Dating of pre hispanic ceramics from the archaeological zone of Zoque by thermoluminescence method

International Nuclear Information System (INIS)

Valdes, J.V.; Gonzalez, P.R.; Mendoza, D.; Tenorio, D.; Terreros, E.; Ramirez, A.

2007-01-01

Full text: The dating of pre hispanic ceramics resides permitting us to located them in a certain period of the history; allows us to verify it origin. The thermoluminescence is a technique that permits us to estimate the absolute age of the archaeological samples. The present work is directed in determining the age by the method of thermoluminescence of archaeological samples of the grotto of Concubac, located in the Serrana Region of Tabasco. To determine the mineralogical composition of the samples, analysis of diffraction of X rays and Energy Dispersive X-ray Spectroscopy (EDS) have been conducted. The radiation emitted by the ground where the samples were buried and the contribution of the cosmic radiation was measured with thermoluminescent dosimeters of LiF:Mg,Cu,P+PTFE. The feasibility of dating of the studied samples is broadly disputed in function of the contents of minerals, as well as the procedure and management of the sample. (Author)

Aberrant thermoluminescence dates obtained from primary volcanic quartz

International Nuclear Information System (INIS)

Guerin, Gilles; Samper, Agnes

2007-01-01

This study deals with the dating by thermoluminescence (TL) of quartz from six volcanic formations of the Saint Lucia Island (Lesser Antilles Arc). Quartz microcrystals up to one millimetre in size were extracted from dacites and pumice flows and prepared in a way similar to the well-known inclusion technique. The TL properties of these quartz were used to estimate apparent palaeodoses using the multi-aliquot protocol. The quartz TL was studied in three different spectral domains: red, green and ultraviolet/blue. The calculated annual dose-rates yielded a set of 18 age-estimates. For some samples complementary dates were obtained using high temperature TL (HTTL) of plagioclase feldspars. These latter dates combined with previously determined radiocarbon and unspiked K-Ar dates were used to explore the validity of ages computed from the TL of quartz. Individual values for quartz appear to be scattered and do not match ages deduced from 14 C, unspiked K-Ar or HTTL on plagioclase dates. These results indicate that when conventional TL methodologies derived from the inclusion method are applied to volcanic quartz major dating problems are to be expected

Aberrant thermoluminescence dates obtained from primary volcanic quartz

Energy Technology Data Exchange (ETDEWEB)

Guerin, Gilles [Laboratoire des Sciences du Climat et de l' Environnement, CEA-CNRS, avenue de la Terrasse, 91191 Gif-sur-Yvette (France)], E-mail: gilles.guerin@u-psud.fr; Samper, Agnes [Laboratoire de geochronologie multitechnique (UPS-IPGP), Universite de Paris-Sud Orsay, 91405 Orsay Cedex (France)

2007-10-15

This study deals with the dating by thermoluminescence (TL) of quartz from six volcanic formations of the Saint Lucia Island (Lesser Antilles Arc). Quartz microcrystals up to one millimetre in size were extracted from dacites and pumice flows and prepared in a way similar to the well-known inclusion technique. The TL properties of these quartz were used to estimate apparent palaeodoses using the multi-aliquot protocol. The quartz TL was studied in three different spectral domains: red, green and ultraviolet/blue. The calculated annual dose-rates yielded a set of 18 age-estimates. For some samples complementary dates were obtained using high temperature TL (HTTL) of plagioclase feldspars. These latter dates combined with previously determined radiocarbon and unspiked K-Ar dates were used to explore the validity of ages computed from the TL of quartz. Individual values for quartz appear to be scattered and do not match ages deduced from {sup 14}C, unspiked K-Ar or HTTL on plagioclase dates. These results indicate that when conventional TL methodologies derived from the inclusion method are applied to volcanic quartz major dating problems are to be expected.

Thermoluminescence dating of sand dunes at Roonka, South Australia

International Nuclear Information System (INIS)

Prescott, J.R.

1983-01-01

Thermoluminescence has been used to date sediments associated with the archaeological excavations at Roonka. An age of 65,000 +- 12,000 years has been found for the terra rossa soil immediately underlying the oldest 14 C dated feature at the main site (18,000 years). At the East Bank site, an age of 2700 +- 300 years is found for the top of the dune at a depth of 30 cm. An age of 14,500 +- 2000 years is found for a stratigraphically distinct and sealed layer at a depth of 1 m. A similar (or possibly older) date is found at 1.7 m. These ages are consistent with the archaeological and geomorphological evidence. There is some evidence that bleaching of sediments by daylight may not be complete in the field. If this is confirmed the ages will need to be revised downwards. (author)

Thermoluminescence dating of chinese porcelain using a regression method of saturating exponential in pre-dose technique

International Nuclear Information System (INIS)

Wang Weida; Xia Junding; Zhou Zhixin; Leung, P.L.

2001-01-01

Thermoluminescence (TL) dating using a regression method of saturating exponential in pre-dose technique was described. 23 porcelain samples from past dynasties of China were dated by this method. The results show that the TL ages are in reasonable agreement with archaeological dates within a standard deviation of 27%. Such error can be accepted in porcelain dating

Preparation of archaeological samples for its dating by thermoluminescence

International Nuclear Information System (INIS)

Mejia F, D.

2000-01-01

The present work shows the results of the preparation of archaeological samples for their dating by thermoluminescence (Tl) using the Fine grain technique established by Zimmerman but with the varying of such preparation was realized in normal daylight conditions, only the taking of the Tl readings were realized in dark room and red light. In the chapter 1 basic concepts are described about: matter constitution, radioactivity, units and radiation magnitudes, and thermoluminescence. In the chapter 2 some theoretical aspects on dating are showed. It is described how realizing the samples collection, the fine grain method, the determination of the accumulated dose through the years or paleodoses (P=Q+I) by mean of the increasing to obtain the dose equivalent dose (Q) and the signal regeneration method to obtain the correction factor by supra linearity (1), the determination of the annual dose rate to apply the age equation and the evaluation of the age uncertainty with the error limits. The development of experimental part with samples from the archaeological site named Edzna in Campeche, Mexico is described in the chapter 3. The results are presented in the chapter 4. It was obtained an age for the sample named CH7 it was obtained an age of 389 ± years. In conclusion the preparation of the archaeological samples for their dating by Tl in the conditions before mentioned is reliable, but they must be realized more studies with samples of well known age, preparing them in normal daylight conditions and simultaneously in dark room with red light. In order to observe how respond the minerals present in the sample at different dose rapidity, the same samples must be radiated with radiation sources with different dose rate. (Author)

Solid track detectors used for the dating by thermoluminescence

International Nuclear Information System (INIS)

Miallier, D.

1982-10-01

A new α counting technic is presented in the field of the thermoluminescent dating method. It is based upon α particles registration in plastic detectors LR-115 Kodak in close contact with archeological or geological samples. The control of etching and counting conditions allowed to improve the usual precision of the detector. The following data are collected: α and β dose rates deposited by Uranium and Thorium series; an approximative value for the Uranium-Thorium ratio; spatial distribution of α emittors within samples and the radon escape rated. This method was used simultaneously with the ''quartz inclusion technic'' to date several samples: volcanic lava flows from the ''Chaine des Puys'' (Center France); the Butte de Clermont basaltic maar; a neolithic ''cardial'' pot-sherd and bricks from a minoaan palace (Mallia, Crete) [fr

Thermoluminescence dating of Brazilian indigenous ceramics

International Nuclear Information System (INIS)

Farias, T. M. B.; Gennari, R. F.; Etchevarne, C.; Watanabe, S.

2009-01-01

Two indigenous ceramics fragments, one from Lagoa Queimada (LQ) and another from Barra dos Negros (BN), both sites located on Bahia state (Brazil), were dated by thermoluminescence (TL) method. Each fragment was physically prepared and divided into two fractions, one was used for TL measurement and the other for annual dose determination. The TL fraction was chemically treated, divided in sub samples and irradiated with several doses. The plot extrapolation from TL intensities as function of radiation dose enabled the determination of the accumulated dose (D ac ), 3.99 Gy and 1.88 Gy for LQ and BN, respectively. The annual dose was obtained through the uranium, thorium and potassium determination by ICP-MS. The annual doses (D an) obtained were 2.86 and 2.26 mGy/year. The estimated ages were ∼1375 and 709 y for BN and LQ ceramics, respectively. The ages agreed with the archaeologists' estimation for the Aratu and Tupi tradition periods, respectively. (authors)

Dating the Morasko meteorite fall by natural thermoluminescence of the fusion crust

Directory of Open Access Journals (Sweden)

Fedorowicz Stanisław

2016-09-01

Full Text Available The date of fall of the Morasko iron meteorite was determined by means of thermoluminescence measurements of the fusion crust and related local materials. Three small pieces, commonly referred to as ‘shrapnel’, were used. The results obtained are 4.5-5.0 ka, which is in good agreement with previous estimates of 4-6 ka on the basis of radiometric, do-simetric and palynological methods.

The problem of low thermoluminescence age estimates in geological dating

International Nuclear Information System (INIS)

Nambi, K.S.V.

1983-01-01

A systematic underestimate of the geological age by the TL technique has been observed in a variety of CaCO 3 samples of Quaternary to Precambrian ages. It is concluded that the TL dating clock in the CaCO 3 lattice stops when the alpha palaeodose =alpha (rad a -1 )x geological age (a) reaches about 100,000 rad. At this dose the natural thermoluminescence reaches perhaps a dynamic equilibrium level determined solely by the alpha activity of the sample. There are indications that the limiting alpha palaeodose beyond which TL dating is invalid is more or less the same for CaSO 4 and silicate samples, and it is convenient to note a limiting value of 3 million for the product of alpha activity (cph from 13.86 cm 2 ) and geological age (a). (author)

Thermoluminescence dates for the Lake Mungo aboriginal fireplaces and the implications for radiocarbon dating

International Nuclear Information System (INIS)

Bell, W.T.

1991-01-01

During the Quaternary period in Australia large areas of western New South Wales and northern Victoria were covered by hundreds of lakes, both large and small. Nearly all are dry today but some may still be recognized by the long low dunes that follow the eastern shorelines. Many traces of early human occupation have been found along the shorelines of nearly all the major lakes and some of the best exposures have occurred on the lunette along the eastern shore of Lake Mungo. This lunette, has suffered massive erosion in recent times and this has uncovered the sites of many ancient fireplaces. Charcoal from some of these fireplaces has been dated by Barbetti and Polach (1973) using the radiocarbon method and the ages place the lakeside dwellers at Mungo in an area of Australian prehistory around 30 000 years ago. The baked sediment from below the fireplaces appears to have been heated to a temperature in excess of 400 o C according to archaeomagnetic studies carried out by Barbetti (1973) and this indicated that the fireplaces might lend themselves to the technique of thermoluminescence (TL) dating. The results of the TL dating programme are described elsewhere. (author)

Thermoluminescence dates for the Lake Mungo aboriginal fireplaces and the implications for radiocarbon dating

Energy Technology Data Exchange (ETDEWEB)

Bell, W T [Australian National Univ., Canberra (Australia)

1991-02-01

During the Quaternary period in Australia large areas of western New South Wales and northern Victoria were covered by hundreds of lakes, both large and small. Nearly all are dry today but some may still be recognized by the long low dunes that follow the eastern shorelines. Many traces of early human occupation have been found along the shorelines of nearly all the major lakes and some of the best exposures have occurred on the lunette along the eastern shore of Lake Mungo. This lunette, has suffered massive erosion in recent times and this has uncovered the sites of many ancient fireplaces. Charcoal from some of these fireplaces has been dated by Barbetti and Polach (1973) using the radiocarbon method and the ages place the lakeside dwellers at Mungo in an area of Australian prehistory around 30 000 years ago. The baked sediment from below the fireplaces appears to have been heated to a temperature in excess of 400{sup o}C according to archaeomagnetic studies carried out by Barbetti (1973) and this indicated that the fireplaces might lend themselves to the technique of thermoluminescence (TL) dating. The results of the TL dating programme are described elsewhere. (author).

Thermoluminescence dating of Rio Claro and Piracununga formations

International Nuclear Information System (INIS)

Ferreira, Sandra Regina; Chang, Maria Rita Caetano

2008-01-01

The Rio Claro and Piracununga formations cover extensive areas of the Paulista Peripheral Depression, dominantly in the region of Rio Claro and Piracununga cities. These units lie over the Corumbatai and Piramboia formations, exhibiting discordant contacts. The Rio Claro and Piracununga formations are composed of fine to medium sand facies, showing local cross-stratifications and parallel beddings with thin interbeddings of mud and gravel. These sands were dated by the Thermoluminescence Method, which indicated they were from the Pleistocene age. The oldest age (745,000 years BP) was found in deposits of the Rio Claro Formation; the other ages varied from 400,000 years BP to 145,000 years BP, for both formations. The youngest age (15,000 years BP - close to Pleistocene/ Holocene limit) was found in colluvial deposits, which rest on the Piracununga Formation. (author)

Provenance Study of Archaeological Ceramics from Syria Using XRF Multivariate Statistical Analysis and Thermoluminescence Dating

OpenAIRE

Bakraji, Elias Hanna; Abboud, Rana; Issa, Haissm

2014-01-01

Thermoluminescence (TL) dating and multivariate statistical methods based on radioisotope X-ray fluorescence analysis have been utilized to date and classify Syrian archaeological ceramics fragment from Tel Jamous site. 54 samples were analyzed by radioisotope X-ray fluorescence; 51 of them come from Tel Jamous archaeological site in Sahel Akkar region, Syria, which fairly represent ceramics belonging to the Middle Bronze Age (2150 to 1600 B.C.) and the remaining three samples come from Mar-T...

Thermoluminescence characteristics and dating of some egyptian rocks using gamma-rays

International Nuclear Information System (INIS)

Sharaf, M.M.; Mohamed, R.I.; Rabie, N.

1994-01-01

The thermoluminescence (T L) characteristics and dating of some natural samples which were collected from different areas in the eastern desert of egypt have been studied. The T L- glow curves of all natural samples show three peaks, shallow peak, dosimetric peak and dating peak. T L response to gamma rays for the samples under examination shows a linear response from 4.5 Gy up to 7.5 kGy followed by saturation. Ages of these geological rocks from the selected areas A (hutait), B(Urga), C(Tendba), D(Sebaya) and E(Atad) in the Eastern desert were found to be 4 X 108, 1.5 X 109, 0.5 X 108, 2.5 X 107 and 3 X 107 years, respectively. It can be concluded that these geological rocks belong to the precambrian period of the history. 4 figs., 4 tabs

Thermoluminescence characteristics and dating of some egyptian rocks using gamma-rays

Energy Technology Data Exchange (ETDEWEB)

Sharaf, M M; Mohamed, R I; Rabie, N [Acodemy of Scientific Research and Technology, National Institute for Standards, Pyramids, Giza (Egypt)

1994-12-31

The thermoluminescence (T L) characteristics and dating of some natural samples which were collected from different areas in the eastern desert of egypt have been studied. The T L- glow curves of all natural samples show three peaks, shallow peak, dosimetric peak and dating peak. T L response to gamma rays for the samples under examination shows a linear response from 4.5 Gy up to 7.5 kGy followed by saturation. Ages of these geological rocks from the selected areas A (hutait), B(Urga), C(Tendba), D(Sebaya) and E(Atad) in the Eastern desert were found to be 4 X 108, 1.5 X 109, 0.5 X 108, 2.5 X 107 and 3 X 107 years, respectively. It can be concluded that these geological rocks belong to the precambrian period of the history. 4 figs., 4 tabs.

Tests of thermoluminescence dating of the Menez-Dregan site (Brittany, France)

International Nuclear Information System (INIS)

Sanzelle, S.; Montret, M.; Pilleyre, T.; Miallier, D.; Fain, J.

1997-01-01

This paper reports on tests of thermoluminescence datings of quartz samples of the Paleolithic site of Menez Dregan in Brittany (France). The archaeological site comprises 3 fossil beaches in rocky shelters. The layer under study is on the top of the most recent fossil beach and contains built fireplaces associated with a Colombanian industry. Samples have received a dose comprised between natural irradiation and 6.8 kGy to 10.5 kGy additional doses. Paleo-doses obtained with different methods (between 1 to 3.5 kGy) are not compatible with each others and do not allow the determination of a precise age. (J.S.)

Thermoluminescence dating of burnt cherts from the Alice Boer site (Brazil)

International Nuclear Information System (INIS)

Beltrao, M. da C.M.C.; Enriquez, C.R.; Danon, J.; Zuleta, E.

1983-01-01

More than 40 culturally burnt cherts from the Alice Boer site near Rio Claro, Sao Paulo State, have been studied by thermoluminescence (TL). Nine of these were found to be sufficiently heated by early man to reset the TL clock to zero and thereby be suitable for TL dating. These cherts define, for the upper half of the uppermost cultural layer (layer III), a time scale for the presence of man from 2,220 to 11,000 years. This time range is in essential agreement with the geological-paleoclimatological age estimate for the end of deposition of this layer, as well as with radiocarbon dates. In particular, it lends support to a radiocarbon age of 14,000 BP for a deeper level. The overall geochronologic results are not in contradiction with earlier statements that the deepest cultural layer (layer V) at Alice Boer might have been deposited at least 20,000 years ago. (Author) [pt

Dating implications from solar bleaching of thermoluminescence of ancient marble

International Nuclear Information System (INIS)

Liritzis, I.; Galloway, R.B.

1999-01-01

Measurements of Thermoluminescence (TL) from Greek marble quarried at Paros, Naxos, Pendeli, Hymitos, Thassos, which have been known since ancient time are presented. The results concern i) the solar bleaching of TL, ii) the solar transmission through marble thicknesses up to 16 mm, and iii) the implications for potential dating of ancient carbed marble monuments/objects. The bleaching rate for marbles is very fast during the first hour of exposure. The solar penetration is at least 35 mm for long exposures. Beyond the 2 mm marble slab for exposure times 90-120 hours of sunshine, the residual bleached TL level is not reached. The bleached TL reaches a plateau which serves as the 'zero time' upon which the archaeological TL dose subsequently builds up and gives the age of a marble monument. (author)

Rethinking About Chronology Of Chichen Itza: By Thermoluminescence Dating Of Volcanic Glass.

Science.gov (United States)

Chung, H.; Gonzalez, P.; Ramirez, A.; Schaaf, P.; Lee, I.

One of the most frequently recurring questions in archaeology concerns the age of the studied objects. To date, determining the chronology of the Puuc and Chichen Slate pottery of Chchen Itza, based on the stylistic change in the pottery, has been problematic. The Thermoluminescence method of dating pottery was applied to samples of Chichen Itza, Yucatan, Mexico, which contain volcanic glass as temper. They were analyzed using the fine grain technique. The radisotopes that contribute to the accumulate annual dose in ceramic samples (40K, 238U, 232Th) were determined by means of Energy Dispersive X-ray Spectroscopy and Neutron Activation Analysis technique, while the artificial irradiation of the samples was carried out using 90Sr source beta radiation. We obtained results indicating the following dates; 875 ± 88; 1055 ± 85; 1063 ± 47, 1154 ± 76; 1110 ± 53, 1132 ± 69, 1221 ± 30, 1532 ± 26. The results demonstrate a chronological order of dates. Most results are in accordance with the established dates of Chichen Itza. However, Puuc and Chichen Slate did not show differences of 200 years as previously proposed, and there is evidence of an earlier period than those two pottery periods. This necessitates a reconsideration of the chronology of Chichen Itza.

Irradiation of dates: insect disinfestation, microbial and chemical assessments, and use of thermoluminescence technique

Energy Technology Data Exchange (ETDEWEB)

Al-Kahtani, Hassan A.; Abu-Tarboush, Hamza M.; Ahmed, Mohamed A.; Bajaber, Adnan S. [Food Science and Nutrition Department, College of Agriculture, King Saud University, Riyadh (Saudi Arabia); Al-Dryhim, Yousif N.; Adam, El-Shami E. [Plant Protection Department, College of Agriculture, King Saud University, Riyadh (Saudi Arabia); El-Mojaddidi, Mohamed A. [King Faisal Specialist Hospital and Research Center, Riyadh (Saudi Arabia)

1998-08-01

Irradiation of dates (Khalas variety) at 0.9 kGy was sufficient to eliminate single insect infestation (Oryzaephilus surinamensis) and mixed infestation (O. surinamensis and Tribolium castaneum), whereas 0.3 kGy was effective only in controlling single infestation. Sensory properties were not affected but irradiation contributed to some reduction in microbial counts immediately after irradiation and counts remained low till the end of 6 months storage period. All sugars were significantly reduced immediately after irradiation but they increased gradually with increasing storage time. Thermoluminescence (TL) technique was useful in discriminating between irradiated and unirradiated dates during the entire storage period but was less sensitive as far as the dose estimation is concerned.

Irradiation of dates: insect disinfestation, microbial and chemical assessments, and use of thermoluminescence technique

International Nuclear Information System (INIS)

Al-Kahtani, Hassan A.; Abu-Tarboush, Hamza M.; Ahmed, Mohamed A.; Bajaber, Adnan S.; Al-Dryhim, Yousif N.; Adam, El-Shami E.; El-Mojaddidi, Mohamed A.

1998-01-01

Irradiation of dates (Khalas variety) at 0.9 kGy was sufficient to eliminate single insect infestation (Oryzaephilus surinamensis) and mixed infestation (O. surinamensis and Tribolium castaneum), whereas 0.3 kGy was effective only in controlling single infestation. Sensory properties were not affected but irradiation contributed to some reduction in microbial counts immediately after irradiation and counts remained low till the end of 6 months storage period. All sugars were significantly reduced immediately after irradiation but they increased gradually with increasing storage time. Thermoluminescence (TL) technique was useful in discriminating between irradiated and unirradiated dates during the entire storage period but was less sensitive as far as the dose estimation is concerned

Thermoluminescence dating of a tephra level from Baume Moula-Guercy (Soyons, Ardeche, France)

International Nuclear Information System (INIS)

Sanzelle, S.; Montret, M.; Pilleyre, T.; Miallier, D.; Fain, J.

1998-01-01

The Baume Moula-Guercy site (Ardeche, France) is a cave that overhangs the Rhone river valley at a hundred meters height. Since its discovery, it has been assimilated as a shelter with an upper part opened towards the sky. It contains an upper Pleistocene sequence inside which a 2-3 cm localized volcanic layer has been identified. This layer is attributed to an important phreato-magmatic emission from the Vivarais region located at about 50 km SW of the site. The filling of this cave contains neanderthalian remains in a lower level and middle Paleolithic lithic industries in a upper level. Thus, the dating of the tephra level would be of great archaeological importance as it could be used as a chronostratigraphic reference. An estimation of the age obtained by thermoluminescence dating has been requested. This report presents the dating procedure performed on quartz samples extracted from the tephra level and the estimation of the site dosimetry. (J.S.)

Dating of the archaeological site 'El Tigre' by the thermoluminescent method; Fechamiento del sitio arqueologico 'El Tigre' por el metodo de termoluminiscencia

Energy Technology Data Exchange (ETDEWEB)

Portilla, R. De la [ENAH, Periferico Sur y Zapote, 14030 Mexico D.F. (Mexico); Gonzalez, P.R.; Mendoza, D. [ININ, 52750 La Marquesa, Ocoyoacac, Estado de Mexico (Mexico); Vargas, E. [Instituto de Investigaciones Antropologicas, UNAM, 04510 Mexico D.F. (Mexico); Ramirez, A. [Instituto de Geofisica, UNAM, 04510 Mexico D.F. (Mexico)

2007-07-01

Full text: The dating of pre hispanic pottery, is supported by techniques such as stratigraphy, typology, in physical and chemical procedures, as the analysis of {sup 14}C and the thermoluminescence (TL). The last one permits us obtain absolute dating of archaeological pottery with an acceptable precision. In this work we apply the applied the thermoluminescent technique to verify the age of the Pre-Classic and Classic Terminal periods proposed for the archaeological site 'El Tigre', Campeche. The samples were obtained during a work period and the radiation of the ground of background (emitted by the ground), as well as the contribution of the cosmic radiation was measured with thermoluminescent dosemeters of LiF: Mg,Cu,P + PTFE, put in the sample zone. The preliminary results indicate that not all the analyzed samples can be dated. The viability of the dating of the samples is discussed based on the fact and function of the presence of certain crystalline phases such as calcite and quartz. The discussion is complemented emphsizing the importance of handling the conditions of handling of samples. (Author)

Middle Pleistocene volcanic activity dated by red thermoluminescence (RTL) - a case study from Lanzarote (Canary Islands)

Science.gov (United States)

von Suchodoletz, H.; Blanchard, H.; Rittner, S.; Radtke, U.; Fuchs, M.; Dietze, M.; Zöller, L.

2009-04-01

On Lanzarote (Canary Islands) soils were baked by Quaternary lava flows. This offers the possibility to date phases of eruptive activity by red thermoluminescence (RTL). We dated soil material baked by two different lava flows originating from the "Las Calderetas de Guatiza" volcanic chain in the northeast of the island by RTL. Furthermore, three samples of Helicidae-mollusk shells overlying one of the lava flows (site Mála) were dated using electron spin resonance (ESR). RTL datings were carried out using quartz grains 63-200 µm from baked material that were originally brought by eolian transport from the nearby Saharan desert. It appears that in spite of a baking temperature Lanzarote by RTL thus offers the possibility to further investigate the yet fragmentary Middle and Late Quaternary eruptive history of these islands.

Thermoluminescence as a dating method applied to the Morocco Neolithic

International Nuclear Information System (INIS)

Ousmoi, M.

1989-09-01

Thermoluminescence is an absolute dating method which is well adapted to the study of burnt clays and so of the prehistoric ceramics belonging to the Neolithic period. The purpose of this study is to establish a first absolute chronology of the septentrional morocco Neolithic between 3000 and 7000 years before us and some improvements of the TL dating. The first part of the thesis contains some hypothesis about the morocco Neolithic and some problems to solve. Then we study the TL dating method along with new process to ameliorate the quality of the results like the shift of quartz TL peaks or the crushing of samples. The methods which were employed using 24 samples belonging to various civilisations are: the quartz inclusion method and the fine grain technique. For the dosimetry, several methods were used: determination of the K 2 O contents, alpha counting, site dosimetry using TL dosimeters and a scintillation counter. The results which were found bring some interesting answers to the archeologic question and ameliorate the chronologic schema of the Northern morocco Neolithic: development of the old cardial Neolithic in the North, and perhaps in the center of Morocco (the region of Rabat), between 5500 and 7000 before us. Development of the recent middle Neolithic around 4000-5000 before us, with a protocampaniforme (Skhirat), little older than the campaniforme recognized in the south of Spain. Development of the bronze age around 2000-4000 before us [fr

Dating of Chichen Itza ceramics by the method of thermoluminescence

International Nuclear Information System (INIS)

Gonzalez M, P.R.; Mendoza A, D.; Cuapio O, L.A.; Ramirez L, A.; Schaaf, P.; Chung, H.

2005-01-01

In this work we present some results about thermoluminescent dating of some archaeological ceramic samples belonging to Chichen Itza, Yucatan, Mexico: CH11, CH13, CH14 and CH15. The analysis was realized using the fine grained mode in a Daybreak model 1100 reader Tl System. The radioisotopes that contribute in the accumulate annual dose in ceramic samples ( 40 K, 238 U, 232 Th) were determined by means of techniques such as Energy Dispersive X-ray Spectroscopy (EDS) and Neutron Activation Analysis (NAA), while the artificial irradiation of samples was carried out with a 90 Sr source beta radiation. The resulting mean CH11 ceramic sample was 934 ±45 years old, CH13 was 465 ± 26, CH14 was 888 ± 34 and CH15 was 867 ± 42. These results are in agreement with results obtained through other methods. (Author)

Thermoluminescence dating analysis at the site of an ancient brick structure at Pengkalan Bujang, Malaysia

International Nuclear Information System (INIS)

Sabtu, Siti Norbaini; Mahat, Rosli Hj; Amin, Yusoff Mohd; Price, David M; Bradley, D.A.; Maah, Mohd Jamil

2015-01-01

Bujang Valley is a well-known historical complex found in the north-west of peninsular Malaysia; more than 50 ancient monuments and hundreds of artefacts have been discovered throughout the area. The discovery of these suggests Bujang Valley to have been an important South East Asian trading centre over the period from the 10th to 14th centuries. Present work concerns thermoluminescence (TL) dating analysis of shards collected from a historic monument located at Pengkalan Bujang in Bujang Valley. All the shards were prepared using the fine grain technique and the additive dose method was applied in determining the paleodose of each shard. The annual dose rate was obtained by measuring the concentration of naturally occurring radionuclides (U, Th and K) in the samples and their surroundings. The TL ages of the shards were found to range between 330±21 years and 920±69 years, indicative of the last firing of the bricks and tiles from which the shards originated, some dating back to the period during which the historical complex remained active. - Highlights: • Thermoluminescence analysis of shards sample from Pengkalan Bujang. • Fine grain technique and additive dose method were applied to determine paleodose. • Measuring concentration of U, Th and K in the samples and their surroundings. • TL ages obtained indicative of the last firing of the shards.

Thermoluminescence dating of CaCO3 nodules from buried soil of the lower Narmada Valley

International Nuclear Information System (INIS)

Nambi, K.S.V.; Hegde, K.T.M.

1982-01-01

Calcium carbonate nodules excavated at an archaeological site in Lower Narmada River Valley have been dated by the thermoluminescence technique. Tiny, sensitive TL dosimeters using natural CaF 2 as the phosphor, were employed to evaluate the natural radiation levels at the excavation site over a period of a year. The estimated TL age value is 22890 yrs B.P. with an uncertainty of about +/- 8%. The reported 14 C age of these nodules is 22452 +/- 550 years B.P

Some results about the dating of pre hispanic mexican ceramics by the thermoluminescence method

International Nuclear Information System (INIS)

Gonzalez M, P.; Mendoza A, D.; Ramirez L, A.; Schaaf, P.

2004-01-01

One of the most frequently recurring questions in Archaeometry concerns the age of the studied objects. The some first dating methods were based in historical narrations, style of buildings manufacture techniques. However, has been observed that as consequence the continuous irradiation from naturally occurring radioisotopes and from cosmic rays some materials, such as archaeological ceramic, accumulate certain quantity of energy. These types of material can, in principle, be dated through the analysis of these accumulate energy. In that case, ceramic dating can be realized by thermoluminescence (TL) dating. In this work, results obtained by our research group about TL dating of ceramic belonging to several archaeological zones like to Edzna (Campeche), Calixtlahuaca and Teotenango (Mexico State) and Hervideros (Durango) are presented. The analysis was realized using the fine grained mode in a Daybreak model 1100 reader TL system. The radioisotopes that contribute in the accumulate annual dose in ceramic samples ( 40 K, 238 U, 232 Th) were determined by means of techniques such as Energy Dispersive X-ray Spectroscopy (EDS) and Neutron Activation Analysis (AAN). Our results are agree with results obtained through other methods. (Author) 7 refs., 2 tabs., 5 figs

Archaeological and Geological dating by means of thermoluminescence

International Nuclear Information System (INIS)

Gonzalez M, P.R.

1999-01-01

In this thesis an specific method for dating local archaeological and geological samples based on the phenomenon of thermoluminescence (TL) using the fine grain and quartz inclusion techniques is developed. Taking into account that this work is interesting for professionals working in the fields of Physics, Chemistry, Archaeology, Anthropology and related sciences, some basic concepts are described to have a better comprehension. Chapter 1 describes the concept of radioactivity, remarking the importance of the different decay types as well as the main radioactive series and the energy liberated in the process. The causes of radioactive desequilibrium are also considered in the case for radon. Another important aspect taken into account in this chapter is the radioisotope production and its relationship with the neutron activation analysis used for the determination of the Uranium and Thorium concentrations in the samples. The TL phenomenon is described in Chapter 2, emphasizing the importance of the process of thermally stimulated luminescence best known as TL and its application for dating minerals of different origin. Chapter 3 shows some important antecedents remarking some aspects of the techniques commonly used for dating purposes. Chapter 4 shows the different methods used for the sample preparation. The techniques used for the 40 K, 238 U and 232 Th determination as well as for the cosmic radiation measurement using locally made TLD are also described. The methods used for the determination of the paleodosis as a function of the TL intensity of each sample are described: special emphasis is taken on the moisture effects as well as in the error limits in the age estimation. Results and conclusions of this study are presented in Chapter 5. These results gave an age of 980 ± 90 years for the Edzna ceramic and 1520 ± 90 years for the Calixtlahuaca ceramics. The age of the Teotihuacan ceramics was not estimated due to the lack of a stable region of the traps

Thermoluminescence dating of soils in a semi-arid environment, Yucca Mountain area, Southern Nevada, USA

International Nuclear Information System (INIS)

Mahan, S.A.; Paces, J.B.; Peterman, Z.E.

1995-01-01

Yucca Mountain, Nevada, is currently being investigated as a potential nuclear waste repository. Because radionuclides must be isolated over a ten to several hundred thousand year time span, an assessment of the performance depends in part on accurate reconstruction of the Quaternary geologic and hydrologic history of the mountain. Reliable geochronology in an oxidizing environment dominated by coarse-grained, clastic surficial deposits has become a central issue for several studies including paleoseismic reconstruction, determination of rates of erosion and deposition, and the history of regional water-table fluctuations documented by ground-water discharge deposits. Thermoluminescence (TL) dating of polymineralic silt fractions in a variety of surface deposits has become an important component of the Quaternary dating strategy, along with uranium-series disequilibrium dating of secondary carbonate and opaline silica, and to a lesser extent, radiocarbon dating of carbonate components. Although the complex mineralogy of these materials contributes to greater amounts of scatter in their TL response relative to typical quartzofeldspathic loess and dune deposits, the derived ages are reproducible, consistent with internal stratigraphy, and generally concordant with other available geochronology

Thermoluminescence kinetics in materials exposed to the low doses applicable to dating and dosimetry

International Nuclear Information System (INIS)

Levy, P.W.

1984-11-01

Thermoluminescence (TL) kinetics have been investigated for low dose situations applicable to dating, dosimetry, and recent geological deposits. Studied were the general one-trap kinetic equation, which reduces to the well known 1st and 2nd order kinetic equations when various assumptions apply, and the interactive kinetic equations, which describes TL in materials exhibiting more than one glow peak. In materials with one glow peak area varies linearly with dose; however, peak height is not linear with dose unless the TL obeys 1st order kinetics at all doses. In materials with two or more glow peaks neither peak height nor peak area varies linearly with dose, except in special situations. In fact, many peak height vs dose curves will be supralinear with the initial low-slope region occurring at relatively low doses. These considerations indicate: (1) Dating and dosimetry technique based on assumed linear peak height vs dose curves will usually underestimate the accumulated dose. (2) Dating techniques can be improved and/or made more reliable by determining the TL kinetics of the glow peaks measured

Study of Syrian archaeological pottery by the combined application of thermoluminescence (TL) dating, X-ray fluorescence analysis and statistical multivariate analysis

International Nuclear Information System (INIS)

Bakraji, E.H.

2012-01-01

X-ray fluorescence method and the technique of thermoluminescence (TL) dating have been utilized for the study of archaeological pottery fragment samples, fairly representative of Romanian period between 1 st century B.C. and 4th century A.D, from Judaidet Yabous site, which is located north-west of Damascus city, Syria. Four samples were chosen randomly among the forty six samples for dating using thermoluminescence technique and the results were in good agreement with the date assigned by archaeologists. The samples were irradiated for 1000 s live time twice, first using a Mo X-ray Tube and second using a 109 Cd radioactive source. Fifteen elements (K, Ca, Ti, Mn, Fe, Ni, Cu, Zn, Ga, Rb, Sr, Y, Zr, Nb, and Pb) were determined. The elemental concentrations have been processed using two multivariate statistical methods. The purpose of the study was to characterize by means of elements contents the pottery paste from Judaidet Yabous archaeological site and providing new data to the Syrian databases for future studies. From an archaeological point of view the results indicated that most of the potteries, were locally produced. (author)

Application of radioisotope XRF and thermoluminescence (TL) dating in investigation of pottery from Tell AL-Kasra archaeological site, Syria

International Nuclear Information System (INIS)

Abboud, R.; Issa, H.; Abed-Allah, Y.D.; Bakraji, E.H.

2015-01-01

Statistical analysis based on chemical composition, using radioisotope X-ray fluorescence, have been applied on 39 ancient pottery fragments coming from the excavation at Tell Al-Kasra archaeological site, Syria. Three groups were defined by applying Cluster and Factor analysis statistical methods. Thermoluminescence (TL) dating was investigated on three sherds taken from the bathroom (hammam) on the site. Multiple aliquot additive dose (MAAD) was used to estimate the paleodose value, and the gamma spectrometry was used to estimate the dose rate. The average age was found to be 715±36 year. - Highlights: • Providing new additional data of Syrian archaeological ceramics. • This work investigates both elemental content and dating of Syrian ceramics. • Elemental analysis and dating were performed by XRF and TL dating respectively.

Dating of a representative pottery sample from the basin of Sayula, Jalisco in Mexico using the thermoluminescence method

Energy Technology Data Exchange (ETDEWEB)

Mercado U, H. [CINVESTAV, Unidad Monterrey, Nuevo Leon (Mexico); Schaaf, P.; Ramirez, A. [Instituto de Geofisica, UNAM, 04510 Mexico D.F. (Mexico); Gonzalez, P.R. [ININ, 52750 Ocoyoacac, Estado de Mexico (Mexico); Brunet, J. [CUCSH, Universidad de Guadalajara, Jalisco (Mexico)

2006-07-01

In this work is presented a study of dating of the representative pottery sample from the west of Mexico, in a predominantly saline region. The study is carried out with the thermoluminescence method and the fine grain technique. The archaeological region was begun to study from 1990. This work also presents an historical and geographical context of the region and its relevance in the western culture of Mexico. (Author)

Dating of a representative pottery sample from the basin of Sayula, Jalisco in Mexico using the thermoluminescence method

International Nuclear Information System (INIS)

Mercado U, H.; Schaaf, P.; Ramirez, A.; Gonzalez, P.R.; Brunet, J.

2006-01-01

In this work is presented a study of dating of the representative pottery sample from the west of Mexico, in a predominantly saline region. The study is carried out with the thermoluminescence method and the fine grain technique. The archaeological region was begun to study from 1990. This work also presents an historical and geographical context of the region and its relevance in the western culture of Mexico. (Author)

Dating by thermoluminescence of some costal sand deposits of last climatic cycle, from the northeastern region of Rio Grande do Sul State, Brazil

International Nuclear Information System (INIS)

Poupeau, G.; Rivera, A.

1988-01-01

Six coastal quartz sand deposits from the northeastern region of the Rio Grande do Sul State (Brazil), with reasonnably well known ages, from ∼ 1700 yr to ∼ 120.000 yr, were dated by thermoluminescence. (M.W.O.) [pt

Equipment for observing thermoluminescence

International Nuclear Information System (INIS)

Sette Camara, Alexandre; Cogneau, Michel; Ristori, Christian; Vargas, Jose Israel

1971-06-01

A detailed description is given of an apparatus for investigating thermoluminescence properties. Chopping of the emitted light and subsequent amplification of the electric signal derived led to high stability and sensitivity [fr

Dating of pre hispanic ceramics from the archaeological zone of Zoque by thermoluminescence method; Datacion de ceramica prehispanica de la zona arqueologica Zoque por el metodo de termoluminiscencia (TL)

Energy Technology Data Exchange (ETDEWEB)

Valdes, J.V. [UAEM, Facultad de Quimica, 50120 Toluca, Estado de Mexico (Mexico); Gonzalez, P.R.; Mendoza, D.; Tenorio, D. [ININ, 52045 Ocoyoacac, Estado de Mexico (Mexico); Terreros, E. [Museo Templo Mayor, INAH, Seminario No. 8, Col. Centro, 06060 Mexico D.F. (Mexico); Ramirez, A. [Instituto de Geofisica, UNAM, 04510 Mexico D.F. (Mexico)

2007-07-01

Full text: The dating of pre hispanic ceramics resides permitting us to located them in a certain period of the history; allows us to verify it origin. The thermoluminescence is a technique that permits us to estimate the absolute age of the archaeological samples. The present work is directed in determining the age by the method of thermoluminescence of archaeological samples of the grotto of Concubac, located in the Serrana Region of Tabasco. To determine the mineralogical composition of the samples, analysis of diffraction of X rays and Energy Dispersive X-ray Spectroscopy (EDS) have been conducted. The radiation emitted by the ground where the samples were buried and the contribution of the cosmic radiation was measured with thermoluminescent dosimeters of LiF:Mg,Cu,P+PTFE. The feasibility of dating of the studied samples is broadly disputed in function of the contents of minerals, as well as the procedure and management of the sample. (Author)

The combined application of PIXE analysis and thermoluminescence (TL) dating for elucidating the origin of iron manufacturing in Japan

International Nuclear Information System (INIS)

Hagihara, N.; Miono, S.; Chengzhi, Z.; Nakayama, Y.; Hanamoto, K.; Manabe, S.

1999-01-01

For elucidating the origin of iron manufacturing in Japan, the usefulness of PIXE analysis was reconfirmed and a new technique of thermoluminescence (TL) dating was applied. Through reproducing experiments of iron manufacturing and forging, PIXE analysis was tested for classifying the iron slag produced from these two different process. The TL dating method was improved for experiments with the iron manufacturing furnace, burnt at high temperature (about 1300 K) and irradiated with relatively low dose. Utilizing PIXE analysis, the iron manufacturing furnace can be distinguished from the older forging furnace used for the imported iron plate. Adopting TL dating, the oldest iron manufacturing furnace can be found out. Some ancient samples in Japan were used as a test of this combined application, and the results were positive, thus proving the suitability of the method

Thermoluminescence of zircon: a kinetic model

CERN Document Server

Turkin, A A; Vainshtein, D I; Hartog, H W D

2003-01-01

The mineral zircon, ZrSiO sub 4 , belongs to a class of promising materials for geochronometry by means of thermoluminescence (TL) dating. The development of a reliable and reproducible method for TL dating with zircon requires detailed knowledge of the processes taking place during exposure to ionizing radiation, long-term storage, annealing at moderate temperatures and heating at a constant rate (TL measurements). To understand these processes one needs a kinetic model of TL. This paper is devoted to the construction of such a model. The goal is to study the qualitative behaviour of the system and to determine the parameters and processes controlling TL phenomena of zircon. The model considers the following processes: (i) Filling of electron and hole traps at the excitation stage as a function of the dose rate and the dose for both (low dose rate) natural and (high dose rate) laboratory irradiation. (ii) Time dependence of TL fading in samples irradiated under laboratory conditions. (iii) Short time anneali...

Application of thermoluminescence dating on pressed crystalline samples to determine the geological age at some areas in Eastern South, Vietnam

International Nuclear Information System (INIS)

Do Duy Khiem; Luu Anh Tuyen; Phan Trong Phuc; Nguyen Thi Ngoc Hue; Pham Thi Hue; La Ly Nguyen; Ha Quang Hai

2016-01-01

The terrestrial part of eastern margin of the Mekong Basin is formed by outcrop of the pre-Holocen Cenozoic sequence. Almost previous studies concerned in using relative methods in geologic dating at the Mekong Basin, therefore, the ages of its stratigraphy are still unclear. The thermoluminescence (TL) dating was considered as one of the precise methods in geologic dating. In our study, we used TL dating for some areas at Eastern South, Vietnam including Ba Mieu Formation and the Thu Duc Formation at some areas in Dong Nai province and Ho Chi Minh City. This work has been the first application of TL for in geologic dating by a domestic laboratory. Experimental measurements of TL were performed using pressed crystalline quartz specimens from sediment samples. The results show that the Ba Mieu Formation was deposited about 238±22 ka and the Thu Duc Formation was deposited about 199±21 ka. (author)

Radiocarbon and thermoluminescence dating of quaternary sediments in Deception Bay, southeast Queensland: some problems encountered

International Nuclear Information System (INIS)

Cotter, M.M.

1999-01-01

Full text: Radiocarbon and Thermoluminescence dating of sediment facies were utilised to develop a chronometric framework for the quaternary coastal evolution of Deception Bay southeast Queensland (Cotter 1996). This chronometric framework was developed in the context of a broader geoarchaeological and palaeogeographical investigation of the indigenous cultural landscape of the area. The TL analysis confirmed the presence of previously undated Pleistocene sands within the study area. However in the course of dating one sedimentary sequence, conventional radiocarbon analysis of Notispisula sheldls produced an age of 5190± 90 years BP (Beta-85415) whilst an overlying sandy unit (shown by particle size analysis and SEM surface textural analysis to be aeolian transported) subject to TL-dating produced an age of 14,900 ± 3300 years BP (W1942). This poster highlights the considerations made in order to reconcile this obvious anomaly. In effect, previously obtained radiometric data within the study area (Flood 1981; Hall 1996), in conjunction with an examination of the adequacy of the sampled materials for radiocarbon and TL age determinations point to the TL determination being in error. Similar anomalies have been shown to occur elsewhere in southeast Queensland (Tejan-Kella et al. 1990) explanations for which have been related to selective rather than total bleaching of Holocene sands (Prescott personal communication). Re-dating of the sand sequence using the selective bleach method is required to examine whether the dating anomaly shown for Deception Bay parallels selective bleaching effects determined for other sequences within southeast Queensland. Unfortunately this is beyond the scope and funds of this geoarchaeological study

Setting a date

International Nuclear Information System (INIS)

Moore, Glenis.

1987-01-01

Dating techniques are discussed and explained. The age range and sensitivity of different techniques are given. Potassium/argon dating, amino-acid dating, radiocarbon dating, dendrochronology, thermoluminescence and geomagnetic field dating are all mentioned. Each technique is explained and a brief history given. The techniques and equipment used by the British Museum, and some examples of archaeological articles dated are mentioned. (UK)

Thermoluminescent dosimetry and assessment of personal dose

International Nuclear Information System (INIS)

Boas, J.F.; Martin, L.J.; Young, J.G.

1982-01-01

Thermoluminescence is discussed in terms of the energy band structure of a crystalline solid and the trapping of charge carriers by point defects. Some general properties of thermoluminescent materials used for dosimetry are outlined, with thermoluminescence of CaSO 4 :Dy being described in detail. The energy response function and the modification of the energy response of a dosimeter by shielding are discussed. The final section covers the connection between exposure, as recorded by a TLD badge, and the absorbed dose to various organs from gamma radiation in a uranium mine; the conversion from absorbed dose to dose equivalent; and uncertainties in assessment of dose equivalent

Thermoluminescence dating of potteries excavated at Bhagwanpura and Mathura

International Nuclear Information System (INIS)

Nambi, K.S.V.; Sasidharan, R.; Soman, S.D.

1979-01-01

Thermoluminescence (TL) dating attempts were made on sherds of freshly excavated potteries from Bhagwanpura and Mathura sites. TL measurements were generally made from the fine grains of the potsherds; attempts were also made to separate the quartz inclusions from some of the potsherds and evaluate the TL. Dose-rate estimations were made from an analysis of natural radioactivity of the samples; TLD estimation of the environmental gamma dose-rate component was also attempted for the Mathura sites. The TL age estimates ranged between 2000 and 5000 years, B.P. for the Bhagwanpura series and between 1400 and 3000 years, B.P. for the Mathura series. Distinctly different trends were seen in the ages of graywares and redwares from Bhagwanpura: with increasing depth at the site, the grayware ages diminished (upto 1.3 depth beyond which they do not occur) while the redware ages remain the same upto 1.3 m depth and increase regularly beyond. In the case of eight Mathura potsherds for which the archaeologists' expected age values were available, a good to fair (+- 2 to +- 19%) agreement with the TL ages could be seen for four sherds. The estimated accuracies of the TL ages range between +- 9 to +- 19% and such a high value stems from the generous allowance made for all possible values of water content in pottery and soil over the archaeological period; if reasonable values for the actual degree of wetness could be provided, the TL ages can be estimated with accuracies of the order of +- 5%. (auth.)

A study of the high-temperature signal characteristics in the thermoluminescence of porcelain

International Nuclear Information System (INIS)

Yin Gongming

2001-01-01

The thermoluminescence pre-dose technique for dating ancient porcelain was developed in many laboratories. This technique was the only method which could directly determine the age of old porcelain. But the thermoluminescence high-temperature signal (over 200 degree C) had not been studied. The authors conduced a preliminary study of the characteristic of thermoluminescence high-temperature signal, such as the TL natural glow curve, and the glow curves after beta or alpha irradiation. Most of the 32 ancient porcelains had thermoluminescence high temperature signal, and only one peak in their TL glow curve was found

Thermoluminescence: Potential Applications in Forensic Science

Science.gov (United States)

Ingham, J. D.; Lawson, D. D.

1973-01-01

In crime laboratories one of the most difficult operations is to determine unequivocally whether or not two samples of evidence of the same type were originally part of the same thing or were from the same source. It has been found that high temperature thermoluminescence (room temperature to 723 K) can be used for comparisons of this type, although work to date indicates that there is generally a finite probability for coincidental matching of glass or soil samples. Further work is required to determine and attempt to minimize these probabilities for different types of materials, and to define more clearly the scope of applicability of thermoluminescence to actual forensic situations.

Observations on some thermoluminescence emission centres in geological quartz

International Nuclear Information System (INIS)

Scholefield, R.B.; Prescott, J.R.; Fox, P.J.; Franklin, A.D.

1994-01-01

We report measurements of three-dimensional thermoluminescence emission spectra of samples of geological quartz, derived from Australian sediments. The emphasis is on peaks of particular practical interest for thermoluminescence sediment dating, viz. the 110 o C peak, which is used for pre-dose dating and the peak at 325 o C, which is of significance for partial and selective bleach techniques and for optically stimulated luminescence (OSL) dating. Because the 325 o C peak can be bleached to essentially zero, it can be isolated in a given spectrum by subtracting the bleached spectrum from the unbleached spectrum. By including both peaks in the same spectrum, it is demonstrated that they do not emit at the same wavelength, although this does not necessarily mean that the emission is from different emission centres. The 375 o C peak, which is important in total bleach methods, emits at a distinguishable wavelength. The use of bleaching and subtraction in practical dating is discussed. (Author)

Dating archaeological ceramics from the valley of Vitor-Arequipa by the thermoluminescence (TL) method

International Nuclear Information System (INIS)

Cano, N.F.; Yauri, J.M.; Watanabe, S.; Cuevas A, E.; Ayala A, J.S.

2006-01-01

In this work, we determined the age of an ancient pottery from the Valley of Vitor in the region of Arequipa-Peru by the thermoluminescence method. For dating 325 C TL peak was used and irradiation with γ-dose from 5 to 500 Gy was carried out for the additive method and from 0.4 to 5 Gy for the regeneration method. For these dose-values the TL intensity grows linearly, and we obtained the accumulated dose of D ac = (1.62 ± 0.09) Gy and D ac = (1.36 ± 0.03) Gy for the additive and regeneration method, respectively. The age (E) of the sample was calculated by the two methods, being E = (984 ± 184) years A.C. for the additive method and, E = (1073 ± 146) years A.C. for the regeneration method. Both results are within 800 to 1200 years, which is period of the Wari culture. (Author)

Dating archaeological ceramics from the valley of Vitor-Arequipa by the thermoluminescence (TL) method

Energy Technology Data Exchange (ETDEWEB)

Cano, N.F.; Yauri, J.M.; Watanabe, S. [Institute of Physics, University of Sao Paulo, CP 66318, 05315-970, Sao Paulo (Brazil); Cuevas A, E.; Ayala A, J.S. [University of San Agustin of Arequipa, Av. Independencia s/n, Arequipa (Peru)

2006-07-01

In this work, we determined the age of an ancient pottery from the Valley of Vitor in the region of Arequipa-Peru by the thermoluminescence method. For dating 325 C TL peak was used and irradiation with {gamma}-dose from 5 to 500 Gy was carried out for the additive method and from 0.4 to 5 Gy for the regeneration method. For these dose-values the TL intensity grows linearly, and we obtained the accumulated dose of D{sub ac}= (1.62 {+-} 0.09) Gy and D{sub ac} = (1.36 {+-} 0.03) Gy for the additive and regeneration method, respectively. The age (E) of the sample was calculated by the two methods, being E = (984 {+-} 184) years A.C. for the additive method and, E = (1073 {+-} 146) years A.C. for the regeneration method. Both results are within 800 to 1200 years, which is period of the Wari culture. (Author)

Application of radioisotope XRF and thermoluminescence (TL) dating in investigation of pottery from Tell AL-Kasra archaeological site, Syria.

Science.gov (United States)

Abboud, R; Issa, H; Abed-Allah, Y D; Bakraji, E H

2015-11-01

Statistical analysis based on chemical composition, using radioisotope X-ray fluorescence, have been applied on 39 ancient pottery fragments coming from the excavation at Tell Al-Kasra archaeological site, Syria. Three groups were defined by applying Cluster and Factor analysis statistical methods. Thermoluminescence (TL) dating was investigated on three sherds taken from the bathroom (hammam) on the site. Multiple aliquot additive dose (MAAD) was used to estimate the paleodose value, and the gamma spectrometry was used to estimate the dose rate. The average age was found to be 715±36 year. Copyright © 2015 Elsevier Ltd. All rights reserved.

Environmental radiation studies relevant to thermoluminescence dating

International Nuclear Information System (INIS)

Murray, A.S.; Bowman, S.G.E.; Aitken, M.J.

1980-01-01

To determine the age of a potsherd by the thermoluminescence (TL) technique, one must have an accurate knowledge of the cosmic and environmental gamma dose rate in quartz. This is obtained by leaving a sensitive TL dosimeter buried as near as possible to the position from which the sherd was removed. The ratios of the response of a quartz-like dosimeter to those of CaF 2 and LiF have been measured. This experiment used a 1-m cube of concrete containing 3000 ppM of uranium and its daughters. Smaller, less active matrixes of 40 K and thorium and its daughters have also been constructed. A means of making direct dose-rate determinations when the site context remains but burial of a dosimeter is impractical was developed using a NaI(Tl) system. The equipment was field tested on approx. 40 Peruvian archaeological sites, and results are compared with CaF 2 measurements

Instrumentation in thermoluminescence dosimetry

International Nuclear Information System (INIS)

Julius, H.W.

1986-01-01

In the performance of a thermoluminescence dosimetry (TLD) system the equipment plays an important role. Crucial parameters of instrumentation in TLD are discussed in some detail. A review is given of equipment available on the market today - with some emphasis on automation - which is partly based on information from industry and others involved in research and development. (author)

Second Quaternary dating workshop

Energy Technology Data Exchange (ETDEWEB)

NONE

1999-11-01

The second Quaternary dating methods workshop was held at Lucas Heights and sponsored by ANSTO and AINSE. Topics covered include, isotope and thermoluminescence dating, usage of accelerator and thermal ionisation mass spectrometry in environmental studies emphasizing on the methodologies used and sample preparation

Second Quaternary dating workshop

International Nuclear Information System (INIS)

1999-01-01

The second Quaternary dating methods workshop was held at Lucas Heights and sponsored by ANSTO and AINSE. Topics covered include, isotope and thermoluminescence dating, usage of accelerator and thermal ionisation mass spectrometry in environmental studies emphasizing on the methodologies used and sample preparation

Thermoluminescence and applications

International Nuclear Information System (INIS)

Rodrigues, G.V.

1986-01-01

The theory of thermoluminescent emission, the characteristics of main thermoluminescent phosphorus, and some applications are presented. The main thermoluminescent dosemeters used in dosimetry are related. (M.C.K.)

Thermoluminescence in alkali halides irradiated at 80K

International Nuclear Information System (INIS)

Jimenez de Castro, M.

1978-01-01

The thermoluminescence, the thermally stimulated currents and the thermal stability of the F centres induced in pure NaCl and KC1 crystals by X irradiation at 80K have been studied in detail, in the range between 80 and 300K. The thermoluminescent processes induced by illumination at 80K with F light in samples previously irradiated at room temperature has also been studied. It has been clearly observed the existence of thermoluminescent processes due to electrons and holes thermally released from traps, in which the F centres are not involved. The existence of hole-F centre recombination has not been observed. There are several thermoluminescent processes in both materials which are scribed to the recombination of F centres with mobile interstitial halogen atoms thermally released from traps, which are likely monovalent impurities in this temperature interval. The light emitting stage in these processes is originated by the formation of self trapped excitons. (Author) 66 refs

Use of thermoluminescence dosimetry for evaluation of internal beta dose-rate in archaeological dating

Energy Technology Data Exchange (ETDEWEB)

Bailiff, I K; Aitken, M J [Oxford Univ. (UK). Research Lab. for Archaeology

1980-07-01

An experimental technique is described for the absolute determination of beta dose-rate in pottery. The calibrated system utilizes thermoluminescent dosimeters (natural calcium fluoride) which are located external to the pottery sample. These measurements give an evaluation of the dose-rate at the centre of the pottery that is effectively independent of the relative importance of the thorium, uranium and potassium content (typically 12 ppm Th, 3 ppm U and 1% K/sub 2/O in pottery). This has been checked using analysed uranium, thorium and potassium materials. A dose-rate evaluation may be made after 10-14 d with an accuracy of +-5%, where the dose-rate to the dosimeter is of the order of 0.3 mrad d/sup -1/. Although the background dose-rate due to cosmic radiation and that arising from radioactive impurities in the calcium fluoride is significant (one third), measurements have shown that it may be accurately established. The technique described is to be preferred to other systems used in pottery dating because of its independence of relative radioisotope concentration.

Thermoluminescence dating of a tephra deposit of the ''Toya'' volcano (Hokkaido, Japan)

International Nuclear Information System (INIS)

Sanzelle, S.; Pilleyre, Th.; Miallier, D.; Fain, J.; Ganzawa, Y.

2000-01-01

Toya caldera which has a diameter of about 10 km and a hexagonal form is situated in the southern part of Hokkaido, northern Japan. The water level of the caldera lake is 84 m and the highest altitude of the central dome in the lake, Nakajima is 454 m. The volcanic activity is divided into 4 stages of the Toya Pyroclastic Flow Deposits 1 to 4. This tephra is composed of rhyolitic ash which is rich in glass and associated with hornblende, pyroxene and quartz. In a previous work, the age of eruption was estimated by utilising several dating methods and the stratigraphical correlation with other tephra. The ages which resulted from FT (Fission Tracks) dating and TL (Thermoluminescence) dating indicated 130±30 ka and 103-134 ka, respectively. The overall estimated age, received from other information such as the environmental change of mineral marine deposits, has been accepted as 100-120 ka by Quaternary Researchers. Because this tephra can be found widely in the Quaternary field, many researchers can use it as an appropriate age indicator of the 5c or 5d Isotope Stage, the middle age of the Last Internal Glacial Age. A new dating program was initiated, using the red TL of quartz grains extracted from the tephra. The samples studied in the present work came from the southern part of the deposits, around 15 km away from the centre of the caldera. The TL measurements, using the red signal of xenolithic quartz grains from the tephra, were made at Aubiere. Three distinct sets of samples were measured. The first two differ from each other by grain size, 250-350 μm (TOYA2, Aset2) and 150-250 μm (TOYA1,Bset3), and were irradiated in Japan and the third one, 250-350 μm (TOYA2, Cset2) was irradiated at Aubiere. The annual dose rate experienced by the samples during burial was estimated from a compilation of radionuclide contents evaluated in Japan using NAA and in France, using low level gamma spectroscopy (Aubiere) and ICPMS (CRPG, Nancy). In situ water content (as dug

Thermoluminescence dating of Indian archaeological sites

International Nuclear Information System (INIS)

Singhvi, A.K.; Sharma, Y.P.; Agrawal, D.P.

1983-01-01

In an attempt to provide a chronology for Indian archaeological sites, an extensive pottery dating programme was initiated during 1978-1979. So far we have provided a chronology for seven important Indian archaeological sites. The dated cultures include: 1) the Ochre Colour Ware culture, 2) the Pre-Harappan culture, 3) the megalithic culture and 4) the Painted Grey Ware culture. A complete survey of recently measured TL dates are presented in a model format similar to that used in Radiocarbon. (author)

Dating by thermoluminescence 127 pottery fragments collected from 4 archaeological sites in Taquari valley, Rio grande do Sul state, Brazil

International Nuclear Information System (INIS)

Watanabe, Shigueo; Cano, Nilo F.; Gennari, R.F.; Goncalves, D.C.; Machado, Neli T.G.

2011-01-01

127 fragments of pottery from excavation of four archaeological sites in Taquari Valley, close to Lajeado, State of Rio Grande do Sul, Brazil have been dated by thermoluminescence. After usual crushing, sieving, immersing in HCl solution and then in HF solution, accumulated dose, Dac, (or equivalent or paleodose) has been measured using additive method. The annual dose rate of natural radiation was estimated from uranium, thorium and potassium content in both soil from where these fragments have been collected and in fragments itselves. Cosmic ray contribution was added. The interesting finding is that the glow curves of quartz grains from sites enumerated 101, 110 and 114 indicated rare variety of quartz known as reddish quarts, whereas the glow curves of quartz grains, from the site numbered 107 are equal to these of usual quartz (hyaline). Results of dating and the properties of reddish quartz will be discussed. (author)

Comparative analysis of dose rates in bricks determined by neutron activation analysis, alpha counting and X-ray fluorescence analysis for the thermoluminescence fine grain dating method

Czech Academy of Sciences Publication Activity Database

Bártová, H.; Kučera, Jan; Musílek, L.; Trojek, T.

2014-01-01

Roč. 104, NOV (2014), s. 393-397 ISSN 0969-806X. [1st International Conference on Dosimetry and its Applications (ICDA). Prague, 23.6.2013-28.6.2013] R&D Projects: GA MŠk(XE) LM2011019 Institutional support: RVO:61389005 Keywords : Alpha coutning * neutron activation analysis * X-ray fluorescence * thermoluminescence dating * dose rate Subject RIV: CB - Analytical Chemistry, Separation Impact factor: 1.380, year: 2014

Handbook of thermoluminescence

CERN Document Server

Furetta, Claudio

2010-01-01

This second edition of the Handbook of Thermoluminescence enlarges on all the subjects which were treated in the first edition and adds further arguments, including the theory of thermoluminescent dose measurement, several examples concerning the kinetics parameters determination using various methods such as peak shape, isothermal decay, and so on. A special section is devoted to food irradiation, an important subject at the present time, and to the thermoluminescent characterization of the minerals extracted from the irradiated food. Another new section is devoted to the thermoluminescent ph

Influence of thermoluminescence signal for debris flow surface materials by sunlight bleaching

International Nuclear Information System (INIS)

Song Bo; Wei Mingjian; He Youbing; Zhou Rui; Zhao Qiuyue; Zhang Bin

2013-01-01

Thermoluminescence was utilized for measuring the thermoluminescence signals of the standard debris flow samples which were bleached by simulated sunlight and debris flow samples after real sunlight bleaching. The experiment results demonstrate that light bleaching phenomenon of the debris flow occurs when it experiences a period of exposure. The thermoluminescence signal of the samples weakens gradually with the increase of depth. The optical bleaching phenomenon is obvious. Within a certain depth, light bleaching phenomenon is enhanced with the increase of light intensity. The annealing depth of simulated sunlight bleaching experiment is about 1 mm, and the actual annealing depth of sunlight bleaching is about 6 mm. According to the equivalent dose variation with depth, the mud of natural debris flow can be divided into two stages. It has fundamental significance in the application of thermoluminescence dating techniques to divide the stages of debris flow sediments. (authors)

Spatially-resolved thermoluminescence from snail opercula using an EMCCD

DEFF Research Database (Denmark)

Duller, G.A.T.; Kook, Myung Ho; Stirling, R.J.

2015-01-01

In recent years opercula of the snail species Bithynia tentaculata have been shown to emit thermoluminescence (TL) signals that can be used to determine equivalent dose, and may be capable of dating events throughout the entire Quaternary period. Concentric growth lines are a notable feature of a...

Thermoluminescence and their applications

International Nuclear Information System (INIS)

Rodrigues, G.V.

1986-01-01

The theory involved in the phenomenon of thermoluminescence emission, the characteristics of the main thermoluminescent phosphorus and some of their applications are presented. Some of the main thermoluminescent dosemeters used in dosimetry are described. (M.C.K.) [pt

Archaeological and Geological dating by means of thermoluminescence; Fechamiento geologico y arqueologico por termoluminiscencia

Energy Technology Data Exchange (ETDEWEB)

Gonzalez M, P R

1999-07-01

In this thesis an specific method for dating local archaeological and geological samples based on the phenomenon of thermoluminescence (TL) using the fine grain and quartz inclusion techniques is developed. Taking into account that this work is interesting for professionals working in the fields of Physics, Chemistry, Archaeology, Anthropology and related sciences, some basic concepts are described to have a better comprehension. Chapter 1 describes the concept of radioactivity, remarking the importance of the different decay types as well as the main radioactive series and the energy liberated in the process. The causes of radioactive desequilibrium are also considered in the case for radon. Another important aspect taken into account in this chapter is the radioisotope production and its relationship with the neutron activation analysis used for the determination of the Uranium and Thorium concentrations in the samples. The TL phenomenon is described in Chapter 2, emphasizing the importance of the process of thermally stimulated luminescence best known as TL and its application for dating minerals of different origin. Chapter 3 shows some important antecedents remarking some aspects of the techniques commonly used for dating purposes. Chapter 4 shows the different methods used for the sample preparation. The techniques used for the {sup 40} K, {sup 238} U and {sup 232} Th determination as well as for the cosmic radiation measurement using locally made TLD are also described. The methods used for the determination of the paleodosis as a function of the TL intensity of each sample are described: special emphasis is taken on the moisture effects as well as in the error limits in the age estimation. Results and conclusions of this study are presented in Chapter 5. These results gave an age of 980 {+-} 90 years for the Edzna ceramic and 1520 {+-} 90 years for the Calixtlahuaca ceramics. The age of the Teotihuacan ceramics was not estimated due to the lack of a stable

Archaeological and Geological dating by means of thermoluminescence; Fechamiento geologico y arqueologico por termoluminiscencia

Energy Technology Data Exchange (ETDEWEB)

Gonzalez M, P.R

1999-07-01

In this thesis an specific method for dating local archaeological and geological samples based on the phenomenon of thermoluminescence (TL) using the fine grain and quartz inclusion techniques is developed. Taking into account that this work is interesting for professionals working in the fields of Physics, Chemistry, Archaeology, Anthropology and related sciences, some basic concepts are described to have a better comprehension. Chapter 1 describes the concept of radioactivity, remarking the importance of the different decay types as well as the main radioactive series and the energy liberated in the process. The causes of radioactive desequilibrium are also considered in the case for radon. Another important aspect taken into account in this chapter is the radioisotope production and its relationship with the neutron activation analysis used for the determination of the Uranium and Thorium concentrations in the samples. The TL phenomenon is described in Chapter 2, emphasizing the importance of the process of thermally stimulated luminescence best known as TL and its application for dating minerals of different origin. Chapter 3 shows some important antecedents remarking some aspects of the techniques commonly used for dating purposes. Chapter 4 shows the different methods used for the sample preparation. The techniques used for the {sup 40} K, {sup 238} U and {sup 232} Th determination as well as for the cosmic radiation measurement using locally made TLD are also described. The methods used for the determination of the paleodosis as a function of the TL intensity of each sample are described: special emphasis is taken on the moisture effects as well as in the error limits in the age estimation. Results and conclusions of this study are presented in Chapter 5. These results gave an age of 980 {+-} 90 years for the Edzna ceramic and 1520 {+-} 90 years for the Calixtlahuaca ceramics. The age of the Teotihuacan ceramics was not estimated due to the lack of a stable

A Survey of Archaeological Samples Dated in 1985

DEFF Research Database (Denmark)

Mejdahl, Vagn

1986-01-01

A survey is given of archaeological samples received for dating in 1985 at the Nordic Laboratory for Thermoluminescence Dating. A total of 66 samples were dated, 42 of which were burnt stones. All results were corrected for short-term fading as measured for samples stored at room temperature...

Luminescence dating at Rose cottage cave: a progress report

CSIR Research Space (South Africa)

Woodborne, S

1997-10-01

Full Text Available Deal with infrared-stimulated luminescence and thermoluminescence dates from Rose Cottage Cave in South Africa. Discrepancy between luminescence and radiocarbon dates; Concentration of radioactive elements in sediments before and after leaching...

A Survey of Archaeological Samples Dated in 1984

DEFF Research Database (Denmark)

Mejdahl, Vagn

A survey is given of archaeological samples dated in 1984 at the Nordic Laboratory for Thermoluminescence Dating. A total of 79 samples were dated, 49 of which were burnt stones. All results were corrected for fading as measured for samples stored for four weeks at room temperature. The alpha dose...

ESR-dating of subfossil mollusc shells: the problem of absorbed paleodose fading

International Nuclear Information System (INIS)

Molod'kov, A.

1988-01-01

Detailed investigation of paleodosimetric prperties of subfossil mollusc shells has been carried out with respect to their dating by ESR-spectroscopy. Attention has been paid to the connection between the absorbed paleodose value and factors on the upper dating limit. Energetic parameters of the CO 3 3- centres have been determined in the calcareous shell skeleton serving as a paleodetector: E=1.515 eV, ν 0 =8x10 13 s -1 , τ=1.14x10 6 years at 5 deg C. Mathematical models have been elaborated for the accumulation of paleodose in natural conditions. New paleodosimetric equations proposed for calculating the age of shells and some minerals may be applied both to ESR- and thermoluminescence-dating. The proposed method enables one to date the shells within the time span of nx10 2 -nx10 6 years

Design and development of low cost thermoluminescence measurement system using PIC16F877 microcontroller

International Nuclear Information System (INIS)

Neelamegam, P; Rajendran, A

2006-01-01

A real time microcontroller based thermoluminescence system has been developed to measure light intensity and temperature and to control linear heating. This instruments permits to conduct investigations on thermoluminescent materials, such as alkali halides, phosphors and related compounds, which have important applications in materials science and in dosimetry. A low cost dedicated PIC16F877 based microcontroller board was employed for the hardware. The detail of its interface and software to measure thermoluminescence and to send data to PC is explained in this paper

Design and development of low cost thermoluminescence measurement system using PIC16F877 microcontroller

Energy Technology Data Exchange (ETDEWEB)

Neelamegam, P [Department of Electronics and Instrumentation Engineering, Shunmuga Arts, Science, Technology and Research Academy (SASTRA), Deemed University, Thanjavur-613 402, Tamil Nadu (India); Rajendran, A [PG and Research Department of Applied Physics, Nehru Memorial College (Autonomous), Puthanampatti-621 007, Tiruchirappalli, Tamil Nadu (India)

2006-05-15

A real time microcontroller based thermoluminescence system has been developed to measure light intensity and temperature and to control linear heating. This instruments permits to conduct investigations on thermoluminescent materials, such as alkali halides, phosphors and related compounds, which have important applications in materials science and in dosimetry. A low cost dedicated PIC16F877 based microcontroller board was employed for the hardware. The detail of its interface and software to measure thermoluminescence and to send data to PC is explained in this paper.

Dating by the method of thermoluminescence of a prehistoric campfire found in the archaeological site of Baixa do Umbuzeiro, RN, Brazil

International Nuclear Information System (INIS)

Azevedo, Renata L.; Santana, Sergio T.; Khoury, Helen J.; Sullasi, Henry L.; Borges, Fabio M.; Avila, Gabriela M.; Pessis, Anne-Marie

2011-01-01

In this work it was carried out the dating of a prehistoric campfire found in the archaeological site of Baixa do Umbuzeiro - RN, by the method of thermoluminescence (TL). To perform the dating, were collected five sediment samples from different parts of the campfire. The accumulated dose in these samples was obtained by the method of regenerative doses in which the natural TL intensity is compared with the TL intensity of doses supplied in artificial laboratory through a Co-60 source. The determination of the annual dose rate was performed by the determination of the levels of U, Th and K in the samples by gamma spectrometry with germanium hyper pure detector (GeHP). The five values found for accumulated dose were evaluated by the statistical test ANOVA, having been discarded one of these. The accumulated dose average is 12.5 ± 1.5 Gy and the annual dose rate is 3.31 ± 0.60 mGy/year. These values provided an age of about 3776 ± 821 years for the campfire of Baixa do Umbuzeiro. (author)

Study on thermoluminescence dating for Nideping terrace of Dongchuan, Yunnan province

International Nuclear Information System (INIS)

Zhang Bin; Wei Mingjian; Liu Chao; Zhang Yongdong; Zhou Rui; Liu Junxin; Liu Tiantian; Zhao Qiuyue; Song Bo

2013-01-01

The sequence of geological age on Nideping terrace in Dongchuan, Yunnan Province was established by thermoluminescence. The result shows that the age of the terrace is 9.3-57.1 ka. The vertical age of ancient debris flow terraces was established, and the time structure of Nideping mud was received. The age data was provided for the restoration ancient environment of the debris flow. It is shown that the debris flow deposits have discontinuities through age data and exist age inversion. The radioactive elements such as uranium, thorium, potassium may be leaching deposition affected by the presence of local rainfall and the annual dose rate increases with depth. (authors)

Year 2000 compliance concerns with the ISA Thermoluminescent Dosimetry Data Processing (TL-DP) software system

Energy Technology Data Exchange (ETDEWEB)

Saviz, K.

1998-05-26

The year 2000 is rapidly approaching, and there is a good chance that computer systems that utilize two digit year dates will experience problems in retrieval of date information. The ISA Thermoluminescent Dosimetry Data Processing (TL-DP) software and computer system has been reviewed for Year 2000 compliance issues.

Year 2000 compliance concerns with the ISA Thermoluminescent Dosimetry Data Processing (TL-DP) software system

International Nuclear Information System (INIS)

Saviz, K.

1998-01-01

The year 2000 is rapidly approaching, and there is a good chance that computer systems that utilize two digit year dates will experience problems in retrieval of date information. The ISA Thermoluminescent Dosimetry Data Processing (TL-DP) software and computer system has been reviewed for Year 2000 compliance issues

Dating and classification of Syrian excavated pottery from Tell Saka Site, by means of thermoluminescence analysis, and multivariate statistical methods, based on PIXE analysis

International Nuclear Information System (INIS)

Bakraji, E.H.; Ahmad, M.; Salman, N.; Haloum, D.; Boutros, N.; Abboud, R.

2011-01-01

Thermoluminescence (TL) dating and Proton Induced X-ray Emission (PIXE) techniques have been utilized for the study of archaeological pottery fragment samples from Tell Saka Site, which is located at 25 km south east of Damascus city, Syria. Four samples were chosen randomly from the site, two from third level and two from fourth level for dating using TL technique and the results were in good agreement with the date assigned by archaeologists. Twenty-eight sherds were analyzed using PIXE technique in order to identify and characterize the elemental composition of pottery excavated from third and fourth levels, using 3 MV tandem accelerator in Damascus. The analysis provided almost 20 elements (Na, Mg, Al, Si, P, S, K, Ca, Ti, Mn, Fe, Co, Ni, Cu, Zn, Rb, Sr, Y, Zr, Nb). However, only 14 elements as follows: K, Ca, Ti, Mn, Fe, Co, Ni, Cu, Zn, Rb, Sr, Y, Zr, Nb were chosen for statistical analysis and have been processed using two multivariate statistical methods, Cluster and Factor analysis. The studied pottery were classify into two well defined groups. (author)

Study of natural thermoluminescence of quartzite in a gold and uranium mineralized zone (Canavieiras, Jacobina, Brazil)

International Nuclear Information System (INIS)

Ferreira, J.; Nordemann, D.

1976-01-01

The quartzite of the Canavieiras gold mine (Jacobina, Bahia, Brazil) exhibits a high temperature peak (280 +- 2) 0 C in its natural thermoluminescence glow curve. It was experimentally determined that the amount of light in this peak could be reproduced to within 5% for grain sizes between 80 and 100 mesh (0.149 and 0.177 mm). A positive correlation was found between the amount of this thermoluminescence and the uranium content with saturation beginning to be detected at the maximum (700 ppm) amount of uranium found. Assuming that the thermoluminescence peak used is at a temperature high enough to permit accumulation and stability at room temperatures, the thermoluminescence found could have accumulated in (12.1 +- 0.3) x 10 6 years. This may date a complete liberation of trapped electrons in conjunction with a well documented initiation of weathering. (author) [pt

THERMOLUMINESCENT DOSIMETRY

Energy Technology Data Exchange (ETDEWEB)

Malsky, Stanley J.; Amato, Charles G.; Roswit, Bernard

1963-06-15

The performance of CaF/sub 2/: Mn and LiF as thermoluminescent in vivo dosimeters is studied. The facility with which this type of dosimeter can be inserted into the body is discussed. The dosimeter is inserted into the body by trocar or catheter techniques and exposed to radiation; it is then removed and heated, and the thermoluminescence is measured and used as an indication of the absorbed dose. (T.F.H.)

Thermoluminescent dosimetry: theory, materials and applications

International Nuclear Information System (INIS)

Rosa, L.A.R.da.

1978-01-01

A survey about the thermoluminescence theory, the properties of the main thermoluminescent phosphors and their applications is presented. Some of the most important thermoluminescent readers are also mentioned [pt

Thermoluminescence and cathodoluminescence studies of calcite and MgO: surface defects and heat treatment

International Nuclear Information System (INIS)

Goeksu, H.Y.; Brown, L.M.

1988-01-01

Some of the problems which preclude accurate thermoluminescence (TL) dating of geologically formed calcite stem from different sample pre-treatment procedures, such as grinding, drilling or pre-heating. It has long been known that grinding can introduce spurious TL in calcite, but there have been wide differences of opinion as to the magnitude of the influence and its importance. Therefore, various grinding and acid-washing procedures have been suggested to avoid spurious thermoluminescence. Various models have been developed to explain the mechanism. We have studied the changes in thermoluminescence (TL) and cathodoluminescence (CL) properties as well as in the spectral composition of the glow from calcite and MgO due to surface defects and heat treatment. It is found that both laboratory heat treatment and surface indents give rise to changes in TL efficiency. (author)

Thermoluminescence albedo-neutron dosimetry

International Nuclear Information System (INIS)

Strand, T.; Storruste, A.

1986-10-01

The report discusses neutron detection with respect to dosimetry and compares different thermoluminescent dosimetry materials for neutron dosimetry. Construction and calibration of a thermoluminescence albedo neutron dosemeter, developed by the authors, is described

Analytical investigations of thermoluminescence glow curve on quartz for luminescence dating

International Nuclear Information System (INIS)

Kim, K.B.; Hong, D.G.

2015-01-01

Investigations of bleaching and thermoluminescence (TL) response to radiation dose of quartz are importance in luminescence dating. Although such research has been extensively carried out for various types of quartz, most work was performed on the basis of TL intensity integrated for a particular temperature range on the glow curve, without any peak separation. In this study we investigated bleaching by a blue light stimulation and radiation dose behaviour for separated TL glow peaks of quartz, which are thermally stable, by using the computerized glow curve deconvolution (CGCD) method combined with the T_m–T_s_t_o_p method. The T_m–T_s_t_o_p method indicates that the glow curve of quartz is the superposition of at least seven components (P1–P7) in the temperature range between room temperature and 450 °C. A bleaching experiment for four thermally stable glow peaks (P4–P7) using a blue light stimulation revealed that the bleaching rate of peak P4 exhibits three different exponential decays, whereas the peaks P5, P6 and P7 are bleached with two different exponential decays. After bleaching of 12 h, the TL intensity of peaks P4, P5, P6 and P7 were reduced to approximately 6%, 16%, 26% and 68% of the initial value, respectively. Additionally, in a study of the radiation dose response of the four thermally stable glow peaks, all peaks have a similar pattern, which are well fitted by a single saturating exponential function. - Highlights: • We studied the physical characteristics of the separated TL glow peaks on quartz. • The kinetic parameters of each separated glow peak are evaluated by a CGCD method. • The separated peaks were bleached with two or three exponential decays. • The dose responses for the separated peaks showed a similar growth curve.

Luminescence dating

International Nuclear Information System (INIS)

Rieser, U.

2013-01-01

The luminescence techniques have evolved over the last 40 years to a powerful dating instrument in archaeology and geoscience. Depending on how the luminescence is stimulated, one distinguishes the phenomena of thermoluminescence (TL), optically stimulated luminescence (OSL) and infrared stimulated luminescence (IRSL). Each of these phenomena has its specific potential for dating various archaeological materials in the time range from medieval back to palaeolithic periods, or, speaking in geological terms, for dating of Holocene and late Pleistocene objects. The OSL and IRSL techniques are sometimes treated together as 'optical dating'. The luminescence techniques differ from other major dating techniques, such as 14 C, essentially by their applicability to inorganic materials, their wide age-range from about 100 years to more than 100,000 years and the kind of datable events which are the last exposure to heat or to light. (author). 10 refs., 3 figs.

Luminescence dating

International Nuclear Information System (INIS)

Rieser, U.

2009-01-01

The luminescence techniques have evolved over the last 40 years to a powerful dating instrument in archaeology and geoscience. Depending on how the luminescence is stimulated, one distinguishes the phenomena of thermoluminescence (TL), optically stimulated luminescence (OSL) and infrared stimulated luminescence (IRSL). Each of these phenomena has its specific potential for dating various archaeological materals in the time range from medieval back to palaeolithic periods, or, speaking in geological terms, for dating of Holocene and late Pleistocene objects. The OSL and IRSL techniques are sometimes treated together as 'optical dating'. The luminescence techniques differ from other major dating techniques, such as 14 C, essentially by their applicability to inorganic materials, their wide age-range from about 100 years to more than 100,000 years and the kind of datable events which are the last exposure to heat or to light. (author). 10 refs., 3 figs.

Luminescence dating

International Nuclear Information System (INIS)

Rieser, U.

2008-01-01

The luminescence techniques have evolved over the last 40 years to a powerful dating instrument in archaeology and geoscience. Depending on how the luminescence is stimulated, one distinguishes the phenomena of thermoluminescence (TL), optically stimulated luminescence (OSL) and infrared stimulated luminescence (IRSL). Each of these phenomena has its specific potential for dating various archaeological materals in the time range from medieval back to palaeolithic periods, or, speaking in geological terms, for dating of Holocene and late Pleistocene objects. The OSL and IRSL techniques are sometimes treated together as 'optical dating'. The luminescence techniques differ from other major dating techniques, such as 14 C, essentially by their applicability to inorganic materials, their wide age-range from about 100 years to more than 100,000 years and the kind of datable events which are the last exposure to heat or to light. (author). 10 refs., 3 figs

Luminescence dating

International Nuclear Information System (INIS)

Rieser, U.

2012-01-01

The luminescence techniques have evolved over the last 40 years to a powerful dating instrument in archaeology and geoscience. Depending on how the luminescence is stimulated, one distinguishes the phenomena of thermoluminescence (TL), optically stimulated luminescence (OSL) and infrared stimulated luminescence (IRSL). Each of these phenomena has its specific potential for dating various archaeological materials in the time range from medieval back to palaeolithic periods, or, speaking in geological terms, for dating of Holocene and late Pleistocene objects. The OSL and IRSL techniques are sometimes treated together as 'optical dating'. The luminescence techniques differ from other major dating techniques, such as 14 C, essentially by their applicability to inorganic materials, their wide age-range from about 100 years to more than 100,000 years and the kind of datable events which are the last exposure to heat or to light. (author). 10 refs., 3 figs.

Luminescence dating

International Nuclear Information System (INIS)

Rieser, U.

2009-01-01

The luminescence techniques have evolved over the last 40 years to a powerful dating instrument in archaeology and geoscience. Depending on how the luminescence is stimulated, one distinguishes the phenomena of thermoluminescence (TL), optically stimulated luminescence (OSL) and infrared stimulated luminescence (IRSL). Each of these phenomena has its specific potential for dating various archaeological materals in the time range from medieval back to palaeolithic periods, or, speaking in geological terms, for dating of Holocene and late Pleistocene objects. The OSL and IRSL techniques are sometimes treated together as 'optical dating'. The luminescence techniques differ from other major dating techniques, such as 14 C, essentially by their applicability to inorganic materials, their wide age-range from about 100 years to more than 100,000 years and the kind of datable events which are the last exposure to heat or to light. (author). 10 refs., 3 figs

Thermoluminescence kinetics of pyrite (FeS2)

International Nuclear Information System (INIS)

Silverman, A.N; Levy, P.W.; Kierstead, J.A.

1990-01-01

Thermoluminescence of pyrite (FeS 2 ) has been investigated to study the kinetics of single peak glow curves. The material used normally exhibits one large and four small peaks. However a glow curve can be obtained with only the large single peak that is suitable for testing thermoluminescence kinetics. Glow curves from aliquots of a single natural pyrite crystal studied in detail contain two low intensity thermoluminescence (TL) peaks at ∼90 degree and ∼250 degree C, and two chemiluminescence (CL) peaks at ∼350 degree and ∼430 degree C. The CL peaks are largely removable by initially heating the sample chamber under vacuum, pumping through liquid nitrogen traps, and recording glow curves immediately after helium is introduced, procedures which reduce system contaminants that react with pyrite. The shape, the variation of the temperature of the peak maximum (T max ) with dose, and the retrapping to recombination cross section ratio σ of the large 250 degree C peak are better described by the general one trap (GOT) kinetic equation, the basic equation from which the 1st and 2nd order kinetic equations are obtained as special cases (see text), than by the 1st and 2nd order equations. 12 refs., 7 figs

Radiometric dating methods

International Nuclear Information System (INIS)

Bourdon, B.

2003-01-01

The general principle of isotope dating methods is based on the presence of radioactive isotopes in the geologic or archaeological object to be dated. The decay with time of these isotopes is used to determine the 'zero' time corresponding to the event to be dated. This paper recalls the general principle of isotope dating methods (bases, analytical methods, validation of results and uncertainties) and presents the methods based on natural radioactivity (Rb-Sr, Sm-Nd, U-Pb, Re-Os, K-Ar (Ar-Ar), U-Th-Ra- 210 Pb, U-Pa, 14 C, 36 Cl, 10 Be) and the methods based on artificial radioactivity with their applications. Finally, the methods based on irradiation damages (thermoluminescence, fission tracks, electron spin resonance) are briefly evoked. (J.S.)

Thermoluminescence dating in the South-West Pacific region

International Nuclear Information System (INIS)

Prescott, J.R.

1982-01-01

The archaeometry laboratory of the University of Adelaide has undertaken a variety of dating projects for archaeologists in the region. For example, a survey of Pacific Island pottery has shown that themoluminescence dating is likely to be severely limited in usefulness on islands remote from the continental shelf i.e., the andesitic island arcs and oceanic islands. On the mainland of Australia, we have dated prehistoric campsites using ovenstones from fireplaces and have compared C-14 ages with themoluminescent ages. Where there is a close stratigraphic association of the C-14 and TL materials, there is good agreement between the two methods. (author)

Thermoluminescent dosimeter system

International Nuclear Information System (INIS)

Felice, P.E.; Gonzalez, J.L.; Seidel, J.G.

1979-01-01

An improved thermoluminescent dosimeter system and apparatus for sensing alpha particle emission is described. A thermoluminescent body is sealed between a pair of metallized plastic films. The dosimeter is mounted within a protective inverted cup or a tube closed at one end, which is disposed in a test hole for exposure to radioactive radon gas which is indicaive of uranium deposits

Induced thermoluminescence as a method for dating recent volcanism: Hawaii County, Hawaii, USA

Science.gov (United States)

Sears, Derek W. G.; Sears, Hazel; Sehlke, Alexander; Hughes, Scott S.

2018-01-01

We have measured the induced thermoluminescence (TL) properties of fifteen samples of basalts collected from the Big Island of Hawaii in order to continue our investigation into the possible utility of this technique as a chronometer. Previous studies of basalts from Idaho have suggested the induced TL of basalts increases with age. Meteorite data suggest two possible explanations for this observation which are that (1) the initial glassy or amorphous phases crystalize with time to produce feldspar, the mineral producing the TL signal, and (2) feldspars lose Fe as they equilibrate and since Fe is a quencher of TL this would cause an increase in TL. The old basalts from Kohala (> 100 ka), which are mostly alkali basalts, have TL sensitivities 10-100 times higher than the much younger tholeiites from Kilauea and Mauna Loa (data, the slope of the regression line for the plot of log TL sensitivity against historic or radiometric age for the Hawaii basalts is within 2 sigma of the regression line for the analogous plot for the Idaho basalts, although the Hawaii line is much shallower (0.0015 ± 0.0012 for Hawaii cf. 0.0039 ± - 0.0014 for Idaho, 2σ uncertainties). However, the intercepts are significantly different (0.78 ± 0.18 for Hawaii cf. - 0.079 ± 0.28 for Idaho, 2σ uncertainties). These results suggest that TL sensitivity has the potential to be a means of dating volcanism in the 0-800 ka range, although the scatter in the data - especially for the < 50 ka samples - needs to be understood, and a means found for its removal, before the technique has the possibility of being practically useful.

Unraveling thermoluminescence

CERN Document Server

Sunta, C M

2014-01-01

The book is essentially about the theoretical aspects of thermoluminescence (TL). It is structured and written in a manner which will specially be of interest to the fresh undergraduate students and young researchers planning to take up work in the field of thermoluminescence. It is arranged into seven chapters, starting with the historical growth of the subject of TL and an overview of the luminescence phenomena. A Physical model involving thermally disconnected deep traps is specially described. Using this model expressions are derived for the TL intensity growth curve, the supralinearity fa

Thermoluminescence of LaAlO3

International Nuclear Information System (INIS)

Morales H, A.; Zarate M, J.; Rivera M, T.; Azorin N, J.

2015-10-01

In this paper the thermoluminescent properties of doped lanthanum aluminate (LaAlO 3 ) with dysprosium ion (Dy) were studied. The thermoluminescence characteristics in the samples were obtained using an ultraviolet radiation of 220 nm. The LaAlO 3 :Dy samples were prepared by the modified Pechini method (Spray Dryer). The structural and morphological characterization was obtained by X-ray diffraction (XRD) and scanning electron microscopy (Sem) techniques respectively. The size particle composing the agglomerate was determined by Sem, agglomerated particles composed size of 2μm were observed. The thermoluminescence response of LaAlO 3 :Dy was compared with that obtained with the undoped sample. Thermoluminescence brightness curves of LaAlO 3 :Dy showed a peak centered at 185 grades C. Sensitivity of doped sample was greater, about 100 times compared with the undoped sample. Thermoluminescence response in function of the wavelength showed a maximum at 220 nm. Also the fading in thermoluminescence response was studied. (Author)

Mexican gems as thermoluminescent dosimeters

International Nuclear Information System (INIS)

Azorin N, J.

1979-01-01

The possibility of using naturally ocurring mexican gems as thermoluminescent dosimeters (TLD) was investigated. Twelve types of gems were irradiated with X and gamma rays in order to determinate their dosimetric properties. Three of these gems showed favorable thermoluminescent characteristics compared with commercial thermoluminescent dosimeters. The plots of their thermoluminescent response as a function of gamma dose are straight lines on full log paper in the dose range 10 -2 to 10 2 Gy. The energy dependence is very strong to low energies of the radiation. Their fading was found to be about 5%/yr. and they may be annealed as reused without loss in sensitivity. Therefore, these gems can be used as X and gamma radiation dosimeters. (author)

Bleaching of the thermoluminescence of feldspars by sunlight

International Nuclear Information System (INIS)

Robertson, G.B.; Prescott, J.R.; Hutton, J.T.

1991-01-01

Feldspars are an important component of materials used for thermoluminescence (TL) and photoluminescence (PL) dating of sediments; and successful dating implies a knowledge of the degree of re-setting by exposure to sunlight of the stored luminescence energy. We have studied the bleaching by full sunlight of the TL of six alkali feldspars of representative composition and of one oligoclase. The high potassium and high sodium feldspars are the brightest, and are also the least easily bleached, whereas those of intermediate (K-Na) composition bleach quickly. On a time scale of upwards of 16 h, all samples would have bleached enough for them to be useful for TL dating. A search was made for individual glow curve peaks that bleach particularly quickly (and are thus similar to the well-known 325 o C peak used in the TL dating of quartz). In the samples studied, there was only one glow curve peak that was selectively susceptible to bleaching: the 280 o C peak in oligoclase. (author)

Thermoluminescence, a universal tool for dosimetry

International Nuclear Information System (INIS)

Barthe, J.

1999-01-01

Radio-thermoluminescence is a transient light emission occurring when certain substances, which have been exposed to ionizing radiation, are heated. Under some conditions the quantity of emitted light is proportional to the absorbed dose. This linearity allows thermoluminescence to be used in various fields such as dosimetry, geology and age determination. Dosimeters based on thermoluminescence are passive, they do not require a source of energy and they can sustain high temperatures and high levels of irradiation. Thermoluminescence has been applied for determining the dose absorbed by meteorites and lunar rocks

Method for detecting radiation dose utilizing thermoluminescent material

International Nuclear Information System (INIS)

Miller, S.D.; McDonald, J.C.; Eichner, F.N.; Durham, J.S.

1992-01-01

The amount of ionizing radiation to which a thermoluminescent material has been exposed is determined by first cooling the thermoluminescent material and then optically stimulating the thermoluminescent material by exposure to light. Visible light emitted by the thermoluminescent material as it is allowed to warm up to room temperature is detected and counted. The thermoluminescent material may be annealed by exposure to ultraviolet light. 5 figs

Dating of Chichen Itza ceramics by the method of thermoluminescence; Datacion de ceramica de Chichen Itza por el metodo de termoluminiscencia

Energy Technology Data Exchange (ETDEWEB)

Gonzalez M, P.R.; Mendoza A, D.; Cuapio O, L.A. [ININ, 52045 Ocoyoacac, Estado de Mexico (Mexico); Ramirez L, A.; Schaaf, P. [Instituto de Geofisica-UNAM, 04510 Mexico D.F. (Mexico); Chung, H. [Dept. of Anthropology, Duksung University, Seoul (Korea, Republic of); FFL-UNAM, 04510 Mexico D.F. (Mexico)

2005-07-01

In this work we present some results about thermoluminescent dating of some archaeological ceramic samples belonging to Chichen Itza, Yucatan, Mexico: CH11, CH13, CH14 and CH15. The analysis was realized using the fine grained mode in a Daybreak model 1100 reader Tl System. The radioisotopes that contribute in the accumulate annual dose in ceramic samples ({sup 40} K, {sup 238} U, {sup 232} Th) were determined by means of techniques such as Energy Dispersive X-ray Spectroscopy (EDS) and Neutron Activation Analysis (NAA), while the artificial irradiation of samples was carried out with a {sup 90} Sr source beta radiation. The resulting mean CH11 ceramic sample was 934 {+-}45 years old, CH13 was 465 {+-} 26, CH14 was 888 {+-} 34 and CH15 was 867 {+-} 42. These results are in agreement with results obtained through other methods. (Author)

Quaternary dating methods

International Nuclear Information System (INIS)

Mahaney, W.C.

1984-01-01

The papers in this book cover absolute, relative and multiple dating methods, and have been written by specialists from a number of different earth sciences disciplines - their common interest being the dating of geological materials within the Quaternary. Papers on absolute dating methods discuss radiocarbon, uranium-series, potassium argon, 40 Ar/ 39 Ar, paleomagnetic, obsidian hydration, thermoluminescence, amino acid racemization, tree rings, and lichenometric techniques. Those on relative dating include discussions on various geomorphic relative age indicators such as drainage density changes, hypsometric integrals, bifurcation ratios, stream junction angles, spur morphology, hillslope geometry, and till sheet characteristics. The papers on multiple dating cite examples from the Rocky Mountains, Australia, Lake Agassiz Basin, and the Southern Andes. Also included is the panel discussion which reviews and assesses the information presented, and a field trip guide which discusses the sequences of Wisconian tills and interlayered lacustrine and fluvial sediments. (orig.)

Thermoluminescent system for low temperatures

International Nuclear Information System (INIS)

Rosa, L.A.R. da; Caldas, L.V.E.; Leite, N.G.

1988-09-01

A system for measurements of the thermoluminescent glow curve, the thermoluminescent emission spectrum and the optical absorption spectrum of solid samples, from liquid nitrogen temperature up to 473 K, is reported. A specially designed temperature programmer provides a linear heating of the sample at a wide range of selectable heating rates, as also long term steady-state temperatures for annealing and isothermal decay studies. The system operates at a pressure of 1.33 x 10 -3 Pa. Presently it is being used for lithium fluoride low temperature thermoluminescent studies. (author) [pt

A survey of archaeological samples dated in 1984

International Nuclear Information System (INIS)

Mejdahl, V.

1985-10-01

A survey is given of archaeological samples dated in 1984 at the Nordic Laboratory for Thermoluminescence Dating. A total of 79 samples were dated, 49 of which were burnt stones. All results were corrected for fading as measured for samples stored for four weeks at room temperature. The alpha dose contribution from uranium in the quartz and feldspar grains was included assuming an alpha efficiency facotr of 0.1 for quartz and 0.2 for feldspars. (author)

Thermoluminescence du quartz naturel et artificiel pur ou dopé des ions Fe++ et Fe+++: application à la datation des poteries

Directory of Open Access Journals (Sweden)

1978-01-01

Full Text Available La thermoluminescence constatée sur les échantillons de poteries et conduisant à la datation archéologique de celles-ci, est due aux inclusions de quartz initialement contenues dans l'argile. Nous présentons une étude de la thermoluminescence d'échantillons de quartz monocristallin synthétique dans lesquels des impuretés ont été volontairement ajoutées et appliquons les résultats à une nouvelle technique de datation, la méthode DATE (différence d'atténuation temporelle des émissions. La termoluminiscencia constatada en muestras de cerámica permite una datación arqueológica es debida a las inclusiones de cuarzo inicialmente contenidas en la arcilla. Se presenta un estudio de la termoluminiscencia de muestras de cuarzo monocristalino sintético en las cuales han sido colocadas voluntariamente impurezas se han aplicado los resultados de una nueva técnica de fechado, el método DATE (Diferencia de atenuación temporal de emisiones. The thermoluminescence observed on samples of pottery and leading to their archaeological dating is a result of the presence of quartz particles originally enclosed in the clay. We offer a study of the termoluminescence of samples of synthetic mono-crystalline quartz doped in with impurities and apply the results to a new dating technique, the 'DATE' method, based upon difference in time attenuation of the emissions.

Nuclear analysis techniques as a component of thermoluminescence dating

Energy Technology Data Exchange (ETDEWEB)

Prescott, J R; Hutton, J T; Habermehl, M A [Adelaide Univ., SA (Australia); Van Moort, J [Tasmania Univ., Sandy Bay, TAS (Australia)

1997-12-31

In luminescence dating, an age is found by first measuring dose accumulated since the event being dated, then dividing by the annual dose rate. Analyses of minor and trace elements performed by nuclear techniques have long formed an essential component of dating. Results from some Australian sites are reported to illustrate the application of nuclear techniques of analysis in this context. In particular, a variety of methods for finding dose rates are compared, an example of a site where radioactive disequilibrium is significant and a brief summary is given of a problem which was not resolved by nuclear techniques. 5 refs., 2 tabs.

Nuclear analysis techniques as a component of thermoluminescence dating

Energy Technology Data Exchange (ETDEWEB)

Prescott, J.R.; Hutton, J.T.; Habermehl, M.A. [Adelaide Univ., SA (Australia); Van Moort, J. [Tasmania Univ., Sandy Bay, TAS (Australia)

1996-12-31

In luminescence dating, an age is found by first measuring dose accumulated since the event being dated, then dividing by the annual dose rate. Analyses of minor and trace elements performed by nuclear techniques have long formed an essential component of dating. Results from some Australian sites are reported to illustrate the application of nuclear techniques of analysis in this context. In particular, a variety of methods for finding dose rates are compared, an example of a site where radioactive disequilibrium is significant and a brief summary is given of a problem which was not resolved by nuclear techniques. 5 refs., 2 tabs.

Preparation of thermoluminescent materials

International Nuclear Information System (INIS)

1976-01-01

Thermoluminescent materials have been found to be suitable for measuring long term exposures to low level ionizing radiation. Oxyhalides of lanthanum, gadolinium and yttrium, including the oxychlorides and oxybromides are activated with terbium and have been found to be most efficient oxygendominated phosphors having thermoradiant efficiencies with excitation by low level ionizing radiation. Thermoluminescence response increases when the previous materials have hafnium and zirconium additives

Thermoluminescence in alkali halides irradiated at 80K; Termoluminiscencia en haluros alcalinos irradiados a 80K

Energy Technology Data Exchange (ETDEWEB)

Jimenez de Castro, M

1978-07-01

The thermoluminescence, the thermally stimulated currents and the thermal stability of the F centres induced in pure NaCl and KC1 crystals by X irradiation at 80K have been studied in detail, In the range between 80 and 300K. The thermoluminescent processes induced by illumination at 80K with F light in samples previously irradiated at room temperature has also been studied. It has been clearly observed the existence of thermoluminescent processes due to electrons and holes thermally released from traps, in which the F centres are not involved. The existence of hole-F centre recombination has not been observed. There are several thermoluminescent processes in both materials which are scribed to the recombination of F centres with mobile interstitial halogen atoms thermally released from traps, which are likely monovalent impurities in this temperature interval. The light emitting stage in these processes is originated by the formation of self trapped excitons. (Author) 66 refs.

Potassium-argon dating: an access to the dynamics and the history of the Planet Earth

International Nuclear Information System (INIS)

Gillot, P.Y.

1993-01-01

Today, scientists, concerned by the history and the evolution of our planet, have a wide range of dating methods. Among these, potassium-argon dating with a field of application that now largely covers that of dating by thermoluminescence or by carbon 14

Selected references on thermoluminescent dosemeters for personnel monitoring

International Nuclear Information System (INIS)

Lawson, Helen

1976-08-01

This bibliography contains references on: specific thermoluminescent dosemeters used for personnel dosimetry; comparisons of thermoluminescent and other dosemeters for personnel monitoring and read-out apparatus for thermoluminescent dosemeters. An appendix contains selected foreign language references. (author)

Thermoluminescence: its understanding and applications

International Nuclear Information System (INIS)

Nambi, K.S.V.

1977-01-01

The phenomenon of thermoluminescence is treated exhaustively both mathematically and physically. All the possible applications of the phenomenon are briefly described and an optimistic picture of the future trends in this field is projected. A review of latest information on thermoluminescence instrumentation and phosphors is also included [pt

New thermoluminescence techniques for mineral exploration

International Nuclear Information System (INIS)

Levy, P.W.; Holmes, R.J.; Ypma, P.J.; Chen, C.C.; Swiderski, H.S.

1977-01-01

The thermoluminescence of carbonate host rock in the vicinity of known lead-zinc and lead-zinc-fluorite mineralization was reexamined for possible development as an exploration technique. The measurements were made with equipment for determining the thermoluminescence spectrum at closely spaced temperature intervals. Radiation-induced thermoluminescence was also measured. Samples were studied from five localities in Mexico, Southwest Africa, and the United States. Four thermoluminescence properties were found to vary with ''distance-from-ore'' in a systematic manner. These include the glow peak intensity and temperature and the emission spectrum peak energy and full width at half-maximum. For example, in both limestone and dolomite, the high-temperature glow peak intensities are low or negligible within the ore and as the distance from the contact increases the intensity rises rapidly to a maximum, or maxima, and then decreases irregularly to constant value slightly above that in the ore. Depending on the thickness of the ore, the thermoluminescence characteristics associated with the mineralization extended from ten to a hundred or so meters from the ore host rock contact. 5 figures

Methods of dating

Energy Technology Data Exchange (ETDEWEB)

Gatty, B

1986-04-01

Scientific methods of dating, born less than thirty years ago, have recently improved tremendously. First the dating principles will be given; then it will be explained how, through natural radioactivity, we can have access to the age of an event or an object; the case of radiocarbon will be especially emphasized. The principle of relative methods such as thermoluminescence or paleomagnetism will also be shortly given. What is the use for dating. The fields of its application are numerous; through these methods, relatively precise ages can be given to the major events which have been keys in the history of universe, life and man; thus, dating is a useful scientific tool in astrophysics, geology, biology, anthropology and archeology. Even if certain ages are still subject to controversies, we can say that these methods have confirmed evolution's continuity, be it on a cosmic, biologic or human scale, where ages are measured in billions, millions or thousands of years respectively.

Physical principles of thermoluminescence and recent developments in its measurement

International Nuclear Information System (INIS)

Levy, P.W.

1974-01-01

The physical principles which are the basis of thermoluminescence techniques for dating and authenticating archaeological and fine art objects are described in non-technical terms. Included is a discussion of the interaction of alpha particles, beta rays, i.e., energetic electrons, and gamma rays with solids, particularly electron-hole ion pair formation, and the trapping of charges by crystal imperfections. Also described is the charge-release process induced by heating and the accompanying emission of luminescence resulting from charge recombination and retrapping. The basic procedure for dating and/or authenticating an artifact is described in a ''how it is done'' manner. Lastly, recently developed apparatus is described for simultaneously measuring luminescent light intensity and wavelength and sample temperature. Examples of studies made with this ''3-D'' apparatus are given and applications to dating and authenticating are described. (U.S.)

Thermoluminescence studies having applications to geology and archaeometry

International Nuclear Information System (INIS)

Levy, P.N.

1978-01-01

Mineral thermoluminescence (TL) studies, undertaken as geophysics investigations, appear to have archaeometric applications. Measurements were made with equipment which records TL emission spectra at closely spaced temperatures. Carbonate rock containing lead-zinc deposits exhibit radiation induced TL against distance-from-ore patterns useful for mineral exploration and locating worked-out deposits. The feldspar albite has second-order TL kinetics, which can introduce dating errors. Heat induced changes in the albite TL emission spectra could be used as a paleotemperature indicator. Quartz remembers previous exposure to radiation, a property influencing TL intensity against dose curves but useful for uranium exploration

Thermoluminescent Signals Caused by Disturbing Effects

International Nuclear Information System (INIS)

German, U.; Weinstein, M.; Ben-Shachar, B.

1999-01-01

One of the major sources of uncertainty in the measurement of low radiation doses by means of thermoluminescence dosemeters is the presence of disturbing thermoluminescence signals, especially luminescence caused by visible light, and by materials attached to the heated areas. Glow curves of thermoluminescence dosemeters contain useful information that can improve the accuracy and the reliability of the thermoluminescent measurements. The influence of the various disturbing effects can be recognised in the shape of the glow curves and can sometimes be separated from the exposure. Some examples are presented of signals arising from the two disturbing effects mentioned above, the signal contributed by Teflon used in the TLD-100 cards of Bicron/Harshaw and some abnormal glow curves due to dirt attached to the cards. Subtraction of the contributions due to these effects is suggested to obtain the net exposure signal. (author)

A survey of archaeological samples dated in 1987

International Nuclear Information System (INIS)

Mejdahl, V.

1988-10-01

A survey is given of archaeological samples dated in 1987 at the Nordic Laboratory for Thermoluminescence Dating. A total of 74 samples were dated. The results were corrected for short-term fading of feldspars as measured for samples stored at room temperature for four weeks or at 100 deg. C for two weeks. The beta dose from potassium and rubidium in feldspar, and the alpha dose from uranium and thorium in quartz and feldspar were included, assuming alpha efficiency factors of 0.1 for quartz and 0.2 for feldspar. (author) 20 tabs., 29 refs

A survey of archaeological samples dated in 1985

International Nuclear Information System (INIS)

Mejdahl, V.

1986-11-01

A survey is given of archaeological samples received for dating in 1985 at the Nordic Laboratory for Thermoluminescence Dating. A total of 66 samples were dated, 42 of which were burnt stones. All results were corrected for short- term fading as measured for samples stored at room temperature for four weeks. The beta dose from potassium and rubidium in feldspar and the alpha dose from uranium and thorium in quarts and feldspar were included assuming alpha efficiency factors of 0.1 for quartz and 0.2 for feldspar. (author)

A survey of archaeological samples dated in 1986

International Nuclear Information System (INIS)

Mejdahl, V.

1987-10-01

A survey is given of archaeological samples dated in 1986 at the Nordic Laboratory for Thermoluminescence Dating. A total of 56 samples were dated. The results were corrected for shortterm fading measured for samples stored for four weeks at room temperature or at 100 deg. C. The beta dose from potassium and rubidium in feldspar and the alpha dose from uranium and thorium in quartz and feldspar grain were included assuming alpha efficiency factors of 0.1 and 0.2 for quartz and feldspar, respectively. 21 refs. (author)

Research of thermoluminescence dating for ancient debris flow materials in Qingshui river basin of Beijing

International Nuclear Information System (INIS)

Liu Junxin; Wei Mingjian; Zhou Rui; Zhang Bin; Liu Tiantian

2012-01-01

The thermoluminescence age of the samples for ancient debris flow terraces material of Lingshan and Hongshuikou, which are in Qingshui River Basin of Beijing, was studied using the thermo luminescence technology. The age increases with the increasing depth of two ancient debris flow profile, and the deeper debris flow deposits material the more of the environmental radiation dose is. The trend with depth of U, Th and K contents and annual dose is consistency. And the change with depth of Th content is more discrete than that of U, K contents. (authors)

Personnel radiation monitoring by thermoluminescence dosimetry (2000-2001)

International Nuclear Information System (INIS)

Mi-Cho-Cho, Daw; Hla-Hla-Win, Daw; Thin-Thin-Kraing

2001-01-01

Thermoluminescence dosimetry service was introduced in 1991. Personnel who exposed directly or indirectly to radiation is monitored by thermoluminescent dosimeter. TL materials used for thermoluminescent dosimeter are in the form of thin disc. Personnel whole-body and extremity doses are measured by thermoluminescence dosimetry. The Harshaw Model 4500 TLD reader and Vinten 654E TLD reader are used for TLD evaluation. At present about 600 radiation workers are provided with TLD for routine monitoring. It was found that most personnel had received within permissible dose recommended by the International Commission on Radiological Protection (ICRP). (author)

A theoretical description of complex thermoluminescence curves: 2

International Nuclear Information System (INIS)

Kantorovich, L.N.; Fogel, G.M.

1989-01-01

Thermoluminescence kinetics is discussed using a model with one type of recombination centre and an arbitrary number of trapping centre types, assuming that electron retrapping is dominant. A distinctive feature of the suggested method is that an integral equation is obtained for the one-time function z(t) through which both the intensity of the thermoluminescence curve (TLC) and the concentration of charge carriers are expressed. Using a series of approximations, which are analysed in detail, analytical solutions of the integral equation are obtained for an arbitrary elementary peak in a complex TLC consisting of a number of slightly overlapping peaks. The comparison of the theoretical results with the numerical ones obtained by the Runge-Kutta method shows that the obtained analytical expression is precise for the first peak and describes the following TLC peaks satisfactorily. The possibility of using the results of the present study for computer division of a complex TLC into elementary components, even in the case of considerably overlapping peaks, is also discussed. (author)

Reactor Gamma Heat Measurements with Calorimeters and Thermoluminescence Dosimeters

DEFF Research Database (Denmark)

Haack, Karsten; Majborn, Benny

1973-01-01

Intercomparison measurements of reactor γ-ray heating were carried out with calorimeters and thermoluminescence dosimeters. Within the measurement uncertainties the two methods yield coincident results. In the actual measurement range thermoluminescence dosimeters are less accurate than calorimet......Intercomparison measurements of reactor γ-ray heating were carried out with calorimeters and thermoluminescence dosimeters. Within the measurement uncertainties the two methods yield coincident results. In the actual measurement range thermoluminescence dosimeters are less accurate than...... calorimeters, but possess advantages such as a small probe size and the possibility of making simultaneous measurements at many different positions. Hence, thermoluminescence dosimeters may constitute a valuable supplement to calorimeters for reactor γ-ray heating measurements....

TL and EPR dating: some applications

Energy Technology Data Exchange (ETDEWEB)

Watanabe, S. [Institute of Physics, University of Sao Paulo, Sao Paulo (Brazil)

2006-07-01

The intensity of thermoluminescence light emitted by a crystal is a function of radiation dose. The number of defects or of radicals in a crystal or organic substances is also a function of radiation dose. Since such defects or radicals present EPR signals, the EPR intensity is also a function of radiation dose. These facts are basis for radiation dosimetry and can be applied in dating of archaeological potteries or other materials, as well as in dating geological substances such as sediments, caves speleothemes, animal teeth and bones. Recent investigation on sensitized quartz based dosimeters and dating calcite covering ancient wall painting to find early settlers in Brazil will be presented. (Author)

Radiation effects in the polycarbonate of bisphenol-A. Thermoluminescence electron spin resonance and charged particle track studies

International Nuclear Information System (INIS)

Edmonds, E.A.

1978-09-01

A detailed investigation is presented of the thermoluminescence observable above room temperature from the polycarbonate of bisphenol-A after its exposure to different radiations. A correlation study is described by which features of the complex thermoluminescence glow curve from a commercial grade of the polycarbonate of bisphenol-A are related to the etchability of charged particle damage trails and the radiogenic ESR signal. A model is presented whereby the etchability of charged particle damage trails is associated with chain scission caused by the high local dose of radiation in the vicinity of the trajectories of charged particles. Methods by which activation constants controlling the thermoluminescence glow curve can be evaluated are discussed and results are presented. It is concluded that glow peaks associated with the ESR signal or enhanced etchability are related to small-scale motions in the molecular matrix of the polycarbonate of bisphenol-A. These motions are thermally activated in accord with the simple Boltzmann relation usually incorporated into theories of thermoluminescence. Another component glow peak of the thermoluminescence glow curve is shown to be associated with the glass-rubber transition in the polycarbonate of bisphenol-A. Different features of the thermoluminescence glow curve can be related to relaxations of the polymer matrix and decomposition of the matrix. It is confirmed that the dominant bulk effect of radiation in the polycarbonate of bisphenol-A exposed to large doses of radiation is chain scission. (author)

Thermoluminescent response of LaAlO3:Pr

International Nuclear Information System (INIS)

Morales H, A.; Zarate M, J.; Azorin N, J.; Rivera M, T.

2015-10-01

In this study, the thermoluminescence response of doped lanthanum aluminate (LaAlO 3 ) with praseodymium ion (Pr) obtained by the Pechini method and drying by the spraying technique Spry Dryer was studied. The obtained powders were analyzed structurally by the X-ray diffraction technique; the morphological characterization was by the scanning electron microscopy technique. The obtained powders at 800 degrees C presented crystallinity and showed a Rhombohedral crystal structure, this phase was observed by X-ray diffraction patterns. Thermoluminescence response of LaAlO 3 :Pr showed a brightness curve with a peak centered at 157 degrees C. The sensitivity of the doped samples was improved about 90 times in comparison with the undoped sample. Thermoluminescence response in function of the wavelength showed a maximum at 230 nm, reproducibility of thermoluminescence response was ±50%. Also the fading in thermoluminescence response was studied. (Author)

A survey of archaeological samples dated in 1988

International Nuclear Information System (INIS)

Mejdahl, V.

1989-08-01

A survey is given of archaeological samples dated in 1988 at the Nordic Laboratory for Thermoluminescence Dating. A total of 67 samples were dated. The results were corrected for short-term fading of feldspars as measured for samples stored at room temperature for four weeks or at 100 deg. C for two weeks. The beta dose from potassium and rubidium in feldspar, and the alpha dose from uranium and thorium in quartz and feldspar were included assuming alpha efficiency factors of 0.1 for quartz and 0.2 for feldspar. (author) 22 tabs., 1 ill., 14 refs

On the second kinetic order thermoluminescent glow curves

International Nuclear Information System (INIS)

Dang Thanh Luong; Nguyen Hao Quang; Hoang Minh Giang

1995-01-01

The kinetic parameters of thermoluminescent material such as CaF 2 -N and CaSO 4 -Dy with the different grain sizes are investigated in detail using the least square method of fitting. It was found that the activation energy E (or trap depth) and peak temperature T m ax are changed with the elapsed time between the irradiation and read-out for the low temperature glow curve peaks. The similar TL glow curve shapes are obtained for the different CaSO 4 -Dy grain size. (author). 7 refs., 5 figs., 2 tabs

Progress in TL Dating at Risø

DEFF Research Database (Denmark)

Mejdahl, V.

1972-01-01

This article outlines the thermoluminescent dating technique employed at Risö. The intensity of beta and gamma radiation is determined by means of the TL phosphors CaSO4:Mn and CaSO4:Dy, and the determination of accumulated exposure is based on quartz and feldspar inclusions with a size of 0.......3–0.5 mm. Results are presented of a dating programme comprising sherds, bricks, burned stones and burned clay (from kilns) from seventeen excavation sites. The age of the sites ranged from a.d. 1600 to 4000 b.c....

Thermoluminescent measurement in space radiation dosimetry

International Nuclear Information System (INIS)

Chen Mei; Qi Zhangnian; Li Xianggao; Huang Zengxin; Jia Xianghong; Wang Genliang

1999-01-01

The author introduced the space radiation environment and the application of thermoluminescent measurement in space radiation dosimetry. Space ionization radiation is charged particles radiation. Space radiation dosimetry was developed for protecting astronauts against space radiation. Thermoluminescent measurement is an excellent method used in the spaceship cabin. Also the authors mentioned the recent works here

Dating of aragonite and dolomite from Devil's cave - SP, by dosimetric thermoluminescent method (DTL) and ESR

International Nuclear Information System (INIS)

Tatumi, S.H.

1987-01-01

We have investigated TL (Thermoluminescence) and ESR (electron spin resonance) properties of aragonite and dolomite found at ''Caverna do Diabo (Devil's cave)'' in the state of Sao Paulo to determine the ages of these geological materials. The aragonite, which is not a thermoluminescent material, shows one ESR signal whit g = 2.003. We obtained the age of 1.1 x 10 5 years and the growth rate of 1 μ m/year by the sample calibration with additional Y irradiation. The dolomite gives a TL glow curve with three distinct peaks at 261, 334 and 395 0 C. We found that the fit for the TL glow curve to second-order kinetics can be considerered as very acceptable. Using the second TL peak we obtained the age of 9.4 x 10 5 years and the compatible values of the activation energy (1.90 ± 0,07 eV) by the following methods: Hyperbolic heating, isothermal decay and fractional glow technique. We observed many ESR absorption signals in the dolomite. Three principal signal com g = 2.002, 2.003 and 2.005 were studied. We found that the first and second ESR signals were atributed to the CO 2 - and/or CO 3 3- centers and the last to the CO 3 - centers, and observed that the first ESR signal might related with the second TL peak and the TL sensitivity were associated with the concentration of Mn 2+ [pt

Dating of archaeological objects using Carbon-14 facilities

International Nuclear Information System (INIS)

Kamisah Hj Alias; Noraishah Othman; Nasasni Nasrol

2004-01-01

Dating is the key to organising all archaeological evidence. Furthermore, the development of dating methods, whether traditional or scientific, illustrates the ingenuity and lateral thinking that make archaeological problem-solving such a fascinating exercise. The development of MINT radiocarbon dating procedures is reviewed. Basic principles and counting techniques are discussed. A sample is converted by chemical methods into a suitable form, such as carbon dioxide followed by the acetylene gas, and the benzene end-product is placed inside a proportional counter to measure the radioactivity of 14 C. Not until some years ago did absolute dates by radiocarbon dating become a reality for prehistoric archaeology in Malaysia where thermoluminescence and fission-track dating had begun to provide a locally applicable dating method some decades earlier. Applications of radiocarbon dating procedures in the fields of archaeology are also discussed. (Author)

Thermoluminescence from natural calcites

International Nuclear Information System (INIS)

Calderon, T.; Jaque, F.; Coy-yll, R.

1984-01-01

Thermoluminescence (TL) as well as absorption and EPR spectra of x-irradiated natural calcites have been obtained. Irradiation produces UV absorption bands and a decrease of the Mn 2+ EPR spectrum. A correlation of each TL peak with the bleaching steps of UV absorption bands and the recovering in intensity of the Mn 2+ EPR spectrum has been found. These experimental results support a new model for the radiation damage and thermoluminescence process in calcites. The main point in this model is that holes become trapped at impurities, and the electrons are trapped at dislocations in the form of CO 3 3- . (author)

Characteristic of 120 degree C thermoluminescence peak of iceland spar

International Nuclear Information System (INIS)

Lu Xinwei; Han Jia

2006-01-01

The basic characteristic of 120 degree C thermoluminescence peak of iceland spar was studied. The experimental result indicates the longevity of 120 degree C thermoluminescence peak of iceland spar is about 2 h under 30 degree C. The thermoluminescence peak moves to the high temperature when the heating speed increasing. The intensity of 120 degree C thermoluminescence peak of iceland spar is directly proportional to radiation dose under 15 Gy. (authors)

Numerical analysis of thermoluminescence glow curves

International Nuclear Information System (INIS)

Gomez Ros, J. M.; Delgado, A.

1989-01-01

This report presents a method for the numerical analysis of complex thermoluminescence glow curves resolving the individual glow peak components. The method employs first order kinetics analytical expressions and is based In a Marquart-Levenberg minimization procedure. A simplified version of this method for thermoluminescence dosimetry (TLD) is also described and specifically developed to operate whit Lithium Fluoride TLD-100. (Author). 36 refs

Personal radiation monitoring with thermoluminescent dosemeters

International Nuclear Information System (INIS)

Miano, S.C.

1987-01-01

The technique of personal dosimetry used by SAPRA (Servico de Assessoria e Protecao Radiologica S/C Ltda., Brazil) is presented. Thermoluminescent monitors and CaSO 4 : Dy are used in pastilles united by teflon. Characteristics of the dosemeters are briefly reported. The system of thermoluminescent measurement, designed and constructed by SAPRA, and the system of personal monitoring are described. (M.A.C.) [pt

Clay as Thermoluminescence Dosemeter in diagnostic Radiology ...

African Journals Online (AJOL)

This paper reports the investigation of the basic thermoluminescence properties of clay at x-rays in the diagnostic radiology range, including dose monitoring in abdominal radiography. Clay sourced from Calabar, Nigeria, was tested for thermoluminescence response after irradiation at diagnostic radiology doses, including ...

Thermal activation and radiation quenching effects in pre-dose dating of porcelain

International Nuclear Information System (INIS)

Wang Weida; Xia Junding

2005-01-01

The pre-dose technique is very useful for thermoluminescence dating of porcelain. It incorporates two characteristics in the porcelain dating, i.e. thermal activation and radiation quenching. Two methods, activation method and quenching method, for evaluation of paleodose were introduced. The results show that activation method and quenching method one suitable for dating of lower limit age (less than 100 years B.P.) and upper limit age (greater than 1000 years B.P.), respectively. When both methods are co-used, the dating will be more accurate. (authors)

Dating of fossil hominid: problems and perspectives

International Nuclear Information System (INIS)

Poupeau, G.; Danon, J.; Baksi, A.K.

1984-01-01

The hominid dating anterior to the Homo Erectus has been based up to now on the rocks and minerals geochronology of vulcanic origem in stratigraphic relation with the fossils. Two methods are widely used, potassium-argon and uranium fission track dating. The vulcanic material dating; lava, lephra, associated with the hominid leavings show big difficults essentially connected to several types of contamination and modification. Two available examples inside the east-african rift show the probelms linked to these dating. The current progresses in the dating methods can contribute by one hand to a better utilization of the K-Ar and fisson track methods for the vulcanic materials. By other hand, with the introduction of new dating methods (thermoluminescence and electron paramagnetic resonance) will be possible to date directly whether the fossil bone itself or the associated sedimentar material. This open new perspectives in particular for every sites which are not inter-stratified with the vulcanic material. (L.C.) [pt

Investigations on low temperature thermoluminescence centres in quartz

International Nuclear Information System (INIS)

Bernhardt, H.

1984-01-01

The present paper will help to understand the often investigated process of thermoluminescence of quartz which is of high complexity. A lot of traps exist in quartz crystals which compete with each other with respect to the trapping of charge carriers during the X-ray treatment. That is why a variety of processes takes place after X-irradiation at liquid nitrogen temperature (LNT) of quartz which complicate the phenomenology of low temperature thermoluminescence. This competition in the trapping process leads to the so-called 'sensibilization' or 'desensibilization' effects of thermoluminescence, respectively, which are described in this paper for the first time. This effect means the dependence of the LNT thermoluminescence intensity on a pre-irradiation dose applied at room temperature (RT). The influence of this pre-irradiation is understood assuming the saturation of competitive traps. This favours an enhanced trapping of charge carriers at LNT-(shallow) traps instead of the preferential trapping on the deep traps in the case of X-ray treatment of the as-grown crystal at LNT. To get the afore mentioned model we take into account not only thermoluminescence but also coloration, ir- and vuv-absorption measurements. (author)

Thermoluminescence of meteorites and their orbits

Science.gov (United States)

Melcher, C. L.

1981-01-01

The thermoluminescence levels of 45 ordinary chondrites are measured in order to provide information on the orbital characteristics of the meteorites before impact. Glow curves of the photon emission response of powdered samples of the meteorites to temperatures up to 550 C in the natural state and following irradiation by a laboratory test dose of 110,000 rad were obtained as functions of terrestrial age and compared to those of samples of the Pribram, Lost City and Innisfree meteorites, for which accurate orbital data is available. The thermoluminescence levels in 40 out of 42 meteorites are found to be similar to those of the three control samples, indicating that the vast majority of ordinary chondrites that survive atmospheric entry have perihelia in the range 0.8-1 AU. Of the remaining two, Farmville is observed to exhibit an unusually large gradient in thermoluminescence levels with sample depth, which may be a result of a temperature gradient arising in a slowly rotating meteorite. Finally, the thermoluminescence measured in the Malakal meteorite is found to be two orders of magnitude lower than control samples, which is best explained by thermal draining by solar heating in an orbit with a perihelion distance of 0.5 to 0.6 AU.

Dental tissue as a thermoluminescence dosimetry dosimeter

International Nuclear Information System (INIS)

Solaimani, F.; Zahmatkesh, M.H.; Akhlaghpoor, Sh.

2003-01-01

Background: Thermoluminescence dosimetry is one of the dosimetry procedures used widely as routine and personal dosimeters. In order to extend this kind of dosimeters, dental tissue has been examined and was found promising as a Thermoluminescence Dosimetry dosimeter. Materials and Methods: In this study, 70 health teeth were collected. The only criterion, wich was considered for selection of the teeth, was the healthiness of them regardless of age and gender of the donors. All collected samples were washed and cleaned and milled uniformly. The final powder had a uniform grain size between 100-300 micrometer. The sample was divided into four groups. Group A and B were used for measurement of density and investigation of variation of thermoluminescent characteristics with temperature respectively. Groups C and D were used for investigation of variation of thermoluminescent intensity with dose and fading of this intensity with time. In all cases the results obtained with dental tissue were compared to a standard LiF, thermoluminescence dosimetry dosimeter. Results: It was found that, average density of the dental tissue was 1.570 g/cm 3 , which is comparable to density of LiF, which is 1.612g/cm 3 . It was also concluded that the range of 0-300 d ig C , dental tissue has a simple curve with two specific peaks at 140 and 25 d ig C respectively. The experiment also showed that, the variation of relative intensity versus dose is linear in the range of 0.04-0.1 Gy. The fading rate of dental tissue is higher than LiF but still in the acceptable range (14% per month in compare to 5.2% per month). Conclusion: Dental tissue as a natural dosimeter is comparable with Thermoluminescence Dosimetry and can be used in accidental events with a good approximation

Thermoluminescence - physics and applications

International Nuclear Information System (INIS)

Sunta, C.M.

1992-01-01

The interaction of ionizing radiations with matter leads to various effects, some of which leave memory in the target material. These memory effects can be seen as the after-effects of the irradiation. Thermoluminescence is one such phenomenon in the insulating solids. This paper describes the sequence of the physical events beginning with the incidence of an ionizing particle, leading to a trail of atomic and electronic displacements which stabilize in the form of so called defect centres. These defects - interstitials, colour centres, etc., store energy in their configuration. Most of the damage effects are reversible. The return of the displaced entities to their original site leads to the release of the stored energy. Thermoluminescence is the result of the re-adjustment (relaxation) of the displaced electrons. The stimulation for the relaxation process is provided by heating of the irradiated sample. The kinetics of the thermoluminescence process has been explained phenomenologically. The correspondence between the defect centres and the TL glow peaks has remained vague or ambiguous even in the most widely studied TL materials. Notwithstanding this deficiency, the phenomenon has found many practical applications. The paper deals mainly with the physical processes involved in the TL emission and alludes briefly to its involvement in applied areas.(author). 6 refs., 2 figs

A theoretical description of complex thermoluminescence curves: Pt. 1

International Nuclear Information System (INIS)

Kantorovich, L.N.; Fogel, G.M.; Gotlib, V.I.

1988-01-01

Thermoluminescence kinetics has been discussed within the framework of a band model assuming an extensive retrapping of charge carriers in comparison with their recombination. Assuming that a luminophor has one type of recombination centre and an arbitrary number of trapping centres we succeeded in analysing complex thermoluminescence curves with an arbitrary number of peaks. It has been shown for an elementary peak that its form almost coincides with the Randall-Wilkins curve, and its intensity is proportional to the square of the absorbed dose. The effect of both the processes of localised charge carriers accumulation (irradiation and isothermal decay) and their redistribution on trapping centres during the thermoluminescence process have been dealt with taking into account the form and intensity of the thermoluminescence peaks. (author)

TELDE thermoluminescent dosimetry system

International Nuclear Information System (INIS)

Shvarts, K.K.; Nemiro, E.A.; Bichev, V.R.; Gotlib, V.I.; Grant, Z.A.; Grube, M.M.; Gubatova, D.J.

1981-01-01

The TELDE dosimetric set designed for measurement of x- and γ- rays doses with energy more than 10 keV is described. The set consists of thermoluminescent detectors from LiF (Ca, Mg, Ti). The detectors are polycrystalline pellets with diameter 3.5+-0.3 mm and thickness 2+-0.2 mm. In the thermoluminescence detectors both the peak and integral measurement methods are realized. Apart from this the TELDE set comprises the electron unit for the pre-irradiation thermal treatment of detectors, special bones for detectors storage and transportation, devices for their package in polyethelene film and containers to wear the detectors. The TELDE set allows to perform measurements on people or animals in radiobiological experiments as well as in water, solid or porous phantoms [ru

Thermoluminescence spectra measured with a Michelson interferometer

International Nuclear Information System (INIS)

Haschberger, P.

1991-01-01

A Michelson interferometer was redesigned to prove its capabilities in the measurement of short-lived, low-intensity thermoluminescence spectra. Interferograms are collected during heating up the thermoluminescent probe in a heater plate. A personal computer controls the data acquisition and processes the Fourier transform. As the results show, even a comparatively simple and limited setup leads to relevant and reproducible spectra. (author)

Absorbed dose from a beta source as shown by thermoluminescence dosimetry

International Nuclear Information System (INIS)

Wintle, A.G.; Aitken, M.J.

1977-01-01

The depth-dose curve was obtained for a 90 Sr- 90 Y beta source using a fine grain TL phosphor to measure the observed dose, aluminium absorbers being interposed between the source and the detector; the curve went through a maximum at an absorber thickness of about 40 mg cm -2 . This curve was then used to predict the average dose rate to various thicknesses of calcium fluoride which has a similar absorption characteristic to aluminium; these values were compared with experimentally determined dose rates. This work was done in connection with thermoluminescence dating of flint and calcite in archaeology and geology. (author)

Luminescence dating in archaeology

International Nuclear Information System (INIS)

Wintle, A.G.

2001-01-01

Thermoluminescence (TL) dating is routinely applied to burnt lithic material. Simple fires are capable of enabling stones weighing a few hundred grams to reach 450 o C, thus zeroing the TL signal. TL dates have been obtained for Upper and Lower Paleolithic sites in Europe and the Near East. TL dating continues to be used for dating pottery and for authentification of ceramic works of art. Some recent studies report the use of optically stimulated luminescence (OSL) (also know as photoluminescence) for dating very small samples of quartz, e.g. from small pieces of pottery or frm metallurgical slag The major recent advance has been in the development of a reliable laboratory procedure for using the OSL signal from quartz to obtain the past radiation exposure. The quartz OSL signal is extremely sensitive to light and is reduced to a negligible level on exposure to direct sunlight for radionuclides during burial, signal to date san.sized quartz grains extracted from sediments, The OSL signal is stimulated by 470 nm light from emitting diodes and the detected using flirters centred on 340 nm A similar signal can be obtained from feldspar grain when are exposed to infrared wavelengths around 880 nm. The infrared stimulated luminescence (IRSL) signals is also rapidly depleted by exposure to sunlight, and dating of colluvial deposits from archaeological sites has been reported

Issues in the reconstruction of environmental doses on the basis of thermoluminescence measurements in the Techa riverside

Science.gov (United States)

Bougrov, N. G.; Goksu, H. Y.; Haskell, E.; Degteva, M. O.; Meckbach, R.; Jacob, P.; Neta, P. I. (Principal Investigator)

1998-01-01

The potential of thermoluminescence measurements of bricks from the contaminated area of the Techa river valley, Southern Urals, Russia, for reconstructing external exposures of affected population groups has been studied. Thermoluminescence dating of background samples was used to evaluate the age of old buildings available on the river banks. The anthropogenic gamma dose accrued in exposed samples is determined by subtracting the natural radiation background dose for the corresponding age from the accumulated dose measured by thermoluminescence. For a site in the upper Techa river region, where the levels of external exposures were extremely high, the depth-dose distribution in bricks and the dependence of accidental dose on the height of the sampling position were determined. For the same site, Monte Carlo simulations of radiation transport were performed for different source configurations corresponding to the situation before and after the construction of a reservoir on the river and evacuation of the population in 1956. A comparison of the results provides an understanding of the features of the measured depth-dose distributions and height dependencies in terms of the source configurations and shows that bricks from the higher sampling positions are likely to have accrued a larger fraction of anthropogenic dose from the time before the construction of the reservoir. The applicability of the thermoluminescent dosimetry method to environmental dose reconstruction in the middle Techa region, where the external exposure was relatively low, was also investigated.

Annual dose measurements and TL-dating of ancient Egyptian pottery

Energy Technology Data Exchange (ETDEWEB)

Abdel-Wahab, M S; El-Fiki, S A; Abdel-Kariem, S; El-Faramawy, N [Ain Shams University, Cairo (Egypt). Faculty of Science; EL-Fiki, M A [National Institute of Standards, Cairo (Egypt); Gomaa, M [Atomic Energy Establishment, Cairo (Egypt). Nuclear Research Center

1996-05-01

In the course of the dating of ancient Egyptian pottery, pottery sherds were collected from three archaeological tombs in Nazlet El Samman region, Giza zone (Egypt). The annual dose from natural background was measured by gamma spectrosocopic technique as well as thermoluminescence (TL) measurements. The results of both methods are in good agreement with a consistency of 99.69%. The extracted quartz exhibited TL dating peaks at about (305 {+-} 5){sup o}C. The TL dating shows an age of 4301 {+-} 100 years for the examined pottery which belongs to the ``Fourth Dynasty`` in the ``OlKingdom`` . The uncertainties in TL dating using the additive method are much lower than that of archaeologists. (author).

Annual dose measurements and TL-dating of ancient Egyptian pottery

Science.gov (United States)

Abdel-Wahab, M. S.; El-Fiki, S. A.; El-Fiki, M. A.; Gomaa, M.; Abdel-Kariem, S.; El-Faramawy, N.

1996-05-01

In the course of the dating of ancient Egyptian pottery, pottery sherds were collected from three archaeological tombs in Nazlet El Samman region, Giza zone (Egypt). The annual dose from natural background was measured by gamma spectroscopic technique as well as thermoluminescence (TL) measurements. The results of both methods are in good agreement with a consistency of 99.69%. The extracted quartz exhibited TL dating peaks at about(305 ± 5|4)°C. The TL dating shows an age of 4301 ± 100 years for the examined pottery which belongs to the "Fourth Dynasty" in the "Old Kingdom". The uncertainties in TL dating using the additive method are much lower than that of archeologists.

Annual dose measurements and TL-dating of ancient Egyptian pottery

International Nuclear Information System (INIS)

Abdel-Wahab, M.S.; El-Fiki, S.A.; Abdel-Kariem, S.; El-Faramawy, N.; Gomaa, M.

1996-01-01

In the course of the dating of ancient Egyptian pottery, pottery sherds were collected from three archaeological tombs in Nazlet El Samman region, Giza zone (Egypt). The annual dose from natural background was measured by gamma spectrosocopic technique as well as thermoluminescence (TL) measurements. The results of both methods are in good agreement with a consistency of 99.69%. The extracted quartz exhibited TL dating peaks at about (305 ± 5) o C. The TL dating shows an age of 4301 ± 100 years for the examined pottery which belongs to the ''Fourth Dynasty'' in the ''OlKingdom'' . The uncertainties in TL dating using the additive method are much lower than that of archaeologists. (author)

Thermoluminescent phosphor

Science.gov (United States)

Lasky, Jerome B.; Moran, Paul R.

1978-01-01

A thermoluminescent phosphor comprising LiF doped with boron and magnesium is produced by diffusion of boron into a conventional LiF phosphor doped with magnesium. Where the boron dopant is made to penetrate only the outer layer of the phosphor, it can be used to detect shallowly penetrating radiation such as tritium beta rays in the presence of a background of more penetrating radiation.

Application of numerical methods in spectroscopy : fitting of the curve of thermoluminescence

International Nuclear Information System (INIS)

RANDRIAMANALINA, S.

1999-01-01

The method of non linear least squares is one of the mathematical tools widely employed in spectroscopy, it is used for the determination of parameters of a model. In other hand, the spline function is among fitting functions that introduce the smallest error. It is used for the calculation of the area under the curve. We present an application of these methods, with the details of the corresponding algorithms, to the fitting of the thermoluminescence curve. [fr

Application of thermoluminescence measurements to detect irradiated strawberries

International Nuclear Information System (INIS)

Heide, L.; Guggenberger, R.; Bogl, K.W.

1990-01-01

The thermoluminescence intensity of unirradiated and irradiated strawberries was studied with regard to dose response, storage time, and different varieties. An identification method could finally be developed. Further investigations were carried out to determine the origin of the thermoluminescence effect, which was found to be attributable to mineral grains adhering to the sample surface

Protocols for Thermoluminescence and Optically Stimulated Luminescence Research at DOSAR

International Nuclear Information System (INIS)

Bernal, SM

2004-01-01

The Life Sciences Division (LSD) of Oak Ridge National Laboratory (ORNL) has a long record of radiation dosimetry research at the Dosimetry Applications Research (DOSAR) facility complex. These facilities have been used by a broad segment of the research community to perform a variety of experiments in areas including, but not limited to, radiobiology, radiation dosimeter and instrumentation development and calibration, and materials testing in a variety of radiation environments. Collaborations with the University of Tennessee-Knoxville (UTK) have also led to important contributions in the area of archaeometry, particularly as it relates to the use of radiation dosimetry to date archaeological artifacts. This manual is to serve as the primary instruction and operation manual for dosimetric and archaeometric research at DOSAR involving thermoluminescence (TL) and optically stimulated luminescence (OSL). Its purpose is to (1) provide protocols for common practices associated with the research, (2) outline the relevant organizational structure, (3) identify the Quality Assurance plan, and (4) describe all the procedures, operations, and responsibilities for safe and proper operation of associated equipment. Each person who performs research at DOSAR using TL/OSL equipment is required to read the latest revision of this manual and be familiar with its contents, and to sign and date the manual's master copy indicating that the manual has been read and understood. The TL/OSL Experimenter is also required to sign the manual after each revision to signify that the changes are understood. Each individual is responsible for completely understanding the proper operation of the TL/OSL equipment used and for following the guidance contained within this manual. The instructions, protocols, and operating procedures in this manual do not replace, supersede, or alter the hazard mitigation controls identified in the Research Safety Summary (''Thermoluminescence/Optically Stimulated

Personnel monitoring of radiations with thermoluminescent dosemeters

International Nuclear Information System (INIS)

Miano, S.C.

1987-01-01

The basics of personnel dosimetry technics, used by the Radiologic Protetion and Assessorie Service (SAPRA) are presented, consisting on use of thermoluminescent and CaSO 4 :Dy monitors in aggregated pellets by Teflon. The characteristics of this dosemeters, relating to the sensitivity, energetic dependence, spike temperature, characteristic emission curve, decay and light effect are shown. The thermoluminescent dosemeter measure system and the personnel monitoring system are also described. (C.G.C.) [pt

TL dating of vases with elephant ears in Yuan Dynasty

International Nuclear Information System (INIS)

Xia Junding; Wang Weida; Leung, P.L.

2005-01-01

Thermoluminescence (TL) dating using an activation method in pre-dose technique was described. Three vases in underglaze blue with elephant ears and one vase in underglaze red with elephant ears in Yuan Dynasty were dated by this method. The results show that the TL ages are all less than 100 a B.P., and in which sbc 648 and sbc 649 were imitated in recent years. This method is quick, convenient and reliable for porcelain dating with the age of less than 1000 a B.P.. As a comparison, a porcelain sample with underglaze blue in Yuan Dynasty was dated too, and its TL age is 620 ± 140 B.P.. In addition, some complex factors associated with dating have been discussed and a resolution has been raised, which will help improve the accuracy of TL dating. (authors)

Dating ancient monuments by nuclear radiation

International Nuclear Information System (INIS)

Goedicke, C.

2000-01-01

In the fifties and sixties several disciplines dealing with chronologies but lacking precise methods of measurements (geology, biology, archaeology and art history) became aware of the radioactive decay as a tool of measuring elapsed time. Among the disciplines that benefit most from physical methods archaeology has to be named first. So was archaeological work revolutionised by the introduction of the C-14 dating method. A wider selection of material became datable after the introduction of luminescence techniques using the effect of nuclear radiation on semiconductors. These minerals are widespread among archaeological materials. In ancient monuments, the objective of this paper, semiconductors almost exclusively form the material basis. Over the last four millennia wood, stone, mortar and fired bricks have been used for the construction of buildings. After discussing methods taking wood as a dating material, a broader view will be given on the results achieved by luminescence dating of fired bricks, mortar and stone. For many years brick dating was performed by thermoluminescence, the recipes followed those of ceramic dating. Preferably multiple aliquot additive dose protocols were used on polymineral fine grain fractions (1-10 μm). It was expected that the error in dating monuments would be smaller compared to ceramic dating, because of the constancy of the environmental conditions which a brick experiences during its lifetime. However, the variability of firing temperatures in brick kilns overthrows this advantage. Therefore, the demands of art historians to fall short of an error margin of 5% could generally not be fulfilled. Especially in medieval or renaissance times the temporal resolution of thermoluminescence is inferior to traditional stylistic dating as long as specific stylistic forms are present. New optical luminescence techniques and a new philosophy of dose evaluation, based on single aliquot regeneration protocols, produce less scatter, and in

Thermoluminescent behavior of diamond thin films exposed to ultraviolet radiation

International Nuclear Information System (INIS)

Barboza F, M.; Gastelum, S.; Melendrez, R.; Chernov, V.; Bernal, R.; Cruz V, C.; Brown, F.

2002-01-01

In this work the thermoluminescent properties of diamond thin films are discussed which are grown up through the chemical vapor method exposed to ultraviolet radiation of 200-280 nm. The films with thickness 3, 6, 9, 12, 180 and 500 microns were grown up using a precursor gas formed of H 2 -CH 4 -CO excited through microwave energy or hot filament.The structure and morphology of the films were examined through scanning electron microscopy, indicating the formation of different diamond polycrystal structures which depend on the type of heating of the precursor gas used as well as the film dimensions. In general, the brilliance curve depends on the sample and the wavelength of the irradiation ultraviolet light, however it presents clearly thermoluminescence bands in 148, 160, 272, 304, 320 and 324 C degrees. The maximum of the thermoluminescence efficiency is obtained for the case of sample exposure with light of 214 nm. The sample of 500 microns is what exhibits greater thermoluminescent efficiency of those studied samples. The thermoluminescent behavior in function of radiation dose presents regions of linearity and supra linearity for higher and small doses respectively. The disappearance of the thermoluminescent signal depends on the characteristics of the film and it can reach until a 30 % of loss before to reach the stability. (Author)

The dating and interpretation of a Mode 1 site in the Luangwa Valley, Zambia

DEFF Research Database (Denmark)

Barham, Lawrence; Phillips, William M.; Maher, Barbara A.

2011-01-01

depositional history of the site prevented the calculation of reliable age models. A relative chronology for the full Manzi sequence was constructed, however, from the magnetostratigraphy of the deposit (N>R>N sequence). Isothermal thermoluminescence (ITL) dating of the upper Mode 3 layers also provided...

Thermoluminescent analysis of archaeological ceramic from Teotenango, Mexico

International Nuclear Information System (INIS)

Dominguez R, R.; Mondragon, M.; Villa S, G.; Gonzalez M, P.R.; Mendoza A, D.

2006-01-01

Of all the kind of artifacts which may be found at archaeological sites, ceramics are surely among the most important. A ceramic material is highly durable, and virtually unchanged after hundred of years from its date of manufacture. Because of this, a ceramic will always be an important object for serious studies to determine which culture produced it, to date cultures, reconstruct economic patterns and social organization, and establish routes of trade or simply to classify the different types of ceramics. The aim of this paper was to perform a thermoluminescent analysis of archaeological ceramic samples belonging to Teotenango, Mexico. The analysis is complemented with a physicochemical characterization by Scanning Electron Microscopy (SEM), Energy Dispersive X-ray Spectroscopy (EDS), X-Ray Diffraction (XRD). TL analysis shows some differences when the samples are exposed to ionizing radiation field, while SEM analysis shows a porous and granular structure in all samples, EDS analysis shows oxygen (O), aluminum (Al), silicon (Si), iron (Fe), sodium (Na), phosphorus (P), potassium (K) and calcium (Ca) in significant amounts. These results allow establishing differences among ceramic samples belonging to the same place. (Author)

Thermoluminescent analysis of archaeological ceramic from Teotenango, Mexico

Energy Technology Data Exchange (ETDEWEB)

Dominguez R, R. [Centro INAH Estado de Mexico, Morelos Ote. 502, Col. San Sebastian, 50090 Toluca, Estado de Mexico (Mexico); Mondragon, M. [Museo Roman Pina Chan, Teotenango 1024 (Mexico); Villa S, G.; Gonzalez M, P.R.; Mendoza A, D. [ININ, 52750 Ocoyoacac, Estado de Mexico (Mexico)

2006-07-01

Of all the kind of artifacts which may be found at archaeological sites, ceramics are surely among the most important. A ceramic material is highly durable, and virtually unchanged after hundred of years from its date of manufacture. Because of this, a ceramic will always be an important object for serious studies to determine which culture produced it, to date cultures, reconstruct economic patterns and social organization, and establish routes of trade or simply to classify the different types of ceramics. The aim of this paper was to perform a thermoluminescent analysis of archaeological ceramic samples belonging to Teotenango, Mexico. The analysis is complemented with a physicochemical characterization by Scanning Electron Microscopy (SEM), Energy Dispersive X-ray Spectroscopy (EDS), X-Ray Diffraction (XRD). TL analysis shows some differences when the samples are exposed to ionizing radiation field, while SEM analysis shows a porous and granular structure in all samples, EDS analysis shows oxygen (O), aluminum (Al), silicon (Si), iron (Fe), sodium (Na), phosphorus (P), potassium (K) and calcium (Ca) in significant amounts. These results allow establishing differences among ceramic samples belonging to the same place. (Author)

Neutron dosimetry using activation of thermoluminescent CaSO 4

Science.gov (United States)

Azorín, Juan; Gutiérrez, Alicia

1984-11-01

Sulfur activation in calcium sulfate doped with dysprosium (CaSO 4:Dy) thermoluminescent powder, which is bound in pure sulfur, has been used to measure the fast neutron dose at the tangential beam port of a Triga Mark III reactor. After a post-irradiation time of 3 d, the dosimeters were annealed at 600°C for 30 min in order to erase all the thermoluminescence acquired during the irradiation. The dosimeters were then stored to allow self-irradiation by betas from 32P produced by sulfur activation. The thermoluminescent signal accumulated during a post-irradiation time of 20 d due to a neutron fluence of 2.2 × 10 11 n/cm 2 was equivalent to an absorbed dose of 10 mGy of 60Co gamma rays. The thermoluminescence as a function of fast neutron dose fitted to a straight line on a log-log scale from 1 Gy to 10 4Gy.

Kerma determination in air on mamma by thermoluminescence

International Nuclear Information System (INIS)

Palacios P, L. L.; Rivera M, T.

2009-10-01

In this work the experimental results of the entrance exposition are shown and Kerma in air [mGy] in mamma obtained by irradiation of accreditation phantom of American College of Radiology (ACR). The irradiations were realized in a conventional mammography equipment of Hospital Juarez in Mexico; the technique used during the irradiations was of automatic exposition; the thickness for the phantom ACR obtained by the technique were of 4.2 and 4.5 cm; the kilo voltage pick was of 24 kV p , the time and the milli amperage per second variable. The measuring of Kerma in air was obtained with thermoluminescent dosemeters of solid state, of nano particles of zirconium dioxide prepared by the precipitation method. The dosemeters were homogenized previously in low energies of X-rays that are those used for mammography. The thermoluminescent dosemeters of ZrO 2 were calibrated by means of an ionization chamber for different expositions. The calibration curve is reported for the exposition and Kerma in air against thermoluminescent intensity obtained by reading of thermoluminescent dosemeters of ZrO 2 , as well as the technique employee for the Kerma determination in air and entrance exposition in mamma. (Author)

ESR dating method and the age determination of Peking-Man

International Nuclear Information System (INIS)

Jin Sizhao; Liang Renyou; Huang Peihua

1991-01-01

ESR dating method and the age determination of the first skull of Zhoukoudian Beijing-Man have been introduced in this paper. Some animal fossil teeth, which are contemporaneous with the Beijing-Man, were used for determination of accumulative dose. The internal and environmental doses of the tooth samples were determined by neutron activation analysis and embeded thermoluminescence dosimeter at the site, respectively. The age of 578 ka of the first skull of Beijing-Man is calculated by the linear uranium accumulation model. According to the ESR dating results, author has given a chronological scale of the cave deposits Loc. 1, Beijing-man site and discussed the mean-life of trapped electron for dating

Authenticity test in ceramics and archaeological figures by thermoluminescence

International Nuclear Information System (INIS)

Ramirez L, A.; Schaaf, P.; Filloy, L.

1999-01-01

At present exists quite a lot of false archaeological pieces which provokes doubts about the legitimacy of the pieces. In this work it is presented the Authenticity test by Thermoluminescence realized at the urn of the goddess 13 serpent of the zapotec culture of Oaxaca which is exposed in Mexico City. The original piece contains crystalline structures which present hardly the thermoluminescence phenomena by the presence of 238 U, 232 Th, and 40 K getting with this the form and intensity of the natural thermoluminescence curve of an archaeological piece which shows a Tl peak and allows to know so if it was made recently or not. (Author)

Towards Luminescence Dating Of Mosaic Glass

Science.gov (United States)

Galli, A.; Martini, M.; Sibila, E.; Villa, I.

The possibility of dating archaeological glass by means of luminescent techniques has been investigated in recent years, despite the difficulties of this application, mainly linked to the amorphous structure of the material. We focused in particular on mosaic glass, after the encouraging results obtained on byzantine and medieval samples. Further studies were devoted to the comprehension of the luminescent mechanisms in silica glasses, and to the investigation of the relationships between luminescence, colouring or opacifier ions and crystalline phase of the vitreous matrix. The results of a study on the dosimetric characteristics of thermoluminescence (TL) and Optically Stimulated Luminescence (OSL) of a few medieval blue-green mosaic glasses from the San Lorenzo church (Milan) are presented, and the experimental protocols established to identify their suitability for dating are discussed.

The influence of thyroid geometry on the response of LiF and CaSO4 thermoluminescent discs to 131I and 125I irradiation

International Nuclear Information System (INIS)

O'Connor, M.K.; Malone, J.F.; Cullen, M.J.

1978-01-01

Recent work has demonstrated that LiF and CaSO 4 thermoluminescent discs may be used to monitor the effective half-life of radioiodine in the thyroid in man. To provide a firm basis for the work, the radiation field presented by model thyroids to thermoluminescent discs on the surface of a neck phantom has been examined in detail. The influence of thyroid mass, depth and lobe separation, factors which in practice are highly variable, has also been determined. The results demonstrate that the method is sufficiently sensitive to measure less than 0.5 μCi of 131 I or 125 I in the human thyroid, and that effective half-life determinations should not be influenced by minor positioning errors which may be encountered when placing thermoluminescent discs on the neck surface. (author)

Thermoluminescence of LiF: Mg, Ti between 77 and 315 K

International Nuclear Information System (INIS)

Rosa, L.A.R. da.

1989-01-01

A special thermoluminescent system was developed. It is able to operate right from liquid nitrogen temperature and also permits the determination of the sample thermoluminescent emission spectrum. Using this system, the thermoluminescence displayed by 77 K irradiated LiF:Mg,Ti (TLD-100), from the irradiation temperature to 315 K, was studied. In this temperature range seven glow peaks, at 139, 153, 194, 240, 260, 283 and 300 K, were determined. (author)

Optical stimulated luminescence (OSL) dating

International Nuclear Information System (INIS)

Banerjee, D.

1999-01-01

Since the pioneering work by Huntley et al. (1985), optical dating is being increasingly recognised as an important technique for establishing a time frame of deposition of sediments (Aitken, 1998). Optical dating differs from thermoluminescence (TL) dating in that visible/infrared light from lasers or LEDs (light-emitting-diodes) is used as a means of stimulation, in contrast to thermal stimulation. It has several advantages over TL dating: (i) the resetting of the OSL (optically stimulated luminescence) clock is more effective than that of TL clock; for sediments transported under water or in other situations where the sediment grains have undergone inhomogeneous bleaching, this property ensures that ages based on optical dating are generally more reliable than TL ages, (ii) the optical dating technique is non-destructive, and multiple readouts of the optical signal is possible; this feature has resulted in the development of single-aliquot and single-grain protocols (Murray and Wintle, 1999; Banerjee et al. 1999), (iii) the sample is not heated as in TL; thus, spurious luminescence is avoided and there is a significant reduction in blackbody radiation. Dating of materials which change phase on heating is also practical, and finally, (iv) thermal quenching of luminescence is negligible, allowing accurate estimation of kinetic parameters using standard techniques and providing access to deep OSL traps. This characteristic may be helpful in extending the limits of optical dating beyond the last 150 ka from a global point of view

Comparison of thermoluminescence detection methods for irradiated spices

International Nuclear Information System (INIS)

Kawamura, Y.; Murayama, M.; Uchiyama, S.; Saito, Y.

1996-01-01

Thermoluminescence (TL) analysis has been shown to be one of the most applicable methods for the detection of γ-irradiated spices. This analysis was introduced as a detection technique for irradiated spices using the whole sample. It was then found that the origin of the TL response to be mineral dust adhering to the spices. TL measurements on separated minerals and the normalised TL measurement by re-irradiation was then established. This paper details investigations on TL measurements carried out using clean powdered spices stored for one year after being irradiated with doses of 1, 5, 10 and 30 kGy in order to clarify their applicable dose range, the effect of storage and mineral content. The effect of the mineral separation was also studied. (author)

The thermoluminescent curve as parameter to compare archaeological ceramics

International Nuclear Information System (INIS)

Dominguez R, I.R.; Ramirez C, G.A.; Gonzalez M, P.R.; Mendoza A, D.; Martinez C, G.

2006-01-01

Most mineral materials, including the constituents of pottery, have the property of thermoluminescence (TL), where part of the energy from radioactive decay in the mineral is stored and later released as light upon strong heating. The intensity of emitted light as a function of temperature is the thermoluminescence glow curve. However, it is well-know the thermoluminescence glow curve form depends of several factors associates with the incident radiation and type of materials. Between the factors associated with the materials, it can be mentioned the quantity and type of crystalline phases, and quantity and type of impurities that they could be present in the material. That is to say, materials with different physicochemical characteristics will produce different thermoluminescence glow curve, although, they have been irradiated under the same conditions. In accordance with the above mentioned, it is possible to identified differences between pre hispanic ceramic belonging to a same site and other sites. In this work a discussion about advantages and disadvantages is presented. Some specific examples in ceramic artifacts belonging to the Matlatzinca and Teotihuacan cultures are included. (Author)

Comparative analysis of dose rates in bricks determined by neutron activation analysis, alpha counting and X-ray fluorescence analysis for the thermoluminescence fine grain dating method

Science.gov (United States)

Bártová, H.; Kučera, J.; Musílek, L.; Trojek, T.

2014-11-01

In order to evaluate the age from the equivalent dose and to obtain an optimized and efficient procedure for thermoluminescence (TL) dating, it is necessary to obtain the values of both the internal and the external dose rates from dated samples and from their environment. The measurements described and compared in this paper refer to bricks from historic buildings and a fine-grain dating method. The external doses are therefore negligible, if the samples are taken from a sufficient depth in the wall. However, both the alpha dose rate and the beta and gamma dose rates must be taken into account in the internal dose. The internal dose rate to fine-grain samples is caused by the concentrations of natural radionuclides 238U, 235U, 232Th and members of their decay chains, and by 40K concentrations. Various methods can be used for determining trace concentrations of these natural radionuclides and their contributions to the dose rate. The dose rate fraction from 238U and 232Th can be calculated, e.g., from the alpha count rate, or from the concentrations of 238U and 232Th, measured by neutron activation analysis (NAA). The dose rate fraction from 40K can be calculated from the concentration of potassium measured, e.g., by X-ray fluorescence analysis (XRF) or by NAA. Alpha counting and XRF are relatively simple and are accessible for an ordinary laboratory. NAA can be considered as a more accurate method, but it is more demanding regarding time and costs, since it needs a nuclear reactor as a neutron source. A comparison of these methods allows us to decide whether the time- and cost-saving simpler techniques introduce uncertainty that is still acceptable.

Dating stalagmite from Caverna do Diabo (Devil´S Cave by TL and EPR techniques

Directory of Open Access Journals (Sweden)

SHIGUEO WATANABE

Full Text Available ABSTRACT A cylindrical fragment of stalagmite from Caverna do Diabo, State of São Paulo, Brazil, has been studied and dated by thermoluminescence and electron paramagnetic resonance techniques. The thermoluminescence glow curves of stalagmite samples and subsequently gamma irradiated, have shown rise of three peaks at 135, 180 and 265 °C. From electron paramagnetic resonance spectra of stalagmite was possible to clearly identify three paramagnetic centers in the g = 2.0 region: Centers I, II and III are due to , and , respectively. The additive method was applied to calculate the accumulated dose using thermoluminescence peak at 265 °C and the electron paramagnetic resonance signal at g = 1.9973 of CO- 2 radical. The ages of the different slices of stalagmite were determined from the Dac- values and Dan- value, obtaining an average of 86410 for central slice, 53421 for second slice, 31490 for third slice and 46390 years B.P. for the central region of upper end.

Thermoluminescence of zirconium oxide nanostructured to mammography X-ray beams

International Nuclear Information System (INIS)

Palacios, L.L.; Rivera, T.; Roman, J.; Azorín, J.; Gaona, E.

2012-01-01

In the present work thermoluminescent (TL) response of zirconium oxide (ZrO 2 ) nanostructured induced by mammography X-ray radiation was investigated. Measurements were made of the response per unit air kerma of ZrO 2 with mammography equipment parameters (semiautomatic exposure control, 24 kVp and 108 mAs). The calibration curves were obtained by simultaneously irradiating ZrO 2 samples and ion chamber. Samples of ZrO 2 showed a linear response as a function of entrance skin air kerma. The observed results in TL properties suggest that ZrO 2 nanostructured could be considered as an effective material for X-ray beams dosimetry if appropriate calibration procedures are performed. - Highlights: ► X-ray low energy thermoluminescent of ZrO 2 dosimeter is developed. ► Air kerma measurements were made by thermoluminescent dosimeter ZrO 2 using mammography equipment parameters. ► Entrance surface skin doses were made using thermoluminescent dosimeter of ZrO 2 to X-ray beam quality control.

Effect of pre-dose irradiation in the quartz and its use for archaelogical dating

International Nuclear Information System (INIS)

Yukimitu, K.

1985-01-01

The technique of pre-dose for dating ceramics, using the thermoluminescent properties of quartz is presented. The behavior of thermoluminescent (TL) sensitivity of the 110 0 C peak of Brazilian quartz, in its geologic state, submitted to thermal treatments from 600 to 900 0 C, is studied. The samples were tritured for separating the quartz crystals from clay. The quartz grains were submitted to leaching with chloric acid solution followed by leaching with running water. The samples were irradiated in laboratory, with gamma radiation using Co-60 and Cs-137 sources, for calibration. A sensitivity enhancement rate of 2% per rad was observed for samples annealed at 900 0 C, was observed. (M.C.K.) [pt

Thermoluminescence dosimetry in Northwest Puerto Rico

International Nuclear Information System (INIS)

Block, A.M.; Clements, R.G.; Rosa, L.I.; Santos, F.

1975-01-01

In October, 1973, the Puerto Rico Water Resources Authority sought the initiation of studies aimed at determining background radiological characteristics of the northwestern quadrant of Puerto Rico using thermoluminescent dosemeters. Some of the studies were required for supporting data for the environmental report submitted as part of the licensing procedure in the establishment of thermonuclear electric power generation facilities in Barrio Islote, Arecibo, Puerto Rico. Previous studies of radiological characteristics of the area had been made using sodium iodide sensing equipment in an airplane flying at an altitude of 500 ft. The results are expressed in counts per second, and provide useful comparative levels for radioactivity measured with the thermoluminescent detectors. (U.S.)

Ceramics baking temperature influence on the dosimetric parameters essential in TL dating

International Nuclear Information System (INIS)

Krumpschmid, K.R.

1986-11-01

Thermoluminescence in quartz is used for dating of ceramics. The main problem is the 'intercept', i.e. the deviation from linearity in the relationship thermoluminescence versus absorbed dose of natural radiation. This deviation is most probably dependent on the fabrication method of the ceramics. In the present work the hypothesis is tested that the most important parameter, in this respect, is the baking temperature. Four types of ceramic bricks were fabricated, with four burning cycles of end temperatures of 550 0 C, 650 0 C, 900 0 C and 1200 0 C respectively, then irradiated and finally underwent the TL-procedure. The results are discussed with regard of the maximum of glow curve, intensity, fading, sensitivity to beta radiation and to additional alpha radiation and the intercept. (qui)

Dose measurements in dental radiology using thermoluminescent dosimetry

International Nuclear Information System (INIS)

Chiara, Ana Claudia M. de; Costa, Alessandro M.; Pardini, Luiz Carlos

2009-01-01

The aim of this work was the implementation of a code of practice for dosimetry in dental radiology using the technique of thermoluminescent dosimetry. General principles for the use of thermoluminescent dosimeters were followed. The irradiations were performed using ten X-ray equipment for intra-oral radiography and an X-ray equipment for panoramic radiography. The incident air kerma was evaluated for five different exposure times used in clinical practice for intra-oral radiographs. Using a backscatter factor of 1.2, it was observed that approximately 40% of the entrance skin dose values found for intra-oral radiographs are above the diagnostic reference level recommended in national regulation. Different configurations of voltage and current were used representing the exposure as a child, woman and man for panoramic radiographs. The results obtained for the air kerma area product were respectively 53.3 +- 5.2 mGy.cm 2 , 101.5 +- 9.5 mGy.cm 2 and 116.8 +- 10.4 mGy.cm 2 . The use of thermoluminescent dosimetry requires several procedures before a result is recorded. The use of dosimeters with ionization chambers or semiconductors provides a simple and robust method for routine measurements. However, the use of thermoluminescent dosimetry can be of great value to large-scale surveys to establish diagnostic reference levels. (author)

Obtention of a thermoluminescent material for dosimetry of ionizing radiation

International Nuclear Information System (INIS)

Gonzalez M, P.R.

1990-01-01

The thermoluminescent dosemeters are small crystals which suffer changes in their structure by the radiation effect, being displaced the electrons toward higher energy levels. On heating the previously irradiated crystals, the electrons come back to their base state emitting light photons. The light quantity emitted is proportional to the received radiation dose. The light quantity emitted is proportional to the received radiation dose. The lithium fluoride is one of the thermoluminescent materials considered as tissue equivalents by having a low effective atomic number (Z ef ). At present, the more used commercial product used of this type is the TLD-100*. In this work the obtained results in the preparation of the lithium fluoride thermoluminescent material are presented. This is activated with magnesium (Mg) and titanium (Ti), which we have labelled as: LiF: Mg, Ti. The results from the tests performed for verifying his thermoluminescent properties are presented too, as powder form as in pellets form. These tests were performed in simultaneous form with TLD-100 samples, which is considered as reference. The LiF: Mg, Ti thermoluminescent material manufactured in the ININ presents similar dosimetric characteristics to those ones of the TLD-100. Therefore being able to replace the imported dosemeters. * (TLD-100 is a commercial trademark registered by Harshaw/Filtrol (US) for LiF: Mg, Ti Tl dosemeters) (Author)

Auto-regenerative TL dating with zircon inclusions from fired materials

International Nuclear Information System (INIS)

Templer, R.H.; Smith, B.W.

1988-01-01

In this paper it is shown that it is possible to date fired material using zircon inclusions. The effects of zoning and anomalous fading are overcome using an auto-regenerative dating procedure. The high radioactivity of the grains gives a measurable self-induced TL (thermoluminescence) signal within a few months. Comparison of this ''auto-regenerated'' TL with the natural TL (which has accumulated since the firing) yields the age of the material. A sensitive TL reader capable of recording the auto-regenerated signal after 6 months is also described, and the results of age determinations on a number of known age samples are presented. (author)

Dating and characterization of archaeological ceramics of the Araruama area at Rio de Janeiro, Brazil

International Nuclear Information System (INIS)

Vinagre Filho, Ubirajara M.; Bellido, Alfredo V.B.; Latini, Rose M.; Rossi, Alexandre M.

2000-01-01

Ceramic of three archaeological sites (Serrano, Morro Grande, and condominium Bela Vista) of the Araruama area (Rio de Janeiro/Brazil), are being dated by the thermoluminescence technique. These ceramics are being characterized, in your elementary chemical composition, by INAA. Preliminary results are presented and the samples treatment method is described. (author)

CaSO4: Dy + Teflon thermoluminescent dosemeters

International Nuclear Information System (INIS)

Campos, L.L.

1986-01-01

A pellet dosemeter of CaSO 4 : Dy + Teflon was developed at IPEN. CaSO 4 : Dy thermoluminescent phosphor, grown in the Dosimetric Materials Production Laboratory was chosen, due to its high sensitivity, ease of preparation and comparatively low cost. Pellets were produced by cold pressing and sintering a mixture of CaSO 4 : Dy and Teflon powders. Extensive work was done to study in detail all CaSO 4 : Dy pellets characteristics from the point of view of dosimetry with the purpose of introducing it in the routine use. A filter combination providing an energy independent response from 20 KeV to 1,25 MeV was obtained. The dosemeter consists of three pellets sealed between two thin plastic sheets and placed under plastic and lead filters. The combination of these tree filters allows the exposure as well as the energy determination of an unknown source. (Author) [pt

Thermoluminescence of zirconium oxide nanostructured to mammography X-ray beams

Energy Technology Data Exchange (ETDEWEB)

Palacios, L.L. [Centro de Investigacion en Ciencia Aplicada y Tecnologia Avanzada-Legaria, IPN. Av. Legaria 694, 11500 Mexico D.F. (Mexico); Rivera, T., E-mail: trivera@ipn.mx [Centro de Investigacion en Ciencia Aplicada y Tecnologia Avanzada-Legaria, IPN. Av. Legaria 694, 11500 Mexico D.F. (Mexico); Roman, J. [Centro de Investigacion en Ciencia Aplicada y Tecnologia Avanzada-Legaria, IPN. Av. Legaria 694, 11500 Mexico D.F. (Mexico); Azorin, J. [Universidad Autonoma Metropolitana-Iztapalapa. Av. San Rafael Atlixco 187, 09340 Mexico D.F. (Mexico); Gaona, E. [Universidad Autonoma Metropolitana-Xochimilco. Calz. Del Hueso 1100, 04960 Mexico D.F. (Mexico)

2012-07-15

In the present work thermoluminescent (TL) response of zirconium oxide (ZrO{sub 2}) nanostructured induced by mammography X-ray radiation was investigated. Measurements were made of the response per unit air kerma of ZrO{sub 2} with mammography equipment parameters (semiautomatic exposure control, 24 kVp and 108 mAs). The calibration curves were obtained by simultaneously irradiating ZrO{sub 2} samples and ion chamber. Samples of ZrO{sub 2} showed a linear response as a function of entrance skin air kerma. The observed results in TL properties suggest that ZrO{sub 2} nanostructured could be considered as an effective material for X-ray beams dosimetry if appropriate calibration procedures are performed. - Highlights: Black-Right-Pointing-Pointer X-ray low energy thermoluminescent of ZrO{sub 2} dosimeter is developed. Black-Right-Pointing-Pointer Air kerma measurements were made by thermoluminescent dosimeter ZrO{sub 2} using mammography equipment parameters. Black-Right-Pointing-Pointer Entrance surface skin doses were made using thermoluminescent dosimeter of ZrO{sub 2} to X-ray beam quality control.

Thermoluminescence properties of Yb-Tb-doped SiO2 optical fiber subject to 6 and 10 MV photon irradiation

Science.gov (United States)

Sahini, M. H.; Wagiran, H.; Hossain, I.; Saeed, M. A.; Ali, H.

2014-08-01

This paper reports thermoluminescence characteristics of thermoluminescence dosimetry 100 chips and Yb-Tb-doped optical fibers irradiated with 6 and 10 MV photons. Thermoluminescence response of both dosimeters increases over a wide photon dose range from 0.5 to 4 Gy. Yb-Tb-doped optical fibers demonstrate useful thermoluminescence properties and represent a good candidate for thermoluminescence dosimetry application with ionizing radiation. The results of this fiber have been compared with those of commercially available standard thermoluminescence dosimetry-100 media. Commercially available Yb-Tb-doped optical fibers and said standard media are found to yield a linear relationship between dose- and thermoluminescence signal, although Yb-Tb-doped optical fibers provide only 10 % of the sensitivity of thermoluminescence dosimetry-100. With better thermoluminescence characteristics such as small size (125 μm diameter), high flexibility, easy of handling and low cost, as compared to other thermoluminescence materials, indicate that commercial Yb-Tb-doped optical fiber is a promising thermoluminescence material for variety of applications.

Some thermoluminescence ages in Queensland: a problem resolved

International Nuclear Information System (INIS)

Prescott, J.R.

1997-01-01

In a previous paper (Tejan-Kella et al Aust J. Soil Res. 28, 465, 1990), thermoluminescence (TL) dates were presented for a soil horizon at five sites in a chronosequence of freely-drained podzols at Cooloola and North Stradbroke Island, Queensland. The TL ages followed the expected order based on geomorphological evidence; and the TL age of 120 ±11 ka for the Amity dune on North Stradbroke Island agreed with uranium series dates for underlying coral recovered during sand mining. Nevertheless, several features of the TL results gave rise to some concern and were noted in the above mentioned paper. Specifically, the apparent TL age of 11 ± 2 ka for the Kings Bore site was widely at variance with the inferred age of about 0.5 ka based on geomorphological and soil profile evidence. Further, an apparent TL age of about 8 ka was found for samples from the Carlo sand blow. The Carlo samples were taken at mean depths of 1.0 m and 1.5 m from within the advancing toe of the dune, which is obviously mobile since it is encroaching on living vegetation. The time since last exposure to sunlight could scarcely exceed a decade. New measurements are reported, designed to resolve the former discrepancies. All sites have been re-dated, together with a new one, CA5S/1 (Chalambar) and a reduced value have been obtained. The fact that the TL age is somehow smaller than the U-series age may reflect the expectation that the summit of the dune be younger than the base

Sediment dating in review

International Nuclear Information System (INIS)

Prescott, J.R.; Robertson, G.B.

1997-01-01

The paper will comment on a few issues of particular relevance to Australasia. Thermoluminescent (TL) methods applied to open sites have been demonstrated to be effective. A particularly good example of this is to be found in the South East of South Australia, where a sequence of low ranges runs roughly parallel with the coast. They represent relict sand dunes left behind, on a slowly rising land surface by successive interglacial incursions of the sea at roughly 120 ka intervals. Comparison with ages established on independent geological grounds allows a test of quartz TL and IRSL ages that is believable back to 500 ka. Older than this, we do not yet understand the physics of the quartz well enough to go unequivocally forward (backward?). Similar results are emerging elsewhere. With dating limits being pushed ever further back, the time variation of the environmental radiation giving rise to the stored luminescent energy needs to be addressed. Particularly at wet sites, radioactive disequilibrium must be considered. In any case, a time profile of the radiation dose rate needs to be determined.In dating a given site or sites the value of ages obtained by any dating method,including C-14, is enhanced by parallel measurements with an different method

Radiation induced defects and thermoluminescence mechanism in aluminum oxide

Energy Technology Data Exchange (ETDEWEB)

Atobe, K.; Kobayashi, T.; Awata, T. [Naruto Univ. of Education, Tokushima (Japan); Okada, M. [Kyoto Univ., Kumatori, Osaka (Japan). Research Reactor Inst; Nakagawa, M. [Kagawa Univ., Faculty of Education, Takamatsu, Kagawa (Japan)

2001-01-01

The thermoluminescence of the irradiated aluminum oxides were measured to study the radiation induced defects and their behaviors. Neutron and {gamma}-ray irradiation were performed for a shingle crystal of the high purity aluminum oxide. The thermoluminescence glow curve and its activation energy were measured. The spectroscopy measurement on the thermoluminescence and the absorption are also carried out. The observed 430 and 340 nm peaks are discussed relating to the F{sup +} and F centers, respectively. Activation state of the F center transits to 3P state through 1P state by emitting phonons. Trapped electron on 3P state emits phonon of 2.9 eV (430 nm) during transition to the ground state. The above reaction can be written by the equation. F{sup +} + e {yields} (F){sup *} {yields} F + h{nu}(2.9 eV, 470 nm). (Katsuta, H.)

Thermoluminescence of films of metal oxides and its application to the low energy ionizing radiation dosimetry

International Nuclear Information System (INIS)

Azorin N, J.; Rivera M, T.; Furetta, C.; Falcony G, C.; Martinez S, E.; Garcia H, M.

2002-01-01

The obtained results from 1997 to date in the project S tudy of the thermoluminescence of metal oxides and their application to the ionizing radiation as regards to the development of ZrO 2 and of Al 2 O 3 doped and without doped films with rare earths are presented. The obtained results irradiating ZrO 2 and of Al 2 O 3 films with ultraviolet light and visible light have been satisfactory; whereas these materials have resulted promising to measure beta particles, X-rays and low energy gamma rays. (Author)

Dose-rate dependence of thermoluminescence response

International Nuclear Information System (INIS)

McKeever, S.W.S.; Chen, R.; Groom, P.J.; Durrani, S.A.

1980-01-01

The previously observed dose-rate effect of thermoluminescence in quartz at high dose-rates is given at theoretical formulation. Computer calculations simulating the experimental conditions yield similar results to the experimental ones. (orig.)

Study of some thermoluminescent phosphors for the dosimetry of ionizing radiations

International Nuclear Information System (INIS)

Jaafari, M.

1983-01-01

Thermoluminescence dosimetry techniques are reviewed and interactions radiation matter are recalled. The need for new phosphors is evidenced. Numerous phosphors are examined and calcium, strontium and barium sulfides are synthetized and deposited on glass supports. The thermoluminescence of the dosimeters obtained with these materials is analyzed [fr

Thermoluminescence properties of micro and nano structure hydroxyapatite after gamma irradiation

Energy Technology Data Exchange (ETDEWEB)

Shafaei, Mostafa; Ziaie, Farhood; Hajiloo, Nahid [Nuclear Science and Technology Research Institute, Tehran (Iran, Islamic Republic of). Radiation Application Research School

2016-12-15

The goal of this study is to compare the thermoluminescence properties of nano and micro structure hydroxyapatite. Nano structure hydroxyapatite was synthesized via hydrolysis method, while the micro structure one was from Merck Company. X-ray diffraction and fourier transform infrared spectroscopy were used to determine the crystal structure and chemical composition of the hydroxyapatite samples. Particles sizes of each sample were estimated using Scherer equation and transmission electron microscopy system. Thermoluminescence properties of the samples were investigated under gamma irradiation. The glow curves of micro and nano structure samples show a peak at 150 C and 200 C, respectively. Thermoluminescence responses of both the samples were linear in the range of 25 - 1 000 Gy where, nano structure sample show a greater slope and stronger linearity in comparison to the micro sample. The results show that the thermoluminescence response of micro sample faded rapidly in comparison to the nano sample due to the existence of the peak at higher temperature.

Thermoluminescence sensitivity variations in LiF PTFE dosemeters incurred by improper handling procedures

CERN Document Server

Mason, E W; MacKinlay, Alistair F; Saunders, D

1975-01-01

A systematic study of some anomalous darkening effects and thermoluminescence sensitivity variations observed in LiF:PTFE thermoluminescent dosemeters is described. Various likely causes of such effects have been investigated. The manufacturer's recommended cleaning procedures have been found to be inadequate and, in some cases, have been found to actually promote discolouration of the dosemeters. Recommendations are given for the successful use of LiF:PTFE thermoluminescent dosemeters in personal dosimetry.

Thermoluminescence of strontium tetraborate

International Nuclear Information System (INIS)

Santiago, M.; Caselli, E.; Lester, M.

1999-01-01

The thermoluminescent properties of crystalline strontium tetraborate are reported. Without activators it has an efficiency comparable to that of TLD-700 powder. Its fading after 40 days amount to less than 2%. The isometric plot shows that most of the emitted light is concentrated at wavelengths ranging from 350 to 450 nm, which accounts partially for the high efficiency. (author)

An improved approach to identify irradiated dog feed by electron paramagnetic resonance study and thermoluminescence measurements

International Nuclear Information System (INIS)

Sanyal, Bhaskar; Chawla, S.P.; Sharma, Arun

2011-01-01

In the present study, probably for the first time, a detailed analysis of the radiation induced radical species and thermoluminescence measurements of irradiated dog feed are reported. The EPR spectrum of non-irradiated ready-to-eat dog feed was characterized by singlet g=2.0047±0.0003. Irradiated samples exhibited a complex EPR spectrum. During high power (50.0 mW) EPR spectroscopy, a visible change in the shape of the EPR spectrum was observed and characterized by EPR spectrum simulation technique. An axially symmetric anisotropic signal with g || =2.0028 and g perpendicular =1.9976 was identified. However, a negligible change in the matrix of irradiated edible dog chew was observed using EPR spectroscopy. Therefore, thermoluminescence study of the isolated minerals from dog chew was carried out. The composition of the poly-minerals was studied using SEM and EDX analysis and a complete verdict on identification of irradiation is proposed.

An improved approach to identify irradiated dog feed by electron paramagnetic resonance study and thermoluminescence measurements

Energy Technology Data Exchange (ETDEWEB)

Sanyal, Bhaskar, E-mail: bhaskar_sanyal@rediffmail.co [Food Technology Division, Bhabha Atomic Research Centre, Mumbai-400 085 (India); Chawla, S.P.; Sharma, Arun [Food Technology Division, Bhabha Atomic Research Centre, Mumbai-400 085 (India)

2011-05-15

In the present study, probably for the first time, a detailed analysis of the radiation induced radical species and thermoluminescence measurements of irradiated dog feed are reported. The EPR spectrum of non-irradiated ready-to-eat dog feed was characterized by singlet g=2.0047{+-}0.0003. Irradiated samples exhibited a complex EPR spectrum. During high power (50.0 mW) EPR spectroscopy, a visible change in the shape of the EPR spectrum was observed and characterized by EPR spectrum simulation technique. An axially symmetric anisotropic signal with g{sub ||}=2.0028 and g{sub perpendicular}=1.9976 was identified. However, a negligible change in the matrix of irradiated edible dog chew was observed using EPR spectroscopy. Therefore, thermoluminescence study of the isolated minerals from dog chew was carried out. The composition of the poly-minerals was studied using SEM and EDX analysis and a complete verdict on identification of irradiation is proposed.

Variation in thermoluminescence of irradiated brands of foodstuffs: a test for hygienic quality

International Nuclear Information System (INIS)

Mamoon, A.; Zaheer, A.; Abu-Abdullah, S.

1996-01-01

Thermoluminescence of irradiated foodstuffs such as herbs and spices, is mostly due to attached dust or soil particles. Different brands of the same foodstuff sometimes give thermoluminescent signals of different intensities, apparently due to different degrees of dust contamination. It is of obvious importance to choose brands of foodstuffs that appear to have less dust contamination, i.e. of better hygienic quality. Several food items were investigated with respect to their thermoluminescent (TL) emission in order to assess TL usefulness as an indicator of hygienic quality for foods prone to contamination by dust. In this regard some foodstuff were artificially contaminated with a soil sample and their thermoluminescent emission was obtained. (author)

Thermoluminescence of Zn O thin films deposited by chemical bath

International Nuclear Information System (INIS)

Camacho A, M. C.; Cruz V, C.; Bernal H, R.; Berman M, D.; Castano M, V. M.

2015-10-01

Full text: Zn O films on Si were synthesized using a deposition method by chemical bath and thermally treated at 900 degrees C for 12 h in air. The morphological characterization by scanning electron microscopy reveals that uniform films were obtained. To investigate the thermoluminescent properties of the films were exposed to irradiation with beta particles with doses in the range from 0.5 to 128 Gy. The brightness curves obtained using a heating rate of 5 degrees C have two peaks, one at 124 and another at 270 degrees C, and a linear dependence of the integrated thermoluminescence as a function of dose. The second maximum reveals the existence of localized trapping states of potential utility in thermoluminescent dosimetry. (Author)

Thermoluminescent response of LiF before variation of the heating rate

International Nuclear Information System (INIS)

Barrios, R.; Avila, O.

2003-01-01

Comparisons of glow curves of lithium fluoride dosemeters TLD-100 measured to two heating rates with the purpose of quantifying the change in the temperature of the peaks 5 and 7 for the thermoluminescent reader equipment Harshaw 4000 of the thermoluminescence laboratory of the ININ were carried out. (Author)

Thermoluminescence of LaAlO{sub 3}; Termoluminescencia de LaAlO{sub 3}:Dy

Energy Technology Data Exchange (ETDEWEB)

Morales H, A.; Zarate M, J. [Universidad Michoacana de San Nicolas de Hidalgo, Instituto de Investigacion en Metalurgia y Materiales, Ciudad Universitaria, Edif. U, 58060 Morelia, Michoacan (Mexico); Rivera M, T. [IPN, Centro de Investigacion en Ciencia Aplicada y Tecnologia Avanzada, Av. Legaria 694, 11500 Mexico D. F. (Mexico); Azorin N, J., E-mail: feyo_yo@hotmail.com [Universidad Autonoma Metropolitana, Unidad Iztapalapa, Av. San Rafael Atlixco 186, Col. Vicentina, 09340 Mexico D. F. (Mexico)

2015-10-15

In this paper the thermoluminescent properties of doped lanthanum aluminate (LaAlO{sub 3}) with dysprosium ion (Dy) were studied. The thermoluminescence characteristics in the samples were obtained using an ultraviolet radiation of 220 nm. The LaAlO{sub 3}:Dy samples were prepared by the modified Pechini method (Spray Dryer). The structural and morphological characterization was obtained by X-ray diffraction (XRD) and scanning electron microscopy (Sem) techniques respectively. The size particle composing the agglomerate was determined by Sem, agglomerated particles composed size of 2μm were observed. The thermoluminescence response of LaAlO{sub 3}:Dy was compared with that obtained with the undoped sample. Thermoluminescence brightness curves of LaAlO{sub 3}:Dy showed a peak centered at 185 grades C. Sensitivity of doped sample was greater, about 100 times compared with the undoped sample. Thermoluminescence response in function of the wavelength showed a maximum at 220 nm. Also the fading in thermoluminescence response was studied. (Author)

Food irradiation dosimetry using thermoluminescence of quartz sand

International Nuclear Information System (INIS)

Khan, H.M.; Ehlermann, D.A.E.

1993-01-01

Thermoluminescence of quartz sand, which is inert and concomitant to several food materials, has been investigated for applications in food irradiation dosimetry and detection of irradiated foods. The glow curves consist of at least three overlapping peaks from 100 to 420 C. The peak at lower temperature is not stable and decays quickly at room temperature. However, the peaks at higher temperature are stable and more useful for dosimetry work. The intensity of the peak at 360 C, measured using different optical filters, shows a linear response in the range of 0.05 to 23 kGy. Stability of these signals at different annealing temperatures has been investigated. Thermoluminescence from adhering minerals and contaminating dust in different food materials has been found useful for the detection of irradiation treatment. Since quartz is frequently one of these minerals, further computerized deconvolution of individual glow peaks from the complex glow curves of quartz sand was carried out which improves the dosimetric results. Possible applications of thermoluminescence of quartz sand in food irradiation dosimetry and detection of irradiated foods have been discussed. (orig.)

New color-photographic observation of thermoluminescence from sliced rock samples

International Nuclear Information System (INIS)

Hashimoto, Tetsuo; Kimura, Kenichi; Koyanagi, Akira; Takahashi, Kuniaki; Sotobayashi, Takeshi

1983-01-01

New observation technique has been established for the thermoluminescence photography using extremely high-sensitive color films. Considering future application to the geological fields, a granite was selected as a testing material. The sliced specimens (0.5--0.7 mm in thickness), which were irradiated with a 60 Co source, were mounted on the heater attached with a thermocouple, which was connected to a microcomputer for measuring the temperature. The samples were heated in the temperature range of 80--400 0 C by operating the camera-shutter controlled with the microcomputer. Four commercially available films (Kodak-1000(ASA), -400, Sakura-400, Fuji-400) could give apparently detectable color-images of artificial thermoluminescence above a total absorbed dose of 880 Gy(88 krad). The specimens, irradiated upto 8.4 kGy(840krad), allowed easily to distinguish the distinct appearance of the thermoluminescence images depending on kinds of white mineral constituents. Moreover, such color images were changeable with the heating temperature. Sakura-400 film has proved the most colorful images from aspects of color tone although Kodak-1000 film showed the highest sensitivity. By applying this Kodak-1000, it was found that the characteristic color image due to natural thermoluminescence was significantly observed on the Precambrian granite which was exposed with natural radiation alone since its formation. This simple and interesting technique, obtainable surface information reflecting impurities and local crystal defects in addition to small mineral constituents, was named as the thermoluminescence color imaging (abbreviated to TLCI) technique by the authors and its versatile applications were discussed. (author)

Thermoluminescent dosemeter in a X-ray diffractometer

International Nuclear Information System (INIS)

Mendoza A, D.; Gonzalez M, P.; Falcon B, T.; Castano, V.M.

1999-01-01

In this work it was presented the results obtained of the dosimetry which was realized in a X-ray diffractometer for powders, trademark Siemens D5000, using the thermoluminescent signal generated by the X-rays in the commercial dosemeter TLD-100 of Harshaw, US. In according to the results obtained, the radiation quantity received by an analysed material in the diffractometer, will be proportional to exposure time and it can vary from unities until tenths of grays. These results are very outstanding when are analysed crystalline materials in a diffractometer, for knowing the present crystalline phases, mainly if these are highly sensitive to the ionizing radiation, as it is the case of the thermoluminescent materials. (Author)

Thermoluminescence spectra of amethyst

Energy Technology Data Exchange (ETDEWEB)

Zhang, Q. [Suzhou Railway Teachers College (China). Dept. of Physics; Yang, B. [Beijing Normal University (China). Dept. of Physics; Wood, R.A.; White, D.R.R.; Townsend, P.D.; Luff, B.J. [Sussex Univ., Brighton (United Kingdom). School of Mathematical and Physical Sciences

1994-04-01

Thermoluminescence and cathodoluminescence data from natural and synthetic amethyst and synthetic quartz samples are compared. The spectra include features from the quartz host lattice and from impurity-generated recombination sites. Emission features exist throughout the wavelength range studied, 250-800 nm. The near infrared emission at 740-750 nm appears to be characteristic of the amethyst and is proposed to be due to Fe ion impurity. (Author).

Laser readable thermoluminescent radiation dosimeters and methods for producing thereof

International Nuclear Information System (INIS)

Braunlich, P.F.; Tetzlaff, W.

1989-01-01

Thin layer thermoluminescent radiation dosimeters for use in laser readable dosimetry systems, and methods of fabricating such thin layer dosimeters are disclosed. The thin layer thermoluminescent radiation dosimeters include a thin substrate made from glass or other inorganic materials capable of withstanding high temperatures and high heating rates. A thin layer of a thermoluminescent phosphor material is heat bonded to the substrate using an inorganic binder such as glass. The dosimeters can be mounted in frames and cases for ease in handling. Methods of the invention include mixing a suitable phosphor composition and binder, both being in particulate or granular form. The mixture is then deposited onto a substrate such as by using mask printing techniques. The dosimeters are thereafter heated to fuse and bond the binder and phosphor to the substrate. 34 figs

Thermoluminescence studies on plant seeds of different radiosensitivity

International Nuclear Information System (INIS)

Yamaguchi, Hikoyuki; Eguchi, Hoshio; Koizumi, Yoshinobu.

1975-01-01

The thermoluminescence was found when the pulverized powders from the whole seeds of six plant species or the hypocotyls from the seeds of five soybean varieties were irradiated at a liquid nitrogen temperature with gamma-rays. The spectra of luminescence emitted, the light peak temperature, the decaying after irradiation and the dose relationship of luminescence were determined. A high yield of the rapidly-decaying luminescence occurred in the more radiosensitive variety when irradiated with relatively lower doses. The very drastic decrease of the thermoluminescence was observed in the samples irradiated at room temperature prior to the exposure at 77 0 K. (auth.)

A microcomputer controlled thermoluminescence dosimetry system

International Nuclear Information System (INIS)

Huyskens, C.J.; Kicken, P.J.H.

1980-01-01

Using a microcomputer, an automatic thermoluminescence dosimetry system for personal dosimetry and thermoluminescence detector (TLD) research was developed. Process automation, statistical computation and dose calculation are provided by this microcomputer. Recording of measurement data, as well as dose record keeping for radiological workers is carried out with floppy disk. The microcomputer also provides a human/system interface by means of a video display and a printer. The main features of this dosimetry system are its low cost, high degree of flexibility, high degree of automation and the feasibility for use in routine dosimetry as well as in TLD research. The system is in use for personal dosimetry, environmental dosimetry and for TL-research work. Because of its modular set-up several components of the system are in use for other applications, too. The system seems suited for medium sized health physics groups. (author)

Synthesis and thermoluminescence properties of CaF2:Tm,Ce nanoparticles

Directory of Open Access Journals (Sweden)

M Zahedifar

2013-10-01

Full Text Available Calcium fluoride nanoparticles doped with thulium and cerium were synthesized as a novel nanostructure by using the hydrothermal method. The prepared samples were characterized by X-ray diffraction (XRD and energy dispersive spectrometer (EDS. The crystallite size of about 36 nm was estimated employing Scherer’s formula. Its shape and size were also observed by scanning electron microscope (SEM. Computerized glow curve deconvolution (CGCD technique revealed two overlapping thermoluminescence glow peaks at around 402 and 457 K in the complex thermoluminescence glow curve of this phosphor. Other thermoluminescence characteristics of this phosphor such as fading, reuseability and dose response recommend it as a good candidate for high dose dosimetry.

Some thermoluminescence ages in Queensland: a problem resolved

Energy Technology Data Exchange (ETDEWEB)

Prescott, J.R. [Adelaide Univ., SA (Australia)

1997-12-31

In a previous paper (Tejan-Kella et al Aust J. Soil Res. 28, 465, 1990), thermoluminescence (TL) dates were presented for a soil horizon at five sites in a chronosequence of freely-drained podzols at Cooloola and North Stradbroke Island, Queensland. The TL ages followed the expected order based on geomorphological evidence; and the TL age of 120 {+-}11 ka for the Amity dune on North Stradbroke Island agreed with uranium series dates for underlying coral recovered during sand mining. Nevertheless, several features of the TL results gave rise to some concern and were noted in the above mentioned paper. Specifically, the apparent TL age of 11 {+-} 2 ka for the Kings Bore site was widely at variance with the inferred age of about 0.5 ka based on geomorphological and soil profile evidence. Further, an apparent TL age of about 8 ka was found for samples from the Carlo sand blow. The Carlo samples were taken at mean depths of 1.0 m and 1.5 m from within the advancing toe of the dune, which is obviously mobile since it is encroaching on living vegetation. The time since last exposure to sunlight could scarcely exceed a decade. New measurements are reported, designed to resolve the former discrepancies. All sites have been re-dated, together with a new one, CA5S/1 (Chalambar) and a reduced value have been obtained. The fact that the TL age is somehow smaller than the U-series age may reflect the expectation that the summit of the dune be younger than the base. Paper no. 14; 1 tab., 1 fig.

Relationship between thermoluminescence and X-ray induced luminescence in alkali halides

International Nuclear Information System (INIS)

Aguilar, M.; Lopez, F.J.; Jaque, F.

1978-01-01

The wavelength spectra of thermoluminescence and X-ray induced luminescence in pure and divalent cation doped alkali halides, in the temperature range LNT-RT have been studied. The more important conclusion is that the wavelength spectra in both cases are very similar. This allows a new point of view to be presented on thermoluminescence mechanisms. (author)

The red thermoluminescence of quartz: 3-D spectral measurements

International Nuclear Information System (INIS)

Scholefield, R.B.; Prescott, J.R.

1999-01-01

As part of a general study of the thermoluminescence (TL) of quartz, we have examined the 3-D spectra of samples of quartz extracted from a variety of sediments. Blue emission at about 2.6 eV/475 nm, which is the photon energy region commonly used in luminescence dating, seems ubiquitous. Significant emission in the red, ∼1.9 eV/650 nm, has been found at most glow temperatures in all of our samples of Australian quartz sediments, and it is to this that particular attention is paid in the present work. A limited selection of samples from other countries has also been included. The ratio of the intensities of the red and blue emissions varies widely among samples. We have not found any evidence of a correlation between this ratio, nor the intensity of the red emission, with trace element concentration, including that of Al for which a correlation has been previously observed. In the context of luminescence dating, all samples have been examined to see whether they have a rapidly bleaching red component in a similar sense to the well-known 305 deg. C/2.95 eV/420 nm peak in quartz: some samples have such a component--some do not. A suggestive parallelism is found between the blue and red spectra, in that there are 'slowly bleaching' and 'rapidly bleaching' components at similar temperatures in the both red and the blue. However, there is no red component associated with the 110 deg. C peak used in pre-dose dating

Thermoluminescence dosemeter for personal dose equivalent assessment

International Nuclear Information System (INIS)

Silva, T.A. da; Rosa, L.A.R. da; Campos, L.L.

1995-01-01

The possibility was investigated of utilising a Brazilian thermoluminescence individual dosemeter, usually calibrated in terms of photon dose equivalent, for the assessment of the personal dose equivalent, H p (d), at depths of 0.07 and 10 mm. The dosemeter uses four CaSO 4 :Dy thermoluminescent detectors, between different filters, as the sensitive materials. It was calibrated in gamma and X radiation fields in the energy range from 17 to 1250 keV. Linear combinations of the responses of three detectors, in this energy range, allow the evaluation of H p (0.07) and H p (10), for radiation incidence angles varying from 0 to 60 degrees, with an accuracy better than 35%. The method is not applicable to mixed photon-beta fields. (author)

Thermoluminescence dating of loess from the Potwar Plateau, northern Pakistan

International Nuclear Information System (INIS)

Rendell, H.M.; Gamble, I.J.A.; Townsend, P.D.

1983-01-01

The loess deposits of northern Pakistan present a good opportunity for establishing a chronology using fine grain TL dating. The TL response of the 2-10 μm size fraction of polymineral (predominantly quartz/feldspar) mixtures is well behaved with linear dose-dependence and no anomalous fading. The loess horizons have very similar uranium and thorium contents, thus minimising dosimetry problems, and the fairly arid climatic conditions reduce the errors in water content estimation, at least for the uppermost horizons. A series of laboratory bleaching experiments reveal uncertainties in the absolute age estimates but not in their relative values. (author)

Thermoluminescence dosimetry environmental monitoring system

International Nuclear Information System (INIS)

Bortoluzzi, S.

1989-01-01

In this report, characteristics and performances of an environmental monitoring system with thermoluminescence dosimetry are presented. Most of the work deals with the main physical parameters necessary for measurements of ambiental dose. At the end of this report some of level doses in the environment around the site of the ENEA Center of Energy Research Salluggia (Italy) are illustrated

Thermoluminescent dosimetry of new phosphors of Zn O exposed to beta radiation

International Nuclear Information System (INIS)

Cruz V, C.; Burruel I, S.E.; Grijalva M, H.; Barboza F, M.; Bernal, R.

2004-01-01

In this work, we report the thermoluminescence dosimetry of a new Zn O phosphor obtained by annealing of Zn S powder precipitated when Zn S films were grown by employing a CBD method. The collected Zn S powder was pressed in a die to form pellets which were subjected to different thermal treatments under air atmosphere. X-ray diffraction (XRD) patterns and energy-dispersive X-ray Spectrometry (EDS) analyses confirmed the transformation of Zn S to Zn O. The phosphors thus obtained were exposed to high doses of beta radiation and their thermoluminescent dosimetry show that these new phosphors are materials suitable to be used in high dose thermoluminescence dosimetry. (Author)

Thermoluminescence of magnesium doped zirconium oxide (ZrO2:Mg) UV irradiated

International Nuclear Information System (INIS)

Rivera Montalvo, Teodoro; Furetta, Claudio

2008-01-01

Full text: The monitoring of ultraviolet radiation (UVR) different thermoluminescent (TL) materials have been used to measure UVR. UV dosimetry using thermoluminescence phenomena has been suggested in the past by several authors. This technique has an advantage over others methods due to the readout of the samples. Other advantages of these phosphors are their small size, portability, lack of any power requirements, linear response to increasing radiation dose and high sensitivity. Zirconium oxide, recently received full attention in view of their possible use as thermoluminescent dosimeter (TLD), if doped with suitable activators, in radiation dosimetry. In the present investigation thermoluminescent (TL) properties of magnesium doped zirconium oxide (ZrO 2 :Mg) under ultraviolet radiation (UVR) were studied. The ZrO 2 :Mg powder of size 30-40 nm, having mono clinical structure, exhibit a thermoluminescent glow curve with one peak centered at 180 C degrees. The TL response of ZrO 2 :Mg as a function ultraviolet radiation exhibits four maxima centered at 230, 260, 310 and 350 nmn. TL response of ZrO 2 :Mg as a function of spectral irradiance of UV Light was linear in a wide range. Fading and reusability of the phosphor were also studied. The results showed that ZrO 2 :Mg nano powder has the potential to be used as a UV dosemeter in UVR dosimetry. (author)

A new mathematical approximation of sunlight attenuation in rocks for surface luminescence dating

Energy Technology Data Exchange (ETDEWEB)

Laskaris, Nikolaos, E-mail: nick.laskaris@gmail.com [University of the Aegean, Department of Mediterranean Studies, Laboratory of Archaeometry, 1 Demokratias Avenue, Rhodes 85100 (Greece); Liritzis, Ioannis, E-mail: liritzis@rhodes.aegean.gr [University of the Aegean, Department of Mediterranean Studies, Laboratory of Archaeometry, 1 Demokratias Avenue, Rhodes 85100 (Greece)

2011-09-15

The attenuation of sunlight through different rock surfaces and the thermoluminescence (TL) or Optical stimulated luminescence (OSL) residuals clock resetting derived from sunlight induced eviction of electrons from electron traps, is a prerequisite criterion for potential dating. The modeling of change of residual luminescence as a function of two variables, the solar radiation path length (or depth) and exposure time offers further insight into the dating concept. The double exponential function modeling based on the Lambert-Beer law, valid under certain assumptions, constructed by a quasi-manual equation fails to offer a general and statistically sound expression of the best fit for most rock types. A cumulative log-normal distribution fitting provides a most satisfactory mathematical approximation for marbles, marble schists and granites, where absorption coefficient and residual luminescence parameters are defined per each type of rock or marble quarry. The new model is applied on available data and age determination tests. - Highlights: > Study of aattenuation of sunlight through different rock surfaces. > Study of the thermoluminescence (TL) or Optical stimulated luminescence (OSL) residuals as a function of depth. > A Cumulative Log-Normal Distribution fitting provides the most satisfactory modeling for marbles, marble schists and granites. > The new model (Cummulative Log-Norm Fitting) is applied on available data and age determination tests.

A new mathematical approximation of sunlight attenuation in rocks for surface luminescence dating

International Nuclear Information System (INIS)

Laskaris, Nikolaos; Liritzis, Ioannis

2011-01-01

The attenuation of sunlight through different rock surfaces and the thermoluminescence (TL) or Optical stimulated luminescence (OSL) residuals clock resetting derived from sunlight induced eviction of electrons from electron traps, is a prerequisite criterion for potential dating. The modeling of change of residual luminescence as a function of two variables, the solar radiation path length (or depth) and exposure time offers further insight into the dating concept. The double exponential function modeling based on the Lambert-Beer law, valid under certain assumptions, constructed by a quasi-manual equation fails to offer a general and statistically sound expression of the best fit for most rock types. A cumulative log-normal distribution fitting provides a most satisfactory mathematical approximation for marbles, marble schists and granites, where absorption coefficient and residual luminescence parameters are defined per each type of rock or marble quarry. The new model is applied on available data and age determination tests. - Highlights: → Study of aattenuation of sunlight through different rock surfaces. → Study of the thermoluminescence (TL) or Optical stimulated luminescence (OSL) residuals as a function of depth. → A Cumulative Log-Normal Distribution fitting provides the most satisfactory modeling for marbles, marble schists and granites. → The new model (Cummulative Log-Norm Fitting) is applied on available data and age determination tests.

Detection and thermoluminescence of coriander (Coriandrum sativum L.) irradiated with 60Co

International Nuclear Information System (INIS)

Ruiz G, B.; Cruz Z, E.; Barboza F, M.

2009-10-01

The fresh and dried coriander (Coriandrum sativum L.) is a spice of high commercial value as food for consumption in Mexico. Their hygienic quality is often poor due to some factors: contaminants present in irrigation water and the cultivation atmosphere, harvesting and post harvest handling, mainly. The process by radiation is an alternative to achieve the sterilization to adequate dose for the hygienic quality for its consumption. However, irradiation also involves food detection exposed to radiation. This paper presents detected results on the dried coriander that was obtained from fresh samples and thermoluminescent properties such as glow curves structure from low doses (0.5 Gy) to high (15 kGy), the dose response, thermoluminescent signal decay, in order to determine the loss of stability during the storage of the poly mineral fraction. We obtained the inorganic fraction separation of the organic part of particle sizes of 10 μm by the Zimmerman method. The samples were exposed at two dose ranges; 0.5-400 Gy and 0.5-15 kGy of gamma radiation with 60 Co. The limit of thermoluminescent detection of the irradiated coriander samples was from 1 Gy. The glow curves were at a broad band of 35-400 C, with a maximum thermoluminescence around 182-196 C, and run at 164 C for high doses of 15 kGy. The range of linear response to dose was 4-25 Gy, whereas higher doses than the kGy order the response increase with the dose. The thermoluminescent properties of the coriander poly mineral fraction, show it can be used to identify irradiated food at gamma doses relatively low and even in doses of commercial interest due to the high stability of thermoluminescent signals. (Author)

Thermoluminescent dosimetric characterization of the perovskite, KMgF3, activated with lanthanum

International Nuclear Information System (INIS)

Sepulveda M, F.

2003-01-01

The new ICRP regulation about the Radiological Protection allows to the different groups to study new thermoluminescent materials highly sensitive for dosimetric applications (personal and environmental). This work reports the relative experimental results to the thermoluminescent characteristic of a new preparation of the fluorine perovskite activated with lanthanum absorbed in polytetrafluoroethylene (KMgF 3 : LaF 3 + Ptfe). The main thermoluminescent properties investigated were: the TL response like a function of the absorbed dose, the attainable accuracy in the dose measurement, the reproducibility of the TL readings and the threshold dose. The obtained results were compared with the requirements of the ANSI protocol for the environmental dosimetry, resulting in a very good agreement with the required yields. (Author)

Study on carbonated hydroxyapatite as a thermoluminescence dosimeter

International Nuclear Information System (INIS)

Shafaei, M.; Sardari, D.; Ziaie, F.; Larijani, M.M.

2015-01-01

In this study, carbonated hydroxyapatite nanoparticles were used for thermoluminescence dosimetry. The nano-structure carbonated hydroxyapatite synthesized via hydrolysis of CaHPO 4 and CaCO 3 . The obtained nano powders were characterized by XRD technique and FTIR spectroscopy system. The carbonated hydroxyapatite samples were irradiated at different doses using 60 Co gamma rays, and were subjected to thermoluminescence measurement system, consequently. The TL glow curve exhibited two distinguishable peaks centered at around of 165 C and 310 C. The TL response of carbonated hydroxyapatite samples as a function of absorbed dose was linear in the range of 25-1000 Gy. Other dosimetric features of the carbonated hydroxyapatite nanoparticles including fading and reproducibility were also investigated.

Thermoluminescence dosimetric characteristics of thulium doped ZnB2O4 phosphor

International Nuclear Information System (INIS)

Annalakshmi, O.; Jose, M.T.; Madhusoodanan, U.; Subramanian, J.; Venkatraman, B.; Amarendra, G.; Mandal, A.B.

2014-01-01

Polycrystalline powder samples of rare earth doped Zinc borates were synthesized by high temperature solid state diffusion technique. Dosimetric characteristics of the phosphor like thermoluminescence glow curve, TL emission spectra, dose–response, fading studies, reproducibility and reusability studies were carried out on the synthesized phosphors. Among the different rare earth doped phosphors, thulium doped zinc borate was found to have a higher sensitivity. Hence detailed dosimetric characteristics of this phosphor were carried out. It is observed that the dose–response is linear from 10 mGy to 10 3 Gy in this phosphor. EPR measurements were carried out on unirradiated, gamma irradiated and annealed phosphors to identify the defect centers responsible for thermoluminescence. A TL model is proposed based on the EPR studies in these materials. Kinetic parameters were evaluated for the dosimetric peaks using various methods. The experimental results show that this phosphor can have potential applications in radiation dosimetry applications. -- Highlights: • Polycrystalline powder samples of rare earth doped zinc borates were synthesized. • Thulium was observed to be the most efficient dopant in ZnB 2 O 4 lattice. • TL intensity of the dosimetric peak is around 20 times that of TLD-100. • Based on EPR studies a TL mechanism is proposed in zinc borate. • Deconvolution of the glow curve carried out

Report on the results of the third intercomparison study of thermoluminescent dosimeters for environmental measurements

International Nuclear Information System (INIS)

Driscoll, C.M.H.

1988-01-01

Scientific laboratories within the Member States of the European Communities have a continuing interest in the use and development of both thermoluminescent dosimeters and thermoluminescence measurement techniques for the assessment of exposure from environmental gamma radiation. In the United Kingdom, for example, environmental thermoluminescent dosimeters have been developed by the National Radiological Protection Board (NRPB) and used in a national survey of indoor radiation exposure. Other laboratories in various Member States are currently involved in similar studies of natural radiation exposure or are using thermoluminescent dosimeters for environmental measurements at reactor sites. Therefore, it is appropriate that such laboratories have facilities within the European Community for standardization and intercomparison of their environmental measurement techniques

Effect of particle size on the thermoluminescent response of hydroxyapatite

International Nuclear Information System (INIS)

Barrera V, A.; Zarate M, J.; Contreras, M. E.; Rivera M, T.

2016-10-01

We present the study of the structural characterization and the thermoluminescent response of the hydroxyapatite as a function of the calcination temperature and the effect of the particle size. For precipitation synthesis, calcium nitrate (Ca(NO_3)_2 and dibasic ammonium phosphate ((NH_4)_2HPO_4) were used as precursors and ammonium hydroxide (NH_4OH) as a ph controlling agent. The characterization of the samples was carried out by the techniques of X-ray diffraction, scanning electron microscopy and infrared spectroscopy. The powders obtained are composed of hydroxyapatite, with a different degree of dehydroxylation. The thermoluminescent characterization indicates that at higher calcination temperature there is a higher thermoluminescent response, the calcined powders at 1300 degrees Celsius show a very well defined brightness curve with a higher intensity, with its maximum intensity located at a temperature of 210 degrees Celsius, which indicates that this material can be used as a dosimeter. (Author)

Positional glow curve simulation for thermoluminescent detector (TLD) system design

International Nuclear Information System (INIS)

Branch, C.J.; Kearfott, K.J.

1999-01-01

Multi- and thin element dosimeters, variable heating rate schemes, and glow-curve analysis have been employed to improve environmental and personnel dosimetry using thermoluminescent detectors (TLDs). Detailed analysis of the effects of errors and optimization of techniques would be highly desirable. However, an understanding of the relationship between TL light production, light attenuation, and precise heating schemes is made difficult because of experimental challenges involved in measuring positional TL light production and temperature variations as a function of time. This work reports the development of a general-purpose computer code, thermoluminescent detector simulator, TLD-SIM, to simulate the heating of any TLD type using a variety of conventional and experimental heating methods including pulsed focused or unfocused lasers with Gaussian or uniform cross sections, planchet, hot gas, hot finger, optical, infrared, or electrical heating. TLD-SIM has been used to study the impact on the TL light production of varying the input parameters which include: detector composition, heat capacity, heat conductivity, physical size, and density; trapped electron density, the frequency factor of oscillation of electrons in the traps, and trap-conduction band potential energy difference; heating scheme source terms and heat transfer boundary conditions; and TL light scatter and attenuation coefficients. Temperature profiles and glow curves as a function of position time, as well as the corresponding temporally and/or spatially integrated glow values, may be plotted while varying any of the input parameters. Examples illustrating TLD system functions, including glow curve variability, will be presented. The flexible capabilities of TLD-SIM promises to enable improved TLD system design

Thermoluminescent and optical processes in alkaline halogenides dosemeters contaminated with Europium

International Nuclear Information System (INIS)

Barboza F, M.; Melendrez, R.; Castaneda, B.; Pedroza M, M.; Chernov, V.; Perez S, R.; Aceves, R.

2000-01-01

Recent research results are presented about the properties of the optical processes of photo transferred thermoluminescence (TLFT), optical whitening (BO), thermoluminescence induced by light (TLL) and its effect in the thermoluminescent curve (Tl) produced by ionizing and non-ionizing radiation. The systematic analysis of all these processes, acquires a singular importance due that actually the alkaline halogenide crystals are object of intense investigations which analyse their potential applications as detectors and radiation dosemeters through stimulated optical luminescence techniques or thermoluminescence. The obtained data show that the Tl curve of material with this nature can be enormously affected by exposure of phosphorus to the environmental light or UV. This is in part due to liberation processes of charge bearers are shouted and makes a subsequent trapping in less temperature traps; at the same time that induce changes in the intensity of determined Tl bands. Additionally, also it is observed that mentioned phenomena are related as with wavelength of incident light as of the illumination time. Finally, the obtained information allows to conclude that although the illumination effect is extremely complex, it is associated and can be explained mainly with phenomena that implicate the electrons excitation trapped in form of F centers and trapping mechanisms or radioactive and non-radioactive recombination. (Author)

Thermoluminescence properties of irradiated commercial color pencils for accidental retrospective dosimetry

International Nuclear Information System (INIS)

Meriç, Niyazi; Şahiner, Eren; Bariş, Aytaç; Polymeris, George S.

2015-01-01

Color pencils are widely used mostly in kindergartens, in schools and could be found in all houses with families having young children. Their wide spread use in modern times as well as their chemical composition, consisting mostly of Si and Al, constitute two strong motivations towards exploiting their use as accidental retrospective thermoluminescent dosimeters. The present manuscript reports on the study of colored pencils manufactured by a commercial brand in China which is very common throughout Turkey. The preliminary results discussed in the present work illustrated encouraging characteristics, such as the presence of a trapping level giving rise to natural TL in a temperature range that is sufficiently high. Specific thermoluminescence features of this peak, such as glow peak shape and analysis, anomalous fading, thermal quenching, reproducibility, linearity and recovery ability to low attributed doses were studied. The results suggest that the color pencils could be effectively used in the framework of retrospective thermoluminescent dosimetry with extreme caution, based on multiple aliquot protocols. - Highlights: • Thermoluminescence of the inner part of commercial colored pencils was studied. • The presence of a trapping level giving rise to natural TL at 260 °C was yielded. • Deco analysis, anomalous fading, thermal quenching, reproducibility, linearity and recovery ability of this peak were studied

Fast neutron dosimetry using CaSO4:Dy thermoluminescent dosimeters

International Nuclear Information System (INIS)

Azorin, N.G.; Salvi, C.R.; Rubio, J.L.; Gutierrez, C.A.

1980-01-01

The use of CaSO 4 :Dy phosphor powder in fast neutron dose measurements using the activation of sulphur from the 32 S(n,p) 32 P reaction is described. The thermoluminescence induced during the irradiation and that due to the decay of short-lived activation products, is erased by annealing the dosimeters after a post-irradiation time of 3 days. The self-induced thermoluminescence measured at different intervals of post-irradiation time, gives an estimation of the fast neutron dose to which the dosimeters were exposed

Effect of the radiation in the thermoluminescent properties of lava

CERN Document Server

Correcher, V; García, J

2003-01-01

Blue thermoluminescence (Tl) emission from different lavas of many places (Costa Rica, Canary Islands, Hawaii Islands, Iceland and Italy) corresponding to different eruptions has been studied to know its potential use in the field of dating and retrospective dosimetry. Due to the light emission is linked to the point defects of the crystalline lattice structure, X-ray diffraction analyses were performed to determine the components of this poly mineral material that mostly are cristobalite, plagioclase and phyllosilicates. Exposures to different doses (in a range of 1-25 Gy) were given to each sample to determine the evolution of the Tl signal with the irradiation under laboratory conditions. In all cases, a linear response could be observed and no saturation has been detected in this range of doses. Both natural (NTL) and induced (ITL) Tl signal exhibit a complex glow curve structure associated to a continuous trap distribution over 100 C that could be attributed to the formation-annihilation [Al0 sub 4 /alka...

Thermoluminescence dosimeters with narrow bandpass filters

Science.gov (United States)

Walker, Scottie W.

2004-07-20

A dosimetry method exposes more than one thermoluminescence crystals to radiation without using conventional filters, and reads the energy stored in the crystals by converting the energy to light in a conventional manner, and then filters each crystal output in a different portion of the spectrum generated by the crystals.

Rare earth oxyhalogenide base thermoluminescent material

International Nuclear Information System (INIS)

Rabatin, J.G.

1976-01-01

A process is described that consists to expose a thermoluminescent material to ionizing radiations, the material being a rare earth oxyhalogenide with terbium additions, to heat this material up to the emission of visible radiations and to measure the emitted radiations which are proportional to the ionizing radiation dose [fr

Photoluminescence, trap states and thermoluminescence decay ...

Indian Academy of Sciences (India)

Administrator

Photoluminescence, trap states and thermoluminescence decay process study of Ca2MgSi2O7 : Eu. 2+. , Dy. 3+ phosphor. RAVI SHRIVASTAVA*, JAGJEET KAUR, VIKAS DUBEY and BEENA JAYKUMAR. Govt. VYT PG Autonomous College, Durg 491 001, (C.G.) India. MS received 9 July 2013; revised 5 December 2013.

Thermoluminescent response of aluminium oxide thin films subject to gamma irradiation

Energy Technology Data Exchange (ETDEWEB)

Arrieta, A.; Escobar A, L.; Camps, E.; Villagran, E.; Gonzalez, P.R

2006-07-01

The thermoluminescent (TL) properties of amorphous aluminium oxide thin films (thicknesses as low as 0.3 {mu}m) subjected to gamma (Co-60) irradiation are reported. Aluminium oxide thin films were prepared by laser ablation from an Al{sub 2}O{sub 3} target using a Nd: YAG laser with emission at the fundamental line. The films were exposed to gamma radiation (Co-60) in order to study their TL response. Thermoluminescence glow curves exhibited two peaks at 110 and 176 C. The high temperature peak shows good stability and 30% fading in the first 5 days after irradiation. A linear relationship between absorbed dose and the thermoluminescent response for doses span from 150 mGy to 100 Gy was observed. These results suggest that aluminium oxide thin films are suitable for detection and monitoring of gamma radiation. (Author)

Analysis of the thermoluminescent signal in the hydroxyapatite synthesized by the sol-gel method

International Nuclear Information System (INIS)

Mendoza A, D.; Gonzalez, P.R.; Lobato, M.; Rubio, E.; Rodriguez L, V.; Custodio, E.

2004-01-01

The physical properties of the ceramics are related with the chemical bonds and the crystalline structure, because the elements that constitute it can be united by ionic bonds or partially ionic giving a covalent character, this last causes that the outer layer is full of electrons. This property makes that the ceramic ones become interesting materials for thermoluminescent applications, as it demonstrates through the recent works presented on the hydroxyapatite that is a ceramic biomaterials that has shown an interesting thermoluminescent signal when being exposed to gamma radiation. In this sense, this work presents the thermoluminescent signal analysis induced by the UV and gamma radiation in a particular type of hydroxyapatite synthesized by sol gel method in which the temperature synthesis is varied. The final thermoluminescent sensitivity of materials is correlated with the crystalline degree, which is analysed through X-ray diffraction. (Author)

Thermoluminescence studies in geology

International Nuclear Information System (INIS)

Sankaran, A.V.; Sunta, C.M.; Nambi, K.S.V.; Bapat, V.N.

1980-01-01

Even though the phenomenon of thermoluminescence is well studied, particularly over last 3 decades, its potentialities in the field of geology have not been adequately evaluated. In this report several useful applications of TL in mineralogy, petrogenesis, stratigraphy, tectonics, ore-prospecting and other branches have been identified with particular emphasis to the Indian scene. Important areas in the country that may provide the basic material for such studies are indicated at the end along with brief geological or mineralogical accounts. (auth.)

Stream sediment detailed geochemical survey for Date Creek Basin, Arizona

International Nuclear Information System (INIS)

Butz, T.R.; Tieman, D.J.; Grimes, J.G.; Bard, C.S.; Helgerson, R.N.; Pritz, P.M.; Wolf, D.A.

1981-01-01

The purpose of the Date Creek Supplement is to characterize the chemistry of sediment samples representing stream basins in which the Anderson Mine (and related prospects) occur. Once characterized, the chemistry is then used to delineate other areas within the Date Creek Basin where stream sediment chemistry resembles that of the Anderson Mine area. This supplementary report examines more closely the data from sediment samples taken in 239 stream basins collected over a total area of approximately 900 km 2 (350 mi 2 ). Cluster and discriminant analyses are used to characterize the geochemistry of the stream sediment samples collected in the Date Creek Basin. Cluster and discriminant analysis plots are used to delineate areas having a potential for uranium mineralization similar to that of the Anderson Mine

Study of a new glass matrix by the thermoluminescence technique

International Nuclear Information System (INIS)

Ferreira, Pamela Z.; Vedovato, Uly P.; Cunha, Diego M. da; Dantas, Noelio O.; Silva, Anielle C.A.; Neves, Lucio P.; Perini, Ana P.; Carrera, Betzabel N.S.; Watanabe, Shigueo

2015-01-01

The thermoluminescence technique is widely used for both personal and for high-dose dosimetry. In this work, the thermoluminescence technique was utilized to study a new glass matrix, with nominal composition of 20Li 2 CO 3 .10Al 2 O 3 .20BaO.50B 2 O 3 (mol%), irradiated with different doses in a 60 Co source. The glow curves and the dose-response curve were obtained for radiation doses between 50 Gy and 900 Gy. The results showed that this new glass matrix presents potential use in high-dose dosimetry. (author)

Thermoluminescence study of quartzite in a gold and uranium mineralized zone (Canavieiras, Jacobina-Bahia)

International Nuclear Information System (INIS)

Ferreira, J.

1973-01-01

The quartzite of Canavieiras gold mine (Jacobina-Bahia, Brazil) shows in its natural glow curve, a high temperature. The study of the reproductibility of this peak resulted in the standartization of measurement for grain sizes between 80 and 100 mesh. ''In Situ'' total gamma-ray profiles were made using a scintillation detector for the study the distribution of radioactive elements near the pirite, uranium and gold strike. In the interpretation of the profiles it was possible to shown a positive correlation between thermoluminescence and uranium yields. The thermoluminescence peak is sufficiently high temperature peak to let thermoluminescence accumulate at ambient temperatures. It was used in attempt to estimate the time and the event that enitiated the accumulation of thermoluminescence. The result obtained, (7 - + 4).10 6 years, may correspond to the last heating of the rocks at relatively recent time. (C.D.G.) [pt

Import control of irradiated foods by the thermoluminescence method

International Nuclear Information System (INIS)

Pinnioja, S.; Autio, T.; Niemi, E.; Pensala, O.

1993-01-01

A thermoluminescence (TL) method was applied for the import control of irradiated foods. The method is based on the determination of the TL of mineral contaminants in foods. Detection of irradiation was incorporated in official Finnish control procedures in spring 1990. For foodstuffs with a reduced microbe content and in which no fumigant residues are found, possible irradiation is investigated by the TL method. The minerals are separated from the foods in different ways: picking is used for spices; water rinsing for herbs, spices, berries and mushrooms; high-density liquid to separate the organic material from the mineral fraction in seafood; and carbon tetrachloride for foods forming gels with water. To date about 140 food samples have been analysed for control purposes: 50 samples of herbs and spices, 25 samples of berries and mushrooms and 65 samples of seafood. Of these, 14 samples of herbs and spices and 5 samples of seafood were shown to have been irradiated. Differences in TL intensity between irradiated and unirradiated samples were at least 1 and usually 3-4 orders of magnitude. (orig.)

Surface dating of bricks, an application of luminescence techniques

Science.gov (United States)

Galli, Anna; Martini, Marco; Maspero, Francesco; Panzeri, Laura; Sibilia, Emanuela

2014-05-01

Luminescence techniques are a powerful tool to date archaeological ceramic materials and geological sediments. Thermoluminescence (TL) is widely used for bricks dating to reconstruct the chronology of urban complexes and the development of human cultures. However, it can sometimes be inconclusive, since TL assesses the firing period of bricks, which can be reused, even several centuries later. This problem can be circumvented using a dating technique based on a resetting event different from the last heating. OSL (Optically Stimulated Luminescence) exploits the last light exposition of the brick surface, which resets the light-sensitive electron traps until the surface is definitely shielded by mortar and superimposed bricks. This advanced application (surface dating) has been successfully attempted on rocks, marble and stone artifacts, but not yet on bricks. A recent conservation campaign at the Certosa di Pavia gave the opportunity to sample some bricks belonging to a XVII century collapsed wall, still tied to their mortars. This was an advantageous condition to test this technique, comparing the dating results with precise historical data. This attempt gave satisfactory results, allowing to identify bricks surely reused and to fully confirm that the edification of the perimetral wall occurred at the end of XVII century.

Historical note: thermoluminescent dosimetry (LiF) 1950-51

International Nuclear Information System (INIS)

Heckelsberg, L.F.

1980-01-01

The early history of thermoluminescent dosimetry has not been adequately described and one of the first workers in this field takes this opportunity to record more fully the history of the period. (author)

Thermoluminescence in some copper-doped compounds

International Nuclear Information System (INIS)

Patil, R.R.; Moharil, S.V.; Dhopte, S.M.; Muthal, P.L.; Kondawar, V.K.

2003-01-01

Thermoluminescence (TL) in various Cu + -doped materials is studied. A good correlation between the presence of copper in the Cu + form and TL sensitivity is observed. Correlation between TL emission spectra and photoluminescence suggests that Cu + acts as the emission center in the TL process. (copyright 2003 WILEY-VCH Verlag GmbH and Co. KGaA, Weinheim) (orig.)

Irradiated black pepper identification based on thermoluminescence of silicate minerals

International Nuclear Information System (INIS)

Faycal Kharfi; Randa Ketfi

2018-01-01

In this work we have successfully implemented thermoluminescence TL method for irradiated food identification. First tests are performed on Indian black pepper and show promising results to extend the proposed method to many other foods. The X-ray diffraction (XRD) shows that SiO 2 (p3 2 21) is the main component of the separated mineral phase. A saturation dose of ∼ 100 Gy is determined for this pepper above which all thermoluminescent centers of the quartz are activated. Thus, above this threshold dose, only the pepper irradiation will be confirmed but no accuracy on the exact dose received. (author)

Preparation and structural characterization of the thermoluminescent material CaSO4: Dy

International Nuclear Information System (INIS)

Sanchez R, A.; Azorin, J.; Gonzalez M, P.R.; Rivera, T.

2005-01-01

The grade of crystallinity of a material is important so that the one is presented the thermoluminescence phenomenon; for what is necessary to study those structural characteristic of a TL material and to correlate them with its TL response when being irradiated with ionizing radiation. The calcium sulfate activated with Dysprosium (CaSO 4 : Dy) it is a material that has demonstrated its efficiency in the dosimetry of the ionizing radiation for the thermoluminescence method. In this work the structural characterization of this prepared material for the recrystallization method by means of the evaporation of the solvent and their relationship with their TL response is presented. The results showed that the best material to be used in thermoluminescent dosimetry presents a crystalline structure in orthorhombic phase and a particle size in the interval of 80 μm to 200 μm. (Author)

Numerical analysis of thermoluminescence glow curves; Analisis numerico de las cruvas de termoluminiscencia

Energy Technology Data Exchange (ETDEWEB)

Gomez Ros, J M; Delgado, A

1989-07-01

This report presents a method for the numerical analysis of complex thermoluminescence glow curves resolving the individual glow peak components. The method employs first order kinetics analytical expressions and is based In a Marquart-Levenberg minimization procedure. A simplified version of this method for thermoluminescence dosimetry (TLD) is also described and specifically developed to operate whit Lithium Fluoride TLD-100. (Author). 36 refs.

Quality control of thermoluminesce personal dose monitoring

International Nuclear Information System (INIS)

Shang Aiguo; He Wenchang; Zhao Fengtao

2006-01-01

In order to evaluate the influence factor to thermoluminesce personal dose monitoring result, the every question that can appear based on the fact was analyzed. The results show that the detector, annealing, measuring process can influence the monitoring result. It gives some measures to enhance monitoring quality. (authors)

Calibration procedure for thermoluminescent dosemeters in water absorbed doses for Iridium-192 high dose rate sources

International Nuclear Information System (INIS)

Reyes Cac, Franky Eduardo

2004-10-01

Thermoluminescent dosimeters are used in brachytherapy services quality assurance programs, with the aim of guaranteeing the correct radiation dose supplied to cancer patients, as well as with the purpose of evaluating new clinical procedures. This work describes a methodology for thermoluminescent dosimeters calibration in terms of absorbed dose to water for 192 Ir high dose rate sources. The reference dose used is measured with an ionization chamber previously calibrated for 192 Ir energy quality, applying the methodology proposed by Toelli. This methodology aims to standardizing the procedure, in a similar form to that used for external radiotherapy. The work evolves the adaptation of the TRS-277 Code of the International Atomic Energy Agency, for small and big cavities, through the introduction for non-uniform experimental factor, for the absorbed dose in the neighborhood of small brachytherapy sources. In order to simulate a water medium around the source during the experimental work, an acrylic phantom was used. It guarantees the reproducibility of the ionization chamber and the thermoluminescent dosimeter's location in relation to the radiation source. The values obtained with the ionization chamber and the thermoluminescent dosimeters, exposed to a 192 Ir high dose rate source, were compared and correction factors for different source-detector distances were determined for the thermoluminescent dosimeters. A numeric function was generated relating the correction factors and the source-detector distance. These correction factors are in fact the thermoluminescent dosimeter calibration factors for the 192 Ir source considered. As a possible application of this calibration methodology for thermoluminescent dosimeters, a practical range of source-detector distances is proposed for quality control of 192 Ir high dose rate sources. (author)

Measurement conditions of natural soil thermoluminescence and their application in a granite type uranium deposit

International Nuclear Information System (INIS)

Chen Yue; Yang Yaxin; Liu Qingcheng

2009-01-01

A measuring method of natural soil thermoluminescence is used for prospecting of uranium deposits. The better effects are obtained by using the method, but the parameters selected have significant effects on the intensity of soil thermoluminescent. So, the measuring parameters are selected according to the different soil samples. Based on the measuring 1 000 soil samples of granite type uranium deposit,the optimum heating up program of natural soil thermoluminescence is obtained, that is, preheating, lasting heating, constant temperature and the halting heating. The parameters selected are as follows: the heating rate being 15 degree C/s, the temperatures of the first and second constant temperature being 135 degree C and 400 degree C respectively. Using the selected parameters for measuring soil samples from a known mining area in Guangdong province, the result indicates that the abnormities of thermoluminescence have corresponding relations with the underground orebodies. (authors)

Needle-type differential thermoluminescent dosemeter

International Nuclear Information System (INIS)

Kubu, M.

1988-01-01

The dosemeter serves to measure the depth distribution of absorbed dose in a phantom in mixed neutron and gamma radiation fields. It consists of a stratified cylindrical absorber in which alternate moderator and cadmium layers. Inside are two bores along the longitudinal axis for tubes filled with 6 LiF and 7 LiF powder thermoluminescent dosemeters. The device is easily portable and allows to carry out measurements with a high level of reproducibility. (J.B.). 4 figs

An intercomparison of the thermoluminescent efficiency of various preparations of lithium fluoride

CERN Document Server

Driscoll, C M H

1977-01-01

Possible alternative sources of supply of lithium fluoride to that used at present in the NRPB automated TLD system dosemeter are being considered on the grounds of economy and quality control. Initial measurements on the thermoluminescent properties and efficiency of various preparations of lithium fluoride are described, including the Harshaw TLD-700 which is currently in use in the automated thermoluminescent dosemeter. Material obtained from British Nuclear Fuels Ltd (which may be an atypical batch) showed 75% of the sensitivity of the Harshaw material, with around 20% fading of the signal after 1 month's storage. French material, obtained from Desmarquest and Carbonisation Entreprise et Ceramique and used by the Commissariat a l'Energie Atomique, showed good fading resistance but, after standard preparational treatments, was only half as sensitive in the thermoluminescent response. Without additional treatments to improve the characteristics of these materials, they cannot be considered as being satisfac...

Statistical methods to evaluate thermoluminescence ionizing radiation dosimetry data

International Nuclear Information System (INIS)

Segre, Nadia; Matoso, Erika; Fagundes, Rosane Correa

2011-01-01

Ionizing radiation levels, evaluated through the exposure of CaF 2 :Dy thermoluminescence dosimeters (TLD- 200), have been monitored at Centro Experimental Aramar (CEA), located at Ipero in Sao Paulo state, Brazil, since 1991 resulting in a large amount of measurements until 2009 (more than 2,000). The data amount associated with measurements dispersion, since every process has deviation, reinforces the utilization of statistical tools to evaluate the results, procedure also imposed by the Brazilian Standard CNEN-NN-3.01/PR- 3.01-008 which regulates the radiometric environmental monitoring. Thermoluminescence ionizing radiation dosimetry data are statistically compared in order to evaluate potential CEA's activities environmental impact. The statistical tools discussed in this work are box plots, control charts and analysis of variance. (author)

Thermoluminescence dosimetric characteristics of thulium doped ZnB{sub 2}O{sub 4} phosphor

Energy Technology Data Exchange (ETDEWEB)

Annalakshmi, O. [Radiological Safety Division, Indira Gandhi Centre for Atomic Research, Kalpakkam-603102 (India); Jose, M.T., E-mail: mtj@igcar.gov.in [Radiological Safety Division, Indira Gandhi Centre for Atomic Research, Kalpakkam-603102 (India); Madhusoodanan, U. [Radiological Safety Division, Indira Gandhi Centre for Atomic Research, Kalpakkam-603102 (India); Subramanian, J. [Central Leather Research Institute, Council of Scientific and Industrial Research, Chennai (India); Venkatraman, B. [Radiological Safety Division, Indira Gandhi Centre for Atomic Research, Kalpakkam-603102 (India); Amarendra, G. [Materials Physics Division, Indira Gandhi Centre for Atomic Research, Kalpakkam-603102 (India); Mandal, A.B. [Central Leather Research Institute, Council of Scientific and Industrial Research, Chennai (India)

2014-02-15

Polycrystalline powder samples of rare earth doped Zinc borates were synthesized by high temperature solid state diffusion technique. Dosimetric characteristics of the phosphor like thermoluminescence glow curve, TL emission spectra, dose–response, fading studies, reproducibility and reusability studies were carried out on the synthesized phosphors. Among the different rare earth doped phosphors, thulium doped zinc borate was found to have a higher sensitivity. Hence detailed dosimetric characteristics of this phosphor were carried out. It is observed that the dose–response is linear from 10 mGy to 10{sup 3} Gy in this phosphor. EPR measurements were carried out on unirradiated, gamma irradiated and annealed phosphors to identify the defect centers responsible for thermoluminescence. A TL model is proposed based on the EPR studies in these materials. Kinetic parameters were evaluated for the dosimetric peaks using various methods. The experimental results show that this phosphor can have potential applications in radiation dosimetry applications. -- Highlights: • Polycrystalline powder samples of rare earth doped zinc borates were synthesized. • Thulium was observed to be the most efficient dopant in ZnB{sub 2}O{sub 4} lattice. • TL intensity of the dosimetric peak is around 20 times that of TLD-100. • Based on EPR studies a TL mechanism is proposed in zinc borate. • Deconvolution of the glow curve carried out.

Thermoluminescent response of LaAlO{sub 3}:Pr; Respuesta termoluminiscente de LaAlO{sub 3}:Pr

Energy Technology Data Exchange (ETDEWEB)

Morales H, A.; Zarate M, J. [Universidad Michoacana de San Nicolas de Hidalgo, Instituto de Investigacion en Metalurgia y Materiales, Ciudad Universitaria, Edif. U, 58060 Morelia, Michoacan (Mexico); Azorin N, J. [Universidad Autonoma Metropolitana, Unidad Iztapalapa, Av. San Rafael Atlixco 186, Col. Vicentina, 09340 Mexico D. F. (Mexico); Rivera M, T., E-mail: feyo_yo@hotmail.com [IPN, Centro de Investigacion en Ciencia Aplicada y Tecnologia Avanzada, Av. Legaria 694, 11500 Mexico D. F. (Mexico)

2015-10-15

In this study, the thermoluminescence response of doped lanthanum aluminate (LaAlO{sub 3}) with praseodymium ion (Pr) obtained by the Pechini method and drying by the spraying technique Spry Dryer was studied. The obtained powders were analyzed structurally by the X-ray diffraction technique; the morphological characterization was by the scanning electron microscopy technique. The obtained powders at 800 degrees C presented crystallinity and showed a Rhombohedral crystal structure, this phase was observed by X-ray diffraction patterns. Thermoluminescence response of LaAlO{sub 3}:Pr showed a brightness curve with a peak centered at 157 degrees C. The sensitivity of the doped samples was improved about 90 times in comparison with the undoped sample. Thermoluminescence response in function of the wavelength showed a maximum at 230 nm, reproducibility of thermoluminescence response was ±50%. Also the fading in thermoluminescence response was studied. (Author)

Method of preparing a thermoluminescent phosphor

Science.gov (United States)

Lasky, Jerome B.; Moran, Paul R.

1979-01-01

A thermoluminescent phosphor comprising LiF doped with boron and magnesium is produced by diffusion of boron into a conventional LiF phosphor doped with magnesium. Where the boron dopant is made to penetrate only the outer layer of the phosphor, it can be used to detect shallowly penetrating radiation such as tritium beta ays in the presence of a background of more penetrating radiation.

Thermoluminescence of sulfated zircon exposed to gamma radiation

International Nuclear Information System (INIS)

Rubio, E.; Castano, V.M.; Mendoza A, E.; Gonzalez, P.R.

2003-01-01

In this work, the thermoluminescent (Tl) signal induced by gamma radiation in zirconia and sulfated zirconia samples embedded in Ptfe pellets is reported and discussed. In this case, samples were obtained through sol-gel method using zirconium n-propoxide and H 2 SO 4 as precursors, and later were subjected to thermal treatment at 600 C to obtain, the tetragonal phase accordingly to X-ray diffraction analysis. Experimental results show that the thermoluminescent glow peak depends on both, the crystalline structure and sulfate concentration. Two maximum peaks were observed located at 147 C and 274 C arising from the electronic transitions. Tl response as a function of the absorbed dose shows a linear increase for a wide of range exposure as well as good stability in time. The high sensitivity, dose linearity and signal stability of this material open the potential possibility to be used for the dosimetry applications. (Author)

Investigation of the thermal stability of 210 deg. C TL peak of quartz and dating the components of terrazzo from the monastery church of Tegernsee

International Nuclear Information System (INIS)

Goeksu, H.Y.; Schwenk, P.; Semiochkina, N.

2001-01-01

The lifetime of the thermoluminescence (TL) peak of quartz observed at 210 deg. C using 5 deg. C/s heating rate is assessed using well-dated thermally isolated bricks from a monastery and exposed bricks from warmer climatic zones by comparing the absorbed dose obtained using the 210 deg. C TL peak with those obtained from 310 deg. C TL peak. The lifetimes of the 210 deg. C TL peak calculated for samples collected from thermally isolated excavations and exposed buildings are found to be clustered around 8000-10000 and 600-800 years, respectively. The results proved that 210 deg. C TL peak could be used for dating of samples younger than 1000 years without thermal correction if the samples are thermally isolated from their environment. TL ages are obtained using quartz, polyminerals from brick pieces as well as flint splinters, and other quartz inclusions extracted from the mortar of the terrazzo floor of the monastery church. The measured TL ages and the consistency of the results are discussed. The fine grains in the mortar, which contained calcite/aragonite, could not be dated using thermoluminescence due to presence of a very strong non-radiation induced TL glow

Thermoluminescence method for detection of irradiated food

International Nuclear Information System (INIS)

Pinnioja, S.

1998-01-01

A method of thermoluminescence (TL) analysis was developed for the detection of irradiated foods. The TL method is based on the determination of thermoluminescence of adhering or contaminating minerals separated from foods by wet sieving and treatment with high density liquid. Carbon tetrachloride provided a suitable alternative for foods that form gels with water. Thermoluminescence response of minerals in a first TL measurement is normalised with a second TL measurement of the same mineral sample after calibration irradiation to a dose of 5 kGy. The decision about irradiation is made on the basis of a comparison of the two TL spectra: if the two TL glow curves match in shape and intensity the sample has been irradiated, and if they are clearly different it has not been irradiated. An attractive feature of TL analysis is that the mineral material itself is used for calibration; no reference material is required. Foods of interest in the investigation were herbs, spices, berries and seafood. The presence of minerals in samples is a criterion for application of the method, and appropriate minerals were found in all herbs, spices and berries. The most common minerals in terrestrial food were tecto-silicates - quartz and feldspars - which with their intense and stable thermoluminescence were well suited for the analysis. Mica proved to be useless for detection purposes, whereas carbonate in the form of calcite separated from intestines of seafood was acceptable. Fading of the TL signal is considerable in the low temperature part of the glow curve during a storage of several months after irradiation. However, spices and herbs could easily be identified as irradiated even after two years storage. Conditions for seafood, which is stored in a freezer, are different, and only slight fading was observed after one year. The effect of mineral composition and structure on TL was studied for feldspars. Feldspars originating from subtropical and tropical regions exhibit lower TL

Thermoluminescence method for detection of irradiated food

Energy Technology Data Exchange (ETDEWEB)

Pinnioja, S

1998-12-31

A method of thermoluminescence (TL) analysis was developed for the detection of irradiated foods. The TL method is based on the determination of thermoluminescence of adhering or contaminating minerals separated from foods by wet sieving and treatment with high density liquid. Carbon tetrachloride provided a suitable alternative for foods that form gels with water. Thermoluminescence response of minerals in a first TL measurement is normalised with a second TL measurement of the same mineral sample after calibration irradiation to a dose of 5 kGy. The decision about irradiation is made on the basis of a comparison of the two TL spectra: if the two TL glow curves match in shape and intensity the sample has been irradiated, and if they are clearly different it has not been irradiated. An attractive feature of TL analysis is that the mineral material itself is used for calibration; no reference material is required. Foods of interest in the investigation were herbs, spices, berries and seafood. The presence of minerals in samples is a criterion for application of the method, and appropriate minerals were found in all herbs, spices and berries. The most common minerals in terrestrial food were tecto-silicates - quartz and feldspars - which with their intense and stable thermoluminescence were well suited for the analysis. Mica proved to be useless for detection purposes, whereas carbonate in the form of calcite separated from intestines of seafood was acceptable. Fading of the TL signal is considerable in the low temperature part of the glow curve during a storage of several months after irradiation. However, spices and herbs could easily be identified as irradiated even after two years storage. Conditions for seafood, which is stored in a freezer, are different, and only slight fading was observed after one year. The effect of mineral composition and structure on TL was studied for feldspars. Feldspars originating from subtropical and tropical regions exhibit lower TL

Thermoluminescence sensitivity of ulexite after UV irradiation

Energy Technology Data Exchange (ETDEWEB)

Topaksu, M., E-mail: mats@cu.edu.tr [Cukurova University, Arts-Sciences Faculty, Physics Department, 01330 Adana (Turkey); CIEMAT, Av. Complutense 22, 28040 Madrid (Spain); Correcher, V. [CIEMAT, Av. Complutense 22, 28040 Madrid (Spain); Garcia-Guinea, J. [Museo Nacional de Ciencias Naturales, (CSIC), C/José Gutiérrez Abascal 2, 28006 Madrid (Spain)

2015-04-15

Highlights: •UV-induced thermoluminescence emission of Turkish ulexite was studied. •There are three groups of components. •The UV exposures were performed at controlled temperatures. -- Abstract: The effects of UV radiation on the thermoluminescence (TL) properties of natural materials, in contrast to synthetic materials, have been scarcely studied. We report on the UV-induced thermoluminescence emission of a Turkish ulexite (NaCaB{sub 5}O{sub 6}(OH){sub 6}·5H{sub 2}O) that displays very complex TL glow curves, with at least three groups of components peaked at 130–140 °C, 240 °C and, 340 °C, wherein the last group is weaker. Such emission could be associated with structural changes in the lattice as well as alkali self-diffusion processes. The UV exposure performed at controlled temperatures (at room temperature (RT), 50 °C and 100 °C) produced a (i) different evolutions of the intensities of each maximum, which are directly related to the controlled thermal treatment; (ii) different intensity ratios among the groups of components; (iii) different activation energies (E{sub a}) (1.13 eV for RT, 0.99 eV for 50 °C and 0.49 eV for 100 °C) calculated using the initial rise method; and (iv) similar scattering values (12.4%, 8.2% and 12.8%), which were not a function of the controlled temperature. The thermal stability tests conducted on this borate at different temperatures, based on the T{sub stop} protocol, confirm the presence of a continuum in the distribution of the trap system with progressively increasing E{sub a} (from 0.60 to 0.90 eV)

Thermoluminescence characterization of LiMgF3: DyF3 phosphors exposed to beta radiation

International Nuclear Information System (INIS)

Bernal, R.; Alday S, K.R.; Brown, F.; Cruz V, C.; Furetta, C.; Cruz Z, E.; Kitis, G.

2006-01-01

LiMgF 3 : DyF 3 phosphors were obtained as polycrystalline solids from the melting of component salts, with two DyF 3 concentrations, 2.02 % mol, and 4.04 % mol. In order to guarantee the homogeneity of composition, the samples were crushed and the resulting powder was pressed to form pellet-shaped phosphors, some of which were sintered at 700 C for 5 h under air atmosphere. Thermoluminescence measurements of beta irradiated samples show that these phosphors exhibit adequate properties to be considered for development of thermoluminescence dosimeters. Integrated thermoluminescence as a function of dose displays a linear dependence with dose for doses below 20.0 Gy. (Author)

Thermoluminescence authentication of T'ang and Han Dynasty pottery

International Nuclear Information System (INIS)

Price, D.M.

1997-01-01

More than 80 pieces of T'ang Dynasty and 40 Han Dynasty style ceramic wares have been analysed to determine the amount of thermoluminescence (TL) accumulated since the initial firing of the object and the level of the radiation flux which has created the TL. This paper presents a summary of the thermoluminescence analysis results. Approximately 60% of Han ceramics and 45% of the T'ang pottery authenticated have been shown to belong to periods other than that stylistically suggested. Items which have been found not to be of the anticipated antiquity generally fall into distinct age groups. Of the T'ang wares the most commonly copied item is found to be the horse and for the Han pieces, human figures and ewers/pots/vases represent the most frequently reproduced wares

The thermoluminescence of carp otoliths: A fingerprint in ...

African Journals Online (AJOL)

use

2011-12-14

Dec 14, 2011 ... provide a quick and qualitative means for environmental assessments in lake pollution. Key words: Thermoluminescence, fish otolith, heavy-metal elements, lake, pollution. INTRODUCTION. Fish otoliths are widely .... cleaned HDPE plastic bottles that have been rinsed with sample three times prior to use.

The Properties of CaSO{sub 4}: Mn Thermoluminescence Dosimeters

Energy Technology Data Exchange (ETDEWEB)

Bjaerngard, Bengt

1963-06-15

The properties of the radio thermoluminescence of CaSO{sub 4}:Mn, used for dosimetry of gamma and roentgen radiation, have been investigated. The light yield of the luminophore has been determined to 1.5 percent for 1 MeV gamma radiation. The dependence of the thermoluminescence light sum on the exposure, the exposure rate, and the exposure time can qualitatively be described by the first order process model, modified by a broad energy distribution of the electron trap depths. Some applications are discussed. The cheapness of the dosimeters, the convenient read-out, and the broad range of measurable exposures suggest that CaSO{sub 4}:Mn can be a valuable complement to other dosimetry systems.

The thermoluminescence as tool in the reconstruction of volcanic events

International Nuclear Information System (INIS)

Ramirez L, A.; Schaaf, P.; Martin del Pozzo, A.L.; Gonzalez M, P.

2000-01-01

Within the Mexican land a great number of volcanoes are situated which a considerable part of them are still active. The relevance of dating pomex deposits, ash or lava of these poly genetic volcanoes is to determine the periodicity and magnitude of the volcanic events happened. In this work is presented the preliminary result of the dating by thermoluminescence in a pomex of a pyroclastic flux coming from a volcano in the state of Puebla with the purpose of providing elements to the knowledge which describe the eruptive history of the explosive volcanism at center of Mexico. For the sample dating the volcanic glasses of pomex were separated and it was applied the fine grain technique with a grain size between 4-11 μ m. In order to calculate the rate of annual dose it was carried out the following: in the determination of 238 U and 232 Th radioisotope concentration was used the neutron activation technique in a nuclear reactor, in the determination of the K 40 radioisotope was used a scanning electron microscope, the rate of environmental and cosmic dose was measured arranging Tl dosemeters of CaSO 4 : Dy in the sampling place. In order to calculate the paleodoses it was carried out the following: the equivalent dose (Q) was determined starting form the additive method and the supra linearity factor (I) starting from regenerative method and in both methods the irradiated process was realized with a 90 Sr beta source. With the above determinations it was calculated a paleodoses of 231 Gy and a rate of annual dose of 6.074 x 10 -3 Gy/year, estimating an age of: Age pomez = 231 Gy / 6.074 Gy x 10 -3 Gy /year = 38030 ± 4000 years. (Author)

Preliminary U-series disequilibrium and thermoluminescence ages of surficial deposits and paleosols associated with Quaternary fault, Eastern Yucca Mountain

International Nuclear Information System (INIS)

Paces, J.B.; Menges, C.M.; Bush, C.A.; Futa, K.; Millard, H.T.; Maat, P.B.; Whitney, J.W.; Widmann, B.; Wesling, J.R.

1994-01-01

Geochronological control is an essential component of paleoseismic evaluation of faults in the Yucca Mountain region. New U-series disequilibrium and thermoluminescence age estimates for pedogenic deposits that bracket surface-rupture events are presented from four sites exposing the Paintbrush Canyon, Bow Ridge and Stagecoach Road faults. Ages show an internal consistency with stratigraphic relationships as well as an overall concordancy between the two independent geochronometers. Age estimates are therefore interpreted to date depositional events or episodes of pedogenic carbonate mobility that can be used to establish a paleoseismic fault chronology. Ultimately, this type of chronological information will be used to evaluate seismic hazards at Yucca Mountain

Synthesis and thermoluminescence of LaAlO3:Pr3+ to UVC radiation dosimetry

International Nuclear Information System (INIS)

Morales-Hernández, A.; Zarate-Medina, J.; Contreras-García, M.E.; Azorín-Nieto, J.; Rivera-Montalvo, T.

2016-01-01

Thermoluminescent (TL) response of trivalent praseodymium ion doped lanthanum aluminate (LaAlO 3 :Pr 3+ ) obtained by Pechini method and Spray Dryer was studied. TL response of LaAlO 3 :Pr 3+ powders submitted at 1600 °C exhibited one peak centered at 157 °C. Sensitivity of LaAlO 3 :Pr 3+ was improved in around 90 times compared with undoped LaAlO 3 . TL response as a function of wavelength showed a maximum in 230 nm. Dosimetric characteristics of LaAlO 3 :Pr 3+ under UVR radiation effects were analyzed. Evaluation of activation energy was obtained by Glow Fit v.1.3 software. Experimental results about thermoluminescent characteristics of LaAlO 3 :Pr 3+ suggest as good candidate to be employed as a complementary thermoluminescent device with other TL phosphors as aluminum oxide - Highlights: • High sensitivity of new phosphor to UVC dosimetry was is studied. • Thermoluminescence response of LaAlO 3 :Pr 3+ is presented. • LaAlO 3 :Pr 3+ is suggested as UVCR dosimeter. • TL response of LaAlO 3 :Pr 3+ has dependence on sintering temperature.

Thermoluminescent characteristics of CaSO4:Dy+PTFE irradiated with high energy electron beams

International Nuclear Information System (INIS)

Alvarez, R.; Rivera, T.; Calderon, J. A.; Jimenez, Y.; Rodriguez, J.; Oviedo, O.; Azorin, J.

2011-10-01

In the present work thermoluminescent response of dysprosium doped calcium sulfate embedded in polytetrafluorethylene (CaSO 4 :Dy+PTFE) under high electron beam irradiations from linear accelerator for clinical applications was investigated. The irradiations were carried out using high electron beams (6 to 18 MeV) from a linear accelerator Varian, C linac 2300C/D, for clinical practice purpose. The electron irradiations were obtained by using the water solid in order to guarantee electronic equilibrium conditions. Field shaping for electron beams was obtained with electron cones. Glow curve and other thermoluminescent characteristics of CaSO 4 :Dy+PTFE were conducted under high electron beams irradiations. The thermoluminescent response of the pellets showed and intensity peak centered at around 235 C. Thermoluminescent response of CaSO 4 :Dy+PTFE as a function of high electron absorbed dose showed a linearity in a wide range. To obtain reproducibility characteristic, a set of pellets were exposed repeatedly for the same electron absorbed dose. The results obtained in this study can suggest the applicability of CaSO 4 :Dy+PTFE pellets for high electron beam dosimetry, provided fading is correctly accounted for. (Author)

The Chernobyl fallout in Greece and its effects on the dating of archaeological materials

International Nuclear Information System (INIS)

Liritzis, Y.

1987-01-01

The effects of the fallout from the nuclear reactor accident at Chernobyl have been monitored at various sites in Greece. Here we present the first estimates of gamma dose rates, an essential parameter in the dating of archaeological materials by thermoluminescence (TL) and ESR methods. The dose rates are derived from the long-lived radionuclides of 137 Cs, 134 Cs, 106 Ru and 144 Ce (with t 1/2 ≥ 1 yr). The present dose rates vary between 30 and 60 mrad/yr, but maximum values of around 811 mrad/yr have also been recorded, for ground-surface exposures. These dose rate values must be regarded as very significant to TL and ESR dating of samples from now on and a correction factor should be applied. (orig.)

Assessment of the potential for dating secondary calcite and quartz in fault zones

International Nuclear Information System (INIS)

Morency, Maurice

1982-03-01

Calcite and quartz occur frequently as secondary minerals in faults. In many instances these minerals are not deformed. Calcite, for example, often exhibits an undisturbed fibrous habit or appears as euhedral crystals. Direct dating of euhedral crystals would provide a minimum age of the last movement along a fault, whereas dating of fibrous crystals would furnish the real age of the last movement. This information would be essential in the evaluation and selection of sites for both nuclear power reactors and nuclear waste disposal. In the Canadian context, to be successful, the technique should be able to date minerals as old as tens of millions of years. In this study both isotopic and radioactive damage techniques were considered. It was found that thermoluminescence, thermally stimulated current, and electron spin resonance offer possibilities. Recent electron spin resonance studies of ancient flints have yielded dates of several hundred million years. It is anticipated that in the near future a combination of the above techniques will be extensively used in the field of geochronology

Thermoluminescence of pyramid stones

International Nuclear Information System (INIS)

Gomaa, M.A.; Eid, A.M.

1982-01-01

It is the aim of the present study to investigate some thermoluminescence properties of pyramid stones. Using a few grammes of pyramid stones from Pyramids I and II, the TL glow peaks were observed at 250 and 310 0 C, respectively. The TL glow peaks of samples annealed at 600 0 C, then exposed to 60 Co γ-rays were observed at 120, 190 and 310 0 C, respectively. The accumulated dose of natural samples is estimated to be around 310 Gray (31 krad). By assuming an annual dose is 1 mGy, the estimated age of pyramid stones is 0.31 M year. (author)

Thermoluminescence of pyramid stones

Energy Technology Data Exchange (ETDEWEB)

Gomaa, M A; Eid, A M [Atomic Energy Establishment, Cairo (Egypt)

1982-01-01

It is the aim of the present study to investigate some thermoluminescence properties of pyramid stones. Using a few grammes of pyramid stones from Pyramids I and II, the TL glow peaks were observed at 250 and 310/sup 0/C, respectively. The TL glow peaks of samples annealed at 600/sup 0/C, then exposed to /sup 60/Co ..gamma..-rays were observed at 120, 190 and 310/sup 0/C, respectively. The accumulated dose of natural samples is estimated to be around 310 Gray (31 krad). By assuming an annual dose is 1 mGy, the estimated age of pyramid stones is 0.31 M year.

N.R.P.B.'s new record-keeping service and thermoluminescent dosemeter

International Nuclear Information System (INIS)

Dennis, J.A.; Marshall, T.O.; Shaw, K.B.; Kendall, G.M.

1977-01-01

With the approval of the Health and Safety Executive the National Radiological Protection Board is introducing a radiation dose record keeping service in association with a thermoluminescent dosimeter. This service will relieve employers of the responsibility for maintaining and keeping dose records. Both the record keeping and dosimeter systems are described, including the documents which will be produced for employers. The thermoluminescent dosimeter is more accurate and less sensitive to environmental factors than the film dosimeter, which it replaces. It also reduces the consumption of materials and, with automated processing, is labour saving. (author)

Retrospective dosimetry assessment using the 380 deg. C thermoluminescence peak of tooth enamel

Energy Technology Data Exchange (ETDEWEB)

Secu, C.E. [National Institute for Materials Physics, PO Box MG-7, 77125 Bucharest-Magurele (Romania); Cherestes, M. [Dozimed Ltd., Dosimetry Laboratory, 77125 Bucharest-Magurele (Romania); Secu, M., E-mail: msecu@infim.ro [National Institute for Materials Physics, PO Box MG-7, 77125 Bucharest-Magurele (Romania); Cherestes, C.; Paraschiva, V. [Dozimed Ltd., Dosimetry Laboratory, 77125 Bucharest-Magurele (Romania); Barca, C. [Faculty of Physics, University of Bucharest, 77125 Bucharest-Magurele (Romania)

2011-10-15

The thermoluminescence (TL) response to gamma-ray irradiation of tooth enamel is reported. The tooth enamel was separated from dentine by using mechanical and physico-chemical procedures followed by grinding (grain size {approx}100 {mu}m) and etching. The TL was attributed to the recombination of CO{sub 2}{sup -} radicals incorporated into or attached to the surface of hydroxyapatite crystals. The growth of the {approx}380 deg. C TL peak with absorbed dose was examined with irradiated tooth enamel samples and reconstructed doses evaluated for tooth enamel samples from four human subjects. - Highlights: > Thermoluminescence response after gamma-ray irradiation of tooth enamel was investigated. > Thermoluminescence was attributed to the recombination of CO{sub 2}{sup -} radicals. > CO{sub 2}{sup -} radicals are produced inside or at the surface of hydroxyapatite crystals. > From the growth of the 380C peak reconstructed doses have been evaluated.

Mortar and surface dating with Optically Stimulated Luminescence (OSL): Innovative techniques for the age determination of buildings

International Nuclear Information System (INIS)

Panzeri, L.

2013-01-01

In this work the results of a dating study on bricks and mortars using both Thermoluminescence (TL) and Optically Stimulated Luminescence (OSL) are shown. The samples came from the outside walls of the Certosa di Pavia, located in northern Italy and independently dated (XVII-XVIII century). TL dating, applied to bricks using the fine grain technique, allowed to determine the time of manufacture of the bricks (XII century), that resulted therefore re-used. To circumvent this problem the application of two innovative dating techniques, OSL surface dating and mortar dating, was attempted. The first was applied to the light-shielded surfaces of bricks and allowed to successfully determine the edification of the wall (XVII century). Mortar dating gave instead severe age overestimation: the results obtained on coarse grain quartz with the SAR technique both on multi-grains aliquots and with single-grain analyses were highly dispersed indicating an incomplete bleaching of the quartz grains. The shine-down curves were in fact characterized by the absence of the so-called fast component, as confirmed by Linear Modulated OSL technique.

Use of signal subtraction methods in ESR dating of burned flint

International Nuclear Information System (INIS)

Porat, Naomi; Schwarcz, H.P.

1991-01-01

Geological samples of chert display some of the characteristics of electron spin resonance (ESR) signals of quartz. When chert is heated in a fireplace, most of these signals are annealed. The signals grow again in fire-heated chert buried in archaeological sites, as a result of internal and external radiation doses. The date of the heating event can be determined from the acquired dose (AD) and the dose rate. The E' and Al signals are best suited for dating. Although many cherts, when heated to a sufficient temperature, acquire a carbon radical (C) signal that largely obscures the E' signal, it can be subtracted from digitized spectra. The E' signal also appears to saturate at relatively low doses, restricting the time range of dating to between 200 and 600 ka, depending on the dose rates. The Al signal shows no saturation, but is also interfered with by organic signals, present in burnt and unburned flint. These can also be subtracted to reveal the ''pure'' Al signal. Applying the E' signal to date flint from Yabroud, we obtain an age between 100 and 125 ka, while both thermoluminescence (TL) dating of the flint and ESR dating of tooth enamel give 195 and 225 ka, respectively; the discrepancy may be due to an overestimate of the α-efficiency. At Nahr Ibrahim, the age (c. 80 ka) is consistent with archaeological estimates. (author)

Chernobyl fallout in Greece and its effects on the dating of archaeological materials

Energy Technology Data Exchange (ETDEWEB)

Liritzis, Y

1987-10-15

The effects of the fallout from the nuclear reactor accident at Chernobyl have been monitored at various sites in Greece. Here we present the first estimates of gamma dose rates, an essential parameter in the dating of archaeological materials by thermoluminescence (TL) and ESR methods. The dose rates are derived from the long-lived radionuclides of /sup 137/Cs, /sup 134/Cs, /sup 106/Ru and /sup 144/Ce (with t/sub 1/2/ greater than or equal to 1 yr). The present dose rates vary between 30 and 60 mrad/yr, but maximum values of around 811 mrad/yr have also been recorded, for ground-surface exposures. These dose rate values must be regarded as very significant to TL and ESR dating of samples from now on and a correction factor should be applied.

A survey of archaeological and geological samples dated in 1990

International Nuclear Information System (INIS)

Mejdahl, V.

1991-01-01

A survey of dated archaeological and geological samples is given, using thermoluminescence dating. Some of the sediment samples were also dated by means of optically stimulated luminescence (OSL) using a newly developed infrared diode system. In most cases the luminescence dates are in accordance with archaeological and geological estimates. Some discrepancies were found because some feldspar samples exhibited severe anomalous fading. It may be possible to avoid this problem by basing the dating on OSL of quartz. For sediment samples of Eemian or Early Weichselian age severe underestimates were encountered with both methods. The reason might be related to the large difference between the natural dose rate and that used in laboratory irradiations. Traps corresponding to low-temperature peaks such as the 150 deg. C peak in feldspars will remain almost empty under natural conditions, but will fill up to saturation under laboratory irradiation and thereby more charges will be captured in high-temperature traps. As a result, natural growth curves and laboratory produced luminescence growth curves will have different slopes and this will lead to underestimation. This problem might avoided by holding samples at an elevated temperature during laboratory irradiation, thus keeping the low-temperature traps empty. Preliminary experiments where feldspar samples were held at 130 deg. C during irradiation have given promising results. (AB) (31 refs.)

S K Date

Indian Academy of Sciences (India)

Home; Journals; Bulletin of Materials Science. S K Date. Articles written in Bulletin of Materials Science. Volume 23 Issue 2 April 2000 pp 97-101 Magnetic Materials. Comparison of the irreversible thermomagnetic behaviour of some ferro- and ferrimagnetic systems · P S Anil Kumar P A Joy S K Date · More Details Abstract ...

Preliminary research on thermoluminescence application in complicated geological situation

International Nuclear Information System (INIS)

Gong Gelian; Liu Chunsheng

2003-01-01

Thermoluminescent phenomenon resulting from two kinds of complicated geological situation, Ordos Basin and Huainan deposits in Anhui Province, is studied by the means of thermoluminescence counting method. It is shown that: (1) there are no apparent abnormalities of natural TL detected from the rock samples selected in the first 1000 meter depth of the Earth, and these natural TL are accumulated through natural radiation effects; (2) the natural TL shows statistically obvious reducing trends for the rock samples selected under the 2000 meter depth, and even no detectable TL is found for those rocks selected at 4000 meter depth. (3) the natural TL peaks corresponding to high temperature generally shift to the direction of higher temperature for the quartz-related rock samples, and several thermal events which occurred during the geological times might be responsible for this case

Models and methods in thermoluminescence

International Nuclear Information System (INIS)

Furetta, C.

2005-01-01

This work contains a conference that was treated about the principles of the luminescence phenomena, the mathematical treatment concerning the thermoluminescent emission of light as well as the Randall-Wilkins model, the Garlick-Gibson model, the Adirovitch model, the May-Partridge model, the Braunlich-Scharman model, the mixed first and second order kinetics, the methods for evaluating the kinetics parameters such as the initial rise method, the various heating rates method, the isothermal decay method and those methods based on the analysis of the glow curve shape. (Author)

Models and methods in thermoluminescence

Energy Technology Data Exchange (ETDEWEB)

Furetta, C. [ICN, UNAM, A.P. 70-543, Mexico D.F. (Mexico)

2005-07-01

This work contains a conference that was treated about the principles of the luminescence phenomena, the mathematical treatment concerning the thermoluminescent emission of light as well as the Randall-Wilkins model, the Garlick-Gibson model, the Adirovitch model, the May-Partridge model, the Braunlich-Scharman model, the mixed first and second order kinetics, the methods for evaluating the kinetics parameters such as the initial rise method, the various heating rates method, the isothermal decay method and those methods based on the analysis of the glow curve shape. (Author)

Natural dose level determination at Johor State with thermoluminescence dosimetry

International Nuclear Information System (INIS)

Ahmad Termizi Ramli; Yusof Jasman

1995-01-01

This paperwork presented the results of using thermoluminescence dosimetry (TLD) method in measuring background dose level, which is done at State of Johor, South Malaysia. The problems faced also discussed

Application of thermoluminescence dosimeter on the measurement of hard X-ray pulse energy spectrum

International Nuclear Information System (INIS)

Song Zhaohui; Wang Baohui; Wang Kuilu; Hei Dongwei; Sun Fengrong; Li Gang

2003-01-01

This paper introduces the application of thermoluminescence dosimeter (TLD) which composed by TLD-3500 reader and GR-100 M chips on the measurement of hard X-ray pulse energy spectrum. The idea using Filter Fluorescence Method (FFM) and TLD to measure hard X-ray pulse energy spectrum (from 10 keV to 100 keV) is discussed in details. Considering all the factors of the measuring surrounding, the measurement system of hard X-ray pulse has been devised. The calibration technique of absolute energy response of TLD is established. This method has been applied successfully on the radiation parameters measurement of the huge pulse radiation device-high-power pulser I. Hard X-ray pulse energy spectrum data of the pulser are acquired

Storage Telemetry of Radionuclide Tracers by Implantable Thermoluminescent Dosimeters

DEFF Research Database (Denmark)

Bojsen, J.; Møller, U.; Christensen, Poul

1977-01-01

A storage telemetrical method using thermoluminescent (TL) dosimeters for long-term measurements of incorporated radioactive substances in unrestrained rats has been developed. The system has been used in combination with radiotelemetrical registration of the circadian temperature rhythm. By sequ...

Thermoluminescence characterization of CVD diamond film exposed to UV and beta radiation

International Nuclear Information System (INIS)

Barboza-Flores, M.; Melendrez, R.; Gastelum, S.; Chernov, V.; Bernal, R.; Cruz-Vazquez, C.; Brown, F.; Pedroza-Montero, M.; Gan, B.; Ahn, J.; Zhang, Q.; Yoon, S.F.

2003-01-01

Thermoluminescence (TL) properties of diamond films grown by microwave and hot filament CVD techniques were studied. The main purpose of the present work was to characterize the thermoluminescence response of diamond films to ultraviolet and beta radiation. The thermoluminescence excitation spectrum exhibits maximum TL efficiency around 210-215 nm. All samples presented a glow curve composed of at least one TL peak and showed regions of linear as well as supralinear behavior as a function or irradiation dose. The linear dose dependence was found for up to sixteen minutes of monochromatic UV irradiation and 300 Gy for beta irradiated samples. The activation energy and the frequency factor were determined and found in the range of 0.33-1.7 eV and 5.44 x 10 2 -5.67 x 10 16 s -1 , respectively. The observed TL performance is reasonable appropriate to justify further investigation of diamond films as radiation dosimeters keeping in mind that diamond is an ideal TL dosemeter since it is tissue-equivalent and biological compatible. (copyright 2003 WILEY-VCH Verlag GmbH and Co. KGaA, Weinheim) (orig.)

The thermoluminescence of carp otoliths: A fingerprint in ...

African Journals Online (AJOL)

This paper reports a pilot study on the thermoluminescence (TL) of carbonate minerals of carp otoliths from the heavily polluted Baiyangdian Lake (BYD) in Hebei Province and non-polluted Miyun Water Reservoir (MY) in Beijing Municipality of China. Analyses on trace elements of otoliths and water show that the heavy ...

Imprints left by natural radioactivity in geological materials: uranium fission tracks and thermoluminescence applications in earth sciences

International Nuclear Information System (INIS)

Broquet, P.; Chambaudet, A.; Rebetez, M.; Charlet, J.M.

1994-01-01

In a rock, all minerals which contain uranium are host to a number of spontaneous fission phenomena forming a single damaged area called a ''latent track'', observations of which may lead to dating, uranium mapping and finding paleo-geo-thermometers (thermal history, used in oil exploration). The radioactive elements during the decay process release energy which is trapped as electrons into the physical or chemical defects of the crystalline lattice; this energy can be later released by heating the mineral (thermic stimulated luminescence); the thermoluminescence is characterized by a glow which spectrum constitutes a typical feature of the mineral, its crystallization conditions and the subsequent evolution of the material. Natural and induced glow curve may be produced. 6 figs., 52 refs

Thermoluminescence properties of Eu-doped and Eu/Dy-codoped Sr2 Al2 SiO7 phosphors.

Science.gov (United States)

Jadhaw, Akhilesh; Sonwane, Vivek D; Gour, Anubha S; Jha, Piyush

2017-11-01

We report the thermoluminescence properties of Sr 1.96 Al 2 SiO 7 :Eu 0.04 and Sr 1.92 Al 2 SiO 7 :Eu 0.04 Dy 0.04 phosphors. These phosphors were prepared by a high-temperature solid-state reaction method. The prepared phosphors were characterized by X-ray diffraction. A 254 nm source was used for ultraviolet (UV) irradiation and a 60 Co source was used for γ-irradiation. The effect of heating rate and UV-exposure were examined. The thermoluminescence temperature shifts to higher values with increasing heating rate and thermoluminescence intensity increases with increasing UV exposure time. The trapping parameters such as activation energy (E), order of kinetics and frequency factor (s) were calculated by peak shape method. The effect of γ- and UV-irradiation on thermoluminescence studies was also examined. Copyright © 2017 John Wiley & Sons, Ltd.

TL and radiocarbon dating of neolithic sepultures from Sudan: intercomparison of results

International Nuclear Information System (INIS)

Guibert, P.; Ney, C.; Bechtel, F.; Schvoerer, M.; Geus, F.

1994-01-01

Thermoluminescence dating of a set of 29 pottery sherds excavated at the neolithic sites of El Kadada and El Ghaba (near Shendi, Central Sudan) was carried out at Bordeaux University. The archaeological dose was measured using the fine grain technique. The annual dose was determined by analytical techniques (neutron activation analysis, ICP spectrometry, XRF, low background gamma spectrometry) and by ''on-site'' measurements of the environmental radioactivity (gammametry). The crystalline inclusions of the samples were characterized by optical microscopy and cathodoluminescence: the TL minerals mainly consist of quartz and K-feldspar crystals. In some cases, radioactive inclusions of zircons and monazites are observed. The TL and the radiocarbon dates show a good agreement, verifying the validity of the radiocarbon ages which were suspected to be too old because of the nature of the dated material (shells). Taking into account all the chronological data, it is shown that El Ghaba and El Ghaba necropolis were used respectively within the 4800-3300 B.C. and 4200-3000 B.C. date-ranges for neolithic cultures, the occupation of El Kadada starting five or six centuries later than El Ghaba. (Author)

Phosphor for thermoluminescent type radiation dosimeter

International Nuclear Information System (INIS)

Nada, N.; Yamashita, T.

1975-01-01

This has the accumulation effect of radiation energy and is mainly used as the element for thermoluminescent type radiation dosimeters. It has as the principal constituent a phosphor consisting of calcium sulfate as the principal constituent and other impurity elements such as dysprosium, thulium and the like. It is more sensitive by the order of 1 to 2 or more figures than the conventional ones and is excellent in the retention of absorbed radiation energy. (U.S.)

A pocket type thermoluminescent personnel dosimeter

International Nuclear Information System (INIS)

Vora, K.G.; Nagpal, J.S.; Pendurkar, H.K.; Gangadharan, P.

1979-01-01

A pocket type thermoluminescent personnel dosemeter using CaSO 4 : Dy phosphor is described. Two glass capillaries containing the phosphor are fitted into a plastic tube and covered by a cylindrical filter. The combination is fitted into an ink barrel of a fountain pen. The response of this Dy glass dosimeter was studied for various incident photon energies. A uniform response over the energy range from 33 keV to 1250 keV is achieved. (A.K.)

Thermoluminescence dating of abyssal deposits in the north region of the South China Sea

International Nuclear Information System (INIS)

Peng Xiaoxian

1988-01-01

The ages of abyssal deposits have been studied by TL dating. The ages of the deposits from the wells Weima 1, 5 and 6 at the slope in the north of the South China Sea are 36,100 and 128 thousand years respectively

Application of numerical analysis methods to thermoluminescence dosimetry

International Nuclear Information System (INIS)

Gomez Ros, J. M.; Delgado, A.

1989-01-01

This report presents the application of numerical methods to thermoluminescence dosimetry (TLD), showing the advantages obtained over conventional evaluation systems. Different configurations of the analysis method are presented to operate in specific dosimetric applications of TLD, such as environmental monitoring and mailed dosimetry systems for quality assurance in radiotherapy facilities. (Author) 10 refs

Thermoluminescence dosimetry of gamma rays from the fallout of the Semipalatinsk nuclear tests

International Nuclear Information System (INIS)

Takada, J.; Hoshi, M.; Endo, S.; Yamamoto, M.; Nagatomo, T.; Gusev, B.I.; Rozenson, R.I.; Apsalikov, K.N.; Tchaijunusova, N.J.

1996-01-01

Field missions were sent to several settlements near the Semipalatinsk nuclear test site out in order to investigate dosimetry for the residents in 1995. The results of measurements of environmental radiation doses and thermoluminescence dosimetry in some villages near the Semipalatinsk nuclear test site are presented. The radiation levels in several villages are the natural background level in 1995, 6 years after the final nuclear explosion. On the other hand, thermoluminescence dosimetry revealed significant radiation exposure to residents in this area due to nuclear tests. (author)

Image in nuclear dosimetry using thermoluminescent dosimetry

International Nuclear Information System (INIS)

Guinsburg, G.; Matsuoka, M.; Watanabe, S.

1987-01-01

A low cost methodology to produce images of internal sick organs by radioisotopic intake, is presented. Dosimetries of thermoluminescent material and Teflon (ratio:50%) in bidimensional matrix shape are used with a Pb collimator. This collimator-bidimensional matrix system was tested ''in vivo'' and in thyroid phantoms using 99m Tc. A comparative evaluation between this method and the scintigraphy one is presented. (M.A.C.) [pt

Optical dating of potteries excavated from Pungnabtoseong earthen wall, Seoul

Energy Technology Data Exchange (ETDEWEB)

Kim, Myung Jin; Park, Mi Seon [Neosiskorea Co., Daejeon (Korea, Republic of); Lee, Sung Joon; Nah, Hye Rim; Hong, Hyung Woo [National Research Institute of Cultural Heritage, Daejeon (Korea, Republic of)

2012-05-15

Thermoluminescence (TL) and optically stimulated luminescence (OSL) emitted from natural crystalline mineral, usually quartz, feldspar, and so on, are mainly used to evaluate the paleodose for the age determination of archaeological and geological sample and the equivalent dose for retrospective dosimetry. TL/OSL age can be calculated as the ratio of paleodose to total annual dose rate which is determined from surrounding soil. In this study, we chemically extracted the quartz samples from potteries excavated in Pungnabtoseong earthen wall and observed the TL/OSL characteristics for paleodose determination. With the converted annual dose rate from the concentration of radioactive isotopes in its surrounding soil, optical date was evaluated and finally illustrated for interpreting the construction stage of Pungnabtoseong

The fast neutron response of 7LiF thermoluminescent dosemeters

International Nuclear Information System (INIS)

Knipe, A.D.

1990-02-01

A series of experiments was performed in 1982 to determine the neutron energy response of the 7 LiF thermoluminescent dosemeter (TLD) employed in European zero power fast reactor gamma-ray energy deposition studies. Preliminary results of this work were included in a 1985 International experimental data-base of TLD neutron sensitivities and provided the most consistent set of data within the 7 LiF compilation. A more detailed interpretation of these data has improved the results still further, giving a mean relative neutron to gamma efficiency of 0.118±0.005. The main objective of this re-evaluation was to establish recommended neutron energy response values to replace a 1974 data set for the analysis of in-core fast reactor measurements. This was achieved by combining the mean experimental relative efficiency of 0.118 with calculated energy dependent kerma factors. The kerma factors for the TLD were based on US National Bureau of Standards values and a composition determined by chemical analysis. Adoption of the revised neutron energy response data set produces a small increase in the measured gamma-ray energy deposition of typically 2% relative to the 1974 data. However, more importantly, the detailed analysis of the experimental response data has significantly improved confidence in the neutron corrections applied to in-core TLD gamma-ray energy deposition measurements. (author)

Chronology of Chichen Izta, evidences by thermoluminescence

International Nuclear Information System (INIS)

Ramirez, A.; Schaaf, P.; Gonzalez, P.R.; Chung, H.

2002-01-01

The establishment of the chronology of Chichen Itza is argued by its stylistic evocations, architectural and iconographical as well as its history related in the sources, as the Chilam Balam, where is named the arrival of foreign tribes as the Xiu and the Itzaes and its settlement in Chichen Itza as well as the return to its origin place. The material evidence of such transition is reflected in the ceramic change of the Pizarra Puuc to the Pizarra Chichen, however, in 13 stratigraphic wells realized in different points of Chichen Itza, it was not found evidence of the layer of the Pizarra Puuc period. In this work the obtained ages of dating by thermoluminescence (TL) are presented, of four samples of ceramics found in the different wells. When our results are compared with the estimated ages for the different groups of ceramics, it was observed that none of they corresponded to the Pizarra Puuc period. These results strenghten the observations realized during excavations, causing the suggestion of new inferences related to the Chichen Itza boom and its relationship with the Maya Classic Period. The used technique for the TL dating was that of fine grain. The interval of artificial dose, of beta radiation of Strontium 90 was between 2 and 30 Gy. The TL signal was obtained heating the samples at 10 C/s until reaching 500 C in the TL Daybreak reader equipment. In order to know the annual dose rate of concentration of potassium ( 40 K) by means of the microanalysis technique in the scanning electron microscope was determined, while the uranium content (2 38 U) and thorium ( 232 Th) were determined by means of the neutron activation analysis technique using the TRIGA Mark III nuclear reactor. The contribution of the gamma radiation of the soil as well as the contribution of the cosmic radiation was measured with TL dosemeters of CaSO 4 :Dy + Ptfe once the paleodose was known and the annual dose rate of each sample of its age was estimated. (Author)

Thermoluminescent properties of CaSO4:Dy prepared by precipitation method

International Nuclear Information System (INIS)

Roman, J.; Rivera, T.; Azorin, J.

2009-10-01

This paper reports the synthesis and thermoluminescent (Tl) characterization of CaSO 4 :Dy obtained by the precipitation method. Thermoluminescent CaSO 4 :Dy powder and Teflon (PTFE) were mixed in order to obtain samples in pellets form. Samples of CaSO 4 :Dy were exposed to a radiation gamma source of 60 Co and 90 Sr beta particles. Tl response of CaSO 4 :Dy showed a glow curve with two peaks centered at around 164 and 302 C. Tl phosphor showed a good linearity in the range from 0.5 to 30 Gy. Fading of the Tl information was 5.19 % in 37 days and presented a standard deviation of 4% for reproducibility. (Author)

Optically stimulated luminescence dating of archaeological ceramics from Osvaldo and Lago Grande sites in central Amazon

International Nuclear Information System (INIS)

Hazenfratz, Roberto; Tudela, Diego R.G.; Munita, Casimiro S.; Mittani, Juan C.R.; Tatumi, Sonia H.

2013-01-01

Thermoluminescence (TL) and optically stimulated luminescence (OSL) dating are two important techniques for dating archaeological and geological material, especially suitable for archaeological ceramics, where samples for 14 C dating are not available. In this work, five pottery shards from Osvaldo and Lago Grande archaeological sites were dated by OSL. For measurements, it was used the SAR protocol. The annual dose rates were estimated by the contents of U, Th and K, determined by instrumental neutron activation analysis (INAA) of the pottery shards and clay samples near both sites. Lago Grande and Osvaldo represent a microcosm of the region, and their proximity and high density of archaeological record turn them interesting to study possible relations of cultural and/or commercial exchange. Calculations showed that the water content is an important variable that cannot be neglected in OSL dating of pottery shards from central Amazon, due to the high humidity in regional soils. The results between 867 ± 101 and 1154 ± 62 years AD agreed with the average time span for the archaeological sites occupation found in the literature. (author)

Optically stimulated luminescence dating of archaeological ceramics from Osvaldo and Lago Grande sites in central Amazon

Energy Technology Data Exchange (ETDEWEB)

Hazenfratz, Roberto; Tudela, Diego R.G.; Munita, Casimiro S., E-mail: robertohm@ipen.br [Instituto de Pesquisas Energeticas e Nucleares (IPEN/CNEN-SP), Sao Paulo, SP (Brazil); Mittani, Juan C.R.; Tatumi, Sonia H. [Universidade Federal de Sao Paulo (UNIFESP), Santos, SP (Brazil)

2013-07-01

Thermoluminescence (TL) and optically stimulated luminescence (OSL) dating are two important techniques for dating archaeological and geological material, especially suitable for archaeological ceramics, where samples for {sup 14}C dating are not available. In this work, five pottery shards from Osvaldo and Lago Grande archaeological sites were dated by OSL. For measurements, it was used the SAR protocol. The annual dose rates were estimated by the contents of U, Th and K, determined by instrumental neutron activation analysis (INAA) of the pottery shards and clay samples near both sites. Lago Grande and Osvaldo represent a microcosm of the region, and their proximity and high density of archaeological record turn them interesting to study possible relations of cultural and/or commercial exchange. Calculations showed that the water content is an important variable that cannot be neglected in OSL dating of pottery shards from central Amazon, due to the high humidity in regional soils. The results between 867 ± 101 and 1154 ± 62 years AD agreed with the average time span for the archaeological sites occupation found in the literature. (author)

Thermoluminescence: how safe are we? ask the crystals

International Nuclear Information System (INIS)

Madiyal, Ananya; Alva, Priyadharshini

2013-01-01

Thermoluminescence means 'light emitted from heat'. Thermoluminescent dosimeter (TLD) is a type of radiation measuring instrument used for the measurement of actual dose received by the operator or patient as a result of radiographic exposure. TLD calculates the ionising radiation exposure by measuring the amount of visible light emitted from a crystal in the detector when the crystal is heated. The two types of TLD are Calcium Fluoride type and the Lithium Fluoride type. The former is used for environmental detection of radiation exposure while the latter is used for detection of personal radiation exposure. A TLD card consists of a nickel plated aluminium plate and 3 filters. The equipment used to heat the exposed material and measure the emitted light produced by heat is called TLD reader. It comprises of a heater, a photomultiplier tube and the electronic system. TLD is used to measure the dose received by a patient while undergoing radiotherapy, for radio-diagnosis and as personnel monitoring devices. It has the advantage of being small in size, chemically inert, accurate and gives a reproducible reading. (author)

An experimental system for thermoluminescent dosimetry

International Nuclear Information System (INIS)

Perry, K.E.G.; George, E.

1965-08-01

A thermoluminescent dosimeter (T.L.D.) reader has been developed for experimental investigations on the use of lithium fluoride for 'finger tip' dosimetry. The design of the reader is based on the maximum use of standard electronic units in the A.E.R.E. Type 2000 series but some new unit development has been necessary. The reader gives improved experimental facilities over present commercially-available designs. The technique for 'finger-tip' dosimetry is described and the initial experimental results are given. (author)

Treatment verification and in vivo dosimetry for total body irradiation using thermoluminescent and semiconductor detectors

International Nuclear Information System (INIS)

Oliveira, F.F.; Amaral, L.L.; Costa, A.M.; Netto, T.G.

2014-01-01

The objective of this work is the characterization of thermoluminescent and semiconductor detectors and their applications in treatment verification and in vivo dosimetry for total body irradiation (TBI) technique. Dose measurements of TBI treatment simulation performed with thermoluminescent detectors inserted in the holes of a “Rando anthropomorphic phantom” showed agreement with the prescribed dose. For regions of the upper and lower chest where thermoluminescent detectors received higher doses it was recommended the use of compensating dose in clinic. The results of in vivo entrance dose measurements for three patients are presented. The maximum percentual deviation between the measurements and the prescribed dose was 3.6%, which is consistent with the action level recommended by the International Commission on Radiation Units and Measurements (ICRU), i.e., ±5%. The present work to test the applicability of a thermoluminescent dosimetric system and of a semiconductor dosimetric system for performing treatment verification and in vivo dose measurements in TBI techniques demonstrated the value of these methods and the applicability as a part of a quality assurance program in TBI treatments. - Highlights: • Characterization of a semiconductor dosimetric system. • Characterization of a thermoluminescent dosimetric system. • Application of the TLDs for treatment verification in total body irradiation treatments. • Application of semiconductor detectors for in vivo dosimetry in total body irradiation treatments. • Implementation of in vivo dosimetry as a part of a quality assurance program in radiotherapy

The application of thermoluminescence dosimeter on the measurement of hard X-ray pulse energy spectrum

International Nuclear Information System (INIS)

Song Zhaohui; Wang Baohui; Wang Kuilu; Hei Dongwei; Sun Fengrong; Li Gang

2001-01-01

This paper introduce the application of thermoluminescence dosimeter (TLD) which composed by TLD-3500 Reader and TLD-100M chips on the measurement of hard X-ray pulse energy spectrum. The idea, using Filter Fluorescence Method (FFM) and TLD to measure hard X-ray pulse energy spectrum (from 10 keV to 100 keV), is discussed in details. Considering all the factors of the measuring surroundings, the measurement system of hard X-ray pulse has been devised. The calibration technique of absolute energy response of TLD is established. This method has been applied successfully on the radiation parameters measurement of the huge pulse radiation device -high-power pulser I. Hard X-ray pulse energy spectrum data of the pulser are acquired

Performance tests on the NRPB thermoluminescent dosemeter

CERN Document Server

Shaw, K B

1977-01-01

Performance tests on the thermoluminescent dosemeter, designed at NRPB for use in the automated personal dosimetry system, are described. An ultra-thin lithium borate dosemeter has been developed for skin absorbed dose measurement. The X-ray, gamma-ray and beta-ray energy response of the dosemeter has been investigated and the angular response for the dosemeter has been examined. The annealing, read-out and stabilisation procedures for the dosemeter are described.

Comparative study of thermoluminescence detection methods for irradiated spices

International Nuclear Information System (INIS)

Kawamura, Y.; Kojima, K.; Sugita, T.; Yamada, T.; Saito, Y.

1995-01-01

The thermoluminescence (TL) detection methods for irradiated spices were compared using spice samples obtained on the Japanese market, irradiated at doses of 1, 5, 10 and 30 kGy and stored for 1 year before analysis. The TL intensities of irradiated spices were stable for 1 year after irradiation. Measurement with whole samples failed to identify irradiated samples. Minerals were separated from spices in sodium tungstate saturated solution and/or sodium polytungstate solution. The TL intensity of minerals which had undergone irradiation was significantly increased for all samples. However, the ranges of TL intensity of irradiated and unirradiated samples overlapped. Clear discrimination has been obtained between the TL ratios of irradiated and unirradiated spices by using normalized measurement with reirradiation. The detection limit in terms of irradiation dose is 1 kGy even in a sample that has been irradiated 1 year prior to analysis. Normalization is the best technique currently available for thermoluminescence analysis to identify irradiated spices

Thermoluminescence as a probe in bioactivity studies; the case of 58S sol-gel bioactive glass

International Nuclear Information System (INIS)

Polymeris, George S; Tsirliganis, Nestor C; Goudouri, Ourania Menti; Paraskevopoulos, Konstantinos M; Kontonasaki, Eleana; Kitis, George

2011-01-01

The formation of a carbonated hydroxyapatite (HCAp) layer on the surface of bioactive materials is the main reaction that takes place upon their immersion in physiological fluids. To date, all techniques used for the identification of this HCAp formation are rather time consuming and not well suited to detailed and rapid monitoring of changes in the bioactivity response of the material. The aim of this work is to explore the possibility of using thermoluminescence (TL) for the discrimination between different bioactive responses in the case of the 58S bioactive glass. Results provided strong indications that the 110 deg. C TL peak of quartz can be used effectively in the study of the bioactive behaviour of 58S bioactive glass, since it is unambiguously present in all samples and does not require deconvolution analysis. Furthermore, the intensity of the 110 deg. C TL peak is proven to be very sensitive to the different bioactive responses, identifying the loss of silica which takes place at the first stages of the sequence. The discontinuities of the 110 deg. C TL peak intensity plot versus immersion time at 8 and 1440 min provide experimental indications regarding the timescale for both the beginning of amorphous CaP formation as well as the end of crystalline hydroxyl-apatite formation respectively, while the spike in the sensitization of the 110 deg. C TL peak, which was observed for immersion times ranging between 20 and 40 min, could be an experimental feature indicating the beginning of the crystalline HCAp formation.

Thermoluminescence of irradiated foods

International Nuclear Information System (INIS)

Wagner, U.; Helle, N.; Boegl, K.W.; Schreiber, G.A.

1993-01-01

This report describes developments and applications of the thermoluminescence (TL) analysis of mineral contaminants in foods. Procedures are presented to obtain minerals from most different products such as pepper, mangos, shrimps and mussels. The effect of light exposure during the storage of foods on the TL intensity of minerals is examined and corresponding conclusions for routine control are drawn. It is also shown that the normalization of TL intensities - the essential step to identify irradiated samples - can not only be achieved by γ, X or β rays but also by UV radiation. The results allow the conclusion that a clear identification of any food which has been irradiated with more than 1 kGy is possible if enough minerals can be isolated. (orig.)

Accuracy and precision in thermoluminescence dosimetry

International Nuclear Information System (INIS)

Marshall, T.O.

1984-01-01

The question of accuracy and precision in thermoluminescent dosimetry, particularly in relation to lithium fluoride phosphor, is discussed. The more important sources of error, including those due to the detectors, the reader, annealing and dosemeter design, are identified and methods of reducing their effects on accuracy and precision to a minimum are given. Finally, the accuracy and precision achievable for three quite different applications are discussed, namely, for personal dosimetry, environmental monitoring and for the measurement of photon dose distributions in phantoms. (U.K.)

Thermoluminescent dosemeters characterization for patient dosimetry in diagnostic radiology preliminary results

International Nuclear Information System (INIS)

Castro, William J.; Squair, Peterson L.; Gonzaga, Natalia B.; Nogueira, Maria S.; Silva, Teogenes A. da

2009-01-01

The determination of the metrological characteristics of thermoluminescent (TL) dosimeters plays an important role in dosimetry of patients submitted to x-ray examinations for diagnostic purpose. Entrance surface doses can be measured with TL dosimeters to verify the compliance with the diagnostic reference levels. Organ doses can be estimated through TL measurements in an anthropomorphic phantom which it allows the radiation risk assessment. In this work, LiF:Mg,Ti (TLD-100) rod and chip thermoluminescent dosimeters were characterized considering their use for patient dosimetry in computerized tomography and mammography. Preliminary results showed that TL dosimeters have a response reproducibility of 7.8% and 4.8% and homogeneity of 18.4% and 6.5% for rod and chip shapes, respectively. (author)

Persistent luminescence and thermoluminescence of UV/VIS -irradiated SrAl2O4: Eu2+, Dy3+ phosphor

International Nuclear Information System (INIS)

Pereyda-Pierre, C.; Meléndrez, R.; García, R.; Pedroza-Montero, M.; Barboza-Flores, M.

2011-01-01

The persistent luminescence and thermoluminescence properties of SrAl 2 O 4 : Eu 2+ , Dy 3+ phosphors excited with UV–VIS light in the 200–500 nm region were investigated. The thermoluminescence glow curve was found to be composed of peaks around 70, 125 and 245 °C. The persistent luminescence and thermoluminescence excitation spectra exhibited a broad band around 300–500 nm centered at 400 and 420 nm respectively. A linear behavior of the integrated thermoluminescence intensity and persistent luminescence versus irradiation time was found for the first 60 s. The charge detrapping from the 70 °C trapping levels was the major contributor to the observed persistent luminescence at room temperature. The SrAl 2 O 4 : Eu 2+ , Dy 3+ phosphors have suitable properties to be applied as storage and persistent luminescence UV–VIS irradiation dose phosphor. -- Highlights: ► SrAl 2 O 4 :Eu 2+ , Dy 3+ persistent luminescence and thermoluminescence was measured. ► The phosphor was irradiated with UV–VIS photons in the 200–500 nm wavelength range. ► SrAl 2 O 4 :Eu 2+ , Dy 3+ behaves adequately as persistent and storage UV–VIS dosimeter. ► The persistent luminescence dosimetry does not require heat or light stimulation.

Development of a nano structured system based on zirconia and Co nanoparticles for thermoluminescent applications: sensor of gamma and UV radiation

International Nuclear Information System (INIS)

Villa S, G.

2014-01-01

Powders of zirconium IV oxide as well as systems composed of zirconia nano crystals and cobalt nanoparticles (ZrO 2 :NPCo) with dimensions of nanometers were synthesized by the sol-gel method. Zirconia and ZrO 2 :NPCo systems have crystalline structure tetragonal or monoclinic is the heat treatment was to 500 and 1000 degrees Celsius respectively. The characterization of the synthesized materials consisted of a morphological and structural analysis, the information obtained was correlated to its thermoluminescent response induced by gamma and ultraviolet radiation. Thermoluminescent behavior was analyzed on different concentrations of cobalt nanoparticles incorporated during the synthesis process of the zirconium oxide. The monoclinic structure has the highest sensitivity thermoluminescent induced by ultraviolet and gamma radiation. Moreover, the thermoluminescence intensity decreased considerably in ZrO 2 :NPCo systems and was induced the growth of a glow peak at 280 degrees Celsius. In most of the materials analyzed the relation of the thermoluminescence intensity depending the time of irradiation with ultraviolet light showed the saturation of the traps in the material after 60 s of irradiation. Using gamma radiation is observed a behavior linear in the applied dose range between 0.25 Gy and 450 Gy. The growth of a glow peak at 280 degrees Celsius is the most important change in the thermoluminescence characteristics of zirconia. The ZrO 2 :NPCo systems can be used in the development of thermoluminescent dosimeters for detecting gamma radiation fields mainly. (Author)

Thermoluminescent dose measurements on board Salyut type orbital stations

International Nuclear Information System (INIS)

Akatov, Yu.A.; Arkhangelskij, V.V.; Aleksandrov, A.P.

1984-06-01

A small, vibration- and shock-resistant thermoluminescent dosemeter (TLD) system - named PILLE - was developed for orbital stations at the Central Research Institute for Physics, Hungary, to measure the cosmic radiation dose on-board. The first on-board measurements with this system were performed by B. Farkas, the Hungarian astronaut, on the Salyut-6 space station in 1980. The same instrument was used by other crews in the following years. Doses measured at different sites in Salyut-6 are presented. The dose rates varied from 0.7 to 0.11 mGy.day -1 . After the first cosmic measurements, the system was further developed. The minimum detectable dose of the new TLD system is 1 μGy, i.e. less by one order of magnitude than that of the former system. The self-irradiation dose rate of the TLD bulbs is also reduced by more than an order of magnitude to 10 nGy.h -1 , by use of potassium-free glass for the bulb envelope. This new type of PILLE TLD system is currently on-board Salyut-7. The dose rates (0.12-0.23 mGy.day -1 ) measured in 1983 are presented in detail. (author)

Thermoluminescence dosimetry materials: properties and uses

International Nuclear Information System (INIS)

McKeever, S.W.S.; Moscovitch, M.; Townsend, P.D.

1995-01-01

This book selects a range of the most popular thermoluminescence dosemeter (TLD) materials in use today and provides a critical account of their thermoluminescence (TL) and dosimetric properties. The information provided includes in-depth discussions of TL mechanisms, including an account of luminescence properties, and relevant information regarding dosimetric characteristics. The book is intended for those involved in TLD materials research, and for technicians and workers involved in the practical application of these materials in TL dosimetry. The advent of modern spectroscopic methods for measuring TL emission spectra (the so-called ''3-D'' presentation) seemed to the authors to be an invitation to compile such spectra for all the major TLD materials. Further consideration led to an expansion of the initial idea to include a compilation of dosimetric properties. One intention is to provide a synopsis of the TL and dosimetric properties of the most widely used TLD materials currently available and to form a link between the solid state defect properties of these materials and their actual dosimetric properties. A second intention is to provide a solid framework from which future studies of TLD materials could be launched. Too often in the past research into TLD materials has been haphazard, to say the least. By illustrating the links between solid state physics and the radiation dosimetry properties of these materials the book points to the future and to the pressing need for enhanced research on TLD materials. (Author)

Evaluation of glasses containing cadmium for high dose dosimetry by the thermoluminescence technique

International Nuclear Information System (INIS)

Carvalho, Gabriel Soares Marchiori de; Ferreira, Pamela Zati; Cunha, Diego Merigue da; Dantas, Noelio Oliveira; Silva, Anielle C.A.; Perini, Ana Paula; Neves, Lucio Pereira; Carrera, Betzabel Noemi Silva; Watanabe, Shigueo

2016-01-01

New glass matrices were evaluated for high dose dosimetry by the thermoluminescence technique. Their nominal composition are 20Li_2CO_3.10Al_2O_3.15CdO.55B_2O_3 and 20Li_2CO_3.10Al_2O_3.20CdO.50B_2O_3 (mol%). The glass matrices were irradiated with different doses: 50, 100, 200, 500, 700 and 900 Gy, and the thermoluminescence emission curves were obtained for each of these values. The results show a great potential of using these matrices in high dose dosimetry. (author)

Synthesis and thermoluminescence characterization of Na6Mg(SO4)4:RE (RE = Ce, Tb) phosphors

International Nuclear Information System (INIS)

Kore, Bhushan P.; Dhoble, N.S.; Dhoble, S.J.

2014-01-01

Thermoluminescence (TL) properties of sulfate-based phosphors activated by different rare earths have received tremendous attention to the field of radiation dosimetry. Those TL materials based on CaSO 4 have been widely applied for medical and environmental dosimetry. Taking this fact into account we have synthesized Na 6 Mg(SO 4 ) 4 doped with Ce and Tb by wet chemical method. The prepared phosphor was characterized by XRD, FTIR, photoluminescence (PL) and thermoluminescence. For TL study, the phosphor is irradiated with γ-rays from 60 Co source. For studying luminescence properties, the prepared phosphor was annealed at different temperatures and effects of these annealing temperatures on Na 6 Mg(SO 4 ) 4 samples are investigated and quantified. The changes in the glow curve and PL emission spectrum are also investigated as a function of annealing temperature and the annealing temperature was optimized. For calculation of trapping parameters various methods such as peak shape (PS) method, initial rise (IR) method, various heating rate (VHR) method, and computerized glow curve deconvolution (CGCD) are employed. - Highlights: • Na 6 Mg(SO 4 ) 4 phosphor was successfully prepared by wet chemical method. • Effect of annealing temperatures on PL and TL properties has been studied. • Different trap analysis methods were used for calculating the trapping parameters. • Effect of these methods on activation energies were investigated in detail

Recent research into thermoluminescent dosimetry

Energy Technology Data Exchange (ETDEWEB)

Nakajima, T [National Inst. of Radiological Sciences, Chiba (Japan)

1979-04-01

The trend of basic research in thermoluminescent dosimetry (TLD), the results, and developing fields in which it can be applied are reported. This trend is outlined from the viewpoint fields of application, a new trend in TLD readers, the conditions of development of new photogenic substances, and research in the radiation characteristics of photogenic substances (radiosensitivity to particle rays and ultraviolet rays, dose rate dependence, temperature dependence at irradiation, and ..gamma.. ray energy dependence). Utilization of TLD in the medical field for measurement of environmental radiation and as a monitor for workers exposed to radiation is discussed. An international comparison of dose was necessary in order to prove its universal validity.

Thermoluminescence study of lithium fluorides

CERN Document Server

Abu-Alazm, S M

2003-01-01

The spectrum of the light emitted during thermoluminescence (TL) from irradiated lif sample with different doses of Xe, Kr and electrons have been studied. The results show a main peak for all samples irradiated and unirradiated at temperature about 200 degree C. Morcever when the reaches to the value 5x10 sup 1 1 ion/cm sup 2 a new two bands begin to appear in case of Xe and Kr ion irradiation. The TL spectra under Kr and Xe ion irradiation similar at the same dose. However, the spectra under electron irradiation were found to be rather different than under heavy ions irradiation.

Investigation and measurement of radio thermoluminescence properties of some calci tic mollusc shells of the Persian Gulf and the Oman Sea (for γ radiation dosimetry)

International Nuclear Information System (INIS)

Ghafourian, H.; Rabbani, M.; Rouhi, U.

2000-01-01

Biogenic Calcium Carbonate, particularly as naturally thermoluminescent calci tic mollusc shells may serve as excellent radio thermoluminescent dosimeters. In this study the radio thermoluminescence properties of 8 different bivalves of the Persian Gulf, the Oman Sea and the internal calcite shell of Sepia sp. are investigated. The results of this investigation have shown that the shells of Sepia sp., Pinctata radiata and Card ita bicolor as appropriate dosimeters for both personal and industrial dosimetry purposes, among which Sepia sp. is the most sensitive one. Callista umbonella and Mactra sp. are relatively less thermoluminescent while Saccostrea Cucullata and Chlamys ruschenbergerii are completely inert with respect to γ - thermoluminescence. Thermoluminescence properties of Anadara refescens and Anadara secticostata decrease surprisingly by an increase in the absorbed dose of γ radiation, which can mainly be interpreted as the result of crystal lattice destruction caused by ionizing radiation

Thermoluminescence detected in Magicicada sp. exoskeletons

International Nuclear Information System (INIS)

Fields, D.E.; Randall, R.B.; Bauman, C.E. III

1979-01-01

Thermoluminescent emission from the irradiated exoskeletons of cicada have been observed. At a heating rate of approximately 60 0 C/min. the peak light emission temperature was 183 +- 3 0 C. This effect corresponds to charge-carrier trap parameters of Esub(a) = 0.82 +- 0.04 eV and w 0 = 10sup(9.1 +- 0.5) sec -1 . Response to filtered γ radiation of 50-kV peak energy was on the order of 3.2 x 10 6 photons/R/g. Insect exoskeletons are thus potentially useful as dosimeters. (author)

Thermoluminescent properties of ZnS:Mn nanocrystalline powders

International Nuclear Information System (INIS)

Ortiz-Hernández, Arturo Agustín; Méndez García, Víctor Hugo; Pérez Arrieta, María Leticia; Ortega Sígala, José Juan

2015-01-01

Thermoluminescent ZnS nanocrystals doped with Mn 2+ ions were synthesized by chemical co-precipitation method. From X-ray diffraction studies it was observed that the synthesized nanoparticles have cubic zinc blende structure with average sizes of about 40–50 nm. Morphology was analyzed by TEM. Photoluminescence studies showed two transitions, one of them close to 396 nm and other close to 598 nm, which is enhanced with increasing dopant concentration, this behavior was also observed in the cathodoluminescence spectrum. The thermoluminescence gamma dose-response has linear behavior over dose range 5–100 mGy, the glow curve structure shows two glow peaks at 436 K and at 518 K that were taken into account to calculate the kinetic parameters using the Computerized Glow Curve Deconvolution procedure. - Highlights: • Nanocrystals in powder of ZnS:Mn were synthesized using the co-precipitation method. • The integrated TL spectra has a linear behavior on the dose range 5–100 mGy of γ-radiation. • The kinetic parameters were obtained by the CGCD procedure. • Results support the possible use of nanocrystalline ZnS:Mn as a new γ-dose nanoTLD

Quality control of dosimetric systems using thermoluminescent crystals

International Nuclear Information System (INIS)

Mahecha, L.; Plazas, M. C.; Machado, M.; Perea, M. D.

2006-01-01

To achieve an optimal tumoral control to prostate cancer in early and locally advanced stages, it is necessary to increase the dose with a low mobility probability at the vesicle an rectal level. This is achieved through conformal radiotherapy. The Instituto Nacional de Cancerologia uses this technique, but two questions arise from the medical-physicists and medical radio-oncologist: In accordance with clinical protocols, the conformal radiotherapy delivers a low dose to the adjacent healthy tissues. What experimental method exists that can prove with certainly the veracity of this affirmation?. And, Do the dosimetric simulation system calculate suitable the dose for each tissues?. Through thermoluminescent dosimetry and the use of a physical simulator,we measured the absorbed dose at the target volume and the adjacent tissues using conformal and conventional radiotherapy. We proved that organs such as the rectum and bladder, receiver a minor dose in conformal radiotherapy, hence reducing their mobility probability. In addition, the readings from the thermoluminescent dosimeters and the doses calculated by the ECLIPSE dosimetric system were compared, concluding that the patient's prescribed dose is effectively delivered as recommended by the quality control program in radiotherapy. (Author)

Thermoluminescence of double fluorides doped with rare earths

International Nuclear Information System (INIS)

Azorin N, J.; Sanchez R, A.; Khaidukov, N.M.

2004-01-01

In this work the thermoluminescent characteristics of double fluorides K 2 YF 5 , K 2 GdF 5 and K 2 LuF 5 doped are presented with Tb 3+ , studied in the interval of temperature from 30 to 400 C. The materials that presented better answer to the irradiation with particles beta and with ultraviolet light they were the K 2 YF 5 : Tb (1% at. Tb 3+ ) and the K 2 LuF 5 : Tb (1% at. Tb 3+ ); while the K 2 YF 5 : Tb to high concentrations (10% and 20% at. Tb 3+ ) and the K 2 LuF 5 : Tb (1% at. Tb 3+ ) and the K 2 LuF 5 : Tb (1% at. Tb 3+ ) they presented an acceptable answer in front of the gamma radiation. The intensity of the Tl answer induced in these materials is a decisive factor to continue studying its dosimetric characteristics, what allows to consider them as the base for the development of potential materials to use them in the dosimetry of beta particles, of the UV light of the gamma radiation using the thermoluminescence method. (Author)

Thermo-luminescent dosimetry

Energy Technology Data Exchange (ETDEWEB)

Reither, M; Schorn, B; Schneider, E

1981-01-01

The development of paediatric radiology which began in the late 195O's has been characterised by the need to limit the dose of ionising radiation to which the child is subjected. The aim has been to keep radiation exposure as low as possible by the introduction of suitable techniques and by the development of new methods. It is therefore surprising that studies in dosimetry in the paediaytric age range have only been carried out in recent years. One reason for this may have been the fact that a suitable technique of measurement was not available at the time. The introduction of solid state dosimetry based on thermo-luminescence, first into radiotherapy (1968) and subsequently into radiodiagnosis, has made it possible to abandon the previously widely used ionisation chamber. The purpose of the present paper is to indicate the suitability of this form of dose measurement for paediatric radiological purposes and to stimulate its application in this field.

Thermoluminescence induced by X-rays in silica materials with metallic impurities

International Nuclear Information System (INIS)

Mendoza A, D.; Gonzalez M, P.; Espinosa P, M.; Salas, P.; Castano, V.M.

1999-01-01

Diverse materials of silica with Fe, Cu, Mg, and Mn impurities were synthesized by the sol-gel method, using tetraethyl orthosilicate as precursor. The materials obtained were subjected to thermal treatment at 500, 700 and 1000 Centigrade also they were irradiated with X-ray generated by a X-ray diffractometer which is installed in the ININ. The thermoluminescent signal was analysed and correlated with the type of impurities that are present in the material and with the grade of crystallinity produced by the thermal treatment in them. In according to the results obtained these materials show a thermoluminescent signal which is influenced by the crystallinity grade. It was analysed the behavior of the response for different doses, with the purpose of utilizing them to quantify very intense fields of radiation. (Author)

Thermoluminescent response of Y2O3:Ce,Eu irradiated with X-rays

International Nuclear Information System (INIS)

Sanchez J, F. del R.; Sosa A, M. A.

2017-10-01

The thermoluminescent response of various materials has been studied when irradiated with X-rays, and the parameters that characterize the order of the kinetics of the material, depth of traps and frequency have been determined. The objective of this project was to characterize the thermoluminescent response of dosimeters based on yttrium oxide (Y 2 O 3 ) irradiated with X-rays. To do this, the thermoluminescent response of the Y 2 O 3 :Ce,Eu dosimeter was measured and exposed to an X-ray radiation field; five levels of radiation were used: in the first, a potential of 53.5 kv was used and a working load of 5.6 m As, in the second: 70.0 kv, 12.5 m As; in the third: 81.0 kv, 20.0 m As; in the fourth: 109 kv, 32 m As, in the fifth: 121 kv, 80.0 m As, applying an exposure range between 17.7 and 40 R. The irradiation was performed exposing the sample at 104 cm from the focus of the X-ray tube. To obtain the readings of the thermoluminescent response, a Harshaw TLD 3500 reader was used. The data captured by the reader was processed using the WinREMS software. The deletion protocol was as follows: the dosimeters already read were placed, one hour in the Terlab MA12D muffle at a temperature of (400 ± 1) degrees centigrade, the dosimeters were removed and left at room temperature of 20 degrees centigrade for 20 minutes. Then they were placed in the Binder high temperature oven ED23 at 100 ± 1 centigrade degrees for 2 hours. The brightness curves were de convolved using the WebPlotDigitizer v 3.8 software and the individual peaks of the brightness curves were obtained. We found that: the synthesized materials presented a good thermoluminescent response when irradiated with X-rays. However, only one of the dosimeters, of Yttrium oxide doped with 0.5% Cerium, showed a relatively linear response in the applied dose range. The analysis made to the brightness curve of the Yttrium oxide doped with Cerium at 0.5%, applying the method of the three points for the parameters

An evaluation of the Panasonic model UD513AC-1 Thermoluminescence Dosimetry system

International Nuclear Information System (INIS)

Durrer, R.E. Jr.

1991-12-01

An evaluation of the Panasonic UD513AC-1 Thermoluminescence Dosimetry system was performed to determine the system's capabilities as a general purpose thermoluminescence dosimeter measuring device. The tests that were performed included a critique of the user's manual, delimitation of the operating parameters, the quality of construction, and an evaluation of the features that were unique to this system. The UD513AC-1 was found to be an adequate measuring device for most dosimetric applications. It was not well suited for experimental work with thermoluminescence materials due to a low sensitivity displayed by the photomultiplier tube to commonly used materials. The system was well constructed and did not suffer hardware failure during this research. Major attributes of the UD513AC-1 were automatic data storage, highly reproducible heating ramps, an excellent infrared light filter and a unique feature to a single phosphor unit, a dose determination function. Negative aspects of the system included a limited data manipulation capability within the controlling program, a poorly written user's manual, inadequate sensitivity on the part of the photomultiplier tube, and insufficient capability to adjust the hot N 2 gas flow to desired levels

Radioluminescence and thermoluminescence of albite at low temperature

International Nuclear Information System (INIS)

Can, N.; Garcia-Guinea, J.; Kibar, R.; Cetin, A.; Ayvacikli, M.; Townsend, P.D.

2011-01-01

Feldspar as an archaeological and geological natural material for dating and retrospective dosimetry is receiving more and more attention because of its useful luminescence properties. In this study, the 25-280 K thermoluminescence (TL) and radioluminescence (RL) spectra in albite, which is a component of the two main feldspar series, the alkali feldspar (Na, K)AlSi 3 O 8 and the plagioclases (NaAlSi 3 O 8 -CaAl 2 Si 2 O 8 ) have been presented for aliquots along (001) and (010) crystallographic orientations. There are four main emission bands that are considered to arise from complexes of intrinsic defects linked in larger complexes with impurities such as Na + , Mn 2+ or Fe 3+ ions. The consequence of their association is to produce different luminescence efficiencies that produce wavelength sensitive TL curves. Radioluminescence data at low temperature for albites is distorted by contributions from the TL sites, even when the RL is run in a cooling cycle. This indicates the potential for a far more general problem for analysis of low temperature RL in insulating materials. - Highlights: → TL and RL spectra in albite were presented for different orientations. → There are 4 emission bands that are considered to arise from complexes of intrinsic. → RL data at low temperature for albite is distorted by contributions from TL sites. → This indicates the potential problem for analysis of low temperature RL.

Evaluation of glasses containing cadmium for high dose dosimetry by the thermoluminescence technique

Energy Technology Data Exchange (ETDEWEB)

Carvalho, Gabriel Soares Marchiori de; Ferreira, Pamela Zati; Cunha, Diego Merigue da; Dantas, Noelio Oliveira; Silva, Anielle C.A.; Perini, Ana Paula; Neves, Lucio Pereira, E-mail: lucio.neves@ufu.br [Universidade Federal de Uberlandia (INFIS/UFU), MG (Brazil). Instituto de Fisica; Caldas, Linda V.E. [Instituto de Pesquisas Energeticas e Nucleares (IPEN-CNEN/SP), Sao Paulo, SP (Brazil); Carrera, Betzabel Noemi Silva; Watanabe, Shigueo [Universidade de Sao Paulo (IF/USP), SP (Brazil). Instituto de Fisica

2016-07-01

New glass matrices were evaluated for high dose dosimetry by the thermoluminescence technique. Their nominal composition are 20Li{sub 2}CO{sub 3}.10Al{sub 2}O{sub 3}.15CdO.55B{sub 2}O{sub 3} and 20Li{sub 2}CO{sub 3}.10Al{sub 2}O{sub 3}.20CdO.50B{sub 2}O{sub 3} (mol%). The glass matrices were irradiated with different doses: 50, 100, 200, 500, 700 and 900 Gy, and the thermoluminescence emission curves were obtained for each of these values. The results show a great potential of using these matrices in high dose dosimetry. (author)

Study of a new glass matrix by thermoluminescent technique for high-dose dosimetry

Energy Technology Data Exchange (ETDEWEB)

Ferreira, Pamela Z.; Carvalho, Gabriel S. Marchiori de; Cunha, Diego M. da; Dantas, Noelio O.; Silva, Anielle C.A.; Neves, Lucio P.; Perini, Ana P., E-mail: anapaula.perini@ufu.br [Universidade Federal de Uberlandia (UFU), MG (Brazil). Instituto de Fisica; Linda, V.E. Caldas [Instituto de Pesquisas Energeticas e Nucleares (IPEN/CNEN-SP), Sao Paulo, SP (Brazil); Carrera, Betzabel N.S.; Watanabe, Shigueo [Universidade de Sao Paulo (IF/USP), Sao Paulo, SP (Brazil). Instituto de Fisica

2016-07-01

The thermoluminescence technique is widely used for both personal and for high-dose dosimetry. In this work, the thermoluminescence technique was utilized to study a new glass matrix, with nominal composition of 20Li{sub 2}CO{sub 3}.10Al{sub 2}O{sub 3}.30BaO.40B{sub 2}O{sub 3} (mol%), irradiated with different doses in a {sup 60}Co source. The glow curves and the dose-response curve were obtained for radiation doses of 10, 50, 100, 200 e 700 Gy. The results showed that this new glass matrix has potential use in high-dose dosimetry. (author)

Oxidation/reduction effects on sapphire thermoluminescent detectors

International Nuclear Information System (INIS)

Molnar, G.; Borossay, J.; Suevegh, K.; Vertes, A.

1998-01-01

Complete text of publication follows. The thermoluminescence (TL) and thermally stimulated exoemission (TSEE) properties of Al 2 O 3 has been extensively studied during the past 40 years. It has been suggested as a dosemeter for both ultraviolet light and ionising radiation. Nevertheless the connection between the structure (point defects) of alumina and thermally stimulated relaxation processes has not yet been clearly explained. In this work α-Al 2 O 3 single crystal samples were studied in order to determine the mechanism of electron-hole processes of thermoluminescence and thermally stimulated exoelectron emission peaks. Single crystals prepared in highly reducing conditions were treated in different atmospheres (reducing/oxidising) and their optical absorption (after isochronous annealing), fluorescence, positron-annihilation and TL properties were investigated. Changes of optical absorption and positron annihilation spectra of oxidised samples suggest that Schottky-type defect formation occurred - the concentration of Al-vacancies increased while that of O-vacancies decreased. Also we observed the oxidation of Ti 3+ to Ti 4+ . The reduction of an oxidised sample led to the diminution of Al-vacancy concentration while that of O-vacancies has not been changed. This suggest a Frenkel-type cationic defect. We also tried to correlate these changes to changes of TL glow curves and to explain the origin of some TL peaks

Ultraviolet radiation monitoring in makkah city, Saudi Arabia, using thermoluminescence material CaF2:Tm

International Nuclear Information System (INIS)

Al-Ghorabie, F.H.; Natto, S.S.; AL-Lehyani, S.A.

2005-01-01

The aim of the present study is to explore the possibility of using Ca F2:Tm thermoluminescence material for measuring and monitoring of solar UV R in Makkah City, Saudi Arabia. Several laboratory experiments, prior to the field measurements, were performed included study of the effects of ultraviolet wavelengths on the response of the phosphor, study of the effect of increasing ultraviolet radiation dose on the intensity of thermoluminescence and study the effect of time factor on the thermoluminescence fading of Ca F 2 :Tm. The phosphor was then exposed directly for one hour to sunlight radiation on a daily basis for 90 days in an open field inside Umm Al-Qura university campus. The field measurements were performed during the months of June, July and August 2003 at 1:00 p.m. The laboratory and field results of this study showed that Ca F 2 :Tm can be used as a suitable dosimeter for solar UV R

TL-dating applied to building archaeology: The case of the medieval church Notre-Dame-Sous-Terre (Mont-Saint-Michel, France)

Energy Technology Data Exchange (ETDEWEB)

Blain, Sophie [IRAMAT-CRP2A-UMR 5060, CNRS-Universite de Bordeaux 3, Maison de l' Archeologie, F-33 607 Pessac (France); Luminescence Laboratory, Department of Archaeology, University of Durham, South Road, DH1 3LE Durham (United Kingdom)], E-mail: blain.sophie@gmail.com; Guibert, Pierre [IRAMAT-CRP2A-UMR 5060, CNRS-Universite de Bordeaux 3, Maison de l' Archeologie, F-33 607 Pessac (France)], E-mail: guibert@u-bordeaux3.fr; Bouvier, Armel [IRAMAT-CRP2A-UMR 5060, CNRS-Universite de Bordeaux 3, Maison de l' Archeologie, F-33 607 Pessac (France)], E-mail: bouvier_armel@yahoo.fr; Vieillevigne, Emmanuelle [IRAMAT-CRP2A-UMR 5060, CNRS-Universite de Bordeaux 3, Maison de l' Archeologie, F-33 607 Pessac (France)], E-mail: evieillevign@u-bordeaux3.fr; Bechtel, Francoise [IRAMAT-CRP2A-UMR 5060, CNRS-Universite de Bordeaux 3, Maison de l' Archeologie, F-33 607 Pessac (France); Sapin, Christian [Laboratoire Archeologie, Culture et Societe-UMR 8894, CNRS-Universite de Bourgogne, Dijon (France)], E-mail: sapin.christian@wanadoo.fr; Bayle, Maylis [Laboratoire de medievistique occidentale de Paris, UMR 8589, CNRS-Universite de Paris 1 (France)], E-mail: maylis.bayle@wanadoo.fr

2007-10-15

The recent application of thermoluminescence (TL) dating to young building materials is being increasingly developed for use in the field of buildings archaeology [; ; ]. Ensuring the accuracy of the dating method is of the utmost importance in order to achieve results which are pertinent enough to have archaeological significance. This paper deals with an archaeological building study of the first church built on the Mont-Saint-Michel (France) and improvements made to the TL-protocol in Bordeaux. The aim is to achieve precise dates for the material under analysis and therefore, a better understanding of the evolution of the building. For this study, 14 bricks have been sampled from eight different masonries and submitted for TL dating analysis. With the exception of one sample which appears to be non-contemporaneous to the others, the date results range from 900{+-}80 to 1020{+-}60 AD. The results were then averaged according to the two phases established by the archaeological building study. The first two stages of the primitive church both date from the 10th century.

TL-dating applied to building archaeology: The case of the medieval church Notre-Dame-Sous-Terre (Mont-Saint-Michel, France)

International Nuclear Information System (INIS)

Blain, Sophie; Guibert, Pierre; Bouvier, Armel; Vieillevigne, Emmanuelle; Bechtel, Francoise; Sapin, Christian; Bayle, Maylis

2007-01-01

The recent application of thermoluminescence (TL) dating to young building materials is being increasingly developed for use in the field of buildings archaeology [; ; ]. Ensuring the accuracy of the dating method is of the utmost importance in order to achieve results which are pertinent enough to have archaeological significance. This paper deals with an archaeological building study of the first church built on the Mont-Saint-Michel (France) and improvements made to the TL-protocol in Bordeaux. The aim is to achieve precise dates for the material under analysis and therefore, a better understanding of the evolution of the building. For this study, 14 bricks have been sampled from eight different masonries and submitted for TL dating analysis. With the exception of one sample which appears to be non-contemporaneous to the others, the date results range from 900±80 to 1020±60 AD. The results were then averaged according to the two phases established by the archaeological building study. The first two stages of the primitive church both date from the 10th century

Methods for implementation of in vivo dosimetry (entrance dose) using thermoluminescent dosimeters during radiotherapy treatment with photon beam

International Nuclear Information System (INIS)

Barsanelli, Cristiane

2006-01-01

Selection, calibration procedure to convert TLD signal into absorbed dose and physical characteristics at the thermoluminescent dosimeters, as well as the determination of correction factors and the methodology to determine expected entrance dose, are described in this work. Practical aspects and the utility of entrance dose measures with thermoluminescent dosimeters were investigated, as well as the exactness and the reproducibility of the daily dose release. The entrance dose measures were performed in five patients with diagnosis of breast cancer treated with a 6 MV photon beam. The measured dose and the expected dose values agreed in ± 5%, due to excellent treatment equipment stability, to automatic verification system and the good exactness in the daily treatment adjustment. Good precision can be achieved when the correction factors for each parameter of influence in the dosimeter response are carefully determined and applied to convert the thermoluminescent signal into absorbed dose. The study demonstrates the viability of thermoluminescent dosimeters use for in vivo dosimetry and its utility as part of a quality assurance program in a radiation therapy service. (author)

The thermoluminescent curve as parameter to compare archaeological ceramics; La curva termoluminiscente como parametro para comparar ceramica arqueologica

Energy Technology Data Exchange (ETDEWEB)

Dominguez R, I.R.; Ramirez C, G.A. [Centro INAH Estado de Mexico. Morelos Ote. 502, Col. San Sebastian, 50090 Toluca, Estado de Mexico (Mexico); Gonzalez M, P.R.; Mendoza A, D. [lNIN, Carr. Mexico-Toluca S/N, La Marquesa, 52750 Ocoyoacac, Estado de Mexico (Mexico); Martinez C, G. [Coordinacion Nacional de Conservacion del Patrimonio Cultural, INAH, Mexico D.F. (Mexico)

2006-07-01

Most mineral materials, including the constituents of pottery, have the property of thermoluminescence (TL), where part of the energy from radioactive decay in the mineral is stored and later released as light upon strong heating. The intensity of emitted light as a function of temperature is the thermoluminescence glow curve. However, it is well-know the thermoluminescence glow curve form depends of several factors associates with the incident radiation and type of materials. Between the factors associated with the materials, it can be mentioned the quantity and type of crystalline phases, and quantity and type of impurities that they could be present in the material. That is to say, materials with different physicochemical characteristics will produce different thermoluminescence glow curve, although, they have been irradiated under the same conditions. In accordance with the above mentioned, it is possible to identified differences between pre hispanic ceramic belonging to a same site and other sites. In this work a discussion about advantages and disadvantages is presented. Some specific examples in ceramic artifacts belonging to the Matlatzinca and Teotihuacan cultures are included. (Author)

Characterization, analysis and dating of archaeological ceramics from the Amazon basin through nuclear techniques

International Nuclear Information System (INIS)

Latini, Rose Mary

1998-01-01

The aim of this work is to contribute to the research in the reconstruction of part of the pre-history of the Amazon Basin by means of an analytical methods combined with multivariate analysis, given a analytic basis that can be continued by the archaeological work, through the identification, classification, provenance and dating the ceramics found in different archaeological sites of the Hydro graphic Basin of the Purus river. Neutron activation analysis in conjunction multivariate statistical methods were used for the identification and classification and thermoluminescence was used for the dating. Chemical composition results were in better agreement with archaeological classification for the archaeologically define Iquiri, Quinan and Xapuri phases and less characteristics the Iaco and Jacuru archaeological phase were not well characterized. An homogeneous group was established by most of the samples collected from the Los Angeles Archaeological Site (LA) and was distinct from all the other groups analysed. The provenance studies made with ceramics collected at this site shows that they were made with clay from nearby river (Rio Ina). From the LA ceramics dating the average date of site occupation was 1660 years. The ceramic dating results from the external wall of a circular earth wall construction confirm the relation with the local pre-history. Beyond the Acre material two urns were dated from the Archaeological Site Morro Grande and Sao Jose at Araruama, Rio de Janeiro. (author)

Investigations on thermoluminescent dosimetry (TLD) with doped alumina ceramics

International Nuclear Information System (INIS)

Janas, R.; Huebner, K.

1976-01-01

Alumina ceramics doped and burned under various conditions have been investigated with regard to their suitability for thermoluminescent dosimetry. The production of ceramics is described. The properties essential for dosimetric purposes, such as glow curve, energy dose characteristics, fading, recoverability, lower detection limit and energy dependence, are indicated. The advantages and disadvantages of alumina ceramics are compared. (author)

Thermically stimulated exoelectronic emissions and thermoluminescence of MgO

International Nuclear Information System (INIS)

Chubaci, J.F.D.

1987-01-01

In this work, studies were performed on the following topics: i) thermically stimulated exoelectronic emission (TSEE) in pure MgO single crystals ion implanted, submitted to thermal treatment with fast on slow cooling and water adsorption; ii) ultraviolet light effect on TSEE; iii) thermoluminescent emission; iv) crystallization of FeCoB amorphous alloys. (A.C.A.S.) [pt

Development of a highly sensitive lithium fluoride thermoluminescence dosimeter

International Nuclear Information System (INIS)

Moraes da Silva, Teresinha de; Campos, Leticia Lucente

1995-01-01

In recent times, LiF: Mg, Cu, P thermoluminescent phosphor has been increasingly in use for radiation monitoring due its high sensitivity and ease of preparation. The Dosimetric Materials Production Laboratory of IPEN, (Nuclear Energy Institute) has developed a simple method to obtain high sensitivity LiF. The preparation method is described. (author). 4 refs., 1 fig., 1 tab

A study of the thermoluminescent properties of CVD diamond detectors

International Nuclear Information System (INIS)

Marczewska, B.; Bilski, P.; Olko, P.; Rebisz, M.; Nesladek, M.; Waligorski, M.P.R.

2002-01-01

A batch of 20 diamond detectors obtained by the chemical vapour deposition (CVD) method at the Institute for Materials Research at the Limburg University, Belgium, was investigated with respect to their thermoluminescent (TL) properties. The investigated detectors demonstrate TL sensitivity similar to that of the standard LiF:Mg, Ti (MTS) thermoluminescent detectors, lack of fading after two weeks from irradiation and apparent linearity of dose response. In spite of the persistent fluctuation of individual detector sensitivity observed in this batch, a new annealing procedure improved the stability of the TL signal. It has been concluded that 1 h annealing at 350 C assures the highest reproducibility for this set of detectors. A 30% discrepancy of the value of the TL signal between individual detectors from the batch may be caused by non-uniform distribution of dopants in the volume of the CVD diamond. A prototype of a planar TL reader equipped with a CCD camera was employed in this investigation. (Abstract Copyright [2002], Wiley Periodicals, Inc.)

On the phototransferred thermoluminescence in MgB4O7:Dy

International Nuclear Information System (INIS)

Richmond, R.G.

1987-01-01

On exposure to ionizing radiations, the normal traps in MgB 4 0 7 :Dy can be emptied by the readout process only or by annealing at suitable temperatures, leaving the deep traps still intact. Subsequently, it is possible to repopulate the dosimetric peak by illuminating with u.v. light. Charge carriers released from the traps during the second readout give rise to a thermoluminescent output proportional to the ionizing radiation exposure and the u.v. radiant energy. This is called phototransferred thermoluminescence (PTTL). The PTTL method can be utilized for the reassessment of the initial γ-ray exposure. This paper presents the measurements of the intrinsic response of the commercially available MgB 4 0 7 :Dy to u.v. radiation, with a demonstration of its use for γ-ray dose re-estimation using the PTTL technique. (author)

Emission properties of thermoluminescence from natural quartz - blue and red TL response to absorbed dose

International Nuclear Information System (INIS)

Hashimoto, T.; Yokosaka, K.; Habuki, H.

1987-01-01

The TL spectrometry of natural quartz exposed to a gamma radiation dose of 8.8 kGy proved that the red TL, mainly from volcanically originated quartz, has a broad emission band with a peak around 620 nm, while the blue TL from plutonically originated quartz also has a broad emission band giving a peak around 470 nm. These typical red or blue intrinsic colours were also confirmed on the thermoluminescence colour images (TLCI). Exceptionally, a pegmatite quartz changed its TLCI colour from red to blue when the absorbed dose was increased. By using colour filter assemblies, all these quartz samples were shown to emit mainly blue and red TLs, which have distinctly different TL responses to the absorbed dose; the blue invariably showed a supralinearity relation between 1 and 10 kGy dose. For the purpose of dating, the use of red TL, is preferable. The red TL component is related to the impurity Eu content in quartz minerals. (author)

Authenticity test in ceramics and archaeological figures by thermoluminescence; Prueba de Autenticidad en ceramicas y figuras arqueologicas por termoluminiscencia

Energy Technology Data Exchange (ETDEWEB)

Ramirez L, A.; Schaaf, P. [Laboratorio de Termoluminiscencia, Instituto de Geofisica-UNAM (Mexico); Filloy, L. [Museo Nacional de Antropologia e Historia, Ciudad de Mexico (Mexico)

1999-07-01

At present exists quite a lot of false archaeological pieces which provokes doubts about the legitimacy of the pieces. In this work it is presented the Authenticity test by Thermoluminescence realized at the urn of the goddess 13 serpent of the zapotec culture of Oaxaca which is exposed in Mexico City. The original piece contains crystalline structures which present hardly the thermoluminescence phenomena by the presence of {sup 238} U, {sup 232} Th, and {sup 40} K getting with this the form and intensity of the natural thermoluminescence curve of an archaeological piece which shows a Tl peak and allows to know so if it was made recently or not. (Author)

Thermoluminescence of novel MgO–CeO_2 obtained by a glycine-based solution combustion method

International Nuclear Information System (INIS)

Barrón, Victor Ramón Orante; Ochoa, Flor María Escobar; Vázquez, Catalina Cruz; Bernal, Rodolfo

2016-01-01

Thermoluminescence dosimetry properties of novel MgO–CeO_2 obtained by solution combustion synthesis in a glycine-nitrate process, are presented for the very first time. X-ray diffraction indicates the presence of cubic MgO and cerianite (CeO_2) for the annealed powder samples. Dosimetry features such as linear behaviour of the dose response without saturation in the dose interval studied, as well as asymptotic behaviour of the thermoluminescent signal fading place MgO–CeO_2 phosphor as a promising material for low-dose radiation dosimetry applications. - Highlights: • Thermoluminescence (TL) dosimetry properties of novel MgO–CeO_2 are presented. • TL glow curves display stable and dosimetric components. • Dose response showed a linear trend in the dose interval studied. • TL fading decay curve showed an asymptotic behaviour. • MgO–CeO_2 is suitable for personal, environmental and medical dosimetry.

NRC [Nuclear Regulatory Commission] TLD [thermoluminescent dosimeter] direct radiation monitoring network

International Nuclear Information System (INIS)

Struckmeyer, R.; McNamara, N.

1989-09-01

This report provides the status and results of the NRC Thermoluminescent Dosimeter (TLD) Direct Radiation Monitoring Network. It presents the radiation levels measured in the vicinity of NRC licensed facility sites throughout the country for the second quarter of 1989

Thermoluminescence as a criterium in the acquisition of ceramic art objects

International Nuclear Information System (INIS)

Erlach, R.; Pichler, B.

1985-01-01

Thermoluminescence is a measure for the external archeological dose received and can be used for age estimation. Examples are given of Egyptian objects where the age is known independently and thereby the accuracy of the method can be evaluated. (G.Q.)

Utilization of thermoluminescent dosemeters in radiation field studies for different materials

International Nuclear Information System (INIS)

Carron, W.; Guilardi Neto, T.

1987-01-01

The dose conversion factor of lithium fluoride thermoluminescent for the follows materials: water, wood and soil, the dose curve surveying in function of depth and the regression equations that better adapt to the dose curves were calculated. (C.G.C.) [pt

Thermoluminescent kinetic parameters of the perovskite, KMgF3, activated with lanthanum

International Nuclear Information System (INIS)

Sepulveda M, F.; Azorin N, J.; Rivera M, T.; Furetta, C.; Sanipoli, C.

2004-01-01

The thermoluminescent curves induced by the beta radiation in the perovskite KMgF 3 were investigated activated with lanthanum. The classic methods were used to determine the kinetic parameters (the kinetic order b, the activation energy E and the frequency of escape intent s) associated with the peaks of the thermoluminescent curve (Tl) in the KMgF 3 activated with lanthanum after the irradiation with beta rays. The method is based on the position of the thermoluminescent peaks, obtained of the temperature change of the peak in the maximum emission caused by the change in the heating rapidity to which the samples were measured. In this work, the samples in form of pellets were re cooked previously at 400 C during one hour before irradiating them with beta particles. The Tl measures were made with a Tl reader system using three different heating rapidities and storing the glow curves. To calculate the depth of the E traps and the frequency factor s, the parameters of the glow curve were determined experimentally of the shame of the glow curve by means of the mensuration of the shame of the maximum temperature of the peak, T M like a function of the heating rapidity. The results indicate that the values of the kinetic parameters are very near among if when they are obtained indistinctly of anyone of the different methods. (Author)

In vivo dosimetry using thermoluminescent detector in cancer therapy of head and neck

International Nuclear Information System (INIS)

Viegas, Claudio C.B.; Batista, D.V.; Campos, A.M.; Lopes, R.T.

2002-01-01

The viability and implementation of a routine in vivo dosimetry, using thermoluminescent dosemeters (TLD), at the radiotherapy section of the National Institute of Cancer in Brazil, in the case of head and neck treatment is shown. In order to reach that aim, the characteristics of the response of the LiF:Mg;Ti (TLD-100) thermoluminescent detectors in powder form were determined. The performed of this detector for in vivo dosimetry was testes using an RANDO Alderson anthropomorphic phantom and, once their adequability proved for the kind of measurements proposed , it was used for dose assessment in the case of tumour treatments in the head and neck regions, for Cobalt-60 irradiations. (author)

Thermoluminescence glow curve of CaZrO3 phosphor doped with Eu3+

International Nuclear Information System (INIS)

Tiwari, Neha; Kuraria, R.K.; Kuraria, S.R.

2014-01-01

Behaviour displayed by thermoluminescence analysis of Eu 3+ doped CaZrO 3 phosphor prepared by combustion synthesis technique. The sample was synthesized by combustion method because it is less time taking method as well as low temperature synthesis. For the thermoluminescence study the prepared sample irradiated by UV lamp the wavelength is 254 nm. Every time 2 mg of sample used for TL record at fixed heating rate 5℃ s -1 , sample shows well resolved higher temperature peak at 273℃. The high temperature peak shows more stability and less fading in prepared phosphor which is suitable for TL dosimetry. Also the variation with UV dose (5 to 30 min) shows sublinear response with dose

Thermoluminescent dosimetry for LDEF experiment M0006

International Nuclear Information System (INIS)

Chang, J.Y.; Giangano, D.; Kantorcik, T.; Stauber, M.; Snead, L.

1992-01-01

Experiment M0006 on the Long Duration Exposure Facility had as its objective the investigation of space radiation effects on various electronic and optical components, as well as on seed germination. The Grumman Corporate Research Center provided the radiation dosimetric measurements for M0006, comprising the preparation of thermoluminescent dosimeters (TLD) and the subsequent measurement and analysis of flight exposed and control samples. In addition, various laboratory exposures of TLD's with gamma rays and protons were performed to obtain a better understanding of the flight exposures

Deconvolution of the thermoluminescent emission curve. Second order kinetics

International Nuclear Information System (INIS)

Moreno y M, A.; Moreno B, A.

1999-01-01

In this work it is described the Randall and Wilkins second order kinetics in Microsoft Excel language, which allows its expression as the sum of Gaussian and the correction factors corresponding. These factors are obtained of the differences between the real thermoluminescent curve and the Gaussian proposed. The results obtained justify the Gaussian expression added to the correction factor. (Author)

The application of thermoluminescence dosimeters to studies of released activity distributions

International Nuclear Information System (INIS)

Ruden, B.I.

1969-06-01

In this report the theoretical conditions necessary for the study of the behaviour of released activity by the use of CaSO 4 : Mn thermoluminescence dosimeters are considered. A method is derived for calculating exposure distributions from drifting volume activity. The correlation between exposure distributions and concentration distributions is discussed. One of thirty experiments where Br 82 was released into water through a nozzle some metres above the bottom is described. The resulting exposure distribution was measured in a vertical plane at distances of 10, 50 and 200 metres by CaSO 4 : Mn thermoluminescence dosimeters. The measured exposures are described and discussed. The advantages and disadvantages of the technique are compared with other methods. The method using exposure measurements for the study of active release in water has given satisfactory results in practice. The measurements have been made at concentration levels which are considerably below that permissible for drinking water according to the recommendations by ICRPA special advantage with this method is that the measurements can be made simultaneously at a large number of places and that integration is possible over sufficiently long periods of time. An experiment is described where Ar 41 was released in free air at a height of one metre above ground and the resulting exposure distribution was measured in a vertical plane at 100 and 250 metres distance by CaSO 4 : Mn thermoluminescence dosimeters. Shielding problems in connection with the experiments have been small since the method permits the measurement of very small doses. An account is given of the possibility of using the beta emitting isotope Kr 85 instead of the gamma emitting Ar 41 for diffusion experiments in air. The results obtained from some experiments are presented and discussed. The thermoluminescent signal from the dosimeters are, at the same concentration and exposure time, 2.5 times greater for Kr 85 than for Ar 41. The Kr

An optical fibre-type silicate glass thermoluminescent detector

International Nuclear Information System (INIS)

Zheng Zheng; Dai Honggui; Hu Shangze; Liu Jian; Fang Jie

1991-01-01

A description of dosimetric properties and the preparation method of an optical fibre-type silicate glass thermoluminescent detector (TLD) is presented. Results showed that this new phosphor is a good one which could be used as a routine dosimeter in the range 10 -1 -10 3 Gy. The preparation method is a new one which differs greatly from all previous ones. Furthermore this kind of detector is small and of low weight. (orig.)

Thermoluminescent dosimetry of ionizing radiations using ZrO2 prepared at low temperatures

International Nuclear Information System (INIS)

Rivera M, T.; Diaz G, J.A.I.; Olvera T, L.; Azorin N, J.; Barrera S, M.; Soto E, A.M.

2005-01-01

The thermoluminescent dosimetry (TLD) it is a versatile tool for an evaluation of dose of ionizing radiation. A great variety of ceramic materials and their different physical forms allow a determination of the ionizing radiation in a wide dose interval. In this work the results of studying those thermoluminescent characteristics (TL) of the zirconium oxide obtained by means of the sol-gel technique to low temperatures are presented. To these temperatures the material was obtained in its amorphous state (ZrO 2 -a). The structural characteristics of ZrO 2 -a they were obtained by means of X-ray diffraction. The TL characteristics studied were: TL curve, reproducibility of the TL signal and the fading of the information. The powders of ZrO 2 -a, previously irradiated with beta particles of 90 Sr/ 90 Y, they presented a thermoluminescent curve with two peaks at 150 and 260 C. The fading of the information of the one ZrO 2 -a it was of 20% during the first two hours starting from this time there was one lost of information of 5% to the finish of the 30 days. The reproducibility of the information was of ± 2.5% in standard deviation. (Author)

Modelling the optical bleaching of the thermoluminescence of K2YF5:Pr3+

International Nuclear Information System (INIS)

Marcazzó, J.; Santiago, M.; Khaidukov, N.; Caselli, E.

2012-01-01

Optical bleaching of the thermoluminescence (TL) curve of K 2 YF 5 :Pr 3+ has been observed after optically stimulated luminescence (OSL) readout of pre-irradiated crystals. The traps being responsible for the TL signal are not emptied completely by the optical stimulation. Furthermore, if the illumination time is increased a constant intensity level of the residual TL glow curve is eventually achieved. On the other hand, if the low temperature peak of the glow curve is thermally cleaned, no subsequent OSL is measured. This behavior has been successfully explained by assuming that part of the electrons in the trap being responsible for the low temperature glow peak of K 2 YF 5 :Pr 3+ recombine with holes via localized transitions during optical stimulation. During TL all trapped electrons recombine via delocalized transitions. Simulations have been carried out in order to demonstrate the feasibility of the model. - Highlights: ► The optical bleaching of the thermoluminescence of K2YF5:Pr 3+ has been studied. ► A model accounting for the optical bleaching has been put forward. ► Thermoluminescence occurs via delocalized transitions. ► Localized transitions occur during optical stimulation.

Thermoluminescence of thin films deposited by laser ablation; Termoluminiscencia de peliculas delgadas depositadas por ablacion laser

Energy Technology Data Exchange (ETDEWEB)

Escobar A, L.; Camps, E.; Arrieta, A.; Romero, S.; Gonzalez, P.R.; Olea M, O.; Diaz E, R. [Depto. de Fisica, ININ, A.P. 18-1027, 11801 Mexico D.F. (Mexico)

2003-07-01

Materials in thin film form have received great attention in the last few years mainly because of their singular properties, which may differ significantly from their bulk attributes making them attractive for a wide variety of applications. In particular, thermoluminescence (Tl) properties of thin films have been studied recently owing to their potential applications in detection for both ionizing and non ionizing radiation. The aim of the present work is to report the synthesis and characterization of C Nx, aluminum oxide and titanium oxide thin films. Thermoluminescence response of the obtained thin films was studied after subject thin films to UV radiation (254 nm) as well as to gamma radiation (Co-60). Thermoluminescence glow curves exhibited a peak centered at 150 C for CN{sub x} whereas for titanium oxide the glow curve shows a maximum peaking at 171 C. Characterization of the physical properties of the deposited materials is presented. (Author)

Thermoluminescence in medical dosimetry

International Nuclear Information System (INIS)

Rivera, T.

2011-10-01

The dosimetry by thermoluminescence (Tl) is applied in the entire world for the dosimetry of ionizing radiations specially to personal and medical dosimetry. This dosimetry method has been very interesting for measures in vivo because the Tl dosimeters have the advantage of being very sensitive in a very small volume and they are also equivalent to tissue and they do not need additional accessories (for example, cable, electrometer, etc.) The main characteristics of the diverse Tl materials to be used in the radiation measures and practical applications are: the Tl curve, the share homogeneity, the signal stability after the irradiation, precision and exactitude, the response in function with the dose and the energy influence. In this work a brief summary of the advances of the radiations dosimetry is presented by means of the thermally stimulated luminescence and its application to the dosimetry in radiotherapy. (Author)

Thermally stimulated conductivity and thermoluminescence from Al2O3 : C

DEFF Research Database (Denmark)

Agersnap Larsen, N.; Bøtter-Jensen, L.; McKeever, S.W.S.

1999-01-01

Simultaneous measurements of thermoluminescence (TL) and thermally stimulated conductivity (TSC) are reported on single-crystal dosimetry-quality Al2O3:C following gamma irradiation at room temperature. Analysis of the data reveals a superposition of several first-order TL and TSC peaks caused...

Measurement of the dose by dispersed radiation in a lineal accelerator using thermoluminescent dosimeters of CaSO4:Dy

International Nuclear Information System (INIS)

Chavez C, N.; Torijano, E.; Azorin, J.; Herrera, A.

2014-08-01

The thermoluminescence (Tl) is based on the principle of the luminescent in a material when is heated below their incandescence temperature. Is a technique very used in dosimetry that is based on the property that have most of the crystalline materials regarding the storage of the energy that they absorb when are exposed to the ionizing radiations. When this material has been irradiated previously, the radioactive energy that contains is liberated in form of light. In general, the principles that govern the thermoluminescence are in essence the same of those responsible for all the luminescent processes and, this way, the thermoluminescence is one of the processes that are part of the luminescence phenomenon. For this work, the dispersed radiation was measured in the therapy area of the lineal accelerator of medical use type Elekta, using thermoluminescent dosimeters of CaSO 4 :Dy + Ptfe developed and elaborated in the Universidad Autonoma Metropolitana, Unidad Iztapalapa. With the dosimeters already characterized and calibrated, we proceeded to measure the dispersed radiation being a patient in treatment. The results showed values for the dispersed radiation the order of a third of the dose received by the patient on the treatment table at 30 cm of the direct beam and the order of a hundredth in the control area (4 m of the direct beam, approximately). The conclusion is that the thermoluminescent dosimeters of CaSO 4 : Dy + Ptfe are appropriate to measure dispersed radiation dose in radiotherapy. (author)

Performance tests of a CaSO4:Dy based thermoluminescence personal dosemeter

International Nuclear Information System (INIS)

Azorin, J.; Gutierrez, A.; Niewiadomski, T.

1986-01-01

In order to replace LiF commercial thermoluminescence dosemeters (TLDs) now used in personnel monitoring, we developed a TLD personnel monitoring badge based on pellets of CaSO 4 :Dy bound in pure KBr placed in plastic holders provided with 0.8 mm Pb filters to compensate for the energy dependence of CaSO 4 :Dy. Performance tests, based on the proposals of international standards for TLDs intended to be used as general deep tissue personal dosemeters, were done by developing the detailed test methods both for the tests required by the International Atomic Energy Agency (fading, linearity, effect of fluorescent light and sunlight and stability under standard climatic conditions) and to meet the requirements of the International Electrotechnical Commission (batch homogeneity, detection threshold, stability of zero point repeatibility and residual). Initial tests showed a high residual and an increase of inhomogeneity. However, these drawbacks were overcome by changing the annealing procedure and the readout conditions. Using these new conditions TLDs met all the requirements for personal dosemeters. (author)

Effect of Mineral Composition on Thermoluminescence Analysis of Irradiated Garlics

International Nuclear Information System (INIS)

Sookkasem, Atitaya; Wanwisa, Sudprasert; Vitittheeranon, Arag

2009-07-01

Full text: Thermoluminescence (TL) is one of the most popular techniques used for identification of irradiated foods such as spices, herbs and dried fruits in accordance with the Codex Standards. TL analysis is based on the determination of TL of adhering or contaminating minerals in foods. This research aimed to study the effect of mineral composition on the TL intensity. The composited minerals were extracted from 3 types of non-irradiated and irradiated garlic powders by sodium polytungstate solution. X-ray diffraction (XRD) spectroscopy was employed to investigate the type and amount of minerals present in garlic powders. TL of separated minerals were analysed using a Harshaw 4500 TL reader. The results showed that the mineral composition of garlic powders was mainly quartz of varying amounts depending on types of garlics. The TL intensity linearly increased with the amount of quartz present in the samples. It can be concluded that the amount of minerals affect the TL intensity which might influence the identification of irradiated tretment of garlics by thermoluminescence

Measurement of dose enhancement close to high atomic number media using optical fibre thermoluminescence dosimeters

International Nuclear Information System (INIS)

Alalawi, Amani I.; Hugtenburg, R.P.; Abdul Rahman, A.T.; Barry, M.A.; Nisbet, A.; Alzimami, Khalid S.; Bradley, D.A.

2014-01-01

Present interest concerns development of a system to measure photoelectron-enhanced dose close to a tissue interface using analogue gold-coated doped silica-fibre thermoluminescence detectors and an X-ray set operating at 250 kVp. Study is made of the dose enhancement factor for various thicknesses of gold; measurements at a total gold thickness of 160 nm (accounting for incident and exiting photons) produces a mean measured dose enhancement factor of 1.33±0.01 To verify results, simulations of the experimental setup have been performed. - Highlights: • Dose enhancement • Thermoluminescence dosimeter • Monte Carlo simulation

Incompatibility of sensitisation and re-estimation of lithium fluoride thermoluminescent phosphor

International Nuclear Information System (INIS)

Bartlett, D.T.; Sandford, D.J.

1978-01-01

A technique of useful sensitisation of lithium fluoride thermoluminescent phosphor has been reported by Mayhugh and Fullerton, (USAEC Report COO-1105-209, 1974). This technique differs from that previously described (Cameron and Zimmerman, USAEC Report COO-1105-102, 1965) in that during the anneal at 300 degrees C which follows the high pre-dose, the phosphor is simultaneously exposed to 254 nm ultraviolet light. It is reported that this method removes interfering centres and hence reduces the lowest detectable dose. Sensitisation also has the advantages of improved tissue equivalence and increased range of linearity. However, a disadvantage of both techniques of sensitisation is that for sensitised phosphor, absorbed doses cannot be re-estimated by photo-transferred thermoluminescence. Results are compared for discs of lithium fluoride in PTFE, some of which were sensitised by each method, and some left unsensitised. It is concluded that for routine personal dosimetry the disadvantages of the loss of the facility to re-estimate absorbed dose outweighs the reported advantages of sensitisation. (author)

Thermoluminescence dosimetry: State-of-the-art and frontiers of future research

International Nuclear Information System (INIS)

Horowitz, Y.S.

2014-01-01

The state-of-the-art in the use of thermoluminescence for the measurement of energy imparted by ionizing radiation is discussed. Emphasis is on the advantages obtainable by the use of computerized glow curve analysis in (i) quality control, (ii) low dose environmental dosimetry, (iii) medical applications (especially precision) and microdosimetric applications, and (iv) mixed field ionization-density–dosimetry. Possible frontiers of future research are highlighted: (i) vector representation in glow curve analysis, (ii) combined OSL/TL measurements, (iii) detection of sub-ionization electrons, (iv) requirements for new TL materials and (v) theoretical subjects involving kinetic modeling invoking localized/delocalized recombination applied to dose response and track structure theory including creation of defects. - Highlights:: • State of the art in thermoluminescence dosimetry. • Benefits of computerized glow curve deconvolution. • Frontiers of future research:new materials, mixed-field dosimetry. • Localized/delocalized kinetic theory:ionization density dependence. • Kinetic theory:creation of defects:track structure theory

Proposal of a methodology for quality control in thermoluminescent dosimetry laboratory

International Nuclear Information System (INIS)

Feital, Joao Carlos da S.; Almeida, Claudio Domingues de; Bezerra, Marcos A.

2005-01-01

Taken into account that in thermoluminescence dosimetry adequate selection procedures as well as accurate TLD readings are necessary, this paper presents results of methodology that can be applied as part of quality control programs in thermoluminescence dosimetry laboratories. For the experiment, a set of 200 TLDs ( LiF 100 ) were used and 9 from which were selected, a standard source of Cs -137 , a PTW kiln, a TL 'Harshaw' reader - model 5500 operating under the 'Win Rem' software and a Sr 90 / Y 90 'Bicron' irradiator. In the proceeding the selected dosimeters were irradiated and read 28 times during 18 months, then by one of the standard deviation properties, values up to 14 % were found, for a confidence level of 95 %. The results found and the bibliographic data related to the responses (arbitrary reading) in the crystals used in TLDs, have shown that this methodology can be applied in quality control programs. (author)

Study of a new dosimetric radio-thermoluminescent systems

International Nuclear Information System (INIS)

Cazac, T.C.

1980-01-01

This is the first Romanian study to investigate conditions to obtain the radio-thermo-luminescent systems: MgB 4 O 7 :A(A-Nd,Sm,Eu,Dy,Tb,Dy+Sm and Tb+Sm) MgF 2 A (A=Mn,Dy,Tb,Sm,Li), their essential dosimetric characters, as well as the (MgF 2 =Mn) thermophosphorus mixture with a ( 6 LiF) lithium target. An investigation was developed upon a new category of radio-thermoluminescent detectors with low radiation energy dependence and fading, magnesjum boride activated by several elements of the lanthanides class (Nd,Sm,Eu,Dy,Tb). A new radio-thermoluminescent dosimetric system with high sensitivity and moderate dependence on energy radiation - (Mnsup(2+)) manganese activated magnesium fluoride - was also studied. The author explored application of investigated detectors MgF 2 =Mn, MgB 4 O 7 =Dy and MgB 4 O 7 :Tb in neutron dosimetry in complex gamma-neutron fields. It is deemed that by using the dosimetric systems reported in the thesis in order to measure gamma, beta and neutron radiation doses, dosimetric control can be ensured both in professional dosimetry and in nuclear accident dosimetry, as well as in various basic and applicative investigations. A modest contribution is thus made towards achieving the national nuclear program through an extension of the thermophosphorus range with practical applications in nuclear radiation dosimetry. (author)

Dose measurements in dental radiology using thermoluminescent dosimetry;Medicoes de dose em radiodiagnostico odontologico utilizando dosimetria termoluminescente

Energy Technology Data Exchange (ETDEWEB)

Chiara, Ana Claudia M. de; Costa, Alessandro M. [Universidade de Sao Paulo (FFCLRP/USP), Ribeirao Preto, SP (Brazil). Faculdade de Filosofia, Ciencias e Letras; Pardini, Luiz Carlos [Universidade de Sao Paulo (FORP/USP), Ribeirao Preto, SP (Brazil). Faculdade de Odontologia

2009-07-01

The aim of this work was the implementation of a code of practice for dosimetry in dental radiology using the technique of thermoluminescent dosimetry. General principles for the use of thermoluminescent dosimeters were followed. The irradiations were performed using ten X-ray equipment for intra-oral radiography and an X-ray equipment for panoramic radiography. The incident air kerma was evaluated for five different exposure times used in clinical practice for intra-oral radiographs. Using a backscatter factor of 1.2, it was observed that approximately 40% of the entrance skin dose values found for intra-oral radiographs are above the diagnostic reference level recommended in national regulation. Different configurations of voltage and current were used representing the exposure as a child, woman and man for panoramic radiographs. The results obtained for the air kerma area product were respectively 53.3 +- 5.2 mGy.cm{sup 2}, 101.5 +- 9.5 mGy.cm{sup 2} and 116.8 +- 10.4 mGy.cm{sup 2}. The use of thermoluminescent dosimetry requires several procedures before a result is recorded. The use of dosimeters with ionization chambers or semiconductors provides a simple and robust method for routine measurements. However, the use of thermoluminescent dosimetry can be of great value to large-scale surveys to establish diagnostic reference levels. (author)

Thermoluminescence as a complementary technique for the toxicological evaluation of chemicals in photosynthetic organisms

Energy Technology Data Exchange (ETDEWEB)

Repetto, Guillermo, E-mail: grepkuh@upo.es [Departamento de Biología Molecular e Ingeniería Bioquímica, Área de Toxicología, Universidad Pablo de Olavide, Carretera de Utrera km. 1, 41013 Seville (Spain); Zurita, Jorge L. [Departamento de Biología Molecular e Ingeniería Bioquímica, Área de Toxicología, Universidad Pablo de Olavide, Carretera de Utrera km. 1, 41013 Seville (Spain); Roncel, Mercedes; Ortega, José M. [Instituto de Bioquímica Vegetal y Fotosíntesis, Universidad de Sevilla-CSIC, Américo Vespucio 49, 41092 Seville (Spain)

2015-01-15

Highlights: • There are very few toxicological applications of thermoluminescence. • It is a luminescence emission induced by heating the sample in the dark. • It is useful for study the photosystem II function and the level of lipid peroxidation. - Abstract: Thermoluminescence is a simple technique very useful for studying electron transfer reactions on photosystem II (standard thermoluminescence) or the level of lipid peroxidation in membranes (high temperature thermoluminescence) in photosynthetic organisms. Both techniques were used to investigate the effects produced on Chlorella vulgaris cells by six compounds: the chemical intermediates bromobenzene and diethanolamine, the antioxidant propyl gallate, the semiconductor indium nitrate, the pesticide sodium monofluoroacetate and the antimalarial drug chloroquine. Electron transfer activity of the photosystem II significantly decreased after the exposure of Chlorella cells to all the six chemicals used. Lipid peroxidation was slightly decreased by the antioxidant propyl gallate, not changed by indium nitrate and very potently stimulated by diethanolamine, chloroquine, sodium monofluoroacetate and bromobenzene. For five of the chemicals studied (not bromobenzene) there is a very good correlation between the cytotoxic effects in Chlorella cells measured by the algal growth inhibition test, and the inhibition of photosystem II activity. The results suggest that one very important effect of these chemicals in Chlorella cells is the inhibition of photosynthetic metabolism by the blocking of photosystem II functionality. In the case of sodium monofluoroacetate, diethanolamine and chloroquine this inhibition seems to be related with the induction of high level of lipid peroxidation in cells that may alter the stability of photosystem II. The results obtained by both techniques supply information that can be used as a supplement to the growth inhibition test and allows a more complete assessment of the effects of

Thermoluminescence as a complementary technique for the toxicological evaluation of chemicals in photosynthetic organisms

International Nuclear Information System (INIS)

Repetto, Guillermo; Zurita, Jorge L.; Roncel, Mercedes; Ortega, José M.

2015-01-01

Highlights: • There are very few toxicological applications of thermoluminescence. • It is a luminescence emission induced by heating the sample in the dark. • It is useful for study the photosystem II function and the level of lipid peroxidation. - Abstract: Thermoluminescence is a simple technique very useful for studying electron transfer reactions on photosystem II (standard thermoluminescence) or the level of lipid peroxidation in membranes (high temperature thermoluminescence) in photosynthetic organisms. Both techniques were used to investigate the effects produced on Chlorella vulgaris cells by six compounds: the chemical intermediates bromobenzene and diethanolamine, the antioxidant propyl gallate, the semiconductor indium nitrate, the pesticide sodium monofluoroacetate and the antimalarial drug chloroquine. Electron transfer activity of the photosystem II significantly decreased after the exposure of Chlorella cells to all the six chemicals used. Lipid peroxidation was slightly decreased by the antioxidant propyl gallate, not changed by indium nitrate and very potently stimulated by diethanolamine, chloroquine, sodium monofluoroacetate and bromobenzene. For five of the chemicals studied (not bromobenzene) there is a very good correlation between the cytotoxic effects in Chlorella cells measured by the algal growth inhibition test, and the inhibition of photosystem II activity. The results suggest that one very important effect of these chemicals in Chlorella cells is the inhibition of photosynthetic metabolism by the blocking of photosystem II functionality. In the case of sodium monofluoroacetate, diethanolamine and chloroquine this inhibition seems to be related with the induction of high level of lipid peroxidation in cells that may alter the stability of photosystem II. The results obtained by both techniques supply information that can be used as a supplement to the growth inhibition test and allows a more complete assessment of the effects of

Automation of TL brick dating by ADAM-1

International Nuclear Information System (INIS)

Cechak, T.; Gerndt, J.; Hirsl, P.; Jirousek, P.; Kubelik, M.; Musilek, L.; Kanaval, J.

2000-01-01

Thermoluminescence has become an established dating method for ceramics and more recently for bricks. Based on the experiences of the work carried out since the late 1970's at the Rathgen-Forschungslabor in Berlin on the dating of bricks from historic architecture, and after evaluating all commercially available and some individually built automated and semi-automated TL-readers, a specially adapted machine for the fine grain dating of bricks was constructed in an interdisciplinary research project, undertaken by a team recruited from three faculties of the Czech Technical University in Prague. The result is the automated TL-reader ADAM-1 (Automated Dating Apparatus for Monuments) for the dating of historic architecture. Both the specific adaptation of the technique and the necessary optimal automation have influenced the design of this TL-reader. The principle advantage of brick as opposed to ceramic TL-dating emerges from the possibility of being able to obtain both a large number of samples and an above average quantity of datable material from each sample. This, together with the specific physical and chemical conditions in a brick wall, allowed a rethinking of the traditional error calculation and thus lower error margins as those obtained when dating ceramic shards. The TL-reader must therefore be able to measure and evaluate automatically numerous samples. The annular sample holder of ADAM-1 has 60 sample positions, which allow the irradiation and evaluation of samples taken from two locations. The thirty samples from one sampling point are divided into subgroups, which are processed in various ways. Three samples serve for a rough estimate of the TL sensitivity of the brick material. Nine samples are used for the measurement of 'natural TL' of the material. A further nine samples are used for testing the sensitivity of the material to beta radiation. The last nine samples serve for the testing of the sensitivity to alpha radiation. To determine the

Rare-earths influence in the thermoluminescent response of monoclinic ZrO{sub 2}; Influencia de tierras raras en la respuesta termoluminiscente de ZrO{sub 2} monoclinico

Energy Technology Data Exchange (ETDEWEB)

Mendoza A, D.; Gonzalez M, P.R. [ININ, 52045 Ocoyoacac, Estado de Mexico (Mexico); Vasquez L, M.J.; Rubio R, E. [Centro Universitario de Vinculacion, BUAP, 72000 Puebla (Mexico)

2005-07-01

Zirconium oxide (ZrO{sub 2}) with rare-earths (Nd, Dy, Eu and Y) as dopant were prepared by sol gel method and irradiated with gamma radiation. The thermoluminescent (TL) signal was studied as function of the impurities present for temperatures from 50 to 350 C. Pure ZrO{sub 2} produces a strong TL signal induced by gamma radiation, with a maximum located at 150 C, while ZrO{sub 2} doped with Nd, Dy and Y showed a TL signal with minor intensity, but with a maximum like to pure ZrO{sub 2}. However, when Eu is present as impurity the TL signal is much smaller than pure ZrO{sub 2}, with a maximum very enlarged. These results indicate that exits a strong influence of the rare-earths presents in the TL response and opens the possibility to control the TL signal in a wide range of dosages allowing to use these systems as a wide range dosimeter. Details of the thermoluminescent behavior of pure and doped ZrO{sub 2} will be discussed. (Author)

Curve thermoluminescent analysis of ZrO2 doped with nanoparticles and Ag nano fibers

International Nuclear Information System (INIS)

Mendoza A, D.; Villa S, G.; Gutierrez W, C.; Perez H, R.; Gonzalez M, P.

2008-01-01

This paper presents the results obtained from the analysis of the high temperature thermoluminescence response induced by UV radiation in pure zirconium (ZrO 2 ) and doped with Ag nanoparticles and Ag nano fibers. The zirconium samples were obtained by the sol-gel method and irradiated with a UV lamp for different times. The results showed that the presence of the dopants change the characteristics of the traps associated with the high temperature peak which is located at 230 C for pure zirconium, and that the greater influence is due the presence of Ag nano fibers, inducing a shift to lower temperatures. It also presents the thermoluminescence response as a function of irradiation time. (Author)

Dosimetric behavior of thermoluminescent dosimeters at low doses in diagnostic radiology

International Nuclear Information System (INIS)

Del Sol F, S.; Garcia S, R.; Guzman M, J.; Sanchez G, D.; Rivera M, T.; Ramirez R, G.; Gaona, E.

2015-10-01

Thermoluminescent (Tl) characteristics of TLD-100, LiF:Mg,Cu,P, and CaSO 4 : Dy the under homogeneous field of X-ray beams of diagnostic irradiation and its verification using thermoluminescent dosimetry is presented. The irradiations were performed utilizing an X-ray beam generated by a Radiology Mexican Company: MRH-II E GMX 325-AF SBV-1 model, with Rotating Anode X-Ray Tube installed in the Hospital Juarez Norte de Mexico in Mexico City. Different thermoluminescent characteristics of dosimetric material were studied, such as, batch homogeneity, Tl glow curve, Tl response as a function of X-ray dose, reproducibility and fading. Materials were calibrated in terms of absorbed dose to the standard calibration distance and positioned in a generic Phantom was used. Dose verification and comparison with the measurements made with that obtained by TLD-100 were analyzed. Preliminary results indicate the dosimetric peak appears at 243, 236 and 277 ± 5 degrees C respectively, these peaks are in agreement with that reported in the literature. Tl glow curve as a function of X-ray dose showed a linearity in the range from 1.76 mGy up to 14.70 mGy for all materials. Fading for a period of one month at room temperature showed low fading LiF:Mg,Cu,P, medium and high for TLD-100 and CaSO 4 : Dy. The results suggest that the three materials are suitable for measurements at low doses in radiodiagnostic, however, for its dosimetric characteristics are most effective for individual applications: personal dosimetry and monitors limb (LiF:Mg,Cu,P), clinical dosimetry and environmental (TLD-100 and CaSO 4 : Dy). (Author)

Thermoluminescence property of LiMgF{sub 3} erbium activated phosphor

Energy Technology Data Exchange (ETDEWEB)

Munoz, I.C. [Departamento de Ciencias Quimico Biologicas, Universidad de Sonora, A.P. 130, Hermosillo, Sonora 83000 (Mexico); Cruz-Zaragoza, E., E-mail: ecruz@nucleares.unam.mx [Instituto de Ciencias Nucleares, Universidad Nacional Autonoma de Mexico, A.P. 70-543, Mexico 04510 D.F. (Mexico); Favalli, A. [Los Alamos National Laboratory, Los Alamos, NM 87545 (United States); Furetta, C. [Touro University Rome, Division of Touro College New York, Circne Gianicolense 15-17, 00153 Rome (Italy)

2012-05-15

The perovskite-like LiMgF{sub 3}:ErF{sub 3} pellets were obtained from the melt formed by LiF and MgF{sub 2} mixed salts in the stoichiometric ratio. The perovskite material was doped with 1, 2 and 4 mol% of ErF{sub 3} impurity. The pellets samples were {sup 60}Co gamma irradiated and their thermoluminescence (TL) properties were analyzed, i.e., dose-response, fading at RT and under UV irradiation, TL signal reproducibility, and kinetic parameters. The intensity of the TL response against irradiation dose was increased remarkably by the high concentration of impurity, and a linear dose-response was observed in the range of 1-10 Gy. The fading observed at RT was about 10-30% after 24 h from irradiation. All samples were exposed from 1 to 200 Gy gamma dose range. The TL glow peaks were found around 367-376, 438-447, 509-521, and 594-611 K, when the doped samples were 1, 2 and 4 mol% of the erbium impurity concentration. The thermoluminescence kinetics parameters of the glow curves have been analyzed using the Computerized Glow Curve Deconvolution (CGCD) method. - Highlights: Black-Right-Pointing-Pointer Perovskite-like LiMgF{sub 3} pellets were doped with 1, 2, and 4 mol% of ErF{sub 3} impurity. Black-Right-Pointing-Pointer Thermoluminescence properties and kinetics parameters were analyzed. Black-Right-Pointing-Pointer Dose-response, fading at RT and under UV irradiation and reproducibility are reported. Black-Right-Pointing-Pointer Four TL glow peaks were observed between 367 and 611 K, for all samples. Black-Right-Pointing-Pointer Glow curves have been analyzed using the CGCD method.

High dose thermoluminescence dosimetry performance of Sol-gel synthesized TiO{sub 2} phosphors

Energy Technology Data Exchange (ETDEWEB)

Salas J, Ch. J.; Cruz V, C. [Universidad de Sonora, Departamento de Investigacion en Polimeros y Materiales, Apdo. Postal 130, 83000 Hermosillo, Sonora (Mexico); Castillo U, D. M.; Flores M, K. [Universidad de Sonora, Departamento de Ciencias Quimico Biologicas, Apdo. Postal 130, 83000 Hermosillo, Sonora (Mexico); Bernal, R. [Universidad de Sonora, Departamento de Investigacion en Fisica, Apdo. Postal 5-088, 83190 Hermosillo, Sonora (Mexico); Castano, V. M., E-mail: castillouzeta@gmail.com [UNAM, Instituto de Fisica, Centro de Fisica Aplicada y Tecnologia Avanzada, Apdo. Postal 1-1010, Queretaro, Qro. (Mexico)

2015-10-15

Full text: TiO{sub 2} is a ceramic material with many applications due to their different crystalline phases (rutile, anatase and brookite). It has attracted attention in several fields because their high mechanical strength, chemical stability and ion-conducting properties. Moreover, in recent years, some research groups gained interest in the thermoluminescence features of TiO{sub 2} concerning their potential use as thermoluminescence dosimeter. In this work, we present experimental results obtained in the first stage of a long-term research project focused in the synthesis of TiO{sub 2} phosphors for dosimetric applications. The thermoluminescent characterization of samples was carried out after being exposed to beta particle irradiation. TiO{sub 2} was prepared by alkoxide sol-gel route using titanium tetrabutoxide as precursor, ethanol, water and ammonia as catalyst. Pellet-shaped samples were annealed at 700 degrees C for 6 h in air atmosphere followed by slow cooling, and then were exposed to radiation doses from 25 to 400 Gy. The glow curves display maxima located at 103 and 238 degrees C when a 5 C/s heating rate is used. From the experimental results here presented, we conclude that TiO{sub 2} is a promising material to develop high dose Tl dosimeters. (Author)

Evaluation of new and conventional thermoluminescent phosphors for environmental monitoring using automated thermoluminescent dosimeter readers

International Nuclear Information System (INIS)

Rathbone, B.A.; Endres, A.W.; Antonio, E.J.

1994-10-01

In recent years, there has been considerable interest in a new generation of super-sensitive thermoluminescent (TL) phosphors for potential use in routine personnel and environmental monitoring. Two of these phosphors, α-Al 2 O 3 :C and LiF:Mg,Cu,P, are evaluated in this paper for selected characteristics relevant to environmental monitoring, along with two conventional phosphors widely used in environmental monitoring, LiF:Mg,Ti and CaF 2 :Dy. The characteristics evaluated are light-induced fading, light-induced background, linearity and variability at low dose, and the minimum measurable dose. These characteristics were determined using an automated commercial dosimetry system (Harshaw System 8800) and routine processing protocols. Annealing and readout protocols for each phosphor were optimized for use in a large-scale environmental monitoring program

TL dating of pottery sherds and baked soil from the Xian Terracotta Army Site, Shaanxi Province, China

International Nuclear Information System (INIS)

Lu Yanchou; Zhang Jingzhao; Xie Jun

1988-01-01

Six ceramics and two baked soil samples collected from the famous Xian Terracotta Army Site have been dated by using fine grain (2-8 μ) thermoluminescence (TL) technique. Five samples of pottery sherds exhibited peak TL at about 275 0 C and 395 0 C gave the TL age ranges from 2.13 ± 0.14 ka to 2.25 ± 0.14 ka and a mean TL age of 2.20 ± 0.15 ka, with a good plateau in the range of 290-400 0 C. Another sample, however, showed a larger peak at 365 0 C and could not be dated because of serious fading. TL ages of 1.93 ± 0.13 ka and 2.20 ± 0.19 ka have been also obtained from the baked soil samples with a plateau between 300 and 350 0 C. The TL dates of the ceramics and baked soil are consistent with C-14 dates on charcoal samples taken from the same layer in Xian Terracotta Army Site. It is consistent with other evidence that the Terracotta Army figures were made about 2200 yr ago and that the site burned down soon afterwards. (author)

Study of thermoluminescence response of purple to violet amethyst quartz from Balikesir, Turkey

International Nuclear Information System (INIS)

Nur, N.; Yeğingil, Z.; Topaksu, M.; Kurt, K.; Doğan, T.; Sarıgül, N.; Yüksel, M.; Altunal, V.; Özdemir, A.; Güçkan, V.; Günay, I.

2015-01-01

Highlights: • We reported on dosimetric characterisation of natural amethyst quartz specimens from Turkey, using TL technique. • The thermoluminescence characterisation tests were performed under the beta radiation exposure. • The IT peaks ∼230 °C show superlinear dose response behavior (g(D) > 1) between 1 Gy and 5 kGy. The HT peaks ∼300 °C show linear behavior (g(D) = 1) at low dose levels (1 < D < 20 Gy) and superlinearity (g(D) > 1) between 20 Gy < D < 2 kGy. • Deviations were determined for recycling measurements for various dose values of 0.1, 0.5, 0.8 and 1 kGy. • Amethyst quartz has great potential to be investigated for dosimetry purpose. - Abstract: In thermoluminescence (TL) dosimetry, the phosphor amethyst quartz as a thermoluminescent, appears to be one of the materials arousing the highest interest. In this study the dosimetric characteristics of natural amethyst quartz crystals collected from Balikesir–Dursunbey (Turkey) were investigated for the purpose of determination of the general properties that phosphors should have in order to be useful for thermoluminescence dosimetry. The natural thermoluminescence was drained by annealing the powder samples at 450 °C for 1.5 h. The effects of high temperature annealing, dose response curves, glow curves after a postirradiation annealing, reusability of the samples and storage of trapped electrons in dark at room temperature were clarified through irradiating the samples with the desired exposures by 90 Sr/ 90 Y beta particles. Isothermal annealing before and after irradiation was found to have a definite effect upon the TL glow curve of amethyst crystal powder. The same sample varied in sensitivity depending upon its previous thermal and radiation history. The peak heights of the glow peaks were examined with respect to dose response at dose levels between 1 Gy and 5 kGy. The intermediate temperature (IT) and high temperature (HT) peaks of 230 °C and 300 °C, respectively, exhibit dose�

Study of thermoluminescence response of purple to violet amethyst quartz from Balikesir, Turkey

Energy Technology Data Exchange (ETDEWEB)

Nur, N., E-mail: nnur@adiyaman.edu.tr [Adiyaman University, Engineering Faculty, Department of Electrical and Electronic Engineering, 02040 Adiyaman (Turkey); Yeğingil, Z.; Topaksu, M. [Cukurova University, Art and Sciences Faculty, Physics Department, 01330 Adana (Turkey); Kurt, K. [University of Mersin, Science and Art Faculty, Physics Department, 33343 Mersin (Turkey); Doğan, T. [Cukurova University, Vocational School of Imamoglu, Department of Technical Programs, 01700 Adana (Turkey); Sarıgül, N. [Institute of Nuclear Science, Hacettepe University, 06532 Ankara (Turkey); Yüksel, M.; Altunal, V.; Özdemir, A.; Güçkan, V. [Cukurova University, Art and Sciences Faculty, Physics Department, 01330 Adana (Turkey); Günay, I. [Cukurova University, Medicine Faculty, Biophysics Department, Adana (Turkey)

2015-09-01

Highlights: • We reported on dosimetric characterisation of natural amethyst quartz specimens from Turkey, using TL technique. • The thermoluminescence characterisation tests were performed under the beta radiation exposure. • The IT peaks ∼230 °C show superlinear dose response behavior (g(D) > 1) between 1 Gy and 5 kGy. The HT peaks ∼300 °C show linear behavior (g(D) = 1) at low dose levels (1 < D < 20 Gy) and superlinearity (g(D) > 1) between 20 Gy < D < 2 kGy. • Deviations were determined for recycling measurements for various dose values of 0.1, 0.5, 0.8 and 1 kGy. • Amethyst quartz has great potential to be investigated for dosimetry purpose. - Abstract: In thermoluminescence (TL) dosimetry, the phosphor amethyst quartz as a thermoluminescent, appears to be one of the materials arousing the highest interest. In this study the dosimetric characteristics of natural amethyst quartz crystals collected from Balikesir–Dursunbey (Turkey) were investigated for the purpose of determination of the general properties that phosphors should have in order to be useful for thermoluminescence dosimetry. The natural thermoluminescence was drained by annealing the powder samples at 450 °C for 1.5 h. The effects of high temperature annealing, dose response curves, glow curves after a postirradiation annealing, reusability of the samples and storage of trapped electrons in dark at room temperature were clarified through irradiating the samples with the desired exposures by {sup 90}Sr/{sup 90}Y beta particles. Isothermal annealing before and after irradiation was found to have a definite effect upon the TL glow curve of amethyst crystal powder. The same sample varied in sensitivity depending upon its previous thermal and radiation history. The peak heights of the glow peaks were examined with respect to dose response at dose levels between 1 Gy and 5 kGy. The intermediate temperature (IT) and high temperature (HT) peaks of 230 °C and 300 °C, respectively

Thermoluminescent dosimetric properties of Descalvado sand

International Nuclear Information System (INIS)

Teixeira, M.I.; Caldas, L.V.E.

2006-01-01

Sand samples proceeding from Descalvado, Sao Paulo, were studied with regard to their dosimetric properties using the thermoluminescence technique (TL) for high doses. These sand samples present steady physical and chemical characteristics to the end items, and they are used in the glass industry and for casting. The TL curves of the samples were obtained after an irradiation at the Gamma-Cell system ( 60 Co), of IPEN. The glow curves present two peaks at 80 C and 220 C approximately. Calibration curves were obtained for doses between 50 Gy and 5 kGy. The results indicate that the sand samples can be used for high-doses dosimetry in several areas of applications of ionizing radiation. (Author)

Thermoluminescent dosimetry in veterinary diagnostic radiology

International Nuclear Information System (INIS)

Hernández-Ruiz, L.; Jimenez-Flores, Y.; Rivera-Montalvo, T.; Arias-Cisneros, L.; Méndez-Aguilar, R.E.; Uribe-Izquierdo, P.

2012-01-01

This paper presents the results of Environmental and Personnel Dosimetry made in a radiology area of a veterinary hospital. Dosimetry was realized using thermoluminescent (TL) materials. Environmental Dosimetry results show that areas closer to the X-ray equipment are safe. Personnel Dosimetry shows important measurements of daily workday in some persons near to the limit established by ICRP. TL results of radiation measurement suggest TLDs are good candidates as a dosimeter to radiation dosimetry in veterinary radiology. - Highlights: ► Personnel dosimetry in laboratory veterinary diagnostic was determined. ► Student workplaces are safe against radiation. ► Efficiency value of apron lead was determined. ► X-ray beams distribution into veterinarian laboratory was measured.

Thermoluminescent dosimetric properties of Descalvado sand

Energy Technology Data Exchange (ETDEWEB)

Teixeira, M.I.; Caldas, L.V.E

2006-07-01

Sand samples proceeding from Descalvado, Sao Paulo, were studied with regard to their dosimetric properties using the thermoluminescence technique (TL) for high doses. These sand samples present steady physical and chemical characteristics to the end items, and they are used in the glass industry and for casting. The TL curves of the samples were obtained after an irradiation at the Gamma-Cell system ({sup 60} Co), of IPEN. The glow curves present two peaks at 80 C and 220 C approximately. Calibration curves were obtained for doses between 50 Gy and 5 kGy. The results indicate that the sand samples can be used for high-doses dosimetry in several areas of applications of ionizing radiation. (Author)

Effect of low irradiation temperature on the thermoluminescent response of doped crystal NaCl:XCl2 :MnCl2(X=Ca, Cd)

International Nuclear Information System (INIS)

Ortiz M, A.; Cruz Z, E.; Furetta, C.; Kitis, G.

2009-10-01

Production of crystalline materials suitable thermoluminescent properties over a wide range of doses is becoming more important to evaluate different radiation fields. However, the thermoluminescence response and the structure of the glow curves may be modified by the participation of defects to low irradiation temperature. In this work it is analyzed the effect of the irradiation temperature, 77 and 200 K on the thermoluminescence response of crystal NaCl:XCl 2 :MnCl 2 (X=Ca, Cd) doubly doped. The glow curves obtained were analyzed using a deconvolution program of CGCD, and the response linearity was analyzed by supra linearity index. (Author)

Comparative measurements of soil gas radon concentration using thermoluminescent and track detectors

Czech Academy of Sciences Publication Activity Database

Turek, Karel; Gelev, M.; Dimov, I.

2004-01-01

Roč. 38, spec. iss. (2004), s. 843-846 ISSN 1350-4487 Institutional research plan: CEZ:AV0Z1048901 Keywords : soil gas * radon concentration * thermoluminescent detectors Subject RIV: BG - Nuclear, Atomic and Molecular Physics, Colliders Impact factor: 0.664, year: 2004

Obtention of a thermoluminescent material for dosimetry of ionizing radiation; Obtencion de un material termoluminiscente para dosimetria de la radiacion ionizante

Energy Technology Data Exchange (ETDEWEB)

Gonzalez M, P R

1990-07-01

The thermoluminescent dosemeters are small crystals which suffer changes in their structure by the radiation effect, being displaced the electrons toward higher energy levels. On heating the previously irradiated crystals, the electrons come back to their base state emitting light photons. The light quantity emitted is proportional to the received radiation dose. The light quantity emitted is proportional to the received radiation dose. The lithium fluoride is one of the thermoluminescent materials considered as tissue equivalents by having a low effective atomic number (Z{sub ef}). At present, the more used commercial product used of this type is the TLD-100*. In this work the obtained results in the preparation of the lithium fluoride thermoluminescent material are presented. This is activated with magnesium (Mg) and titanium (Ti), which we have labelled as: LiF: Mg, Ti. The results from the tests performed for verifying his thermoluminescent properties are presented too, as powder form as in pellets form. These tests were performed in simultaneous form with TLD-100 samples, which is considered as reference. The LiF: Mg, Ti thermoluminescent material manufactured in the ININ presents similar dosimetric characteristics to those ones of the TLD-100. Therefore being able to replace the imported dosemeters. * (TLD-100 is a commercial trademark registered by Harshaw/Filtrol (US) for LiF: Mg, Ti Tl dosemeters) (Author)

Determination of the dose rapidity of a 90 Sr beta radiation source using thermoluminescent dosemeters

International Nuclear Information System (INIS)

Gonzalez M, P.R.; Azorin N, J.; Rivera M, T.

2000-01-01

The thermoluminescent dosemeters developed in Mexico, have been used efficiently in environmental and personal dosimetry. When the dose rate of some source is not known can be estimated with the use of thermoluminescent dosemeters taking in account the geometrical array used in the irradiations for reproducibility of the results in posterior irradiations. In this work it was estimated the dose rate of a 90 Sr- 90 Y beta radiation source which is property of the Nuclear Sciences Institute, UNAM, therefore it was l ended to the Metropolitan Autonomous University- Iztapalapa Unit for the characterization of new Tl materials, taking account of the institutional collaboration agreements. (Author)

Thermoluminescent of induced calcite by gamma and ultraviolet radiation

International Nuclear Information System (INIS)

Lima, J.F. de.

1987-01-01

Samples of brazilian calcite, exposed to gamma radiation in laboratory and heated at constant rate of 2.7 0 C/s, showed three glow peaks at 150, 250 and 350 0 C in their thermoluminescent emission curves. The analysis of these peaks, using different models, indicated that they follow a second order kinetics; it has been obtained, for the activation energy, 1.3, 1.5 and 1.7 eV, and, for the pre-exponential factors, 8.1 x 10 14 , 6.8 x10 13 and 2.4 x 10 12 s -1 . Although the total thermoluminescent emission has stayed constant, the relative height of glow peaks has changed with the temperature of annealing in the range of 400 to 700 0 C. Exposed samples were also illuminated with ultraviolet light and the resultant curves showed partial or total bleaching or some glow peaks and the growth of peaks at lower temperatures. Samples of virgin calcite, submited to increasing exposures of gamma rays, showed a corresponding enhancement of the optical absorption bands in the range of 25000 to 47000 cm -1 A subsequent illumination of these samples with ultraviolet light produced a decrease of the optical absorption bands at the same range. (author) [pt

The initial rise method extended to multiple trapping levels in thermoluminescent materials

Energy Technology Data Exchange (ETDEWEB)

Furetta, C. [CICATA-Legaria, Instituto Politecnico Nacional, 11500 Mexico D.F. (Mexico); Guzman, S. [Instituto de Ciencias Nucleares, Universidad Nacional Autonoma de Mexico, A.P. 70-543, 04510 Mexico D.F. (Mexico); Ruiz, B. [Instituto de Ciencias Nucleares, Universidad Nacional Autonoma de Mexico, A.P. 70-543, 04510 Mexico D.F. (Mexico); Departamento de Agricultura y Ganaderia, Universidad de Sonora, A.P. 305, 83190 Hermosillo, Sonora (Mexico); Cruz-Zaragoza, E., E-mail: ecruz@nucleares.unam.m [Instituto de Ciencias Nucleares, Universidad Nacional Autonoma de Mexico, A.P. 70-543, 04510 Mexico D.F. (Mexico)

2011-02-15

The well known Initial Rise Method (IR) is commonly used to determine the activation energy when only one glow peak is presented and analysed in the phosphor materials. However, when the glow peak is more complex, a wide peak and some holders appear in the structure. The application of the Initial Rise Method is not valid because multiple trapping levels are considered and then the thermoluminescent analysis becomes difficult to perform. This paper shows the case of a complex glow curve structure as an example and shows that the calculation is also possible using the IR method. The aim of the paper is to extend the well known Initial Rise Method (IR) to the case of multiple trapping levels. The IR method is applied to minerals extracted from Nopal cactus and Oregano spices because the thermoluminescent glow curve's shape suggests a trap distribution instead of a single trapping level.

The initial rise method extended to multiple trapping levels in thermoluminescent materials

International Nuclear Information System (INIS)

Furetta, C.; Guzman, S.; Ruiz, B.; Cruz-Zaragoza, E.

2011-01-01

The well known Initial Rise Method (IR) is commonly used to determine the activation energy when only one glow peak is presented and analysed in the phosphor materials. However, when the glow peak is more complex, a wide peak and some holders appear in the structure. The application of the Initial Rise Method is not valid because multiple trapping levels are considered and then the thermoluminescent analysis becomes difficult to perform. This paper shows the case of a complex glow curve structure as an example and shows that the calculation is also possible using the IR method. The aim of the paper is to extend the well known Initial Rise Method (IR) to the case of multiple trapping levels. The IR method is applied to minerals extracted from Nopal cactus and Oregano spices because the thermoluminescent glow curve's shape suggests a trap distribution instead of a single trapping level.

Thermoluminescence of KI:Eu2+ Stimulated by Ultraviolet Irradiation at Different Temperatures

International Nuclear Information System (INIS)

Aguirre de Carcer, I.; Jaque, F.; Townsend, P.D.

1999-01-01

The thermoluminescence (TL) of KI:Eu 2+ after ultraviolet (254 nm) irradiation at different temperatures from -40 deg. C to +40 deg. C has been studied. Two main glow peaks and some minor features have been identified on the thermoluminescence glow curves. Irradiating at low temperature gives a strong peak at γ5 deg. C and a less pronounced one at 230 deg. C. The TL glow peak emission spectra were analysed as consisting of the addition of several Gaussian shaped emission bands. The position of the Gaussian peaks, and their widths, are coincident with divalent europium emission at different sites of the KI:Eu 2+ system. A new emission band centred at 3.05 eV, 0.16 eV FWHM for Eu 2+ has been observed from the TL emission spectra. The changes in the spectral distribution of the TL emission with irradiation temperature are discussed. (author)

Personnel radiation monitoring by thermoluminescence dosimetry (1995-96)

International Nuclear Information System (INIS)

Daw Mi Cho Cho; Daw Yi Yi Khin; Daw San San; U Maung Maung Tin; Daw Hla Hla Win

2001-01-01

Personnel radiation monitoring which is the dose assessment of individual doses from external radiation received by radiation workers has been carried out by Thermoluminescence Dosimetry system consisting of a Vinten Toledo TLD reader, LiF dosimeters and associated equipment. The exposed TLD dosimeters were measured by TLD reader and the dose evaluation and dose registration were done on personal computer. Due to the records of 1995-96, most of the radiation workers complied with the permissible dose recommended by IAEA and ICRP 60. (author)

Method of making isodose curve using thermoluminescence dosemeter

International Nuclear Information System (INIS)

Bakar Ramain, A.

1975-01-01

Line source of 60 Co in the form of needles and tubes are extensively used in radiotherapy in moulds, implants, and intracavitary techniques for the treatment of malignant lesions. It is important to have isodose distributions in tissue for those source for purposes of treatment planning. The isodose distributions have been obtained experimentally by using tinny lithium-fluoride (Lsub(i)F) thermoluminescent dosemeters (TLD) and they are compared to the theoretical results. The distinct advantages of Lsub(i)F (TLD) in such measurements are briefly discussed. (author)

Thermoluminescent properties of CVD diamond: applications to ionising radiation dosimetry

International Nuclear Information System (INIS)

Petitfils, A.

2007-09-01

Remarkable properties of synthetic diamond (human soft tissue equivalence, chemical stability, non-toxicity) make this material suitable for medical application as thermoluminescent dosimeter (TLD). This work highlights the interest of this material as radiotherapy TLD. In the first stage of this work, we looked after thermoluminescent (TL) and dosimetric properties of polycrystalline diamond made by Chemically Vapor Deposited (CVD) synthesis. Dosimetric characteristics are satisfactory as TLD for medical application. Luminescence thermal quenching on diamond has been investigated. This phenomenon leads to a decrease of dosimetric TL peak sensitivity when the heating rate increases. The second part of this work analyses the use of synthetic diamond as TLD in radiotherapy. Dose profiles, depth dose distributions and the cartography of an electron beam obtained with our samples are in very good agreement with results from an ionisation chamber. It is clearly shown that CVD) diamond is of interest to check beams of treatment accelerators. The use of these samples in a control of treatment with Intensity Modulated Radiation Therapy underlines good response of synthetic diamond in high dose gradient areas. These results indicate that CVD diamond is a promising material for radiotherapy dosimetry. (author)

Luminescence dating: methodological research and application to volcanism in the Laschamp environment

International Nuclear Information System (INIS)

Bassinet, C.

2007-03-01

The aim of this work was to date lava flows from the Chaine des Puys (Massif Central, France) which were chronologically situated during the period of the Laschamp paleo-magnetic event (30-50 ka). The methods used were thermoluminescence and optically stimulated luminescence applied to quartz grains and quartz pebbles extracted from sediments baked by the lava flows. These minerals often emit luminescence signals exhibiting erratic behaviour. Thus, their radiation doses were tentatively determined by various methods to select those which were most likely to yield reliable results. These intercomparisons highlighted a dispersion of results beyond what could be expected from the uncertainties usually associated with each measurement. In the majority of cases, these observations forced us to propose a relatively wide interval in which the most probable age of the sample is included. (author)

Statistics and the additive dose method in TL dating

International Nuclear Information System (INIS)

Scott, E.M.

1988-01-01

Estimation of the palaeo-dose and its associated error in thermoluminescence (TL) dating requires assumptions to be made concerning the error structures of both the TL signal and dose. In this paper, we consider the sensitivity of palaeo-dose estimation to different error structures and describe techniques for estimation of the resultant palaeo-dose errors. We also indicate how the validity of the assumptions may be verified. We have taken the approach that procedures for the analysis of a glow curve at a single temperature must first be proved prior to their inclusion in a full analysis of the glow curves over a series of temperatures. Thus, the paper deals mainly with the analysis of the univariate structure of glow curves, i.e. estimation of the palaeo-dose and error at each temperature, but in the final section of the paper, we discuss briefly the multivariate structure of the results including automatic detection of plateau regions. (author)

Development of Mg B4 O7:Dy thermoluminescent solid dosemeter for using on the thermal neutron dosimetry

International Nuclear Information System (INIS)

Potiens Junior, A.J.; Campos, L.L.; Todo, A.S.

1992-01-01

The magnesium tetraborate doped with dysprosium (Mg B 4 O 7 :O y ) thermoluminescent phosphor is developed, containing boron, which boron 10 isotope has high cross section for thermal neutrons by 10 B (n,α) 7 Li reaction. The nitric acid concentration, the number of washing for removing the excess of boric acid, the powder granulation of Mg B 4 O 7 :O y , the percentage of teflon used as binder and the reproducibility of thermoluminescent answer are also presented. (C.G.C.)

Personnel radiation dosimetry laboratory accreditation programme for thermoluminescent dosimeters : a proposal

International Nuclear Information System (INIS)

Bhatt, B.C.; Srivastava, J.K.; Iyer, P.S.; Venkatraman, G.

1993-01-01

Accreditation for thermoluminescent dosimeters is the process of evaluating a programme intending to use TL personnel dosimeters to measure, report and record dose equivalents received by radiation workers. In order to test the technical competence for conducting personnel dosimetry service as well as to decentralize personnel monitoring service, it has been proposed by Radiological Physics Division (RPhD) to accredit some of the laboratories, in the country. The objectives of this accreditation programme are: (i) to give recognition to competent dosimetry processors, and (ii) to provide periodic evaluation of dosimetry processors, including review of internal quality assurance programme to improve the quality of personnel dosimetry processing. The scientific support for the accreditation programme will be provided by the scientific staff from Radiological Physics Division (RPhD) and Radiation Protection Services Division (RPSD). This paper describes operational and technical requirements for the Personnel Radiation Dosimetry Laboratory Accreditation Programme for Thermoluminescent Dosimeters for Personnel Dosimetry Processors. Besides, many technical documents dealing with the TL Personnel Dosimeter System have been prepared. (author). 5 refs., 2 figs

A thermoluminescence study of vempalle dolomites and its depositional environments

International Nuclear Information System (INIS)

Bhattacharya, A.K.; Rao, C.N.; Kaul, I.K.

1976-01-01

An attempt has been made to interpret the depositional environment of Vempalle dolomites (India) by thermoluminescence method. It has been demonstrated that glow curve patterns reflect the environmental condition of deposition for carbonate sediments. The glow curves were obtained for natural samples as well as samples irradiated by Co 60 and compared. A majority of the samples were concluded to be diagenetic. (A.K.)

The initial rise method extended to multiple trapping levels in thermoluminescent materials.

Science.gov (United States)

Furetta, C; Guzmán, S; Ruiz, B; Cruz-Zaragoza, E

2011-02-01

The well known Initial Rise Method (IR) is commonly used to determine the activation energy when only one glow peak is presented and analysed in the phosphor materials. However, when the glow peak is more complex, a wide peak and some holders appear in the structure. The application of the Initial Rise Method is not valid because multiple trapping levels are considered and then the thermoluminescent analysis becomes difficult to perform. This paper shows the case of a complex glow curve structure as an example and shows that the calculation is also possible using the IR method. The aim of the paper is to extend the well known Initial Rise Method (IR) to the case of multiple trapping levels. The IR method is applied to minerals extracted from Nopal cactus and Oregano spices because the thermoluminescent glow curve's shape suggests a trap distribution instead of a single trapping level. Copyright © 2010 Elsevier Ltd. All rights reserved.

Thermoluminescence study of aluminium oxide doped germanium prepared by combustion synthesis method

Directory of Open Access Journals (Sweden)

Saharin Nurul Syazlin Binti

2017-01-01

Full Text Available The present paper reports the optimum concentration of germanium (Ge dopant in aluminium oxide (AhO3 samples prepared by combustion synthesis (CS method for thermoluminescence (TL studies. The samples were prepared at various Ge concentration i.e. 1 to 5% mol. The phase formation of un-doped and Ge-doped Al2O3 samples was determined using X-ray Diffraction (XRD. The sharp peaks present in the XRD pattern confirms the crystallinity of the samples. The samples were then exposed to 50 Gy Cobalt-60 sources (Gamma cell 220. TL glow curves were measured and recorded using a Harshaw Model 3500 TLD reader. Comparison of TL peaks were observed to obtain the best composition of Ge dopants. A simple glow curves TL peak at around 175̊C for all composition samples was observed. It was also found that the composition of aluminium oxide doped with 3.0% of germanium exhibits the highest thermoluminescence (TL intensity which is 349747.04 (a.u.

Measurement of thermoluminescence - a new method for detecting radiation treatment of spices. Die Messung der Thermolumineszenz - ein neues Verfahren zur Identifizierung strahlenbehandelter Gewuerze

Energy Technology Data Exchange (ETDEWEB)

Heide, L; Boegl, W

1984-12-01

By the experiments described in this report it was examined in 14 different spices to which extent measurements of thermoluminescence intensity of up to 300/sup 0/C are suitable for detecting treatment with ionizing radiation. The optimal weight of each spice was first determined for a later investigation of the dependence of thermoluminescence intensity on dose and postirradiation storage. In most spices, radiation treatment is detectable as long as after a storage period of over 2 months. In general it may be stated that thermoluminescence measurement is a reliable method for detecting radiation treatment in supplement to chemiluminescence measurement.

Thermoluminescent dosemeter in a X-ray diffractometer; Dosimetria termoluminiscente en un difractometro de rayos X

Energy Technology Data Exchange (ETDEWEB)

Mendoza A, D.; Gonzalez M, P.; Falcon B, T. [Instituto Nacional de Investigaciones Nucleares, A.P. 18-1027, Mexico D.F. (Mexico); Castano, V.M. [Instituto de Fisica, UNAM, Laboratorio Juriquilla, A.P. 1-1010, C.P. 76001, Queretaro (Mexico)

1999-07-01

In this work it was presented the results obtained of the dosimetry which was realized in a X-ray diffractometer for powders, trademark Siemens D5000, using the thermoluminescent signal generated by the X-rays in the commercial dosemeter TLD-100 of Harshaw, US. In according to the results obtained, the radiation quantity received by an analysed material in the diffractometer, will be proportional to exposure time and it can vary from unities until tenths of grays. These results are very outstanding when are analysed crystalline materials in a diffractometer, for knowing the present crystalline phases, mainly if these are highly sensitive to the ionizing radiation, as it is the case of the thermoluminescent materials. (Author)

An integral equation method for discrete and continuous distribution of centres in thermoluminescence kinetics

International Nuclear Information System (INIS)

Kantorovich, L.N.; Fogel, G.M.; Gotlib, V.I.

1990-01-01

Thermoluminescence kinetics is discussed within the framework of a band model containing an arbitrary number of types of recombination and trapping centres at an arbitrary correlation of all centre parameters. It is shown that the initial system of kinetic equations is reduced to an equivalent system consisting of two integro-differential equations which permit one to perform an accurate generalisation, in the case of a continuous centre distribution, to their parameters for the description of irradiation and thermoluminescence, taking into account charge carrier redistribution to both types of centre. In addition, if only one electron (hole) channel is taken into account, only one integro-differential equation is obtained. On the basis of this equation a precise algebraic equation is obtained for calculation of the area of an arbitrary part of the thermoluminescence curve (TLC), consisting of one or several peaks, which slightly overlap with other peaks. It is shown that at doses which are less than the saturation dose, when the centres are not completely filled by the charge carriers, the dose dependences of such a part of the TLC may have a non-linear character at a simultaneous linear dependence of the area of the whole TLC. At doses which are greater than the saturation dose, the dose dependences of the area of the whole TLC, as well as of its separate parts, undergo breaks at the saturation doses. (author)

Dosimetry of accidents using thermoluminescence of dental restorative porcelains

International Nuclear Information System (INIS)

Mauricio, C.L.P.; Rosa, L.A.R. da; Cunha, P.G. da

1986-01-01

The thermoluminescence (TL) properties of dental restorative porcelain were investigated with the aim of using this material as a TL dosemeter to estimate high doses in radiological accidents. The irradiations were carried out with a 60 Co gamma source and X rays with effective energies from 29 to 95 KeV. The samples have a limit of detection at about 50R and their reproducibility is better than 15%. Linearity was observed from 50 to 5000R. (Author) [pt

Dose profile measurement in computerized axial tomography equipment using thermoluminescent dosemeters

International Nuclear Information System (INIS)

Azorin V, J.C.; Falcony, C.; Azorin N, J.

2000-01-01

In this work are presented the results about measuring the radiation dose profile in two equipment of computerized axial tomography (Tac). Thermoluminescent dosemeters (Dtl) of LiF, Mg, Cu, P + Ptfe in form of disks were used which were developed and made in Mexico. The results showed that Dtl are appropriated for these type of studies. (Author)

ESR dating of marine fossil shells

International Nuclear Information System (INIS)

Radtke, U.; Mangini, A.; Gruen, R.

1985-01-01

In order to establish the relatively new ESR dating method for marine shells a detailed comparison with the independent U-series technique was carried out. Agreement of both dating methods with the geological classification is strongly dependent on the species investigated and environmental conditions. Several problems encountered in the determination of the accumulated dose as well as the annual dose are discussed. (author)

ESR dating of marine fossil shells

Energy Technology Data Exchange (ETDEWEB)

Radtke, U; Mangini, A; Gruen, R

1985-01-01

In order to establish the relatively new ESR dating method for marine shells a detailed comparison with the independent U-series technique was carried out. Agreement of both dating methods with the geological classification is strongly dependent on the species investigated and environmental conditions. Several problems encountered in the determination of the accumulated dose as well as the annual dose are discussed.

NRC TLD [thermoluminescent dosimeter] Direct Radiation Monitoring Network: Progress report, January-March 1988

International Nuclear Information System (INIS)

Struckmeyer, R.; McNamara, N.

1988-06-01

This report provides the status and results of the NRC Thermoluminescent Dosimeter (TLD) Direct Radiation Monitoring Network. It presents the radiation levels measured in the vicinity of NRC licensed facility sites throughout the country for the first quarter of 1988

Thermoluminescence of Stoichiometric Magnesium-Aluminium Spinel Defects

International Nuclear Information System (INIS)

Kobyakov, V.A.; Gritsina, V.T.; Kazarinov, Yu.G.; Volokitin, V.N.

2005-01-01

The investigations of thermoluminescence of spinel single crystals MgAl 2 O 4 after UV- and X-ray irradiation was provided by using method of self consisting heating. It was shown, that observed maxima at temperatures of ∼360 and ∼530 K in UV- and green ranges of spectra, respectively, are complex and consist of several strongly overlapping partial maxima. By using method of self consisting heating we have revealed the approximate position of partial maxima, which are included in maxima of ∼360 and ∼530 K, and for some partial maxima there was obtained the order of kinetics, activation energies, and frequency factors

Thermoluminescent dosimetry of beta radiations of 90 Sr/ 90 Y using amorphous ZrO2

International Nuclear Information System (INIS)

Rivera M, T.; Olvera T, L.; Azorin N, J.; Barrera R, M.; Soto E, A.M.

2005-01-01

In this work the results of studying the thermoluminescent properties (Tl) of the zirconium oxide in its amorphous state (ZrO 2 -a) before beta radiations of 90 Sr/ 90 Y are presented. The amorphous powders of the zirconium oxide were synthesized by means of the sol-gel technique. The sol-gel process using alkoxides like precursors, is an efficient method to prepare a matrix of zirconium oxide by hydrolysis - condensation of the precursor to form chains of Zr-H 3 and Zr-O 2 . One of the advantages of this technique is the obtention of gels at low temperatures with very high purity and homogeneity. The powders were characterized by means of thermal analysis and by X-ray diffraction. The powders of ZrO 2 -a, previously irradiated with beta particles of 90 Sr/ 90 Y, presented a thermoluminescent curve with two peaks at 150 and 257 C. The dissipation of the information of the one ZrO 2 -a was of 40% the first 2 hours remaining constant the information for the following 30 days. The reproducibility of the information was of ± 2.5% in standard deviation. The studied characteristics allow to propose to the amorphous zirconium oxide as thermoluminescent dosemeter for the detection of beta radiation. (Author)

Thermoluminescent dosimetry of beta radiations of 90 Sr/ 90 Y using ZrO2: Eu

International Nuclear Information System (INIS)

Olvera T, L.; Azorin N, J.; Barrera S, M.; Soto E, A.M.; Rivera M, T.

2005-01-01

In this work the results of studying the thermoluminescent properties (TL) of the doped zirconium oxide with europium (ZrO 2 : Eu 3+ ) before beta radiations of 90 Sr/ 90 Y are presented. The powders of ZrO 2 : Eu 3+ were obtained by means of the sol-gel technique and they were characterized by means of thermal analysis and by X-ray diffraction. The powders of ZrO 2 : Eu 3+ , previously irradiated with beta particles of 90 Sr/ 90 Y, presented a thermoluminescent curve with two peaks at 204 and 292 C respectively. The TL response of the ZrO 2 : Eu 3+ as function of the absorbed dose was lineal from 2 Gy up to 90 Gy. The fading of the information of the ZrO 2 : Eu 3+ was of 10% the first 2 hours remaining almost constant the information by the following 30 days. The ZrO 2 doped with the (Eu 3+ ) ion it was found more sensitive to the beta radiation that the one of zirconium oxide without doping (ZrO 2 ) obtained by the same method. Those studied characteristics allow to propose to the doped zirconium oxide with europium like thermoluminescent dosemeter for the detection of the beta radiation. (Author)

Energy absorption buildup factors for thermoluminescent dosimetric materials and their tissue equivalence

DEFF Research Database (Denmark)

Manohara, S.R.; Hanagodimath, S.M.; Gerward, Leif

2010-01-01

Gamma ray energy-absorption buildup factors were computed using the five-parameter geometric progression (G-P) fitting formula for seven thermoluminescent dosimetric (TLD) materials in the energy range 0.015-15 MeV, and for penetration depths up to 40 mfp (mean free path). The generated energy-absorption...

Thermoluminescence of Zn O thin films deposited by chemical bath; Termoluminiscencia de peliculas delgadas de ZnO depositadas por bano quimico

Energy Technology Data Exchange (ETDEWEB)

Camacho A, M. C.; Cruz V, C. [Universidad de Sonora, Departamento de Investigacion en Polimeros y Materiales, Apdo. Postal 130, 83000 Hermosillo, Sonora (Mexico); Bernal H, R.; Berman M, D. [Universidad de Sonora, Departamento de Investigacion en Fisica, Apdo. Postal 5-088, 83190 Hermosillo, Sonora (Mexico); Castano M, V. M., E-mail: carmencamacho@gimmunison.com [UNAM, Instituto de Fisica, Centro de Fisica Aplicada y Tecnologia Avanzada, Apdo. Postal 1-1010, 76000 Queretaro, Qro. (Mexico)

2015-10-15

Full text: Zn O films on Si were synthesized using a deposition method by chemical bath and thermally treated at 900 degrees C for 12 h in air. The morphological characterization by scanning electron microscopy reveals that uniform films were obtained. To investigate the thermoluminescent properties of the films were exposed to irradiation with beta particles with doses in the range from 0.5 to 128 Gy. The brightness curves obtained using a heating rate of 5 degrees C have two peaks, one at 124 and another at 270 degrees C, and a linear dependence of the integrated thermoluminescence as a function of dose. The second maximum reveals the existence of localized trapping states of potential utility in thermoluminescent dosimetry. (Author)

Thermoluminescence glow curve analysis and CGCD method for erbium doped CaZrO{sub 3} phosphor

Energy Technology Data Exchange (ETDEWEB)

Tiwari, Ratnesh, E-mail: 31rati@gmail.com [Department of Physics, Bhilai Institute of Technology, Raipur, 493661 (India); Chopra, Seema [Department Physics, G.D Goenka Public School (India)

2016-05-06

The manuscript report the synthesis, thermoluminescence study at fixed concentration of Er{sup 3+} (1 mol%) doped CaZrO{sub 3} phosphor. The phosphors were prepared by modified solid state reaction method. The powder sample was characterized by thermoluminescence (TL) glow curve analysis. In TL glow curve the optimized concentration in 1mol% for UV irradiated sample. The kinetic parameters were calculated by computerized glow curve deconvolution (CGCD) techniaue. Trapping parameters gives the information of dosimetry loss in prepared phosphor and its usability in environmental monitoring and for personal monitoring. CGCD is the advance tool for analysis of complicated TL glow curves.

Thermoluminescent response of dosemeters TLD-100 exposed to distinct baker protocols, irradiation and reading

International Nuclear Information System (INIS)

Estrada E, D.

2002-01-01

The interest that motivated the realization of this work is the opposing discrepancy among the values of the efficiency thermoluminescent of heavy charged particles (PCP) regarding gamma radiation (η PCP , γ) reported in different works and gathered recently for Horowitz (Ho 01). The measures of relative thermoluminescent efficiency have importance in relation to the dosimetry associated to medical therapy with heavy charged particle. The measurement of η PCP , γ depends of multiple experimental factors. To understand this dependence it was quantified the effect of using different procedures experimental in the estimate of the relative thermoluminescent efficiency of dosemeters TLD-100 (LiF: Ti; Mg) for protons of 3 MeV regarding gamma rays of 60 Co (η PCP , γ), varying the lot, the presentation, the one baked and the team reader. When was used the same global procedure values they were obtained for (η PCP , γ) inside the interval [0.30, 0.58] for the peak 5 and [0.35, 0.76] for the total thermoluminescent signal (Tl). At the use different equipment, baked and lot are obtained maximum differences of 30%, 12% and 6% respectively in the values of (η PCP , γ) for the peak 5, and 25%, 28% and 7% for the total Tl signal. The changes more significant of 36% and 44% for peak 5 and total signal respectively are obtained when changing the presentation of the dosemeter. As a complementary investigation it was studied the distribution of the Tl signal of each peak in the deconvolution of the curve of brightness with regard to the total signal in exposed dosemeters to high fluence of protons (1x10 10 p/cm 2 ) varying the experimental protocol. It was found that the distribution of the Tl signal has a difference of the order of 5% when changing the used reading team. It was observed that the contribution of the peak 5 regarding the total signal are preserved when changing baked and that it results to be 8% greater for the presentation in dosemeters of 1 x 1 x 1 mm 3

A comparative thermoluminescence and electron spin resonance study of synthetic carbonated A-type hydroxyapatite

International Nuclear Information System (INIS)

Oliveira, L.C.; Rossi, A.M.; Baffa, O.

2012-01-01

Intensity of the 150 °C thermoluminescence peak of beta-irradiated carbonated synthetic A-type hydroxyapatite is approximately 12 times higher than that of the noncarbonated material. Deconvolution of the glow curve showed that this peak is a result of a trap distribution. An attempt was made to relate this thermoluminescence peak enhanced by carbonation with the ESR signal of the CO 2 − radical in natural or synthetic hydroxyapatite. - Highlights: ► Synthetic hydroxyapatite was carbonated with CO 2 . ► TL enhanced by 12 times in carbonated synthetic A-type hydroxyapatite. ► EPR and TL were performed to find out a relation between CO 2 − center and the TL. ► No direct relation was found between the CO 2 − center and TL enhancement.

Thermoluminescence as a tool for monitoring ozone-stressed plants

Energy Technology Data Exchange (ETDEWEB)

Skotnica, J.; Gilbert, M.; Weingart, I.; Wilhelm, C

2003-05-01

Thermoluminescence parameters are more sensitive to ozone than fluorescence parameters (F{sub 0}, F{sub M}, F{sub v}/F{sub M}). - The effect of ozone (6 h, various concentrations from 0 to 350 ppb) on barley (Hordeum vulgare L., cv. Bomi) and tomato (Lycopersicon esculentum L., cv. Yellow Cherry) leaves was investigated in parallel by thermoluminescence (TL) and fluorescence (FL) methods. Several significant changes were found in TL glow curves measured after excitation by one single turnover flash at +2 deg. C in the temperature range from 2 to 170 deg. C immediately after ozone exposure. Contrary to TL, ozone induced only negligible changes in FL parameters F{sub 0}, F{sub M} and F{sub v}/F{sub M}. Measurements done 24 h after ozone exposure showed partial recovery of ozone-induced changes. The extent of recovery was not the same in different parts of TL curves. Fluorescence parameters were not significantly changed. The results demonstrate that TL parameters are more sensitive to ozone than conventially used FL parameters F{sub 0}, F{sub M} and F{sub v}/F{sub M}. Moreover, TL measurements seem to give information not only about the PSII electron transport, but also about the extent of oxidative damage and membrane lipid peroxidation. It is concluded, that TL can be a highly informative tool for monitoring the impact of ozone on plants.

Thermoluminescent response of LiF before variation of the heating rate; Respuesta termoluminiscente de LiF ante variacion de la tasa de calentamiento

Energy Technology Data Exchange (ETDEWEB)

Barrios, R. [Facultad de Quimica, UAEM, 50000 Toluca, Estado de Mexico (Mexico); Avila, O. [ININ, 52045 Ocoyoacac, Estado de Mexico (Mexico)

2003-07-01

Comparisons of glow curves of lithium fluoride dosemeters TLD-100 measured to two heating rates with the purpose of quantifying the change in the temperature of the peaks 5 and 7 for the thermoluminescent reader equipment Harshaw 4000 of the thermoluminescence laboratory of the ININ were carried out. (Author)

Confrontation of thermoluminescence models in lithium fluoride with experimental data

International Nuclear Information System (INIS)

Niewiadomski, T.

1976-12-01

The thermoluminescent properties of lithium fluoride depend on numerous factors and are much more complex than those of other phosphors. The so far developed fragmentary models are meant to explain the relationships between crystal defect structure and the processes involved in TL. An attempt has been made to compare these models with the veryfied experimental data and to point out the observations which are inconsistant with the models. (author)

Substance for thermoluminescent dosimetry of photon radiation in adipose tissue

International Nuclear Information System (INIS)

Kalmykov, L.Z.; Kandel', T.G.

1983-01-01

Substance composition for thermoluminescent photon dosimetry in adipose tissue is proposed which makes it possible to simplify dosimetric measurements and to improve their accuracy. The substance consists of powder-like thermoluminophor Li 2 B 4 O 7 (0.03%Mn) 48-52 mass % and bistriethylammonium dodecahydrododecaborane - 48-52 mass %. The above substance is equivalent in respect to dosimetry to adipose tissue within the 10 keV - 10 MeV energy range

Irradiated Foods Detection by Thermoluminescence (TL) and DEFT/APC Analysis

International Nuclear Information System (INIS)

Choi, I.D.; Kang, E.K.; Yang, J.S.

2004-01-01

Irradiated food detection methods such as Thermoluminescence (TL) and Direct Epifluorescent Filter Technique and Aerobic Plate Count (DEFT/APC) methods were evaluated. Fresh green-onion, onion, and ginger were irradiated at 0, 0.3, 0.6, and 0.9 kGy. Difference in log DEFT/APC units between irradiated and un-irradiated samples was less than 2 long units, below the average threshold value (3-4 long units) of international researches

Thermal and radiation history of meteorites as revealed by their thermoluminescence records

International Nuclear Information System (INIS)

Bhandari, N.

1985-01-01

Attempts are described to derive information about important parameters of the thermal and radiation history of meteorites from a study of depth profile of thermoluminescence coupled to appropriate annealing studies. In this review some possibilities are examined, emphasizing various factors cardinal to any meaningful application of TL in meteoritics. (author)

Solid thermoluminescent dosemeter of sodium tetraborate and brazilian fluoride sensitive to thermal neutrons

International Nuclear Information System (INIS)

Fratin, L.

1988-01-01

The techniques of compacting sodium tetraborate and natural fluoride mixtures were studied in this work, with the aim of producing a solid dosimeter sensitive to thermal neutrons. The production procedure involves the vitrification of the sodium tetraborate, the grinding, mixture, cold pressing and the sinterization of the pellets. A special arrangement was built for irradiation where paraffin was used as moderator for neutrons from a 241 Am-Be source. Two different mass ratios of sodium tetraborate and flourite showed a linear thermoluminescent response to the neutron fluence in the range of 1.0 to 7.0 x 10 8 n (sub)tcm -2 . Solid dosimeters, manufactured from natural fluorite and sodium chloride, showed a response to gamma radiation similar to the response of the dosimeters sensitive to neutrons. These dosimeters are need to identify the proportion of thermoluminescent response due to gamma radiation present in a neutron field. (author) [pt

Macroscopic polarization and thermoluminescence of barium niobate - sodium niobate

International Nuclear Information System (INIS)

Gorban', I.S.; Gumenyuk, A.F.; Omel'yanenko, V.A.

1989-01-01

Thermoluminescence (TL) of initial and thermally treated purposely undoped crystals of barium niobate - sodium has been studied within 85-400 K. The TL intensity is found to depend on the temperature to which the sample has been heated. A conclusion is drawn that nonstationarity of the TL properties is due to slowly occuring processes of compensation of pyrocharge, which depend on the temperatural prehistory of the sample. A mechanism of the traps transformation in a strong pyrofield of high-impedance crystals is discussed

Study on the fast neutron sensitivity of thermoluminescent detectors

International Nuclear Information System (INIS)

Szabo, P.P.; Palfalvi, J.

1984-03-01

Fast neutron (14.7 MeV) sensitivity of several thermoluminescent detectors was determined. The investigated detectors were MTS-N type pellets (made in Poland) used routinely in the authors' institute for personnel dosimetry, 7 LiF powder used for accident dosimetry, CaSO 4 :Dy and CaSO 4 :Tm powders (made in Hungary) used for enviromental monitoring and space dosimetry. Both free-in-air and on-phantom irradiations were performed. The new results are compared with responses calculated and measured earlier. (author)

TL sensitivity constancy of quartz upon UV+(β,γ) irradiation cycle: An improvement on dating methodology

International Nuclear Information System (INIS)

Souza, J.H.

1985-01-01

Thermoluminescence (TL) sensivitivy of natural quartz (beaches, paleobeaches and fixed dunes) to Beta and Gamma rays has been studied in a temperature range between 250-400 0 C, before and after bleaching by solar irradiation. A first TL glow growth curve was obtained through Beta irradiation of 'as found' samples and a second glow growth curve was obtained by bleaching through solar irradiation the TL acquired either through an excitation Gamma dose or through environmental radiation to finally re-irradiate the samples under Beta rays. Experimental results showing the constancy of sensitivity, for doses of until about 10K rads, are the basis for a proposal to improve TL dating methodology expanding its present limits. (Author) [pt

Thermoluminescence properties of CaO powder obtained from chicken eggshells

International Nuclear Information System (INIS)

Nagabhushana, K.R.; Lokesha, H.S.; Satyanarayana Reddy, S.; Prakash, D.; Veerabhadraswamy, M.; Bhagyalakshmi, H.; Jayaramaiah, J.R.

2017-01-01

Eggshell wastage has created serious problem in disposal of the food processing industry which has been triggered the thoughts of researchers to use wasted eggshells as good source of calcium. In the present work, calcium oxide (CaO) has been synthesized by combustion process in furnace (F–CaO) and microwave oven (M–CaO) using the source of chicken eggshells. The obtained F–CaO and M–CaO are characterized by XRD, SEM with EDX and thermoluminescence (TL) technique. XRD pattern of both the samples show cubic phase with crystallite size 45–52 nm. TL glow curves are recorded for various gamma radiation dose (300–4000 Gy). Two TL glows, a small peak at 424 K and stronger peak at 597 K are observed. TL response of M–CaO is 2.67 times higher than F–CaO sample. TL kinetic parameters are calculated by computerized curve deconvolution analysis (CCDA) and discussed. - Highlights: • Calcium oxide powders have been synthesized using chicken egg shells as raw material. • Crystallite size was found to be 45–52 nm. • CaO derived from eggshells shows good thermoluminescence TL response. • TL response of the M–CaO is 2.67 times higher than the F–CaO sample.

Adjustment model of thermoluminescence experimental data

International Nuclear Information System (INIS)

Moreno y Moreno, A.; Moreno B, A.

2002-01-01

This model adjusts the experimental results for thermoluminescence according to the equation: I (T) = I (a i * exp (-1/b i * (T-C i )) where: a i , b i , c i are the i-Th peak adjusted to a gaussian curve. The adjustments of the curve can be operated manual or analytically using the macro function and the solver.xla complement installed previously in the computational system. In this work it is shown: 1. The information of experimental data from a LiF curve obtained from the Physics Institute of UNAM which the data adjustment model is operated in the macro type. 2. A LiF curve of four peaks obtained from Harshaw information simulated in Microsoft Excel, discussed in previous works, as a reference not in macro. (Author)

Age determination in archeometry

International Nuclear Information System (INIS)

Vagner, G.

1984-01-01

Definition of archeometry is given. Physical and chemical methods for dating used in archaeology at present are briefly considered. Among them a radiocarbon method widely used in archaeological laboratories the world, K-Ar method used seldom and for specimens of more then 10 5 years old. Uranium methods 230 Th/ 234 U, 231 Pa/ 235 U are used for dating calcium incrustations in paleolithic cavities, 210 Pb/ 226 Ra are used for establishing authenticity of pictures containing lead pigment. Me-- thods based on the phenomenon of residual thermomagnetism, chemical reactions are also used. Methods for dating thermoluminescent and fission tracks are considered in detail

Ultraviolet dosimetry using thermoluminescent phosphors - an update

International Nuclear Information System (INIS)

Nagpal, J.S.

1998-04-01

Intrinsic response of various thermoluminescent (TL) materials such as CaSO 4 (Dy, Eu, Mn, Sm, Tb, or Tm), LiF (Mg, Cu, P), Mg 2 SiO 4 :Tb, CaF 2 :Dy, CaF 2 :Tb, ThO 2 :Tb and Al 2 O 3 (Si, Ti); cathodoluminescent phosphors Y 3 Al 5 O 12 :Ce, Y 3 Al 5 O 12 :Tb and Y(V,P)O 4 :Eu; and fluorescent lamp phosphors calcium halophosphate (Mn,Sb) and Ce Mg aluminate (Eu, Tb) to ultraviolet (UV) radiations has been studied. Intrinsic TL response of most of the phosphors is rate (radiant flux) dependent. For the first time, UV response of the materials is reported for a fixed total radiant energy (total UV dose), at a single radiant flux (260 μW.cm -2 ), for an appropriate comparison. A wide range of UV sensitivity is observed. Studies conducted using UV radiation from two unfiltered low pressure mercury lamps show significant differences in glow curves, as compared to those obtained with nearly monochromatic UV radiations. Photons of wavelength 365 nm induce bleaching of TL induced by 254 nm photons, in most of the materials. Sequential/tandem exposures to 254 nm and 365 nm photons have yielded new but alarming results in CaF 2 :Tb. Preferential induction and bleaching of specific TL glow peaks by 365 nm and 254 nm photons are interesting characteristics discovered in CaSO 4 :Eu. Photoluminescence studies of Tb 3+ and Eu 3+ activated phosphors have augmented the inferences drawn from the bleaching effects produced by 365 nm photons. Earlier work carried out on phototransferred thermoluminescence of CaSO 4 :Dy-teflon dosimeters, TLD-100, Mg 2 SiO 4 :Tb and Al 2 O 3 (Si,Ti) has also been reviewed. (author)

History of radiocarbon dating

Energy Technology Data Exchange (ETDEWEB)

Libby, W F [Department of Chemistry and Institute of Geophysics, University of California, Los Angeles, CA (United States)

1967-08-15

The development is traced of radiocarbon dating from its birth in curiosity regarding the effects of cosmic radiation on Earth. Discussed in historical perspective are: the significance of the initial measurements in determining the course of developments; the advent of the low-level counting technique; attempts to avoid low-level counting by the use of isotopic enrichment; the gradual appearance of the environmental effect due to the combustion of fossil fuel (Suess effect); recognition of the atmosphere ocean barrier for carbon dioxide exchange; detailed understanding of the mixing mechanism from the study of fallout radiocarbon; determination of the new half-life; indexing and the assimilation problem for the massive accumulation of dates; and the proliferation of measurement techniques and the impact of archaeological insight on the validity of radiocarbon dates. (author)

Study of 225 deg C thermoluminescent of quartz inclusions extracted from cementitious building materials

International Nuclear Information System (INIS)

Campos, Simara S.; Almeida, Geangela M. de; Souza, Suzana O.

2009-01-01

Incidents of excessive exposure of the population to ionizing radiation could result from a nuclear explosion, the direct exposure to a source theft or loss or an accidental exposure to a source without shielding, for example. During these incidents the victims seldom are using individual protection equipment used in the measurement and control of the doses that were exposed. One of the ways found to the doses assessment due to exposure to this type of accident is the retrospective dosimetry, which determines the excessive doses of radiation exposure, whether chronological or acute, using common materials available in the public domain. The methodology for the application of retrospective dosimetry for thermoluminescence in buildings previously burned, as bricks, it is already well established. Interest is now turning to the use of cementitious building materials such as mortar and concrete to enlarge the scope of application. This study aimed to examine some of these materials and techniques for their possible application in the doses assessment from an accidental irradiation by thermoluminescence. For this the peak about 225 deg C of natural quartz and it extracted of mortar and concrete was certain your stability for the plateau and storage tests, and also the dependence of your luminescent intensity with radiation dose. Presenting a life relatively tans compared enough to that of the accumulation of natural and long radiation sign for dosimetric applications, besides other favorable characteristics, the mortar presented evidence that is possible for retrospective dosimetry through thermoluminescence. (author)

Performance of thermoluminescent materials for high dose dosimetry

International Nuclear Information System (INIS)

Texeira, Maria I.; Cecatti, Sonia G.P.; Caldas, Linda V.E.

2008-01-01

Cases involving high-doses of ionizing radiation are becoming increasingly common.The objective of this work was to characterize thermoluminescent materials for the dosimetry of workers exposed to high doses. Samples of TLD-200, TLD-400 and TLD-800 pellets from Thermo Electron Corporation were studied in gamma high-doses. Dose-response curves were obtained for doses between 100 mGy and 100 Gy. The reproducibility, the lower detection limits and dose-response curves were obtained for all three materials. The different kinds of detectors show usefulness for dosimetry of workers exposed accidentally to high doses. (author)

Development of BaSO4:Eu thermoluminescence phosphor

International Nuclear Information System (INIS)

Madhusoodanan, U.; Jose, M.T.; Lakshmanan, A.R.

1999-01-01

A highly sensitive thermoluminescence (TL) phosphor based on BaSO 4 :Eu was developed following the coprecipitation technique and firing in argon atmosphere at 1123 K. Photoluminescence studies confirm that firing in argon atmosphere instead of air increased the incorporation of Eu ions in 2+ valence state. At low γ-ray doses, its TL sensitivity is nearly 2 to 3 times higher than that of CaSO 4 :Dy phosphor. The other salient features of this BaSO 4 :Eu TL phosphor are a constant glow curve shape and a nearly linear γ-ray dose response

Preparation of lithium fluoride for thermoluminescent detectors of ionizing radiation

Energy Technology Data Exchange (ETDEWEB)

Mironenko, S.N.; Nepomnyashchikh, A.I.; Ikrami, D.D.; Paramzin, A.S.; Rakhimov, M.Eh.

1985-03-01

The thermostimulated luminescence (TSL) of lithium fluoride monocrystals depending on the method of preparation of starting raw material and features of its preliminary processing is investigated. It is shown that only lithium fluoride of high purity prepared through the stage of formation of hydrofluoride and its subsequent decomposition can be used without any additional processing for manufacturing monocrystal detectors of thermoluminescent dosimetry of the ionizing radiation with low intensity of low temperature peaks.

Thermoluminescence properties of graphene–nano ZnS composite

International Nuclear Information System (INIS)

Sharma, Geeta; Gosavi, S.W.

2014-01-01

This work describes the thermoluminescence (TL) of graphene oxide (GO), reduced graphene oxide (RGO) and graphene–nano ZnS composite. Graphene oxide was synthesized using Hummer's method and then reduced to graphene by hydrazine hydrate. G–ZnS was synthesized via in-situ reduction of graphene oxide (GO) and zinc nitrate [Zn(NO 3 ) 2 ] by sodium sulfide (Na 2 S). The structures of samples were characterized by X-ray diffraction (XRD) and transmission electron microscope (TEM). XRD pattern confirmed the formation of graphene oxide, reduced graphene oxide and G–ZnS lattice. The p-XRD spectrum of G–ZnS shows peaks of ZnS superimposed on those of graphene and the particle size of ZnS in the complex is less than 10 nm. Ultra thin graphene and graphene oxide sheets with size ranging between tens to several hundreds of square nanometers are observed in TEM images. The TEM micrographs of G–ZnS show that ZnS particles are embedded in graphene sheets and the average particle size of ZnS particles in the composite is less than 10 nm. Samples of RGO, GO and G–ZnS were exposed to different doses of γ-rays in the range of 1 Gy to 50 kGy. The reduced graphene oxide (RGO) did not show any thermoluminescence emission. The thermoluminescence glow curve of GO has a single broad peak whose peak position varied between 500 and 550 K with an absorbed dose increasing from 1 Gy to 5000 Gy. GO shows most intense TL peak, positioned at 523.6 K for a dose of 10 kGy. The glow curves of G–ZnS over the entire range of irradiation have single peak positioned between 492 and 527 K with variation in dose from 1 Gy to 50 kGy. G–ZnS shows the most intense TL glow curve for a dose of 50 kGy. The TL response curve of G–ZnS is found to be linear over a larger dose range from 1 Gy to 50 kGy whereas the response curve of GO shows linearity only at low doses up to 100 Gy. -- Highlights: • Graphene oxide, reduced graphene oxide and graphene–nano ZnS were synthesized. • TL of

Correlation between the thermoluminescence and the F centre thermal stability in KBr, KI, NaCl and NaF irradiated at room temperature

International Nuclear Information System (INIS)

Mariani, D. F.

1977-01-01

Over the years several models have been proposed to explain the thermoluminescence in irradiated alkali halides. To verify these models, the thermoluminescence and the thermal stability of the F centres in KBr, K l, NaCl and NaF single crystals irradiated at room temperature with x or gamma rays have been studied. It has been concluded that both phenomena, the thermoluminescence and the F centre thermal stability are two different aspects of the same basic phenomenon, i.e. the recombination of mobile interstitials thermally released from traps with F centres (Ausin V. and Alvarez Rivas J.L. 1972). It has been found in some cases, that the H centres also play the role of recombination centres for interstitials. (Author) 42 refs

Main Achievements 2003-2004 - Interdisciplinary Research - Radiation detection methods for health, earth and environmental sciences - Thermoluminescence (TL) detectors

International Nuclear Information System (INIS)

2005-01-01

The IFJ has over 35 years of experience in the development, production and application of new types of thermoluminescence (TL) detectors, particularly LiF:Mg,Ti and LiF:Mg,Cu,P. Over 600,000 LiF detectors produced at the IFJ PAN are routinely applied in dosimetry services and hospitals in 30 countries. The current research in the field of thermoluminescence concentrates in space dosimetry and novel 2-dimensional detectors for medical applications. The space project (named Matroshka), organized by the European Space Agency, is one of the most ambitious dosimetry experiments in space. In February 2004 an anatomical model of the human body (a humanoid phantom), equipped with over 3500 dedicated thermoluminescent detectors (TLD), developed and produced at IFJ and tested at the Chiba heavy ion accelerator in Japan, was installed outside the International Space Station (ISS) to determine the cosmic radiation doses absorbed in human organs, which would be experienced by astronauts in open space. The phantom will remain in space for one year, after which the detectors will be returned to the IFJ for analysis

Fading of CaSO4 thermoluminescent detectors after exposure to charged particles

Czech Academy of Sciences Publication Activity Database

Pachnerová Brabcová, Kateřina; Štěpán, Václav; Kubančák, Ján; Davídková, Marie; Ambrožová, Iva

2017-01-01

Roč. 106, č. 12 (2017), s. 569-572 ISSN 1350-4487 R&D Projects: GA ČR GJ15-16622Y Institutional support: RVO:61389005 Keywords : thermoluminescent detectors * CaSO4:Dy * fading * charged particles Subject RIV: BG - Nuclear, Atomic and Molecular Physics, Colliders OBOR OECD: Nuclear physics Impact factor: 1.442, year: 2016

Determination of the kinetic parameters of BeO thermoluminescent samples using different methods

Energy Technology Data Exchange (ETDEWEB)

Algarve, Fábio J.; Caldas, Linda V.E., E-mail: fjalgarve@ipen.br, E-mail: lcaldas@ipen.br [Instituto de Pesquisas Energéticas e Nucleares (IPEN/CNEN-SP), São Paulo, SP (Brazil)

2017-07-01

The objective of this work was to determine the kinetic parameters of BeO thermoluminescent (TL) samples. The knowledge of the kinetic parameters is important for the general description of the physical characteristics of a thermoluminescent material. Using a linear heating rate of 5K/s{sup -1}, the BeO peak temperatures obtained were (474.7 ± 1.2) K and (620.5 ± 1.2) K, respectively, for the first and second TL peaks. The peak shape and the glow curve area measurement methods and the Urbach formula have been used for the trap parameter determination. A kinetic order of about two was determined for the first peak, whereas the second peak followed the first-order kinetics according to the geometrical factor. The energy activation values obtained using different kinds of measurements are in good agreement, including the Kitis method for deconvolution of the glow curve. Furthermore the results agree with those presented by other authors. (author)

Thermoluminescent properties of nanocrystalline ZnTe thin films: Structural and morphological studies

Science.gov (United States)

Rajpal, Shashikant; Kumar, S. R.

2018-04-01

Zinc Telluride (ZnTe) is a binary II-VI direct band gap semiconducting material with cubic structure and having potential applications in different opto-electronic devices. Here we investigated the effects of annealing on the thermoluminescence (TL) of ZnTe thin films. A nanocrystalline ZnTe thin film was successfully electrodeposited on nickel substrate and the effect of annealing on structural, morphological, and optical properties were studied. The TL emission spectrum of as deposited sample is weakly emissive in UV region at ∼328 nm. The variation in the annealing temperature results into sharp increase in emission intensity at ∼328 nm along with appearance of a new peak at ∼437 nm in visible region. Thus, the deposited nanocrystalline ZnTe thin films exhibited excellent thermoluminescent properties upon annealing. Furthermore, the influence of annealing (annealed at 400 °C) on the solid state of ZnTe were also studied by XRD, SEM, EDS, AFM. It is observed that ZnTe thin film annealed at 400 °C after deposition provide a smooth and flat texture suited for optoelectronic applications.

Bleaching of the thermoluminescence of feldspars by selected wavelengths present in sunlight

International Nuclear Information System (INIS)

Robertson, G.B.; Prescott, J.R.; Hutton, J.T.

1993-01-01

Feldspars occur in many sediments, and dating them by thermoluminescence (TL) requires a knowledge of how efficiently sunlight bleaches these minerals. The relative bleaching efficiencies of various wavelengths have been investigated for four alkali feldspars and an oligoclase, using the natural TL of the samples and the artificial TL induced by laboratory irradiation, bleached by wavelengths in the range 322-550 nm. Ultraviolet wavelengths are more efficient than the longer wavelengths at bleaching all the glow-curve peaks and are responsible for most of the phototransfer from high-temperature peaks to low-temperature peaks. Some feldspars show an initial increase in TL intensity with bleaching. Two sanidines of similar bulk composition but different TL glow curves show different dependences on bleaching wavelength. In a sodic sanidine with a dominant 240 o C peak the energy required to bleach to 50% was a thousand times greater at 550 nm than at 322 nm. In contrast, another sanidine with a complex glow curve between 150 and 450 o C showed a much slower change in the 330 o C peak with wavelength - a factor of 10 between 322 and 550 nm - with a region between 400 and 500 nm which was almost independent of wavelength. This behaviour is explained by competing mechanisms of phototransfer and bleaching which depend on wavelength in different ways. (author)

Thermoluminescent dosimetry of new phosphors of Zn O exposed to beta radiation; Dosimetria termoluminiscente de nuevos fosforos de ZnO expuestos a radiacion beta

Energy Technology Data Exchange (ETDEWEB)

Cruz V, C.; Burruel I, S.E.; Grijalva M, H. [UNISON, A.P. 130, Hermosillo, Sonora (Mexico); Barboza F, M.; Bernal, R. [CIF, UNISON, A.P. 5-088, Hermosillo, Sonora (Mexico)

2004-07-01

In this work, we report the thermoluminescence dosimetry of a new Zn O phosphor obtained by annealing of Zn S powder precipitated when Zn S films were grown by employing a CBD method. The collected Zn S powder was pressed in a die to form pellets which were subjected to different thermal treatments under air atmosphere. X-ray diffraction (XRD) patterns and energy-dispersive X-ray Spectrometry (EDS) analyses confirmed the transformation of Zn S to Zn O. The phosphors thus obtained were exposed to high doses of beta radiation and their thermoluminescent dosimetry show that these new phosphors are materials suitable to be used in high dose thermoluminescence dosimetry. (Author)

Crystal scintillators for use in check-light source for thermoluminescent systems

Science.gov (United States)

Nagpal, J. S.; Sabharwal, S. C.; Chougaonkar, M. P.; Godbole, S. V.

1999-08-01

Beta ( 63Ni, Emax 0.063 MeV) excited radioluminescence of indigenously grown crystal scintillators CsI(Tl), Bi 4Ge 3O 12 and CdWO 4 has been studied for its use in check-light source needed for thermoluminescence systems. Temperature coefficient of the light output over 298-323 K and the beta-induced TL of the scintillators over 298-553 K are reported.

Re-use of radio-thermoluminescent LiF without regeneration; Reemploi sans regeneration du LiF radiothermoluminescent

Energy Technology Data Exchange (ETDEWEB)

Portal, G; Francois, H; Blanchard, Ph [Commissariat a l' Energie Atomique, Fontenay-aux-Roses (France). Centre d' Etudes Nucleaires

1969-07-01

There is at the present time a rapid development of dosimetry techniques using thermoluminescence. Amongst the many substance actually in use, research laboratories generally employ lithium fluoride which is of particular interest for dosing {beta} radiation and low-energy X and {gamma} radiation. It might also be of use in radioprotection if its practical application were simpler. It has in effect unstable traps situated just below the surface which adversely affect the measurements if the material is not regenerated before each operation; this process considerably complicates the carrying out of measurements in the field of radioprotection. We have prepared a lithium fluoride giving unstable peaks which are less pronounced that those of the commercially available product and which can therefore be used without regeneration. In this report we compare the thermoluminescence curves for these two products. An analysis is given of the reasons for which this radio-thermoluminescent product has a stable luminescence curve and can be used almost one hundred times without being regenerated. We show that this quality can be retained when the LiF is used as a filler for teflon for applications in detectors. (authors) [French] On assiste a un developpement rapide des techniques de dosimetrie par thermoluminescence. Parmi les nombreux materiaux actuellement utilises, les laboratoires de recherche font generalement porter leur preference sur le fluorure de lithium qui est particulierement interessant pour la dosimetrie des rayonnements {beta} et des rayonnements X et {gamma} de faible energie. Ses qualites seraient egalement appreciees en radioprotection si sa mise en oeuvre etait plus simple. Il presente en effet des pieges instables situes a une faible profondeur qui alterent les mesures si l'on ne procede pas, avant chaque utilisation, a la regeneration du materiau, operation qui alourdit considerablement les mesures pratiquees en radioprotection. Nous avons prepare un

Thermoluminescence analysis for detection of irradiated food - luminescence characteristics of minerals for different types of radiation and radiation doses

International Nuclear Information System (INIS)

Soika, C.; Delincée, H.

2000-01-01

Federal Research Centre for Nutrition, Institute of Nutritional Physiology, Haid-und-Neu-Straße 9, 76131 Karlsruhe (Germany) Thermoluminescence analysis is used to detect radiation processing of foods which are contaminated with sand or dust. Silicate minerals are isolated, their radiation-induced luminescence is measured and compared to the thermoluminescence from a second measurement after exposure to a dexned radiation dose (normalization). In the present study, the mineral mixture *sand+ and its main components feldspar and quartz were investigated for their thermoluminescence behaviour using different types of radiation, in order to determine adequate radiation sources for the purpose of normalization. The material was irradiated with types of ionizing radiation commonly used for commercial food irradiation, i.e. accelerated electrons with beam energies of 5 MeV as well as 10 MeV, and 60 Co--rays. After thermoluminescence measurements, samples were re-irradiated using either accelerated electrons with beam energies of 2 MeV, 5 MeV or 10 MeV, or 60 Co--rays, 90 Sr--rays or ultraviolet rays (200}280 nm). Evaluation of the xrst and corresponding second glow curve revealed that their shapes depend on the type of minerals in the mixture. The second radiation treatment (normalization) is satisfactory when accelerated electrons (2, 5 and 10 MeV) as well as 60 Co--rays and 90 Sr--rays are employed. Normalization with ultraviolet rays, however, has only a limited range of use

Characterization of the personal thermoluminescent dosemeter of LiF: Mg, Ti + Ptfe

International Nuclear Information System (INIS)

Azorin N, J.; Gutierrez C, A.; Gonzalez M, P.

1991-01-01

The objective of this work is to characterize the thermoluminescent dosemeters taken place in the laboratory in form of pellets of LiF: Mg, Ti + Ptfe like personal dosemeters, subjecting them to the operation tests proposed by the international standards and comparing them with the TLD-100, the Tl dosemeter more used at the moment for personal dosimetry

Thermoluminescence property of nano scale Al{sub 2}O{sub 3}: C by combustion method

Energy Technology Data Exchange (ETDEWEB)

Bharthasaradhi, R.; Nehru, L. C. [Department of Medical Physics, School of Physics, Bharathidasan University, Tiruchirappalli-620 024, Tamilnadu (India)

2016-05-23

In this study, thermoluminescence dosimetry material of carbon doped aluminium oxide by combustion method using Aluminium nitrate and Glycine. The Structure of the prepared Sample was carried out by XRD. The sample was nano crystalline in nature. Having hexagonal structure with unit cell parameters a=4.75Å, C=12.99Å. The surface morphology of the prepared nanopowder was carried out through (SEM). The morphology of the prepared sample is platelet structure and functional group analysis carried out through FT-IR Spectrum. The prepared sample was irradiated through γ-ray CO{sup 60} (100 Gy) was used as γ-ray source. The thermoluminescence glow curve of the irradiated sample showed an isolated peak at around 200°C. The result suggest the prepared nanopowder is suitable for medical radiation dosimetry.

Thermoluminescence spectra of natural CaF2 irradiated by 10MeV electrons

International Nuclear Information System (INIS)

Manrique, J.; Angulo, S.; Pardo, M.P.; Gastesi, R.; De la Cruz, A.; Perez, A.

2006-01-01

The spectra of thermoluminescence from natural and electron-irradiated fluorite in the 350-800nm spectral range were studied between room temperature and 500 o C. The sample came from Asturias (Spain) and was analyzed by X-ray diffractometry and inductively coupled plasma-mass spectrometry. Glow peaks appeared at 115, 205 and 310 o C. Main emissions occurred at 475, 575, 650 and 745nm, attributed to the Dy +3 ion and, at 410nm, from electron-hole recombination. The fractional glow technique and the general order model were employed to study the emission at 575nm in detail. The results showed that the 115 and 205 o C glow peaks originate at traps with activation energies of 1.6 and 1.9eV, respectively, on the kinetic order of 1.5 and 1.3 and frequency factors of 1.7x10 19 and 2.7x10 19 s -1 , respectively. Spectrally resolved fading produced by storage was observed, and we concluded that the emission was due to large defect complexes. The dosimetric study showed that there was saturation at doses higher than 2kGy

Study of the thermoluminescent properties of lava from different origins

International Nuclear Information System (INIS)

Molina, D.; Correcher, V.; Delgado, A.; Garcia G, J.

2002-01-01

In this work has been studied the thermoluminescent signal (Tl) of lava from different geographical area (Costa Rica, the Canary Islands, Hawaii, Iceland and Italy) and originating in distinct eruptions, for its possible use such as in the dating field (geological and archaeological) as in retrospective dosimetry. Due that the light emission is intimately related with the punctual defects existent in the structure of material associated to the presence of different mineral phases, it was realized a study by X-ray diffraction for determining the main components of the lava observing the presence, in distinct proportions of cristobalite, plagioclases (chalcosodic feldspars) and philosilicates (augite, montmorillonite, forsterite and actinolite). All the detected mineral components present Tl emission in the blue region. Each one of the lava were artificially irradiated for proving the dependence of the luminescent signal with the dose in the range 1 to 25 Gy, observing a linear response with the dose in all the cases and not appreciating saturation in the Tl emission. Such the appropriate signal of natural samples (TLN) as the irradiated samples in the laboratory (TLI) show a complex structure associated with a continuous distribution of traps at temperature higher than 100 C which could be explained as consequence of the dynamic formation-annihilation of centers [AlO 4 /alkali] + and [AlO 4 ] 0 . In TLI was observed that a nearer to 85 C appeared a maximum whose structure correspond a discrete distribution of traps, coexisting therefore the two types of traps structure. (Author)

Technical recommendations for the use of thermoluminescence for dosimetry in individual monitoring for photons and electrons from external sources

International Nuclear Information System (INIS)

1975-01-01

The principles of thermoluminescence dosimetry and the role it may play in the field of personnel dosimetry are presented. Technical recommendations are made as an indication of what is generally regarded as good practice and they are intended to be of assistance in avoiding the common sources of error. Errors due to: the detector; the evaluation procedure; the thermal treatment; at the sensitivity of the detector to neutrons. The recommendations are concerned with: the choice of detector material; design of thermoluminescent dosemeters; read-out procedure; reader; handling procedures; dose evaluations; automation; documentation and data handling

On the set up of a thermoluminescent dosimetric system

International Nuclear Information System (INIS)

Furetta, C.

2000-01-01

In this work are treated the following features: Introduction to the thermoluminescent dosimetric systems, their prerequisites, Initialisation procedure, Batch homogeneity, Procedure for batch homogeneity (IEC), Reference and field dosimeters, Thermal treatments and its general considerations, as well as its initialisation treatment, erasing treatment or standard annealing (also called pre-irradiation annealing), post-irradiation or pre-readout annealing. Also is presented the performance of the annealing study, with its suggested procedures such as: a first and second procedures. Finally, it is showed about experimental data of the annealing treatments and its diagrams. (Author)

Use of thermoluminescent dosimetry in gamma radiation fields studies

International Nuclear Information System (INIS)

Carron, W.

1987-01-01

The depth-dose curves for gamma rays in material of interest to agronomy were obtained using lithium fluoride thermoluminescent dosimeters. The dose conversion factors for LiF were determined from curves of the absorved dose versus depth in water, wood and soil. Mathematics equations were chosen to best fit these curves. In the view of the results we came to the conclusion that in the studied materials the absorved radiation dose presents a great variation to the depth and could be correlated through of the exponential regression. (author)

Thermoluminescent determination of prehistoric heat treatment of chert artifacts

International Nuclear Information System (INIS)

Melcher, C.L.; Zimmerman, D.W.

1977-01-01

In recent years archeologists have become interested in the extent to which prehistoric peoples heat-treated chert prior to shaping it into tools. Thermoluminescent determination of the radiation dose accumulated by an artifact since it was formed or last heated provides a simple, reliable test for such heat treatment. This test can be applied to single artifacts without the need for raw source material for comparison. Results on 25 artifacts from four sites indicate that, for many chert sources, color and luster are not useful indicators of heat treatment by prehistoric peoples

Thermoluminescence in KBr:D electron irradiated at room temperature

International Nuclear Information System (INIS)

Paredes Campoy, J.C.; Lopez Carranza, E.

1991-07-01

The thermoluminescence of KBr:D samples electron irradiated at room temperature after thermal annealing at 673 K for 1 hour have been studied in the temperature range 360-730 K. The experimental TL-curve was discomposed by computer analysis in seven overlapping TL peaks, giving for them the order of the kinetics of thermal stimulation, the activation energy, the frequency factor, the relative values of the electronic concentration in traps at the initial heating temperature and the temperature at the maximum of the peak. (author). 18 refs, 1 fig., 3 tabs

How AMS dating changed my life

International Nuclear Information System (INIS)

Spriggs, M.

2001-01-01

Accelerator mass spectrometry (AMS) radiocarbon dating was developed in the late 1970s. Remembering back to a time before AMS dating was available to archaeologists is a bit like trying to remember how we ever survived without desktop computers, email or automatic teller machines. My own particular interest in AMS dating was an inevitable offshoot from my long-established interest in chronometric hygiene, or 'getting the dates right'. In this paper I attempt to illustrate that accurate dating matters, by discussing some examples of AMS dating projects with which I have been involved over the last six years or so. In relation to these projects, AMS has given us the ability to date sites which we could not before. It has enabled us to provide more detailed stratigraphies when datable materials are rare. It has allowed us to date materials we could not date before, such as rock art pigments. It has been able to provide indications of the degree of site disturbance in the absence of other obvious forms of evidence. And it has allowed us to assess claims for the antiquity of particular material cultural types and faunal introductions. (author). 41 refs

Development of BASIC program for radiocarbon dating

International Nuclear Information System (INIS)

Omoto, Kunio

1982-01-01

The continuous improvement of the system and the needs have produced the successful radiocarbon dating system of today to detect very low energy β-radioactivity. However, it still takes longer than 1,000 minutes for a sample counting. In a gas counting system, it is very difficult to keep the drift of impressed high voltage for a proportional counter less than 5 volts throughout the counting time. The temperature and the characteristics of gas itself also change during experiment. The accumulation of the above drift and errors are closely concerned with the accuracy and reliability of the radiocarbon date. The detection and reduction of the errors are only possible by using a ''fully automatic radiocarbon dating system'' linked to a personal computer system. In this paper, the author presents the BASIC (Beginners All-purpose Symbolic Instruction Code) program for a fully automatic radiocarbon dating system. In this paper, the outline of the system and software development are described. The details of the program include the description for gas-collection, gas-enclosing, plateau counting, β-ray counting, age calculation and data file maintenance. The author wrote numerous remark statements into the program so that it can be understood by users without detailed knowledge of the operation of a personal computer system or of the radiocarbon dating. Using this system, the author found that the radiocarbon dating has greatly progressed in speed and labour-saving, and that the accuracy and reliability of the date itself has also improved much than former manual systems. (Wakatsuki, Y.)

Thermal neutron detection by activation of CaSO4:Dy + KBr thermoluminescent phosphors

International Nuclear Information System (INIS)

Gordon, A.M.P.L.; Muccillo, R.

1979-01-01

Thermoluminescence (TL) studies to detect thermal neutrons were performed in cold-pressed CaSO 4 :0,1%Dy + KBr samples. The detection is based on the self-irradiation of the CaSO 4 :Dy TL phosphor by the Br isotopes activated by exposure to a mixed neutron-gamma field. (Author) [pt

The thermoluminescence and optically stimulated luminescence properties of Cr-doped alpha alumina transparent ceramics

International Nuclear Information System (INIS)

Liu, Qiang; Yang, Qiu Hong; Zhao, Guang Gen; Lu, Shen Zhou; Zhang, Hao Jia

2013-01-01

Highlights: •Polycrystalline Cr:α-Al 2 O 3 transparent ceramics were obtained with vacuum sintering method. •The influence of different concentration of Cr 2 O 3 on the thermoluminescence and optical stimulated luminescence properties of Cr:α-Al 2 O 3 transparent ceramics was studied. •It had a main peak at 503 K of very high intensity and linear concentration dependence up to high concentration. •It showed so interesting results with high TL sensitivity and high stability of OSL signal that Cr:α-Al 2 O 3 transparent ceramics might be a promising material in TL dosimetry and replace Cr:α-Al 2 O 3 crystals. -- Abstract: Polycrystalline Cr:α-Al 2 O 3 transparent ceramics were fabricated by conventional solid-state processing under vacuum condition. The SEM microstructure photographs of Cr:α-Al 2 O 3 transparent ceramics doped with different content of Cr 2 O 3 were investigated. The absorption, emission spectra, thermoluminescence and optical stimulated luminescence of Cr:α-Al 2 O 3 transparent ceramics were comparable to those of Cr:α-Al 2 O 3 crystals. The influence of different concentration of Cr 2 O 3 on the thermoluminescence and optical stimulated luminescence properties of Cr:α-Al 2 O 3 transparent ceramics was discussed. It showed so interesting results with high TL sensitivity and high stability of OSL signal that Cr:α-Al 2 O 3 transparent ceramics might be a promising material in TL dosimetry and replace Cr:α-Al 2 O 3 crystals

Thermoluminescence properties of zinc oxide obtained by solution combustion synthesis

Energy Technology Data Exchange (ETDEWEB)

Orante B, V. R.; Escobar O, F. M.; Cruz V, C. [Universidad de Sonora, Departamento de Investigacion en Polimeros y Materiales, Apdo. Postal 130, 83000 Hermosillo, Sonora (Mexico); Bernal, R., E-mail: victor.orante@polimeros.uson.mx [Universidad de Sonora, Departamento de Investigacion en Fisica, Apdo. Postal 5-088, 83190 Hermosillo, Sonora (Mexico)

2014-08-15

High-dose thermoluminescence dosimetry properties of novel zinc oxide obtained by solution combustion synthesis in a glycine-nitrate process, with a non-stoichiometric value of the elemental stoichiometric coefficient (Φ{sub c}) are presented in this work. Zn O powder samples obtained were annealed afterwards at 900 grades C during 2 h in air. Sintered particles of sizes between ∼ 0.5 and ∼ 2 μm were obtained, according to scanning electron microscopy results. X-ray diffraction indicates the presence of the hexagonal phase of Zn O for the powder samples obtained, before and after thermal annealing, without any remaining nitrate peaks observed. Thermoluminescence glow curves of Zn O obtained after being exposed to beta radiation consists of two maxima; one located at ∼ 149 grades C and another at ∼ 308 grades C, being the latter the dosimetric component of the curve. Dosimetric characterization of non-stoichiometric zinc oxide provided experimental evidence like asymptotic behavior of the Tl signal fading for times greater than 16 h between irradiation and the corresponding Tl readout, as well as the linear behaviour of the dose response without saturation in the dose interval studied (from 12.5 up to 400 Gy). Such characteristics place Zn O phosphors obtained in this work as a promising material for high-dose radiation dosimetry applications (e.g., radiotherapy and food industry). (author)

Effect of thermal decomposition of hydroxyapatite on the thermoluminescent response

International Nuclear Information System (INIS)

Sandoval C, K. J.; Zarate M, J.; Lemus R, J.; Rivera M, T.

2014-08-01

In this work, a study on the thermoluminescence (Tl) induced by gamma radiation in synthetic hydroxyapatite (Hap) annealed at different temperatures obtained by the precipitation method is presented. Synthesis of hydroxyapatite Hap was carried out starting from inorganic precursors [Ca(NO 3 ) 2 ·4H 2 O and (NH 4 ) 2 HPO 4 ]. The precipitate was filtered, washed, dried and then the powder was calcined at different temperatures until the Hap decomposition. The structural and morphological characterization was carried out using both X-ray diffraction (XRD) and scanning electron microscopy (Sem) techniques. Thermoluminescent (Tl) properties of Hap powders were irradiated at different gamma radiation doses. According to X ray diffraction patterns, the tricalcium diphosphate phase (Tcp) appear when the Hap was calcined at 900 grades C. Tl glow curve showed two peaks located at around 200 and 300 grades C, respectively. Tl response as a function of gamma radiation dose was in a wide range from 25 to 100 Gy. The fading of the Tl response at 134 days after irradiation was measured. Experimental results showed that the synthetic hydroxyapatite obtained by precipitation technique may have dosimetric applications when is annealed at temperature of 900 grades C, where the Tcp phase appears and contributes to Tl response, which opens the possibility of using this biomaterials in the area of dosimetry, as they are generally used for biomedical implants. (author)

A preliminary approach to identify irradiated foods by thermoluminescence measurements

International Nuclear Information System (INIS)

Shin, Choonshik; Kim, Hyoung-Ook; Lim, Yoongho

2012-01-01

Thermoluminescence (TL) is one of the physical methods for the identification of irradiated foods. Among the currently developed methods, TL is the most widely used method for the identification of irradiated foods. However, in order to use this method, silicate minerals should be isolated from food samples. The process for the isolation of silicate minerals is time consuming and laborious. In this work, we have investigated the applicability of the TL method using iron-containing minerals instead of silicate minerals. In the TL analyses of dried spices, TL glow curves of iron-containing minerals showed maximum temperatures between 150 and 250 °C which were the same as those of silicate minerals. The process for the mineral separation of the proposed method is simple, fast, easy, and reliable. Moreover, the analysis results including TL ratio have not shown significant differences compared with the silicate minerals method. As a result, the TL measurements using the iron-containing minerals could be an excellent method for the identification of the irradiated foods, including dried spices. - Highlights: ► A thermoluminescence method using iron-containing minerals is proposed. ► Current method using silicate minerals is time consuming and laborious. ► However, the proposed method is simple, fast, easy, and reliable. ► Analysis results are similar to those of the silicate minerals method.

Thermoluminescence properties of zinc oxide obtained by solution combustion synthesis

International Nuclear Information System (INIS)

Orante B, V. R.; Escobar O, F. M.; Cruz V, C.; Bernal, R.

2014-08-01

High-dose thermoluminescence dosimetry properties of novel zinc oxide obtained by solution combustion synthesis in a glycine-nitrate process, with a non-stoichiometric value of the elemental stoichiometric coefficient (Φ c ) are presented in this work. Zn O powder samples obtained were annealed afterwards at 900 grades C during 2 h in air. Sintered particles of sizes between ∼ 0.5 and ∼ 2 μm were obtained, according to scanning electron microscopy results. X-ray diffraction indicates the presence of the hexagonal phase of Zn O for the powder samples obtained, before and after thermal annealing, without any remaining nitrate peaks observed. Thermoluminescence glow curves of Zn O obtained after being exposed to beta radiation consists of two maxima; one located at ∼ 149 grades C and another at ∼ 308 grades C, being the latter the dosimetric component of the curve. Dosimetric characterization of non-stoichiometric zinc oxide provided experimental evidence like asymptotic behavior of the Tl signal fading for times greater than 16 h between irradiation and the corresponding Tl readout, as well as the linear behaviour of the dose response without saturation in the dose interval studied (from 12.5 up to 400 Gy). Such characteristics place Zn O phosphors obtained in this work as a promising material for high-dose radiation dosimetry applications (e.g., radiotherapy and food industry). (author)

Environmental radiation measurements using lithium fluoride thermoluminescence dosemeters

Energy Technology Data Exchange (ETDEWEB)

Driscoll, C.M.H.; Green, B.M.R.; McKinlay, A.F.; Richards, D.J. (National Radiological Protection Board, Harwell (UK))

1984-01-01

The National Radiological Protection Board is involved in a large scale environmental survey of radiation levels in homes throughout the United Kingdom. Passive radon and gamma ray dosemeters are posted to a representative sample of households. Lithium fluoride thermoluminescence dosemeters are used to assess natural gamma radiation and are left in the measurement location for a period of six months before being returned to the Board for processing. As a preliminary to the national survey, the Board has been engaged on several limited surveys in regions of igneous and sedimentary geology. Experience gained in these limited surveys and from standardisation studies using environmental dosemeters are reported.

Thermoluminescent characteristics of ZrO2:Nd films

International Nuclear Information System (INIS)

Vera B, G.; Rivera M, T.; Azorin N, J.; Falcony G, C.; Garcia H, M.; Martinez S, E.

2002-01-01

In this work it is exposed the obtained results after analysing the photo luminescent and thermoluminescent characteristics of activated zirconium oxide with neodymium (ZrO 2 :Nd) and its possible application in the UV radiation dosimetry. The realized experiments had as objective to study the characteristics such as the optimum thermal erased treatment, the influence of light on the response, the response depending on the wavelength, the fadeout of the information, the temperature effect, the response depending on the time and the recurring of the response. The results show that the ZrO 2 :Nd is a promising material to be used as Tl dosemeter for the UV radiation. (Author)

PTFE Additive and Re-annealing Effect on Thermoluminescence Response of CaSO4:Dy Derived from Co-precipitation Method

Science.gov (United States)

Nuraeni, Nunung; Dwi Septianto, Ricky; Iskandar, Ferry; Haryanto, Freddy; Waris, Abdul; Hiswara, Eri

2017-07-01

Effect of re-annealing treatment in thermoluminescence response of thermoluminescent dosimeter (TLD) CaSO4:Dy and CaSO4:Dy with PTFE (Polytetrafluoroethylene) addition was investigated. CaSO4:Dy was prepared by a co-precipitation method. The PTFE was added before re-annealing treatment which the mass ratio of CaSO4:Dy and PTFE was fixed to 2:3. The re-annealing treatments of the samples were done at temperature 700 °C for 1 hr. The obtained samples were characterized using a Fourier-transform infrared (FTIR) and X-ray diffraction (XRD) to observe the molecule bonding in sample and crystal properties, respectively. From the experimental results, it was observed that the thermoluminescence intensity of CaSO4:Dy, CaSO4:Dy re-annealed at 700 °C, and CaSO4:Dy + PTFE re-annealed at 700 °C are 57.03, 75.15, and 1191.11 nC, respectively. The intensity of 700 °C-re-annealed CaSO4:Dy increased significantly after PTFE addition.

Suitability of the thermoluminescence method for detection of irradiated foods

International Nuclear Information System (INIS)

Pinnioja, S.

1993-01-01

Irradiated foods can be detected by thermoluminescence (TL) of contaminating minerals. Altogether about 300 lots of herbs, spices, berries, mushrooms and seafood were studied by the TL method. Irradiated herbs and spices were easily differentiated from unirradiated ones two years after irradiation of a 10 kGy dose. The mineral composition of seafood was variable; and while calcite was suitable for the TL analysis, aragonite and smectite gave unreliable results. Control analyses during two years confirmed the reliability of TL method. (author)

A computerized glow curve analysis (GCA) method for WinREMS thermoluminescent dosimeter data using MATLAB

International Nuclear Information System (INIS)

Harvey, John A.; Rodrigues, Miesher L.; Kearfott, Kimberlee J.

2011-01-01

A computerized glow curve analysis (GCA) program for handling of thermoluminescence data originating from WinREMS is presented. The MATLAB program fits the glow peaks using the first-order kinetics model. Tested materials are LiF:Mg,Ti, CaF 2 :Dy, CaF 2 :Tm, CaF 2 :Mn, LiF:Mg,Cu,P, and CaSO 4 :Dy, with most having an average figure of merit (FOM) of 1.3% or less, with CaSO 4 :Dy 2.2% or less. Output is a list of fit parameters, peak areas, and graphs for each fit, evaluating each glow curve in 1.5 s or less. - Highlights: → Robust algorithm for performing thermoluminescent dosimeter glow curve analysis. → Written in MATLAB so readily implemented on variety of computers. → Usage of figure of merit demonstrated for six different materials.

Improved processes in therapy dosimetry with solid LiF thermoluminescent detectors

International Nuclear Information System (INIS)

Toivonen, M.

1991-08-01

The thesis presents criteria for thermoluminescence dosimetry systems suitable for precision measurements and, moreover, a detailed examination of the sources of systematic and random error. Instructions are given for annealing processes, calibration procedures, quality control, and operational rules, which are necessary in modem TLD. The performances of some principally different systems are compared. The old LiF-powder-based TLD system, with an overall uncertainty of measurement of about 1.6 percent for ten repeated readouts and for irradiations under calibration conditions with Co-60, is still the best but a comparable, although slightly lower, accuracy of about 1.7 percent can be reached more conveniently with solid LiF detectors. In measurements where absolute system calibration is not of interest (i.e., in depth-dose curve measurements, etc.), the advantages of the simple powder-based system are even more concrete. An integrated TLD process is presented for progressive utilization of automation in precision measurements. The sources of random error and unknown systematic error in current readout instruments are examined. Mechanical tolerances in critical parts of the readout instruments are thought to be the reason why the method of heating with hot gas has not been superior with respect to the precision of measurements, in spite of the excellent repeatability of the glow curve shape observed for successive readouts

Assessing the potential for using biogenic calcites as dosemeters for luminescence dating

International Nuclear Information System (INIS)

Duller, G.A.T.; Penkman, K.E.H.; Wintle, A.G.

2009-01-01

Calcium carbonate emits an intense thermoluminescence (TL) signal and previous work has explored the potential of using this signal to date both inorganic carbonates such as limestones and stalagmites and biogenic calcite produced by marine organisms. Luminescence analysis of biogenic calcites directly dates the secretion of the mineral by the organism and is therefore not reliant upon exposure of the sample to daylight. A method is outlined for using the TL signals from slug plates, from the Limacidae family, and opercula from the snail Bithynia tentaculata to construct a single-aliquot regenerative-dose growth curve. Analysis of slug plates from a number of Quaternary sites show that the equivalent dose (D e ) of a late Holocene sample is close to zero and that the D e increases with age over the last 500 ka. The TL signal from snail opercula is shown to increase up to doses over 4000 Gy. Replicate measurements from 16 opercula from a site ∼220 ka show a broad distribution. Potential causes of this scatter are discussed along with recommendations about how it could be reduced. The major challenge which remains to be solved before slug plates or snail opercula could be used to calculate ages is to develop methods for calculating the dose rate received during burial.

Thermal annealing of high dose radiation induced damage at room temperature in alkaline. Stored energy, thermoluminescence and coloration

International Nuclear Information System (INIS)

Delgado, L.

1980-01-01

The possible relation between stored energy, thermoluminescence and colour centre annealing in gamma and electron irradiated alkali halides is studied. Thermoluminescence occurs at temperature higher than the temperature at which the main stored energy peak appears. No stored energy release is detected in additively coloured KC1 samples. Plastic deformation and doping with Ca and Sr induce a stored energy spectrum different from the spectrum observed in pure and as cleaved samples, but the amount of stored energy does not change for a given irradiation dose.Capacity of alkali halides to store energy by irradiation increases as the cation size decreases. (Author) 51 refs

Detailed Safety Review of Anthrax Vaccine Adsorbed

National Research Council Canada - National Science Library

2001-01-01

To date, 18 human studies have assessed the safety of anthrax vaccination. These studies, some stretching back almost 50 years, reported adverse events after vaccination in varying degrees of detail...