiles we will both map the identity and concentration of defect distributions

  16. Thermobarometry and electron-microprobe Th-U-Pb monazite dating in garnet metapelites from the Capelinha Formation, Aracuai Orogen, Brazil

    Energy Technology Data Exchange (ETDEWEB)

    Queiroga, Glaucia Nascimento; Martins, Maximiliano de Souza; Castro, Marco Paulo de; Jordt-Evangelista, Hanna; Silva, Ana Lucia da, E-mail: glauciaqueiroga@yahoo.com.br, E-mail: maximilianomartins@yahoo.com.br, E-mail: marco_pcastro@yahoo.com, E-mail: hanna@degeo.ufop.br, E-mail: alucia.silva@hotmail.com [Universidade Federal de Ouro Preto (UFOP), Ouro Preto, MG (Brazil). Escola de Minas. Departamento de Geologia; Pedrosa-Soares, Antonio Carlos, E-mail: pedrosa@igc.ufmg.br [Universidade Federal de Minas Gerais (UFMG), Belo Horizonte, MG (Brazil). Instituto de Geociencias. Departamento de Geologia; Schulz, Bernhard, E-mail: bernhard.schulz@mineral.tu-freiberg.de [TU Bergakademie - Institute of Mineralogy, Freiberg - Saxony (Germany)

    2016-01-15

    The Capelinha Formation (Macaubas Group) consists of a lower quartzitic unit with metamafic intercalations and an upper metapelitic sequence. It occurs in a complex tectono-metamorphic sector of the Aracuai orogen, where post-collisional collapse-related structures superimposed collisional structures. The garnet-bearing assemblages started crystallization in the collisional deformation stage that formed the main regional foliation around 570 Ma. Garnet porphyroblasts display a well developed growth zonation of Fe-Mg-Ca-Mn and show, from core to rim, increasing almandine and pyrope contents in contrast with decreasing grossular and spessartine contents. Mineral relations and microstructures provide criteria for local equilibria and a structurally controlled application of geothermobarometry based on cation exchange and net transfer reactions. The P-T values calculated from cores to rims of garnets, aligned along clockwise trends, resulted in increasing temperatures (from 500 deg C up to 620 deg C) under decompression conditions (from 8.0 kbar to 4.5 kbar). The Th-UPb dating of homogeneous monazites by electron microprobe revealed a recrystallization period at around 490 - 480 Ma. These ages can be related to the tectono-thermal event associated with the gravitational collapse, constraining the youngest time limit for metamorphic processes in the Aracuai orogen. (author)

  17. Dedicated accelerator and microprobe line

    International Nuclear Information System (INIS)

    Malmqvist, K.G.; Hylten, G.; Hult, M.; Haakansson, K.; Knox, J.M.; Larsson, N.P.O.; Nilsson, C.; Pallon, J.; Schofield, R.; Swietlicki, E.; Tapper, U.A.S.; Yang Changyi

    1993-01-01

    The development of a dedicated facility for nuclear microprobe analysis and the experiences from using it are discussed. The general properties of the present Lund nuclear microprobe will be described and the advantages of using a dedicated accelerator discussed. (orig.)

  18. In-Situ Microprobe Observations of Dispersed Oil with Low-Temperature Low-Vacuum Scanning Electron Microscope

    International Nuclear Information System (INIS)

    Mohsen, H.T.

    2010-01-01

    A low cost cryostat stage from high heat capacity material is designed and constructed, in attempt to apply size distribution techniques for examination of oil dispersions. Different materials were tested according to their heat capacity to keep the liquid under investigation in frozen state as long as possible during the introduction of the cryostat stage to the low-vacuum scanning electron microscope. Different concentrations of non ionic surfactant were added to artificially contaminated with 10000 ppm Balayeam base oil in 3.5 % saline water, where oil and dispersing liquid have been added and shacked well to be investigated under the microscope as fine frozen droplets. The efficiency of dispersion was examined using low temperature low-vacuum scanning electron microscope. The shape and size distributions of freeze oil droplets were studied by digital imaging processing technique in conjunction with scanning electron microscope counting method. Also elemental concentration of oil droplets was analyzed.

  19. The Melbourne proton microprobe

    International Nuclear Information System (INIS)

    Legge, G.J.F.; McKenzie, C.D.; Mazzolini, A.P.

    1979-01-01

    A scanning proton microprobe is described which operates in ultra-high vacuum with a resolution of ten microns. The operating principles and main features of the design are discussed and the ability of such an instrument to detect trace elements down to a few ppm by mass is illustrated

  20. Corrosion phenomena in electron, proton and synchrotron X-ray microprobe analysis of Roman glass from Qumran, Jordan

    Science.gov (United States)

    Janssens, K.; Aerts, A.; Vincze, L.; Adams, F.; Yang, C.; Utui, R.; Malmqvist, K.; Jones, K. W.; Radtke, M.; Garbe, S.; Lechtenberg, F.; Knöchel, A.; Wouters, H.

    1996-04-01

    A series of 89 glass fragments of Roman glass are studied using electron, proton and synchrotron radiation induced X-ray emission from microscopic areas on the sample surface. The glass originates from Qumran, Jordan and was buried for 1900 years. The weathering layers that result from the extended contact with ground water have been studied, next to the trace composition of the original glass of these pieces. The latter information indicates that at Qumran, large quantities of glass objects were being used in Ancient times. Cross-sectional profiles of the glass show a complex migration behaviour of various groups of major and trace elements.

  1. Arсhaeomineralogy of Ancient Nonferrous Metallurgy Pieces of the Perm Region: Experience of Usage of Electron Microprobe Analysis

    Directory of Open Access Journals (Sweden)

    I. I. Chaykovsky

    2016-12-01

    Full Text Available A series of archaeological features has been studied by means of the scanning electronic microscopy. It was shown that due to the oxidation process, the surface layer is enriched with some elements, which were present at unaltered metal (Ag, Pb and those included later (As, Zn, Pb. It imposes meaningful limitation for use of the X-ray fluorescence and spectral analysis, which allow obtaining only total (patina + metal composition. Sixteen minerals (oxides, carbonates, sulphates, chlorides, phosphates, sulfides and native phases are established in patina composition. Tin bronze structure contains the impurities, which may be an evidence of import to Perm Region of tin and silver possibly from Altai, tin and lead possibly from Karelia during "harinsky" and "rodanovsky" cultures respectively. Various composition of the alloys used for casting and filigree witnesses that ancient metallurgists had known about alloys handling. The presence of barium and fluorine can tell us about composition of the used furnacecharge. The obtained data may be the basis for chemical-metallurgical typification of pieces from nonferrous (and noble metals.

  2. PIXE macro and microprobe techniques in archaeometry

    International Nuclear Information System (INIS)

    Brissaud, I.; Lagarde, G.; Houdayer, A.

    1987-01-01

    PIXE analysis method is applied to archaeometry problems. Advantages and disadvantages are emphasized. Some examples are presented which show the difficulties: especially important heterogeneities of ceramics, old coins and metals restrain from the use of this technique. Other analysis systems, less expensive, like electron microbrobe or x-ray fluorescence spectrometry, are compared with conventional PIXE method. The importance of proton microprobe is explained. (author) 40 refs.; 7 figs.; 5 tabs

  3. Beam developments for the Harwell microprobe system

    International Nuclear Information System (INIS)

    Read, P.M.; Cookson, J.A.; Alton, G.D.

    1986-01-01

    A consequence of the rapid development of micron and submicron size electronic devices is the diminished applicability of high energy ion microprobes with their present resolution limitations to the study of such components. Although submicron beams have been reported the available beam current is barely sufficiently for PIXE and is not adequate for RBS. This lack of lateral resolution is due to low beam brightness at the microprobe object and aberrations in the focusing elements. As part of a program to address these problems the Harwell microprobe lens has been relocated on a new 5 MV Laddertron accelerator. The increased brightness and improved stability of this facility has so far led to a reduction in beam size from 3 x 3 μm 2 to about 2 x 2 μm 2 . The feasibility of using a liquid metal ion source has been examined with a view to achieving more substantial increases in brightness. While such sources have brightness approximately 10 5 times greater than conventional gaseous sources the highly divergent nature of the beam presents problems for the beam transport system. The use of a liquid metal source on the accelerator has been successfully demonstrated but it indicates the need for a special low aberration injection lens if brightness is to be maintained

  4. Mineralogy and electron microprobe studies of magnetite in the Sarab-3 iron Ore deposit, southwest of the Shahrak mining region (east Takab

    Directory of Open Access Journals (Sweden)

    Mohammad Maanijou

    2018-04-01

    Full Text Available Introduction There is an iron mining complex called Shahrak 60 km east of the Takab town, NW Iran. The exploration in the Shahrak deposit (general name for all iron deposits of the area started in 1992 by the Foolad Saba Noor Co. and continued in several periods until 2008. The Shahrak deposit is comprised of 10 ore deposits including Sarab-1, Sarab-2, Sarab-3, Korkora-1, Korkora-2, Shahrak-1, Shahrak-2, Shahrak-3, Cheshmeh and Golezar deposits (Sheikhi, 1995 with a total 60 million tons of proven ore reserves. The Fe grade ranges from 45 to 65% (average 50%. The ore reserves of these deposits are different. Sarab-3 ore deposit with 9 million tons of 54% Fe and 8.95% S is located at the northeast of Kurdistan and in the Sanandaj-Sirjan structural zone at the latitude of 36°20´ and longitude of 47°32´. Materials and methods Sixty thin-polished, polished and thin sections are made for the study of mineralogy and petrology, and among them six thin-polished sections were selected for EPMA (Electron Probe Micro Analysis on magnetite and hematite. EPMA was performed using the Cameca Sx100 electron microprobe at the Iran Mineral Processing Research Center (IMPRC with wavelength-dispersive spectrometers. Results and discussion Based on field observations and petrographic studies, lithologic composition of intrusion (Miocene age ranges within the diorite-leucodiorite, monzodiorite-quartz monzodiorite, granodiorite-granite. With the intrusion of those igneous bodies into carbonate rocks of the Qom Formation, contact metamorphism was formed. The formation of Sarab-3 iron deposit occurred at the three stages of metamorphism, skarnification and supergene. Based on field geology of the deposit, it is composed of endoskarn, exoskarn including Fe ore±sulfides. At the metamorphic stage, after intrusion of intrusive bodies in carbonate rocks, recrystallization took place and marble was formed. With more crystallization of magma, evolved hydrothermal fluids

  5. Microprobe analysis of human fibroblasts

    International Nuclear Information System (INIS)

    Allan, G.L.; Zhu, J.; Legge, G.J.F.

    1985-01-01

    The Melbourne Proton Microprobe has been used to study the copper content in human skin fibroblast cells derived from patients with the genetic disease Menkes Syndrome. Both normal and diseased cells have been studied to investigate any elemental differences occurring between the two cell types. This paper details the preparatory techniques necessary for individual cell analysis and presents the elemental information with a new three dimensional contour mapping technique. These maps are used to highlight elemental differences between normal and mutant fibroblasts. The work also confirms the expected copper excess found in the Menkes cell and indicates that the microprobe can be used for rapid identification of a Menkes carrier

  6. The upgraded Amsterdam nuclear microprobe

    International Nuclear Information System (INIS)

    Vis, R.D.; Kramer, J.L.A.M.; Tros, G.H.J.; Langevelde, F. van; Mars, L.

    1993-01-01

    The improvement of the facilities at our University consists of three phases. In phase 1, a 1.7 MV NEC tandem-Pelletron accelerator has been installed. The accelerator serves as injector for two beam lines, subsequently for macro- and micro-analysis. Moreover, an interconnection has been made with a beam line from our 400 kV high voltage Van de Graaff accelerator in order to enable injection of these very intense low energy beams in these two lines. Apart from new vacuum equipment and conventional beam steering and focussing elements, the experimental facilities are replaced from the cyclotron experimental hall to the newly organised experimental hall. In the phases 2 and 3, which are not yet completed, a second ion source for the Pelletron and a new or extended focussing unit for the microprobe will complete the overall operation. (orig.)

  7. Novel imaging techniques for the nuclear microprobe

    International Nuclear Information System (INIS)

    Saint, A.

    1998-01-01

    Many of the developments of the scanning electron microscope (SEM) have been paralleled during the development of the scanning nuclear microprobe. Secondary electrons were used in the early development of both devices to provide specimen imaging due to the large numbers of secondaries produced per incident charged particle. Other imaging contrast techniques have also been developed on both machines. These include X-ray analysis, scattering contrast, transmission microscopy, channelling induced charge and others. The 'cross-section dependent' imaging techniques such as PIXE, RBS, NRA, etc., rely on the beam current on target for a given resolution. This has prompted research and development of brighter ion sources to maintain probe resolution at high beam current. Higher beam current bring problems with beam damage to the specimen. Low beam current techniques however rely on high countrate data collection systems, but this is only for spectroscopy. To produce an image we can increase beam currents to produce live-time images for specimen manipulation and observation. The work presented here will focus on some developments in live-time imaging with a nuclear micro probe that have taken place recently at the School of Physics, Microanalytical Research Centre (MARC), University of Melbourne

  8. Biological analysis with a nuclear microprobe

    International Nuclear Information System (INIS)

    Cookson, J.A.; Legge, G.J.F.

    1975-01-01

    Most low-energy nuclear accelerators are now partly used on analytical studies in support of sciences other than nuclear physics. This paper gives a short review of such analytical techniques (X-ray analysis, elastic scattering analysis, nuclear reaction analysis, and the nuclear microprobe) with particular reference to biological applications and also emphasizes the role of the positional analysis that can be performed with a focused beam of ions - the nuclear microprobe. (author)

  9. X-ray microprobe for the microcharacterization of materials

    International Nuclear Information System (INIS)

    Sparks, C.J.; Ice, G.E.

    1988-01-01

    The unique properties of x rays offer many advantages over those of electrons and other charged particles for the microcharacterization of materials. X rays are more efficient in exciting characteristic x-ray fluorescence and produce higher fluorescent signal-to-background ratios than obtained with electrons. Such x-ray microprobes will also produce unprecedentedly low levels of detection in diffraction, EXAFS, Auger, and photoelectron spectroscopies for structural and chemical characterization and elemental identification. These major improvements in microcharacterization capabilities will have wide-ranging ramifications not only in materials science but also in physics, chemistry, geochemistry, biology, and medicine. 24 refs., 6 figs., 2 tabs

  10. New generation nuclear microprobe systems

    International Nuclear Information System (INIS)

    Jamieson, David N.

    2001-01-01

    Over the past 20 years, the minimum probe size for nuclear microscopy has stayed around 1 μm with only a few groups reporting a sub-micron probe size around 0.5 μm. No breakthroughs in nuclear microprobe design have been forthcoming to produce dramatic improvements in spatial resolution. The difficulties of breaking the constraints that are preventing reduction of the probe size have been well recognised in the past. Over the past 5 years it has become clear that some of these constraints may not be as limiting as first thought. For example, chromatic aberration clearly is not as significant as implied from first-order ion optics calculations. This paper reviews the constraints in view of the increased understanding of the past 5 years and looks at several new approaches, presently being evaluated in Melbourne and elsewhere, on how to make progress. These approaches include modified RF ion sources for improved beam brightness and exploitation of relaxed constraints on some lens aberrations allowing the use of high demagnification probe forming lens systems

  11. The INS nuclear microprobe and its application

    International Nuclear Information System (INIS)

    Coote, G.E.

    1986-01-01

    The nuclear microprobe directs a well-focused beam of high-energy protons or deuterons at a solid specimen inside a vacuum chamber. Atomic and nuclear reactions are induced in those elements in a layer about 20 micro m thick, leading to the emission of characteristic x-rays, gamma rays, and charged particles as well as Rutherford scattering of the incident beam. These radiations impinge on several detectors near the specimen (NaI, Ge(Li), Si(Li) and Si surface barrier). Using proton-excited x-rays all elements above Na may be detected with sensitivities 10 or 100 times that of the electron probe, while elements which can be estimated from their gamma rays include C, N, O, F, Na and Al. In most of our projects the distribution of a trace or minor element (e.g. F, N) is compared to that of a major element (e.g. Ca or Fe). Recent areas of application include archaeometry (diffusion profiles of F in bones and teeth; depth profiles of sodium in obsidian), geology (F concentrations in mineral grains; studies of the Cretaceous-Tertiary boundary), metallurgy (C, O, N in steel and in welds; S, O, C in corrosion layers), fisheries management (Zn, Sr in otoliths; F in dogfish fin spines and vertebrae), biology (Fe, Sr, N in egg shells; trace elements in human hair), and dental research

  12. Beam optics on the Melbourne proton microprobe

    International Nuclear Information System (INIS)

    Jamieson, D.N.; Colman, R.A.; Allan, G.L.; Legge, G.J.F.

    1985-01-01

    This review paper summarises results of ion optics development work conducted on the Melbourne Proton Microprobe and the associated Pelletron accelerator. The properties of a field ionization ion source have been investigated with the aim of replacing the existing R.F. ion source in the accelerator in order to obtain a brighter beam for the microprobe. The electrostatic emitter lens in the terminal of the accelerator has also been investigated with the aim of improving the focus of the accelerated beam. Finally, the aberrations of the probe forming lens system have been studied and it is shown how some of these may be corrected with an octupole lens

  13. X-ray Microprobe for Fluorescence and Diffraction Analysis

    International Nuclear Information System (INIS)

    Ice, G.E.

    2005-01-01

    X-ray diffraction (see unit 1.1) and x-ray excited fluorescence analysis are powerful techniques for the nondestructive measurement of crystal structure and chemical composition. X-ray fluorescence analysis is inherently nondestructive with orders of magnitude lower power deposited for the same detectable limit as with fluorescence excited by charged particle probes (Sparks, 1980). X-ray diffraction analysis is sensitive to crystal structure with orders-of-magnitude greater sensitivity to crystallographic strain than electron probes (Rebonato, et al. 1989). When a small-area x-ray microbeam is used as the probe, chemical composition (Z>14), crystal structure, crystalline texture, and crystalline strain distributions can be determined. These distributions can be studied both at the surface of the sample and deep within the sample (Fig. 1). Current state-of-the-art can achieve an ∼1 mm-D x-ray microprobe and an ∼0.1 mm-D x-ray microprobe has been demonstrated (Bilderback, et al., 1994). Despite their great chemical and crystallographic sensitivities, x-ray microprobe techniques have until recently been restricted by inefficient x-ray focusing optics and weak x-ray sources; x-ray microbeam analysis was largely superseded by electron techniques in the 50's. However, interest in x-ray microprobe techniques has now been revived (Howells, et al., 1983; Ice and Sparks, 1984; Chevallier, et al., 1997; Riekel 1992; Thompson, el al., 1992; and Making and Using... 1997) by the development of efficient x-ray focusing optics and ultra-high intensity synchrotron x-ray sources (Buras and Tazzari, 1984; Shenoy, et al., 1988). These advances have increased the achievable microbeam flux by more than 11 orders of magnitude (Fig. 2) (Ice, 1997); the flux in a tunable 1 mm-D beam on a 'so called' 3rd-generation synchrotron source such as the APS can exceed the flux in a fixed-energy mm2 beam on a conventional source. These advances make x-ray microfluorescence and x

  14. Mapping of trace elements with photon microprobes: x-ray fluorescence with focussed synchrotron radiation

    International Nuclear Information System (INIS)

    Hanson, A.L.; Jones, K.W.; Gordon, B.M.; Pounds, J.G.; Rivers, M.L.; Schidlovsky, G.

    1985-04-01

    High energy electron synchrotron storage rings provide copious quantities of polarized photons that make possible the mapping of many trace elements with sensitivities at the parts per billion (ppB) level with spatial resolutions in the micrometer range. The brightness of the x-ray ring of the National Synchrotron Light Source (NSLS), presently being commissioned, will be five orders of magnitude larger than that of the bremsstrahlung spectrum of state-of-the-art rotating anode tubes. We will discuss mapping trace elements with a photon microprobe presently being constructed for use at the NSLS. This microprobe will have micrometer spatial resolution

  15. Scanning deep level transient spectroscopy using an MeV ion microprobe

    Energy Technology Data Exchange (ETDEWEB)

    Laird, J S; Bardos, R A; Saint, A; Moloney, G M; Legge, G F.J. [Melbourne Univ., Parkville, VIC (Australia)

    1994-12-31

    Traditionally the scanning ion microprobe has given little or no information regarding the electronic structure of materials in particular semiconductors. A new imaging technique called Scanning Ion Deep Level Transient Spectroscopy (SIDLTS) is presented which is able to spatially map alterations in the band gap structure of materials by lattice defects or impurities. 3 refs., 2 figs.

  16. Scanning deep level transient spectroscopy using an MeV ion microprobe

    Energy Technology Data Exchange (ETDEWEB)

    Laird, J.S.; Bardos, R.A.; Saint, A.; Moloney, G.M.; Legge, G.F.J. [Melbourne Univ., Parkville, VIC (Australia)

    1993-12-31

    Traditionally the scanning ion microprobe has given little or no information regarding the electronic structure of materials in particular semiconductors. A new imaging technique called Scanning Ion Deep Level Transient Spectroscopy (SIDLTS) is presented which is able to spatially map alterations in the band gap structure of materials by lattice defects or impurities. 3 refs., 2 figs.

  17. Mixed beams for the nuclear microprobe

    Energy Technology Data Exchange (ETDEWEB)

    Saint, A.; Breese, M.B.H.; Legge, G.L.F. [Melbourne Univ., Parkville, VIC (Australia). School of Physics

    1996-12-31

    Recently the Micro-Analytical Research Centre (MARC) at Melbourne University has developed a technique to provide mixed beams of ions for a magnetically focussed nuclear microprobe. Such a mixed beam is defined as two (or more) beams of different species ions that can quickly and easily be made to have the same magnetic rigidity R{sub m} = (mE/q{sup 2}) and therefore be transported, focused and scanned the same in a magnetic nuclear microprobe. The production of mixed beams in an electrostatically focussed micro- probe have already been demonstrated. This paper will show how mixed beams can be produced on a single-ended accelerator. Indications of how to produce them on a tandem will also be given. Applications of these mixed beams in micro-lithography, scanning transmission ion microscopy (STIM) imaging and ion beam induced charge (IBIC) imaging will also be presented. 3 refs., 3 figs.

  18. Mixed beams for the nuclear microprobe

    Energy Technology Data Exchange (ETDEWEB)

    Saint, A; Breese, M B.H.; Legge, G L.F. [Melbourne Univ., Parkville, VIC (Australia). School of Physics

    1997-12-31

    Recently the Micro-Analytical Research Centre (MARC) at Melbourne University has developed a technique to provide mixed beams of ions for a magnetically focussed nuclear microprobe. Such a mixed beam is defined as two (or more) beams of different species ions that can quickly and easily be made to have the same magnetic rigidity R{sub m} = (mE/q{sup 2}) and therefore be transported, focused and scanned the same in a magnetic nuclear microprobe. The production of mixed beams in an electrostatically focussed micro- probe have already been demonstrated. This paper will show how mixed beams can be produced on a single-ended accelerator. Indications of how to produce them on a tandem will also be given. Applications of these mixed beams in micro-lithography, scanning transmission ion microscopy (STIM) imaging and ion beam induced charge (IBIC) imaging will also be presented. 3 refs., 3 figs.

  19. Biomedical application of the nuclear microprobe

    International Nuclear Information System (INIS)

    Lindh, U.

    1987-01-01

    The Studsvik Nuclear Microprobe (SMP) has mainly been devoted to applications in the biomedical field. Its ultimate resolution is reached at 2.9x2.9 μm 2 with a proton current of 100 pA. With this performance the SMP has been used in a wide range of disciplines covering environmental hygiene, toxicology, various aspects of internal medicine and trace element physiology. Examples of recent applications in these fields are described. (orig.)

  20. Development of a nuclear microprobe at IGCAR

    International Nuclear Information System (INIS)

    Ramesh, C.; Nair, K.G.M.; Thampi, N.S.; Saha, B.; Mathews, C.K.

    1988-01-01

    A nuclear microprobe is being developed at IGCAR. The system is being built to determine the profiles of light elements, specially carbon in clad and other structural materials of a fast breeder reactor. By scanning a focussed charged particle beam on the sample surface and by detecting the charged particle induced emissions, an elemental map of the surface is obtained. The paper gives the basic design considerations and present status. (author)

  1. Chemical history with a nuclear microprobe

    International Nuclear Information System (INIS)

    Maggiore, C.J.; Benjamin, T.M.; Burnett, D.S.; Hyde, P.J.; Rogers, P.S.Z.; Srinivasan, S.; Tesmer, T.; Woolum, D.S.

    1983-01-01

    A nuclear microprobe cannot give direct information on the chemical state of an element, but the spatial distribution of elements in a specimen is often determined by the chemical history of the sample. Fuel cells and minerals are examples of complex systems whose elemental distributions are determined by past chemical history. The distribution of catalyst in used fuel cell electrodes provides direct information on the chemical stability of dispersed catalysts under operating conditions. The authors have used spatially resolved Rutherford backscattering to measure the migration of platinum and vanadium from intermetallic catalysts and to determine their suitability for use under the extreme operating conditions found in phosphoric acid fuel cells. Geologic materials are complex, heterogeneous samples with small mineral grains. The trace element distribution within the individual mineral grains and between different mineral phases is sensitive to the details of the mineral formation and history. The spatial resolution and sub-100-ppm sensitivity available with a nuclear microprobe open up several new classes of experiments to the geochemist. Geochemistry and electrochemistry are two areas proving particularly fruitful for application of the nuclear microprobe

  2. Quantitative microanalysis with a nuclear microprobe

    International Nuclear Information System (INIS)

    Themner, Klas.

    1989-01-01

    The analytical techniques of paticle induced X-ray emission (PIXE) and Rutherford backscattering (RBS), together with the nuclear microprobe, form a very powerful tool for performing quantitative microanalysis of biological material. Calibration of the X-ray detection system in the microprobe set-up has been performed and the accuracy of the quantitative procedure using RBS for determination of the areal mass density was investigated. The accuracy of the analysis can be affected by alteration in the elemental concentrations during irradiation due to the radiation damage induced by the very intense beams of ionixing radiation. Loss of matrix elements from freeze-dried tissue sections and polymer films have been studied during proton and photon irradiation and the effect on the accuracy discussed. Scanning the beam over an area of the target, with e.g. 32x32 pixels, in order to produce en elemental map, yields a lot of information and, to be able to make an accurate quantitatification, a fast algorithm using descriptions of the different spectral contributions is of need. The production of continuum X-rays by 2.55 MeV protons has been studied and absolute cross-sections for the bremsstrahlung production from thin carbon and some polymer films determined. For the determination of the bremsstrahlung background knowledge of the amounts of the matrix elements is important and a fast program for the evaluation of spectra of proton back- and forward scattering from biological samples has been developed. Quantitative microanalysis with the nuclear microprobe has been performed on brain tissue from rats subjected to different pathological conditions. Increase in calcium levels and decrease in potssium levels for animals subjected to crebral ischaemia and for animals suffering from epileptic seizures were observed coincidentally with or, in some cases before, visible signs of cell necrosis. (author)

  3. PROTON MICROPROBE ANALYSIS OF TRACE-ELEMENT VARIATIONS IN VITRINITES IN THE SAME AND DIFFERENT COAL BEDS.

    Science.gov (United States)

    Minkin, J.A.; Chao, E.C.T.; Blank, Herma; Dulong, F.T.

    1987-01-01

    The PIXE (proton-induced X-ray emission) microprobe can be used for nondestructive, in-situ analyses of areas as small as those analyzed by the electron microprobe, and has a sensitivity of detection as much as two orders of magnitude better than the electron microprobe. Preliminary studies demonstrated that PIXE provides a capability for quantitative determination of elemental concentrations in individual coal maceral grains with a detection limit of 1-10 ppm for most elements analyzed. Encouraged by the earlier results, we carried out the analyses reported below to examine trace element variations laterally (over a km range) as well as vertically (cm to m) in the I and J coal beds in the Upper Cretaceous Ferron Sandstone Member of the Mancos Shale in central Utah, and to compare the data with the data from two samples of eastern coals of Pennsylvanian age.

  4. Microprobe channeling analysis of pyrite crystals

    International Nuclear Information System (INIS)

    Jamieson, D.N.; Ryan, C.G.

    1992-01-01

    Nuclear microprobe analysis has provided much useful information about the composition of microscopic inclusions in minerals, mainly through the use of Particle Induced X-ray Emission (PIXE). However this technique, while powerful, does not provide any direct information about the chemical state, in particular the lattice location, of the elements in the mineral. This information is often of crucial importance in understanding the ore genesis. The technique of ion channeling may be used to identify lattice location, but many minerals occur as microscopic crystals. Therefore it is necessary to utilize a nuclear microprobe with the technique of Channeling Contrast Microscopy (CCM). As many minerals contain interesting trace elements, it is necessary to measure both the yield of backscattered particles and the induced x-rays to get a clear picture of the lattice location of the elements in the crystal. CCM with PIXE was used to analyse natural pyrite crystals containing a variety of substitutional and non-substitutional elements and natural pyrite crystals from a gold bearing ore. In the latter case, evidence was obtained for two habits for Au in the 400 μm crystals: one as inclusions of Au rich minerals, the other substituted on the pyrite lattice sites. 31 refs., 3 tabs., 6 figs

  5. Proton microprobe study of tin-polymetallic deposits

    Energy Technology Data Exchange (ETDEWEB)

    Murao, S. [Geological Survey of Japan, Tsukuba, Ibaraki (Japan); Sie, S.H.; Suter, G.F. [Commonwealth Scientific and Industrial Research Organisation (CSIRO), North Ryde, NSW (Australia). Div. of Exploration Geoscience

    1996-12-31

    Tin-polymetallic vein type deposits are a complex mixture of cassiterite and sulfides and they are the main source of technologically important rare metals such as indium and bismuth. Constituent minerals are usually fine grained having wide range of chemical composition and often the elements of interest occur as trace elements not amenable to electron microprobe analysis. PIXE with a proton microprobe can be an effective tool to study such deposits by delineating the distribution of trace elements among carrier minerals. Two representative indium-bearing deposits of tin- polymetallic type, Tosham of India (Cu-ln-Bi-Sn-W-Ag), and Mount Pleasant of Canada (Zn-Cu-In-Bi-Sn-W), were studied to delineate the distribution of medical/high-tech rare metals and to examine the effectiveness of the proton probe analysis of such ore. One of the results of the study indicated that indium and bismuth are present in chalcopyrite in the deposits. In addition to these important rare metals, zinc, copper, arsenic, antimony, selenium, and tin are common in chalcopyrite and pyrite. Arsenopyrite contains nickel, copper, zinc, silver, tin, antimony and bismuth. In chalcopyrite and pyrite, zinc, arsenic, indium, bismuth and lead are richer in Mount Pleasant ore, but silver is higher at Tosham. Also thallium and gold were found only in Tosham pyrite. The Tosham deposit is related to S-type granite, while Mount Pleasant to A-type. It appears that petrographic character of the source magma is one of the factors to determine the trace element distribution in tin-polymetallic deposit. 6 refs., 2 figs.

  6. Proton microprobe study of tin-polymetallic deposits

    Energy Technology Data Exchange (ETDEWEB)

    Murao, S [Geological Survey of Japan, Tsukuba, Ibaraki (Japan); Sie, S H; Suter, G F [Commonwealth Scientific and Industrial Research Organisation (CSIRO), North Ryde, NSW (Australia). Div. of Exploration Geoscience

    1997-12-31

    Tin-polymetallic vein type deposits are a complex mixture of cassiterite and sulfides and they are the main source of technologically important rare metals such as indium and bismuth. Constituent minerals are usually fine grained having wide range of chemical composition and often the elements of interest occur as trace elements not amenable to electron microprobe analysis. PIXE with a proton microprobe can be an effective tool to study such deposits by delineating the distribution of trace elements among carrier minerals. Two representative indium-bearing deposits of tin- polymetallic type, Tosham of India (Cu-ln-Bi-Sn-W-Ag), and Mount Pleasant of Canada (Zn-Cu-In-Bi-Sn-W), were studied to delineate the distribution of medical/high-tech rare metals and to examine the effectiveness of the proton probe analysis of such ore. One of the results of the study indicated that indium and bismuth are present in chalcopyrite in the deposits. In addition to these important rare metals, zinc, copper, arsenic, antimony, selenium, and tin are common in chalcopyrite and pyrite. Arsenopyrite contains nickel, copper, zinc, silver, tin, antimony and bismuth. In chalcopyrite and pyrite, zinc, arsenic, indium, bismuth and lead are richer in Mount Pleasant ore, but silver is higher at Tosham. Also thallium and gold were found only in Tosham pyrite. The Tosham deposit is related to S-type granite, while Mount Pleasant to A-type. It appears that petrographic character of the source magma is one of the factors to determine the trace element distribution in tin-polymetallic deposit. 6 refs., 2 figs.

  7. Proton microprobe study of tin-polymetallic deposits

    International Nuclear Information System (INIS)

    Murao, S.; Sie, S.H.; Suter, G.F.

    1996-01-01

    Tin-polymetallic vein type deposits are a complex mixture of cassiterite and sulfides and they are the main source of technologically important rare metals such as indium and bismuth. Constituent minerals are usually fine grained having wide range of chemical composition and often the elements of interest occur as trace elements not amenable to electron microprobe analysis. PIXE with a proton microprobe can be an effective tool to study such deposits by delineating the distribution of trace elements among carrier minerals. Two representative indium-bearing deposits of tin- polymetallic type, Tosham of India (Cu-ln-Bi-Sn-W-Ag), and Mount Pleasant of Canada (Zn-Cu-In-Bi-Sn-W), were studied to delineate the distribution of medical/high-tech rare metals and to examine the effectiveness of the proton probe analysis of such ore. One of the results of the study indicated that indium and bismuth are present in chalcopyrite in the deposits. In addition to these important rare metals, zinc, copper, arsenic, antimony, selenium, and tin are common in chalcopyrite and pyrite. Arsenopyrite contains nickel, copper, zinc, silver, tin, antimony and bismuth. In chalcopyrite and pyrite, zinc, arsenic, indium, bismuth and lead are richer in Mount Pleasant ore, but silver is higher at Tosham. Also thallium and gold were found only in Tosham pyrite. The Tosham deposit is related to S-type granite, while Mount Pleasant to A-type. It appears that petrographic character of the source magma is one of the factors to determine the trace element distribution in tin-polymetallic deposit. 6 refs., 2 figs

  8. Rapid rock analysis and microprobe scanning of dermatological material using proton-induced x-ray and γ-ray emission

    International Nuclear Information System (INIS)

    Carlsson, L.E.

    1983-01-01

    The dissertation report comprises 6 articles that have or will appear in open literature. The use of PIXE and PIGE analysis techniques on geological materials, and also on drill cores, is discussed. The accuracy of the methods have been tested on standards. The effect of sample thickness has been studied. A proton microprobe has been compared with an electron microprobe on human skin sections. Both probes give highly reproducible results, but a small systematic deviation between the probes is found. (author)

  9. The new scanning nuclear microprobe in Uppsala

    International Nuclear Information System (INIS)

    Sunde, T.; Nystroem, J.; Lindh, U.

    1991-01-01

    During 1989/90 a scanning microprobe, developed for 2-4 MeV protons and submicron resolution, is being installed at the EN-tandem accelerator at the The Svedberg Laboratory, Uppsala University, Sweden. The probe-forming units (object diaphragm, aperture diaphragm and triplet of spark-eroded quadrupoles), the scanning unit of current-controlled ferrite cores and a current digitizer are of Oxford design. The other parts are commercial products or are constructed by ourselves. The latter includes the equipment for optical alignment by interference, a feedback-controlled magnetic beam steerer and stabiliser, a fast beam deflector, specially designed mechanical vibration reducers and dedicated AT expansion cards for scanning control and data acquisition. (orig.)

  10. Trace elemental analysis of bituminous coals using the Heidelberg proton microprobe

    Energy Technology Data Exchange (ETDEWEB)

    Chen, J R; Kneis, H; Martin, B; Nobiling, R; Traxel, K [Max-Planck-Institut fuer Kernphysik, Heidelberg (Germany, F.R.); Heidelberg Univ. (Germany, F.R.). Physikalisches Inst.); Chao, E C.T.; Minkin, J A [Geological Survey, Reston, VA (USA)

    1981-03-01

    Trace elements in coal can occur as components of either the organic constituents (macerals) or the inorganic constituents (minerals). Studies of the concentrations and distribution of the trace elements are vital to understanding the geochemical milieu in which the coal was formed and in evaluating the attempts to recover rare but technologically valuable metals. In addition, information on the trace element concentrations is important in predicting the environmental impact of burning particular coals, as many countries move toward greater utilization of coal reserves for energy production. Traditionally, the optical and the electron microscopes and more recently the electron microprobe have been used in studying the components of coal. The proton-induced X-ray emission (PIXE) microprobe offers a new complementary approach with an order of magnitude or more better minimum detection limit. We present the first measurements with a PIXE microprobe of the trace element concentrations of bituminous coal samples. Elemental analyses of the coal macerals-vitrinite, exinite, and inertinite - are discussed for three coal samples from the Eastern U.S.A., three samples from the Western U.S.A., and one sample from the Peoples Republic of China.

  11. Applications of nuclear microprobes in the semiconductor industry

    International Nuclear Information System (INIS)

    Takai, M.

    1996-01-01

    Possible nuclear microprobe applications in semiconductor industries are discussed. A unique technique using soft-error mapping and ion beam induced current measurements for reliability testing of dynamic random access memories such as soft-error immunity and noise carrier suppression has been developed for obtaining design parameters of future memory devices. Nano-probes and small installation areas are required for the use of microprobes in the semiconductor industry. Issues arising from microprobe applications such as damage induced by the probe beam are clarified. (orig.)

  12. Nuclear scanning microprobe: state of the art, applications and progress trends

    International Nuclear Information System (INIS)

    Ponomarev, A.G.

    2011-01-01

    The physical principles of nuclear scanning microprobe are considered. The analysis of state of the art of the microprobe setup from point of view of its spatial resolution and sensitivity of microanalysis techniques is given. The regions of nuclear microprobe applications are reviewed. The ways of spatial resolution and data acquisition system improvement under consideration of microprobe setup progress trends are considered. (authors)

  13. Elemental microanalysis of botanical specimens using the Melbourne Proton Microprobe

    International Nuclear Information System (INIS)

    Mazzolini, A.P.J.; Legge, G.J.F.

    1978-01-01

    A proton microprobe has been used to obtain the distribution of elements of various botanical specimens. This paper presents preliminary results obtained by the irradiation of certain organs of the wheat plant

  14. Optimization of the electrostatic structure of the ion microprobe

    Directory of Open Access Journals (Sweden)

    I. G. Ignat'ev

    2012-03-01

    Full Text Available The paper presents optimization data obtained for an immersion probe-forming system of the ion microprobe to be used in 3 MeV H+ ion accelerator generating 0,4 μm beam spot for normalized acceptance of 7 μm2 · mrad2 · MeV. To achieve higher microprobe resolution it is intended to place an electrostatic lens between the collimators and the accelerating tube.

  15. Subgroup report on hard x-ray microprobes

    International Nuclear Information System (INIS)

    Ice, G.E.; Barbee, T.; Bionta, R.; Howells, M.; Thompson, A.C.; Yun, W.

    1994-01-01

    The increasing availability of synchrotron x-ray sources has stimulated the development of advanced hard x-ray (E≥5 keV) microprobes. New x-ray optics have been demonstrated which show promise for achieving intense submicron hard x-ray probes. These probes will be used for extraordinary elemental detection by x-ray fluorescence/absorption and for microdiffraction to identify phase and strain. The inherent elemental and crystallographic sensitivity of an x-ray microprobe and its inherently nondestructive and penetrating nature makes the development of an advanced hard x-ray microprobe an important national goal. In this workshop state-of-the-art hard x-ray microprobe optics were described and future directions were discussed. Gene Ice, Oak Ridge National Laboratory (ORNL), presented an overview of the current status of hard x-ray microprobe optics and described the use of crystal spectrometers to improve minimum detectable limits in fluorescent microprobe experiments. Al Thompson, Lawrence Berkeley Laboratory (LBL), described work at the Center for X-ray Optics to develop a hard x-ray microprobe based on Kirkpatrick-Baez (KB) optics. Al Thompson also showed the results of some experimental measurements with their KB optics. Malcolm Howells presented a method for bending elliptical mirrors and Troy Barbee commented on the use of graded d spacings to achieve highest efficiency in KB multilayer microfocusing. Richard Bionta, Lawrence Livermore National Laboratory (LLNL), described the development of the first hard x-ray zone plates and future promise of so called open-quotes jelly rollclose quotes or sputter slice zone plates. Wenbing Yun, Argonne National Laboratory (ANL), described characterization of jelly roll and lithographically produced zone plates and described the application of zone plates to focus extremely narrow bandwidths by nuclear resonance. This report summarizes the presentations of the workshop subgroup on hard x-ray microprobes

  16. The new nuclear microprobe at Livermore

    International Nuclear Information System (INIS)

    Roberts, M.L.; Bench, G.S.; Heikkinen, D.W.; Morse, D.H.; Bach, P.R.; Pontau, A.E.

    1994-10-01

    Lawrence Livermore National Laboratory (LLNL) and Sandia National Laboratories/California have jointly constructed a new nuclear microprobe beamline. This beamline is located on the LLNL 10 MV tandem accelerator and can be used for multidisciplinary research using PIXE, PIGE, energy loss tomography, or IBS techniques. Distinctive features of the beamline include incorporation of magnet power supplies into the accelerator control system, computer controlled object and image slits, automated target positioning to sub-micron resolution, and video optics for beam positioning and observation. Mitigation of vibrations was accomplished with vibration isolators and a rigid beamline design while integral beamline shielding was used to shield from stray magnetic fields. Available detectors include a wavelength dispersive X-ray spectrometer, a High-Purity Germanium detector (HPGe), a Lithium-Drifted Silicon X-Ray detector (SiLi), and solid state surface barrier detectors. Along with beamline performance, results from recent measurements on determination of trace impurities in an International Thermonuclear Experimental Reactor (ITER) super conducting wire strand, determination of Ca/Sr ratios in seashells, and determination of minor and trace element concentrations in sperm cells are presented

  17. Deep Space 2: The Mars Microprobe Mission

    Science.gov (United States)

    Smrekar, Suzanne; Catling, David; Lorenz, Ralph; Magalhães, Julio; Moersch, Jeffrey; Morgan, Paul; Murray, Bruce; Presley-Holloway, Marsha; Yen, Albert; Zent, Aaron; Blaney, Diana

    The Mars Microprobe Mission will be the second of the New Millennium Program's technology development missions to planetary bodies. The mission consists of two penetrators that weigh 2.4 kg each and are being carried as a piggyback payload on the Mars Polar Lander cruise ring. The spacecraft arrive at Mars on December 3, 1999. The two identical penetrators will impact the surface at ~190 m/s and penetrate up to 0.6 m. They will land within 1 to 10 km of each other and ~50 km from the Polar Lander on the south polar layered terrain. The primary objective of the mission is to demonstrate technologies that will enable future science missions and, in particular, network science missions. A secondary goal is to acquire science data. A subsurface evolved water experiment and a thermal conductivity experiment will estimate the water content and thermal properties of the regolith. The atmospheric density, pressure, and temperature will be derived using descent deceleration data. Impact accelerometer data will be used to determine the depth of penetration, the hardness of the regolith, and the presence or absence of 10 cm scale layers.

  18. Ion microprobe analysis of metallic pigments

    International Nuclear Information System (INIS)

    Pelicon, P.; Simcic, J.; Budnar, M.; Klanjsek-Gunde, M.; Kunavaer, M.

    2001-01-01

    Full text: Metallic paints consist of metallic flakes dispersed m a resinous binder, i.e. a light-element polymer matrix. The spatial distribution and orientation of metallic flakes inside the matrix determines the covering efficiency of the paint, glossiness, and its angular-dependent properties such as lightness flop or color flop (two-tone). Such coatings are extensively used for a functional (i.e. security) as well as decorative purpose. The ion microbeam analysis of two types of silver paint with imbedded metallic flake has been performed to test the ability of the ion microbeam spectroscopic methods on this type of samples. The average sizes of the aluminium flakes were 23 (size distribution 10-37) and 49 (size distribution 34-75) micrometers, respectively. The proton beam with the size of 2x2 micrometers at Ljubljana ion microprobe has been used to scan the surface of the pigments. PIXE mapping of Al Kα map shows lateral distribution of the aluminum flakes, whereas the RBS slicing method reveals tomographic image of the flakes in uppermost 5 micrometers of the pigment layer. The flake distribution in the larger layer depths has been accessed by RBS analysis in a point mode. (author)

  19. Proton microprobe analysis of pancreatic. beta. cells

    Energy Technology Data Exchange (ETDEWEB)

    Lindh, U [Uppsala Univ. (Sweden). Gustaf Werner Inst.; Juntti-Berggren, L; Berggren, P O; Hellman, B [Uppsala Univ. (Sweden)

    1985-01-01

    Freeze-dried pancreas sections from obese hyperglycemic mice were subjected to proton bombardment and the elemental contents in the ..beta.. cells and the exocrine part were obtained from the characteristic X-rays emitted. Quantitative data were provided for 18 different elements. The mole ratio between K and Na exceeded 10, implying that neither the sample preparation nor the irradiation had induced significant diffuse changes. With the demonstration of this high K/Na ratio it seems likely that also the ..beta.. cells are equipped with an efficient Na/sup +//K/sup +/ pump. The ..beta.. cells contained about 70 mmoles Cl per litre cell water. Observed amounts of Ca and Mg were equivalent to those previously recorded by electrothermal atomic absorption spectroscopy. The significant role of Zn for the storage of insulin was emphasized by the demonstration of 3 times as much of this element in the ..beta.. cells as compared with the exocrine pancreas. In addition, the sensitivity of the proton microprobe enabled measurements of various trace elements such as Rb, Cr, Cu, Al and Pb not previously demonstrated in the pancreatic ..beta.. cells.

  20. The Mars Microprobe Mission: Advanced Micro-Avionics for Exploration Surface

    Science.gov (United States)

    Blue, Randel

    2000-01-01

    The Mars Microprobe Mission is the second spacecraft developed as part of the New Millennium Program deep space missions. The objective of the Microprobe Project is to demonstrate the applicability of key technologies for future planetary missions by developing two probes for deployment on Mars. The probes are designed with a single stage entry, descent, and landing system and impact the Martian surface at speeds of approximately 200 meters per second. The microprobes are composed of two main sections, a forebody section that penetrates to a depth below the Martian surface of 0.5 to 2 meters, and an aftbody section that remains on the surface. Each probe system consists of a number of advanced technology components developed specifically for this mission. These include a non-erosive aeroshell for entry into. the atmosphere, a set of low temperature batteries to supply probe power, an advanced microcontroller to execute the mission sequence, collect the science data, and react to possible system fault conditions, a telecommunications subsystem implemented on a set of custom integrated circuits, and instruments designed to provide science measurements from above and below the Martian surface. All of the electronic components have been designed and fabricated to withstand the severe impact shock environment and to operate correctly at predicted temperatures below -100 C.

  1. ;Study of secondary hydriding at high temperature in zirconium based nuclear fuel cladding tubes by coupling information from neutron radiography/tomography, electron probe micro analysis, micro elastic recoil detection analysis and laser induced breakdown spectroscopy microprobe

    Science.gov (United States)

    Brachet, Jean-Christophe; Hamon, Didier; Le Saux, Matthieu; Vandenberghe, Valérie; Toffolon-Masclet, Caroline; Rouesne, Elodie; Urvoy, Stéphane; Béchade, Jean-Luc; Raepsaet, Caroline; Lacour, Jean-Luc; Bayon, Guy; Ott, Frédéric

    2017-05-01

    This paper gives an overview of a multi-scale experimental study of the secondary hydriding phenomena that can occur in nuclear fuel cladding materials exposed to steam at high temperature (HT) after having burst (loss-of-coolant accident conditions). By coupling information from several facilities, including neutron radiography/tomography, electron probe micro analysis, micro elastic recoil detection analysis and micro laser induced breakdown spectroscopy, it was possible to map quantitatively, at different scales, the distribution of oxygen and hydrogen within M5™ clad segments having experienced ballooning and burst at HT followed by steam oxidation at 1100 and 1200 °C and final direct water quenching down to room temperature. The results were very reproducible and it was confirmed that internal oxidation and secondary hydriding at HT of a cladding after burst can lead to strong axial and azimuthal gradients of hydrogen and oxygen concentrations, reaching 3000-4000 wt ppm and 1.0-1.2 wt% respectively within the β phase layer for the investigated conditions. Consistent with thermodynamic and kinetics considerations, oxygen diffusion into the prior-β layer was enhanced in the regions highly enriched in hydrogen, where the α(O) phase layer is thinner and the prior-β layer thicker. Finally the induced post-quenching hardening of the prior-β layer was mainly related to the local oxygen enrichment. Hardening directly induced by hydrogen was much less significant.

  2. X-ray microprobe characterization of materials: the case for undulators on advanced storage rings

    International Nuclear Information System (INIS)

    Sparks, C.J. Jr.

    1984-01-01

    The unique properties of X rays offer many advantages over electrons and other charged particles for the microcharacterization of materials. X rays are more efficient in exciting characteristic X-ray fluorescence and produce higher fluorescent signals to backgrounds than obtained with electrons. Detectable limits for X rays are a few parts per billion and are 10 -3 to 10 -5 less than for electrons. Energy deposition in the sample by X rays is 10 -3 to 10 -4 less than for electrons for the same detectable concentration. High-brightness storage rings, especially in the 6 GeV class with undulators, will be approximately 10 3 brighter in the X-ray energy range from 5 keV to 35 keV than existing storage rings and provide for X-ray microprobes that are as bright as the most advanced electron probes. Such X-ray microprobes will produce unprecedented low levels of detection in diffraction, EXAFS, Auger, and photoelectron spectroscopies for both chemical characterization and elemental identification. These major improvements in microcharacterization capabilities will have wide-ranging ramifications not only in materials science but also in physics, chemistry, geochemistry, biology, and medicine

  3. Environmental applications of the LANL nuclear microprobe

    International Nuclear Information System (INIS)

    Hickmott, D.D.; Herrin, J.M.; Abell, R.; George, M.; Gauerke, E.R.; Denniston, R.F.

    1997-01-01

    The LANL nuclear microprobe has been used to study the distributions of trace elements (TE) of environmental interest including: (1) metals in coal and fly ash, (2) Pb in the Bandelier Tuff (BT), (3) Ba in tree rings, (4) Mn, Fe, Sr and Y in Yucca Mountain calcites. Micro-PIXE (MP) analyses with 5-10 micrometer spatial resolution provide constraints on processes that redistribute contaminants in the environment, and hence may help answer environmental problems where fine-scale chemical records are important. MP analyses of particulates in coal and ash show that pyrite contains As, Se, Hg and Pb; macerals contain Cr, halogens and S; cenospheres contain As, Se and Ni; and hematite ash contains Ni and As. Understanding these elemental modes of occurrence allows prediction of metal behavior in boilers and may enhance compliance with the Clean Air Act Amendments. Fine-grained high-Pb minerals were identified using SEM and MP analyses of BT minerals. These minerals were from samples associated with deep-groundwater wells containing Pb at levels greater than regulatory limits. Pb is concentrated in Pb minerals (e.g. cerussite), smectite, and hematite formed during low-T alteration of tuff. Understanding mineralogic speciation of metals may provide insights into sources of groundwater pollution. Tree rings from ponderosa pines that grew in a Ba-contaminated drainage were analyzed using MP. Ba concentrations are typically higher in rings that formed after operations discharging Ba to the environment began. Such tree-ring analyses may ultimately provide information on rates of contaminant migration in the environment. TE in zoned calcites from Yucca Mountain were analyzed by MP. Calcites from the saturated zone (SZ) have distinct chemical signatures (high Fe, Mn and low Y). No calcites in the unsaturated zone with SZ chemical signatures were found using MP

  4. “Study of secondary hydriding at high temperature in zirconium based nuclear fuel cladding tubes by coupling information from neutron radiography/tomography, electron probe micro analysis, micro elastic recoil detection analysis and laser induced breakdown spectroscopy microprobe

    Energy Technology Data Exchange (ETDEWEB)

    Brachet, Jean-Christophe, E-mail: jean-christophe.brachet@cea.fr [DEN-Service de Recherches Métallurgiques Appliquées (SRMA), CEA, Université Paris-Saclay, 91191 Gif-sur-Yvette (France); Hamon, Didier; Le Saux, Matthieu [DEN-Service de Recherches Métallurgiques Appliquées (SRMA), CEA, Université Paris-Saclay, 91191 Gif-sur-Yvette (France); Vandenberghe, Valérie [DEN-Service de Recherches Métallurgiques Appliquées (SRMA), CEA, Université Paris-Saclay, 91191 Gif-sur-Yvette (France); DEN-Service d’Etudes Mécaniques et Thermiques (SEMT), CEA, Université Paris-Saclay, 91191 Gif-sur-Yvette (France); Toffolon-Masclet, Caroline; Rouesne, Elodie; Urvoy, Stéphane [DEN-Service de Recherches Métallurgiques Appliquées (SRMA), CEA, Université Paris-Saclay, 91191 Gif-sur-Yvette (France); Béchade, Jean-Luc [DEN-Service de Recherches Métallurgiques Appliquées (SRMA), CEA, Université Paris-Saclay, 91191 Gif-sur-Yvette (France); DEN-Service de Recherches de Métallurgie Physique (SRMP), CEA, Université Paris-Saclay, 91191 Gif-sur-Yvette (France); Raepsaet, Caroline [LEEL, CEA, Université Paris-Saclay, 91191 Gif-sur-Yvette (France); NIMBE, CEA, CNRS, Université Paris-Saclay, 91191 Gif-sur-Yvette Cedex (France); and others

    2017-05-15

    This paper gives an overview of a multi-scale experimental study of the secondary hydriding phenomena that can occur in nuclear fuel cladding materials exposed to steam at high temperature (HT) after having burst (loss-of-coolant accident conditions). By coupling information from several facilities, including neutron radiography/tomography, electron probe micro analysis, micro elastic recoil detection analysis and micro laser induced breakdown spectroscopy, it was possible to map quantitatively, at different scales, the distribution of oxygen and hydrogen within M5™ clad segments having experienced ballooning and burst at HT followed by steam oxidation at 1100 and 1200 °C and final direct water quenching down to room temperature. The results were very reproducible and it was confirmed that internal oxidation and secondary hydriding at HT of a cladding after burst can lead to strong axial and azimuthal gradients of hydrogen and oxygen concentrations, reaching 3000–4000 wt ppm and 1.0–1.2 wt% respectively within the β phase layer for the investigated conditions. Consistent with thermodynamic and kinetics considerations, oxygen diffusion into the prior-β layer was enhanced in the regions highly enriched in hydrogen, where the α(O) phase layer is thinner and the prior-β layer thicker. Finally the induced post-quenching hardening of the prior-β layer was mainly related to the local oxygen enrichment. Hardening directly induced by hydrogen was much less significant. - Highlights: •More than 50% of the gaseous hydrogen produced by the inner clad oxidation absorbed and trapped into prior-β layer. •High hydrogen and oxygen local concentrations, up to 3000–4000 wt. ppm and 1.0–1.2 wt.% respectively, within the β phase. •Enhanced oxygen diffusion into hydrogen enriched prior-β layer, with locally thinner α(O) and thicker prior-β layers. •Post-quenching hardening of the prior-β structure mainly related to the (local) oxygen concentration.

  5. The new confocal heavy ion microprobe beamline at ANSTO: The first microprobe resolution tests and applications for elemental imaging and analysis

    Science.gov (United States)

    Pastuovic, Z.; Siegele, R.; Cohen, D. D.; Mann, M.; Ionescu, M.; Button, D.; Long, S.

    2017-08-01

    The Centre for Accelerator Science facility at ANSTO has been expanded with the new NEC 6 MV ;SIRIUS; accelerator system in 2015. In this paper we present a detailed description of the new nuclear microprobe-Confocal Heavy Ion Micro-Probe (CHIMP) together with results of the microprobe resolution testing and the elemental analysis performed on typical samples of mineral ore deposits and hyper-accumulating plants regularly measured at ANSTO. The CHIMP focusing and scanning systems are based on the OM-150 Oxford quadrupole triplet and the OM-26 separated scan-coil doublet configurations. A maximum ion rigidity of 38.9 amu-MeV was determined for the following nuclear microprobe configuration: the distance from object aperture to collimating slits of 5890 mm, the working distance of 165 mm and the lens bore diameter of 11 mm. The overall distance from the object to the image plane is 7138 mm. The CHIMP beamline has been tested with the 3 MeV H+ and 6 MeV He2+ ion beams. The settings of the object and collimating apertures have been optimized using the WinTRAX simulation code for calculation of the optimum acceptance settings in order to obtain the highest possible ion current for beam spot sizes of 1 μm and 5 μm. For optimized aperture settings of the CHIMP the beam brightness was measured to be ∼0.9 pA μm-2 mrad-2 for 3 MeV H+ ions, while the brightness of ∼0.4 pA μm-2 mrad-2 was measured for 6 MeV He2+ ions. The smallest beam sizes were achieved using a microbeam with reduced particle rate of 1000 Hz passing through the object slit apertures several micrometers wide. Under these conditions a spatial resolution of ∼0.6 μm × 1.5 μm for 3 MeV H+ and ∼1.8 μm × 1.8 μm for 6 MeV He2+ microbeams in horizontal (and vertical) dimension has been achieved. The beam sizes were verified using STIM imaging on 2000 and 1000 mesh Cu electron microscope grids.

  6. Microprobe analysis of PuO2--UO2 nuclear fuel

    International Nuclear Information System (INIS)

    Clark, W.I.; Rasmussen, D.E.; Carlson, R.L.; Highley, D.M.

    1977-01-01

    For the preirradiation characterization of FFTF UO 2 --PuO 2 fuel, a program was developed to determine the preirradiation porosity, grain structure, and microcomposition of the fuel. Two computer programs, MITRAN and MERIT, were developed to evaluate the homogeneity of the fuel. These programs use elemental composition data generated by the electron microprobe. MITRAN determines information on the size and frequency of individual regions, whereas MERIT provides an index of the thermal performance of the fuel and calculated statistical data for comparison to other fuel batches

  7. Structural and electrical characterisation of semiconductor materials using a nuclear microprobe

    International Nuclear Information System (INIS)

    Jamieson, D.N.

    1998-01-01

    The domain of high-resolution imaging techniques (sub-micron) traditionally belongs to low-energy ion beams (ke V ion microprobe), electrons (transmission or scanning electron microscopy), light (near field microscopy), or all variants of scanning probe microscopies. Now, nuclear techniques of analysis, with a nuclear microprobe, have entered this domain, bringing a range of unique techniques for making images. In addition to-conventional techniques like Rutherford (and non-Rutherford) backscattering spectrometry and particle induced x-ray emission for structural characterisation, new ion beam analysis techniques have been developed for electrical characterisation as well. Foremost of these new techniques is ion beam induced charge (IBIC) which has seen an explosion of applications in the last five years to the study of charge transport properties of a variety of materials including polycrystalline diamond and silicon. An additional novel technique is ionoluminescence, which may be used to image various electronic properties of the material. Presented here are some examples of these imaging techniques in a variety of semiconductor materials. In all these examples, the specimens display structural inhomogeneities on the scale of 10 micrometres, making it essential to employ a focused beam. (author)

  8. Structural and electrical characterisation of semiconductor materials using a nuclear microprobe

    Energy Technology Data Exchange (ETDEWEB)

    Jamieson, D.N. [Melbourne Univ., Parkville, VIC (Australia). School of Physics, Microanalytical Centre

    1998-06-01

    The domain of high-resolution imaging techniques (sub-micron) traditionally belongs to low-energy ion beams (ke V ion microprobe), electrons (transmission or scanning electron microscopy), light (near field microscopy), or all variants of scanning probe microscopies. Now, nuclear techniques of analysis, with a nuclear microprobe, have entered this domain, bringing a range of unique techniques for making images. In addition to-conventional techniques like Rutherford (and non-Rutherford) backscattering spectrometry and particle induced x-ray emission for structural characterisation, new ion beam analysis techniques have been developed for electrical characterisation as well. Foremost of these new techniques is ion beam induced charge (IBIC) which has seen an explosion of applications in the last five years to the study of charge transport properties of a variety of materials including polycrystalline diamond and silicon. An additional novel technique is ionoluminescence, which may be used to image various electronic properties of the material. Presented here are some examples of these imaging techniques in a variety of semiconductor materials. In all these examples, the specimens display structural inhomogeneities on the scale of 10 micrometres, making it essential to employ a focused beam. (author). Extended abstract. 18 refs. 4 figs.

  9. Proton microprobe analysis of zinc in skeletal tissues

    Science.gov (United States)

    Doty, S. B.; Jones, K. W.; Kraner, H. W.; Shroy, R. E.; Hanson, A. L.

    1981-03-01

    A proton microprobe with windowless exit port has been used to study zinc distributions in various types of skeletal tissues. The use of an external beam facilitated positioning of the targets for examination of particular points of interest. The proton microprobe is uniquely suited to this work since it combines high sensitivity for zinc determination in thick samples with good spatial resolution. Our measurements on rat and rabbit Achilles tendon showed a significant increase in zinc concentrations as the beam moved from the unmineralized collagen into the mineralized attachment site. Cartilage gave a similar result, with calcified cartilage having a greater zinc level than the articular surface on unmineralized epiphyseal cartilage.

  10. The CEA nuclear microprobe. Description, possibilities, application examples

    International Nuclear Information System (INIS)

    Engelmann, C.; Bardy, J.

    1986-05-01

    The nuclear microprobe installed on one of the beam lines of a 4 MV Van de Graaff located in the Research Center of Bruyeres-le-Chatel is described. The various possibilities, particularly the imaging system, and the performances of the instrument are exposed. Two typical application examples concerning, the first, the determination of the deuterium and tritium in glass microballons, the second, the detection and the localization of carbon and oxygen in the superficial layer of lithium hydride pellets, are given. Preliminary results of some other application examples are also presented. The advantages of the nuclear microprobe over the other ponctual analysis techniques are emphasized. 7 refs, 19 figs [fr

  11. The remote control of nuclear microprobes over the Internet

    International Nuclear Information System (INIS)

    Churms, C.L.; Prozesky, V.M.; Springhorn, K.A.

    1999-01-01

    Whereas the concept of remote control is not new, the required equipment and data link have typically been costly and specialized. With the growing availability of reliable Internet connection, it has however become possible and increasingly attractive to be able to control complex equipment remotely over the Internet. Some methods of Internet Remote control are discussed, bearing in mind the specific needs of nuclear microprobe control. One such system has been implemented at the NAC nuclear microprobe, and even though improvements are envisaged, it is already functioning satisfactorily

  12. Extraterrestrial materials examined by mean of nuclear microprobe

    Science.gov (United States)

    Khodja, H.; Smith, T.; Engrand, C.; Herzog, G.; Raepsaet, C.

    2013-07-01

    Comet fragments, micrometeorites, and Interplanetary Dust Particles (IDPs) are small objects (purpose, we need instruments and methods that provide both microanalysis and detailed imaging. In these respects, the nuclear microprobe offers many potential advantages: (i) the spatial resolution, ∼1 μm is well-matched to the typical object dimensions, (ii) with some reservations, it is non-destructive when carefully conducted, (iii) it is quantitative, and especially sensitive for light elements. At the Saclay nuclear microprobe, we have been performing analyses of extraterrestrial objects for many years. We review some of these studies, emphasizing the specific requirements for successful analyses. We also discuss the potential pitfalls that may be encountered.

  13. Proton microprobe analysis of zinc in skeletal tissues

    International Nuclear Information System (INIS)

    Doty, S.B.; Jones, K.W.; Kraner, H.W.; Shroy, R.E.; Hanson, A.L.

    1980-06-01

    A proton microprobe with windowless exit port was used to study zinc distributions in various types of skeletal tissues. The use of an external beam facilitated positioning of the targets for examination of particular points of interest. The proton microprobe is uniquely suited to this work since it combines high sensitivity for zinc determinations in thick samples with good spatial resolution. Measurements on rat and rabbit Achilles tendon showed a significant increase in zinc concentrations as the beam moved from the unmineralized collagen into the mineralized attachment site. Cartilage gave a similar result, with calcified cartilage having a greater zinc level than the articular surface on unmineralized epiphyseal cartilage

  14. Multidimensional elemental analysis with the Sandia nuclear microprobe

    International Nuclear Information System (INIS)

    Doyle, B.L.

    1988-01-01

    It is well known that many of the ion beam analysis techniques such as Rutherford backscattering spectrometry, elastic recoil detection, resonant and nonresonant nuclear reaction analysis can be used to nondestructively obtain concentration depth profiles of elements in solids. When these techniques are combined with the small beam spot capabilities of a scanned nuclear microprobe, sample composition can be determined in up to three dimensions. This paper will review the various procedures used to collect and analyze multidimensional data using the Sandia nuclear microprobe. In addition, examples of how these data are being used in the study of materials will be shown. (author)

  15. Synchrotron radiation XRF microprobe study of human bone tumor slice

    International Nuclear Information System (INIS)

    Huang Yuying; Zhao Limin; Wang Zhouguang; Shao Hanru; Li Guangcheng; Wu Yingrong; He Wei; Lu Jianxin; He Rongguo

    1999-01-01

    The experimental apparatus of X-ray fluorescence (XRF) microprobe analysis at Beijing Synchrotron Radiation Facility (BSRF) is described. Using the bovine liver as the standard reference, the minimum detection limit (MDL) of trace element was measured to determine the capability of biological sample analysis by synchrotron radiation XRF microprobe. The relative change of the content of the major or trace element in the normal and tumor part of human bone tissue slice was investigated. The experimental result relation to the clinical medicine was also discussed. (author)

  16. An SU-8-based microprobe with a nanostructured surface enhances neuronal cell attachment and growth

    Science.gov (United States)

    Kim, Eunhee; Kim, Jin-Young; Choi, Hongsoo

    2017-12-01

    Microprobes are used to repair neuronal injury by recording electrical signals from neuronal cells around the surface of the device. Following implantation into the brain, the immune response results in formation of scar tissue around the microprobe. However, neurons must be in close proximity to the microprobe to enable signal recording. A common reason for failure of microprobes is impaired signal recording due to scar tissue, which is not related to the microprobe itself. Therefore, the device-cell interface must be improved to increase the number of neurons in contact with the surface. In this study, we developed nanostructured SU-8 microprobes to support neuronal growth. Nanostructures of 200 nm diameter and depth were applied to the surface of microprobes, and the attachment and neurite outgrowth of PC12 cells on the microprobes were evaluated. Neuronal attachment and neurite outgrowth on the nanostructured microprobes were significantly greater than those on non-nanostructured microprobes. The enhanced neuronal attachment and neurite outgrowth on the nanostructured microprobes occurred in the absence of an adhesive coating, such as poly- l-lysine, and so may be useful for implantable devices for long-term use. Therefore, nanostructured microprobes can be implanted without adhesive coating, which can cause problems in vivo over the long term.

  17. High resolution techniques using scanning proton microprobe (SPM)

    International Nuclear Information System (INIS)

    Cholewa, M.; Saint, A.; Prawer, S.; Laird, J.S.; Legge, G.J.F.; Bardos, R.A.; Moorhead, G.F.; Taylor, G.N.; Stuart, S.A.; Howard, J.

    1994-01-01

    The very high resolution (down to 50 nm) achieved with low beam currents (fA) in a scanning ion microprobe have lead to many nondestructive techniques of microanalysis. This paper discusses recent developments and applications in the use of 3-D STIM (scanning transmission ion microscopy) Tomography, channeling STIM and IBIC (ion beam induced charge). (orig.)

  18. The French AEC nuclear microprobe: description and first application examples

    International Nuclear Information System (INIS)

    Engelmann, C.; Bardy, J.

    1983-05-01

    The major components of the microprobe are briefly described. The performances and the varying possibilities authorized by the instrument are given. Some application examples concerning especially the determination of concentration profiles in an aqueous leached glass and the distribution of deuterium in a graphite sample exposed to plasma in a Tokamak device are presented

  19. Use of the ion microprobe in geological dating

    International Nuclear Information System (INIS)

    Compston, W.; Williams, I.S.; Black, L.P.

    1983-01-01

    SHRIMP, the Sensitive High Resolution Ion Microprobe with computerised control and data acquisition system, has recently been commissioned. It is used within the Research School of Earth Sciences, Australian National University, for the isotopic analysis of geological samples. Principles of operation and geological applications are outlined. One example described is the application to Pb-U dating of zircon

  20. Elemental composition of paint cross sections by nuclear microprobe analysis

    International Nuclear Information System (INIS)

    Nens, B.; Trocellier, P.; Engelmann, C.; Lahanier, C.

    1982-09-01

    Physico-chemical characterization of pigments used in artistic painting give precious indications on age of paintings and sometimes on geographical origin of ores. After recalling the principle of protons microprobe, first results obtained by microanalysis of painting cross sections for non destructive microanalysis of impurities in white lead are given [fr

  1. Single ion hit detection set-up for the Zagreb ion microprobe

    Science.gov (United States)

    Smith, R. W.; Karlušić, M.; Jakšić, M.

    2012-04-01

    Irradiation of materials by heavy ions accelerated in MV tandem accelerators may lead to the production of latent ion tracks in many insulators and semiconductors. If irradiation is performed in a high resolution microprobe facility, ion tracks can be ordered by submicrometer positioning precision. However, full control of the ion track positioning can only be achieved by a reliable ion hit detection system that should provide a trigger signal irrespectively of the type and thickness of the material being irradiated. The most useful process that can be utilised for this purpose is emission of secondary electrons from the sample surface that follows the ion impact. The status report of the set-up presented here is based on the use of a channel electron multiplier (CEM) detector mounted on an interchangable sample holder that is inserted into the chamber in a close geometry along with the sample to be irradiated. The set-up has been tested at the Zagreb ion microprobe for different ions and energies, as well as different geometrical arrangements. For energies of heavy ions below 1 MeV/amu, results show that efficient (100%) control of ion impact can be achieved only for ions heavier than silicon. The successful use of the set-up is demonstrated by production of ordered single ion tracks in a polycarbonate film and by monitoring fluence during ion microbeam patterning of Foturan glass.

  2. U-Pb geochronology of zircons form lunar Breccia 73217 using a sensitive high mass-resolution ion microprobe

    International Nuclear Information System (INIS)

    Compston, W.; Williams, I.S.

    1984-01-01

    U-Pb age determinations on four lunar zircons from existing thin-sections of one highland breccia, 73217, using the recently constructed ion microprobe SHRIMP, are reported. The analytical reproducibility of SHRIMP is demonstrated, and procedures for measuring Pb/U, Th/U, and corecting for initial Pb are explained. Electron microprobe analyses for the zircons are also reported. The results show that the four zircons survived the lunar cataclysm without any identifiable effects on their U-Pb systematics. All four indicate a single age of 4356 +23 or -14 m.y. The zircons have experienced small variable amounts of Pb loss since crystallization, from almost zero up to about 10 percent. If this occurred during one later event, then age of the latter is between 1100 and 2300 m.y. 18 references

  3. Idade pulmonar em mulheres com obesidade mórbida

    Directory of Open Access Journals (Sweden)

    Fabiana Sobral Peixoto-Souza

    2013-06-01

    Full Text Available OBJETIVO: Verificar a influência da obesidade mórbida na idade pulmonar de mulheres e correlacionar com a massa corporal, índice de massa corporal (IMC e variáveis ventilatórias. MÉTODOS: Estudo longitudinal realizado com 72 obesas mórbidas e grupo controle constituído de mulheres eutróficas. As voluntárias realizaram um teste de função pulmonar para determinação da idade pulmonar e os resultados foram correlacionados com as variáveis antropométricas e volumes pulmonares. RESULTADOS: As obesas mórbidas apresentaram uma idade pulmonar significativamente superior (50,1 ± 6,8 anos às eutróficas (38,8 ± 11,4 anos. Não houve diferença entre a idade cronológica entre os grupos. Houve uma correlação significativa e positiva entre idade cronológica, massa corporal e IMC com a idade pulmonar (r = 0,3647, 0,4182, 0,3743, respectivamente. Houve uma correlação negativa entre a capacidade vital forçada (CVF, volume expiratório forçado no primeiro segundo (VEF1, razão (VEF1/CVF e volume de reserva expiratório (VRE com a idade pulmonar (r = -0.7565, -0.8769, -0.2723, -0.2417, respectivamente. CONCLUSÃO: A idade pulmonar das obesas mórbidas encontra-se aumentada e está associada com o aumento da massa corporal e IMC.

  4. Early works on the nuclear microprobe for microelectronics irradiation tests at the CEICI (Sevilla, Spain)

    International Nuclear Information System (INIS)

    Palomo, F.R.; Morilla, Y.; Mogollon, J.M.; Garcia-Lopez, J.; Labrador, J.A.; Aguirre, M.A.

    2011-01-01

    Particle radiation effects are a fundamental problem in the use of numerous electronic devices for space applications, which is aggravated with the technology shrinking towards smaller and smaller scales. The suitability of low-energy accelerators for irradiation testing is being considered nowadays. Moreover, the possibility to use a nuclear microprobe, with a lateral resolution of a few microns, allows us to evaluate the behavior under ion irradiation of specific elements in an electronic device. The CEICI is the new CEnter for Integrated Circuits Irradiation tests, created into the facilities at the Centro Nacional de Aceleradores (CNA) in Sevilla-Spain. We have verified that our 3 MV Tandem accelerator, typically used for ion beam characterization of materials, is also a valuable tool to perform irradiation experiments in the low LET (Linear Energy Transfer) region.

  5. Optical system optimization of the microprobe beamline of the Ion Implantation Laboratory (IF-UFRGS), Brazil

    International Nuclear Information System (INIS)

    Bauer, Deiverti de Vila

    2015-01-01

    The aim of the present work is to optimize the microprobe beamline of the Ion Implantation Laboratory (IF-UFRGS). In short, an ion microprobe consists of charged particles focused to the dimensions of a few micrometers. The focusing system is made of two slits for demagnification, a set of magnetic lenses with scanning capability and a reaction chamber. By changing the parameters related to this system, one can optimize the features of the beam. To that end, samples of poly(tereftalate etylene) were irradiated with 2.2 MeV H+ ions and etched, yielding 2D microstructures with high aspect ratio. The analysis of the structures with Scanning Electron Microscopy proved to be an important tool in order to establish a correlation between the size of the microstructures and the parameters of the focusing system. In this work, the causes leading to a beam enlargement are discussed, as well as the aberrations which affect the system. Finally, the advantages of using ions for lithography purposes is pointed out. (author)

  6. Characterization of semiconductor and frontier materials by nuclear microprobe technology

    International Nuclear Information System (INIS)

    Zhu Jieqing; Li Xiaolin; Yang Changyi; Lu Rongrong; Wang Jiqing; Guo Panlin

    2002-01-01

    The nuclear microprobe technology is used to characterize the properties of semiconductor and other frontier materials at the stages of their synthesis, modification, integration and application. On the basis of the beam current being used, the analytical nuclear microprobe techniques being used in this project can be divided into two categories: high beam current (PIXE, RBS, PEB) or low beam current (IBIC, STIM) techniques. The material properties measured are the thickness and composition of a composite surface on a SiC ceramic, the sputtering-induced surface segregation and depth profile change in a Ag-Cu binary alloy, the irradiation effects on the CCE of CVD diamond, the CCE profile at a polycrystalline CVD diamond film and a GaAs diode at different voltage biases and finally, the characterization of individual sample on an integrated material chip. (author)

  7. Applications of the ion microprobe to geochemistry and cosmochemistry

    International Nuclear Information System (INIS)

    Shimizu, N.; Hart, S.R.

    1982-01-01

    When a solid surface is subjected to a bombardment of energetic ions, material is ejected from the surface in a process known as sputtering. A part of the sputtered material is ionized and these secondary ions can be analyzed with a mass spectrometer according to a technique known as secondary ion mass spectrometry (SIMS). A description is presented of the present status of geochemical and cosmochemical applications of the ion microprobe. Attention is given to the sputtering event, molecular ion interferences, aspects of isotopic fractionation, secondary ion intensities in polycomponent materials, and questions of trace element analysis. Geochemical applications of the ion microprobe are based on certain advantages over other analytical techniques. These advantages are related to high sensitivity, low background, and the capability of in situ analysis of isotopic composition. The distribution of trace elements in minerals is considered, along with isotope anomalies, isotope zoning, diffusion studies, and depth profiling

  8. Installation and performance of the Budapest-Hamburg proton microprobe

    International Nuclear Information System (INIS)

    Kovacs, I.; Kocsonya, A.; Kostka, P.; Szokefalvi-Nagy, Z.; Schrang, K.; Krueger, A.; Niecke, M.

    2005-01-01

    A new scanning proton microprobe has been installed at the 5 MV Van de Graaff accelerator of the KFKI Research Institute for Particle and Nuclear Physics. It is the energy-upgraded version of the Hamburg proton microprobe dismantled in 2001. The probe forming system includes a pair of focusing quadrupoles and an additional quadrupole pair in front of it, which is applied to increase the proton beam divergence. The average probe size at 2.5 MeV proton energy is 2.2 μm x 1.1 μm. The test results on stability and the preliminary experiments on cement corrosion and fish otoliths are also presented

  9. Wavelength dispersive μPIXE setup for the ion microprobe

    Energy Technology Data Exchange (ETDEWEB)

    Fazinić, S., E-mail: stjepko.fazinic@irb.hr [Laboratory for Ion Beam Interactions, Division of Experimental Physics, Rudjer Bošković Institute, Bijenicka cesta 54, 10000 Zagreb (Croatia); Božičević Mihalić, I.; Tadić, T.; Cosic, D.; Jakšić, M. [Laboratory for Ion Beam Interactions, Division of Experimental Physics, Rudjer Bošković Institute, Bijenicka cesta 54, 10000 Zagreb (Croatia); Mudronja, D. [Croatian Conservation Institute, Grškovićeva 23, 10000 Zagreb (Croatia)

    2015-11-15

    We have developed a small wavelength dispersive X-ray spectrometer to explore the possibility of performing chemical speciation on microscopic samples utilizing focused ion beams available at the Rudjer Boskovic Institute ion microprobe. Although PIXE spectra are in principle chemically invariant, small influence of chemical effects could be observed even with Si(Li) or SDD detectors. Such chemical effects can be clearly seen with high resolution crystal X-ray spectrometers having energy resolution of several eV. A dedicated vacuum chamber, housing the diffraction crystal, sample holder and CCD X-ray detector, was constructed and positioned behind the main ion microprobe vacuum chamber. Here we will briefly describe the spectrometer, and illustrate its capabilities on measured K X-ray spectra of selected sulfur compounds. We will also demonstrate its abilities to resolve K and M X-ray lines irresolvable by solid state ED detectors usually used in PIXE.

  10. Development of a nuclear microprobe and its application to neurobiology

    International Nuclear Information System (INIS)

    Tapper, Staffan.

    1989-01-01

    A nuclear microprobe has been developed at the Pelletron accelerator in Lund. The design of the achromatic beam focusing system as well as of the beam scanning system is described. The focusing system consists of three magnetic- and three electrostatic quadrupole lenses together forming an chromatic quadrupole triplet with symmetric focusing properties. The beam quality from the accelerator has been improved by use of ultrathin stripper foils. The nuclear microprobe set-up has been applied to investigation of brain tissue specimens. The elemantal disorder following epileptic seizures has been studied by micro-PIXE analysis. A combination of macro- and micro-PIXE analysis have been utilized in an investigaiton of elemental differences between normal human brain and human brain tumours. In the context of the quantification procedure in micro-PIXE analysis, callibration and X-ray detector response function are discussed. (author)

  11. Raman microprobe study of heat-treated pitches

    Energy Technology Data Exchange (ETDEWEB)

    Cottinet, D.; Couderc, P.; Saint Romain, J.L.; Dhamelincourt, P.

    1988-01-01

    A series of heat-treated pitches from the same coal-tar precursor is investigated by means of a Raman microprobe. Separated Raman spectra are obtained for the isotropic phase and the mesophase. The evolutions observed are characteristic of the structural rearrangement change in the two phases. They correlate well with the observations reported in literature and obtained by using different methods of structural investigations.

  12. Design considerations for an x-ray microprobe

    International Nuclear Information System (INIS)

    Howells, M.R.; Hastings, J.B.

    1982-01-01

    The optical design of a fluorescent microprobe covering the x-ray region from 2 to 16 keV is considered for the NSLS x-ray ring. The limit on detectability is from total flux (photons/μm 2 ) and several design choices are considered to match the optical system to the storage ring to maximize throughput. The tradeoffs in image quality and energy resolution of these designs have been considered and within these constraints two firm proposals are presented

  13. 7th international conference on Nuclear microprobe technology and applications

    International Nuclear Information System (INIS)

    2000-01-01

    This colloquium gives an up-to-date report on the continuously advancing applications and development of microbeam technology. It presents abstracts and oral contributions in the following domains: microprobes facilities, analysis techniques, imaging techniques, micro-ion beam modification of materials, microelectronics, applications in Material Sciences in Biology in Medicine in earth and planetary Sciences in environment in art in archaeology, alternative techniques. (A.L.B.)

  14. Applications of heavy ion microprobe for single event effects analysis

    International Nuclear Information System (INIS)

    Reed, Robert A.; Vizkelethy, Gyorgy; Pellish, Jonathan A.; Sierawski, Brian; Warren, Kevin M.; Porter, Mark; Wilkinson, Jeff; Marshall, Paul W.; Niu, Guofu; Cressler, John D.; Schrimpf, Ronald D.; Tipton, Alan; Weller, Robert A.

    2007-01-01

    The motion of ionizing-radiation-induced rogue charge carriers in a semiconductor can create unwanted voltage and current conditions within a microelectronic circuit. If sufficient unwanted charge or current occurs on a sensitive node, a variety of single event effects (SEEs) can occur with consequences ranging from trivial to catastrophic. This paper describes the application of heavy ion microprobes to assist with calibration and validation of SEE modeling approaches

  15. A study of VMS ore deposits by the proton microprobe

    International Nuclear Information System (INIS)

    Huston, D.L.; Large, R.R.; Bottril, R.S.; Sie, S.H.; Ryan, C.G.

    1991-01-01

    As part of studies into the mineralogical distribution of gold in volcanogenic massive sulfide (VMS) ore deposits PIXE analysis by the proton microprobe has been used to determine the gold content of pyrite and arsenopyrite from the Rosebery, Mt. Chalmers and Mt. Lyell deposits. In addition, the concentrations of Co, Ni, Cu, Zn, As, Sr, Y, Zr, Mo, Ag, Sb, Te, Au, Tl, Pb and Bi were also determined. 4 refs., 1 tab

  16. Digital pulse processor for ion beam microprobe imaging

    International Nuclear Information System (INIS)

    Bogovac, M.; Jaksic, M.; Wegrzynek, D.; Markowicz, A.

    2009-01-01

    Capabilities of spectroscopic ion beam analysis (IBA) techniques that are available in ion microprobe facilities can be greatly improved by the use of digital pulse processing. We report here development of a digital multi parameter data acquisition system suitable for IBA imaging applications. Input signals from charge sensitive preamplifier are conditioned by using a simple circuit and digitized with fast ADCs. The digitally converted signals are processed in real time using FPGA. Implementation of several components of the system is presented.

  17. The nuclear microprobe of the CENBG: the choices

    International Nuclear Information System (INIS)

    Llabador, Y.

    1987-04-01

    A microbeam line with a spatial resolution of the micrometer order has been set on the Van de Graaf of the Bordeaux-Gradignan nuclear center. This report presents the different stages of the microprobe design: the experimental device which has been chosen, the reason of the different choices, the traps to keep out of during the construction (for instance, the accuracy of the mechanical standards) [fr

  18. The Fudan nuclear microprobe set-up and performance

    International Nuclear Information System (INIS)

    Zhong, L.; Zhuang, W.; Shen, H.; Mi, Y.; Wu, Y.; Liu, B.; Yang, M.; Cheng, H.

    2007-01-01

    A new scanning nuclear microprobe has been constructed at the Institute of Modern Physics in Fudan University, to replace the old microbeam system which had been running for more than ten years. The key parts were purchased from Oxford Microbeams Ltd., including triplet quadrupole lens (model OM-150), collimator slits, scanning system, target chamber, and data acquisition system. Ion beams are provided from a NEC 9SDH-2 Tandem accelerator. Three CCD cameras and multiple monitors were installed to assist beam adjust. The design of beam line and beam monitors is described. Beam optics calculations were carried out based on the specific Fudan microprobe system geometry, and the results regarding beam line performance and limitations of the spacial resolution are presented and discussed here. A comparison with experimental results is given as well. About 1.5 μm beam spot size could be achieved with a 3 MeV proton beam at a current of around 10 pA. Recently, the new microprobe is applied to obtain information of fly ash particle, algae cell and otoliths

  19. Depth Probing Soft X-ray Microprobe (DPSXRM) for High Resolution Probing of Earth's Microstructural Samples

    Science.gov (United States)

    Dikedi, P. N.

    2015-12-01

    The Cambrian explosion; occurrence of landslides in very dry weather conditions; rockslides; dead, shriveled-up and crumbled leaves possessing fossil records with the semblance of well preserved, flat leaves; abundance of trilobite tracks in lower and higher rock layers; and sailing stones are enigmas demanding demystifications. These enigmas could be elucidated when data on soil structure, texture and strength are provided by some device with submicrometre accuracy; for these and other reasons, the design of a Depth Probing Soft X-ray Microprobe (DPSXRM), is being proposed; it is expected to deliver soft X-rays, at spatial resolution, ϛ≥600nm and to probe at the depth of 0.5m in 17s. The microprobe is portable compared to a synchrotron radiation facility (Diamond Light Source has land size of 43,300m2); spatial resolution,ϛ , of the DPSXRM surpasses those of the X-ray Fluorescence microanalysis (10µm), electron microprobe (1-3µm) and ion microprobe (5->30µm); the DPSXRM has allowance for multiple targets. Vanadium and Manganese membranes are proposed owing to respective 4.952KeV VKα1 and 5.899KeV MnKα1 X-rays emitted, which best suits micro-probing of Earth's microstructural samples. Compound systems like the Kirk-Patrick and Baez and Wolter optics, aspheric mirrors like elliptical and parabolic optics, small apertures and Abbe sine condition are employed to reduce or remove astigmatism, obliquity, comatic and spherical aberrations—leading to good image quality. Results show that 5.899KeV MnKα1 and 4.952KeV VKα1 soft X-rays will travel a distance of 2.75mm to form circular patches of radii 2.2mm and 2.95mm respectively. Zone plate with nth zone radius of 1.5mm must be positioned 1.5mm and 2mm from the electron gun if circular patches must be formed from 4.952KeV VKα1 and 5.899KeV MnKα1 soft X-rays respectively. The focal lengths of 0.25μm≤ƒ≤1.50μm and 0.04μm≤ƒ≤0.2μm covered by 4.952KeV VKα1 and 5.899KeV Mn Kα1 soft X-Rays, will

  20. Ion channelling analysis of pre-amorphised silicon diodes using a nuclear microprobe

    International Nuclear Information System (INIS)

    Thornton, J.; Paus, K.C.

    1988-01-01

    Aligned and random ion channelling analysis was performed on p + n diode structures in silicon, with the Surrey nuclear microprobe. Three different types of diode were investigated, each pre-amorphised by a different ion (Si + , Ge + or Sn + ) before the p + region was formed by BF 2 + implantation. The ion channelling measurements are presented and compared with previously published electrical measurements on these diodes. Relatively large residual disorder and junction leakage currents were found for the Si + pre-amorphised diodes; however, all the diodes were leaky. The results are consistent with dislocation loops within the depletion regions of the diodes causing both the residual disorder and the large leakage currents. Cross-sectional transmission electron microscopy studies support this model. (author)

  1. Microprobe and SEM Analysis of a Meteorite from the Campo del Cielo Fall

    International Nuclear Information System (INIS)

    Cabanillas, E. D.; Palacios, T. A.

    2003-01-01

    Full Text: Meteorites are unique pieces in nature having not only the enigmatic connotations of the unknown but also are the easier obtained samples of the exterior universe. Furthermore they are the unique alloys that suffered modifications done during enormous periods of time in space and in land The Campo del Cielo fall, occurred more than 5000 years ago, gave hundredths of pieces some of them well studied. We have studied one of the minor pieces from the fall and with microprobe and scanning electronic microscopy analysis we determined the composition of Schreibersite and Rhabdite phosphides of iron and nickel. This study was performed to establish relationships between the duration of alloys and the design of disposal of high level and long lived radioactive waste

  2. Ion beam induced luminescence from diamond using an MeV ion microprobe

    Energy Technology Data Exchange (ETDEWEB)

    Bettiol, A A; Jamieson, D N; Prawer, S; Allen, M G [Melbourne Univ., Parkville, VIC (Australia). School of Physics

    1994-12-31

    Analysis of the luminescence induced by a MeV ion beam offers the potential to provide useful information about the chemical properties of atoms in crystals to complement the information provided by more traditional Ion Beam Analysis (IBA) such as Rutherford Backscattering Spectrometry (RBS), ion channeling and Particle Induced X-ray Emission (PIXE). Furthermore, the large penetration depth of the MeV ion beam offers several advantages over the relatively shallow penetration of keV electrons typically employed in cathodoluminescence. An Ion Beam Induced Luminescence (IBIL) detection system was developed for the Melbourne microprobe that allows the spatial mapping of the luminescence signal along with the signals from RBS and PIXE. Homoepitaxial diamond growth has been studied and remarkable shifts in the characteristic blue luminescence of diamond towards the green were observed in the overgrowth. This has been tentatively identified as being due to transition metal inclusions in the epitaxial layers. 8 refs., 2 refs.

  3. Study of ancient Islamic gilded pieces combining PIXE-RBS on external microprobe with sem images

    International Nuclear Information System (INIS)

    Ynsa, M.D.; Gutierrez, P.C.; Enguita, O.; Chamon, J.; Pardo, A.I.; Arroyo, M.; Barrio, J.; Gomez-Morilla, I.; Ferretti, M.; Climent-Font, A.

    2008-01-01

    Numerous metallic objects with very aesthetic and technological qualities have been recovered by archaeological excavations. Adequate processes of restoration and conservation treatments require the accurate determination of the elemental composition and distribution within the objects, as well as the identification of the nature and distribution of the corrosion products. Ideally the identification method should cause no alteration in the sample. In this work, different archaeological pieces with a gilded look have been characterized using simultaneously PIXE and RBS at the CMAM external microprobe in order to study the gilding metalworking done in the Iberian Peninsula during the Middle Ages. The gold layer thickness and its elemental concentrations of Ag, Au and Hg were determined by both techniques and compared with the scanning electron microscopy images obtained for some fragments of pieces. (orig.)

  4. Microprobe study of fission product behavior in high-burnup HTR fuels

    International Nuclear Information System (INIS)

    Kleykamp, H.

    Electron microprobe analysis of irradiated coated particles with high burnup (greater than 50 percent fima) gives detailed information on the chemical state and the transport behavior of the fission products in UO 2 and UC 2 kernels and in the coatings. In oxide fuel kernels, metallic inclusions and ceramic precipitations are observed. The solubility behavior of the fission products in the fuel matrix has been investigated. Fission product inclusions could not be detected in carbide fuel kernels; post irradiation annealed UC 2 kernels, however, give information on the element combinations of some fission product phases. Corresponding to the chemical state in the kernel, Cs, Sr, Ba, Pd, Te and the rare earths are released easily and diffuse through the entire pyrocarbon coating. These fission products can be retained by a silicon carbide layer. The initial stage of a corrosive attack of the SiC coating by the fission products is evidenced

  5. Ion beam induced luminescence from diamond using an MeV ion microprobe

    Energy Technology Data Exchange (ETDEWEB)

    Bettiol, A.A.; Jamieson, D. N.; Prawer, S.; Allen, M.G. [Melbourne Univ., Parkville, VIC (Australia). School of Physics

    1993-12-31

    Analysis of the luminescence induced by a MeV ion beam offers the potential to provide useful information about the chemical properties of atoms in crystals to complement the information provided by more traditional Ion Beam Analysis (IBA) such as Rutherford Backscattering Spectrometry (RBS), ion channeling and Particle Induced X-ray Emission (PIXE). Furthermore, the large penetration depth of the MeV ion beam offers several advantages over the relatively shallow penetration of keV electrons typically employed in cathodoluminescence. An Ion Beam Induced Luminescence (IBIL) detection system was developed for the Melbourne microprobe that allows the spatial mapping of the luminescence signal along with the signals from RBS and PIXE. Homoepitaxial diamond growth has been studied and remarkable shifts in the characteristic blue luminescence of diamond towards the green were observed in the overgrowth. This has been tentatively identified as being due to transition metal inclusions in the epitaxial layers. 8 refs., 2 refs.

  6. A tunable x-ray microprobe using synchrotron radiation

    International Nuclear Information System (INIS)

    Wu, Y.; Thompson, A.C.; Underwood, J.H.; Giauque, R.D.; Chapman, K.; Rivers, M.L.; Jones, K.W.

    1989-08-01

    We describe an x-ray microprobe using multilayer mirrors. Previously, we had demonstrated a Kirkpatrick-Baez type focusing system working at both 8 and 10 keV and successfully applied it to a variety of applications, including the determination of elemental contents in fluid inclusions. In this paper, we show that the usable excitation energy for this microprobe is not restricted to between 8 and 10 keV, and furthermore, it can be simply tuned in operation. A 10-keV x-ray fluorescence microprobe can be used to measure the concentration of the elements form potassium (Z = 19) to zinc (Z = 30) using K x-ray lines, and from cadmium (Z = 48) to erbium (Z = 68) using L x-ray lines. There are a number of geologically important elements in the gap between gallium (Z = 31) and silver(Z = 47) and also with Z > 68. In order to cover this range, a higher excitation energy is required. On the other hand, for samples that contain major elements with absorption edges lower than the excitation energy, it would be hard to detect other mirror elements because of the strong signal from the major elements and the background they produce. In this case, a tunable x-ray source can be used to avoid the excitation of the major elements. We demonstrate that, with the existing setup, it is possible to tune the excitation energy from 6 keV to 14 keV, in this range, the intensity does not decrease by more than one order of magnitude. As an illustration, a geological sample was examined by using two different excitation energy range as well as the possibility of improving the intensity. 11 refs., 5 figs

  7. Proton microprobe analysis of zinc in skeletal tissues

    International Nuclear Information System (INIS)

    Doty, S.B.; Jones, K.W.; Kraner, H.W.; Shroy, R.E.; Hanson, A.L.

    1981-01-01

    A proton microprobe with windowless exit port has been used to study zinc distributions in various types of skeletal tissues. The use of an external beam facilitated positioning of the targets for examination of particular points of interest. The proton micorprobe is uniquely suited to this work since it combines high sensitivity for zinc determinations in thick samples with good spatial resolution. Our measurements on rat and rabbit Achilles tendon showed a significant increase in zinc concentrations as the beam moved from the unmineralized collagen into the mineralized attachment site. Cartilage gave a similar result, with calcified cartilage having a greater zinc level than the articular surface on unmineralized epiphyseal cartilage. (orig.)

  8. Enhancements to the analytical facilities at the GNS proton microprobe

    International Nuclear Information System (INIS)

    Barry, B.J.; Markwitz, A.; Kennedy, V.J.; Trompetter, W.J.

    2005-01-01

    In recent years a number of detection systems have been added to the proton microprobe facility at GNS Science. Particular additions have been a large area HPGe detector and a system for scanning transmission imaging microscopy. The HPGe detector has improved detection sensitivity, particularly for higher energy K x-rays where energy resolution is of lesser importance. The scanning microscopy system has enabled mapping of areal densities in biological samples to give accurate elemental maps. Examples are given of these applications. (author). 22 refs., 7 figs

  9. Operation and acquisition automation of a nuclear microprobe

    International Nuclear Information System (INIS)

    Simond, Isabelle

    1990-01-01

    The purpose of this work was to design the hardware and the software parts of data acquisition and its graphical analyses of a nuclear microprobe. Our realisation was built from a microprocessor 68020 and specialized co-processors on a VME bus. The more important demand was the amount of time required to collect the data and to perform the graphical analyses during the acquisition. To overcome this problem, we adapted a real time operating system and its kernel to our need, and built special graphical processes. (author) [fr

  10. Lentes de contacto em idade pediátrica

    OpenAIRE

    Mota, M; Vendrell, C; Ramalho, M; Santos, C; Pedrosa, C; Coutinho, I; Lopes, AS; Silva, D

    2015-01-01

    Revisão sobre os tipos de lentes de contacto para utilização na idade pediátrica. Regras de adaptação, indicações e contraindicações ao uso de lentes de contacto na criança. Descrição das melhores opções na afaquia.

  11. New improvements in the characterization of refractory gold in pyrites: an electron microprobe, Moessbauer spectrometry and ion microprobe study

    International Nuclear Information System (INIS)

    Marion, P.; Holliger, P.; Boiron, M.C.; Cathelineau, M.; Wagner, F.E.

    1991-01-01

    Studies of pyrites by Moessbauer spectroscopy have shown the presence of gold in a combined state probably inserted within the lattice. In order to enhance detection limits for in-situ quantitative gold analyses, new SIMS investigations have been made thanks to a Resistive Anode Encorder record of the ion emissions, which provides digital images or scans of any part of the analyzed volume. Quantitative analysis of gold have been carried out thanks to 2 MeV ion implantation of gold in reference sulfide crystals, and the bulk composition of a pyrite grain has been determined. Some strong enrichments in gold and arsenic at the crystal margin attest fluctuations in the fluid chemistry and may be interpreted as a final growth zone, which is similar to that observed on arsenopyrite crystals. This multidisciplinary approach constitutes a powerful tool for the investigation of the insertion and distribution of trace elements within crystals, especially gold in sulfides at low contents down to a few ppm. (author)

  12. Realtime control system for microprobe beamline at PLS

    Energy Technology Data Exchange (ETDEWEB)

    Yoon, J.C.; Lee, J.W.; Kim, K.H.; Ko, I.S. [Pohang Accelerator Laboratory, POSTECH, Pohang (Korea)

    1998-11-01

    The microprobe beamline of the Pohang Light Source (PLS) consists of main and second slits, a microprobe system, two ion chambers, a video-microscope, and a Si(Li) detector. These machine components must be controlled remodely through the computer system to make user's experiments precise and speedy. A real-time computer control system was developed to control and monitor these components. A VMEbus computer with an OS-9 real-time operating system was used for the low-level data acquisition and control. VME I/O modules were used for the step motor control and the scalar control. The software has a modular structure for the maximum performance and the easy maintenance. We developed the database, the I/O driver, and the control software. We used PC/Windows 95 for the data logging and the operator interface. Visual C{sup ++} was used for the graphical user interface programming. RS232C was used for the communication between the VME and the PC. (author)

  13. Microprobe analysis of teeth by synchrotron radiation: environmental contamination

    International Nuclear Information System (INIS)

    Pinheiro, T.; Carvalho, M.L.; Casaca, C.; Barreiros, M.A.; Cunha, A.S.; Chevallier, P.

    1999-01-01

    An X-ray fluorescence set-up with microprobe capabilities, installed at the Laboratoire pour l'Utilisation du Rayonnement Electromagnetique (LURE) synchrotron (France) was used for elemental determination in teeth. To evaluate the influence of living habits in dental elemental composition nine teeth collected post-mortem were analysed, five from a miner and four from a fisherman. All teeth from the fisherman were healthy. From the miner some teeth were carious and one of them was filled with metallic amalgam. Teeth were sliced under the vertical plane and each slice was scanned from the root to the enamel for elemental profile determination. The synchrotron microprobe resolution was of 100 μm and incident photons of 18 keV energy were used. The elemental concentration values found suggest heterogeneity of the teeth material. Moreover, the distinct profiles for Mn, Sr, Br and Pb were found when teeth from the miner and from the fisherman are compared which can be associated with dietary habits and environmental influence. Higher concentrations of Mn and Sr were found for the fisherman teeth. In addition, Br was only observed in this group of teeth. Pb levels are higher for the miner teeth in particular for dentine regions. The influence of amalgam, such as, increase of Zn and Hg contents in the teeth material, is only noticed for the immediate surroundings of the treated cavity

  14. Stained glasses under the nuclear microprobe: A window into history

    Energy Technology Data Exchange (ETDEWEB)

    Vilarigues, M. [Dep. de Conservacao e Restauro and R and D Unit Vidro e da Ceramica Para as Artes, FCT-UNL, Quinta da Torre, 2829-516 Caparica (Portugal)], E-mail: mgv@fct.unl.pt; Fernandes, P. [Dep. de Conservacao e Restauro and R and D Unit Vidro e da Ceramica Para as Artes, FCT-UNL, Quinta da Torre, 2829-516 Caparica (Portugal); Alves, L.C.; Silva, R.C. da [Dep. Fisica, LFI, ITN, E.N.10, 2686-953 Sacavem (Portugal)

    2009-06-15

    Stained glass fragments from the 15th, 16th and 20th centuries, belonging to Mosteiro de Santa Maria da Vitoria, Batalha (Portugal), were characterised non-destructively in a nuclear microprobe. The work aimed at finding the composition of the glasses and glass paintings and relating these with the corresponding production periods. The elemental compositions of the glass fragments were obtained by means of scanning micro-beam Particle Induced X-ray Emission ({mu}-PIXE) spectrometry in selected cross-sections. These were complemented by micro X-Ray fluorescence spectrometry. Characterisation of colour was performed by optical absorption spectroscopy in the UV-vis range, while the corrosion products were identified by optical microscopy and {mu}-FTIR (Fourier Transform Infra Red) spectroscopy in combination with the data generated by {mu}-PIXE. Nuclear microprobe analysis allowed unveiling the compositions and structures, in particular of glass paintings and corrosion products. While it is not surprising that Fe, Cu and Pb were the main elements identified in the grisaille paintings of all studied periods, as well as Ag and Cu found in the glasses decorated with yellow silver painting, their distribution gave important clues on the materials and techniques used to manufacture these stained glasses. Furthermore, it allowed establishing a definite relation between the compositions found and the periods of production, with the added bonus of correctly reassigning the manufacturing period of some samples.

  15. Artesanato na terceira idade: um estudo na cidade de Sinop

    Directory of Open Access Journals (Sweden)

    Rosane Marlene Weber

    2012-06-01

    Full Text Available O presente artigo sobre o artesanato e a Terceira Idade, pesquisa realizada em 2011, teve como metodologia o Estudo de Caso do tipo etnográfico. A metodologia de investigação ocorreu por meio de entrevistas semiestruturadas, orais e transcritas, observação e fotografias dos artesanatos em locais de venda e nas residências dos artesãos. Os sujeitos da pesquisa foram: a presidente da Associação da Casa do Artesão de Sinop-MT e oito artesãos. O objetivo foi mostrar a importância do artesanato como atividade educacional e como produtora de autonomia e autoria para os artesãos da Terceira Idade, motivados em realizar este trabalho nesta fase da vida. Para o embasamento teórico utilizou-se obras de Paulo Freire, Moacir Gadotti e sobre a Terceira Idade a coleção de Vivaidade com a organizadora Anita Liberalesso Neri. A análise das entrevistas mostrou que o artesanato traz autonomia educacional quando o idoso busca sozinho aprender sobre o objeto a ser realizado, assim como autonomia financeira, uma vez que a venda do artesanato proporciona certa independência econômica. Em relação ao sentimento de autoria das peças criadas constatou-se muita satisfação e realização, o que motiva a continuar sendo úteis e produtivos na Terceira Idade com muita criatividade. Palavras-chave: educação; terceira idade; artesanato; autonomia; autoria.

  16. General theory of three-dimensional radiance measurements with optical microprobes RID A-1977-2009

    DEFF Research Database (Denmark)

    FukshanskyKazarinova, N.; Fukshansky, L.; Kuhl, M.

    1997-01-01

    Measurements of the radiance distribution and fluence rate within turbid samples with fiber-optic radiance microprobes contain a large variable instrumental error caused by the nonuniform directional sensitivity of the microprobes. A general theory of three-dimensional radiance measurements...

  17. A new scanning proton microprobe with long focus

    International Nuclear Information System (INIS)

    Zhu Jieqing; Li Minqian; Mao Yu; Chen Hanmin; Gu Yingmei; Yang Changyi; Sheng Kanglong

    1991-01-01

    A new scanning proton microprobe equipped with a long focus Russian magnetic quadruplet is set up. With excellent performances of ion optics, it can be used to do experiments of PIXE, RBS, RFS, NRA and channelling simultaneously within a micron-region. The power supplies for quadruplet and scanning coils are controlled by an IBM-PC computer and a scanning graphical monitor based on an Apple IIe microcomputer provides convenience of searching for an interesting area to scan. The advanced modes of the fast random scan and the event-by-event data collection make it possible to treat the multi-parameter and multi-detector data by means of the strategy of TQSA (Total quantitative scanning analysis). There are three types of graphical display including the innovation of three dimensional contour mapping

  18. Implementation of ionoluminescence in the AGLAE scanning external microprobe

    International Nuclear Information System (INIS)

    Pichon, L.; Calligaro, T.; Gonzalez, V.; Lemasson, Q.; Moignard, B.; Pacheco, C.

    2015-01-01

    The scope of this work is to present the implementation of an IBIL imaging system in the scanning external microprobe of the AGLAE facility so as to correlate luminescence and composition maps provided by PIXE, RBS and PIGE. The challenging integration of the optical spectrometer, due to incompatibility of acquisition timings and data formats with the other IBA channels has motivated the development of a specific acquisition system. This article details the IBIL setup and explains the technical solutions retained for the coupling of IBIL with IBA techniques in order to produce fast and large IBIL-IBA maps. The IBIL maps stored in the same format as the PIXE, RBS and PIGE ones can be visualised and compared using the dedicated AGLAEmap program or the PyMCA processing package. An example of such a coupled mapping on Mesoamerican jade is presented to emphasise the interest of performing simultaneously IBA and IBIL large mappings

  19. Wireless cardiac action potential transmission with ultrasonically inserted silicon microprobes

    International Nuclear Information System (INIS)

    Shen, C J; Ramkumar, A; Lal, A; Gilmour, R F Jr

    2011-01-01

    This paper reports on the integration of ultrasonically inserted horn-shaped cardiac probes with wireless transmission of 3D cardiac action potential measurement for applications in ex vivo preparations such as monitoring the onset of ventricular fibrillation. Ultrasonically inserted silicon horn probes permit reduced penetration force during insertion, allowing silicon, a brittle material, to penetrate cardiac tissue. The probes also allow recording from multiple sites that are lithographically defined. An application-specific integrated circuit has been designed with a 40 dB amplifying stage and a frequency modulating oscillator at 95 MHz to wirelessly transmit the recorded action potentials. This ultrasonically inserted microprobe wireless system demonstrates the initial results in wireless monitoring of 3D action potential propagation, and the extraction of parameters of interest including the action potential duration and diastolic interval

  20. Nuclear microprobe imaging of gallium nitrate in cancer cells

    Science.gov (United States)

    Ortega, Richard; Suda, Asami; Devès, Guillaume

    2003-09-01

    Gallium nitrate is used in clinical oncology as treatment for hypercalcemia and for cancer that has spread to the bone. Its mechanism of antitumor action has not been fully elucidated yet. The knowledge of the intracellular distribution of anticancer drugs is of particular interest in oncology to better understand their cellular pharmacology. In addition, most metal-based anticancer compounds interact with endogenous trace elements in cells, altering their metabolism. The purpose of this experiment was to examine, by use of nuclear microprobe analysis, the cellular distribution of gallium and endogenous trace elements within cancer cells exposed to gallium nitrate. In a majority of cellular analyses, gallium was found homogeneously distributed in cells following the distribution of carbon. In a smaller number of cells, however, gallium appeared concentrated together with P, Ca and Fe within round structures of about 2-5 μm diameter located in the perinuclear region. These intracellular structures are typical of lysosomial material.

  1. Nuclear microprobe imaging of gallium nitrate in cancer cells

    International Nuclear Information System (INIS)

    Ortega, Richard; Suda, Asami; Deves, Guillaume

    2003-01-01

    Gallium nitrate is used in clinical oncology as treatment for hypercalcemia and for cancer that has spread to the bone. Its mechanism of antitumor action has not been fully elucidated yet. The knowledge of the intracellular distribution of anticancer drugs is of particular interest in oncology to better understand their cellular pharmacology. In addition, most metal-based anticancer compounds interact with endogenous trace elements in cells, altering their metabolism. The purpose of this experiment was to examine, by use of nuclear microprobe analysis, the cellular distribution of gallium and endogenous trace elements within cancer cells exposed to gallium nitrate. In a majority of cellular analyses, gallium was found homogeneously distributed in cells following the distribution of carbon. In a smaller number of cells, however, gallium appeared concentrated together with P, Ca and Fe within round structures of about 2-5 μm diameter located in the perinuclear region. These intracellular structures are typical of lysosomial material

  2. Data acquisition for X ray microprobe. User's manual

    International Nuclear Information System (INIS)

    2002-01-01

    A modified data acquisition software for X ray microprobe was developed by the Physics Group, Instrumentation Unit, IAEA Laboratories at Seibersdorf, with assistance from M. Bogovac, Croatia. The software consists of data acquisition (scanning and calibration), automatic positioning and micro-movement of sample, data reduction and evaluation. The acquisition software was designed in order to support different measurement set-ups which are applied in low-energy nuclear physics. The modification was done in 1999-2000 under the projects Nuclear Spectrometry and Utilization of Particle Accelerators. The manual supersedes the first version entitled Microanalysis Data Acquisition and Control Program published under Computer Manual Series, No. 9 in 1996. The software described in this manual is freely available from the IAEA upon request

  3. Ion microprobe U-Pb dating of a dinosaur tooth

    International Nuclear Information System (INIS)

    Sano, Yuji; Terada, Kentaro; Ly, Chi V.; Park, Eun Ju

    2006-01-01

    Ion microprobe U-Pb dating of apatite is applied to a fossil tooth of a Allosaurid derived from the Hasandong Formation in the Gyeongsang basin, southeastern Korea. Twelve spots on a single fragment of the fossil dentine yield a Tera-Wasserburg concordia intercept age of 115±10 Ma (2σ, MSWD=0.59) on a 238 U/ 206 Pb- 207 Pb/ 206 Pb- 204 Pb/ 206 Pb diagram. The age provides a constraint on the depositional age of the fossil in its host Hassandong Formation as Early Aptian. The success of the ion microprobe dating depends on the heterogeneities of diagenetically incorporated U and Pb at the few hundred μm scale, the consequent variations in Pb isotopic compositions due to radioactive decay and the closed-system behavior of U and Pb. There are at least three end-members to explain the variations of minor chemical components such as FeO, SiO 2 and Al 2 O 3 , and trace elements as Th, U and rare earth elements (REE) in the sample by a simple mixing model. They are (1) very low minor and REE, very high common Pb with variable U abundances, (2) low common Pb, high minor, REE, and U abundances, and (3) low minor, common Pb, and U with intermediate REE abundances, even though groups (2) and (3) may consist of a larger group. Various contributions of the three (and/or two) end-members during diagenetic processes may cause the elemental fractionation of U and Pb in a fossil tooth. (author)

  4. Milliprobe and microprobe analysis of gold items of ancient jewellery

    International Nuclear Information System (INIS)

    Demortier, G.; Hackens, T.

    It has long been accepted that the presence of cadmium implies a condemnation of the authenticity of an ancient gold object, or at least, of the part of the object where the cadmium is detected. An analysis in Paris of a recently excavated object from Roman times has shown cadmium. Meanwhile, systematic observations were made at L.A.R.N. on objects dating from Hellenistic to Byzantine times with different given origins (objects from a museum and from private collections). By using PIXE with a 3 MeV proton milliprobe (700 μm beam diameter) in a non vacuum geometry, relative amounts of copper, silver, cadmium and gold at the surface of more than 30 gold objects expected to be ancient have been determined. Traces or significant concentrations of cadmium have been detected at several points on or in the neighbourhood of solders on many objects which seem to be from Roman to early Byzantine times. Cadmium concentrations range between 2 to 100 parts per thousand. This range of variations and the relative concentrations of Au, Ag, Cu and Cd at the surface of the objects studied are often different from the figures obtained during analyses of modern soldering alloys. Experiments with the L.A.R.N. proton microprobe (5 μm x 10 μm area) allow a still better topographical resolution and more significative comparison of the relative amounts of the elements of interest in modern soldering alloys and supposedly old solders. The usefulness of the microprobe is demonstrated. (author)

  5. Analysis of biological materials using a nuclear microprobe

    Science.gov (United States)

    Mulware, Stephen Juma

    The use of nuclear microprobe techniques including: Particle induced x-ray emission (PIXE) and Rutherford backscattering spectrometry (RBS) for elemental analysis and quantitative elemental imaging of biological samples is especially useful in biological and biomedical research because of its high sensitivity for physiologically important trace elements or toxic heavy metals. The nuclear microprobe of the Ion Beam Modification and Analysis Laboratory (IBMAL) has been used to study the enhancement in metal uptake of two different plants. The roots of corn (Zea mays) have been analyzed to study the enhancement of iron uptake by adding Fe (II) or Fe(III) of different concentrations to the germinating medium of the seeds. The Fe uptake enhancement effect produced by lacing the germinating medium with carbon nanotubes has also been investigated. The aim of this investigation is to ensure not only high crop yield but also Fe-rich food products especially from calcareous soil which covers 30% of world's agricultural land. The result will help reduce iron deficiency anemia, which has been identified as the leading nutritional disorder especially in developing countries by the World Health Organization. For the second plant, Mexican marigold (Tagetes erecta ), the effect of an arbuscular mycorrhizal fungi (Glomus intraradices ) for the improvement of lead phytoremediation of lead contaminated soil has been investigated. Phytoremediation provides an environmentally safe technique of removing toxic heavy metals (like lead), which can find their way into human food, from lands contaminated by human activities like mining or by natural disasters like earthquakes. The roots of Mexican marigold have been analyzed to study the role of arbuscular mycorrhizal fungi in enhancement of lead uptake from the contaminated rhizosphere.

  6. Use of a synchrotron radiation x-ray microprobe for elemental analysis at the National Synchrotron Light Source

    International Nuclear Information System (INIS)

    Gordon, B.M.

    1980-01-01

    The National Synchrotron Light Source (NSLS) is a facility consisting of a 700 MeV and a 2.5 GeV electron storage ring and dedicated to providing synchrotron radiation in the energy range from the vacuum ultraviolet to high energy x rays. Some of the properties of synchrotron radiation that contribute to its usefulness for x-ray fluorescence are: a continuous, tunable energy spectrum, strong collimation in the horizontal plane, high polarization in the storage ring plane, and relatively low energy deposition. The highest priority is for the development of an x-ray microprobe beam line capable of trace analysis in the parts per million range with spatial resolution as low as one micrometer. An eventual capability for bulk sample analysis is also planned with sensitivities in the more favorable cases beings low as 50 parts per billion in dry biological tissue. The microprobe technique has application to a variety of fields including the geological, medical, materials and environmental sciences. Examples of investigations include multielemental trace analysis across grain boundaries for the study of diffusion and cooling processes in geological and materials sciences samples; in leukocytes and other types of individual cells for studying the relationship between trace element concentrations and disease or nutrition; and in individual particles in air pollution samples

  7. Examination of Laser Microprobe Vacuum Ultraviolet Ionization Mass Spectrometry with Application to Mapping Mars Returned Samples

    Science.gov (United States)

    Burton, A. S.; Berger, E. L.; Locke, D. R.; Lewis, E. K.; Moore, J. F.

    2018-04-01

    Laser microprobe of surfaces utilizing a two laser setup whereby the desorption laser threshold is lowered below ionization, and the resulting neutral plume is examined using 157nm Vacuum Ultraviolet laser light for mass spec surface mapping.

  8. Laser microprobe for the study of noble gases and nitrogen in single ...

    Indian Academy of Sciences (India)

    R. Narasimhan (Krishtel eMaging) 1461 1996 Oct 15 13:05:22

    Planetary and Geosciences Division, Physical Research Laboratory, Ahmedabad 380 009, India. ∗e-mail: murty@prl.ernet.in. A laser microprobe capable of analysing nitrogen and noble gases in .... tion properties for light radiation, with some.

  9. Microprobe PIXE analysis and EDX analysis on the brain of patients with Alzheimer's disease

    International Nuclear Information System (INIS)

    Yumoto, S.; Horino, Y.; Mokuno, Y.; Fujii, K.; Kakimi, S.; Mizutani, T.; Matsushima, H.; Ishikawa, A.

    1996-01-01

    To investigate the cause of Alzheimer's disease (senile dementia of Alzheimer's disease type), we examined aluminium (Al) in the brain (hippocampus) of patients with Alzheimer's disease using heavy ion (5 MeV Si 3+ ) microprobe particle-induced X-ray emission (PIXE) analysis. Heavy ion microprobes (3 MeV Si 2+ ) have several times higher sensitivity for Al detection than 2 MeV proton microprobes. We also examined Al in the brain of these patients by energy dispersive X-ray spectroscopy (EDX). (1) Al was detected in the cell nuclei isolated from the brain of patients with Alzheimer's disease using 5 MeV Si 3+ microprobe PIXE analysis, and EDX analysis. (2) EDX analysis demonstrated high levels of Al in the nucleolus of nerve cells in frozen sections prepared from the brain of these patients. Our results support the theory that Alzheimer's disease is caused by accumulation of Al in the nuclei of brain cells. (author)

  10. Deep PIXE: finding diamonds with the proton microprobe

    International Nuclear Information System (INIS)

    Griffin, W.L.; Ryan, C.G.

    1991-01-01

    Since 1987 the CSIRO Div. of Exploration Geoscience has carried out a program of proton-microprobe (PIXE) analysis aimed at using trace-element data on indicator minerals to discriminate between those from diamondiferous and barren source rocks. The results have provided both important new tools for the exploration industry, and significant new information on the conditions and processes of diamond growth. Cr-pyrope garnet has been used as Ni thermometer while chromites, in partcular their Zn content, has allowed correlation of chromite composition with temperature. The two techniques described provide a significant increase in exploration efficiency, through early recognition and rejection of barren targets and concentration of resources on more promising targets. They also provide direct cost savings in evaluation of ore bodies once they are found. It is estimated that evaluation of a prospect by conventional bulk testing is expensive ($100-500K) and time-consuming; an evaluation by PIXE methods is done quickly for a tiny fraction of that cost. 1 refs., 4 figs

  11. Synchrotron radiation microprobe quantitative analysis method for biomedical specimens

    International Nuclear Information System (INIS)

    Xu Qing; Shao Hanru

    1994-01-01

    Relative changes of trace elemental content in biomedical specimens are obtained easily by means of synchrotron radiation X-ray fluorescence microprobe analysis (SXRFM). However, the accurate assignment of concentration on a g/g basis is difficult. Because it is necessary to know both the trace elemental content and the specimen mass in the irradiated volume simultaneously. the specimen mass is a function of the spatial position and can not be weighed. It is possible to measure the specimen mass indirectly by measuring the intensity of Compton scattered peak for normal XRF analysis using a X-ray tube with Mo anode, if the matrix was consisted of light elements and the specimen was a thin sample. The Compton peak is not presented in fluorescence spectrum for white light SXRFM analysis. The continuous background in the spectrum was resulted from the Compton scattering with a linear polarization X-ray source. Biomedical specimens for SXRFM analysis, for example biological section and human hair, are always a thin sample for high energy X-ray, and they consist of H,C,N and O etc. light elements, which implies a linear relationship between the specimen mass and the Compton scattering background in the high energy region of spectrum. By this way , it is possible to carry out measurement of concentration for SXRFM analysis

  12. Raman microprobe measurements of stress in ion implanted materials

    Energy Technology Data Exchange (ETDEWEB)

    Nugent, K W; Prawer, S; Weiser, P S; Dooley, S P [Melbourne Univ., Parkville, VIC (Australia). School of Physics

    1994-12-31

    Raman microprobe measurements of ion implanted diamond and silicon have shown significant shifts in the Raman line due to stresses in the materials. The Raman line shifts to higher energy if the stress is compressive and to lower energy for tensile stress{sup 1}. The silicon sample was implanted in a 60 {mu}m square with 2.56 x 10{sup 17} ions per square centimeter of 2 MeV Helium. This led to the formation of raised squares with the top 370mm above the original surface. In Raman studies of silicon using visible light, the depth of penetration of the laser beam into the sample is much less than one micron. It was found that the Raman line is due to the silicon overlying the damage region. The diamond sample was implanted with 2 x 10{sup 15} ions per square centimeter of 2.8 MeV carbon. It was concluded that the Raman spectrum could provide information concerning both the magnitude and the direction of stress in an ion implanted sample. It was possible in some cases to determine whether the stress direction is parallel or perpendicular to the sample surface. 1 refs., 2 figs.

  13. Using the ion microprobe mass analyser for trace element analysis

    International Nuclear Information System (INIS)

    Schilling, J.H.

    1978-01-01

    Most techniques for the analysis of trace elements are capable of determining the concentrations in a bulk sample or solution, but without reflecting their distribution. In a bulk analysis therefore elements which occur in high concentration in a few precipitates would still be considered trace elements even though their local concentration greatly exceed the normally accepted trace elements concentration limit. Anomalous distribution is also shown by an oxide layer, a few hundred Angstrom thick, on an aluminium sample. A low oxide concentration would be reported if it were included in the bulk analysis, which contradicts the high surface concentration. The importance of a knowledge of the trace element distribution is therefore demonstrated. Distributional trace element analysis can be carried out using the ion microprobe mass analyser (IMMA). Since the analytical technique used in this instrument, namely secondary ion mass spectrometry (SIMS), is not universally appreciated, the instrument and its features will be described briefly followed by a discussion of quantitative analysis and the related subjects of detection limit and sample consumption. Finally, a few examples of the use of the instrument are given

  14. Nuclear microprobe analysis of lead profile in crocodile bones

    Energy Technology Data Exchange (ETDEWEB)

    Orlic, I. E-mail: ivo@ansto.gov.au; Siegele, R.; Hammerton, K.; Jeffree, R.A.; Cohen, D.D

    2003-09-01

    Elevated concentrations of lead were found in Australian free ranging saltwater crocodile (Crocodylus porosus) bone and flesh. Lead shots were found as potential source of lead in these animals. ANSTO's heavy ion nuclear microprobe was used to measure the distribution of Pb in a number of bones and osteoderms. The aim was to find out if elevated Pb concentration remains in growth rings and if the concentration is correlated with the blood levels recorded at the time. Results of our study show a very distinct distribution of accumulated Pb in bones and osteoderms as well as good correlation with the level of lead concentration in blood. To investigate influence of ion species on detection limits measurements of the same sample were performed by using 3 MeV protons, 9 MeV He ions and 20 MeV carbon ions. Peak to background ratios, detection limits and the overall 'quality' of obtained spectra are compared and discussed.

  15. Raman microprobe measurements of stress in ion implanted materials

    Energy Technology Data Exchange (ETDEWEB)

    Nugent, K.W.; Prawer, S.; Weiser, P.S.; Dooley, S.P. [Melbourne Univ., Parkville, VIC (Australia). School of Physics

    1993-12-31

    Raman microprobe measurements of ion implanted diamond and silicon have shown significant shifts in the Raman line due to stresses in the materials. The Raman line shifts to higher energy if the stress is compressive and to lower energy for tensile stress{sup 1}. The silicon sample was implanted in a 60 {mu}m square with 2.56 x 10{sup 17} ions per square centimeter of 2 MeV Helium. This led to the formation of raised squares with the top 370mm above the original surface. In Raman studies of silicon using visible light, the depth of penetration of the laser beam into the sample is much less than one micron. It was found that the Raman line is due to the silicon overlying the damage region. The diamond sample was implanted with 2 x 10{sup 15} ions per square centimeter of 2.8 MeV carbon. It was concluded that the Raman spectrum could provide information concerning both the magnitude and the direction of stress in an ion implanted sample. It was possible in some cases to determine whether the stress direction is parallel or perpendicular to the sample surface. 1 refs., 2 figs.

  16. Nuclear micro-probe analysis of Arabidopsis thaliana leaves

    International Nuclear Information System (INIS)

    Ager, F.J.; Ynsa, M.D.; Dominguez-Solis, J.R.; Lopez-Martin, M.C.; Gotor, C.; Romero, L.C.

    2003-01-01

    Phytoremediation is a cost-effective plant-based approach for remediation of soils and waters which takes advantage of the remarkable ability of some plants to concentrate elements and compounds from the environment and to metabolize various molecules in their tissues, such as toxic heavy metals and organic pollutants. Nowadays, phytoremediation technology is becoming of paramount importance when environmental decontamination is concerned, due to the emerging knowledge of its physiological and molecular mechanisms and the new biological and engineering strategies designed to optimize and improve it. In addition, the feasibility of using plants for environmental cleanup has been confirmed by many different trials around the world. Arabidopsis thaliana plants can be used for basic studies to improve the technology on phytoremediation. Making use of nuclear microscopy techniques, in this paper we study leaves of wild type and transgenic A. thaliana plants grown in a cadmium-rich environment under different conditions. Micro-PIXE, RBS and SEM analyses, performed on the scanning proton micro-probe at the CNA in Seville (Spain), prove that cadmium is preferentially sequestered in the central region of epidermal trichome and allow comparing the effects of genetic modifications

  17. Nuclear microprobe studies of elemental distributions in dormant seeds of Burkea africana

    Science.gov (United States)

    Witkowski, E. T. F.; Weiersbye-Witkowski, I. M.; Przybyłowicz, W. J.; Mesjasz-Przybyłowicz, J.

    1997-07-01

    Seed nutrient stores are vital post-germination for the establishment of seedlings in harsh and unpredictable environments. Plants of nutrient-poor environments allocate a substantial proportion of total acquired nutrients to reproduction (i.e. seeds). We propose that differential allocation of mineral resources to specific seed tissues is an indication of a species germination and establishment strategy. Burkea africana Hook is a leguminous tree typical of broad-leaved nutrient-poor savannas in southern Africa. Elemental distributions in dormant B. africana seed structures were obtained using the true elemental imaging system (Dynamic Analysis) of the NAC Van de Graaff nuclear microprobe. Raster scans of 3.0 MeV protons were complemented by simultaneous BS and PIXE point analyses. Mineral nutrient concentrations varied greatly between seed tissues. Elevated levels of metals known to play an important role as plant enzyme co-factors were found in the seed lens and embryonic axis. Distributions of most of these metals (Ca, Mn, Fe and Zn, but not K or Cu) were positively correlated with embryonic P distribution, and probably represent phytin deposits. The distribution of metals within seed structures is 'patchy' due to their complexation with P as electron-dense globoid phytin crystals, which constrains the interpretation of PIXE point analyses.

  18. Development of an external beam nuclear microprobe on the Aglae facility of the Louvre museum

    Energy Technology Data Exchange (ETDEWEB)

    Calligaro, T.; Dran, J.-C. E-mail: dran@culture.fr; Ioannidou, E.; Moignard, B.; Pichon, L.; Salomon, J

    2000-03-01

    The external beam line of our facility has been recently equipped with the focusing system previously mounted on a classical nuclear microprobe. When using a 0.1 {mu}m thick Si{sub 3}N{sub 4} foil for the exit window and flowing helium on the sample under analysis, a beam spot as small as 10 {mu}m is attainable at a distance of 3 mm from the window. Elemental micromapping is performed by mechanical scanning. An electronic device has been designed which allows XY scanning by moving the sample under the beam by steps down to 0.1 {mu}m. Beam monitoring is carried out by means of the weak X-ray signal emitted by the exit foil and detected by a specially designed Si(Li) detector cooled by Peltier effect. The characteristics of external beams of protons and alpha particles are evaluated by means of resonance scanning and elemental mapping of a grid. An example of application is presented, dealing with elemental micro-mapping of inclusions in gemstones.

  19. Fabrication and surface-modification of implantable microprobes for neuroscience studies

    International Nuclear Information System (INIS)

    Cao, H; Nguyen, C M; Chiao, J C

    2012-01-01

    In this work implantable micro-probes for central nervous system (CNS) studies were developed on silicon and polyimide substrates. The probes which contained micro-electrode arrays with different surface modifications were designed for implantation in the CNS. The electrode surfaces were modified with nano-scale structures that could greatly increase the active surface area in order to enhance the electrochemical current outputs while maintaining micro-scale dimensions of the electrodes and probes. The electrodes were made of gold or platinum, and designed with different sizes. The silicon probes were modified by silicon nanowires fabricated with the vapor–liquid–solid mechanism at high temperatures. With polyimide substrates, the nanostructure modification was carried out by applying concentrated gold or silver colloid solutions onto the micro-electrodes at room temperature. The surfaces of electrodes before and after modification were observed by scanning electron microscopy. The silicon nanowire-modified surface was characterized by cyclic voltammetry. Experiments were carried out to investigate the improvement in sensing performance. The modified electrodes were tested with H 2 O 2 , electrochemical L-glutamate and dopamine. Comparisons between electrodes with and without nanostructure modification were conducted showing that the modifications have enhanced the signal outputs of the electrochemical neurotransmitter sensors

  20. Fabrication and surface-modification of implantable microprobes for neuroscience studies

    Science.gov (United States)

    Cao, H.; Nguyen, C. M.; Chiao, J. C.

    2012-06-01

    In this work implantable micro-probes for central nervous system (CNS) studies were developed on silicon and polyimide substrates. The probes which contained micro-electrode arrays with different surface modifications were designed for implantation in the CNS. The electrode surfaces were modified with nano-scale structures that could greatly increase the active surface area in order to enhance the electrochemical current outputs while maintaining micro-scale dimensions of the electrodes and probes. The electrodes were made of gold or platinum, and designed with different sizes. The silicon probes were modified by silicon nanowires fabricated with the vapor-liquid-solid mechanism at high temperatures. With polyimide substrates, the nanostructure modification was carried out by applying concentrated gold or silver colloid solutions onto the micro-electrodes at room temperature. The surfaces of electrodes before and after modification were observed by scanning electron microscopy. The silicon nanowire-modified surface was characterized by cyclic voltammetry. Experiments were carried out to investigate the improvement in sensing performance. The modified electrodes were tested with H2O2, electrochemical L-glutamate and dopamine. Comparisons between electrodes with and without nanostructure modification were conducted showing that the modifications have enhanced the signal outputs of the electrochemical neurotransmitter sensors.

  1. Pequenos para idade gestacional: fator de risco para mortalidade neonatal

    Directory of Open Access Journals (Sweden)

    Almeida Márcia Furquim de

    1998-01-01

    Full Text Available OBJETIVO: Estudar as variáveis contempladas na Declaração de Nascimento (DN como possíveis fatores de risco para nascimentos pequenos para a idade gestacional (PIG e o retardo de crescimento intra-uterino como fator de risco para a mortalidade neonatal. MATERIAL E MÉTODO: As variáveis existentes na DN foram obtidas diretamente de prontuários hospitalares. Os dados referem-se a uma coorte de nascimentos obtida por meio da vinculação das declarações de nascimento e óbito, correspondendo a 2.251 nascimentos vivos hospitalares, de mães residentes, ocorridos no Município de Santo André, Região Metropolitana de São Paulo, no período de l/1 a 30/6/1992, e aos óbitos neonatais verificados nessa coorte. RESULTADOS: Obteve-se a proporção de 4,3% de nascimentos PIG, significativamente maior entre os recém-nascidos de pré-termo e pós-termo, entre os nascimentos cujas mães tinham mais de 35 anos de idade e grau de instrução inferior ao primeiro grau completo. Os recém-nascidos PIG apresentam maior risco de morte neonatal que aqueles que não apresentavam sinais de retardo de crescimento intra-uterino. CONCLUSÕES: Em áreas com menor freqüência de baixo peso ao nascer, é importante investigar a presença de retardo de crescimento intra-uterino entre os nascimentos prematuros e não apenas nos nascimentos de termo. O registro da data da última menstruação (ou da idade gestacional em semanas não agregadas na DN facilitaria a detecção de PIGs na população de recém-nascidos.

  2. Efeito da Idade Materna sobre os Resultados Perinatais

    Directory of Open Access Journals (Sweden)

    Azevedo George Dantas de

    2002-01-01

    Full Text Available Objetivo: analisar a relação entre a idade materna e a ocorrência de resultados perinatais adversos na população do Rio Grande do Norte. Métodos: foram analisados os registros oficiais de 57.088 nascidos vivos no Estado do Rio Grande do Norte no ano de 1997. Os dados foram obtidos do Sistema de Informação sobre Nascidos Vivos do Ministério da Saúde. A população estudada foi dividida em Grupos I, II e III, segundo a faixa etária materna: 10 a 19, 20 a 34 e 35 anos ou mais, respectivamente. As variáveis analisadas foram: duração da gestação, peso ao nascer e tipo de parto. A análise estatística foi realizada utilizando-se o teste chi². Resultados: observamos uma maior incidência de parto pré-termo no Grupo I (4,3 %, em comparação ao Grupo II (3,7% (p = 0,0028. A taxa de cesariana foi menor nos Grupos I e III, em comparação ao Grupo II (p<0,0001. Evidenciamos freqüência significativamente maior de recém-nascidos de baixo peso nos Grupos I (8,4% e III (8,3%, quando comparados ao Grupo II (6,5% (p<0,0001. Conclusões: a gravidez nos extremos da vida reprodutiva esteve associada com maior freqüência de parto pré-termo e baixo peso ao nascer, entretanto, com relação ao tipo de parto, foi observada maior freqüência de parto normal do que no grupo de gestantes com idade entre 20 e 34 anos.

  3. Ion microprobe imaging of 44Ca-labeled mammalian chromosomes

    International Nuclear Information System (INIS)

    Levi-Setti, R.; Gavrilov, K.L.; Strissel, P.L.; Strick, R.

    2004-01-01

    In our previous investigation, we showed for the first time high-resolution analytical images of the cation composition of mammalian interphase and mitotic cells as well as of isolated metaphase chromosomes using the University of Chicago scanning ion microprobe (UC-SIM). In order to preserve the ionic integrity of the analyzed cells and prevent the well known occurrence of analytical artifacts due to the high diffusivity of cations in biological samples we used fast cryo-preservation methods (freeze-drying and freeze fracture), without any pre-fixations or washes. We identified the role of the cations in chromosome structure and maintenance using SIMS imaging and immunfluorescence methodologies. Importantly, we determined that the above cations are essential participants in chromosome condensation and maintenance of chromatin higher order structure, through their presumed function in DNA electrostatic neutralization and the direct interaction of Ca 2+ , in particular, with structural proteins. In addition, both Ca 2+ and Mg 2+ showed the same cell cycle regulation where during interphase both cations were enriched in the cytosol, particularly in organelles then at mitosis became specifically bound to chromatin. Our present research interest focuses on a more detailed analysis of the distribution of Ca 2+ throughout the different cell cycle stages, e.g. G1, G2 and mitosis. We have chosen the stable isotope 44 Ca as a tracer to follow Ca 2+ throughout the cell cycle. This nuclide occurs naturally in the ratio 44 Ca/ 40 Ca+ 44 Ca of 2.06%, so that incorporation at higher concentrations into chromatin or other cellular components should be easily detected by SIMS. Such incorporation can be obtained either by growing cells in a medium where ordinary Ca is replaced entirely by 44 Ca, or by replacing the cell culture medium with the 44 Ca medium for a gated time span (pulsing), after appropriate cell cycle stage synchronization. In this paper, we describe our

  4. Assessment of dye distribution in sensitized solar cells by microprobe techniques

    Energy Technology Data Exchange (ETDEWEB)

    Barreiros, M.A., E-mail: alexandra.barreiros@lneg.pt [Laboratório Nacional de Energia e Geologia, LEN/UES, Estrada do Paço do Lumiar, 22, 1649-038 Lisboa (Portugal); Corregidor, V. [IPFN, Instituto Superior Técnico, Universidade de Lisboa, E.N. 10, 2686-953 Sacavém (Portugal); Alves, L.C. [C2TN, Campus Tecnológico e Nuclear, Instituto Superior Técnico, Universidade de Lisboa, E.N. 10, 2686-953 Sacavém (Portugal); Guimarães, F. [Laboratório Nacional de Energia e Geologia, LGM/UCTM, Rua da Amieira, Apartado 1089, 4466-901 S. Mamede de Infesta (Portugal); Mascarenhas, J.; Torres, E.; Brites, M.J. [Laboratório Nacional de Energia e Geologia, LEN/UES, Estrada do Paço do Lumiar, 22, 1649-038 Lisboa (Portugal)

    2015-04-01

    Dye sensitized solar cells (DSCs) have received considerable attention once this technology offers economic and environmental advantages over conventional photovoltaic (PV) devices. The PV performance of a DSC relies on the characteristics of its photoanode, which typically consists of a nanocrystalline porous TiO{sub 2} film, enabled with a large adsorptive surface area. Dye molecules that capture photons from light during device operation are attached to the film nanoparticles. The effective loading of the dye in the TiO{sub 2} electrode is of paramount relevance for controlling and optimizing solar cell parameters. Relatively few methods are known today for quantitative evaluation of the total dye adsorbed on the film. In this context, microprobe techniques come out as suitable tools to evaluate the dye surface distribution and depth profile in sensitized films. Electron Probe Microanalysis (EPMA) and Ion Beam Analytical (IBA) techniques using a micro-ion beam were used to quantify and to study the distribution of the Ru organometallic dye in TiO{sub 2} films, making use of the different penetration depth and beam sizes of each technique. Different 1D nanostructured TiO{sub 2} films were prepared, morphologically characterized by SEM, sensitized and analyzed by the referred techniques. Dye load evaluation in different TiO{sub 2} films by three different techniques (PIXE, RBS and EPMA/WDS) provided similar results of Ru/Ti mass fraction ratio. Moreover, it was possible to assess dye surface distribution and its depth profile, by means of Ru signal, and to visualize the dye distribution in sample cross-section through X-ray mapping by EPMA/EDS. PIXE maps of Ru and Ti indicated an homogeneous surface distribution. The assessment of Ru depth profile by RBS showed that some films have homogeneous Ru depth distribution while others present different Ru concentration in the top layer (2 μm thickness). These results are consistent with the EPMA/EDS maps obtained.

  5. Planktonic foraminiferal oxygen isotope analysis by ion microprobe technique suggests warm tropical sea surface temperatures during the Early Paleogene

    Science.gov (United States)

    Kozdon, Reinhard; Kelly, D. Clay; Kita, Noriko T.; Fournelle, John H.; Valley, John W.

    2011-09-01

    Cool tropical sea surface temperatures (SSTs) are reported for warm Paleogene greenhouse climates based on the δ18O of planktonic foraminiferal tests. These results are difficult to reconcile with models of greenhouse gas-forced climate. It has been suggested that this "cool tropics paradox" arises from postdepositional alteration of foraminiferal calcite, yielding erroneously high δ18O values. Recrystallization of foraminiferal tests is cryptic and difficult to quantify, and the compilation of robust δ18O records from moderately altered material remains challenging. Scanning electron microscopy of planktonic foraminiferal chamber-wall cross sections reveals that the basal area of muricae, pustular outgrowths on the chamber walls of species belonging to the genus Morozovella, contain no mural pores and may be less susceptible to postdepositional alteration. We analyzed the δ18O in muricae bases of morozovellids from the central Pacific (Ocean Drilling Program Site 865) by ion microprobe using 10 μm pits with an analytical reproducibility of ±0.34‰ (2 standard deviations). In situ measurements of δ18O in these domains yield consistently lower values than those published for conventional multispecimen analyses. Assuming that the original δ18O is largely preserved in the basal areas of muricae, this new δ18O record indicates Early Paleogene (˜49-56 Ma) tropical SSTs in the central Pacific were 4°-8°C higher than inferred from the previously published δ18O record and that SSTs reached at least ˜33°C during the Paleocene-Eocene thermal maximum. This study demonstrates the utility of ion microprobe analysis for generating more reliable paleoclimate records from moderately altered foraminiferal tests preserved in deep-sea sediments.

  6. Proton microprobe analysis of zinc in skeletal tissues. [Proton induced x-ray emission analysis

    Energy Technology Data Exchange (ETDEWEB)

    Doty, S B; Jones, K W; Kraner, H W; Shroy, R E; Hanson, A L

    1980-06-01

    A proton microprobe with windowless exit port was used to study zinc distributions in various types of skeletal tissues. The use of an external beam facilitated positioning of the targets for examination of particular points of interest. The proton microprobe is uniquely suited to this work since it combines high sensitivity for zinc determinations in thick samples with good spatial resolution. Measurements on rat and rabbit Achilles tendon showed a significant increase in zinc concentrations as the beam moved from the unmineralized collagen into the mineralized attachment site. Cartilage gave a similar result, with calcified cartilage having a greater zinc level than the articular surface on unmineralized epiphyseal cartilage.

  7. An x-ray microprobe using focussing optics with a synchrotron radiation source

    International Nuclear Information System (INIS)

    Thompson, A.C.; Underwood, J.H.; Wu, Y.; Giauque, R.D.

    1989-01-01

    An x-ray microprobe can be used to produce maps of the concentration of elements in a sample. Synchrotron radiation provides x-ray beams with enough intensity and collimation to make possible elemental images with femtogram sensitivity. The use of focussing x-ray mirrors made from synthetic multilayers with a synchrotron x-ray beam allows beam spot sizes of less than 10 μm /times/ 10 μm to be produced. Since minimal sample preparation is required and a vacuum environment is not necessary, there will be a wide variety of applications for such microprobes. 8 refs., 6 figs

  8. The PNC/XOR x-ray microprobe station at APS sector 20

    International Nuclear Information System (INIS)

    Heald, S. M.; Cross, J. O.; Brewe, D. L.; Gordon, R. A.

    2007-01-01

    The X-ray microprobe is the most popular experimental setup at the PNC/XOR insertion device beamline located at sector 20 at the Advanced Photon Source. To satisfy user demand and to simplify the setup, we have developed a dedicated station with multiple detection options. This paper will describe the setup in detail and demonstrate the capabilities with some example imaging, micro-XAS and microdiffraction data. In the future, an improved version of the microprobe will be installed on a dedicated undulator. The improvements planned for this station are based on our operational experience and will also be discussed

  9. Polymer SU-8 Based Microprobes for Neural Recording and Drug Delivery

    Science.gov (United States)

    Altuna, Ane; Fernandez, Luis; Berganzo, Javier

    2015-06-01

    This manuscript makes a reflection about SU-8 based microprobes for neural activity recording and drug delivery. By taking advantage of improvements in microfabrication technologies and using polymer SU-8 as the only structural material, we developed several microprobe prototypes aimed to: a) minimize injury in neural tissue, b) obtain high-quality electrical signals and c) deliver drugs at a micrometer precision scale. Dedicated packaging tools have been developed in parallel to fulfill requirements concerning electric and fluidic connections, size and handling. After these advances have been experimentally proven in brain using in vivo preparation, the technological concepts developed during consecutive prototypes are discussed in depth now.

  10. POLYMER SU-8 BASED MICROPROBES FOR NEURAL RECORDING AND DRUG DELIVERY

    Directory of Open Access Journals (Sweden)

    Ane eAltuna

    2015-06-01

    Full Text Available This manuscript makes a reflection about SU-8 based microprobes for neural activity recording and drug delivery. By taking advantage of improvements in microfabrication technologies and using polymer SU-8 as the only structural material, we developed several microprobe prototypes aimed to: a minimize injury in neural tissue, b obtain high-quality electrical signals and c deliver drugs at a micrometer precision scale. Dedicated packaging tools have been developed in parallel to fulfill requirements concerning electric and fluidic connections, size and handling. After these advances have been experimentally proven in brain using in vivo preparation, the technological concepts developed during consecutive prototypes are discussed in depth now.

  11. The new Schonland PIXE microprobe and applications to geological and archaeological samples

    Energy Technology Data Exchange (ETDEWEB)

    Przybylowicz, W J; Watterson, J I.W.; Annegarn, H J; Connell, S H; Fearick, R W; Andeweg, A H; Sellschop, J P.F. [Schonland Research Centre for Nuclear Sciences, Univ. of the Witwatersrand, Johannesburg (South Africa)

    1993-04-01

    The new positive ion microprobe at the Schonland Centre is described and details are given of its configuration, its imaging system and software. In a unique configuration, the microprobe has access to two accelerators, a 6 MV EN tandem and a 2.5 MV single-ended machine. The imaging system uses a CAMAC based system and runs on a personal computer under OS/2. The implementation of PIXE and treatment of thick-target data are presented. Applications discussed are analysis of tin artifacts from the prehistory of metallurgy in South Africa; a diamond-containing rock; carbonado, gold contained in pyrite and cogenetic minerals included in diamond. (orig.).

  12. The new Schonland PIXE microprobe and applications to geological and archaeological samples

    International Nuclear Information System (INIS)

    Przybylowicz, W.J.; Watterson, J.I.W.; Annegarn, H.J.; Connell, S.H.; Fearick, R.W.; Andeweg, A.H.; Sellschop, J.P.F.

    1993-01-01

    The new positive ion microprobe at the Schonland Centre is described and details are given of its configuration, its imaging system and software. In a unique configuration, the microprobe has access to two accelerators, a 6 MV EN tandem and a 2.5 MV single-ended machine. The imaging system uses a CAMAC based system and runs on a personal computer under OS/2. The implementation of PIXE and treatment of thick-target data are presented. Applications discussed are analysis of tin artifacts from the prehistory of metallurgy in South Africa; a diamond-containing rock; carbonado, gold contained in pyrite and cogenetic minerals included in diamond. (orig.)

  13. Theory of equidistant three-dimensional radiance measurements with optical microprobes RID A-1977-2009

    DEFF Research Database (Denmark)

    FukshanskyKazarinova, N.; Fukshansky, L.; Kuhl, Morten

    1996-01-01

    Fiber-optic radiance microprobes, increasingly applied for measurements of internal light fields in living tissues, provide three-dimensional radiance distribution solids and radiant energy fluence rates at different depths of turbid samples. These data are, however, distorted because of an inher...... of application is presented. The limitations of this theory and the prospects for this approach are discussed....... of an inherent feature of optical fibers: nonuniform angular sensitivity. Because of this property a radiance microprobe during a single measurement partly underestimates light from the envisaged direction and partly senses light from other directions. A theory of three-dimensional equidistant radiance...

  14. Combination of synchrotron radiation X-ray microprobe and nuclear microprobe for chromium and chromium oxidation states quantitative mapping in single cells

    International Nuclear Information System (INIS)

    Ortega, Richard; Deves, Guillaume; Fayard, Barbara; Salome, Murielle; Susini, Jean

    2003-01-01

    Hexavalent chromium compounds are established carcinogens but their mechanism of cell transformation has not been elucidated yet. In this study, chromium oxidation state distribution maps in cells exposed to soluble (Na 2 CrO 4 ), or insoluble (PbCrO 4 ), Cr(VI) compounds have been obtained by use of the ESRF ID-21 X-ray microscope. In addition, the quantitative maps of element distributions in cells have been determined using the nuclear microprobe of Bordeaux-Gradignan. Nuclear microprobe quantitative analysis revealed interesting features on chromium, and lead, cellular uptake. It is suggested that cells can enhance PbCrO 4 solubility, resulting in chromium, but not lead uptake. The differential carcinogenic potential of soluble and insoluble Cr(VI) compounds is discussed with regard to chromium intracellular quantitative distribution

  15. Preferência alimentar do bicudo-do-algodoeiro por frutos de diferentes cultivares e idades

    Directory of Open Access Journals (Sweden)

    Busoli Antonio Carlos

    2004-01-01

    Full Text Available O objetivo deste trabalho foi avaliar a preferência alimentar de adultos do bicudo-do-algodoeiro, Anthonomus grandis Boheman, 1843 (Coleoptera: Curculionidae, por duas cultivares de algodão (Gossypium hirsutum L. com frutos de diferentes idades. Foram realizados quatro experimentos em laboratório, avaliando-se o número de orifícios de alimentação. Maçãs de 2, 8 e 12 dias de idade, das cultivares IAC-20 e Reba P288, foram oferecidas aos insetos, confinados em recipientes, com opção de escolha quanto à idade e cultivar (primeiro experimento, sem opção de escolha quanto à idade e cultivar (segundo experimento, sem opção de escolha quanto à cultivar e com opção quanto a idade (terceiro experimento e sem opção quanto à idade e com opção de escolha quanto à cultivar (quarto experimento. Observou-se preferência por maçãs da cultivar IAC-20 com dois dias de idade, com uma redução de danos de 23,53% e 78,43%, respectivamente, aos oito e aos doze dias de idade.

  16. Qualidade da carne de frangos caipiras abatidos em diferentes idades

    Directory of Open Access Journals (Sweden)

    X.R. Souza

    2012-04-01

    Full Text Available Neste trabalho, foram avaliadas as características físico-químicas e de composição centesimal da carne de frangos machos de três linhagens utilizadas para criação semi-intensiva: Redbro Cou Nu - Vermelho de Pescoço Pelado (Pescoço Pelado; Redbro Plumé - Vermelho de Pescoço Emplumado (Pesadão e Gris Barre Plumé (Carijó. Foram analisadas diferenças em relação à linhagem e à idade de abate (70, 85 e 110 dias. Na carne do peito, não foi verificado efeito de linhagem sobre os parâmetros de cor (L*, a* e b* e pH final. Houve comportamento diferenciado para as aves em relação a qualidade da carne do peito, com menores valores de maciez para linhagem Pesadão e de Perda de Peso por Cozimento para linhagem Carijó. A linhagem Carijó apresentou, para a carne de peito aos 110 dias, os menores valores de umidade e as maiores médias de proteína. Os valores de proteina reduziram para linhagem Pescoço Pelado a partir de 85 dias. Na coxa, a partir de 110 dias, foi verificada redução dos valores de L* (luminosidade e aumento das médias de a* (vermelho. Os valores de força de cisalhamento e extrato etéreo aumentaram para peito e coxa a partir dos 110 dias. As linhagens Pesadão e Pescoço Pelado apresentaram de forma geral, melhores aspectos físico-quimicos, que são os atributos de maior preferência pelo consumidor em função deste tipo de produto.

  17. Data acquisition and analysis system for the ion microprobe mass analyzer

    International Nuclear Information System (INIS)

    Darby, D.M.; Cristy, S.S.

    1979-02-01

    A computer was interfaced to an ion microprobe mass analyzer for more rapid data acquisition and analysis. The interface is designed to allow data acquisition, independent of the computer. A large data analysis package was developed and implemented. Performance of the computerized system was evaluated and compared to manual operation

  18. Round robin: Quantitative lateral resolution of PHI XPS microprobes Quantum 2000/Quantera SXM

    International Nuclear Information System (INIS)

    Scheithauer, Uwe; Kolb, Max; Kip, Gerard A.M.; Naburgh, Emile; Snijders, J.H.M.

    2016-01-01

    Highlights: • The quantitative lateral resolution of 7 PHI XPS microprobes has been estimated in a round robin. • An ellipsoidally shaped quartz crystal monochromatizes the Alkα radiation and refocuses it from the Al anode to the sample surface. • The long tail contributions of the X-ray beam intensity distribution were measured using a new and innovative approach. • This quantitative lateral resolution has a significantly larger value than the nominal X-ray beam diameter. • The quantitative lateral resolution follows a trend in time: The newer the monochromator so much the better the quantitative lateral resolution. - Abstract: The quantitative lateral resolution is a reliable measure for the quality of an XPS microprobe equipped with a focused X-ray beam. It describes the long tail contributions of the X-ray beam intensity distribution. The knowledge of these long tail contributions is essential when judging on the origin of signals of XPS spectra recorded on small-sized features. In this round robin test the quantitative lateral resolution of 7 PHI XPS microprobes has been estimated. As expected, the quantitative lateral resolution has significantly larger values than the nominal X-ray beam diameter. The estimated values of the quantitative lateral resolution follow a trend in time: the newer the monochromator of an XPS microprobe so much the better the quantitative lateral resolution.

  19. Round robin: Quantitative lateral resolution of PHI XPS microprobes Quantum 2000/Quantera SXM

    Energy Technology Data Exchange (ETDEWEB)

    Scheithauer, Uwe, E-mail: scht.uhg@googlemail.com [82008 Unterhaching (Germany); Kolb, Max, E-mail: max.kolb@airbus.com [Airbus Group Innovations, TX2, 81663 Munich (Germany); Kip, Gerard A.M., E-mail: G.A.M.Kip@utwente.nl [Universiteit Twente, MESA+ Nanolab, Postbus 217, 7500AE Enschede (Netherlands); Naburgh, Emile, E-mail: e.p.naburgh@philips.com [Materials Analysis, Philips Innovation Services, High Tech Campus 11, 5656 AE Eindhoven (Netherlands); Snijders, J.H.M., E-mail: j.h.m.snijders@philips.com [Materials Analysis, Philips Innovation Services, High Tech Campus 11, 5656 AE Eindhoven (Netherlands)

    2016-07-15

    Highlights: • The quantitative lateral resolution of 7 PHI XPS microprobes has been estimated in a round robin. • An ellipsoidally shaped quartz crystal monochromatizes the Alkα radiation and refocuses it from the Al anode to the sample surface. • The long tail contributions of the X-ray beam intensity distribution were measured using a new and innovative approach. • This quantitative lateral resolution has a significantly larger value than the nominal X-ray beam diameter. • The quantitative lateral resolution follows a trend in time: The newer the monochromator so much the better the quantitative lateral resolution. - Abstract: The quantitative lateral resolution is a reliable measure for the quality of an XPS microprobe equipped with a focused X-ray beam. It describes the long tail contributions of the X-ray beam intensity distribution. The knowledge of these long tail contributions is essential when judging on the origin of signals of XPS spectra recorded on small-sized features. In this round robin test the quantitative lateral resolution of 7 PHI XPS microprobes has been estimated. As expected, the quantitative lateral resolution has significantly larger values than the nominal X-ray beam diameter. The estimated values of the quantitative lateral resolution follow a trend in time: the newer the monochromator of an XPS microprobe so much the better the quantitative lateral resolution.

  20. Characterization of Alq3 thin films by a near-field microwave microprobe.

    Science.gov (United States)

    Hovsepyan, Artur; Lee, Huneung; Sargsyan, Tigran; Melikyan, Harutyun; Yoon, Youngwoon; Babajanyan, Arsen; Friedman, Barry; Lee, Kiejin

    2008-09-01

    We observed tris-8-hydroxyquinoline aluminum (Alq3) thin films dependence on substrate heating temperatures by using a near-field microwave microprobe (NFMM) and by optical absorption at wavelengths between 200 and 900 nm. The changes of absorption intensity at different substrate heating temperatures are correlated to the changes in the sheet resistance of Alq3 thin films.

  1. Microprobe investigation of brittle segregates in aluminum MIG and TIG welds

    Science.gov (United States)

    Larssen, P. A.; Miller, E. L.

    1968-01-01

    Quantitative microprobe analysis of segregated particles in aluminum MIG /Metal Inert Gas/ and TIG /Tungsten Inert Gas/ welds indicated that there were about ten different kinds of particles, corresponding to ten different intermetallic compounds. Differences between MIG and TIG welds related to the individual cooling rates of these welds.

  2. Evaluation of an x-ray microprobe technique as a possible aid to detect salmonellae

    International Nuclear Information System (INIS)

    Richter, E.R.; Banwart, G.J.

    1982-01-01

    Specific bacterial antigen (Salmonella) increased in phosphorus and sqlfur after reaction with the flukrescain isothiocyanate-tagged anti-Salmonella antibody, while nonspecific antigen (Escherichia coli) did not. X-ray microprobe analysis may be useful in detecting salmonellae or other bacteria by determining increases in the elemental constituents of bacterial cells when reacted with elemental-tagged antibodies

  3. Microprobe PIXE analysis and EDX analysis on the brain of patients with Alzheimer`s disease

    Energy Technology Data Exchange (ETDEWEB)

    Yumoto, S. [Tokyo Univ. (Japan). Faculty of Medicine; Horino, Y.; Mokuno, Y.; Fujii, K.; Kakimi, S.; Mizutani, T.; Matsushima, H.; Ishikawa, A.

    1996-12-31

    To investigate the cause of Alzheimer`s disease (senile dementia of Alzheimer`s disease type), we examined aluminium (Al) in the brain (hippocampus) of patients with Alzheimer`s disease using heavy ion (5 MeV Si{sup 3+}) microprobe particle-induced X-ray emission (PIXE) analysis. Heavy ion microprobes (3 MeV Si{sup 2+}) have several times higher sensitivity for Al detection than 2 MeV proton microprobes. We also examined Al in the brain of these patients by energy dispersive X-ray spectroscopy (EDX). (1) Al was detected in the cell nuclei isolated from the brain of patients with Alzheimer`s disease using 5 MeV Si{sup 3+} microprobe PIXE analysis, and EDX analysis. (2) EDX analysis demonstrated high levels of Al in the nucleolus of nerve cells in frozen sections prepared from the brain of these patients. Our results support the theory that Alzheimer`s disease is caused by accumulation of Al in the nuclei of brain cells. (author)

  4. Developments of new generation nuclear microprobe systems at the University of Melbourne

    International Nuclear Information System (INIS)

    Rout, B.; Jamieson, D.N.; Hopt, R.; Hearne, S.; Szymaski, R.

    2002-01-01

    Full text: A review of the recent developments in fabricating a new generation nuclear microprobe systems at University of Melbourne, Melbourne, will be presented. These new generation systems present high spatial resolution (less than 1 micrometer) with increasing current density (in excess of 100 pA/micrometer 2 ) of the probing ion beam. Detectors with large solid angles and high brightness of the ion source of the accelerator increase the capabilities of these microprobes many fold. Some of the key ingredients of these microprobes are (i) novel magnetic quadrupole lens quintuplet probe forming system (ii) integrated fast data acquisition system to handle high count rates (excess of 100 KHz) due to increasing current density as well as large detector solid angles up to 4 detector stations. Full dead time corrected and charge normalised maps are also implemented to counter the problems normally associated with such high count rate systems. First version of these systems is presently under operation at CSIRO, Sydney. Another similar system is currently being installed at Dutch Institute for Nuclear and High Energy Physics, Amsterdam, Netherlands. A further optimised version of the CSIRO/MARC quintuplet probe forming systems is currently being fabricated at University of Melbourne. Some of the applications involve microelectronic materials, superconductors and geological samples. We will be presenting exciting results arising out of investigations into these materials. We will be demonstrating ultimate spatial resolution of the new microprobe being fabricated at Melbourne

  5. Elemental microanalysis of biological and medical specimens with a scanning proton microprobe

    International Nuclear Information System (INIS)

    Legge, G.J.F.; Mazzolini, A.P.

    1979-01-01

    The scanning proton microprobe is shown to be a sensitive instrument for elemental microanalysis of cells and tissues in biological and medical specimens. The preparation of specimens and their behaviour under irradiation are crucial and the application of quantitative scanning analysis to the monitoring of such problems is illustrated

  6. A novel technique for producing antibody-coated microprobes using a thiol-terminal silane and a heterobifunctional crosslinker.

    Science.gov (United States)

    Routh, V H; Helke, C J

    1997-02-01

    Antibody-coated microprobes are used to measure neuropeptide release in the central nervous system. Although they are not quantitative, they provide the most precise spatial resolution of the location of in vivo release of any currently available method. Previous methods of coating antibody microprobes are difficult and time-consuming. Moreover, using these methods we were unable to produce evenly coated antibody microprobes. This paper describes a novel method for the production of antibody microprobes using thiol-terminal silanes and the heterobifunctional crosslinker, 4-(4-N-maleimidophenyl)butyric acid hydrazide HCl 1/2 dioxane (MPBH). Following silation, glass micropipettes are incubated with antibody to substance P (SP) that has been conjugated to MPBH. This method results in a dense, even coating of antibody without decreasing the biological activity of the antibody. Additionally, this method takes considerably less time than previously described methods without sacrificing the use of antibody microprobes as micropipettes. The sensitivity of the microprobes for SP is in the picomolar range, and there is a linear correlation between the log of SP concentration (M) and B/B0 (r2 = 0.98). The microprobes are stable for up to 3 weeks when stored in 0.1 M sodium phosphate buffer with 50 mM NaCl (pH 7.4) at 5 degrees C. Finally, insertion into the exposed spinal cord of an anesthetized rat for 15 min produces no damage to the antibody coating.

  7. IMAP: A complete Ion Micro-Analysis Package for the nuclear microprobe

    International Nuclear Information System (INIS)

    Antolak, A.J.; Hildner, M.L.; Morse, D.H.; Bench, G.S.

    1993-01-01

    Microprobe techniques using scanned, focused MeV ions are routinely used in Livermore for materials characterization. Comprehensive data analysis with these techniques is accomplished with the computer software package IMAP, for Ion Micro-Analysis Package. IMAP consists of a set of command language procedures for data processing and quantitative spectral analysis. Deconvolution of the data is achieved by spawning sub-processes within IMAP which execute analysis codes for each specific microprobe technique. IMAP is structured to rapidly analyze individual spectra or multi-dimensional data blocks which classify individual events by the two scanning dimensions, the energy of the detected radiation and, when necessary, one sample rotation dimension. Several examples are presented to demonstrate the utility of the package

  8. Charge collection control using retrograde well tested by proton microprobe irradiation

    International Nuclear Information System (INIS)

    Sayama, Hirokazu; Takai, Mikio; Kimura, Hiroshi; Ohno, Yoshikazu; Satoh, Shinichi; Sonoda, Kenichirou; Katani, Norihiko.

    1993-01-01

    Soft error reduction by high-energy ion-implanted layers has been investigated by novel evaluation techniques using high-energy proton microprobes. A retrograde well formed by 160 and 700 keV boron ion implantation could completely suppress soft errors induced by the proton microprobes at 400 keV. The proton-induced current revealed the charge collection efficiency for the retrograde well structure. The collected charge for the retrograde well in the soft-error mapping was proved to be lower than the critical charge of the measured DRAMs(dynamic random-access memories). Complementary use of soft-error mapping and ion-induced-current measurement could clarify well structures immune against soft errors. (author)

  9. Combining Raman Microprobe and XPS to Study High Temperature Oxidation of Metals

    International Nuclear Information System (INIS)

    Windisch, Charles F.; Henager, Charles H.; Engelhard, Mark H.; Bennett, Wendy D.

    2011-01-01

    Raman microprobe spectroscopy was applied in studies of high-temperature air oxidation of a ferritic alloy (HT-9) in the absence and presence of zirconia coatings with the objective of evaluating the technique as a way to quickly screen candidate cladding materials and actinide-based mixed oxide fuel mixtures for advanced nuclear reactors. When oxidation was relatively uniform, Raman spectra collected using microscope optics with low spatial resolution were found to be similar to those collected with conventional Raman spectroscopy. These spectra could be used to identify major oxide corrosion products and follow changes in the composition of the oxides due to heating. However, when the oxidation films were comprised of multiple layers of varying composition, or with layers containing metallic phases, techniques with higher depth resolution and sensitivity to zero-valence metals were necessary. The requirements were met by combining Raman microprobe using different optical configurations and x-ray photoelectron spectroscopy.

  10. Study of ion tracks by micro-probe ion energy loss spectroscopy

    Czech Academy of Sciences Publication Activity Database

    Vacík, Jiří; Havránek, Vladimír; Hnatowicz, Vladimír; Horák, Pavel; Fink, Dietmar; Apel, P. Yu.

    2014-01-01

    Roč. 332, AUG (2014), s. 308-311 ISSN 0168-583X. [21st International Conference on Ion Beam Analysis (IBA). Seattle, 23.06.2013-28.06.2013] R&D Projects: GA ČR(CZ) GBP108/12/G108; GA MŠk(XE) LM2011019 Institutional support: RVO:61389005 Keywords : ion energy loss spectrometry * single ion track * microprobe * tomography Subject RIV: BM - Solid Matter Physics ; Magnetism Impact factor: 1.124, year: 2014

  11. Lateral diffusion study of the Pt-Al system using the NAC nuclear microprobe.

    Science.gov (United States)

    de Waal, H.; Pretorius, R.

    1999-10-01

    In this study a nuclear microprobe (NMP) was used to analyse phase formation during reaction in Pt-Al lateral diffusion couples. Phase identification was done by Rutherford backscattering spectroscopy. These results were compared with phase formation during conventional thin film Pt-Al interactions. The co-existence of multiple phases in lateral diffusion couples is discussed with reference to the effective heat of formation (EHF) model.

  12. Lateral diffusion study of the Pt-Al system using the NAC nuclear microprobe

    Energy Technology Data Exchange (ETDEWEB)

    Waal, H. de E-mail: dewalla@nac.ac.za; Pretorius, R

    1999-09-02

    In this study a nuclear microprobe (NMP) was used to analyse phase formation during reaction in Pt-Al lateral diffusion couples. Phase identification was done by Rutherford backscattering spectroscopy. These results were compared with phase formation during conventional thin film Pt-Al interactions. The co-existence of multiple phases in lateral diffusion couples is discussed with reference to the effective heat of formation (EHF) model.

  13. U and Pb isotope analysis of uraninite and galena by ion microprobe

    Energy Technology Data Exchange (ETDEWEB)

    Evins, L.Z.; Sunde, T.; Schoeberg, H. [Swedish Museum of Natural History, Stockholm (Sweden). Laboratory for Isotope Geology; Fayek, M. [Univ. of Tennessee, Knoxville, TN (United States). Dept. of Geological Sciences

    2001-10-01

    Accurate isotopic analysis of minerals by ion microprobe, or SIMS (Secondary Ion Mass Spectrometry) usually requires a standard to correct for instrumental mass bias effects that occur during analysis. We have calibrated two uraninite crystals and one galena crystal to be used as ion probe standards. As part of this study we describe the analytical procedures and problems encountered while trying to establish fractionation factors for U and Pb isotopes measured in galena and uraninite. Only the intra-element isotopic mass fractionation is considered and not the interelement fractionation. Galena and uraninite were analysed with TIMS (Thermal Ionisation Mass Spectrometry) prior to SIMS. One uraninite crystal (P88) comes from Sweden and is ca 900 Ma old, the other from Maine, USA (LAMNH-30222) and is ca 350 Ma old. The galena sample comes from the Paleoproterozoic ore district Bergslagen in Sweden. SIMS analyses were performed at two different laboratories: the NORDSM facility in Stockholm, which has a high resolution Cameca IMS 1270 ion microprobe, and the Oak Ridge National Laboratory (ORNL) in Tennessee, which has a Cameca IMS 4f ion microprobe. The results show that during the analysis of galena, Pb isotopes fractionate in favour of the lighter isotope by as much as 0.5%/amu. A Pb isotope fractionation factor for uraninite was more difficult to calculate, probably due to the formation of hydride interferences encountered during analysis with the Cameca IMS 1270 ion microprobe. However, drying the sample in vacuum prior to analysis, and using high-energy filtering and a cold trap during analysis can minimise these hydride interferences. A large fractionation of U isotopes of ca 1.4%/amu in favour of the lighter isotope was calculated for uraninite.

  14. Total quantitative recording of elemental maps and spectra with a scanning microprobe

    International Nuclear Information System (INIS)

    Legge, G.J.F.; Hammond, I.

    1979-01-01

    A system of data recording and analysis has been developed by means of which simultaneously all data from a scanning instrument such as a microprobe can be quantitatively recorded and permanently stored, including spectral outputs from several detectors. Only one scanning operation is required on the specimen. Analysis is then performed on the stored data, which contain quantitative information on distributions of all elements and spectra of all regions

  15. Application of the microprobe dredging operation in the treatment of the meibomian gland dysfunction(MGD

    Directory of Open Access Journals (Sweden)

    Qing-Qiang Wang

    2014-07-01

    Full Text Available AIM: To evaluate the function of the microprobe dredging technology in the treatment of meibomian gland dysfunction(MGDand to provide fast, efficient, economical and practical method of treatment for meibomian gland dysfunction(MGD. METHODS:The 100μm diameter stainless steel wire was made as the microprobe with the total length of 3cm, which the needle was about 5mm and hand shank was about 2.5cm. Selected 140 cases with dry eyes of meibomian gland dysfunction(MGD, patients were divided into two groups and made them have comparability. Observation group(n=70used microprobe to dredge meibomian gland pipe accompanied with drugs, hot compress and meibomian gland massage treatment. The control group(n=70was given conventional drugs, hot compress and meibomian massage treatment. To compare the tear break-up time(BUT, efficient rate and the cure rate of the two groups after treatment of 1d, 1wk, 2wk, 1 mo, 2mo and 3mo.RESULTS: BUT were significantly prolonged in observation group and control group after treatment, and the observation group improved more obviously; the efficient rate and cure rate of the observation group were significantly higher than that of the control group after 1d, 1wk, 2wk, 1mo, 2mo and 3mo treatment. CONCLUSION:Using microprobe to unclog the meibomian gland tube can provide the fast and efficient, economical and practical treatment for meibomian gland dysfunction(MGD, which can be promoted in the clinical practice.

  16. U and Pb isotope analysis of uraninite and galena by ion microprobe

    International Nuclear Information System (INIS)

    Evins, L.Z.; Sunde, T.; Schoeberg, H.; Fayek, M.

    2001-10-01

    Accurate isotopic analysis of minerals by ion microprobe, or SIMS (Secondary Ion Mass Spectrometry) usually requires a standard to correct for instrumental mass bias effects that occur during analysis. We have calibrated two uraninite crystals and one galena crystal to be used as ion probe standards. As part of this study we describe the analytical procedures and problems encountered while trying to establish fractionation factors for U and Pb isotopes measured in galena and uraninite. Only the intra-element isotopic mass fractionation is considered and not the interelement fractionation. Galena and uraninite were analysed with TIMS (Thermal Ionisation Mass Spectrometry) prior to SIMS. One uraninite crystal (P88) comes from Sweden and is ca 900 Ma old, the other from Maine, USA (LAMNH-30222) and is ca 350 Ma old. The galena sample comes from the Paleoproterozoic ore district Bergslagen in Sweden. SIMS analyses were performed at two different laboratories: the NORDSM facility in Stockholm, which has a high resolution Cameca IMS 1270 ion microprobe, and the Oak Ridge National Laboratory (ORNL) in Tennessee, which has a Cameca IMS 4f ion microprobe. The results show that during the analysis of galena, Pb isotopes fractionate in favour of the lighter isotope by as much as 0.5%/amu. A Pb isotope fractionation factor for uraninite was more difficult to calculate, probably due to the formation of hydride interferences encountered during analysis with the Cameca IMS 1270 ion microprobe. However, drying the sample in vacuum prior to analysis, and using high-energy filtering and a cold trap during analysis can minimise these hydride interferences. A large fractionation of U isotopes of ca 1.4%/amu in favour of the lighter isotope was calculated for uraninite

  17. Distribution of copper and other elements in ryegrass roots, determined with a scanning proton microprobe

    International Nuclear Information System (INIS)

    Mazzolini, A.P.; Legge, G.J.F.

    1982-01-01

    A scanning proton microprobe has been used to determine the distribution of Cu and other elements in Wimmera ryegrass roots grown in solution cultures. Cu was found to be localized on or near the surface of the roots in randomly distributed discrete zones. The distribution of Cu was partially correlated with those of Fe, P and Ca and possibly indicates some form of association; co-precipitation in a precipitate of ferric phosphate or hydroxy-oxide is favoured

  18. The study of voids in the AuAl thin-film system using the nuclear microprobe

    Science.gov (United States)

    de Waal, H. S.; Pretorius, R.; Prozesky, V. M.; Churms, C. L.

    1997-07-01

    A Nuclear Microprobe (NMP) was used to study void formation in thin film gold-aluminium systems. Microprobe Rutherford Backscattering Spectrometry (μRBS) was utilised to effectively obtain a three-dimensional picture of the void structure on the scale of a few nanometers in the depth dimension and a few microns in the in-plane dimension. This study illustrates the usefulness of the NMP in the study of materials and specifically thin-film structures.

  19. Quantitative elemental imaging of octopus stylets using PIXE and the nuclear microprobe

    Energy Technology Data Exchange (ETDEWEB)

    Doubleday, Zoe [Marine Research Laboratories, Tasmanian Aquaculture and Fisheries Institute, University of Tasmania, Private Bag 49, Tasmania 7001 (Australia)], E-mail: zoeanned@utas.edu.au; Belton, David [CSIRO Exploration and Mining, University of Melbourne (School of Physics), Melbourne 3010 (Australia); Pecl, Gretta; Semmens, Jayson [Marine Research Laboratories, Tasmanian Aquaculture and Fisheries Institute, University of Tasmania, Private Bag 49, Tasmania 7001 (Australia)

    2008-01-15

    By utilising targeted microprobe technology, the analysis of elements incorporated within the hard bio-mineralised structures of marine organisms has provided unique insights into the population biology of many species. As hard structures grow, elements from surrounding waters are incorporated effectively providing a natural 'tag' that is often unique to the animal's particular location or habitat. The spatial distribution of elements within octopus stylets was investigated, using the nuclear microprobe, to assess their potential for determining dispersal and population structure in octopus populations. Proton Induced X-ray Emission (PIXE) was conducted using the Dynamic Analysis method and GeoPIXE software package, which produced high resolution, quantitative elemental maps of whole stylet cross-sections. Ten elements were detected within the stylets which were heterogeneously distributed throughout the microstructure. Although Ca decreased towards the section edge, this trend was consistent between individuals and remained homogeneous in the inner region of the stylet, and thus appears a suitable internal standard for future microprobe analyses. Additional analyses used to investigate the general composition of the stylet structure suggested that they are amorphous and largely organic, however, there was some evidence of phosphatic mineralisation. In conclusion, this study indicates that stylets are suitable for targeted elemental analysis, although this is currently limited to the inner hatch region of the microstructure.

  20. Quantitative elemental imaging of octopus stylets using PIXE and the nuclear microprobe

    International Nuclear Information System (INIS)

    Doubleday, Zoe; Belton, David; Pecl, Gretta; Semmens, Jayson

    2008-01-01

    By utilising targeted microprobe technology, the analysis of elements incorporated within the hard bio-mineralised structures of marine organisms has provided unique insights into the population biology of many species. As hard structures grow, elements from surrounding waters are incorporated effectively providing a natural 'tag' that is often unique to the animal's particular location or habitat. The spatial distribution of elements within octopus stylets was investigated, using the nuclear microprobe, to assess their potential for determining dispersal and population structure in octopus populations. Proton Induced X-ray Emission (PIXE) was conducted using the Dynamic Analysis method and GeoPIXE software package, which produced high resolution, quantitative elemental maps of whole stylet cross-sections. Ten elements were detected within the stylets which were heterogeneously distributed throughout the microstructure. Although Ca decreased towards the section edge, this trend was consistent between individuals and remained homogeneous in the inner region of the stylet, and thus appears a suitable internal standard for future microprobe analyses. Additional analyses used to investigate the general composition of the stylet structure suggested that they are amorphous and largely organic, however, there was some evidence of phosphatic mineralisation. In conclusion, this study indicates that stylets are suitable for targeted elemental analysis, although this is currently limited to the inner hatch region of the microstructure

  1. Electron microprobe analyses of glasses from Kīlauea tephra units, Kīlauea Volcano, Hawaii

    Science.gov (United States)

    Helz, Rosalind L.; Clague, David A.; Mastin, Larry G.; Rose, Timothy R.

    2014-01-01

    This report presents approximately 2,100 glass analyses from three tephra units of Kīlauea Volcano: the Keanakākoʻi Tephra, the Kulanaokuaiki Tephra, and the Pāhala Ash. It also includes some new analyses obtained as part of a re-evaluation of the MgO contents of glasses in two of the three original datasets; this re-evaluation was conducted to improve the consistency of glass MgO contents among the three datasets. The glass data are a principal focus of Helz and others (in press), which will appear in the AGU Monograph Hawaiian Volcanoes—From Source to Surface. The report is intended to support this publication, in addition to making the data available to the scientific community.

  2. Method validation for chemical composition determination by electron microprobe with wavelength dispersive spectrometer

    Science.gov (United States)

    Herrera-Basurto, R.; Mercader-Trejo, F.; Muñoz-Madrigal, N.; Juárez-García, J. M.; Rodriguez-López, A.; Manzano-Ramírez, A.

    2016-07-01

    The main goal of method validation is to demonstrate that the method is suitable for its intended purpose. One of the advantages of analytical method validation is translated into a level of confidence about the measurement results reported to satisfy a specific objective. Elemental composition determination by wavelength dispersive spectrometer (WDS) microanalysis has been used over extremely wide areas, mainly in the field of materials science, impurity determinations in geological, biological and food samples. However, little information is reported about the validation of the applied methods. Herein, results of the in-house method validation for elemental composition determination by WDS are shown. SRM 482, a binary alloy Cu-Au of different compositions, was used during the validation protocol following the recommendations for method validation proposed by Eurachem. This paper can be taken as a reference for the evaluation of the validation parameters more frequently requested to get the accreditation under the requirements of the ISO/IEC 17025 standard: selectivity, limit of detection, linear interval, sensitivity, precision, trueness and uncertainty. A model for uncertainty estimation was proposed including systematic and random errors. In addition, parameters evaluated during the validation process were also considered as part of the uncertainty model.

  3. Determination of xenon in irradiated nuclear fuel using a shielded electron microprobe

    International Nuclear Information System (INIS)

    Jenson, E.D.

    1983-06-01

    The technique described produces a semi-quantitative determination of the distribution of xenon present in a section of fuel pin along a predetermined line. The x-ray counting technique chosen is to drive the spectrometer over the peak in small increments, counting at each step, then to integrate the resulting data over the entire peak. Counting times are usually 10 sec at each step and there are 30 to 40 steps over a peak. Interferences and possible loss of Xe due to local heating are discussed. Comparison with independent analysis is presented

  4. Elemental analysis of some West Malaysian limestones using neutron activation, delayed neutron and electron microprobe analysis

    International Nuclear Information System (INIS)

    Amin, Y.M.; Kamaluddin, B.; Mahat, R.H.

    1990-01-01

    Limestone stratigraphy in Malaysia has been and is dependent almost entirely in palaeontology. However fossil localities are sporadic and as such a new fossil discovery mean the necessity for a complete re-appraisal of the stratigraphy. The almost complete dependence upon palaeontology results from the difficulties of stratigraphy correlation of isolated outcrops, from the cover of tropical vegetation and from the often complex folding and faulting which has been imposed on the geosyn-clinical rocks by the Indonesian-Thai-Malayan orogeny. So by studying the elemental composition of limestones accurately, we would be able to correlate outcrops and other stratigraphic samples independent of fossil finds. The use of delayed neutron analysis would also determine the concentration of uranium and thorium accurately. This study, in conjunction with thermoluminescence and fission track studies, would able us to date the age of the limestones

  5. Automated electron microprobe identification of minerals in stream sediments for the national uranium resources evaluation program

    International Nuclear Information System (INIS)

    Mosley, W.C. Jr.

    1979-01-01

    Over 500 stream sediment particles have been analyzed. About 96% have been identified as distinct minerals. Most of the others appeared to be mixtures. Only zinc-bearing gahnite had to be analyzed further for positive identification. Monazite and zircon were the only minerals with concentrations of uranium significantly above the detection limit. The Frantz Isodynamic Magnetic Separator isolated the monazite into the 1.0 fraction. Monazite particles in anomalous sediments contained up to 3.7 wt % uranium. This uranium concentration is unusually high for monazite, which normally has about 0.5 wt % uranium, and may be the cause of the anomaly

  6. Use of X-ray microprobe to diagnose bone tissue demineralization after caffeine administration Use of X-ray microprobe to diagnose bone tissue demineralization after caffeine administration

    Directory of Open Access Journals (Sweden)

    Marek Tomaszewski

    2012-10-01

    Full Text Available Caffeine is a methylxanthine which permeates the placenta. In studies on animals, it has been
    shown to produce teratogenic and embryotoxic effects in large doses. The objective of this study was to
    assess the influence of caffeine on the development of bone tissue, with particular reference to elemental
    bone composition using an X-ray microprobe. The research was conducted on rats. The fertilized females
    were randomly divided into an experimental and a control group. The experimental group was
    given caffeine orally in 30 mg/day doses from the 8th to the 21st day of pregnancy, while the control group
    was given water. The fetuses were used to assess the growth and mineralization of the skeleton. On the
    basis of double dyeing, a qualitative analysis of the bone morphology and mineralization was conducted.
    For calcium and potassium analysis, an X-ray microprobe was used. In 67 fetuses from the experimental
    group, changes in skeleton staining with the alcian-alizarin method were noticed. The frequency of the
    development of variants in the experimental group was statistically higher. In the experimental group,
    a significant decrease in the calcium level, as well as an increase in the potassium level, was observed.
    The X-ray microprobe’s undoubted advantage is that is offers a quick qualitative and quantitative analysis
    of the elemental composition of the examined samples. Employing this new technique may furnish us
    with new capabilities when investigating the essence of the pathology process.Caffeine is a methylxanthine which permeates the placenta. In studies on animals, it has been
    shown to produce teratogenic and embryotoxic effects in large doses. The objective of this study was to
    assess the influence of caffeine on the development of bone tissue, with particular reference to elemental
    bone composition using an X-ray microprobe. The research was conducted on

  7. A petrologic and ion microprobe study of a Vigarano Type B refractory inclusion - Evolution by multiple stages of alteration and melting

    Science.gov (United States)

    Macpherson, Glenn J.; Davis, Andrew M.

    1993-01-01

    A Type B Ca-, Al-rich 6-m-diam inclusion (CAI) found in the Vigarano C3V chondrite was inspected using optical and scanning electron microscopies and ion microprobe analyses. It was found that the primary constituents of the CAI inclusion are (in percent), melilite (52), fassaite, (20), anorthite (18), spinel (10), and trace Fe-Ni metal. It is noted that, while many of the properties of the inclusion indicate solidification from a melt droplet, the Al-26/Mg-26 isotopic systematics and some textural relationships are incompatible with single-stage closed system crystallization of a homogeneous molten droplet, indicating that the history of this inclusion must have been more complex than melt solidification alone. Moreover, there was unusually high content of Na in melilite, suggesting that the droplet did not form by melting of pristine high-temperature nebular condensates.

  8. A Variable-Energy Soft X-Ray Microprobe to Investigate Mechanisms of the Radiation-Induced Bystander Effect

    International Nuclear Information System (INIS)

    Folkard, Melvyn; Vojnovic, Borivoj; Schettino, Giuseppe; Atkinson, Kirk; Prise, Kevin M.; Michael, Barry D.

    2007-01-01

    The Gray Cancer Institute has pioneered the use of X ray focusing techniques to develop systems for micro irradiating individual cells and sub cellular targets in vitro. Cellular micro irradiation is now recognized as a highly versatile technique for understanding how ionizing radiation interacts with living cells and tissues. The strength of the technique lies in its ability to deliver precise doses of radiation to selected individual cells (or sub cellular targets). The application of this technique in the field of radiation biology continues to be of great interest for investigating a number of phenomena currently of concern to the radiobiological community. One important phenomenon is the so called ''bystander effect'' where it is observed that unirradiated cells can also respond to signals transmitted by irradiated neighbors. Clearly, the ability of a microbeam to irradiate just a single cell or selected cells within a population is well suited to studying this effect. Our prototype ''tabletop'' X-ray microprobe was optimized for focusing 278 eV C-K X rays and has been used successfully for a number of years. However, we have sought to develop a new variable energy soft X-ray microprobe capable of delivering focused CK (0.28 keV), Al-K (1.48 keV) and notably, Ti-K (4.5 keV) X rays. Ti-K X rays are capable of penetrating several cell layers and are therefore much better suited to studies involving tissues and multi cellular layers. In our new design, X-rays are generated by the focused electron bombardment of a material whose characteristic-K radiation is required. The source is mounted on a 1.5 x 1.0 meter optical table. Electrons are generated by a custom built gun, designed to operate up to 15 kV. The electrons are focused using a permanent neodymium iron boron magnet assembly. Focusing is achieved by adjusting the accelerating voltage and by fine tuning the target position via a vacuum position feedthrough. To analyze the electron beam properties, a custom

  9. Preditores das atitudes negativas face ao envelhecimento e face à sexualidade na terceira idade

    OpenAIRE

    Pereira, Diane; Ponte, Filomena; Costa, Eleonora

    2018-01-01

    Este estudo analisou as diferenças entre jovens e idosos ao nível das atitudes e dos conhecimentos face ao envelhecimento e face à sexualidade na terceira idade, a relação entre as variáveis em estudo, e os preditores das atitudes negativas face ao envelhecimento e das atitudes negativas face à sexualidade na terceira idade. Cento e cinquenta e três jovens universitários e 42 idosos participaram no estudo. Os resultados indicaram que os jovens apresentam um menor nível de conhecimentos acerca...

  10. Idade dos ratos versus idade humana: qual é a relação? Rat's age versus human's age: what is the relationship?

    Directory of Open Access Journals (Sweden)

    Nelson Adami Andreollo

    2012-03-01

    Full Text Available RACIONAL: Milhões de ratos são empregados anualmente em pesquisas e no ensino. A exata relação entre a idade dos ratos, comparada com a idade dos humanos ainda é assunto de discussão e controvérsias. OBJETIVO: É revisar a literatura, analisando a idade dos ratos em comparação com a idade dos homens. MÉTODOS: Foram revisadas as publicações existentes sobre o assunto contidas nas bases Medline/Pubmed, Scielo, Biblioteca Cochrane e Lilacs cruzando os descritores ratos, cirurgia experimental e fisiologia. RESULTADOS: Ratos desenvolvem rapidamente durante a infância e se tornam sexualmente maduros com cerca de seis semanas de idade, mas atingem a maturidade social cinco a seis meses mais tarde. Na idade adulta, a cada mês do animal é aproximadamente equivalente a 2,5 anos humanos. Vários autores realizaram trabalhos experimentais em ratos e afirmaram existir correspondência de 30 dias de vida do homem para cada dia de vida do rato. CONCLUSÃO: As diferenças na anatomia, fisiologia, desenvolvimento e fenômenos biológicos devem ser levados em consideração quando são analisados os resultados de qualquer pesquisa em ratos em que a idade é um fator crucial. Cuidado especial é necessário ser tomado quando os estudos efetuados pretendem produzir correlação com a vida humana. Para isso, atenção especial é necessária para verificar a fase em dias do animal e sua correlação com os anos em humanos.BACKGROUND: Millions of mice are used annually in research and teaching. The exact relationship between age of the animals compared with the age of humans is still subject to discussion and controversy. OBJECTIVE: Literature review analyzing the age of rats in comparison with men age. METHODS: Were reviewed the existing publications on the subject contained in Medline / Pubmed, Scielo, The Cochrane Database of Systematic Reviews and Lilacs crossing the headings rats, experimental surgery and physiology. RESULTS: Rats rapidly develop

  11. Electronics

    Science.gov (United States)

    2001-01-01

    International Acer Incorporated, Hsin Chu, Taiwan Aerospace Industrial Development Corporation, Taichung, Taiwan American Institute of Taiwan, Taipei, Taiwan...Singapore and Malaysia .5 - 4 - The largest market for semiconductor products is the high technology consumer electronics industry that consumes up...Singapore, and Malaysia . A new semiconductor facility costs around $3 billion to build and takes about two years to become operational

  12. Application of tomographic techniques to two-dimensional surface analysis using the Harwell nuclear microprobe

    International Nuclear Information System (INIS)

    Huddleston, J.; Hutchinson, I.G.; Pierce, T.B.

    1983-01-01

    Nuclear methods of surface analysis are discussed briefly, and the circumstances are described in which a two-dimensional analysis of the sample surface is desirable to enable the surface composition to be mapped accurately. Tomographic techniques of data manipulation are outlined. Data acquisition in the present case is performed by moving the sample in a defined sequence of positions, at each of which analytical data are gathered by the proton microprobe. The method and equipment are outlined. Data processing leading to the reconstruction of the image is summarised. (U.K.)

  13. New 2-stage ion microprobes and a move to higher energies

    Energy Technology Data Exchange (ETDEWEB)

    Legge, G.J.F.; Dymnikov, A.; Moloney, G.; Saint, A. [Melbourne Univ., Parkville, VIC (Australia). School of Physics; Cohen, D. [Australian Nuclear Science and Technology Organisation, Lucas Heights, NSW (Australia)

    1996-12-31

    Recent moves in Ion Beam Microanalysis towards the use of a rapidly growing number of very high resolution, low current and single ion techniques has led to the need for high demagnification and greatly improved beam quality. There is also a move to apply Microbeams at higher energies and with heavier ions. This also puts demands on the focusing system and beam control. This paper describes the recent development of 2-stage lens systems to be applied here and overseas, both at very high resolution and at high energies with heavy ions. It looks at new ion beam analysis applications of such ion microprobes. 8 refs., 1 tab., 1 fig.

  14. A new Krakow scanning nuclear microprobe performance tests and early application experienc

    CERN Document Server

    Lebed, S; Polak, W; Potempa, A W; Stachura, Z; Paszkowski, M

    2001-01-01

    A new scanning nuclear microprobe (MP) with a short-length probe forming system was designed,installed and tested at the 3MV Van de Graaff accelerator in Krakow.The MP resolution of 3.3 mu m was reached for 2.4 MeV proton beam in the high-current mode (>= 100pA).The MP facility provides a local,non-destructive,quantitative elemental microanalysis using a Proton Induced X-ray Emission (PIXE) technique.As example of possible application an analysis of a geological sample containing monazite crystals investigated by PIXE method is presented.

  15. New 2-stage ion microprobes and a move to higher energies

    Energy Technology Data Exchange (ETDEWEB)

    Legge, G J.F.; Dymnikov, A; Moloney, G; Saint, A [Melbourne Univ., Parkville, VIC (Australia). School of Physics; Cohen, D [Australian Nuclear Science and Technology Organisation, Lucas Heights, NSW (Australia)

    1997-12-31

    Recent moves in Ion Beam Microanalysis towards the use of a rapidly growing number of very high resolution, low current and single ion techniques has led to the need for high demagnification and greatly improved beam quality. There is also a move to apply Microbeams at higher energies and with heavier ions. This also puts demands on the focusing system and beam control. This paper describes the recent development of 2-stage lens systems to be applied here and overseas, both at very high resolution and at high energies with heavy ions. It looks at new ion beam analysis applications of such ion microprobes. 8 refs., 1 tab., 1 fig.

  16. Characterisation of candidate reference materials by PIXE analysis and nuclear microprobe PIXE imaging

    International Nuclear Information System (INIS)

    Jaksic, M.; Pastuovic, Z.; Bogdanovic, I.; Tadic, T.

    2002-01-01

    In order to test whether some candidate reference materials show homogeneity that can satisfy quality control of the PIXE technique, six bottles of each of the two Candidate RM's - Lichen (IAEA 338) and Algae (IAEA 413) were tested. Four different tests were performed. First, two pellets from each bottle were prepared and analysed using broad beam (φ = 5 mm) PIXE. Second and third was analysis of homogeneity using scanning focussed beam at the nuclear microprobe. Scans of 50x50 μm 2 and 240x260 μm 2 were performed. Finally, individual grains with composition differing from the rest of the sample, were analysed using PIXE and RBS. (author)

  17. Cometary and interstellar dust grains - Analysis by ion microprobe mass spectrometry and other techniques

    Science.gov (United States)

    Zinner, Ernst

    1991-01-01

    A survey of microanalytical measurements on interplanetary dust particles (IDPs) and interstellar dust grains from primitive meteorites is presented. Ion-microprobe mass spectrometry with its capability to determine isotopic compositions of many elements on a micron spatial scale has played a special role. Examples are measurements of H, N, and O isotopes and refractory trace elements in IDPs; C, N, Mg, and Si isotopes in interstellar SiC grains; and C and N isotopes and H, N, Al, and Si concentrations in interstellar graphite grains.

  18. CMB v. 1.1 Data Acquisition and Evaluation System of the Cracow Nuclear Microprobe

    International Nuclear Information System (INIS)

    Lekki, J.; Hajduk, R.; Potempa, A.; Pieprzyca, T.; Stachura, Z.; Zieblinski, M.; Styczen, J.; Lebed, S.

    2000-11-01

    An overview of the Cracow nuclear microprobe together with its data acquisition and control system is presented. Magnetic deflection was applied for beam scanning, while detector signals acquisition is performed by the NIM/CAMAC modules under supervision of a Windows operating system running on a PC equipped with the GPIB controller card. Total spectra from every detector are accessible on-line during the measurement, while full information about detected energy and beam position is stored to a disk file in the list mode to allow off-line data analysis. System hardware and software setups together with software operations and data formats used for information storing are described. (author)

  19. A digital squarer system for positive mass identification on the ARL ion microprobe mass analyser

    International Nuclear Information System (INIS)

    Woods, K.N.; Grant, L.D.V.; Rawsthorne, E.D.; Strydom, H.J.; Gries, W.H.

    1984-01-01

    The original analogue squarer for mass scale linearisation in the Ion Microprobe Mass Analyser (IMMA) has been replaced by a programmable digital squarer system which permits reliable mass number identification throughout the tested range 1 to 240. The digital squarer provides signals to both a digital direct reading mass number display and to an X-Y recorder where it provides a linear mass scale correct to within 0,3 mass units. An additional output to a computer can provide binary or BCD mass number data

  20. X-ray microprobe measurements of the chemical compositions of ALH84001 carbonate globules

    International Nuclear Information System (INIS)

    Flynn, G.J.; Sutton, S.R.; Keller, L.P.

    2004-01-01

    We measured minor element contents of carbonate from ALH84001 and report trends in tbe Ca, V, Mn and Sr in carbonate and the associated magnetite bands. McKay et al. suggested that carbonate globules in the ALH84001 meteorite from Mars contained evidence consistent with the development of bacterial life early in the history of Mars. This result provoked an extensive study of the ALH84001 meteorite. More recently Thomas-Keprta et al. have published a study showing that the magnetite associated with carbonate rims are of the size and shape produced by terrestrial bacteria. This paper has revived interest in ALH84001. The typical ALH84001 carbonate globule consists of four regions: a core of Fe-rich carbonate, a thin magnetite-rich band, a rim of Mn-rich carbonate, and another thin magnetite-rich band. Trace element analysis of each of these phases may allow us to address several important questions about these carbonates: (1) The origin of the magnetite-rich bands in the ALH84001 carbonate globules. If the magnetites are derived from the underlying carbonate through thermal decomposition (as proposed by Golden et al.), then we expect to see 'inherited' trace elements in these magnetite bands. (2) The origin of the rim carbonate, by determining whether the carbonate in the core has the same trace elements as the rim carbonates. (3) The age of the rim carbonate. Borg et al. dated the formation of the rim carbonate using the Rb/Sr chronometer. Borg et al. performed their measurements on an aliquot of what they called a high-Rb, low-Sr carbonate separate from the rim. We previously measured the trace element contents of chips from core and rim carbonates from an ALH84001 carbonate globule using an X-Ray Microprobe on Beamline X26A at the National Synchrotron Light Source. These measurements showed the rim carbonate had a very low Rb content, with Sr>>Rb, inconsistent with the ∼5 ppm Rb reported by Borg et al. in the sample they dated by the Rb/Sr chronometer. The large

  1. Individual precipitates in Al alloys probed by the Bonn positron microprobe

    Energy Technology Data Exchange (ETDEWEB)

    Balarisi, Osman; Eich, Patrick; Haaks, Matz; Klobes, Benedikt; Korff, Bjoern; Maier, Karl; Sottong, Reinhard [Helmholtz-Institut fuer Strahlen- und Kernphysik, Nussallee 14-16, 53115 Bonn (Germany); Huehne, Sven-Martin; Mader, Werner [Institut fuer Anorganische Chemie, Roemerstrasse 164, 53117 Bonn (Germany); Staab, Torsten [Fraunhofer ISC, Neunerplatz 2, 97082 Wuerzburg (Germany)

    2010-07-01

    Positron annihilation spectroscopy (PAS) is a unique tool for the characterization of open-volume defects such as vacancies. Therefore, age hardenable Al alloys, whose decomposition is mainly driven by the vacancy mechanism of diffusion, are often characterized by PAS techniques. Nevertheless, probing the defect state of individual precipitates grown in Al alloys requires a focused positron beam and has not been carried out up to now. In this respect we present the first investigations of the defect state of individual precipitates utilizing the Bonn Positron Microprobe (BPM). Furthermore, the analysis of the experimental data has to be facilitated by theoretical calculations of the observables of positron annihilation spectroscopy.

  2. Effect of magnetic quadrupole lens alignment on a nuclear microprobe resolution

    International Nuclear Information System (INIS)

    Kolinko, S.V.; Ponomarev, A.G.

    2016-01-01

    The paper reports the research trends in developing probe-forming systems with high demagnification and analysis factors that limit a nuclear microprobe resolution. Parasitic aberrations caused by tilts and offsets of magnetic quadrupoles are studied in terms of their effect on probe parameters on a target. The most common arrangements of probe-forming systems such as a triplet and “Russian quadruplet” with separated geometry are considered. The accuracy prerequisites for the positioning of the quadrupoles are defined, and practical guidelines for alignment of probe-forming systems with high demagnification factors are suggested.

  3. Efeitos de Idade e Sexo no Autoconceito de Crianças Pré-Escolares

    Directory of Open Access Journals (Sweden)

    Alexandra Pinto

    2015-09-01

    Full Text Available Poucas são as investigações sobre o autoconceito realizadas com crianças de idade pré-escolar. Neste estudo procuramos contribuir para uma melhor compreensão do desenvolvimento normativo do autoconceito, no período pré-escolar, nomeadamente, através da análise dos efeitos que o sexo e a idade têm no mesmo. Tratando-se de um estudo longitudinal, a amostra foi composta por 83 crianças portuguesas, avaliadas no seu autoconceito aos quatro e aos cinco anos de idade, através da Pictorial Scale of Perceived Competence and Social Acceptance for Young Children - PSPCSA. As crianças apresentaram resultados muito elevados em todos os domínios do autoconceito, em ambas as idades Os dados parecem indicar que os elevados valores do autoconceito começam a declinar já no fim do período pré-escolar, pelo menos em alguns domínios, sugerindo, dessa forma, um desenvolvimento diferenciado do autoconceito, consoante os diferentes domínios avaliados. Finalmente, parecem existir diferenças no autoconceito relacionadas com o sexo das crianças, favorecendo os rapazes. Os nossos resultados contribuem para uma melhor compreensão do processo de desenvolvimento do autoconceito.

  4. Imunidade celular em caninos neonatos - do nascimento ao 45° dia de idade

    Directory of Open Access Journals (Sweden)

    R.P. Klein

    2014-06-01

    Full Text Available O objetivo do presente trabalho foi acompanhar o desenvolvimento imunológico dos neonatos caninos, a fim de avaliar a imunidade celular pela análise dos leucócitos e linfócitos totais e das subpopulações de linfócitos T (CD4+ e CD8+ pela técnica de citometria de fluxo. Foram utilizados 30 cães neonatos de ambos os sexos, sem raça definida, aos três, 10, 17, 24, 31, 38 e 45 dias de idade. A contagem de leucócitos totais aos 45 dias (11.639±3.574 foi significativamente maior que no terceiro dia de idade (8.740±1.812 (P<0,05; não houve diferença entre a contagem total de linfócitos aos 45 dias em relação ao terceiro dia de idade. Quanto às subpopulações de LT CD4+ e LT CD8+, os percentuais de LT CD4+, aos três dias de idade (24,9±16,8%, foram inferiores quando comparados à média entre o 10°, o 24° e o 31°dia (35,5%, e os de CD8+, ao terceiro dia, menores em relação às médias do 10° e do 31° dia de idade. Pode-se concluir que as subpopulações de LT CD4+ e CD8+ sofrem oscilações durante o desenvolvimento pós-natal, sendo estas crescentes em relação aos níveis obtidos aos três dias de idade. A relação CD4+:CD8+ mostrou superioridade para o primeiro tipo celular, sendo que a maior relação entre CD4+ e CD8+ ocorreu no terceiro dia de idade. Com base nos resultados obtidos neste estudo, notaram-se as diferenças semanais nas populações linfocitárias, o que demonstra a dinâmica dessas células durante o período neonatal.

  5. A hard X-ray scanning microprobe for fluorescence imaging and microdiffraction at the Advanced Photon Source

    International Nuclear Information System (INIS)

    Cai, L.; Lai, B.; Yun, W.; Ilinski, P.; Legnini, D.; Maser, J.; Rodrigues, W.

    1999-01-01

    A hard x-ray scanning microprobe based on zone plate optics and undulator radiation, in the energy region from 6 to 20 keV, has reached a focal spot size (FWHM) of 0.15 microm (v) x 0.6 microm (h), and a photon flux of 4 x 10 9 photons/sec/0.01%BW. Using a slit 44 meters upstream to create a virtual source, a circular beam spot of 0.15 microm in diameter can be obtained with a photon flux of one order of magnitude less. During fluorescence mapping of trace elements in a single human ovarian cell, the microprobe exhibited an imaging sensitivity for Pt (L a line) of 80 attograms/microm 2 for a count rate of 10 counts per second. The x-ray microprobe has been used to map crystallographic strain and multiquantum well thickness in micro-optoelectronic devices produced with the selective area growth technique

  6. In situ titanium dioxide nanoparticles quantitative microscopy in cells and in C. elegans using nuclear microprobe analysis

    Energy Technology Data Exchange (ETDEWEB)

    Le Trequesser, Quentin [Université de Bordeaux, CENBG, Chemin du solarium, 33175 Gradignan (France); CNRS, UMR 5797, CENBG, Chemin du solarium, 33175 Gradignan (France); CNRS, Université de Bordeaux, ICMCB, 87 avenue du Dr. A. Schweitzer, Pessac F-33608 (France); Saez, Gladys; Devès, Guillaume; Michelet, Claire; Barberet, Philippe [Université de Bordeaux, CENBG, Chemin du solarium, 33175 Gradignan (France); CNRS, UMR 5797, CENBG, Chemin du solarium, 33175 Gradignan (France); Delville, Marie-Hélène [CNRS, Université de Bordeaux, ICMCB, 87 avenue du Dr. A. Schweitzer, Pessac F-33608 (France); Seznec, Hervé, E-mail: herve.seznec@cenbg.in2p3.fr [Université de Bordeaux, CENBG, Chemin du solarium, 33175 Gradignan (France); CNRS, UMR 5797, CENBG, Chemin du solarium, 33175 Gradignan (France)

    2014-12-15

    Detecting and tracking nanomaterials in biological systems is challenging and essential to understand the possible interactions with the living. In this context, in situ analyses were conducted on human skin cells and a multicellular organism (Caenorhabditiselegans) exposed to titanium dioxide nanoparticles (TiO{sub 2} NPs) using nuclear microprobe. Coupled to conventional methods, nuclear microprobe was found to be suitable for accurate description of chemical structure of biological systems and also for detection of native TiO{sub 2} NPs. The method presented herein opens the field to NPs exposure effects analyses and more generally to toxicological analyses assisted by nuclear microprobe. This method will show applications in key research areas where in situ imaging of chemical elements is essential.

  7. Fast probing of glucose and fructose in plant tissues via plasmonic affinity sandwich assay with molecularly-imprinted extraction microprobes.

    Science.gov (United States)

    Muhammad, Pir; Liu, Jia; Xing, Rongrong; Wen, Yanrong; Wang, Yijia; Liu, Zhen

    2017-12-01

    Determination of specific target compounds in agriculture food and natural plant products is essential for many purposes; however, it is often challenging due to the complexity of the sample matrices. Herein we present a new approach called plasmonic affinity sandwich assay for the facile and rapid probing of glucose and fructose in plant tissues. The approach mainly relies on molecularly imprinted plasmonic extraction microprobes, which were prepared on gold-coated acupuncture needles via boronate affinity controllable oriented surface imprinting with the target monosaccharide as the template molecules. An extraction microprobe was inserted into plant tissues under investigation, which allowed for the specific extraction of glucose or fructose from the tissues. The glucose or fructose molecules extracted on the microprobe were labeled with boronic acid-functionalized Raman-active silver nanoparticles, and thus affinity sandwich complexes were formed on the microprobes. After excess Raman nanotags were washed away, the microprobe was subjected to Raman detection. Upon being irradiated with a laser beam, surface plasmon on the gold-coated microprobes was generated, which further produced plasmon-enhanced Raman scattering of the silver-based nanotags and thereby provided sensitive detection. Apple fruits, which contain abundant glucose and fructose, were used as a model of plant tissues. The approach exhibited high specificity, good sensitivity (limit of detection, 1 μg mL -1 ), and fast speed (the whole procedure required only 20 min). The spatial distribution profiles of glucose and fructose within an apple were investigated by the developed approach. Copyright © 2017 Elsevier B.V. All rights reserved.

  8. Data smoothing techniques applied to proton microprobe scans of teleost hard parts

    International Nuclear Information System (INIS)

    West, I.F.; Gauldie, R.W.; Coote, G.E.

    1992-01-01

    We use a proton microprobe to examine the distribution of elements in otoliths and scales of teleost (bony) fish. The elements of principal interest are calcium and strontium in otoliths and calcium and fluorine in scales. Changes in the distribution of these elements across hard structures may allow inferences about the life histories of fish. Otoliths and scales of interest are up to a centimeter in linear dimension and to reveal the structures of interest up to 200 sampling points are required in each dimension. The time needed to accumulate high X-ray counts at each sampling point can be large, particularly for strontium. To reduce microprobe usage we use data smoothing techniques to reveal changing patterns with modest X-ray count accumulations at individual data points. In this paper we review performance for revealing pattern at modest levels of X-ray count accumulations of a selection of digital filters (moving average smoothers), running median filters, robust locally weighted regression filters and adaptive spline filters. (author)

  9. Millimeter length micromachining using a heavy ion nuclear microprobe with standard magnetic scanning

    International Nuclear Information System (INIS)

    Nesprías, F.; Debray, M.E.; Davidson, J.; Kreiner, A.J.

    2013-01-01

    In order to increase the scanning length of our microprobe, we have developed an irradiation procedure suitable for use in any nuclear microprobe, extending at least up to 400% the length of our heavy ion direct writing facility using standard magnetic exploration. Although this method is limited to patterns of a few millimeters in only one direction, it is useful for the manufacture of curved waveguides, optical devices such Mach–Zehnder modulators, directional couplers as well as channels for micro-fluidic applications. As an example, this technique was applied to the fabrication of 3 mm 3D-Mach–Zehnder modulators in lithium niobate with short Y input/output branches and long shaped parallel-capacitor control electrodes. To extend and improve the quality of the machined structures we developed new scanning control software in LabView™ platform. The new code supports an external dose normalization, electrostatic beam blanking and is capable of scanning figures at 16 bit resolution using a National Instruments™ PCI-6731 High-Speed I/O card. A deep and vertical micromachining process using swift 35 Cl ions 70 MeV bombarding energy and direct write patterning was performed on LiNbO 3 , a material which exhibits a strong natural anisotropy to conventional etching. The micromachined structures show the feasibility of this method for manufacturing micro-fluidic channels as well

  10. Millimeter length micromachining using a heavy ion nuclear microprobe with standard magnetic scanning

    Energy Technology Data Exchange (ETDEWEB)

    Nesprías, F. [Gerencia de Investigación y Aplicaciones, Comisión Nacional de Energía Atómica, Av. Gral Paz 1499 (1650), San Martín, Buenos Aires (Argentina); Debray, M.E., E-mail: debray@tandar.cnea.gov.ar [Gerencia de Investigación y Aplicaciones, Comisión Nacional de Energía Atómica, Av. Gral Paz 1499 (1650), San Martín, Buenos Aires (Argentina); Escuela de Ciencia y Tecnología. Universidad Nacional de Gral. San Martín, M. De Irigoyen 3100 (1650), San Martín, Buenos Aires (Argentina); Davidson, J. [Gerencia de Investigación y Aplicaciones, Comisión Nacional de Energía Atómica, Av. Gral Paz 1499 (1650), San Martín, Buenos Aires (Argentina); CONICET, Avda. Rivadavia 1917 (C1033AAJ), Ciudad Autónoma de Buenos Aires (Argentina); Kreiner, A.J. [Gerencia de Investigación y Aplicaciones, Comisión Nacional de Energía Atómica, Av. Gral Paz 1499 (1650), San Martín, Buenos Aires (Argentina); Escuela de Ciencia y Tecnología. Universidad Nacional de Gral. San Martín, M. De Irigoyen 3100 (1650), San Martín, Buenos Aires (Argentina); CONICET, Avda. Rivadavia 1917 (C1033AAJ), Ciudad Autónoma de Buenos Aires (Argentina); and others

    2013-04-01

    In order to increase the scanning length of our microprobe, we have developed an irradiation procedure suitable for use in any nuclear microprobe, extending at least up to 400% the length of our heavy ion direct writing facility using standard magnetic exploration. Although this method is limited to patterns of a few millimeters in only one direction, it is useful for the manufacture of curved waveguides, optical devices such Mach–Zehnder modulators, directional couplers as well as channels for micro-fluidic applications. As an example, this technique was applied to the fabrication of 3 mm 3D-Mach–Zehnder modulators in lithium niobate with short Y input/output branches and long shaped parallel-capacitor control electrodes. To extend and improve the quality of the machined structures we developed new scanning control software in LabView™ platform. The new code supports an external dose normalization, electrostatic beam blanking and is capable of scanning figures at 16 bit resolution using a National Instruments™ PCI-6731 High-Speed I/O card. A deep and vertical micromachining process using swift {sup 35}Cl ions 70 MeV bombarding energy and direct write patterning was performed on LiNbO{sub 3}, a material which exhibits a strong natural anisotropy to conventional etching. The micromachined structures show the feasibility of this method for manufacturing micro-fluidic channels as well.

  11. Ion microprobe mass analysis of plagioclase from 'non-mare' lunar samples

    Science.gov (United States)

    Meyer, C., Jr.; Anderson, D. H.; Bradley, J. G.

    1974-01-01

    The ion microprobe was used to measure the composition and distribution of trace elements in lunar plagioclase, and these analyses are used as criteria in determining the possible origins of some nonmare lunar samples. The Apollo 16 samples with metaclastic texture and high-bulk trace-element contents contain plagioclase clasts with extremely low trace-element contents. These plagioclase inclusions represent unequilibrated relicts of anorthositic, noritic, or troctolitic rocks that have been intermixed as a rock flour into the KREEP-rich matrix of these samples. All of the plagioclase-rich inclusions which were analyzed in the KREEP-rich Apollo 14 breccias were found to be rich in trace elements. This does not seem to be consistent with the interpretation that the Apollo 14 samples represent a pre-Imbrium regolith, because such an ancient regolith should have contained many plagioclase clasts with low trace-element contents more typical of plagioclase from the pre-Imbrium crust. Ion-microprobe analyses for Ba and Sr in large plagioclase phenocrysts in 14310 and 68415 are consistent with the bulk compositions of these rocks and with the known distribution coefficients for these elements. The distribution coefficient for Li (basaltic liquid/plagioclase) was measured to be about 2.

  12. Nuclear microprobe studies of elemental distribution in the seagrass Thalassodendron ciliatum

    Energy Technology Data Exchange (ETDEWEB)

    Barnabas, A.D. E-mail: alban@pixie.udw.ac.za; Przybylowicz, W.J.; Mesjasz-Przybylowicz, J.; Pineda, C.A

    1999-09-02

    Elemental levels and distributions in various organs (leaves, upright stems, rhizomes and roots) of the seagrass Thalassodendron ciliatum were determined using the NAC nuclear microprobe. Elemental distributions were obtained using the true elemental imaging system Dynamic Analysis (DA). Cl was the most abundant element present in the organs, occurring in all tissues, but present in relatively low concentrations in epidermal cells of leaves and roots. Na, K, S and Mg were also abundant and occurred in all organ tissues. Ca concentration was highest in the leaves, especially in the epidermis. Low concentrations of P were found and its tissue distribution was limited. Although Fe, Cu, Zn, Mn, Br, Ti and Si were present in relatively small amounts, enrichment of the epidermis with Fe, Ti and Si in all organs, was observed. Fe concentration was the highest in rhizomes while Si concentration was highest in upright stems. The significance of these elemental distribution patterns and the value of the nuclear microprobe in elemental analysis of seagrasses are discussed.

  13. An extended magnetic quadrupole lens for a high-resolution nuclear microprobe

    Energy Technology Data Exchange (ETDEWEB)

    Breese, M.B.H. E-mail: m.breese@surrey.ac.uk; Grime, G.W.; Linford, W.; Harold, M

    1999-09-02

    This paper describes the design requirements and initial performance of a new style of magnetic quadrupole lens for use in a high-resolution nuclear microprobe, which is presently being constructed in Oxford. Such a microprobe necessitates the use of a small image distance from the exit face of the final quadrupole lens to the image plane in order to produce a large demagnification. This means that the final lens should be as close to the sample chamber as possible. However, with conventional magnetic quadrupoles the current-carrying coils protrude by a typical distance of 10-20 mm beyond the pole face, thereby significantly limiting the minimum image distance. The approach taken here is to recess the coils into the body of the lens, so that they are almost flush with the pole pieces and lens yoke, enabling an image distance of 55 mm. Three-dimensional magnetic field calculations within this lens structure predict that the field in the extended pole piece 'nose' region is only slightly less than that in the main lens body. Experimental field profiles, measured using a Hall probe, are used to confirm these calculations.

  14. An extended magnetic quadrupole lens for a high-resolution nuclear microprobe

    International Nuclear Information System (INIS)

    Breese, M.B.H.; Grime, G.W.; Linford, W.; Harold, M.

    1999-01-01

    This paper describes the design requirements and initial performance of a new style of magnetic quadrupole lens for use in a high-resolution nuclear microprobe, which is presently being constructed in Oxford. Such a microprobe necessitates the use of a small image distance from the exit face of the final quadrupole lens to the image plane in order to produce a large demagnification. This means that the final lens should be as close to the sample chamber as possible. However, with conventional magnetic quadrupoles the current-carrying coils protrude by a typical distance of 10-20 mm beyond the pole face, thereby significantly limiting the minimum image distance. The approach taken here is to recess the coils into the body of the lens, so that they are almost flush with the pole pieces and lens yoke, enabling an image distance of 55 mm. Three-dimensional magnetic field calculations within this lens structure predict that the field in the extended pole piece 'nose' region is only slightly less than that in the main lens body. Experimental field profiles, measured using a Hall probe, are used to confirm these calculations

  15. Development of a scanning proton microprobe - computer-control, elemental mapping and applications

    International Nuclear Information System (INIS)

    Loevestam, Goeran.

    1989-08-01

    A scanning proton microprobe set-up has been developed at the Pelletron accelerator in Lund. A magnetic beam scanning system and a computer-control system for beam scanning and data aquisition is described. The computer system consists of a VMEbus front-end computer and a μVax-II host-computer, interfaced by means of a high-speed data link. The VMEbus computer controls data acquisition, beam charge monitoring and beam scanning while the more sophisticated work of elemental mapping and spectrum evaluations is left to the μVax-II. The calibration of the set-up is described as well as several applications. Elemental micro patterns in tree rings and bark has been investigated by means of elemental mapping and quantitative analysis. Large variations of elemental concentrations have been found for several elements within a single tree ring. An external beam set-up has been developed in addition to the proton microprobe set-up. The external beam has been used for the analysis of antique papyrus documents. Using a scanning sample procedure and particle induced X-ray emission (PIXE) analysis, damaged and missing characters of the text could be made visible by means of multivariate statistical data evaluation and elemental mapping. Also aspects of elemental mapping by means of scanning μPIXE analysis are discussed. Spectrum background, target thickness variations and pile-up are shown to influence the structure of elemental maps considerably. In addition, a semi-quantification procedure has been developed. (author)

  16. Study of the toughening mechanisms in bone and biomimetic hydroxyapatite materials using Raman microprobe spectroscopy.

    Science.gov (United States)

    Pezzotti, Giuseppe; Sakakura, Seiji

    2003-05-01

    A Raman microprobe spectroscopy characterization of microscopic fracture mechanisms is presented for a natural hydroxyapatite material (cortical bovine femur) and two synthetic hydroxyapatite-based materials with biomimetic structures-a hydroxyapatite skeleton interpenetrated with a metallic (silver) or a polymeric (nylon-6) phase. In both the natural and synthetic materials, a conspicuous amount of toughening arose from a microscopic crack-bridging mechanism operated by elasto-plastic stretching of unbroken second-phase ligaments along the crack wake. This mechanism led to a rising R-curve behavior. An additional micromechanism, responsible for stress relaxation at the crack tip, was recognized in the natural bone material and was partly mimicked in the hydroxyapatite/silver composite. This crack-tip mechanism conspicuously enhanced the cortical bone material resistance to fracture initiation. A piezo-spectroscopic technique, based on a microprobe measurement of 980 cm(-1) Raman line of hydroxyapatite, enabled us to quantitatively assess in situ the microscopic stress fields developed during fracture both at the crack tip and along the crack wake. Using the Raman piezo-spectroscopy technique, toughening mechanisms were assessed quantitatively and rationally related to the macroscopic fracture characteristics of hydroxyapatite-based materials. Copyright 2003 Wiley Periodicals, Inc.

  17. Trace element analysis in geochemistry using a nuclear microprobe. Ionoluminescence and particle induced X-ray emission

    International Nuclear Information System (INIS)

    Homman, P.

    1994-01-01

    In PIXE analysis of geological specimens based on X-ray detection with Si(Li) detectors, effects of detector tailing, pulse pileup, and gamma-ray production are pronounced. In this work the tailing effect has been addressed through characterization of the response function of a Si(Li) detector using an absorber technique. The pileup interval, in the pulse forming electronics of a PIXE detection system, has been improved to 100 ns X-ray energies above 8 keV by means of pulse shape analysis. Pulses due to tailing effects were also isolated but no major improvement was obtained. A means of reducing the increased background in the PIXE spectrum due to Compton scattering of high energetic gamma-rays in the Si(Li) crystal has been investigated by installation of an anti-Compton shield consisting of an organic scintillator mounted inside the detector cryostat and read out by a photomultiplier. Ionoluminescence, a new analytical technique for the nuclear microprobe, has shown to be a technique that can be employed as a fast diagnostic tool in imaging applications. The technique is based on analysis of the light that often can be observed when an ion beam impinges on a geological specimen. This light, luminescence, can often be associated with impurities in the crystal lattice or other structural defects. It can therefore be employed for revealing some chemical information about the specimens in contradiction to PIXE which is rather insensitive to chemical variations. The potential of the method is demonstrated and discussed both as an imaging tool and for spectroscopic studies. 19 refs, 10 figs

  18. Microprobe analyses of uranium and thorium in uraninite from the Witwatersrand, South Africa, and Blind River, Ontario, Canada

    International Nuclear Information System (INIS)

    Grandstaff, D.E.

    1981-01-01

    Microprobe analyses of uranium and thorium in uraninite grains from the Witwatersrand, South Africa, and Blind River, Ontario, reveal that although individual grains are fairly homogeneous, the assemblage of grains is quite heterogeneous. This heterogeneity appears to favor genetic concepts advocating a detrital, placer origin for the uraninite

  19. U/Th dating by SHRIMP RG ion-microprobe mass spectrometry using single ion-exchange beads

    Science.gov (United States)

    Bischoff, J.L.; Wooden, J.; Murphy, F.; Williams, Ross W.

    2005-01-01

    We present a new analytical method for U-series isotopes using the SHRIMP RG (Sensitive High mass Resolution Ion MicroProbe) mass spectrometer that utilizes the preconcentration of the U-series isotopes from a sample onto a single ion-exchange bead. Ion-microprobe mass spectrometry is capable of producing Th ionization efficiencies in excess of 2%. Analytical precision is typically better than alpha spectroscopy, but not as good as thermal ionization mass spectroscopy (TIMS) and inductively coupled plasma multicollector mass spectrometry (ICP-MS). Like TIMS and ICP-MS the method allows analysis of small samples sizes, but also adds the advantage of rapidity of analysis. A major advantage of ion-microprobe analysis is that U and Th isotopes are analyzed in the same bead, simplifying the process of chemical separation. Analytical time on the instrument is ???60 min per sample, and a single instrument-loading can accommodate 15-20 samples to be analyzed in a 24-h day. An additional advantage is that the method allows multiple reanalyses of the same bead and that samples can be archived for reanalysis at a later time. Because the ion beam excavates a pit only a few ??m deep, the mount can later be repolished and reanalyzed numerous times. The method described of preconcentrating a low concentration sample onto a small conductive substrate to allow ion-microprobe mass spectrometry is potentially applicable to many other systems. Copyright ?? 2005 Elsevier Ltd.

  20. DESENVOLVIMENTO PSICOMOTOR DE CRIANÇAS PRÉ- TERMO EM IDADE PRÉ-ESCOLAR

    Directory of Open Access Journals (Sweden)

    Ana Rita Bodas

    2016-07-01

    Conclusões: O impacto negativo da prematuridade no DPM de crianças em idade pré-escolar é significativo e com frequência pouco perceptível para os pais. Favorece-se a implementação de estratégias de vigilância e identificação precoce nestas crianças, mesmo na ausência de outros indicadores ou factores de risco de atraso do DPM.

  1. Efeitos da perda auditiva, escolaridade e idade no processamento temporal de idosos

    Directory of Open Access Journals (Sweden)

    Isabela Mizani da Silva Lima

    2016-02-01

    Full Text Available RESUMO Objetivo: avaliar o efeito da perda auditiva, escolaridade e idade no processamento temporal de idosos. Métodos: foram avaliados 30 idosos, 15 com perda auditiva e baixa escolaridade e (Grupo 1 e 15 com audição normal e maior escolaridade (Grupo 2. Os participantes foram submetidos a avaliação audiológica, triagem cognitiva e avaliação do processamento temporal (resolução e ordenação temporal. Resultados: nota-se que os além da escolaridade os grupos se diferem em relação a idade, os idosos do Grupo 1 são mais velhos (p=0,024 e menos escolarizados (p=0.002. Os idosos do Grupo 1 apresentaram maior limiar e menor porcentagem de reconhecimento de gaps no ruido quando comparados ao desempenho dos idosos do Grupo 2 (GIN Limiar p=0,002; GIN % p=0,005. Os participantes de ambos os grupos apresentaram desempenhos similares na habilidade de ordenação temporal (p=0,691. Nesta amostra houve correlação negativa entre escolaridade e limiar de acuidade temporal (p=0,045, ou seja, quanto maior a escolaridade (em anos menor o limiar de reconhecimento de gaps. Apesar dos grupos serem distintos em relação a faixa etaria, a idade dos idosos não afetou o desempenho para os testes comportamentais do processamento temporal. Conclusão: Idosos com perda de audição e menor escolaridade apresentam maior prejuizo na habilidade de resolução temporal. Não houve correlação da idade com desempenho nos testes temporais.

  2. Nível de atividade física, comorbidades e idade de pacientes hipertensos

    Directory of Open Access Journals (Sweden)

    Denise Rodrigues Bueno

    2013-09-01

    Full Text Available No envelhecimento, hábito inativo está associado a doenças crônicas. Existem diferentes domínios da atividade física, tais como: tempo livre e locomoção. O objetivo foi analisar associações entre diferentes domínios de atividade física, comorbidades e idade em hipertensos. Foram entrevistados 192 hipertensos. Classificados em menos ativos e mais ativos para atividades no lazer, locomoção, ocupação e total e estratificados em grupos etários. A circunferência de cintura foi avaliada e comorbidades auto referidas. O teste Qui-quadrado analisou as associações e o teste ANOVA one way comparou os grupos etários, adotando significância estatística quando p<0,05. As médias de atividade física ocupacional e total foram menores para idade igual ou acima dos 60 e 70 anos, respectivamente. A atividade ocupacional esteve associada à idade em mulheres e, ao colesterol e diabetes em homens, que também tiveram atividade física de locomoção associada à circunferência de cintura. Em síntese a atividade física de hipertensos associa-se a comorbidades para diferentes grupos etários e sexos.

  3. Microprobe monazite constraints for and early (ca. 790 Ma) Braziliano orogeny: The Embu Terrane, southeastern Brazil

    International Nuclear Information System (INIS)

    Vlach, Silvio R.F

    2001-01-01

    The evolution of the Mantiqueira Orogenetic System, Southeastern Brazil, comprises discrete episodes of tectonic collage and docking of remnants of Rodinia break-up in the borders of the Sao Francisco Craton. This system is related to the closure of the Adamastor ocean and assemblage of the western Gondwana super-continent during Neoproterozoic times (ca. 610-530 Ma, Brito Neves et al., 1999; Campos Neto, 2000). This report presents monazite microprobe dating results for metassediments from the Embu Complex, an important lithological unit from the Ribeira Belt, currently included in the Juiz de Fora terrane, a unit added to the Sao Francisco Craton at ca. 600-580 Ma. (Campos Neto, 2000). The age results unravel a main metamorphic episode and related orogeny at ca. 790 Ma and bring new insights concerning the agglutination of Gondwana in this region during the Neoproterozoic (au)

  4. The non-destructive analysis of fluid inclusions in minerals using the proton microprobe

    Energy Technology Data Exchange (ETDEWEB)

    Ryan, C.G.; Van Achterbergy, E. [Commonwealth Scientific and Industrial Research Organisation (CSIRO), North Ryde, NSW (Australia). Div. of Exploration Geoscience; Heinrich, C.A. [ETH Zentrum, Zurich, (Switzerland). Department Erdwissenschaften; Mernagh, T.P. [Max-Planck-Institut fuer Chemie (Otto-Hahn-Institut), Mainz (Germany); Zaw, K. [Tasmania Univ., Sandy Bay, TAS (Australia)

    1996-12-31

    The study of ore forming fluids trapped as fluid inclusions in minerals is the key to understanding fluid flow paths at the time of ore formation and to predicting the location of ore bodies within large-scale magmatic hydrothermal systems. The large penetration depths and the predictable nature of MeV proton trajectories and X-ray absorption enables reliable modelling of PIXE yields and the development of standardless quantitative analytical methods. This permits quantitative microanalysis of minerals at ppm levels, and more recently has enabled the development of methods for quantitative trace-element imaging and the quantitative, non-destructive analysis of individual fluid inclusions. This paper reports on recent developments in Proton Microprobe techniques with special emphasis on ore systems and fluid inclusion analysis. 6 refs., 2 figs.

  5. Trace element partitioning between aqueous fluids and silicate melts measured with a proton microprobe

    Energy Technology Data Exchange (ETDEWEB)

    Adam, J.; Green, T.H. [Macquarie Univ., North Ryde, NSW (Australia). School of Earth Sciences; Sie, S.H. [Commonwealth Scientific and Industrial Research Organisation (CSIRO), North Ryde, NSW (Australia). Div. of Exploration Geoscience

    1996-12-31

    A series of experiments were performed to examine the capacity of H{sub 2}O-fluids to concentrate and transport incompatible elements through peridotitic mantle and metamorphosed (eclogitic) ocean crust. Two naturally occurring rock compositions, trondhjemitic and basanitic, were used in experiments. The proton microprobe was used to determine the trace element concentrations in the solutes from H{sub 2}O-fluids equilibrated at 900-1100 degree C, 2.0 GPa with water saturated melts of trondhjemitic and basanitic compositions. Partitioning data for H{sub 2}O-fluids and silicate melts show that H{sub 2}O-fluids equilibrated with mantle peridotites will not be strongly enriched in trace elements relative to their wallrocks, and thus they melts do not strongly concentrate alkaline earths Th and U, relative to high-field strength elements. 3 refs., 1 tab., 2 figs.

  6. The non-destructive analysis of fluid inclusions in minerals using the proton microprobe

    Energy Technology Data Exchange (ETDEWEB)

    Ryan, C G; Van Achterbergy, E [Commonwealth Scientific and Industrial Research Organisation (CSIRO), North Ryde, NSW (Australia). Div. of Exploration Geoscience; Heinrich, C A [ETH Zentrum, Zurich, (Switzerland). Department Erdwissenschaften; Mernagh, T P [Max-Planck-Institut fuer Chemie (Otto-Hahn-Institut), Mainz (Germany); Zaw, K [Tasmania Univ., Sandy Bay, TAS (Australia)

    1997-12-31

    The study of ore forming fluids trapped as fluid inclusions in minerals is the key to understanding fluid flow paths at the time of ore formation and to predicting the location of ore bodies within large-scale magmatic hydrothermal systems. The large penetration depths and the predictable nature of MeV proton trajectories and X-ray absorption enables reliable modelling of PIXE yields and the development of standardless quantitative analytical methods. This permits quantitative microanalysis of minerals at ppm levels, and more recently has enabled the development of methods for quantitative trace-element imaging and the quantitative, non-destructive analysis of individual fluid inclusions. This paper reports on recent developments in Proton Microprobe techniques with special emphasis on ore systems and fluid inclusion analysis. 6 refs., 2 figs.

  7. Elemental analysis of single phytoplankton cells using the Lund nuclear microprobe

    International Nuclear Information System (INIS)

    Pallon, Jan; Elfman, Mikael; Kristiansson, Per; Malmqvist, Klas; Graneli, Edna; Sellborn, Anders; Karlsson, Chatarina

    1999-01-01

    The occurrence of annual marine phytoplankton blooms is becoming a global problem. In Europe, the NUTOX project supported by the EC investigates if unbalanced nutrient compositions in the water promote the dominance of harmful phytoplankton species. One of the tasks is the determination of the elemental composition of single phytoplankton cells. This is carried out using the Lund Nuclear Microprobe with a special focus on C, N, P and K. The overall aim is to understand the mechanism leading to toxin production, model it and eventually propose a counteracting method. The preparative method, used to isolate single living cells while reducing their salt environment, is an important part of the analytical procedure. A comparison of light element detection using backscattering from protons and nuclear reaction analysis using deuterons is made

  8. Laser microprobe mass spectrometry: Potential and limitations for inorganic and organic micro-analysis. Pt. 1

    International Nuclear Information System (INIS)

    Vaeck, I. van; Gijbels, R.

    1990-01-01

    Laser microprobe mass spectrometry (LMMS) employs a highly focused UV laser beam to ionise a microvolume in the order of 1 μm 3 . The ions produced are then mass-separated in a time-of-flight (TOF) or a Fourier Transform (FT) mass spectrometer. TOF LMMS allows element localisation, detailed speciation of inorganic substances and structural information of organic molecules. Quantitation is difficult. This paper focuses on instrumental aspects and inorganic analysis. Organic applications are treated in part II of this series. Selected examples illustrate that TOF LMMS is a valuable tool for the qualitative characterisation of micro-samples. Also, the applicability to the analysis with high spatial resolution is shown. The current technology and the prospects from the recent FTMS development are discussed. (orig.)

  9. Laser microprobe mass spectrometry: Potential and limitations for inorganic and organic micro-analysis. Pt. 2

    International Nuclear Information System (INIS)

    Vaeck, I. van; Gijbels, R.

    1990-01-01

    Laser microprobe mass spectrometry (LMMS) employs a highly focused UV laser beam to ionise a microvolume in the order of 1 μm 3 . The produced ions are then mass-separated in a time-of-flight (TOF) or a Fourier Transform (FT) mass spectrometer. The technique allows element localisation, detailed speciation of inorganic substances and structural information of organic molecules. Inorganic applications are treated in the preceding part. This paper will focus on the organic aspects. Selected examples illustrate that TOF LMMS can achieve structural characterisation of molecules, untractable by conventional mass spectrometric techniques. Applicability to the analysis with high spatial resolution is shown and the need for surface availability of organic target molecules is discussed. The recently developed FT LMMS may fulfil the need for better mass resolution. However, the comparability of FT LMMS results with TOF LMMS data is not yet obvious. (orig.)

  10. Elemental characterization of individual glia and glioma cells in the nuclear microprobe

    International Nuclear Information System (INIS)

    Lindh, U.

    1982-01-01

    To investigate whether variations in levels of microelements are reflected at the cellular level, a study of cultured cells was undertaken. For elemental characterization were chosen human glia and glioma cell lines. The cells were freeze-dried and about 1000 cells of each line were analyzed in the nuclear microprobe with a probe diameter of 10 μm. Scanning of the specimens under the beam made possible heat reduction and the X-ray spectrum induced was continuously recorded and subsequently processed in the computer. Elemental maps of the cells were then generated and the information from each member of the cell populations could be considered as well as the population statistics. Mass determination was accomplished by means of the bremsstrahlung continuum intensity. The main feature resulting from the characterization was that the glioma cells in average held appreciably higher contents of copper and zinc than did the glia cells. (orig.)

  11. A new method for true quantitative elemental imaging using PIXE and the proton microprobe

    Energy Technology Data Exchange (ETDEWEB)

    Ryan, C G [Commonwealth Scientific and Industrial Research Organisation (CSIRO), North Ryde, NSW (Australia). Div. of Exploration Geoscience; Jamieson, D N [Melbourne Univ., Parkville, VIC (Australia). School of Physics; Churms, C L; Pilcher, J V [National Accelerator Centre, Faure (South Africa)

    1994-12-31

    Traditional methods for X-ray imaging using PIXE and the Proton Microprobe have used a simple gate set on an X-ray peak in a spectrum from a Si(Li) detector to provide an image of the distribution of an element. This method can produce artefacts in images, due to overlapping X-ray lines from interfering elements, charge collection tails on peaks, background variation, Si escape peaks and pileup, all of which can render images misleading or qualitative at best. To address this problem, a matrix transform method has been developed at the CSIRO which not only eliminates most artefacts, but can be implemented on-line. The method has been applied to study trace gold distribution in a complex gold bearing ore from Fiji , and more recently has been installed for direct on-line elemental imaging at the NAC in South Africa. 4 refs., 2 figs.

  12. Laser ablation microprobe inductively coupled plasma mass spectrometry study on diffusion of uranium into cement materials

    International Nuclear Information System (INIS)

    Sugiyama, D.; Chida, T.; Cowper, M.

    2008-01-01

    The diffusion of uranium (U(VI)) in solid cement monoliths of ordinary portland cement (OPC) and low-heat portland cement containing 30 wt.% fly ash (FAC) was measured by an in-diffusion technique. Detailed sharp depth profiles of uranium in the solid cement matrices were successively and quantitatively measured using laser ablation microprobe inductively coupled plasma mass spectrometry (LAMP-ICP-MS), and the apparent (D a ) and effective (D e ) diffusion coefficient of uranium in cement matrix were calculated as: D a =∝ 4 x 10 -16 m 2 s -1 and D e =∝ 3 x 10 -11 m 2 s -1 for OPC, and D a =∝ 2 x 10 -17 m 2 s -1 and D e =∝ 6 x 10 -13 m 2 s -1 for FAC. (orig.)

  13. Progress of the new CSIRO-GEMOC nuclear microprobe: first results, performance and recent applications

    International Nuclear Information System (INIS)

    Ryan, C.G.; Cripps, G.; Sie, S.H.; Suter, G.F.; Jamieson, D.N.; Griffin, W.L.; Commonwealth Scientific and Industrial Research Organisation

    1999-01-01

    The new CSIRO-GEMOC Nuclear Microprobe (NMP) features a number of technical advances for high resolution, high sensitivity microanalysis. It was designed at the CSIRO and developed as collaboration between the CSlRO, the GEMOC key-centre at Macquarie University and the MARC group of the University of Melbourne. For imaging applications, it also features a software system using a powerful algorithm called Dynamic Analysis, developed at the CSIRO for unmixing elemental signatures in proton induced X-ray emission (PIXE) data, to provide a tool for rapid quantitative imaging of trace and major element spatial distribution in minerals. This paper reports on the performance of the NMP and examples of its application over the past 6 months since completion

  14. A new method for true quantitative elemental imaging using PIXE and the proton microprobe

    Energy Technology Data Exchange (ETDEWEB)

    Ryan, C.G. [Commonwealth Scientific and Industrial Research Organisation (CSIRO), North Ryde, NSW (Australia). Div. of Exploration Geoscience; Jamieson, D.N. [Melbourne Univ., Parkville, VIC (Australia). School of Physics; Churms, C.L.; Pilcher, J.V. [National Accelerator Centre, Faure (South Africa)

    1993-12-31

    Traditional methods for X-ray imaging using PIXE and the Proton Microprobe have used a simple gate set on an X-ray peak in a spectrum from a Si(Li) detector to provide an image of the distribution of an element. This method can produce artefacts in images, due to overlapping X-ray lines from interfering elements, charge collection tails on peaks, background variation, Si escape peaks and pileup, all of which can render images misleading or qualitative at best. To address this problem, a matrix transform method has been developed at the CSIRO which not only eliminates most artefacts, but can be implemented on-line. The method has been applied to study trace gold distribution in a complex gold bearing ore from Fiji , and more recently has been installed for direct on-line elemental imaging at the NAC in South Africa. 4 refs., 2 figs.

  15. Development of a shielded ion microprobe analyzer (SIMA) and its application to fast reactor fuel elements

    International Nuclear Information System (INIS)

    Yuji, E.; Junji, K.; Sadamu, Y.; Toshiyuki, I.

    1983-01-01

    A shielded ion microprobe analyzer for elemental and isotopic analyses of irradiated fast reactor fuel and fuel component has been developed and installed in an alpha-gamma hot cell. Radiation shielding of the equipment ensures the radiation dose of -7 C/kg) for 5 Ci (1.85 x 10 11 Bq) of a 60 Co source. Hot samples can be automatically transferred from the cell to the sample chamber of the analyzer. Contamination inside the equipment through sputtering of the radioactive materials can be reduced with a special device. Distribution and migration of fission products, such as 137 Cs, 138 Ba, and 90 Sr, and of fissile materials, such as 235 U and 239 Pu in irradiated mixed-oxide fuel, and isotopic ratios of the elements can be obtained very precisely and quickly

  16. Development of a shielded ion microprobe analyzer (SIMA) and its application to fast reactor fuel elements

    International Nuclear Information System (INIS)

    Enokido, Y.; Itaki, T.; Komatsu, J.; Yamanouchi, S.

    1983-01-01

    A shielded ion microprobe analyzer for elemental and isotopic analyses of irradiated fast reactor fuel and fuel component has been developed and installed in an alpha-gamma hot cell. Radiation shielding of the equipment ensures the radiation dose of -7 C/kg) for 5 Ci (1.85 X 10 11 Bq) of a 60 Co source. Hot samples can be automatically transferred from the cell to the sample chamber of the analyzer. Contamination inside the equipment through sputtering of the radioactive materials can be reduced with a special device. Distribution and migration of fission products, such as 137 Cs, 138 Ba, and 90 Sr, and of fissile materials, such as 235 U and 239 Pu in irradiated mixed-oxide fuel, and isotopic ratios of the elements can be obtained very precisely and quickly

  17. Experimental investigations into sample preparation of Alzheimer tissue specimens for nuclear microprobe analysis

    Energy Technology Data Exchange (ETDEWEB)

    Pinheiro, T [CEC-JRC, Central Bureau for Nuclear Measurements, Geel (Belgium); Tapper, U A.S. [Dept. of Nuclear Physics, Lund Inst. of Science and Tech. (Sweden); Sturesson, K; Brun, A [Div. of Neuropathology, Dept. of Pathology, Lund University Hospital (Sweden)

    1991-03-01

    Nuclear microprobe analysis was applied to the study of elemental distribution in brains sections of patients with a diagnosis of Alzheimer's disease. Stained and nonstained cryosections were studied. The work carried out shows that serious elemental losses follow the sample staining procedure. Major losses occurred in a simple rinse of the tissue section, probably reducing most of the in-vivo gradients, which show that generally very little information can be gained from stained sections. However, in many cases stained sections are compulsory because of the requirement to recognize the area which is to be studied. All the elemental maps obtained for the neurofibrillary deposits indicate a localized concentration for Si and probably also Al, associated with the senile plaque core. Neither of these elements were found in the staining solutions used. The validity of the results is discussed as well as the possible link of Al and/or Si in the development of Alzheimer's desease. (orig.).

  18. Trace element partitioning between aqueous fluids and silicate melts measured with a proton microprobe

    Energy Technology Data Exchange (ETDEWEB)

    Adam, J; Green, T H [Macquarie Univ., North Ryde, NSW (Australia). School of Earth Sciences; Sie, S H [Commonwealth Scientific and Industrial Research Organisation (CSIRO), North Ryde, NSW (Australia). Div. of Exploration Geoscience

    1997-12-31

    A series of experiments were performed to examine the capacity of H{sub 2}O-fluids to concentrate and transport incompatible elements through peridotitic mantle and metamorphosed (eclogitic) ocean crust. Two naturally occurring rock compositions, trondhjemitic and basanitic, were used in experiments. The proton microprobe was used to determine the trace element concentrations in the solutes from H{sub 2}O-fluids equilibrated at 900-1100 degree C, 2.0 GPa with water saturated melts of trondhjemitic and basanitic compositions. Partitioning data for H{sub 2}O-fluids and silicate melts show that H{sub 2}O-fluids equilibrated with mantle peridotites will not be strongly enriched in trace elements relative to their wallrocks, and thus they melts do not strongly concentrate alkaline earths Th and U, relative to high-field strength elements. 3 refs., 1 tab., 2 figs.

  19. Hg diffusion in books of XVIII and XIX centuries by synchrotron microprobe

    International Nuclear Information System (INIS)

    Pessanha, S.; Carvalho, M.L.; Manso, M.; Guilherme, A.; Marques, A.F.; Perez, C.A.

    2009-01-01

    The pigment vermilion (HgS) was used to color the fore edge, tail and head of books. Dissemination and quantification of Hg present in the ink used to color books from XVIII and XIX centuries are reported. Mercury is a very toxic element for the human body, therefore it is extremely important to know whether Hg tends to disseminate throughout the paper or stays confined to the borders of the books with less danger for readers. Synchrotron X-ray microprobe was used to evaluate Hg dissemination from the border to the centre of the paper sheet. The diffusion pattern of Hg was compared with the results obtained by a portable X-ray fluorescence spectrometer and mean quantitative calculations were obtained by a stationary X-ray fluorescence system with triaxial geometry. The results showed high concentrations of Hg in the external regions, but no diffusion was observed for the inner parts of the paper.

  20. Trace element composition and distribution in micron area of dinosaur eggshell fossils determined by proton microprobe

    International Nuclear Information System (INIS)

    Chen Youhong; Zhu Jieqing; Wang Xiaohong; Wang Yimin

    1997-01-01

    The scanning proton microprobe and micro-PIXE quantitative analysis technique have been used to determine composition and distribution of the trace elements in micron areas of dinosaur eggshell fossils from the stratum of Upper Cretaceous system at Nanxiong Basin in Guangdong Province, China. The study shows that the trace elements mainly include Ti, V, Cr, Mn, Co, Ni, Cu, Zn, As, Rb, Sr, Y, Zr, Sb, Ba and Pb in the micron area, but they present different distributions. While the element Sr is mainly enriched in the near surface layer, others mainly reside in the near inner layer. A preliminary discussion on the reason of the dinosaur extinction is given based on the above study

  1. Trace element composition and distribution in micron area of dinosaur eggshell fossils determined by proton microprobe

    International Nuclear Information System (INIS)

    Chen Youhong; Zhu Jieqing; Wang Xiaohong; Wang Yimin

    1997-01-01

    The scanning proton microprobe and micro-PIXE quantitative analysis technique have been used to determine composition and distribution of the trace elements in micron areas of dinosaur eggshell fossils from the stratum of Upper Cretaceous system at Nanxiong Basin in Guangdong Province, China. The study shows that the trace elements mainly include Ti, V, Cr, Mn, Co, Ni, Cu, Zn, As, Rb, Sr, Y, Zr, Sb, Ba and Pb in the micron area, but they present different distributions. While the elements Sr is mainly enriched in the near surface layer, others mainly reside in the near inner layer. A preliminary discussion on the reason of the dinosaur extinction is given based on the above study

  2. Measurements of impurity migration in graphite at high temperatures using a proton microprobe

    International Nuclear Information System (INIS)

    Shroy, R.E.; Soo, P.; Sastre, C.A.; Schweiter, D.G.; Kraner, H.W.; Jones, K.W.

    1978-01-01

    The migration of fission products and other impurities through the graphite core of a High Temperature Gas Cooled Reactor is of prime importance in studies of reactor safety. Work in this area is being carried out in which graphite specimens are heated to temperatures up to 3800 0 C to induce migration of trace elements whose local concentrations are then measured with a proton microprobe. This instrument is a powerful device for such work because of its ability to determine concentrations at a part per million (ppm) level in a circular area as small as 10 μm while operating in an air environment. Studies show that Si, Ca, Cl, and Fe impurities in graphite migrate from hotter to cooler regions. Also Si, S, Cl, Ca, Fe, Mn, and Cr are observed to escape from the graphite and be deposited on cooler surfaces

  3. Nuclear microprobe analysis of muscle biopsies: Applications in pathology and clinic

    International Nuclear Information System (INIS)

    Moretto, Ph.; Coquet, M.; Gherardi, R.K.; Stoedzel, P.

    2000-01-01

    The nuclear microprobe analysis of muscle biopsy sections has been recently applied to investigate different muscle disorders. This technique, employed as a complementary examination in the frame of pathological studies, permitted to confirm the diagnosis for a first pathology and to elucidate the cause of a second. In skeletal muscles of a young patient suffering from a slow progressive myopathy, calcium accumulations have been demonstrated in histologically abnormal fibers. These findings have been compared to histopathological characteristics previously described. On the other hand, we have evaluated muscle sections from two patients who presented symptoms of an inflammatory myopathy, a rare pathology that recently emerged in France. The chemical analyses permitted us to highlight local aluminium infiltration in muscles. The hypothesis of an unusual reaction to intramuscular aluminium accumulation has been advanced. These studies demonstrate the capability for ion beam microanalytical techniques to address acute problems in pathology

  4. Present status of research and development on X-ray microprobe

    International Nuclear Information System (INIS)

    Koike, Masaki; Suzuki, I.H.

    1991-01-01

    X-ray beam micro-analysis has advanced rapidly in these years in conjunction with the development of powerful X-ray sources. Among a variety of methods being attempted, the method using a collimated narrow beam has been important because of high brightness, and of usability in both regions of soft and hard X-rays. In the soft X-ray region, the focused beam is formed by a fresnel zone plate or a Schwaltzschild mirror assembly, and can be used for scanning transmission microscope or scanning photoelectron microscope. In the hard X-ray region, the beam is formed by grazing incidence mirrors, and can be used for X-ray fluorescence micro-analysis for obtaining elemental mapping. In this report, the recent progress on the soft X-ray scanning microscopy and the X-ray microprobe has been surveyed, together with the improvement on the related optical elements. (author) 84 refs

  5. Characterization of PE-g-HEMA films prepared by gamma irradiation through nuclear microprobe techniques

    International Nuclear Information System (INIS)

    Ferreira, L.M.; Rodrigues, P.A.; Falcao, A.N.; Leal, J.P.

    2011-01-01

    Complete text of publication follows. The functional success of a copolymer as biomaterial depends fundamentally on their mechanical properties (stemming from the material matrix) and on the characteristics of its surface. For biomedical applications, among all the other important properties, the biocompatibility of the surface acquires extreme importance and can dictate its rejection. One of the issues regarding biocompatibility is cytotoxicity which strongly depends on the contamination level at surface. Ion beam analysis techniques associated to Nuclear Microprobe (PIXE, RBS and STIM) allows a rigorous and precise analysis of the concentration (ppm) and distribution of elements contamination, and may also provide information on its near-surface structure. In this work PE-g-HEMA films with different grafting yields were prepared by mutual gamma irradiation at a 60 Co source and were analyzed through nuclear microprobe. Data collected allowed the qualitative and quantitative evaluation of contaminants distribution observed in the different samples as well as the clarification of some processes occurred during the copolymerization reaction. Qualitative analysis showed a random and no homogeneous distribution of the contaminant elements, independent of the grafting degree, suggesting the existence of several sources of contamination at different stages of their preparation. Results also suggest that this 'phased' contamination occurs simultaneously with mechanisms of agglomeration/entrapment of impurities during the gamma induced copolymerization reaction. Moreover, quantitative data showed that all contaminants found in the copolymeric films are natural contaminants of their reagents of preparation, although at concentrations without toxicological hazard, which points to a low cytotoxic potential. The combined analysis of these data with data from SEM and AFM allowed a better understanding of the surface structure and other properties already observed in these

  6. Fabrication of wear-resistant silicon microprobe tips for high-speed surface roughness scanning devices

    Science.gov (United States)

    Wasisto, Hutomo Suryo; Yu, Feng; Doering, Lutz; Völlmeke, Stefan; Brand, Uwe; Bakin, Andrey; Waag, Andreas; Peiner, Erwin

    2015-05-01

    Silicon microprobe tips are fabricated and integrated with piezoresistive cantilever sensors for high-speed surface roughness scanning systems. The fabrication steps of the high-aspect-ratio silicon microprobe tips were started with photolithography and wet etching of potassium hydroxide (KOH) resulting in crystal-dependent micropyramids. Subsequently, thin conformal wear-resistant layer coating of aluminum oxide (Al2O3) was demonstrated on the backside of the piezoresistive cantilever free end using atomic layer deposition (ALD) method in a binary reaction sequence with a low thermal process and precursors of trimethyl aluminum and water. The deposited Al2O3 layer had a thickness of 14 nm. The captured atomic force microscopy (AFM) image exhibits a root mean square deviation of 0.65 nm confirming the deposited Al2O3 surface quality. Furthermore, vacuum-evaporated 30-nm/200-nm-thick Au/Cr layers were patterned by lift-off and served as an etch mask for Al2O3 wet etching and in ICP cryogenic dry etching. By using SF6/O2 plasma during inductively coupled plasma (ICP) cryogenic dry etching, micropillar tips were obtained. From the preliminary friction and wear data, the developed silicon cantilever sensor has been successfully used in 100 fast measurements of 5- mm-long standard artifact surface with a speed of 15 mm/s and forces of 60-100 μN. Moreover, the results yielded by the fabricated silicon cantilever sensor are in very good agreement with those of calibrated profilometer. These tactile sensors are targeted for use in high-aspect-ratio microform metrology.

  7. The mutual diffusion coefficient for (meth)acrylate monomers as determined with a nuclear microprobe

    International Nuclear Information System (INIS)

    Leewis, Christian M.; Mutsaers, Peter H.A.; Jong, Arthur M. de; Ijzendoorn, Leo J. van; Voigt, Martien J.A. de; Ren, Min Q.; Watt, Frank; Broer, Dirk J.

    2004-01-01

    The value of the mutual diffusion coefficient D V of two acrylic monomers is determined with nuclear microprobe measurements on a set of polymer films. These films have been prepared by allowing the monomers to diffuse into each other for a certain time and subsequently applying fast ultraviolet photo-polymerization, which freezes the concentration profile. The monomer diffusion profiles are studied with a scanning 2.1 MeV proton microprobe. Each monomer contains a marker element, e.g., Cl and Si, which are easily detected with proton induced x-ray emission. From the diffusion profiles, it is possible to determine the mutual diffusion coefficient. The mutual diffusion coefficient is dependent of concentration, which is concluded from the asymmetry in the Cl- and Si-profiles. A linear dependence of the mutual diffusion coefficient on the composition is used as a first order approximation. The best fits are obtained for a value of b=(0.38±0.15), which is the ratio of the diffusion coefficient of 1,3-bis(3-methacryloxypropyl)-1, 1,3,3-tetramethyldisiloxane in pure 2-chloroethyl acrylate and the diffusion coefficient of 2-chloroethyl acrylate in pure 1,3-bis(3-methacryloxypropyl)-1,1,3,3-tetramethyldisiloxane. Under the assumption of a linear dependence of the mutual diffusion coefficient D V on monomer composition, it follows that D V =(2.9±0.6)·10 -10 m 2 /s at a 1:1 monomer ratio. With Flory-Huggins expressions for the monomer chemical potentials, one can derive approximate values for the individual monomer diffusion coefficients

  8. Fabrication of an 8:1 ellipsoidal mirror for a synchrotron x-ray microprobe

    International Nuclear Information System (INIS)

    Jones, K.W.; Takacs, P.Z.; Hastings, J.B.; Casstevens, J.M.; Pionke, C.D.

    1987-01-01

    The fabrication of an 8:1 demagnifying ellipsoidal mirror to be used for an x-ray microprobe at the National Synchrotron Light Source X-26 beam port is described. The design aim was to produce a mirror that could be used over the photon energy range from about 3 to 17 keV. The 300-mm long mirror was required to operate at a grazing angle of 5 mr. The semimajor axis was 4500 mm and the semiminor axis 14.142 mm. Surface roughness of 1 nm or less and slope errors of 1 arc second parallel to the long axis and 200 arc seconds parallel to the short direction were specified. Production of the first electroless nickel-coated aluminum mirror using a diamond-turning technique has been completed. The mirror meets the 1 arc sec surface figure specification except for areas near the ends of the mirror. The reasons for these deviations arise from subtle details of the diamond-turning process which have not been fully incorporated in to the computer program that controls the diamond-turning machines. Further work in computer correction of repeatable errors of the diamond-turning machine can eliminate the waviness at the ends of the mirror. The diamond-turned mirror surface was not fully polished under this effort and therefore does not meet the roughness specification; however, surface smoothness of a fully polished cylindrical mirror manufactured using the same techniques does not meet the specification. It can be concluded that it is now technically feasible to meet the required specifications for the mirror and that the x-ray microprobe based on its use can be achieved

  9. Study of ocular aberrations with age Estudo das aberrações oculares e idade

    Directory of Open Access Journals (Sweden)

    Helaine Vinche Zampar Athaide

    2009-10-01

    Full Text Available INTRODUCTION: Aging has various effects on visual system. Vision deteriorate, contrast sensitivity decreases and ocular aberrations apparently make the optical quality worse across the years. PURPOSE: To prospective evaluate ocular aberrations along the ages. METHODS: Three hundred and fifteen patients were examined, 155 were male (39.36% and 160 were female (60.63%. Ages ranged from 5 to 64 year-old, the study was performed from February to November, 2004. Patients were divided into 4 age-groups according to IBGE (Instituto Brasileiro de Geografia e Estatística classification: 68 patients from 5 to 14 year-old, 55 patients from 15 to 24 year-old, 116 from 25 to 44 year-old and 76 from 45 to 67 year-old. All patients had the following characteristics: best corrected visual acuity > 20/25, emmetropia or spherical equivalent INTRODUÇÃO: A idade afeta o sistema visual. A qualidade da visão se deteriora progressivamente com a idade, a sensibilidade ao contraste diminui e as aberrações oculares aumentam contribuindo para a piora da qualidade visual. OBJETIVO: Estudar prospectivamente as aberrações oculares entre as idades de 5 a 64 anos. MÉTODOS: Foram examinados 315 pacientes, 155 homens (39,36% e 160 mulheres (60,63% com idades entre 5 a 64 anos. O estudo foi realizado entre fevereiro a novembro de 2004. Os pacientes foram divididos em quatro grupos etários de acordo com a classificação do IBGE (Instituto Brasileiro de Geografia e Estatística: 68 pacientes entre 5 a 14 anos, 55 pacientes entre 15 a 24 anos, 116 pacientes entre 25 a 44 anos e 76 pacientes entre 45 a 67 anos de idade. Todos apresentavam acuidade visual corrigida para longe >20/25, emetropia ou equivalente esférico <3,5 DE, astigmatismo <1,75 DC ao exame sob cicloplegia, exame oftalmológico normal e sem cirurgia oftalmológica prévia. O Comitê de Ética da Universidade Federal de São Paulo aprovou esse protocolo. As aberrações foram medidas usando o sensor H

  10. Artesanato na terceira idade: um estudo na cidade de Sinop no ano de 2011

    Directory of Open Access Journals (Sweden)

    Rosane Marlene Weber

    2015-04-01

    Full Text Available Essa pesquisa tem como objetivo mostrar a importância do artesanato na Terceira Idade como atividade educacional e de autonomia para os idosos. Por existir uma preocupação com a qualidade de vida da Terceira Idade e sua autonomia, nesta fase que muitos acabam ficando dependentes dos membros da família, espera-se encontrar através da arte uma motivação e uma forma de demonstrar a autoria por meio do fazer, criar e recriar com o artesanato. Aprender e ensinar são um processo contínuo na vida do ser humano, independente da idade, para Paulo Freire precisamos ter consciência de que somos inacabados, e sendo conscientes de nossa inconclusão, devemos viver num permanente movimento de busca. Essa é uma das causas pelas quais será pesquisada a prática formativa/educacional por meio do artesanato na Terceira Idade. Os motivos que levaram a escolha desta pesquisa com o artesanato na Terceira Idade é o fato de ter vivido uma experiência de trabalho na ala geriátrica de um hospital. Já o artesanato é a arte que fascina, e acreditamos que sempre há tempo para recomeçar, para descobrir algo que possa trazer qualidade para nossa vida. Devido ao crescimento cada vez maior da expectativa de vida em nosso país, cria-se uma preocupação com a qualidade de vida das pessoas da Terceira Idade. Em relação aos aspectos educacionais e culturais, esta pesquisa deseja compreender como o artesanato pode trazer motivação para as pessoas da Terceira Idade como forma de autoria e autonomia, nesta fase da vida, na cidade de Sinop, e quais os motivos que os levam a realizar esse tipo de atividade. Para investigação teórica desta pesquisa do Artesanato na Terceira Idade: um estudo na cidade de Sinop em 2011 usaremos bibliografia de vários autores, mas em especial os que dedicam seus estudos a esta faixa etária, como a coleção de Vivaidade, que tem como organizadora principal Anita Liberalesso Neri. Os autores desta coleção nos trazem a reflex

  11. Use of scanning electron microscopy and microanalysis to determine chloride content of concrete and raw materials.

    Science.gov (United States)

    2013-02-01

    Standard sample sets of cement and mortar formulations with known levels of Cl as well as concrete samples subject to Cl diffusion were all prepared for and analyzed with scanning electron microscopy (SEM) and electron microprobe (EPMA). Using x-ray ...

  12. NENIMF: Northeast National Ion Microprobe Facility - A Multi-User Facility for SIMS Microanalysis

    Science.gov (United States)

    Layne, G. D.; Shimizu, N.

    2002-12-01

    The MIT-Brown-Harvard Regional Ion Microprobe Facility was one of the earliest multi-user facilities enabled by Dan Weill's Instrumentation and Facilities Program - and began with the delivery of a Cameca IMS 3f ion microprobe to MIT in 1978. The Northeast National Ion Microprobe Facility (NENIMF) is the direct descendant of this original facility. Now housed at WHOI, the facility incorporates both the original IMS 3f, and a new generation, high transmission-high resolution instrument - the Cameca IMS 1270. Purchased with support from NSF, and from a consortium of academic institutions in the Northeast (The American Museum of Natural History, Brown University, The Lamont-Doherty Earth Observatory, MIT, Rensselaer Polytechnic Institute, WHOI) - this latest instrument was delivered and installed during 1996. NENIMF continues to be supported by NSF EAR I&F as a multi-user facility for geochemical research. Work at NENIMF has extended the original design strength of the IMS 1270 for microanalytical U-Pb zircon geochronology to a wide variety of novel and improved techniques for geochemical research. Isotope microanalysis for studies in volcanology and petrology is currently the largest single component of facility activity. This includes the direct measurement of Pb isotopes in melt inclusions, an application developed at NENIMF, which is making an increasingly significant contribution to our understanding of basalt petrogenesis. This same technique has also been extended to the determination of Pb isotopes in detrital feldspar grains, for the study of sedimentary provenance and tectonics of the Himalayas and other terrains. The determination of δ11B in volcanic melt inclusions has also proven to be a powerful tool in the modeling of subduction-related magmatism. The recent development of δ34S and δ37Cl determination in glasses is being applied to studies of the behavior of these volatile elements in both natural and experimental systems. Other recent undertakings

  13. Comportamento de lactentes nascidos a termo pequenos para a idade gestacional no primeiro trimestre da vida

    OpenAIRE

    Mello,Bernadete Balanin A.; Gonçalves,Vanda M. Gimenes; Souza,Elisabete Abib P.

    2004-01-01

    O objetivo foi comparar o comportamento de lactentes nascidos a termo com peso adequado (AIG) a lactantes pequenos para a idade gestacional (PIG), no primeiro trimestre de vida. A amostra foi de 20 lactentes, avaliados no 1º, 2º e 3º meses. Foram utilizadas as Escalas Bayley de Desenvolvimento Infantil - II, com ênfase na Escala de Classificação do Comportamento (ECC). Houve diferença significativa entre os grupos no 2º mês, com maior número de lactentes PIG classificados como alterados na EC...

  14. A cartography of childhood: a rereading exercise of A idade do serrote, by Murilo Mendes

    Directory of Open Access Journals (Sweden)

    Francisco Thiago Camêlo

    2016-12-01

    Full Text Available This paper challenges traditional readings of Murilo Mendes’ work A idade do serrote (1968, and investigates the power of a “language childhood” in connection with Mendes’ writing. For this exercise, some chapters of his memoirs are discussed in a dialogue with philosophical propositions expressed by Gilles Deleuze, Giorgio Agamben, Jean-François Lyotard, and Walter Benjamin. By promoting an encounter between artistic expression and philosophical thinking, this article aims at showing childhood power as a discursive operator.

  15. Valores Humanos e Bullying: Idade e Sexo Moderam essa Relação?

    OpenAIRE

    Monteiro, Renan Pereira; Medeiros, Emerson Diógenes de; Pimentel, Carlos Eduardo; Soares, Ana Karla Silva; Medeiros, Hermógenes Acácio de; Gouveia, Valdiney Veloso

    2017-01-01

    Resumo São perceptíveis as consequências graves que perpassam o bullying, sendo importante conhecer variáveis que possam predizer este padrão de comportamento entre escolares. O presente estudo objetivou conhecer em que medida os valores humanos predizem o bullying, testando o papel moderador das variáveis sexo e idade. Participaram 300 crianças (M = 11,07; DP = 1,31) de escolas públicas e particulares, as quais responderam a Escala de Comportamentos de Bullying, o Questionário dos Valores Bá...

  16. Nebulosas planetárias galácticas: idades e cinemática

    Science.gov (United States)

    Lago, L. G.; Maciel, W. J.

    2003-08-01

    As nebulosas planetárias são formadas a partir de estrelas com massas entre 0.8 e 8 massas solares na sequência principal, formando um conjunto de objetos com idades e populações diferentes. Esse fato torna as nebulosas interessantes ao estudo da rotação galáctica, uma vez que as populações mais jovens devem estar claramente associadas ao disco fino da Galáxia, enquanto que as populações mais velhas estariam associadas ao disco espesso ou mesmo ao halo galáctico. Neste trabalho, utilizamos uma grande amostra de nebulosas com velocidades radiais conhecidas para determinar a curva de rotação da Galáxia. Para minimizar os erros decorrentes das incertezas nas distâncias, usamos quatro diferentes escalas estatísticas. Para a atribuição da idade dos objetos, utilizamos o método proposto recentemente por Maciel et al. (Astron. Astrophys. 397, 667, 2003), em um estudo da variação temporal dos gradientes de abundâncias. Com esse método, é possível obter uma classificação das nebulosas por grupos de idade, totalmente independente de outros sistemas de classificação, uma vez que as idades são estimadas individualmente, a partir das metalicidades das nebulosas. Nossos resultados são comparados com as previsões dos tipos de Peimbert, e mostram que os desvios médios das curvas obtidas são sensivelmente menores nos casos dos objetos mais jovens, associados ao disco fino, com relação aos objetos mais velhos do disco espesso, levando à determinação de uma curva de rotação semelhante à dos objetos de população I jovem. (CNPq)

  17. Numerical studies of triplet and Russian quadruplet quadrupole lens systems with the given spot size on the target, for use in a microprobe

    Energy Technology Data Exchange (ETDEWEB)

    Brazhnik, V A; Lebed, S A; Ponomarev, A G; Storizhko, V E [Ukrainian Academy of Sciences, Sumy (Ukraine). Applied Physics Institute; Dymnikov, A D [University of St Petersburg, Stary (Russian Federation). Institute of Computational Mathematics and Control Processes; Jamieson, D N; Legge, S A [Melbourne Univ., Parkville, VIC (Australia). School of Physics

    1994-12-31

    In a nuclear microprobe the focusing system is an essential component which determines the beam spot size, i.e. the microprobe resolution. A small beam cross section at the target is the most important of the many conflicting requirements imposed on the beam The second most important factor is the current of the beam which at the given brightness is proportional to the phase volume (or emittance) of the beam. Existing microprobes frequently use a triplet or a Russian quadruplet as the focusing systems. This paper describes the numerical studies of some optimal quadrupole lens systems consisting of three or four lenses suitable for use in a nuclear microprobe taking into account geometrical aberrations of third order. The maximum emittance of changed particle beams for these systems has been found. It is shown how the maximum emittance depends on the spot size. 2 refs., 2 figs.

  18. Numerical studies of triplet and Russian quadruplet quadrupole lens systems with the given spot size on the target, for use in a microprobe

    Energy Technology Data Exchange (ETDEWEB)

    Brazhnik, V.A.; Lebed, S.A.; Ponomarev, A.G.; Storizhko, V.E. [Ukrainian Academy of Sciences, Sumy (Ukraine). Applied Physics Institute; Dymnikov, A.D. [University of St Petersburg, Stary (Russian Federation). Institute of Computational Mathematics and Control Processes; Jamieson, D.N.; Legge, S.A. [Melbourne Univ., Parkville, VIC (Australia). School of Physics

    1993-12-31

    In a nuclear microprobe the focusing system is an essential component which determines the beam spot size, i.e. the microprobe resolution. A small beam cross section at the target is the most important of the many conflicting requirements imposed on the beam The second most important factor is the current of the beam which at the given brightness is proportional to the phase volume (or emittance) of the beam. Existing microprobes frequently use a triplet or a Russian quadruplet as the focusing systems. This paper describes the numerical studies of some optimal quadrupole lens systems consisting of three or four lenses suitable for use in a nuclear microprobe taking into account geometrical aberrations of third order. The maximum emittance of changed particle beams for these systems has been found. It is shown how the maximum emittance depends on the spot size. 2 refs., 2 figs.

  19. Numerical studies of triplet and Russian quadruplet quadrupole lens systems with the given spot size on the target, for use in a microprobe

    International Nuclear Information System (INIS)

    Brazhnik, V.A.; Lebed, S.A.; Ponomarev, A.G.; Storizhko, V.E.; Dymnikov, A.D.; Jamieson, D.N.; Legge, S.A.

    1993-01-01

    In a nuclear microprobe the focusing system is an essential component which determines the beam spot size, i.e. the microprobe resolution. A small beam cross section at the target is the most important of the many conflicting requirements imposed on the beam The second most important factor is the current of the beam which at the given brightness is proportional to the phase volume (or emittance) of the beam. Existing microprobes frequently use a triplet or a Russian quadruplet as the focusing systems. This paper describes the numerical studies of some optimal quadrupole lens systems consisting of three or four lenses suitable for use in a nuclear microprobe taking into account geometrical aberrations of third order. The maximum emittance of changed particle beams for these systems has been found. It is shown how the maximum emittance depends on the spot size. 2 refs., 2 figs

  20. Ion beam analysis - development and application of nuclear reaction analysis methods, in particular at a nuclear microprobe

    International Nuclear Information System (INIS)

    Sjoeland, K.A.

    1996-11-01

    This thesis treats the development of Ion Beam Analysis methods, principally for the analysis of light elements at a nuclear microprobe. The light elements in this context are defined as having an atomic number less than approx. 13. The work reported is to a large extent based on multiparameter methods. Several signals are recorded simultaneously, and the data can be effectively analyzed to reveal structures that can not be observed through one-parameter collection. The different techniques are combined in a new set-up at the Lund Nuclear Microprobe. The various detectors for reaction products are arranged in such a way that they can be used for the simultaneous analysis of hydrogen, lithium, boron and fluorine together with traditional PIXE analysis and Scanning Transmission Ion Microscopy as well as photon-tagged Nuclear Reaction Analysis. 48 refs

  1. Morfologia e Crescimento dos 6 aos 10 anos de idade em Viana do Castelo, Portugal

    Directory of Open Access Journals (Sweden)

    Luis Paulo Rodrigues

    2008-09-01

    Full Text Available Ao longo de quatro anos, o Estudo Morfofuncional da Criança Vianense observou 1911 crianças entre os 6e os 10 anos de idade, resultando em 4064 observações individuais(2054 de raparigas, 2006 de rapazes.Os resultados encontrados nos indicadores morfológicos simples(altura, peso, pregas adiposas, diâmetros ósseos e perímetros muscularese no somatótipo, são descritos normativamente (valores percentílicose comparados com outros estudos nacionais e internacionais. As crianças vianenses demonstraram possuir uma estatura média ligeiramente superior às reportadas nos estudos portugueses e um ritmo de crescimento diferente das norte-americanas; peso semelhante ao das congéneres nacionais mas inferior ao das EUA; valores de pregas adiposas geralmente inferiores aos encontrados em Portugal e EUA; perímetros musculares e diâmetros ósseos semelhantes aos seus pares portugueses; e uma tendência para o aumento, com a idade, do ectomorfismo nos rapazes e do endomorfismo em ambos os sexos. Este panorama parece indicar que as crianças vianenses apresentam características de aptidão morfologia que estão longe de espelhar as preocupações internacionais nesta matéria.

  2. Nuclear microprobe analysis of serpentine from the mid-Atlantic ridge

    International Nuclear Information System (INIS)

    Orberger, Beate; Metrich, Nicole; Mosbah, Michelle; Mevel, Catherine; Fouquet, Yves

    1999-01-01

    At mid-ocean ridges, ultramafic rocks are serpentinized by interaction with seawater-derived fluids. Elements, dissolved in large quantities in seawater, e.g., Na, K, Cl, Br, Ca and Sr, can be, in small amounts, incorporated as traces into the crystal structure of the various serpentine minerals (Mg 3 Si 2 O 5 (OH) 4 ). These trace elements can be used to track the composition of the reacting fluids and to constrain physico-chemical conditions. This paper represents the first application of particle-induced X- and γ-ray emission (PIXE/PIGE) analysis to serpentine using the nuclear microprobe at the Laboratoire Pierre Suee (CEA-CNRS). Three types of serpentine, belonging to two different serpentinization generations, have been analysed in samples collected from the Mid-Atlantic Ridge (14 deg. 45'N/45 deg. W) that exposes serpentinized peridotites on which the Logachev black smoker is placed. The trace elements Cl, F, S, Cu, Zn, Ca, K, Ni, Cr and Mn were detected from several tens to several thousands of ppm. Bromine, As and Sr are close to the detection limit of about 5 ppm. The trace element concentrations and interelement relationships in serpentines vary (a) with the serpentine type and (b) with the geographic location to the black smoker. Chlorine and in part S originated from seawater, whereas Cu, Zn, Ca, K, Ni, Cr and Fe and the major amount of S were mobilized from the unaltered host rock and partitioned between the serpentine and the aqueous solution

  3. The use of field indentation microprobe in measuring mechanical properties of welds

    International Nuclear Information System (INIS)

    Haggag, F.M.; Wong, H.; Alexander, D.J.; Nanstad, R.K.

    1989-01-01

    A field indentation microprobe (FIM) was conceived for evaluating the structural integrity of metallic components (including base metal, welds, and heat-affected zones) in situ in a nondestructive manner. The FIM consists of an automated ball indentation (ABI) unit for determining the mechanical properties (yield strength, flow properties, estimates of fracture toughness, etc.) and a nondestructive evaluation (NDE) unit (consisting of ultrasonic transducers and a video camera) for determining the physical properties such as crack size, material pileup around indentation, and residual stress presence and orientation. The laboratory version used in this work performs only ABI testing. ABI tests were performed on stainless steel base metal (type 316L), heat-affected zone, and welds (type 308). Excellent agreement was obtained between yield strength and flow properties (true-stress/true-plastic-strain curve) measured by the ABI tests and those from uniaxial tensile tests conducted on 308 stainless steel welds, thermally aged at 343/degree/C for different times, and on the base material. 4 refs., 17 figs

  4. Ion microprobe analyses of aluminous lunar glasses - A test of the 'rock type' hypothesis

    Science.gov (United States)

    Meyer, C., Jr.

    1978-01-01

    Previous soil survey investigations found that there are natural groupings of glass compositions in lunar soils and that the average major element composition of some of these groupings is the same at widely separated lunar landing sites. This led soil survey enthusiasts to promote the hypothesis that the average composition of glass groupings represents the composition of primary lunar 'rock types'. In this investigation the trace element composition of numerous aluminous glass particles was determined by the ion microprobe method as a test of the above mentioned 'rock type' hypothesis. It was found that within any grouping of aluminous lunar glasses by major element content, there is considerable scatter in the refractory trace element content. In addition, aluminous glasses grouped by major elements were found to have different average trace element contents at different sites (Apollo 15, 16 and Luna 20). This evidence argues that natural groupings in glass compositions are determined by regolith processes and may not represent the composition of primary lunar 'rock types'.

  5. Raman and luminescence spectroscopy of zirconium oxide with the use of the MOLE microprobe

    International Nuclear Information System (INIS)

    Doyle, T.E.; Alvarez, J.L.

    1984-01-01

    Raman and luminescence spectroscopy with the use of the MOLE microprobe has been used to characterize ZrO 2 originating from oxidized fuel-rod cladding in nuclear accidents. Micro-Raman analysis of samples from Three Mile Island Unit 2 and the Power Burst Facility identified tetragonal and cubic ZrO 2 . The tetragonal and cubic phases are high-temperature polymorphs of ZrO 2 and provide information about temperatures and hydrogen formation in the TMI-2 core. The data suggest that the tetragonal ZrO 2 in TMI-2 samples was stabilized by a crystallite size effect, whereas cubic ZrO 2 in PBF debris samples was stabilized by impurities. Luminescence was used to differentiate yttria-stabilized ZrO 2 ceramics and oxidized fuel-rod cladding in PBF debris samples. The ZrO 2 ceramics produced strong, sharp luminescence peaks which indicated the presence of titanium and yttria in the ZrO 2 . Oxidized fuel-rod cladding displayed no luminescence

  6. A study of aluminium-exposed fish using a scanning proton microprobe

    Energy Technology Data Exchange (ETDEWEB)

    Cholewa, M; Legge, G L.F. [Melbourne Univ., Parkville, VIC (Australia). School of Physics; Eeckhaoudt, S; Van Grieken, R [Universitaire Instelling Antwerpen, Antwerp (Belgium)

    1994-12-31

    A major problem has arisen in Europe with the depopulation of fresh water fish in lakes and streams collecting acid rain. The sensitivity to acidification is species specific and appears to be associated with metal levels. The Scanning Proton Microprobe (SPMP) at the Micro Analytical Research Centre of the University of Melbourne was used to study the subcellular distribution of aluminium and other elements in the gills of fish exposed to acidified water with elevated Al-levels. Experiments were performed on thin sections taken from fish exposed to media with different pH and aluminium concentration. Aluminium was found on the surface of the gill lamellae, but also inside the tissue. Bulk analysis of the gills showed much higher concentrations in the aluminium-exposed fish, compared to the control ones, but no information regarding the actual accumulation sites can be inferred. Extensive study of damage done to the sample by intense proton beams during elemental analysis was performed with scanning transmission ion microscopy. 3 refs., 3 figs.

  7. Application of a nuclear microprobe to the study of calcified tissues

    Science.gov (United States)

    Coote, Graeme E.; Vickridge, Ian C.

    1988-03-01

    The mineral fraction of calcified tissue is largely calcium hydroxyapatite (bones and teeth) or calcium carbonate (shells and fish otoliths). Apatite has such a strong affinity for fluoride ions that the F/Ca ratio can vary markedly with position in a bone or tooth, depending on the amount of fluoride present at the time of calcification or partial recrystallization. New biological information can be obtained by introducing extra fluoride into the diet of an animal and using a microprobe later to scan sections of bones or teeth. In suitable burial sites extra fluoride is introduced after death, and the new distribution may have applications in forensic science and archaeology. Fish otoliths are also of interest since a new carbonate layer is formed each day and the distribution of trace elements may record some aspects of the fish's life history. Results from the following studies are presented: fluorine distributions in the teeth of sheep which ingested extra fluoride for known periods; distributions of calcium and fluorine in femurs of rats which drank water high in fluoride for periods from 2 to 15 weeks; calcium and fluorine distributions in artificially-prepared lesions in tooth enamel; diffusion profiles in archaeological human teeth and animal bones; patterns in the strontium/calcium ratio in sectioned otoliths of several species of fish.

  8. A study of aluminium-exposed fish using a scanning proton microprobe

    Energy Technology Data Exchange (ETDEWEB)

    Cholewa, M.; Legge, G.L.F. [Melbourne Univ., Parkville, VIC (Australia). School of Physics; Eeckhaoudt, S.; Van Grieken, R. [Universitaire Instelling Antwerpen, Antwerp (Belgium)

    1993-12-31

    A major problem has arisen in Europe with the depopulation of fresh water fish in lakes and streams collecting acid rain. The sensitivity to acidification is species specific and appears to be associated with metal levels. The Scanning Proton Microprobe (SPMP) at the Micro Analytical Research Centre of the University of Melbourne was used to study the subcellular distribution of aluminium and other elements in the gills of fish exposed to acidified water with elevated Al-levels. Experiments were performed on thin sections taken from fish exposed to media with different pH and aluminium concentration. Aluminium was found on the surface of the gill lamellae, but also inside the tissue. Bulk analysis of the gills showed much higher concentrations in the aluminium-exposed fish, compared to the control ones, but no information regarding the actual accumulation sites can be inferred. Extensive study of damage done to the sample by intense proton beams during elemental analysis was performed with scanning transmission ion microscopy. 3 refs., 3 figs.

  9. Performance of a high-resolution x-ray microprobe at the Advanced Photon Source

    International Nuclear Information System (INIS)

    Cai, Z.; Lai, B.; Yun, W.; McNulty, I.; Khounsary, A.; Maser, J.; Ilinski, P.; Legnini, D.; Trakhtenberg, E.; Xu, S.; Tieman, B.; Wiemerslage, G.; Gluskin, E.

    1999-01-01

    The authors have developed a x-ray microprobe in the energy region from 6 to 20 keV using undulator radiation and zone-plate optics for microfocusing-based techniques and applications at a beamline at the Advanced Photon Source (APS). The performance of the beamline was shown to meet the design objectives, including preservation of the source brilliance and coherence, selectable transverse coherence length and energy bandwidth, high angular stability, and harmonic suppression of the beam. These objectives were achieved by careful thermal management and use of a novel mirror and crystal monochromator cooling geometry. All beamline optical components are water cooled, and the x-ray beam in the experiment station is stable in beam intensity, energy, and position over many days with no active feedback. Using a double-crystal Si(111) monochromator, they have obtained a focal spot size (FWHM) of 0.15 (micro)m (v) x 1.0 (micro)m (h), and a photon flux of 4 x 10 9 photons/sec at the focal spot, and thus a photon flux density gain of 15,000. A circular beam spot of 0.15 (micro)m in diameter can be achieved by reducing the horizontal source size using a white beam slit located 43.5 meters upstream of the zone plate, with an order of magnitude less flux in the focal spot

  10. A novel ultra-short scanning nuclear microprobe: Design and preliminary results

    International Nuclear Information System (INIS)

    Lebed, S.; Butz, T.; Vogt, J.; Reinert, T.; Spemann, D.; Heitmann, J.; Stachura, Z.; Lekki, J.; Potempa, A.; Styczen, J.; Sulkio-Cleff, B.

    2001-01-01

    The paper describes an optimized scanning nuclear microprobe (MP) with a new ultra-short (total length of 1.85 m) probe forming system based on a divided Russian quadruplet (DRQ) of magnetic quadrupole lenses. Modern electrostatic accelerators have a comparatively high beam brightness of about 10-25 pA/μm 2 /mrad 2 /MeV. This allows the MP proposed to provide a high lateral resolution even with large (1%) parasitic (sextupole and octupole) pole tip field components in all lenses. The features of the design permit the MP operation in the high current and low current modes with a short working distance and inexpensive quadrupole lenses. A new quadrupole doublet design has been developed for the MP. In the present work the calculated features of the new MP are compared with preliminary experimental results obtained with a similar system (total length of 2.3 m) at the INP in Cracow. The new MP is promising for studies of solids or biological samples with high resolutions (0.08-2 μm) in both modes under ambient conditions. A vertical version of the ultra-short MP can be very useful for single ion bombardments of living cells

  11. Development of an optical fiber SERS microprobe for minimally invasive sensing applications

    Science.gov (United States)

    Mamun, Md Abdullah Al; Juodkazis, Saulius; Mahadevan-Jansen, Anita; Stoddart, Paul R.

    2018-02-01

    Numerous potential biomedical sensing applications of surface-enhanced Raman scattering (SERS) have been reported, but its practical use has been limited by the lack of a robust sensing platform. Optical fiber SERS probes show great promise, but are limited by the prominent silica Raman background, which requires the use of bulky optics for filtering the signal collection and excitation delivery paths. In the present study, a SERS microprobe has been designed and developed to eliminate the bottlenecks outlined above. For efficient excitation and delivery of the SERS signal, both hollow core photonic crystal fiber and double clad fiber have been investigated. While the hollow core fiber was still found to have excessive silica background, the double clad fiber allows efficient signal collection via the multi-mode inner cladding. A micro filtering mechanism has been designed, which can be integrated into the tip of the optical fiber SERS probe, providing filtering to suppress silica Raman background and thus avoiding the need for bulky optics. The design also assists in the efficient collection of SERS signal from the sample by rejecting Rayleigh scattered light from the sample. Optical fiber cleaving using ultra-short laser pulses was tested for improved control of the fiber tip geometry. With this miniaturized and integrated filtering mechanism, it is expected that the developed probe will promote the use of SERS for minimally invasive biomedical monitoring and sensing applications in future. The probe could potentially be placed inside a small gauge hypodermic needle and would be compatible with handheld portable spectrometers.

  12. Characterisation of Inorganic Pigments Used by Selected Painters by Using Ion Microprobe and Other Complementary Techniques

    International Nuclear Information System (INIS)

    Fazinic, S.; Pastuovic, Z.; Jaksic, M.; Kusijanovic, K.; Mudronja, D.; Braun, M.; Desnica, V.

    2011-01-01

    The aim of the presentation is to show results of the collaboration between the Croatian Conservation Institute (CCI) and the Laboratory for Ion Beam Interactions of the Rudjer Boskovic Institute (RBI) established within the present CRP. CCI is the central Croatian institution for conservation and restoration of cultural heritage objects. Prior to restoration/conservation CCI performs scientific analysis of an object, primarily to enable selection of the best strategy for its restoration/conservation. In many occasions such analysis is also helpful to resolve issues such as clarification of authenticity and/or authorship of an object. CCI has its analytical laboratory which is fully dedicated to the analysis of cultural heritage and art objects. CCI analytical laboratory is equipped with various microscopy techniques, photography methods, portable X-ray Fluorescence Spectrometer (XRF) and X-ray radiography instrumentation. Access to complementary microanalytical techniques like Raman Spectroscopy or Ion Beam Analytical (IBA) techniques is provided through already long and successful collaboration with RBI. The RBI Laboratory for Ion Beam Interactions provides complementary analysis of layered microsamples by using IBA techniques, such as Particle Induced X-ray Emission (PIXE) and Rutherford Back-scattering (RBS), and for the miniature samples by using ion microprobe. (author)

  13. Using Synchrotron X-ray Fluorescence Microprobes in the Study of Metal Homeostasis in Plants

    International Nuclear Information System (INIS)

    Punshon, T.; Guerinot, M.; Lanzirotti, A.

    2009-01-01

    Background and Aims: This Botanical Briefing reviews the application of synchrotron X-ray fluorescence (SXRF) microprobes to the plant sciences; how the technique has expanded our knowledge of metal(loid) homeostasis, and how it can be used in the future. Scope: The use of SXRF microspectroscopy and microtomography in research on metal homeostasis in plants is reviewed. The potential use of SXRF as part of the ionomics toolbox, where it is able to provide fundamental information on the way that plants control metal homeostasis, is recommended. Conclusions: SXRF is one of the few techniques capable of providing spatially resolved in-vivo metal abundance data on a sub-micrometre scale, without the need for chemical fixation, coating, drying or even sectioning of samples. This gives researchers the ability to uncover mechanisms of plant metal homeostasis that can potentially be obscured by the artefacts of sample preparation. Further, new generation synchrotrons with smaller beam sizes and more sensitive detection systems will allow for the imaging of metal distribution within single living plant cells. Even greater advances in our understanding of metal homeostasis in plants can be gained by overcoming some of the practical boundaries that exist in the use of SXRF analysis.

  14. Direct localised measurement of electrical resistivity profile in rat and embryonic chick retinas using a microprobe

    Directory of Open Access Journals (Sweden)

    Harald van Lintel

    2010-01-01

    Full Text Available We report an alternative technique to perform a direct and local measurement of electrical resistivities in a layered retinal tissue. Information on resistivity changes along the depth in a retina is important for modelling retinal stimulation by retinal prostheses. Existing techniques for resistivity-depth profiling have the drawbacks of a complicated experimental setup, a less localised resistivity probing and/or lower stability for measurements. We employed a flexible microprobe to measure local resistivity with bipolar impedance spectroscopy at various depths in isolated rat and chick embryo retinas for the first time. Small electrode spacing permitted high resolution measurements and the probe flexibility contributed to stable resistivity profiling. The resistivity was directly calculated based on the resistive part of the impedance measured with the Peak Resistance Frequency (PRF methodology. The resistivity-depth profiles for both rat and chick embryo models are in accordance with previous mammalian and avian studies in literature. We demonstrate that the measured resistivity at each depth has its own PRF signature. Resistivity profiles obtained with our setup provide the basis for the construction of an electric model of the retina. This model can be used to predict variations in parameters related to retinal stimulation and especially in the design and optimisation of efficient retinal implants.

  15. Practical aspects of quantitative laser Raman microprobe spectroscopy for the study of fluid inclusions

    International Nuclear Information System (INIS)

    Pasteris, J.D.; Wopenka, B.; Seitz, J.C.

    1988-01-01

    This paper is addressed to both geologists who use laser Raman microprobe (LRM) spectroscopy to analyze fluid inclusions and to those who want to evaluate analyses done by this technique. Emphasis is on how to obtain quantitative analyses of fluid inclusions. The authors discuss the basic method of fluid inclusion analysis by LRM spectroscopy and the levels of accuracy and precision attainable with this technique. They evaluate which kinds of fluid inclusions and host mineral matrices will yield the most reliable compositional data. Necessary sample preparations, detection limits, problems with fluorescence, dependence of Raman scattering efficiencies on density, and many other questions asked at the workshop on Raman spectroscopy during the 1987 ACROFI meeting also are addressed. The complementary nature, advantages, and disadvantages of both LRM spectroscopy and microthermometry, the two techniques most frequently used for the analysis of individual fluid inclusions, are emphasized. Some discussions are intended to held LRM users calibrate, and evaluate the optical characteristics of, their particular instruments. It is hoped that this paper will further LRM users in finding a common ground on which to discuss the differences and similarities among different LRM instruments, and that it will encourage a future consensus on efficient means of calibration and on interlaboratory standards

  16. The use of the RBI nuclear microprobe in conservation process studies of a church portal

    Energy Technology Data Exchange (ETDEWEB)

    Pastuovic, Z. [Ruder Boskovic Institute, Bijenicka c. 54, 10000 Zagreb (Croatia)]. E-mail: pastu@irb.hr; Fazinic, S. [Ruder Boskovic Institute, Bijenicka c. 54, 10000 Zagreb (Croatia); Jaksic, M. [Ruder Boskovic Institute, Bijenicka c. 54, 10000 Zagreb (Croatia); Krstic, D. [Croatian Conservation Institute, Nike Grskovica 23, 10000 Zagreb (Croatia); Mudronja, D. [Croatian Conservation Institute, Nike Grskovica 23, 10000 Zagreb (Croatia)

    2005-04-01

    The southern portal of the St. Marko church in Zagreb, Croatia, is currently under the process of conservation. The conservation treatments on calcareous sandstone consist of (i) removal of harmful sulfates (gypsum) from the surface of the material by saturated solution of ammonium carbonate; and (ii) treatment of the material surface with a 10% solution of barium hydroxide in order to convert the remaining dissolvable sulfates into non-dissolvable compounds and to strengthen the material surface. The nuclear microprobe has been used to measure the level of gypsum induced damage, and quality of conservation. More specifically, the surface quantity and depth concentration profiles of sulfur have been determined in several samples taken from the portal before and after the treatment with the solution of ammonium carbonate. To test the quality of treatment by the barium hydroxide solution, the depth concentration of barium in the samples has been determined after the treatment. Both sulfur and barium concentration levels have been determined by scanning the focused proton beam over the samples, detecting PIXE spectra and creating elemental distribution maps. Beside portal samples, the efficiency of the barium hydroxide treatment was tested on sandstone samples from nearby stone pit assumed to be the origin of material used for portal construction.

  17. A study of aluminium-exposed fish using a scanning proton microprobe

    International Nuclear Information System (INIS)

    Cholewa, M.; Legge, G.L.F.

    1993-01-01

    A major problem has arisen in Europe with the depopulation of fresh water fish in lakes and streams collecting acid rain. The sensitivity to acidification is species specific and appears to be associated with metal levels. The Scanning Proton Microprobe (SPMP) at the Micro Analytical Research Centre of the University of Melbourne was used to study the subcellular distribution of aluminium and other elements in the gills of fish exposed to acidified water with elevated Al-levels. Experiments were performed on thin sections taken from fish exposed to media with different pH and aluminium concentration. Aluminium was found on the surface of the gill lamellae, but also inside the tissue. Bulk analysis of the gills showed much higher concentrations in the aluminium-exposed fish, compared to the control ones, but no information regarding the actual accumulation sites can be inferred. Extensive study of damage done to the sample by intense proton beams during elemental analysis was performed with scanning transmission ion microscopy. 3 refs., 3 figs

  18. The use of the RBI nuclear microprobe in conservation process studies of a church portal

    International Nuclear Information System (INIS)

    Pastuovic, Z.; Fazinic, S.; Jaksic, M.; Krstic, D.; Mudronja, D.

    2005-01-01

    The southern portal of the St. Marko church in Zagreb, Croatia, is currently under the process of conservation. The conservation treatments on calcareous sandstone consist of (i) removal of harmful sulfates (gypsum) from the surface of the material by saturated solution of ammonium carbonate; and (ii) treatment of the material surface with a 10% solution of barium hydroxide in order to convert the remaining dissolvable sulfates into non-dissolvable compounds and to strengthen the material surface. The nuclear microprobe has been used to measure the level of gypsum induced damage, and quality of conservation. More specifically, the surface quantity and depth concentration profiles of sulfur have been determined in several samples taken from the portal before and after the treatment with the solution of ammonium carbonate. To test the quality of treatment by the barium hydroxide solution, the depth concentration of barium in the samples has been determined after the treatment. Both sulfur and barium concentration levels have been determined by scanning the focused proton beam over the samples, detecting PIXE spectra and creating elemental distribution maps. Beside portal samples, the efficiency of the barium hydroxide treatment was tested on sandstone samples from nearby stone pit assumed to be the origin of material used for portal construction

  19. Metallographic study of ferrite → sigma transformation using ferromagnetic colloid, microprobe analysis, and color etching

    International Nuclear Information System (INIS)

    Gray, R.J.; Crouse, R.S.; Sikka, V.K.; King, R.T.

    1976-01-01

    The mechanical properties of ferrite-containing austenitic stainless steel base metal and weldments are usually adversely affected by prolonged exposure to temperatures in the 482-900 0 C (900-1652 0 F) range. One cause of the property alteration is related to the transformation of relatively ductile delta-ferrite to less ductile sigma-phase. Attempts to identify sigma and delta ferrite phases by color staining techniques alone are well documented; however, the results are often questionable due to the difficulty in maintaining consistent color identifications. This investigation is concerned with the microstructural responses of the ferromagnetic delta-ferrite phase and the paramagnetic sigma-phase to a ferromagnetic iron colloid in a magnetic field. Such positive or negative responses of the two phases to the colloid offer a more definitive identification. With this technique, the identification of small amounts of these phases in the microstructure is limited only by the highest magnification and resolution of the optical microscope. The procedure is substantiated in this metallographic study with microprobe analysis and color metallography. Several examples of the correlative use of these three techniques in identifying varying amounts of delta-ferrite yields sigma transformation are presented

  20. Microprobe PIXE study of Ni–Ge interactions in lateral diffusion couples

    Energy Technology Data Exchange (ETDEWEB)

    Chilukusha, D. [Department of Physics, University of Zambia, P.O. Box 32379, Lusaka 10101 (Zambia); Pineda-Vargas, C.A. [iThemba LABS, National Research Foundation, P.O. Box 722, Somerset West 7129 (South Africa); Faculty of Health & Wellness Sciences, CPUT, Bellville (South Africa); Nemutudi, R. [iThemba LABS, National Research Foundation, P.O. Box 722, Somerset West 7129 (South Africa); Habanyama, A. [Department of Physics, Copperbelt University, P.O. Box 21692, Jambo Drive, Riverside, Kitwe 10101 (Zambia); Comrie, C.M. [iThemba LABS, National Research Foundation, P.O. Box 722, Somerset West 7129 (South Africa)

    2015-11-15

    Rutherford backscattering spectrometry on the nuclear microprobe (μRBS) is often used in studies of lateral diffusion couples. RBS requires that the positions of the interacting species on the periodic table are not too close in terms of atomic number and therefore do not produce excessive RBS peak overlap. In order to satisfactorily characterize systems that have atomic numbers which are close, it is necessary to find techniques which can complement μRBS. The aim of this study was to determine the extent to which particle induced X-ray emission (PIXE) could be applied in the lateral diffusion couple study of a system with relatively close atomic numbers. This was with a view that it may eventually be adopted to study systems where the atomic numbers are too close for RBS analysis. The system studied here was the Ni–Ge binary system. Since RBS is an established technique for studying lateral diffusion couples, we used it as a standard for comparison. The PIXE results showed a maximum error of 12% with reference to the RBS standard. In order to achieve the most effective use of PIXE in lateral diffusion couple studies we recommend the use of the technique in such a way as to obtain depth information and the use of relatively thick sample layers.

  1. Optimization of the working distance of an ion microprobe-forming system

    International Nuclear Information System (INIS)

    Melnik, K.I.; Magilin, D.V.; Ponomarev, A.G.

    2009-01-01

    A high-resolution ion microprobe necessitates the use of a small working distance (the distance from the final quadrupole lens of a probe-forming system to the specimen) in order to produce a large demagnification. But at the same time a small working distance is a source of a number of practical difficulties. We have presented an approach for determining a working distance that provides the best spatial resolution with the main practical limitations taken into account. We used a probe-forming system acceptance as a criterion of optimality. The calculations have revealed the existence of an optimal working distance in a set of common probe-forming systems, but it can be achieved only after changing of a design of a final quadrupole lens. We proposed a possible design of conic lens that allows solving the problem of detectors location and creating a short focus system. Three-dimensional calculations of magnetic field within this lens predicted a good quality of field structure.

  2. Deposition of corrosion products from dowels on human dental root surfaces measured with proton microprobe technique

    International Nuclear Information System (INIS)

    Brune, D.; Brunell, G.; Lindh, U.

    1982-01-01

    Distribution of copper, mercury and zinc on human teeth root surfaces adjacent to dowels of gold alloy or brass as well as dowels of brass in conjunction with an amalgam crown has been measured with a proton microprobe using PIXE techniques. Upper limits of the contents of gold and silver on the root surfaces were established. Pronounced concentration profiles of copper and zinc were observed on the root surfaces of teeth prepared with dowels of brass. The dowel of gold alloy revealed only zinc deposition. The major part of copper on the root surfaces is assumed to arise from corrosion of the dowels, and has been transported to the surface by diffusion through the dential tubuli. Zinc in the volume analysed is a constituent of dentin tissue as well as a corrosion product of the brass dowel. Part of the zinc level could also be ascribed to erosion of the zinc phosphate cement matrix. The volumes analysed were (25 x 25 x 25)μm 3 . The levels of copper, mercury and zinc on the tooth root surfaces attained values up to about 200, 20 and 600 ppm, respectively. (orig.)

  3. Deposition of corrosion products from dowels on human dental root surfaces measured with proton microprobe technique

    Science.gov (United States)

    Brune, D.; Brunell, G.; Lindh, U.

    1982-06-01

    Distribution of copper, mercury and zinc on human teeth root surfaces adjacent to dowels of gold alloy or brass as well as dowels of brass in conjunction with an amalgam crown has been measured with a proton microprobe using PIXE techniques. Upper limits of the contents of gold and silver on the root surfaces were established. Pronounced concentration profiles of copper and zinc were observed on the root surfaces of teeth prepared with dowels of brass. The dowel of gold alloy revealed only zinc deposition. The major part of copper on the root surfaces is assumed to arise from corrosion of the dowels, and has been transported to the surface by diffusion through the dential tubuli. Zinc in the volume analysed is a constituent of dentin tissue as well as a corrosion product of the brass dowel. Part of the zinc level could also be ascribed to erosion of the zinc phosphate cement matrix. The volumes analysed were (25×25×25)μm 3. The levels of copper, mercury and zinc on the tooth root surfaces attained values up to about 200, 20 and 600 ppm, respectively.

  4. Estimativa da prevalência de déficit de altura/idade a partir da prevalência de déficit de peso/idade em crianças brasileiras

    Directory of Open Access Journals (Sweden)

    Victora Cesar G.

    1998-01-01

    Full Text Available INTRODUÇÃO: A antropometria é amplamente utilizada para avaliação nutricional de indivíduos e de grupos populacionais. Em anos recentes, diagnósticos comunitários têm sido realizados por profissionais dos serviços de saúde em diversas regiões brasileiras, com o objetivo de complementar os dados obtidos através de vigilância nutricional. Um obstáculo importante à realização destes diagnósticos é a difícil mensuração da altura em inquéritos domiciliares. MÉTODO: Foram identificados 38 inquéritos antropométricos com crianças de 0 a 5 anos de idade, realizados no Brasil, que utilizaram o padrão de referência NCHS e o percentual de crianças abaixo de -2 escore Z para definição da prevalência de déficit de peso/idade e altura/idade. A análise foi realizada a partir das correlações entre as prevalências de déficits de altura/idade e peso/idade definidas. RESULTADOS: A análise mostrou que devido à baixa prevalência de déficits de peso/altura há forte correlação entre peso/idade e altura/idade, em nível populacional. Cerca de 90% da variabilidade de altura/idade (A/I é explicada pelo peso/idade (P/I. CONCLUSÃO: Através da equação (Prev. A/I = 0,74 + 2,34 (Prev. P/I - 0,03 (Prev. P/I2, é possível estimar os déficits de altura, desde que se conheça os déficits de peso. Espera-se que os resultados possam contribuir para a simplificação dos inquéritos antropométricos realizados no âmbito dos serviços e favorecer sua disseminação.

  5. Perfil dos idosos usuários das academias ao ar livre para a terceira idade

    Directory of Open Access Journals (Sweden)

    Wesley Lessa Pinheiro

    2017-03-01

    Full Text Available Objetivo: Descrever o perfil dos idosos usuários das academias ao ar livre para a terceira idade de Fortaleza,Ceará. Métodos: Estudo transversal, envolvendo uma amostra de 374 idosos com idade maior ou igual a 60 anos, realizado entre os meses de outubro de 2015 e abril de 2016, nas academias ao ar livre para a terceira idade em Fortaleza, Ceará. Aplicou-se um questionário contendo questões sobre dados sociodemográficos, condições de saúde e hábitos de vida autorrelatados, e sobre a utilização dos equipamentos. Mensurou-se o peso e a altura para a obtenção do índice de massa corporal (IMC. Resultados: A maioria dos entrevistados era mulher (56,7%, n=212 e com faixa etária entre 60 e 69 anos (66,8%, n=250. As principais condições de saúde autorrelatadas foram hipertensão (40,9%, n=153, colesterol alto (32,4%, n=121 e osteoartrite (26,2%, n=98. Entre os hábitos de vida, o consumo de bebida alcoólica (31,6%, n=118 foi o mais relatado. Verificou-se que 42,8% (n=160 encontrava-se com excesso de peso. A maioria utilizava os equipamentos há mais de um ano (68,2%, n=255, até 30 minutos por dia (49,5%, n=185, cinco ou mais dias durante a semana (51%, n=191, tendo em grande parte percebido melhora na saúde (93,6%, n=350. Conclusão: Os idosos apresentaram um perfil jovem e ativo, cujas condições de saúde de maior prevalência podem ser facilmente manejadas com a prática de atividade física, e apresentam características semelhantes independentemente da situação econômica em que se encontram inseridos.

  6. Nuclear microprobe study of heavy metal uptake and transport in aquatic plant species

    International Nuclear Information System (INIS)

    Kertesz, Zs.; Kocsar, I.; Szikszai, Z.; Lakatos, Gy.

    2005-01-01

    Complete text of publication follows. In aquatic ecosystems water contamination by trace metals is one of the main types of pollution that may stress the biotic community. Although some metals are needed as micronutrients for autotrophic organisms, they can have toxic effects at higher concentration. Aquatic plants can take up large quantities of nutrients and metals from the environment, they can live under extreme environmental conditions therefore they are being increasingly used in remediation processes to reduce contamination. Besides the usually applied bulk analytical techniques quantitative micro-PIXE investigation of the macro, micro and trace element distribution within the root can lead to a better understanding of the heavy metal up-take, transport and detoxification mechanisms of the plants and thus helps to select the proper species for the remedial activity, or possibly to increase the efficiency of the remediation. In this work we determined the elemental distributions in root cross sections and along the roots of reed (Phragmaties australis), bulrush (Typha angustifolia) and sea club-rush (Bolboschoemus maritimus) using the Debrecen nuclear microprobe. The plants originate from the dried units of the wastewater sedimentation pond system of the tannery of Kunszentmarton. 1500 m 3 waste water containing lime, sodium-salts, ammonium-salts, chromium-salts, sodium, chlorine and magnesium ions, sulphur and organic material was released to the pond system every day till 1988. The chosen species are the dominant species of the area, composing 85-90% of the green plant covering. This heavily contaminated area has been regularly monitored by the colleagues of the Dept. of Applied Ecology of the Univ. of Debrecen since 1998. They focused their work the potentially toxic heavy metal chromium. In order to conserve the samples in the living state, the roots were frozen in liquid nitrogen. 16-20 μm thick cross sections were made with cryo-microtome, and all the

  7. DANÇAS MACABRAS: UMA CRÍTICA SOCIAL NA BAIXA IDADE MÉDIA

    Directory of Open Access Journals (Sweden)

    José Carlos Gimenez

    2011-09-01

    Full Text Available Este artigo realiza uma reflexão sobre o significado da morte retratado nas manifestações culturais conhecidas como Danças Macabras ou Danças da Morte; um gênero alegórico muito difundido no final da Idade Média e início do período Renascentista e que tem por objetivo discutir a fragilidade do homem diante da presença inevitável da morte. A análise é feita a partir da leitura do texto anônimo Danza General de Muerte, escrito entre os séculos XIV e XV.

  8. Tempos de aprender: a produção histórica da idade escolar

    Directory of Open Access Journals (Sweden)

    Maria Cristina Soares de Gouveia

    2012-02-01

    Full Text Available A emergência de um tempo escolar, nas sociedades ocidentais, com o advento da Modernidade, relaciona-se com a definição de um marco cronológico no decorrer da vida do indivíduo, ao longo do qual este deveria inserir-se na escola, a chamada idade escolar. Esse marco constitui não um recorte absoluto, mas é fruto de uma construção histórica, ao longo da qual se modificaram os parâmetros de sua definição. Para analisar essa relação, cabe compreender a produção da representação da infância como período de formação para a vida adulta, no interior da instituição escolar, de acordo com princípios pedagógicos característicos de tal instituição. Princípios esses centrados no pressuposto da educabilidade desse período de vida. Tal pressusposto tornou possível a emergência, no decorrer do século XIX, em diferentes países, das leis de obrigatoriedade escolar, que conferiram visibilidade social à idade da meninice (por volta dos 7 aos 14 anos entendida como idade escolar. Tendo como fontes primárias a legislação educacional e a documentação referente à instrução pública, busca-se analisar, no contexto da província mineira, o significado da noção de idade escolar ao longo do período e suas características, de modo que se apreendam suas permanências e deslocamentos. Abstract The emergence of a “scholar time” in occidental societies in modernity is related with the historical conformation process of an “scholar age”. In this sense, its necessary to understand the construction of childhood as the period of life when the individuate must be prepared to adult society, according to pedagogical principles in a school institution.Those principles are centred on the idea of childhood specificity, there educability. That notion turned possible the school, and the emergence of the “obligation scholar laws”, in differents nations, during the nineteen century, that institucionalized a scollar time into social

  9. Nuclear microprobe analysis of serpentine from the mid-Atlantic ridge

    Energy Technology Data Exchange (ETDEWEB)

    Orberger, Beate E-mail: orberger@geol.u-psud.fr; Metrich, Nicole; Mosbah, Michelle E-mail: mosbah@drecam.cea.fr; Mevel, Catherine; Fouquet, Yves

    1999-09-02

    At mid-ocean ridges, ultramafic rocks are serpentinized by interaction with seawater-derived fluids. Elements, dissolved in large quantities in seawater, e.g., Na, K, Cl, Br, Ca and Sr, can be, in small amounts, incorporated as traces into the crystal structure of the various serpentine minerals (Mg{sub 3}Si{sub 2}O{sub 5}(OH){sub 4}). These trace elements can be used to track the composition of the reacting fluids and to constrain physico-chemical conditions. This paper represents the first application of particle-induced X- and {gamma}-ray emission (PIXE/PIGE) analysis to serpentine using the nuclear microprobe at the Laboratoire Pierre Suee (CEA-CNRS). Three types of serpentine, belonging to two different serpentinization generations, have been analysed in samples collected from the Mid-Atlantic Ridge (14 deg. 45'N/45 deg. W) that exposes serpentinized peridotites on which the Logachev black smoker is placed. The trace elements Cl, F, S, Cu, Zn, Ca, K, Ni, Cr and Mn were detected from several tens to several thousands of ppm. Bromine, As and Sr are close to the detection limit of about 5 ppm. The trace element concentrations and interelement relationships in serpentines vary (a) with the serpentine type and (b) with the geographic location to the black smoker. Chlorine and in part S originated from seawater, whereas Cu, Zn, Ca, K, Ni, Cr and Fe and the major amount of S were mobilized from the unaltered host rock and partitioned between the serpentine and the aqueous solution.

  10. Nuclear microprobe analysis and source apportionment of individual atmospheric aerosol particles

    International Nuclear Information System (INIS)

    Artaxo, P.; Rabello, M.L.C.; Watt, F.; Grime, G.; Swietlicki, E.

    1993-01-01

    In atmospheric aerosol reserach, one key issue is to determine the sources of the airborne particles. Bulk PIXE analysis coupled with receptor modeling provides a useful, but limited view of the aerosol sources influencing one particular site or sample. The scanning nuclear microprobe (SNM) technique is a microanalytical technique that gives unique information on individual aerosol particles. In the SNM analyses a 1.0 μm size 2.4 MeV proton beam from the Oxford SNM was used. The trace elements with Z>11 were measured by the particle induced X-ray emission (PIXE) method with detection limits in the 1-10 ppm range. Carbon, nitrogen and oxygen are measured simultaneously using Rutherford backscattering spectrometry (RBS). Atmospheric aerosol particles were collected at the Brazilian Antarctic Station and at biomass burning sites in the Amazon basin tropical rain forest in Brazil. In the Antarctic samples, the sea-salt aerosol particles were clearly predominating, with NaCl and CaSO 4 as major compounds with several trace elements as Al, Si, P, K, Mn, Fe, Ni, Cu, Zn, Br, Sr, and Pb. Factor analysis of the elemental data showed the presence of four components: 1) Soil dust particles; 2) NaCl particles; 3) CaSO 4 with Sr; and 4) Br and Mg. Strontium, observed at 20-100 ppm levels, was always present in the CaSO 4 particles. The hierarchical cluster procedure gave results similar to the ones obtained through factor analysis. For the tropical rain forest biomass burning aerosol emissions, biogenic particles with a high organic content dominate the particle population, while K, P, Ca, Mg, Zn, and Si are the dominant elements. Zinc at 10-200 ppm is present in biogenic particles rich in P and K. The quantitative aspects and excellent detection limits make SNM analysis of individual aerosol particles a very powerful analytical tool. (orig.)

  11. Sulphur isotope variations in the mantle from ion microprobe analyses of micro-sulphide inclusions

    International Nuclear Information System (INIS)

    Chaussidon, M.; Albarede, F.; Sheppard, S.M.F.

    1989-01-01

    21 samples of sulphide trapped either as liquid globules or grains in various minerals (olivine, pyroxenes, ilmenite and garnet) or rocks (basalt glasses, peridotites, eclogites and kimberlites) of mantle origin, have been analysed for their sulphur isotope, and their Cu, Ni, Fe compositions by ion microprobe. The results show a wide range of δ 34 S values between -4.9±1 and +8±1per mille. Sulphides with high nickel contents (up to 40% pentlandite), corresponding mostly to residual peridotites, have δ 34 S values ranging from -3.2per mille to +3.6per mille with a mode of +3±1per mille, compared to low Ni content sulphides, mostly contained in pyroxenites, OIB and kimberlites, ranging from -3.6per mille to +8per mille with a mode of +1±1per mille. The δ 34 S of sulphides originating from within the mantle are variable. The sulphide globules with high Ni contents and δ 34 S values close to +3per mille, are probably produced by 10-20% partial melting of a mantle source containing 300 ppm sulphur as an upper limit and having a δ 34 S value of +0.5±0.5per mille. This difference in δ 34 S values suggests a high-temperature S-isotope fractionation of ≅+3per mille between liquid sulphide and the sulphur dissolved in the silicate liquid. The sulphur isotopes balance in the system upper mantle + oceanic crust + continental crust + seawater requires a mean δ 34 S value of the primitive upper mantle of +0.5per mille, slightly but significantly different from that of chondrites (+0.2±0.2per mille). (orig.)

  12. Quantifying trace elements in individual aquatic protist cells with a synchrotron x-ray fluorescence microprobe

    International Nuclear Information System (INIS)

    Twining, B.S.; Baines, S.B.; Fisher, N.S.; Maser, J.; Vogt, S.; Jacobsen, C.; Tovar-Sanchez, A.; Sanudo-Wihelmy, S.A.

    2003-01-01

    The study of trace metal cycling by aquatic protists is limited by current analytical techniques. Standard 'bulk' element analysis techniques that rely on physical separations to concentrate cells for analysis cannot separate cells from co-occurring detrital material or other cells of differing taxonomy or trophic function. Here we demonstrate the ability of a synchrotron-based X-ray fluorescence (SXRF) microprobe to quantify the elements Si, Mn, Fe, Ni, and Zn in individual aquatic protist cells. This technique distinguishes between different types of cells in an assemblage and between cells and other particulate matter. Under typical operating conditions, the minimum detection limits are 7.0 x 10 -16 mol μm -2 for Si and between 5.0 x 10 -20 and 3.9 x 10 -19 mol μm -2 for Mn, Fe, Ni, and Zn; this sensitivity is sufficient to detect these elements in cells from even the most pristine waters as demonstrated in phytoplankton cells collected from remote areas of the Southern Ocean. Replicate analyses of single cells produced variations of <5% for Si, Mn, Fe, and Zn and <10% for Ni. Comparative analyses of cultured phytoplankton cells generally show no significant differences in cellular metal concentrations measured with SXRF and standard bulk techniques (spectrophotometry and graphite furnace atomic absorption spectrometry). SXRF also produces two-dimensional maps of element distributions in cells, thereby providing information not available with other analytical approaches. This technique enables the accurate and precise measurement of trace metals in individual aquatic protists collected from natural environments.

  13. Electronic microscopy application in artificial minerals

    International Nuclear Information System (INIS)

    Gomez, L E.

    1995-07-01

    One of the uses of electronic microscopy in combination with the analysis microprobe EDAX is to characterize the properties of the minerals. The technique consist of studying the chemical composition by elements or by oxides of particles which can be enlarged successfully up to 100000x. With the help of the optical microscope one is able to determine the textual characteristics, the form, cleavage and other cristallographic properties which, combined with microprobe analysis enable one to determine its classification. The industrial processes which use ovens usually have problems due to the formation of impurities, spots and abnormal aspects which are reflected in a lower quality of the final material produced. These types of defects appear in minerals which are made in laboratories; knowing the natural minerals one can exercise a better quality control since this permits to know the behaviour of the raw material at a particular temperature and its reactions depending on the additives used

  14. Integration of a silicon-based microprobe into a gear measuring instrument for accurate measurement of micro gears

    International Nuclear Information System (INIS)

    Ferreira, N; Krah, T; Jeong, D C; Kniel, K; Härtig, F; Metz, D; Dietzel, A; Büttgenbach, S

    2014-01-01

    The integration of silicon micro probing systems into conventional gear measuring instruments (GMIs) allows fully automated measurements of external involute micro spur gears of normal modules smaller than 1 mm. This system, based on a silicon microprobe, has been developed and manufactured at the Institute for Microtechnology of the Technische Universität Braunschweig. The microprobe consists of a silicon sensor element and a stylus which is oriented perpendicularly to the sensor. The sensor is fabricated by means of silicon bulk micromachining. Its small dimensions of 6.5 mm × 6.5 mm allow compact mounting in a cartridge to facilitate the integration into a GMI. In this way, tactile measurements of 3D microstructures can be realized. To enable three-dimensional measurements with marginal forces, four Wheatstone bridges are built with diffused piezoresistors on the membrane of the sensor. On the reverse of the membrane, the stylus is glued perpendicularly to the sensor on a boss to transmit the probing forces to the sensor element during measurements. Sphere diameters smaller than 300 µm and shaft lengths of 5 mm as well as measurement forces from 10 µN enable the measurements of 3D microstructures. Such micro probing systems can be integrated into universal coordinate measuring machines and also into GMIs to extend their field of application. Practical measurements were carried out at the Physikalisch-Technische Bundesanstalt by qualifying the microprobes on a calibrated reference sphere to determine their sensitivity and their physical dimensions in volume. Following that, profile and helix measurements were carried out on a gear measurement standard with a module of 1 mm. The comparison of the measurements shows good agreement between the measurement values and the calibrated values. This result is a promising basis for the realization of smaller probe diameters for the tactile measurement of micro gears with smaller modules. (paper)

  15. Novel Magnetic Microprobe with Benzoboroxole-Modified Flexible Multisite Arm for High-Efficiency cis-Diol Biomolecule Detection.

    Science.gov (United States)

    Chen, Guosheng; Huang, Siming; Kou, Xiaoxue; Zhang, Jin'ge; Wang, Fuxin; Zhu, Fang; Ouyang, Gangfeng

    2018-03-06

    With regard to regulating a variety of biological events, including molecular recognition, signal transduction, cell adhesion, and immune response, cis-diol biomolecules, such as saccharides and glycoproteins, play vital roles. However, saccharides and glycoproteins in living systems usually exist in very low abundance, along with abundant interfering components. High-efficiency detection of saccharides and glycoproteins is a challenging yet highly impactful area of research. Herein, we reported a novel magnetic microprobe with a benzoboroxole-modified flexible multisite arm (PEG 2000-grafted PAMAM dendrimers; the microprobe was denoted as BFMA-MNP) for high-efficiency saccharides detection. The extraction capacity was significantly improved by ∼2 orders of magnitude, because of the integration of the enhanced hydrophilicity and multivalency effects in benzoboroxoles and the enhanced accessibility of the binding sites within the PEG 2000-grafted PAMAM dendrimers. As a result, the proposed approach possessed several advantages, compared with previous boronic acid-based methods, including ultrahigh sensitivity (limit of detection was <1 ng/mL), wide linear range (ranged from 0.5 μM to 2000 μM), and applicable in physiological pH condition. Furthermore, we established a general BFMA-MNP/glycoproteins/AuNPs sandwich assay to realize the visual glycoprotein qualitative screening for the first time. The unique sandwich assay possessed the dual nature of the magnetic separation by BFMA-MNPs and specific coloration by citrate-coated AuNPs. This visual sandwich assay enabled fast differentiation of the existence of glycoproteins in complicated samples without any advanced instruments. We believe the proposed BFMA-MNP microprobe herein will advance the ideas to detect and identify trace saccharides and glycoproteins in important fields such as glycomics and glycoproteomics.

  16. Preliminary study of Tl and Cd uptake in the heavy metal accumulating Brassica napus using the Debrecen proton microprobe

    International Nuclear Information System (INIS)

    Kertesz, Zs.; Haag-Kerwer, A.; Povh, B.

    2003-01-01

    The high biomass producing crop plants, Brassica juncea L. and Brassica napus are very promising plant species for phytoremediation. The aim of further research is to help a better understanding of the transport mechanism within roots and roots to shoots of heavy metals, and to find out their distribution and translocation among different cell types in the root of these species. The distribution and concentration of major and trace elements was determined along the roots of Cd and Tl treated as well as control plants of Brassica napus on the ATOMKI proton microprobe. (R.P.)

  17. Application of the nuclear microprobe to the study of organic and inorganic composition of teeth irradiated by a laser beam

    International Nuclear Information System (INIS)

    Sommer, F.; Engelmann, Ch.; Couble, Ml.; Magloire, H.; Bonnin, P.

    1986-01-01

    The nuclear microprobe uses both direct observation of nuclear reactions induced by deuterons and X ray emission induced by protons or deuterons. Thanks to these techniques, concentration profiles of the main elements (C, N, P, Ca...) contained in different parts of healthy teeth (enamel, dentine and cementum) are drawn in control zones and laser irradiated zones. The results obtained show that important perturbations appear during the irradiation by the laser beam; we observe successively, depleted zones in carbon and nitrogen which contain calcium and phosphorus and hypomineralized zones which contain organic material. 10 refs [fr

  18. Redeposition of sputtered material in a glow-discharge lamp measured by means of an ion microprobe mass analyser

    International Nuclear Information System (INIS)

    Ferreira, N.P.; Bueger, P.A.

    1978-01-01

    The redeposition of sputtered material on the target in a Grimm-type glow-discharge lamp was studied by means of an ion microprobe mass analyser (IMMA) using 16 O 2 + ions as bombarding species. The target was an aluminium disc with a cylindrical copper insertion, one mm in diameter. The lamp was operated at currents of 50 mA and 100 mA and a voltage of 1200 V. It is estimated that 17% of the copper atoms sputtered are redeposited and may be resputtered. (orig.) [de

  19. Evolution of the Gondwanaland Archaean Shield: ion microprobe zircon dating and southwestern Australia/Wilkes Land, Antartica

    International Nuclear Information System (INIS)

    Lovering, J.F.; Comaford, D.J.

    1979-01-01

    The ion microprobe has been used to study 207 Pb/ 206 Pb ages on 20μm-sized sites on single zircon grains from coastal rocks on either side of the rift in the Gondwanaland Archaean Shield between southwestern Australia and Wilkes Land, Antarctica. The ages on individual sites on zircon grains from a variety of rock types from southwestern Australia show a range from 1600 m.y. to about 3400 m.y., with an inverse dependence on the uranium abundance at each site. Ages of zircons from rocks from the Antartic region show a range from 1600 m.y. to 3100 m.y

  20. Pequenos para idade gestacional: fator de risco para mortalidade neonatal Small for gestational age

    Directory of Open Access Journals (Sweden)

    Márcia Furquim de Almeida

    1998-06-01

    Full Text Available OBJETIVO: Estudar as variáveis contempladas na Declaração de Nascimento (DN como possíveis fatores de risco para nascimentos pequenos para a idade gestacional (PIG e o retardo de crescimento intra-uterino como fator de risco para a mortalidade neonatal. MATERIAL E MÉTODO: As variáveis existentes na DN foram obtidas diretamente de prontuários hospitalares. Os dados referem-se a uma coorte de nascimentos obtida por meio da vinculação das declarações de nascimento e óbito, correspondendo a 2.251 nascimentos vivos hospitalares, de mães residentes, ocorridos no Município de Santo André, Região Metropolitana de São Paulo, no período de l/1 a 30/6/1992, e aos óbitos neonatais verificados nessa coorte. RESULTADOS: Obteve-se a proporção de 4,3% de nascimentos PIG, significativamente maior entre os recém-nascidos de pré-termo e pós-termo, entre os nascimentos cujas mães tinham mais de 35 anos de idade e grau de instrução inferior ao primeiro grau completo. Os recém-nascidos PIG apresentam maior risco de morte neonatal que aqueles que não apresentavam sinais de retardo de crescimento intra-uterino. CONCLUSÕES: Em áreas com menor freqüência de baixo peso ao nascer, é importante investigar a presença de retardo de crescimento intra-uterino entre os nascimentos prematuros e não apenas nos nascimentos de termo. O registro da data da última menstruação (ou da idade gestacional em semanas não agregadas na DN facilitaria a detecção de PIGs na população de recém-nascidos.INTRODUCTION: Variables of birth certificates were analysed as risk factors of SGA (Small for Gestational Age infantis, and with a view to discovering if retarded intra-uterine growth was a risk factor neonatal mortality. MATERIAL AND METHOD: Data were obtained directly from 11 hospital medical records. A cohort of 2.251 hospital live births was obtained. Linkage of the death and birth certificates was undertaken to identify the neonatal deaths. The

  1. CONCH: A Visual Basic program for interactive processing of ion-microprobe analytical data

    Science.gov (United States)

    Nelson, David R.

    2006-11-01

    A Visual Basic program for flexible, interactive processing of ion-microprobe data acquired for quantitative trace element, 26Al- 26Mg, 53Mn- 53Cr, 60Fe- 60Ni and U-Th-Pb geochronology applications is described. Default but editable run-tables enable software identification of secondary ion species analyzed and for characterization of the standard used. Counts obtained for each species may be displayed in plots against analysis time and edited interactively. Count outliers can be automatically identified via a set of editable count-rejection criteria and displayed for assessment. Standard analyses are distinguished from Unknowns by matching of the analysis label with a string specified in the Set-up dialog, and processed separately. A generalized routine writes background-corrected count rates, ratios and uncertainties, plus weighted means and uncertainties for Standards and Unknowns, to a spreadsheet that may be saved as a text-delimited file. Specialized routines process trace-element concentration, 26Al- 26Mg, 53Mn- 53Cr, 60Fe- 60Ni, and Th-U disequilibrium analysis types, and U-Th-Pb isotopic data obtained for zircon, titanite, perovskite, monazite, xenotime and baddeleyite. Correction to measured Pb-isotopic, Pb/U and Pb/Th ratios for the presence of common Pb may be made using measured 204Pb counts, or the 207Pb or 208Pb counts following subtraction from these of the radiogenic component. Common-Pb corrections may be made automatically, using a (user-specified) common-Pb isotopic composition appropriate for that on the sample surface, or for that incorporated within the mineral at the time of its crystallization, depending on whether the 204Pb count rate determined for the Unknown is substantially higher than the average 204Pb count rate for all session standards. Pb/U inter-element fractionation corrections are determined using an interactive log e-log e plot of common-Pb corrected 206Pb/ 238U ratios against any nominated fractionation-sensitive species pair

  2. Efeito idade-periodo-coorte na mortalidade por cancer do colo uterino

    Directory of Open Access Journals (Sweden)

    Karina Cardoso Meira

    2013-06-01

    Full Text Available OBJETIVO: Estimar o efeito da idade, período e coorte de nascimento na mortalidade por câncer do colo do útero. MÉTODOS: Foram analisados dados de mortalidade por câncer do colo do útero em mulheres ≥ 30 anos nos municípios do Rio de Janeiro, RJ, e São Paulo, SP, de 1980 a 2009. Os dados foram extraídos do Sistema de Informação Sobre Mortalidade. A variação percentual anual estimada foi calculada para os períodos de 1980-1994 e 1995-2009. O efeito da idade, período e coorte de nascimento foi calculado pelo modelo de regressão de Poisson, utilizando funções estimáveis: desvios, curvaturas e drift , por meio da biblioteca Epi do programa estatístico R versão 2.7.2. RESULTADOS: A taxa de mortalidade média do período por 100.000 mulheres foi 15,90 no Rio de Janeiro e 15,87 em São Paulo. Houve redução significativa na mortalidade por câncer do colo do útero nos dois períodos: no Rio de Janeiro, -1,20% (IC95% -2,20;-0,09 e -1,46% (IC95% -2,30;-0,61, e em São Paulo, -2,58% (IC95% -3,41;-1,76 e -3,30% (IC95% -4,30;-2,29. A análise da curvatura dos efeitos indicou tendência de redução do risco de morte nas sucessivas coortes (RR < 1 nas mulheres nascidas após a década de 1960. Observou-se redução acentuada no risco relativo (RR a partir dos anos 2000. CONCLUSÕES: O estudo evidenciou efeito de período na redução das taxas de mortalidade por câncer do colo do útero no período analisado, tendo em vista que houve efeito de proteção (RR < 1 a partir dos anos 2000 e nas mulheres nascidas após a década de 1960.

  3. Bipolar disorder and age-related functional impairment Prejuízo funcional associado à idade e transtorno bipolar

    Directory of Open Access Journals (Sweden)

    Alice Aita Cacilhas

    2009-12-01

    Full Text Available OBJECTIVE: Although bipolar disorder is a major contributor to functional impairment worldwide, an independent impact of bipolar disorder and ageing on functioning has yet to be demonstrated. The objective of the present study was to evaluate the effect of bipolar disorder on age-related functional status using matched controls as a standard. METHOD: One-hundred patients with bipolar disorder and matched controls were evaluated for disability. Age-related effects controlled for confounders were cross-sectionally evaluated. RESULTS: Patients were significantly more impaired than controls. Regression showed effects for aging in both groups. The effect, size, however, was significantly stronger in patients. CONCLUSION: Bipolar disorder was an important effect modifier of the age impact on functioning. While a longitudinal design is needed to effectively demonstrate this different impact, this study further depicts bipolar disorder as a chronic and progressively impairing illness.OBJETIVO: O transtorno bipolar é responsável por importante parcela do prejuízo funcional ao redor do mundo. Um efeito independente do transtorno bipolar e da idade no funcionamento ainda não foi demonstrado. O presente estudo tem o objetivo de avaliar o efeito do transtorno bipolar no prejuízo funcional relacionado à idade, com controles pareados como padrão. MÉTODO: Cem pacientes com transtorno bipolar e controles pareados foram avaliados para incapacidade. Efeitos relacionados à idade, com controle para confundidores, foram investigados. RESULTADOS: Pacientes tiveram significativamente mais prejuízo que controles. A regressão mostrou efeito para a idade em ambos os grupos, e o efeito foi significativamente mais forte nos pacientes. CONCLUSÃO: O transtorno bipolar foi um importante modificador de efeito no impacto da idade no funcionamento. Enquanto um desenho de estudo longitudinal é necessário para efetivamente demonstrar este impacto diferencial, este

  4. CARACTERÍSTICAS ESTRUTURAIS DA MADEIRA DE Pinus elliottii Engelm AOS 30 ANOS DE IDADE

    Directory of Open Access Journals (Sweden)

    Clovis Roberto Haselein

    2000-09-01

    Full Text Available No presente estudo, seis árvores de um povoamento de Pinus elliottii com 30 anos de idade foram coletadas e transformadas em toras de 2,5 m de comprimento. De cada uma das duas primeiras toras, retirou-se um pranchão central, do qual foram confeccionados, segundo a norma ASTM D143-93 (1995, nas regiões próximas à medula e à casca, os corpos de prova utilizados nos ensaios de flexão estática. As propriedades de flexão (módulos de elasticidade e de ruptura e massa específica básica a 12% de umidade foram relacionados como número de anéis de crescimento e a porcentagem de lenho tardio determinados na secção transversal para cada corpo de prova. Os resultados evidenciaram, para as propriedades estudadas, a existência de diferenças significativas entre as posições.

  5. Idade: A manifestação de Cronos nos jornais paulistanos

    Directory of Open Access Journals (Sweden)

    Maria Helena Villas Bôas Concone

    2010-02-01

    Full Text Available A leitura dos recortes de jornais analisados nos trouxe à lembrança o pequeno livro O Papalagui. O livrinho traz as muitas reflexões de Tuiávii, dentre as quais aquelas sobre o modo pelo qual o “branco” (o Papalagui lida com o tempo. Os comentários do chefe de Tiavéa acusam a preocupação “ocidental” com o tempo, como uma espécie de compulsão e de urgência, quando não de loucura: o tempo é dividido, demarcado, contado, reificado, usado; de fato, Tuiávii faz uma distinção entre o usufruir do tempo e o usar o tempo num sentido utilitário. Palavras-chave: Tempo; Cronos; Jornais paulistas; Idade Age: The manifestation of Chronos in Sao Paulo newspapers ABSTRACT: The reading of newspaper clippings analyzed brought to our mind the small book The Papalagui. The book includes the many reflections of Tuiavii, among which there are those on the way in which the “white” (the Papalagui deals with time. The comments from the Tiavea chief accuse “western” concern with time as a kind of compulsion and urgency, if not madness: the time is divided, marked, counted, objectified, used actually. Tuiavii distinguishes between enjoying time and using time in a utilitarian sense. Keywords: Time; Chronos; Sao Paulo newspapers; Age

  6. Os efeitos da idade na seleção de carga perceptual

    Directory of Open Access Journals (Sweden)

    Vanessa Coelho de Sousa

    Full Text Available Algumas pesquisas sugerem a existência de momentos distintos de maturação do sistema atentivo. O presente estudo investigou os padrões de seleção da informação visual através de uma tarefa de carga perceptual executada por três grupos etários: crianças, adultos e idosos. De maneira geral os resultados obtidos indicaram uma diminuição da eficiência no processo de seleção da informação em condições de baixa carga perceptual na população de idosos e uma diminuição da eficiência da seleção em condições de alta e baixa carga perceptual na população composta por crianças. Estes resultados sugerem a existência de padrões específicos na seleção da informação visual em função da idade e da carga perceptual a ser processada pelo sistema visual.

  7. O grupo como fator de inclusão socioafetiva na terceira idade

    Directory of Open Access Journals (Sweden)

    Alexandra Cardoso da Silva

    2013-09-01

    Full Text Available http://dx.doi.org/10.5007/1807-0221.2013v10n15p44 O objetivo deste trabalho é o de demonstrar que a Dinâmica de Grupos - Grupo de Encontros Rogeriano - é fator de interação social na Terceira Idade, promovendo a integração dos idosos em grupos substitutivos devolvendo-lhes a auto-estima e cidadania. A experiência foi realizada no NETI / UFSC, com vários grupos a partir de 2001. Efetuaram-se 30 encontros com duração de duas horas cada sessão, ministrado por 2 facilitadoras . Como conclusão constatou-se que existe um processo adaptativo na velhice estimulando a formação dessas mudanças é multidimensional: a área emcional facilita a expressão dos sentimentos positivos; na cognitiva estimula aprendizagens relativas ao seu Eu e ao dos Outros; na comportamental á competência pessoal e social.

  8. Curva dos valores normais de peso fetal estimado por ultra-sonografia segundo a idade gestacional

    Directory of Open Access Journals (Sweden)

    José Guilherme Cecatti

    Full Text Available Este trabalho teve por objetivo avaliar a evolução do peso fetal estimado em gestações normais de 20 a 42 semanas. Quanto ao desenho e métodos empregados na pesquisa, realizou-se estudo descritivo de um universo constituído por 2.874 gestantes normais da cidade de Campinas, efetuando-se exame ultra-sonográfico obstétrico de rotina com medida da biometria fetal e utilizando-se, para o cálculo do peso fetal, a fórmula de Hadlock et al. (1991. Calcularam-se os valores dos percentis 10, 50 e 90 do peso fetal, por idade gestacional, com construção de curva posteriormente alisada mediante ajuste polinomial de 2º grau. Como resultado, obteve-se que o valor do percentil 50 foi de 368 gramas na 20ª semana, 1.512 gramas na 30ª semana, atingindo 3.417 gramas na 42ª semana. Constatou-se ter havido ganho médio de 200 gramas de peso por semana, de 27 a 38 semanas, a partir de quando o incremento diminuiu. Concluiu-se que a disponibilidade de curva brasileira do peso fetal estimado normal permitirá o diagnóstico pré-natal de seus desvios pela ultra-sonografia.

  9. Application of PIXE analysis to environmental samples stable element distribution in sea algae by scanning microprobe analysis

    International Nuclear Information System (INIS)

    Ishikawa, M.; Kitao, K.; Imaseki, H.; Ishii, T.; Uchida, S.

    1984-01-01

    The resolution of a 33+-3 μm microprobe focussed with quadrupole doublet installed at the 3 MV Van de Graaff of the National Institute of Radiological Sciences, Japan, was used for the present analysis. Brown algae, Hizikia fusiforme was the sample target bombarded with a 2 MeV proton beam collimated mechanically into a rectangular image of 100 μm x 700 μm. Scanning across the sample target prepared into a longitudinal section from the caulis of the algae provided the following observations. More than 12 elements such as Al, Si, P, Cl, Ca, Mn, Fe, Cu, Zn, As, Br and Sr were determined simultaneously, together with their distributional information across the diameter. In the medullary layer, Mn and Zn were specific in their accumulation, while the deposition of Fe, Cu, As and Br were observed to be high in the epithelial layer, especially Fe and Cu which were found on the surface, where they contacted ambient sea water, but no significant change in pattern was indicated for such elements as Al, P and Cl. The PIXE microprobe analysis was, therefore, effective in its detectability for elements below a few ppm level, resultantly providing further possibilities for collecting information from bio-medical and environmental samples on trace characterization of elements. (author)

  10. Contribution to the application of nuclear microprobe in geochemistry. Carbon and nitrogen microanalysis in glasses and minerals

    International Nuclear Information System (INIS)

    Mosbah, M.

    1988-01-01

    The morphological complexity of geological materials implies the use of microanalysis techniques utilization. Nuclear microprobe allows selective and no destructive light elements determination, through nuclear reactions. Nuclear microanalysis has been used to characterize carbon and nitrogen in volatile phase dissolved in magmatic samples. The application of some microanalysis techniques in geochemistry are discussed, nuclear microprobe theory and techniques are developed. Minerals, glasses and glassy inclusions are described, and more particularly, the interest of these investigations. Optimal conditions of carbon and nitrogen analysis ( 12 C(d.p) 13 C and 14 N(d,p) 15 N reaction respectively), as deuteron energy and observation angle are studied. A methodology has been established for this purpose. Several results are exposed: Punctual analysis, carbon concentration profile in depth surface scanning, surficial mapping in glassy inclusions. The carbon content interpretation in glassy inclusions measured conveniently for the first time agrees with data obtained through other techniques. In conclusion, degazing schedule improvements require more analysis. Perspective research axis are evocated [fr

  11. Quantification and localization of trace metals in natural plankton using a synchrotron x-ray fluorescence microprobe

    International Nuclear Information System (INIS)

    Twining, B. S.; Baines, S. B.; Fisher, N. S.; Jacobsen, C.; Maser, J.; State Univ. of New York at Stony Brook

    2003-01-01

    The accumulation of trace metals by planktonic protists influences the growth of primary producers, metal biogeochemical cycling, and metal bioaccumulation in aquatic food chains. Despite their importance, unequivocal measurements of trace element concentrations in individual plankton cells have not been possible to date. We have used the 2-ID-E side-branch hard x-ray microprobe at the Advanced Photon Source to measure trace elements in individual marine plankton cells. This microprobe employs zoneplate optics to produce the sub-micron spatial resolution and low background fluorescence required to produce trace element maps of planktonic protist cells ranging in size from 3 to >50 (micro)m. We have developed preservation, rinsing, and mounting protocols that remove most of the salt from our marine samples, thus simplifying the identification of unknown cells and reducing high Cl-related background fluorescence. We have also developed spectral modeling techniques that account for the frequent overlap of adjacent fluorescence peaks and non-uniform detector response. Finally, we have used parallel soft x-ray transmission and epifluorescence microscopy images to estimate C normalized trace element concentrations, identify functional cell types (e.g., photosynthetic vs. non-photosynthetic), and correlate cell structures with spatial patterns in trace element fluorescence

  12. Quantification and localization of trace metals in natural plancton using a synchrotron x-ray fluorescence microprobe.

    Energy Technology Data Exchange (ETDEWEB)

    Twining, B. S.; Baines, S. B.; Fisher, N. S.; Jacobsen, C.; Maser, J.; State Univ. of New York at Stony Brook

    2003-03-01

    The accumulation of trace metals by planktonic protists influences the growth of primary producers, metal biogeochemical cycling, and metal bioaccumulation in aquatic food chains. Despite their importance, unequivocal measurements of trace element concentrations in individual plankton cells have not been possible to date. We have used the 2-ID-E side-branch hard x-ray microprobe at the Advanced Photon Source to measure trace elements in individual marine plankton cells. This microprobe employs zoneplate optics to produce the sub-micron spatial resolution and low background fluorescence required to produce trace element maps of planktonic protist cells ranging in size from 3 to >50 {micro}m. We have developed preservation, rinsing, and mounting protocols that remove most of the salt from our marine samples, thus simplifying the identification of unknown cells and reducing high Cl-related background fluorescence. We have also developed spectral modeling techniques that account for the frequent overlap of adjacent fluorescence peaks and non-uniform detector response. Finally, we have used parallel soft x-ray transmission and epifluorescence microscopy images to estimate C normalized trace element concentrations, identify functional cell types (e.g., photosynthetic vs. non-photosynthetic), and correlate cell structures with spatial patterns in trace element fluorescence.

  13. Optically continuous silcrete quartz cements of the St. Peter Sandstone: High precision oxygen isotope analysis by ion microprobe

    Science.gov (United States)

    Kelly, Jacque L.; Fu, Bin; Kita, Noriko T.; Valley, John W.

    2007-08-01

    A detailed oxygen isotope study of detrital quartz and authigenic quartz overgrowths from shallowly buried (ratio by laser fluorination, resulting in an average δ 18O of 10.0 ± 0.2‰ (1SD, n = 109). Twelve thin sections were analyzed by CAMECA-1280 ion microprobe (6-10 μm spot size, analytical precision better than ±0.2‰, 1SD). Detrital quartz grains have an average δ 18O of 10.0 ± 1.4‰ (1SD, n = 91) identical to the data obtained by laser fluorination. The ion microprobe data reveal true variability that is otherwise lost by homogenization of powdered samples necessary for laser fluorination. Laser fluorination uses samples that are one million times larger than the ion microprobe. Whole rock (WR) samples from the 53 rocks were analyzed by laser fluorination, giving δ 18O between 9.8‰ and 16.7‰ ( n = 110). Quartz overgrowths in thin sections from 10 rocks were analyzed by ion microprobe and average δ 18O = 29.3 ± 1.0‰ (1SD, n = 161). Given the similarity, on average, of δ 18O for all detrital quartz grains and for all quartz overgrowths, samples with higher δ 18O(WR) values can be shown to have more cement. The quartz cement in the 53 rocks, calculated by mass balance, varies from outlier at 33 vol.% cement. Eolian samples have an average of 11% cement compared to marine samples, which average 4% cement. Two models for quartz cementation have been investigated: high temperature (50-110 °C) formation from ore-forming brines related to Mississippi Valley Type (MVT) mineralization and formation as silcretes at low temperature (10-30 °C). The homogeneity of δ 18O for quartz overgrowths determined by ion microprobe rules out a systematic regional variation of temperature as predicted for MVT brines and there are no other known heating events in these sediments that were never buried to depths >1 km. The data in this study suggest that quartz overgrowths formed as silcretes in the St. Peter Sandstone from meteoric water with δ 18O values of -10

  14. Imagem corporal em mulheres adultas vs. meia-idade e idosas praticantes e não praticantes de hidroginástica

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    Simone Valéria Dias Souto

    2016-06-01

    Full Text Available O objetivo do presente estudo foi comparar a imagem corporal de mulheres adultas vs. meia-idade e idosas praticantes e não praticantes de hidroginástica. A amostra foi constituída por 300 mulheres brasileiras com idades compreendidas entre 20 e 83 anos (48.96 ± 15.41, divididas em quatro grupos: Grupo 1 = 75 mulheres adultas não praticantes com idades entre 20 e 49 anos; Grupo 2 = 75 mulheres de meia-idade e idosas não praticantes com idades entre 50 e 82 anos; Grupo 3 = 75 mulheres de meia-idade e idosas praticantes com idade entre 50 e 83 anos e Grupo 4 = 75 mulheres adultas praticantes com idade entre 20 e 49 anos. O instrumento utilizado para determinar à imagem corporal actual e desejada foi a Escala de Desenhos de Silhuetas descrita por Stunkard. Os resultados demonstram que não houve diferenças significativas com a insatisfação da imagem corporal entre os grupos de mulheres adultas vs. meia-idade e idosas vs. praticantes vs. não praticantes (p>0.05. Entretanto, houve diferenças significativas entre a insatisfação com a imagem corporal actual vs. ideal para todos os grupos do estudo (p<0.05. Conclui-se que a idade e a prática da hidroginástica não são factores determinantes na percepção que as mulheres têm da imagem corporal.

  15. Isotopic Investigations of Nebular and Parent Body Processes with a High Sensitivity Ion Microprobe

    Science.gov (United States)

    McKeegan, Kevin D.

    2005-01-01

    NASA supported the development of the CAMECA ims 1270 ion microprobe at UCLA for applications in cosmochemistry. The primary investigations centered on measuring the microscopic distributions of key isotopic abundances in primitive meteoritic materials as a means of constraining the nature of important thermal and chemical processes in the solar nebula and the timescales associated with those processes. Our prior work on oxygen isotope anomalies in a wide variety of meteoritic materials had led us to a view of a spatially heterogeneous nebula, and in particular, a restricted region for CAI formation that is characterized by O-16-rich gas. Because of its production of CAIs in the energetic local environment near the protosun, the existence of a natural transport mechanism via bipolar outflows, and a general astrophysical plausibility, we were attracted to the fluctuating X-wind model which had been put forward by Frank Shu, Typhoon Lee, and colleagues. With our collaborators, we undertook a series of investigations to test the viability of this hypothesis; this work led directly to the discovery of live Be in CAIs and a clear demonstration of the existence of 160-rich condensates, which necessarily implies an O-16-rich gaseous reservoir in the nebula. Both of these observations fit well within the context of X-wind type models, i.e. formation of CAIs (or condensation of their precursors) in the reconnection ring sunward of the inner edge of the accretion disk, however much work remains to be done to test whether the physical parameters of the model can quantitatively predict not only the thermal histories of CAIs but also their radioactivity. The issue of spatial heterogeneity in the nebula, central to the X-wind model, is also at the heart of any chronology based on short-lived radioisotopes. In this work, we followed up on strong hints for presence of exireme:j: (53 day) short-lived Be-7, and have prepared a manuscript (in revision). We also measured A1-Mg

  16. The bio-PIXE setup on the Debrecen scanning proton microprobe

    International Nuclear Information System (INIS)

    Kertesz, Zs.; Szikszai, Z.; Uzonyi, I.; Simon, A.; Kiss, A.Z.

    2004-01-01

    Complete text of publication follows. Besides the ongoing applications in archeometry, geology, material science and atmospheric aerosol study, in recent years the IBA Group in Debrecen has joined several biological and biomedical research projects. Such studies require the knowledge of accurate quantitative elemental concentrations and distributions in organic, inhomogeneous thin samples on a microscopic scale. In most cases, to carry out quantitative investigations on biomedical samples down to the cell level, the combination of proton induced X-ray emission (PIXE), Rutherford backscattering (RBS) spectrometry and scanning transmission ion microscopy (STIM) analytical methods are used simultaneously. STIM provides information on the density and structure of the sample, PIXE measures the concentration of the inorganic major and trace elements, and finally RBS serves to characterize the organic matrix, to determine the beam dose, and sometimes the sample thickness. The drawback of this combined method is that to evaluate the RBS data the hydrogen to carbon ratio in the sample must be known. The setup developed at the Debrecen microprobe facility [1] is based on the combined application of on-axis STIM and simultaneous PIXE-PIXE analytical techniques. In the PIXE-PIXE method the sample matrix is determined directly by measuring X-rays from all elements in the sample including the light elements such as carbon and oxygen, using two Si(Li) X-ray detectors. In this arrangement an ultra thin windowed Si(Li) X-ray detector serves to characterize the matrix by measuring low energy X-ray lines (0.2-9 keV) while a large area Be-windowed detector is used to detect the medium and high energy X-ray lines (>4 keV). In this way elements with atomic number higher than 5 can be detected simultaneously, reducing both radiation damage of the sample and measurement time. In addition, the knowledge of the hydrogen content of the sample is not needed, since it influences the

  17. Análise química do bambu-gigante (Dendrocalamus giganteus Wall. ex Munro em diferentes idades

    Directory of Open Access Journals (Sweden)

    Nelson Potenciano Marinho

    2012-06-01

    Full Text Available http://dx.doi.org/10.5902/198050985749O bambu é uma planta monocotiledônea de origem tropical, de rápido crescimento, sendo considerado um importante regenerador ambiental devido ao seu sistema radicular. O Dendrocalamus giganteus é popularmente conhecido por bambu-gigante, sendo uma espécie entouceirante de grande porte, cujos colmos podem variar de 24 a 40 metros de altura, com diâmetros entre 10 e 20 cm. Esse trabalho teve como objetivo analisar quimicamente os colmos do bambu-gigante visando fornecer informações sobre a sua composição química nas idades de 2 a 6 anos. Os colmos do bambu foram coletados na área Experimental Agrícola do Departamento de Engenharia Mecânica da UNESP-Bauru, onde é realizado o manejo sistemático de diversas espécies de bambu para fins de pesquisas e divulgação dessa planta. Foram retiradas amostras da base entre bambus com idade de 2 a 6 anos de uma mesma touceira, totalizando 5 amostras, com 2 metros de altura cada, colhidas na lua minguante no mês de março. As análises químicas foram feitas com os entrenós, utilizando as normas e procedimentos da TAPPI. A porcentagem média de extrativos em água quente, extrativos em água fria, extrativos totais e teor de cinzas não apresentaram relação direta com a idade. A maior porcentagem de extrativos em água quente, com valor de 12,04%, extrativos em água fria, com 10,25%, e extrativos totais, com 12,91%, foi observada aos 2 anos de idade. A maior porcentagem de cinzas foi obtida aos três anos, com valores de 1,09%. O teor médio de extrativos em NaOH diminui de 25,72% aos dois anos para 20,17% aos seis anos de idade. O mesmo comportamento foi observado para os extrativos em etanol tolueno, diminuindo de 10,91% para 4,61%. O teor médio de lignina não sofreu influência da idade, variando de 22,66 a 24,11%.

  18. Interferência da idade sobre a qualidade seminal Interference of age on semen quality

    Directory of Open Access Journals (Sweden)

    Marcelo Borges Cavalcante

    2008-11-01

    Full Text Available OBJETIVO: avaliar a influência da idade sobre a qualidade seminal de homens com quadro de infertilidade conjugal submetidos a análises espermáticas em um serviço de reprodução humana. MÉTODOS: estudo retrospectivo, no qual foram avaliados os espermogramas de todos os homens em processo de investigação para infertilidade conjugal no período de Setembro de 2002 a Dezembro de 2004, em um serviço de reprodução assistida do nordeste do Brasil. Foram incluídos 531 indivíduos submetidos a 531 avaliações espermáticas. Foram analisados os seguintes parâmetros: volume, concentração, motilidade e morfologia espermática. O total de investigados foi dividido em grupos, de acordo com resultados obtidos de cada variável estudada. Os grupos referentes ao volume seminal foram: hipoespermia, normoespermia e hiperespermia. Os grupos referentes à concentração espermática foram: azoospermia, oligoospermia, normospermia e poliespermia. Os grupos referentes à motilidade foram: motilidade normal e astenospermia. Os grupos referentes à morfologia foram: morfologia normal e teratospermia. As médias das idades dos pacientes entre os grupos com parâmetros normais foram comparadas com as de grupos alterados, sendo utilizado o teste t. Para análise estatística, foi utilizado o programa XLSTAT (pPURPOSE: to evaluate the influence of age on the quality of semen in men submitted to spermatic analysis in a human reproduction service, in cases of conjugal infertility. METHODS: a retrospective study in which the spermiograms of all men in process of investigation for conjugal infertility in a service of assisted reproduction in the Northeast of Brazil were evaluated from September 2002 to December 2004. A number of 531 individuals submitted to 531 spermatic evaluations were included in the study. The following parameters have been analyzed: spermatic volume, concentration, motility and morphology. The men under investigation have been divided in

  19. Transtorno de personalidade na terceira idade Personality disorders in an elderly patient

    Directory of Open Access Journals (Sweden)

    Fernanda Speggiorin Pereira

    2007-01-01

    Full Text Available CONTEXTO: Dificuldades interpessoais, instabilidade afetiva, distorções da relação médico-paciente e respostas imprevisíveis às intervenções são características centrais aos transtornos de personalidade que são encontradas tanto em pacientes jovens, como em adultos idosos. RELATO DE CASO: Encontra-se aqui descrito um caso de transtorno de personalidade em paciente de 68 anos de idade, com transtorno de personalidade do tipo histriônica e outras comorbidades psiquiátricas. CONCLUSÃO: Transtorno de personalidade é um diagnóstico raramente aventado no tratamento psiquiátrico no paciente idoso de difícil manejo. Deve-se nestes casos fazer uma investigação mais aprofundada do funcionamento da personalidade, pois a presença e a severidade do transtorno de personalidade têm implicações no plano da assistência de ambos os tratamentos psicológico e farmacológico.CONTEXT: Interpersonal difficulties, affective instability, distortions of the clinician-patient relationship, and unpredictable responses to clinical interventions, are characteristics found in older adults as well as in younger patients with personality disorders. CASE REPORT: We report the case of a 68 years old patient with histrionic personality disorder and other psychiatric comorbidities. CONCLUSION: Personality disorders are frequently overlooked in the diagnostic workout of complex psychogeriatric syndromes, and require a comprehensive assessment of personality traits. The correct identification of personality disorders and their subtypes is critical for planning the therapeutic approach, including pharmacotherapy and psychological management.

  20. Estilos parentais e compreensão emocional de crianças em idade pré-escolar

    OpenAIRE

    Sá, Vanessa

    2017-01-01

    A compreensão emocional, bem como, a comunicação das emoções são competências relevantes na idade pré-escolar, com impacto em diversas áreas do desenvolvimento. Nestas idades, os Estilos Parentais adotados pela mãe e pelo pai podem assumir um papel central nas experiências das crianças ao nível emocional, nomeadamente, no auto-conhecimento, auto-regulação e no ajuste das suas interações com os outros. Neste sentido, analisou-se as relações entre os estilos parentais e a compree...

  1. The role of nuclear microprobes in the study of technology, provenance and corrosion of cultural heritage: The case of gold and silver items

    International Nuclear Information System (INIS)

    Guerra, M.F.; Tissot, I.

    2013-01-01

    This work gives an overview of the main questions raised by gold and silver items kept in museum collections and of the role of nuclear microprobes in their study and conservation. The different approached questions are illustrated by examples; analytical data is given and discussed; and the advantages of IBA are considered: spatial resolution, penetration depth, limits of detection, mapping, etc

  2. Ion microprobe analyses of oxygen three-isotope ratios of chondrules from the Sayh al Uhaymir 290 CH chondrite using a multiple-hole disk

    Digital Repository Service at National Institute of Oceanography (India)

    Nakashima, D.; Ushikubo, T.; Gowda, R.N.; Kita, N.T.; Valley, J.W.; Naga, K.

    Author version: Meteorit. Planet. Sci., vol.46(6); 2011; 857-874 Ion microprobe analyses of oxygen three isotope ratios of chondrules from the Sayh al Uhaymir 290 CH chondrite using a multiple-hole disk Daisuke Nakashima 1,2,* , Takayuki Ushikubo...

  3. Estimular o empreendedorismo na terceira idade DOI:10.5007/1807-0221.2011v8n12p109

    Directory of Open Access Journals (Sweden)

    Ana Lucia Ferraresi Schmitz

    2011-12-01

    Full Text Available O artigo aborda um estudo de caso com pessoas da terceira idade inseridas no Programa do Núcleo de Estudos da Terceira Idade da Universidade Federal de Santa Catarina (NETI/UFSC. O estudo foi realizado entre os anos 2008 e 2009 e contou com 24 participantes. Objetivou despertar capacidades empreendedoras nos participantes, a partir de suas habilidades pessoais, por meio da aplicação de aulas participativas, visando ao aprimoramento da teoria e da prática empreendedora na terceira idade. Os métodos utilizados passaram por adaptações necessárias para o tipo de público, incluindo aulas expositivas, projeção de vídeos e dinâmicas vivenciais. O resultado foi alcançado, tendo em vista a avaliação positiva feita pelos participantes no questionário aplicado no início e no final das atividades didáticas de cada curso. Evidenciou-se a importância do estímulo para o empreendedorismo nessa faixa etária, visto que os participantes apresentaram alteração das atitudes de participação e predisposição para a inovação. A proatividade ficou estampada no comportamento pessoal com definição de metas e relato de sonhos empreendedores.

  4. Development of a new measurement method for fast breeder reactor fuel burnup using a shielded ion microprobe analyzer

    International Nuclear Information System (INIS)

    Mizuno, M.; Enokido, Y.; Itaki, T.; Kono, K.; Unno, I.; Yamanouchi, S.

    1985-01-01

    A new method of burnup measurement using a shielded ion microprobe analyzer (SIMA) has been developed. The method is based on the isotope analysis of uranium, plutonium, and fission products in irradiated mixed oxide fuel by means of secondary ion mass spectrometry (SIMS). Fourteen samples irradiated in the Japanese experimental fast reactor JOYO were examined. The maximum local burnup of JOYO MK-I core fuels was about5.1 at. %. The axial burnup distribution of the fuel pin was in good agreement with that of the sibling pin in the same subassembly, measured by surface ionization mass spectrometry, which requires the chemical separation of fission products and heavy metals. The new method facilitates the rapid and accurate measurement of fast breeder reactor fuel burnup without human radiation exposure during sample preparation and analysis

  5. Iron distribution in cancer cells following doxorubicin exposure using proton and X-ray synchrotron radiation microprobes

    International Nuclear Information System (INIS)

    Ortega, R.; Deves, G.; Bohic, S.; Simionovici, A.; Menez, B.; Bonnin-Mosbah, M.

    2001-01-01

    Chemical studies have shown that doxorubicin, a well-established anticancer agent, is a powerful iron chelator and the resultant iron-drug complex is an efficient catalyst of the conversion of hydrogen peroxide to the highly reactive hydroxyl radical. However, the intracellular complexation of doxorubicin with iron is still debated. Using nuclear microprobe analysis (NMPA), we previously observed in human ovarian cancer cells exposed to 20 μM iodo-doxorubicin (IDX) that iodine and iron cellular distributions were spatially correlated, suggesting a mechanism of intracellular iron chelation by the anthracycline compound. Because maximal plasma drug concentrations in patients are expected to be around 5 μM, NMPA and X-ray absorption near edge spectroscopy (XANES) experiments for iron speciation analysis were performed on cultured cells exposed to pharmacological doses of 2 μM IDX or doxorubicin

  6. A scanning proton microprobe study of stinging emergences from the leaf of the common stinging nettle urtica dioica l.

    Science.gov (United States)

    Hughes, N. P.; Perry, C. C.; Williams, R. J. P.; Watt, F.; Grime, G. W.

    1988-03-01

    Proton-induced X-ray emission (PIXE) combined with the Oxford scanning proton microprobe (SPM) was used to investigate the abundance and spatial distribution of inorganic elements in mineralising stinging emergences from the leaf of the Common Stinging Nettle, Urtica dioica L. Elemental maps and point analytical data were collected for emergences at two stages of maturity. In all emergences calcium and silicon were spatially organised and present at high concentration. The inorganic elements K, P, S and Mn were also spatially organised during mineralisation, but at maturity these elements were present only at background levels and then showed no specific localisation. The observed changes in the inorganic content of the emergences are obviously related to the mineralisation processes. The possible biochemical significance of the distribution of the elements is discussed.

  7. On the identification of carbonaceous aerosols via 14C accelerator mass spectrometry, and laser microprobe mass spectrometry

    International Nuclear Information System (INIS)

    Currie, L.A.; Fletcher, R.A.; Klouda, G.A.

    1987-01-01

    Carbon isotopic measurements ( 12 C, 14 C), derived from chemical measurements of total carbon plus AMS measurements of 14 C/ 12 C have become an accepted means for estimating fossil and contemporary carbon source contributions to atmospheric carbon. Because of the limited sensitivity of these techniques, however, such measurements are restricted to 'bulk' samples comprising at least 10-100 μg of carbon. Laser microprobe mass spectrometry (LMMS) offers an important complementary opportunity to investigate the chemical nature of individual particles as small as 0.1 μm in diameter. Although there is little hope to measure 14 C/ 12 C in such small samples, the compositional and structural information available with the laser microprobe is of interest for possible source discrimination. Also, the analysis of individual particles, which may reflect individual sources, yields significant potential increases in spatial, temporal and source resolution, in comparison to bulk sample analysis. Results of our exploratory investigation of known sources of carbonaceous particles, using LMMS, are presented. By applying multivariate techniques to laser mass spectra of soot from the combustion of heptane and wood, we found striking differences in the alkali metals (notably potassium) in the positive ion mass spectra. For ambient particles, 14 C has proved to be a crucial adjunct for the development and validation of the LMMS approach to single particle source assignment via carbon cluster pattern recognition. The combined techniques offer great promise for objective modeling (number and types of carbon sources) and for extension of the dichotomous carbon apportionment (fossil, contemporary) to subclasses such as soot from wood and agricultural burning, and that from coal and petroleum combustion. (orig.)

  8. Perfil cognitivo aos sete anos de idade de crianças nascidas prematuras e com peso inferior a 1.500 gramas

    OpenAIRE

    Alexandre Ferreira Campos

    2009-01-01

    Objetivo: Conhecer o desempenho cognitivo, aos sete anos de idade, de crianças nascidas prematuras no Hospital das Clínicas da Universidade Federal de Minas Gerais (HC/UFMG), com idade gestacional até 34 semanas e peso ao nascimento inferior a 1500 gramas, adequado à idade gestacional. Essas crianças tiveram seguimento longitudinal interdisciplinar no Ambulatório da Criança de Risco (ACRIAR), e apresentavam inteligência e exame neurológico normais aos sete anos. Métodos: Participaram do estud...

  9. Efeito da Universidade Aberta à Terceira Idade sobre a qualidade de vida do idoso

    Directory of Open Access Journals (Sweden)

    Keika Inouye

    2017-08-01

    Full Text Available Resumo A educação na velhice tem como finalidade promover conhecimentos que determinam redimensionamentos para o fomento da qualidade de vida a partir de pressupostos de interdisciplinaridade, participação social e promoção da saúde. Este estudo teve como objetivo avaliar o efeito do programa Universidade Aberta à Terceira Idade (UATI na qualidade de vida (QV de alunos idosos. Para tanto, foram realizadas medidas antes e após a intervenção (no início e término do ano letivo e comparações com os escores de um grupo que não frequentava a UATI. Os instrumentos usados para coleta de dados foram: Ficha de Caracterização do Participante, Critério de Classificação Econômica Brasil e Escala de Avaliação da Qualidade de Vida (QdV-DA. Todos os dados obtidos foram digitados em um banco no programa Statistical Program for Social Sciences para realização de análises estatísticas não paramétricas. Os dados mostraram que: (a existe diferença entre os escores totais de QV de idosos alunos da UATI antes e após a intervenção (no início e término do ano letivo e esta diferença é positiva (Z = - 4,541; p < 0,001; (b após a participação na UATI, as percepções de QV são mais elevadas quando comparadas ao grupo de indivíduos que não participava do programa (χ2 = 7,448; df = 1; p = 0,006. Os resultados deste estudo apontaram que a participação na UATI é favorável para o fomento das percepções de QV.

  10. Trabalho feminino e saúde na terceira idade Women's work and health among Brazilian elderly

    Directory of Open Access Journals (Sweden)

    Luana Giatti

    2002-01-01

    Full Text Available O objetivo deste estudo é estimar e caracterizar a participação de idosas no mercado de trabalho e investigar diferenciais de saúde, segundo sua inserção nesse mercado, após considerar a influência de fatores sociodemográficos. O estudo incluiu 4.607 com 65 anos e mais, residentes em dez regiões metropolitanas brasileiras e participantes da PNAD/98. Foram definidas as categorias: trabalhando, aposentada e outra. A análise incluiu o qui-quadrado e o odds ratio estimado através de regressão logística multinomial. Quase 10% das mulheres trabalhavam, 42% eram aposentadas e 48% não trabalhavam nem eram aposentadas. As idosas ocupadas eram mais jovens, tinham maior renda, e de 4 a 7 anos de escolaridade. O fato de estar trabalhando esteve associado à melhor percepção da própria saúde, menor relato de doenças crônicas, plano privado de saúde, menor relato de consulta e internação hospitalar, melhores indicadores de autonomia e mobilidade física e maior freqüência de consulta odontológica. A permanência das idosas na vida ativa é inferior à dos homens brasileiros no mesmo período. Os diferenciais de saúde relacionados ao trabalho são mais acentuados entre as mulheres. É fundamental determinar se os diferenciais de saúde observados entre idosas, também são encontrados nas mulheres em idade ativa.The objective of this study is to estimate and describe the participation of aged women in the labour market, and to investigate health differentials according to their working position, after considering the influence of social and demographic factors. This study comprises 4.607 females aged 65 or more, residents in 10 Brazilian metropolitan regions and participants of PNAD conducted in 1998. The following working categories have been defined: working, retired and other. The analysis was based on qui-square tests and odds ratios were obtained by multinomial logistic regression. Almost 10% of the aged women worked, 42% were

  11. Automedicação em idade pediátrica

    Directory of Open Access Journals (Sweden)

    Nídia Belo

    2017-12-01

    Full Text Available A automedicação pediátrica consiste na administração de medicação à criança ou adolescente pelos seus cuidadores, ou pelo próprio no caso de crianças maiores e adolescentes, sem observação médica prévia. Os dados nacionais sobre a prevalência e segurança desta prática são escassos. Este estudo pretendeu avaliar a prevalência de automedicação em idade pediátrica, identificar os fármacos mais utilizados e os principais fatores motivacionais. Foi efetuado um estudo transversal, observacional, descritivo e retrospetivo. Amostra de conveniência obtida através da aplicação de um questionário online de autopreenchimento pelos pais/cuidadores de crianças e adolescentes. Foram obtidos 209 questionários, referentes a crianças e adolescentes até aos 17 anos (mediana dois anos, sem diferença de género. A maioria dos inquiridos (64% afirmou já ter automedicado os filhos, dos quais 24% no mês anterior ao estudo. A noção de que se trataria de um problema de saúde simples e recomendação da mesma atuação em situação anterior semelhante constituíram os principais fatores motivacionais. Os antipiréticos foram os fármacos mais utilizados (paracetamol em 84,7% e ibuprofeno em 53,1%, verificando-se grande variabilidade na dose administrada. Antitússicos/mucolíticos, antieméticos e antidiarreicos foram utilizados por 26% da amostra. As reações adversas decorrentes da automedicação ocorreram em 1,4% crianças e adolescentes. A prevalência de automedicação encontrada neste estudo foi elevada, resultado consistente com estudos internacionais sobre o tema. Os principais fármacos utilizados são medicamentos não sujeitos a receita médica. Salienta-se a elevada utilização de medicamentos sem eficácia comprovada ou desaconselhados em pediatria. A desadequação da dose administrada ao peso da criança foi um dos fatores de risco identificados no estudo, constatando-se casos com potencial toxicidade. É necess

  12. Results from the nuclear microprobe PIXE analysis of selected rare earth fluor compounds

    International Nuclear Information System (INIS)

    Hollerman, William A.; Gates, Earl; Boudreaux, Philip; Glass, Gary A.

    2002-01-01

    Most previous research measures fluorescence properties over the macroscopic regime. Properties of individual microscopic grains could be significantly different than those measured over the macroscopic scale. Until recently, it was difficult to measure properties of individual fluor grains. Existing characterization techniques like scanning electron microscopy are not practical, since the resulting fluorescence masks the electron surface profile. Starting in September 2000, a research program was initiated at the Acadiana Research Laboratory to determine microscopic fluorescence properties for selected inorganic rare earth compounds. The initial phase of this program utilized microscopic proton induced X-ray emission (μPIXE) to characterize the elemental composition of individual fluor grains. Results show that both individual grains and small clusters of grains could be seen using μPIXE. Maps of this type can be used to estimate grain dimensions for the selected rare earth fluor. This technique is a new and innovative method to characterize a fluor material

  13. Produção do Superprecoce a Partir de Bezerros Desmamados aos 72 ou 210 Dias de Idade

    Directory of Open Access Journals (Sweden)

    Restle João

    2002-01-01

    Full Text Available O experimento foi conduzido com o objetivo de avaliar o desempenho em confinamento, dos 210 aos 408 dias de idade, de bezerros previamente desmamados aos 72 (T72 ou 210 (T210 dias. Foram utilizados 36 machos não castrados da raça Braford (5/8 Hereford 3/8 Nelore. O peso médio no início do experimento foi de 209 kg (T72 e 192 kg (T210. O confinamento compreendeu 30 dias de adaptação dos animais e 168 dias de avaliação, sendo dividido em quatro períodos de 42 dias. A relação volumoso:concentrado foi de 60:40 para o 1º e 2º períodos, 50:50 para o 3º período e 45:55 para o 4º período. Não houve interação entre idade de desmame e período de avaliação em confinamento para os parâmetros relativos aos consumos médios por animal de matéria seca (CMS e de energia digestível (CED, expressos em kg/dia e Mcal/dia (CMSD e CEDD, por 100 kg de peso vivo (CMSP e CEDP e por unidade de tamanho metabólico (CMSM e CEDM, ao ganho de peso médio diário (GMD, à conversão alimentar (CA e eficiência energética (EE. Animais desmamados aos 210 dias apresentaram maiores CMSP (2,25 contra 2,07% PV e CEDP (7,05 contra 6,48% PV em relação aos animais desmamados ao 72 dias de idade. Não houve diferença no CMSD (6,75 contra 6,98 kg/dia, no GMD (1,066 contra 1,074 kg/dia, na eficiência de conversão da matéria seca (6,42 contra 6,72 kg de MS/kg ganho de PV e da energia digestível consumida (20,18 contra 21,13 Mcal/kg ganho de PV em ganho de peso vivo para os animais desmamados aos 72 ou 210 dias de idade, respectivamente. Os pesos de abate e de carcaça quente foram similares entre as duas idades, sendo, respectivamente, de 424 e 232 kg para os animais do T72 e de 406 e 221 kg para dos T210. Os resultados mostram que animais desmamados aos 72 dias de idade apresentaram desempenho durante a terminação, pesos de abate e de carcaça similares aos desmamados aos 210 dias.

  14. Degeneração macular relacionada à idade: novas perspectivas Age-related macular degeneration: new perspectives

    Directory of Open Access Journals (Sweden)

    Marcio Bittar Nehemy

    2006-12-01

    Full Text Available A degeneração macular relacionada à idade (DMRI é a principal causa de cegueira legal em indivíduos acima de 50 anos de idade. Embora estudos recentes tenham mostrado que o fator genético é significativo, a patogênese da degeneração macular relacionada à idade permanece obscura, e os fatores de risco não estão ainda completamente estabelecidos. Estudos multicêntricos randomizados, publicados nos últimos anos, demonstraram que uma combinação de vitaminas e minerais é eficaz na redução do risco de desenvolvimento de neovascularização e de progressão para os estágios mais avançados da degeneração macular relacionada à idade. De maneira análoga, a terapia fotodinâmica (PDT e a terapia antiangiogênica também tiveram sua eficácia comprovada no tratamento de membrana neovascular coroideana subfoveal associada à degeneração macular relacionada à idade. Ambas reduzem o risco de perda de visão e, eventualmente, permitem melhora temporária da acuidade visual. Outras modalidades de tratamento, tais como fotocoagulação a laser, remoção cirúrgica da membrana e termoterapia transpupilar (TTT, podem beneficiar apenas um pequeno subgrupo de pacientes. Uma melhor compreensão dos mecanismos fisiopatológicos e dos eventos moleculares nas diversas fases da doença deverão propiciar, em futuro próximo, melhores estratégias para o controle e tratamento da degeneração macular relacionada à idade.Age-related macular degeneration (ARMD is a major source of legal blindness in individuals older than 50 years. Even though recent reports suggest that genetics plays an important role, its pathogenesis remains puzzling and the risk factors for its occurrence are not completely established. Vitamin and mineral supplementation reduced the risk of development of choroidal neovascularization (CNV or progression to the most advanced stages of age-related macular degeneration. Photodynamic therapy (PDT and antiangiogenic therapy

  15. High-intensity positron microprobe at the Thomas Jefferson National Accelerator Facility

    International Nuclear Information System (INIS)

    Golge, S.; Vlahovic, B.; Wojtsekhowski, B.

    2014-01-01

    We present a conceptual design for a novel continuous wave electron-linac based high-intensity high-brightness slow-positron production source with a projected intensity on the order of 10 10  e + /s. Reaching this intensity in our design relies on the transport of positrons (T + below 600 keV) from the electron-positron pair production converter target to a low-radiation and low-temperature area for moderation in a high-efficiency cryogenic rare gas moderator, solid Ne. This design progressed through Monte Carlo optimizations of: electron/positron beam energies and converter target thickness, transport of the e + beam from the converter to the moderator, extraction of the e + beam from the magnetic channel, a synchronized raster system, and moderator efficiency calculations. For the extraction of e + from the magnetic channel, a magnetic field terminator plug prototype has been built and experimental results on the effectiveness of the prototype are presented. The dissipation of the heat away from the converter target and radiation protection measures are also discussed.

  16. High-intensity positron microprobe at the Thomas Jefferson National Accelerator Facility

    Energy Technology Data Exchange (ETDEWEB)

    Golge, S., E-mail: serkan.golge@nasa.gov; Vlahovic, B. [North Carolina Central University, Durham, North Carolina 27707 (United States); Wojtsekhowski, B. [Jefferson Laboratory, 12000 Jefferson Ave., Newport News, Virginia 23606 (United States)

    2014-06-21

    We present a conceptual design for a novel continuous wave electron-linac based high-intensity high-brightness slow-positron production source with a projected intensity on the order of 10{sup 10 }e{sup +}/s. Reaching this intensity in our design relies on the transport of positrons (T{sub +} below 600 keV) from the electron-positron pair production converter target to a low-radiation and low-temperature area for moderation in a high-efficiency cryogenic rare gas moderator, solid Ne. This design progressed through Monte Carlo optimizations of: electron/positron beam energies and converter target thickness, transport of the e{sup +} beam from the converter to the moderator, extraction of the e{sup +} beam from the magnetic channel, a synchronized raster system, and moderator efficiency calculations. For the extraction of e{sup +} from the magnetic channel, a magnetic field terminator plug prototype has been built and experimental results on the effectiveness of the prototype are presented. The dissipation of the heat away from the converter target and radiation protection measures are also discussed.

  17. Relação entre idade e variação da flexibilidade de bailarinas

    Directory of Open Access Journals (Sweden)

    Aline Huber da Silva

    2008-10-01

    Full Text Available O objetivo deste estudo foi verificar se o comportamento da flexibilidade, após 8 semanas de aplicação da técnica de alongamento por Facilitação Neuromuscular Proprioceptiva em bailarinas, tem relação com suas idades. A amostra foi obtida de forma intencional, composta por 11 bailarinas na faixa etária de 13 a 16 anos. Realizou-se avaliação da flexibilidade angular dos movimentos de flexão (com o joelho estendido, abdução e rotação externa do quadril através da goniometria e da flexibilidade linear com a Caixa de Sentar e Alcançar de Wells, antes e após o período experimental de oito semanas, com duas intervenções semanais, utilizando a técnica de FNP. Para análise, usou-se estatística descritiva, teste t e correlação linear de Pearson. Adotou-se significância de 5%. Somente a variação da rotação externa e da Caixa de Sentar e Alcançar, durante o período experimental, apresentaram correlação estatisticamente significativa com a idade das bailarinas, porém, essa correlação ainda assim foi bastante fraca. Pode-se perceber que praticamente não houve relação entre a variação da flexibilidade com a idade da amostra.

  18. Characterization of flux-grown Trace-element-doped titanite using the high-mass-resolution ion microprobe (SHRIMP-RG)

    Science.gov (United States)

    Mazdab, F.K.

    2009-01-01

    Crystals of titanite can be readily grown under ambient pressure from a mixture of CaO, TiO2 and SiO2 in the presence of molten sodium tetraborate. The crystals produced are euhedral and prismatic, lustrous and transparent, and up to 5 mm in length. Titanite obtained by this method contains approximately 4300 ppm Na and 220 ppm B contributed from the flux. In addition to dopant-free material, titanite containing trace alkali and alkaline earth metals (K, Sr, Ba), transition metals (Sc, Cr, Ni, Y, Zr, Nb, Hf and Ta), rare-earth elements (REE), actinides (Th, U) and p-block elements (F, S, Cl, Ge, Sn and Pb) have been prepared using the same procedure. Back-scattered electron (BSE) imaging accompanied by ion-microprobe (SHRIMP-RG) analysis confirms significant incorporation of selected trace-elements at structural sites. Regardless of some zonation, the large size of the crystals and broad regions of chemical homogeneity make these crystals useful as experimental starting material, and as matrix-matched trace-element standards for a variety of microbeam analytical techniques where amorphous titanite glass, heterogeneous natural titanite or a non-titanite standard may be less than satisfactory. Trace-element-doped synthetic crystals can also provide a convenient proxy for a better understanding of trace-element incorporation in natural titanite. Comparisons with igneous, authigenic and high-temperature metasomatic titanite are examined. The use of high-mass-resolution SIMS also demonstrates the analytical challenges inherent to any in situ mass-spectrometry-based analysis of titanite, owing to the production of difficult-to-resolve molecular interferences. These interferences are dominated by Ca-Ca, Ca-Ti and Ti-Ti dimers that are significant in the mass range of 80-100, affecting all isotopes of Sr and Zr, as well as 89Y and 93Nb. Methods do exist for the evaluation of interferences by these dimers and of polyatomic interferences on the LREE.

  19. Padrões motores de escolares de oito a nove anos de idade da cidade de Santa Rosa, RS

    OpenAIRE

    Loi, Luiz Serafim de Mello

    1999-01-01

    Dissertação (mestrado) - Universidade Federal de Santa Catarina, Centro de Desportos. O desenvolvimento motor é um assunto que necessita maiores estudos, haja vista a importância cada vez maior do desenvolvimento pleno da criança, desde os primeiros anos de vida. Este estudo utilizando como Marco Referencial Teórico (MRT) o modelo de desenvolvimento motor de Gallahue & Ozmun (1998) teve por objetivo verificar o perfil motor de escolares de oito e nove anos de idade, da cidade de Santa Rosa...

  20. Psicodinâmica da mulher trabalhadora de meia-idade em fase de pré-aposentadoria

    OpenAIRE

    Leão,Marluce Auxiliadora Borges Glaus; Gíglio,Joel Salles

    2002-01-01

    Este estudo analisa o processo de aposentar-se como um fenômeno de transição na meia-idade, investigando como uma mulher trabalhadora, com alto nível de qualificação profissional, vivencia a proximidade da aposentadoria e o que orienta suas expectativas de vida. Utiliza entrevista e procedimento de desenhos-estórias como técnica de investigação clínica da personalidade, analisando qualitativamente os dados à luz da Psicologia Analítica. Constata que, nessa mulher, a proximidade da perda da id...

  1. Grupo de crescimento pessoal e reintegração criação laborativa na terceira idade

    OpenAIRE

    Grünewald, Virginia

    2001-01-01

    Tese (doutorado) - Universidade Federal de Santa Catarina, Centro Tecnológico. Programa de Pós-Graduação em Engenharia de Produção O trabalho GRUPO DE CRESCIMENTO PESSOAL E REINTEGRAÇÃO/CRIAÇÃO LABORATIVA NA TERCEIRA IDADE: AUTO CONHECIMENTO E PENSAMENTO ERGONÔMICO, desenvolveu-se com dois objetivos: 1) Possibilitar a aposentados o resgate, desenvolvimento e fortalecimento da auto-descoberta do seu potencial criativo para Ser e nortear suas ações; a reflexão e transformação das atuais visõ...

  2. Desenvolvimento corporal e desempenho produtivo de novilhas de corte prenhas aos 13/15 meses de idade

    OpenAIRE

    Carolina Balbé de Oliveira de Souza

    2014-01-01

    O trabalho conduzido na Fazenda Rancho Santa Zelina, Júlio de Castilhos/RS, avaliou o desenvolvimento corporal e o desempenho produtivo de 64 novilhas de um rebanho comercial Angus da concepção aos 13/15 meses de idade, submetidas a quatro sistemas alimentares durante a gestação: pastagem de Brachiaria com suplementação + pastagem natural no terço final de gestação (BRACS-PN}, pastagem natural com suplementação+ pastagem natural no terço final de gestação (PNCS-PN), pastagem de Brachiara + pa...

  3. Fontes proteicas e idades de abate sobre a estrutura e ultraestrutura do intestino delgado de leitões desmamados

    Directory of Open Access Journals (Sweden)

    Maria Cristina Thomaz

    2011-10-01

    Full Text Available Foram realizados dois experimentos (experimento 1 - alimentação convencional e experimento 2 - alimentação das matrizes, a partir de 109 dias de gestação, na lactação e dos leitões lactentes com ração sem farelo de soja, com o objetivo de avaliar os efeitos de fontes proteicas (farelo de soja - FS, soja semi-integral extrusada - SSIE e produtos lácteos - PL sobre a morfologia intestinal de leitões abatidos aos 0,5 e 15 dias após a desmama. Foram utilizados 27 leitões, desmamados aos 25 dias de idade, sendo que em cada idade, nove leitões foram abatidos. Utilizou-se o delineamento em blocos ao acaso, em esquema fatorial 3 x 3 (três dietas x três idades de abate. Os resultados demonstraram que os animais recebendo FS apresentaram menores alturas das vilosidades e relação vilosidade:cripta, quando comparados àqueles que receberam SSIE ou PL, não havendo, entretanto, diferenças entre estes. A altura da vilosidade e a relação vilosidade:cripta não foram afetadas pela alimentação diferenciada das matrizes e dos leitões antes da desmama. A profundidade das criptas não foi afetada pelas dietas ou idades de abate, dentro de cada experimento, em nenhum dos segmentos estudados, sendo, no entanto, menor no duodeno e maior no jejuno e íleo dos animais do exp. 2, quando comparados àqueles do exp. 1. Concluiu-se que o FS afetou negativamente a altura das vilosidades e a relação vilosidade:cripta após a desmama; que a morfologia intestinal foi mais afetada aos cinco dias, mostrando sinais de recuperação aos 15 dias após a desmama e que a alimentação das matrizes não afetou a morfologia dos segmentos do intestino delgado.

  4. Oxidation kinetics and auger microprobe analysis of some oxidized zirconium alloys

    International Nuclear Information System (INIS)

    Ploc, R.A.

    1989-01-01

    Oxidation kinetics at 300 o C in dry oxygen of 0.5 wt% binary alloys of iron, nickel, and chromium in zirconium were determined for several surface preparations. Further, chemical profiles of the oxides as they existed on the matrix and on the precipitates were obtained by sputtering and Auger electron analysis. The appearance of 'breakaway' oxidation was controlled by the surface finish of the alloy, a variable that could be used to eliminate the phenomenon for all alloys except the Zr/Ni binary, which required β-quenching to accomplish the same purpose. (author)

  5. Quantification of the distribution of hydrogen by nuclear microprobe at the Laboratory Pierre Sue in the width of zirconium alloy fuel clad of PWR reactors

    International Nuclear Information System (INIS)

    Raepsaet, C.; Bossis, Ph.; Hamon, D.; Bechade, J.L.; Brachet, J.C.

    2007-01-01

    Among the analysis techniques by ions beams, the micro ERDA (Elastic Detection Analysis) is an interesting technique which allows the quantitative distribution of the hydrogen in materials. In particular, this analysis has been used for hydride zirconium alloys, with the nuclear microprobe of the Laboratory Pierre Sue. This probe allows the characterization of radioactive materials. The technique principles are recalled and then two examples are provided to illustrate the fuel clad behavior in PWR reactors. (A.L.B.)

  6. Detailed petrographic descriptions and microprobe data for drill holes USW-G2 and UE25b-1H, Yucca Mountain, Nevada

    International Nuclear Information System (INIS)

    Broxton, D.; Vaniman, D.; Caporuscio, F.; Arney, B.; Heiken, G.

    1982-10-01

    Drill holes USW-G2 and UE25b-1H at Yucca Mountain, Nevada penetrate a thick sequence of volcanic rocks consisting of voluminous ash-flow tuffs, intercalated with thin bedded tuffs and minor lavas. This report provides detailed petrologic descriptions that were summarized in an earlier report. Microprobe analyses of feldspars and mafic phenocrysts as well as secondary feldspars are tabulated for these drill holes for the first time in this report

  7. 7th international conference on Nuclear microprobe technology and applications; 7. conference internationale sur la technologie et les applications des microsondes nucleaires

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    2000-07-01

    This colloquium gives an up-to-date report on the continuously advancing applications and development of microbeam technology. It presents abstracts and oral contributions in the following domains: microprobes facilities, analysis techniques, imaging techniques, micro-ion beam modification of materials, microelectronics, applications in Material Sciences in Biology in Medicine in earth and planetary Sciences in environment in art in archaeology, alternative techniques. (A.L.B.)

  8. Transporte de ovos férteis: Influência das idades das matrizes, tempos de estocagem e das estradas

    Directory of Open Access Journals (Sweden)

    Aérica C. Nazareno

    2014-03-01

    Full Text Available Propôs-se, com esta pesquisa, avaliar a influência de diferentes idades das matrizes e tempos de estocagem no número de ovos trincados durante a operação de transporte em diferentes estradas. A pesquisa foi conduzida na empresa integradora avícola em Mogi-Mirim - SP, por meio do acompanhamento de três carregamentos em diferentes estações do ano (primavera, verão e outono. Foi utilizado um caminhão climatizado do tipo baú com capacidade para 592 caixas de ovos. Foram registrados, por meio de quatro acelerômetros, os níveis de vibração (m s-2 e choques em percursos realizados nas estradas de terra e asfalto. O número de ovos trincados foi obtido por meio da contabilização de 18 caixas de ovos transportadas que apresentavam três idades de matrizes e três tempos de estocagem, pelo método visual. Foi utilizado o delineamento experimental inteiramente aleatorizado com esquema fatorial 3 x 3. Conclui-se que as matrizes velhas e intermediárias apresentaram o maior número de ovos trincados; os maiores níveis de vibração e choques da carga ocorreram no sentido horizontal enquanto a estrada de asfalto ofereceu as piores condições para o transporte de ovos.

  9. Diagnóstico de saúde das mulheres em idade fértil de Sergipe

    Directory of Open Access Journals (Sweden)

    Alzira Maria D'avila Nery Guimarães

    1996-03-01

    Full Text Available Relato parcial de uma pesquisa realizada pela Secretária de Estado da Saúde em parceria com o UNICEF, intitulado de Diagnóstico Matemo-lnfantil cio Estado de Sergipe. Nesta pesquisa as autoras realizam uma abordagem parcial sobre a saúde das mulheres em idade fértil. Objetivo: Medir por amostragem a nível estadual os indicadores: estado civil, idade da menarca, início da vida sexual, gravidez, abortos, prevenção do câncer cérvico-uterino e mama, anticoncepção e utilização dos serviços de saúde. Os resultados foram coletados através da aplicação de um formulário estruturado, abrangendo variáveis préconcepcionais, biológicas e sociais. Os dados obtidos fornecem subsídios para ampla discussão sobre a saúde das mulheres em Sergipe.

  10. Avaliação da eqüidade da Previdência no meio rural do Brasil

    Directory of Open Access Journals (Sweden)

    Ana Cecília Kreter

    2006-09-01

    Full Text Available Este trabalho avalia a eqüidade do sistema brasileiro de aposentadorias pagas no meio rural, dando ênfase à década de 1990. Entende-se como eqüidade a distribuição de aposentadorias sem viés de cor (ou raça, sexo e nível de educação. Motivado pela Constituição Federal de 1988, as Leis nº 8.212 e nº 8.213, de 1991 permitiram que homens (com 60 anos de idade ou mais e mulheres (com 55 anos de idade ou mais que tivessem comprovado exercício da atividade rural pudessem obter aposentadoria de um salário mínimo, mesmo não tendo contribuído com o sistema previdenciário. Tais mudanças foram significativas, pois igualaram os direitos de mulheres e homens e fixaram um valor mínimo das aposentadorias. Usando a análise tabular de microdados da PNAD (para os anos de 1992, 1996 e 1999 o trabalho comprova que essa nova sistemática previdenciária permitiu o aumento da renda per capita dos aposentados no meio rural, sem causar aumento da desigualdade da distribuição de renda. A mesma análise tabular dos dados sugere a presença de vieses na concessão das aposentadorias em favor de homens (em relação às mulheres, dos brancos (em relação aos negros e dos mais instruídos (em relação aos menos instruídos, o que foi estatisticamente comprovado através da estimativa do modelo próbite. O trabalho se encerra sugerindo algumas medidas que possam minimizar essa ineqüidade na distribuição das aposentadorias pagas no meio rural.This paper evaluates the equality of the Brazilian system of pensions paid in rural areas during the 1990s. The equality implies equal access to the social security benefits, regardless ethnic, sex and education differences among retired persons. Basing on 1988 Federal Constitution, Laws 8,212 and 8,213, both from 1991, have instituted the old age pension equal to one minimum wage for men (60 years or older and for women (55 years or older if they can prove they were rural workers. These old citizens can

  11. Idade de desmame e suplementação no desenvolvimento e em características de carcaças de novilhos de corte

    Directory of Open Access Journals (Sweden)

    Almeida Luciane Salgueiro Pio de

    2003-01-01

    Full Text Available O experimento foi conduzido na Estação Experimental da Universidade Federal do Rio Grande do Sul, município de Eldorado do Sul, Brasil, a fim de avaliar o desempenho de 40 bezerros filhos de vacas cruzas Bos indicus x Bos taurus até os dois anos de idade, desmamados precocemente (DP, com média de idade de 91 dias e mínimo de 70 kg de peso vivo, ou desmamados à idade convencional (DC, média de 170 dias de idade e peso médio de 131,2 kg, suplementados (Su ou não (NSu com ração energético-protéica com 14% de proteína bruta e 75% de nutrientes digestíveis totais, durante 91 dias no primeiro inverno. O delineamento experimental utilizado foi o delineamento completamente casualizado. Os novilhos do DP foram mais leves até um ano de idade (DP=208,7 kg x DC=233,5 kg. Aos 18-20 meses de idade, os novilhos não eram mais estatisticamente diferentes em seus pesos vivos (DP=279,9 kg x DC=292,5 kg. Ao abate, os pesos vivos médios foram de 432,3 kg (DC e 414,0 kg (DP, não diferindo também no rendimento, acabamento, conformação e classificação das carcaças. O desmame precoce não impediu o desenvolvimento e o abate dos novilhos aos dois anos de idade. A suplementação no primeiro inverno não alterou o desempenho dos novilhos ao abate.

  12. Sulfur isotope composition of orogenic spinel lherzolite massifs from Ariege (north-eastern pyrenees, France): An ion microprobe study

    Energy Technology Data Exchange (ETDEWEB)

    Chaussidon, M. (Centre de Recherches Petrographiques et Geochimiques, Vandoeuvre-les-Nancy (France)); Lorand, J. (Unite associee au CNRS, Paris (France))

    1990-10-01

    The orogenic spinel lherzolite massifs from Ariege, which represent tectonically emplaced fragments of the sub-continental upper mantle, are composed mainly of variously depleted peridotites. These rocks are crosscut by two generations of pyroxenites. The first is made up of layered pyroxenites, which are interpreted either as crystal segregates from Triassic continental tholeiites or as subducted parts of the oceanic crust re-injected within the upper mantle. The second consists of amphibole-rich dikes separated from Cretaceous alkali basalts. Forty sulfide grains, occurring either as inclusions within silicates or as interstitial grains, were investigated by ion microprobe for their sulfur isotopic compositions. Comparison between sulfide inclusions in silicates and interstitial sulfide grains strongly suggests that serpentinization and pyrenean metamorphism had no significant effect don the {delta}{sup 34}S values. Likewise, these values are broadly independent of the degree of partial melting. The negative {delta}{sup 34}S values of the massive peridotites could represent an ancient depletion event in the upper mantle. By contrast, the positive {delta}{sup 34}S values observed in the layered pryoxenites and the amphibole-rich dikes indicate that the two parent magmas had in common a mantle source variously enriched in {sup 34}S. Therefore, the present study reveals two extreme reservoirs characterized by different {delta}{sup 34}S values in the upper mantle. This range of variations can explain most {delta}{sup 34}S values found in MORB, continental tholeiites, and alkali basalts.

  13. Microscopic and microprobe analysis of fine roots in healthy and declining spruce (Picea abies (L. ) Karst. ) from different sites

    Energy Technology Data Exchange (ETDEWEB)

    Stienen, H; Bauch, J; Barckhausen, R; Schaub, H

    1984-09-01

    In order to contribute to the identification of primary causes of the spruce decline - evident in many regions of the Federal Republic of Germany - fine roots of 30 trees from altogether 14 healthy and damage forest locations were investigated microscopically, anatomically, histometrically and by cellular microprobe analysis. In addition, fine roots of young plants grown in hydroponic cultures at different pH levels and Al input were studied. Fine roots of declining trees developed cortex cells with a reduced diameter and at the same time thicker cell walls; in addition accessory compounds were accumulated in this presumably protective tissue. Tannins were deposited in the parenchyma of the vascular cylinder of fine roots from declining trees, and many pit membranes of the primary xylem often did not differentiate fully. The X-ray energy-dispersive analysis of individual cells revealed, in particular, an insufficient uptake of Ca and Mg in the fine roots of declining trees. Compared with healthy trees, the concentration of aluminium increased in the cortex of the fine roots; this, in turn, had an antagonistic effect on the uptake of Ca and Mg. Moreover, the concentration of iron and sulphur increased in the fine roots of declining trees. This evidence of alterations and damages in the fine roots of damaged spruce indicates that, besides the direct detrimental impact on the needles through the atmosphere serious damage is inflicted also indirectly through the soil.

  14. PIXE and light element analysis (C,N) in glass inclusions trapped in meteorites with the nuclear microprobe

    International Nuclear Information System (INIS)

    Varela, M.E.; Mosbah, M.; Metrich, N.; Duraud, J.P.; Kurat, G.

    1999-01-01

    Proton-induced X-ray emission (PIXE) and light element analysis have been performed with the nuclear microprobe at the Laboratoire Pierre Suee (Saclay-France) in glass inclusions of the carbonaceous chondrites: Allende, Kaba and Renazzo, and in the achondrite meteorite: Chassigny. Carbon contents in olivine of chondrules are below the nuclear reactions analysis (NRA) detection limit, however, glasses from glass inclusions hosted by these grains, contain an appreciable and highly variable quantities of carbon (200-1600 ppm). This could indicate variable amounts of C trapped during glass inclusion formation. On the other hand, nitrogen is present in highly variable amounts in glasses of both, chondrites and achondrites minerals. Its abundance, correlated with depth from the section surface which suggests loss of N during analyses and therefore the possible existence of a very mobile (volatile?) species. A chondritic Rb/Sr and K/Rb ratio obtained by PIXE analyses in the glass-bearing inclusions of the Chassigny meteorite points towards a primitive source for the glass precursor of Chassigny inclusions

  15. Determination of the chemical properties of residues retained in individual cloud droplets by XRF microprobe at SPring-8

    International Nuclear Information System (INIS)

    Ma, C.-J.; Tohno, S.; Kasahara, M.; Hayakawa, S.

    2004-01-01

    To determine the chemical properties of residue retained in individual cloud droplets is primarily important for the understanding of rainout mechanism and aerosol modification in droplet. The sampling of individual cloud droplets were carried out on the summit of Mt. Taiko located in Tango peninsula, Kyoto prefecture, during Asian dust storm event in March of 2002. XRF microprobe system equipped at SPring-8, BL-37XU was applied to the subsequent quantification analysis of ultra trace elements in residues of individual cloud droplets. It was possible to form the replicas of separated individual cloud droplets on the thin collodion film. The two dimensional XRF maps for the residues in individual cloud droplets were clearly drawn by scanning of micro-beam. Also, XRF spectra of trace elements in residues were well resolved. From the XRF spectra for individual residues, the chemical mixed state of residues could be assumed. The chemical forms of Fe (Fe +++ ) and Zn (Zn + ) could be clearly characterized by their K-edge micro-XANES spectra. By comparison of Z/Si mass ratios of residues in cloud droplets and those of the original sands collected in desert areas in China, the aging of ambient dust particles and their in cloud modification were indirectly assumed

  16. Pb, U, Ti, Hf and Zr distributions in zircons determined by proton microprobe and fission track techniques

    International Nuclear Information System (INIS)

    Clark, G.J.; Gulson, B.L.; Cookson, J.A.

    1979-01-01

    A proton microprobe has been used to determine Pb, Tl, Hf and Zr distributions across four single zircon crystals separated from a 'rapakivi' granite. The Pb and Zr data are quantitative: Pb and Tl concentrations were below the measurable limits for determinations in situ by most other techniques. The distribution of U in the same crystals was determined by the fission track technique. Limits on precision of U allow only a qualitative correlation of U and Pb, whereas the Tl and Pb correlation is more exactly determined. Zircons with distinct cores and overgrowths exhibited uniform Zr and Hf concentrations across the crystals, whereas the high U rims and 'inclusions' (domains) also had high Tl and Pb contents. Since almost all the Pb in these zircons is derived by radioactive decay of U, the Tl substitution has paralleled that of U. The results indicate that the high U domains are 'hot spots' rather than a separate mineral phase. The strong positive correlation of U and Pb indicates that there is little U daughter product migration relative to U, within the crystal. However, for the zircon population investigated here, the data are equivocal on the question of whether U addition to zircon crystals is associated with new zircon growth or not. In either case, the heterogeneous U and Pb distributions complicate any interpretations of U-Pb isotopic analysis for such zircon populations. (author)

  17. Distribution of elements in rat peripheral axons and nerve cell bodies determined by x-ray microprobe analysis

    Energy Technology Data Exchange (ETDEWEB)

    LoPachin, R.M. Jr.; Lowery, J.; Eichberg, J.; Kirkpatrick, J.B.; Cartwright, J. Jr.; Saubermann, A.J.

    1988-09-01

    X-ray microprobe analysis was used to determine concentrations (millimoles of element per kilogram dry weight) of Na, P, Cl, K, and Ca in cellular compartments of frozen, unfixed sections of rat sciatic and tibial nerves and dorsal root ganglion (DRG). Five compartments were examined in peripheral nerve (axoplasm, mitochondria, myelin, extraaxonal space, and Schwann cell cytoplasm), and four were analyzed in DRG nerve cell bodies (cytoplasm, mitochondria, nucleus, and nucleolus). Each morphological compartment exhibited characteristic concentrations of elements. The extraaxonal space contained high concentrations of Na, Cl, and Ca, whereas intraaxonal compartments exhibited lower concentrations of these elements but relatively high K contents. Nerve axoplasm and axonal mitochondria had similar elemental profiles, and both compartments displayed proximodistal gradients of decreasing levels of K, Cl, and, to some extent, Na. Myelin had a selectively high P concentration with low levels of other elements. The elemental concentrations of Schwann cell cytoplasm and DRG were similar, but both were different from that of axoplasm, in that K and Cl were markedly lower whereas P was higher. DRG cell nuclei contained substantially higher K levels than cytoplasm. The subcellular distribution of elements was clearly shown by color-coded images generated by computer-directed digital x-ray imaging. The results of this study demonstrate characteristic elemental distributions for each anatomical compartment, which doubtless reflect nerve cell structure and function.

  18. Detection of delta-ferrite to sigma transformation using metallographic techniques involving ferromagnetic colloid, color etching, and microprobe analysis

    International Nuclear Information System (INIS)

    Gray, R.J.; Sikka, V.K.; King, R.T.

    1976-01-01

    The mechanical properties of ferrite-containing austenitic stainless steel base metal and weldments are usually adversely affected by prolonged exposure to temperatures in the 482 to 900 0 C (900 to 1652 0 F) range. One cause of the property alteration is related to the transformation of relatively ductile delta-ferrite to less ductile sigma-phase. Attempts to identify sigma and delta-ferrite phases by color staining techniques alone are well documented; however, the results are often questionable due to the difficulty in maintaining consistent color identifications. This investigation is concerned with the microstructural responses of the ferromagnetic delta-ferrite phase and the paramagnetic sigma-phase to a ferromagnetic iron colloid in a magnetic field. Such positive or negative responses of the two phases to the colloid offer a more definitive identification. With this technique, the identification of small amounts of these phases in the microstructure is limited only by the highest magnification and resolution of the optical microscope. The procedure is substantiated in this metallographic study with microprobe analysis and color metallography. Several examples of the correlative use of these three techniques in identifying varying amounts of delta-ferrite → sigma transformation are presented

  19. Application of synchrotron microprobe methods to solid-phase speciation of metals and metalloids in house dust.

    Science.gov (United States)

    Walker, S R; Jamieson, H E; Rasmussen, P E

    2011-10-01

    Determination of the source and form of metals in house dust is important to those working to understand human and particularly childhood exposure to metals in residential environments. We report the development of a synchrotron microprobe technique for characterization of multiple metal hosts in house dust. We have applied X-ray fluorescence for chemical characterization and X-ray diffraction for crystal structure identification using microfocused synchrotron X-rays at a less than 10 μm spot size. The technique has been evaluated by application to archived house dust samples containing elevated concentrations of Pb, Zn, and Ba in bedroom dust, and Pb and As in living room dust. The technique was also applied to a sample of soil from the corresponding garden to identify linkages between indoor and outdoor sources of metals. Paint pigments including white lead (hydrocerussite) and lithopone (wurtzite and barite) are the primary source of Pb, Zn, and Ba in bedroom dust, probably related to renovation activity in the home at the time of sampling. The much lower Pb content in the living room dust shows a relationship to the exterior soil and no specific evidence of Pb and Zn from the bedroom paint pigments. The technique was also successful at confirming the presence of chromated copper arsenate treated wood as a source of As in the living room dust. The results of the study have confirmed the utility of this approach in identifying specific metal forms within the dust.

  20. Laser Raman microprobe spectroscopy as a diagnostic for the characterisation of diamond and diamond like carbon (DLC) thin films

    International Nuclear Information System (INIS)

    Johnston, C.

    1990-10-01

    Invariably when manufacturing an artificial diamond film a mixture of carbon is deposited - tetragonally bonded (diamond), trigonally bonded (graphite) and other allotropic crystalline forms and amorphous carbons. This imposes a need for careful analysis to determine exactly what carbon types constitute the films. Raman spectroscopy is particularly sensitive to crystal and atomic structure and has a number of advantages which make it one of the most useful techniques for interrogating diamond and DLC thin films. Although Raman spectroscopy alone cannot fully characterise the film, it can give more information than simply what particular form of carbon or other impurities are present in the film. It can be used to determine the ratio of sp 2 to sp 3 bonding within the film, and to some extent the crystallite or domain size and the internal stress of the film. The use of laser Raman microprobe spectroscopy as a diagnostic tool in the analysis of diamond and DLC thin films is demonstrated for a variety of carbon films on various substrates and the characterisation of these films is discussed. (author)

  1. Microprobe determination of the α/(α+β) boundary for the Zr-Nb system

    International Nuclear Information System (INIS)

    Bethune, I.T.; Williams, C.D.

    1968-07-01

    Electron probe microanalysis has been used to locate the position of the α/(α+β) boundary in the Zr-Nb phase diagram by measuring the phase compositions in specimens of a Zr-2.5 wt.% Nb-0.12 wt% 0 alloy annealed at temperatures in the range 600-850 o C. The solubility of Nb in α-Zr at 600 o C is shown to be 1.1 ± 0.1 wt.%. The concentration of Nb in the a-phase annealed for short intervals at 850 o C is also close to 1%, decreasing to 0.85 ± 0.05 wt.% with prolonged annealing at this temperature. A precise determination of the (α+β)/β boundary has not been made; extrapolation of non-equilibrium compositions indicate that the monotectoid composition is close to 20 wt.% Nb, as shown in earlier phase diagram work. (author)

  2. Electron probe microanalysis for clinical investigations: Microdrop and soft tissue analysis

    International Nuclear Information System (INIS)

    Ingram, M.J.; Ingram, F.D.

    1984-01-01

    The most important advantage offered by electron probe microanalysis (EPA) for clinical investigations is the ability to analyze smaller volumes of tissue than is possible with conventional techniques. The sample can be a biological soft tissue specimen, which involves subcellular localization, or a picoliter fluid droplet. In either case, the analysis can be nondestructive and permit multiple analyses for a number of elements in a given sample. The most highly developed electron microprobe analytical technique is fluid drop analysis, popularly referred to as microdrop analysis. This method provides the investigator with an analytic capability that has an accuracy of measurement often 1% or better on 20 to 30 picoliter fluid droplets. Electron microprobe techniques have been used for studies of animal hard tissue and for studies that involve insoluble inclusions. However, the development of techniques for studies of labile constituents in animal soft tissue has been much slower. It has been necessary not only to develop appropriate methods of tissue preparation, but also to establish sound techniques for tissue collection. Although there are adequate methods for collection of most types of tissue from laboratory animals, many of these methods are not suitable for human subjects. In order to provide the reader with a better understanding of the capabilities and potential for the application of electron microprobe methodology to problems in clinical medicine, the authors discuss some of their experiences with liquid droplet analysis and quantitative electrolyte distribution measurements in animal soft tissue

  3. Efeito da idade de desmame e suplementação no desenvolvimento de novilhas de corte Effect of weaning age and supplementation on beef heifers growth

    Directory of Open Access Journals (Sweden)

    Luciane Salgueiro Pio de Almeida

    2004-12-01

    Full Text Available O experimento foi conduzido com o objetivo de avaliar o desempenho de 47 novilhas de corte cruzas Bos taurus x Bos indicus até os dois anos de idade, desmamadas precocemente (DP, com idade média de 91 dias e peso mínimo de 70 kg de peso vivo, ou desmamadas à idade convencional (DC, com média de 170 dias de idade e 130,3 kg, suplementadas (Su ou não (NSu com suplemento comercial com 14% de proteína bruta e 75% de NDT, durante 91 dias no primeiro inverno pós-desmame. Os animais do DP e o grupo não-suplementado apresentaram menores pesos vivos até um ano de idade. A idade do desmame não influenciou a taxa de prenhez das novilhas (77,3 e 72%, para o DP e DC, respectivamente. A suplementação no primeiro inverno não influenciou o desempenho das novilhas aos dois anos de idade. O desmame precoce não afetou o desenvolvimento e a fertilidade das novilhas aos dois anos de idade, quando comparado ao desmame à idade convencional.The experiment was conducted to evaluate the performance of 47 Bos taurus x Bos indicus beef heifers until two years of age. Heifers were early weaned (EW with average age of 91 days and minimum of 70 kg of liveweight or weaned at conventional age with average of 170 days and average liveweight of 130.3 kg (CW, supplemented (Su or not (NSu with concentrate containing 14% crude protein and 75% total digestible nutrients (TDN during 91 days in the first winter. The early weaning and the no supplemented group were lightier until one year of age. Weaning age did not affect pregnancy rate (77.3% and 72% to EW and CW, respectively. The supplementation during the first winter did not affect the heifers performance until two years of age. Early weaning did not affected the growth and the fertility of heifers until two years of age when compaired with the weaning at the conventional age.

  4. The identification of growth lines in abalone shell using a nuclear microprobe

    International Nuclear Information System (INIS)

    Bettiol, A.A.; Yang, C.; Hawkes, G.P.; Jamieson, D.N.; Malmqvist, K.G.; Day, R.W.

    1999-01-01

    Ionoluminescence (IL) combined with particle induced X-ray emission (PIXE) imaging has been employed to identify intrinsic growth bands in the spire region, and extrinsic bands at the growth edge of Australian Black-lip abalone shell (Haliotis rubra). Previous studies using optical flood cathodoluminescence, scanning electron microscope cathodoluminescence (SEM-CL) and Raman spectroscopy on samples from the same population suggest that the visible luminescence is due to Mn 2+ activated calcium carbonate. In this study we confirm Mn 2+ as the activator in both the spire and growth edge regions of the shell. The sensitivity of ionoluminescence to the co-ordination environment of the Mn 2+ activators in the shell allows for the spatial identification of the calcium carbonate polymorph responsible for the growth lines observed optically. Furthermore the detection and mapping of trace elements such as Mn and Sr with the PIXE technique enables comparisons to be made between calcite and aragonite biomineralized in the wild and under laboratory conditions

  5. The identification of growth lines in abalone shell using a nuclear microprobe

    Energy Technology Data Exchange (ETDEWEB)

    Bettiol, A.A.; Yang, C.; Hawkes, G.P.; Jamieson, D.N. E-mail: dnj@physics.unimelb.edu.au; Malmqvist, K.G.; Day, R.W

    1999-09-02

    Ionoluminescence (IL) combined with particle induced X-ray emission (PIXE) imaging has been employed to identify intrinsic growth bands in the spire region, and extrinsic bands at the growth edge of Australian Black-lip abalone shell (Haliotis rubra). Previous studies using optical flood cathodoluminescence, scanning electron microscope cathodoluminescence (SEM-CL) and Raman spectroscopy on samples from the same population suggest that the visible luminescence is due to Mn{sup 2+} activated calcium carbonate. In this study we confirm Mn{sup 2+} as the activator in both the spire and growth edge regions of the shell. The sensitivity of ionoluminescence to the co-ordination environment of the Mn{sup 2+} activators in the shell allows for the spatial identification of the calcium carbonate polymorph responsible for the growth lines observed optically. Furthermore the detection and mapping of trace elements such as Mn and Sr with the PIXE technique enables comparisons to be made between calcite and aragonite biomineralized in the wild and under laboratory conditions.

  6. Exigência de metionina + cistina para frangas de reposição na fase cria de sete a 12 semanas de idade

    Directory of Open Access Journals (Sweden)

    P. D'Agostini

    2012-12-01

    Full Text Available Determinou-se a exigência de metionina + cistina para frangas de sete a 12 semanas de idade e verificou-se seu efeito sobre a fase de postura. O experimento foi dividido em duas fases, de cria e de produção, esta de 22 a 33 semanas de idade. Na primeira fase, utilizaram-se 640 aves - 50% Lohmann LSL e 50% Lohmann Brown - com sete a 12 semanas de idade, distribuídas em delineamento inteiramente ao acaso, em esquema fatorial 5x2 (porcentagem de met+cis e linhagem, com quatro repetições e 16 aves por repetição. As porcentagens de met+cis total estudadas foram 0,471; 0,541; 0,611; 0,681 e 0,751%. Ao atingirem 22 semanas de idade, 240 aves foram utilizadas para verificar o efeito residual das dietas fornecidas na fase de cria. A dieta fornecida nesta fase foi igual para todas as aves. As exigências de metionina + cistina para aves de reposição, leves e semipesadas, no período de sete a 12 semanas de idade, foram de 0,710 % de met+cis total (0,639% de met+cis digestível e 0,706% de met+cis total (0,635% de met+cis digestível, respectivamente.

  7. An ion microprobe study of CAIs from CO3 meteorites. [Abstract only

    Science.gov (United States)

    Russell, S. S.; Greenwood, R. C.; Fahey, A. J.; Huss, G. R.; Wasserburg, G. J.

    1994-01-01

    When attempting to interpret the history of Ca, Al-rich inclusions (CAIs) it is often difficult to distinguish between primary features inherited from the nebula and those produced during secondary processing on the parent body. We have undertaken a systematic study of CAIs from 10 CO chondrites, believed to represent a metamorphic sequence with the goal of distinguishing primary and secondary features. ALHA 77307 (3.0), Colony (3.0), Kainsaz (3.1), Felix (3.2), ALH 82101 (3.3), Ornans (3.3), Lance (3.4), ALHA 77003 (3.5), Warrenton (3.6), and Isna (3.7) were examined by Scanning Electron Microscopy (SEM) and optical microscopy. We have identified 141 CAIs within these samples, and studied in detail the petrology of 34 inclusions. The primary phases in the lower petrologic types are spinel, melilite, and hibonite. Perovskite, FeS, ilmenite, anorthite, kirschsteinite, and metallic Fe are present as minor phases. Melilite becomes less abundant in higher petrologic types and was not detected in chondrites of type 3.5 and above, confirming previous reports that this mineral easily breaks down during heating. Iron, an element that would not be expected to condense at high temperatures, has a lower abundance in spinel from low-petrologic-type meteorites than those of higher grade, and CaTiO3 is replaced by FeTiO3 in meteorites of higher petrologic type. The abundance of CAIs is similar in each meteorite. Eight inclusions have been analyzed by ion probe. The results are summarized. The results obtained to date show that CAIs in CO meteorites, like those from other meteorite classes, contain Mg* and that Mg in some inclusions has been redistributed.

  8. A estética do corpo na filosofia e na arte da Idade Média: texto e imagem

    Directory of Open Access Journals (Sweden)

    Ricardo Luiz Silveira da Costa

    2012-01-01

    Full Text Available A ideia de beleza - e sua consequente fruição estética - variou conforme as transformações das sociedades humanas, no tempo. Durante a Idade Média, coexistiram diversas concepções de qual era o papel do corpo na hierarquia dos valores estéticos, tanto na Filosofia quanto na Arte. Nossa proposta é apresentar a estética do corpo medieval que alguns filósofos desenvolveram em seus tratados (particularmente Isidoro de Sevilha, Hildegarda de Bingen, João de Salisbury, Bernardo de Claraval e Tomás de Aquino, além de algumas representações corporais nas imagens medievais (iluminuras e esculturas, e assim analisar o tema em três vertentes: a o corpo como cárcere da alma, b o corpo como instrumento, e c o corpo como desregramento.

  9. A tríade “Verdadeiro-Bom-Belo”: O lugar da beleza na Idade Média

    Directory of Open Access Journals (Sweden)

    Jan A. Aertsen

    2008-06-01

    Full Text Available Neste artigo, Jan Aertsen discute a compreensão da tríade “Verdadeiro-Belo-Bom” como representante de um conjunto de questões clássicas em filosofia, a qual corresponderia, do ponto de vista moderno, à suposição de que o sujeito possui três modos distintos de se relacionar com o mundo: cognitivo, estético e prático. O autor sugere que a tríade foi formulada explicitamente pela primeira vez na Idade Média; neste período, entretanto, a beleza não era considerada um problema “estético”.

  10. Study on mineral components of rat calvaria by means of X-ray powder diffraction analysis and Raman microprobe spectroscopy

    Energy Technology Data Exchange (ETDEWEB)

    Tamura, Norihiro [Meikai Univ., Sakado, Saitama (Japan). School of Dentistry

    2000-07-01

    The present study was designed to examine the occurrence of the precursor minerals of hydroxyapatite (HA) during the process of HA formation in the rat calvaria. Dried and powdered rat calvaria and synthetic samples, such as HA, dicalcium phosphate dihydrate (DCPD), octacalcium phosphate (OCP), ({beta}-calcium pyrophosphate) and ({beta}-tricalcium phosphate), were used. Determinations were carried out by X-ray powder diffraction and Raman microprobe spectrometry. In general, significant widening of the diffraction peaks was shown to occur after the plasma ashing was performed for the X-ray diffraction. As a result, two adjacent peaks seen normally in the diffraction angles (2 {theta}) 30-35 deg, which is a characteristic feature of HA, were found to fuse with each other, forming a widened single peak. Also, there was a tendency for the intensity of the diffraction peaks to increase with age. With regard to the effect of plasma ashing on the crystallograms of synthetic specimens, all specimens manifested sharp peak patterns except DCPD and OCP. In contrast, a widening of diffraction peaks was observed in the DCPD and OCP samples, indicating that crystallinity had changed during the pretreatment. Results obtained from both vital and synthetic samples after heat treatment at 1000 deg C were as follow: Clearcut diffraction patterns, characteristics of HA, were obtained in all of the calvaria samples. Further, {beta}-TCP was produced by heat treatment of OCP, and its pattern was detected in the samples from rats younger than 6 days of age. Amounts of {beta}-TCP in percentage were disclosed to be 40.2% in embryonal samples, 28.4% in newborn samples, and 18.6% in 6-day-old samples. But no {beta}-TCP could be detected in the 12-week-old samples, indicating that the amount of {beta}-TCP in calvaria decreased with age. We also found that ashing pretreatment did not cause any changes in the samples of HA, {beta}-CPP, and {beta}-TCP. Further, DCPD and {beta}-CPP samples shared

  11. Study on mineral components of rat calvaria by means of X-ray powder diffraction analysis and Raman microprobe spectroscopy

    International Nuclear Information System (INIS)

    Tamura, Norihiro

    2000-01-01

    The present study was designed to examine the occurrence of the precursor minerals of hydroxyapatite (HA) during the process of HA formation in the rat calvaria. Dried and powdered rat calvaria and synthetic samples, such as HA, dicalcium phosphate dihydrate (DCPD), octacalcium phosphate (OCP), (β-calcium pyrophosphate) and (β-tricalcium phosphate), were used. Determinations were carried out by X-ray powder diffraction and Raman microprobe spectrometry. In general, significant widening of the diffraction peaks was shown to occur after the plasma ashing was performed for the X-ray diffraction. As a result, two adjacent peaks seen normally in the diffraction angles (2 θ) 30-35 deg, which is a characteristic feature of HA, were found to fuse with each other, forming a widened single peak. Also, there was a tendency for the intensity of the diffraction peaks to increase with age. With regard to the effect of plasma ashing on the crystallograms of synthetic specimens, all specimens manifested sharp peak patterns except DCPD and OCP. In contrast, a widening of diffraction peaks was observed in the DCPD and OCP samples, indicating that crystallinity had changed during the pretreatment. Results obtained from both vital and synthetic samples after heat treatment at 1000 deg C were as follow: Clearcut diffraction patterns, characteristics of HA, were obtained in all of the calvaria samples. Further, β-TCP was produced by heat treatment of OCP, and its pattern was detected in the samples from rats younger than 6 days of age. Amounts of β-TCP in percentage were disclosed to be 40.2% in embryonal samples, 28.4% in newborn samples, and 18.6% in 6-day-old samples. But no β-TCP could be detected in the 12-week-old samples, indicating that the amount of β-TCP in calvaria decreased with age. We also found that ashing pretreatment did not cause any changes in the samples of HA, β-CPP, and β-TCP. Further, DCPD and β-CPP samples shared the same diffraction pattern, and OCP

  12. Significados Atribuídos ao Lazer na Terceira Idade: Observação Participante em Encontros Musicais

    Directory of Open Access Journals (Sweden)

    Fábio Francisco de Araujo

    2016-10-01

    Full Text Available Este estudo buscou investigar os significados atribuídos ao lazer em grupo por consumidores idosos. O estudo parte de uma revisão da literatura sobre consumo e lazer na Terceira Idade, enfatizando a passagem de uma perspectiva negativa, baseada em restrições ao consumo, para uma visão mais positiva do envelhecimento, nos estudos mais recentes. A pesquisa utilizou métodos oriundos da etnografia urbana, em particular a observação participante e as entrevistas em profundidade, adequados à natureza do fenômeno investigado. Foi escolhido, para a realização do trabalho de campo, um grupo de encontros musicais que se reúne no Palácio do Catete, no Rio de Janeiro. No decorrer da observação participante foram realizadas entrevistas informais com participantes, registradas em diário de campo, além do uso de fotografias e vídeos. Ao final da observação participante, que durou seis meses, foram realizadas 16 entrevistas em profundidade, gravadas e transcritas. Utilizaram-se técnicas de análise de discurso. Seis diferentes categorias de significados emergiram do trabalho de campo: (1 significado hedônico; (2 espaço de sociabilidade; (3 nostalgia; (4 qualidade de vida; (5 (reconstrução da identidade e; (6 aprendizado. Verificou-se que a imersão nesta atividade de lazer permitiu aos idosos participantes produzirem uma ressignificação da Terceira Idade.

  13. Infecção urinária comunitária: etiologia segundo idade e sexo

    Directory of Open Access Journals (Sweden)

    Denise Swei Lo

    2013-06-01

    Full Text Available INTRODUÇÃO: A escolha do antimicrobiano para tratamento inicial de infecção de trato urinário (ITU costuma ser empírica e deve considerar a prevalência dos uropatógenos nas diversas faixas etárias e sexo. OBJETIVO: Avaliar a prevalência de uropatógenos em ITU comunitária e sua relação com idade e sexo. MÉTODOS: Estudo transversal conduzido em pronto socorro (PS de hospital geral, de janeiro a dezembro, 2010, em pacientes menores de 15 anos com suspeita clínica de ITU, que colheram urocultura quantitativa. Definida ITU como urocultura com crescimento de agente único > 100.000 unidades formadoras de colônia (ufc/mL na coleta por jato médio ou > 50.000 ufc/mL na coleta por sondagem vesical. RESULTADOS: Ocorreram 63.464 atendimentos no PS. Foram obtidas 2.577 uroculturas; destas, 291 foram positivas para ITU (prevalência = 11,3% das suspeitas clínicas e 0,46% dos atendimentos; 212 casos (72,8% em meninas, mediana de idade = 2,6 anos. O uropatógeno predominante foi E.coli (76,6%, seguido por Proteus mirabilis (10,3% e Staphylococcus saprophyticus (4,1%. Em lactentes 10 anos (24,4% x 0,4%; OR = 79,265; p 10 anos e de Proteus mirabilis em meninos.

  14. Carrier phases for iodine in the Allende meteorite and their associated 129Xer/127I ratios: A laser microprobe study

    International Nuclear Information System (INIS)

    Kirschbaum, C.

    1988-01-01

    A new mass spectrometer of high sensitivity coupled to a laser microprobe sample extraction system was used to determine the 129 Xe r /I ratios of minerals which carry 129 Xe r in the Allende meteorite. In sodalite-rich fine-grained inclusions Ok correlates with Cl verifying that sodalite carries the majority of I. One sample heated above the decomposition point of sodalite had a small amount of residual I indicating the presence of at least one other carrier. The Cl/I ratio of the matrix was different from that of the fine-grained inclusions and the 129 Xe r correlates with trapped Xe. This implies either a different Cl/I ratio for sodalite in the matrix or a different carrier for I in matrix. In melilite from one coarse-grained inclusion, I is variable and correlates with both Xe and, surprisingly, 131 Xe produced from Ba during the irradiation. In coarse-grained inclusions with Cl-rich alteration products in cracks, most of the 129 Xe r is found in those cracks. A residual amount of 129 Xe r is present in melilite samples which show no Cl-rich alteration products, and is a trace impurity in the melilite. The 129 Xe r / 127 I ratio of sodalite from the fine-grained inclusions, and matrix is similar--between 1.25 and 1.35 x 10 -4 . This implies an age for these samples within 2 million years of a Bjurbole chondrule included in the irradiation as a standard. The 129 Xe r / 127 I ratio of a sample of a fine-grained inclusion heated to 1,100 degree C is 2.4 x 10 -4 or 16 million years before the Bjurbole chondrule. A coarse-grained inclusion on the other hand showed a 129 Xe r / 127 I ratio of 3.15 x 10 -5 or 35 million years after the Bjurbole chondrule

  15. Life habitability in the solar system: testing the universality of biology on Europa with microprobes or lander

    International Nuclear Information System (INIS)

    Chela-Flores, J.

    2007-05-01

    We discuss whether it is possible to test the universality of biology, a quest that is of paramount relevance for one of its most recent branches, namely astrobiology. We review this topic in terms of the relative roles played on the Earth biota by contingency and evolutionary convergence. We raise the related question of whether the molecular events that were precursors to the origin of life on Earth are bound to occur elsewhere in the solar system, wherever the environmental conditions are similar to the terrestrial ones. The set of hypotheses for addressing the question of the universality of biology can be tested by future experiments that are feasible with current technology. We focus on landing on the Jovian satellite Europa and its broader implications, including selecting a landing site. We also discuss the corresponding miniaturized equipment that is already in existence. The second objective is to discuss in more detail whether sulphur traces on Jupiter's moon Europa could be of biogenic origin, and could be tested with the present level of technology readiness. To achieve reliable biosignatures in the solar system in the foreseeable future, it seems essential to go back to Europa, in addition to continuing the multiple well-funded Mars programmes. Our work highlights the type of biogenic signatures that can be searched, when probing Europa's icy and patchy surface. Definite answers can be retrieved in situ on the icy surface with instrumentation for the corresponding biogeochemistry. The measurements can be performed by, for instance, microprobes, or by landers (of the type of the original JPL studies that sadly have been suspended). Such on-site measurements could make a modest contribution to the overall question of settling one of the most significant problems in astrobiology, namely the origin of the surficial sulphur on Europa. (author)

  16. Micro-PIXE on thin plant tissue samples in frozen hydrated state: A novel addition to JSI nuclear microprobe

    International Nuclear Information System (INIS)

    Vavpetič, P.; Pelicon, P.; Vogel-Mikuš, K.; Grlj, N.; Pongrac, P.; Jeromel, L.; Ogrinc, N.; Regvar, M.

    2013-01-01

    Recently we completed a construction of a cryostat at Jožef Stefan Institute (JSI) nuclear microprobe enabling us to analyze various types of biological samples in frozen hydrated state using micro-PIXE/STIM/RBS. Sample load-lock system was added to our existing setup to enable us to quickly insert a sample holder with frozen hydrated tissue samples onto a cold goniometer head cooled with liquid nitrogen inside the measuring chamber. Cryotome-cut slices of frozen hydrated plant samples were mounted between two thin silicon nitride foils and then attached to the sample holder. Sufficient thermal contact between silicon nitride foils and sample holder must be achieved, as well as between the sample holder and the cold goniometer head inside the measuring chamber to prevent melting of the samples. Matrix composition of frozen hydrated tissue is consisted mostly of ice. Thinning of the sample as well as water evaporation during high vacuum and proton beam exposure was inspected by the measurements with RBS and STIM method simultaneously with micro-PIXE. For first measuring attempts a standard micro-PIXE configuration for tissue mapping was used with proton beam cross section of 1.2 × 1.2 μm 2 and a beam current of 100 pA. The temperature of the cold goniometer head was kept below 130 K throughout the entire proton beam exposure. First measurements of thin plant tissue samples in frozen hydrated state show minute sample degradation during the 10 h period of micro-PIXE measurements

  17. Elemental distribution and sample integrity comparison of freeze-dried and frozen-hydrated biological tissue samples with nuclear microprobe

    Energy Technology Data Exchange (ETDEWEB)

    Vavpetič, P., E-mail: primoz.vavpetic@ijs.si [Jožef Stefan Institute, Jamova 39, SI-1000 Ljubljana (Slovenia); Vogel-Mikuš, K. [Biotechnical Faculty, Department of Biology, University of Ljubljana, Jamnikarjeva 101, SI-1000 Ljubljana (Slovenia); Jeromel, L. [Jožef Stefan Institute, Jamova 39, SI-1000 Ljubljana (Slovenia); Ogrinc Potočnik, N. [Jožef Stefan Institute, Jamova 39, SI-1000 Ljubljana (Slovenia); FOM-Institute AMOLF, Science Park 104, 1098 XG Amsterdam (Netherlands); Pongrac, P. [Biotechnical Faculty, Department of Biology, University of Ljubljana, Jamnikarjeva 101, SI-1000 Ljubljana (Slovenia); Department of Plant Physiology, University of Bayreuth, Universitätstr. 30, 95447 Bayreuth (Germany); Drobne, D.; Pipan Tkalec, Ž.; Novak, S.; Kos, M.; Koren, Š.; Regvar, M. [Biotechnical Faculty, Department of Biology, University of Ljubljana, Jamnikarjeva 101, SI-1000 Ljubljana (Slovenia); Pelicon, P. [Jožef Stefan Institute, Jamova 39, SI-1000 Ljubljana (Slovenia)

    2015-04-01

    The analysis of biological samples in frozen-hydrated state with micro-PIXE technique at Jožef Stefan Institute (JSI) nuclear microprobe has matured to a point that enables us to measure and examine frozen tissue samples routinely as a standard research method. Cryotome-cut slice of frozen-hydrated biological sample is mounted between two thin foils and positioned on the sample holder. The temperature of the cold stage in the measuring chamber is kept below 130 K throughout the insertion of the samples and the proton beam exposure. Matrix composition of frozen-hydrated tissue is consisted mostly of ice. Sample deterioration during proton beam exposure is monitored during the experiment, as both Elastic Backscattering Spectrometry (EBS) and Scanning Transmission Ion Microscopy (STIM) in on–off axis geometry are recorded together with the events in two PIXE detectors and backscattered ions from the chopper in a single list-mode file. The aim of this experiment was to determine differences and similarities between two kinds of biological sample preparation techniques for micro-PIXE analysis, namely freeze-drying and frozen-hydrated sample preparation in order to evaluate the improvements in the elemental localisation of the latter technique if any. In the presented work, a standard micro-PIXE configuration for tissue mapping at JSI was used with five detection systems operating in parallel, with proton beam cross section of 1.0 × 1.0 μm{sup 2} and a beam current of 100 pA. The comparison of the resulting elemental distributions measured at the biological tissue prepared in the frozen-hydrated and in the freeze-dried state revealed differences in elemental distribution of particular elements at the cellular level due to the morphology alteration in particular tissue compartments induced either by water removal in the lyophilisation process or by unsatisfactory preparation of samples for cutting and mounting during the shock-freezing phase of sample preparation.

  18. REVISÃO DE ESTUDOS SOBRE DETERMINAÇÃO DA IDADE ATRAVÉS DE OTÓLITOS DOS PEIXES MARINHOS BRASILEIROS

    Directory of Open Access Journals (Sweden)

    Mônica Rocha Oliveira

    2014-10-01

    Full Text Available Neste trabalho foi revisada a idade de 35 espécies de peixes marinhos da região costeira do Brasil. Um total de 42 artigos foi utilizado, sendo os dados categorizados de acordo com a década de publicação, par de otólitos usados para estimar a idade, métodos de validação, causas da formação do anel etário e a idade dos peixes. Os resultados mostram um aumento em número de estudos realizados em relação a idade e crescimento dos peixes marinhos. O par de otólito sagittae foi o mais utilizado para estudos de estimação de idade. Em geral, as marcas de crescimento nos otólitos foram relacionadas com a atividade reprodutiva dos peixes e a temperatura. Foram encontrados de 1 a 76 anéis (média=16 nos peixes marinhos do Brasil. Podemos concluir com essa revisão que é possível estimar a idade de peixes que habitam ambientes marinhos tropicais através de otólitos. É de fundamental importância para os estudos biológicos básicos que fornecem subsídios para tomadas de medidas na gestão e conservação dos estoques naturais de peixes. Palavras-chave: anéis de crescimento, crescimento, sagittae, região costeira brasileira, recursos pesqueiros. DOI: http://dx.doi.org/10.18561/2179-5746/biotaamazonia.v4n3p125-131

  19. Surface characterization by energy distribution measurements of secondary electrons and of ion-induced electrons

    International Nuclear Information System (INIS)

    Bauer, H.E.; Seiler, H.

    1988-01-01

    Instruments for surface microanalysis (e.g. scanning electron or ion microprobes, emission electron or ion microscopes) use the current of emitted secondary electrons or of emitted ion-induced electrons for imaging of the analysed surface. These currents, integrating over all energies of the emitted low energy electrons, are however, not well suited to surface analytical purposes. On the contrary, the energy distribution of these electrons is extremely surface-sensitive with respect to shape, size, width, most probable energy, and cut-off energy. The energy distribution measurements were performed with a cylindrical mirror analyser and converted into N(E), if necessary. Presented are energy spectra of electrons released by electrons and argon ions of some contaminated and sputter cleaned metals, the change of the secondary electron energy distribution from oxidized aluminium to clean aluminium, and the change of the cut-off energy due to work function change of oxidized aluminium, and of a silver layer on a platinum sample. The energy distribution of the secondary electrons often shows detailed structures, probably due to low-energy Auger electrons, and is broader than the energy distribution of ion-induced electrons of the same object point. (author)

  20. Estrabismo em idade ambliogénica: estudo retrospectivo de 12 meses consecutivos de referenciação oftalmológica hospitalar

    OpenAIRE

    Monteiro, Sílvia

    2017-01-01

    Introdução: O objectivo deste trabalho é a análise do estado actual da referenciação oftalmológica hospitalar de casos de estrabismo em idade pediátrica.Métodos: Estudo retrospectivo e descritivo dos processos clínicos das crianças com idade menor ou igual a 10 anos referenciadas à Consulta de Oftalmologia Pediátrica do Centro Hospitalar do Porto entre Julho de 2011 e Julho de 2012.Resultados: Das 649 crianças referenciadas, 267 (41.1%) foram por suspeita de estrabismo. Em 109 (40.8%) dessas ...

  1. Um olhar sobre o crime de pedopornografia : importância do uso de fotografia da face na estimativa da idade

    OpenAIRE

    Alves, Sindia Gabriela Pereira

    2014-01-01

    A estimativa da idade de vítimas de pedopornografia tem vindo a desempenhar um papel essencial na prática forense, devido ao elevado número de casos de pornografia infantil observado nas últimas décadas. No sentido de tentar combater este problema, vários peritos são chamados a depor em tribunal. Tendo em mente o propósito do presente projecto, na verificação da importância do uso de fotografias da face, na estimativa da idade em casos de pedopornografia, procedeu-se à análi...

  2. Mulheres em idade fértil: causas de internação em Unidade de Terapia Intensiva e resultados

    OpenAIRE

    Cátia Millene Dell Agnolo; Angela Andréia França Gravena; Tiara Cristina Romeiro-Lopes; Sheila Cristina Rocha-Brischiliari; Maria Dalva de Barros Carvalho; Sandra Marisa Pelloso

    2014-01-01

    Introdução: Pacientes obstétricas representam uma fração significativa das admissões em unidades de cuidado intensivo e consistem em um desafio para a equipe. Objetivo: Analisar as principais causas de internação e morte materna de mulheres em idade fértil ocorridas em unidades de terapia intensiva de hospitais de um município do Noroeste do Paraná, Sul do Brasil. Métodos: Estudo exploratório, descritivo, retrospectivo, realizado com mulheres em idade fértil (10 a 49 anos) internadas em três ...

  3. Padrão alimentar, nutricional e estilos de vida relacionados com a degenerescência macular relacionada com a idade na população portuguesa

    OpenAIRE

    Barreto, Patrícia Susana Correia Lopes

    2016-01-01

    Dissertação de mestrado em Saúde Pública, apresentada à Faculdade de Medicina da Universidade de Coimbra Introdução e Objetivos: A Degenerescência Macular Relacionada com a Idade (DMI) é uma das principais causas de perda de visão central e cegueira a nível mundial em indivíduos com idade superior a 55 anos. A prevalência mundial dos estadios iniciais da DMI foi estimada em 8,01% e a dos estadios tardios em 0,37%. Atualmente, o tratamento da DMI continua limitado às formas tard...

  4. Judicialização da política pública de assistência farmacêutica e eqüidade "Judicialization" of public health policy for distribution of medicines

    Directory of Open Access Journals (Sweden)

    Ana Luiza Chieffi

    2009-08-01

    Full Text Available O fornecimento de medicamentos por ação judicial, pela Secretaria de Estado da Saúde de São Paulo (SES-SP, tornou-se uma prática rotineira e cada vez mais freqüente. A judicialização do sistema de saúde entra em confronto com princípios básicos do SUS, como o da eqüidade. Este trabalho caracterizou as demandas judiciais para obtenção de medicamentos sob a ótica da judicialização da política pública e da quebra do princípio da eqüidade na dimensão coletiva. O estudo é um trabalho descritivo dos processos judiciais de solicitação de medicamentos à SES-SP relacionados no Sistema de Controle Jurídico (SCJ no ano 2006. A maioria das ações analisadas foi ajuizada por advogados particulares; 47% dos pacientes possuíam receitas da rede privada e cerca de 73% dos processos foram provenientes de pacientes residentes nos três estratos de menor vulnerabilidade social do Município de São Paulo, Brasil. Os dados demonstram que essas demandas judiciais não respeitam princípios do SUS como o da eqüidade, privilegiando indivíduos com melhor poder aquisitivo e com acesso à informação.The supply of medicines in response to court orders or injunctions has become a common practice in the State of São Paulo, Brazil. This "judicialization" of the health system clashes with basic principles of the Brazilian Unified National Health System (SUS, such as equal opportunity to access health services. The aim of this paper is to analyze the legal action used to obtain medicines through the São Paulo State Health Department, from two main angles: judicialization of public policies and breach of the equity principle. This is a descriptive study of legal action taken to obtain medicines through the São State Health Department, as listed in the Electronic Court Docket System for the year 2006. Most cases were filed through private attorneys; 47% of the patients had obtained their prescriptions through private care; and 73% of the cases

  5. Influência da idade e do estresse cíclico de calor no perfil bioquímico sérico em frangos de corte

    Directory of Open Access Journals (Sweden)

    João Paulo Rodrigues Bueno

    2017-06-01

    Full Text Available Objetivou-se avaliar a influência da idade e do estresse cíclico por calor durante uma hora por dia, nas concentrações das proteínas, metabólitos e enzimas séricas em frangos de corte de 21 a 42 dias de idade. Foram utilizados 420 pintos de corte machos, da linhagem Cobb Avian48TM, em um delineamento inteiramente casualizado, composto de dois tratamentos e seis repetições. Os tratamentos foram constituídos de dois ambientes térmicos: um para frangos de corte criados em condições naturais de temperatura e umidade do primeiro ao 42° dia de idade (controle; e outro para estressados por calor à 36 °C do 16° ao 42° dia, durante uma hora do dia (12h00m às 13h00m. No 21º, 28º, 35º e 42º dias de idade, foram coletados em duas aves por repetição aproximadamente 5mL de sangue por punção cardíaca. Foram determinadas em cada amostra de soro as concentrações de proteína total, albumina, globulinas, relação A/G, aspartato aminotransferase, alanina aminotransferase, gama glutamiltransferase, ácido úrico, creatinina, colesterol total, triacilgliceróis, lipoproteínas de alta densidade, lipoproteínas de muito baixa densidade, lipoproteínas de baixa densidade e glicose. Para as concentrações de glicose, ácido úrico, alanina aminotransferase, triacilgliceróis e lipoproteínas de muito baixa densidade, não houve diferenças significativas para ambiente e idade. Observou-se interação significativa entre ambiente e idade para os valores de colesterol e lipoproteínas de baixa densidade. Aos 21 dias de idade o colesterol e as LDL-C foram maiores nas aves em estresse comparados àquelas do tratamento controle, o que não ocorreu nas demais idades. A aspartato aminotransferase nos frangos sob estresse cíclico de calor foi maior em comparação ao tratamento controle e apresentou efeito cúbico para ambiente. A idade das aves influenciou os valores de proteínas totais, albumina, globulina, albumina: globulina, creatinina

  6. The laser microprobe mass analyser for determining partitioning of minor and trace elements among intimately associated macerals: an example from the Swallow Wood coal bed, Yorkshire, UK

    Science.gov (United States)

    Lyons, P.C.; Morelli, J.J.; Hercules, D.M.; Lineman, D.; Thompson-Rizer, C. L.; Dulong, F.T.

    1990-01-01

    A study of the elemental composition of intimately associated coal macerals in the English Swallow Wood coal bed was conducted using a laser microprobe mass analyser, and indicated a similar trace and minor elemental chemistry in the vitrinite and cutinite and a different elemental signature in the fusinite. Three to six sites were analysed within each maceral during the study by laser micro mass spectrometry (LAMMS). Al, Ba, Ca, Cl, Cr, Dy, F, Fe, Ga, K, Li, Mg, Na, S, Si, Sr, Ti, V, and Y were detected by LAMMS in all three macerals but not necessarily at each site analysed. The signal intensities of major isotopic peaks were normalized to the signal intensity of the m z 85 peak (C7H) to determine the relative minor- and trace-element concentrations among the three dominant macerals. The vitrinite and the cutinite were depleted in Ba, Ca, Dy, Li, Mg, Sr, and Y relative to their concentrations observed in the fusinite. The cutinite was distinguished over vitrinite by less Ti, V, Cr and Ca, and K Ca $ ??1 (relative signal intensities). The fusinite, relative to the cutinite and vitrinite, was relatively depleted in Cr, Sc, Ti, and V. The fusinite, as compared with both the cutinite and vitrinite, was relatively enriched in Ba, Ca, Dy, Li, Mg, Sr, and Y, and also showed the most intense m z 64, 65, 66 signals (possibly S2+, HS2+, H2S2+, respectively). The LAMMS data indicate a common source for most elements and selective loss from the maceral precursors in the peat or entrapment of certain elements as mineral matter, most likely during the peat stage or during early diagenesis. The relatively high amounts of Ba, Ca, Dy, Li, Mg, Sr, and Y in the fusinite are consistent with micron and submicron mineral-matter inclusions such as carbonates and Ca-Al phosphates (probably crandallite group minerals). Mineralogical data on the whole coal, the LAMMS chemistry of the vitrinite and cutinite, and scanning electron microscopy/energy dispersive X-ray analysis (SEM/EDAX) of

  7. OFICINAS SOBRE QUEDAS E ACIDENTES DOMÉSTICOS GERAIS EM PESSOAS IDOSAS NO PROGRAMA UniversIDADE

    Directory of Open Access Journals (Sweden)

    Jane Kelly Oliveira Friestino

    2016-08-01

    Full Text Available O envelhecimento é um processo normal do desenvolvimento do ser humano, caracterizado por mudanças fisiológicas (senescência ou patológicas (senilidade. Com o avançar da idade, as comorbidades podem estar presentes no idoso. O desempenho das atividades de vida diária fica prejudicado e, devido a alterações sensório-motoras, cognitivas e psicossociais, aumenta a vulnerabilidade para a ocorrência de quedas e acidentes domésticos, comprometendo a capacidade funcional e podendo levar à morte. O objetivo deste trabalho é apresentar o relato de experiência do oferecimento de oficinas intituladas: “Acidentes domésticos com pessoa idosa: prevenção e ação” a um grupo de idosos participantes de um programa específico para essa faixa etária. As oficinas foram ofertadas como parte do Programa de Extensão Universitária–UniversIDADE de uma Universidade pública do interior de São Paulo. Os encontros da oficina foram realizados entre maio e agosto de 2015, com duração de uma hora cada encontro, totalizando sete encontros. Uma enfermeira e uma fisioterapeuta foram mediadoras voluntárias. Os temas abordados foram: quedas, alterações sensoriais, estratégias de prevenção e ação em acidentes domésticos, queimaduras e hemorragias. Quanto aos resultados das oficinas destacaram-se a participação ativa dos idosos nas discussões dos temas abordados e a relevância dos mesmos para a prevenção dos acidentes domésticos e da ocorrência de queda. Considerou-se importante a atuação dos idosos como agentes multiplicadores das informações adquiridas nas atividades, com extensão aos seus familiares, a outros idosos de seu convívio e para sua própria qualidade de vida. Palavras-chave: Extensão Universitária, Relações Comunidade-Instituição, Acidentes domésticos, Prevenção, Saúde do Idoso.   Workshops on falls and general domestic accidents in elderly people in the UniversIDADE Program Abstract: Aging is a natural

  8. Technique Development to Support Clean-up and/or Disposal of Actinide Contaminated Soils and Sediments: Coupling Fission Tract Analysis with Synchroton X-ray Microprobe Analysis

    International Nuclear Information System (INIS)

    Sue Clark

    2003-01-01

    The overall goal of this project was to develop quantitative FTA to provide images of the microscale spatial distributions of high fissile actinides sorbed to environmental particles such as sediments and colloids. We developed methods to provide absolute actinide surface concentrations on the particles, regardless of particle size. We are also working to provide particle size information by our approach. We also coupled our newly devised FTA methods with the quantitative determination of stable element distributions in the same particles using synchrotron x-ray microprobe analysis

  9. Laser microprobe mass analysis (LAMMA) of aluminum and lead in fine roots and their ectomycorrhizal mantles of Norway spruce (Picea abies (L.) Karst.).

    Science.gov (United States)

    Eeckhaoudt, S; Vandeputte, D; Van Praag, H; Van Grieken, R; Jacob, W

    1992-03-01

    Fine roots and ectomycorrhizal root tips were sampled in a Norway spruce (Picea abies (L.) Karst.) stand in the eastern part of the Belgian Ardennes. The cellular and partly subcellular localizations of aluminum and lead were identified by the micro-analytical laser microprobe mass analysis (LAMMA) technique. In fine roots with secondary structure, localization of aluminum was limited to the peripheral cell layers. Lead was found in the outer layers, and also in the primary phloem. Aluminum penetrated the mycorrhizal mantle, but lead was seldom detected in ectomycorrhizae.

  10. Progress in element analysis on a high-voltage electron microscope

    International Nuclear Information System (INIS)

    Tivol, W.F.; Barnard, D.; Guha, T.

    1985-01-01

    X-Ray microprobe (XMA) and electron energy-loss (EELS) spectrometers have been installed on the high-voltage electron microscope (HVEM). The probe size has been measured and background reduction is in progress for XMA and EELS as are improvements in electron optics for EELS and sensitivity measurements. XMA is currently useful for qualitative analysis and has been used by several investigators from our laboratory and outside laboratories. However, EELS background levels are still too high for meaningful results to be obtained. Standards suitable for biological specimens are being measured, and a library for quantitative analysis is being compiled

  11. A new standardless quantitative electron probe microanalysis technique applied to III-V compound semiconductors

    International Nuclear Information System (INIS)

    Zangalis, K.P.; Christou, A.

    1982-01-01

    The present paper introduces a new standardless quantitative scheme for off-line electron microprobe analysis applications. The analysis is based on standard equations of the type Isub(i)=Csub(i)fsub(ZAF)βsub(i) and is specifically suitable for compound semiconductors. The roots to the resultant nth-degree polynomial are the unknown concentrations. Methods for computing Csub(i) when coefficients βsub(i) are unknown are also outlined. Applications of standardless analysis to GaAs and InP specimens are compared with results obtained by Auger electron spectroscopy and quantitative electron probe analysis with standards. (Auth.)

  12. Teoria da Mente: efeito da idade, do sexo e do uso de atores animados e inanimados na inferência de estados mentais

    Directory of Open Access Journals (Sweden)

    Roazzi Antonio

    1999-01-01

    Full Text Available O estudo foi realizado com 72 crianças de NSE médio, entre quatro e cinco anos de idade, visando a investigar a idade de aquisição da habilidade das crianças para distinguirem seus próprios estados mentais e os estados mentais de outros e se a manifestação da habilidade, na tarefa de falsa crença, depende do ator envolvido - inanimado (boneca versus animado (outras crianças. Os resultados indicaram não haver diferenças entre atores animados e inanimados e que é a partir de cinco anos de idade que as crianças começam a ter uma compreensão acerca dos estados mentais de outras pessoas, no tocante a falsa crença. Este último dado diverge dos obtidos em estudos anteriores, que encontraram esta capacidade já desenvolvida aos quatro anos de idade. Contrariamente à hipótese inatista e de acordo com os dados obtidos no Brasil (no que se refere às crianças de orfanato nossos resultados revelam que a universalidade quanto à época em que se encontra desenvolvida esta capacidade é passível de ser questionada.

  13. High-density volatiles in the system C-O-H-N for the calibration of a laser Raman microprobe

    Science.gov (United States)

    Chou, I.-Ming; Pasteris, J.D.; Seitz, J.C.

    1990-01-01

    Three methods have been used to produce high-density volatiles in the system C-O-H-N for the calibration of a laser Raman microprobe (LRM): synthetic fluid-inclusion, sealed fused-quartz-tube, and high-pressure-cell methods. Because quantitative interpretation of a Raman spectrum of mixed-volatile fluid inclusions requires accurate knowledge of pressure- and composition-sensitive Raman scattering efficiencies or quantification factors for each species, calibrations of these parameters for mixtures of volatiles of known composition and pressure are necessary. Two advantages of the synthetic fluid-inclusion method are that the inclusions can be used readily in complementary microthermometry (MT) studies and that they have sizes and optical properties like those in natural samples. Some disadvantages are that producing H2O-free volatile mixtures is difficult, the composition may vary from one inclusion to another, the exact composition and density of the inclusions are difficult to obtain, and the experimental procedures are complicated. The primary advantage of the method using sealed fused-quartz tubes is its simplicity. Some disadvantages are that exact compositions for complex volatile mixtures are difficult to predict, densities can be approximated only, and complementary MT studies on the tubes are difficult to conduct. The advantages of the high-pressure-cell method are that specific, known compositions of volatile mixtures can be produced and that their pressures can be varied easily and are monitored during calibration. Some disadvantages are that complementary MT analysis is impossible, and the setup is bulky. Among the three methods for the calibration of an LRM, the high-pressure-cell method is the most reliable and convenient for control of composition and total pressure. We have used the high-pressure cell to obtain preliminary data on 1. (1) the ratio of the Raman quantification factors for CH4 and N2 in an equimolar CH4N2 mixture and 2. (2) the

  14. Idade da matriz e tempo de estocagem dos ovos no desempenho e rendimento de carcaça de frangos de corte

    Directory of Open Access Journals (Sweden)

    Nayara Spindola Francisco

    2012-09-01

    Full Text Available Este trabalho teve o objetivo de avaliar a influência da idade da matriz e o tempo de estocagem dos ovos sobre o desempenho e rendimento de carcaça de frangos de corte criados até aos 42 dias de idade. Para isto, utilizou-se 2916 pintos de corte machos da linhagem Ross 308® onde foram avaliados: peso médio inicial (PMI, peso médio final (PMF, ganho de peso médio (GPM, consumo de ração (CRM, conversão alimentar (CA, mortalidade (MORT e rendimento de carcaça. Utilizou-se delineamento inteiramente casualizado em esquema fatorial 3x3, referente à três idades das matrizes (33, 43 e 61 semanas e três períodos de estocagem dos ovos (24, 72 e 120 horas. Na fase de 1 a 7 dias de idade, houve interação (p0,05. Na fase de 1 a 35 dias, o PMF, GPM e MORT não foram influenciados (p>0,05. Para CRM e CA houve interação (p0,05 pelos tratamentos. Para CA, houve interação, assim como a MORT, já o rendimento de carcaça não apresentou interação entre os fatores. Nas condições em que foi conduzido este trabalho, conclui-se que frangos de corte tendem a apresentar melhores resultados de desempenho de 1 a 7 dias de idade quando oriundos de matrizes mais velhas (com 61 semanas de idade e ovos estocados por período de até 72 horas. No entanto, estes resultados são diluídos com o aumento da idade dos frangos até os 42 dias não influenciando no rendimento de carcaça ao abate.

  15. Características de carcaça de cordeiros Suffolk abatidos em diferentes idades Carcass characteristics of Suffolk lambs slaughtered at different ages

    Directory of Open Access Journals (Sweden)

    Mauro Sartori Bueno

    2000-12-01

    Full Text Available Foram avaliadas as proporções dos componentes não-carcaça e as características de carcaça de 35 cordeiros Suffolk, abatidos com idades médias de 90, 130 ou 170 dias, alimentados com silagem de milho e ração concentrada (19,6% de PB. O aumento da idade de abate acarretou incremento linear dos pesos de abate e de carcaça e diminuição linear na proporção de alguns componentes não-carcaça, como sangue, cabeça, patas e vísceras cheias, o que resultou em aumento linear do rendimento de carcaça. As proporções dos componentes da carcaça foram alteradas pelo aumento da idade de abate, observando-se aumento linear na porcentagem de gordura, diminuição linear na de ossos e nenhuma alteração na de músculos. Os cortes efetuados nas carcaças mostraram diminuição linear da porcentagem de traseiro, nenhuma alteração na de dianteiro e aumento linear na de costilhar, com o aumento da idade de abate. As medidas de carcaça e compacidade mostraram aumento linear com o aumento da idade de abate. A idade de abate de cordeiros Suffolk criados intensivamente para produzir carcaças adequadas ao mercado consumidor da região Centro-Sul do Brasil fica entre 110 e 130 dias de idade.The effect of slaughter age on non-carcass components and carcass characteristics was evaluated in 35 Suffolk lambs slaughtered at average age of 90, 130 or 170 days, fed corn silage and concentrate (19.6% CP. As the slaughter age increased, animal live weight and carcass weight linearly increased, and some non-carcass components as blood, head, legs and full viscera percentage linearly decreased, leading to a linear increase in carcass yield. As the slaughter age increase, it was observed change in the proportion of carcass components with a linear increase of fat percentage, a linear decrease in bones percentage and no change in the muscle percentage. A linear decrease in the hindquarter, a linear increase in the ribs and no change in the forequarter carcass

  16. Lisina digestível para frangos de corte machos entre 12 e 22 dias de idade

    Directory of Open Access Journals (Sweden)

    P Takeara

    2010-12-01

    Full Text Available Avaliou-se nível de lisina digestível para 1050 frangos de corte dos 12 aos 22 dias de idade. O delineamento experimental foi inteiramente ao acaso, com cinco tratamentos, sete repetições e 30 aves por unidade experimental. Os tratamentos foram: 1,05; 1,10; 1,15; 1,20 e 1,25% de lisina digestível. Avaliaram-se ganho de peso, consumo de ração, conversão alimentar, composição e deposição de nutrientes corporais. Foram constatados efeitos quadráticos de lisina digestível no consumo de ração e resposta linear ascendente no peso da carcaça. Na composição química da carcaça, houve resposta quadrática do nível de lisina na concentração de proteína. As taxas de deposição proteica, deposição de água, da carcaça e do corpo total tiveram aumento linear em resposta ao acréscimo de lisina na dieta. O aumento da concentração de lisina, todavia, coincidiu com a redução da matéria mineral nas vísceras e sangue e no corpo total. Considerado o desempenho, o nível 1,1% de lisina digestível atendeu às necessidades do frango de corte entre o 12º e o 22º dia de idade. Consideradas a composição química e as taxas de deposição dos nutrientes corporais, a demanda pelo aminoácido digestível torna-se igual ou maior que 1,25%

  17. A restrição do crescimento fetal influencia a composição corporal na idade escolar?

    Directory of Open Access Journals (Sweden)

    Marilia C. Lima

    2011-02-01

    Full Text Available OBJETIVO: Verificar a influência do baixo peso de crianças nascidas a termo sobre a composição corporal na idade escolar. MÉTODO: Este estudo consistiu de um corte transversal aninhado em uma coorte de 375 crianças recrutadas ao nascimento em 1993-1994 no estado de Pernambuco. Aos 8 anos de idade, 213 crianças tiveram a composição corporal avaliada através da mensuração da espessura das pregas cutâneas tricipital e subescapular e da circunferência do braço. A regressão linear multivariada foi utilizada para identificar a influência do baixo peso ao nascer, das condições socioeconômicas, do estado nutricional materno e morbidade da criança na prega cutânea tricipital. RESULTADOS: As médias das pregas cutâneas tricipital e subescapular, da circunferência do braço e das áreas muscular e de gordura do braço foram menores nas crianças nascidas com baixo peso em relação às nascidas com peso adequado; no entanto, essas diferenças não foram estatisticamente significantes. Na análise de regressão linear multivariada, as variáveis socioeconômicas explicaram o maior percentual da variação da prega cutânea tricipital (12,3%, especialmente a renda familiar per capita (9,1%, seguida da ocorrência de anemia e da hospitalização anterior, que juntas explicaram 5,6%, e do índice de massa corporal materna, que contribuiu com 2,4% dessa variação. O baixo peso ao nascer não influenciou no depósito de gordura subcutânea tricipital nessa faixa etária. CONCLUSÃO: Os fatores socioeconômicos e a morbidade anterior da criança apresentaram uma maior influência na composição corporal de escolares nascidos a termo em detrimento do baixo peso ao nascer.

  18. Comparação entre metodologias de idade-período-coorte para o estudo de uma medida da progressão escolar no Brasil

    Directory of Open Access Journals (Sweden)

    Raquel Rangel de Meireles Guimarães

    2011-12-01

    Full Text Available Este artigo procura realizar um exercício de comparação metodológica de dois estimadores dos modelos idade-período-coorte: o estimador convencional obtido pelos modelos lineares generalizados restritos (MLGR; e o estimador intrínseco (EI. O objeto de interesse são as contribuições dos efeitos de idade, período e coorte nas mudanças temporais na probabilidade de progressão (PPS para a 5ª série do ensino fundamental das mulheres brasileiras. A modelagem IPC se justifica uma vez que os efeitos de idade, período e coorte podem impactar de forma significativa a probabilidade de progressão escolar: efeitos de idade refletem tanto a idade mínima de entrada no sistema de ensino como também o dilema entre trabalho e estudo que surge ao longo da carreira educacional; efeitos de período estão associados às diferentes conjunturas econômica e política, bem como ao estado das políticas educacionais; por fim, efeitos de coorte refletem características sociais peculiares a determinados grupos de indivíduos. Os dois instrumentais foram contrapostos em termos da eficiência, significância e estimativa dos parâmetros. Os resultados revelam a potencialidade da solução para o modelo IPC baseada no estimador intrínseco, o qual apresenta parâmetros com variância inferior aos estimados pelo modelo linear generalizado restrito. Desta forma, projeções das PPS baseadas na extrapolação do erro-padrão dos parâmetros obtidos pelo estimador intrínseco podem ser promissoras.

  19. Aproximações à medicina monástica em Portugal na Idade Média

    Directory of Open Access Journals (Sweden)

    Dulce O. Amarante dos Santos

    2012-06-01

    Full Text Available Este texto investiga os indícios da existência de uma medicina monástica no reino de Portugal na Idade Média, antes e depois da fundação da Universidade em 1290, realizada por D. Dinis. O corpus de fontes analisado inclui regras beneditinas e agostinianas, costumeiros ou liber ordinis, catálogo das livrarias de mão do mosteiro de Santa Cruz de Coimbra, legislação conciliar. Assinala dois momentos basilares nessa história, sendo o primeiro a criação da regra beneditina no IV século, que resultou na criação de dois espaços próprios para o exercício da medicina monástica associados à prática da virtude da caridade: a enfermaria e o hospital. O segundo momento, no século XIII, constitui-se na institucionalização da escolástica médica e, ao mesmo tempo, nas tentativas de coibir a prática médica pelos religiosos nos sínodos regionais e no IV Concílio de Latrão (1215.

  20. IMUNOGLOBULINAS DO POTRO PURO SANGUE DE CORRIDA (PSC DO NASCIMENTO AO SEXTO MÊS DE IDADE

    Directory of Open Access Journals (Sweden)

    Inês Nicoloso Castro da Luz

    1992-04-01

    Full Text Available Sessenta potros PSC foram divididos em dois grupos de acordo com a ocorrência de sinais clínicos de doença. Avaliou-se os níveis de Imunoglobulina (Ig sérica das 3h até o sexto mês de idade. A TSZ pelo espectrofotômetro ou visualmente indicou bem a Ig determinada por eletroforese. A concentração de Ig decresceu no fim do primeiro mês, tanto nos doentes como nos sadios, elevando-se 1 a 2 semanas após. Isso poderia indicar a passagem da imunidade passiva para a própria. A concentração mínima de Ig de 400mg/dl sugerida na literatura não é compatível com a aqui encontrada nos potros sadios; sugere-se estabelecer um novo nível mínimo de Ig de 800mg/dl. Este pode ser considerado a exigência mínima para avaliação de potros de alto risco, no entanto, não deve ser encarado isoladamente; o ambiente e o manejo parecem desempenhar um papel bem mais importante no contexto da imunidade do que se supunha até o momento.

  1. FISIOTERAPIA AQUÁTICA COMO PREVENÇÃO DE QUEDAS NA TERCEIRA IDADE: REVISÃO DE LITERATURA

    Directory of Open Access Journals (Sweden)

    Tabada Samantha Rosa

    2013-11-01

    Full Text Available Objetivo: verificar se a fisioterapia aquática pode ser um meio preventivo na quedas dos indivíduos da terceira idade. Metodo: levantamento bibliográfico no período de janeiro de 1992 a dezembro de 2012, em artigos de idioma português e inglês, utilizando artigos de periódicos pelas bases de dados nacionais e internacionais. Foram utilizados os termos "hidroterapia”, “fisioterapia aquática”, “reabilitação aquática”, “envelhecimento”, “quedas”, “hydrotherapy”, “aquatic therapy”, “aquatic rehabilitation”, “aging”, “falls”. Considerações Finais: A literatura refere que, em idosos, o equilíbrio postural e a autonomia funcional apresentam comprometimentos. Este desequilíbrio corporal possibilita quedas. Assim, a terapia aquática possibilita independência na manutenção de posturas, fazendo com que idosos tenham melhor condição de movimentar-se. Portanto, esta conduta terapêutica, visando à prevenção da queda pela melhora da estabilidade postural, deverá influenciar, de maneira benéfica, a qualidade de vida dos idosos.

  2. Spectral Light Measurements in Microbenthic Phototrophic Communities with a Fiberoptic Microprobe Coupled to a Sensitive Diode-Array Detector Rid A-1977-2009

    DEFF Research Database (Denmark)

    KUHL, M.; JØRGENSEN, BB

    1992-01-01

    with microelectrode measurements of oxygenic photosynthesis in the coastal sediment. With an incident light intensity of 200 muEinst m-2 s-1, photon scalar irradiance reached a maximum of 283 muEinst m-2 s-1 at the sediment surface. The lower boundary of the euphotic zone was 2.2 mm below the surface at a light......A diode array detector system for microscale light measurements with fiber-optic microprobes was developed; it measures intensities of 400-900-nm light over >6 orders of magnitude with a spectral resolution of 2-5 nm. Fiber-optic microprobes to measure field radiance or scalar irradiance were...... extinction maxima in measured radiance spectra at 430-550 nm (Chl a and carotenoids), 620-625 nm (phycocyanin), 675 nm (Chl a), 745-750 nm (BChl c), 800-810 nm, and 860-880 nm (BChl a). Scalar irradiance spectra exhibited a different spectral composition and a higher light intensity at the sediment surface...

  3. Microprobe measurements to determine phase boundaries and diffusion paths in ternary phase diagrams taking a Cu-Ni-Al system as an example

    International Nuclear Information System (INIS)

    Rudolph, G.

    1983-01-01

    With the aid of quantitative microprobe tests, diffusion phenomena and phase formation in the ternary CuNiAl system at 600 - 900 0 C were investigated taking as an example the diffusion couple CuNi5Al5-nickel. The diffusion paths in the ternary system are dependent on temperature and assume an S-form in the copper corner of the phase diagram. In the copper corner, the curves swing away from the more rapid component aluminium towards the copper. Due to this non-linear course of the curves, the intermetallic theta-phase of the type (Ni,Cu) 3 Al can be observed as a layer at all temperatures in the boundary zone. At 800 0 C and to a lesser extend at 900 0 C the solubility of α-CuNi40 for aluminium, at around 5 mass-%, is higher than the value given by W.O. Alexander (1938). As far as it is possible with the diffusion couple under analysis, the microprobe measurements taken otherwise conform at 700 and 600 0 C the position of the phase boundary α-(Cu,Ni)/(α+theta)-miscibility gap indicated in W.O. Alexander (1938). (Author)

  4. Electronics and electronic systems

    CERN Document Server

    Olsen, George H

    1987-01-01

    Electronics and Electronic Systems explores the significant developments in the field of electronics and electronic devices. This book is organized into three parts encompassing 11 chapters that discuss the fundamental circuit theory and the principles of analog and digital electronics. This book deals first with the passive components of electronic systems, such as resistors, capacitors, and inductors. These topics are followed by a discussion on the analysis of electronic circuits, which involves three ways, namely, the actual circuit, graphical techniques, and rule of thumb. The remaining p

  5. Eqüidade em saúde: uma análise crítica de conceitos Health equity: a critical analysis of concepts

    Directory of Open Access Journals (Sweden)

    Ligia Maria Vieira-da-Silva

    2009-01-01

    Full Text Available A eqüidade em saúde tem sido estudada principalmente a partir de uma perspectiva epidemiológica e pouca atenção tem sido dada às questões conceituais. Em grande parte dos estudos revisados, a eqüidade tem sido utilizada como sinônimo de igualdade, e seu oposto, a iniqüidade, como sinônimo de desigualdade. As tentativas de melhor precisar seus significados têm sido, em boa parte, descritivas, com lacunas no que diz respeito à discussão das relações entre eqüidade em saúde, justiça e o processo de determinação social da saúde-doença. Neste ensaio, pretendemos analisar criticamente a série significante diversidade, diferença, desigualdade, iniqüidade, distinção no que concerne à produção da saúde-doença-cuidado em grupos sociais e suas possibilidades de articulação a uma teoria social da saúde. Nesse percurso, estaremos apoiados, por um lado, no conceito de Perelman de eqüidade e em alguns dos argumentos de Heller sobre a justiça e, por outro lado, na sociologia das práticas de Bourdieu, com o objetivo de melhor desenvolver esses conceitos, procurando discutir implicações para a formulação de políticas públicas no campo da saúde.Health inequalities have been studied mainly from an epidemiological perspective, with limited attention to conceptual issues. The terms "equity" and "equality" have often been used as synonyms, as have their opposites, "inequity" and "inequality". The few attempts to establish their meanings have been either purely descriptive or have failed to add to an understanding of the underlying dynamics in health-disease-related phenomena. The present essay explores the semantic series that includes difference, diversity, distinction, inequality, and inequity and its relationship to health phenomena in light of Perelman's concept of equity, Bourdieu's sociology, and some arguments in Heller's theory of justice, with the aim of contributing to the development of these concepts, while

  6. O Impacto da Idade Materna Avançada sobre os Resultados da Gravidez Impact of Advanced Maternal Age on the Outcome of Pregnancy

    Directory of Open Access Journals (Sweden)

    José G. Cecatti

    1998-08-01

    Full Text Available Objetivo: identificar o efeito da idade sobre os resultados maternos e perinatais das gestações ocorridas em mulheres com 40 anos ou mais. Métodos: comparamos 494 gestantes com mais de 40 anos, com 988 gestantes com idade entre 20 e 29 anos, pareando-as por paridade. Após controlar possíveis variáveis confundidoras pela análise multivariada, a idade materna avançada manteve associação com a maior prevalência de hipertensão arterial, apresentação anômala, parto por cesária, hemorragia puerperal, índice de Apgar baixo, morte perinatal, natimortalidade e sofrimento fetal intraparto. Resultados: a idade materna avançada esteve isoladamente associada à hipertensão arterial, apresentação anômala, diagnóstico de sofrimento fetal intraparto, parto por cesária e hemorragia puerperal. Com relação aos resultados neonatais, a idade materna avançada estava associada independentemente apenas ao baixo índice de Apgar, morte perinatal e óbito fetal. Conclusões: esses achados mostram a necessidade de assistência obstétrica adequada com atenção especial a esses fatores para procurar melhorar os resultados maternos e perinatais das gestantes com idade avançada.Most authors agree on the negative impact of pregnancy in women with advanced maternal age on maternal and perinatal outcome. However, it is not usual to evaluate if some considered risk factors are only confounders because they are present in women over forty years. In order to identify the isolated effect of age on maternal and perinatal outcome of pregnancies in women over forty, 494 pregnancies from this age group were compared to 988 pregnancies among women aged 20 to 29 years, matched by parity. After controlling possible confounding variables through multivariate analysis, advanced maternal age maintained its association with a higher prevalence of hypertension, malpresentation, cesarean section, postpartum hemorrhage, low Apgar score, perinatal death, late fetal

  7. Testes cutâneos de hipersensibilidade imediata com o evoluir da idade Positive skin test and age

    Directory of Open Access Journals (Sweden)

    Wilma Carvalho Neves Forte

    2001-04-01

    Full Text Available OBJETIVO: avaliação da positividade aos testes cutâneos de hipersensibilidade imediata em crianças com asma brônquica e/ou rinite alérgica em diferentes faixas etárias. CASUÍSTICA E MÉTODOS: foi observada a positividade aos testes cutâneos de hipersensibilidade imediata, por testes de puntura, frente a diferentes alérgenos de mesma procedência: poeira total e Dermatophagóides sp, Dermatophagoides pteronyssinus, Dermatophagoides farinae e Blomia tropicalis, Penicillium sp, Alternaria alternata, Cladosporium herbarium, Aspergillus fumigatus, grama bermuda, capim de pasto, epitélio de cão, epitélio de gato, penas, Blatella germanica, lã. Foram selecionadas 713 crianças divididas em grupos conforme a faixa etária: grupo I (6 a 11 meses, II (1 a 3 anos e 11 meses, III (4 a 8 anos e 11 meses e IV (9 a 15 anos. Para análise estatística utilizou-se o cálculo do qui-quadrado. RESULTADOS: o total de diferenças significativas entre os vários grupos foi: I e II = 5; II e III = 5; II e IV = 5; III e IV = 6; I e III = 10 e I e IV = 10 CONCLUSÃO: concluiu-se que a positividade ao teste de hipersensibilidade imediata foi maior com o evoluir da idade, havendo positividade já aos doze meses de vida, sendo esta positividade significativamente maior a partir de quatro anos de idade.OBJECTIVE: to evaluate positive responses to skin tests for immediate hypersensitivity to allergens in children with asthma and rhinitis at different ages. METHOD: we observed positive skin test reactivity in prick tests using fifteen allergens of same origin (total dust and Dermatophagoides sp.; Dermatophagoides pteronyssinus; Dermatophagoides farinae; Blomia tropicalis; Penicillium sp; Alternaria alternata; Cladosporium herbarium; Aspergillus fumigatus; Bermuda grass; forage grass; dog and cat epithelia; feathers; Blatella germanica and wool. We placed 713 selected patients into different age groups - Group I: 6 to 11 months; Group II: 1 to 3 years and 11

  8. Desenvolvimento das universidades e bibliotecas universitárias na Idade Média até à Modernidade

    Directory of Open Access Journals (Sweden)

    Fabiene Castelo Branco Diógenes

    2017-01-01

    Full Text Available O artigo analisa a origem das universidades, suas lutas pela autonomia, organização das estruturas administrativa e curricular e relata a existência das bibliotecas ligadas às universidades, desde a Idade Média até a Modernidade. No século XIX a educação é assumida pelo Estado, criando uma cobertura legal que garante às universidades a liberdade científica e pedagógica. A biblioteca universitária teve o seu desenvolvimento ao longo dos séculos, tentando acompanhar essas mudanças. Mas, é no decorrer desse século que alguns serviços e foram surgindo os entendimentos da relação da biblioteca com a universidade. Entretanto, foi a partir da Segunda Guerra que o ensino começa a ter característica de atividade de massa, e a biblioteca universitária se torna uma parte importante na universidade. Cresce a ênfase ao acesso às coleções, há financiamento do Estado para desenvolvimento de coleções e estruturação de suas bibliotecas, dão-se início às atividades de cooperação e de automação. Estas começam a mudar a forma como são oferecidos os serviços e produtos das bibliotecas universitárias. A partir de 1970, as novas tecnologias penetram nessas áreas, e as universidades e suas bibliotecas são afetadas por tais tecnologias. Propostas de reformas surgem gerando novos desafios para estas duas instituições centenárias.

  9. Os efeitos de diferentes pesos de mochila no alinhamento postural de crianças em idade escolar.

    Directory of Open Access Journals (Sweden)

    Lílian Gerdi Kittel Ries

    2013-01-01

    Full Text Available O objetivo deste estudo foi analisar o efeito imediato de diferentes pesos de mochila na postura corporal e avaliar a confiabilidade dessas medidas. Foram avaliados 50 escolares com idades entre oito e 14 anos. Os escolares foram fotografados no plano coronal anterior e sagital, com diferentes cargas relativas ao peso: sem mochila, com o peso habitualmente utilizado, com 10% do peso corporal (PC, 15 % do PC e 20% do PC. Para comparar os ângulos de assimetria da cabeça, de ombros, pélvica, do trocanter, dos joelhos, maleolar, corporal, sagital da cabeça, sagital dos ombros e sagital corporal foi utilizada a Análise de Variância para Medidas Repetidas e o Teste de Friedman. A confiabilidade foi analisada por meio do Coeficiente de Correlação Intraclasse (ICC. Foram observadas diferenças estatisticamente significativas no ângulo sagital cervical (p < .00, no ângulo sagital corporal (p < .00 e no ângulo sagital dos ombros (p < .01 com o aumento da carga. Também obteve-se alta confiabilidade inter-avaliador (ICC entre .83 a .99 para todos os ângulos avaliados nas diferentes posturas (p < .05. Este estudo não sustenta a recomendação de que o peso da mochila não deve exceder 10% do PC, já que cargas inferiores também ocasionaram anteriorização da cabeça e do corpo.

  10. Hemograma e proteínas de fase aguda de bezerros sadios do nascimento aos 30 dias de idade

    Directory of Open Access Journals (Sweden)

    Thaís G. Rocha

    2013-12-01

    Full Text Available O conhecimento da dinâmica das alterações nos parâmetros hematológicos e na cinética das proteínas de fase aguda em animais saudáveis nas primeiras semanas de vida é essencial para a interpretação correta dessas avaliações em situações de morbidez e para diferenciar animais sadios e enfermos de forma confiável. Com o intuito de avaliar a cinética desses parâmetros no primeiro mês de vida de bezerros de corte sadios, filhos de vacas primíparas ou pluríparas, amostras de sangue foram coletadas antes da ingestão de colostro e 1, 2, 7, 15 e 30 dias após o nascimento. Os parâmetros eritrocitários foram influenciados pelo número de partos das vacas e o leucograma mostrou alterações características de influência do cortisol fetal liberado por ocasião do nascimento. O teor sérico de proteína total aumentou significativamente após a ingestão do colostro. As concentrações de ceruloplasmina, haptoglobina e proteínas de pesos moleculares 33 kDa e 23 kDa aumentaram significativamente no primeiro dia de vida, seja pela resposta ao nascimento ou pela ingestão do colostro, enquanto os teores de transferrina, albumina e α1-glicoproteína ácida mantiveram-se relativamente estáveis nos primeiros dias de vida, aumentando gradualmente até os 30 dias de idade.

  11. Factores associados à importância da atividade sexual na idade sénior: o papel da qualidade de vida

    OpenAIRE

    Matias, Vera Maria Das Neves Gomes Pereira

    2015-01-01

    Dissertação de Mestrado apresentada ao ISPA - Instituto Universitário O objectivo geral deste estudo é analisar as variáveis preditores da importância que tem para o idoso a actividade sexual neste período da vida. Como objectivo específico destaca-se a análise da qualidade de vida e sua influência na importância que o sujeito dá ao sexo na idade sénior. A amostra foi constituída por 445 homens e mulheres com idade igual ou superior a 65 anos, não institucionalizados. Os instrumentos incl...

  12. Habilidades auditivas e medidas da imitância acústica em crianças de 4 a 6 anos de idade

    OpenAIRE

    Toscano,Rafaela Della Giacoma Prado; Anastasio,Adriana Ribeiro Tavares

    2012-01-01

    OBJETIVO: avaliar o desempenho em habilidades auditivas e as condições de orelha média de crianças de 4 a 6 anos de idade. MÉTODO: foram aplicados os testes de detecção sonora (audiômetro pediátrico em 20dBNA), a Avaliação Simplificada do Processamento Auditivo (ASPA) e as medidas de imitância acústica (handtymp com tom de 226Hz) em 61 crianças com média de idade de 5,65 anos. Para comparar os resultados das provas de habilidades auditivas e das medidas da imitância acústica foi aplicado o te...

  13. Estudo da marcha de crianças em idade escolar que transportam mochilas às costas usando cinemática

    OpenAIRE

    Rocha, Daniela; Rocha, João; Barbosa, Tiago M.; Queijo, Luís; San Juan, Manuel

    2010-01-01

    Este estudo teve como objectivo analisar a cinemática do ciclo da marcha de crianças em idade escolar, transportando mochilas às costas. Foram estudadas 4 crianças (3 do sexo masculino e 1 do sexo feminino) do 3º ano do primeiro ciclo do ensino básico (8 anos idade). Cada criança caminhou num tapete rolante a velocidades incrementais (1.11 m.s-1, 1.38 m.s -1e 1.67 m.s -1) e com diferentes cargas relativas à massa corporal (0 %, 10 % e 20 %) numa mochila escolar. Todos os procedimentos foram f...

  14. Judicialização da política pública de assistência farmacêutica e eqüidade

    OpenAIRE

    Chieffi,Ana Luiza; Barata,Rita Barradas

    2009-01-01

    O fornecimento de medicamentos por ação judicial, pela Secretaria de Estado da Saúde de São Paulo (SES-SP), tornou-se uma prática rotineira e cada vez mais freqüente. A judicialização do sistema de saúde entra em confronto com princípios básicos do SUS, como o da eqüidade. Este trabalho caracterizou as demandas judiciais para obtenção de medicamentos sob a ótica da judicialização da política pública e da quebra do princípio da eqüidade na dimensão coletiva. O estudo é um trabalho descritivo d...

  15. A method based on Monte Carlo simulations and voxelized anatomical atlases to evaluate and correct uncertainties on radiotracer accumulation quantitation in beta microprobe studies in the rat brain

    Science.gov (United States)

    Pain, F.; Dhenain, M.; Gurden, H.; Routier, A. L.; Lefebvre, F.; Mastrippolito, R.; Lanièce, P.

    2008-10-01

    The β-microprobe is a simple and versatile technique complementary to small animal positron emission tomography (PET). It relies on local measurements of the concentration of positron-labeled molecules. So far, it has been successfully used in anesthetized rats for pharmacokinetics experiments and for the study of brain energetic metabolism. However, the ability of the technique to provide accurate quantitative measurements using 18F, 11C and 15O tracers is likely to suffer from the contribution of 511 keV gamma rays background to the signal and from the contribution of positrons from brain loci surrounding the locus of interest. The aim of the present paper is to provide a method of evaluating several parameters, which are supposed to affect the quantification of recordings performed in vivo with this methodology. We have developed realistic voxelized phantoms of the rat whole body and brain, and used them as input geometries for Monte Carlo simulations of previous β-microprobe reports. In the context of realistic experiments (binding of 11C-Raclopride to D2 dopaminergic receptors in the striatum; local glucose metabolic rate measurement with 18F-FDG and H2O15 blood flow measurements in the somatosensory cortex), we have calculated the detection efficiencies and corresponding contribution of 511 keV gammas from peripheral organs accumulation. We confirmed that the 511 keV gammas background does not impair quantification. To evaluate the contribution of positrons from adjacent structures, we have developed β-Assistant, a program based on a rat brain voxelized atlas and matrices of local detection efficiencies calculated by Monte Carlo simulations for several probe geometries. This program was used to calculate the 'apparent sensitivity' of the probe for each brain structure included in the detection volume. For a given localization of a probe within the brain, this allows us to quantify the different sources of beta signal. Finally, since stereotaxic accuracy is

  16. Electron microprobe analysis (WDS EPMA) of Zhamanshin glass reveals the impactor and a common role of accretion in the origin of splash-form impact glass

    International Nuclear Information System (INIS)

    Vetvicka, I; Frank, J; Drtina, J

    2010-01-01

    Impact glass samples collected during expeditions to the Zhamashin and Lonar craters were subjected to a morphology survey and compared to Wabar, Henbury and Darwin impact glasses to reveal that the accretion of fibres and spherules is not exclusive for irghizites but occurs in other splash form glasses over the world. WDS EPMA and LA-ICP-MS assays of Zhamanshin and Lonar glasses enabled the definition of akmurynites as Zhamanshin glass of specific morphology, chemistry and absence of extraterrestrial contamination. However, extraterrestrial contamination in irghizites was verified and further WDS EPMA analyses led to the conclusion that the Zhamanshin crater had been formed by the impact of a primitive achondrite of Lodran chemistry.

  17. Pesquisa em saúde, política de saúde e eqüidade na América Latina

    Directory of Open Access Journals (Sweden)

    Alberto Pellegrini Filho

    2004-06-01

    Full Text Available O autor analisa as relações entre pesquisa de saúde, políticas de saúde e eqüidade na América Latina. Descreve novas tendências no modo de produção do conhecimento, que permitem maior integração entre as necessidades sociais e a pesquisa, facilitando o vínculo entre esta e o processo de definição de políticas. Analisa as manifestações das novas tendências na América Latina e finaliza com a descrição de algumas iniciativas promovidas pela OPAS no sentido de aproveitar as oportunidades abertas pelas novas tendências para a melhoria das condições de saúde na região. Busca defender a tese de que a informação e o conhecimento são bens públicos essenciais e que as iniqüidades de acesso a esses bens são importantes determinantes das iniqüidades em saúde. Para que as políticas de saúde e as políticas de pesquisa em saúde se integrem e se consolidem como políticas públicas voltadas a atender ao interesse público e à promoção da eqüidade, é necessário o fortalecimento do processo democrático de definição das mesmas, multiplicando os atores envolvidos, os espaços e oportunidades de interação entre eles e instrumentando sua participação com o acesso eqüitativo a informações e conhecimentos científicos pertinentes que permitam a defesa fundamentada de seus interesses.

  18. Role of diffraction and electron analysis in the fast reactor programme

    Energy Technology Data Exchange (ETDEWEB)

    Ferguson, I. F. [ed.

    1975-09-15

    After first discussing irradiation damage, the whole range of new methods of probe analysis were reviewed with a special reference to the study of surfaces. Further papers discussed scanning auger microscopy and the nuclear microprobe. Current diffraction studies were then described on uranium dioxide and the neutron poisons: boron carbide and europia. Finally, new techniques were covered with special reference to the scanning electron microscope and the application of the Harwell 6000 series electronics to x-ray diffraction. Separate records were prepared for each paper covered.

  19. A influência do gênero e idade no desempenho das habilidades locomotoras de crianças de primeira infância

    Directory of Open Access Journals (Sweden)

    Dayana da Silva Oliveira

    2013-12-01

    Full Text Available Na primeira infância é esperada uma melhora no desempenho de habilidades locomotoras com o avanço da idade. Pode também haver diferenças entre meninos e meninas devido à especificidade da tarefa motora. Este estudo teve como objetivo analisar o desempenho de crianças em habilidades locomotoras de acordo com idade e gênero. O desempenho locomotor de 389 pré-escolares de três a cinco anos da cidade do Recife - PE foi avaliado mediante o TGMD-2. Os resultados mostraram que: crianças mais velhas apresentaram melhor desempenho motor; no geral, meninos obtiveram melhor desempenho no correr, salto horizontal, deslize lateral e escore total locomotor, e meninas no saltitar com um pé aos cinco anos de idade; na análise da progressão do desenvolvimento motor, comportamentos motores mais complexos ocorreram após aqueles considerados menos complexos. Conclui-se que o desenvolvimento locomotor dos pré-escolares recifenses obedeceu aos princípios da progressividade e do aumento da complexidade, entretanto, meninos e meninas mostraram diferenças no seu desempenho dependendo da tarefa.

  20. Proteinas do liquido cefalorraqueano: II. Valores normais das frações proteicas obtidas por eletroforese (variações ligadas a cor, sexo e idade

    Directory of Open Access Journals (Sweden)

    Lucia M. Singer Vermes

    1983-03-01

    Full Text Available Mediante dosagens de proteínas totais e eletroforese sobre acetato de celulose de 213 amostras de LCR normal, obtidas por punção da cisterna magna, foram efetuados estudos para verificação de variações ligadas à cor, sexo e idade. Os resultados obtidos permitiram concluir que: 1. não existem diferenças ligadas à cor no proteinograma do LCR; 2. em crianças, os fatores sexo e idade não influem nos valores estudados; 3. as taxas de proteínas totais e frações protéicas do LCR normal de criança diferem das de homens e de mulheres; 4. em adultos ocorrem variações ligadas ao sexo no proteinograma do LCR; 5. em adultos, proteínas totais e todas frações protéicas, quando expressas em mg/100 ml, aumentam com o avançar da idade. Foram estabelecidas, para a metodologia usada, as taxas fisiológicas do proteinograma do LCR de crianças, homens e mulheres, separadamente.

  1. Light Penetration and Light-Intensity in Sandy Marine-Sediments Measured with Irradiance and Scalar Irradiance Fiberoptic Microprobes Rid A-1977-2009

    DEFF Research Database (Denmark)

    KUHL, M.; LASSEN, C.; JØRGENSEN, BB

    1994-01-01

    Fiber-optic microprobes for determining irradiance and scalar irradiance were used for light measurements in sandy sediments of different particle size. Intense scattering caused a maximum integral light intensity [photon scalar irradiance, E0(400 to 700 rim) and E0(700 to 880 nm)] at the sediment...... diffuse. Our results demonstrate the importance of measuring scalar irradiance when the role of light in photobiological processes in sediments, e.g. microbenthic photosynthesis, is investigated....... surface ranging from 180 % of incident collimated light in the coarsest sediment (250 to 500 mum grain size) up to 280 % in the finest sediment ( 1 mm in the coarsest sediments. Below 1 mm, light was attenuated exponentially with depth in all sediments. Light attenuation coefficients decreased...

  2. A method for improving the efficiency of proton microprobe profiling of strontium in otoliths using a vacuum compatible NaI detector

    International Nuclear Information System (INIS)

    Barry, B.; Markwitz, A.

    2004-01-01

    The precision of proton microprobe measurements of Sr in otoliths by proton induced X-ray emission (PIXE) has been improved significantly by use of a large area low resolution NaI(Tl) detector. This is achieved by scanning the sample simultaneously with a high resolution Si(Li) detector to measure the main constituent Ca and to confirm the absence of other elements in the counting window used by the large area detector. In our experimental setup the count rate for Sr was improved by a factor of 30. We took advantage of this to improve precision and achieve higher sample throughput in studies of diadromous fish, i.e. those whose life cycles may include both marine and freshwater stages

  3. Nuclear microprobe characterization of surface hardening by precipitation of chromium carbides after laser beam treatment of a Ni-Cr substrate

    International Nuclear Information System (INIS)

    Mosbah, M.; Gosset, J.; Trocellier, P.; Puig, T.; Cantarel, M.; Condat, M.

    1989-01-01

    Surface treatment by laser provides interesting solutions to the problem of accelerated wear of materials. The aim of the present study is the characterization of chromium carbides rich surface alloys after laser beam melting of a Ni 70 Cr 30 carbon precoated substrate. The carbon profiling of the lasered surface was performed by nuclear microprobe using the 12 C(d,p 0 ) 13 C reaction, Ni and Cr were evaluated by means of PIXE (Particle Induced X Ray Emission). The specificity of the method and the experimental conditions are explained. Wear results are very satisfactory and close to those obtained by injection of chromium carbide powders into the laser beam in the case of a Nimonic alloy: wear rates are divided by two orders of magnitude

  4. Application of synchrotron-radiation-based x-ray microprobe techniques for the analysis of recombination activity of metals precipitated at Si/SiGe misfit dislocations

    CERN Document Server

    Vyvenko, O F; Istratov, A A; Weber, E R; Kittler, M; Seifert, W

    2002-01-01

    In this study we report application of synchrotron-radiation-based x-ray microprobe techniques (the x-ray-beam-induced current (XBIC) and x-ray fluorescence (mu-XRF) methods) to the analysis of the recombination activity and space distribution of copper and iron in the vicinity of dislocations in silicon/silicon-germanium structures. A combination of these two techniques enables one to study the chemical nature of the defects and impurities and their recombination activity in situ and to map metal clusters with a micron-scale resolution. XRF analysis revealed that copper formed clearly distinguishable precipitates along the misfit dislocations. A proportional dependence between the XBIC contrast and the number of copper atoms in the precipitates was established. In hydrogen-passivated iron-contaminated samples we observed clusters of iron precipitates which had no recombination activity detectable by the XBIC technique as well as iron clusters which were not completely passivated.

  5. Development of an x-ray fluorescence microprobe at the National Synchrotron Light Source, Brookhaven National Laboratory: Early results: Comparison with data from other techniques

    International Nuclear Information System (INIS)

    Smith, J.V.; Rivers, M.L.; Sutton, S.R.; Jones, K.W.; Hanson, A.L.; Gordon, B.M.

    1986-01-01

    Theoretical predictions for the detection levels in x-ray fluorescence analysis with a synchrotron storage ring are being achieved experimentally at several laboratories. This paper is deliberately restricted to the state of development of the Brookhaven National Laboratory/University of Chicago instruments. Analyses at the parts per million (ppM) level are being made using white light apertured to 20 μm and an energy dispersive system. This system is particularly useful for elements with Z > 20 in materials dominated by elements with Z < 20. Diffraction causes an interference for crystalline materials. Development of a focusing microprobe for tunable monochromatic x-rays and a wavelength dispersive spectrometer (WDS) is delayed by problems in shaping an 8:1 focusing mirror to the required accuracy. Reconnaissance analyses with a wiggler source on the CHESS synchrotron have been made in the K spectrum up to Z = 80

  6. In vivo optical microprobe imaging for intracellular Ca2+ dynamics in response to dopaminergic signaling in deep brain evoked by cocaine

    Science.gov (United States)

    Luo, Zhongchi; Pan, Yingtian; Du, Congwu

    2012-02-01

    Ca2+ plays a vital role as second messenger in signal transduction and the intracellular Ca2+ ([Ca2+]i) change is an important indicator of neuronal activity in the brain, including both cortical and subcortical brain regions. Due to the highly scattering and absorption of brain tissue, it is challenging to optically access the deep brain regions (e.g., striatum at >3mm under the brain surface) and image [Ca2+]i changes with cellular resolutions. Here, we present two micro-probe approaches (i.e., microlens, and micro-prism) integrated with a fluorescence microscope modified to permit imaging of neuronal [Ca2+]i signaling in the striatum using a calcium indicator Rhod2(AM). While a micro-prism probe provides a larger field of view to image neuronal network from cortex to striatum, a microlens probe enables us to track [Ca2+]i dynamic change in individual neurons within the brain. Both techniques are validated by imaging neuronal [Ca2+]i changes in transgenic mice with dopamine receptors (D1R, D2R) expressing EGFP. Our results show that micro-prism images can map the distribution of D1R- and D2R-expressing neurons in various brain regions and characterize their different mean [Ca2+]i changes induced by an intervention (e.g., cocaine administration, 8mg/kg., i.p). In addition, microlens images can characterize the different [Ca2+]i dynamics of D1 and D2 neurons in response to cocaine, including new mechanisms of these two types of neurons in striatum. These findings highlight the power of the optical micro-probe imaging for dissecting the complex cellular and molecular insights of cocaine in vivo.

  7. Mulheres em idade fértil: causas de internação em Unidade de Terapia Intensiva e resultados

    Directory of Open Access Journals (Sweden)

    Cátia Millene Dell Agnolo

    2014-08-01

    Full Text Available Introdução: Pacientes obstétricas representam uma fração significativa das admissões em unidades de cuidado intensivo e consistem em um desafio para a equipe. Objetivo: Analisar as principais causas de internação e morte materna de mulheres em idade fértil ocorridas em unidades de terapia intensiva de hospitais de um município do Noroeste do Paraná, Sul do Brasil. Métodos: Estudo exploratório, descritivo, retrospectivo, realizado com mulheres em idade fértil (10 a 49 anos internadas em três unidades de terapia intensiva existentes em um município do Noroeste do Paraná, por causas obstétricas e não obstétricas, no período de janeiro de 2005 a dezembro de 2009. Resultados: Foram encontradas 775 internações de mulheres em idade fértil, com uma média de idade de 33,7±10,3 anos, com duração média de internação de 5,0±8,4 dias. A maior parte das mulheres era do município estudado (67,2%, com baixa escolaridade (nível primário, 68,2%. Entre as causas obstétricas de internação, a pré-eclâmpsia grave e a eclâmpsia se constituíram na principal causa (71,3%; a pielonefrite se destacou sob outras condições no período gestacional (53%. Não foi encontrada associação estatística entre internações por causas obstétricas em unidade de terapia intensiva e óbito. Conclusão: As causas não obstétricas representaram a maioria das internações de mulheres em idade fértil nas unidades de terapia intensiva do município, no período estudado e, entre as causas obstétricas, a pré-eclâmpsia grave e eclampsia constituíram a principal causa.

  8. Fatores associados ao consumo precoce de leite de vaca integral por crianças menores de um ano de idade

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    Luciano Pamplona de Goes Cavalcanti

    2015-12-01

    Full Text Available Objetivo: Avaliar a frequência e fatores associados ao uso do leite de vaca integral nas crianças menores de um ano na cidade de Fortaleza, Ceará. Métodos: Realizou-se estudo transversal e analítico envolvendo 575 mães de crianças menores de um ano de idade residentes em Fortaleza, Ceará. Aplicou-se questionário semiestruturado para coleta de dados sociodemográficos, história reprodutiva da mãe, dados referentes ao parto e à criança. Resultados: A mediana de idade das mães foi de 26,5 anos, tendo 80,5% (n=463 renda familiar de 1 a 5 salários mínimos. A maior parte (83,2%, n=475 realizou mais de seis consultas de pré-natal, mas apenas 86,2% (n=494 declararam ter recebido informações sobre aleitamento materno. Entre as crianças que receberam outro tipo de leite, 53,8% (n=191 consumiram leite de vaca integral, e destas, 31,7% (n=113 referem ter recebido orientação do pediatra. O consumo do leite de vaca foi relacionado à idade materna (menores de 18 anos de idade, (p=0,015, renda inferior a cinco salários mínimos (p<0,001, baixa escolaridade (p<0,001, mães que não trabalhavam (p<0,001, baixo número de consultas de pré-natal (p=0,019, ter nascido em hospital público (p<0,001, não ter amamentado antes de sair da maternidade (p<0,001 e não ter plano de saúde (p<0,001. Conclusão: O consumo precoce do leite de vaca integral por crianças menores de um ano apresentou alta prevalência e sofreu influência de fatores como renda, escolaridade e pouca idade da mãe. Portanto, é preciso sensibilizar os profissionais de saúde para que qualifiquem melhor as orientações prestadas durante as consultas de pré-natal e puerpério.

  9. Nível de proteína bruta para bezerros de corte desmamados aos 66 dias de idade

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    Pascoal Leonir Luiz

    2000-01-01

    Full Text Available O objetivo deste trabalho foi avaliar o consumo médio diário de matéria seca (CMS, CMS por 100 kg de peso vivo (CMSP, CMS por unidade de peso metabólico (CMSM, a conversão alimentar (CA e o ganho de peso médio diário (GMD de bezerros de corte, alimentados com diferentes níveis de proteína bruta (PB na dieta. Foram utilizados 47 bezerros inteiros, da raça Braford, desmamados aos 66 dias de idade com peso médio de 76,4 kg. Os animais foram alimentados à vontade com silagem de aveia e concentrado (50/50, com níveis de 13, 15, 17 e 19% de PB na dieta total. O período de adaptação ao alimento e manejo foi de 21 dias. Os animais foram pesados com jejum de sólidos de 14 horas, a intervalos regulares de 21 dias durante o período experimental de 84 dias. Verificou-se, por meio da análise de regressão linear e múltipla, que não ocorreram efeitos significativos relacionando o CMS, CMSP, CMSM, CA e GMD e o nível de PB na dieta. Observou-se que CMS, CMSP e CMSM aumentaram linearmente com o avanço do período experimental, demonstrando o aumento da capacidade de ingestão com o aumento do peso vivo. Os valores de GMD obtidos foram de 644; 701; 693 e 730 g/dia para os níveis de 13; 15; 17 e 19% de PB na dieta, respectivamente. Os ganhos de peso foram superiores àqueles normalmente atingidos ao pé da vaca em condições de campo nativo ou desmamados precocemente e mantidos em pastagem cultivada.

  10. Impacto do aleitamento materno no coeficiente de inteligência de crianças de oito anos de idade

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    Ana L. M. Fonseca

    2013-08-01

    Full Text Available OBJETIVO: O objetivo deste estudo foi determinar a influência do aleitamento materno na capacidade intelectual de crianças pertencentes a uma coorte de um país em desenvolvimento, controlando para os principais fatores de confusão. MÉTODOS: Foi realizado um estudo de coorte prospectiva com todos os recém-nascidos nos hospitais de uma cidade de porte médio e acompanhou-se uma amostra aleatória destes aos 30, 90 e 180 dias de vida e aos 8 anos. No acompanhamento foram avaliados diversos aspectos da amamentação e, aos 8 anos, foi realizada avaliação da capacidade intelectual geral aplicando-se o Teste de Raven. As análises estatísticas utilizaram Teste T, ANOVA e regressão linear e logística, considerando como associações estatisticamente significativas aquelas cujo valor de p foi inferior a 0,05. RESULTADOS: Aos 8 anos 560 crianças participaram da avaliação com o Teste de Raven. A média da pontuação das crianças no teste foi de 22,56 pontos com desvio padrão de 5,93. A diferença de médias entre os grupos em aleitamento materno ou não, aos seis meses, foi de 1,33 (p = 0,008. Permaneceram associadas ao desfecho, após regressão linear e logística, a cor materna e da criança, classe socioeconômica, escolaridade e tabagismo maternos e o aleitamento materno aos 6 meses de idade (p = 0,007. CONCLUSÕES: As crianças que mamaram por seis meses ou mais tiveram melhor desempenho na avaliação intelectual geral, mesmo após ajuste para os principais fatores de confundimento.

  11. Acompanhamento sistematizado da hiperbilirrubinemia em recém-nascidos com 35 a 37 semanas de idade gestacional

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    Elizabete Punaro

    2011-08-01

    Full Text Available OBJETIVOS: Identificar os resultados do acompanhamento da bilirrubinemia na primeira semana de vida em uma coorte de recém-nascidos (RNs de 35(0/7 a 37(6/7 semanas de idade gestacional e estabelecer fatores de risco para reinternação para fototerapia pós-alta hospitalar (bilirrubinemia total > 18 mg/dL. MÉTODOS: Estudo de coorte retrospectivo em hospital público universitário. Os recém-nascidos tiveram acompanhamento da bilirrubina total plasmática ou transcutânea pré- e pós-alta da enfermaria de alojamento conjunto para avaliação da necessidade de fototerapia. Foi empregada uma abordagem sistematizada, utilizando-se os percentis de risco de uma curva de referência. RESULTADOS: Foram estudados 392 RNs. Uma consulta ambulatorial foi necessária em 61,7% dos RNs. Tiveram valores máximos de bilirrubinemia total > 20 mg/dL 34 RNs (8,7%, e três RNs (0,8% apresentaram bilirrubinemia total entre 25-30 mg/dL. Fototerapia foi indicada após alta em 74 RNs (18,9%. Os fatores de risco foram a perda de peso do nascimento até o primeiro retorno e os percentis à alta acima do P40. A bilirrubinemia total à alta acima do P95 foi associada ao maior risco de reinternação [RR = 49,5 (6,6-370,3]. A perda de peso até o primeiro retorno foi o único preditor clínico independente [RR = 1,16 (1,04-1,17]. CONCLUSÃO: A abordagem sistematizada da bilirrubinemia na 1ª semana foi efetiva na prevenção de hiperbilirrubinemias perigosas. O suporte à amamentação e a alta hospitalar após a estabilização da perda de peso podem ser medidas preventivas da reinternação por hiperbilirrubinemia

  12. Academia da Melhor Idade: motivos para ingresso, permanência e satisfação dos idosos participantes

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    Mauren da Silva Salin

    2014-01-01

    Full Text Available DOI: http://dx.doi.org/10.5007/1980-0037.2014v16n2p152   Academias da saúde vêm sendo implantadas em diversos parques públicos e a população idosa tem sido beneficiada com a promoção de exercícios físicos (EF nesses locais. O estudo teve como objetivo descrever a percepção dos idosos do Programa Academia da Melhor Idade (AMI, no município de Joinville - Santa Catarina (SC, quanto à moti-vação para o ingresso e permanência, satisfação e sugestões dos serviços prestados. Foram entrevistados 163 idosos (117 mulheres e 46 homens participantes de 15 AMIs instaladas em praças públicas de Joinville. A coleta de dados se deu por meio de uma entrevista se-miestruturada. Utilizaram-se estatística descritiva para os dados quantitativos e análise de conteúdo temática para os dados qualitativos.   A motivação intrínseca foi preponderante no ingresso e permanência dos idosos nas AMIs, destacando-se a busca por saúde (ingresso e a percepção dos benefícios que a prática de EF proporciona (permanência. O incentivo de terceiros foi o principal fator de motivação extrínseco para o ingresso e a sociabilização, principal motivo para a permanência. Os idosos estão satisfeitos com o atendimento pres-tado e a infraestrutura, mas sugerem melhorias como: ampliação no número de atividades nas academias, capacitação dos monitores, instalação de banheiros públicos, bebedouros e cobertura. Concluiu-se que os idosos apresentam, principalmente, motivações intrínsecas para ingressar e permanecer nas AMIs. A maioria está satisfeita, mas recomenda melhorias em termos de recursos humanos e infraestrutura, a fim de subsidiar a implementação de novas estratégias para a promoção de EF em praças públicas e o atendimento a um maior número de usuários.

  13. PADRÃO E PROCESSO SUCESSIONAIS EM FLORESTAS SECUNDÁRIAS DE DIFERENTES IDADES NA AMAZÔNIA ORIENTAL

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    Débora Veiga Aragão

    2005-11-01

    Full Text Available A maioria dos estudos de sucessão em florestas secundárias na Amazônia avalia sítios de diferentes idades, que representam uma cronoseqüência sucessional, em vez de monitorar um único sítio por vários anos pelo inventário contínuo. Este estudo comparou a composição e estrutura florísticas de espécies arbóreas com diâmetro a 1,3 m de altura (DAP ≥ 1 cm, em sítios com 4 e 12 anos na Amazônia Oriental, e avaliou a mortalidade e o recrutamento em ambos os sítios baseados em dados de inventário contínuo durante 4 anos de estudo. As áreas de estudo foram abandonadas após múltiplos ciclos de uso agrícola de 7 a 10 anos, desde ~1940. Ambos os sítios são dominados pelas espécies arbóreas Lacistema pubescens e Vismia guianensis, com densidade de indivíduos, diâmetro, altura, área basal e riqueza de espécies significativamente maiores no sítio de 12 anos. A densidade de indivíduos, ao longo do tempo, foi crescente no sítio de 4 anos e decrescente no de 12 anos; o diâmetro, a altura e a área basal aumentaram nos dois sítios. No sítio de 4 anos, foi constatada uma taxa de recrutamento líquido crescente entre 2000-2001 e 2001-2002, que diminuiu entre 2002-2003, indicando redução gradual na colonização. No sítio de 12 anos, foi observada alta mortalidade líquida (13 e 11%, sobretudo nas duas primeiras avaliações, indicando o processo de autodesbaste. A combinação dos métodos de cronoseqüência e inventário contínuo aumenta substancialmente o entendimento do desenvolvimento sucessional.

  14. Marcas de expressão e repressão: Reflexões sobre a homossexualidade na terceira idade

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    Byanca Eugênia Duarte Silva

    2016-09-01

    Full Text Available Sabe-se que a homossexualidade existe desde os primórdios, sendo vivenciada de forma livre. Entretanto, a sociedade atual é composta subjetivamente de muito preconceito, considerando a homossexualidade, uma afronta às normas sociais. Quando a homossexualidade atrela-se ao idoso, o tabu e discriminação intensificam-se, principalmente devido ao julgamento social de que pessoas idosas não sentem atratividade ou não são mais aptas a praticar o sexo. Assim, torna-se importante analisar as dificuldades enfrentadas pelos idosos que são homossexuais, problemática essa que gera muita polêmica, preconceito e estereótipos. A homossexualidade no idoso é um assunto pouco estudado, partindo do pressuposto da escassez de referenciais bibliográficos. Portanto, faz-se necessário a realização de mais pesquisas e estratégias, no intuito de ampliar o grau de conhecimento em relação ao tema. Nesse sentido, este estudo trata-se de uma pesquisa bibliográfica, a partir de artigos científicos, na expectativa de tentar entender o surgimento dessa problemática, como também, tentar encontrar as explicações relacionadas ao estigma da sexualidade no idoso, tendo em vista, que esta era vista de forma natural na antiguidade. Os resultados confirmaram a existência de um tabu em relação à homossexualidade na terceira idade agregado a dois fatores: a homossexualidade e o envelhecimento. Dois temas carregados de preconceitos advindos de uma sociedade heterossexista. Brand expression and repression: Reflections on homosexuality in old age Abstract: It is known that homosexuality has existed since the early days, and lived freely. However, today's society is made up of a lot of prejudice subjectively considering homosexuality an affront to social norms. When homosexuality harnesses to the elderly, the taboo and discrimination intensify if, mainly due to social judgment that older people do not feel attractive or are no longer able to have sex. Thus

  15. Terceira idade: nova identidade, reinvenção da velhice ou experiência geracional? Third age: new identity, reformulation of the old age or generational experience?

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    Luna Rodrigues Freitas Silva

    2008-01-01

    Full Text Available Este artigo trata das inovações acerca dos modos e das experiências de envelhecer que se vêm configurando nos últimos anos. Hábitos, imagens, crenças e condutas atreladas ao envelhecimento vêm-se alterando de forma significativa, determinando o surgimento do que se convenciona chamar de experiência da terceira idade. Mas, ainda que represente inovação e, sob muitos aspectos, seja descrita como uma reformulação extremamente positiva das possibilidades de envelhecer, o surgimento da terceira idade gera também questionamento e debate. Para compreender o estatuto desta experiência que surge no cenário contemporâneo, procederemos a um mapeamento da discussão acerca da terceira idade na literatura especializada, mais especificamente no que se refere a seu caráter de inovação em relação à identidade da velhice. Três hipóteses se destacam nesta análise: a primeira sugere que a terceira idade pode ser entendida como uma nova identidade, autônoma e diferenciada da identidade da velhice; a segunda, que seu surgimento pode ser compreendido como uma negação social da velhice propriamente dita; e, finalmente, a terceira hipótese supõe que as características da terceira idade são tributárias da experiência geracional de determinado grupo social. As principais hipóteses de entendimento da terceira idade são apresentadas e discutidas tendo em vista as possibilidades de criação, diversificação e inovação da experiência subjetiva.This paper deals with innovations on the ways and on the experience of aging set up in recent years. Habits, images, beliefs and behaviors related to aging have changed determining the emergence of what is usually called the third age experience. But although it represents innovation and, in many ways, is described as a very positive reformulation of the possibilities of aging, the emergence of the third age also generates questioning and debate. In order to understand the status of this

  16. Nutritive value of the elephant-grass obtained on different cut ages Valor nutritivo do capim-elefante obtido em diferentes idades de corte

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    Joanis Tilemahos Zervoudakis

    2008-09-01

    Full Text Available The present work aimed to determine the chemical composition, the parameters of the dry matter (DM and neutral detergent fiber (NDF in situ degrability, the MS (IVDMD in vitro dry matter digestibility and the content of total digestible nutrients (NDT of grass-elephant obtained in different cut ages, in rainy season. The grass-elephant was submitted to the cut at the ages of 30, 45, 60, 75, 90 and 105 days, from December to March. The samples were analyzed for dry matter (MS, crude protein (PB, ash, ether extract (EE, total carbohydrates (CT, neutral detergent fiber (NDF and acid (FDA, indigestible NDF (INDF and insoluble protein in acid detergent (ADIP. Additionally, the samples were weighted in bags of nylon, incubated in the rumen of three bovine canulated, and the residues were analyzed for DM and NDF residual. Subsequently, it were submitted to in vitro incubation with liquid ruminal and solution of acid pepsin for dry matter in vitro digestibility (IVDMDdetermination, of which values were utilized for content of total digestible nutrients (NDT estimation. The content of CP was reduced in a linear way by the advancement of the cut age, while the contents of NDF, ADF, INDF and ADIP increased. The fraction “a” of the DM was reduced and the NDF I fraction was increased with the cut age advancement. The IVDMD and TDN presented quadratic behaviors (P<0,05, in function of cut age , with maximum values of 69.00% and 57.21%, to the ages of 19.64 and 48.98 days, respectively.Objetivou-se determinar a composição químico-bromatológica, os parâmetros da degradabilidade in situ da matéria seca (MS e fibra em detergente neutro (FDN, a digestibilidade in vitro da MS (DIVMS e o teor de nutrientes digestíveis totais (NDT do capim-elefante obtido em diferentes idades de corte, na época das águas. A forrageira foi submetida ao corte nas idades de 30, 45, 60, 75, 90 e 105 dias, de dezembro a março. As amostras foram analisadas para matéria seca

  17. Avaliação nutricional do capim-elefante (Cameroon em diferentes idades de rebrotação Nutritional evaluation of elephantgrass at different regrowth ages

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    Polyana Albino Silva Machado

    2008-06-01

    Full Text Available Objetivou-se determinar o consumo e as digestibilidades aparente total, ruminal e intestinal de matéria seca (MS e seus componentes: matéria orgânica (MO, proteína bruta (PB, extrato etéreo (EE, fibra em detergente neutro (FDN e carboidratos não-fibrosos (CNF do capim-elefante em diferentes idades de rebrotação e quantificar a produção de proteína microbiana. Utilizaram-se quatro novilhos mestiços, fistulados no rúmen e abomaso, alimentados à vontade com capim-elefante e sal mineral. O experimento foi avaliado considerando-se o grupo de animais como uma amostra aleatória simples, sendo os períodos de avaliação correspondentes às idades crescentes de rebrotação (33, 48, 63, 78 e 93 dias e cada animal como medidas repetidas. Os consumos de matéria seca (MS, nutrientes digestíveis totais (NDT e as digestibilidades totais dos demais nutrientes diminuíram linearmente com o aumento da idade de rebrotação. Os teores de MO, CNF e FDN apresentaram máximos consumos aos 44,43; 51,05 e 60,50 dias de rebrotação, respectivamente. O mínimo consumo de PB ocorreu aos 94,27 dias de rebrotação do capim. As digestibilidades ruminais da MS e MO aumentaram linearmente com o avanço da idade. Os compostos nitrogenados microbianos sofreram redução linear com o aumento da idade do capim-elefante. Recomenda-se usar o capim-elefante com idade entre 30 e 35 dias de rebrotação, quando se observou maior valor nutritivo da planta.The objective of this trial was to determine the intake and the total, ruminal and intestinal apparent digestibilidade of dry matter (DM and its components: organic matter (OM, crude protein (CP, ether extract (EE, in neutral detergent fiber (NDF and no-fiber carbohydrates (NFC of the elephantgrass in different regrowth ages and to quantify the microbial protein production. Four crossbred steers fitted with ruminal and abomasal cannula were fullfed with elephantgrass and mineral salt. The experiment was evaluated

  18. Measles vaccination: influence of age on its efficacy Vacinação contra o sarampo: influência da idade em sua eficácia

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    Marta Heloísa Lopes

    1989-10-01

    Full Text Available The authors compare the serologic efficacy and the clinical protection afforded by three different measles vaccination schemes in adequately nourished children in São Paulo city, Brazil. Two hundred forty two children were divided into three groups. Group A, comprising 117 children who had received the vaccine before 12 months of age and a second dose at 12 months of age or more. Group B, comprising 46 children who had received only one dose, before 12 months of age. Group C, comprising 79 children who had received only one dose, at 12 months of age or more. The geometric mean titer of antibodies in Group A was 790.1; in Group B, 251.1; and in Group C, 550.3. There was no statistically significant difference between Groups A and C. The exposure to the measles virus was probably similar in all groups, and the children in Groups A and C had similar chances of acquiring the disease after vaccination whereas in Group B the chances were higher when compared to the other two groups. The results obtained in this study favor the use, in developing countries, of a vaccination program against measles that includes an early first dose at eight months of age and revaccination after 12 months of age.Os autores comparam a eficácia sorológica e a proteção clinica obtidas com três esquemas diferentes de vacinação contra o sarampo, em crianças eutróficas, na cidade de São Paulo, Brasil. Duzentas e quarenta e duas crianças foram divididas em três grupos. Grupo A, compreendendo 117 crianças primovacinadas antes dos 12 meses de idade e revacinadas com 12 ou mais meses de idade. Grupo B, compreendendo 46 crianças vacinadas com dose única, antes dos 12 meses de idade. Grupo C, compreendendo 79 crianças vacinadas com dose única, aos 12 ou mais meses de idade. A média geométrica do título de anticorpos no grupo A foi 790,1; no grupo B, 251,1; e no grupo C, 550,3. Não houve diferença estatisticamente significante entre os grupos A e C. A exposi

  19. Idade e sexo na maciez da carne de ovinos da raça Corriedale Meat lamb tenderness influenced by age and sex in Corriedale lineage

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    Márcia Arocha Gularte

    2000-06-01

    Full Text Available A maciez da carne geralmente é o atributo mais importante para o consumidor. Vários são os fatores que influem sobre esSe aspecto no animal, como por exemplo: genótipo, idade, sexo, entre outros. Neste estudo, verificou-se a influência da idade e do sexo na maciez do músculo Longissimus dorsi de ovinos da raça Corriedale, através de métodos sensoriais e instrumentais. Após o abate, realizou-se a avaliação visual da textura do músculo pela granulação da superfície do mesmo. As amostras foram congeladas por 5 meses. Após a cocção, foi analisada a maciez da carne pelo equipamento Warner-Bratzler shear medindo a força de cisalhamento, e por avaliação sensorial realizada por uma equipe treinada de julgadores. Resultados obtidos pela avaliação sensorial e instrumental indicaram que o músculo Longissimus dorsi de fêmeas e de animais de menor idade foram mais macios.The meat tenderness is the most important atribute to the consumer. Several factors have influence in this aspect, for exemple: genotype, age, sex and others. The objective of this work was to study the influence of age and sex on Longissimus dorsi muscle tenderness of Corriedale lineage lamb, through sensory and instrumental methods. After slaughter Longissimus dorsi, texture was evaluated by granite’s surface method. The samples were frozen for five months. After thawing and cooking, meat tenderness was evaluated by Warner-Bratzler shear and sensory evaluation by a group of trained judges. The results indicated that female and younger animals produced more tender meat.

  20. Efeitos do fumo ambiental no trato respiratório inferior de crianças com até 5 anos de idade

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    Pereira Eanes DB

    2000-01-01

    Full Text Available OBJETIVO: Avaliar a associação do fumo passivo com morbidade respiratória em crianças abaixo de 5 anos de idade. MÉTODOS: Estudo transversal incluindo 1.104 crianças abaixo de 5 anos de idade residentes na cidade de Fortaleza, Ceará. Por meio de um questionário com os pais das crianças, foram obtidas informações sobre sintomas e doenças respiratórias, história familiar de morbidade respiratória, presença de fumantes nas casas e condições de moradia. RESULTADOS: Foram estudados 546 meninas e 558 meninos. Das 611 crianças fumantes passivas, 82% tinham problemas respiratórios ("odds ratio" = 1,64; IC 95%:1,21-2,20. As queixas respiratórias mais freqüentes foram: chiado no peito ("odds ratio" =1,66; IC 95%: 1,21-2,27, dispnéia ("odds ratio"=1,91; IC 95%:1,36-2,67, tosse e/ou expectoração("odds ratio" =1,58; IC 95%: 1,13-2,84. A chance de apresentar asma, bronquite ou pneumonia foi maior para as crianças fumantes passivas ("odds ratio" =1,60; IC 95%: 1.11-2.31. CONCLUSÕES: Os principais fatores de risco com chance de predizer morbidade respiratória em crianças com idade de 0 a 5 anos foram: crianças que conviviam com mães fumantes, pais fumantes, presença de mofo em casa, historia familiar de asma ou rinite.

  1. Idades e crescimento da cioba, Ocyururs chrysurus, da Costa Central do Brasil Age and growth of yellowtail snapper, Ocyururs chrysurus, from Central Coast of Brazil

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    Júlio Neves de Araújo

    2002-01-01

    Full Text Available A idade e o crescimento da cioba da costa central do Brasil foram estudados a partir de leituras de otólitos obtidos em amostragens mensais de desembarques comerciais, realizados nas cidades de Vitória e Vila Velha, entre os anos de 1998 e 1999. Através da análise do incremento marginal, foi verificada a formação anual de uma zona translúcida a partir do final do outono e durante o inverno. Foram observadas ciobas de 2 a 19 anos. Os comprimentos furcais (CF médios retrocalculados variaram de 108 mm para idade 1 a 524 mm para idade 19. A equação de Von Bertalanffy ajustada aos CF médios retrocalculados foi CFt = 567,1 (1 - e -0.130 (t + 0.773. A relação comprimento peso foi P = 2,68x10-5CF2.914, onde P = peso total em gramas. O crescimento é lento, com os incrementos anuais em peso aumentando gradativamente até atingir o máximo de 164 g entre as idades 7 e 8 anos. Os resultados deste trabalho indicam que a cioba tem longa expectativa de vida e baixas taxas de crescimento somático, características das espécies mais sensíveis à exploração pesqueira.To age and study the growth of yellowtail snapper, we analyzed readings of otoliths obtained in monthly samplings from commercial landings in the cities of Vitória and Vila Velha, from 1998 to 1999. Marginal increment analysis showed that the formation of a translucent zone occurred in the early fall and during the winter. The observed ages range from 2 to 19 years. Mean back-calculated fork lengths (FL range from 108 mm for age 1 to 524 mm for age 19. The Von Bertalanffy growth equation fitted to the mean back-calculated FL was FLt = 567,1 (1 - e -0.130 (t + 0.773, The length-weight relationship was W= 2,68x10-5FL2.914, where W = whole weight in grams. Yellowtail snapper has a slow growth with annual growth increments in weight raising progressively to the maximum of 164 g between the 7 and 8 years. The yellowtail snapper has long lifespan and slow growth rates, features of

  2. Progênie de Palmistichus elaeisis Delvare & LaSalle (Hymenoptera: Eulophidae) parasitando pupas de Bombyx mori L. (Lepidoptera: Bombycidae) de diferentes idades

    OpenAIRE

    Pereira, Fabricio F; Zanuncio, José C; Serrão, José E; Oliveira, Harley N; Fávero, Kellen; Grance, Elizangela L V

    2009-01-01

    Palmistichus elaeisis Delvare & LaSalle é um parasitóide pupal natural de pupas de lepidópteros desfolhadores de eucalipto e é considerado um promissor agente de controle biológico. No entanto, o desenvolvimento de técnicas de criação eficientes desse inimigo natural é inicialmente necessário para que ele possa ser utilizado em programas de controle biológico. Pupas de Bombyx mori L. são hospedeiras alternativas em potencial para criação massal de P. elaeisis. Por isto, nós avaliamos a idade ...

  3. Estudo do perfil lipídico de crianças e jovens até 19 anos de idade

    Directory of Open Access Journals (Sweden)

    Seki Mario

    2001-01-01

    Full Text Available Foi realizado levantamento retrospectivo de 624 casos, de ambos os sexos, com idades variando de 3 a 19 anos, que realizaram exames do perfil lipídico (PL em laboratório privado de Londrina-PR. A prevalência das dislipidemias - adotando os valores de referência estabelecidos pelo Segundo Consenso Brasileiro sobre Dislipidemias (SCBD - é alarmante na casuística estudada. As autoridades necessitam estender a investigação aos usuários do sistema público de saúde para avaliar a dimensão real do problema na população geral.

  4. Proteína Bruta e Proteína Ideal para Frangos de Corte no Período de 1 a 21 Dias de Idade

    OpenAIRE

    Araújo,LF; Junqueira,OM; Araújo,CSS; Laurentiz,AC; Almeida,JG; Serrano,PP

    2001-01-01

    Dois experimentos foram realizados com o objetivo de avaliar o desempenho de frangos de corte no período de 1 a 21 dias alimentados com dietas formuladas nos conceitos de proteína bruta e proteína ideal. No primeiro experimento, foram utilizados 400 pintos machos de um dia de idade da linhagem Cobb, distribuídos em delineamento inteiramente casualizado, com 2 tratamentos (proteína total e proteína ideal) e 5 repetições de 40 aves cada. No segundo experimento, foram utilizados 800 pintos, 400 ...

  5. O efeito agudo do chocolate amargo sob a função endotelial é dependente da idade em hipertensos com baixo risco cardiovascular

    OpenAIRE

    Jenifer Palma dEl-Rei Pinto

    2011-01-01

    Dados recentes indicam uma relação inversa entre doença cardiovascular e consumo de flavonóides. O objetivo do estudo foi identificar parâmetros clínicos e vasculares de pacientes hipertensos tratados que apresentaram efeitos benéficos na função vascular após o consumo de chocolate amargo com 70% de cacau por sete dias. Vinte e um pacientes hipertensos em tratamento medicamentoso, ambos os sexos, com idades entre 40-65 anos, foram incluídos em um ensaio clínico intervencional com aferição de...

  6. Optimization of Actinide Quantification by Electron Probe Microanalysis

    International Nuclear Information System (INIS)

    Moy, A.; Merlet, C.; Llovet, X.; Dugne, O.

    2013-06-01

    Conventional quantitative electron probe microanalysis of actinides requires the use of reference standard samples. However, for such elements, standards are generally not available. To overcome this difficulty, standard-less methods of analysis are used, in which the x-ray intensity emitted by the standard is calculated. To be reliable, such calculations require accurate knowledge of physical data such as the x-ray production cross section. However, experimental data of this quantity are not always available for actinide elements. In the present work, experimental L and M x-ray production cross sections were measured for elements uranium and lead. Measurements were performed with two electron microprobes using wavelength-dispersive spectrometers using thin self-supporting targets. Experimental results are compared with calculated cross sections obtained from different analytical formulae, and, whenever possible, with experimental data obtained from the literature. (authors)

  7. Microprobing the Molecular Spatial Distribution and Structural Architecture of Feed-type Sorghum Seed Tissue (Sorghum Bicolor L.) using the Synchrotron Radiation Infrared Microspectroscopy Technique

    International Nuclear Information System (INIS)

    Yu, P.

    2011-01-01

    Sorghum seed (Sorghum bicolor L.) has unique degradation and fermentation behaviours compared with other cereal grains such as wheat, barley and corn. This may be related to its cell and cell-wall architecture. The advanced synchrotron radiation infrared microspectroscopy (SR-IMS) technique enables the study of cell or living cell biochemistry within cellular dimensions. The objective of this study was to use the SR-IMS imaging technique to microprobe molecular spatial distribution and cell architecture of the sorghum seed tissue comprehensively. High-density mapping was carried out using SR-IMS on beamline U2B at the National Synchrotron Light Source (Brookhaven National Laboratory, NY, USA). Molecular images were systematically recorded from the outside to the inside of the seed tissue under various chemical functional groups and their ratios [peaks at ∼1725 (carbonyl C=O ester), 1650 (amide I), 1657 (protein secondary structure α-helix), 1628 (protein secondary structure β-sheet), 1550 (amide II), 1515 (aromatic compounds of lignin), 1428, 1371, 1245 (cellulosic compounds in plant seed tissue), 1025 (non-structural CHO, starch granules), 1246 (cellulosic material), 1160 (CHO), 1150 (CHO), 1080 (CHO), 930 (CHO), 860 (CHO), 3350 (OH and NH stretching), 2960 (CH 3 anti-symmetric), 2929 (CH 2 anti-symmetric), 2877 (CH 3 symmetric) and 2848 cm -1 (CH 2 asymmetric)]. The relative protein secondary structure α-helix to β-sheet ratio image, protein amide I to starch granule ratio image, and anti-symmetric CH 3 to CH 2 ratio image were also investigated within the intact sorghum seed tissue. The results showed unique cell architecture, and the molecular spatial distribution and intensity in the sorghum seed tissue (which were analyzed through microprobe molecular imaging) were generated using SR-IMS. This imaging technique and methodology has high potential and could be used for scientists to develop specific cereal grain varieties with targeted food and feed

  8. Electronic technology

    International Nuclear Information System (INIS)

    Kim, Jin Su

    2010-07-01

    This book is composed of five chapters, which introduces electronic technology about understanding of electronic, electronic component, radio, electronic application, communication technology, semiconductor on its basic, free electron and hole, intrinsic semiconductor and semiconductor element, Diode such as PN junction diode, characteristic of junction diode, rectifier circuit and smoothing circuit, transistor on structure of transistor, characteristic of transistor and common emitter circuit, electronic application about electronic equipment, communication technology and education, robot technology and high electronic technology.

  9. Influência das condições do ambiente e idade de carregamento na fluência por secagem do CAA

    Directory of Open Access Journals (Sweden)

    A. C. Marques

    Full Text Available A fluência é um fenômeno que ocorre devido à movimentação de água no interior do concreto e é afetada por vários fatores que agem simultaneamente. Dentre estes fatores estão às condições do ambiente (umidade relativa do ar e temperatura ao qual o elemento, ou corpo de prova, está submetido. Neste trabalho são feitas comparações entre resultados experimentais de fluência por secagem de corpos de prova carregados em idades diferentes e mantidos em ambiente controlado (câmara climatizada e não controlado. Além disso, são feitas comparações entre estes resultados com os fornecidos por modelos de previsão disponíveis na literatura. A partir dos resultados pode-se notar que alterações da umidade durante o primeiro mês de ensaio apresentam maior influência nas deformações e que concretos carregados com maiores idades apresentam menores deformações por fluência. Foi observado na comparação entre modelos de previsão que o modelo do ACI e GL melhor preveem a fluência.

  10. Relação da idade óssea com antropometria e aptidão física em jovens praticantes de voleibol

    Directory of Open Access Journals (Sweden)

    Suzet de Araujo Tinoco Cabral

    2016-03-01

    Full Text Available Resumo O estudo teve como objetivo correlacionar a idade óssea, os componentes antropométricos e a aptidão física em 149 crianças de 8 a 14 anos. Foram aferidos estatura, massa corporal, perímetros de braço e de perna, perímetros de braço e de perna corrigidos, diâmetros bicristailíaco e biacromial, dobras cutâneas tricipital e perna, teste motores de agilidade, velocidade de membros superiores e força explosiva de membros inferiores e superiores e o exame de raios X de mão e punho para verificar maturação. Nos resultados, encontramos correlação positiva entre a idade óssea e as demais variáveis, com exceção das dobras cutâneas tricipital, de perna e teste de agilidade. Dessa forma, verificamos a influência da maturação sobre componentes antropométricos e motores. Assim, possibilitamos uma melhor forma de controle dos processos de detecção, seleção e orientação esportiva.

  11. Motivação intrínseca e extrínseca: diferenças no sexo e na idade

    Directory of Open Access Journals (Sweden)

    Simone Maria Pansera

    Full Text Available Resumo A orientação motivacional é um determinante crítico do nível e da qualidade da aprendizagem. Este estudo investigou os níveis de orientação motivacional e as possíveis diferenças entre idade e sexo em 142 crianças de nove e 10 anos alunos de escolas públicas. A "Scale of Intrisic versus Extrinsic Orientation in Classroom" de Harter (1980 foi o instrumento utilizado para a coleta de dados. A escala foi aplicada individualmente e lidaem voz alta pela pesquisadora para melhor compreensão da criança. Os resultados apontam para: (1 níveis moderados de motivação intrínseca em todas as dimensões investigadas; (2 semelhanças na orientação motivacional entre meninos e meninas; (3 semelhanças na orientação motivacional entre as idades. Os níveis moderados de motivação intrínseca apresentados indicam que as crianças deste estudo manifestam interesse nas tarefas e se envolvem com o processo de aprendizagem.

  12. The Electron

    Energy Technology Data Exchange (ETDEWEB)

    Thomson, George

    1972-01-01

    Electrons are elementary particles of atoms that revolve around and outside the nucleus and have a negative charge. This booklet discusses how electrons relate to electricity, some applications of electrons, electrons as waves, electrons in atoms and solids, the electron microscope, among other things.

  13. CL-imaging and ion microprobe dating of single zircons from a high-grade rock from the Central Zone, Limpopo Belt, South Africa: Evidence for a single metamorphic event at ˜2.0 Ga

    Science.gov (United States)

    Mouri, H.; Brandl, G.; Whitehouse, M.; de Waal, S.; Guiraud, M.

    2008-02-01

    The combination of ion microprobe dating and cathodoluminescence (CL) imaging of zircons from a high-grade rock from the Central Zone of the Limpopo Belt were used to constrain the age of metamorphic events in the area. Zircon grains extracted from an orthopyroxene-gedrite-bearing granulite were prepared for single crystal CL-imaging and ion microprobe dating. The grains display complex zoning when using SEM-based CL-imaging. A common feature in most grains is the presence of a distinct core with a broken oscillatory zoned structure, which clearly appears to be the remnant of an original grain of igneous origin. This core is overgrown by an unzoned thin rim measuring about 10-30 μm in diameter, which is considered as new zircon growth during a single metamorphic event. Selected domains of the zircon grains were analysed for U, Pb and Th isotopic composition using a CAMECA IMS 1270 ion microprobe (Nordsim facility). Most of the grains define a near-concordant cluster with some evidence of Pb loss. The most concordant ages of the cores yielded a weighted mean 207Pb/ 206Pb age of 2689 ± 15 (2 σ) Ma, interpreted as the age of the protolith of an igneous origin. The unzoned overgrowths of the zircon grains yielded a considerably younger weighted mean 207Pb/ 206Pb age of ˜2006.5 ± 8.0 Ma (2 σ), and these data are interpreted to reflect closely the age of the ubiquitous high-grade metamorphic event in the Central Zone. This study shows clearly, based on both the internal structure of the zircons and the data obtained by ion microprobe dating, that only a single metamorphic event is recorded by the studied 2.69 Ga old rocks, and we found no evidence of an earlier metamorphic event at ˜2.5 Ga as postulated earlier by some workers.

  14. Valores de energia metabolizável de alguns alimentos obtidos com aves de diferentes idades Metabolizable energy values of feedstuffs obtained from poultry at different ages

    Directory of Open Access Journals (Sweden)

    Heloisa Helena de Carvalho Mello

    2009-05-01

    Full Text Available Foram realizados quatro ensaios de metabolismo com a finalidade de determinar a energia metabolizável aparente (EMA e a energia metabolizável aparente corrigida (EMAn de dez alimentos em aves em diversas idades. Os alimentos testados foram: milho, farelo de soja, sorgo, farelo de trigo, farelo de arroz integral, duas farinhas de penas, duas farinhas de vísceras e plasma sangüíneo. Utilizou-se o método de coleta total de excretas, em delineamento experimental inteiramente casualizado, com 11 tratamentos (dez alimentos e uma ração-referência e seis repetições. No primeiro ensaio, foram utilizados 528 pintos de corte machos de 10 a 17 dias de idade, totalizando oito aves por repetição; no segundo ensaio, 396 frangos de corte machos de 26 a 33 dias de idade, com seis aves por repetição; no terceiro ensaio, 264 frangos de corte machos de 40 a 47 dias de idade, com quatro aves por repetição; e, no quarto ensaio, 132 galos, com duas aves por repetição. A idade das aves influenciou os valores de EMA e EMAn do farelo de soja, do sorgo, do farelo de arroz integral, das farinhas de penas e do plasma sangüíneo, enquanto, para o farelo de trigo, teve efeito apenas sobre a EMAn.Four assays were carried out to determine the apparent metabolizable energy (AME and the corrected apparent nitrogen metabolizable energy (AMEn of ten feeds for poultry at different poultry ages. The feeds studied were: corn grain, soybean meal, ground sorghum, wheat bran, integral rice bran, two kinds of feather meal, two kinds of poultry viscera meal and spray-dried plasma. The method of total excreta collection was used to determine the AME and AMEn values. The broiler chicks were distributed on a completely randomized experimental design, with 11 treatments, six replications, with different number of animals by replication according to the assay. In the first assay, 528 male broiler chicks in the period from 10 to 17 days of age were used, with eight animals

  15. Hard electronics; Hard electronics

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    1997-03-01

    Hard material technologies were surveyed to establish the hard electronic technology which offers superior characteristics under hard operational or environmental conditions as compared with conventional Si devices. The following technologies were separately surveyed: (1) The device and integration technologies of wide gap hard semiconductors such as SiC, diamond and nitride, (2) The technology of hard semiconductor devices for vacuum micro- electronics technology, and (3) The technology of hard new material devices for oxides. The formation technology of oxide thin films made remarkable progress after discovery of oxide superconductor materials, resulting in development of an atomic layer growth method and mist deposition method. This leading research is expected to solve such issues difficult to be easily realized by current Si technology as high-power, high-frequency and low-loss devices in power electronics, high temperature-proof and radiation-proof devices in ultimate electronics, and high-speed and dense- integrated devices in information electronics. 432 refs., 136 figs., 15 tabs.

  16. Penetration of UV-A, UV-B, blue, and red light into leaf tissues of pecan measured by a fiber optic microprobe system

    Science.gov (United States)

    Qi, Yadong; Bai, Shuju; Vogelmann, Thomas C.; Heisler, Gordon M.

    2003-11-01

    The depth of light penetration from the adaxial surfaces of the mature leaves of pecan (Carya illinoensis) was measured using a fiber optic microprobe system at four wavelengths: UV-B (310nm), UV-A (360 nm), blue light (430nm), and red light (680nm). The average thickness of the leaf adaxial epidermal layer was 15um and the total leaf thickness was 219um. The patterns of the light attenuation by the leaf tissues exhibited strong wavelength dependence. The leaf adaxial epidermal layer was chiefly responsible for absorbing the UV-A UV-B radiation. About 98% of 310 nm light was steeply attenuated within the first 5 um of the adaxial epidermis; thus, very little UV-B radiation was transmitted to the mesophyll tissues where contain photosynthetically sensitive sites. The adaxial epidermis also attenuated 96% of the UV-A radiation. In contrast, the blue and red light penetrated much deeper and was gradually attenutated by the leaves. The mesophyll tissues attenuated 17% of the blue light and 42% of the red light, which were available for photosynthesis use. Since the epidermal layer absorbed nearly all UV-B light, it acted as an effective filter screening out the harmful radiation and protecting photosynthetically sensitive tissues from the UV-B damage. Therefore, the epidermal function of the UV-B screening effectiveness can be regarded as one of the UV-B protection mechanisms in pecan.

  17. The Stanford-U.S. Geological Survey SHRIMP ion microprobe--a tool for micro-scale chemical and isotopic analysis

    Science.gov (United States)

    Bacon, Charles R.; Grove, Marty; Vazquez, Jorge A.; Coble, Matthew A.

    2012-01-01

    Answers to many questions in Earth science require chemical analysis of minute volumes of minerals, volcanic glass, or biological materials. Secondary Ion Mass Spectrometry (SIMS) is an extremely sensitive analytical method in which a 5–30 micrometer diameter "primary" beam of charged particles (ions) is focused on a region of a solid specimen to sputter secondary ions from 1–5 nanograms of the sample under high vacuum. The elemental abundances and isotopic ratios of these secondary ions are determined with a mass spectrometer. These results can be used for geochronology to determine the age of a region within a crystal thousands to billions of years old or to precisely measure trace abundances of chemical elements at concentrations as low as parts per billion. A partnership of the U.S. Geological Survey and the Stanford University School of Earth Sciences operates a large SIMS instrument, the Sensitive High-Resolution Ion Microprobe with Reverse Geometry (SHRIMP–RG) on the Stanford campus.

  18. Ted Hall and the science of biological microprobe X-ray analysis: a historical perspective of methodology and biological dividends.

    Science.gov (United States)

    Gupta, B L

    1991-06-01

    This review surveys the emergence of electron probe X-ray microanalysis as a quantitative method for measuring the chemical elements in situ. The extension of the method to the biological sciences under the influence of Ted Hall is reviewed. Some classical experiments by Hall and his colleagues in Cambridge, UK, previously unpublished, are described; as are some of the earliest quantitative results from the cryo-sections obtained in Cambridge and elsewhere. The progress of the methodology is critically evaluated from the earliest starts to the present state of the art. Particular attention has been focused on the application of the method in providing fresh insights into the role of ions in cell and tissue physiology and pathology. A comprehensive list of references is included for a further pursuit of the topics by the interested reader.

  19. Electron radiography

    Science.gov (United States)

    Merrill, Frank E.; Morris, Christopher

    2005-05-17

    A system capable of performing radiography using a beam of electrons. Diffuser means receive a beam of electrons and diffuse the electrons before they enter first matching quadrupoles where the diffused electrons are focused prior to the diffused electrons entering an object. First imaging quadrupoles receive the focused diffused electrons after the focused diffused electrons have been scattered by the object for focusing the scattered electrons. Collimator means receive the scattered electrons and remove scattered electrons that have scattered to large angles. Second imaging quadrupoles receive the collimated scattered electrons and refocus the collimated scattered electrons and map the focused collimated scattered electrons to transverse locations on an image plane representative of the electrons' positions in the object.

  20. Influência da idade na geração de modelos de espectroscopia NIR, para predição de propriedades da madeira de Eucalyptus spp.

    Directory of Open Access Journals (Sweden)

    Flaviana Reis Milagres

    2013-12-01

    Full Text Available O objetivo deste trabalho foi o desenvolvimento de modelos NIRS para predizer as propriedades físicas e químicas de madeiras de Eucalyptus, com idades variando de 3 a 7 anos. Foram utilizadas 136 amostras e realizadas análises laboratoriais de densidade básica, teores de lignina e extrativos. Amostras de cavacos foram moídas em moinho tipo ciclone, para coleta de espectros NIR. Os modelos foram desenvolvidos por regressão de mínimos quadrados parciais (PLS, sendo testadas transformações matemáticas. Para validação dos modelos, foram utilizados grupos de amostras externas com diferentes idades, que não participaram no desenvolvimento do modelo. Os modelos desenvolvidos resultaram em consideráveis coeficientes de determinação para densidade básica (R² 0,84 a 0,89 e lignina (R² 0,72 a 0,88, mas os melhores valores foram encontrados para o teor de extrativos (R² 0,92 a 0,98. Pelos valores de relação de desempenho de desvio (RPD, verificou-se que amostras com idades diferentes das utilizadas no desenvolvimento dos modelos não apresentaram boas predições, exceto para densidade básica cujos modelos desenvolvidos especificamente para as idades de 3 e 7 anos, predisseram satisfatoriamente amostras com idades entre 4 e 6 anos.

  1. X-ray microprobe analysis of the retina and RPE in sheep with ovine ceroid-lipofuscinosis

    International Nuclear Information System (INIS)

    Samuelson, D.A.; Armstrong, D.; Jolly, R.

    1990-01-01

    Ovine ceroid-lipofuscinosis (OCL) is one animal model for the human condition, and because autofluorescent lipopigments are prominent in the brain and eye, it may also prove useful as a model for aging. For example, a progressive decline in electrical recording from brain and retina are observed in both aging and OCL. Samples of retinal and retinal pigment epithelial (RPE) tissues were obtained from a young control. 2 animals with OCL and a normal aged sheep. Specimens were cryo-fractured and examined by scanning electron microscopy/x-ray microanalysis. Measurements made of 6 individual cells in the ganglion layer of OCL specimens, the remainder of the retina, and RPE showed age-related changes in zinc, iron, and copper which were associated with lipopigment accumulation in the RPE. There was marked decrease in phosphate, sulfur, and manganese levels, as photoreceptor cells and their outer segments are lost in the disease process. This is the first report of metal analysis in the retina and RPE in a disease entity, and as a function of normal aging

  2. Silage quality of pearl millet cultivars produced in different cutting agesQualidade da silagem de cultivares de milheto produzidas em diferentes idades de corte

    Directory of Open Access Journals (Sweden)

    Welma Santos Cruvinel

    2012-06-01

    Full Text Available The millet has being prominent in recent years, especially with the arrival of early genotypes with high nutritional value and productive potential, coming from breeding. As these genotypes are new, little information exists about them. Thus, it is important to obtain technical information, supported by scientific studies about the behavior of these materials considering the nutritional value and harvest for silage production. The objective of this research was to evaluate the silage quality of pearl millet genotypes grown in different cuts age. The experiment was carried out on the campus of the Agronomy, of the Rio Verde University. The experimental design was randomized blocks with four replications in a 5 x 3 factorial, with five genotypes of millet: ARD 500, ADR 7010, LAB 0730, LAB 0731 and LAB 0732 and three cuts ages: 57, 65 and 73 days after sowing (DAS. The results showed that silages produced by millet, regardless of genotype, could be considered of nutritional value. Since this is a precocious material the best age that provided the best quality of these silages was when the materials were harvested at 57 DAS.O milheto vem ganhando destaque nos últimos anos, principalmente com a chegada de genótipos precoces e de alto valor nutritivo e potencial produtivo, oriundos do melhoramento genético. Por se tratarem de materiais novos, existem poucas informações sobre esses genótipos. Nesse sentido, é importante obter informações técnicas, apoiadas em estudos científicos, sobre o comportamento desses materiais em relação ao valor nutritivo e época de colheita para a produção de silagens. Diante disso, objetivou-se avaliar a qualidade de silagem de genótipos de milheto produzidas em diferentes idades de cortes. O experimento foi conduzido no Campus da Faculdade de Agronomia da Universidade de Rio Verde. O delineamento experimental utilizado foi de blocos ao acaso, com quatro repetições, em esquema fatorial 5 x 3, sendo, cinco

  3. Avaliação da influência da idade no potencial evocado auditivo de tronco encefálico

    Directory of Open Access Journals (Sweden)

    Anias C. R.

    2004-01-01

    Full Text Available O potencial evocado auditivo de tronco encefálico (ABR é um método simples, objetivo e não invasivo de avaliação das vias auditivas do tronco encefálico, que pode ser realizado em qualquer idade e que detecta a atividade elétrica desde a orelha interna até o colículo inferior. O ABR é composto por 7 ondas (I - VII, sendo as ondas I, III e V os componentes mais importantes. O nível de sensação (NS é uma unidade de estímulo que se baseia no limiar psicoacústico do indivíduo e a esse limiar acrescenta-se uma determinada intensidade de estímulo em decibel (dB, com o objetivo de fornecer a mesma quantidade de energia acústica em caso de perdas auditivas assimétricas. OBJETIVO: Avaliar a influência da idade no ABR em homens, utilizando o NS como unidade de estímulo. FORMA DE ESTUDO: Observacional coorte com corte transversal. MATERIAL E MÉTODO: Quinze indivíduos do sexo masculino entre 20 e 30 anos e 15 do sexo masculino a partir de 60 anos passaram por um critério clínico de seleção a fim de afastar outros fatores que pudessem influenciar os resultados. Foram determinadas as latências absolutas das ondas I, III, e V e as latências interpicos (LIPs I-III, III-V e I-V nos 2 grupos e os dados obtidos foram analisados estatisticamente. RESULTADOS: As latências absolutas e interpicos do ABR foram semelhantes nos 2 grupos estudados. CONCLUSÃO: No grupo etário analisado e nas condições pré-estabelecidas neste estudo, a idade não representou um fator de influência nos achados do ABR.

  4. Avaliação do tratamento cirúrgico da cardiopatia congênita em pacientes com idade superior a 16 anos

    Directory of Open Access Journals (Sweden)

    Luiz Fernando Caneo

    2012-05-01

    Full Text Available FUNDAMENTO: O número crescente de crianças com cardiopatias congênitas em evolução demanda maior preparo dos profissionais e das instituições que as manuseiam. OBJETIVO: Descrever o perfil dos pacientes com idade superior a 16 anos com cardiopatia congênita operados e analisar os fatores de risco preditivos de mortalidade hospitalar. MÉTODOS: Mil, quinhentos e vinte pacientes (idade média 27 ± 13 anos foram operados entre janeiro de 1986 e dezembro de 2010. Foram realizadas análise descritiva do perfil epidemiológico da população estudada e análise dos fatores de risco para mortalidade hospitalar, considerando escore de complexidade, ano em que a cirurgia foi realizada, procedimento realizado pelo cirurgião pediátrico ou não e presença de reoperação. RESULTADOS: Ocorreu um crescimento expressivo no número de casos a partir do ano 2000. A média do escore de complexidade foi 5,4 e os defeitos septais corresponderam a 45% dos casos. A mortalidade geral foi 7,7% e o maior número de procedimentos (973 ou 61,9% com maior complexidade foi realizado por cirurgiões pediátricos. Complexidade (OR 1,5, reoperação (OR 2,17 e cirurgião pediátrico (OR 0,28 foram fatores de risco independentes que influenciaram a mortalidade. A análise multivariada mostrou que o ano em que a cirurgia foi realizada (OR 1,03, a complexidade (OR 1,44 e o cirurgião pediátrico (OR 0,28 influenciaram no resultado. CONCLUSÃO: Observa-se um número crescente de pacientes com idade superior a 16 anos e que, apesar do grande número de casos simples, os mais complexos foram encaminhados para os cirurgiões pediátricos, que apresentaram menor mortalidade, em especial nos anos mais recentes. (Arq Bras Cardiol. 2012; [online].ahead print, PP.0-0

  5. Influência da idade do hospedeiro e da aprendizagem no comportamento quimiotáxico e no parasitismo de Trichogramma pretiosum

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    Camila C. Vargas

    Full Text Available RESUMO Trichogramma pretiosum Riley, 1879 mantido em ovos de Ephestia kuehniella Zeller, 1879, tem sido utilizado no controle biológico de Spodoptera frugiperda (J. E. Smith, 1797. No entanto, fatores como idade do hospedeiro e experiência prévia, podem influenciar o parasitismo e o comportamento do parasitoide. Esse estudo avaliou a influência da idade dos ovos e da experiência em ovos e extrato de ovos de S. frugiperda no comportamento quimiotáxico e no parasitismo de T. pretiosum. Ovos de S. frugiperda com 24, 48 e 72 horas, foram expostos a fêmeas de T. pretiosum. Também foi avaliado o tempo de experiência do parasitoide, no mesmo hospedeiro, por 1, 3, 4, 5, 6 e 24 horas, assim como, seu tempo de exposição (1, 2, 3 e 24 horas. As respostas quimiotáxicas de T. pretiosum (experiente e não experiente em extrato de ovos de S. frugiperda foram observadas em olfatômetro tipo Y. As taxas de parasitismo foram registradas em teste de escolha, com insetos experientes e inexperientes com ovos e extrato de ovos de S. frugiperda. O parasitismo em S. frugiperda foi significativamente maior em ovos com 24 horas de idade. Fêmeas inexperientes e experientes por 1, 3 e 4 horas, apresentaram uma menor taxa de parasitismo, quando comparadas a fêmeas expostas por 5, 6 e 24 horas. Não houve diferença de parasitismo em fêmeas expostas por 2, 3 e 24 horas, comparadas às expostas por uma hora. Fêmeas experientes foram mais atraídas ao extrato de ovos de S. frugiperda, do que ao controle (hexano. A porcentagem de parasitismo, em fêmeas inexperientes, foi maior em ovos de E. kuehniella (hospedeiro de origem, no entanto, o mesmo resultado não foi observado em fêmeas experientes.

  6. Consumo alimentar entre crianças brasileiras com idade de 6 a 59 meses Food consumption Brazilian children by 6 to 59 months of age

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    Gisele Ane Bortolini

    2012-09-01

    Full Text Available O objetivo foi avaliar o consumo alimentar em crianças brasileiras de 6-59 meses de idade, por região e zona de residência. Trata-se de estudo descritivo transversal com 4.322 crianças investigadas na Pesquisa Nacional de Demografia e Saúde (2006/2007. Observou-se baixo consumo diário de verduras (12,7%, legumes (21,8%, carnes (24,6% e elevado consumo de refrigerantes (40,5%, alimentos fritos (39,4%, salgadinhos (39,4%, doces (37,8%, na frequência de uma a três vezes na semana. Comparando-se as regiões, as crianças residentes no Sul, Sudeste e Centro-oeste consumiram com mais frequência arroz, pão, batata, feijão, verdura de folha, legumes e carne, mas também consumiram, mais frequentemente, alimentos não recomendados para a idade, como doces e refrigerantes. Crianças da zona rural apresentaram menor consumo dos alimentos recomendados para a idade e, também, dos não recomendados, quando comparadas às crianças da zona urbana. O consumo alimentar evidenciado neste estudo não está de acordo com recomendações de alimentação saudável para crianças.The aim of this study was to assess food consumption in Brazilian children 6 to 59 months of age by region of the country and area of residence. This was a descriptive cross-sectional study of 4,322 children in the National Demographic and Health Survey (2006-2007. The data showed low daily consumption of leafy vegetables (12.7%, vegetables (21.8%, and meat (24.6% and high consumption (1-3 times a week of soft drinks (40.5%, fried foods (39.4%, salty snacks (39.4%, and sweets (37.8%. Comparing the regions of Brazil, children in the South, Southeast, and Central-West consumed more rice, bread, potatoes, beans, greens, vegetables, and meat, but they also ate more foods not recommended for their age, like sweets and soft drinks (soda. Rural children showed lower consumption of foods recommended for their age and also those not recommended for their age, as compared to their urban

  7. Gênero, sexualidade e idade: tramas heteronormativas nas práticas pedagógicas da educação física escolar

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    Priscila Gomes Dornelles

    2015-12-01

    Full Text Available Resumo O artigo analisa a produção da (heteronormalização do gênero e da sexualidade em articulação com a idade na trama da educação física escolar. Apresenta parte dos resultados de uma pesquisa que buscou analisar as práticas pedagógicas desenvolvidas por docentes que ministram aulas de educação física em escolas estaduais distribuídas em sete cidades dos nove municípios que compõem a região do Vale do Jiquiriçá (BA. Para acessar esses sujeitos, foi realizado um seminário de formação de professores e utilizaram-se grupo focal e entrevistas como estratégias metodológicas. Tomando como referências teórico-metodológicas e políticas os estudos feministas pós-estruturalistas, a teoriaqueer e os estudos foucaultianos, discute-se como a dimensão cronológica é tratada de forma fixa e etapista e torna-se definidora do que se pode conhecer e de como se pode conhecer na escola. A pesquisa aponta para certa conexão, por vezes contínua e, em outros momentos, descontínua, entre gênero, sexualidade e idade nas aulas de educação física da região investigada. Por um lado, docentes indicam que a sexualidade se manifesta na escola desde cedo, ainda na infância, em função de fatores regionais, e de forma exacerbada nos meninos. Por outro lado, a idade cronológica dos corpos dos estudantes funciona como uma norma regulatória quando se trata dos temas da sexualidade, o que contribui para reforçar a promoção/assunção do pressuposto sexo-gênero-prática heterossexual como natural a partir da adolescência.

  8. Nutrição precoce de neonatos prematuros estáveis e pequenos para a idade gestacional: um ensaio clínico randomizado

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    Shmuel Arnon

    2013-08-01

    Full Text Available OBJETIVO: Examinar o efeito da nutrição precoce sobre o tempo para atingir a nutrição completa em neonatos prematuros (PIG estáveis pequenos para a idade gestacional. MÉTODO: Os neonatos prematuros com idade gestacional inferior a 37 semanas e peso ao nascer inferior a 10% foram alocados aleatoriamente para um regime de nutrição precoce (nas primeiras 24 horas de vida ou tardia (após as primeiras 24 horas de vida. Todos os neonatos apresentaram uma evidência intrauterina de fluxo diastólico reverso ou ausente. Os neonatos incapazes de iniciar uma nutrição precoce foram excluídos. O tempo para a alimentação completa, a progressão da nutrição e morbidez correspondente foram comparados. A eletrogastrografia (EGG foi utilizada para mensurar a motilidade gástrica pré e pós-prandial no segundo e no sétimo dias após o início da nutrição. RESULTADOS: Foram incluídos 60 neonatos no estudo, sendo 30 em cada grupo. Os neonatos incluídos no regime de nutrição precoce atingiram a nutrição enteral completa antes dos neonatos do grupo de controle (98±80-157 em comparação a 172±1 23-261 horas de idade, respectivamente; p = 0,004 e recebiam alta hospitalar antes (p = 0,04. Nenhuma enterocolite necrosante (ECN foi comprovada em ambos os grupos de estudo. A motilidade gástrica melhorou no sétimo dia após o início da nutrição em ambos os grupos de estudo, sem diferença entre eles. CONCLUSÕES: Os neonatos prematuros PIG estáveis em regime de nutrição precoce atingiram alimentação enteral completa e receberam alta hospitalar significativamente antes que aqueles em regime de nutrição tardio, sem morbidez excedente.

  9. Percepções dos professores sobre a influência da alergia nos comportamentos e desempenho cognitivo das crianças em idade escolar

    OpenAIRE

    Jesus, António C.; Carvalho, Graça Simões de

    2008-01-01

    Estudos realizados pela Sociedade Portuguesa de Alergologia e Imunologia Clínica (SPAIC) em 1998 apontam para uma prevalência de rinite alérgica de 9,55% na população portuguesa. Neste estudo, pretende-se saber qual a percepção dos Professores do 1º Ciclo do Ensino Básico sobre o impacto da patologia alérgica em crianças em idade escolar. Foram distribuídos 230 inquéritos em zona rural e urbana, sendo recolhidos 108, elaborados a partir de 10 questões consideradas fundamentais na área da s...

  10. Influência da idade da planta e da maturação dos frutos no momento da colheita na qualidade do café

    OpenAIRE

    Borges,Fernanda Barbosa; Jorge,José Tadeu; Noronha,Regina

    2002-01-01

    São de grande importância os cuidados no preparo do café desde a colheita até o consumo e o estudo de parâmetros que possam influenciar na classificação comercial do grão e na qualidade da bebida. Teve-se como objetivos analisar a influência da idade das plantas, pertencentes à mesma variedade, e dos estágios de maturação dos grãos (secos, cerejas e verdes) no resultado da classificação comercial e na qualidade da bebida. Realizou-se a colheita, por derriça no pano, de uma área com café arábi...

  11. Correlação entre a Autofluorescência de Fundo e o SD-OCT na Degenerescência Macular Ligada à Idade Exsudativa

    OpenAIRE

    Miranda, Ana Filipa

    2016-01-01

    Introdução: Estudos têm mostrado que na degenerescência macular ligada à idade (DMLI) exsudativa uma maior área de alteração do epitélio pigmentar retiniano (EPR) na autofluorescência de fundo (FAF) está associada a perda da acuidade visual (AV). Não existe, no entanto, nenhum estudo realizado nestes doentes que integre as alterações verificadas na FAF com a informação anatómica da tomografia de coerência óptica spectral domain (SD-OCT). Objectivo: Investigar a correlação entre a FAF e os res...

  12. Influência das condições do ambiente e idade de carregamento na fluência por secagem do CAA

    OpenAIRE

    Marques,A. C.; Bittencourt,T. N.; Barbosa,M. P.

    2013-01-01

    A fluência é um fenômeno que ocorre devido à movimentação de água no interior do concreto e é afetada por vários fatores que agem simultaneamente. Dentre estes fatores estão às condições do ambiente (umidade relativa do ar e temperatura) ao qual o elemento, ou corpo de prova, está submetido. Neste trabalho são feitas comparações entre resultados experimentais de fluência por secagem de corpos de prova carregados em idades diferentes e mantidos em ambiente controlado (câmara climatizada) e não...

  13. Avaliação dos benefícios da ginástica localizada sobre a postura e a flexibilidade de mulheres na terceira idade

    OpenAIRE

    Lima,Hélia Cristina Oliveira; Aguiar,Jaina Bezerra de; Paredes,Paulo Fernando Machado; Gurgel,Luilma Albuquerque

    2010-01-01

    Desvios posturais e redução na flexibilidade são alterações observadas com o avançar da idade, podendo desencadear dor e dificuldades de movimentação. Este estudo buscou avaliar a influência de um programa de ginástica, de dois meses de duração, sobre a postura e flexibilidade de idosas institucionalizadas (n = 10, 60-75 anos). A postura foi avaliada através do uso de simetrógrafo, fotografias e do teste de equilíbrio sagital pélvico, e a flexibilidade através do teste de sentar e alcançar. C...

  14. Lino: game eletrônico para auxiliar na educação ambiental de crianças em idade escolar

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    Aldo Nascimento Pontes

    2017-12-01

    Full Text Available O caráter lúdico dos games, nas últimas décadas, tem mostrado seu rico potencial na dinamização de processos de ensino-aprendizagem. Este trabalho tem por objetivo apresentar os resultados de uma pesquisa que desenvolveu um game eletrônico para auxiliar na Educação Ambiental de crianças em idade escolar. Assim, por meio de uma pesquisa experimental, desenvolveu-se e implementou-se o jogo Lino, o qual foi submetido a uma avaliação de funcionalidades.  Os resultados mostraram que o Lino representa um caminho lúdico, agradável e didático para expandir a conscientização e a atitude das crianças sobre a questão ambiental.

  15. Vitaminas e antioxidantes na degeneração macular relacionada à idade Vitamins and antioxidants in age-related macular degeneration

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    Pedro Durães Serracarbassa

    2006-06-01

    Full Text Available O autor descreve os efeitos bioquímicos e estruturais das vitaminas e antioxidantes na retina. Apresenta as principais substâncias presentes na dieta alimentar e na suplementação vitamínica envolvidas na gênese da degeneração macular relacionada à idade. Relata ainda os resultados de estudos prospectivos multicêntricos relacionados ao assunto, por meio de revisão bibliográfica.The author describes biochemical and structural effects of vitamins and antioxidants on the retina. The main substances present in diet food and vitamin supplies involved in the genesis of age-related macular degeneration are shown. Also reports on the outcomes of prospective studies related to the subject, by literature review are presented.

  16. Stress, satisfação e expectativas parentais em mães e pais de crianças em idade escolar

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    Vieira, Simone Frazão

    2015-01-01

    Tese de mestrado, Psicologia (Secção de Psicologia Clínica e da Saúde, Núcleo de Psicologia Clínica Dinâmica), Universidade de Lisboa, Faculdade de Psicologia, 2015 O presente estudo, com mães e pais de crianças em idade escolar, tem os seguintes objetivos: 1) analisar se as mães e os pais se distinguem no stress parental e na satisfação e expectativas parentais; 2) explorar a relação entre o stress parental e a satisfação e expectativas parentais; 3) averiguar a relação das referidas dime...

  17. Relação entre cintura-quadril e imagem corporal em mulheres de meia-idade e idosas ativas fisicamente

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    Priscila Gonçalves Soares

    2014-06-01

    Full Text Available O estudo busca relacionar autoimagem com a relação cintura-quadril e avaliar, assim, a satisfação com a autoimagem em mulheres com idade média de 60,5(±11,12 anos. Para avaliar a satisfação com a imagem corporal, usou-se a Escala de Desenhos de Silhuetas de Stunkard, Sorensen e Schulsinger (1983. A maior parte das mulheres está insatisfeita com sua imagem corporal. Intervenções neste grupo se fazem necessárias através de trabalhos psicológicos e nutricionais, além de atividade física.  

  18. Fatores de risco para internação por doença respiratória aguda em crianças até um ano de idade

    OpenAIRE

    Macedo,Silvia Elaine Cardozo; Menezes,Ana Maria Baptista; Albernaz,Elaine; Post,Paulo; Knorst,Marli

    2007-01-01

    OBJETIVO: Avaliar fatores de risco para hospitalização por doença respiratória aguda em crianças até um ano de idade. MÉTODOS: Estudo de casos e controles na cidade de Pelotas, RS. Os casos foram crianças de até um ano de idade, que se hospitalizaram por doença respiratória aguda, de agosto de 1997 a julho de 1998. Os controles foram crianças da comunidade, da mesma idade, sem hospitalização prévia por essa doença. Um questionário investigando exposição a fatores de risco foi aplicado às mães...

  19. RELAÇÃO ENTRE IDADE E CAPACIDADE FUNCIONAL DE IDOSAS RESIDENTES EM INSTITUIÇÕES DE LONGA PERMANÊNCIA NA CIDADE DE FORTALEZA/CE

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    Darling Kescia Araújo Peixoto Braga

    2014-12-01

    Full Text Available Introdução: O envelhecimento gera desgastes fisiológicos próprios. O sistema de valores socioculturais ocidentais e a atual configuração dos arranjos familiares associados aumenta a institucionalização de idosos, que pela fragilidade podem ter déficits na execução das atividades básicas de vida diária (ABVD's e cognição. Objetivo: Avaliar o desempenho nas ABVD, considerando a faixa etária de mulheres idosas residentes em duas Instituições de Longa Permanência para Idosos (ILPI´s na cidade de Fortaleza/CE. Métodos: Estudo seccional, realizado no período de Outubro a Dezembro de 2013 através de um censo com 24 idosas residentes em duas ILPI's. A coleta de dados foi realizada em duas etapas: formulário com caracterização da amostra e o questionário de ABVD de Barthel. Resultados: A amostra possui idade média de 80,04 anos (± 7,91; mín, = 65,0 e máx. = 90,0, eram solteira (66,6%, com baixa escolaridade (33,3% analfabetas e 33,3% com primário completo, procedentes do interior do Estado (58,3% e residiam na instituição há menos de cinco anos (58,3%. O Índice de Barthel revelou que a maioria (75% eram independentes para a realização das ABVDs, sem influenciada da faixa etária. Conclusão: As idosas residentes nas ILPI apresentam independência funcional nas ABVD e sem influência da idade.

  20. Capacidade para o trabalho, saúde e ausência por doença de trabalhadoras de um centro de pesquisa por grupos de idade

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    Maria Silvia Monteiro

    Full Text Available Este estudo avaliou a capacidade para o trabalho de trabalhadoras brasileiras por grupo de idade e ocupação e analisou as ausências por doença registradas durante um ano. A capacidade para o trabalho das mulheres foi avaliada através do Índice de Capacidade para o Trabalho, desenvolvido por pesquisadores finlandeses. Este instrumento é baseado na autopercepção dos trabalhadores e é composto de sete itens. A pesquisa foi desenvolvida no Centro de Pesquisa e Desenvolvimento de uma companhia de alta tecnologia. A taxa de resposta final dos sujeitos foi de 38%. Este artigo inclui somente as trabalhadoras (n=43. A idade dos sujeitos variou de 35 a 54 anos e 79% deles tinham curso universitário. O índice de capacidade para o trabalho médio foi semelhante no grupo mais jovem e no grupo mais velho. A análise dos itens do índice mostrou diferença estatisticamente significante em relação às exigências físicas do trabalho na direção do grupo mais jovem. Em relação ao número de doenças com diagnóstico médico, à ausência por doença no último ano e aos recursos mentais, o grupo mais velho teve melhor desempenho. A promoção de atividades deve ser planejada com o objetivo de reduzir a carga física de trabalho das trabalhadoras mais velhas e de prevenir as doenças mais prevalentes entre todas as trabalhadoras.