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Sample records for delamination growth behavior

  1. Delamination growth behavior in cross-ply composites under compressive cyclic (fatigue) loading

    Science.gov (United States)

    Pelegri, Assimina A.

    A mode dependent fatigue delamination growth law for anisotropic composite plates is presented in this thesis. The novelty of the presented law lies in the mode dependency of the material and laminate constants m(Psi) and C(Psi). The model describing the mode dependent delamination growth law consists of an initial postbuckling solution accounting for general delaminated composites, i.e. with no restrictive assumptions on the delamination dimensions, and a fracture mechanics solution. A numerical code was developed for the implementation of the closed form solution which gives the loading and geometrical quantities as well as the energy release rates and the mode mixities. The computer code was especially designed for parametric studies. Parameters assigned in this particular investigation were: end conditions, delamination position (h/T), and applied strain. The effect of the end conditions, i.e. clamped-clamped versus simply-supported ends on the initial postbuckling and growth behavior of delaminated plates was also investigated. In conjunction with the previous analysis, a detailed experimental study was designed and carried out in order to validate the proposed model. The tests were designed so that the effect of certain parameters on the delamination growth behavior could be evaluated. The parameters included in the investigation were: initial delamination length, applied strain and delamination position (h/T). Compressive static, compressive fatigue (constant displacement amplitude), and double cantilever beam (DCB) tests were conducted. Data acquisition and analysis for these tests were performed. By comparing analytical and experimental results it is shown that a very good correlation exists, and the presented mode dependent fatigue delamination growth law can accurately predict fatigue lives of delaminated composite structures.

  2. The concept of fatigue fracture toughness in fatigue delamination growth behavior

    NARCIS (Netherlands)

    Yao, L.; Alderliesten, R.C.; Benedictus, R.

    2015-01-01

    This paper provides a study on mode I fatigue delamination growth in composite laminates using energy principles. Experimental data has been obtained from fatigue tests conducted on Double Cantilever Beam (DCB) specimens at various stress ratios. A concept of fatigue fracture toughness is proposed t

  3. Buckling and Delamination Growth Analysis of Composite Laminates Containing Embedded Delaminations

    Science.gov (United States)

    Hosseini-Toudeshky, H.; Hosseini, S.; Mohammadi, B.

    2010-04-01

    The objective of this work is to study the post buckling behavior of composite laminates, containing embedded delamination, under uniaxial compression loading. For this purpose, delamination initiation and propagation is modeled using the softening behavior of interface elements. The full layer-wise plate theory is also employed for approximating the displacement field of laminates and the interface elements are considered as a numerical layer between any two adjacent layers which delamination is expected to propagate. A finite element program was developed and the geometric non-linearity in the von karman sense is incorporated to the strain/displacement relations, to obtain the buckling behavior. It will be shown that, the buckling load, delamination growth process and buckling mode of the composite plates depends on the size of delamination and stacking sequence of the laminates.

  4. NUMERICAL ANALYSIS OF DELAMINATION GROWTH FOR STIFFENED COMPOSITE LAMINATED PLATES

    Institute of Scientific and Technical Information of China (English)

    白瑞祥; 陈浩然

    2004-01-01

    A study of postbuckling and delamination propagation behavior in delaminated stiffened composite plates was presented. A methodology was proposed for simulating the multi-failure responses, such as initial and postbuckling, delamination onset and propagation, etc. A finite element analysis was conducted on the basis of the Mindlin first order shear effect theory and the von-Krmn nonlinear deformation assumption. The total energy release rate used as the criteria of delamination growth was estimated with virtual crack closure technique (VCCT). A self-adaptive grid moving technology was adopted to model the delamination growth process. Moreover, the contact effect along delamination front was also considered during the numerical simulation process. By some numerical examples, the influence of distribution and location of stiffener, configuration and size of the delamination, boundary condition and contact effect upon the delamination growth behavior of the stiffened composite plates were investigated. The method and numerical conclusion provided should be of great value to engineers dealing with composite structures.

  5. Compressive behavior of composite panels with deeply embedded delamination%Compressive behavior of composite panels with deeply embedded delamination

    Institute of Scientific and Technical Information of China (English)

    FU Hui-min; PENG Bo

    2012-01-01

    The compressive behavior of laminates with a deeply embedded circular delamination was studied numerically and experimentally.In the finite element analysis(FEA),virtual crack closure technique(VCCT) and B-K law were employed to simulate the delamination growth,and the contact of the two substrates was considered.The effect of the delamination size and through-thickness position on the compressive behavior of laminates with an artificially embedded circular delamination was discussed.It is found that the through-thickness position affects the buckling mode,which then strongly influences delamination growth speed and direction,as well as the dominant component energy release rate(ERR).The numerical results agreed well with the experimental results.

  6. Characterization of delamination onset and growth in a composite laminate

    Science.gov (United States)

    Obrien, T. K.

    1981-01-01

    The onset and growth of delaminations in unnotched (+ or - 30/+ or - 30/90/90 bar) sub S graphite epoxy laminates is described quantitatively. These laminates, designed to delaminate at the edges under tensile loads, were tested and analyzed. Delamination growth and stiffness loss were monitored nondestructively. Laminate stiffness decreased linearly with delamination size. The strain energy release rate, G, associated with delamination growth, was calculated from two analyses. A critical G for delamination onset was determined, and then was used to predict the onset of delaminations in (+45 sub n/-45 sub n/o sub n/90 sub n) sub s (n=1,2,3) laminates. A delamination resistance curve (R curve) was developed to characterize the observed stable delamination growth under quasi static loading. A power law correlation between G and delamination growth rates in fatigue was established.

  7. Development of a Benchmark Example for Delamination Fatigue Growth Prediction

    Science.gov (United States)

    Krueger, Ronald

    2010-01-01

    The development of a benchmark example for cyclic delamination growth prediction is presented and demonstrated for a commercial code. The example is based on a finite element model of a Double Cantilever Beam (DCB) specimen, which is independent of the analysis software used and allows the assessment of the delamination growth prediction capabilities in commercial finite element codes. First, the benchmark result was created for the specimen. Second, starting from an initially straight front, the delamination was allowed to grow under cyclic loading in a finite element model of a commercial code. The number of cycles to delamination onset and the number of cycles during stable delamination growth for each growth increment were obtained from the analysis. In general, good agreement between the results obtained from the growth analysis and the benchmark results could be achieved by selecting the appropriate input parameters. Overall, the results are encouraging but further assessment for mixed-mode delamination is required.

  8. On the Through-the-Width Multiple Delamination, and Buckling and Postbuckling Behaviors of Symmetric and Unsymmetric Composite Laminates

    Science.gov (United States)

    Liu, P. F.; Zheng, J. Y.

    2013-12-01

    Multiple delamination causes severe degradation of the stiffness and strength of composites. Interactions between multiple delamination, and buckling and postbuckling under compressive loads add the complexity of mechanical properties of composites. In this paper, the buckling, postbuckling and through-the-width multiple delamination of symmetric and unsymmetric composite laminates are studied using 3D FEA, and the virtual crack closure technique with two delamination failure criteria: B-K law and power law is used to predict the delamination growth and to calculate the mixed-mode energy release rate. The compressive load-strain curves, load-central deflection curves and multiple delamination process for eight composite specimens with different initial delamination sizes and their distributions as well as two angle-ply configurations 04//(± θ)6//04 ( θ = 0° and 45°, and "//" denotes the delaminated interface) are comparatively studied. From numerical results, the unsymmetry decreases the local buckling load and initial delamination load, but does not affect the global buckling load compared with the symmetric laminates. Besides, the unsymmetry affects the unstable delamination and buckling behaviors of composite laminates largely when the initial multiple delamination sizes are relatively small.

  9. Cyclic delamination behavior of plasma-sprayed hydroxyapatite coating on Ti-6Al-4V substrates in simulated body fluid.

    Science.gov (United States)

    Otsuka, Yuichi; Kawaguchi, Hayato; Mutoh, Yoshiharu

    2016-10-01

    This study aimed to clarify the effect of a simulated body fluid (SBF) on the cyclic delamination behavior of a plasma-sprayed hydroxapatite (HAp) coating. A HAp coating is deposited on the surfaces of surgical metallic materials in order to enhance the bond between human bone and such surfaces. However, the HAp coating is susceptible to delamination by cyclic loading from the patient's gait. Although hip joints are subjected to both positive and negative moments, only the effects of tensile bending stresses on vertical crack propagation behavior have been investigated. Thus, the cyclic delamination behavior of a HAp coating was observed at the stress ratio R=-1 in order to determine the effects of tensile/compressive loading on the delamination behavior. The delamination growth rate increased with SBF immersion, which decreased the delamination life. Raman spectroscopy analysis revealed that the selective phase dissolution in the HAp coating was promoted at interfaces. Finite element analysis revealed that the energy release rate Gmax showed a positive value even in cases with compressive loading, which is a driving force for the delamination of a HAp coating. A prediction model for the delamination growth life was developed that combines a fracture mechanics parameter with the assumed stress-dependent dissolution rate. The predicted delamination life matched the experimental data well in cases of lower stress amplitudes with SBF. Copyright © 2016 Elsevier B.V. All rights reserved.

  10. Characterization of Mode I and Mode II delamination growth and thresholds in AS4/PEEK composites

    Science.gov (United States)

    Martin, Roderick H.; Murri, Gretchen Bostaph

    1990-01-01

    Composite materials often fail by delamination. The onset and growth of delamination in AS4/PEEK, a tough thermoplastic matrix composite, was characterized for mode 1 and mode 2 loadings, using the Double Cantilever Beam (DCB) and the End Notched Flexure (ENF) test specimens. Delamination growth per fatigue cycle, da/dN, was related to strain energy release rate, G, by means of a power law. However, the exponents of these power laws were too large for them to be adequately used as a life prediction tool. A small error in the estimated applied loads could lead to large errors in the delamination growth rates. Hence strain energy release rate thresholds, G sub th, below which no delamination would occur were also measured. Mode 1 and 2 threshold G values for no delamination growth were found by monitoring the number of cycles to delamination onset in the DCB and ENF specimens. The maximum applied G for which no delamination growth had occurred until at least 1,000,000 cycles was considered the threshold strain energy release rate. Comments are given on how testing effects, facial interference or delamination front damage, may invalidate the experimental determination of the constants in the expression.

  11. Characterization of Mode 1 and Mode 2 delamination growth and thresholds in graphite/peek composites

    Science.gov (United States)

    Martin, Roderick H.; Murri, Gretchen B.

    1988-01-01

    Composite materials often fail by delamination. The onset and growth of delamination in AS4/PEEK, a tough thermoplastic matrix composite, was characterized for mode 1 and mode 2 loadings, using the Double Cantilever Beam (DCB) and the End Notched Flexure (ENF) test specimens. Delamination growth per fatigue cycle, da/dN, was related to strain energy release rate, G, by means of a power law. However, the exponents of these power laws were too large for them to be adequately used as a life prediction tool. A small error in the estimated applied loads could lead to large errors in the delamination growth rates. Hence strain energy release rate thresholds, G sub th, below which no delamination would occur were also measured. Mode 1 and 2 threshold G values for no delamination growth were found by monitoring the number of cycles to delamination onset in the DCB and ENF specimens. The maximum applied G for which no delamination growth had occurred until at least 1,000,000 cycles was considered the threshold strain energy release rate. Comments are given on how testing effects, facial interference or delamination front damage, may invalidate the experimental determination of the constants in the expression.

  12. Development and Application of Benchmark Examples for Mode II Static Delamination Propagation and Fatigue Growth Predictions

    Science.gov (United States)

    Krueger, Ronald

    2011-01-01

    The development of benchmark examples for static delamination propagation and cyclic delamination onset and growth prediction is presented and demonstrated for a commercial code. The example is based on a finite element model of an End-Notched Flexure (ENF) specimen. The example is independent of the analysis software used and allows the assessment of the automated delamination propagation, onset and growth prediction capabilities in commercial finite element codes based on the virtual crack closure technique (VCCT). First, static benchmark examples were created for the specimen. Second, based on the static results, benchmark examples for cyclic delamination growth were created. Third, the load-displacement relationship from a propagation analysis and the benchmark results were compared, and good agreement could be achieved by selecting the appropriate input parameters. Fourth, starting from an initially straight front, the delamination was allowed to grow under cyclic loading. The number of cycles to delamination onset and the number of cycles during delamination growth for each growth increment were obtained from the automated analysis and compared to the benchmark examples. Again, good agreement between the results obtained from the growth analysis and the benchmark results could be achieved by selecting the appropriate input parameters. The benchmarking procedure proved valuable by highlighting the issues associated with choosing the input parameters of the particular implementation. Selecting the appropriate input parameters, however, was not straightforward and often required an iterative procedure. Overall the results are encouraging, but further assessment for mixed-mode delamination is required.

  13. Development of Benchmark Examples for Quasi-Static Delamination Propagation and Fatigue Growth Predictions

    Science.gov (United States)

    Krueger, Ronald

    2012-01-01

    The development of benchmark examples for quasi-static delamination propagation and cyclic delamination onset and growth prediction is presented and demonstrated for Abaqus/Standard. The example is based on a finite element model of a Double-Cantilever Beam specimen. The example is independent of the analysis software used and allows the assessment of the automated delamination propagation, onset and growth prediction capabilities in commercial finite element codes based on the virtual crack closure technique (VCCT). First, a quasi-static benchmark example was created for the specimen. Second, based on the static results, benchmark examples for cyclic delamination growth were created. Third, the load-displacement relationship from a propagation analysis and the benchmark results were compared, and good agreement could be achieved by selecting the appropriate input parameters. Fourth, starting from an initially straight front, the delamination was allowed to grow under cyclic loading. The number of cycles to delamination onset and the number of cycles during delamination growth for each growth increment were obtained from the automated analysis and compared to the benchmark examples. Again, good agreement between the results obtained from the growth analysis and the benchmark results could be achieved by selecting the appropriate input parameters. The benchmarking procedure proved valuable by highlighting the issues associated with choosing the input parameters of the particular implementation. Selecting the appropriate input parameters, however, was not straightforward and often required an iterative procedure. Overall the results are encouraging, but further assessment for mixed-mode delamination is required.

  14. Development of Benchmark Examples for Static Delamination Propagation and Fatigue Growth Predictions

    Science.gov (United States)

    Kruger, Ronald

    2011-01-01

    The development of benchmark examples for static delamination propagation and cyclic delamination onset and growth prediction is presented and demonstrated for a commercial code. The example is based on a finite element model of an End-Notched Flexure (ENF) specimen. The example is independent of the analysis software used and allows the assessment of the automated delamination propagation, onset and growth prediction capabilities in commercial finite element codes based on the virtual crack closure technique (VCCT). First, static benchmark examples were created for the specimen. Second, based on the static results, benchmark examples for cyclic delamination growth were created. Third, the load-displacement relationship from a propagation analysis and the benchmark results were compared, and good agreement could be achieved by selecting the appropriate input parameters. Fourth, starting from an initially straight front, the delamination was allowed to grow under cyclic loading. The number of cycles to delamination onset and the number of cycles during stable delamination growth for each growth increment were obtained from the automated analysis and compared to the benchmark examples. Again, good agreement between the results obtained from the growth analysis and the benchmark results could be achieved by selecting the appropriate input parameters. The benchmarking procedure proved valuable by highlighting the issues associated with the input parameters of the particular implementation. Selecting the appropriate input parameters, however, was not straightforward and often required an iterative procedure. Overall, the results are encouraging but further assessment for mixed-mode delamination is required.

  15. Evaluation of Delamination Growth Characterization Methods Under Mode I Fatigue Loading

    Science.gov (United States)

    Murri, Gretchen B.

    2012-01-01

    Reliable delamination characterization data for laminated composites are needed for input to analytical models of structures to predict delamination. The double-cantilevered beam (DCB) specimen is used with laminated composites to measure fracture toughness, G(sub Ic), delamination onset strain energy release rate, and growth rate data under cyclic loading. In the current study, DCB specimens of IM7/8552 graphite/epoxy supplied by two different manufacturers were tested in static and fatigue to compare the measured characterization data from the two sources, and to evaluate a proposed ASTM standard for generating Paris Law equations. Static results were used to generate compliance calibration constants for the fatigue data, and a delamination resistance curve, G(sub IR), which was used to determine the effects of fiber-bridging on delamination growth. Specimens were tested in fatigue at a cyclic G(sub Imax) level equal to 50, 40 or 30% of G(sub Ic), to determine a delamination onset curve and delamination growth rate. The delamination onset curve equations had similar exponents and the same trends. Delamination growth rate was calculated by fitting a Paris Law to the da/dN versus G(sub Imax) data. Both a 2-point and a 7-point data reduction method were used and the Paris Law equations were compared. To determine the effects of fiber-bridging, growth rate results were normalized by the delamination resistance curve for each material and compared to the non-normalized results. Paris Law exponents were found to decrease by 31% to 37% due to normalizing the growth data. Normalizing the data also greatly reduced the amount of scatter between the different specimens. Visual data records from the fatigue testing were used to calculate individual compliance calibration constants from the fatigue data for some of the specimens. The resulting da/dN versus G(sub Imax) plots showed much improved repeatability between specimens. Gretchen

  16. Evaluation of Delamination Onset and Growth Characterization Methods under Mode I Fatigue Loading

    Science.gov (United States)

    Murri, Gretchen B.

    2013-01-01

    Double-cantilevered beam specimens of IM7/8552 graphite/epoxy from two different manufacturers were tested in static and fatigue to compare the material characterization data and to evaluate a proposed ASTM standard for generating Paris Law equations for delamination growth. Static results were used to generate compliance calibration constants for reducing the fatigue data, and a delamination resistance curve, GIR, for each material. Specimens were tested in fatigue at different initial cyclic GImax levels to determine a delamination onset curve and the delamination growth rate. The delamination onset curve equations were similar for the two sources. Delamination growth rate was calculated by plotting da/dN versus GImax on a log-log scale and fitting a Paris Law. Two different data reduction methods were used to calculate da/dN. To determine the effects of fiber-bridging, growth results were normalized by the delamination resistance curves. Paris Law exponents decreased by 31% to 37% after normalizing the data. Visual data records from the fatigue tests were used to calculate individual compliance constants from the fatigue data. The resulting da/dN versus GImax plots showed improved repeatability for each source, compared to using averaged static data. The Paris Law expressions for the two sources showed the closest agreement using the individually fit compliance data.

  17. Development of Benchmark Examples for Delamination Onset and Fatigue Growth Prediction

    Science.gov (United States)

    Krueger, Ronald

    2011-01-01

    An approach for assessing the delamination propagation and growth capabilities in commercial finite element codes was developed and demonstrated for the Virtual Crack Closure Technique (VCCT) implementations in ABAQUS. The Double Cantilever Beam (DCB) specimen was chosen as an example. First, benchmark results to assess delamination propagation capabilities under static loading were created using models simulating specimens with different delamination lengths. For each delamination length modeled, the load and displacement at the load point were monitored. The mixed-mode strain energy release rate components were calculated along the delamination front across the width of the specimen. A failure index was calculated by correlating the results with the mixed-mode failure criterion of the graphite/epoxy material. The calculated critical loads and critical displacements for delamination onset for each delamination length modeled were used as a benchmark. The load/displacement relationship computed during automatic propagation should closely match the benchmark case. Second, starting from an initially straight front, the delamination was allowed to propagate based on the algorithms implemented in the commercial finite element software. The load-displacement relationship obtained from the propagation analysis results and the benchmark results were compared. Good agreements could be achieved by selecting the appropriate input parameters, which were determined in an iterative procedure.

  18. Discrete Spring Model for Predicting Delamination Growth in Z-Fiber Reinforced DCB Specimens

    Science.gov (United States)

    Ratcliffe, James G.; OBrien, T. Kevin

    2004-01-01

    Beam theory analysis was applied to predict delamination growth in Double Cantilever Beam (DCB) specimens reinforced in the thickness direction with pultruded pins, known as Z-fibers. The specimen arms were modeled as cantilever beams supported by discrete springs, which were included to represent the pins. A bi-linear, irreversible damage law was used to represent Z-fiber damage, the parameters of which were obtained from previous experiments. Closed-form solutions were developed for specimen compliance and displacements corresponding to Z-fiber row locations. A solution strategy was formulated to predict delamination growth, in which the parent laminate mode I critical strain energy release rate was used as the criterion for delamination growth. The solution procedure was coded into FORTRAN 90, giving a dedicated software tool for performing the delamination prediction. Comparison of analysis results with previous analysis and experiment showed good agreement, yielding an initial verification for the analytical procedure.

  19. The effect of transverse shear on the postbuckling and growth characteristics of delaminations in composites

    Energy Technology Data Exchange (ETDEWEB)

    Ferrie, C.H.; Sheinman, I.; Kardomateas, G.A.

    1999-10-01

    A geometrically nonlinear formulation for the behavior of composite delaminated beams of arbitrary stacking sequence, and with the effects of transverse shear deformation included, is presented. The formulation is based on a first-order shear deformation kinematic model, which incorporates the bending-stretching coupling effect and also assumes an arbitrary initial imperfection. The nonlinear differential equations are solved by Newton's method using a finite-difference scheme. The growth of the delamination is also studied by applying the J-integral in order to derive a formula for the energy release rate, which includes transverse shear. Results are presented which illustrate the shear effect, especially with respect to the ratio of the in-plane extensional over shear modulus and with respect to the ratio of plate length over thickness. It is seen that transverse shear can affect largely the displacement profiles, rendering the structure more compliant, and can promote growth by increasing the energy release rate, but this latter effect is moderate and mainly noticeable only at the later stages in the postbuckling regime.

  20. In situ characterization of delamination and crack growth of a CGO–LSM multi-layer ceramic sample investigated by X-ray tomographic microscopy

    DEFF Research Database (Denmark)

    Bjørk, Rasmus; Esposito, Vincenzo; Lauridsen, Erik Mejdal;

    2014-01-01

    The densification, delamination and crack growth behavior in a Ce0.9Gd0.1O1.95 (CGO) and (La0.85Sr0.15)0.9MnO3 (LSM) multi-layer ceramic sample was studied using in situ X-ray tomographic microscopy (microtomography) to investigate the critical dynamics of crack propagation and delamination...... in a multilayered sample. Naturally occurring defects, caused by the sample preparation process, are shown not to be critical in sample degradation. Instead defects are nucleated during the debinding step. Crack growth is significantly faster along the material layers than perpendicular to them, and crack growth...

  1. Buckling-driven delamination growth in composite laminates: Guidelines for assessing the threat posed by interlaminar matrix delamination

    DEFF Research Database (Denmark)

    Bhushan, Karihaloo; Stang, Henrik

    2008-01-01

    This paper is concerned with development of a simple procedure to assess the threat posed by interlaminar matrix delaminations to the integrity of composite laminates when they are situated in a compressive stress field. Depending upon the size of the delamination, its location below the surface...

  2. Fatigue Crack and Delamination Growth in Fibre Metal Laminates under Variable Amplitude Loading

    NARCIS (Netherlands)

    Khan, S.

    2013-01-01

    This thesis presents the investigation into the fatigue propagation and delamination growth of Fibre Metal Laminates under variable amplitude loading. As explained in the first chapter, the motivation of the research is twofold: first, to obtain a clear understanding and detailed characterization of

  3. Methods for the prediction of fatigue delamination growth in composites and adhesive bonds: A critical review

    NARCIS (Netherlands)

    Pascoe, J.A.; Alderliesten, R.C.; Benedictus, R.

    2013-01-01

    An overview is given of the development of methods for the prediction of fatigue driven delamination growth over the past 40 years. Four categories of methods are identified: stress/strain-based models, fracture mechanics based models, cohesive-zone models, and models using the extended finite eleme

  4. Non-destructive evaluation of delamination growth in glass fiber composites using optical coherence tomography

    Science.gov (United States)

    Liu, Ping; Groves, Roger M.; Benedictus, Rinze

    2014-03-01

    Based on low coherence interferometry, a robust optical coherence tomography (OCT) system has been built. The system was used to monitor the growth of a delamination between the middle layers of a glass fiber composite under a static loading. Firstly specimens of the material used for the spar webs in wind turbines were prepared with an interlaminar crack from free edges. Then they were statically loaded by a customized tensile test stage to extend the delamination length and simultaneously scanned by the OCT system. To process the acquired data, an optimized signal processing algorithm was developed. The cross-sectional images clearly show the microstructure and the crack within the specimen. The 3D crack profiles show the application of OCT to determine the evolution of the crack structure inside the composite material during the propagation of the delamination, for the first time to the best of our knowledge.

  5. Mode Mixity for Orthotropic Interface Delamination in Laminated Composites

    Institute of Scientific and Technical Information of China (English)

    FAN Xue-ling; SUN Qin; YUAN Mei-ni; Masanori Kikuchi

    2009-01-01

    The mode mixity is defined based on nonoscillatory strain energy release rate components of delamination between two different orthotropic materials to evaluate the delamination behavior of laminated composites.The result showes that the relative location of the delamination through the thickness influences the mode mixity in a relatively well-regulated way,and that the reinforcement directions of the adjacent plies along the delamination front have a more complicated impact on the mode mixity.This is caused by the bending/twist coupling and bending/bending coupling in the stress field at the crack tip for delamination between multidirectional plies,which completely modifies the stress and strain fields ahead of the crack tip.These kinds of couplings account for the non-uniform distribution of mode mixity values along the delamination front.Application of appropriate mode mixity values is necessary for accurate prediction of delamination growth.

  6. In Search of a Time Efficient Approach to Crack and Delamination Growth Predictions in Composites

    Science.gov (United States)

    Krueger, Ronald; Carvalho, Nelson

    2016-01-01

    Analysis benchmarking was used to assess the accuracy and time efficiency of algorithms suitable for automated delamination growth analysis. First, the Floating Node Method (FNM) was introduced and its combination with a simple exponential growth law (Paris Law) and Virtual Crack Closure technique (VCCT) was discussed. Implementation of the method into a user element (UEL) in Abaqus/Standard(Registered TradeMark) was also presented. For the assessment of growth prediction capabilities, an existing benchmark case based on the Double Cantilever Beam (DCB) specimen was briefly summarized. Additionally, the development of new benchmark cases based on the Mixed-Mode Bending (MMB) specimen to assess the growth prediction capabilities under mixed-mode I/II conditions was discussed in detail. A comparison was presented, in which the benchmark cases were used to assess the existing low-cycle fatigue analysis tool in Abaqus/Standard(Registered TradeMark) in comparison to the FNM-VCCT fatigue growth analysis implementation. The low-cycle fatigue analysis tool in Abaqus/Standard(Registered TradeMark) was able to yield results that were in good agreement with the DCB benchmark example. Results for the MMB benchmark cases, however, only captured the trend correctly. The user element (FNM-VCCT) always yielded results that were in excellent agreement with all benchmark cases, at a fraction of the analysis time. The ability to assess the implementation of two methods in one finite element code illustrated the value of establishing benchmark solutions.

  7. Experimental approach for mixed-mode fatigue delamination crack growth with large-scale bridging in polymer composites

    DEFF Research Database (Denmark)

    Holmes, John W.; Liu, Liu; Sørensen, Bent F.

    2014-01-01

    of delaminations in a typical fibre-reinforced polymer composite was investigated under a constant cyclic loading amplitude. Pure mode I, mode II and mixed-mode crack growth conditions were examined. The results, analysed using a J-integral approach, show that the double cantilever beam loaded with uneven bending......An experimental apparatus utilizing double cantilever beam specimens loaded with uneven bending moments was developed to study the mixed-mode fatigue crack growth in composites. The approach is suitable when large-scale bridging of cracks is present. To illustrate the testing method, cyclic growth...... crack growth rate observed. In addition to details concerning the equipment, a general discussion of the development of cyclic bridging laws for delamination growth in the presence of large-scale bridging is provided....

  8. Characterization of Mode I and mixed-mode delamination growth in T300/5208 graphite/epoxy

    Science.gov (United States)

    Ramkumar, R. L.; Whitcomb, J. D.

    1985-01-01

    The roles played by Mode I and Mode II strain-energy release rates (G-I and G-II, respectively) in inducing delamination growth under static and fatigue loading were investigated, using T300/5208 graphite/epoxy specimens. Double cantilever beam (DCB) specimens and cracked lap shear (CLS) specimens were used for pure Mode I and mixed-mode tests, respectively. Fatigue-induced delamination growth was characterized by constant-amplitude fatigue tests at a minimum to maximum cyclic load ratio of 0.05 and a frequency of 10 Hz. During the tests, the maximum and minimum strain-energy release rates (Gmax, Gmin) and the delamination growth rate (da/dN) were monitored. Static tests on mixed-mode CLS specimens measured the total strain-energy release rate, which was broken into G-I and G-II components using finite-element analysis. A power-law relationship between da/dN and G-Imax, and da/dN and Gmax were obtained from fatigue test results on DCB and CLS specimens, respectively. The power law for a pure Mode II delamination was derived from CLS results by subtracting the contribution due to G-I.

  9. Effects of voids on delamination behavior under static and fatigue mode I and mode II

    Science.gov (United States)

    Abdelal, Nisrin Rizek

    Composite materials have become materials of choice for wind turbine blade manufacturing due to their high specific stiffness, strength and fatigue life. Glass fiber composites are used extensively in light-weight structural components for wind turbines, aircrafts, marine craft and high performance automobile because glass fiber is inexpensive and usually provides high strength to weight ratio and good in-plane mechanical properties. The high cycle fatigue resistance of composite materials used in wind turbine blades has been recognized as a major uncertainty in predicting the reliability of wind turbines over their design lifetime. Blades are expected to experience 108 to 109 fatigue cycles over a 20 to 30 year lifetime. Delamination or interlaminar failure is a serious failure mode observed in composite structures. Even partial delamination will lead to a loss of local stiffness, which can preclude buckling failure. Manufacturing process defects such as voids and fiber waviness degrade the fatigue life and delamination resistance of the blade's composite. This research describes the effect of voids on static and fatigue interlaminar fracture behavior under mode I and mode II loading of wind turbine glass fiber composites. Samples with different void volume fractions in the 0.5%-7% range were successfully obtained by varying the vacuum in the hand layup vacuum bagging manufacturing process. Void content was characterized using four different methods; ultrasonic scanning, epoxy burn off, serial sectioning and X-Ray computed tomography. The effect of voids on both mode I and mode II interlaminar fracture toughness under static and fatigue loading was investigated. Finally, fractographic analysis (using optical and scanning electron microscopy) was conducted. The results showed that voids leads to slight reduction in static modes I and II interlaminar fracture toughness. In addition, voids lead to a decrease in modes I and II maximum cyclic strain energy release

  10. Mode I fatigue delamination growth in composite laminates with fibre bridging

    NARCIS (Netherlands)

    Yao, L.

    2015-01-01

    Advanced composite materials have been commonly used in aerospace engineering, because of their good mechanical properties and attractive potential for creating lightweight structures. Susceptibility to delamination is one of the most important issues in the applications of these materials. This

  11. STUDY ON FAILURE PROCESS OF DELAMINATED STIFFENED COMPOSITE PLATES UNDER COMPRESSION

    Institute of Scientific and Technical Information of China (English)

    陈浩然; 白瑞祥; 王蔓

    2003-01-01

    Failure behavior of the delaminated stiffened composite plates under compression is studied by the finite element method, based on a Global-Local variational model. A virtual crack closure technique and a self-adaptive grid moving scheme are proposed to predict the delamination growth process. The contact effect along the delamination front is considered. The numerical results show that the influences of the distribution and location of the stiffeners, the configuration and size of the delamination, the boundary condition and the contact upon the failure behavior of the plates are significant.

  12. Influence of Mixed Mode I-Mode II Loading on Fatigue Delamination Growth Characteristics of a Graphite Epoxy Tape Laminate

    Science.gov (United States)

    Ratcliffe, James G.; Johnston, William M., Jr.

    2014-01-01

    Mixed mode I-mode II interlaminar tests were conducted on IM7/8552 tape laminates using the mixed-mode bending test. Three mixed mode ratios, G(sub II)/G(sub T) = 0.2, 0.5, and 0.8, were considered. Tests were performed at all three mixed-mode ratios under quasi-static and cyclic loading conditions, where the former static tests were used to determine initial loading levels for the latter fatigue tests. Fatigue tests at each mixed-mode ratio were performed at four loading levels, Gmax, equal to 0.5G(sub c), 0.4G(sub c), 0.3G(sub c), and 0.2G(sub c), where G(sub c) is the interlaminar fracture toughness of the corresponding mixed-mode ratio at which a test was performed. All fatigue tests were performed using constant-amplitude load control and delamination growth was automatically documented using compliance solutions obtained from the corresponding quasi-static tests. Static fracture toughness data yielded a mixed-mode delamination criterion that exhibited monotonic increase in Gc with mixed-mode ratio, G(sub II)/G(sub T). Fatigue delamination onset parameters varied monotonically with G(sub II)/G(sub T), which was expected based on the fracture toughness data. Analysis of non-normalized data yielded a monotonic change in Paris law exponent with mode ratio. This was not the case when normalized data were analyzed. Fatigue data normalized by the static R-curve were most affected in specimens tested at G(sub II)/G(sub T)=0.2 (this process has little influence on the other data). In this case, the normalized data yielded a higher delamination growth rate compared to the raw data for a given loading level. Overall, fiber bridging appeared to be the dominant mechanism, affecting delamination growth rates in specimens tested at different load levels and differing mixed-mode ratios.

  13. Dynamic behavior of a rotating delaminated composite beam including rotary inertia and shear deformation effects

    Directory of Open Access Journals (Sweden)

    Ramazan-Ali Jafari-Talookolaei

    2015-09-01

    Full Text Available A finite element (FE model is developed to study the free vibration of a rotating laminated composite beam with a single delamination. The rotary inertia and shear deformation effects, as well as the bending–extension, bending–twist and extension–twist coupling terms are taken into account in the FE model. Comparison between the numerical results of the present model and the results published in the literature verifies the validity of the present model. Furthermore, the effects of various parameters, such as delamination size and location, fiber orientation, hub radius, material anisotropy and rotating speed, on the vibration of the beam are studied in detail. These results provide useful information in the study of the free vibration of rotating delaminated composite beams.

  14. Mode I fatigue delamination growth in composite laminates with fibre bridging

    NARCIS (Netherlands)

    Yao, L.

    2015-01-01

    Advanced composite materials have been commonly used in aerospace engineering, because of their good mechanical properties and attractive potential for creating lightweight structures. Susceptibility to delamination is one of the most important issues in the applications of these materials. This dis

  15. An exact solution for the history-dependent material and delamination behavior of laminated plates subjected to cylindrical bending

    Energy Technology Data Exchange (ETDEWEB)

    Williams, Todd O [Los Alamos National Laboratory

    2009-01-01

    The exact solution for the history-dependent behavior of laminated plates subjected to cylindrical bending is presented. The solution represents the extension of Pagano's solution to consider arbitrary types of constitutive behaviors for the individual lamina as well as arbitrary types of cohesive zones models for delamination behavior. Examples of the possible types of material behavior are plasticity, viscoelasticity, viscoplasticity, and damaging. Examples of possible CZMs that can be considered are linear, nonlinear hardening, as well as nonlinear with softening. The resulting solution is intended as a benchmark solution for considering the predictive capabilities of different plate theories. Initial results are presented for several types of history-dependent material behaviors. It is shown that the plate response in the presence of history-dependent behaviors can differ dramatically from the elastic response. These results have strong implications for what constitutes an appropriate plate theory for modeling such behaviors.

  16. Impact Analysis of Embedded Delamination Location in Hybrid Curved Laminated Composite Stiffened Panel

    Science.gov (United States)

    Naini, Jeevan Kumar; P, Ramesh Babu

    2016-08-01

    Modern, aero structures are predominantly of curved construction characterized by a skin and stiffeners. The latest generation of large passenger aircraft also uses mostly composite material in their primary structure and there is trend towards the utilization of bonding of subcomponents. The presence of delamination is a major problem in composite laminated panels and so, it is of great concern to both the academic and aeronautical industrial worlds Indeed delamination can strongly affect the material strength and, sometimes, can cause their breaking up in service. A Pre-damaged configuration is loaded to study the delamination location and mode for delamination initiation and propagation. A parametric study is conducted to investigate the effect of the location of the delamination propagation when delamination is embedded inbetween plies of the skin-stiffener interface, with the cases i) delamination located at front and inbetween plies of the skin-stiffener interface ii) delamination located in middle and inbetween plies of the skin-stiffener interface iii) delamination located at the end and inbetween plies of the skin- stiffener interface. Further the influence of the location of the delamination on load carrying capacity of the panel is investigated. The effect of location of debonds on crack growth and collapse behavior is analyzed using analysis tool. An analysis tool is applied that includes an approach for predicting interlaminar damage initiation and interlaminar damage growth as well as in-plane damage mechanisms to predict the design of defect free panel.

  17. Cracking and delamination behaviors of photovoltaic backsheet after accelerated laboratory weathering

    Science.gov (United States)

    Lin, Chiao-Chi; Lyu, Yadong; Hunston, Donald L.; Kim, Jae Hyun; Wan, Kai-Tak; Stanley, Deborah L.; Gu, Xiaohong

    2015-09-01

    The channel crack and delamination phenomena that occurred during tensile tests were utilized to study surface cracking and delamination properties of a multilayered backsheet. A model sample of commercial PPE (polyethylene terephthalate (PET)/PET/ethylene vinyl acetate (EVA)) backsheet was studied. Fragmentation testing was performed after accelerated aging with and without ultraviolet (UV) irradiation in two relative humidity (RH) levels (5 % RH and 60 % RH) at elevated temperature (85 °C) conditions for 11 days and 22 days. Results suggest that the embrittled surface layer resulting from the UV photo-degradation is responsible for surface cracking when the strain applied on the sample is far below the yielding strain (2.2 %) of the PPE sample. There was no surface cracking observed on the un-aged sample and samples aged without UV irradiation. According to the fragmentation testing results, the calculated fracture toughness (KIC) values of the embrittled surface layer are as low as 0.027 MPa·m1/2 to 0.104 MPa·m1/2, depending on the humidity levels and aging times. Surface analysis using attenuated total reflectance Fourier transform infrared and atomic force microscopy shows the degradation mechanism of the embrittled surface layer is a combination of the photodegradation within a certain degradation depth and the moisture erosion effect depending on the moisture levels. Specifically, UV irradiation provides a chemical degradation effect while moisture plays a synergistic effect on surface erosion, which influences surface roughness after aging. Finally, there was no delamination observed during tensile testing in this study, suggesting the surface cracking problem is more significant than the delamination for the PPE backsheet material and conditions tested here.

  18. Simulation Methods for High-Cycle Fatigue-Driven Delamination using Cohesive Zone Models - Fundamental Behavior and Benchmark Studies

    DEFF Research Database (Denmark)

    Bak, Brian Lau Verndal; Lindgaard, Esben; Turon, A.;

    2015-01-01

    A novel computational method for simulating fatigue-driven delamination cracks in composite laminated structures under cyclic loading based on a cohesive zone model [2] and new benchmark studies with four other comparable methods [3-6] are presented. The benchmark studies describe and compare...... the traction-separation response in the cohesive zone and the transition phase from quasistatic to fatigue loading for each method. Furthermore, the accuracy of the predicted crack growth rate is studied and compared for each method. It is shown that the method described in [2] is significantly more accurate...... than the other methods [3-6]. Finally, studies are presented of the dependency and sensitivity to the change in different quasi-static material parameters and model specific fitting parameters. It is shown that all the methods except [2] rely on different parameters which are not possible to determine...

  19. Delamination tolerance studies in laminated composite panels

    Indian Academy of Sciences (India)

    K L Singh; B Dattaguru; T S Ramamurthy; P D Mangalgiri

    2000-08-01

    Determination of levels of tolerance in delaminated composite panels is an important issue in composite structures technology. The primary intention is to analyse delaminated composite panels and estimate Strain Energy Release Rate (SERR) parameters at the delamination front to feed into acceptability criteria. Large deformation analysis is necessary to cater for excessive rotational deformations in the delaminated sublaminate. Modified Virtual Crack Closure Integral (MVCCI) is used to estimate all the three SERR components at the delamination front from the finite element output containing displacements, strains and stresses. The applied loading conditions are particularly critical and compressive loading on the panel could lead to buckling of the delaminated sublaminate and consequent growth of delamination. Numerical results are presented for circular delamination of varioussizes and delamination at various interfaces (varying depth-wise location) between the base- and the sub-laminates. Numerical data are also presented on the effect of bi-axial loading and in particular on compressive loading in both directions. The results can be used to estimate delamination tolerance at various depths (or at various interfaces) in the laminate.

  20. Effects of Crimped Fiber Paths on Mixed Mode Delamination Behaviors in Woven Fabric Composites

    Science.gov (United States)

    2016-09-01

    figure 3. The force was applied to the loading bar at a constant rate with respect to time. This type of loading is referred to as “ force -control... rate Gc_eff. Once this occurred, strain energy was released and crack growth developed . Failure was based on LEFM through the use of VCCT. The VCCT...Composites Paul V. Cavallaro Andrew W. Hulton NUWC Division Newport Melvin W. Jee U.S. Army Natick Soldier Research, Development & Engineering Center

  1. An high order Mixed Interpolation Tensorial Components (MITC) shell element approach for modeling the buckling behavior of delaminated composites

    DEFF Research Database (Denmark)

    Gaiotti, Marco; Rizzo, Cesare M.; Branner, Kim

    2014-01-01

    of composite laminates of wind turbine blades, results were found valuable for the marine industry as well, because similar laminates are used for the hull shell and stiffeners. Systematic calculations were carried out to assess the effects of an embedded delamination on the buckling load, varying the size...... and through thickness position of the delamination. Different finite element modeling strategies were considered and validated against the experimental results. The one applying the 9 nodes MITC shell elements was found matching the experimental data despite failure modes were different for the two...

  2. Packaging issues: avoiding delamination.

    Science.gov (United States)

    Hall, R

    2005-10-01

    Manufacturers can minimise delamination occurrence by applying the appropriate packaging design and process features. The end user can minimise the impact of fibre tear and reduce subsequent delamination by careful package opening. The occasional inconvenient delamination is a small price to pay for the high level of sterility assurance that comes with the use of Tyvek.

  3. Optical Evaluation on Delamination Buckling of Composite Laminate with Impact Damage

    Directory of Open Access Journals (Sweden)

    J. T. Ruan

    2014-01-01

    Full Text Available The delamination buckling and growth behaviors of a cross-ply composite laminate with damage induced by low velocity impact are investigated optically using three-dimensional digital image correlation (3D-DIC method. For the 3D deformation measurement, the 3D-DIC setup comprised of two CCD cameras was adopted. The rectangle specimen was impacted under the impact energy of 7.0 J using a drop-weight testing machine, and the impact damage was detected by means of X-ray nondestructive evaluation (NDE technique. The 3D deformation field measured with the optical system clearly reveals that the delamination buckling characteristic of the specimen mainly appears local deformation mode under compression after impact test. Moreover, the behavior of delamination growth evaluated by the 3D-DIC optical method reasonably agrees with the NDE observed damage result after compression.

  4. Delamination of Composite Cylinders

    Science.gov (United States)

    Davies, Peter; Carlsson, Leif A.

    The delamination resistance of filament wound glass/epoxy cylinders has been characterized for a range of winding angles and fracture mode ratios using beam fracture specimens. The results reveal that the delamination fracture resistance increases with increasing winding angle and mode II (shear) fraction (GΠ/G). It was also found that interlaced fiber bundles in the filament wound cylinder wall acted as effective crack arresters in mode I loading. To examine the sensitivity of delamina-tion damage on the strength of the cylinders, external pressure tests were performed on filament-wound glass/epoxy composite cylinders with artificial defects and impact damage. The results revealed that the cylinder strength was insensitive to the presence of single delaminations but impact damage caused reductions in failure pressure. The insensitivity of the failure pressure to a single delamination is attributed to the absence of buckling of the delaminated sublaminates before the cylinder wall collapsed. The impacted cylinders contained multiple delaminations, which caused local reduction in the compressive load capability and reduction in failure pressure. The response of glass/epoxy cylinders was compared to impacted carbon reinforced cylinders. Carbon/epoxy is more sensitive to damage but retains higher implosion resistance while carbon/PEEK shows the opposite trend.

  5. Buckling-driven delamination of carbon nanotube forests

    Science.gov (United States)

    Pour Shahid Saeed Abadi, Parisa; Hutchens, Shelby B.; Greer, Julia R.; Cola, Baratunde A.; Graham, Samuel

    2013-06-01

    We report buckling-driven delamination of carbon nanotube (CNT) forests from their growth substrates when subjected to compression. Macroscale compression experiments reveal local delamination at the CNT forest-substrate interface. Results of microscale flat punch indentations indicate that enhanced CNT interlocking at the top surface of the forest accomplished by application of a metal coating causes delamination of the forest from the growth substrate, a phenomenon not observed in indentation of as-grown CNT forests. We postulate that the post-buckling tensile stresses that develop at the base of the CNT forests serve as the driving force for delamination.

  6. 湿热载荷下含损伤夹层板分层扩展判定分析%Delamination Growth of Composite Sandwich under Hygrothermal and Mechanical Loads

    Institute of Scientific and Technical Information of China (English)

    张志民; 李向阳

    2001-01-01

    The local buckling may occur in composite sandwich with delamination induced by impact damage. This often causes delamination growth and structure failure. The delamiantion growth is studied by using the variational method of moving boundary, and the formulas of energy release rate G along the delamination front are obtained. By employing Rayleigh-Ritz method, the hygrothermal effect on buckling character of composite sandwich plates containing delamination between two faceplate laminae is studied.%含面板内分层损伤的复合材料夹层板在承受压缩载荷时,很容易发生局部屈曲,导致分层扩展和结构失效,恶劣的湿热环境更是使之加剧.利用可动边界变分问题对分层扩展进行了分析,导出了分层边界的逐点能量释放率表达式,采用Rayleigh-Ritz法研究了任意的湿热环境对含损伤的复合材料夹层板分层扩展性能的影响.

  7. THE EFFECT OF SUPPORT PLATE ON DRILLING-INDUCED DELAMINATION

    Directory of Open Access Journals (Sweden)

    Navid Zarif Karimi

    2016-02-01

    Full Text Available Delamination is considered as a major problem in drilling of composite materials, which degrades the mechanical properties of these materials. The thrust force exerted by the drill is considered as the major cause of delamination; and one practical approach to reduce delamination is to use a back-up plate under the specimen. In this paper, the effect of exit support plate on delamination in twist drilling of glass fiber reinforced composites is studied. Firstly, two analytical models based on linear fracture mechanics and elastic bending theory of plates are described to find critical thrust forces at the beginning of crack growth for drilling with and without back-up plate. Secondly, two series of experiments are carried out on glass fiber reinforced composites to determine quantitatively the effect of drilling parameters on the amount of delamination. Experimental findings verify a large reduction in the amount of delaminated area when a back-up plate is placed under the specimen.

  8. Vibration of composite beams with two overlapping delaminations

    Institute of Scientific and Technical Information of China (English)

    Christian N. Della; Dongwei Shu; Yapu Zhao

    2005-01-01

    Delaminations in composite laminates may develop from small cracks due to fabrication and impact loading, or from places of high stress concentration. The locations of the delaminations are not determinate. In this research, an analytical solution for the free vibration of a composite beam with two overlapping delaminations is presented. The delaminated beam is analyzed as seven interconnected beams using the delaminations as their boundaries. The continuity and equilibrium conditions are satisfied between the adjoining regions of the beams. Classical beam theory is applied to each of the beams. Complex vibration behaviors emerge for different sizes and locations of the delaminations. Comparison with analytical results reported in the literature verifies the validity of the present solution.

  9. Fractography of composite delamination

    Science.gov (United States)

    Bascom, W. D.

    1990-01-01

    The microdamage that occurs for Mode 1 and Mode 2 delamination was examined by potting delaminated specimens in a clear epoxy, sectioning through the damage, polishing the cut sections and examining using light microscopy. For Mode 1 delamination of unidirectional carbon fiber reinforced plastic (CFRP) composites, the major observation was fiber bridging including large ligaments of fiber bundles. The Mode 2 delamination of unidirectional laminates revealed a very narrow crack opening with only occasional fiber bridging. Impact testing by repetitive impacts with increasing energy was studied and it was found that this technique does not discern changes in the type of damage with increasing cumulative impact energy. Instead, the changes in the impact response, notably stiffness, are the result of changes in the extent of damage. For laminates with a brittle thermoplastic matrix, 3501-6, there were distinct changes in stiffness that corresponded to the development of through the thickness damage and then to the extension of the damage to the specimen edges. For PEEK and polycarbonate, the changes in stiffness were not as abrupt as for the thermoset. None the less, the damage progressed in the same manner.

  10. The effect of delaminations on local buckling in wind turbine blades

    DEFF Research Database (Denmark)

    Haselbach, Philipp Ulrich; Bitsche, Robert; Branner, Kim

    2015-01-01

    was setup in Abaqus and cohesive elements were chosen for modelling delamination growth. For initial delaminations with a width of 30–50% of the cap width the study showed that delamination close to the surface started to grow in load ranges of normal operation conditions and led to local buckling modes....... The local buckling caused high strains and stresses in the surrounding of the delamination, which exceeded the material design properties and therefore should be considered as dangerous. Delaminations placed near the mid-surface of the cap did not have a significant effect on the blade response under normal...... operation conditions. In the simulations the static load exceeded the design load by more than 40% before delamination growth or cap buckling occurred. It could be concluded that delamination induced near-surface buckling modes have to be considered critical due to an onset of local sublaminate buckling...

  11. Integrated global digital image correlation for interface delamination characterization

    KAUST Repository

    Hoefnagels, Johan P.M.

    2013-07-23

    Interfacial delamination is a key reliability challenge in composites and micro-electronic systems due to (high-density) integration of dissimilar materials. Predictive finite element models are used to minimize delamination failures during design, but require accurate interface models to capture (irreversible) crack initiation and propagation behavior observed in experiments. Therefore, an Integrated Global Digital Image Correlation (I-GDIC) strategy is developed for accurate determination of mechanical interface behavior from in-situ delamination experiments. Recently, a novel miniature delamination setup was presented that enables in-situ microscopic characterization of interface delamination while sensitively measuring global load-displacement curves for all mode mixities. Nevertheless, extraction of detailed mechanical interface behavior from measured images is challenging, because deformations are tiny and measurement noise large. Therefore, an advanced I-GDIC methodology is developed which correlates the image patterns by only deforming the images using kinematically-admissible \\'eigenmodes\\' that correspond to the few parameters controlling the interface tractions in an analytic description of the crack tip deformation field, thereby greatly enhancing accuracy and robustness. This method is validated on virtual delamination experiments, simulated using a recently developed self-adaptive cohesive zone (CZ) finite element framework. © The Society for Experimental Mechanics, Inc. 2014.

  12. Buckling-driven delamination in layered spherical shells

    Science.gov (United States)

    Sørensen, Kim D.; Jensen, Henrik M.

    An analysis of buckling-driven delamination of a layer in a spherical, layered shell has been carried out. The effects of the substrate having a double curvature compared to previous studies of delamination on cylindrical substrates turn out to be non-trivial in the sense that additional to the effect of the shape of the substrate, a new non-dimensional geometrical parameter enters the conditions for steady-state delamination. It is shown that this additional geometrical parameter in most cases of practical relevance has insignificant influence on the fracture mechanical parameters involved for the problem. The consequence is that solutions need to be mapped as a function of one rather than two dimensionless parameters. Furthermore, the shape of the substrate has profound influence especially on initiation of delamination growth.

  13. Investigating Delamination Migration in Composite Tape Laminates

    Science.gov (United States)

    Ratcliffe, James G.; DeCarvalho, Nelson V.

    2014-01-01

    A modification to a recently developed test specimen designed to investigate migration of a delamination between neighboring ply interfaces in tape laminates is presented. The specimen is a cross-ply laminated beam consisting of 40 plies with a polytetrafluoroethylene insert spanning part way along its length. The insert is located between a lower 0-degree ply (specimen length direction) and a stack of four 90-degree plies (specimen width direction). The modification involved a stacking sequence that promotes stable delamination growth prior to migration, and included a relocation of the insert from the specimen midplane to the interface between plies 14 and 15. Specimens were clamped at both ends onto a rigid baseplate and loaded on their upper surface via a piano hinge assembly, resulting in a predominantly flexural loading condition. Tests were conducted with the load-application point positioned at various locations along a specimen's span. This position affected the sequence of damage events during a test.

  14. Edge effects and delamination failures

    Science.gov (United States)

    Herakovich, C. T.

    1989-01-01

    The fundamental relationship between the morphology of a composite laminate and the resulting free edge effects is explored and related to delamination failures. Cross-ply, angle-ply, and quasi-isotropic laminates are discussed in detail. It is shown that the local mismatch in elastic properties of adjacent layers and the global stacking sequence of a laminate both have a significant influence on the interlaminar stresses and delamination failures.

  15. Characterizing Delamination Migration in Carbon/Epoxy Tape Laminates

    Science.gov (United States)

    Ratcliffe, James G.; Czabaj, Michael W.; Obrien, Thomas K.

    2012-01-01

    A new test method is presented for the purpose of investigating migration of a delamination between neighboring ply interfaces in fiber-reinforced, polymer matrix tape laminates. The test is a single cantilever beam configuration consisting of a cross-ply laminate with a polytetrafluoroethylene (PTFE) insert implanted at the mid-plane and spanning part way along the length of the specimen. The insert is located between a 0-degree ply (specimen length direction) and a stack of four 90-degree plies (specimen width direction). The specimen is clamped at both ends onto a rigid baseplate and is loaded on its upper surface via a piano hinge. Tests were conducted with the load-application point located on the intact portion of the specimen in order to initiate delamination growth onset followed by migration of the delamination to a neighboring 90/0 ply interface by kinking through the 90- degree ply stack. Varying this position was found to affect the distance relative to the load-application point at which migration initiated. In each specimen, migration initiated by a gradual transition of the delamination at the 0/90 interface into the 90- degree ply stack. In contrast, transition of the kinked crack into the 90/0 interface was sudden. Fractography of the specimens indicated that delamination prior to migration was generally mixed mode-I/II. Inspection of the kink surface revealed mode-I fracture. In general, use of this test allows for the observation of the growth of a delamination followed by migration of the delamination to another ply interface, and should thus provide a means for validating analyses aimed at simulating migration.

  16. Progressive delamination in polymer matrix composite laminates: A new approach

    Science.gov (United States)

    Chamis, C. C.; Murthy, P. L. N.; Minnetyan, L.

    1992-01-01

    A new approach independent of stress intensity factors and fracture toughness parameters has been developed and is described for the computational simulation of progressive delamination in polymer matrix composite laminates. The damage stages are quantified based on physics via composite mechanics while the degradation of the laminate behavior is quantified via the finite element method. The approach accounts for all types of composite behavior, laminate configuration, load conditions, and delamination processes starting from damage initiation, to unstable propagation, and to laminate fracture. Results of laminate fracture in composite beams, panels, plates, and shells are presented to demonstrate the effectiveness and versatility of this new approach.

  17. Micromechanical models of delamination in aluminum-lithium alloys

    Science.gov (United States)

    Messner, Mark Christian

    Aluminum lithium (Al-Li) alloys are lighter, stiffer, and tougher than conventional aerospace aluminum alloys. Replacing conventional aluminums with Al-Li could substantially decrease the weight and cost of aerospace structures. However, Al-Li alloys often fracture intergranularly via a mechanism called delamination cracking. While secondary delamination cracks can improve the effective toughness of a component, no current model accurately predicts the initiation and growth of intergranular cracks. Since simulations cannot incorporate delamination into a structural model, designers cannot quantify the effect of delamination cracking on a particular component. This uncertainty limits the application of Al-Li alloys. Previous experiments identify microstructural features linked to delamination. Fractography of failed surfaces indicates plastic void growth triggers intergranular failure. Furthermore, certain types of soft/stiff grain boundaries tend to localize void growth and nucleate delamination cracks. This dissertation develops a mechanism for the initiation of delamination on the microscale that accounts for these experimental observations. Microscale simulations of grain boundaries near a long primary crack explore the delamination mechanism on the mesoscale. In these simulations, a physically-based crystal plasticity (CP) model represents the constitutive response of individual grains. This CP model incorporates plastic voriticity correction terms into a standard objective stress rate integration, to accurately account for the kinematics of lattice deformation. The CP model implements slip system hardening with a modular approach to facilitate quick testing and calibration of different theories of hardening. The microscale models reveal soft/stiff grain boundaries develop elevated mean stress and plastic strain as a consequence of the mechanics of the interface. These elevated stresses and strain drive plastic void growth. The results indicate plastic void

  18. Assessment of Static Delamination Propagation Capabilities in Commercial Finite Element Codes Using Benchmark Analysis

    Science.gov (United States)

    Orifici, Adrian C.; Krueger, Ronald

    2010-01-01

    With capabilities for simulating delamination growth in composite materials becoming available, the need for benchmarking and assessing these capabilities is critical. In this study, benchmark analyses were performed to assess the delamination propagation simulation capabilities of the VCCT implementations in Marc TM and MD NastranTM. Benchmark delamination growth results for Double Cantilever Beam, Single Leg Bending and End Notched Flexure specimens were generated using a numerical approach. This numerical approach was developed previously, and involves comparing results from a series of analyses at different delamination lengths to a single analysis with automatic crack propagation. Specimens were analyzed with three-dimensional and two-dimensional models, and compared with previous analyses using Abaqus . The results demonstrated that the VCCT implementation in Marc TM and MD Nastran(TradeMark) was capable of accurately replicating the benchmark delamination growth results and that the use of the numerical benchmarks offers advantages over benchmarking using experimental and analytical results.

  19. Energy based study of quasi-static delamination as a low cycle fatigue process

    NARCIS (Netherlands)

    Amaral, L.; Yao, L.; Alderliesten, R.C.; Benedictus, R.

    2015-01-01

    This work proposes to treat quasi-static mode I delamination growth of CFRP as a low-cycle fatigue process. To this end, mode I quasi-static and fatigue delamination tests were performed. An average physical Strain Energy Release Rate (SERR), derived from an energy balance, is used to characterize t

  20. Energy based study of quasi-static delamination as a low cycle fatigue process

    NARCIS (Netherlands)

    Amaral, L.; Yao, L.; Alderliesten, R.C.; Benedictus, R.

    2015-01-01

    This work proposes to treat quasi-static mode I delamination growth of CFRP as a low-cycle fatigue process. To this end, mode I quasi-static and fatigue delamination tests were performed. An average physical Strain Energy Release Rate (SERR), derived from an energy balance, is used to characterize

  1. Thermally induced delamination of multilayers

    DEFF Research Database (Denmark)

    Sørensen, Bent F.; Sarraute, S.; Jørgensen, O.

    1998-01-01

    Steady-state delamination of multilayered structures, caused by stresses arising during processing due to thermal expansion mismatch, is analyzed by a fracture mechanics model based on laminate theory. It is found that inserting just a few interlayers with intermediate thermal expansion coefficie...... coefficients may be an effective way of reducing the delamination energy release rate. Uneven layer thickness and increasing elastic mismatch are shown to raise the energy release rate. Experimental work confirms important trends of the model.......Steady-state delamination of multilayered structures, caused by stresses arising during processing due to thermal expansion mismatch, is analyzed by a fracture mechanics model based on laminate theory. It is found that inserting just a few interlayers with intermediate thermal expansion...

  2. Short review: Potential impact of delamination cracks on fracture toughness of structural materials

    Directory of Open Access Journals (Sweden)

    X.C. Arnoult

    2016-02-01

    Full Text Available The current energy policy envisages extended lifetime for the current nuclear power plants (GEN II NPP. This policy imposes a large research effort to understand the ageing of power plant components. In this goal, it is necessary to improve knowledge about safety, reliability and components’ integrity for more than forty years of operation. In Central and Eastern Europe, the majority of NPPs are VVER types, where some of the components are produced from austenitic steel 08Ch18N10T. Irradiated 08Ch18N10T may exhibit brittle behavior, namely delamination cracks are found in some cases on the fracture surface of irradiated 08Ch18N10T with elongated δ-ferrite. Delamination cracks have also been observed on the fracture surface of high-strength steels or aluminum-lithium alloys. This article presents a state-of-the art review to provide a detailed analysis of the influence of delamination cracks on the toughness of metal alloys. In general, the delamination cracks are present in metal alloys having a high texture and microstructure anisotropy. Three types of delamination cracks have been observed and are classified as crack arrester delamination, crack divider delamination and crack splitting delamination. The microscopy characterization, 3D fracture theories and computational studies explaining possible causes and effects of delamination cracks on the mechanical properties of metal alloys are presented.

  3. Delamination behaviour in differently copper laminated REBCO coated conductor tapes under transverse loading

    Energy Technology Data Exchange (ETDEWEB)

    Gorospe, Alking [Department of Mechanical Design Engineering, Andong National University, 1375 Kyungdong-Ro, Andong 760-749 (Korea, Republic of); Department of Engineering, Aurora State College of Technology, Baler Aurora 3200 (Philippines); Nisay, Arman [Department of Mechanical Design Engineering, Andong National University, 1375 Kyungdong-Ro, Andong 760-749 (Korea, Republic of); Shin, Hyung-Seop, E-mail: hsshin@andong.ac.kr [Department of Mechanical Design Engineering, Andong National University, 1375 Kyungdong-Ro, Andong 760-749 (Korea, Republic of)

    2014-09-15

    Highlights: • I{sub c} degradation behavior under transverse tension loading in different CC tape structure. • Weibull distribution analysis applied on delamination mechanism of CC tape. • Delamination mechanism on CC tapes depending on copper lamination type. • SEM and WDS mapping analysis of delamination sites under transverse loading. - Abstract: Laminated HTS coated conductor (CC) tapes having a unique multi-layer structure made them vulnerable when exposed to transverse loading. Electromechanical transport properties of these CC tapes can be affected by excessive transverse stresses. Due to the coefficient of thermal expansion (CTE) mismatch and incompatibility among constituent materials used in coil applications, delamination among layers occurs and causes critical current, I{sub c} degradation in the CC tapes. In this study, the delamination behaviors in copper (Cu) solder-laminated CC tapes by soldering and surround Cu-stabilized ones by electroplating under transverse tension loading were investigated. Similarly to the surround Cu-stabilized CC tapes in our previous reports, the Cu solder-laminated CC tapes also showed an abrupt and gradual I{sub c} degradation behavior. However, the Cu solder-laminated CC tapes showed different delamination morphologies as compared to the surround Cu-stabilized CC tapes; the superconducting side and the substrate side of the Cu solder laminated CC tapes were totally separated by delamination. On the other hand, the brass laminate did not show any significant effect on the delamination strength when it is added upon the surround Cu-stabilized CC tapes.

  4. Simulation of cusp formation in mode II delamination

    NARCIS (Netherlands)

    Sluys, L.J.; Van der Meer, F.P.

    2014-01-01

    On the microlevel, cusps are formed during delamination crack growth under mode II loading conditions. In this work, two different approaches to simulate this process are presented. Firstly a cohesive zone method where cohesive segments are introduced between a pair of neighbouring elements when the

  5. Buckle Driven Delamination in Thin Hard Film Compliant Substrate Systems

    Directory of Open Access Journals (Sweden)

    Bahr D.F.

    2010-06-01

    significantly from behavior predicted by rigid elastic solutions. To address this issue we developed a finite element analysis technique that employed a cohesive zone model to simulate interfacial crack growth. Specifying the traction-separation relationship, cohesive strength, and work of separation along with film thickness, film stress, and film and substrate properties, buckle width and height were determined as a function of interfacial toughness. The simulations indicate that an analysis based on rigid substrate solutions significantly underestimate toughness for prescribed buckle widths: a result consistent with an analysis by Yu and Hutchinson [5] that pieced together a solution based on non-linear plate theory with a solution for the linear film on substrate problem. More importantly, the results defined a lower limiting bound to seemingly disparate buckle deflection data (Figure 2. The variance from linear elastic behavior, especially for the small buckles, indicates more than substrate compliance is controlling behavior. Comparison of the experimental results with cohesive zone simulations suggests that the two buckle behaviors are associated with different levels of substrate yielding. In this presentation we will use the results to show how substrate compliance and deformation affect delamination and buckling of films on compliant substrates and provide a means to predict device performance.

  6. Buckle Driven Delamination in Thin Hard Film Compliant Substrate Systems

    Science.gov (United States)

    Moody, N. R.; Reedy, E. D.; Corona, E.; Adams, D. P.; Kennedy, M. S.; Cordill, M. J.; Bahr, D. F.

    2010-06-01

    behavior predicted by rigid elastic solutions. To address this issue we developed a finite element analysis technique that employed a cohesive zone model to simulate interfacial crack growth. Specifying the traction-separation relationship, cohesive strength, and work of separation along with film thickness, film stress, and film and substrate properties, buckle width and height were determined as a function of interfacial toughness. The simulations indicate that an analysis based on rigid substrate solutions significantly underestimate toughness for prescribed buckle widths: a result consistent with an analysis by Yu and Hutchinson [5] that pieced together a solution based on non-linear plate theory with a solution for the linear film on substrate problem. More importantly, the results defined a lower limiting bound to seemingly disparate buckle deflection data (Figure 2). The variance from linear elastic behavior, especially for the small buckles, indicates more than substrate compliance is controlling behavior. Comparison of the experimental results with cohesive zone simulations suggests that the two buckle behaviors are associated with different levels of substrate yielding. In this presentation we will use the results to show how substrate compliance and deformation affect delamination and buckling of films on compliant substrates and provide a means to predict device performance.

  7. The Delamination Theory of Wear

    Science.gov (United States)

    1974-09-01

    junctions, it is still based on the assumption that the deformation occurs at the asperities. Rabinowicz [14] advanced an adhesion theory of friction...shown that bronze particles were indeed bigger than steel particles. The compilation of wear particle sizes given by Rabinowicz [14] also indicates...Waterhouse [32] has shown that, in fact, fretting occurs by delamination. 6) Minimum Load for Loose Particle Formation Rabinowicz [14] found that no wear

  8. Dynamic fracture mechanics analysis for an edge delamination crack

    Science.gov (United States)

    Rizzi, Stephen A.; Doyle, James F.

    1994-01-01

    A global/local analysis is applied to the problem of a panel with an edge delamination crack subject to an impulse loading to ascertain the dynamic J integral. The approach uses the spectral element method to obtain the global dynamic response and local resultants to obtain the J integral. The variation of J integral along the crack front is shown. The crack behavior is mixed mode (Mode 2 and Mode 3), but is dominated by the Mode 2 behavior.

  9. Delaminated rotator cuff tear: extension of delamination and cuff integrity after arthroscopic rotator cuff repair.

    Science.gov (United States)

    Gwak, Heui-Chul; Kim, Chang-Wan; Kim, Jung-Han; Choo, Hye-Jeung; Sagong, Seung-Yeob; Shin, John

    2015-05-01

    The purpose of this study was to evaluate the extension of delamination and the cuff integrity after arthroscopic repair of delaminated rotator cuff tears. Sixty-five patients with delaminated rotator cuff tears were retrospectively reviewed. The delaminated tears were divided into full-thickness delaminated tears and partial-thickness delaminated tears. To evaluate the medial extension, we calculated the coronal size of the delaminated portion. To evaluate the posterior extension, we checked the tendon involved. Cuff integrity was evaluated by computed tomography arthrography. The mean medial extension in the full-thickness and partial-thickness delaminated tears was 18.1 ± 6.0 mm and 22.7 ± 6.3 mm, respectively (P = .0084). The posterior extension into the supraspinatus and the infraspinatus was 36.9% and 32.3%, respectively, in the full-thickness delaminated tears, and it was 27.7% and 3.1%, respectively, in the partial-thickness delaminated tears (P = .0043). With regard to cuff integrity, 35 cases of anatomic healing, 10 cases of partial healing defects, and 17 cases of retear were detected. Among the patients with retear and partial healing of the defect, all the partially healed defects showed delamination. Three retear patients showed delamination, and 14 retear patients did not show delamination; the difference was statistically significant (P = .0001). The full-thickness delaminated tears showed less medial extension and more posterior extension than the partial-thickness delaminated tears. Delamination did not develop in retear patients, but delamination was common in the patients with partially healed defects. Copyright © 2015 Journal of Shoulder and Elbow Surgery Board of Trustees. Published by Elsevier Inc. All rights reserved.

  10. Regional adaptive delaminating algorithm for rapid prototyping

    Institute of Scientific and Technical Information of China (English)

    CAI Daosheng; SHI Yusheng; HUANG Shuhuai

    2005-01-01

    With the development of rapid prototyping (RP) technology, the contradiction between fabricating speed and precision becomes more and more acute. In order to solve the contradiction, a regional effective adaptive delaminating algorithm is proposed in this paper. It is different from the traditional method that the regional adaptive delaminating method divides slicing contours into several regions and adaptively delaminates in respective region only according to the contours information. Namely, this method can not only adaptively delaminate at different height of CAD model but also adaptively delaminate different regions in one slicing layer. Furthermore, because the two-dimensional contour data adopted in this method are necessary for rapid prototyping system, this regional effective adaptive delaminating method is suitable for all RP systems. A comparative study is used to analyze the effectiveness of this method, which can demonstrate that this method can increase the fabricating speed and reduce the running cost under the condition of ensuring fabricating precision.

  11. Optimizing the delamination failure in bamboo fiber reinforced polyester composite

    Directory of Open Access Journals (Sweden)

    N. Abilash

    2016-01-01

    Full Text Available Delamination is represented to be the most prevalent failure in composite structures. The use of composites in the manufacturing sector plays a very important role in the industry in general. Moreover these materials have unique characteristics when analyzed separately from constituents which are a part of them. In this paper, a partially ecological composite was made, using natural fibers as reinforcement (bamboo fiber, in the polyester resin matrix to form a composite, seeking to improve the mechanical behavior among its class of materials. The characteristics of a composite material are determined by how it behaves while machining, Drilling is the most predominant machining process because of its cost effectiveness when compared with other processes. Obviously delamination is the major problem that is focused by many researchers while selecting drilling as the machining process in polymeric composites. This research mainly emphasizes on the critical parameters by varying its speed, feed, and diameter of the cutting tool, their contribution to delamination was analyzed. Reduced delaminations were identified by varying the speed and feed rate.

  12. Revisiting the Numerical Convergence of Cohesive-Zone Models in Simulating the Delamination of Composite Adhesive Joints by Using the Finite-Element Analysis

    Science.gov (United States)

    Liu, P. F.; Gu, Z. P.; Hu, Z. H.

    2016-11-01

    Delamination is the dominating failure mechanism in composite adhesive joints. A deep insight into the delamination failure mechanism requires advanced numerical methods. Currently, cohesive-zone models (CZMs), in combination with the finite-element analysis (FEA), have become powerful tools for modeling the initiation and growth of delaminations in composites. However, ensuring the numerical convergence in the CZMs used for a delamination analysis of three-dimensional (3D) composite structures is always a challenging issue due to the "snap-back" instability in the nonlinear implicit FEA, which arises mainly from the cohesive softening behavior. Based on the midplane interpolation technique, first numerical techniques for implementing 3D bilinear and exponential CZMs by using ABAQUS-UEL (user element subroutine) are developed in this paper. In particular, a viscous regularization by introducing the damping effect into the stiffness equation is used to improve the convergence. Two examples, a single-lap composite joint and a composite skin/stiffener panel under tension, demonstrate the numerical technique developed. Then, the effect of cohesion parameters on the numerical convergence based on the viscous regularization is studied.

  13. Mixed-Mode Decohesion Finite Elements for the Simulation of Delamination in Composite Materials

    Science.gov (United States)

    Camanho, Pedro P.; Davila, Carlos G.

    2002-01-01

    A new decohesion element with mixed-mode capability is proposed and demonstrated. The element is used at the interface between solid finite elements to model the initiation and non-self-similar growth of delaminations. A single relative displacement-based damage parameter is applied in a softening law to track the damage state of the interface and to prevent the restoration of the cohesive state during unloading. The softening law for mixed-mode delamination propagation can be applied to any mode interaction criterion such as the two-parameter power law or the three-parameter Benzeggagh-Kenane criterion. To demonstrate the accuracy of the predictions and the irreversibility capability of the constitutive law, steady-state delamination growth is simulated for quasistatic loading-unloading cycles of various single mode and mixed-mode delamination test specimens.

  14. Delamination of Compressed Thin Layers at Corners

    DEFF Research Database (Denmark)

    Sørensen, Kim D.; Jensen, Henrik Myhre; Clausen, Johan

    2008-01-01

    An analysis of delamination for a thin elastic layer under compression, attached to a substrate at a corner is carried out. The analysis is performed by combining results from interface fracture mechanics and the theory of thin shells. In contrast with earlier results for delamination on a flat...... layers, Fracture mechanics, Crack closure, Steady state crack propagation....

  15. Delamination of Compressed Thin Layers at Corners

    DEFF Research Database (Denmark)

    Sørensen, Kim Dalsten; Jensen, Henrik Myhre; Clausen, Johan

    2008-01-01

    An analysis of delamination for a thin elastic layer under compression, attached to a substrate at a corner is carried out. The analysis is performed by combining results from interface fracture mechanics and the theory of thin shells. In contrast with earlier results for delamination on a flat...

  16. Delamination Detection Using Guided Wave Phased Arrays

    Science.gov (United States)

    Tian, Zhenhua; Yu, Lingyu; Leckey, Cara

    2016-01-01

    This paper presents a method for detecting multiple delaminations in composite laminates using non-contact phased arrays. The phased arrays are implemented with a non-contact scanning laser Doppler vibrometer (SLDV). The array imaging algorithm is performed in the frequency domain where both the guided wave dispersion effect and direction dependent wave properties are considered. By using the non-contact SLDV array with a frequency domain imaging algorithm, an intensity image of the composite plate can be generated for delamination detection. For the proof of concept, a laboratory test is performed using a non-contact phased array to detect two delaminations (created through quasi-static impact test) at different locations in a composite plate. Using the non-contact phased array and frequency domain imaging, the two impact-induced delaminations are successfully detected. This study shows that the non-contact phased array method is a potentially effective method for rapid delamination inspection in large composite structures.

  17. Assembly induced delaminations in composite structures

    Science.gov (United States)

    Goering, J.; Bohlmann, R.; Wanthal, S.; Kautz, E.; Neri, Lawrence M.

    1992-01-01

    Experimental and analytical studies of the development of delaminations around fastener holes in composite structures are presented. This type of delamination is known to occur in composite skins that are mechanically fastened to a poorly mating substructure. Results of an experimental study to determine the resistance of laminates to the initiation of assembly induced delaminations and the residual strength of assembly damaged coupons are presented for AS4/3501-6, IM7/8551-7A, and AS4/PEEK material systems. A survey of existing analytical models for predicting the residual strength and stability of delaminations is presented, and the development of a new model for predicting the initiation of delaminations around a fastener hole is outlined. The fastener hole damage initiation model utilizes a finite element based Fourier series solution, and is validated through comparisons of analytical and experimental results.

  18. Dynamic buckling analysis of delaminated composite plates using semi-analytical finite strip method

    Science.gov (United States)

    Ovesy, H. R.; Totounferoush, A.; Ghannadpour, S. A. M.

    2015-05-01

    The delamination phenomena can become of paramount importance when the design of the composite plates is concerned. In the current study, the effect of through-the-width delamination on dynamic buckling behavior of a composite plate is studied by implementing semi-analytical finite strip method. In this method, the energy and work integrations are computed analytically due to the implementation of trigonometric functions. Moreover, the method can lead to converged results with comparatively small number of degrees of freedom. These features have made the method quite efficient. To account for delamination effects, displacement field is enriched by adding appropriate terms. Also, the penetration of the delamination surfaces is prevented by incorporating an appropriate contact scheme into the time response analysis. Some selected results are validated against those available in the literature.

  19. Guidelines and Parameter Selection for the Simulation of Progressive Delamination

    Science.gov (United States)

    Song, Kyongchan; Davila, Carlos G.; Rose, Cheryl A.

    2008-01-01

    Turon s methodology for determining optimal analysis parameters for the simulation of progressive delamination is reviewed. Recommended procedures for determining analysis parameters for efficient delamination growth predictions using the Abaqus/Standard cohesive element and relatively coarse meshes are provided for single and mixed-mode loading. The Abaqus cohesive element, COH3D8, and a user-defined cohesive element are used to develop finite element models of the double cantilever beam specimen, the end-notched flexure specimen, and the mixed-mode bending specimen to simulate progressive delamination growth in Mode I, Mode II, and mixed-mode fracture, respectively. The predicted responses are compared with their analytical solutions. The results show that for single-mode fracture, the predicted responses obtained with the Abaqus cohesive element correlate well with the analytical solutions. For mixed-mode fracture, it was found that the response predicted using COH3D8 elements depends on the damage evolution criterion that is used. The energy-based criterion overpredicts the peak loads and load-deflection response. The results predicted using a tabulated form of the BK criterion correlate well with the analytical solution and with the results predicted with the user-written element.

  20. Delamination Growth in Composites under Fatigue Loading

    NARCIS (Netherlands)

    Khan, R.

    2013-01-01

    Fiber reinforced composites are attractive for aerospace applications due to high specific strength and stiffness. Their use has been gradually increased to 50% by weight of the aircraft over past decades. As a consequence, modern aircraft utilize composites in the primary structures like wing skin

  1. Delamination Growth in Composites under Fatigue Loading

    NARCIS (Netherlands)

    Khan, R.

    2013-01-01

    Fiber reinforced composites are attractive for aerospace applications due to high specific strength and stiffness. Their use has been gradually increased to 50% by weight of the aircraft over past decades. As a consequence, modern aircraft utilize composites in the primary structures like wing skin

  2. Combined effect of matrix cracking and stress-free edge on delamination

    Science.gov (United States)

    Salpekar, S. A.; Obrien, T. K.

    1990-01-01

    The effect of the stress-free edge on the growth of local delaminations initiating from a matrix crack in (0 sub 2/90 sub 4) sub s and (+ or - 45.90 sub 4) sub s glass epoxy laminates is investigated using 3-D finite element analysis. The presence of high interlaminar normal stresses at the intersection (corner) of the matrix crack with the stress-free edge, suggests that a mode I delamination may initiate at the corners. The strain energy release rates (G) were calculated by modeling a uniform through-width delamination and two inclined delaminations at 10.6 deg and 45 deg to the matrix crack. All components of G have high values near the free edges. The mode I component of G is high at small delamination length and becomes zero for a delamination length of one-ply thickness. The total G values near the free edge agreed well with previously derived closed form solution. The quasi-3D solutions agreed well with the 3-D interior solutions.

  3. A Test for Characterizing Delamination Migration in Carbon/Epoxy Tape Laminates

    Science.gov (United States)

    Ratcliffe, James G.; Czabaj, Michael W.; O'Brien, Thomas K.

    2013-01-01

    A new test method is presented for the purpose of investigating migration of a delamination between neighboring ply interfaces in fiber-reinforced, polymer matrix tape laminates. The test is a single cantilever beam configuration consisting of a cross-ply laminate with a polytetrafluoroethylene insert implanted at the mid-plane and spanning part way along the length of the specimen. The insert is located between a 0- degree ply (specimen length direction) and a stack of four 90-degree plies (specimen width direction). The specimen is clamped at both ends onto a rigid baseplate and is loaded on its upper surface via a piano hinge. Tests were conducted with the load-application point located on the intact portion of the specimen in order to initiate delamination growth onset followed by migration of the delamination to a neighboring 90/0 ply interface by kinking through the 90-degree ply stack. Varying this position was found to affect the distance relative to the load-application point at which migration initiated. In each specimen, migration initiated by a gradual transition of the delamination at the 0/90 interface into the 90-degree ply stack. In contrast, transition of the kinked crack into the 90/0 interface was sudden. Fractography of the specimens indicated that delamination prior to migration was generally mixed mode-I/II. Inspection of the kink surface revealed mode-I fracture. In general, use of this test allows for the observation of the growth of a delamination followed by migration of the delamination to another ply interface, and should thus provide a means for validating analyses aimed at simulating migration.

  4. Internal-Notched Flexure Test for Measurement of Mode II Delamination Resistance of Fibre-Reinforced Polymers

    Directory of Open Access Journals (Sweden)

    Chengye Fan

    2013-01-01

    Full Text Available This paper introduces a new test, method, named internal-notched flexure (INF test, that is designed to measure the critical energy release rate of fibre-reinforced polymers for delamination growth in shear mode (mode II. The INF test generates stable delamination growth, with a monotonic increase of load and displacement in a nearly linear fashion. Values of the mode II delamination toughness were deduced using experimental compliance fitting method. Good repeatability of the results was obtained. Compared with the end-notched flexure (ENF test using the same material, the INF test yielded higher delamination resistance, possibly due to the bridging fibres found between fracture surfaces of the INF test specimens.

  5. Orogenic delamination - dynamics, effects, and geological expression

    Science.gov (United States)

    Ueda, Kosuke; Gerya, Taras

    2010-05-01

    Unbundling of continental lithosphere and removal of its mantle portion have been described by two mutually rather exclusive models, convective thinning and integral delamination. Either disburdens the remaining lithosphere, weakens the remainder, and causes uplift and extension. Increased heat flux is likely to promote high-degree crustal melting, and has been viewed as a source for voluminous granitic intrusions in late or collapsing orogenic settings. Collapse may be driven by any of gravitational potential differences from orogen to foreland, by stress inversion in the unburdened domain, or by suction of a retreating trench. In this study, we investigate prerequisites, mechanism, and development paths for orogeny-related mantle lithosphere removal. Our experiments numerically reproduce delamination which self-consistently results from the dynamics of a decoupling collision zone. In particular, it succeeds without a seed facilitating initial separation of layers. External shortening of a continent - ocean - continent assembly, such as to initiate oceanic subduction, is lifted before the whole oceanic part is consumed, leaving slab pull to govern further convergence. Once buoyant continental crust enters, the collision zone locks, and convergence diminishes. Under favourable conditions, delamination then initiates close to the edge of the mantle wedge and at deep crustal levels. While it initially separates upper crust from lower crust according to the weakness minimum in the lithospheric strength profile, the lower crust is eventually also delaminated from the subducting lithospheric mantle, owing to buoyancy differences. The level of delamination within the lithosphere seems thus first rheology-controlled, then density-controlled. Subduction-coupled delamination is contingent on retreat and decoupling of the subducting slab, which in turn is dependent on effective rheological weakening of the plate contact. Weakening is a function of shear-heating and hereby of

  6. An automated dynamic fracture procedure and a continuum damage mechanics based model for finite element simulations of delamination failure in laminated composites

    Science.gov (United States)

    Aminjikarai Vedagiri, Srinivasa Babu

    An active field of research that has developed due to the increasing use of computational techniques like finite element simulations for analysis of highly complex structural mechanics problems and the increasing use of composite laminates in varied industries such as aerospace, automotive, bio-medical, etc. is the development of numerical models to capture the behavior of composite materials. One of the big challenges not yet overcome convincingly in this field is the modeling of delamination failure which is one of the primary modes of damage in composite laminates. Hence, the primary aim of this work is to develop two numerical models for finite element simulations of delamination failure in composite laminates and implement them in the explicit finite element software DYNA3D/LS-DYNA. Dynamic fracture mechanics is an example of a complex structural analysis problem for which finite element simulations seem to be the only possible way to extract detailed information on sophisticated physical quantities of the crack-tip at any instant of time along a highly transient history of fracture. However, general purpose, commercial finite element software which have capabilities to do fracture analyses are still limited in their use to stationary cracks and crack propagation along trajectories known a priori. Therefore, an automated dynamic fracture procedure capable of simulating dynamic propagation of through-thickness cracks in arbitrary directions in linear, isotropic materials without user-intervention is first developed and implemented in DYNA3D for its default 8-node solid (brick) element. Dynamic energy release rate and stress intensity factors are computed in the model using integral expressions particularly well-suited for the finite element method. Energy approach is used to check for crack propagation and the maximum circumferential stress criterion is used to determine the direction of crack growth. Since the re-meshing strategy used to model crack growth

  7. Crystal Growth Behaviors of Silicon during Melt Growth Processes

    Directory of Open Access Journals (Sweden)

    Kozo Fujiwara

    2012-01-01

    Full Text Available It is imperative to improve the crystal quality of Si multicrystal ingots grown by casting because they are widely used for solar cells in the present and will probably expand their use in the future. Fine control of macro- and microstructures, grain size, grain orientation, grain boundaries, dislocation/subgrain boundaries, and impurities, in a Si multicrystal ingot, is therefore necessary. Understanding crystal growth mechanisms in melt growth processes is thus crucial for developing a good technology for producing high-quality Si multicrystal ingots for solar cells. In this review, crystal growth mechanisms involving the morphological transformation of the crystal-melt interface, grain boundary formation, parallel-twin formation, and faceted dendrite growth are discussed on the basis of the experimental results of in situ observations.

  8. Problem of Delamination in RC Beams Strengthened by FRP with Rheological Model of Adhesive Leyer

    Science.gov (United States)

    Kula, Krzysztof; Socha, Tomasz

    2016-12-01

    This paper deals with one of the most dangerous failure modes in layered structures, namely delamination. The strengthening layer is modelled by a solid-shell finite element. The mechanical modelling of delamination onset and propagation is based upon a cohesive zone model implemented into a cohesive element located between adhesive layer and a concrete structure. The long time behavior of epoxy adhesive layer is modelled with the five-parameter rheological model. The numerical simulations are accomplished within the commercial software package Abaqus by the implementation of a user-written finite element and user-written material.

  9. Delamination detection using methods of computational intelligence

    Science.gov (United States)

    Ihesiulor, Obinna K.; Shankar, Krishna; Zhang, Zhifang; Ray, Tapabrata

    2012-11-01

    Abstract Reliable delamination prediction scheme is indispensable in order to prevent potential risks of catastrophic failures in composite structures. The existence of delaminations changes the vibration characteristics of composite laminates and hence such indicators can be used to quantify the health characteristics of laminates. An approach for online health monitoring of in-service composite laminates is presented in this paper that relies on methods based on computational intelligence. Typical changes in the observed vibration characteristics (i.e. change in natural frequencies) are considered as inputs to identify the existence, location and magnitude of delaminations. The performance of the proposed approach is demonstrated using numerical models of composite laminates. Since this identification problem essentially involves the solution of an optimization problem, the use of finite element (FE) methods as the underlying tool for analysis turns out to be computationally expensive. A surrogate assisted optimization approach is hence introduced to contain the computational time within affordable limits. An artificial neural network (ANN) model with Bayesian regularization is used as the underlying approximation scheme while an improved rate of convergence is achieved using a memetic algorithm. However, building of ANN surrogate models usually requires large training datasets. K-means clustering is effectively employed to reduce the size of datasets. ANN is also used via inverse modeling to determine the position, size and location of delaminations using changes in measured natural frequencies. The results clearly highlight the efficiency and the robustness of the approach.

  10. Delamination of Compressed thin Layers at Corners

    DEFF Research Database (Denmark)

    Clausen, Johan; Jensen, Henrik Myhre; Sørensen, Kim Dalsten

    2008-01-01

    An analysis of delamination for a thin elastic film, attached to a substrate with a corner, is carried out. The film is in compression and the analysis is performed by combining results from fracture mechanics and the theory of thin shells. The results show a very strong dependency of the angle...

  11. Failure and Delamination in Microelectronic Packages

    NARCIS (Netherlands)

    Sadeghinia, M.

    2013-01-01

    Thin layers of dissimilar materials are used in most microelectronic components in order to achieve special functional requirements. Generally, the interface between two adjacent materials forms a weak link, not only because of the relatively low delamination strength, but also because of the existi

  12. Bending strength of delaminated aerospace composites.

    Science.gov (United States)

    Kinawy, Moustafa; Butler, Richard; Hunt, Giles W

    2012-04-28

    Buckling-driven delamination is considered among the most critical failure modes in composite laminates. This paper examines the propagation of delaminations in a beam under pure bending. A pre-developed analytical model to predict the critical buckling moment of a thin sub-laminate is extended to account for propagation prediction, using mixed-mode fracture analysis. Fractography analysis is performed to distinguish between mode I and mode II contributions to the final failure of specimens. Comparison between experimental results and analysis shows agreement to within 5 per cent in static propagation moment for two different materials. It is concluded that static fracture is almost entirely driven by mode II effects. This result was unexpected because it arises from a buckling mode that opens the delamination. For this reason, and because of the excellent repeatability of the experiments, the method of testing may be a promising means of establishing the critical value of mode II fracture toughness, G(IIC), of the material. Fatigue testing on similar samples showed that buckled delamination resulted in a fatigue threshold that was over 80 per cent lower than the static propagation moment. Such an outcome highlights the significance of predicting snap-buckling moment and subsequent propagation for design purposes.

  13. Mechanisms governing the interfacial delamination of thermal barrier coating system with double ceramic layers

    Science.gov (United States)

    Xu, Rong; Fan, Xueling; Wang, T. J.

    2016-05-01

    A systematic study of factors affecting the interfacial delamination of thermal barrier coating system (TBCs) with double ceramic layers (DCL) is presented. Crack driving forces for delaminations at two weak interfaces are examined. The results show that a thicker outermost ceramic layer can induce dramatic increase in crack driving force and make the interface between two ceramic coatings become more prone to delamination. The behavior is shown to be more prominent in TBCs with stiffer outmost coating. The thickness ratio of two ceramic layers is an important parameter for controlling the failure mechanisms and determining the lifetime of DCL TBCs under inservice condition. By accounting for the influences of thickness ratio of two ceramic layers and interfacial fracture toughnesses of two involved interfaces, the fracture mechanism map of DCL TBCs has been constructed, in which different failure mechanisms are identified. The results quanlitatively agree with the aviliable experimental data.

  14. Behavior analysis and the growth of behavioral pharmacology.

    Science.gov (United States)

    Laties, Victor G

    2003-01-01

    Psychologists, particularly those influenced by the work of B. F. Skinner, played a major part in the development of behavioral pharmacology in the 1950s and 1960s. Revolutionary changes in pharmacology and psychiatry, including the discovery of powerful therapeutic agents such as chlorpromazine and reserpine, had produced a surge of interest in drug research. Pharmaceutical companies began hiring psychologists with operant conditioning backgrounds so as to compete successfully in the search for new drugs. Psychologists, most of whom were skilled in the behavior-analytic approach, started to assume prominent positions as authors and editors for the Journal of Pharmacology and Experimental Therapeutics as its emphasis on behavior increased. This also proved true with the other publications founded to deal with the popularity of behavioral pharmacology. Especially important were contributions by B. F. Skinner, Peter B. Dews, and Joseph V. Brady.

  15. Enhancement of delamination strength in Cu-stabilized coated conductor tapes through additional treatments under transverse tension at room temperature

    Energy Technology Data Exchange (ETDEWEB)

    Shin, Hyung Seop; Bautista, Zhierwinjay [Andong National University, Andong (Korea, Republic of); Moon, Seung Hyun; Lee, Jae Hun; Mean, Byoung Jean [SuNAM Co Ltd., Anseong (Korea, Republic of)

    2017-06-15

    In superconducting coil applications particularly in wet wound coils, coated conductor (CC) tapes are subjected to different type of stresses that could affect its electromechanical transport property. These include hoop stress acting along the length of the CC tape and the Lorentz force acting perpendicular to the CC tape’s surface. Since the latter is commonly associated with the delamination problem of multi-layered REBCO CC tapes, more understanding and attention on the delamination phenomena induced in the case of coil applications are needed. Difference on the coefficient of thermal expansion (CTE) of each constituent layer of the CC tape, the bobbin, and the impregnating materials is the main causes of delamination in CC tapes when subjected to thermal and mechanical cycling. In the design of degradation-free superconducting coils, therefore, characterization of the delamination behaviors including mechanism and strength in the multi-layered REBCO CC tapes becomes a critical issue. Various trials to increase the delamination strength by improving interface characteristics at interlayers have been performed. In this study, in order to investigate the influences of laser cleaning and Ag annealing treated at the substrate side surface, transverse tensile tests were conducted under different sample configurations using 4.5mm x 8 mm upper anvil. The mechanical delamination strength of differently processed CC samples was examined at room temperature (RT). As a result, the Sample 1 with the additional laser cleaning and Ag annealing processes and the Sample 2 with additional Ag annealing process only showed higher mechanical delamination strength as compared to the Sample 3 without such additional treatments. Sample 3 showed quite different behavior when the loading direction is to the substrate side where the delamination strength much lower as compared to other cases.

  16. Influence of substrate topography on cathodic delamination of anticorrosive coatings

    DEFF Research Database (Denmark)

    Sørensen, Per Aggerholm; Kiil, Søren; Dam-Johansen, Kim

    2009-01-01

    The cathodic delamination of a commercial magnesium silicate and titanium dioxide pigmented epoxy coating on abrasive cleaned cold rolled steel has been investigated. The rate of delamination was found to depend on interfacial transport from the artificial defect to the delamination front...... and thereby the substrate topography, whereas the coating thickness had little influence. The presence of a significant potential gradient between the anode and the cathode and the dependency of the delamination rate on the tortuosity of the steel surface suggests that cathodic delamination is controlled...... by migration of cations from the defect to the delamination front. This means that abrasive blasting, to some extent, can be applied to control and minimize the observed rate of cathodic delamination. The lifetime of the species causing disbondment suggested that sodium hydroxide or potassium hydroxide...

  17. Behavior analysis and the growth of behavioral pharmacology

    OpenAIRE

    Laties, Victor G.

    2003-01-01

    Psychologists, particularly those influenced by the work of B. F. Skinner, played a major part in the development of behavioral pharmacology in the 1950s and 1960s. Revolutionary changes in pharmacology and psychiatry, including the discovery of powerful therapeutic agents such as chlorpromazine and reserpine, had produced a surge of interest in drug research. Pharmaceutical companies began hiring psychologists with operant conditioning backgrounds so as to compete successfully in the search ...

  18. Middle Archean continent formation by crustal delamination

    Science.gov (United States)

    Zegers, Tanja E.; van Keken, Peter E.

    2001-12-01

    The processes that created the first large cratonic areas such as the Pilbara and the Kaapvaal remain poorly understood. Models based on the uniformitarian extrapolation of present-day arc volcanic processes to a hotter early Earth have not adequately explained the observations in these terranes. Here we propose an alternative mechanism for the formation of the earliest continental crust. The formation of continental crust may be achieved by delamination of the lower eclogitic part of an oceanic plateau like protocrust. Such delamination results in uplift, extension, and the production of tonalite, trondhjemite, and granodiorite (TTG) suites as recorded in Middle Archean cratons. The available geologic and geophysical observations in combination with model calculations permit this scenario as an alternative to subduction-based hypotheses.

  19. Fiber Optic Thermal Detection of Composite Delaminations

    Science.gov (United States)

    Wu, Meng-Chou; Winfree, William P.

    2011-01-01

    A recently developed technique is presented for thermographic detection of delaminations in composites by performing temperature measurements with fiber optic Bragg gratings. A single optical fiber with multiple Bragg gratings employed as surface temperature sensors was bonded to the surface of a composite with subsurface defects. The investigated structure was a 10-ply composite specimen with prefabricated delaminations of various sizes and depths. Both during and following the application of a thermal heat flux to the surface, the individual Bragg grating sensors measured the temporal and spatial temperature variations. The data obtained from grating sensors were analyzed with thermal modeling techniques of conventional thermography to reveal particular characteristics of the interested areas. Results were compared and found to be consistent with the calculations using numerical simulation techniques. Also discussed are methods including various heating sources and patterns, and their limitations for performing in-situ structural health monitoring.

  20. Delamination-Indicating Thermal Barrier Coatings

    Science.gov (United States)

    Eldridge, Jeffrey I.

    2007-01-01

    The risk of premature failure of thermal barrier coatings (TBCs), typically composed of yttria-stabilized zirconia (YSZ), compromises the reliability of TBCs used to provide thermal protection for turbine engine components. Unfortunately, TBC delamination proceeds well beneath the TBC surface and cannot be monitored by visible inspection. Nondestructive diagnostic tools that could reliably probe the subsurface damage state of TBCs would alleviate the risk of TBC premature failure by indicating when the TBC needs to be replaced before the level of TBC damage threatens engine performance or safety. To meet this need, a new coating design for thermal barrier coatings (TBCs) that are self-indicating for delamination has been successfully implemented by incorporating a europium-doped luminescent sublayer at the base of a TBC composed of YSZ. The luminescent sublayer has the same YSZ composition as the rest of the TBC except for the addition of low-level europium doping and therefore does not alter TBC performance.

  1. DELAMINATION FORMATION AND DELAMINATION PROPAGATION OF COMPOSITE LAMINATES UNDER COMPRESSIVE FATIGUE LOADING

    Institute of Scientific and Technical Information of China (English)

    2000-01-01

    Fatigue tests of the smooth composite laminates and the notched composite laminates under compressive cyclic loading have been carried out. The damage mechanism is discussed and analyzed. Damage evolution is monitored using stiffness decay. From these tests, it is found that the initial delamination occurs at the free boundary of smooth specimens, or the notch boundary of notched specimens, subjected to the compression-compression cyclic load. A point of view in relation to two-phases of compression fatigue delamination of composites is proposed, namely, compression-compression delamination consists of the delamination formation phase and the delamination propagation, and there is a "damage transition point" to separate this two-phases. Furthermore, an empirical modulus degradation formula and its parameters fitting method are presented. According to the test data handling results, it is shown that this formula is univocal and can fit the test data conveniently. In addition, two kinds of new anti-buckling devices are designed for these tests. At last, the E-N curves, the D-N curves and the S-N curve of the smooth carbon fiber reinforced composite laminates of T300/648C are determined to predict the fatigue life of the notched composite laminate. And the E-N curve of the notched specimens at the given load ratio R=10 and minimum load P min=-0.45 kN is also measured to verify the estimated result of fatigue life.

  2. Compressive strength of delaminated aerospace composites.

    Science.gov (United States)

    Butler, Richard; Rhead, Andrew T; Liu, Wenli; Kontis, Nikolaos

    2012-04-28

    An efficient analytical model is described which predicts the value of compressive strain below which buckle-driven propagation of delaminations in aerospace composites will not occur. An extension of this efficient strip model which accounts for propagation transverse to the direction of applied compression is derived. In order to provide validation for the strip model a number of laminates were artificially delaminated producing a range of thin anisotropic sub-laminates made up of 0°, ±45° and 90° plies that displayed varied buckling and delamination propagation phenomena. These laminates were subsequently subject to experimental compression testing and nonlinear finite element analysis (FEA) using cohesive elements. Comparison of strip model results with those from experiments indicates that the model can conservatively predict the strain at which propagation occurs to within 10 per cent of experimental values provided (i) the thin-film assumption made in the modelling methodology holds and (ii) full elastic coupling effects do not play a significant role in the post-buckling of the sub-laminate. With such provision, the model was more accurate and produced fewer non-conservative results than FEA. The accuracy and efficiency of the model make it well suited to application in optimum ply-stacking algorithms to maximize laminate strength.

  3. Delamination-Debond Behaviour of Composite T- Joints in Wind Turbine Blades

    Science.gov (United States)

    Gulasik, H.; Coker, D.

    2014-06-01

    Wind turbine industry utilizes composite materials in turbine blade structural designs because of their high strength/stiffness to weight ratio. T-joint is one of the design configurations of composite wind turbine blades. T-joints consist of a skin panel and a stiffener co-bonded or co-cured together with a filler material between them. T-joints are prone to delaminations between skin/stiffener plies and debonds between skin-stiffener-filler interfaces. In this study, delamination/debond behavior of a co-bonded composite T-joint is investigated under 0° pull load condition by 2D finite element method. Using Abaqus® commercial FE software, zero-thickness cohesive elements are used to simulate delamination/debond in ply interfaces and bonding lines. Pulling load at 0° is applied and load-displacement behavior and failure scenario are observed. The failure sequence consists of debonding of filler/stringer interface during one load drop followed by a second drop in which the 2nd filler/stringer debonds, filler/skin debonding and skin delamination leading to total loss of load carrying capacity. This type of failure initiation has been observed widely in the literature. When the debond strength is increased 30%, failure pattern is found to change in addition to increasing the load capacity by 200% before total loss of loading carrying capacity occurs. Failure initiation and propagation behavior, initial and max failure loads and stress fields are affected by the property change. In all cases mixed-mode crack tip loading is observed in the failure initiation and propagation stages. In this paper, the detailed delamination/debonding history in T-joints is predicted with cohesive elements for the first time.

  4. Growth-dependent behavioral difference in bacterial chemotaxis

    Science.gov (United States)

    Zhang, Chi; Zhang, Rongjing; Yuan, Junhua

    2017-06-01

    Cells can adjust to their growth environments and regulate their behavior accordingly. To study how cells accomplish this growth-dependent adjustment from the molecular to the behavioral level, we used bacterial chemotaxis as a model system to explore the behavioral difference for bacteria grown in nutrient-rich and nutrient-poor media. We found that bacteria grown in a nutrient-poor medium exhibit faster chemotaxis adaptation, and this enables them to respond more rapidly to a changing environment and increases their ability to localize to a nutrient concentration peak. We identified the molecular mechanisms behind this behavioral difference through coarse-grained modeling, and demonstrated its physiological consequences by simulating bacterial chemotactic motion in spatiotemporally varying environments and in a static environment with a nutrient concentration peak.

  5. Grain Growth Behavior in Sintered Nd-Fe-B Magnets

    Institute of Scientific and Technical Information of China (English)

    Liu Xianglian; Zhou Shouzeng

    2007-01-01

    The Nd2Fe14B grain growth behavior in sintered Nd-Fe-B magnets was quantitatively described. The effects of sintering temperature and time, and alloy powder size and its distribution on grain growth process were analyzed. Hence, possible grain growth mechanisms in these magnets were qualitatively discussed. The Nd2Fe14B grain growth proceeded at quite a high rate in the initial 0~1 h of sintering and from then onwards the grain growth rate decreased. A large average particle size or a wide particle size distribution of initial alloy powders was found to remarkably accelerate the grain growth process and even result in the occurrence of abnormal grain growth. On the basis of experimental results, two grain growth mechanisms were considered to operate during sintering of Nd-Fe-B magnets, that is, dissolution and re-precipitation of Nd2Fe14B particles, and Nd2Fe14B particle growth by coalescence. It was believed that Nd2Fe14B particle growth by coalescence not only produced a large average grain size and a wide grain size distribution, but also was the fundamental reason for the formation of abnormally large grains in the microstructure of sintered Nd-Fe-B magnets.

  6. Monitoring Delamination of Thermal Barrier Coatings During Interrupted High-Heat-Flux Laser Testing using Luminescence Imaging

    Science.gov (United States)

    Eldridge, Jeffrey I.; Zhu, Dongming; Wolfe, Douglas E.

    2011-01-01

    This presentation showed progress made in extending luminescence-base delamination monitoring to TBCs exposed to high heat fluxes, which is an environment that much better simulates actual turbine engine conditions. This was done by performing upconversion luminescence imaging during interruptions in laser testing, where a high-power CO2 laser was employed to create the desired heat flux. Upconverison luminescence refers to luminescence where the emission is at a higher energy (shorter wavelength) than the excitation. Since there will be negligible background emission at higher energies than the excitation, this methods produces superb contrast. Delamination contrast is produced because both the excitation and emission wavelengths are reflected at delamination cracks so that substantially higher luminescence intensity is observed in regions containing delamination cracks. Erbium was selected as the dopant for luminescence specifically because it exhibits upconversion luminescence. The high power CO2 10.6 micron wavelength laser facility at NASA GRC was used to produce the heat flux in combination with forced air backside cooling. Testing was performed at a lower (95 W/sq cm) and higher (125 W/sq cm) heat flux as well as furnace cycling at 1163C for comparison. The lower heat flux showed the same general behavior as furnace cycling, a gradual, "spotty" increase in luminescence associated with debond progression; however, a significant difference was a pronounced incubation period followed by acceleration delamination progression. These results indicate that extrapolating behavior from furnace cycling measurements will grossly overestimate remaining life under high heat flux conditions. The higher heat flux results were not only accelerated, but much different in character. Extreme bond coat rumpling occurred, and delamination propagation extended over much larger areas before precipitating macroscopic TBC failure. This indicates that under the higher heat flux (and

  7. Effect of oxidation on delamination of ultrahigh-molecular-weight polyethylene tibial components.

    Science.gov (United States)

    Bell, C J; Walker, P S; Abeysundera, M R; Simmons, J M; King, P M; Blunn, G W

    1998-04-01

    Whether oxidation of ultrahigh-molecular-weight polyethylene (UHMWPE) causes delamination of the plastic in total knee arthroplasties (TKAs) was investigated. Examination of retrieved TKAs has shown that oxidation of UHMWPE can be caused by postirradiation damage leading to a subsurface band or, to a lesser extent, by mechanical forces during use leading to surface oxidation. Delamination cracks propagated through the subsurface oxidized band. In wear tests, delamination occurred in artificially aged UHMWPE where only subsurface oxidized bands had formed. Increased surface wear predominated where oxidation was associated with the surface of the plastic. Similarly, in tensile and fatigue tests of oxidized UHMWPE, there was a significant reduction in the ultimate tensile strength and in the fatigue resistance of specimens that had developed a subsurface band. Oxidation increased fatigue crack growth rate. It was observed that UHMWPE from different manufacturers varied in its resistance to oxidation. This study demonstrates that the effect of oxidation, which results in the development of a subsurface white band, combined with high subsurface shear forces observed in TKAs, is to enhance delamination wear.

  8. Development and Applications of Benchmark Examples for Static Delamination Propagation Predictions

    Science.gov (United States)

    Krueger, Ronald

    2013-01-01

    The development and application of benchmark examples for the assessment of quasistatic delamination propagation capabilities was demonstrated for ANSYS (TradeMark) and Abaqus/Standard (TradeMark). The examples selected were based on finite element models of Double Cantilever Beam (DCB) and Mixed-Mode Bending (MMB) specimens. First, quasi-static benchmark results were created based on an approach developed previously. Second, the delamination was allowed to propagate under quasi-static loading from its initial location using the automated procedure implemented in ANSYS (TradeMark) and Abaqus/Standard (TradeMark). Input control parameters were varied to study the effect on the computed delamination propagation. Overall, the benchmarking procedure proved valuable by highlighting the issues associated with choosing the appropriate input parameters for the VCCT implementations in ANSYS® and Abaqus/Standard®. However, further assessment for mixed-mode delamination fatigue onset and growth is required. Additionally studies should include the assessment of the propagation capabilities in more complex specimens and on a structural level.

  9. FINITE ELEMENT IMPLEMENTATION OF DELAMINATION IN COMPOSITE PLATES

    Directory of Open Access Journals (Sweden)

    Milan Žmindák

    2012-12-01

    Full Text Available Modelling of composite structures by finite element (FE codes to effectively model certain critical failure modes such as delamination is limited. Previous efforts to model delamination and debonding failure modes using FE codes have typically relied on ad hoc failure criteria and quasi-static fracture data. Improvements to these modelling procedures can be made by using an approach based on fracture mechanics. A study of modelling delamination using the finite element code ANSYS was conducted. This investigation demonstrates the modelling of composites through improved delamination modelling. Further developments to this approach may be improved.

  10. Subduction to Continental Delamination: Insights From Laboratory Experiments

    Science.gov (United States)

    Gogus, O. H.; Corbi, F.; Faccenna, C.; Pysklywec, R. N.

    2009-05-01

    The evolution of the lithosphere through subduction-collision and delamination and its surface/crustal response (topography/deformation) is investigated in this work. We present a series of lithosphere scale two dimensional (2-D) and three dimensional (3-D) laboratory experiments to better understand such processes. In these experiments, an idealized viscously deforming crust-mantle lithosphere-mantle system is configured with silicone putty (representing lithospheric mantle and upper crust) and glucose syrup (representing the upper mantle and lower crust). The initial focus was to investigate the physical development of delamination versus continental subduction without plate convergence. Experiments show that the delamination or continental subduction is strongly dependent on the density of the crust (both crust and mantle lithosphere subducts when crust has a higher density, instead of delamination), while in the investigated range, the viscosity of the weak layer does not have much influence on the process. In all the experiments, the topography is asymmetric with subsidence above the delaminating hinge due to the dynamic vertical pulling driven by the delaminating slab, and uplift above the delaminated region due to the buoyancy of asthenosphere. Our investigation on the oceanic subduction with a convergence rate of ~ 3cm/year plate velocity suggests that subduction -collision - delamination is well defined and at the end, the delaminating crust from the lithosphere is overthrusted on top of the overriding plate. Our results provide integrated insights on the Alpine-Himalayan type orogenies, in particular the neotectonic evolution of Eastern Anatolian plateau.

  11. Sensing delamination in epoxy encapsulant systems with fiber Bragg gratings

    Science.gov (United States)

    Jones, Brad H.; Rohr, Garth D.; Kaczmarowski, Amy K.

    2016-05-01

    Fiber Bragg gratings (FBGs) are well-suited for embedded sensing of interfacial phenomena in materials systems, due to the sensitivity of their spectral response to locally non-uniform strain fields. Over the last 15 years, FBGs have been successfully employed to sense delamination at interfaces, with a clear emphasis on planar events induced by transverse cracks in fiber-reinforced plastic laminates. We have built upon this work by utilizing FBGs to detect circular delamination events at the interface between epoxy films and alumina substrates. Two different delamination processes are examined, based on stress relief induced by indentation of the epoxy film or by cooling to low temperature. We have characterized the spectral response pre- and post-delamination for both simple and chirped FBGs as a function of delamination size. We show that delamination is readily detected by the evolution of a non-uniform strain distribution along the fiber axis that persists after the stressing condition is removed. These residual strain distributions differ substantially between the delamination processes, with indentation and cooling producing predominantly tensile and compressive strain, respectively, that are well-captured by Gaussian profiles. More importantly, we observe a strong correlation between spectrally-derived measurements, such as spectral widths, and delamination size. Our results further highlight the unique capabilities of FBGs as diagnostic tools for sensing delamination in materials systems.

  12. Guided Wave Delamination Detection and Quantification With Wavefield Data Analysis

    Science.gov (United States)

    Tian, Zhenhua; Campbell Leckey, Cara A.; Seebo, Jeffrey P.; Yu, Lingyu

    2014-01-01

    Unexpected damage can occur in aerospace composites due to impact events or material stress during off-nominal loading events. In particular, laminated composites are susceptible to delamination damage due to weak transverse tensile and inter-laminar shear strengths. Developments of reliable and quantitative techniques to detect delamination damage in laminated composites are imperative for safe and functional optimally-designed next-generation composite structures. In this paper, we investigate guided wave interactions with delamination damage and develop quantification algorithms by using wavefield data analysis. The trapped guided waves in the delamination region are observed from the wavefield data and further quantitatively interpreted by using different wavenumber analysis methods. The frequency-wavenumber representation of the wavefield shows that new wavenumbers are present and correlate to trapped waves in the damage region. These new wavenumbers are used to detect and quantify the delamination damage through the wavenumber analysis, which can show how the wavenumber changes as a function of wave propagation distance. The location and spatial duration of the new wavenumbers can be identified, providing a useful means not only for detecting the presence of delamination damage but also allowing for estimation of the delamination size. Our method has been applied to detect and quantify real delamination damage with complex geometry (grown using a quasi-static indentation technique). The detection and quantification results show the location, size, and shape of the delamination damage.

  13. Phase transitions in tumor growth: III vascular and metastasis behavior

    Science.gov (United States)

    Llanos-Pérez, J. A.; Betancourt-Mar, J. A.; Cocho, G.; Mansilla, R.; Nieto-Villar, José Manuel

    2016-11-01

    We propose a mechanism for avascular, vascular and metastasis tumor growth based on a chemical network model. Vascular growth and metastasis, appear as a hard phase transition type, as "first order", through a supercritical Andronov-Hopf bifurcation, emergence of limit cycle and then through a cascade of bifurcations type saddle-foci Shilnikov's bifurcation. Finally, the thermodynamics framework developed shows that the entropy production rate, as a Lyapunov function, indicates the directional character and stability of the dynamical behavior of tumor growth according to this model.

  14. Eating behavior, prenatal and postnatal growth in Angelman syndrome

    DEFF Research Database (Denmark)

    Mertz, Line Granild Bie; Christensen, Rikke; Vogel, Ida;

    2014-01-01

    The objectives of the present study were to investigate eating behavior and growth parameters in Angelman syndrome. We included 39 patients with Angelman syndrome. Twelve cases had a larger Class I deletion, eighteen had a smaller Class II deletion, whereas paternal uniparental disomy (pUPD) or a...

  15. Free vibrations of delaminated unidirectional sandwich panels with a transversely flexible core—a modified Galerkin approach

    Science.gov (United States)

    Schwarts-Givli, H.; Rabinovitch, O.; Frostig, Y.

    2007-03-01

    A theoretical approach for the free vibration analysis of delaminated unidirectional sandwich panels is developed. The theoretical model accounts for the flexibility of the core in the out of plane (vertical) direction and the resulting high-order displacement, acceleration, and velocity fields within the core. The analytical approach is based on Hamilton's variational principle along with the high-order unidirectional sandwich panel theory and the modified Galerkin method. The two types of models investigated include delaminated regions with and without contact. The ability of the model to describe the high-order effects such as the pumping phenomenon and the localized effects in the vicinity of the delaminated regions is examined. A numerical example that focuses on the free vibration behavior of simply supported delaminated unidirectional sandwich panels is presented and discussed. A parametric study that examines the influence of the length of the delaminated region, its location, and the mechanical properties of the core material is presented. The numerical results are also compared with finite element analysis and with some special asymptotic cases for which the free vibrations behavior is analytically evaluated. A summary and conclusions close the paper.

  16. Prediction of cyclic delamination lives of plasma-sprayed hydroxyapatite coating on Ti-6Al-4V substrates with considering wear and dissolutions.

    Science.gov (United States)

    Otsuka, Yuichi; Kojima, Daisuke; Mutoh, Yoshiharu

    2016-12-01

    This study aims at developing the prediction model of cyclic delamination lives of plasma-sprayed HAp coating on Ti-6Al-4V substrate by considering wear by interface contacts and dissolution effect by Simulated Body Fluid (SBF). Delamination of HAp coating can lead to loosening of implants stem and final failure in vivo. In the fracture mechanism of interfaces between HAp coating with Ti substrates, only adhesive strength (interracial tensile strength) or fatigue behavior by longitudinal cracking have been observed. Cyclic delamination mechanism by considering various loading modes and corrosion effect has not been revealed yet. The interface delamination rates by cyclic loading were much higher than those by static loading tests. The result clearly demonstrated that the interface demalination behaviors are dominated not by maximum stress, but by stress range. Surface profile measurement and SEM observation also demonstrated damages by interface contact or third body wear at delamination tips of HAp coating only in the cases of compressions. The mechanisms of acceleration on the delaminations are third-body wear or wedge effect by worn particles which increased mean stress level during cyclic loading. Cyclic loading tests under SBF also revealed that cyclic delamination lives were shortened probably due to crevice corrosion at interfaces. Dissolutions at the tips of delaminations were observed by SEM images under tensile loading condition in SBF. Linearly adding the effects of wear and dissolutions into Paris law could successfully predict the delamination lives of HAp coating for various loading ratios in SBF. Copyright © 2016 The Authors. Published by Elsevier Ltd.. All rights reserved.

  17. Nanotube attachment for prevention of interfacial delamination

    Science.gov (United States)

    Mukhopadhyay, Sharmila M.; Karumuri, Anil K.

    2010-09-01

    A new approach to suppressing interfacial delamination in composites has been investigated. It involves growing strongly attached nanotubes on the surface of the core phase prior to matrix infiltration. Unusually durable interfaces between epoxy and graphite have been demonstrated using this technique. Two types of graphitic core materials have been studied: complex cellular foams having open-interconnected porosity and highly oriented pyrolitic graphite (HOPG) providing a model flat interface. When untreated foam is infiltrated with epoxy, the resulting composite is brittle, and shatters before 10% compression. However, when carbon nanotubes (CNTs) are grown on the foam prior to epoxy infiltration, the specimen becomes pliable, and visibly flattens out rather than fracturing. Model studies on a flat graphite-epoxy interface were performed by joining two HOPG specimens with a thin layer of epoxy, and testing the flexural response of the 'seam' using the three-point bend test. The untreated HOPG sandwich fails easily, whereas nanotube-attached HOPG sandwich shows an over three times increase in flexural load-carrying capacity, close to that of seamless monolithic graphite having identical dimensions. Microscopic evaluations of fractured interfaces indicate that, in all geometries, CNT grafting prevents delamination at the graphite-epoxy interface, and forces any crack(s) to propagate through the graphitic phase. This added inter-laminar strength and toughness can be related to the hierarchical morphology of the interface created by CNT attachment, and unprecedented composite structures can be envisioned.

  18. The Effect of Substrate Topography on Coating Cathodic Delamination

    DEFF Research Database (Denmark)

    Weinell, Claus E.; Sørensen, Per A.; Kiil, Søren

    2011-01-01

    This article describes the effect of steel substrate topography on coating cathodic delamination. The study showed that the surface preparation can be used to control and minimize the rate of cathodic delamination. The coating should have maximum wetting properties so that substrates with high...

  19. Buckling-driven Delamination in Layered Spherical Shells

    DEFF Research Database (Denmark)

    Sørensen, Kim Dalsten; Jensen, Henrik Myhre

    2008-01-01

    An analysis of buckling-driven delamination of a thin film on a spherical substrate has been carried out. The effects of the substrate having a double curvature compared to previous studies of delamination on cylindrical substrates turn out to be non-trivial: In addition to the effect of the shap...

  20. Gas permeation and temperature effects in laser-induced delamination

    NARCIS (Netherlands)

    Fedorov, Alexander; Vellinga, Willem-Pier; De Hosson, Jeff

    Laser-induced delamination (LID) is a technique aimed at measuring the work of adhesion of thin polymer coatings on metal substrates. A laser Pulse is used to create a blister that initiates delamination of the film under pressure. The stress fields in the blister wall and the work of adhesion of

  1. Volumetric characterization of delamination fields via angle longitudinal wave ultrasound

    Science.gov (United States)

    Wertz, John; Wallentine, Sarah; Welter, John; Dierken, Josiah; Aldrin, John

    2017-02-01

    The volumetric characterization of delaminations necessarily precedes rigorous composite damage progression modeling. Yet, inspection of composite structures for subsurface damage remains largely focused on detection, resulting in a capability gap. In response to this need, angle longitudinal wave ultrasound was employed to characterize a composite surrogate containing a simulated three-dimensional delamination field with distinct regions of occluded features (shadow regions). Simple analytical models of the specimen were developed to guide subsequent experimentation through identification of optimal scanning parameters. The ensuing experiments provided visual evidence of the complete delamination field, including indications of features within the shadow regions. The results of this study demonstrate proof-of-principle for the use of angle longitudinal wave ultrasonic inspection for volumetric characterization of three-dimensional delamination fields. Furthermore, the techniques developed herein form the foundation of succeeding efforts to characterize impact delaminations within inhomogeneous laminar materials such as polymer matrix composites.

  2. Experimental Vibration Study on the Healthy and Delaminated Composite Plates

    Energy Technology Data Exchange (ETDEWEB)

    Ullah, Israr; Sinha, Jyoti K, E-mail: Jyoti.Sinha@manchester.ac.uk [School of Mechanical, Aerospace and Civil Engineering, University of Manchester, Manchester M13 9PL (United Kingdom)

    2011-07-19

    Vibration based damage, in particular delamination detection, in the composite structures is an active research area. The present study is also on the dynamics of the composite plates with and without delamination based on the experimental study. The test plate made of E-glass fibre and epoxy resins has been used here. A piezo-electric shaker has been used to excite the composite plate and the acceleration responses were measured using the number of accelerometers. The dynamics of the delaminated composite plates were then compared with a healthy composite plate when the vibration experiments have been conducted at the lower modes. The paper will discuss the observations made on the measured vibration responses from both the healthy and the delaminated plates and the possibility of the delamination detection from the experimental vibration data.

  3. Extended layerwise method for laminated composite plates with multiple delaminations and transverse cracks

    Science.gov (United States)

    Li, D. H.; Zhang, X.; Sze, K. Y.; Liu, Y.

    2016-10-01

    In this paper, the extended layerwise method (XLWM), which was developed for laminated composite beams with multiple delaminations and transverse cracks (Li et al. in Int J Numer Methods Eng 101:407-434, 2015), is extended to laminated composite plates. The strong and weak discontinuous functions along the thickness direction are adopted to simulate multiple delaminations and interlaminar interfaces, respectively, whilst transverse cracks are modeled by the extended finite element method (XFEM). The interaction integral method and maximum circumferential tensile criterion are used to calculate the stress intensity factor (SIF) and crack growth angle, respectively. The XLWM for laminated composite plates can accurately predicts the displacement and stress fields near the crack tips and delamination fronts. The thickness distribution of SIF and thus the crack growth angles in different layers can be obtained. These information cannot be predicted by using other existing shell elements enriched by XFEM. Several numerical examples are studied to demonstrate the capabilities of the XLWM in static response analyses, SIF calculations and crack growth predictions.

  4. Anomalous mechanical behavior and crack growth of oxide glasses

    Science.gov (United States)

    Seaman, Jared Hilliard

    This thesis is concerned with analytically describing anomalous mechanical behaviors of glass. A new slow crack growth model is presented that considers a semi-elliptical crack in a cylindrical glass rod subjected to 4-point bending that is both loaded statically and under a time-dependent load. This model is used to explain a suppression of the loading-rate dependency of ion-exchanged strengthened glass. The stress relaxation behavior of an ion-exchanged strengthened glass is then analyzed in view of a newly observed water-assisted surface stress relaxation mechanism. By making refinements to a time-dependent Maxwell material model for stress buildup and relaxation, the anomalous subsurface compressive stress peak in ion-exchanged strengthened glass is explained. The notion of water-assisted stress relaxation is extended to the crack tip, where high tensile stresses exist. A toughening effect has historically been observed for cracks aged at subcritical stress intensity factors, where crack tip stress relaxation is hypothesized. A simple fracture mechanics model is developed that estimates a shielding stress intensity factor that is then superimposed with the far-field stress intensity factor. The model is used to estimate anomalous "restart" times for aged cracks. The same model predicts a non-linear crack growth rate for cracks loaded near the static fatigue limit. Double cantilever beam slow crack growth experiments were performed and new slow crack growth data for soda-lime silicate glass was collected. Interpretation of this new experimental slow crack growth data suggests that the origin of the static fatigue limit in glass is due to water-assisted stress relaxation. This thesis combines a number of studies that offer a new unified understanding of historical anomalous mechanical behaviors of glass. These anomalies are interpreted as simply the consequence of slow crack growth and water-assisted surface stress relaxation.

  5. Development and Application of Benchmark Examples for Mixed-Mode I/II Quasi-Static Delamination Propagation Predictions

    Science.gov (United States)

    Krueger, Ronald

    2012-01-01

    The development of benchmark examples for quasi-static delamination propagation prediction is presented. The example is based on a finite element model of the Mixed-Mode Bending (MMB) specimen for 50% mode II. The benchmarking is demonstrated for Abaqus/Standard, however, the example is independent of the analysis software used and allows the assessment of the automated delamination propagation prediction capability in commercial finite element codes based on the virtual crack closure technique (VCCT). First, a quasi-static benchmark example was created for the specimen. Second, starting from an initially straight front, the delamination was allowed to propagate under quasi-static loading. Third, the load-displacement as well as delamination length versus applied load/displacement relationships from a propagation analysis and the benchmark results were compared, and good agreement could be achieved by selecting the appropriate input parameters. The benchmarking procedure proved valuable by highlighting the issues associated with choosing the input parameters of the particular implementation. Overall, the results are encouraging, but further assessment for mixed-mode delamination fatigue onset and growth is required.

  6. A finite element model for the analysis of buckling driven delaminations of thin films on rigid substrates

    Science.gov (United States)

    Gruttmann, F.; Pham, V. D.

    2008-02-01

    The delamination process of thin films on rigid substrates is investigated. Such systems are typically subject to high residual compression and modest adhesion causing them to buckling driven blisters. In certain cases buckles with the shape of telephone cords are observed. A finite element model for quasi-static delamination growth is developed. Applying a Reissner-Mindlin shell kinematic for the film allows C 0- continuous shape functions. The traction vector at the film-substrate interface is obtained from the derivative of a cohesive free energy. Incorporation of loading and unloading conditions is considered for the irreversible process. The equilibrium state is computed iteratively in dependence of the compressive residual stresses. The computed telephone cord delaminations are stable asymmetric configurations whereas the symmetric configurations are unstable.

  7. Eating behavior, prenatal and postnatal growth in Angelman syndrome.

    Science.gov (United States)

    Mertz, Line G B; Christensen, Rikke; Vogel, Ida; Hertz, Jens M; Østergaard, John R

    2014-11-01

    The objectives of the present study were to investigate eating behavior and growth parameters in Angelman syndrome. We included 39 patients with Angelman syndrome. Twelve cases had a larger Class I deletion, eighteen had a smaller Class II deletion, whereas paternal uniparental disomy (pUPD) or a verified UBE3A mutation were present in five and four cases, respectively. Eating behavior was assessed by a questionnaire. Anthropometric measures were obtained from medical records and compared to Danish reference data. Children with pUPD had significantly larger birth weight and birth length than children carrying a deletion or a UBE3A mutation. We found no difference in birth weight or length in children with Class I or Class II deletions. When maternal birth weight and/or birth weight of siblings were taken into consideration, children with Class I deletion had a lower weight at birth than expected, and the weight continued to be reduced during the investigated initial five years of life. In contrast, children with pUPD showed hyperphagic behavior and their weight increased significantly after the age of two years. Accordingly, their body mass index was significantly increased as compared to children with a deletion. At birth, one child showed microcephaly. At five years of age, microcephaly was observed in half of the deletion cases, but in none of the cases with a UBE3A mutation or pUPD. The apparently normal cranial growth in the UBE3A and pUPD patients should however be regarded as the result of a generally increased growth. Eating behavior, pre- and postnatal growth in children with Angelman syndrome depends on genotype. Copyright © 2014 Elsevier Ltd. All rights reserved.

  8. A subregional model for delamination prediction of rubber composite under fatigue loading

    Institute of Scientific and Technical Information of China (English)

    TIAN Zhen-hui; TAN Hui-feng

    2005-01-01

    Results from fatigue experiments of cross-laminated steel cord-rubber composites (SCRC) indicate that fatigue damage life can be categorized into three regimes. In terms of fatigue modes, a subregional fatigue model is developed to describe the damages evolution of SCRC under fatigue loads. Firstly, finite element analysis is introduced to determine interply stress distribution of the specimen. Then, based on the experimental fatigue data, subregional models are introduced to simulate relations between maximum strain, effective stiffness,delamination shear stress and fatigue cycles. Relations between crack density, delamination length growth rate,macro crack density and cycles are modeled by two semi-empirical models. A reasonable prediction result was achieved by the current model, where model parameters can be determined by basic outputs of fatigue testing.

  9. Near-criticality underlies the behavior of early tumor growth

    Science.gov (United States)

    Remy, Guillaume; Cluzel, Philippe

    2016-04-01

    The controlling factors that underlie the growth of tumors have often been hard to identify because of the presence in this system of a large number of intracellular biochemical parameters. Here, we propose a simplifying framework to identify the key physical parameters that govern the early growth of tumors. We model growth by means of branching processes where cells of different types can divide and differentiate. First, using this process that has only one controlling parameter, we study a one cell type model and compute the probability for tumor survival and the time of tumor extinction. Second, we show that when cell death and cell division are perfectly balanced, stochastic effects dominate the growth dynamics and the system exhibits a near-critical behavior that resembles a second-order phase transition. We show, in this near-critical regime, that the time interval before tumor extinction is power-law distributed. Finally, we apply this branching formalism to infer, from experimental growth data, the number of different cell types present in the observed tumor.

  10. Floating Carpets and the Delamination of Elastic Sheets

    KAUST Repository

    Wagner, Till J. W.

    2011-07-22

    We investigate the deformation of a thin elastic sheet floating on a liquid surface and subject to a uniaxial compression. We show that at a critical compression the sheet delaminates from the liquid over a finite region forming a delamination "blister." This blistering regime adds to the wrinkling and localized folding regimes that have been studied previously. The transition from wrinkled to blistered states occurs when delamination becomes energetically favorable compared with wrinkling. We determine the initial blister size and the evolution of blister size with continuing compression before verifying our theoretical results with experiments at a macroscopic scale. © 2011 American Physical Society.

  11. Microscale mechanics for metal thin film delamination along ceramic substrates

    Institute of Scientific and Technical Information of China (English)

    魏悦广

    2000-01-01

    The metal thin film delamination along metal/ceramic interface in the case of large scale yielding is studied by employing the strain gradient plasticity theory and the material microscale effects are considered. Two different f racture process models are used in this study to describe the nonlinear delamination phenomena for metal thin films. A set of experiments have been done on the mechanism of copper films delaminating from silica substrates, based on which the peak interface separation stress and the micro-length scale of material, as well as the dislocation-free zone size are predicted.

  12. Microscale mechanics for metal thin film delamination along ceramic substrates

    Institute of Scientific and Technical Information of China (English)

    2000-01-01

    The metal thin film delamination along metal/ceramic interface in the case of large scale yielding is studied by employing the strain gradient plasticity theory and the material microscale effects are considered.Two different fracture process models are used in this study to describe the nonlinear delamination phenomena for metal thin films.A set of experiments have been done on the mechanism of copper films delaminating from silica substrates,based on which the peak interface separation stress and the micro-length scale of material,as well as the dislocation-free zone size are predicted.

  13. Growth behavior of electroless copper on silicon substrate

    Institute of Scientific and Technical Information of China (English)

    Shin-Shyan Wu; Wei-Long Liu; Ting-Kan Tsai; Shu-Huei Hsieh; Wen-Jauh Chen

    2007-01-01

    The growth behavior containing deposit morphology,growth rate,activation energy,and growth mechanism of copper on silicon substrate,especially at the initial stage,in the electroless plating process was studied.Copper was deposited on the surface of the silicon substrate in an electroless plating bath containing formalin (CH2O 37vol%) as a reducing agent at a pH value of 12.5 and a temperature of 50-75 ℃.The copper deposit was characterized using a field emission scanning electron microscope and transmission electron microscope.The results showed that after the activation process,nanoscale Pd particles were distributed evenly on the surface of the silicon; in the deposition process,copper first nucleated at locations not only near the Pd particles but also between the Pd particles;the growth rate of electroless Cu ranged from 0.517 nm/s at 50 ℃ to 1.929 nm/s at 75 ℃.The activation energy of electroless Cu on Si was 52.97 kJ/mol.

  14. Genomic imprinting in development, growth, behavior and stem cells.

    Science.gov (United States)

    Plasschaert, Robert N; Bartolomei, Marisa S

    2014-05-01

    Genes that are subject to genomic imprinting in mammals are preferentially expressed from a single parental allele. This imprinted expression of a small number of genes is crucial for normal development, as these genes often directly regulate fetal growth. Recent work has also demonstrated intricate roles for imprinted genes in the brain, with important consequences on behavior and neuronal function. Finally, new studies have revealed the importance of proper expression of specific imprinted genes in induced pluripotent stem cells and in adult stem cells. As we review here, these findings highlight the complex nature and developmental importance of imprinted genes.

  15. Growth Trajectories of Health Behaviors from Adolescence through Young Adulthood

    Directory of Open Access Journals (Sweden)

    Nora Wiium

    2015-10-01

    Full Text Available Based on nine waves of data collected during a period of 17 years (1990–2007, the present study explored different developmental trajectories of the following unhealthy behaviors: regular smoking, lack of regular exercise, lack of daily fruit intake, and drunkenness. A baseline sample of 1195 13-year-old pupils was from 22 randomly selected schools in the Hordaland County in western Norway. Latent class growth analysis revealed three developmental trajectories. The first trajectory was a conventional trajectory, comprising 36.3% of participants, who showed changes in smoking, physical exercise, fruit intake, and drunkenness consistent with the prevailing age specific norms of these behaviors in the Norwegian society at the time. The second trajectory was a passive trajectory, comprising 25.5% of participants, who reported low levels of both healthy and unhealthy behaviors during the 17-year period. The third trajectory was an unhealthy trajectory, comprising 38.2% of participants, who had high levels of unhealthy behaviors over time. Several covariates were examined, but only sex and mother’s and father’s educational levels were found to be significantly associated with the identified trajectories. While these findings need to be replicated in future studies, the identification of the different trajectories suggests the need to tailor intervention according to specific needs.

  16. Utilization of Large Cohesive Interface Elements for Delamination Simulation

    DEFF Research Database (Denmark)

    Bak, Brian Lau Verndal; Lund, Erik

    2012-01-01

    This paper describes the difficulties of utilizing large interface elements in delamination simulation. Solutions to increase the size of applicable interface elements are described and cover numerical integration of the element and modifications of the cohesive law.......This paper describes the difficulties of utilizing large interface elements in delamination simulation. Solutions to increase the size of applicable interface elements are described and cover numerical integration of the element and modifications of the cohesive law....

  17. Delaminated graphene at silicon carbide facets: atomic scale imaging and spectroscopy.

    Science.gov (United States)

    Nicotra, Giuseppe; Ramasse, Quentin M; Deretzis, Ioannis; La Magna, Antonino; Spinella, Corrado; Giannazzo, Filippo

    2013-04-23

    Atomic-resolution structural and spectroscopic characterization techniques (scanning transmission electron microscopy and electron energy loss spectroscopy) are combined with nanoscale electrical measurements (conductive atomic force microscopy) to study at the atomic scale the properties of graphene grown epitaxially through the controlled graphitization of a hexagonal SiC(0001) substrate by high temperature annealing. This growth technique is known to result in a pronounced electron-doping (∼10(13) cm(-2)) of graphene, which is thought to originate from an interface carbon buffer layer strongly bound to the substrate. The scanning transmission electron microscopy analysis, carried out at an energy below the knock-on threshold for carbon to ensure no damage is imparted to the film by the electron beam, demonstrates that the buffer layer present on the planar SiC(0001) face delaminates from it on the (112n) facets of SiC surface steps. In addition, electron energy loss spectroscopy reveals that the delaminated layer has a similar electronic configuration to purely sp2-hybridized graphene. These observations are used to explain the local increase of the graphene sheet resistance measured around the surface steps by conductive atomic force microscopy, which we suggest is due to significantly lower substrate-induced doping and a resonant scattering mechanism at the step regions. A first-principles-calibrated theoretical model is proposed to explain the structural instability of the buffer layer on the SiC facets and the resulting delamination.

  18. Self-healing of low-velocity impact and mode-I delamination damage in polymer composites via microchannels

    Directory of Open Access Journals (Sweden)

    M. U. Saeed

    2016-04-01

    Full Text Available Microchannels embedded polymer composites were fabricated by resin infusion process using carbon fabric, epoxy resin and hollow glass tubes (HGTs. The effect of a range of low-velocity impact (LVI and mode-I delamination (M1D damage on the flexural strength of microchanneled carbon- epoxy composites was studied. A self-healing approach was also employed to recover their lost flexural strength due to these damages. Moreover, influence of LVI, M1D damage and healing on the failure behavior of microchanneled carbon- epoxy composites was also investigated. The results of flexural after impact (FAI and flexural after delamination (FAD showed that LVI has more deleterious effect on the flexural strength of carbon- epoxy composites than M1D damage. The loss in flexural strength increased linearly with increase in both impact (by higher impact energies and delamination damage (by longer delamination lengths. Scanning electron microscopic (SEM study revealed that self-healing agent (SHA, stored in HGTs placed within carbon- epoxy composites, effectively healed both LVI and M1D damage with excellent healing efficiencies.

  19. MR imaging of delamination tears of the rotator cuff tendons

    Energy Technology Data Exchange (ETDEWEB)

    Walz, Daniel M.; Chen, Steven [North Shore University Hospital, Department of Radiology, Manhasset, NY (United States); Miller, Theodore T. [Hospital for Special Surgery, Department of Radiology and Imaging, New York, NY (United States); Hofman, Josh [Long Island Jewish Medical Center, New Hyde Park, NY (United States)

    2007-05-15

    The objective was to describe the imaging appearances and location of delamination tears of the rotator cuff tendons on non-contrast conventional MR imaging. This study was reviewed and approved by our Institutional Review Board. The reports of 548 consecutive MR examinations of the shoulder were reviewed, looking for mention or description of delamination tears of the rotator cuff. The images of the identified cases were then reviewed by two radiologists to confirm the findings. Correlation with surgical and arthroscopic information was then performed. Delamination tears were defined as horizontal retraction of either the bursal or articular surface of the tendon, manifest as thickening of the torn retracted edge, and/or interstitial splitting of the tendon, manifest as fluid-like high signal intensity on fat-suppressed T2-weighted oblique coronal images. Fourteen cases of delamination tears were identified in 13 patients. Ten of the cases involved the supraspinatus tendon, all with articular surface involvement. Nine of these supraspinatus cases were isolated tears and one occurred as part of a full thickness tear. All 10 of these supraspinatus cases showed medial retraction of the articular surface of the tendon, with thickening of the retracted edge, and 5 of the 10 had a demonstrable horizontal cleft in the interstitium. Four cases involved the subscapularis tendon, with articular surface disruption in three and pure interstitial delamination in one. Medial subluxation of the tendon of the long head of the biceps was present in all four cases. No delamination tears occurred on the bursal surface. Only three of the 14 shoulders underwent surgical repair with one confirmation of supraspinatus delamination, one confirmation of a subscapularis tear that had become a full thickness tear 10 months after initial imaging and another interstitial subscapularis delamination that was not identified arthroscopically. Delamination tears occur most often in the

  20. Microscopic mechanisms of graphene electrolytic delamination from metal substrates

    Science.gov (United States)

    Fisichella, G.; Di Franco, S.; Roccaforte, F.; Ravesi, S.; Giannazzo, F.

    2014-06-01

    In this paper, hydrogen bubbling delamination of graphene (Gr) from copper using a strong electrolyte (KOH) water solution was performed, focusing on the effect of the KOH concentration (CKOH) on the Gr delamination rate. A factor of ˜10 decrease in the time required for the complete Gr delamination from Cu cathodes with the same geometry was found increasing CKOH from ˜0.05 M to ˜0.60 M. After transfer of the separated Gr membranes to SiO2 substrates by a highly reproducible thermo-compression printing method, an accurate atomic force microscopy investigation of the changes in Gr morphology as a function of CKOH was performed. Supported by these analyses, a microscopic model of the delamination process has been proposed, where a key role is played by graphene wrinkles acting as nucleation sites for H2 bubbles at the cathode perimeter. With this approach, the H2 supersaturation generated at the electrode for different electrolyte concentrations was estimated and the inverse dependence of td on CKOH was quantitatively explained. Although developed in the case of Cu, this analysis is generally valid and can be applied to describe the electrolytic delamination of graphene from several metal substrates.

  1. Epidermal growth factor signaling induces behavioral quiescence in Caenorhabditis elegans.

    Science.gov (United States)

    Van Buskirk, Cheryl; Sternberg, Paul W

    2007-10-01

    The epidermal growth factor receptor (EGFR)/ErbB receptor tyrosine kinases regulate several aspects of development, including the development of the mammalian nervous system. ErbB signaling also has physiological effects on neuronal function, with influences on synaptic plasticity and daily cycles of activity. However, little is known about the effectors of EGFR activation in neurons. Here we show that EGF signaling has a nondevelopmental effect on behavior in Caenorhabditis elegans. Ectopic expression of the EGF-like ligand LIN-3 at any stage induces a reversible cessation of feeding and locomotion. These effects are mediated by neuronal EGFR (also called LET-23) and phospholipase C-gamma (PLC-gamma), diacylglycerol-binding proteins, and regulators of synaptic vesicle release. Activation of EGFR within a single neuron, ALA, is sufficient to induce a quiescent state. This pathway modulates the cessation of pharyngeal pumping and locomotion that normally occurs during the lethargus period that precedes larval molting. Our results reveal an evolutionarily conserved role for EGF signaling in the regulation of behavioral quiescence.

  2. EBSD and Nanoindentation-Correlated Study of Delamination Fracture in Al-Li Alloy 2090

    Science.gov (United States)

    Tayon, Wesley A.; Crooks, Roy E.; Domack, Marcia S.; Wagner, John A.; Elmustafa, A. A.

    2008-01-01

    Al-Li alloys offer attractive combinations of high strength and low density. However, a tendency for delamination fracture has limited their use. A better understanding of the delamination mechanisms may identify methods to control delaminations through processing modifications. A combination of new techniques has been used to evaluate delamination fracture in Al-Li alloys. Both high quality electron backscattered diffraction (EBSD) information and valid nanoindentation measurements were obtained from fractured test specimens. Correlations were drawn between nano-scale hardness variations and local texture along delaminating boundaries. Intriguing findings were observed for delamination fracture through the combined analysis of grain orientation, Taylor factor, and kernel average misorientation.

  3. Buckling induced delamination of graphene composites through hybrid molecular modeling

    Science.gov (United States)

    Cranford, Steven W.

    2013-01-01

    The efficiency of graphene-based composites relies on mechanical stability and cooperativity, whereby separation of layers (i.e., delamination) can severely hinder performance. Here we study buckling induced delamination of mono- and bilayer graphene-based composites, utilizing a hybrid full atomistic and coarse-grained molecular dynamics approach. The coarse-grain model allows exploration of an idealized model material to facilitate parametric variation beyond any particular molecular structure. Through theoretical and simulation analyses, we show a critical delamination condition, where ΔD∝kL4, where ΔD is the change in bending stiffness (eV), k the stiffness of adhesion (eV/Å4), and L the length of the adhered section (Å).

  4. The growth benefits of aggressive behavior vary with individual metabolism and resource predictability

    NARCIS (Netherlands)

    Hoogenboom, Mia O.; Armstrong, John D.; Groothuis, Ton G. G.; Metcalfe, Neil B.

    2013-01-01

    Differences in behavioral responses to environmental conditions and biological interactions are a key determinant of individual performance. This study investigated how the availability and predictability of food resources modulates the growth of animals that adopt different behavioral strategies. R

  5. Repair of prestressed concrete cylinder with localized delamination

    Energy Technology Data Exchange (ETDEWEB)

    Wang, Shen, E-mail: swang@bechtel.com; Munshi, Javeed A., E-mail: jamunshi@bechtel.com

    2015-12-15

    For prestressed concrete cylindrical structures such as nuclear containments, tanks and silos, the curvature effect of the tendons introduces radial tensile stresses in the concrete shell which are generally neglected in the design of such structures. For example, many prestressed concrete nuclear containments in US, especially those which were not designed following radial reinforcement requirement of ACI-359, are reinforced only in the circumferential (hoop) and meridional (vertical) directions but not in the radial direction. This leaves these structures vulnerable to potential laminar cracking and delamination, especially during post-tensioning and/or detensioning process. Should delamination occur, the structure needs to be repaired by either replacing cracked concrete or by “pinning” the delaminated concrete layers together by post-installed anchors. The latter option of post-installed anchors is less invasive from construction stand point and generally suitable for repairing small or localized delamination only. A comprehensive study is undertaken to explore various aspects and design consideration of post-installed anchors for prestressed concrete cylinders. The radial tension demand is first established by combining a mechanical based model with a detailed finite element analysis. With such design demand for post-installed anchors established, the next step aims at developing the tightness requirement of existing delamination cracks for effective use of post-installed anchors. A comprehensive literature search and evaluation is carried out for shear transfer capacity across cracks of various widths. The findings are used to develop specific recommendations for acceptable crack widths to ensure adequate in-plane shear transfer capacity for various design load conditions. A design process for post-installed anchors is proposed for repairing a delaminated prestressed concrete cylindrical structure at the end of the paper, supplemented by an illustrative

  6. Characterization of Multiple Delaminated Composite by Finite Element

    Directory of Open Access Journals (Sweden)

    SUDIP DEY

    2011-09-01

    Full Text Available In this paper, a finite element method is employed to investigate the natural frequencies of twisted rotating composite turbine blades subject to multiple delamination. The turbine blade is idealized as a shallow conical shell model with low aspect ratio. The formulation is based on Mindlin’s theory, QR iteration and multi-point constraint algorithm for moderate rotational speeds neglecting Coriolis effect. Computer codes are developed and the numerical results obtained for multiple delaminated graphite-epoxy cross-ply composite shallow conical shells are the first known non-dimensional frequencies for the type of analyses carried out here.

  7. Modeling Quasi-Static and Fatigue-Driven Delamination Migration

    Science.gov (United States)

    De Carvalho, N. V.; Ratcliffe, J. G.; Chen, B. Y.; Pinho, S. T.; Baiz, P. M.; Tay, T. E.

    2014-01-01

    An approach was proposed and assessed for the high-fidelity modeling of progressive damage and failure in composite materials. It combines the Floating Node Method (FNM) and the Virtual Crack Closure Technique (VCCT) to represent multiple interacting failure mechanisms in a mesh-independent fashion. Delamination, matrix cracking, and migration were captured failure and migration criteria based on fracture mechanics. Quasi-static and fatigue loading were modeled within the same overall framework. The methodology proposed was illustrated by simulating the delamination migration test, showing good agreement with the available experimental data.

  8. The postbuckling analysis of laminated circular plate with elliptic delamination

    Science.gov (United States)

    Chen, Deliang; Chen, Changping; Fu, Yiming

    2011-01-01

    Based on the Von Karman plate theory, considering the effect of transverse shear deformation, and using the method of the dissociated three regions, the postbuckling governing equations for the axisymmetric laminated circular plates with elliptical delamination are derived. By using the orthogonal point collocation method, the governing equations, boundary conditions and continuity conditions are transformed into a group of nonlinear algebraically equation and the equations are solved with the alternative method. In the numerical examples, the effects of various elliptical in shape, delamination depth and different material properties on buckling and postbuckling of the laminated circular plates are discussed and the numerical results are compared with available data.

  9. Probabilistic Delamination Diagnosis of Composite Materials Using a Novel Bayesian Imaging Method

    Data.gov (United States)

    National Aeronautics and Space Administration — In this paper, a probabilistic delamination location and size detection framework is proposed. The delamination probability image using Lamb wave-based damage...

  10. On the nonlinear thermomechanical behavior and delamination of conductive adhesives

    NARCIS (Netherlands)

    Öztürk, B.

    2015-01-01

    Adhesives based on thermoset polymers are used as thermal and electrical interfaces. These adhesives are filled with different particles in order to meet the requirements of heat transfer and electrical properties. Due to the reliability requirements of automotive applications, they are required to

  11. The Effect of Strike Face Geometry on the Dynamic Delamination of Composite Back Plates

    Science.gov (United States)

    2015-01-01

    Information Operations and Reports (0704-0188), 1215 Jefferson Davis Highway, Suite 1204, Arlington, VA 22202-4302. Respondents should be aware that...specimen allowed for capture of dynamic delamination images with high-speed photography . The projected delamination area was quantified using commercially...14 Fig. B-1 Delaminations outlined using tools in Image Pro Plus ..................................................22 Fig. B-2 Yellow

  12. Mode III effects on interface delamination

    DEFF Research Database (Denmark)

    Tvergaard, Viggo; Hutchinson, J.W.

    2008-01-01

    mode III has an effect. Subsequently, the focus is on crack growth along an interface between an elastic-plastic solid and an elastic substrate. The analyses are carried out for conditions of small-scale yielding, with the fracture process at the interface represented by a cohesive zone model. Due......For crack growth along an interface between dissimilar materials the effect of combined modes I, II and III at the crack-tip is investigated. First, in order to highlight situations where crack growth is affected by a mode III contribution, examples of material configurations are discussed where...... to the mismatch of elastic properties across the interface the corresponding elastic solution has an oscillating stress singularity, and this solution is applied as boundary conditions on the outer edge of the region analyzed. For several combinations of modes I, II and III crack growth resistance curves...

  13. Adhesion of polymer coatings studied by laser-induced delamination

    NARCIS (Netherlands)

    Fedorov, A; De Hosson, JTM

    2005-01-01

    This paper concentrates on the laser-induced delamination technique, aimed at measuring the practical work of adhesion of thin polymer coatings on metal substrates. In this technique an infrared laser-pulsed beam is used to create an initial blister. Upon increasing the pulse intensity, the size of

  14. Modeling delamination due to thermal stress in optical storage media

    Science.gov (United States)

    Nkansah, M. A.; Evans, K. E.

    1990-04-01

    Finite element analysis is used to calculate the shape of blisters formed in bilayer optical storage media due to the buildup of thermal stresses during laser writing. It is shown that practically usable blisters may be expected to form in a time period of about 15 ns. Such a thermal stress delamination process may also precede melting in conventional pit formation processes.

  15. Delamination and debonding failure of laminated composite T-joints

    NARCIS (Netherlands)

    Cui, H.

    2014-01-01

    Composites are increasingly being used in aerospace, automotive and other industries. The T-joint (also named stringer stiffened skin) is a typical connection, broadly used in thin-walled structures, such as the wing and fuselage of aircraft. This thesis presents the analysis of the delamination and

  16. Ets-1 confers cranial features on neural crest delamination.

    Directory of Open Access Journals (Sweden)

    Eric Théveneau

    Full Text Available Neural crest cells (NCC have the particularity to invade the environment where they differentiate after separation from the neuroepithelium. This process, called delamination, is strikingly different between cranial and trunk NCCs. If signalings controlling slow trunk delamination start being deciphered, mechanisms leading to massive and rapid cranial outflow are poorly documented. Here, we show that the chick cranial NCCs delamination is the result of two events: a substantial cell mobilization and an epithelium to mesenchyme transition (EMT. We demonstrate that ets-1, a transcription factor specifically expressed in cranial NCCs, is responsible for the former event by recruiting massively cranial premigratory NCCs independently of the S-phase of the cell cycle and by leading the gathered cells to straddle the basal lamina. However, it does not promote the EMT process alone but can cooperate with snail-2 (previously called slug to this event. Altogether, these data lead us to propose that ets-1 plays a pivotal role in conferring specific cephalic characteristics on NCC delamination.

  17. Webbing and Delamination of Drug Eluting Stent Coatings.

    Science.gov (United States)

    Hopkins, C; Sweeney, C A; O'Connor, C; McHugh, P E; McGarry, J P

    2016-02-01

    The advancement of the drug-eluting stent technology raises the significant challenge of safe mechanical design of polymer coated stent systems. Experimental images of stent coatings undergoing significant damage during deployment have been reported; such coating damage and delamination can lead to complications such as restenosis and increased thrombogenicity. In the current study a cohesive zone modeling framework is developed to predict coating delamination and buckling due to hinge deformation during stent deployment. Models are then extended to analyze, for the first time, stent-coating damage due to webbing defects. Webbing defects occur when a bond forms between coating layers on adjacent struts, resulting in extensive delamination of the coating from the strut surfaces. The analyzes presented in this paper uncover the mechanical factors that govern webbing induced coating damage. Finally, an experimental fracture test of a commercially available stent coating material is performed and results demonstrate that the high cohesive strength of the coating material will prevent web fracture, resulting in significant coating delamination during stent deployment.

  18. Modeling the buckling and delamination of thin films

    Science.gov (United States)

    Jagla, E. A.

    2007-02-01

    I study numerically the problem of delamination of a thin film elastically attached to a rigid substrate. A nominally flat elastic thin film is modeled using a two-dimensional triangular mesh. Both compression and bending rigidities are included to simulate compression and bending of the film. The film can buckle (i.e., abandon its flat configuration) when enough compressive strain is applied. The buckled configurations of a piece of film with stripe geometry are investigated as a function of the compressive strain. It is found that the stable configuration depends strongly on the applied strain and the Poisson ratio of the film. Next, the film is considered to be attached to a rigid substrate by springs that can break when the detaching force exceeds a threshold value, producing partial delamination of the film. Delamination is induced by a mismatch of the relaxed configurations of film and substrate. The morphology of the delaminated film can be followed and compared with available experimental results as a function of model parameters. “Telephone-cord,” polygonal, and “brainlike” patterns qualitatively similar to experimentally observed configurations are obtained in different parameter regions. The main control parameters that select the different patterns are the strain mismatch between film and substrate and the degree of in-plane relaxation within the unbuckled regions.

  19. Influence of surface pretreatment of fiber posts on cement delamination

    NARCIS (Netherlands)

    Jongsma, L.A.; Kleverlaan, C.J.; Feilzer, A.J.

    2010-01-01

    Objectives To evaluate the influence of post surface pretreatment on the delamination strength of different cements from a prefabricated FRC post tested in a three-point bending test. Methods Three cements were tested; RelyX Unicem, DC Core Automix, and Panavia F2.0. Per cement, 40 posts (D.T. Light

  20. Impact Delamination and Fracture in Aluminum/Acrylic Sandwich Plates

    Science.gov (United States)

    Liaw, Benjamin; Zeichner, Glenn; Liu, Yanxiong; Bowles, Kenneth J. (Technical Monitor)

    2000-01-01

    Impact-induced delamination and fracture in 6061-T6 aluminum/cast acrylic sandwich plates adhered by epoxy were generated in an instrumented drop-weight impact machine. Although only a small dent was produced on the aluminum side when a hemispherical penetrator tup was dropped onto it from a couple of inches, a large ring of delamination at the interface was observed. The delamination damage was often accompanied by severe shattering in the acrylic substratum. Damage patterns in the acrylic layer include radial and ring cracks and, together with delamination at the interface, may cause peeling-off of acrylic material from the sandwich plate. Theory of stress-wave propagation can be used to explain these damage patterns. The impact tests were conducted at various temperatures. The results also show clearly that temperature effect is very important in impact damage. For pure cast acrylic nil-ductile transition (NDT) occurs between 185-195 F. Excessive impact energy was dissipated into fracture energy when tested at temperature below this range or through plastic deformation when tested at temperature above the NDT temperature. Results from this study will be used as baseline data for studying fiber-metal laminates, such as GLARE and ARALL for advanced aeronautical and astronautical applications.

  1. Behavior of scoliosis during growth in children with osteogenesis imperfecta.

    Science.gov (United States)

    Anissipour, Alireza K; Hammerberg, Kim W; Caudill, Angela; Kostiuk, Theodore; Tarima, Sergey; Zhao, Heather Shi; Krzak, Joseph J; Smith, Peter A

    2014-02-05

    Spinal deformities are common in patients with osteogenesis imperfecta, a heritable disorder that causes bone fragility. The purpose of this study was to describe the behavior of spinal curvature during growth in patients with osteogenesis imperfecta and establish its relationship to disease severity and medical treatment with bisphosphonates. The medical records and radiographs of 316 patients with osteogenesis imperfecta were retrospectively reviewed. The severity of osteogenesis imperfecta was classified with the modified Sillence classification. Serial curve measurements were recorded throughout the follow-up period for each patient with scoliosis. Regression analysis was used to determine the effect of disease severity (Sillence type), patient age, and bisphosphonate treatment on the progression of scoliosis as measured with the Cobb method. Of the 316 patients with osteogenesis imperfecta, 157 had associated scoliosis, a prevalence of 50%. Scoliosis prevalence (68%) and mean progression rate (6° per year) were the highest in the group of patients with the most severe osteogenesis imperfecta (modified Sillence type III). A group with intermediate osteogenesis imperfecta severity, modified Sillence type IV, demonstrated intermediate scoliosis values (54%, 4° per year). The patient group with the mildest form of osteogenesis imperfecta, modified Sillence type I, had the lowest scoliosis prevalence (39%) and rate of progression (1° per year). Early treatment-before the patient reached the age of six years-of type-III osteogenesis imperfecta with bisphosphonate therapy decreased the curve progression rate by 3.8° per year, which was a significant decrease. Bisphosphonate treatment had no demonstrated beneficial effect on curve behavior in patients with other types of osteogenesis imperfecta or in patients of older age. The prevalence of scoliosis in association with osteogenesis imperfecta is high. Progression rates of scoliosis in children with osteogenesis

  2. Synthesis of mullite nanometers microwave from bentonite delaminated; Sintese de mulita nanometrica por microondas a partir bentonitas delaminadas

    Energy Technology Data Exchange (ETDEWEB)

    Gomes, J.; Azevedo, N.A.; Vieira, D.A.; Neves, G.A.; Santana, L.N.L., E-mail: josileido@yahoo.com.br [Universidade Federal de Campina Grande (UFCG), PB (Brazil); Menezes, R.R. [Universidade Federal da Paraiba (UFPB), PB (Brazil)

    2011-07-01

    The smectite clays present as lamellar structure is formed by two layers of silica tetrahedrons and one layer of aluminum octahedra, which can be individually delaminated, reaching a thickness of about 1mm. Mullite is the only thermodynamically stable crystalline phase of SiO{sub 2} and Al2O{sub 3} system and can be synthesized from minerals that exhibit these oxides in its composition. The microwave synthesis offers advantages over conventional methods, the heating is rapid and uniform, avoiding an undesirable grain growth. This study aims to obtain nanometric mullite from bentonites delamined subjected to microwave heating. The samples were initially treated, then rehydrated, frozen and deagglomeration in a ball mill for 4 and 8 hours. Subsequently subjected to centrifugation, drying and microwave heating. The results showed that nano-mullite was obtained for samples subjected to longer heating and dispersions. (author)

  3. Latent Growth Curve Modeling of Child Behavior in Elementary School

    Science.gov (United States)

    DiStefano, Christine; Kamphaus, R. W.

    2008-01-01

    The current study investigated child behavioral change during the early years of elementary school. Behavioral Assessment System for Children (BASC; Reynolds & Kamphaus, 1992) teacher ratings of child behavior were collected over a three-year period. The sample consisted of 162 children measured yearly between first and third grade.…

  4. Effects of Delaminations on the Damped Dynamic Characteristics of Composite Laminates: Mechanics and Experiments

    Science.gov (United States)

    Saravanos, D. A.; Hopkins, D. A.

    1995-01-01

    Analytical and experimental work is presented on the damped free-vibration of delaminated laminates and beams. A laminate theory is developed where the unknown kinematic perturbations induced by a delamination crack are treated as additional degrees of freedom. The generalized stiffness, inertia and damping matrices of the laminate are formulated. An analytical solution is developed for the prediction of natural frequencies, modes and modal damping in composite beams with delamination cracks. Evaluations of the mechanics on various cantilever beams with a central delamination are performed. Experimental results for the modal frequencies and damping of composite beams with a single delamination are also presented and correlations between analytical predictions and measured data are shown. The effects of delamination vary based on crack size, laminate configuration, and mode order. The implications of the mechanics in developing delamination detection techniques are also discussed.

  5. A cohesive finite element formulation for modelling fracture and delamination in solids

    Indian Academy of Sciences (India)

    S Roy Chowdhury; R Narasimhan

    2000-12-01

    In recent years, cohesive zone models have been employed to simulate fracture and delamination in solids. This paper presents in detail the formulation for incorporating cohesive zone models within the framework of a large deformation finite element procedure. A special Ritz-finite element technique is employed to control nodal instabilities that may arise when the cohesive elements experience material softening and lose their stress carrying capacity. A few simple problems are presented to validate the implementation of the cohesive element formulation and to demonstrate the robustness of the Ritz solution method. Finally, quasi-static crack growth along the interface in an adhesively bonded system is simulated employing the cohesive zone model. The crack growth resistance curves obtained from the simulations show trends similar to those observed in experimental studies.

  6. A Simulation Method for High-Cycle Fatigue-Driven Delamination using a Cohesive Zone Model

    DEFF Research Database (Denmark)

    Bak, Brian Lau Verndal; Turon, A.; Lindgaard, Esben;

    2016-01-01

    on parameter fitting of any kind. The method has been implemented as a zero-thickness eight-node interface element for Abaqus and as a spring element for a simple finite element model in MATLAB. The method has been validated in simulations of mode I, mode II, and mixed-mode crack loading for both self......A novel computational method for simulating fatigue-driven mixed-mode delamination cracks in laminated structures under cyclic loading is presented. The proposed fatigue method is based on linking a cohesive zone model for quasi-static crack growth and a Paris' law-like model described......-similar and non-self-similar crack propagation. The method produces highly accurate results compared with currently available methods and is capable of simulating general mixed-mode non-self-similar crack growth problems....

  7. Finite elements modeling of delaminations in composite laminates

    DEFF Research Database (Denmark)

    Gaiotti, m.; Rizzo, C.M.; Branner, Kim;

    2011-01-01

    The application of composite materials in many structures poses to engineers the problem to create reliable and relatively simple methods, able to estimate the strength of multilayer composite structures. Multilayer composites, like other laminated materials, suffer from layer separation, i.e., d...... by finite elements using different techniques. Results obtained with different finite element models are compared and discussed.......The application of composite materials in many structures poses to engineers the problem to create reliable and relatively simple methods, able to estimate the strength of multilayer composite structures. Multilayer composites, like other laminated materials, suffer from layer separation, i...... of the buckling strength of composite laminates containing delaminations. Namely, non-linear buckling and post-buckling analyses are carried out to predict the critical buckling load of elementary composite laminates affected by rectangular delaminations of different sizes and locations, which are modelled...

  8. Fracture and Delamination of Chromium Thin Films on Polymer Substrates

    Science.gov (United States)

    Cordill, M. J.; Taylor, A.; Schalko, J.; Dehm, G.

    2010-04-01

    New emerging technologies in the field of flexible electronic devices require that metal films adhere well and flex with polymer substrates. Common thin film materials used for these applications include copper (Cu) with an adhesion interlayer of chromium (Cr). Copper can be quite ductile and easily move with the polymer substrate. However, Cr is more brittle and fractures at lower strains than Cu. This study aims to examine the fracture and subsequent buckling and delamination of strained Cr films on polyimide (PI). In-situ scanning electron microscope (SEM) straining is used to systematically study the influence of film thickness on fracture and buckling strains. Film fracture and delamination depend on film thickness, and increases in crack and buckle density with decreasing thickness are explored by a shear lag model.

  9. Free-edge delamination - Laminate width and loading conditions effects

    Science.gov (United States)

    Murthy, Pappu L. N.; Chamis, Christos C.

    1989-01-01

    The width and loading conditions effects on free-edge stress fields in composite laminates are investigated using a three-dimensional finite element analysis. This analysis includes a special free-edge region refinement or superelement with progressive substructuring (mesh refinement) and finite thickness interply layers. The different loading conditions include in-plane and out-of-plane bending, combined axial tension and in-plane shear, twisting, uniform temperature and uniform moisture. Results obtained indicate that: axial tension causes the smallest magnitude of interlaminar free edge stress compared to other loading conditions; free-edge delamination data obtained from laboratory specimens cannot be scaled to structural components; and composite structural components are not likely to delaminate.

  10. Free-edge delamination: Laminate width and loading conditions effects

    Science.gov (United States)

    Murthy, P. L. N.; Chamis, C. C.

    1987-01-01

    The width and loading conditions effects on free-edge stress fields in composite laminates are investigated using a three-dimensional finite element analysis. This analysis includes a special free-edge region refinement or superelement with progrssive substructuring (mesh refinement) and finite thickness interply layers. The different loading conditions include in-plane and out-of-plane bending, combined axial tension and in-plane shear, twisting, uniform temperature and uniform moisture. Results obtained indicate that: axial tension causes the smallest magnitude of interlaminar free edge stress compared to other loading conditions; free-edge delamination data obtained from laboratory specimens cannot be scaled to structural components; and composite structural components are not likely to delaminate.

  11. Crack-growth behavior in thick welded plates of Inconel 718 at room and cryogenic temperatures

    Science.gov (United States)

    Forman, R. G.

    1974-01-01

    Results of mechanical-properties and axial-load fatigue and fracture tests performed on thick welded plates of Inconel 718 superalloy are presented. The test objectives were to determine the tensile strength properties and the crack-growth behavior in electron-beam, plasma-arc, and gas tungsten are welds for plates 1.90 cm (0.75 in) thick. Base-metal specimens were also tested to determine the flaw-growth behavior. The tests were performed in room-temperature-air and liquid nitrogen environments. The experimental crack-growth-rate data are correlated with theoretical crack-growth-rate predictions for semielliptical surface flaws.

  12. DETECTION OF DELAMINATION IN A COMPOSITE PLATE BY SEM

    Institute of Scientific and Technical Information of China (English)

    2001-01-01

    A numerical method of integration of Green's functi ons of strip element method (SEM) is proposed. The response of ultrasonic sourc e generated by a transducer on the surface of a multi-ply composite plate conta ining a delamination is analyzed by the use of SEM. The numerical results show that the scanning features of the ultrasonic waves may be used to identify the d elamination inside the composite plate .

  13. Controlled delamination of metal films by hydrogen loading

    Energy Technology Data Exchange (ETDEWEB)

    Nikitin, Eugen

    2008-11-18

    n this work we quantitatively determine the adhesion energy between metal films and their substrates. Therefore a new controlled buckling technique is established, applying the strong compressive in-plane stress that results in thin films clamped on rigid substrates during hydrogen loading. When the elastic energy stored in the H-loaded thin film exceeds the adhesion energy between film and substrate, delamination occurs. At the onset of delamination, a critical hydrogen concentration, a critical stress value and a critical bending of the substrate are present, which are quantitative measures for the adhesion energy and permit its calculation. As the critical values are determined at the onset of delamination, plastic deformation is negligible, which denies the quantitative determination of adhesion energies in conventional test setups. In multilayer-systems, adhesion energies between substrates and films that hardly absorb hydrogen can be measured by the controlled buckling technique, when the films of interest are coated with hydrogen absorbing films (active layer). The measurements are performed easily and can be repeated under the same test conditions, while variables such as the thickness of the coating materials or the boundary surface structure can be varied and optimized. In this work the adhesion energies of different materials on polycarbonate and niobium on sapphire are investigated. (orig.)

  14. Delamination toughness of ultra high molecular weight polyethylene (UHMWPE composites

    Directory of Open Access Journals (Sweden)

    Casas-Rodriguez J.P.

    2012-08-01

    Full Text Available Ultra high molecular weight polyethylene (UHMWPE fibre reinforced composites are an important group of material for armours solutions, where their unique combination of properties could be utilized. A commonly observed failure mode in this kind of unidirectional laminated composites under impact ballistic is delamination between the composite layers. In the present study, an investigation on the delamination toughness behaviour exhibited by UHMWPE composites laminated was made. The interlaminar Mode II critical strain energy release rates of (UHMWPE fibre reinforced composites were characterized using the End Notch Flexural (ENF test. Critical strain energy release rate was obtained from the load – deflection test data using the beam theory expression. It was found that the energy release rate of the composite exhibited a very low value of around 60J/m2 using a moulding pressure of approximately 1200 psi. In order to analyse the delamination resistance of composite, the effects of changing the manufacture process variables and the use of a thermoplastic adhesive film in the composites were investigated. The composite laminates were produced by hot compressing moulding using a film-stacking procedure. It was found that the damage resistance of the UHMWPE composite was influenced by the manufacture method, which affects the Mode II interlaminar fracture toughness and the ballistic response of composites.

  15. Chlorpyrifos-Oxon Disrupts Zebrafish Axonal Growth and Motor Behavior

    OpenAIRE

    Yang, Dongren; Lauridsen, Holly; Buels, Kalmia; Chi, Lai-Har; La Du, Jane; Bruun, Donald A.; Olson, James R.; Tanguay, Robert L.; Lein, Pamela J.

    2011-01-01

    Axonal morphology is a critical determinant of neuronal connectivity, and perturbation of the rate or extent of axonal growth during development has been linked to neurobehavioral deficits in animal models and humans. We previously demonstrated that the organophosphorus pesticide (OP) chlorpyrifos (CPF) inhibits axonal growth in cultured neurons. In this study, we used a zebrafish model to determine whether CPF, its oxon metabolite (CPFO), or the excreted metabolite trichloro-2-pyridinol (TCP...

  16. Innovation and Nested Preferential Growth in Chess Playing Behavior

    CERN Document Server

    Perotti, Juan I; Schaigorodsky, Ana L; Billoni, Orlando V

    2013-01-01

    We study innovation in chess by analyzing how different move sequences are played at the population level. It is found that the probability of exploring a new or innovative move decreases as a power law with the frequency in which the preceding move sequence is played. Chess players also exploit already known move sequences according to their frequencies, following a preferential growth mechanism. Furthermore, innovation in chess exhibits Heaps' law suggesting similarities with the process of vocabulary growth. We propose a robust generative mechanism based on nested Yule-Simon preferential growth processes that reproduces the empirical observations. These results, supporting the self-similar nature of innovations in chess, are important in the context of decision making in a competitive scenario.

  17. Amorphous nanoshell formed through random growth and related plasmonic behaviors

    Science.gov (United States)

    Wang, Yuwei; Shen, Hongming; He, Yingbo; Cheng, Yuqing; Perriat, Pascal; Martini, Matteo; Tillement, Olivier; Gong, Qihuang; Lu, Guowei

    2014-08-01

    The optical properties of gold nanoshell formed through random growth process were numerically investigated by employing finite-difference time-domain method. The growth process can be divided approximately into four stages according to the optical spectra and 3D morphology. The incomplete nanoshell with surface coverage ratio (R) around 70% was found to form surface ‘hot spots' with high field enhancement, which are useful for surface enhanced Raman scattering. Additionally, high Purcell factor and quantum efficiency at the core center for the nanoshells with R ∼ 90% are suitable for encapsulated fluorescent probe that can exploit the high surface plasmonic enhancement effect.

  18. Modeling Pacing Behavior and Test Speededness Using Latent Growth Curve Models

    Science.gov (United States)

    Kahraman, Nilufer; Cuddy, Monica M.; Clauser, Brian E.

    2013-01-01

    This research explores the usefulness of latent growth curve modeling in the study of pacing behavior and test speededness. Examinee response times from a high-stakes, computerized examination, collected before and after the examination was subjected to a timing change, were analyzed using a series of latent growth curve models to detect…

  19. Low-velocity Impact Damage Analysis of Composite Laminates Using Self-adapting Delamination Element Method

    Institute of Scientific and Technical Information of China (English)

    Wang Lipeng; Yan Ying; Wu Dafang; Wu Hao

    2008-01-01

    On the basis of a 2D 4-node Mindlin shell element method, a novel self-adapting delamination finite element method is presented,which is developed to model the delamination damage of composite laminates. In the method, the sublaminate elements are generated automatically when the delamination damage occurs or extends. Thus, the complex process and state of delamination damage can be simulated practically with high efficiency for both analysis and modeling. Based on the self-adapting delamination method, linear dynamic finite element damage analysis is performed to simulate the low-velocity impact damage process of three types of mixed woven composite laminates. Taking the frictional force among sublaminations during delaminating and the transverse normal stress into account,the analytical results ate consistent with those of the experimental data.

  20. Vibration of a delaminated beam-plate relative to buckled states

    Science.gov (United States)

    Yin, W.-L.; Jane, K. C.

    1992-07-01

    Free vibrations of delaminated beam-plates with respect to postbuckled referential states are studied. If the postbuckling deformation of the referential state is symmetric with respect to the mid-point, then the symmetric and antisymmetric vibration modes are uncoupled. Short delaminations which do not significantly degradate the overall stiffness of the beam-plate have little effect on the lowest modes of vibration and their frequencies, while the presence of a long delamination generally introduces additional vibration frequencies, the associated mode shapes of which show out-of-phase motions of the upper and lower delaminated layers. These new vibration modes and frequencies depend sensitively on the delamination length and location and on the magnitude of the postbuckling load. Hence their detection may indicate the presence and the nature of internal delamination damage.

  1. The nanoindentation applied to predict the interface delamination for the C/amorphous Si composite film

    Science.gov (United States)

    Han, Chang-Fu; Huang, Chao-Yu; Wu, Bo-Hsiung; Lin, Jen-Fin

    2009-10-01

    In the present study, the indentation depth corresponding to the pop-in arising in the loading process is found to be quite close to the C/amorphous Si composite film thickness, regardless of the C-film thickness. This load-depth behavior gives a clue that the occurrence of pop-in is perhaps related to the buckling of the composite film, which had already delaminated from the silicon substrate. This indentation depth of buckling predicted by the present model is quite close to the pop-in depth obtained from experimental results, regardless of the change in the C-film thickness. This characteristic reveals that the present model is developed successfully to predict the pop-in depth of a specimen, and the pop-in is indeed created due to the buckling of the composite film under a compression stress.

  2. Retraction pattern of delaminated rotator cuff tears: dual-layer rotator cuff repair

    OpenAIRE

    Cha, Sang-Won; Lee, Choon-Key; Sugaya, Hiroyuki; Kim, Taegyun; Lee, Su-Chan

    2016-01-01

    Background There has been no report to date regarding retraction patterns of delaminated rotator cuff tears. The purpose of this study was to evaluate the incidence and tearing patterns of delamination and repair integrity after the dual-layer repair of delaminated cuff tears. Methods/design A consecutive series of 64 patients with posterosuperior rotator cuff tears underwent arthroscopic rotator cuff repair from August 2011 to September 2012. Among the patients, 53 who received either dual-l...

  3. Delamination Method In English Teaching Can Also Be Applicable In Senior Middle School

    Institute of Scientific and Technical Information of China (English)

    于淑兰; 滕越

    2015-01-01

    The paper makes a research on delamination method in English teaching in senior middle school—a dimension of English teaching.By applying theories of linguistics,the author analyzes the present situation of the application of delamination method in English teaching both in college school and in senior middle school and a conclusion is,then,drawn that delamination English teaching can also be applicable in senior middle school.

  4. Innovation and nested preferential growth in chess playing behavior

    Science.gov (United States)

    Perotti, J. I.; Jo, H.-H.; Schaigorodsky, A. L.; Billoni, O. V.

    2013-11-01

    Complexity develops via the incorporation of innovative properties. Chess is one of the most complex strategy games, where expert contenders exercise decision making by imitating old games or introducing innovations. In this work, we study innovation in chess by analyzing how different move sequences are played at the population level. It is found that the probability of exploring a new or innovative move decreases as a power law with the frequency of the preceding move sequence. Chess players also exploit already known move sequences according to their frequencies, following a preferential growth mechanism. Furthermore, innovation in chess exhibits Heaps' law suggesting similarities with the process of vocabulary growth. We propose a robust generative mechanism based on nested Yule-Simon preferential growth processes that reproduces the empirical observations. These results, supporting the self-similar nature of innovations in chess are important in the context of decision making in a competitive scenario, and extend the scope of relevant findings recently discovered regarding the emergence of Zipf's law in chess.

  5. Ductile film delamination from compliant substrates using hard overlayers

    Science.gov (United States)

    Cordill, M.J.; Marx, V.M.; Kirchlechner, C.

    2014-01-01

    Flexible electronic devices call for copper and gold metal films to adhere well to polymer substrates. Measuring the interfacial adhesion of these material systems is often challenging, requiring the formulation of different techniques and models. Presented here is a strategy to induce well defined areas of delamination to measure the adhesion of copper films on polyimide substrates. The technique utilizes a stressed overlayer and tensile straining to cause buckle formation. The described method allows one to examine the effects of thin adhesion layers used to improve the adhesion of flexible systems. PMID:25641995

  6. Undulatory delamination of thin polymer films on gold surfaces.

    Science.gov (United States)

    Chah, Soonwoo; Noolandi, Jaan; Zare, Richard N

    2005-10-20

    Using two-dimensional surface plasmon resonance measurements, we have observed the formation of traveling waves in the delamination of thin films of polydimethylsilane (PDMS) exposed to methanol. Films were spin-coated on a gold surface and the methanol was added to the top surface. The stress-induced instability caused by the swelling of the PDMS thin film when its edge is pinned to the gold surface leads to wrinkle formation and propagation at the interface. The periodic pattern is thought to be the result of an Asaro-Tiller-Grinfeld (ATG) instability.

  7. A unified approach to modeling delamination and matrix cracking in smart composite structures

    Science.gov (United States)

    Thornburgh, Robert Preston

    The development of smart structures technology has coincided with the increased use of composite materials in structural design. Composite laminates have forms of damage that are not found in other materials, specifically delamination and transverse matrix cracking. An in-depth understanding of the effects of damage on smart composite structures is necessary for predicting not only the life of the structure, but also for modeling any method to be used for damage detection. The objective of this research was to develop a comprehensive model for accurately and efficiently modeling smart composite structures including the effects of composite damage. First, a new, efficient method for modeling smart structures with piezoelectric devices was developed. The coupled model simultaneously solves for the mechanical and electrical response of the system using mechanical displacements and electrical displacements. The developed theory utilizes a refined higher order displacement field that accurately captures the transverse shear deformation in moderately thick laminates. The model was then extended to include internal damage in the form of delamination and matrix cracking. When delamination is present, the sublaminates are modeled as individual plates and continuity is enforced at the interfaces. Matrix cracking was modeled as a reduction in laminate stiffness using parameters determined using finite element analysis of a representative crack. Finally, the simultaneous optimization of both mechanical and electrical parameters in an adaptive structural system was studied. This study demonstrates how multidisciplinary optimization techniques, such as the Kreisselmeier-Steinhauser function, can be utilized to optimize both structural and electrical aspects of an adaptive structural system. Optimization of piezoelectric actuator placement and electrical circuitry was performed on passive electrical damping systems. Results show that the developed model is capable of accurately

  8. [Sonography of fetal growth behavior in maternal diabetes mellitus].

    Science.gov (United States)

    Hielscher, K; Renziehausen, K; Döring, E

    1989-01-01

    In the Gynaecological Hospital affiliated to the District Hospital of Karl-Marx-Stadt, which is a care centre for pregnant diabetic women, 363 diabetic women of classes White A-F 1779 were subjected to ultrasonic examinations between 1982 and 1988. In this connection, nominal-value graphs were prepared to show the biparietal diameter (BIP), the medium thorax diameter and the head-thorax index in dependence upon the gestational age. These nominal-value graphs give a general idea of the specific fetal growth behaviour in case of diabetes mellitus. They permit to reliably diagnose a fetal hypertrophy or hypotrophy. Moreover, they provide a starting point for a more effective coverage of gestational diabetics and open up new prospects for insulinisation.

  9. Numerical and experimental studies of delamination detection in short fiber reinforced composites using Lamb waves

    Science.gov (United States)

    Kudela, Pawel; Radzienski, Maciej; Ostachowicz, Wieslaw

    2016-04-01

    The aim of this paper is to present aspects of Lamb wave propagation in randomly oriented short fiber reinforce composites with delamination. Prediction of elastic constants is based on mechanics of composites, rule of mixture and total mass balance tailored to the spectral element mesh composed of 3D brick elements. Piezoelectric excitation as well as glue layer are taken into account. Complex full wave field includes multiple reflections at short fibers. This wave pattern is also obtained by the use of laser vibrometry confirming good quality of the model. Further studies are related to symmetrical and non-symmetrical delamination in respect to the thickness of the composite plate. Square delamination of the side length 10 mm is investigated. It has been found that reflections from delamination are mostly superimposed with reflections coming from short fibers. Hence, delamination detection by direct analysis of wave propagation pattern on the surface of the plate is ineffective. However, adaptive wavenumber filtering method overcome these difficulties and enables not only to detect the delamination but also is helpful for delamination size estimation. Moreover, the method is more effective if the full wavefield measurements are acquired on the surface of the plate which is closer to the delamination.

  10. Cathodic delamination: Quantification of ionic transport rates along coating-steel interfaces

    DEFF Research Database (Denmark)

    Sørensen, P.A.; Dam-Johansen, Kim; Weinell, C.E.

    2010-01-01

    and Fick's second law, under the assumption of a transport-controlled mechanism, show qualitative agreement with the observed delamination rates in 0.5 M sodium chloride. This confirms that the rate-determining step of cathodic delamination is the transport of sodium ions along the coating-steel interface....

  11. Cathodic delamination: Quantification of ionic transport rates along coating-steel interfaces

    DEFF Research Database (Denmark)

    Sørensen, Per Aggerholm; Dam-Johansen, Kim; Erik Weinell, Claus

    2010-01-01

    and Fick's second law, under the assumption of a transport controlled mechanism, show qualitative agreement with the observed delamination rates in 0.5 M sodium chloride. This confirms that the rate-determining step of cathodic delamination is the transport of sodium ions along the coating-steel interface...

  12. Work of adhesion in laser-induced delamination along polymer-metal interfaces

    NARCIS (Netherlands)

    Fedorov, A.; van Tijum, R.; Vellinga, W. P.; de Hosson, Jeff

    2007-01-01

    Laser-induced delamination is a recent technique aimed at characterizing adhesive strength of thin polymer coatings on metal substrates. A laser pulse is used to create a blister that initiates further delamination of the film under pressure. To process the experimental data a simple elastic model w

  13. Reliability at the Chip Interfaces: Delaminating the Silicon Die from Molding Compound

    NARCIS (Netherlands)

    Schlottig, G.

    2012-01-01

    This book describes a setup that allows to delaminate the Silicon-to-Molding Compound interface for obtaining interfacial fracture parameters: the Mixed Mode Chisel setup (MMC). With this device for the first time the delamination can be initiated and propagated, while preventing the occurrence of r

  14. Buckling of composite beams with two enveloped delaminations: Lower and upper bounds

    NARCIS (Netherlands)

    Parlapalli, M.S.R.; Shu, Dongwei; Chai, Gin B.

    2008-01-01

    Lower and upper bounds of the buckling load of a composite beam with two enveloped delaminations are obtained from newly developed analytical models. The characteristic equation, governing the delamination buckling is derived by using Euler–Bernoulli beam and classical lamination theory, performing

  15. Reliability at the Chip Interfaces: Delaminating the Silicon Die from Molding Compound

    NARCIS (Netherlands)

    Schlottig, G.

    2012-01-01

    This book describes a setup that allows to delaminate the Silicon-to-Molding Compound interface for obtaining interfacial fracture parameters: the Mixed Mode Chisel setup (MMC). With this device for the first time the delamination can be initiated and propagated, while preventing the occurrence of r

  16. Cyclical Behavior of Inventories and Growth Projections Recent Evidence From Europe and the United States

    OpenAIRE

    Alexander W. Hoffmaister; Jens R Clausen

    2010-01-01

    In the United States and a few European countries, inventory behavior is mainly the outcome of demand shocks: a standard buffer-stock model best characterizes these economies. But most European countries are described by a modified buffer-stock model where supply shocks dominate. In contrast to the United States, inventories boost growth with a one-year lag in Europe. Moreover, inventories provide limited information to improve growth forecasts particularly when a modified buffer-stock model ...

  17. Study of multilayer packaging delamination mechanisms using different surface analysis techniques

    Energy Technology Data Exchange (ETDEWEB)

    Garrido-Lopez, Alvaro [Department of Chemistry, University of La Rioja, C/Madre de Dios 51, E-26006 Logrono, La Rioja (Spain); Tena, Maria Teresa, E-mail: maria-teresa.tena@unirioja.es [Department of Chemistry, University of La Rioja, C/Madre de Dios 51, E-26006 Logrono, La Rioja (Spain)

    2010-04-01

    Multilayer packaging, consisting of different layers joined by using an adhesive or an extrusion process, is widely used to promote different products, such as food, cosmetics, etc. The main disadvantage in using this form of packaging is the delamination process. In this work, different surface techniques (X-ray photoelectron spectroscopy, time-of-flight secondary ion mass spectroscopy and attenuated total reflection Fourier transform infrared spectroscopy) are used to analyse the delaminated surfaces in order to study the mechanisms that cause delamination of multilayer packaging. According to our results, the reaction of migrated molecules with adhesive-aluminium bonds is the main cause of the chemical delamination process. In contrast, the delamination of extruded materials would seem to be caused by the breaking of Van der Waals bonds.

  18. The interplay of crack hopping, delamination and interface failure in drying nanoparticle films

    Science.gov (United States)

    Yang, Bin; Sharp, James S.; Smith, Mike I.

    2016-08-01

    Films formed through the drying of nanoparticle suspensions release the build-up of strain through a variety of different mechanisms including shear banding, crack formation and delamination. Here we show that important connections exist between these different phenomena: delamination depends on the dynamics of crack hopping, which in turn is influenced by the presence of shear bands. We also show that delamination does not occur uniformly across the film. As cracks hop they locally initiate the delamination of the film which warps with a timescale much longer than that associated with the hopping of cracks. The motion of a small region of the delamination front, where the shear component of interfacial crack propagation is believed to be enhanced, results in the deposition of a complex zig-zag pattern on the supporting substrate.

  19. Corrosion Fatigue Crack Growth Behavior at Notched Hole in 7075-T6 Under Biaxial and Uniaxial Fatigue with Different Phases

    Science.gov (United States)

    2015-09-17

    CORROSION FATIGUE CRACK GROWTH BEHAVIOR AT NOTCHED HOLE IN 7075-T6 UNDER BIAXIAL AND UNIAXIAL FATIGUE WITH DIFFERENT PHASES... CORROSION FATIGUE CRACK GROWTH BEHAVIOR AT NOTCHED HOLE IN 7075-T6 UNDER BIAXIAL AND UNIAXIAL FATIGUE WITH DIFFERENT PHASES THESIS...UNLIMITED AFIT-ENY-MS-15-S-065 CORROSION FATIGUE CRACK GROWTH BEHAVIOR AT NOTCHED HOLE IN 7075-T6 UNDER BIAXIAL AND UNIAXIAL FATIGUE WITH

  20. Numerical investigation of ductile crack growth behavior in a dissimilar metal welded joint

    Energy Technology Data Exchange (ETDEWEB)

    Wang, H.T. [MOE Key Laboratory of Pressurized System and Safety, School of Mechanical and Power Engineering, East China University of Science and Technology, Shanghai 200237 (China); Wang, G.Z., E-mail: gzwang@ecust.edu.cn [MOE Key Laboratory of Pressurized System and Safety, School of Mechanical and Power Engineering, East China University of Science and Technology, Shanghai 200237 (China); Xuan, F.Z.; Tu, S.T. [MOE Key Laboratory of Pressurized System and Safety, School of Mechanical and Power Engineering, East China University of Science and Technology, Shanghai 200237 (China)

    2011-08-15

    Highlights: > Ductile crack growth behavior in a dissimilar metal welded joint was simulated. > Interface crack growth tends to deviate into material with lower yield stress. > Crack locations and mismatches affect local stress-strain distribution. > Local stress-strain leads to different crack growth resistances and paths. - Abstract: In this paper, the finite element method (FEM) based on GTN model is used to investigate the ductile crack growth behavior in single edge-notched bend (SENB) specimens of a dissimilar metal welded joint (DMWJ) composed of four materials in the primary systems of nuclear power plants. The J-{Delta}a resistance curves, crack growth paths and local stress-strain distributions in front of crack tips are calculated for eight initial cracks with different locations in the DMWJ and four cracks in the four homogenous materials. The results show that the initial cracks with different locations in the DMWJ have different crack growth resistances and growth paths. When the initial crack lies in the centers of the weld Alloy182 and buttering Alloy82, the crack-tip plastic and damage zones are symmetrical, and the crack grow path is nearly straight along the initial crack plane. But for the interface cracks between materials and near interface cracks, the crack-tip plastic and damage zones are asymmetric, and the crack growth path has significant deviation phenomenon. The crack growth tends to deviate into the material whose yield stress is lower between the two materials on both sides of the interface. The different initial crack locations and mismatches in yield stress and work hardening between different materials in the DMWJ affect the local stress triaxiality and plastic strain distributions in front of crack tips, and lead to different ductile crack growth resistances and growth paths. For the accurate integrity assessment for the DMWJ, the fracture toughness data and resistance curves for the initial cracks with different locations in the

  1. Catalystlike behavior of Si adatoms in the growth of monolayer Al film on Si(111).

    Science.gov (United States)

    Teng, Jing; Zhang, Lixin; Jiang, Ying; Guo, Jiandong; Guo, Qinlin; Wang, Enge; Ebert, Philipp; Sakurai, T; Wu, Kehui

    2010-07-07

    The formation mechanism of monolayer Al(111)1x1 film on the Si(111) radical3x radical3-Al substrate was studied by scanning tunneling microscopy and first-principles calculations. We found that the Si adatoms on the radical3x radical3-Al substrate play important roles in the growth process. The growth of Al-1x1 islands is mediated by the formation and decomposition of SiAl(2) clusters. Based on experiments and theoretical simulations we propose a model where free Si atoms exhibit a catalystlike behavior by capturing and releasing Al atoms during the Al film growth.

  2. Living bacteria rheology: population growth, aggregation patterns, and collective behavior under different shear flows.

    Science.gov (United States)

    Patrício, P; Almeida, P L; Portela, R; Sobral, R G; Grilo, I R; Cidade, T; Leal, C R

    2014-08-01

    The activity of growing living bacteria was investigated using real-time and in situ rheology-in stationary and oscillatory shear. Two different strains of the human pathogen Staphylococcus aureus-strain COL and its isogenic cell wall autolysis mutant, RUSAL9-were considered in this work. For low bacteria density, strain COL forms small clusters, while the mutant, presenting deficient cell separation, forms irregular larger aggregates. In the early stages of growth, when subjected to a stationary shear, the viscosity of the cultures of both strains increases with the population of cells. As the bacteria reach the exponential phase of growth, the viscosity of the cultures of the two strains follows different and rich behaviors, with no counterpart in the optical density or in the population's colony-forming units measurements. While the viscosity of strain COL culture keeps increasing during the exponential phase and returns close to its initial value for the late phase of growth, where the population stabilizes, the viscosity of the mutant strain culture decreases steeply, still in the exponential phase, remains constant for some time, and increases again, reaching a constant plateau at a maximum value for the late phase of growth. These complex viscoelastic behaviors, which were observed to be shear-stress-dependent, are a consequence of two coupled effects: the cell density continuous increase and its changing interacting properties. The viscous and elastic moduli of strain COL culture, obtained with oscillatory shear, exhibit power-law behaviors whose exponents are dependent on the bacteria growth stage. The viscous and elastic moduli of the mutant culture have complex behaviors, emerging from the different relaxation times that are associated with the large molecules of the medium and the self-organized structures of bacteria. Nevertheless, these behaviors reflect the bacteria growth stage.

  3. Analysis of Vero cell growth behavior on microcarrier by means of environmental scanning electron microscopy

    Institute of Scientific and Technical Information of China (English)

    SHAO; Manjun(邵曼君); JIANG; Lei(姜蕾); CONG; Wei(丛威); OUYANG; Fan(欧阳藩)

    2002-01-01

    By using environmental scanning electron microscopy, the morphological changes of Vero cells attached to and grown on the microcarrier Cytodex-3 were observed, and their behavior of adhesion, spreading and proliferation was analyzed. The effect of exogenous fibronectin/ laminin on adhesion and spreading of MCC/Vero cell was studied. The images of ESEM showed that expansion of cell growth was directed toward vacancy space. The growth curve and cell concentration change during the whole culture process were obtained from the statistical counting method based on ESEM images and the crystal violet method. The growth rate of Vero cells increases with increasing the concentration of cell inoculation, that is, the specific growth rate increases quickly with increasing the concentration of cell inoculation. When serum concentration in medium #199 ranged from 5% to 10%, experimental results indicated that serum concentration is one of the important factors influencing cell growth, particularly in the cell adhesion and spreading stage.

  4. Skin Conductance Level Reactivity Moderates the Association Between Harsh Parenting and Growth in Child Externalizing Behavior

    Science.gov (United States)

    Erath, Stephen A.; El-Sheikh, Mona; Hinnant, J. Benjamin; Cummings, E. Mark

    2011-01-01

    Skin conductance level reactivity (SCLR) was examined as a moderator of the association between harsh parenting at age 8 years and growth in child externalizing behavior from age 8 to age 10 (N = 251). Mothers and fathers provided reports of harsh parenting and their children’s externalizing behavior; children also provided reports of harsh parenting. SCLR was assessed in response to a socioemotional stress task and a problem-solving challenge task. Latent growth modeling revealed that boys with higher harsh parenting in conjunction with lower SCLR exhibited relatively high and stable levels of externalizing behavior during late childhood. Boys with higher harsh parenting and higher SCLR exhibited relatively low to moderate levels of externalizing behavior at age 8, but some results suggested that their externalizing behavior increased over time, approaching the same levels as boys with higher harsh parenting and lower SCLR by age 10. For the most part, girls and boys with lower harsh parenting were given relatively low and stable ratings of externalizing behavior throughout late childhood. Results are discussed from a developmental psychopathology perspective with reference to models of antisocial behavior in childhood. PMID:21142369

  5. Artificial Plant Root System Growth for Distributed Optimization: Models and Emergent Behaviors

    Directory of Open Access Journals (Sweden)

    Su Weixing

    2016-01-01

    Full Text Available Plant root foraging exhibits complex behaviors analogous to those of animals, including the adaptability to continuous changes in soil environments. In this work, we adapt the optimality principles in the study of plant root foraging behavior to create one possible bio-inspired optimization framework for solving complex engineering problems. This provides us with novel models of plant root foraging behavior and with new methods for global optimization. This framework is instantiated as a new search paradigm, which combines the root tip growth, branching, random walk, and death. We perform a comprehensive simulation to demonstrate that the proposed model accurately reflects the characteristics of natural plant root systems. In order to be able to climb the noise-filled gradients of nutrients in soil, the foraging behaviors of root systems are social and cooperative, and analogous to animal foraging behaviors.

  6. Subcritical crack growth behavior of AI2O3-Glass dental composites

    NARCIS (Netherlands)

    Zhu, Q.; With, G. de; Dortmans, L.J.M.G.; Feenstra, F.

    2003-01-01

    The purpose of this study is to investigate the subcritical crack growth (SCG) behavior of alumina-glass dental composites. Alumina-glass composites were fabricated by infiltrating molten glass to porous alumina preforms. Rectangular bars of the composite were subject to dynamic loading in air, with

  7. Meat supplementation improves growth, cognitive, and behavioral outcomes in Kenyan children

    NARCIS (Netherlands)

    Neumann, C.G.; Murphy, S.P.; Gewa, C.; Grillenberger, M.; Bwibo, N.O.

    2007-01-01

    A randomized, controlled school feeding study was conducted in rural Embu District, Kenya to test for a causal link between animal-source food intake and changes in micronutrient nutrition and growth, cognitive, and behavioral outcomes. Twelve primary schools were randomly assigned to 1 of 4 groups.

  8. How Do Students' Behaviors Relate to the Growth of Their Mathematical Ideas?

    Science.gov (United States)

    Warner, Lisa B.

    2008-01-01

    The purpose of this study is to analyze the relationship between student behaviors and the growth of mathematical ideas (using the Pirie-Kieren model). This analysis was accomplished through a series of case studies, involving middle school students of varying ability levels, who were investigating a combinatorics problem in after-school…

  9. A Longitudinal Study of Children's Social Behaviors and Their Causal Relationship to Reading Growth

    Science.gov (United States)

    Lim, Hyo Jin; Kim, Junyeop

    2011-01-01

    This paper aims at investigating the causal effects of social behaviors on subsequent reading growth in elementary school, using the "Early Childhood Longitudinal Study-Kindergarten" ("ECLS-K") data. The sample was 8,869 subjects who provided longitudinal measures of reading IRT scores from kindergarten (1998-1999) to fifth…

  10. Behavior and sensitivity of an optimal tree diameter growth model under data uncertainty

    Science.gov (United States)

    Don C. Bragg

    2005-01-01

    Using loblolly pine, shortleaf pine, white oak, and northern red oak as examples, this paper considers the behavior of potential relative increment (PRI) models of optimal tree diameter growth under data uncertainity. Recommendations on intial sample size and the PRI iteractive curve fitting process are provided. Combining different state inventories prior to PRI model...

  11. Subcritical crack growth behavior of AI2O3-Glass dental composites

    NARCIS (Netherlands)

    Zhu, Q.; With, G. de; Dortmans, L.J.M.G.; Feenstra, F.

    2003-01-01

    The purpose of this study is to investigate the subcritical crack growth (SCG) behavior of alumina-glass dental composites. Alumina-glass composites were fabricated by infiltrating molten glass to porous alumina preforms. Rectangular bars of the composite were subject to dynamic loading in air, with

  12. The ‘Sticky Elastica’: delamination blisters beyond small deformations

    KAUST Repository

    Wagner, Till J. W.

    2013-01-01

    We consider the form of an elastic loop adhered to a rigid substrate: the \\'Sticky Elastica\\'. In contrast to previous studies of the shape of delamination \\'blisters\\', the theory developed accounts for deflections with large slope (i.e. geometrically nonlinear). Starting from the classical Euler Elastica we provide numerical results for the dimensions of such blisters for a variety of end-end confinements and develop asymptotic expressions that reproduce these results well, even up to the point of self-contact. Interestingly, we find that the width of such blisters does not grow monotonically with increased confinement. Our theoretical predictions are confirmed by simple desktop experiments and suggest a new method for the measurement of the elastocapillary length for deformations that cannot be considered small. We discuss the implications of our results for applications such as flexible electronics. © 2013 The Royal Society of Chemistry.

  13. Ductile film delamination from compliant substrates using hard overlayers

    Energy Technology Data Exchange (ETDEWEB)

    Cordill, M.J. [Erich Schmid Institute of Materials Science, Austrian Academy of Sciences (Austria); Marx, V.M.; Kirchlechner, C. [Max-Plank-Insitut für Eisenforschung GmbH, Düsseldorf (Germany)

    2014-11-28

    Flexible electronic devices call for copper and gold metal films to adhere well to polymer substrates. Measuring the interfacial adhesion of these material systems is often challenging, requiring the formulation of different techniques and models. Presented here is a strategy to induce well defined areas of delamination to measure the adhesion of copper films on polyimide substrates. The technique utilizes a stressed overlayer and tensile straining to cause buckle formation. The described method allows one to examine the effects of thin adhesion layers used to improve the adhesion of flexible systems. - Highlights: • Measuring the adhesion energies of ductile metal–polymer interfaces is difficult. • A Cu film would plastically deform under tensile strain without a Cr overlayer. • A Cr overlayer forces cracking and induces buckling between the crack fragments. • The adhesion energy of the metal–polymer interface can be measured.

  14. Growth behavior and properties of nano Pb quantum islands on Si(111) surfaces at low temperatures

    Science.gov (United States)

    Tsong, Tien T.

    2004-03-01

    Quantum effects can affect the dynamic properties of surface atoms and the growth behavior of nanometer size islands. Using scanning tunneling microscopy (STM), we have studied: 1) Dynamics of atoms and silicon magic clusters on clean Si(111)-7x7 surfaces. 2) How the electronic property affects the growth behavior of Pb ultra-thin quantum-islands on the Si(111) surface. We find the low temperature growth of Pb quantum-islands on the Si(111)-7x7 surface is affected by the electronic standing wave states formed in the normal direction of these islands. The scaling behavior in the growth of these multilayer flat-top quantum islands can be described by a scaling theory of growth of single layer 2D islands with a minor modification. 3) Observed the vertical Friedel oscillation of the electronic Morie patterns formed at the Pb-Si interface and found the decay of the amplitude to follow the inverse square of the distance to the interface. 4) Observed the dynamics of a structure phase transition of monolayer quasi two dimensional Pb islands and its size effect. These and other recent interesting observations of ours will be presented. Coworkers: C-S Chang, I-S Hwang, W-B Su, M-S Ho, W-B Jian, and S-H Chang etc. Work supported by NSC of Taiwan and Academia Sinica (Taiwan).

  15. Monitoring Delamination of Thermal Barrier Coatings by Near-Infrared and Upconversion Luminescence Imaging

    Science.gov (United States)

    Eldridge, J. I.; Martin, R. E.; Singh, Jogender; Wolfe, Doug E.

    2008-01-01

    Previous work has demonstrated that TBC delamination can be monitored by incorporating a thin luminescent sublayer that produces greatly increased luminescence intensity from delaminated regions of the TBC. Initial efforts utilized visible-wavelength luminescence from either europium or erbium doped sublayers. This approach exhibited good sensitivity to delamination of electron-beam physical-vapor-deposited (EB-PVD) TBCs, but limited sensitivity to delamination of the more highly scattering plasma-sprayed TBCs due to stronger optical scattering and to interference by luminescence from rare-earth impurities. These difficulties have now been overcome by new strategies employing near-infrared (NIR) and upconversion luminescence imaging. NIR luminescence at 1550 nm was produced in an erbium plus ytterbium co-doped yttria-stabilized zirconia (YSZ) luminescent sublayer using 980-nm excitation. Compared to visible-wavelength luminescence, these NIR emission and excitation wavelengths are much more weakly scattered by the TBC and therefore show much improved depth-probing capabilities. In addition, two-photon upconversion luminescence excitation at 980 nm wavelength produces luminescence emission at 562 nm with near-zero fluorescence background and exceptional contrast for delamination indication. The ability to detect TBC delamination produced by Rockwell indentation and by furnace cycling is demonstrated for both EB-PVD and plasma-sprayed TBCs. The relative strengths of the NIR and upconversion luminescence methods for monitoring TBC delamination are discussed.

  16. Prenatal corticosterone exposure programs growth, behavior, reproductive function and genes in the chicken

    Directory of Open Access Journals (Sweden)

    Abdelkareem A. Ahmed

    2016-07-01

    Full Text Available The aim of this review paper was to understand the role of prenatal corticosterone exposure on growth, aggressive behavior, reproductive performance and gene expression in the chicken. The phenotype, physiology, reproductive function and behavioral characteristics of an organism are not only influenced by genetic factors, but also by environmental factors that play a critical role in shaping offspring morphology. Exposure to excess glucocorticoids during embryonic development influences offspring growth, physiology and behaviors associated with alterations of hypothalamic-pituitary-adrenal axis, hypothalamic-pituitary-gonadal axis and serotonergic system gene expression. Another influential factor for phenotype, physiology and behavioral development is maternal derived steroid hormones that deposit in the egg. In avian species, maternal influences have aroused much attention after the discovery that avian eggs contain a variety of maternal derived steroid hormones. In addition, the environment condition during ontogeny has played a critical role in behavioral development. In avian species, for example laying chicken, high quality mother care produced chicks that were less fearful. Laying hen maternal care is found to reduce cannibalistic pecking phenomenon. Genetic selection and selection experiments will also play a critical role in animals breeding for the housing systems of the future. To optimize animal welfare and to reduce risks factors such as pecking behavior, fundamental approaches are required that merge selection of the optimal genotype with provision of a positive environment for parents and offspring, both throughout ontogeny and later life.

  17. Ethogram of Immature Green Turtles: Behavioral Strategies for Somatic Growth in Large Marine Herbivores.

    Science.gov (United States)

    Okuyama, Junichi; Nakajima, Kana; Noda, Takuji; Kimura, Satoko; Kamihata, Hiroko; Kobayashi, Masato; Arai, Nobuaki; Kagawa, Shiro; Kawabata, Yuuki; Yamada, Hideaki

    2013-01-01

    Animals are assumed to obtain/conserve energy effectively to maximise their fitness, which manifests itself in a variety of behavioral strategies. For marine animals, however, these behavioral strategies are generally unknown due to the lack of high-resolution monitoring techniques in marine habitats. As large marine herbivores, immature green turtles do not need to allocate energy to reproduction but are at risk of shark predation, although it is a rare occurrence. They are therefore assumed to select/use feeding and resting sites that maximise their fitness in terms of somatic growth, while avoiding predation. We investigated fine-scale behavioral patterns (feeding, resting and other behaviors), microhabitat use and time spent on each behavior for eight immature green turtles using data loggers including: depth, global positioning system, head acceleration, speed and video sensors. Immature green turtles at Iriomote Island, Japan, spent an average of 4.8 h feeding on seagrass each day, with two peaks, between 5∶00 and 9∶00, and between 17∶00 and 20∶00. This feeding pattern appeared to be restricted by gut capacity, and thus maximised energy acquisition. Meanwhile, most of the remaining time was spent resting at locations close to feeding grounds, which allowed turtles to conserve energy spent travelling and reduced the duration of periods exposed to predation. These behavioral patterns and time allocations allow immature green turtles to effectively obtain/conserve energy for growth, thus maximising their fitness.

  18. Ethogram of Immature Green Turtles: Behavioral Strategies for Somatic Growth in Large Marine Herbivores.

    Directory of Open Access Journals (Sweden)

    Junichi Okuyama

    Full Text Available Animals are assumed to obtain/conserve energy effectively to maximise their fitness, which manifests itself in a variety of behavioral strategies. For marine animals, however, these behavioral strategies are generally unknown due to the lack of high-resolution monitoring techniques in marine habitats. As large marine herbivores, immature green turtles do not need to allocate energy to reproduction but are at risk of shark predation, although it is a rare occurrence. They are therefore assumed to select/use feeding and resting sites that maximise their fitness in terms of somatic growth, while avoiding predation. We investigated fine-scale behavioral patterns (feeding, resting and other behaviors, microhabitat use and time spent on each behavior for eight immature green turtles using data loggers including: depth, global positioning system, head acceleration, speed and video sensors. Immature green turtles at Iriomote Island, Japan, spent an average of 4.8 h feeding on seagrass each day, with two peaks, between 5∶00 and 9∶00, and between 17∶00 and 20∶00. This feeding pattern appeared to be restricted by gut capacity, and thus maximised energy acquisition. Meanwhile, most of the remaining time was spent resting at locations close to feeding grounds, which allowed turtles to conserve energy spent travelling and reduced the duration of periods exposed to predation. These behavioral patterns and time allocations allow immature green turtles to effectively obtain/conserve energy for growth, thus maximising their fitness.

  19. Fibroblast growth factor deficiencies impact anxiety-like behavior and the serotonergic system.

    Science.gov (United States)

    Brooks, Leah R; Enix, Courtney L; Rich, Samuel C; Magno, Jinno A; Lowry, Christopher A; Tsai, Pei-San

    2014-05-01

    Serotonergic neurons in the dorsal raphe nucleus (DR) are organized in anatomically distinct subregions that form connections with specific brain structures to modulate diverse behaviors, including anxiety-like behavior. It is unclear if the functional heterogeneity of these neurons is coupled to their developmental heterogeneity, and if abnormal development of specific DR serotonergic subregions can permanently impact anxiety circuits and behavior. The goal of this study was to examine if deficiencies in different components of fibroblast growth factor (Fgf) signaling could preferentially impact the development of specific populations of DR serotonergic neurons to alter anxiety-like behavior in adulthood. Wild-type and heterozygous male mice globally hypomorphic for Fgf8, Fgfr1, or both (Fgfr1/Fgf8) were tested in an anxiety-related behavioral battery. Both Fgf8- and Fgfr1/Fgf8-deficient mice display increased anxiety-like behavior as measured in the elevated plus-maze and the open-field tests. Immunohistochemical staining of a serotonergic marker, tryptophan hydroxylase (Tph), revealed reductions in specific populations of serotonergic neurons in the ventral, interfascicular, and ventrolateral/ventrolateral periaqueductal gray subregions of the DR in all Fgf-deficient mice, suggesting a neuroanatomical basis for increased anxiety-like behavior. Overall, this study suggests Fgf signaling selectively modulates the development of different serotonergic neuron subpopulations. Further, it suggests anxiety-like behavior may stem from developmental disruption of these neurons, and individuals with inactivating mutations in Fgf signaling genes may be predisposed to anxiety disorders.

  20. Mechanism of Electrochemical Delamination of Two-Dimensional Materials from Their Native Substrates by Bubbling

    Directory of Open Access Journals (Sweden)

    Jie Sun

    2015-12-01

    Full Text Available A capacitor-based circuit model is proposed to explain the electrochemical delamination of two-dimensional materials from their native substrates where produced gas bubbles squeeze into the interface. The delamination is actually the electric breakdown of the capacitor formed between the solution and substrate. To facilitate the procedure, the backside of the ubstrate has to be shielded so that the capacitor breakdown voltage can be reached. The screening effect can be induced either by nonreactive ions around the electrode or, more effectively, by an undetachable insulator. This mechanism serves as a guideline for the surface science and applications involving the bubbling delamination.

  1. Cdc42/N-WASP signaling links actin dynamics to pancreatic beta cell delamination and differentiation

    DEFF Research Database (Denmark)

    Kesavan, Gokul; Lieven, Oliver; Mamidi, Anant;

    2014-01-01

    to differentiation remains unknown. Using the developing mouse pancreas as a model system, we show that β cell delamination and differentiation are two independent events, which are controlled by Cdc42/N-WASP signaling. Specifically, we show that expression of constitutively active Cdc42 in β cells inhibits β cell......Delamination plays a pivotal role during normal development and cancer. Previous work has demonstrated that delamination and epithelial cell movement within the plane of an epithelium are associated with a change in cellular phenotype. However, how this positional change is linked...

  2. Corona Formation and Heat Loss on Venus by Coupled Upwelling and Delamination

    Science.gov (United States)

    Smrekar, Suzanne E.; Stofan, Ellen R.

    1997-01-01

    Coronae are volcanotectonic features that are unique to Venus and are interpreted to be small-scale upwellings. A model in which upwelling causes delamination at the edge of the plume head, along with deformation of a pre-existing depleted mantel Layer, can produce the full range of topographic forms of coronae. If half of the coronae are active, delamination of the lower lithosphere could account for about 10% of venus's heat loss, with another 15% due to upwelling. Delamination may occur in other geologic enviroment and could help account for 'Venus' heat loss 'deficit'.

  3. STOCHASTIC CRACKING AND HEALING BEHAVIORS OF THIN FILMS DURING REACTION-DIFFUSION GROWTH

    Institute of Scientific and Technical Information of China (English)

    S.L. Zhu; S.L. Yang; Y.M. Xiong; M.S. Li; S.J. Geng; C.S. Hu; Fuhui Wang; W. T. Wu

    2001-01-01

    The stochastic cracking and healing behaviors of reaction-diffusion growth of thin filmswere studied by means of Markov processes analysis. We chose the thermal growth ofoxide scales on metals as an example of reaction-diffusion growth. The thermal growthof oxide films follows power law when no cracking occurs. Our results showed that thegrowth kinetics under stochastic cracking and healing conditions was different fromthat without cracking. It might be altered to either pseudo-linear or pseudo-power lawsdependent upon the intensity and frequency of the cracking of the films. When thehoping items dominated, the growth followed pseudo-linear law; when the diffusionalitems dominated, it followed pseudo-power law with the exponentials lower than theintrinsical values. The numerical results were in good agreement with the meassuredkinetics of isothermal and cyclic oxidation of NiAl-0.1 Y (at. %) alloys in air at 1273K.

  4. Elevated temperature crack growth in advanced powder metallurgy aluminum alloys

    Science.gov (United States)

    Porr, William C., Jr.; Gangloff, Richard P.

    1990-01-01

    Rapidly solidified Al-Fe-V-Si powder metallurgy alloy FVS0812 is among the most promising of the elevated temperature aluminum alloys developed in recent years. The ultra fine grain size and high volume fraction of thermally stable dispersoids enable the alloy to maintain tensile properties at elevated temperatures. In contrast, this alloy displays complex and potentially deleterious damage tolerant and time dependent fracture behavior that varies with temperature. J-Integral fracture mechanics were used to determine fracture toughness (K sub IC) and crack growth resistance (tearing modulus, T) of extruded FVS0812 as a function of temperature. The alloy exhibits high fracture properties at room temperature when tested in the LT orientation, due to extensive delamination of prior ribbon particle boundaries perpendicular to the crack front. Delamination results in a loss of through thickness constraint along the crack front, raising the critical stress intensity necessary for precrack initiation. The fracture toughness and tensile ductility of this alloy decrease with increasing temperature, with minima observed at 200 C. This behavior results from minima in the intrinsic toughness of the material, due to dynamic strain aging, and in the extent of prior particle boundary delaminations. At 200 C FVS0812 fails at K levels that are insufficient to cause through thickness delamination. As temperature increases beyond the minimum, strain aging is reduced and delamination returns. For the TL orientation, K (sub IC) decreased and T increased slightly with increasing temperature from 25 to 316 C. Fracture in the TL orientation is governed by prior particle boundary toughness; increased strain localization at these boundaries may result in lower toughness with increasing temperature. Preliminary results demonstrate a complex effect of loading rate on K (sub IC) and T at 175 C, and indicate that the combined effects of time dependent deformation, environment, and strain aging

  5. Time-dependent Creep Crack Growth Behavior of Alloy 617 at 800 .deg. C

    Energy Technology Data Exchange (ETDEWEB)

    Kim, Woogon; Kim, Minhwan; Kim, Yongwan [Korea Atomic Energy Research Institute, Daejeon (Korea, Republic of); Park, Jaeyoung; Ekaputra, I. M. W. [Pukyong National Univ., Busan (Korea, Republic of)

    2014-05-15

    The VHTR components are designed to be used for a 60 year lifetime at a high temperature, the creep crack growth (CCG) behavior as well as creep behavior is very important for the design application due to creep damage during the long service life at elevated temperatures. Alloy 617 is a major candidate material for the IHX component. The design of the component, which will operate well into the creep range, will require a good understanding of creep crack growth deformation. Efforts are now being undertaken in the Generation IV program to provide data needed for the design and licensing of the nuclear plants, and with this goal in mind, to meet the needs of the conceptual designers of the VHTR system, 'Gen-IV Materials Handbook DB' is being established through an international collaboration program of several GIF (Gen-IV Forum) countries. CCG experimental data should be prepared to 'the Gen-IV Materials Handbook DB' website, because the CCG data for Alloy 617 are not available in the ASME design code. In this paper, experimental creep crack growth data were obtained through a series of CCG tests performed under different applied loads at 800 .deg. C. The CCG behavior was characterized in terms of the C{sup *} fracture mechanics parameter, and the CCGR equation for Alloy 617 was presented. Experimental CCG data of Alloy 617 were obtained from a series of creep crack growth tests under different applied loads at 800 .deg. C.

  6. Effect of the population heterogeneity on growth behavior and its estimation

    Institute of Scientific and Technical Information of China (English)

    ZHANG HuaiQiang; LU LiLi; YAN XueLan; GAO PeiJi

    2007-01-01

    Different types of the Logistic model are constructed based on a simple assumption that the microbial populations are all composed of homogeneous members and consequently, the condition of design for the initial value of these models has to be rather limited in the case of N(t0)=N0. Therefore, these models cannot distinguish the dynamic behavior of the populations possessing the same N0 from heterogeneous phases. In fact, only a certain ratio of the cells in a population is dividing at any moment during growth progress, termed as θ, and thus, dN/dt not only depends on N, but also on θ. So θis a necessary element for the condition design of the initial value. Unfortunately, this idea has long been neglected in widely used growth models. However, combining together the two factors (N0 and θ) into the initial value often leads to the complexity in the mathematical solution. This difficulty can be overcome by using instantaneous rates (Vinst) to express growth progress. Previous studies in our laboratory suggested that the Vinst curve of the bacterial populations all showed a Guassian function shape and thus,the different growth phases can be reasonably distinguished. In the present study, the Gaussian distribution function was transformed approximately into an analytical form (Yi = αe[-0.5(xi-x0/b)2]) that can be conveniently used to evaluate the growth parameters and in this way the intrinsic growth behavior of a bacterial species growing in heterogeneous phases can be estimated. In addition, a new method has been proposed, in this case, the lag period and the double time for a bacterial population can also be reasonably evaluated. This approach proposed could thus be expected to reveal important insight of bacterial population growth. Some aspects in modeling population growth are also discussed.

  7. Effect of the population heterogeneity on growth behavior and its estimation

    Institute of Scientific and Technical Information of China (English)

    2007-01-01

    Different types of the Logistic model are constructed based on a simple assumption that the microbial populations are all composed of homogeneous members and consequently, the condition of design for the initial value of these models has to be rather limited in the case of N(t0)=N0. Therefore, these models cannot distinguish the dynamic behavior of the populations possessing the same N0 from heteroge-neous phases. In fact, only a certain ratio of the cells in a population is dividing at any moment during growth progress, termed as θ, and thus, ddNt not only depends on N, but also on θ. So θ is a necessary element for the condition design of the initial value. Unfortunately, this idea has long been neglected in widely used growth models. However, combining together the two factors (N0 and θ ) into the initial value often leads to the complexity in the mathematical solution. This difficulty can be overcome by using instantaneous rates (Vinst) to express growth progress. Previous studies in our laboratory sug-gested that the Vinst curve of the bacterial populations all showed a Guassian function shape and thus, the different growth phases can be reasonably distinguished. In the present study, the Gaussian dis-tribution function was transformed approximately into an analytical form (0.5x ibxYi αe=20) that can be conveniently used to evaluate the growth parameters and in this way the intrinsic growth behavior of a bacterial species growing in heterogeneous phases can be estimated. In addition, a new method has been proposed, in this case, the lag period and the double time for a bacterial population can also be reasonably evaluated. This approach proposed could thus be expected to reveal important insight of bacterial population growth. Some aspects in modeling population growth are also discussed.

  8. Evaluation of NaCl Effect on Vibration-Delaminated Metal-Polymer Composites by Improved Micro-Raman Methodology

    Directory of Open Access Journals (Sweden)

    E. Zumelzu

    2013-01-01

    Full Text Available Polyethylene terephthalate (PET is a polymer coating that protects the electrolytic chromium coated steel (ECCS against aggressive electrolytes like NaCl. It is widely accepted by manufacturers that NaCl has no effect on the PET coating, which is inert. However, we showed that there are some effects at the structural level, caused by vibrations, and facilitated by defects on the layers. The vibrations occurring during the transportation of food containers produce delaminations at given points of the metal-polymer interface, known as antinodes, which in turn may produce PET degradation affecting food quality. The former can be determined by electrochemical measurements, and the changes in composition or structural order can be characterized by Raman. The present work applied this latter technique in experimental samples of PET-coated ECCS sheets by performing perpendicular and parallel analyses to the surface, and determined that it constitutes a new potential methodology to determine the behavior of the composite under the above conditions. The results demonstrated that the delamination areas on the PET facilitated polymer degradation by the electrolyte. Moreover, the Raman characterization evidenced the presence of multilayers and crystalline orderings, which limited its functionality as a protective coating.

  9. Dynamic Recrystallization and Grain Growth Behavior of 20SiMn Low Carbon Alloy Steel

    Institute of Scientific and Technical Information of China (English)

    DONG Lanfeng; ZHONG Yuexian; MA Qingxian; YUAN Chaolong; MA Lishen

    2008-01-01

    A senes of thermodynamics experiments were used to optimize the hot forging process of 20SiMn low-carbon alloy steel.A dynamic recrystallization and grain growth model was developed for the 20SiMn steel for common production conditions of heavy forgings by doing a nonlinear curve fit of the expenment data.Optimized forging parameters were developed based on the control of the dynamic recrystallization and the MnS secondary phase.The data shows that the initial grain size and the MnS secondary phase all affect the behavior of the 20SiMn dynamic recrystallization and grain growth.

  10. DELAMINATION PREDICTION IN DRILLING OF CFRP COMPOSITES USING ARTIFICIAL NEURAL NETWORK

    Directory of Open Access Journals (Sweden)

    K. PALANIKUMAR

    2011-04-01

    Full Text Available Carbon fibre reinforced plastic (CFRP materials play a major role in the applications of aeronautic, aerospace, sporting and transportation industries. Machining is indispensible and hence drilling of CFRP materials is considered in this present study with respect to spindle speed in rpm, drill size in mm and feed in mm/min. Delamination is one of the major defects to be dealt with. The experiments are carried out using computer numerical control machine and the results are applied to an artificial neural network (ANN for the prediction of delamination factor at the exit plane of the CFRP material. It is found that ANN model predicts the delamination for any given set of machining parameters with a maximum error of 0.81% and a minimum error of 0.03%. Thus an ANN model is highly suitable for the prediction of delamination in CFRP materials.

  11. Failure analysis of multiple delaminated composite plates due to bending and impact

    Indian Academy of Sciences (India)

    P K Parhi; S K Bhattacharyya; P K Sinha

    2001-04-01

    The present work aims at the first ply failure analysis of laminated composite plates with arbitrarily located multiple delaminations subjected to transverse static load as well as impact. The theoretical formulation is based on a simple multiple delamination model. Conventional first order shear deformation is assumed using eight-noded isoparametric quadratic elements to develop the finite element analysis procedure. Composite plates are assumed to contain both single and multiple delaminations. For the case of impact, Newmark time integration algorithm is employed for solving the time dependent multiple equations of the plate and the impactor. Tsai-Wu failure criterion is used to check for failure of the laminate for both the cases. To investigate the first ply failure, parametric studies are made for different cases by varying the size and number of delaminations as well as the stacking sequences and boundary conditions.

  12. Comparison of Nondestructive Testing Methods on Detection of Delaminations in Composites

    Directory of Open Access Journals (Sweden)

    Liang Cheng

    2012-01-01

    Full Text Available Delamination is one of the most common defects in carbon fibre reinforced plastic (CFRP components, such as those used in aircraft and wind turbine blades. To detect delaminations, different NDT methods such as ultrasonic (UT, eddy current (EC scanning, flash thermography, and recent developed pulsed-eddy-current-(PEC- simulated thermography are conducted for comparison and evaluation of the new developed PEC thermography system at Nanjing University of Aeronautics and Astronautics (NUAA, China through UK-China collaboration. A PEC-stimulated thermography system is built at NUAA, extended from previous joint work between Newcastle and Bath Universities. Using these NDT systems, man-made, dedicated delaminations with varied diameters and depths are investigated and studied. Through this comparison, PEC-stumilated and flash thermography show relatively good indications of the shape of delaminations. The joint studies also show that PEC-stimulated thermography has unique advantage for fibre orientation evaluation.

  13. Reduction of cathodic delamination rates of anticorrosive coatings using free radical scavengers

    DEFF Research Database (Denmark)

    Sørensen, Per Aggerholm; Weinell, C. E.; Dam-Johansen, Kim

    2010-01-01

    Cathodic delamination is one of the major modes of failure for anticorrosive coatings subjected to a physical damage and immersed in seawater. The cause of cathodic delamination has been reported to be the result of a chemical attack at the coating-steel interface by free radicals and peroxides...... formed as intermediates in the cathodic reaction during the corrosion process. In this study, antioxidants (i.e., free radical scavengers and peroxide decomposers) have been incorporated into various generic types of coatings to investigate the effect of antioxidants on the rate of cathodic delamination...... of epoxy coatings on cold rolled steel. The addition of cathodic delamination by up to 50% during seawater immersion, while peroxide decomposers had a limited effect. Testing using substrates prepared from stainless steel...

  14. Interaction of Guided Lamb Waves with Delaminations and Discontinuities in Composite Plate-Like Structures

    Science.gov (United States)

    Balasubramaniam, Krishnan; Ramadas, C.; Padiyar, Janardhan; Krishnamurthy, C. V.

    2011-06-01

    Delamination is one of the critical failure modes that laminated composites structures encounter during their fabrication and/or in-service. When guided Lamb wave (Ao) is employed for sizing of delamination, it is necessary to understand the wave interaction with the defect. Studies were carried out on the interaction of Ao mode with symmetric and asymmetric delaminations and transmission of turning modes in the sub-laminates. An attempt was also made to understand the propagation of Ao mode in composite structural T-joint. During the interaction of Ao mode with structural discontinuity in a T-joint, generation of a new mode, So, and propagation of turning modes were observed. Length and width of interface delamination in composite T-joint have been worked out using D-scan and B-scan respectively. All studied were carried out through numerical simulations and experimental verifications through Non- Contact Ultrasound (NCU) technique.

  15. Application of the Refined Zigzag Theory to the Modeling of Delaminations in Laminated Composites

    Science.gov (United States)

    Groh, Rainer M. J.; Weaver, Paul M.; Tessler, Alexander

    2015-01-01

    The Refined Zigzag Theory is applied to the modeling of delaminations in laminated composites. The commonly used cohesive zone approach is adapted for use within a continuum mechanics model, and then used to predict the onset and propagation of delamination in five cross-ply composite beams. The resin-rich area between individual composite plies is modeled explicitly using thin, discrete layers with isotropic material properties. A damage model is applied to these resin-rich layers to enable tracking of delamination propagation. The displacement jump across the damaged interfacial resin layer is captured using the zigzag function of the Refined Zigzag Theory. The overall model predicts the initiation of delamination to within 8% compared to experimental results and the load drop after propagation is represented accurately.

  16. Debonding/Delamination of Composites (Le Decollement et le Delaminage des Materiaux Composites)

    Science.gov (United States)

    1992-12-01

    bouthS sides of the delamination. Fig 8a. Ithese cratcks coincide with the delamination length Linder conipressise loadingthe 1.1D-sublaminate buckles like...Scientific 115] R.O. Duda, PE. Hart , "Pattern classification and scene Research (NFWO) for its funding Considerable help was also analysis", John...unidirectional laminates were performed with the technology of differential 2 MATERIALS AND PREPARATIONS scanning calorimetry A Du Pont DSC system, model 910, was

  17. Phase-field modeling of void anisotropic growth behavior in irradiated zirconium

    Energy Technology Data Exchange (ETDEWEB)

    Han, G. M.; Wang, H.; Lin, De-Ye; Zhu, X. Y.; Hu, S. Y.; Song, H. F.

    2017-06-01

    A three-dimensional (3D) phase field model was developed to study the effects of surface energy and diffusivity anisotropy on void growth behavior in irradiated Zr. The gamma surface energy function, which is used in the phase field model, was developed with the surface energy anisotropy calculated from the molecular dynamics (MD) simulations. It is assumed that vacancies have much larger mobility in c-axis than a- and b- axes while interstitials have much larger mobility in basal plane then that in c-axis. With the model, the equilibrium void morphology and the effect of defect concentrations and defect mobility anisotropy on void growth behavior were simulated. The simulations demonstrated that 1) The developed phase-field model can correctly reproduce the faceted void morphology predicted by the Wullf construction. 2) With isotropic diffusivity the void prefers to grow on the basal plane. 3) When the vacancy has large mobility along c-axis and interstitial has a large mobility on the basal plane of hexagonal closed packed (hcp) Zr alloys a platelet void grows in c-direction and shrinks on the basal plane, which is in agreement with the experimental observation of void growth behavior in irradiated Zr.

  18. Tunable and purified luminescence via energy transfer and delamination of LRH (R=Tb, Y) composites with 8-hydroxypyrene-1,3,6-trisulphonate.

    Science.gov (United States)

    Su, Feifei; Liu, Chenyu; Yang, Yan; Ma, Shulan; Sun, Genban; Yang, Xiaojing

    2017-06-15

    This work demonstrates tunable and purified luminescence via one-step delamination of HPTS/OS-LRH composites (HPTS is trisodium 8-hydroxy-pyrene-1,3,6-trisulphonate, OS is sodium salt of 1-octane sulfonic acid, LRH is layered rare-earth hydroxide, R=Tb, Y) along with energy transfer. The HPTSxOS1-x-LTbyY1-yH composites presented varied luminescence behavior depending on their physical state. In solid state, dual-color luminescence was observed: blue-dominant emissions (437nm) for HPTSxOS1-x-LTbH, and blue- (437nm) to green-dominant (516nm) luminescence for HPTS0.02OS0.98-LTbyY1-yH. In delaminated state in famamide, purified luminescence was present: pure blue emission (440nm) for HPTSxOS1-x-LTbH and HPTS0.02OS0.98-LTbyY1-yH (y≥0.5), while pure bluish-green emission (498nm) for HPTS0.02OS0.98-LTbyY1-yH (y≤0.3). Both the delamination of the composites and energy transfer from layer Tb(3+) to HPTS contributed to the blue luminescence. The intriguing energy transfer process between photoactive inorganic hosts and organic guests can be utilized to fabricate hybrid materials with superior luminescence property.

  19. Effects of coating thickness and interfacial roughness on cracking and delamination strength of WC-Co coating measured by ring compression test

    Science.gov (United States)

    Kato, Masahiko; Nazul, Mahmoud; Itti, Takeshi; Akebono, Hiroyuki; Sugeta, Atsushi; Mitani, Eiji

    2014-08-01

    The effects of coating thickness and interfacial roughness on the interfacial fracture toughness of tungsten carbide-cobalt (WC-Co) coatings were evaluated using a ring compression test. WC-Co powder was sprayed on steel (JIS:SS400) rings by a high-velocity air- fuel method in coatings with various thicknesses and values of interfacial roughness. The ring compression test was carried out, and the cracking and delamination behavior of the coatings was observed using charge-coupled-device cameras. The results showed that cracking perpendicular to the loading direction occurred in the coatings during the ring compression test, and the cracking strength obtained from the ring compression test decreased slightly with increasing coating thickness, but was independent of the interfacial roughness. Upon further increase of the compression load, the coatings delaminated from the substrate. The interfacial fracture toughness calculated from the delamination of the coatings during the ring compression test decreased with increasing coating thickness and increased with increasing interfacial roughness.

  20. Detection of drilling-induced delamination in aeronautical composites by noncontact laser ultrasonic method.

    Science.gov (United States)

    Zhou, Zhenggan; Sun, Guangkai; Chen, Xiucheng; Wang, Jie

    2014-04-20

    A novel application of the laser ultrasonic technique for the detection of drilling-induced delamination in composite components of aircrafts is proposed. Numerous key components of aircrafts are made of composite materials, and drilling is often a final operation during assembly. Drilling-induced delamination significantly reduces the structural reliability, and it is rather difficult to be detected effectively and automatically. The laser ultrasonic technique is a promising method to solve the problem. This paper investigates the characterization of drilling-induced delamination in composites by a noncontact laser ultrasonic method. A carbon fiber reinforced plastic laminate with drilling holes is prepared as a specimen. The characterization of drilling-induced delamination with laser-generated ultrasonic waves is investigated theoretically and experimentally, and the morphology features of the delamination are obtained by laser ultrasonic C-scan testing. The results prove that the laser ultrasonic technique is effective for the detection of drilling-induced delamination in composite components, and it is a feasible solution for evaluating the drilling quality during assembly.

  1. Delamination detection in composite laminates using dispersion change based on mode conversion of Lamb waves

    Science.gov (United States)

    Okabe, Yoji; Fujibayashi, Keiji; Shimazaki, Mamoru; Soejima, Hideki; Ogisu, Toshimichi

    2010-11-01

    A new ultrasonic propagation system has been constructed using macrofiber composite (MFC) actuators and fiber Bragg grating (FBG) sensors. The MFCs and FBGs can be integrated into composite laminates because of their small size and high fracture strain. The developed system can send and receive broadband Lamb waves. In this research, this system was used to detect delamination damage in composite laminates. First, the multiple modes of Lamb waves in a carbon-fiber-reinforced plastic (CFRP) quasi-isotropic laminate were identified by transmitting and receiving the symmetric and antisymmetric modes separately. Then, the mode conversions at both tips of a delamination were investigated through an experiment and a two-dimensional finite element analysis (FEA). A new delamination detection method was proposed on the basis of the mode conversions, and experiments were carried out on laminates with an artificial delamination. When antisymmetric modes were excited, the frequency dispersion of the received A1 mode changed, depending on the delamination length owing to the mode conversion between the A1 mode and the S0 mode. This phenomenon was confirmed through the FEA and these results prove that this new method is effective in detecting a delamination in CFRP laminates.

  2. Scattering of the fundamental anti-symmetric Lamb wave at delaminations in composite laminates.

    Science.gov (United States)

    Ng, Ching-Tai; Veidt, Martin

    2011-03-01

    An analysis of the scattering characteristics of the fundamental anti-symmetric (A(0)) Lamb wave at a delamination in a quasi-isotropic composite laminate is presented. Analytical solutions for this problem do not exist due to the anisotropic nature and multilayer characteristics of composite laminates. This study uses a three-dimensional finite element (FE) method and experimental measurements to provide physical insight into the scattering phenomena. Good agreement is found between simulations and experimental measurements. The results show that the A(0) Lamb wave scattering at a delamination in composite laminates is much more complicated than the scattering at a defect in isotropic plates. Scatter amplitudes and scatter directivity distributions depend on the delamination size to wavelength ratio and the through-thickness location of the delamination damage. The study also investigates the feasibility of the common experimental practice of simulating delamination damage by bonding masses to the surface of composite laminates for guided wave damage detection and characterization methodologies verifications. The results suggest that care is required to use bonded masses to simulate delamination damage for verifying and optimizing damage characterization techniques. In summary, the results of the investigation help to further advance the use of the A(0) Lamb wave for damage detection and characterization.

  3. Mechanistic Study of Delamination Fracture in Al-Li Alloy C458 (2099)

    Science.gov (United States)

    Tayon, W. A.; Crooks, R. E.; Domack, M. S.; Wagner, J. A.; Beaudoin, A. J.; McDonald, R. J.

    2009-01-01

    Delamination fracture has limited the use of lightweight Al-Li alloys. In the present study, electron backscattered diffraction (EBSD) methods were used to characterize crack paths in Al-Li alloy C458 (2099). Secondary delamination cracks in fracture toughness samples showed a pronounced tendency for fracture between grain variants of the same deformation texture component. These results were analyzed by EBSD mapping methods and simulated with finite element analyses. Simulation procedures include a description of material anisotropy, local grain orientations, and fracture utilizing crystal plasticity and cohesive zone elements. Taylor factors computed for each grain orientation subjected to normal and shear stresses indicated that grain pairs with the largest Taylor factor differences were adjacent to boundaries that failed by delamination. Examination of matching delamination fracture surface pairs revealed pronounced slip bands in only one of the grains bordering the delamination. These results, along with EBSD studies, plasticity simulations, and Auger electron spectroscopy observations support a hypothesis that delamination fracture occurs due to poor slip accommodation along boundaries between grains with greatly differing plastic response.

  4. Numerical investigation of nonlinear interactions between multimodal guided waves and delamination in composite structures

    Science.gov (United States)

    Shen, Yanfeng

    2017-04-01

    This paper presents a numerical investigation of the nonlinear interactions between multimodal guided waves and delamination in composite structures. The elastodynamic wave equations for anisotropic composite laminate were formulated using an explicit Local Interaction Simulation Approach (LISA). The contact dynamics was modeled using the penalty method. In order to capture the stick-slip contact motion, a Coulomb friction law was integrated into the computation procedure. A random gap function was defined for the contact pairs to model distributed initial closures or openings to approximate the nature of rough delamination interfaces. The LISA procedure was coded using the Compute Unified Device Architecture (CUDA), which enables the highly parallelized computation on powerful graphic cards. Several guided wave modes centered at various frequencies were investigated as the incident wave. Numerical case studies of different delamination locations across the thickness were carried out. The capability of different wave modes at various frequencies to trigger the Contact Acoustic Nonlinearity (CAN) was studied. The correlation between the delamination size and the signal nonlinearity was also investigated. Furthermore, the influence from the roughness of the delamination interfaces was discussed as well. The numerical investigation shows that the nonlinear features of wave delamination interactions can enhance the evaluation capability of guided wave Structural Health Monitoring (SHM) system. This paper finishes with discussion, concluding remarks, and suggestions for future work.

  5. Cdc42/N-WASP signaling links actin dynamics to pancreatic β cell delamination and differentiation

    Science.gov (United States)

    Kesavan, Gokul; Lieven, Oliver; Mamidi, Anant; Öhlin, Zarah Löf; Johansson, Jenny Kristina; Li, Wan-Chun; Lommel, Silvia; Greiner, Thomas Uwe; Semb, Henrik

    2014-01-01

    Delamination plays a pivotal role during normal development and cancer. Previous work has demonstrated that delamination and epithelial cell movement within the plane of an epithelium are associated with a change in cellular phenotype. However, how this positional change is linked to differentiation remains unknown. Using the developing mouse pancreas as a model system, we show that β cell delamination and differentiation are two independent events, which are controlled by Cdc42/N-WASP signaling. Specifically, we show that expression of constitutively active Cdc42 in β cells inhibits β cell delamination and differentiation. These processes are normally associated with junctional actin and cell-cell junction disassembly and the expression of fate-determining transcription factors, such as Isl1 and MafA. Mechanistically, we demonstrate that genetic ablation of N-WASP in β cells expressing constitutively active Cdc42 partially restores both delamination and β cell differentiation. These findings elucidate how junctional actin dynamics via Cdc42/N-WASP signaling cell-autonomously control not only epithelial delamination but also cell differentiation during mammalian organogenesis. PMID:24449844

  6. Clay-polymer nanocomposite material from the delamination of kaolinite in the presence of sodium polyacrylate.

    Science.gov (United States)

    Letaief, Sadok; Detellier, Christian

    2009-09-15

    A chemical route for the delamination of kaolinite in a polymeric matrix is reported in this work. The strategy that was used is based on mixing polyelectrolytes of opposite charges, an organic polyanion, polyacrylate, with an inorganic polycation resulting from the modification of the internal surfaces of kaolinite. The delamination was carried out by the reaction of sodium polyacrylate (PANa) with kaolinite whose internal aluminol surfaces were previously grafted with triethanolamine and subsequently quaternized with iodomethane (TOIM-K) to form an extended lamellar inorganic polycation. X-ray diffraction as well as scanning electron microscopy (SEM) confirmed the complete delamination of the kaolinite particles. 13C CP/MAS NMR showed the removal of the ammonium groups resulting from hydrolysis of the internal surfaces once exposed, and 29Si CP/MAS NMR spectra were in agreement with the retention of the 1:1 aluminosilicate kaolinite layers structures. From the thermogravimetry (TG) data, the respective percentages in mass of PA and kaolinite in the delaminated nanocomposite could be estimated to be 61% and 39%, respectively, in the conditions of the particular experiment. The procedure was repeated several times to show the reproducibility of the delamination. The interlayer functionalization of kaolinite was crucial for the success of the delamination procedure. SEM pictures show that some individual kaolinite platelets fold and form curved structures.

  7. Buckling delamination induced microchannel: Flow regulation in microfluidic devices

    Science.gov (United States)

    Kang, Jingtian; Wang, Changguo; Xue, Zhiming; Liu, Mengxiong; Tan, Huifeng

    2016-09-01

    The buckling delamination induced microchannel is employed to regulate fluid flow as a microvalve which can be utilized in microfluidic devices. This microvalve consists of a soft substrate and a stiff thin film, between which there is a pre-set small imperfection. Two critical strain values, namely, on-off strain and failure strain, have been proposed to determine the working strain interval using analytical predictions. Within this interval, the cross-sectional area of the microchannel can be controlled and predicted by different compressive strains of the film/substrate system. The fluid flow rate within this microchannel can be then estimated by both analytical and numerical simulations and adjusted to satisfy different values by alternating the compressive strain. In addition, a demonstrative experiment has been taken to verify the feasibility of this approach. This flexible microvalve has potential in the application where the use of traditional rigid microvalves is improper in flexible microfluidic devices. The method and approach of this paper can provide a general guide for flow rate control in microfluidic devices.

  8. Effect of Isothermal Temperature on Growth Behavior of Nanostructured Bainite in Laser Cladded Coatings.

    Science.gov (United States)

    Guo, Yanbing; Yao, Chengwu; Feng, Kai; Li, Zhuguo; Chu, Paul K; Wu, Yixiong

    2017-07-14

    The growth and propagation behavior of austenite-to-bainite isothermal transformation in laser-cladded, Si-rich, and Fe-based coatings is investigated. The crystallographic features, orientation relationship at different isothermal temperatures, and the morphology of the nanostructured bainite are determined. The Nishiyama-Wassermann type orientation relationship is observed at a high temperature and at a low temperature, and mixed Nishiyama-Wassermann and Kurdjumov-Sach mechanisms are seen. The growth direction is investigated by the partial dislocation theory and an extrapolated model based on the repeated formation of lenticular-shaped subunits and pile-up along the close-packed directions of the close-packed planes. The variants of the bainite growth directions would be more selective at the high transformation temperature.

  9. Mating behavior, population growth, and the operational sex ratio: a periodic two-sex model approach.

    Science.gov (United States)

    Jenouvrier, Stéphanie; Caswell, Hal; Barbraud, Christophe; Weimerskirch, Henri

    2010-06-01

    We present a new approach to modeling two-sex populations, using periodic, nonlinear two-sex matrix models. The models project the population growth rate, the population structure, and any ratio of interest (e.g., operational sex ratio). The periodic formulation permits inclusion of highly seasonal behavioral events. A periodic product of the seasonal matrices describes annual population dynamics. The model is nonlinear because mating probability depends on the structure of the population. To study how the vital rates influence population growth rate, population structure, and operational sex ratio, we used sensitivity analysis of frequency-dependent nonlinear models. In nonlinear two-sex models the vital rates affect growth rate directly and also indirectly through effects on the population structure. The indirect effects can sometimes overwhelm the direct effects and are revealed only by nonlinear analysis. We find that the sensitivity of the population growth rate to female survival is negative for the emperor penguin, a species with highly seasonal breeding behavior. This result could not occur in linear models because changes in population structure have no effect on per capita reproduction. Our approach is applicable to ecological and evolutionary studies of any species in which males and females interact in a seasonal environment.

  10. AE analysis of delamination crack propagation in carbon fiber-reinforced polymer materials

    Energy Technology Data Exchange (ETDEWEB)

    Yoon, Sang Jae; Arakawa, Kazuo [Kyushu University, kasuga (Japan); Chen, Dingding [National University of Defense Technology, Changsha (China); Han, Seung Wook; Choi, Nak Sam [Hanyang University, Seoul (Korea, Republic of)

    2015-01-15

    Delamination fracture behavior was investigated using acoustic emission (AE) analysis on carbon fiber-reinforced polymer (CFRP) samples manufactured using vacuum-assisted resin transfer molding (VARTM). CFRP plate was fabricated using unidirectional carbon fiber fabric with a lay-up of six plies [+30/-30]6 , and a Teflon film was inserted as a starter crack. Test pieces were sectioned from the inlet and vent of the mold, and packed between two rectangular epoxy plates to load using a universal testing machine. The AE signals were monitored during tensile loading using two sensors. The average tensile load of the inlet specimens was slightly larger than that of the vent specimens; however, the data exhibited significant scattering due to non-uniform resin distribution, and there was no statistically significant different between the strength of the samples sectioned from the inlet or outlet of the mold. Each of the specimens exhibited similar AE characteristics, regardless of whether they were from the inlet or vent of the mold. Four kinds of damage mechanism were observed: micro-cracking, fiber-resin matrix debonding, fiber pull-out, and fiber failure; and three stages of the crack propagation process were identified.

  11. Effect of behavior training on learning and memory of young rats with fetal growth restriction

    Institute of Scientific and Technical Information of China (English)

    Li Xuelan; Gou Wenli; Huang Pu; Li Chunfang; Sun Yunping

    2008-01-01

    Objective: To investigate the effect of behavior training on the learning and memory of young rats with fetal growth restriction (FGR). Methods: The model of FGR was established by passive smoking method to pregnant rats.The new-born rats were divided into FGR group and normal group, and then randomly subdivided into trained and untrained group respectively. Morris water maze behavior training was performed on postnatal months 2 and 4, then learning and memory abilities of young rats were measured by dark-avoidance testing and step-down testing. Results: In the dark-avoidance and step-down testing, the young rats' performance of FGR group was worse than that of control group, and the trained group was better than the untrained group significantly. Conclusion: FGR young rats have descended learning and memory abilities. Behavior training could improve the young rats' learning and memory abilities, especially for the FGR young rats.

  12. Complex Nonlinear Behavior in Metabolic Processes: Global Bifurcation Analysis of Escherichia coli Growth on Multiple Substrates

    Directory of Open Access Journals (Sweden)

    Hyun-Seob Song

    2013-09-01

    Full Text Available The nonlinear behavior of metabolic systems can arise from at least two different sources. One comes from the nonlinear kinetics of chemical reactions in metabolism and the other from nonlinearity associated with regulatory processes. Consequently, organisms at a constant growth rate (as experienced in a chemostat could display multiple metabolic states or display complex oscillatory behavior both with potentially serious implications to process operation. This paper explores the nonlinear behavior of a metabolic model of Escherichia coli growth on mixed substrates with sufficient detail to include regulatory features through the cybernetic postulate that metabolic regulation is the consequence of a dynamic objective function ensuring the organism’s survival. The chief source of nonlinearity arises from the optimal formulation with the metabolic state determined by a convex combination of reactions contributing to the objective function. The model for anaerobic growth of E. coli was previously examined for multiple steady states in a chemostat fed by a mixture of glucose and pyruvate substrates under very specific conditions and experimentally verified. In this article, we explore the foregoing model for nonlinear behavior over the full range of parameters, γ (the fractional concentration of glucose in the feed mixture and D (the dilution rate. The observed multiplicity is in the cybernetic variables combining elementary modes. The results show steady-state multiplicity up to seven. No Hopf bifurcation was encountered, however. Bifurcation analysis of cybernetic models is complicated by the non-differentiability of the cybernetic variables for enzyme activities. A methodology is adopted here to overcome this problem, which is applicable to more complicated metabolic networks.

  13. Effects of transforming growth interacting factor on biological behaviors of gastric carcinoma cells

    Institute of Scientific and Technical Information of China (English)

    Zhong-Liang Hu; Ji-Fang Wen; De-Sheng Xiao; Hui Zhen; Chun-Yan Fu

    2005-01-01

    AIM:Transforming growth interacting factor (TGIF) is an inhibitor of both transforming growth factor β (TGF-β) and retinoid signaling pathways. Moreover, the activation of MAPK pathway can prolong its half-life. However, its role in carcinogenesis is still unknown. Thus we attempted to investigate the effect of TGIF on biologic behaviors of gastric carcinoma cells.METHODS: Gastric carcinoma cell line, SGC-7901, was stably transfected with plasmid PcDNA3.1-TGIF. Western blotting and cell immunohistochemistry screening for the highly expressing clone of TGIF were employed. The growth of transfected cells was investigated by MTT and colonyformation assays, and apoptosis was measured by flow cytometry (FCM) and transmission electron microscopy.Tumorigenicity of the transfectant cells was also analyzed.RESULTS: TGIF had no effect on the proliferation, cell cycle and apoptosis of SGC-7901 cells, but cellular organelles of cells transfected with TGIF were richer than those of vector control or parental cells. Its clones were smaller than the control ones in plate efficiency, and its tumor tissues also had no obvious necrosis compared with the vector control or parental cells. Moreover, TGIF could resist TGF-β mediated growth inhibition.CONCLUSION: TGIF may induce differentiation of stomach neoplastic cells. In addition, TGIF can counteract the growth inhibition induced by TGF-β.

  14. Effect of Microstructure on Creep Crack Growth Behavior of a Near- α Titanium Alloy IMI-834

    Science.gov (United States)

    Satyanarayana, D. V. V.; Omprakash, C. M.; Sridhar, T.; Kumar, Vikas

    2009-01-01

    In the present study, the effect of microstructure ( i.e., α + β and transformed β) on creep crack growth (CCG) behavior of a near-alpha (IMI 834) titanium alloy has been explored at temperatures 550 °C and 600 °C. For characterizing the CCG behavior of the alloy, both stress intensity factor ( K) and energy integral parameter ( C t ) were used in the present investigation. The use of stress intensity factor ( K) as crack-tip parameter is not appropriate in the present study as no unique correlation between crack growth rate and K could be obtained from the observed trend due to transients in the creep crack rate data. On the other hand, C t parameter for both microstructural conditions consolidates CCG data into a single trend. The alloy with fully transformed β microstructure exhibits better CCG resistance as compared to bimodal ( α + β) microstructure. This is consistent with the fact that the transformed β structure offers superior creep resistance as compared to α + β microstructure. Microstructural examination has revealed that CCG for both microstructural conditions is accompanied by formation of damage zone in the form of numerous environmental-assisted secondary surface cracks (perpendicular to the stress axis) ahead of the main crack tip. For α + β microstructure of the alloy, the surface creep cracks were formed by growth and coalescence of microcracks nucleated by fracture of primary α particles. While in the interior of the specimens, CCG occurred by growth and coalescence of microvoids nucleated at primary α/transformed β (matrix) interfaces. For β microstructure of the alloy, while the surface creep cracks formed by growth and coalescence of microvoids nucleated at titanium enriched surface oxide particles, in the interior CCG occurred by nucleation of intergranular cavities.

  15. 信息动态%Origin of delamination/adhesion in co-casting and the open structure

    Institute of Scientific and Technical Information of China (English)

    2011-01-01

    PEI and PSf polymer solutions were used for co-casting. Mechanisms for delamination/adhesion were investigated. It was found that the contribution of the coagulation values of membrane solutions is insignificant to the adhesion of two layers. Instead, membrane shrinkage appears to play a significant role because composite membranes were obtained by minimising their shrinkage difference at the thickness direction by the increase of the coagulant temperature. In addition, the PVP in PSf solution also improves the adhesion between PEI and PSf layer. The open structure formation mechanism of PSf membrane was ascribed to a solvent enriched environment caused by the presence of PEI coating layer, which was confirmed by addition of a large amount of solvent into water coagulant. Finally, the concave defects formation on PSf surface was proposed as the impact of the growth of finger-like macrovoids in PEI layer. The results provides a solid theoretical basis for the expanding the application of co-casting technique.

  16. Simulation of Delamination Propagation in Composites Under High-Cycle Fatigue by Means of Cohesive-Zone Models

    Science.gov (United States)

    Turon, Albert; Costa, Josep; Camanho, Pedro P.; Davila, Carlos G.

    2006-01-01

    A damage model for the simulation of delamination propagation under high-cycle fatigue loading is proposed. The basis for the formulation is a cohesive law that links fracture and damage mechanics to establish the evolution of the damage variable in terms of the crack growth rate dA/dN. The damage state is obtained as a function of the loading conditions as well as the experimentally-determined coefficients of the Paris Law crack propagation rates for the material. It is shown that by using the constitutive fatigue damage model in a structural analysis, experimental results can be reproduced without the need of additional model-specific curve-fitting parameters.

  17. Effects of microstructure on fatigue crack growth behavior in cold-rolled dual phase steels

    Energy Technology Data Exchange (ETDEWEB)

    Li, Shengci [School of Materials Science and Engineering, State Key Laboratory for Advanced Metals and Materials, University of Science and Technology Beijing, Beijing 100083 (China); Kang, Yonglin, E-mail: kangylin@ustb.edu.cn [School of Materials Science and Engineering, State Key Laboratory for Advanced Metals and Materials, University of Science and Technology Beijing, Beijing 100083 (China); Kuang, Shuang [Technical Research Institute, Shougang Corporation, Ltd., Beijing 100043 (China)

    2014-08-26

    Fatigue crack growth behaviors of cold-rolled dual phase steels with different microstructures were investigated at room temperature. The ferrite–martensite dual-phase microstructure was obtained by intercritical annealing. Fatigue crack growth (FCG) behaviors were described by both the Paris model and a new exponential model; fatigue fractography and surface morphology near the fracture were arrested by scanning electron microscopy (SEM); the relationship between macroscopic and microcosmic FCG rate was analyzed quantificationally. The results showed that both the models can be used to describe the fatigue crack growth rate of the samples rather well; fatigue striations and secondary cracks were observed in the fracture surface at stable expanding region (II), while the fracture at rapid expanding region (III) combined dimple and quasi-cleavage morphology; the roughness of fracture surface and the degree of secondary cracking increased with an increase in martensite content, leading to a higher threshold value. Moreover, the changes of microcosmic FCG rate were smoother than that of the macroscopic FCG rate.

  18. A parallel process growth mixture model of conduct problems and substance use with risky sexual behavior.

    Science.gov (United States)

    Wu, Johnny; Witkiewitz, Katie; McMahon, Robert J; Dodge, Kenneth A

    2010-10-01

    Conduct problems, substance use, and risky sexual behavior have been shown to coexist among adolescents, which may lead to significant health problems. The current study was designed to examine relations among these problem behaviors in a community sample of children at high risk for conduct disorder. A latent growth model of childhood conduct problems showed a decreasing trend from grades K to 5. During adolescence, four concurrent conduct problem and substance use trajectory classes were identified (high conduct problems and high substance use, increasing conduct problems and increasing substance use, minimal conduct problems and increasing substance use, and minimal conduct problems and minimal substance use) using a parallel process growth mixture model. Across all substances (tobacco, binge drinking, and marijuana use), higher levels of childhood conduct problems during kindergarten predicted a greater probability of classification into more problematic adolescent trajectory classes relative to less problematic classes. For tobacco and binge drinking models, increases in childhood conduct problems over time also predicted a greater probability of classification into more problematic classes. For all models, individuals classified into more problematic classes showed higher proportions of early sexual intercourse, infrequent condom use, receiving money for sexual services, and ever contracting an STD. Specifically, tobacco use and binge drinking during early adolescence predicted higher levels of sexual risk taking into late adolescence. Results highlight the importance of studying the conjoint relations among conduct problems, substance use, and risky sexual behavior in a unified model. Copyright © 2010 Elsevier Ireland Ltd. All rights reserved.

  19. Yolk hormones influence in ovo chemosensory learning, growth, and feeding behavior in domestic chicks.

    Science.gov (United States)

    Bertin, Aline; Meurisse, Maryse; Arnould, Cécile; Leterrier, Christine; Constantin, Paul; Cornilleau, Fabien; Vaudin, Pascal; Burlot, Thierry; Delaveau, Joel; Rat, Christophe; Calandreau, Ludovic

    2016-03-01

    In this study, we assessed whether prenatal exposure to elevated yolk steroid hormones can influence in ovo chemosensory learning and the behavior of domestic chicks. We simulated a maternal environmental challenge by experimentally enhancing yolk progesterone, testosterone, and estradiol concentrations in hen eggs prior to incubation. The embryos from these hormones-treated eggs (HO) as well as sham embryos (O) that had received the vehicle-only were exposed to the odor of fish oil (menhaden) between embryonic Days 11 and 20. An additional group of control embryos (C) was not exposed to the odor. All chicks were tested following hatching for their feeding preferences between foods that were or were not odorized with the menhaden odor. In the 3-min choice tests, the behavior of O chicks differed significantly according to the type of food whereas C and HO chicks showed no preference between odorized and non-odorized food. Our result suggests weaker response in HO chicks. In addition, HO chicks showed impaired growth and reduced intake of an unfamiliar food on the 24-h time scale compared to controls. Our data suggest that embryonic exposure to increased yolk hormone levels can alter growth, chemosensory learning, and the development of feeding behaviors.

  20. Kinetic Behavior of Exchange-Driven Growth with Catalyzed-Birth Processes

    Institute of Scientific and Technical Information of China (English)

    WANG Hai-Feng; LIN Zhen-Quan; KONG Xiang-Mu

    2006-01-01

    Two catalyzed-birth models of n-species (n≥2) aggregates with exchange-driven growth processes are proposed and compared. In the first one, the exchange reaction occurs between any two aggregates Amk and Amj of the same species with the rate kernels Km (k,j)=Kmkj (m=1, 2,..., n, n≥2), and aggregates of An species catalyze a monomer-birth of Al species (l=1,2,..., n-1) with the catalysis rate kernel Jl(k,j)=Jlkjυ. The kinetic behaviors are investigated by means of the mean-field theory. We find that the evolution behavior of aggregate-size distribution alk(t) of Al species depends crucially on the value of the catalysis rate parameter v: (i) alk(t) obeys the conventional scaling law in the case of υ≤0, (ii) alk (t) satisfies a modified scaling form in the case of υ>0. In the second model,the mechanism of monomer-birth of An-species catalyzed by Al species is added on the basis of the first model, that is,the aggregates of Al and An species catalyze each other to cause monomer-birth. The kinetic behaviors of Al and Anspecies are found to fall into two categories for the different υ: (i) growth obeying conventional scaling form with υ≤0,(ii) gelling at finite time withυ>0.

  1. Delamination behaviour of GdBCO coated conductor tapes under transverse tension

    Energy Technology Data Exchange (ETDEWEB)

    Gorospe, A. [Department of Mechanical Design Engineering, Andong National University, Andong 760-749 (Korea, Republic of); Department of Engineering, Aurora State College of Technology, Baler 3200 (Philippines); Nisay, A. [Department of Mechanical Design Engineering, Andong National University, Andong 760-749 (Korea, Republic of); Dizon, J.R. [Department of Mechanical Design Engineering, Andong National University, Andong 760-749 (Korea, Republic of); College of Engineering and Architecture, Bataan Peninsula State University, Balanga 2100 (Philippines); Shin, H.S., E-mail: hsshin@andong.ac.kr [Department of Mechanical Design Engineering, Andong National University, Andong 760-749 (Korea, Republic of)

    2013-11-15

    Highlights: •Installation of a test frame which gives precisely aligned transverse load. •Investigation of I{sub c} degradation behaviour depending on the type of sample delamination. •Inhomogeneity of the CC tapes caused large variation on delamination strength. •SEM and EDS analysis of delamination sites under transverse loading. -- Abstract: The electromechanical property behaviour of 2G coated conductor (CC) tapes fabricated by multi-layer deposition process both in the in-plane and transverse direction should be understood. The CC tapes are used in the fabrication of epoxy resin-impregnated coils. In such case, the Lorentz force due to the high magnetic field applied as well as the thermal stress due to the difference in coefficient of thermal expansion (CTE) among constituent layers during cooling to cryogenic temperature will induce transversely applied load to the surface of CC tapes in coils. Hence, the CC tape should have a good mechanical property in the transverse direction in order to maintain its superior performance under magnetic field. In this study, a test frame which gives precisely aligned transverse load was devised. Using the fixture, the delamination behaviours including the delamination strength of the GdBCO CC tapes under transverse tensile loading were investigated. Large variation on the delamination strength of the CC tapes was recorded and might have resulted from the slit edge effect and the inhomogeneity of the CC tapes. The I{sub c} degradation behaviour under transverse load was related to the location where delamination occurred in the sample.

  2. Detection of Delamination in Composite Beams Using Broadband Acoustic Emission Signatures

    Science.gov (United States)

    Okafor, A. C.; Chandrashekhara, K.; Jiang, Y. P.

    1996-01-01

    Delamination in composite structure may be caused by imperfections introduced during the manufacturing process or by impact loads by foreign objects during the operational life. There are some nondestructive evaluation methods to detect delamination in composite structures such as x-radiography, ultrasonic testing, and thermal/infrared inspection. These methods are expensive and hard to use for on line detection. Acoustic emission testing can monitor the material under test even under the presence of noise generated under load. It has been used extensively in proof-testing of fiberglass pressure vessels and beams. In the present work, experimental studies are conducted to investigate the use of broadband acoustic emission signatures to detect delaminations in composite beams. Glass/epoxy beam specimens with full width, prescribed delamination sizes of 2 inches and 4 inches are investigated. The prescribed delamination is produced by inserting Teflon film between laminae during the fabrication of composite laminate. The objectives of this research is to develop a method for predicting delamination size and location in laminated composite beams by combining smart materials concept and broadband AE analysis techniques. More specifically, a piezoceramic (PZT) patch is bonded on the surface of composite beams and used as a pulser. The piezoceramic patch simulates the AE wave source as a 3 cycles, 50KHz, burst sine wave. One broadband AE sensor is fixed near the PZT patch to measure the AE wave near the AE source. A second broadband AE sensor, which is used as a receiver, is scanned along the composite beams at 0.25 inch step to measure propagation of AE wave along the composite beams. The acquired AE waveform is digitized and processed. Signal strength, signal energy, cross-correlation of AE waveforms, and tracking of specific cycle of AE waveforms are used to detect delamination size and location.

  3. AFSC/RACE/FBEP/Ryer: Growth and distributional correlates of behavior in three co-occurring juvenile flatfishes

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — This dataset is from laboratory experiments that explored anti-predator behavior and intrinsic growth in three co-occurring juvenile flatfish species (English sole...

  4. Investigating the crystal growth behavior of biodegradable polymer blend thin films using in situ atomic force microscopy

    CSIR Research Space (South Africa)

    Malwela, T

    2014-01-01

    Full Text Available This article reports the crystal growth behavior of biodegradable polylactide (PLA)/poly[(butylene succinate)-co-adipate] (PBSA) blend thin films using atomic force microscopy (AFM). Currently, polymer thin films have received increased research...

  5. Effects of lead-contaminated sediment and nutrition on mallard duckling behavior and growth

    Science.gov (United States)

    Douglas-Stroebel, E.; Brewer, G.L.; Hoffman, D.J.

    2005-01-01

    Sediment ingestion has become a recognized exposure route for toxicants in waterfowl. The effects of lead-contaminated sediment from the Coeur d?Alene River Basin (CDARB) in Idaho were evaluated on mallard (Anas platyryhnchos) duckling behavior and growth over a five-week period using time-activity budgets. Day-old ducklings received either a clean sediment (24%) supplemented control diet, CDARB sediment (3,449 ug/g lead) supplemented diets at 12% or 24%, or a positive control diet (24% clean sediment with equivalent lead acetate to the 24% CDARB diet). Ten different behaviors were monitored for time spent, including resting, standing, moving, drinking, dabbling, feeding, pecking, preening, bathing and swimming. Contaminated sediment (24% CDARB ) and lead acetate significantly decreased the proportion of time spent swimming. There were also problems with balance and mobility in the 24% CDARB and the lead acetate groups. With a less optimal diet (mixture of two thirds corn and one third standard diet) containing 24% clean sediment, nutrient level alone affected six different behaviors including feeding, pecking, swimming, preening, standing, and dabbling. Nutrient level also significantly decreased the growth rate and delayed the initial time of molt. When the corn diet contained CDARB sediment, the proportion of time spent bathing in the 24% CDARB group significantly decreased with marginal effects on resting and feeding. There were also instances of imbalance with 24% CDARB and corn diet, and duckling weights were significantly lower than in corn diet controls. The decreased time spent swimming or bathing, coupled with problems of balance and mobility, decreased growth, histopathological lesions and altered brain biochemistry (reported elsewhere) illustrate a potential threat to the survival of ducklings in the wild that are exposed to lead-containing sediments within the CDARB or elsewhere.

  6. Geometrical versus Random β-TCP Scaffolds: Exploring the Effects on Schwann Cell Growth and Behavior.

    Science.gov (United States)

    Sweet, Lauren; Kang, Yunqing; Czisch, Christopher; Witek, Lukasz; Shi, Yang; Smay, Jim; Plant, Giles W; Yang, Yunzhi

    2015-01-01

    Numerous studies have demonstrated that Schwann cells (SCs) play a role in nerve regeneration; however, their role in innervating a bioceramic scaffold for potential application in bone regeneration is still unknown. Here we report the cell growth and functional behavior of SCs on β-tricalcium phosphate (β-TCP) scaffolds arranged in 3D printed-lattice (P-β-TCP) and randomly-porous, template-casted (N-β-TCP) structures. Our results indicate that SCs proliferated well and expressed the phenotypic markers p75LNGFR and the S100-β subunit of SCs as well as displayed growth morphology on both scaffolds, but SCs showed spindle-shaped morphology with a significant degree of SCs alignment on the P-β-TCP scaffolds, seen to a lesser degree in the N-β-TCP scaffold. The gene expressions of nerve growth factor (β-ngf), neutrophin-3 (nt-3), platelet-derived growth factor (pdgf-bb), and vascular endothelial growth factor (vegf-a) were higher at day 7 than at day 14. While no significant differences in protein secretion were measured between these last two time points, the scaffolds promoted the protein secretion at day 3 compared to that on the cell culture plates. These results together imply that the β-TCP scaffolds can support SC cell growth and that the 3D-printed scaffold appeared to significantly promote the alignment of SCs along the struts. Further studies are needed to investigate the early and late stage relationship between gene expression and protein secretion of SCs on the scaffolds with refined characteristics, thus better exploring the potential of SCs to support vascularization and innervation in synthetic bone grafts.

  7. Geometrical versus Random β-TCP Scaffolds: Exploring the Effects on Schwann Cell Growth and Behavior.

    Directory of Open Access Journals (Sweden)

    Lauren Sweet

    Full Text Available Numerous studies have demonstrated that Schwann cells (SCs play a role in nerve regeneration; however, their role in innervating a bioceramic scaffold for potential application in bone regeneration is still unknown. Here we report the cell growth and functional behavior of SCs on β-tricalcium phosphate (β-TCP scaffolds arranged in 3D printed-lattice (P-β-TCP and randomly-porous, template-casted (N-β-TCP structures. Our results indicate that SCs proliferated well and expressed the phenotypic markers p75LNGFR and the S100-β subunit of SCs as well as displayed growth morphology on both scaffolds, but SCs showed spindle-shaped morphology with a significant degree of SCs alignment on the P-β-TCP scaffolds, seen to a lesser degree in the N-β-TCP scaffold. The gene expressions of nerve growth factor (β-ngf, neutrophin-3 (nt-3, platelet-derived growth factor (pdgf-bb, and vascular endothelial growth factor (vegf-a were higher at day 7 than at day 14. While no significant differences in protein secretion were measured between these last two time points, the scaffolds promoted the protein secretion at day 3 compared to that on the cell culture plates. These results together imply that the β-TCP scaffolds can support SC cell growth and that the 3D-printed scaffold appeared to significantly promote the alignment of SCs along the struts. Further studies are needed to investigate the early and late stage relationship between gene expression and protein secretion of SCs on the scaffolds with refined characteristics, thus better exploring the potential of SCs to support vascularization and innervation in synthetic bone grafts.

  8. Geometrical versus Random β-TCP Scaffolds: Exploring the Effects on Schwann Cell Growth and Behavior

    Science.gov (United States)

    Czisch, Christopher; Witek, Lukasz; Shi, Yang; Smay, Jim; Plant, Giles W.; Yang, Yunzhi

    2015-01-01

    Numerous studies have demonstrated that Schwann cells (SCs) play a role in nerve regeneration; however, their role in innervating a bioceramic scaffold for potential application in bone regeneration is still unknown. Here we report the cell growth and functional behavior of SCs on β-tricalcium phosphate (β-TCP) scaffolds arranged in 3D printed-lattice (P-β-TCP) and randomly-porous, template-casted (N-β-TCP) structures. Our results indicate that SCs proliferated well and expressed the phenotypic markers p75LNGFR and the S100-β subunit of SCs as well as displayed growth morphology on both scaffolds, but SCs showed spindle-shaped morphology with a significant degree of SCs alignment on the P-β-TCP scaffolds, seen to a lesser degree in the N-β-TCP scaffold. The gene expressions of nerve growth factor (β-ngf), neutrophin–3 (nt–3), platelet-derived growth factor (pdgf-bb), and vascular endothelial growth factor (vegf-a) were higher at day 7 than at day 14. While no significant differences in protein secretion were measured between these last two time points, the scaffolds promoted the protein secretion at day 3 compared to that on the cell culture plates. These results together imply that the β-TCP scaffolds can support SC cell growth and that the 3D-printed scaffold appeared to significantly promote the alignment of SCs along the struts. Further studies are needed to investigate the early and late stage relationship between gene expression and protein secretion of SCs on the scaffolds with refined characteristics, thus better exploring the potential of SCs to support vascularization and innervation in synthetic bone grafts. PMID:26444999

  9. Growth behavior of anodic porous alumina formed in malic acid solution

    Science.gov (United States)

    Kikuchi, Tatsuya; Yamamoto, Tsuyoshi; Suzuki, Ryosuke O.

    2013-11-01

    The growth behavior of anodic porous alumina formed on aluminum by anodizing in malic acid solutions was investigated. High-purity aluminum plates were electropolished in CH3COOH/HClO4 solutions and then anodized in 0.5 M malic acid solutions at 293 K and constant cell voltages of 200-350 V. The anodic porous alumina grew on the aluminum substrate at voltages of 200-250 V, and a black, burned oxide film was formed at higher voltages. The nanopores of the anodic oxide were only formed at grain boundaries of the aluminum substrate during the initial stage of anodizing, and then the growth region extended to the entire aluminum surface as the anodizing time increased. The anodic porous alumina with several defects was formed by anodizing in malic acid solution at 250 V, and oxide cells were approximately 300-800 nm in diameter.

  10. Isotropic and Anisotropic Growth of Metal-Organic Framework (MOF) on MOF: Logical Inference on MOF Structure Based on Growth Behavior and Morphological Feature.

    Science.gov (United States)

    Choi, Sora; Kim, Taeho; Ji, Hoyeon; Lee, Hee Jung; Oh, Moonhyun

    2016-11-02

    The growth of one metal-organic framework (MOF) on another MOF for constructing a heterocompositional hybrid MOF is an interesting research topic because of the curiosity regarding the occurrence of this phenomenon and the value of hybrid MOFs as multifunctional materials or routes for fine-tuning MOF properties. In particular, the anisotropic growth of MOF on MOF is fascinating for the development of MOFs possessing atypical shapes and heterostructures or abnormal properties. Herein, we clarify the understanding of growth behavior of a secondary MOF on an initial MOF template, such as isotropic or anisotropic ways associated with their cell parameters. The isotropic growth of MIL-68-Br on the MIL-68 template results in the formation of core-shell-type MIL-68@MIL-68-Br. However, the unique anisotropic growth of a secondary MOF (MOF-NDC) on the MIL-68 template results in semitubular particles, and structural features of this unknown secondary MOF are successfully speculated for the first time on the basis of its unique growth behavior and morphological characteristics. Finally, the validation of this structural speculation is verified by the powder X-ray diffraction and the selected area electron diffraction studies. The results suggests that the growth behavior and morphological features of MOFs should be considered to be important factors for understanding the MOFs' structures.

  11. Simulation of micro-behaviors including nucleation,growth, and aggregation in particle system

    Institute of Scientific and Technical Information of China (English)

    GU ZhaoLin; SU JunWei; JIAO JianYing; XU X Yun

    2009-01-01

    A new method for the solution of population balance equations (PBE) describing the micro-processes such as nucleation, growth, aggregation of particle swarms in a multiphase system is proposed. The method is based on the fixed pivot moment and allows arbitrary number of moments to be tracked si-multaneously. By expressing PBEs for both batch and continuous operations in a general form, and using weighted residual method to derive the moment equations, different moments can be tracked directly. The numerical density function is assumed to be a summation of several weighted Dirac Delta functions, and the integral and derivative terms in PBEs are transformed to a summation in order to reduce computational cost. Simulations of a batch nucleation-growth process and a continuous ag-gregation-growth process have demonstrated good agreement with the corresponding analytical solu-tions, with relative errors less than 10-8%. Simulation of a combined nucleation-growth-aggregation process, which does not have an analytical solution, is also included, so as to reproduce the mi-cro-behaviors of such a complex system, demonstrating the feasibility and reliability of this method.

  12. Simulation of micro-behaviors including nucleation,growth,and aggregation in particle system

    Institute of Scientific and Technical Information of China (English)

    2009-01-01

    A new method for the solution of population balance equations(PBE) describing the micro-processes such as nucleation,growth,aggregation of particle swarms in a multiphase system is proposed.The method is based on the fixed pivot moment and allows arbitrary number of moments to be tracked si-multaneously.By expressing PBEs for both batch and continuous operations in a general form,and using weighted residual method to derive the moment equations,different moments can be tracked directly.The numerical density function is assumed to be a summation of several weighted Dirac Delta functions,and the integral and derivative terms in PBEs are transformed to a summation in order to reduce computational cost.Simulations of a batch nucleation-growth process and a continuous ag-gregation-growth process have demonstrated good agreement with the corresponding analytical solu-tions,with relative errors less than 108%.Simulation of a combined nucleation-growth-aggregation process,which does not have an analytical solution,is also included,so as to reproduce the mi-cro-behaviors of such a complex system,demonstrating the feasibility and reliability of this method.

  13. Growth and chemosensory behavior of sulfate-reducing bacteria in oxygen-sulfide gradients

    DEFF Research Database (Denmark)

    Sass, Andrea M.; Wieland, Andrea Eschemann; Kühl, Michael;

    2002-01-01

    Growth and chemotactic behavior in oxic–anoxic gradients were studied with two freshwater and four marine strains of sulfate-reducing bacteria related to the genera Desulfovibrio, Desulfomicrobium or Desulfobulbus. Cells were grown in oxygen–sulfide counter-gradients within tubes filled with agar...... chemotactically to lactate, nitrate, sulfate and thiosulfate, and even sulfide functioned as an attractant. In oxic–anoxic gradients the bacteria moved away from high oxygen concentrations and formed bands at the outer edge of the oxic zone at low oxygen concentration (

  14. Recent sexual victimization and drinking behavior in newly matriculated college students: a latent growth analysis.

    Science.gov (United States)

    Griffin, Melissa J; Wardell, Jeffrey D; Read, Jennifer P

    2013-12-01

    College matriculation is a time of developmental and social change and is often a time of heavy drinking. Sexual victimization (SV) is prevalent in late adolescence and poses additional risk for problem drinking behavior. Thus, matriculating students with a SV history may be at heightened risk for maladaptive alcohol use while transitioning through the first year of college. Furthermore, victimization that has occurred close to college matriculation may confer particular risk for problem alcohol use, because the added stressor of coping with a SV while negotiating the transition into college may lead to risky drinking behavior. Therefore, examining the influence of SV timing (i.e., recency) on drinking patterns in freshman year was the aim of the present study. Matriculating undergraduates with a history of SV were assessed at six points during freshman year. Using latent growth curve modeling, we tested differences in trajectories of drinking behavior (i.e., alcohol use, binge drinking) between students who reported a recent SV and those who reported a more distal SV. Students endorsing a recent SV evidenced greater overall levels of alcohol use and higher levels of binge drinking than individuals with SV that was less recent. Moreover, the recent SV group showed significantly more variability in drinking outcomes over freshman year, with escalations mapping onto more salient periods of transition over the first college year. SV that occurs close to college entry is associated with specific and persistent risk for maladaptive drinking behavior in newly matriculated college students.

  15. Pheromone-modulated behavioral suites influence colony growth in the honey bee (Apis mellifera)

    Science.gov (United States)

    Pankiw, Tanya; Roman, Roman; Sagili, Ramesh R.; Zhu-Salzman, Keyan

    2004-12-01

    The success of a species depends on its ability to assess its environment and to decide accordingly which behaviors are most appropriate. Many animal species, from bacteria to mammals, are able to communicate using interspecies chemicals called pheromones. In addition to exerting physiological effects on individuals, for social species, pheromones communicate group social structure. Communication of social structure is important to social insects for the allocation of its working members into coordinated suites of behaviors. We tested effects of long-term treatment with brood pheromone on suites of honey bee brood rearing and foraging behaviors. Pheromone-treated colonies reared significantly greater brood areas and more adults than controls, while amounts of stored pollen and honey remained statistically similar. Brood pheromone increased the number of pollen foragers and the pollen load weights they returned. It appeared that the pheromone-induced increase in pollen intake was directly canalized into more brood rearing. A two-way pheromone priming effect was observed, such that some workers from the same age cohorts showed an increased and extended capacity to rear larvae, while others were recruited at significantly younger ages into pollen-specific foraging. Brood pheromone affected suites of nursing and foraging behaviors allocating worker and pollen resources associated with an important fitness trait, colony growth.

  16. Preliminary study on occurrence of composite material delamination processed by abrasive water jet cutting

    Directory of Open Access Journals (Sweden)

    Popan Ioan Alexandru

    2017-01-01

    Full Text Available The paper presents a preliminary experimental study on processing composite materials (CFRP using abrasive water jet cutting (AWJC process, analysing the possibilities of occurrence of material delamination. AWJC is a proper solution for cutting CFRP because of reduced interface temperature, high flexibility, low mechanical loading and reduced cutting forces. Cutting CFRP using AWJC involves several challenges like material delamination due to the high velocity impact of the jet. To understand the delamination, three experimental tests were made: in the first test the cutting and the drilling was made with high water pressure (350 MPa, in the second test the cutting was made with high water pressure and for drilling was used low water pressure (200 MPa and in last test a pre-drilled hole was used. Within those experiments was observed the CFRP delamination appears just during the drilling, not during the cutting. By decreasing the water jet pressure, the jet energy is decreased and in this way the delamination decrease.

  17. The Effect of Delamination on Damage Path and Failure Load Prediction for Notched Composite Laminates

    Science.gov (United States)

    Satyanarayana, Arunkumar; Bogert, Philip B.; Chunchu, Prasad B.

    2007-01-01

    The influence of delamination on the progressing damage path and initial failure load in composite laminates is investigated. Results are presented from a numerical and an experimental study of center-notched tensile-loaded coupons. The numerical study includes two approaches. The first approach considers only intralaminar (fiber breakage and matrix cracking) damage modes in calculating the progression of the damage path. In the second approach, the model is extended to consider the effect of interlaminar (delamination) damage modes in addition to the intralaminar damage modes. The intralaminar damage is modeled using progressive damage analysis (PDA) methodology implemented with the VUMAT subroutine in the ABAQUS finite element code. The interlaminar damage mode has been simulated using cohesive elements in ABAQUS. In the experimental study, 2-3 specimens each of two different stacking sequences of center-notched laminates are tensile loaded. The numerical results from the two different modeling approaches are compared with each other and the experimentally observed results for both laminate types. The comparisons reveal that the second modeling approach, where the delamination damage mode is included together with the intralaminar damage modes, better simulates the experimentally observed damage modes and damage paths, which were characterized by splitting failures perpendicular to the notch tips in one or more layers. Additionally, the inclusion of the delamination mode resulted in a better prediction of the loads at which the failure took place, which were higher than those predicted by the first modeling approach which did not include delaminations.

  18. Hierarchical fiber-optic delamination detection system for carbon fiber reinforced plastic structures

    Science.gov (United States)

    Minakuchi, Shu; Banshoya, Hidehiko; Shingo, Ii; Takeda, Nobuo

    2012-10-01

    This study develops a delamination detection system by extending our previous approach for monitoring surface cracks in a large-scale composite structure. In the new system, numerous thin glass capillaries are embedded into a composite structure, and internal pressure in the built-in capillary sensors, based on comparative vacuum monitoring (CVM), is maintained as a vacuum. When delamination is induced, the capillary sensors located within the delaminated area are breached, and atmospheric air flows into the capillaries. The consequent pressure change within the capillaries is then converted into axial strain in a surface-mounted optical fiber through a transducing mechanism, which is connected to the capillaries. By monitoring the strain distribution along the optical fiber, it is possible to identify a transducing mechanism in which the pressure change occurred and thus to specify the location of the delamination. This study begins by establishing a novel sensor embedding/extracting method. The airflow characteristic in the capillary sensors is then comprehensively evaluated, determining the basic performance of the new system. The proposed detection technique is validated by taking a step-by-step approach, and finally the hierarchical fiber-optic delamination detection system is demonstrated. A further advance to be combined with a self-healing concept is also discussed.

  19. Detection and characterisation of delamination in PV modules by active infrared thermography

    Science.gov (United States)

    Sinha, A.; Sastry, O. S.; Gupta, R.

    2016-01-01

    The paper presents a fast and efficient method for the detection and characterisation of delamination in photovoltaic (PV) modules by using active infrared thermography approach. A discrete part of PV module was irradiated by step heating and its thermal image sequence was used to detect and analyse delamination. Different types of heating source for thermal excitation for this application have been studied. An electro-thermal model was developed to simulate the active thermography approach for the characterisation of delamination in PV module by equivalent resistance-capacitance (RC) network using a circuit simulator. This simulation approach was used to estimate the extent of delamination in the module and to determine the optimum parameters for the characterisation of delamination. Different applications based on front and backsides of heating the module were also proposed in this paper. The proposed method has the potential to be employed for the quality check of PV modules during inline production as well as for the predictive maintenance of outdoor PV plants.

  20. In situ infrared spectroscopic study of cubic boron nitride thin film delamination

    Institute of Scientific and Technical Information of China (English)

    Yang Hang-Sheng; Zhang Jian-Ying; Nie An-Min; Zhang Xiao-Bin

    2008-01-01

    This paper investigates the procedure of cubic boron nitride(cBN)thin film delamination by Fourier-transform infrared(IR)spectroscopy.It finds that the apparent IR absorption peak area near 1380 cm-1 and 1073 cm-1 attributed to the B-N stretching vibration of sp2-bonded BN and the transverse optical phonon of cBN,respectively,increased up to 195% and 175% of the original peak area after film delamination induced compressive stress relaxation.The increase of IR absorption of sp2-bonded BN is found to be non-linear and hysteretic to film delamination,which suggests that the relaxation of the turbostratic BN(tBN)layer from the compressed condition is also hysteretic to film delamination.Moreover,cross-sectional transmission electron microscopic observations revealed that cBN film delamination is possible from near the aBN(amorphons BN)/tBN interface at least for films prepared by plasma-enhanced chemical vapour deposition.

  1. Effects of physical education, extracurricular sports activities, and leisure satisfaction on adolescent aggressive behavior: A latent growth modeling approach.

    Science.gov (United States)

    Park, Sanghyun; Chiu, Weisheng; Won, Doyeon

    2017-01-01

    The present study aimed to investigate the longitudinal influence of physical education classes, extracurricular sports activities, and leisure satisfaction on aggressive behavior among South Korean adolescents. Data were drawn from the Korea Youth Panel Survey. We used latent growth curve modeling to explain the growth trajectory of adolescent aggressive behaviors and a multi-group analysis to investigate gender differences in aggressive behavior. The results indicated that adolescents' aggressive behavior significantly changed with age. There were significant gender-based differences in the level of and changes in aggressive behavior over time. Both extracurricular sports activities and leisure satisfaction had significant influences on the changes in adolescents' aggressive behavior with age, whereas physical education classes did not.

  2. Inactivation of fibroblast growth factor binding protein 3 causes anxiety-related behaviors.

    Science.gov (United States)

    Yamanaka, Yasunari; Kitano, Ayumi; Takao, Keizo; Prasansuklab, Anchalee; Mushiroda, Taisei; Yamazaki, Keiko; Kumada, Tomohiro; Shibata, Minoru; Takaoka, Yuki; Awaya, Tomonari; Kato, Takeo; Abe, Takaya; Iwata, Nakao; Miyakawa, Tsuyoshi; Nakamura, Yusuke; Nakahata, Tatsutoshi; Heike, Toshio

    2011-01-01

    The neurobiological mechanisms of emotional modulation and the molecular pathophysiology of anxiety disorders are largely unknown. The fibroblast growth factor (FGF) family has been implicated in the regulation of many physiological and pathological processes, which include the control of emotional behaviors. The present study examined mice with a targeted deletion of the fgf-bp3 gene, which encodes a novel FGF-binding protein, in animal models relevant to anxiety. To define the behavioral consequences of FGF-BP3 deficiency, we evaluated fgf-bp3-deficient mice using anxiety-related behavioral paradigms that provide a conflict between the desire to explore an unknown area or objects and the aversion to a brightly lit open space. The fgf-bp3-deficient mice exhibited alterations in time spent in the central area of the open-field arena, were less active in the lit areas of a light/dark transition test, and had a prolonged latency to feed during a novelty-induced hypophagia test. These changes were associated with alterations in light-induced orbitofrontal cortex (OFC) activation in an extracellular signal-regulated kinase (ERK) pathway-dependent manner. These results demonstrate that FGF-BP3 is a potent mediator of anxiety-related behaviors in mice and suggest that distinct pathways regulate emotional behaviors. Therefore, FGF-BP3 plays a critical role in the regulation of emotional states and in the development of anxiety disorders and should be investigated as a therapeutic target for anxiety disease in humans.

  3. Characterization of Delaminations and Transverse Matrix Cracks in Composite Laminates Using Multiple-Angle Ultrasonic Inspection

    Science.gov (United States)

    Johnston, Patrick H.; Appleget, Chelsea D.; Odarczenko, Michael T.

    2012-01-01

    Delaminations and transverse matrix cracks often appear concurrently in composite laminates. Normal-incidence ultrasound is excellent at detecting delaminations, but is not optimum for matrix cracks. Non-normal incidence, or polar backscattering, has been shown to optimally detect matrix cracks oriented perpendicular to the ultrasonic plane of incidence. In this work, a series of six composite laminates containing slots were loaded in tension to achieve various levels of delamination and ply cracking. Ultrasonic backscattering was measured over a range of incident polar and azimuthal angles, in order to characterize the relative degree of damage of the two types. Sweptpolar- angle measurements were taken with a curved phased array, as a step toward an array-based approach to simultaneous measurement of combined flaws.

  4. A hybrid method based upon nonlinear Lamb wave response for locating a delamination in composite laminates.

    Science.gov (United States)

    Yelve, Nitesh P; Mitra, Mira; Mujumdar, P M; Ramadas, C

    2016-08-01

    A new hybrid method based upon nonlinear Lamb wave response in time and frequency domains is introduced to locate a delamination in composite laminates. In Lamb wave based nonlinear method, the presence of damage is shown by the appearance of higher harmonics in the Lamb wave response. The proposed method not only uses this spectral information but also the corresponding temporal response data, for locating the delamination. Thus, the method is termed as a hybrid method. The paper includes formulation of the method and its application to locate a Barely Visible Impact Damage (BVID) induced delamination in a Carbon Fiber Reinforced Polymer (CFRP) laminate. The method gives the damage location fairly well. It is a baseline free method, as it does not need data from the pristine specimen.

  5. A Damage Model for the Simulation of Delamination in Advanced Composites under Variable-Mode Loading

    Science.gov (United States)

    Turon, A.; Camanho, P. P.; Costa, J.; Davila, C. G.

    2006-01-01

    A thermodynamically consistent damage model is proposed for the simulation of progressive delamination in composite materials under variable-mode ratio. The model is formulated in the context of Damage Mechanics. A novel constitutive equation is developed to model the initiation and propagation of delamination. A delamination initiation criterion is proposed to assure that the formulation can account for changes in the loading mode in a thermodynamically consistent way. The formulation accounts for crack closure effects to avoid interfacial penetration of two adjacent layers after complete decohesion. The model is implemented in a finite element formulation, and the numerical predictions are compared with experimental results obtained in both composite test specimens and structural components.

  6. On a multiscale strategy and its optimization for the simulation of combined delamination and buckling

    CERN Document Server

    Saavedra, Karin; Gosselet, Pierre; 10.1002/nme.4305

    2012-01-01

    This paper investigates a computational strategy for studying the interactions between multiple through-the-width delaminations and global or local buckling in composite laminates taking into account possible contact between the delaminated surfaces. In order to achieve an accurate prediction of the quasi-static response, a very refined discretization of the structure is required, leading to the resolution of very large and highly nonlinear numerical problems. In this paper, a nonlinear finite element formulation along with a parallel iterative scheme based on a multiscale domain decomposition are used for the computation of 3D mesoscale models. Previous works by the authors already dealt with the simulation of multiscale delamination assuming small perturbations. This paper presents the formulation used to include geometric nonlinearities into this existing multiscale framework and discusses the adaptations that need to be made to the iterative process in order to ensure the rapid convergence and the scalabi...

  7. Detailed modelling of delamination buckling of thin films under global tension.

    Science.gov (United States)

    Toth, F; Rammerstorfer, F G; Cordill, M J; Fischer, F D

    2013-04-01

    Tensile specimens of metal films on compliant substrates are widely used for determining interfacial properties. These properties are identified by the comparison of experimentally observed delamination buckling and a mathematical model which contains the interface properties as parameters. The current two-dimensional models for delamination buckling are not able to capture the complex stress and deformation states arising in the considered uniaxial tension test in a satisfying way. Therefore, three-dimensional models are developed in a multi-scale approach. It is shown that, for the considered uniaxial tension test, the buckling and associated delamination process are initiated and driven by interfacial shear in addition to compressive stresses in the film. The proposed model is able to reproduce all important experimentally observed phenomena, like cracking stress of the film, film strip curvature and formation of triangular buckles. Combined with experimental data, the developed computational model is found to be effective in determining interface strength properties.

  8. Numerical optimization approach to modelling delamination and buckling of geometrically constrained structures.

    Science.gov (United States)

    Mullineux, G; Hicks, B J; Berry, C

    2012-04-28

    Understanding what happens in terms of delamination during buckling of laminate materials is of importance across a range of engineering sectors. Normally concern is that the strength of the material is not significantly impaired. Carton-board is a material with a laminate structure and, in the initial creation of carton nets, the board is creased in order to weaken the structure. This means that when the carton is eventually folded into its three-dimensional form, correct folding occurs along the weakened crease lines. Understanding what happens during creasing and folding is made difficult by the nonlinear nature of the material properties. This paper considers a simplified approach which extends the idea of minimizing internal energy so that the effects of delamination can be handled. This allows a simulation which reproduces the form of buckling-delamination observed in practice and the form of the torque-rotation relation.

  9. Non-Arrhenius growth behavior, bilayer and reentrant layer growth for ultrathin Co films on Cu(0 0 1)

    CERN Document Server

    Bernhard, T; Winter, H

    2003-01-01

    Grazing scattering of 25 keV He atoms is applied to study island nucleation and growth of Co on Cu(0 0 1) in real time and real space. With decreasing growth temperature, we observe, starting at 470 K, step-flow growth, layer growth, bilayer growth and, below 210 K, reentrant layer growth. The density of nucleated islands shows a complex 'N-shaped' dependence on temperature, which is at variance with standard nucleation theory. Results are explained on the basis of recent density-functional calculations.

  10. Coupled flexural-longitudinal vibration of delaminated composite beams with local stability analysis

    Science.gov (United States)

    Szekrényes, András

    2014-09-01

    A novel analytical model is developed to solve the problem of free vibration of delaminated composite beams. The beam with a single delamination was modelled by six equivalent single layers by establishing the kinematic continuity in the undelaminated portion of the system. In the delaminated region the layers were captured by the traditional theories. First, Timoshenko beam theory is applied to solve the problem, then by reducing the model, the corresponding Euler-Bernoulli solution is presented. Both the free and constrained models were considered. The most important aspect of the present analysis is that the beams of the delaminated region are subjected to normal forces, as well. That is the essential reason for leading to a coupled flexural-longitudinal vibration problem. It is also concluded that delamination buckling can take place if the normal force is compressive in one of the half-periods of the vibration and reaches a critical value. The problem was also investigated experimentally by modal hammer and sweep excitation tests on beams made of E-glass/polyester in order to measure the natural frequencies and mode shapes. The comparison of the analytical and experimental results indicates the importance of the independent rotations provided by Timoshenko beams over the simple beam theory. The delamination buckling of the beams was captured based on the static stability analysis in the first step. Further results show that the problem is more complex than it was thought before, e.g., some nonlinearity, time-dependent stiffness as well as parametric excitation aspects were discovered during the present analysis.

  11. Monitoring Delamination of Plasma-Sprayed Thermal Barrier Coatings by Reflectance-Enhanced Luminescence

    Science.gov (United States)

    Eldridge, Jeffrey I.; Bencic, Timothy J.

    2006-01-01

    Highly scattering plasma-sprayed thermal barrier coatings (TBCs) present a challenge for optical diagnostic methods to monitor TBC delamination because scattering attenuates light transmitted through the TBC and usually degrades contrast between attached and delaminated regions of the TBC. This paper presents a new approach where reflectance-enhanced luminescence from a luminescent sublayer incorporated along the bottom of the TBC is used to identify regions of TBC delamination. Because of the higher survival rate of luminescence reflecting off the back surface of a delaminated TBC, the strong scattering exhibited by plasma-sprayed TBCs actually accentuates contrast between attached and delaminated regions by making it more likely that multiple reflections of luminescence off the back surface occur before exiting the top surface of the TBC. A freestanding coating containing sections designed to model an attached or delaminated TBC was prepared by depositing a luminescent Eu-doped or Er-doped yttria-stabilized zirconia (YSZ) luminescent layer below a plasma-sprayed undoped YSZ layer and utilizing a NiCr backing layer to represent an attached substrate. For specimens with a Eu-doped YSZ luminescent sublayer, luminescence intensity maps showed excellent contrast between unbacked and NiCr-backed sections even at a plasma-sprayed overlayer thickness of 300 m. Discernable contrast between unbacked and NiCr-backed sections was not observed for specimens with a Er-doped YSZ luminescent sublayer because luminescence from Er impurities in the undoped YSZ layer overwhelmed luminescence originating form the Er-doped YSZ sublayer.

  12. Wetting and growth behaviors in adsorbed systems with long-range forces

    Science.gov (United States)

    Nightingale, M. P.; Saam, W. F.; Schick, M.

    1984-10-01

    The growth and possible wetting behaviors of an adsorbed film are studied employing a solid-on-solid model in the presence of a hard wall and external potential V(h) which is of long range. The model is analyzed with the use of position-space renormalization-group methods within the Migdal approximation. The existence of wetting transitions and their nature depends on the asymptotic behavior of V(h) at large distances. We find that critical wetting cannot take place in this model. From what is known of V(h), we conclude that wetting can be observed only along the gas-liquid phase boundary; however, first-order transitions between thin and thick films, which may be experimentally difficult to distinguish from wetting, can be observed along any phase boundary. The nature of the global phase diagram depends on the form of V(h) and several general behaviors are presented. In particular, in the layering subregime we find that the limit of layering critical points is indeed the bulk roughening temperature as had been suggested by de Oliveira and Griffiths. The scaling of these layering critical points is given explicitly.

  13. Floating Node Method and Virtual Crack Closure Technique for Modeling Matrix Cracking-Delamination Interaction

    Science.gov (United States)

    DeCarvalho, N. V.; Chen, B. Y.; Pinho, S. T.; Baiz, P. M.; Ratcliffe, J. G.; Tay, T. E.

    2013-01-01

    A novel approach is proposed for high-fidelity modeling of progressive damage and failure in composite materials that combines the Floating Node Method (FNM) and the Virtual Crack Closure Technique (VCCT) to represent multiple interacting failure mechanisms in a mesh-independent fashion. In this study, the approach is applied to the modeling of delamination migration in cross-ply tape laminates. Delamination, matrix cracking, and migration are all modeled using fracture mechanics based failure and migration criteria. The methodology proposed shows very good qualitative and quantitative agreement with experiments.

  14. Floating Node Method and Virtual Crack Closure Technique for Modeling Matrix Cracking-Delamination Migration

    Science.gov (United States)

    DeCarvalho, Nelson V.; Chen, B. Y.; Pinho, Silvestre T.; Baiz, P. M.; Ratcliffe, James G.; Tay, T. E.

    2013-01-01

    A novel approach is proposed for high-fidelity modeling of progressive damage and failure in composite materials that combines the Floating Node Method (FNM) and the Virtual Crack Closure Technique (VCCT) to represent multiple interacting failure mechanisms in a mesh-independent fashion. In this study, the approach is applied to the modeling of delamination migration in cross-ply tape laminates. Delamination, matrix cracking, and migration are all modeled using fracture mechanics based failure and migration criteria. The methodology proposed shows very good qualitative and quantitative agreement with experiments.

  15. Estimation of Local Delamination Buckling in Orthotropic Composite Plates Using Kirchhoff Plate Finite Elements

    Directory of Open Access Journals (Sweden)

    Zoltán Juhász

    2015-01-01

    Full Text Available We analyse the buckling process of composite plates with through-the-width delamination and straight crack front applying uniaxial compression. We are focusing on the mixed mode buckling case, where the non-uniform distribution of the in-plane forces controls the occurence of the buckling of the delaminated layers. For the analysis, semi-discrete finite elements will be derived based on the Lèvy-type method. The method of harmonic balance is used for taking into account the force distribution that is generally non uniform in-plane.

  16. Buckling and Delamination of Ti/Cu/Si Thin Film During Annealing

    Science.gov (United States)

    Lin, Qijing; Yang, Shuming; Jing, Weixuan; Li, Changsheng; Wang, Chenying; Jiang, Zhuangde; Jiang, Kely

    2014-09-01

    In this paper, the formation of buckling and delamination of sandwiched stacking of Ti/Cu/Si thin film are investigated. The crystallization structures, the composition of the Cu/Ti thin films, and the surface morphology are measured during annealing. The results show that the solid-phase reaction between Cu and Ti occurs at the interface. Buckling is initiated in the thin film annealed at 600°C. The volume expansion promotes the buckling and further produces microcracks. With increasing volume expansion, there are cavities formed in the middle layer when the annealing temperature is up to 700°C. Finally, thin film is delaminated from the substrate.

  17. THE INFLUENCE OF THE TOOL POINT ANGLE AND FEED RATE ON THE DELAMINATION AT DRILLING OF PRE-LAMINATED PARTICLEBOARD

    Directory of Open Access Journals (Sweden)

    Mihai ISPAS

    2015-12-01

    Full Text Available Pre-laminated particleboard is a wood based composite extensively used in the furniture industry. Drilling is the most common machining process which prepares the panels for joining using twist/helical drills in the absolute majority of cases. The point angle of the drill bit and the feed speed during drilling play a major role in gaining a good surface quality and minimizing the delamination tendency of the pre-laminated particleboard. The objective of this study was to measure and analyze the influence of the two above-mentioned factors on the processing quality, evaluated by de size of delaminations, both, at the entrance side and the exit side of the drill bit. To assess the defect, two parameters were used: the delamination factor and the effective area of delamination. The results showed that, in general, the combination of small point angle with low feed rate minimizes the delamination of pre-laminated particleboard panels at drilling.

  18. Growth of laser-induced damage during repetitive illumination of HfO2-SiO2 multilayer mirror and polarizer coatings

    Energy Technology Data Exchange (ETDEWEB)

    Genin, F.Y.; Stolz, C.J.; Kozlowski, M.R.

    1997-01-01

    As peak fluence of high power lasers is increased, it becomes necessary to tolerate damage on mirrors, polarizers. To study how different types of damage morphologies initiate and grow during repetitive illumination, hafnia-silica multilayer mirror and polarizer coatings were laser damage tested. The coatings were prepared by e-beam evaporation and irradiated with a 3-ns pulse at 1064 nm. The damage morphology was recorded after each shot to determine the types of damage that cause massive unstable failure and lower the optic`s functional damage threshold. Results were summarized on damage stability maps plotting the average damage size vs number of shots for fluences ranging from 10 to 40 J/cm{sup 2}. The maps indicate that the commonly observed damage morphologies (pits, flat bottom pits, scalds, outer layer delamination) have distinct growth behaviors and influence the value of the functional damage threshold differently. While pits are stable up to fluences as high as 40 J/cm{sup 2}, flat bottom pits can grow during repetitive illumination above a critical fluence of about 35 J/cm{sup 2}. Scalds are formed in the first shot and never grow at fluences below 40 J/cm{sup 2}. Finally, delaminates are highly unstable and have the potential for damaging the coating catastrophically above 15 J/cm{sup 2}. Results show that delaminate damage should be prevented; this knowledge has allowed coatings development efforts to focus on eliminating the origin of such damage morphology.

  19. Growth, development, and behavior in early childhood following prenatal cocaine exposure: a systematic review.

    Science.gov (United States)

    Frank, D A; Augustyn, M; Knight, W G; Pell, T; Zuckerman, B

    2001-03-28

    Despite recent studies that failed to show catastrophic effects of prenatal cocaine exposure, popular attitudes and public policies still reflect the belief that cocaine is a uniquely dangerous teratogen. To critically review outcomes in early childhood after prenatal cocaine exposure in 5 domains: physical growth; cognition; language skills; motor skills; and behavior, attention, affect, and neurophysiology. Search of MEDLINE and Psychological Abstracts from 1984 to October 2000. Studies selected for detailed review (1) were published in a peer-reviewed English-language journal; (2) included a comparison group; (3) recruited samples prospectively in the perinatal period; (4) used masked assessment; and (5) did not include a substantial proportion of subjects exposed in utero to opiates, amphetamines, phencyclidine, or maternal human immunodeficiency virus infection. Thirty-six of 74 articles met criteria and were reviewed by 3 authors. Disagreements were resolved by consensus. After controlling for confounders, there was no consistent negative association between prenatal cocaine exposure and physical growth, developmental test scores, or receptive or expressive language. Less optimal motor scores have been found up to age 7 months but not thereafter, and may reflect heavy tobacco exposure. No independent cocaine effects have been shown on standardized parent and teacher reports of child behavior scored by accepted criteria. Experimental paradigms and novel statistical manipulations of standard instruments suggest an association between prenatal cocaine exposure and decreased attentiveness and emotional expressivity, as well as differences on neurophysiologic and attentional/affective findings. Among children aged 6 years or younger, there is no convincing evidence that prenatal cocaine exposure is associated with developmental toxic effects that are different in severity, scope, or kind from the sequelae of multiple other risk factors. Many findings once thought

  20. In-Situ Observation of Growth Behavior of Niobium Carbide during Dual-Phase Rapid Solidification of SUS347H

    Science.gov (United States)

    Yonemura, Mitsuharu; Osuki, Takahiro; Hirata, Hiroyuki; Ogawa, Kazuhiro

    2008-01-01

    In order to improve solidification cracking susceptibility, the crystallization of a heterophase such as the niobium carbide in the brittle temperature range is one of the effective techniques. In such a system, not only the growth behavior of dendrites during the rapid cooling but also the crystallization behavior of heterophase is very important. Therefore, diffraction patterns of a dual-phase mode Nb-bearing stainless steel during rapid cooling were investigated by in-situ two-dimensional time-resolved X-ray diffraction for the first time in order to reveal the microstructure formation. We discuss the growth behavior of dendrites with crystallization of niobium carbides. Subsequently, the niobium carbide formed epitaxially to the dendrite of the preferred in-plane orientation, having a small distorted orientation. With undercooling of several degree Celsius, the coherent growth on the δ-ferrite was stable for niobium carbide.

  1. Challenges in Modelling of Lightning-Induced Delamination; Effect of Temperature-Dependent Interfacial Properties

    Science.gov (United States)

    Naghipour, P.; Pineda, E. J.; Arnold, S.

    2014-01-01

    Lightning is a major cause of damage in laminated composite aerospace structures during flight. Due to the dielectric nature of Carbon fiber reinforced polymers (CFRPs), the high energy induced by lightning strike transforms into extreme, localized surface temperature accompanied with a high-pressure shockwave resulting in extensive damage. It is crucial to develop a numerical tool capable of predicting the damage induced from a lightning strike to supplement extremely expensive lightning experiments. Delamination is one of the most significant failure modes resulting from a lightning strike. It can be extended well beyond the visible damage zone, and requires sophisticated techniques and equipment to detect. A popular technique used to model delamination is the cohesive zone approach. Since the loading induced from a lightning strike event is assumed to consist of extreme localized heating, the cohesive zone formulation should additionally account for temperature effects. However, the sensitivity to this dependency remains unknown. Therefore, the major focus point of this work is to investigate the importance of this dependency via defining various temperature dependency profiles for the cohesive zone properties, and analyzing the corresponding delamination area. Thus, a detailed numerical model consisting of multidirectional composite plies with temperature-dependent cohesive elements in between is subjected to lightning (excessive amount of heat and pressure) and delamination/damage expansion is studied under specified conditions.

  2. Hierarchical system for autonomous sensing-healing of delamination in large-scale composite structures

    Science.gov (United States)

    Minakuchi, Shu; Sun, Denghao; Takeda, Nobuo

    2014-10-01

    This study combines our hierarchical fiber-optic-based delamination detection system with a microvascular self-healing material to develop the first autonomous sensing-healing system applicable to large-scale composite structures. In this combined system, embedded vascular modules are connected through check valves to a surface-mounted supply tube of a pressurized healing agent while fiber-optic-based sensors monitor the internal pressure of these vascular modules. When delamination occurs, the healing agent flows into the vascular modules breached by the delamination and infiltrates the damage for healing. At the same time, the pressure sensors identify the damaged modules by detecting internal pressure changes. This paper begins by describing the basic concept of the combined system and by discussing the advantages that arise from its hierarchical nature. The feasibility of the system is then confirmed through delamination infiltration tests. Finally, the hierarchical system is validated in a plate specimen by focusing on the detection and infiltration of the damage. Its self-diagnostic function is also demonstrated.

  3. Finite element modeling of guided wave scattering at delaminations in composite panels

    Science.gov (United States)

    Murat, B. I. S.; Fromme, P.

    2016-04-01

    Carbon fiber laminate composites, consisting of layers of polymer matrix reinforced with high strength carbon fibers, are increasingly employed for aerospace structures. They offer advantages for aerospace applications, e.g., good strength to weight ratio. However, impact during the operation and servicing of the aircraft can lead to barely visible and difficult to detect damage. Depending on the severity of the impact, delaminations can occur, reducing the load carrying capacity of the structure. Efficient structural health monitoring of composite panels can be achieved using guided ultrasonic waves propagating along the structure. The guided ultrasonic wave (A0 Lamb wave mode) scattering at delaminations was modelled using full three-dimensional Finite Element (FE) simulations. The influence of the delamination size was systematically investigated from a parameter study. The angular dependency of the scattered guided wave amplitude was calculated using a baseline subtraction method. A significant influence of the delamination width on the guided wave scattering was found. The sensitivity of guided waves for the detection of barely visible impact damage in composite panels has been predicted.

  4. Effect of Location of Delamination on Free Vibration of Cross-Ply Conical Shells

    Directory of Open Access Journals (Sweden)

    Sudip Dey

    2012-01-01

    Full Text Available Location of delamination is a triggering parameter for structural instability of laminated composites. In this paper, a finite element method is employed to determine the effects of location of delamination on free vibration characteristics of graphite-epoxy cross-ply composite pre-twisted shallow conical shells. The generalized dynamic equilibrium equation is derived from Lagrange's equation of motion neglecting Coriolis effect for moderate rotational speeds. The formulation is exercised by using an eight noded isoparametric plate bending element based on Mindlin's theory. Multi-point constraint algorithm is utilized to ensure the compatibility of deformation and equilibrium of resultant forces and moments at the delamination crack front. The standard eigen value problem is solved by applying the QR iteration algorithm. Finite element codes are developed to obtain the numerical results concerning the effects of location of delamination, twist angle and rotational speed on the natural frequencies of cross-ply composite shallow conical shells. The mode shapes are also depicted for a typical laminate configuration. Numerical results obtained from parametric studies of both symmetric and anti-symmetric cross-ply laminates are the first known non-dimensional natural frequencies for the type of analyses carried out here.

  5. BEM solution of delamination problems using an interface damage and plasticity model

    CERN Document Server

    Panagiotopoulos, C G; Roubicek, T

    2012-01-01

    The problem of quasistatic and rate-independent evolution of elastic-plastic-brittle delamination at small strains is considered. Delamination processes for linear elastic bodies glued by an adhesive to each other or to a rigid outer surface are studied. The energy amounts dissipated in fracture Mode I (opening) and Mode II (shear) at an interface may be different. A concept of internal parameters is used here on the delaminating interfaces, involving a couple of scalar damage variable and a plastic tangential slip with kinematic-type hardening. The so-called energetic solution concept is employed. An inelastic process at an interface is devised in such a way that the dissipated energy depends only on the rates of internal parameters and therefore the model is associative. A fully implicit time discretization is combined with a spatial discretization of elastic bodies by the BEM to solve the delamination problem. The BEM is used in the solution of the respective boundary value problems, for each subdomain sep...

  6. Computational investigation of the delamination of polymer coatings during stent deployment.

    Science.gov (United States)

    Hopkins, C G; McHugh, P E; McGarry, J P

    2010-07-01

    Recent advances in angioplasty have involved the application of polymer coatings to stent surfaces for purposes of drug delivery. Given the high levels of deformation developed in the plastic hinge of a stent during deployment, the achievement of an intact bond between the coating and the stent presents a significant mechanical challenge. Problems with coating delamination have been reported in recent experimental studies. In this paper, a cohesive zone model of the stent-coating interface is implemented in order to investigate coating debonding during stent deployment. Simulations reveal that coatings debond from the stent surface in tensile regions of the plastic hinge during deployment. The critical parameters governing the initiation of delamination include the coating thickness and stiffness, the interface strength between the coating and stent surface, and the curvature of the plastic hinge. The coating is also computed to debond from the stent surface in compressive regions of the plastic hinge by a buckling mechanism. Computed patterns of coating delamination correlate very closely with experimental images. This study provides insight into the critical factors governing coating delamination during stent deployment and offers a predictive framework that can be used to improve the design of coated stents.

  7. Interaction between cracking, delamination and buckling in brittle elastic thin films

    NARCIS (Netherlands)

    Vellinga, W. P.; Van den Bosch, M.; Geers, M. G. D.

    2008-01-01

    A discrete lattice based model for the interaction of cracking, delamination and buckling of brittle elastic coatings is presented. The model is unique in its simultaneous incorporation of the coating and of disorder in the interface and material properties, leading to realistic 3D bending (and buck

  8. On a multiscale strategy and its optimization for the simulation of combined delamination and buckling

    Science.gov (United States)

    Saavedra, K.; Allix, O.; Gosselet, P.

    2012-08-01

    This paper investigates a computational strategy for studying the interactions between multiple through-the-width delaminations and global or local buckling in composite laminates taking into account possible contact between the delaminated surfaces. In order to achieve an accurate prediction of the quasi-static response, a very refined discretization of the structure is required, leading to the resolution of very large and highly nonlinear numerical problems. In this paper, a nonlinear finite element formulation along with a parallel iterative scheme based on a multiscale domain decomposition are used for the computation of 3D mesoscale models. Previous works by the authors already dealt with the simulation of multiscale delamination assuming small perturbations. This paper presents the formulation used to include geometric nonlinearities into this existing multiscale framework and discusses the adaptations that need to be made to the iterative process in order to ensure the rapid convergence and the scalability of the method in the presence of buckling and delamination. These various adaptations are illustrated by simulations involving large numbers of DOFs.

  9. The Mexican hat effect on the delamination buckling of a compressed thin film

    Science.gov (United States)

    Zhang, Yin; Liu, Yun

    2014-12-01

    Because of the interaction between film and substrate, the film buckling stress can vary significantly, depending on the delamination geometry, the film and substrate mechanical properties. The Mexican hat effect indicates such interaction. An analytical method is presented, and related dimensional analysis shows that a single dimensionless parameter can effectively evaluate the effect.

  10. Cracking and delamination of metal organic vapour deposited alumina and silica films

    NARCIS (Netherlands)

    Haanappel, V.A.C.; Haanappel, V.A.C.; van Corbach, H.D.; Fransen, T.; Gellings, P.J.

    1993-01-01

    Amorphous alumina and silica films were deposited on AISI by thermal decomposition at atmospheric pressure of aluminium-tri-sec-butoxide and di-acetoxy-di-tertiary-butoxided-silane respectively. Above a critical coating thickness of the oxide films, cracking and delamination occurred during the

  11. Delamination of a strong film from a ductile substrate during indentation unloading

    NARCIS (Netherlands)

    Abdul-Baqi, A.; van der Giessen, E.

    2001-01-01

    In this work, a finite element method was performed to simulate the spherical indentation of a ductile substrate coated by a strong thin film. Our objective was to study indentation-induced delamination of the film from the substrate. The film was assumed to be linear elastic, the substrate was elas

  12. Simulation of Thermographic Responses of Delaminations in Composites with Quadrupole Method

    Science.gov (United States)

    Winfree, William P.; Zalameda, Joseph N.; Howell, Patricia A.; Cramer, K. Elliott

    2016-01-01

    The application of the quadrupole method for simulating thermal responses of delaminations in carbon fiber reinforced epoxy composites materials is presented. The method solves for the flux at the interface containing the delamination. From the interface flux, the temperature at the surface is calculated. While the results presented are for single sided measurements, with ash heating, expansion of the technique to arbitrary temporal flux heating or through transmission measurements is simple. The quadrupole method is shown to have two distinct advantages relative to finite element or finite difference techniques. First, it is straight forward to incorporate arbitrary shaped delaminations into the simulation. Second, the quadrupole method enables calculation of the thermal response at only the times of interest. This, combined with a significant reduction in the number of degrees of freedom for the same simulation quality, results in a reduction of the computation time by at least an order of magnitude. Therefore, it is a more viable technique for model based inversion of thermographic data. Results for simulations of delaminations in composites are presented and compared to measurements and finite element method results.

  13. Cathodic delamination of seawater-immersed anticorrosive coatings: Mapping of parameters affecting the rate

    DEFF Research Database (Denmark)

    Sørensen, Per Aggerholm; Dam-Johansen, Kim; Weinell, C. E.

    2010-01-01

    -steel interface, where solid iron is oxidized to ferrous ions and oxygen is reduced to hydroxyl ions. In this work, the effects of various parameters on cathodic delamination have been investigated. The parameters are: permeability of the coating, concentration of dissolved oxygen and cations, polarization...

  14. Energy efficiency, human behavior, and economic growth: Challenges to cutting energy demand to sustainable levels

    Energy Technology Data Exchange (ETDEWEB)

    Santarius, Tilman, E-mail: tilman@santarius.de [Visiting Scholar, Institute of European Studies and Energy and Resources Group, University of California, Berkeley, 310 Barrows Hall, Berkeley, CA 94720-3050 (United States)

    2015-03-30

    Increasing energy efficiency in households, transportation, industries, and services is an important strategy to reduce energy service demand to levels that allow the steep reduction of greenhouse gases, and a full fledged switch of energy systems to a renewable basis. Yet, technological efficiency improvements may generate so-called rebound effects, which may ‘eat up’ parts of the technical savings potential. This article provides a comprehensive review of existing research on these effects, raises critiques, and points out open questions. It introduces micro-economic rebound effect and suggests extending consumer-side analysis to incorporate potential ‘psychological rebound effects.’ It then discusses meso-economic rebound effects, i.e. producer-side and market-level rebounds, which so far have achieved little attention in the literature. Finally, the article critically reviews evidence for macro-economic rebound effects as energy efficiency-induced economic growth impacts. For all three categories, the article summarizes assessments of their potential quantitative scope, while pointing out remaining methodological weaknesses and open questions. As a rough “rule of thumb”, in the long term and on gross average, only half the technical savings potential of across-the-board efficiency improvements may actually be achieved in the real world. Policies that aim at cutting energy service demand to sustainable levels are well advised to take due note of detrimental behavioral and economic growth impacts, and should foster policies and measures that can contain them.

  15. Growth behavior of anodic oxide formed by aluminum anodizing in glutaric and its derivative acid electrolytes

    Science.gov (United States)

    Nakajima, Daiki; Kikuchi, Tatsuya; Natsui, Shungo; Suzuki, Ryosuke O.

    2014-12-01

    The growth behavior of anodic oxide films formed via anodizing in glutaric and its derivative acid solutions was investigated based on the acid dissociation constants of electrolytes. High-purity aluminum foils were anodized in glutaric, ketoglutaric, and acetonedicarboxylic acid solutions under various electrochemical conditions. A thin barrier anodic oxide film grew uniformly on the aluminum substrate by glutaric acid anodizing, and further anodizing caused the film to breakdown due to a high electric field. In contrast, an anodic porous alumina film with a submicrometer-scale cell diameter was successfully formed by ketoglutaric acid anodizing at 293 K. However, the increase and decrease in the temperature of the ketoglutaric acid resulted in non-uniform oxide growth and localized pitting corrosion of the aluminum substrate. An anodic porous alumina film could also be fabricated by acetonedicarboxylic acid anodizing due to the relatively low dissociation constants associated with the acid. Acid dissociation constants are an important factor for the fabrication of anodic porous alumina films.

  16. [Growth behavior of spiral ganglion explants on cochlear implant electrodes and their materials].

    Science.gov (United States)

    Hansen, S; Mlynski, R; Volkenstein, S; Stark, T; Schwaab, M; Dazert, S; Brors, D

    2009-04-01

    With the increasing use of cochlear implants (CIs), the insertion of alloplastic material into the inner ear is nowadays an established treatment for severe to profound hearing loss in children and adults. Beyond its widespread use, the biocompatibility of the CI electrode and its interaction with the neural structures of the cochlea is not yet established. To investigate the survival and growth behavior of spiral ganglion neurons on different CI materials, spiral ganglion explants from newborn rats were cultured on silicone and platinum, on a surface combination of silicone and platinum, and, finally, on a CI electrode. The results of this study indicate that the growth of spiral ganglion neurons in vitro is strongly influenced by the different materials and their arrangement, with platinum exhibiting the highest degree of biocompatibility with respect to neurite extension. Level differences in the surface structure between silicone and platinum lead to inhibition of neurite outgrowth. Furthermore, the culturing of spiral ganglion explants on a CI electrode leads to neurite sprouting toward the electrodes made of platinum. The biocompatibility of CI materials with spiral ganglion neurons was shown in this study, but it differs with different CI materials. Besides the material itself, the arrangement of the materials can affect the neurite extension.

  17. Energy efficiency, human behavior, and economic growth: Challenges to cutting energy demand to sustainable levels

    Science.gov (United States)

    Santarius, Tilman

    2015-03-01

    Increasing energy efficiency in households, transportation, industries, and services is an important strategy to reduce energy service demand to levels that allow the steep reduction of greenhouse gases, and a full fledged switch of energy systems to a renewable basis. Yet, technological efficiency improvements may generate so-called rebound effects, which may `eat up' parts of the technical savings potential. This article provides a comprehensive review of existing research on these effects, raises critiques, and points out open questions. It introduces micro-economic rebound effect and suggests extending consumer-side analysis to incorporate potential `psychological rebound effects.' It then discusses meso-economic rebound effects, i.e. producer-side and market-level rebounds, which so far have achieved little attention in the literature. Finally, the article critically reviews evidence for macro-economic rebound effects as energy efficiency-induced economic growth impacts. For all three categories, the article summarizes assessments of their potential quantitative scope, while pointing out remaining methodological weaknesses and open questions. As a rough "rule of thumb", in the long term and on gross average, only half the technical savings potential of across-the-board efficiency improvements may actually be achieved in the real world. Policies that aim at cutting energy service demand to sustainable levels are well advised to take due note of detrimental behavioral and economic growth impacts, and should foster policies and measures that can contain them.

  18. Fatigue crack growth behaviors of a new burn-resistant highly-stabilized beta titanium alloy

    Institute of Scientific and Technical Information of China (English)

    WU Huan; ZHAO Yongqing; ZENG Weidong; QIAN Li

    2009-01-01

    This article presents the fatigue crack growth (FCG) behaviors of a new burn-resistant highly-stabilized beta Ti40 alloy. The FCG rotes were analyzed. The fracture surfaces and the side surfaces of the test samples were explored. The results show that frequency affects the cracking behaviors of Ti40 alloy. Temperature also plays an important role in Ti40 alloy cracking. At room temperature (25℃), when the frequency increases, the cracking rate changes a little in the range of low stress intensity factor (ΔK), while it changes significantly when ΔK is high. At 500℃, the cracking rate of Ti40 alloy changes significantly during all the course of clacking. The frequency also affects the microstructure patterns of Ti40 alloy. A number of secondary cracks appear in the area more than 200 μm from the main crack at a high ΔK when the fre-quency is 1 Hz, but only a few secondary cracks exist when the frequency is 10 Hz. Facet image is the main image of the fracture surfaces when the frequency is 1 Hz. While, ductile striation occupies most of the area of fracture surfaces when the frequency is 10 Hz.

  19. The arc delaminate: a geochemical reservoir twice the size of the continental crust

    Science.gov (United States)

    Jagoutz, O.; Schmidt, M. W.

    2012-12-01

    Most primitive melts in arcs are basaltic in composition but the continental crust or arc average is andesitic. To evolve from a primitive basalt to an andesitic composition, cumulates have to be fractionated and, if gravitationally unstable, can be delaminated. Such lower crustal cumulates are exposed in the Kohistan arc (N Pakistan) in a 10 km section through dunites, wehrlites, websterites, cpx-bearing garnetites and hornblendites, and garnet gabbros. We have compiled primitive melts for nine island arcs from the literature and fitted these with the bulk Kohistan arc [1] or average bulk continental crust [2] and the Kohistan cumulates. By average, ~15 wt% wehrlite + ~20% garnet hornblendite + ~35% garnet gabbro complement ~30% arc or continental crust and explain very well (r2~2) the evolution from a tholeiitic/calc-alkaline primitive high-Mg basalt to the continental crust. The bulk delaminate has 44-48 wt% SiO2, total alkalis of 1.1-1.4 wt% and an XMg of 0.67-0.69. Mass fractions derived from major elements were employed to compare trace elements: cumulates+crust deviate on average only by 25-30% from primitive melts, with the biggest deviations on the subduction-added traces. Relative to the continental or arc crust, the delaminate mass results to 1.8-2.5 times that of the continental crust. The delaminates have rho=3.2-3.5 g/cm3 and VP=7.9-8.2. At the base of the crust, they are thus difficult to distinguish seismically. Once reaching a critical thickness, they may sink into the deeper mantle where they form a geochemical reservoir twice the size of the continental crust. With respect to primitive mantle, the delaminate is enriched in Ba, K, Sr, and P and REE with LREEdelaminate reservoir would develop highly unradiogenic Pb over time and would counterbalance the radiogenic MORB and OIB reservoirs. Delamination of twice as much material as remains in the arc crust increases the flux of primitive melt in arcs threefold. This places the magma

  20. Stress Corrosion Crack Growth Behavior of Titanium Alloy/Bioactive Glasses Sandwiches in Simulated Human Physiological Environment

    Institute of Scientific and Technical Information of China (English)

    2002-01-01

    Based on a series of newly developed bioactive glasses having suitable thermo-mechanical properties to allow application as fixation agents between bone and titanium alloy biomedical implants, the stress corrosion crack growth(SCCG) behavior of their interfaces with Ti6Al4V was investigated in simulated body fluid (SBF) with the objectiveof discerning the salient mechanisms of crack advance and to assess the reliability of the bonds. Results indicatedthat crack growth rates in Ti6Al4V/glass/Ti6Al4V sandwich specimens were nearly the same as or slightly lowerthan those in the bulk glasses at comparable stress intensities; indeed, cracks would prefer to propagate off theinterface, suggesting that the Ti6Al4V/glass interface has relatively good crack-growth resistance. Mechanistically,interfacial crack growth appears to be controlled by the classic stress corrosion mechanisms for silicate glasses, withno discernible effect of bioactivity on the SCCG behavior being observed.

  1. Application of piecewise hierarchical linear growth modeling to the study of continuity in behavioral development of baboons (Papio hamadryas).

    Science.gov (United States)

    Hernández-Lloreda, María Victoria; Colmenares, Fernando; Martínez-Arias, Rosario

    2004-09-01

    In behavioral science, developmental discontinuities are thought to arise when the association between an outcome measure and the underlying process changes over time. Sudden changes in behavior across time are often taken to indicate that a reorganization in the outcome-process relationship may have occurred. The authors proposed in this article the use of piecewise hierarchical linear growth modeling as a statistical methodology to search for discontinuities in behavioral development and illustrated its possibilities by applying 2-piece hierarchical linear models to the study of developmental trajectories of baboon (Papio hamadryas) mothers' behavior during their infants' 1st year of life. The authors provided empirical evidence that piecewise growth modeling can be used to determine whether abrupt changes in development trajectories are tied to changes in the underlying process. ((c) 2004 APA, all rights reserved).

  2. INVESTIGATION OF THE LOW-CYCLE FATIGUE AND FATIGUE CRACK GROWTH BEHAVIORS OF P91 BASE METAL AND WELD JOINTS

    Institute of Scientific and Technical Information of China (English)

    H.C. Yang; Y. Tu; M.M. Yu; J. Zhao

    2004-01-01

    Low cycle fatigue tests and crack growth propagations tests on P91 pipe base metal and its weld joints were conducted at three different temperatures: room temperature,550℃ and 575℃. The strain-life was analyzed, and the changes in fatigue life behavior and fatigue growth rates with increasing temperature were discussed. The different properties of the base metal and its weld joint have been analyzed.

  3. Early protein malnutrition negatively impacts physical growth and neurological reflexes and evokes anxiety and depressive-like behaviors.

    Science.gov (United States)

    Belluscio, Laura M; Berardino, Bruno G; Ferroni, Nadina M; Ceruti, Julieta M; Cánepa, Eduardo T

    2014-04-22

    Malnutrition is a worldwide problem affecting millions of unborn and young children during the most vulnerable stages of their development. In humans, poor maternal nutrition is a major cause of intrauterine growth restriction which is associated with an increased risk of perinatal mortality and long-term morbidity. In addition, intrauterine growth restriction correlates with neurodevelopmental delays and alterations of brain structure and neurochemistry. While there is no doubt that maternal malnutrition is a principal cause of perturbed development of the fetal brain and that all nutrients have certain influence on brain maturation, proteins appear to be the most critical for the development of neurological functions. In the present study we assessed male and female mouse offspring, born to dams protein restricted during pregnancy and lactation, in physical growth and neurobehavioral development and also in social interaction, motivation, anxiety and depressive behaviors. Moreover, we evaluate the impact of the low protein diet on dams in relation to their maternal care and anxiety-related behavior given that these clearly affect pups development. We observed that maternal protein restriction during pregnancy and lactation delayed the physical growth and neurodevelopment of the offspring in a sex-independent manner. In addition, maternal undernutrition negatively affected offspring's juvenile social play, motivation, exploratory activity and risk assessment behaviors. These findings show that protein restriction during critical periods of development detrimentally program progeny behavior. Copyright © 2014 Elsevier Inc. All rights reserved.

  4. Kinetic Behavior of Aggregation-Exchange Growth Process with Catalyzed-Birth

    Institute of Scientific and Technical Information of China (English)

    HAN An-Jia; CHEN Yu; LIN Zhen-Quan; KE Jian-Hong

    2007-01-01

    We propose an aggregation model of a two-species system to mimic the growth of cities' population and assets,in which irreversible coagulation reactions and exchange reactions occur between any two aggregates of the same species,and the monomer-birth reactions of one species occur by the catalysis of the other species.In the case with population-catalyzed birth of assets,the rate kernel of an asset aggregate Bκ of size k grows to become an aggregate Bκ+ 1through a monomer-birth catalyzed by a population aggregate Aj of size j is J(k,j) = Jkjλ.And in mutually catalyzed birth model,the birth rate kernels of population and assets are H(k,j) = Hkjη and J(k,j) = Jkjλ,respectively.The kinetics of the system is investigated based on the mean-field theory.In the model of population-catalyzed birth of assets,the long-time asymptotic behavior of the assets aggregate size distribution obeys the conventional or modified scaling form.In mutually catalyzed birth system,the asymptotic behaviors of population and assets obey the conventional scaling form in the case ofη =λ= 0,and they obey the modified scalingform in the case of η = 0,λ= 1.In the case of η = λ = 1,the total mass of population aggregates and that of asset aggregates both grow much faster than those in population-catalyzed birth of assets model,and they approaches to infinite values in finite time.

  5. Moderate heat challenge increased yolk steroid hormones and shaped offspring growth and behavior in chickens.

    Directory of Open Access Journals (Sweden)

    Aline Bertin

    Full Text Available BACKGROUND: Environmental challenges might affect the maternal organism and indirectly affect the later ontogeny of the progeny. We investigated the cross-generation impact of a moderate heat challenge in chickens. We hypothesized that a warm temperature--within the thermotolerance range--would affect the hormonal environment provided to embryos by mothers, and in turn, affect the morphology and behavioral phenotype of offspring. METHODOLOGY/PRINCIPAL FINDINGS: Laying hens were raised under a standard thermal condition at 21°C (controls or 30°C (experimental for 5 consecutive weeks. A significant increase was observed in the internal temperature of hens exposed to the warm treatment; however plasma corticosterone levels remained unaffected. The laying rate was not affected, but experimental hens laid lighter eggs than the controls during the treatment. As expected, the maternal thermal environment affected yolk hormone contents. Eggs laid by the experimental hens showed significantly higher concentrations of yolk progesterone, testosterone, and estradiol. All chicks were raised under standard thermal conditions. The quality of hatchlings, growth, feeding behavior and emotional reactivity of chicks were analyzed. Offspring of experimental hens (C30 chicks were lighter but obtained better morphological quality scores at hatching than the controls (C21 chicks. C30 chicks expressed lesser distress calls when exposed to a novel food. Unlike C21 chicks, C30 chicks expressed no preference for energetic food. CONCLUSION/SIGNIFICANCE: Our findings suggest that moderate heat challenge triggers maternal effects and modulate the developmental trajectory of offspring in a way that may be adaptive. This suggests that the impact of heat challenges on captive or wild populations might have a cross-generation effect.

  6. Effect of Specimen Orientation on Fatigue Crack Growth Behavior in Friction Stir Welded Al7075-T651 Joints

    Energy Technology Data Exchange (ETDEWEB)

    Jeong, Yeui Han; Kim, Seon Jin [Pukyoung National University, Busan (Korea, Republic of)

    2014-12-15

    The aim of this paper is to investigate the effects of crack orientation on fatigue crack growth behavior in friction stir welded (FSWed) Al 7075-T651. Fatigue crack growth testing was conducted on compact tension (CT) specimens machined from the friction stir welds and the base metal under constant stress intensity factor range control. Tests were performed with the crack propagating nominally perpendicular to the weld line (termed the TL specimen) and the crack propagating in a parallel direction of the weld line (termed the LT specimen), and with three different constant stress intensity factor ranges. Both these specimen orientations were found to have a considerable effect on the fatigue crack growth behavior. Paris’s law was adopted for the analysis of experimental results; the exponent m of the WM-LT specimen was determined to be 3.56, which was the largest value in this experimental conditions.

  7. Photosynthetic behavior, growth and essential oil production of Melissa officinalis L. cultivated under colored shade nets

    Directory of Open Access Journals (Sweden)

    Graziele C Oliveira

    2016-03-01

    Full Text Available The modulation of light is of importance during cultivation of medicinal plants to obtain desirable morphological and physiological changes associated with the maximum production of active principles. This study aimed to evaluate the effect of the light spectrum transmitted by colored shade nets on growth, essential oil production and photosynthetic behavior in plants of lemon balm (Melissa officinalis L. Plants were cultivated in pots for 4-mo under black, red, and blue nets with 50% shading, and full sunlight exposure. Biometric and anatomical variables, essential oil yield, global solar radiation, photon flux density, chlorophyll content, and gas exchange parameters were measured in M. officinalis leaves. The results showed that despite being considered a partial shade plant, this species is able to adapt to full sunlight conditions without increasing biomass production. The spectral changes provided by colored shade nets did not caused any noticeable change in leaf anatomy of M. officinalis. However, the use of blue net resulted in increments of 116% in plant height, 168% in leaf area, 42% in chlorophyll content and 30% in yield of essential oil in lemon balm plants. These plant's qualities make the use of blue net a cultivation practice suitable for commercial use.

  8. Creep and Creep Crack Growth Behaviors for SMAW Weldments of Gr. 91 Steel

    Energy Technology Data Exchange (ETDEWEB)

    Kim, Woo Gon; Yin, Song Nan; Park, Ji Yeon; Hong, Sung Deok; Kim, Yong Wan [Korea Atomic Energy Research Institute, Daejeon (Korea, Republic of); Park, Jae Young [Pukyong National University, Busan (Korea, Republic of)

    2010-05-15

    High Cr ferritic resistance steels with tempered martensite microstructures posses enhanced creep strength at the elevated temperatures. Those steels as represented by a modified 9Cr-1Mo steel (ASME Grade 91, hereafter Gr.91) are regarded as main structural materials of sodium-cooled fast reactors (SFR) and reactor pressure vessel materials of very high temperature reactors (VHTR). The SFR and VHTR systems are designed during long-term duration reaching 60 years at elevated temperatures and often subjected to non-uniform stress and temperature distribution during service. These conditions may generate localized creep damage and propagate the cracks and ultimately may cause a fracture. A significant portion of its life is spent in crack propagation. Therefore, a creep crack growth rate (CCGR) due to creep damage should be assessed for both the base metal (BM) and welded metal (WM). Enough CCGR data for them should be provided for assessing their structural integrities. However, their CCGR data for the Gr. 91 steels is still insufficient. In this study, the CCGR for the BM and the WM of the Gr. 91 steel was comparatively investigated. A series of the CCG tests were conducted under different applied loads for the BM and the WM at 600 .deg. C. The CCGR was characterized in terms of the C parameter, and their CCG behavior were compared, respectively

  9. Phenolic acid degradation potential and growth behavior of lactic acid bacteria in sunflower substrates.

    Science.gov (United States)

    Fritsch, Caroline; Heinrich, Veronika; Vogel, Rudi F; Toelstede, Simone

    2016-08-01

    Sunflower flour provides a high content of protein with a well-balanced amino acid composition and is therefore regarded as an attractive source for protein. The use for human nutrition is hindered by phenolic compounds, mainly chlorogenic acid, which can lead under specific circumstances to undesirable discolorations. In this study, growth behavior and degradation ability of chlorogenic acid of four lactic acid bacteria were explored. Data suggested that significant higher fermentation performances on sunflower flour as compared to sunflower protein concentrate were reached by Lactobacillus plantarum, Pediococcus pentosaceus, Lactobacillus gasseri and Bifidobacterium animalis subsp. lactis. In fermentation with the latter two strains reduced amounts of chlorogenic acid were observed in sunflower flour (-11.4% and -19.8%, respectively), which were more pronounced in the protein concentrate (-50.7% and -95.6%, respectively). High tolerances against chlorogenic acid and the cleavage product quinic acid with a minimum inhibitory concentration (MIC) of ≥20.48 mg/ml after 48 h were recorded for all strains except Bifidobacterium animalis subsp. lactis, which was more sensitive. The second cleavage compound, caffeic acid revealed a higher antimicrobial potential with MIC values of 0.64-5.12 mg/ml. In this proof of concept study, degradation versus inhibitory effect suggest the existence of basic mechanisms of interaction between phenolic acids in sunflower and lactic acid bacteria and a feasible way to reduce the chlorogenic acid content, which may help to avoid undesired color changes.

  10. Growth and corrosion behavior of molybdate passivation film on hot dip galvanized steel

    Institute of Scientific and Technical Information of China (English)

    卢锦堂; 孔纲; 陈锦虹; 许乔瑜; 眭润舟

    2003-01-01

    Hot dip galvanized steel sheets were passivated by molybdate aqueous solution containing 10 g/LNa2 MoO4 @ 2H2O, and the growth behavior and corrosion resistance of the passivation film were investigated. Inthe initial stage of passivation, the mass gain of film increases with passivation time proportionally. The film growsup more quickly and is apt to cracking at grain boundaries of zinc, then the cracks spread gradually on the whole sur-face of the film, and eventually the film will flake off with the increasing of film thickness. XPS results indicate thatMo compounds are present in Mo(Ⅵ) state on the surface of the film, and Mo(Ⅵ) and Mo(Ⅳ ) states inside thefilm. NSS test shows that, the corrosion resistance of the passivation film decreases as the cracks occur, but inAASS test, the thicker the film is, the better the corrosion resistance is, the cracks of film have little effect on thecorrosion resistance.

  11. Geometry and Material Constraint Effects on Creep Crack Growth Behavior in Welded Joints

    Science.gov (United States)

    Li, Y.; Wang, G. Z.; Xuan, F. Z.; Tu, S. T.

    2017-02-01

    In this work, the geometry and material constraint effects on creep crack growth (CCG) and behavior in welded joints were investigated. The CCG paths and rates of two kinds of specimen geometry (C(T) and M(T)) with initial cracks located at soft HAZ (heat-affected zone with lower creep strength) and different material mismatches were simulated. The effect of constraint on creep crack initiation (CCI) time was discussed. The results show that there exists interaction between geometry and material constraints in terms of their effects on CCG rate and CCI time of welded joints. Under the condition of low geometry constraint, the effect of material constraint on CCG rate and CCI time becomes more obvious. Higher material constraint can promote CCG due to the formation of higher stress triaxiality around crack tip. Higher geometry constraint can increase CCG rate and reduce CCI time of welded joints. Both geometry and material constraints should be considered in creep life assessment and design for high-temperature welded components.

  12. CREEP CRACK GROWTH BEHAVIOR OF ALLOY 718 DURING HIGH TEMPERATURE EXPOSURE

    Institute of Scientific and Technical Information of China (English)

    J.X. Dong; M.C. Zhang; Y.P. Zeng; X.S. Xie

    2005-01-01

    Alloy 718 is a precipitation strengthened nickel-based superalloy based on the precipitation ofγ"-Ni3Nb (DO22 structure) and γ-Ni3(Al, Ti) (Ll2 structure) phases. Creep crack growth rate(CCGR) was investigated after high temperature exposure at 593, 650 and 677℃ for 2000h inAlloy 718. In addition to the coalescence of γ'/ γ" and the amount increasing of δ phase, theexistence of a bcc chromium enriched α-Cr phase was observed by SEM, and the weight fraction of α-Cr and other phases were determined by chemical phase analysis methods. The CCGR behavior and regulation have been analyzed by means of strength and structure analysis approaches. The experimental results show higher the exposure temperature and longer the ex posure time, lower the CCGR. This is probably attributed to the interaction of material softening and brittling due to complex structure changes during high temperature exposure. Therefore,despite α-Cr phase formation and amount enhancement were run in this test range. It seems to us a srnall amount of α-Cr will be not harmful for creep crack propagation resistance, which is critical for disk application in aircraft and land-based gas turbine.

  13. Moderate maternal food restriction in mice impairs physical growth, behavior, and neurodevelopment of offspring.

    Science.gov (United States)

    Akitake, Yoshiharu; Katsuragi, Shinji; Hosokawa, Masato; Mishima, Kenichi; Ikeda, Tomoaki; Miyazato, Mikiya; Hosoda, Hiroshi

    2015-01-01

    Intrauterine growth retardation (IUGR) occurs in 3% to 7% of all pregnancies. Recent human studies have indicated that neurodevelopmental disabilities, learning disorders, memory impairment, and mood disturbance are common in IUGR offspring. However, the interactions between IUGR and neurodevelopmental disorders are unclear because of the wide range of causes of IUGR, such as maternal malnutrition, placental insufficiency, pregnancy toxemia, and fetal malformations. Meanwhile, many studies have shown that moderate food restriction enhances spatial learning and improves mood disturbance in adult humans and animals. To date, the effects of maternal moderate food restriction on fetal brain remain largely unknown. In this study, we hypothesized that IUGR would be caused by even moderate food restriction in pregnant females and that the offspring would have neurodevelopmental disabilities. Mid-pregnant mice received moderate food restriction through the early lactation period. The offspring were tested for aspects of physical development, behavior, and neurodevelopment. The results showed that moderate maternal food restriction induced IUGR. Offspring had low birth weight and delayed development of physical and coordinated movement. Moreover, IUGR offspring exhibited mental disabilities such as anxiety and poor cognitive function. In particular, male offspring exhibited significantly impaired cognitive function at 3 weeks of age. These results suggested that a restricted maternal diet could be a risk factor for developmental disability in IUGR offspring and that male offspring might be especially susceptible. Copyright © 2015 Elsevier Inc. All rights reserved.

  14. Effect of tool geometry and cutting parameters on delamination and thrust forces in drilling CFRP/Al-Li

    Science.gov (United States)

    El Bouami, Souhail; Habak, Malek; Franz, Gérald; Velasco, Raphaël; Vantomme, Pascal

    2016-10-01

    Composite materials are increasingly used for structural parts in the aeronautic industries. Carbon Fiber-Reinforced Plastics (CFRP) are often used in combination with metallic materials, mostly aluminium alloys. This raises new problems in aircraft assembly. Delamination is one of these problems. In this study, CFRP/Al-Li stacks is used as experimental material for investigation effect of interaction of cutting parameters (cutting speed and feed rate) and tool geometry on delamination and thrust forces in drilling operation. A plan of experiments, based on Taguchi design method, was employed to investigate the influence of tool geometry and in particular the point angle and cutting parameters on delamination and axial effort. The experimental results demonstrate that the feed rate is the major parameter and the importance of tool point angle in delamination and thrust forces in the stacks were shown.

  15. Wave Propagation Analysis in Composite Laminates Containing a Delamination Using a Three-Dimensional Spectral Element Method

    Directory of Open Access Journals (Sweden)

    Fucai Li

    2012-01-01

    Full Text Available A three-dimensional spectral element method (SEM was developed for analysis of Lamb wave propagation in composite laminates containing a delamination. SEM is more efficient in simulating wave propagation in structures than conventional finite element method (FEM because of its unique diagonal form of the mass matrix. Three types of composite laminates, namely, unidirectional-ply laminates, cross-ply laminates, and angle-ply laminates are modeled using three-dimensional spectral finite elements. Wave propagation characteristics in intact composite laminates are investigated, and the effectiveness of the method is validated by comparison of the simulation results with analytical solutions based on transfer matrix method. Different Lamb wave mode interactions with delamination are evaluated, and it is demonstrated that symmetric Lamb wave mode may be insensitive to delamination at certain interfaces of laminates while the antisymmetric mode is more suited for identification of delamination in composite structures.

  16. Effect of Material Property of Interply Film on the Delamination in Laminated Composites 8

    Institute of Scientific and Technical Information of China (English)

    WeiFENG; QiaoHUANG

    1999-01-01

    The delamination is one of the main failure modes in laminated composites.In order to suppress and /or delay it,considerable research has been devoted to the reduction of the interlaminar stresses at the interfaces between two different plies.This paper studies the effect of isotropic layers placed at ply interface on the interlaminar behaviour of the angle-ply laminated composites.The results of the experiment and numerical analysis show that the material properties of interply film have strong influence on the interlaminar behaviour of laminated composites.In order to suppress delamination,the material of interply film has to been selected carefully due to the fact that different matrials have different results .SOme materials may increase the stress values at the interfaces.Some materials may reduce the stress concertration.

  17. Ag-Coated Heterostructures of ZnO-TiO2/Delaminated Montmorillonite as Solar Photocatalysts

    Science.gov (United States)

    Hinojosa, Mariana; Tobajas, Montserrat; Alvarez, Maria Ariadna; Rodríguez-González, Vicente; Rodriguez, Juan Jose

    2017-01-01

    Heterostructures based on ZnO-TiO2/delaminated montmorillonite coated with Ag have been prepared by sol–gel and photoreduction procedures, varying the Ag and ZnO contents. They have been thoroughly characterized by XRD, WDXRF, UV–Vis, and XPS spectroscopies, and N2 adsorption, SEM, and TEM. In all cases, the montmorillonite was effectively delaminated with the formation of TiO2 anatase particles anchored on the clay layer’s surface, yielding porous materials with high surface areas. The structural and textural properties of the heterostructures synthesized were unaffected by the ZnO incorporated. The photoreduction led to solids with Ag nanoparticles decorating the surface. These materials were tested as photocatalysts for the degradation of several emerging contaminants with different nitrogen-bearing chemical structures under solar light. The catalysts yielded high rates of disappearance of the starting pollutants and showed quite stable performance upon successive applications. PMID:28817106

  18. Segmenting delaminations in carbon fiber reinforced polymer composite CT using convolutional neural networks

    Science.gov (United States)

    Sammons, Daniel; Winfree, William P.; Burke, Eric; Ji, Shuiwang

    2016-02-01

    Nondestructive evaluation (NDE) utilizes a variety of techniques to inspect various materials for defects without causing changes to the material. X-ray computed tomography (CT) produces large volumes of three dimensional image data. Using the task of identifying delaminations in carbon fiber reinforced polymer (CFRP) composite CT, this work shows that it is possible to automate the analysis of these large volumes of CT data using a machine learning model known as a convolutional neural network (CNN). Further, tests on simulated data sets show that with a robust set of experimental data, it may be possible to go beyond just identification and instead accurately characterize the size and shape of the delaminations with CNNs.

  19. The Use of Sprint Interface Element Delamination Simulation of Sandwich Composite Beam

    Science.gov (United States)

    Xu, Geng; Yan, Renjun

    2016-12-01

    Sandwich composite beams have been more and more used in various industries because of their excellent mechanical properties. However, the mismatched performance between face sheet and foam core always lead to such as cracks and damages in the core or face/core interface during the processes of manufacturing or service. Delamination damage at the adhesive interface is the most dangerous and could be one main source that the mechanical capability of the structure is serous degenerated. In this paper, a simple and natural model to evaluate the stiffness of the spring interface elements, which is based on the physics and the geometry of the adhesive layers, is proposed. In order to validate the model, cantilever beam bending test were conducted for marine sandwich composite I-beam. A good comparison has been found between predictions and experimental results, and results indicate that the spring interface element can provide an efficient model for the delamination simulation of sandwich composite structures.

  20. Analysis of vibration for regions above rectangular delamination defects in solids

    Science.gov (United States)

    Oh, Taekeun; Popovics, John S.; Sim, Sung-Han

    2013-04-01

    We propose a semi-analytical approach to predict the natural flexural vibration frequencies of the material overlying a near-surface delamination defect in a solid. The formulation accommodates arbitrary length to depth ratio of the defect and higher-order modes of vibration. The material above the defect is modeled as a semi-clamped rectangular plate, where the dynamic edge effect factors, as deduced by Bolotin's asymptotic method, are estimated. The formulation results are evaluated through comparison to 3-D finite element (FE) simulation and experimental results obtained from impact resonance tests on concrete samples with controlled delamination defects. Good agreement with both experimental and 3-D FE results confirms the accuracy of the formulation in all cases.

  1. Ag-Coated Heterostructures of ZnO-TiO2/Delaminated Montmorillonite as Solar Photocatalysts

    Directory of Open Access Journals (Sweden)

    Carolina Belver

    2017-08-01

    Full Text Available Heterostructures based on ZnO-TiO2/delaminated montmorillonite coated with Ag have been prepared by sol–gel and photoreduction procedures, varying the Ag and ZnO contents. They have been thoroughly characterized by XRD, WDXRF, UV–Vis, and XPS spectroscopies, and N2 adsorption, SEM, and TEM. In all cases, the montmorillonite was effectively delaminated with the formation of TiO2 anatase particles anchored on the clay layer’s surface, yielding porous materials with high surface areas. The structural and textural properties of the heterostructures synthesized were unaffected by the ZnO incorporated. The photoreduction led to solids with Ag nanoparticles decorating the surface. These materials were tested as photocatalysts for the degradation of several emerging contaminants with different nitrogen-bearing chemical structures under solar light. The catalysts yielded high rates of disappearance of the starting pollutants and showed quite stable performance upon successive applications.

  2. Direct observation of anodic dissolution and filament growth behavior in polyethylene-oxide-based atomic switch structures

    Science.gov (United States)

    Krishnan, Karthik; Tsuruoka, Tohru; Aono, Masakazu

    2016-06-01

    We directly observed anodic dissolution and subsequent filament growth behavior in a planar atomic switch structure with Ag salt incorporated polyethylene oxide (Ag-PEO) film using in situ optical microscopy and ex situ scanning electron microscopy. The high ionic conductivities of Ag-PEO films enable the investigation of filament formation under voltage bias, even in micrometer-scaled devices. It was found that the filament formation changes from unidirectional growth to dendritic growth, depending on its distance from the grounded electrode. Based on this understanding of filament growth dynamics in planar devices, highly stable resistive switching was achieved in an Ag/Ag-PEO/Pt stacked device with an Ag-PEO film thickness of 100 nm. The device showed repeated switching operations for more than 102 sweep cycles, with a high ON/OFF resistance ratio of 105.

  3. Delamination of sub-crustal lithosphere beneath the Isthmus of Tehuantepec, Mexico

    Science.gov (United States)

    Manea, Marina; Constantin Manea, Vlad; Ferrari, Luca; Orozco-Esquivel, Maria Teresa

    2015-04-01

    Recent seismic data from a dense seismic array (VEOX), as well as from the permanent broadband network of the Mexican National Seismological Service (SSN), revealed several anomalous structures in the Isthmus of Tehuantepec. Seismic tomography imaged a high velocity body dipping ~30° from the Gulf of Mexico southward. Analysis of seismic noise detected a large well-defined low-velocity anomaly on top of this structure in the vicinity of the Late Miocene-Quaternary Los Tuxtlas volcanic field. The current interpretation of these observations propose the presence of a southward dipping slab resulting from the subduction of oceanic lithosphere prior to the collision of the Yucatán Block with Mexico ~12 Ma ago. However this interpretation contradicts many aspects of well-established models of Caribbean tectonics. Additionally such model does not explain how the southward dipping structure remained at a relatively low dipping angle (~30°) over the last 12 Ma, and why it is not seismically active. We propose an alternative model that reconciles the seismic observations with the tectonic evolution of the region. The south dipping seismic structure is the result of lithospheric delamination produced by a thermal anomaly that migrated upwards through a slab gap in the Cocos slab located at ~200 km depth. Using high-resolution two-dimensional coupled petrological-thermomechanical numerical simulations of subduction, we show that hot and buoyant asthenospheric material flowing through a slab gap in the Cocos plate may have produced a rapid delamination of the lithosphere once it reached its base. The model geometry of the delaminated lithosphere is similar to the observed seismic anomaly, and the hot material from the plume impact is consistent with the low-velocity anomaly located at the north of the Isthmus of Tehuantepec, which feeds the Los Tuxtla volcanic field. Additionally our simulations show that the temperature of the delaminated lithosphere is above 700

  4. Lamb wave sensing using fiber Bragg grating sensors for delamination detection in composite laminates

    Science.gov (United States)

    Takeda, N.; Okabe, Y.; Kuwahara, J.; Kojima, S.

    2005-05-01

    The authors are constructing a damage detection system using ultrasonic waves. In this system, a piezo-ceramic actuator generates Lamb waves in a CFRP laminate. After the waves propagate in the laminate, transmitted waves are received by a fiber Bragg grating (FBG) sensor attached on the laminate using a newly developed high-speed optical wavelength interrogation system. At first, the optimal gauge length of the FBG to detect ultrasonic waves was investigated through theoretical simulations and experiments. Then, the directional sensitivity of the FBG to ultrasonic waves was evaluated experimentally. On the basis of the above results, the 1mm FBG sensors were applied to the detection of Lamb waves propagated in carbon fiber reinforced plastic (CFRP) cross-ply laminates. The piezo-actuator was put on the laminate about 50mm away from the FBG sensor glued on the laminate, and three-cycle sine waves of 300kHz were excited repeatedly. The waveforms obtained by the FBG showed that S0 and A0 modes could be detected appropriately. Then, artificial delamination was made in the laminate by removing of a Teflon sheet embedded in the 0/90 interface after the manufacturing. When the Lamb waves passed through the delamination, the amplitude decreased and a new wave mode appeared. These phenomena could be well simulated using a finite element method. Furthermore, since the amplitude and the velocity of the new mode increased with an increase in the delamination length, this system has a potential to evaluate the interlaminar delamination length quantitatively.

  5. Contribution to interplay between a delamination test and a sensory analysis of mid-range lipsticks.

    Science.gov (United States)

    Richard, C; Tillé-Salmon, B; Mofid, Y

    2016-02-01

    Lipstick is currently one of the most sold products of cosmetics industry, and the competition between the various manufacturers is significant. Customers mainly seek products with high spreadability, especially long-lasting or long wear on the lips. Evaluation tests of cosmetics are usually performed by sensory analysis. This can then represent a considerable cost. The object of this study was to develop a fast and simple test of delamination (objective method with calibrated instruments) and to interplay the obtained results with those of a discriminative sensory analysis (subjective method) in order to show the relevance of the instrumental test. Three mid-range lipsticks were randomly chosen and were tested. They were made of compositions as described by the International Nomenclature of Cosmetic Ingredients (INCI). Instrumental characterization was performed by texture profile analysis and by a special delamination test. The sensory analysis was voluntarily conducted with an untrained panel as blind test to confirm or reverse the possible interplay. The two approaches or methods gave the same type of classification. The high-fat lipstick had the worst behaviour with the delamination test and the worst notation of the intensity of descriptors with the sensory analysis. There is a high correlation between the sensory analysis and the instrumental measurements in this study. The delamination test carried out should permit to quickly determine the lasting (screening test) and in consequence optimize the basic formula of lipsticks. © 2015 Society of Cosmetic Scientists and the Société Française de Cosmétologie.

  6. Analytical Solution for the Free Vibration Analysis of Delaminated Timoshenko Beams

    OpenAIRE

    2014-01-01

    This work presents a method to find the exact solutions for the free vibration analysis of a delaminated beam based on the Timoshenko type with different boundary conditions. The solutions are obtained by the method of Lagrange multipliers in which the free vibration problem is posed as a constrained variational problem. The Legendre orthogonal polynomials are used as the beam eigenfunctions. Natural frequencies and mode shapes of various Timoshenko beams are presented to demonstrate the effi...

  7. Analytical solution for the free vibration analysis of delaminated Timoshenko beams.

    Science.gov (United States)

    Jafari-Talookolaei, Ramazan-Ali; Abedi, Maryam

    2014-01-01

    This work presents a method to find the exact solutions for the free vibration analysis of a delaminated beam based on the Timoshenko type with different boundary conditions. The solutions are obtained by the method of Lagrange multipliers in which the free vibration problem is posed as a constrained variational problem. The Legendre orthogonal polynomials are used as the beam eigenfunctions. Natural frequencies and mode shapes of various Timoshenko beams are presented to demonstrate the efficiency of the methodology.

  8. Comprehensively simulating the mixed-mode progressive delamination in composite laminates

    Science.gov (United States)

    Gao, Zhenyuan

    Delamination, or interlaminar debonding, is a commonly observed failure mechanism in composite laminates. It is of great significance to comprehensively simulate the mixed-mode progressive delamination in composite structures because by doing this, people can save a lot of effort in evaluating the safe load which a composite structure can endure. The objective of this thesis is to develop a numerical approach to simulating double-cantilever beam (DCB) and mixed-mode bending (MMB) tests and also of specifying/validating various cohesive models. A finite element framework, which consists of properly selecting time integration scheme (explicit dynamic), viscosity, load rate and mass scaling, is developed to yield converged and accurate results. Two illustrative cohesive laws (linear and power-law) are programmed with a user- defined material subroutine for ABAQUS/Explicit, VUMAT, and implemented into the finite element framework. Parameters defined in cohesive laws are studied to evaluate their effects on the predicted load-displacement curves. The finite element model, together with the predetermined model parameters, is found to be capable of producing converged and accurate results. The finite element framework, embedded with the illustrative cohesive laws, is found to be capable of handling various interfacial models. The present approach is concluded to be useful in simulating delamination with more sophisticated material models. Together with the method for determining model parameters, it can be used by computer codes other than ABAQUS.

  9. Transient Dynamic Response of Delaminated Composite Rotating Shallow Shells Subjected to Impact

    Directory of Open Access Journals (Sweden)

    Amit Karmakar

    2006-01-01

    Full Text Available In this paper a transient dynamic finite element analysis is presented to study the response of delaminated composite pretwisted rotating shallow shells subjected to low velocity normal impact. Lagrange's equation of motion is used to derive the dynamic equilibrium equation and moderate rotational speeds are considered wherein the Coriolis effect is negligible. An eight noded isoparametric plate bending element is employed in the finite element formulation incorporating rotary inertia and effects of transverse shear deformation based on Mindlin's theory. To satisfy the compatibility of deformation and equilibrium of resultant forces and moments at the delamination crack front a multipoint constraint algorithm is incorporated which leads to unsymmetric stiffness matrices. The modified Hertzian contact law which accounts for permanent indentation is utilized to compute the contact force, and the time dependent equations are solved by Newmark's time integration algorithm. Parametric studies are performed in respect of location of delamination, angle of twist and rotational speed for centrally impacted graphite-epoxy composite cylindrical shells.

  10. Comparison Study on the Effect of Interlayer Hydration and Solvation on Montmorillonite Delamination

    Science.gov (United States)

    Li, Hongliang; Song, Shaoxian; Zhao, Yunliang; Nahmad, Yuri; Chen, Tianxing

    2016-11-01

    The effect of water and isopropanol intercalation on montmorillonite (MMT) delamination was investigated in order to compare the roles of hydration and solvation in the delamination. Transmittance results showed that water has a significant effect on the delamination of MMT compared with isopropanol. This observation was attributed to the difference of the intercalation of water and isopropanol. Thermogravimetric (TG) results illustrate that the intercalation mass of water was greater than that of isopropanol when the pressure remained constant. Weighing test results show that the intercalation mass of water was smaller than that of isopropanol when the volume of MMT remained constant. Molecule dynamic simulation results show that the water and isopropanol molecules were interacting with Na+ and siloxane surface of MMT, respectively. It was demonstrated that the hydration of the MMT interlayer followed two steps: in step 1, the Na+ in the interlayer was hydrated, thereby expanding the interlayer spacing; in step 2, additional water molecules were absorbed into the expanded interlayer space. It was found that step 2 could not be actuated until the completion of step 1. For the solvation of the MMT interlayer with isopropanol, however, only one step was required, in which isopropanol was absorbed onto the siloxane sites of the interlayer while maintaining the interlayer spacing.

  11. Modeling Delamination in Postbuckled Composite Structures Under Static and Fatigue Loads

    Science.gov (United States)

    Bisagni, Chiara; Brambilla, Pietro; Bavila, Carlos G.

    2013-01-01

    The ability of the Abaqus progressive Virtual Crack Closure Technique (VCCT) to model delamination in composite structures was investigated for static, postbuckling, and fatigue loads. Preliminary evaluations were performed using simple Double Cantilever Beam (DCB) and Mixed-Mode Bending (MMB) specimens. The nodal release sequences that describe the propagation of the delamination front were investigated. The effect of using a sudden or a gradual nodal release was evaluated by considering meshes aligned with the crack front as well as misaligned meshes. Fatigue simulations were then performed using the Direct Cyclic Fatigue (DCF) algorithm. It was found that in specimens such as the DCB, which are characterized by a nearly linear response and a pure fracture mode, the algorithm correctly predicts the Paris Law rate of propagation. However, the Abaqus DCF algorithm does not consider different fatigue propagation laws in different fracture modes. Finally, skin/stiffener debonding was studied in an aircraft fuselage subcomponent in which debonding occurs deep into post-buckling deformation. VCCT was shown to be a robust tool for estimating the onset propagation. However, difficulties were found with the ability of the current implementation of the Abaqus progressive VCCT to predict delamination propagation within structures subjected to postbuckling deformations or fatigue loads.

  12. Failure Predictions of Out-of-Autoclave Sandwich Joints with Delaminations Under Flexure Loads

    Science.gov (United States)

    Nordendale, Nikolas A.; Goyal, Vinay K.; Lundgren, Eric C.; Patel, Dhruv N.; Farrokh, Babak; Jones, Justin; Fischetti, Grace; Segal, Kenneth N.

    2015-01-01

    An analysis and a test program was conducted to investigate the damage tolerance of composite sandwich joints. The joints contained a single circular delamination between the face-sheet and the doubler. The coupons were fabricated through out-of-autoclave (OOA) processes, a technology NASA is investigating for joining large composite sections. The four-point bend flexure test was used to induce compression loading into the side of the joint where the delamination was placed. The compression side was chosen since it tends to be one of the most critical loads in launch vehicles. Autoclave cure was used to manufacture the composite sandwich sections, while the doubler was co-bonded onto the sandwich face-sheet using an OOA process after sandwich panels were cured. A building block approach was adopted to characterize the mechanical properties of the joint material, including the fracture toughness between the doubler and face-sheet. Twelve four-point-bend samples were tested, six in the sandwich core ribbon orientation and six in sandwich core cross-ribbon direction. Analysis predicted failure initiation and propagation at the pre-delaminated location, consistent with experimental observations. A building block approach using fracture analyses methods predicted failure loads in close agreement with tests. This investigation demonstrated a small strength reduction due to a flaw of significant size compared to the width of the sample. Therefore, concerns of bonding an OOA material to an in-autoclave material was mitigated for the geometries, materials, and load configurations considered.

  13. Detecting Thermal Barrier Coating Delamination Using Visible and Near-Infrared Luminescence from Erbium-Doped Sublayers

    Science.gov (United States)

    Eldridge, J. I.; Bencic, T. J.; Martin, R. E.; Singh, J.; Wolfe, D. E.

    2007-01-01

    Nondestructive diagnostic tools are needed to monitor early stages of delamination progression in thermal barrier coatings (TBCs) because the risk of delamination induced coating failure will compromise engine performance and safety. Previous work has demonstrated that for TBCs composed of yttria-stabilized zirconia (YSZ), luminescence from a buried europium-doped sublayer can be utilized to identify the location of TBC delamination from the substantially higher luminescence intensity observed from the delaminated regions of the TBC. Luminescence measurements from buried europium-doped layers depend on sufficient transmittance of the 532 nm excitation and 606 nm emission wavelengths through the attenuating undoped YSZ overlayer to produce easily detected luminescence. In the present work, improved delamination indication is demonstrated using erbium-doped YSZ sublayers. For visible-wavelength luminescence, the erbium-doped sublayer offers the advantage of a very strong excitation peak at 517 nm that can be conveniently excited a 514 nm Ar ion laser. More importantly, the erbium-doped sublayer also produces near-infrared luminescence at 1550 nm that is effectively excited by a 980 nm laser diode. Both the 980 nm excitation and the 1550 nm emission are transmitted through the TBC with much less attenuation than visible wavelengths and therefore show great promise for delamination monitoring through thicker or more highly scattering TBCs. The application of this approach for both electron beam physical vapor deposited (EB-PVD) and plasma-sprayed TBCs is discussed.

  14. Incipient mantle delamination, active tectonics and crustal thickening in Northern Morocco: Insights from gravity data and numerical modeling

    Science.gov (United States)

    Baratin, Laura-May; Mazzotti, Stéphane; Chéry, Jean; Vernant, Philippe; Tahayt, Abdelilah; Mourabit, Taoufik

    2016-11-01

    The Betic-Rif orocline surrounding the Alboran Sea, the westernmost tip of the Mediterranean Sea, accommodates the NW-SE convergence between the Nubia and Eurasia plates. Recent GPS observations indicate a ∼4 mm/yr SW motion of the Rif Mountains, relative to stable Nubia, incompatible with a simple two-plate model. New gravity data acquired in this study define a pronounced negative Bouguer anomaly south of the Rif, interpreted as a ∼40 km-thick crust in a state of non-isostatic equilibrium. We study the correlation between these present-day kinematic and geodynamic processes using a finite-element code to model in 2-D the first-order behavior of a lithosphere affected by a downward normal traction (representing the pull of a high-density body in the upper mantle). We show that intermediate viscosities for the lower crust and uppermost mantle (1021-1022Pas) allow an efficient coupling between the mantle and the base of the brittle crust, thus enabling (1) the conversion of vertical movement, resulting from the downward traction, to horizontal movement and (2) shortening in the brittle upper crust. Our results show that incipient delamination of the Nubian continental lithosphere, linked to slab pull, can explain the present-day abnormal tectonics, contribute to the gravity anomaly observed in northern Morocco, and give insight into recent tectonics in the Western Mediterranean region.

  15. Contact behavior evolution induced by damage growth in radio-frequency microelectromechanical system switches

    Science.gov (United States)

    Wu, Y.; Peroulis, D.

    2015-02-01

    This study provides a two-contact-event model to explain the evolution of the contact behavior of microelectromechanical system (MEMS) switches through their lifetime. The succession of two dynamic contact events is carefully considered during actuation inspired by experimental observations. The contact between the MEMS switch tip and the drain can be treated as an effective contact between an elastic hemisphere and a rigid plane. If the first contact event results in elastic deformation, the effective hemisphere will fully recover. Consequently, the subsequent contact event also produces elastic deformation. If, on the other hand, the first contact event induces elastoplastic or plastic deformation, a residual depth will be produced between the hemisphere and the rigid plane. The contact force of the subsequent contact event can be significantly reduced due to this additional residual depth. With the growth of residual depth during the switch cycling process, the modeling results show three possible situations of contact radius evolution: (1) The contact radius increases to a maximum value and then decreases to zero; (2) the contact radius increases to one local maximum value; then decreases to a local minimum value; subsequently increases again to another maximum value, and finally decreases to zero; and (3) the contact radius increases to one maximum value and then decreases to zero; after an intermittent response, the contact radius increases again to another maximum value and finally decreases to zero. Furthermore, the Maxwell spreading formula is applied to determine the contact resistance which is inversely proportional to the contact radius. Three situations of contact resistance evolution corresponding to the evolution of contact radius are obtained. All three situations are also observed and validated by the experimental results.

  16. Growth status related to brain responses, nutrition, home environment, and behavior in infants and toddlers

    Science.gov (United States)

    To investigate whether growth status in infants and toddlers affects processes involved in speech perception and discrimination, cortical event-related potentials (ERPs) to consonant-vowel syllables were recorded from 48 healthy babies: 26 low in growth status (LGS, <25th percentile in growth measur...

  17. Comparing Growth Trajectories of Risk Behaviors from Late Adolescence through Young Adulthood: An Accelerated Design

    Science.gov (United States)

    Brodbeck, Jeannette; Bachmann, Monica S.; Croudace, Tim J.; Brown, Anna

    2013-01-01

    Risk behaviors such as substance use or deviance are often limited to the early stages of the life course. Whereas the onset of risk behavior is well studied, less is currently known about the decline and timing of cessation of risk behaviors of different domains during young adulthood. Prevalence and longitudinal developmental patterning of…

  18. Comparing Growth Trajectories of Risk Behaviors from Late Adolescence through Young Adulthood: An Accelerated Design

    Science.gov (United States)

    Brodbeck, Jeannette; Bachmann, Monica S.; Croudace, Tim J.; Brown, Anna

    2013-01-01

    Risk behaviors such as substance use or deviance are often limited to the early stages of the life course. Whereas the onset of risk behavior is well studied, less is currently known about the decline and timing of cessation of risk behaviors of different domains during young adulthood. Prevalence and longitudinal developmental patterning of…

  19. Effect of maternal activity during gestation on maternal behavior, fetal growth, umbilical blood flow, and farrowing characteristics in pigs.

    Science.gov (United States)

    Harris, E K; Berg, E P; Berg, E L; Vonnahme, K A

    2013-02-01

    Yorkshire gilts either remained in their individual stall from d 40 to term (CON; n = 7) or were subjected to exercise for 30 min 3 times per week from mid to late gestation (EX; n = 7) to determine the impact of increased maternal activity during gestation on maternal behavior, fetal growth, umbilical blood flow, and parturition. In parity 1, maternal body composition (10th rib back fat and LM area), maternal behavior, and farrowing characteristics were recorded. In parities 1 and 2, fetal growth, fetal heart rate, pulsatility index and resistance index, and umbilical blood flow were monitored beginning at d 39 of gestation continuing to d 81 of gestation. Exercise continued until d 104. Gilts allowed to exercise sat less (P gestation in the pig increased umbilical blood flow and appeared to reduce maternal restlessness, impacts on offspring development in postnatal life are not known.

  20. First-order Description of the Mechanical Fracture Behavior of Fine-Grained Surficial Marine Sediments During Gas Bubble Growth

    Science.gov (United States)

    2010-01-01

    10 F04O29 BARRY ET AL.: BUBBLE GROWTH BY FRACTURE P04029 Figure 3. Map of field site. Canard, Nova Scotia, Canada. appears to approximate the...Bottinger. and T. Dahm (2005), Buoyancy-driven fracture ascent: Experiments in layered gelatine. J. Volcano!. Geotherm . Res., 144. 273-285. doi...Journal Article 3. DATES COVERED (From - To) 4. TITLE AND SUBTITLE First-order description of the mechanical fracture behavior of fine-grained

  1. Pacific lamprey (Entosphenus tridentatus) ammocoetes exposed to contaminated Portland Harbor sediments: Method development and effects on survival, growth, and behavior

    Science.gov (United States)

    Unrein, Julia R.; Morris, Jeffrey M.; Chitwood, Rob S.; Lipton, Joshua; Peers, Jennifer; van de Wetering, Stan; Schreck, Carl B.

    2016-01-01

    Many anthropogenic disturbances have contributed to the decline of Pacific lampreys (Entosphenus tridentatus), but potential negative effects of contaminants on lampreys are unclear. Lamprey ammocoetes are the only detritivorous fish in the lower Willamette River, Oregon, USA, and have been observed in Portland Harbor sediments. Their long benthic larval stage places them at risk from the effects of contaminated sediment. The authors developed experimental methods to assess the effects of contaminated sediment on the growth and behavior of field-collected ammocoetes reared in a laboratory. Specifically, they developed methods to assess individual growth and burrowing behavior. Burrowing performance demonstrated high variability among contaminated sediments; however, ammocoetes presented with noncontaminated reference sediment initiated burrowing more rapidly and completed it faster. Ammocoete reemergence from contaminated sediments suggests avoidance of some chemical compounds. The authors conducted long-term exposure experiments on individually held ammocoetes using sediment collected from their native Siletz River, which included the following: contaminated sediments collected from 9 sites within Portland Harbor, 2 uncontaminated reference sediments collected upstream, 1 uncontaminated sediment with characteristics similar to Portland Harbor sediments, and clean sand. They determined that a 24-h depuration period was sufficient to evaluate weight changes and observed no mortality or growth effects in fish exposed to any of the contaminated sediments. However, the effect on burrowing behavior appeared to be a sensitive endpoint, with potentially significant implications for predator avoidance.

  2. Pacific lamprey (Entosphenus tridentatus) ammocoetes exposed to contaminated Portland Harbor sediments: Method development and effects on survival, growth, and behavior.

    Science.gov (United States)

    Unrein, Julia R; Morris, Jeffrey M; Chitwood, Rob S; Lipton, Joshua; Peers, Jennifer; van de Wetering, Stan; Schreck, Carl B

    2016-08-01

    Many anthropogenic disturbances have contributed to the decline of Pacific lampreys (Entosphenus tridentatus), but potential negative effects of contaminants on lampreys are unclear. Lamprey ammocoetes are the only detritivorous fish in the lower Willamette River, Oregon, USA, and have been observed in Portland Harbor sediments. Their long benthic larval stage places them at risk from the effects of contaminated sediment. The authors developed experimental methods to assess the effects of contaminated sediment on the growth and behavior of field-collected ammocoetes reared in a laboratory. Specifically, they developed methods to assess individual growth and burrowing behavior. Burrowing performance demonstrated high variability among contaminated sediments; however, ammocoetes presented with noncontaminated reference sediment initiated burrowing more rapidly and completed it faster. Ammocoete reemergence from contaminated sediments suggests avoidance of some chemical compounds. The authors conducted long-term exposure experiments on individually held ammocoetes using sediment collected from their native Siletz River, which included the following: contaminated sediments collected from 9 sites within Portland Harbor, 2 uncontaminated reference sediments collected upstream, 1 uncontaminated sediment with characteristics similar to Portland Harbor sediments, and clean sand. They determined that a 24-h depuration period was sufficient to evaluate weight changes and observed no mortality or growth effects in fish exposed to any of the contaminated sediments. However, the effect on burrowing behavior appeared to be a sensitive endpoint, with potentially significant implications for predator avoidance. Environ Toxicol Chem 2016;35:2092-2102. © 2016 SETAC.

  3. Ramet population ecology of Panicum virgatum in the field - Competitively random growth of ramets and foraging behavior of ramet populations

    Institute of Scientific and Technical Information of China (English)

    Xinguo Yang; Tianlong Wu; Xu Cheng

    2008-01-01

    The authors investigated the heterogeneous size patterns and dynamic growth of the ramet population of Panicum virgatum, a clonal caespitose plant, limited to the space occupied by a ramet bunch and the time of the ramet yearly life cycle, to understand the ecology of clonal caespitose plants in the field, where the ramet bunch generally consisted of more than one genet. Dynamic life tables for ramet populations were established by the replacement of living ramets at the present time with "dead" ones in past time. These tables revealed stable coexisting patterns of isometric and allometric growing processes of ramets in mass and height respectively, which approximately followed the historic trajectory of a density-independent population. The ecology of clonal caespitose plants is further discussed based on the competitively random growth of ramet individuals, including the scale of foraging behavior. In the field, the ramet population ecol-ogy of switchgrass may be a statistical result of competitively random growth of ramet individuals. The foraging behavior of a ramet population could then be presented as a process in which ramet individuals competed with each other for light and grew randomly, whileat the same time a relatively stable dynamic growth pattern was apparent at the level of the ramet population, and the functional leaves were placed properly in time and space.

  4. Subcritical Crack-Growth and Lifetime Behavior of Glass and SiC under Static Load

    Institute of Scientific and Technical Information of China (English)

    2001-01-01

    Crack initiation and subcritical crack growth in glass sheet and SiC bar specimen under static loading were investigated to study the failure process. It has been demonstrated that the lifetime process of brittle materials involves three possible forms of crack growth: subcritical crack growth,partly subcritical crack growth and instantaneous fracture without subcritical crack growth.Curves of v-K obtained in step-by-step static fatigue tests and in constant loading rate tests showed different trends for borosilicate glass sheet. α-SiC that is generally considered immune to mechanical fatigue effect and environmental attack was also tested under static loading and the lifetime was measured. The results showed that the threshold load to damage effect was over 80% of the initial strength for the SiC.

  5. The Consumer Behavior Challenge: Designing an Assignment to Motivate Student Reflection and Self-Growth

    Science.gov (United States)

    Gravois, Renée; Lopez, Tará Burnthorne; Budden, Michael C.

    2017-01-01

    The tension caused by change pushes students to reflect on their new situation, examine preconceived ideas, and synthesize new with existing knowledge. In the Consumer Behavior Challenge, students are challenged to step outside of their comfort zone by changing a behavior or trying something new for a period of time. Through guided reflection…

  6. Behaviorism

    National Research Council Canada - National Science Library

    Moore, J

    2011-01-01

    .... Watson proposed an alternative: classical S-R behaviorism. According to Watson, behavior was a subject matter in its own right, to be studied by the observational methods common to all sciences...

  7. Individual growth and reproductive behavior in a newly established population of northern snakehead (Channa argus), Potomac River, USA

    Science.gov (United States)

    Landis, Andrew M. Gascho; Lapointe, Nicolas W. R.; Angermeier, Paul L.

    2010-01-01

    Northern snakehead (Channa argus) were first found in the Potomac River in 2004. In 2007, we documented feeding and reproductive behavior to better understand how this species is performing in this novel environment. From April to October, we used electrofishing surveys to collect data on growth, condition, and gonad weight of adult fish. Growth rates of young were measured on a daily basis for several weeks. Mean length-at-age for Potomac River northern snakehead was lower than for fish from China, Russia, and Uzbekistan. Fish condition was above average during spring and fall, but below average in summer. Below-average condition corresponded to periods of high spawning activity. Gonadosomatic index indicated that females began spawning at the end of April and continued through August. Peak spawning occurred at the beginning of June when average temperatures reached 26°C. Larval fish growth rate, after the transition to exogenous feeding, was 2.3 (SD ± 0.7) mm (total length, TL) per day. Although Potomac River northern snakehead exhibited lower overall growth rates when compared to other populations, these fish demonstrated plasticity in timing of reproduction and rapid larval growth rates. Such life history characteristics likely contribute to the success of northern snakehead in its new environment and limit managers’ options for significant control of its invasion.

  8. Effect of graphene oxide ratio on the cell adhesion and growth behavior on a graphene oxide-coated silicon substrate

    Science.gov (United States)

    Jeong, Jin-Tak; Choi, Mun-Ki; Sim, Yumin; Lim, Jung-Taek; Kim, Gil-Sung; Seong, Maeng-Je; Hyung, Jung-Hwan; Kim, Keun Soo; Umar, Ahmad; Lee, Sang-Kwon

    2016-09-01

    Control of living cells on biocompatible materials or on modified substrates is important for the development of bio-applications, including biosensors and implant biomaterials. The topography and hydrophobicity of substrates highly affect cell adhesion, growth, and cell growth kinetics, which is of great importance in bio-applications. Herein, we investigate the adhesion, growth, and morphology of cultured breast cancer cells on a silicon substrate, on which graphene oxides (GO) was partially formed. By minimizing the size and amount of the GO-containing solution and the further annealing process, GO-coated Si samples were prepared which partially covered the Si substrates. The coverage of GO on Si samples decreases upon annealing. The behaviors of cells cultured on two samples have been observed, i.e. partially GO-coated Si (P-GO) and annealed partially GO-coated Si (Annealed p-GO), with a different coverage of GO. Indeed, the spreading area covered by the cells and the number of cells for a given culture period in the incubator were highly dependent on the hydrophobicity and the presence of oxygenated groups on GO and Si substrates, suggesting hydrophobicity-driven cell growth. Thus, the presented method can be used to control the cell growth via an appropriate surface modification.

  9. Slab detachment during continental collision: Influence of crustal rheology and interaction with lithospheric delamination

    Science.gov (United States)

    Duretz, T.; Gerya, T. V.

    2013-08-01

    Collision between continents can lead to the subduction of continental material. If the crust remains coupled to the downgoing slab, a large buoyancy force is generated. This force slows down convergence and promotes slab detachment. If the crust resists to subduction, it may decouple from the downgoing slab and be subjected to buoyant extrusion. We employ two-dimensional thermo-mechanical modelling to study the importance of crustal rheology on the evolution of subduction-collision systems. We propose simple quantifications of the mechanical decoupling between lithospheric levels (σ*) and the potential for buoyant extrusion of the crust (ξ*). The modelling results indicate that a variable crustal rheological structure results in slab detachment, delamination, or the combination of both mechanisms. A strong crust provides coupling at the Moho (low σ*) and remains coherent during subduction (low ξ). It promotes deep subduction of the crust (180 km) and slab detachment. Exhumation occurs in coherent manners via eduction and thrusting. Slab detachment triggers the development of topography (> 4.5 km) close to the suture. A contrasting style of collision occurs using a weak crustal rheology. Mechanical decoupling at the Moho (high σ*) promotes the extrusion of the crust (high ξ), disabling slab detachment. Ongoing shortening leads to buckling of the crust and development of topography on the lower plate. Collisions involving rheologically layered crust allow decoupling at mid-crustal depths. This structure favours both the extrusion of upper crust and the subduction of the lower crust. Such collisions are successively affected by delamination and slab detachment. Topography develops together with the buoyant extrusion of crust onto the foreland and is further amplified by slab detachment. Our results suggest that the occurrence of both delamination (Apennines) and slab detachment (Himalayas) in orogens may indicate differences in the initial crustal structure of

  10. Dense Root Removal by Asymmetric Delamination in Sierra Nevada, California: Insights from Numerical Modeling

    Science.gov (United States)

    Valera, J.; Negredo, A. M.; Billen, M.

    2008-12-01

    Recent studies provide compelling evidence for an event of removal of lithospheric mantle in southern -and possibly central- Sierra Nevada (SN) mountains, California (Zandt et al., Nature, 431, 2004). A sequential history of foundering of the ultramafic root of the Sierra Nevada batholith, with a pronounced asymmetric flow, is proposed to explain a number of geophysical and geological observations, including a fast seismic velocity in the mantle located to the west of the SN crest, a gap in the Moho, recent subsidence and tilting of the Sierra Nevada, and a change in mineralogy of the xenolith population recorded at the surface. In the present study we focus on the quantitative evaluation of this conceptual model. We apply new thermo- mechanical algorithms, developed in MATLAB code, suitable to study the temporal evolution of laterally migrating lithospheric delamination. The motion equation, formulated in terms of the stream function, and the coupled thermal equation are solved applying finite difference techniques. Our physical modeling is shown to properly reproduce the first order features of the conceptual model for lithospheric delamination in the Sierra Nevada. We investigate the evolution of a dense ultramafic root, which brings about a Rayleigh-Taylor gravitational instability. Following our preliminary results, the presence of a fluid-weakened lithosphere, located just east of Sierra Nevada, is required to reproduce the asymmetric development of this instability, as previously proposed by Zandt et al. (2004). This weak rheology zone, which is modeled by means of a reduced viscosity, is shown to enable the ascent of asthenospheric material and westward propagation of delamination. Our predictions are also consistent with the previous inference of the V-shaped cone of crust being dragged down into the downwelling mantle (i.e., the Moho gap). Present results highlight that viscous drag is also likely responsible for present-day surface subsidence.

  11. Modeling the Effects of Beam Size and Flaw Morphology on Ultrasonic Pulse/Echo Sizing of Delaminations in Carbon Composites

    Science.gov (United States)

    Margetan, Frank J.; Leckey, Cara A.; Barnard, Dan

    2012-01-01

    The size and shape of a delamination in a multi-layered structure can be estimated in various ways from an ultrasonic pulse/echo image. For example the -6dB contours of measured response provide one simple estimate of the boundary. More sophisticated approaches can be imagined where one adjusts the proposed boundary to bring measured and predicted UT images into optimal agreement. Such approaches require suitable models of the inspection process. In this paper we explore issues pertaining to model-based size estimation for delaminations in carbon fiber reinforced laminates. In particular we consider the influence on sizing when the delamination is non-planar or partially transmitting in certain regions. Two models for predicting broadband sonic time-domain responses are considered: (1) a fast "simple" model using paraxial beam expansions and Kirchhoff and phase-screen approximations; and (2) the more exact (but computationally intensive) 3D elastodynamic finite integration technique (EFIT). Model-to-model and model-to experiment comparisons are made for delaminations in uniaxial composite plates, and the simple model is then used to critique the -6dB rule for delamination sizing.

  12. Multi-site delamination detection and quantification in composites through guided wave based global-local sensing

    Science.gov (United States)

    Tian, Zhenhua; Leckey, Cara; Yu, Lingyu

    2017-02-01

    This paper presents a guided wave based global-local sensing method for rapid detection and quantification of multi-site delamination damage in large composite panels. The global-local approach uses a hybrid system consisting of a piezoelectric transducer (PZT) for generating guided waves and a non-contact scanning laser Doppler vibrometer (SLDV) for acquiring guided wave data. The global-local method is performed in two steps. First, a phased array configured of a small number of SLDV scan points (for example 10×10 points in a rectangular grid array) performs inspection over the entire plate to detect and locate damage. Local areas are identified as potential damage regions for the second step. Then high density wavefield measurements are taken over the identified areas and wavefield analysis is performed to quantitatively evaluate the damage. For the proof of concept in case with multi-site damage, the global-local approach is demonstrated on a carbon fiber reinforced polymer (CFRP) composite plate with two sites of impact-induced delamination damage. In the first step, the locations of two delamination sites are detected by the phased array method. In the second step, the delamination size and shape are evaluated using wavefield analysis. The detected delamination location, size and shape agree well with those of ultrasonic C-scan and the method led to a 93% reduction in inspection time compared to a full SLDV dense grid scan.

  13. Creep Crack Growth Behavior of Alloys 617 and 800H in Air and Impure Helium Environments at High Temperatures

    Science.gov (United States)

    Grierson, D. S.; Cao, G.; Brooks, P.; Pezzi, P.; Glaudell, A.; Kuettel, D.; Fischer, G.; Allen, T.; Sridharan, K.; Crone, W. C.

    2016-11-01

    The environmental degradation of intermediate heat exchanger (IHX) materials in impure helium has been identified as an area with major ramifications on the design of very high-temperature reactors (VHTR). It has been reported that in some helium environments, non-ductile failure is a significant failure mode for Alloy 617 with long-term elevated-temperature service. Non-ductile failure of intermediate exchangers can result in catastrophic consequences; unfortunately, the knowledge of creep crack initiation and creep crack growth (CCG) in candidate alloys is limited. Current codes and code cases for the candidate alloys do not provide specific guidelines for effects of impure helium on the high-temperature behavior. The work reported here explores creep crack growth characterization of Alloy 617 and Alloy 800H at elevated temperatures in air and in impure helium environments, providing information on the reliability of these alloys in VHTR for long-term service. Alloy 617 was found to exhibit superior CCG resistance compared to Alloy 800H. For Alloy 617 tested at 973 K (700 °C), a notable increase in the resistance to crack growth was measured in air compared to that measured in the helium environment; CCG results for Alloy 800H suggest that air and helium environments produce similar behavior. Testing of grain boundary-engineered (GBE) Alloy 617 samples revealed that, although the technique produces superior mechanical properties in many respects, the GBE samples exhibited inferior resistance to creep crack growth compared to the other Alloy 617 samples tested under similar conditions. Grain size is noted as a confounding factor in creep crack growth resistance.

  14. Creep Crack Growth Behavior of Alloys 617 and 800H in Air and Impure Helium Environments at High Temperatures

    Science.gov (United States)

    Grierson, D. S.; Cao, G.; Brooks, P.; Pezzi, P.; Glaudell, A.; Kuettel, D.; Fischer, G.; Allen, T.; Sridharan, K.; Crone, W. C.

    2017-03-01

    The environmental degradation of intermediate heat exchanger (IHX) materials in impure helium has been identified as an area with major ramifications on the design of very high-temperature reactors (VHTR). It has been reported that in some helium environments, non-ductile failure is a significant failure mode for Alloy 617 with long-term elevated-temperature service. Non-ductile failure of intermediate exchangers can result in catastrophic consequences; unfortunately, the knowledge of creep crack initiation and creep crack growth (CCG) in candidate alloys is limited. Current codes and code cases for the candidate alloys do not provide specific guidelines for effects of impure helium on the high-temperature behavior. The work reported here explores creep crack growth characterization of Alloy 617 and Alloy 800H at elevated temperatures in air and in impure helium environments, providing information on the reliability of these alloys in VHTR for long-term service. Alloy 617 was found to exhibit superior CCG resistance compared to Alloy 800H. For Alloy 617 tested at 973 K (700 °C), a notable increase in the resistance to crack growth was measured in air compared to that measured in the helium environment; CCG results for Alloy 800H suggest that air and helium environments produce similar behavior. Testing of grain boundary-engineered (GBE) Alloy 617 samples revealed that, although the technique produces superior mechanical properties in many respects, the GBE samples exhibited inferior resistance to creep crack growth compared to the other Alloy 617 samples tested under similar conditions. Grain size is noted as a confounding factor in creep crack growth resistance.

  15. Accelerated Near-Threshold Fatigue Crack Growth Behavior of an Aluminum Powder Metallurgy Alloy

    Science.gov (United States)

    Piascik, Robert S.; Newman, John A.

    2002-01-01

    Fatigue crack growth (FCG) research conducted in the near threshold regime has identified a room temperature creep crack growth damage mechanism for a fine grain powder metallurgy (PM) aluminum alloy (8009). At very low DK, an abrupt acceleration in room temperature FCG rate occurs at high stress ratio (R = Kmin/Kmax). The near threshold accelerated FCG rates are exacerbated by increased levels of Kmax (Kmax less than 0.4 KIC). Detailed fractographic analysis correlates accelerated FCG with the formation of crack-tip process zone micro-void damage. Experimental results show that the near threshold and Kmax influenced accelerated crack growth is time and temperature dependent.

  16. Study on the delamination of tungsten thin films on Sb2Te3

    Institute of Scientific and Technical Information of China (English)

    Xu Jia-Qing; Liu Bo; Song Zhi-Tang; Feng Song-Lin; Chen Bomy

    2006-01-01

    To investigate the reliability of electrode materials for chalcogenide random access memory (C-RAM) applications, the geometry and time evolution of the worm-like delamination patterns on a tungsten/Sb2 Te3 bilayer system surface are observed by field emission scanning electronic microscope (FESEM) and optical microscopy. The tungsten film stress and interface toughness are estimated using a straight-side model. After confirming the instability of this system being due to large compressive stress stored in the tungsten film and relative poor interface adhesion, a preliminary solution as the inset of a TiN adhesion layer is presented to improve the system performances.

  17. Fatigue Property of Nano-grained Delaminated Low-carbon Steel Sheet

    Institute of Scientific and Technical Information of China (English)

    X. Li; T.F. Jing; M.M. Lu; R. Xu; B.Y. Liang; J.W. Zhang

    2011-01-01

    Tension-tension fatigue life tests on nano-grained delaminated Iow-carbon steel sheet under different fatigue loads are carried out to study the fatigue properties of the steel. The three-dimensional microstructures of the steel are observed by TEM. In addition, the morphology of the fatigue fracture of the specimen under different loads is observed by SEM. The results show that micro-cracks form on the weak interface of the nano-grained steel under Iow-stress conditions, which hinders the propagation of the main cracks and reduces the fatigue crack propagation rate, resulting in the extending fatigue life of the steel.

  18. Moisture-Induced Delamination Video of an Oxidized Thermal Barrier Coating

    Science.gov (United States)

    Smialek, James L.; Zhu, Dongming; Cuy, Michael D.

    2008-01-01

    PVD TBC coatings were thermally cycled to near-failure at 1150 C. Normal failure occurred after 200 to 300 1-hr cycles with only moderate weight gains (0.5 mg/sq cm). Delamination and buckling was often delayed until well after cooldown (desktop spallation), but could be instantly induced by the application of water drops, as shown in a video clip which can be viewed by clicking on figure 2 of this report. Moisture therefore plays a primary role in delayed desktop TBC failure. Hydrogen embrittlement is proposed as the underlying mechanism.

  19. Highly Effective Delamination of Kaolinite and Emergence of a Novel Nanoclub-like Crystal

    Institute of Scientific and Technical Information of China (English)

    YAN Linlin; ZHANG Cunman; XU Zheng

    2008-01-01

    The delamination of kaolinite was performed via the combination of intercalation and sonication.The morphology including shape,size,and crystal structure before and after the treatment were investigated by using XRD,SEM,TEM and SED(selective electron diffraction).The results not only show that the particle size is significantly reduced after short time sonication treatment,such as BET area up to 52.29m2/g after only 1 h sonication treatment,but also indicate that the treated particles keep good crystal structure.A new aluminum silicate nanoclub-like crystal formed after sonication treatment.

  20. Insulin-like growth factor system regulates oligodendroglial cell behavior : Therapeutic potential in CNS

    NARCIS (Netherlands)

    Chesik, Daniel; De Keyser, Jacques; Wilczak, Nadine

    2008-01-01

    Amongst the many soluble extracellular factors stimulating intracellular signal transduction pathways and driving cellular processes such as proliferation, differentiation and survival, insulin-like growth factors (IGFs) stand out as indispensable factors for proper oligodendrocyte differentiation a

  1. Incubation behavior of silicon nanowire growth investigated by laser-assisted rapid heating

    Science.gov (United States)

    Ryu, Sang-gil; Kim, Eunpa; Allen, Frances I.; Hwang, David J.; Minor, Andrew M.; Grigoropoulos, Costas P.

    2016-08-01

    We investigate the early stage of silicon nanowire growth by the vapor-liquid-solid mechanism using laser-localized heating combined with ex-situ chemical mapping analysis by energy-filtered transmission electron microscopy. By achieving fast heating and cooling times, we can precisely determine the nucleation times for nanowire growth. We find that the silicon nanowire nucleation process occurs on a time scale of ˜10 ms, i.e., orders of magnitude faster than the times reported in investigations using furnace processes. The rate-limiting step for silicon nanowire growth at temperatures in the vicinity of the eutectic temperature is found to be the gas reaction and/or the silicon crystal growth process, whereas at higher temperatures it is the rate of silicon diffusion through the molten catalyst that dictates the nucleation kinetics.

  2. Incubation behavior of silicon nanowire growth investigated by laser-assisted rapid heating

    Energy Technology Data Exchange (ETDEWEB)

    Ryu, Sang-gil; Kim, Eunpa; Grigoropoulos, Costas P., E-mail: cgrigoro@berkeley.edu [Department of Mechanical Engineering, University of California, Berkeley, California 94720-1740 (United States); Allen, Frances I.; Minor, Andrew M. [Department of Materials Science and Engineering, University of California, Berkeley, California 94720-1740 (United States); National Center for Electron Microscopy, Molecular Foundry, Lawrence Berkeley National Laboratory, Berkeley, California 94720 (United States); Hwang, David J. [Department of Mechanical Engineering, Stony Brook University, Stony Brook, New York 11794 (United States)

    2016-08-15

    We investigate the early stage of silicon nanowire growth by the vapor-liquid-solid mechanism using laser-localized heating combined with ex-situ chemical mapping analysis by energy-filtered transmission electron microscopy. By achieving fast heating and cooling times, we can precisely determine the nucleation times for nanowire growth. We find that the silicon nanowire nucleation process occurs on a time scale of ∼10 ms, i.e., orders of magnitude faster than the times reported in investigations using furnace processes. The rate-limiting step for silicon nanowire growth at temperatures in the vicinity of the eutectic temperature is found to be the gas reaction and/or the silicon crystal growth process, whereas at higher temperatures it is the rate of silicon diffusion through the molten catalyst that dictates the nucleation kinetics.

  3. Spore production of Penicillium roqueforti by solid state fermentation: Stoichiometry, growth and sporulation behavior.

    Science.gov (United States)

    Desfarges, C; Larroche, C; Gros, J B

    1987-06-01

    The development of Penicillium roqueforti on buckwheat seeds proceeds roughly into four steps, involving a lag phase and three growth phases. First, it appears as a spore germination and external colonization of the grains by the mycelium. Then, mainly external sporulation and internal colonization of the seeds occur and finally internal sporulation takes place. The Stoichiometry of the growth and the sporulation is established. Kinetic experiments performed in a fixed bed reactor show that the growth of the microorganism (biomass production) may be estimated by the protein content of the medium. This growth occurs with a very low mu(max) value close to 0.030 h(-1). The chitin content of the medium is an indicator of the sporulation, just as the metabolic liquor (mainly water) produced during the course of a cultivation. The values of the observed respiratory quotient are close to those predicted by stoichiometry.

  4. Polymorphism of growth hormone gene and its association with seminal and sexual behavioral traits in crossbred cattle.

    Science.gov (United States)

    Pal, Aruna; Chakravarty, Atish Kumar; Chatterjee, Paresh Nath

    2014-02-01

    The decline in the male reproductive ability in terms of sexual behavior and seminal traits might lead to nonavailability of required number of bulls in a progeny testing program. The present study was conducted in 493 crossbred cattle (Bos taurus × Bos indicus) bulls to study polymorphisms of growth hormone (GH) gene and its association with seminal and sexual behavioral characteristics. A 428-base pair fragment of GH gene spanning over the fourth exon, fourth intron, and fifth exon was amplified and digested with AluI restriction enzyme. Bulls were found to be polymorphic, with two variants, LL and LV, and higher genotypic frequency for LL being 0.88. Twelve nucleotide changes and a single nonsynonymous substitution of Leucine by Valine were observed from GH1 (L) to GH2 (V). Statistical analysis revealed that the genotype of the GH gene had a significant effect on libido score, reaction time, Flehmen response, requirement of mounting stimulus, sperm mass activity, number of semen doses per collection, individual fresh sperm motility, postthaw sperm motility, acrosome integrity, hypo-osmotic swelling test, live and dead count, total morphological abnormality, and head abnormality of sperm in crossbred bulls. Growth hormone gene might be considered a candidate gene for seminal and sexual behavioral traits in crossbred cattle.

  5. Effects of ecological differentiation on Lotka-Volterra systems for species with behavioral adaptation and variable growth rates.

    Science.gov (United States)

    Lacitignola, D; Tebaldi, C

    2005-03-01

    We study the properties of a n2-dimensional Lotka-Volterra system describing competing species that include behaviorally adaptive abilities. We indicate as behavioral adaptation a mechanism, based on a kind of learning, which is not viewed in the evolutionary sense but is intended to occur over shorter time scales. We consider a competitive adaptive n species Lotka-Volterra system, n > or = 3, in which one species is made ecologically differentiated with respect to the others by carrying capacity and intrinsic growth rate. The symmetry properties of the system and the existence of a certain class of invariant subspaces allow the introduction of a 7-dimensional reduced model, where n appears as a parameter, which gives full account of existence and stability of equilibria in the complete system. The reduced model is effective also in describing the time-dependent regimes for a large range of parameter values. The case in which one species has a strong ecological advantage (i.e. with a carrying capacity higher than the others), but with a varying growth rate, has been analyzed in detail, and time-dependent behaviors have been investigated in the case of adaptive competition among four species. Relevant questions, as species survival/exclusion, are addressed focusing on the role of adaptation. Interesting forms of species coexistence are found (i.e. competitive stable equilibria, periodic oscillations, strange attractors).

  6. Abnormal grain growth effects on the mechanical behavior of Ni electrodeposits

    Energy Technology Data Exchange (ETDEWEB)

    Arnould, O. [LMT-Cachan, ENS Cachan/CNRS-UMR 8535/Univ. Paris VI, Cachan (France); Lab. de Mecanique et Genie Civil, Univ. Montpellier II, Montpellier (France); Hubert, O.; Hild, F. [LMT-Cachan, ENS Cachan/CNRS-UMR 8535/Univ. Paris VI, Cachan (France)

    2004-07-01

    The study deals with the long-term reliability of a high precision pressure sensor using bellows. They are mainly made of electroplated Ni whose thermal stability is investigated by DSC. EBSD measurements and SEM observations give some evidence for an abnormal grain growth mechanism whose effects on the elasto-plastic properties of the Ni deposit are experimentally investigated. Abnormal grain growth leads to an increase in the elastic modulus and a strong decrease in the yield strength. (orig.)

  7. Growth and change in attention problems, disruptive behavior, and achievement from kindergarten to fifth grade.

    Science.gov (United States)

    Claessens, Amy; Dowsett, Chantelle

    2014-12-01

    Despite widespread interest in children's adjustment problems, existing research does not provide conclusive evidence regarding the direction of the associations of achievement with classroom attention problems and disruptive behavior over the course of elementary school. Using a nationally representative sample of 16,260 kindergarteners, this study examined the temporal sequence of achievement, classroom attention problems, and disruptive behavior, focusing on how changes in skills and problems unfold across key periods between kindergarten and fifth grade. Results indicate that improvements in attention during the earliest years of schooling predict achievement gains through third grade. However, changes in disruptive behavior do not predict subsequent changes in achievement. Evidence linking changes in achievement to changes in classroom attention problems and disruptive behavior was less consistent. These findings point to the need to develop and examine early interventions that can improve attention skills as a mechanism for improving children's academic trajectories in elementary school.

  8. Mechanical behavior of cells within a cell-based model of wheat leaf growth

    Directory of Open Access Journals (Sweden)

    Ulyana Zubairova

    2016-12-01

    Full Text Available Understanding the principles and mechanisms of cell growth coordination in plant tissue remains an outstanding challenge for modern developmental biology. Cell-based modeling is a widely used technique for studying the geometric and topological features of plant tissue morphology during growth. We developed a quasi-one-dimensional model of unidirectional growth of a tissue layer in a linear leaf blade that takes cell autonomous growth mode into account. The model allows for fitting of the visible cell length using the experimental cell length distribution along the longitudinal axis of a wheat leaf epidermis. Additionally, it describes changes in turgor and osmotic pressures for each cell in the growing tissue. Our numerical experiments show that the pressures in the cell change over the cell cycle, and in symplastically growing tissue, they vary from cell to cell and strongly depend on the leaf growing zone to which the cells belong. Therefore, we believe that the mechanical signals generated by pressures are important to consider in simulations of tissue growth as possible targets for molecular genetic regulators of individual cell growth.

  9. Drosophila Nipped-B Mutants Model Cornelia de Lange Syndrome in Growth and Behavior.

    Directory of Open Access Journals (Sweden)

    Yaning Wu

    2015-11-01

    Full Text Available Individuals with Cornelia de Lange Syndrome (CdLS display diverse developmental deficits, including slow growth, multiple limb and organ abnormalities, and intellectual disabilities. Severely-affected individuals most often have dominant loss-of-function mutations in the Nipped-B-Like (NIPBL gene, and milder cases often have missense or in-frame deletion mutations in genes encoding subunits of the cohesin complex. Cohesin mediates sister chromatid cohesion to facilitate accurate chromosome segregation, and NIPBL is required for cohesin to bind to chromosomes. Individuals with CdLS, however, do not display overt cohesion or segregation defects. Rather, studies in human cells and model organisms indicate that modest decreases in NIPBL and cohesin activity alter the transcription of many genes that regulate growth and development. Sister chromatid cohesion factors, including the Nipped-B ortholog of NIPBL, are also critical for gene expression and development in Drosophila melanogaster. Here we describe how a modest reduction in Nipped-B activity alters growth and neurological function in Drosophila. These studies reveal that Nipped-B heterozygous mutant Drosophila show reduced growth, learning, and memory, and altered circadian rhythms. Importantly, the growth deficits are not caused by changes in systemic growth controls, but reductions in cell number and size attributable in part to reduced expression of myc (diminutive and other growth control genes. The learning, memory and circadian deficits are accompanied by morphological abnormalities in brain structure. These studies confirm that Drosophila Nipped-B mutants provide a useful model for understanding CdLS, and provide new insights into the origins of birth defects.

  10. An Interface Damage Model for the Simulation of Delamination Under Variable-Mode Ratio in Composite Materials

    Science.gov (United States)

    Turon, Albert; Camanho, Pedro P.; Costa, Josep; Davila, Carlos G.

    2004-01-01

    A thermodynamically consistent damage model for the simulation of progressive delamination under variable mode ratio is presented. The model is formulated in the context of the Damage Mechanics (DM). The constitutive equations that result from the variation of the free energy with damage are used to model the initiation and propagation of delamination. A new delamination initiation criterion is developed to assure that the formulation can account for changes in the loading mode in a thermodynamically consistent way. Interfacial penetration of two adjacent layers after complete decohesion is prevented by the formulation of the free energy. The model is implemented into the commercial finite element code ABAQUS by means of a user-written decohesion element. Finally, the numerical predictions given by the model are compared with experimental results.

  11. Free Edge Mixed Mode Delamination Analysis of Laminated Composites with Wrap-Around Configuration: A Finite Element Study

    Science.gov (United States)

    Choudhury, Pannalal; Das, Subhankar; Halder, Sudipta; Pandey, Krishna Murari

    2016-10-01

    Finite element analyses of laminated composites were done in the present study with respect to suppression of free edge delamination by an innovative technique. Wrap-around configuration was considered to determine its effectiveness over the wrapper-less laminated configuration on laminated composites. Nodal stresses were generated ahead of the crack tip through finite element analysis. This was used for determining interlaminar normal stress and inter laminar shear stress distributions at the critical interface. Later virtual crack closure technique was used to estimate the strain energy release rate components for several sizes of virtual crack extensions through a single finite element analysis. Computational analysis predicts Mode-I delamination as dominant mode of failure. This mode of delamination was significantly suppressed with wrap-around configuration on laminated composites.

  12. Measuring laves phase particle size and thermodynamic calculating its growth and coarsening behavior in P92 steels

    DEFF Research Database (Denmark)

    Yao, Bing-Yin; Zhou, Rong-Can; Fan, Chang-Xin;

    2010-01-01

    ) images in scanning electron microscope (SEM). The smaller Laves phase particle size results in higher creep strength and longer creep exposure time at the same conditions. DICTRA software was used to model the growth and coarsening behavior of Laves phase in the three P92 steels. Good agreements were......The growth of Laves phase particles in three kinds of P92 steels were investigated. Laves phase particles can be easily separated and distinguished from the matrix and other particles by atom number contrast using comparisons of the backscatter electrons (BSE) images and the secondary electrons (SE...... attained between measurements in SEM and modeling by DICTRA. Ostwald ripening should be used for the coarsening calculation of Laves phase in P92 steels for time longer than 20000 h and 50000 h at 650°C and 600°C, respectively. © 2010 Chin. Soc. for Elec. Eng....

  13. Orientation and growth behavior of CaHfO3 thin films on non-oxide substrates

    Energy Technology Data Exchange (ETDEWEB)

    Kwon, Y. W. [University of Florida; Norton, David P. [University of Florida; Budai, John D [ORNL

    2007-01-01

    The growth behavior of CaHfO3 on (001) Ni and Ge substrates was examined. CaHfO3 is a perovskite insulator that is suitable for applications as a buffer layer or gate dielectric. The tendency for CaHfO3 growth on both (001) Ni and (001) Ge substrates is to orient with the CaHfO3 (200)+(121) planes parallel to the surface, which corresponds to the (110) orientation in the pseudo-cubic geometry. This differs from that of CaHfO3 on perovskites, such as (001) LaAlO3, where a pseudo-cube-on-cube orientation is observed.

  14. STUDY ON THE SURFACE CRACK GROWTH BEHAVIOR IN 14MnNbq BRIDGE STEEL

    Institute of Scientific and Technical Information of China (English)

    Yanping Liu; Chuanyao Chen; Guoqing Li

    2010-01-01

    Three-dimensional crack closure correction methods are investigated in this paper.The fatigue crack growth tests of surface cracks in 14MnNbq steel for bridge plate subjected to tensile and bending loadings are systematically conducted.The experimentally measured fatigue crack growth rates of surface cracks are compared with those of through-thickness cracks in detail.It is found that the crack growth rates of surface cracks are lower than those of through-thickness cracks.In order to correct their differences in fatigue crack growth rates,a dimensionless crack closure correction model is proposed.Although this correction model is determined only by the experimental data of surface cracks under tensile loading with a constant ratio R=0.05,it can correlate the surface crack growth rates with reasonable accuracy under tensile and bending loadings with various stress ratios ranging from 0 to 0.5.Furthermore,predictions of fatigue life and crack aspect ratio for surface cracks are discussed,and the predicted results are also compared with those obtained from other prediction approaches.Comparison results show that the proposed crack closure correction model gives better prediction of fatigue life than other models.

  15. Maternal behavior in transgenic mice with reduced fibroblast growth factor receptor function in gonadotropin-releasing hormone neurons

    Directory of Open Access Journals (Sweden)

    Brooks Leah R

    2012-09-01

    Full Text Available Abstract Background Fibroblast growth factors (FGFs and their receptors (FGFRs are necessary for the proper development of gonadotropin-releasing hormone (GnRH neurons, which are key activators of the hypothalamo-pituitary-gonadal axis. Transgenic mice that have the targeted expression of a dominant negative FGFR (dnFGFR in GnRH neurons (dnFGFR mice have a 30% decrease of GnRH neurons. Additionally, only 30–40% of the pups born to the transgenic dams survive to weaning age. These data raised the possibility that FGFR defects in GnRH neurons could adversely affect maternal behavior via novel mechanisms. Methods We first determined if defective maternal behavior in dnFGFR mothers may contribute to poor pup survival by measuring pup retrieval and a battery of maternal behaviors in primiparous control (n = 10–12 and dnFGFR (n = 13–14 mothers. Other endocrine correlates of maternal behaviors, including plasma estradiol levels and hypothalamic pro-oxyphysin and GnRH transcript levels were also determined using enzyme-linked immunoassay and quantitative reverse transcription polymerase chain reaction, respectively. Results Maternal behaviors (% time crouching with pups, time off pups but not feeding, time feeding, and total number of nesting bouts were not significantly different in dnFGFR mice. However, dnFGFR dams were more likely to leave their pups scattered and took significantly longer to retrieve each pup compared to control dams. Further, dnFGFR mothers had significantly lower GnRH transcripts and circulating E2, but normal pro-oxyphysin transcript levels. Conclusions Overall, this study suggests a complex scenario in which a GnRH system compromised by reduced FGF signaling leads to not only suboptimal reproductive physiology, but also suboptimal maternal behavior.

  16. The Effect of Veneer Layers on the Bending Shear Strength and Delamination of Laminated Veneer Lumber (LVL) from Oil Palm Trunk (OPT)

    Science.gov (United States)

    Jamaludin, M. A.; Nordin, K.; Bahari, S. A.; Ahmad, M.

    2010-03-01

    The aim of this study was to evaluate the effects of the number of veneer layers on the bending shear strength and delamination of Laminated Veneer Lumber (LVL) from oil palm trunk (OPT). Five (5), Six (6) and Seven (7) veneer layers of OPT LVL were manufactured. The dimension of the boards was 45 cm by 45 cm by 1.9 cm. The boards were hot pressed for 13 minutes at a pressure of 31 kgf per m2. Urea formaldehyde (UF) supplied by a local adhesive manufacturer was used as the binder for the boards. The bending shear tests consisted of the edgewise and flatwise tests, whereas the delamination test consisted of the cold and hot water boil tests. The preparation of the test specimens and tests set-up was in accordance to the Japanese Standards, JAS-1991 [1]. Six replications were used for each test. The results were analyzed by Analysis of Variance (ANOVA) using the Duncan's Multiple Range Test to test for significant differences. The results indicated that as the number of layers increased the strength also increased. All the boards passed the standard. The difference in strength between the different types of samples was significant at 95 percent confidence level. Bending shear failures were primarily in the veneers. It is possible to use the boards as light weight interior building and furniture components. Over the years, the supply of quality timber resources from the natural forest has decrease as the wood-based industry experienced rapid growth. The supply of rubberwood for the furniture industry is also decreasing as a result of increase latex price. Accordingly, OPT LVL can be an alternative or supplementary raw material for the wood-based industry.

  17. Short fatigue cracks growth and closure behavior in an austenitic stainless steel at 600 C and 650 C

    Energy Technology Data Exchange (ETDEWEB)

    Polvora, J.P.; Laiarinandrasana, L.; Drubay, B.; Piques, R.; Martelet, B. [Instituto de Pesquisas Energeticas e Nucleares (IPEN), Sao Paulo, SP (Brazil)

    1995-12-31

    In this work, following fatigue crack growth tests carried out at the CEN-SACLAY (AMORFIS program) by Laiarinandrasana (1994) on 316 L(N) CT specimens at 650{sup 0}C and 600{sup 0}C, short crack behavior of cracks emanating from machined notches is investigated. Experimental results are presented and discussions are directed to notch plasticity effect in relation with variations in crack opening stress intensity factor, K{sub op}, with crack lenght (author). 12 refs., 5 figs., 2 tab.

  18. Effects of Lévy noise and immune delay on the extinction behavior in a tumor growth model

    Science.gov (United States)

    Hao, Meng-Li; Xu, Wei; Gu, Xu-Dong; Qi, Lu-Yuan

    2014-09-01

    The combined effects of Lévy noise and immune delay on the extinction behavior in a tumor growth model are explored. The extinction probability of tumor with certain density is measured by exit probability. The expression of the exit probability is obtained using the Taylor expansion and the infinitesimal generator theory. Based on numerical calculations, it is found that the immune delay facilitates tumor extinction when the stability index α 1. Moreover, larger stability index and smaller noise intensity are in favor of the extinction for tumor with low density. While for tumor with high density, the stability index and the noise intensity should be reduced to promote tumor extinction.

  19. In-Depth Insights into the Key Steps of Delamination of Charged 2D Nanomaterials.

    Science.gov (United States)

    Rosenfeldt, Sabine; Stöter, Matthias; Schlenk, Mathias; Martin, Thomas; Albuquerque, Rodrigo Queiroz; Förster, Stephan; Breu, Josef

    2016-10-07

    Delamination is a key step to obtain individual layers from inorganic layered materials needed for fundamental studies and applications. For layered van der Waals materials such as graphene, the adhesion forces are small, allowing for mechanical exfoliation, whereas for ionic layered materials such as layered silicates, the energy to separate adjacent layers is considerably higher. Quite counterintuitively, we show for a synthetic layered silicate (Na0.5-hectorite) that a scalable and quantitative delamination by simple hydration is possible for high and homogeneous charge density, even for aspect ratios as large as 20000. A general requirement is the separation of adjacent layers by solvation to a distance where layer interactions become repulsive (Gouy-Chapman length). Further hydration up to 34 nm leads to the formation of a highly ordered lamellar liquid crystalline phase (Wigner crystal). Up to eight higher-order reflections indicate excellent positional order of individual layers. The Wigner crystal melts when the interlayer separation reaches the Debye length, where electrostatic interactions between adjacent layers are screened. The layers become weakly charge-correlated. This is indicated by fulfilling the classical Hansen-Verlet and Lindeman criteria for melting. We provide insight into the requirements for layer separation and controlling the layer distances for a broad range of materials and outline an important pathway for the integration of layers into devices for advanced applications.

  20. Glass delamination: a comparison of the inner surface performance of vials and pre-filled syringes.

    Science.gov (United States)

    Zhao, Jianxiu; Lavalley, Virginie; Mangiagalli, Paolo; Wright, Justin M; Bankston, Theresa E

    2014-12-01

    The occurrence of glass delamination is a serious concern for parenteral drug products. Over the past several years, there has been a series of product recalls involving glass delamination in parenteral drugs stored in vials which has led to heightened industry and regulatory scrutiny. In this study, a two-pronged approach was employed to assess the inner surface durability of vials and pre-filled syringes. Non-siliconized syringes were used in order to directly compare glass to glass performance between vials and syringes. The vial and syringe performance was screened with pharmaceutically relevant formulation conditions. The influence of pH, buffer type, ionic strength, and glass type and source was evaluated. In addition, an aggressive but discriminating formulation condition (glutaric acid, pH 11) was used to ascertain the impact of syringe processing. Advanced analytical tools including inductively coupled plasma/mass spectrometry, scanning electron microscopy, atomic force microscopy, and dynamic secondary ion mass spectroscopy showed significant differences in glass performance between vials and syringes. Pre-filled syringes outperform vials for most tests and conditions. The manufacturing conditions for vials lead to glass defects, not found in pre-filled syringes, which result in a less chemically resistant surface. The screening methodology presented in this work can be applied to assess suitability of primary containers for specific drug applications.

  1. Rapid guided wave delamination detection and quantification in composites using global-local sensing

    Science.gov (United States)

    Tian, Zhenhua; Yu, Lingyu; Leckey, Cara

    2016-08-01

    This paper presents a rapid guided ultrasonic wave inspection approach through global inspection by phased array beamforming and local damage evaluation via wavenumber analysis. The global-local approach uses a hybrid system consisting of a PZT wafer and a non-contact laser vibrometer. The overall inspection is performed in two steps. First, a phased array configured by a small number of measurements performs beamforming and beamsteering over the entire plate in order to detect and locate the presence of the damage. A local area is identified as target damage area for the second step. Then a high density wavefield measurement is taken over the target damage area and a spatial wavenumber imaging is performed to quantitatively evaluate the damage. The two-step inspection has been applied to locate and quantify impact-induced delamination damage in a carbon fiber reinforced polymer composite plate. The detected delamination location, size and shape agree well with those of an ultrasonic C-scan. For the test case studied in this work the global-local approach reduced the total composite inspection (damage detection and characterization) time by ∼97% compared to using a full scan approach.

  2. Reactivity of Mg-Al hydrotalcites in solid and delaminated forms in ammonium carbonate solutions

    Science.gov (United States)

    Stoica, Georgiana; Santiago, Marta; Abelló, Sònia; Pérez-Ramírez, Javier

    2010-10-01

    Treatment of Mg-Al hydrotalcites (LDHs, layered double hydroxides) in aqueous (NH 4) 2CO 3 at 298 K leads to composites of dawsonite, hydrotalcite, and magnesium ammonium carbonate. The mechanism and kinetics of this transformation, ultimately determining the relative amounts of these components in the composite, depend on the treatment time (from 1 h to 9 days), the Mg/Al ratio in the hydrotalcite (2-4), and on the starting layered double hydroxide (solid or delaminated form). The materials at various stages of the treatment were characterized by inductive coupled plasma-optical emission spectroscopy, X-ray diffraction, transmission electron microscopy, infrared spectroscopy, thermogravimetry, and nitrogen adsorption at 77 K. The progressive transformation of hydrotalcite towards crystalline dawsonite and magnesium ammonium carbonate phases follows a dissolution-precipitation mechanism. A gradual decrease of the Mg/Al ratio in the resulting solids was observed in time due to magnesium leaching in the reacting medium. Dawsonite-hydrotalcite composite formation is favored at high aluminum contents in the starting hydrotalcite, while the formation of magnesium ammonium carbonate is favored at high Mg/Al ratios. The synthetic strategy comprising hydrotalcite delamination in formamide prior to aqueous (NH 4) 2CO 3 treatment is more reactive towards composite formation than starting from the bulk solid hydrotalcite.

  3. Stability diagram of unilateral buckling patterns of strip-delaminated films.

    Science.gov (United States)

    Parry, G; Cimetière, A; Coupeau, C; Colin, J; Grilhé, J

    2006-12-01

    Thin films deposited on substrates are usually submitted to large residual compression stresses, causing delamination and buckling of the film into various patterns. The present study is focused on the different equilibria arising on strip-shaped delaminated areas. The three most common types of buckling patterns observed on such strips are known as the straight-sided wrinkles, bubble pattern, and telephone cord blisters. The stability of those equilibria as a function of the two stress components of the loading is investigated. The Föppl-Von Karman model for elastic plates is used for theoretical aspects. The post-critical equilibrium paths of the buckling patterns are investigated numerically by means of the finite-element method. The substrate is assumed to be rigid and the contact to be frictionless. The equilibrium solutions can be classified into families of homologous equilibria allowing the identification of dimensionless parameters for the study of stability. A mapping of the different stable post-critical equilibria is given. It is shown that the straight-sided wrinkles and the bubbles are associated with anisotropy of stresses and/or of elastic properties, whereas the telephone cords are stable at high isotropic stresses. The morphological transitions are experimentally evidenced by in situ atomic force microscopy observations of a nickel 50-nm-thick film under stress.

  4. Interface delamination of the thermal barrier coating subjected to local heating

    Institute of Scientific and Technical Information of China (English)

    2010-01-01

    To investigate the possible failure modes of the thermal barrier coating (TBC) used to protect the scramjet combustion chamber, the local heating via laser beam irradiation was utilized to simulate the service condition of high thermal flux and high temperature gradient. Firstly, the experimental method and process were described and the typical fracture morphology of the TBC under test were provided. Then, the theoretical and finite element modeling were carried out to study the temperature, deformation and stresses of the specimen when the top ceramic coat was subjected to local heating, and to demonstrate the mechanism on the failure of the TBC. It is revealed that the interface delamination shall appear and ultimately lead to the failure of the TBC under such thermal loading of local quick heating. According to the outcome of this study, the driving force of the interface delamination is influenced greatly by the key structural parameters and performance matching. Moreover, by utilizing the rules of the effects of these parameters on the fracture driving force, there is some possibility for the designer to optimize the performances of the TBC.

  5. Visualization of thermally induced delamination by means of guided waves processing

    Science.gov (United States)

    Radzienski, Maciej; Kudela, Pawel; Ostachowicz, Wieslaw

    2013-04-01

    The aim of this paper is to present a method for visualization thermally induced delamination in composite material based on guided wave propagation phenomenon. Tested specimen was submitted to short time period high temperature source, which generated thermal degradation. In particular, delamination in material occurred. This procedure simulates some real case scenarios damage like one cased by atmospheric discharge striking wind turbine blade. Proposed method utilizes processing of full wavefield data acquired by the Scanning Doppler Laser Vibrometer. Registered wavefield images are transformed to wavenumber domain where the wave propagation pattern is removed. In this way after transformation signal back to space domain it contains only information about changes in wave propagation and may be used for damage visualization. However, attenuation of waves cause that visualized anomalies has lower amplitudes with increased distance from the actuator. The proposed enhancement of signal processing algorithm enables quantification of the size of the damage. The enhancement is a technique for compensation of the wave attenuation so that the effects of structural damages have the same influence regardless of the location.

  6. Emergent Behavior from A Cellular Automaton Model for Invasive Tumor Growth in Heterogeneous Microenvironments

    CERN Document Server

    Jiao, Yang

    2011-01-01

    Understanding tumor invasion and metastasis is of crucial importance for both fundamental cancer research and clinical practice. In vitro experiments have established that the invasive growth of malignant tumors is characterized by the dendritic invasive branches composed of chains of tumor cells emanating from the primary tumor mass. The preponderance of previous tumor simulations focused on non-invasive (or proliferative) growth. The formation of the invasive cell chains and their interactions with the primary tumor mass and host microenvironment are not well understood. Here, we present a novel cellular automaton (CA) model that enables one to efficiently simulate invasive tumor growth in a heterogeneous host microenvironment. By taking into account a variety of microscopic-scale tumor-host interactions, including the short-range mechanical interactions between tumor cells and tumor stroma, degradation of extracellular matrix by the invasive cells and oxygen/nutrient gradient driven cell motions, our CA mo...

  7. An investigation of fracture and fatigue crack growth behavior of cast niobium aluminide intermetallics

    Energy Technology Data Exchange (ETDEWEB)

    Ye, F.; Soboyejo, W.O. [Ohio State Univ., Columbus, OH (United States). Dept. of Materials Science and Engineering; Farkas, D. [Department of Materials Science and Engineering, Virginia Polytechnic Institute and State University, 213 Holden Hall, Blacksburg, VA 24061-0237 (United States)

    1999-05-31

    This paper presents the results of a combined experimental and theoretical study of fracture toughness and fatigue crack growth in cast Nb-15Al-xTi (x=10, 25 and 40 at%) niobium aluminide-based intermetallics. Fracture toughness and fatigue crack growth resistance are shown to improve significantly in the cast alloy containing 40 at% Ti. The improvements in the fracture toughness of the 40Ti alloy are shown to be due to the combined effects of ligament toughening, crack-tip plasticity and crack-tip blunting. The atomistic simulations show that the increased plasticity in these alloys is associated with their higher Ti content. The micromechanisms of fatigue crack growth are also elucidated. The implications of the results are discussed for potential structural application of niobium aluminide intermetallics. (orig.) 19 refs.

  8. Psychological contract breaches, organizational commitment, and innovation-related behaviors: a latent growth modeling approach.

    Science.gov (United States)

    Ng, Thomas W H; Feldman, Daniel C; Lam, Simon S K

    2010-07-01

    This study examined the relationships among psychological contract breaches, organizational commitment, and innovation-related behaviors (generating, spreading, implementing innovative ideas at work) over a 6-month period. Results indicate that the effects of psychological contract breaches on employees are not static. Specifically, perceptions of psychological contract breaches strengthened over time and were associated with decreased levels of affective commitment over time. Further, increased perceptions of psychological contract breaches were associated with decreases in innovation-related behaviors. We also found evidence that organizational commitment mediates the relationship between psychological contract breaches and innovation-related behaviors. These results highlight the importance of examining the nomological network of psychological contract breaches from a change perspective.

  9. Particle growth in hydrogen-methane plasmas

    Energy Technology Data Exchange (ETDEWEB)

    Shimizu, T. [Centre for Interdisciplinary Plasma Science, Max-Planck Institute for extraterrestrial Physics, Giessenbachstr. 1, D-85741 Garching (Germany); Jacob, W. [Centre for Interdisciplinary Plasma Science, Max-Planck Institute for Plasma Physics, Boltzmanstr. 2, D-85748 Garching (Germany); Thomas, H. [Centre for Interdisciplinary Plasma Science, Max-Planck Institute for extraterrestrial Physics, Giessenbachstr. 1, D-85741 Garching (Germany); Morfill, G. [Centre for Interdisciplinary Plasma Science, Max-Planck Institute for extraterrestrial Physics, Giessenbachstr. 1, D-85741 Garching (Germany); Abe, T. [Department of Electronic Device and Materials, Tohoku Institute of Technology, 35-1, Kasumi-cho, Yagiyama, Taihaku-ku, Sendai 982-8577 (Japan); Watanabe, Y. [Graduate School of Information Science and Electrical Engineering, Kyushu University, 6-10-1, Hakozaki, Higashi-ku, Fukuoka 812-8581 (Japan); Sato, N. [Centre for Interdisciplinary Plasma Science, Max-Planck Institute for extraterrestrial Physics, Giessenbachstr. 1, D-85741 Garching (Germany); Professor Emeritus, Tohoku University, 05, Aramaki-Aza-Aoba, Aoba-ku, Sendai 980-8579 (Japan)

    2006-05-26

    Particle growth and the behavior of particle clouds in hydrogen-methane capacitively coupled rf plasmas are investigated. At room temperature, most for different wall temperatures and gas compositions of these particles are due to flakes of layers delaminated from the electrode surfaces. Heating of the electrodes up to 800 K and dilution by hydrogen (up to H{sub 2}:CH{sub 4} = 20:1) suppresses the production of the particles from the electrode surfaces. The electron temperature in the particle levitation region is controlled by introducing an additional electrode made from a grid (= gridded electrode) in between the levitation electrode and the driven electrode. If we introduce diamond seed particles ({approx} 2.8 {mu}m in diameter) into the plasma with the gridded electrode in place, we observe nucleation of new grains ({approx} 100 nm) on the surfaces of the diamond particles. On the other hand, without the gridded electrode, we do not observe nucleation but growth of amorphous carbon films on them.

  10. Criteria for initiation of delamination in quasi-static punch-shear tests of a carbon-fiber composite material.

    Energy Technology Data Exchange (ETDEWEB)

    Chin, Eric Brian [Sandia National Lab. (SNL-CA), Livermore, CA (United States); English, Shawn Allen [Sandia National Lab. (SNL-CA), Livermore, CA (United States); Briggs, Timothy [Sandia National Lab. (SNL-CA), Livermore, CA (United States)

    2015-09-01

    V arious phenomenological delamination initiation criteria are analyzed in quasi - static punch - shear tests conducted on six different geometries. These six geometries are modeled and analyzed using elastic, large - deformation finite element analysis. Analysis output is post - processed to assess different delamination initiation criteria, and their applicability to each of the geometries. These criteria are compared to test results to assess whether or not they are appropriate based on what occurred in testing. Further, examinations of CT scans and ultrasonic images o f test specimens are conducted in the appendix to determine the sequence of failure in each test geometry.

  11. Eddy current pulsed phase thermography considering volumetric induction heating for delamination evaluation in carbon fiber reinforced polymers

    Science.gov (United States)

    Yang, Ruizhen; He, Yunze

    2015-06-01

    Anisotropy and inhomogeneity of carbon fiber reinforced polymers (CFRPs) result in that many traditional non-destructive inspection techniques are inapplicable on the delamination evaluation. This letter introduces eddy current pulsed phase thermography (ECPPT) for CFRPs evaluation considering volumetric induction heating due to small electrical conductivity, abnormal thermal wave propagation, and Fourier analysis. The proposed methods were verified through experimental studies under transmission and reflection modes. Using ECPPT, the influence of the non-uniform heating effect and carbon fiber structures can be suppressed, and then delamination detectability can be improved dramatically over eddy current pulsed thermography.

  12. COMPOSITIONAL AND THERMAL DIFFERENCES BETWEEN LITHOSPHERIC AND ASTHENOSPHERIC MANTLE AND THEIR INFLUENCE ON CONTINENTAL DELAMINATION

    Directory of Open Access Journals (Sweden)

    A. I. Kiselev

    2015-09-01

    Full Text Available The lower part of lithosphere in collisional orogens may delaminate due to density inversion between the asthenosphere and the cold thickened lithospheric mantle. Generally, standard delamination models have neglected density changes within the crust and the lithospheric mantle, which occur due to phase transitions and compositional variations upon changes of P-T parameters. Our attention is focused on effects of phase and density changes that may be very important and even dominant when compared with the effect of a simple change of the thermal mantle structure. The paper presents the results of numerical modeling for eclogitization of basalts of the lower crust as well as phase composition changes and density of underlying peridotite resulted from tectonic thickening of the lithosphere and its foundering into the asthenosphere. As the thickness of the lower crust increases, the mafic granulite (basalt passes into eclogite, and density inversion occurs at the accepted crust-mantle boundary (P=20 kbar because the newly formed eclogite is heavier than the underlying peridotite by 6 % (abyssal peridotite, according to [Boyd, 1989]. The density difference is a potential energy for delamination of the eclogitic portion of the crust. According to the model, P=70 kbar and T=1300 °C correspond to conditions at the lower boundary of the lithosphere. Assuming the temperature adiabatic distribution within the asthenosphere, its value at the given parameters ranges from 1350 °C to 1400 °C. Density inversion at dry conditions occurs with the identical lithospheric and asthenospheric compositions at the expense of the temperature difference at 100 °C with the density difference of only 0.0022 %. Differences of two other asthenospheric compositions (primitive mantle, and lherzolite KH as compared to the lithosphere (abyssal peridotite are not compensated for by a higher temperature. The asthenospheric density is higher than that of the lithospheric base

  13. Behaviorism

    Science.gov (United States)

    Moore, J.

    2011-01-01

    Early forms of psychology assumed that mental life was the appropriate subject matter for psychology, and introspection was an appropriate method to engage that subject matter. In 1913, John B. Watson proposed an alternative: classical S-R behaviorism. According to Watson, behavior was a subject matter in its own right, to be studied by the…

  14. Behaviorism

    Science.gov (United States)

    Moore, J.

    2011-01-01

    Early forms of psychology assumed that mental life was the appropriate subject matter for psychology, and introspection was an appropriate method to engage that subject matter. In 1913, John B. Watson proposed an alternative: classical S-R behaviorism. According to Watson, behavior was a subject matter in its own right, to be studied by the…

  15. Parent and Child Personality Traits and Children's Externalizing Problem Behavior from Age 4 to 9 Years: A Cohort-Sequential Latent Growth Curve Analysis

    Science.gov (United States)

    Prinzie, P.; Onghena, P.; Hellinckx, W.

    2005-01-01

    Cohort-sequential latent growth modeling was used to analyze longitudinal data for children's externalizing behavior from four overlapping age cohorts (4, 5, 6, and 7 years at first assessment) measured at three annual time points. The data included mother and father ratings on the Child Behavior Checklist and the Five-Factor Personality Inventory…

  16. A Cohort-Sequential Multivariate Latent Growth Curve Analysis of Normative CBCL Aggressive and Delinquent Problem Behavior: Associations with Harsh Discipline and Gender

    Science.gov (United States)

    Prinzie, P.; Onghena, P.; Hellinckx, W.

    2006-01-01

    The aim of this study was to examine the normative developmental trajectories of aggressive and delinquent behavior in young children. Cohort-sequential univariate latent growth modeling (LGM) analyses were employed to conceptualize and analyze intraindividual changes in children's aggressive and delinquent behavior and interindividual differences…

  17. Cell growth behaviors of Clostridium acetobutylicum in a pervaporation membrane bioreactor for butanol fermentation.

    Science.gov (United States)

    Yao, Peina; Xiao, Zeyi; Chen, Chunyan; Li, Weijia; Deng, Qing

    2016-01-01

    Acetone-butanol-ethanol fermentation using Clostridium acetobutylicum was studied in the continuous and closed-circulating fermentation (CCCF) system. The experiment lasting for 192 H was carried out by integrating fermentation with in situ pervaporation. In the entire process, the cell growth profile took place in the following two phases: the logarithmic phase during early 28 H and the linear phase from 130 to 150 H. This was a unique characteristic compared with the curve of traditional fermentation, and the fitting equations of two growth phases were obtained by Origin software according to the kinetic model of cell growth. Besides, the kinetic parameters that include the butanol yield, maximum specific growth rate, average specific formation rate, and volumetric productivity of butanol were measured as 0.19 g g(-1) , 0.345 H(-1) , 0.134 H(-1) and 0.23 g L(-1)  H(-1) , respectively. The C. acetobutylicum in the CCCF system showed good adaptability and fermentation performance, and the prolonged fermentation period and high production were also the main advantages of CCCF technology.

  18. Crack initiation and crack growth behavior of carbon and low-alloy steels

    Energy Technology Data Exchange (ETDEWEB)

    Gavenda, D.J.; Luebbers, P.R.; Chopra, O.K. [Argonne National Lab., IL (United States). Energy Technology Div.

    1997-01-01

    Section III of the ASME Boiler and Pressure Vessel Code specifies fatigue design curves for structural materials. These curves were based on tests of smooth polished specimens at room temperature in air. The effects of reactor coolant environments are not explicitly addressed by the Code design curves, but recent test data illustrate potentially significant effects of LWR coolant environments on the fatigue resistance of carbon and low-alloy steels. Under certain loading and environmental conditions, fatigue lives of test specimens may be a factor of {approx}70 shorter than in air. Results of fatigue tests that examine the influence of reactor environment on crack imitation and crack growth of carbon and low-alloy steels are presented. Crack lengths as a function of fatigue cycles were determined in air by a surface replication technique, and in water by block loading that leaves marks on the fracture surface. Decreases in fatigue life of low-alloy steels in high-dissolved-oxygen (DO) water are primarily caused by the effects of environment during early stages of fatigue damage, i.e., growth of short cracks <100 {micro}m in depth. For crack sizes of >100 {micro}m, crack growth rates in high-DO water are higher than in air by one order of magnitude. The effects of LWR environments on growth of short cracks are discussed.

  19. Differential effect of culture temperature and specific growth rate on CHO cell behavior in chemostat culture.

    Science.gov (United States)

    Vergara, Mauricio; Becerra, Silvana; Berrios, Julio; Osses, Nelson; Reyes, Juan; Rodríguez-Moyá, María; Gonzalez, Ramon; Altamirano, Claudia

    2014-01-01

    Mild hypothermia condition in mammalian cell culture technology has been one of the main focuses of research for the development of breeding strategies to maximize productivity of these production systems. Despite the large number of studies that show positive effects of mild hypothermia on specific productivity of r-proteins, no experimental approach has addressed the indirect effect of lower temperatures on specific cell growth rate, nor how this condition possibly affects less specific productivity of r-proteins. To separately analyze the effects of mild hypothermia and specific growth rate on CHO cell metabolism and recombinant human tissue plasminogen activator productivity as a model system, high dilution rate (0.017 h(-1)) and low dilution rate (0.012 h(-1)) at two cultivation temperatures (37 and 33 °C) were evaluated using chemostat culture. The results showed a positive effect on the specific productivity of r-protein with decreasing specific growth rate at 33 °C. Differential effect was achieved by mild hypothermia on the specific productivity of r-protein, contrary to the evidence reported in batch culture. Interestingly, reduction of metabolism could not be associated with a decrease in culture temperature, but rather with a decrease in specific growth rate.

  20. ASSUMPTIONS ABOUT THE ROLE OF ECONOMIC GROWTH IN THE DEVELOPMENT OF CONSUMER BEHAVIOR IN ROMANIAN ECONOMY

    Directory of Open Access Journals (Sweden)

    Cristina Teodora B L CEANU

    2011-08-01

    Full Text Available This paper aims to identify valences of Romanian consumer profiles and the main influencing factors of income, especially income of labor. Also, we try to establish causal links between economic growth, income and investment on the one hand, and consumption support, on the other hand.

  1. Explaining Entrepreneurial Behavior: Dispositional Personality Traits, Growth of Personal Entrepreneurial Resources, and Business Idea Generation

    Science.gov (United States)

    Obschonka, Martin; Silbereisen, Rainer K.; Schmitt-Rodermund, Eva

    2012-01-01

    Applying a life-span approach of human development and using the example of science-based business idea generation, the authors used structural equation modeling to test a mediation model for predicting entrepreneurial behavior in a sample of German scientists (2 measurement occasions; Time 1, N = 488). It was found that recalled early…

  2. Explaining Entrepreneurial Behavior: Dispositional Personality Traits, Growth of Personal Entrepreneurial Resources, and Business Idea Generation

    Science.gov (United States)

    Obschonka, Martin; Silbereisen, Rainer K.; Schmitt-Rodermund, Eva

    2012-01-01

    Applying a life-span approach of human development and using the example of science-based business idea generation, the authors used structural equation modeling to test a mediation model for predicting entrepreneurial behavior in a sample of German scientists (2 measurement occasions; Time 1, N = 488). It was found that recalled early…

  3. Growth of Cognitive Skills in Preschoolers: Impact of Sleep Habits and Learning-Related Behaviors

    Science.gov (United States)

    Jung, Eunjoo; Molfese, Victoria J.; Beswick, Jennifer; Jacobi-Vessels, Jill; Molnar, Andrew

    2009-01-01

    Research Findings: The present study used a longitudinal design to identify how sleep habits and learning-related behaviors impact the development of cognitive skills in preschoolers (ages 3-5). Sixty- seven children with parental report and cognitive skill assessment data were included. Scores on the Differential Ability Scales (C. Elliott, 1990)…

  4. Distributed fiber optic sensor-enhanced detection and prediction of shrinkage-induced delamination of ultra-high-performance concrete overlay

    Science.gov (United States)

    Bao, Yi; Valipour, Mahdi; Meng, Weina; Khayat, Kamal H.; Chen, Genda

    2017-08-01

    This study develops a delamination detection system for smart ultra-high-performance concrete (UHPC) overlays using a fully distributed fiber optic sensor. Three 450 mm (length) × 200 mm (width) × 25 mm (thickness) UHPC overlays were cast over an existing 200 mm thick concrete substrate. The initiation and propagation of delamination due to early-age shrinkage of the UHPC overlay were detected as sudden increases and their extension in spatial distribution of shrinkage-induced strains measured from the sensor based on pulse pre-pump Brillouin optical time domain analysis. The distributed sensor is demonstrated effective in detecting delamination openings from microns to hundreds of microns. A three-dimensional finite element model with experimental material properties is proposed to understand the complete delamination process measured from the distributed sensor. The model is validated using the distributed sensor data. The finite element model with cohesive elements for the overlay-substrate interface can predict the complete delamination process.

  5. The effects of alloying elements on tensile strength and the occurrence of delamination in cold-drawn hyper-eutectoid steel wires

    Science.gov (United States)

    Park, D. B.; Lee, J. W.; Lee, Y. S.; Park, K. T.; Nam, W. J.

    2009-04-01

    The effects of alloying elements and initial interlamellar spacing on tensile strength and the occurrence of delamination in cold-drawn hyper-eutectoid steel wires were investigated under equivalent drawing conditions. The initial interlamellar spacing showed little influence on the occurrence of delamination. The addition of Cr effectively increased attainable tensile strength, since the added Cr not only increased tensile strength but also delayed delamination. The addition of Ni also increased attainable tensile strength, since the effect of the added Ni on delaying delamination prevailed over the tendency to decrease tensile strength and work hardening. The addition of Cr increased the attainable tensile strength more effectively than the addition of Ni in cold-drawn hyper-eutectoid steel wires, although the added Ni markedly delayed delamination-associated strain.

  6. Cotinine reduces depressive-like behavior and hippocampal vascular endothelial growth factor downregulation after forced swim stress in mice.

    Science.gov (United States)

    Grizzell, J Alex; Mullins, Michelle; Iarkov, Alexandre; Rohani, Adeeb; Charry, Laura C; Echeverria, Valentina

    2014-12-01

    Cotinine, the predominant metabolite of nicotine, appears to act as an antidepressant. We have previously shown that cotinine reduced immobile postures in Porsolt's forced swim (FS) and tail suspension tests while preserving the synaptic density in the hippocampus as well as prefrontal and entorhinal cortices of mice subjected to chronic restraint stress. In this study, we investigated the effect of daily oral cotinine (5 mg/kg) on depressive-like behavior induced by repeated, FS stress for 6 consecutive days in adult, male C57BL/6J mice. The results support our previous report that cotinine administration reduces depressive-like behavior in mice subjected or not to high salience stress. In addition, cotinine enhanced the expression of the vascular endothelial growth factor (VEGF) in the hippocampus of mice subjected to repetitive FS stress. Altogether, the results suggest that cotinine may be an effective antidepressant positively influencing mood through a mechanism involving the preservation of brain homeostasis and the expression of critical growth factors such as VEGF. (PsycINFO Database Record (c) 2014 APA, all rights reserved).

  7. Piglet behavior as a measure of vitality and its influence on piglet survival and growth during lactation.

    Science.gov (United States)

    Muns, R; Manzanilla, E G; Sol, C; Manteca, X; Gasa, J

    2013-04-01

    The aim of the study was to develop a vitality scoring method, based on piglet behavior and relate it to piglet growth and survival. From 21 sows (Sus scrofa), 287 piglets were used. After farrowing (d 0), piglets were weighed and tested for 4 behavioral parameters in a circular enclosure (55 cm diam.): movement capacity (M), udder stimulation (U), number of completed circles around the enclosure (NCC), and screaming (Sc). Piglets were weighed again on d 1, 2, 3, and 17. Piglet rectal temperature (RT) was recorded on d 0, 1, 2, and 3. Farrowing information of the sow was also recorded. Multiple regression analyses for survival and BW gain at weaning as dependent variables were performed. Piglet BW gain at weaning was influenced by BW at birth (P piglets born alive per sow (P Piglet survival during lactation was influenced by BW at birth (P = 0.015), UNCC parameter (P = 0.026), and RT on d 3 (P = 0.085). The sum of U and NCC parameters, in combination with BW at birth and information of the sow, might be useful to predict piglet growth survival during lactation, thus becoming a useful tool to improve piglet management during the first days of lactation. In conclusion, UNCC parameter seems to be an easy and useful way to assess piglet vitality for both scientific and commercial purposes.

  8. Asymptotic behavior of nonlinear semigroup describing a model of selective cell growth regulation.

    Science.gov (United States)

    Arino, O; Kimmel, M

    1991-01-01

    A new scheme of regulation of cell population growth is considered, called the selective growth regulation. The principle is that cells are withdrawn from proliferation depending on their contents of certain biochemical species. The dynamics of the cell population structured by the contents of this species is described by the functional integral equation model, previously introduced by the authors. The solutions of the model equations generate a semigroup of nonlinear positive operators. The main problem solved in this paper concerns stability of the equilibria of the model. This requires stating and proving of an original abstract result on the spectral radius of a perturbation of a semigroup of positive linear operators. Biological applications are discussed.

  9. Mouth breathing: adverse effects on facial growth, health, academics, and behavior.

    Science.gov (United States)

    Jefferson, Yosh

    2010-01-01

    The vast majority of health care professionals are unaware of the negative impact of upper airway obstruction (mouth breathing) on normal facial growth and physiologic health. Children whose mouth breathing is untreated may develop long, narrow faces, narrow mouths, high palatal vaults, dental malocclusion, gummy smiles, and many other unattractive facial features, such as skeletal Class II or Class III facial profiles. These children do not sleep well at night due to obstructed airways; this lack of sleep can adversely affect their growth and academic performance. Many of these children are misdiagnosed with attention deficit disorder (ADD) and hyperactivity. It is important for the entire health care community (including general and pediatric dentists) to screen and diagnose for mouth breathing in adults and in children as young as 5 years of age. If mouth breathing is treated early, its negative effect on facial and dental development and the medical and social problems associated with it can be reduced or averted.

  10. [The growth behavior of mouse fibroblasts on intraocular lens surface of various silicone and PMMA materials].

    Science.gov (United States)

    Kammann, J; Kreiner, C F; Kaden, P

    1994-08-01

    Experience with intraocular lenses (IOL) made of PMMA dates back ca. 40 years, while silicone IOLs have been in use for only about 10 years. The biocompatibility of PMMA and silicone caoutchouc was tested in a comparative study investigating the growth of mouse fibroblasts on different IOL materials. Spectrophotometric determination of protein synthesis and liquid scintillation counting of DNA synthesis were carried out. The spreading of cells was planimetrically determined, and the DNA synthesis of individual cells in direct contact with the test sample was tested. The results showed that the biocompatibility of silicone lenses made of purified caoutchouc is comparable with that of PMMA lenses; there is no statistically significant difference. However, impurities arising during material synthesis result in a statistically significant inhibition of cell growth on the IOL surfaces.

  11. Grain Growth and Precipitation Behavior of Iridium Alloy DOP-26 During Long Term Aging

    Energy Technology Data Exchange (ETDEWEB)

    Pierce, Dean T. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Muralidharan, Govindarajan [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Fox, Ethan E. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Cox, Victoria A. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Geer, Tom [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)

    2017-05-01

    The influence of long term aging on grain growth and precipitate sizes and spatial distribution in iridium alloy DOP-26 was studied. Samples of DOP-26 were fabricated using the new process, recrystallized for 1 hour (h) at 1375 C, then aged at either 1300, 1400, or 1500 C for times ranging from 50 to 10,000 h. Grain size measurements (vertical and horizontal mean linear intercept and horizontal and vertical projection) and analyses of iridium-thorium precipitates (size and spacing) were made on the longitudinal, transverse, and rolling surfaces of the as-recrystallized and aged specimens from which the two-dimensional spatial distribution and mean sizes of the precipitates were obtained. The results obtained from this study are intended to provide input to grain growth models.

  12. Fatigue crack growth rate (FCGR) behavior of nicalon/SiC composites

    Energy Technology Data Exchange (ETDEWEB)

    Miriyala, N.; Liaw, P.K.; Yu, N. [Univ. of Tennessee, Knoxville, TN (United States)] [and others

    1995-04-01

    The objective is to develop a fundamental understanding of fatigue crack growth phenomenon in Nicalon/SiC composites. Ultrasonic measurements were continued on the Nicalon/SiC composite specimens to correlate elastic moduli with percentage porosity in the in-plane as well as through-thickness directions. A micromechanics model based on periodic microstructure was developed to predict the elastic stiffness constants of the Nicalon/SiC composites. The predicted values were in good agreement with the experimental results.

  13. Effects of heating time on the growth and behavior of amorphous carbon nanostructures from ferrocene

    Science.gov (United States)

    Rafiqul Islam, Md; Rashid, A. K. M. B.; Ferdous, Md; Shafiul Azam, Md

    2017-05-01

    Heating time is one of the crucial factors in various methods employed for the synthesis of carbon nanostructures (CNSs) from ferrocene. However, the effects of heating time on the growth and morphology of the nanostructured materials has not been well explored yet, particularly for amorphous carbon. Herein, we investigate how the variation of heating time impacts the growth of CNSs by carrying out the reaction between ferrocene and ammonium chloride in a solvent free condition at 250 °C. Several different forms of carbon nanostructures yielded from this reaction at 25 min (CNS-25), 30 min (CNS-30), 35 min (CNS-35) and 40 min (CNS-40) were analyzed by means of field emission scanning electron microscopy (FESEM) coupled with energy-dispersive x-ray (EDX), Fourier transform infrared (FTIR) and ultraviolet-visible (UV-Vis) spectroscopy. The final product CNS-40 was washed several times with concentrated hydrochloric acid solution to remove the impurities and then characterized by the means of similar techniques. FTIR spectra of all the nanostructures confirmed the presence of several functional groups such as C  =  C, C-O and -OH etc, which are common in carbonaceous nanostructures. However, the FESEM images obtained are significantly different and suggest a gradual growth of the carbon nanostructures ending up with long carbon nanotubes after 40 min. No absorption peak in the visible region of the UV-Vis spectra of the final product confirms the amorphous nature, which is also supported by XRD of the synthesized nanotube. Moreover, a noteworthy redshift in the UV-Vis peaks reflecting a huge increase in length and diameter of the nanostructures indicates the maximum longitudinal growth of the carbon nanotubes occurs during 35 min to 40 min.

  14. Fatigue-crack growth behavior of Type 347 stainless steels under simulated PWR water conditions

    Energy Technology Data Exchange (ETDEWEB)

    Hong, Seokmin; Min, Ki-Deuk; Yoon, Ji-Hyun; Kim, Min-Chul; Lee, Bong-Sang [Korea Atomic Energy Research Institute, Daejeon (Korea, Republic of)

    2015-10-15

    Fatigue crack growth rate (FCGR) curve of stainless steel exists in ASME code section XI, but it is still not considering the environmental effects. The longer time nuclear power plant is operated, the more the environmental degradation issues of materials pop up. There are some researches on fatigue crack growth rate of S304 and S316, but researches of FCGR of S347 used in Korea nuclear power plant are insufficient. In this study, the FCGR of S347 stainless steel was evaluated in the PWR high temperature water conditions. The FCGRs of S347 stainless steel under pressurized-water conditions were measured by using compact-tension (CT) specimens at different levels of dissolved oxygen (DO) and frequency. 1. FCGRs of SS347 were slower than that in ASME XI and environmental effect did not occur when frequency was higher than 1Hz. 2. Fatigue crack growth is accelerated by corrosion fatigue and it is more severe when frequency is slower than 0.1Hz. 3. Increase of crack tip opening time increased corrosion fatigue and it deteriorated environmental fatigue properties.

  15. Fatigue crack growth behavior of the simulated HAZ of 800 MPa grade high-performance steel

    Energy Technology Data Exchange (ETDEWEB)

    Kim, Sanghoon [Division of Materials Science and Engineering, Hanyang University, 17 Haengdang-dong, Seongdong-gu, Seoul 133-791 (Korea, Republic of); Kang, Donghwan; Kim, Tae-Won [School of Mechanical Engineering, Hanyang University, 17 Haengdang-dong, Seongdong-gu, Seoul 133-791 (Korea, Republic of); Lee, Jongkwan [Research Institute of Industrial Science and Technology, 75-9, Youngcheon, Dongtan, Hwaseong, Gyeonggi-do 445-813 (Korea, Republic of); Lee, Changhee, E-mail: chlee@hanyang.ac.kr [Division of Materials Science and Engineering, Hanyang University, 17 Haengdang-dong, Seongdong-gu, Seoul 133-791 (Korea, Republic of)

    2011-03-15

    Research highlights: {yields} Fatigue crack resistances of HSB800 base steel and HAZs: Base steel > FGHAZ > CGHAZ > ICCGHAZ. {yields} In the case of ICCGHAZ, fatigue cracks are rapidly initiated and propagated through massive M-A constituents. {yields} Fatigue crack growth rate of CGHAZ was faster than that of FGHAZ, mainly due to the coarsened prior austenite grain and martensite packet. - Abstract: The present study focuses on the fatigue properties in the weld heat-affected zone (HAZ) of 800 MPa grade high-performance steel, which is commonly used in bridges and buildings. Single- and multi-pass HAZs were simulated by the Gleeble system. Fatigue properties were estimated using a crack propagation test under a 0.3 stress ratio and 0.1 load frequencies. The microstructures and fracture surfaces were analyzed by optical microscopy, scanning electron microscopy, and transmission electron microscopy. The results of the crack propagation test showed that the fatigue crack growth rate of coarse-grained HAZ (CGHAZ) was faster than fine-grained HAZ (FGHAZ), although both regions have identical fully martensite microstructures, because FGHAZ has smaller prior austenite grain and martensite packet sizes, which can act as effective barriers to crack propagation. The fatigue crack growth rate of intercritically reheated CGHAZ (ICCGHAZ) was the fastest among local zones in the HAZ, due to rapid crack initiation and propagation via the massive martensite-austenite (M-A) constituent.

  16. Numerical Investigation for the Microstructural Effects on the Crack Growth Behavior of Particulate Composite Materials

    Science.gov (United States)

    2006-07-26

    When the damage constitutive law is adopted in an analysis, we perform an incremental analysis, just like the case of elastoplasticity (see Okada...isotropic elastoplasticity . 2.4 Some other issues associated with the damage constitutive law-initiation of nonlinear deformation Material...ABSTRACT In present investigation, analyses for the damage evolution behavior of particulate composite materials by using the finite element method

  17. In-situ study of the influence of additives on the growth behavior of copper electrodeposits on copper single crystal

    Science.gov (United States)

    Wu, Aiwen

    . In the presence of MPSA, growth was not confined to nucleation centers, and the (100) symmetry was visible in the main features. However, pyramidal mounds did not develop. None of the existing models described sufficiently the surface growth mechanism for this case. Roughening of copper deposits in oxygen-free solution was faster than in oxygen-saturated solution. The results of scaling analysis and pattern-recognition analysis were in agreement with kinetic studies conducted by other researchers. The presence of dissolved oxygen in solutions did not remarkably affect the scaling behavior for each examined solution.

  18. Growth behavior of intermetallic compounds at Sn–Ag/Cu joint interfaces revealed by 3D imaging

    Energy Technology Data Exchange (ETDEWEB)

    Zhang, Q.K., E-mail: qkzhang@alum.imr.ac.cn [Shenyang National Laboratory for Materials Science, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016 (China); State Key Laboratory of Advanced Brazing Filler Metals & Technology, Zhengzhou Research Institute of Mechanical Engineering, Zhengzhou 450001 (China); Long, W.M. [State Key Laboratory of Advanced Brazing Filler Metals & Technology, Zhengzhou Research Institute of Mechanical Engineering, Zhengzhou 450001 (China); Zhang, Z.F., E-mail: zhfzhang@imr.ac.cn [Shenyang National Laboratory for Materials Science, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016 (China)

    2015-10-15

    In this study, the morphologies of intermetallic compounds (IMCs) at the as-soldered and thermal aged Sn–Ag/Cu joint interfaces were observed by SEM and measured using Laser Confocal Microscope, and their three-dimensional (3D) shapes were revealed using 3D imaging technology. The observation reveal that during the soldering process the Cu{sub 6}Sn{sub 5} grains at the joint interface evolve from hemispheroid to a bamboo shoot-shaped body with increasing liquid state reacting time, and their grain size increases sharply. After thermal aging, the Cu{sub 6}Sn{sub 5} grains change into equiaxed grains, while the top of some prominent Cu{sub 6}Sn{sub 5} grains changes little. Due to the higher active energy of the Sn atoms at the grain boundary, the growth rate of IMC grains around the grain boundaries of the solder is higher during the aging process. From the evolution in morphology of the IMC layer, it is demonstrated that the IMC layer grows through grain boundary diffusion of the Cu and Sn atoms during the aging process, and the volume diffusion is very little. The 3D imaging technology is used to reveal the shape and dimension of the IMC grains. - Highlights: • Morphologies of IMCs at the Sn–Ag/Cu interface were revealed by 3D imaging. • Preferential growth of IMCs around the solder grain boundaries was observed. • Growth behaviors of IMCs during reflowing and aging process were investigated.

  19. Deconstructing the externalizing spectrum: growth patterns of overt aggression, covert aggression, oppositional behavior, impulsivity/inattention, and emotion dysregulation between school entry and early adolescence.

    Science.gov (United States)

    Olson, Sheryl L; Sameroff, Arnold J; Lansford, Jennifer E; Sexton, Holly; Davis-Kean, Pamela; Bates, John E; Pettit, Gregory S; Dodge, Kenneth A

    2013-08-01

    The purpose of this study was to determine whether five subcomponents of children's externalizing behavior showed distinctive patterns of long-term growth and predictive correlates. We examined growth in teachers' ratings of overt aggression, covert aggression, oppositional defiance, impulsivity/inattention, and emotion dysregulation across three developmental periods spanning kindergarten through Grade 8 (ages 5-13 years). We also determined whether three salient background characteristics, family socioeconomic status, child ethnicity, and child gender, differentially predicted growth in discrete categories of child externalizing symptoms across development. Participants were 543 kindergarten-age children (52% male, 81% European American, 17% African American) whose problem behaviors were rated by teachers each successive year of development through Grade 8. Latent growth curve analyses were performed for each component scale, contrasting with overall externalizing, in a piecewise fashion encompassing three developmental periods: kindergarten-Grade 2, Grades 3-5, and Grades 6-8. We found that most subconstructs of externalizing behavior increased significantly across the early school age period relative to middle childhood and early adolescence. However, overt aggression did not show early positive growth, and emotion dysregulation significantly increased across middle childhood. Advantages of using subscales were most clear in relation to illustrating different growth functions between the discrete developmental periods. Moreover, growth in some discrete subcomponents was differentially associated with variations in family socioeconomic status and ethnicity. Our findings strongly affirmed the necessity of adopting a developmental approach to the analysis of growth in children's externalizing behavior and provided unique data concerning similarities and differences in growth between subconstructs of child and adolescent externalizing behavior.

  20. Applicability of various wood species in glued laminated timber: Parameter study on delamination resistance and shear strength

    NARCIS (Netherlands)

    Jiang, Y.; Schaffrath, J.; Knorz, M.; Winter, S.; Van de Kuilen, J.W.G.

    2014-01-01

    In a current research project the gluability of four European timber species and their applicability in glued laminated timber is investigated. The influence of different processing parameters on the adhesive bonding is assessed with regard to shear strength and delamination resistance. Furthermore,

  1. Solvent-starved conditions in confinement cause chemical oscillations excited by passage of a cathodic delamination front.

    Science.gov (United States)

    Iqbal, Danish; Sarfraz, Adnan; Stratmann, Martin; Erbe, Andreas

    2015-11-18

    After passage of a delamination front at a polymer/zinc interface, pH oscillations and oscillations in the quantity of corrosion products are observed. The reason for these oscillations is the low quantity of water in the confined reaction volume, water consumption by oxygen reduction, and water regeneration after precipitation of ZnO.

  2. Quantitative characterization of the interfacial adhesion of Ni thin film on steel substrate: A compression-induced buckling delamination test

    Science.gov (United States)

    Zhu, W.; Zhou, Y. C.; Guo, J. W.; Yang, L.; Lu, C.

    2015-01-01

    A compression-induced buckling delamination test is employed to quantitatively characterize the interfacial adhesion of Ni thin film on steel substrate. It is shown that buckles initiate from edge flaws and surface morphologies exhibit symmetric, half-penny shapes. Taking the elastoplasticity of film and substrate into account, a three-dimensional finite element model for an edge flaw with the finite size is established to simulate the evolution of energy release rates and phase angles in the process of interfacial buckling-driven delamination. The results show that delamination propagates along both the straight side and curved front. The mode II delamination plays a dominant role in the process with a straight side whilst the curved front experiences almost the pure mode I. Based on the results of finite element analysis, a numerical model is developed to evaluate the interfacial energy release rate, which is in the range of 250-315 J/m2 with the corresponding phase angle from -41° to -66°. These results are in agreement with the available values determined by other testing methods, which confirms the effectiveness of the numerical model.

  3. Role of Delamination in Zeolite-Catalyzed Aromatic Alkylation: UCB-3 versus 3-D Al-SSZ-70

    Energy Technology Data Exchange (ETDEWEB)

    Runnebaum, Ron C.; Ouyang, Xiaoying; Edsinga, Jeffrey A.; Rea, Thomas; Arslan, Ilke; Hwang, Son-Jong; Zones, Stacey I.; Katz, Alexander

    2014-07-03

    Delaminated zeolite UCB-3 exhibits 2.4-fold greater catalytic activity relative to its three-dimensional (3D) zeolite counterpart, Al-SSZ-70, and 2.0-fold greater activity (per catalyst mass) when compared with industrial catalyst MCM-22, for the alkylation of toluene with propylene at 523 K. The former increase is nearly equal to the observed relative increase in external surface area and acid sites upon delamination. However, at 423 K for the same reaction, UCB-3 exhibits a 3.5-fold greater catalytic activity relative to 3D Al-SSZ-70. The higher relative rate enhancement for the delaminated material at lower temperature can be elucidated on the basis of increased contributions from internal acid sites. Evidence of possible contributions from such acid sites is obtained by performing catalysis after silanation treatment, which demonstrates that although virtually all catalysis in MCM-22 occurs on the external surface, catalysis also occurs on internal sites for 3D Al-SSZ-70. The additional observed enhancement at low temperatures can therefore be rationalized by greater access to internal active sites as a result of sheet breakage during delamination. Such breakage leads to shorter characteristic internal diffusion paths and was visualized using TEM comparisons of UCB-3 and 3D Al-SSZ-70.

  4. Effects of tensile and compressive in-plane stress fields on adhesion in laser induced delamination experiments

    NARCIS (Netherlands)

    Fedorov, A.; Vellinga, W. P.; De Hosson, J. Th. M.

    2008-01-01

    In this work, the adhesion of a polymer coating on steel substrate subjected to uniaxial tensile plastic deformations was studied with the laser induced delamination technique. A decrease in the practical work of adhesion has been measured as the deformation of the substrate progressed. Moreover, it

  5. Effect of graded interlayer on the mode I edge delamination by residual stresses in multilayer coating-based systems

    Science.gov (United States)

    Zhang, X. C.; Xu, B. S.; Wang, H. D.; Wu, Y. X.

    2008-01-01

    The mode I edge delamination could be initiated due to the presence of the interfacial peeling stresses near the edges of the multilayered systems due to the material mismatches between the adjacent layers. However, the exact peeling stress distributions could not be obtained by using the existing analytical and numerical models. It was proposed recently that the peeling moment resulting from the localized peeling stresses could be used to characterize mode I edge delamination. In this paper, the effect of the graded interlayer on the mode I edge delamination by thermal residual stresses in multilayer coating-based systems was investigated. Following the previous analysis approaches, the exact closed-form solutions for the peeling moments at individual interfaces and the curvatures for bilayer system, typical thermal barrier coating (TBC) system and TBC-based system with a graded interlayer inserted between the metallic layer and the ceramic layer were, respectively, derived. Case studies showed that the edge delamination by thermal stress could be impeded by properly selecting the coating materials and individual layer thicknesses. These studies may provide some important insights for developing fail-safe designing methodologies for multilayered systems.

  6. Surface modified MXene Ti3C2 multilayers by aryl diazonium salts leading to large-scale delamination

    Science.gov (United States)

    Wang, Hongbing; Zhang, Jianfeng; Wu, Yuping; Huang, Huajie; Li, Gaiye; Zhang, Xin; Wang, Zhuyin

    2016-10-01

    Herein we report a simple and facile method to delaminate MXene Ti3C2 multilayers by the assistance of surface modification using aryl diazonium salts. The basic strategy involved the preparation of layered MAX Ti3AlC2 and the exfoliation of Ti3AlC2 into Ti3C2 multilayers, followed by Na+ intercalation and surface modification using sulfanilic acid diazonium salts. The resulting chemically grafted Ti3C2 flakes were characterized by Fourier transform infrared (FT-IR) spectroscopy and X-ray photoelectron spectroscopy (XPS) to confirm the presence of the surface organic species. Ultraviolet-visible spectroscopy revealed that surface-modified MXene Ti3C2 sheets disperse well in water and the solutions obey Lambert-Beer's law. Scanning electron microscopy (SEM), transmission electron microscopy (TEM) and X-ray diffraction (XRD) were used to demonstrate the morphology and structure of delaminating MXene Ti3C2 flakes. The results indicated that chemical modification for MXene multilayers by aryl diazonium salts induced swelling that conversely weakened the bonds between MX layers, hence leading to large-scale delamination of multilayered MXene Ti3C2via mild sonication. Advantages of the present approach rely not only on the simplicity and efficiency of the delamination procedure but also on the grafting of aryl groups to MXene surfaces, highly suitable for further applications of the newly discovered two-dimensional materials.

  7. Environmental crack-growth behavior of high strength pressure vessel alloys

    Science.gov (United States)

    Forman, R. G.

    1975-01-01

    Results of sustained-load environmental crack growth threshold tests performed on six spacecraft pressure vessel alloys are presented. The alloys were Inconel 718, 6Al-4V titanium, A-286 steel, AM-350 stainless steel, cryoformed AISI 301 stainless steel; and cryoformed AISI 304L steel. The test environments for the program were air, pressurized gases of hydrogen, oxygen, nitrogen, and carbon dioxide, and liquid environments of distilled water, sea water, nitrogen tetroxide, hydrazine, aerozine 50, monomethyl hydrazine, and hydrogen peroxide. Surface flaw type specimens were used with flaws located in both base metal and weld metal.

  8. Correlation of Gab2 and IRX2 expression with cell growth and migration behavior in osteosarcoma tissues

    Institute of Scientific and Technical Information of China (English)

    Xue-Jun Zhou

    2016-01-01

    Objective:To study the correlation of Gab2 and IRX2 expression with cell growth and migration behavior in osteosarcoma tissues.Methods:A total of 29 cases of osteosarcoma tissues and 22 cases of osteoid osteoma tissues surgically removed in our hospital between May 2012 and December 2015 were selected as the test specimens, RNA was extracted to determine the mRNA expression ofGab2 andIRX2 as well as cell growth- and migration-related genes, and protein was extracted to determine the protein expression of Gab2 and IRX2 as well as cell growth- and migration-related genes.Results:Gab2 and IRX2 mRNA content and protein content in osteosarcoma tissues were significantly higher than those in osteoid osteoma tissues; TAp73, Beclin1 and Caspase-1 mRNA content and protein content in osteosarcoma tissues were significantly lower than those in osteoid osteoma tissues and negatively correlated with Gab2 and IRX2 mRNA content and protein content while STMN1 and Survivin mRNA content and protein content were significantly higher than those in osteoid osteoma tissues and positively correlated with Gab2, IRX2, CEACAM6, CD44v6 and MMP-9 mRNA content and protein content.Conclusions:Highly expressed Gab2 and IRX2 in osteosarcoma tissue can inhibit the expression of proto-oncogenes and increase the expression of proliferation and migration genes to promote the cell growth and migration in osteosarcoma tissue.

  9. Termovision and electricity capacitance measurements as a evaluation of a helicopter rotor’s blades delamination

    Directory of Open Access Journals (Sweden)

    Gębura Andrzej

    2015-12-01

    Full Text Available The article presents essential elements reached during investigations of heat section of rotor blades which have been done in AFIT. The investigations were related to a valuation of helicopter’s rotor blades delamination. They used a method of thermal field measurement as well as a electricity capacitance between an airframe and a heat element of the installation. A suggestion of such measurements appeared during the disassembly of rotor blade heat sections when some local unglue of heat element’s tape from the structure of blade’s heating pack has seen. Spots nearby separation of adhesive are a potential area of a local temperature increase, both the electric heating element and the mechanical structure of the blade. This is especially dangerous for composite structures. Overheated composite structures characterized by reduced flexibility and becomes prone to cracking. Therefore, the possibility of non-invasive monitoring adhesive spots, without removing the blades would be particularly useful.

  10. ``The Princess and the Pea'' at the Nanoscale: Wrinkling and Delamination of Graphene on Nanoparticles

    Science.gov (United States)

    Yamamoto, Mahito; Pierre-Louis, Olivier; Huang, Jia; Fuhrer, Michael S.; Einstein, Theodore L.; Cullen, William G.

    2012-10-01

    Thin membranes exhibit complex responses to external forces or geometrical constraints. A familiar example is the wrinkling, exhibited by human skin, plant leaves, and fabrics, that results from the relative ease of bending versus stretching. Here, we study the wrinkling of graphene, the thinnest and stiffest known membrane, deposited on a silica substrate decorated with silica nanoparticles. At small nanoparticle density, monolayer graphene adheres to the substrate, detached only in small regions around the nanoparticles. With increasing nanoparticle density, we observe the formation of wrinkles which connect nanoparticles. Above a critical nanoparticle density, the wrinkles form a percolating network through the sample. As the graphene membrane is made thicker, global delamination from the substrate is observed. The observations can be well understood within a continuum-elastic model and have important implications for strain-engineering the electronic properties of graphene.

  11. Interlaminar fracture toughness of composites. II - Refinement of the edge delamination test and application to thermoplastics

    Science.gov (United States)

    Johnston, N. J.; Obrien, T. K.; Morris, D. H.; Simonds, R. A.

    1983-01-01

    The mixed mode interlaminar fracture toughness, G(c), is obtained for the two thermoplastic matrices UDEL P1700 polysulfone and ULTEM polyetherimide by means of edge delamination tensile (EDT) tests on unnotched, eleven-ply graphite fiber reinforced composite specimens. A novel method is used to obtain the stiffness parameter employed in the closed form equation for the calculation of G(c), decreasing the number of stiffness measurements required and simplifying the calculations. The G(Ic) values from double cantilever beam (DCB) measurements on composites of the two thermoplastics were similar to each other, but slightly higher than the G(c) data obtained by EDT. Interfacial resin/fiber failures predominated in both the EDT and DCB tests.

  12. Delamination on GFRP laminates impacted at room and lower temperatures: Comparison between epoxy and vinylester resins

    Science.gov (United States)

    Lopresto, Valentina; Langella, Antonio; Papa, Ilaria

    2016-10-01

    Low velocity impact tests at three different impact energy values and three different temperatures, were performed on glass fibre composite laminates made by infusion technology. Two different resins, epoxy and vinylester, were considered to impregnate the fibres: the first is mainly of aeronautical interest whereas the second one is mainly applied in Naval field. The specimens were first completely destroyed to obtain the complete load-displacement curve. The latter allowed the evaluation of the increasing impact energies, 5, 10 and 20J, used to investigate about the start and propagation of the damage inside the laminates. The delamination was investigated by the very commonly used Ultra Sound technique and the results obtained on the different materials at different temperatures were compared. A general better behaviour of vinylester resin was noted.

  13. Estimating Parameters of Delaminations in GRP Pipes Using Thermal NDE and ANN

    Science.gov (United States)

    Vijayaraghavan, G. K.; Majumder, M. C.; Ramachandran, K. P.; Muruganandam, A.; Govindarajan, L.

    2010-10-01

    Thermographic Non-Destructive Evaluation (TNDE) is one of the techniques that have been widely used over the decades to evaluate the integrity of structures. To meet the increased demand for robust and effective inspection in complex TNDE tasks, Artificial Neural Networks (ANNs) have been recently deployed in many problems. The aim of the paper is to adopt an inverse technique using ANNs in the field of TNDE to estimate various parameters of delamination in Glass Reinforced Polymer (GRP) pipes by supplying thermal contrast evolution data as input. A Radial Basis Network (RBN) is employed with 80 input and 3 output neurons. The estimation capability of the network was evaluated with the data obtained from numerical simulations. The overall absolute errors show that the estimation capability of ANN is good.

  14. Micro-scale delaminating and buckling of thin film on soft substrate

    Science.gov (United States)

    Wu, Dan; Xie, Huimin; Yin, Yajun; Tang, Minjin

    2013-03-01

    In this paper, a simple process is suggested to estimate the interfacial toughness of the material system ‘aluminum film/soft PDMS substrate’. The specimen, i.e. the aluminum film deposited on the soft polydimethylsiloxane (PDMS) substrate, is subject to a tensile load, and delaminating and buckling of aluminum film are observed in the perpendicular direction to the tensile strain. With the aid of the buckling blisters, the interfacial toughness of the material system is estimated. Large deformation is considered during the buckling of the thin film, and the interfacial toughness is deduced from a fracture theory. Besides, the evolution from one single blister to three blisters and then four blisters is observed in situ under microscope. This simplified method has potential applications to flexible electronics in which interfacial toughness of the metal film/soft substrate must be well controlled.

  15. Stability Loss and Buckling Delamination Three-Dimensional Linearized Approach for Elastic and Viscoelastic Composites

    CERN Document Server

    Akbarov, Surkay

    2013-01-01

    This book investigates stability loss and buckling delamination problems of the viscoelastic composite materials and structural members made from these materials within the framework of the Three-Dimensional Linearized Theory of Stability (TDLTS). The investigation of stability loss problems is based on the study of an evolution of the initial infinitesimal imperfection in the structure of the material or of the structural members with time (for viscoelastic composites) or with external compressing forces (for elastic composites). This study is made within the scope of the Three-Dimensional Geometrically Non-Linear Theory of the Deformable Solid Body Mechanics. The solution to the corresponding boundary-value problems is presented in the series form in a small parameter which characterizes the degree of the initial imperfection. The boundary form perturbation technique is employed and nonlinear problems for the domains bounded by noncanonical surfaces are reduced to the same nonlinear problem for the correspo...

  16. Irradiation and annealing effects on delamination toughness in carbon/epoxy composite

    Energy Technology Data Exchange (ETDEWEB)

    Sekulic, D.R. [Institute of Nuclear Sciences, Vinca, POB 522, 11000 Belgrade, Serbia (Serbia )], E-mail: pesikan@vin.bg.ac.yu; Gordic, M.V. [General High School Milutin Milankovic, 11000 Belgrade (Serbia); Djordjevic, I.M. [Institute of Nuclear Sciences, Vinca, POB 522, 11000 Belgrade (Serbia); Petrovic, Z.S. [Kansas Polymer Research Center, Pittsburgh State University (United States); Stevanovic, M.M. [Institute of Nuclear Sciences, Vinca, POB 522, 11000 Belgrade (Serbia)

    2009-01-01

    Gamma irradiation to various doses (4.8-27.2 MGy) was performed on unidirectional carbon fiber/epoxy resin composite plates. Unidirectional composite coupons irradiated to various doses were annealed at 180 and 250 deg. C, in vacuum. The strain energy release rate G{sub IC}, as a measure of delamination fracture toughness, was determined by Mode I fracture testing on double cantilever beam coupons. The glass transition temperature (T{sub g}) of the tested coupons matrices was determined in DMA tests. The effects of irradiation and annealing on G{sub IC} values - the mean values of 10 propagation points (G{sub IC,mean}) and that of fracture initiation (G{sub IC,init}) - were established. These values were analyzed as a function of irradiation dose and annealing temperatures, having in mind glass transition temperature values changes, as well as the possible mechanisms and phenomena of irradiation and annealing.

  17. Which Diet-Related Behaviors in Childhood Influence a Healthier Dietary Pattern? From the Ewha Birth and Growth Cohort

    Science.gov (United States)

    Lee, Hye Ah; Hwang, Hyo Jeong; Oh, Se Young; Park, Eun Ae; Cho, Su Jin; Kim, Hae Soon; Park, Hyesook

    2016-01-01

    This study was performed to examine how childhood dietary patterns change over the short term and which changes in diet-related behaviors influence later changes in individual dietary patterns. Using food frequency questionnaire data obtained from children at 7 and 9 years of age from the Ewha Birth and Growth Cohort, we examined dietary patterns by principal component analysis. We calculated the individual changes in dietary pattern scores. Changes in dietary habits such as eating a variety of food over two years were defined as “increased”, “stable”, or “decreased”. The dietary patterns, termed “healthy intake”, “animal food intake”, and “snack intake”, were similar at 7 and 9 years of age. These patterns explained 32.3% and 39.1% of total variation at the ages of 7 and 9 years, respectively. The tracking coefficient of snack intake had the highest coefficient (γ = 0.53) and that of animal food intake had the lowest (γ = 0.21). Intra-individual stability in dietary habits ranged from 0.23 to 0.47, based on the sex-adjusted weighted kappa values. Of the various behavioral factors, eating breakfast every day was most common in the “stable” group (83.1%), whereas consuming milk or dairy products every day was the least common (49.0%). Moreover, changes in behavior that improved the consumption of milk or dairy products or encouraged the consumption of vegetables with every meal had favorable effects on changes in healthy dietary pattern scores over two years. However, those with worsened habits, such as less food variety and more than two portions of fried or stir-fried food every week, had unfavorable effects on changes in healthy dietary pattern scores. Our results suggest that diet-related behaviors can change, even over a short period, and these changes can affect changes in dietary pattern. PMID:28025537

  18. Effects of seed orientation on the growth behavior of single grain REBCO bulk superconductors

    Energy Technology Data Exchange (ETDEWEB)

    Lee, Hee Gyoun [Korea Polytechnic University, Siheung (Korea, Republic of)

    2017-06-15

    This study presents a simple method to control the seed orientation which leads to the various growth characteristics of a single grain REBCO (RE: rare-earth elements) bulk superconductors. Seed orientation was varied systematically from c-axis to a-axis with every 30 degree rotation around b-axis. Orientations of a REBCO single grain was successfully controlled by placing the seed with various angles on the prismatic indent prepared on the surface of REBCO powder compacts. Growth pattern was changed from cubic to rectangular when the seed orientation normal to compact surface was varied from c-axis to a-axis. Macroscopic shape change has been explained by the variation of the wetting angle of un-reacted melt depending on the interface energy between YBa2Cu3O7-y (Y123) grain and melt. Higher magnetic levitation force was obtained for the specimen prepared using tilted seed with an angle of 30 degree rotation around b-axis.

  19. Fatigue Crack Growth Rate Behavior of Type 347 Stainless Steel in Simulated PWR Water Environment

    Energy Technology Data Exchange (ETDEWEB)

    Min, Ki Deuk; Kim, Seon Jin [Hanyang University, Seoul (Korea, Republic of); Kim, Dae Whan; Lee, Bong Sang [Korea Atomic Energy Research Institute, Daejeon (Korea, Republic of)

    2012-05-15

    The pressurizer surge line of a Korean standard nuclear power plane uses Nb stabilized type 347 stainless steel. The pressurizer surge line is the pipe connecting the pressurizer and the hot leg line, and the path controlling the pressure and temperature of the cooling system of the nuclear reactor, operated at 316 .deg. C and in a 150atm. The pressurizer surge line operated at high temperature and high pressure receives thermal stress by a temperature change and mechanical stress by a pressure change at the same time, and by being exposed to the high temperature and high pressure cooling water environment of a nuclear power plant, environmental fatigue by stress and corrosion is the main damage instrument. As the effect of environmental fatigue has been reported, through low cycle fatigue, fatigue life evaluations of austenite stainless steel have been conducted, but evaluations of fatigue crack growth rate to evaluate the soundness are very poor. In this study, evaluated characteristics of fatigue crack growth rate base on a change of dissolved oxygen in a PWR environment

  20. Molecular genetic investigations of root gravitropism and other complex growth behaviors using Arabidopsis and Brachypodium as models

    Science.gov (United States)

    Masson, Patrick; Barker, Richard; Miller, Nathan; Su, Shih-Hao; Su, Shih-Heng

    2016-07-01

    When growing on hard surfaces, Arabidopsis roots tend to grown downward, as dictated by positive gravitropism. At the same time, surface-derived stimuli promote a wavy pattern of growth that is superimposed to a rightward root-skewing trend. This behavior is believed to facilitate obstacle avoidance in soil. To better understand these complex behaviors, we have isolated and characterized mutations that affect them. Some of these mutations were shown to affect gravitropism whereas others did not. Within the latter group, most of the mutations affected mechanisms that control anisotropic cell expansion. We have also characterized mutations that affect early steps of gravity signal transduction within the gravity-sensing columella cells of the root cap. Upon reorientation within the gravity field, starch-filled plastids sediment to the bottom-side of these cells, triggering a pathway that leads to re-localization of auxin efflux facilitators to the bottom membrane. Lateral auxin transport toward the bottom flank ensues, leading to gravitropic curvature. Several of the mutations we characterized affect genes that encode proteins associated with the vesicle trafficking pathway needed for this cell polarization. Other mutations were shown to affect components of the plastid outer envelope protein import complex (TOC). Their functional analysis suggests an active role for plastids in gravity signal transduction, beyond a simple contribution as sedimenting gravity susceptors. Because most cultivated crops are monocots, not dicots like Arabidopsis, we have also initiated studies of root-growth behavior with Brachypodium distachyon. When responding to a gravistimulus, the roots of Brachypodium seedlings develop a strong downward curvature that proceeds until the tip reaches a ~50-degree curvature. At that time, an oscillatory tip movement occurs while the root continues its downward reorientation. These root-tip oscillations also occur if roots are allowed to simply grow

  1. Crack Initiation and Growth Behavior of Cold-Sprayed Ni Particles on IN718 Alloy

    Science.gov (United States)

    Cavaliere, P.; Silvello, A.

    2017-03-01

    Cold spray processing parameters, governing particle velocity and impact energy, are analyzed in the present paper for pure Ni sprayed on IN718 substrates. Finite element modeling (FEM) was used to calculate the particle impact velocity and temperature as a function of gas temperature and pressure and particle density and dimensions. Experimental evidence underlines the possibility of performing repairing through cold spray thanks to the good level of adhesion achievable by employing optimal combinations of materials and spray processing parameters. In the present paper, the potential repairing of cracked superalloys sheets, by employing cold spray technology, is presented. 30° surface V-notched IN718 panels have been repaired by using pure Ni cold-sprayed powders. The bending behavior of the repaired sheets was analyzed by FEM and mechanical testing in order to compare the properties with those belonging to the unrepaired panels. Simulations and mechanical results showed a reduction in the stress intensity factor, a modification of the crack initiation site and a crack retardation in the repaired structures if compared with the unrepaired ones. The K factor was quantified; the resistance of repaired panels was increased of more than eight times in the case of repairing with Ni cold spray particles. Geometrical and mechanical properties of the coating-substrate interfaces, such as adhesion strength and residual stresses influencing the coatings behavior, were largely analyzed.

  2. Air-coupled guided wave detection and wavenumber filtering to full-field representation of delamination in composite plates

    Science.gov (United States)

    Testoni, N.; De Marchi, L.; Marzani, A.

    2014-03-01

    Delamination faults in composite plates are considered dangerous as they can cause catastrophic failure before being visually assessed. Effects of delaminations are particularly relevant in guided waves scattering, local resonances and mode conversion. Detecting and analyzing these phenomena is relevant for plate characterization. In this work, leaky guided waves are used to detect delamination in composite plates. To such purpose, a hybrid ultrasonic set-up and a dedicated signal processing are proposed. An air-probe with a proper lift-off is used to detect the leakage in terms of air pressure wave over the plate surface. A piezoelectric transducer is used to generate acoustic guided waves in the composite plate. Multiple acquisitions are averaged to increase the SNR for each position of the air-probe. Curvelet Transform (CT) domain processing of the projection coefficients of the acquired elastic wave is exploited to decompose waves that are overlapped both in the time/space and in the frequency/wavenumber domain. In fact, CT is a special member of the family of multiscale and multidimensional transforms whose spatial and temporal localization is very well suited for processing signals which are sparse in the above mentioned domains. In this work this sparsity is exploited to emphasize the information of leaky guided waves scattered by the delamination by removing from the data the information related to the incident wave field. As an application, the presence of a delamination generated by a 21 Joule impact performed on a 4.9 mm thickness composite laminate was detected contactless by exploiting guided wave leakage.

  3. Removal of SU-8 photoresist using buckling-driven delamination assisted with a carbon dioxide snow jet for microfluidics fabrication

    Science.gov (United States)

    Yang, Sheng-Chung; Lin, Yu-Cheng

    2007-12-01

    A new, environmentally friendly, inexpensive and non-destructive method for removing SU-8 after being an electroplating mold in microfluidic fabrication is demonstrated in this paper. A controllable thermal delaminating method assisted by an efficient high-speed aerosol jet consisting of two major steps, delamination followed by removal by lifting, is presented. Experiments with the thermal process, operated at a rising temperature ΔT of 340 °C for 30 min, were carried out. Four delaminations were observed and the critical buckling stresses were calculated to be 38.98, 35.24, 42.04 and 41.26 MPa, respectively. The results show that these delaminations occurred at a rising temperature ΔT of 290, 260.5, 314.7 and 308.5 °C, respectively. The morphology of the thermal buckling-driven delamination was edge initiated and straight sided. The effects of the carbon dioxide (CO2) snow jet at a distance of 10 mm from the nozzle exit as well as the lift force Fdp, drag force Fd and impact force Fi were determined to be 79 × 10-3 N, 0.625 × 10-3 N and (1.65-4.95) × 10-3 N, respectively. Based on the analysis of the lift, drag and impact forces, the lifting force dominates the effects of the CO2 snow jet and is tens of times larger than the others. The experiments and analyses showed that the best distance for the CO2 snow jet to the nozzle exit was 6-10 mm.

  4. The growth and tensile deformation behavior of the silver solid solution phase with zinc

    Energy Technology Data Exchange (ETDEWEB)

    Wu, Jiaqi, E-mail: jiaqw10@uci.edu [Department of Electrical Engineering and Computer Science, University of California, Irvine, CA 92697-2660 (United States); Materials and Manufacturing Technology, University of California, Irvine, CA 92697-2660 (United States); Lee, Chin C. [Department of Electrical Engineering and Computer Science, University of California, Irvine, CA 92697-2660 (United States); Materials and Manufacturing Technology, University of California, Irvine, CA 92697-2660 (United States)

    2016-06-21

    The growth of homogeneous silver solid solution phase with zinc are conducted at two different compositions. X-ray diffraction (XRD) and Scanning electron microscope/Energy dispersive X-ray spectroscopy (SEM/EDX) are carried out for phase identification and chemical composition verification. The mechanical properties of silver solid solution phase with zinc are evaluated by tensile test. The engineering and true stress vs. strain curves are presented and analyzed, with those of pure silver in comparison. According to the experimental results, silver solid solution phase with zinc at both compositions show tempered yield strength, high tensile strength and large uniform strain compared to those of pure silver. Fractography further confirmed the superior ductility of silver solid solution phase with zinc at both compositions. Our preliminary but encouraging results may pave the way for the silver based alloys to be applied in industries such as electronic packaging and structure engineering.

  5. Removal of snow cover inhibits spring growth of Arctic ice algae through physiological and behavioral effects

    DEFF Research Database (Denmark)

    Lund-Hansen, L.C.; Hawes, Ian; Sorrell, Brian Keith

    2014-01-01

    The snow cover of Arctic sea ice has recently decreased, and climate models forecast that this will continue and even increase in future. We therefore tested the effect of snow cover on the optical properties of sea ice and the biomass, photobiology, and species composition of sea ice algae...... at Kangerlussuaq, West Greenland, during March 2011, using a snow-clearance experiment. Sea ice algae in areas cleared of snow was compared with control areas, using imaging variable fluorescence of photosystem II in intact, unthawed ice sections. The study coincided with the onset of spring growth of ice algae......) and filling of brine channels with fluorescing cells. In contrast, in the minus snow area, PAR transmittance increased sixfold and there was an exponential decrease in chl-a and no increase in F o, and the area of fluorescing biomass declined to become undetectable. This study suggests that the onset...

  6. Allelopathic effects of Lantana camara on germination and growth behavior of some agricultural crops in Bangladesh

    Institute of Scientific and Technical Information of China (English)

    Romel Ahmed; Mohammad Belal Uddin; Mohammed Abu Sayed Arfin Khan; Sharif Ahmed Mukul; Mohammed Kamal Hossain

    2007-01-01

    An experiment was conducted to understand the growth inhibitory effects of aqueous extracts derived from Lantana camara L. (a globally recognized invasive alien weed) on six popular agricultural crops of Bangladesh. The test was conducted in sterilized petridishes with a photoperiod of 24 hours and an average temperature of 29℃. The effect of different concentrations of L. Camara leaf extracts were recorded and compared with control (I.e., distil water). Result showed different concentrations of aqueous leaf extracts caused significant inhibitory effect on gemination, root and shoot elongation and development of lateral roots of receptor crops. Bioassays also indicated that the inhibitory effect was proportional to the concentrations of the extracts and higher concentration had the stronger inhibitory effect whereas the lower concentration showed stimulatory effect in some cases. The inhibitory effect was much pronounced in root and lateral root development rather than shoot and germination.

  7. The Time Delays’ Effects on the Qualitative Behavior of an Economic Growth Model

    Directory of Open Access Journals (Sweden)

    Carlo Bianca

    2013-01-01

    Full Text Available A further generalization of an economic growth model is the main topic of this paper. The paper specifically analyzes the effects on the asymptotic dynamics of the Solow model when two time delays are inserted: the time employed in order that the capital is used for production and the necessary time so that the capital is depreciated. The existence of a unique nontrivial positive steady state of the generalized model is proved and sufficient conditions for the asymptotic stability are established. Moreover, the existence of a Hopf bifurcation is proved and, by using the normal form theory and center manifold argument, the explicit formulas which determine the stability, direction, and period of bifurcating periodic solutions are obtained. Finally, numerical simulations are performed for supporting the analytical results.

  8. Kinetic study and growth behavior of template-based electrodeposited platinum nanotubes controlled by overpotential

    Energy Technology Data Exchange (ETDEWEB)

    Yousefi, E. [Department of Materials Science and Engineering, Sharif University of Technology, Azadi Ave., P.O.Box 11155-9466, Tehran (Iran, Islamic Republic of); Dolati, A., E-mail: dolati@sharif.edu [Department of Materials Science and Engineering, Sharif University of Technology, Azadi Ave., P.O.Box 11155-9466, Tehran (Iran, Islamic Republic of); Imanieh, I. [Department of Materials Science and Engineering, Sharif University of Technology, Azadi Ave., P.O.Box 11155-9466, Tehran (Iran, Islamic Republic of); Yashiro, H.; Kure-Chu, S.-Z. [Department of Chemistry and Bioengineering, Faculty of Engineering, Iwate University, 4-3-5 Ueda, Morioka, Iwate, 020-8551 (Japan)

    2017-02-01

    Platinum nanotubes (PtNTs) are fabricated by potentiostatic electrodeposition at various overpotentials (−200 up to −400 mV versus SCE) in polycarbonate templates (PCTs) with pore diameter of 200 nm in a solution containing 5 mM H{sub 2}PtCl{sub 6} and 0.1 M H{sub 2}SO{sub 4}. The synthesized PtNTs are characterized by field emission scanning electron microscopy (FE-SEM), and transmission electron microscopy (TEM). The electrochemical growth mechanism within nanoscopic pores and the relationship between morphological variations and kinetic parameters are investigated for the first time. It is shown that more porous structure of nanotubes forms at high overpotentials possibly due to preferably nucleation. The kinetics of electrodeposition process is studied by electrochemical techniques such as voltammetry and chronoamperometry. The linear diffusion coefficient at the early stage of the deposition and the radial diffusion coefficients at steady state regime are calculated as D = 8.39 × 10{sup −5} and 2.33–13.26 × 10{sup −8} cm{sup 2}/s, respectively. The synthesized PtNT electrode is tested as electrocatalyst for hydrogen peroxide oxidation in phosphate buffer solution (PBS) and shows a sensitivity as high as 2.89 mA per 1 μM that is an indication to its enlarged electrochemical surface area. - Highlights: • PtNT is electrodeposited in a 3-aminopropyltrimethoxysilane-modified PCT. • The electrochemical growth mechanism within nanoscopic pores is discussed. • The kinetics of PtNT electrodeposition is studied based on models for UME arrays. • Relationship between morphological variations vs. kinetic parameters is studied.

  9. Malnutrition during brain growth spurt alters the effect of fluoxetine on aggressive behavior in adult rats.

    Science.gov (United States)

    Barreto-Medeiros, J M; Feitoza, E G; Magalhaes, K; Cabral-Filho, J E; Manhaes-De-Castro, F M; De-Castro, C M; Manhaes-De-Castro, R

    2004-02-01

    Malnutrition effect during the suckling period on aggressive behavior was investigated in adult rats treated and not treated with fluoxetine, a selective serotonin reuptake inhibitor. Sixty-four Wistar male rats were allocated in two groups, according to their mothers' diet during lactation. The well-nourished group was fed by mothers receiving a 23% protein diet; the malnourished one by mothers receiving a 8% protein diet. Following weaning, all rats received the 23% protein diet. On the 90th day after birth, each nutritional group was divided into two subgroups, one receiving a single daily injection of fluoxetine (10 mg/kg) and the other of a saline solution (0.9% NaCl) for 14 days. Treatment with Fluoxetine reduced aggressive response in well-nourished but not in malnourished rats. These findings suggest that the serotoninergic system was affected by malnutrition during the critical period of brain development, and persisted even after a long period of nutritional recovery.

  10. Growth of hierarchical based ZnO micro/nanostructured films and their tunable wettability behavior

    Science.gov (United States)

    Suresh Kumar, P.; Dhayal Raj, A.; Mangalaraj, D.; Nataraj, D.; Ponpandian, N.; Li, Lin; Chabrol, G.

    2011-05-01

    Hierarchical zinc oxide (ZnO) micro/nanostructured thin films were grown onto as-prepared and different annealed ZnO seed layer films by a simple two step chemical process. A cost effective successive ionic layer adsorption and reaction (SILAR) method was employed to grow the seed layer films at optimal temperature (80 °C) and secondly, different hierarchical based ZnO structured thin films were deposited over the seed layered films by chemical bath deposition (CBD). The influence of seed layer on the structural, surface morphological, optical and wettability behavior of the ZnO thin films were systematically investigated. The XRD analysis confirms the high crystalline nature of both the seed layer and corresponding ZnO micro/nanostructured films with a perfect hexagonal structure oriented along (0 0 2) direction. The surface morphology revels a complex and orientated hierarchical based ZnO structured films with diverse shapes from plates to hexagonal rod-like crystal to tube-like structure and even much more complex needle-like shapes during secondary nucleation, by changing the seed layer conditions. The water contact angle (WCA) measurements on hierarchical ZnO structured films are completely examined to study its surface wettability behavior for its suitability in future self-cleaning application. Photoluminescence (PL) spectra of the ZnO structured film exhibit UV and visible emissions in the range of 420-500 nm. The present approach demonstrates its potential for low-temperature, large-scale, controlled synthesis of crystalline hierarchical ZnO nanostructures films.

  11. Kinetic Behaviors of a Competitive Population and Fitness System in Exchange-Driven Growth

    Institute of Scientific and Technical Information of China (English)

    LU Ke; LIN Zhen-Quan; SUN Yun-Fei

    2008-01-01

    We proposed an aggregation model of two species aggregates of fitness and population to study the inter-action between the two species in their exchange-driven processes of the same species by introducing the monomer birth of fitness catalyzed by the population,where the fitness aggregates perform self-death process and the population aggre-gates perform self-birth process.The kinetic behaviors of the aggregate size distributions of the fitness and population were analyzed by the rate equation approach with their exchange rate kernel K1(k,j) = K1kj and K2(k,j) = K2kj,the fitness aggregate's self-death rate kernel J1(k) = J1k,population aggregate's self-birth rate kernel J2(k) = J2k and population-catalyzed fitness birth rate kernel I(k,j) = Ikjv.The kinetic behavior of the fitness was found depending crucially on the parameter v,which reflects the dependence of the population-catalyzed fitness birth rate on the size of the catalyst (population) aggregate.(I) In the v ≤0 case,the effect of catalyzed-birth of fitness is rather weak and the exchange-driven aggregation and self-death of the fitness dominate the process,and the fitness aggregate size distribution ak(t) does not have scale form.(ii) When v > 0,the effect of the population-catalyzed birth of fitness gets strong enough,and the catalyzed-birth and self-death of the fitness aggregates,together with the self-birth of the population aggregates dominate the evolution process of the fitness aggregates.The aggregate size distribution ak(t)approaches a generalized sealing form.

  12. [Changes in ingestive behavior during growth affects the functional maturation of temporomandibular joint nociceptive neurons of rats].

    Science.gov (United States)

    Hiranuma, Maya

    2013-03-01

    Temporomandibular joint (TMJ) loading during development promotes its growth and maintains normal structure/function. Continuous change in diet consistency is related to development and maturation of the peripheral nervous system, including the nociceptive system. However, the functional modulation of TMJ-nociceptive neurons under different ingestive behavior is unclear. We fed growing rats a liquid diet to investigate the effects of low TMJ loading on the response properties of neurons in the trigeminal spinal tract subnucleus caudalis (Sp5C). Forty 2-week-old male rats were used. They were fed chow pellets (n = 20, C group) or a liquid diet (n = 20, LD group) soon after weaning. Firing activities of single sensory units in response to TMJ pressure stimuli were recorded at 4, 5, 7 and 9 weeks. In TMJ-nociceptive neurons, the firing threshold (FT) in the LD group was significantly lower than that in the C group at each recording age. The FT in the C group remained unchanged throughout the recording period, whereas that in the LD group was the highest at 4 weeks, and gradually decreased. On the other hand, the initial firing frequency (IFF) was significantly higher in the LD group than in the C group at each recording age. The IFF in the C group remained unchanged throughout the experimental period, whereas that in the LD group was at its lowest at 4 weeks, and gradually increased. Based on these findings, ingestive behavior that results from continuous changes in the physical consistency of the diet during growth may affect the functional maturation of TMJ-nociceptive neurons.

  13. How domain growth is implemented determines the long-term behavior of a cell population through its effect on spatial correlations

    Science.gov (United States)

    Ross, Robert J. H.; Baker, R. E.; Yates, C. A.

    2016-07-01

    Domain growth plays an important role in many biological systems, and so the inclusion of domain growth in models of these biological systems is important to understanding how these systems function. In this work we present methods to include the effects of domain growth on the evolution of spatial correlations in a continuum approximation of a lattice-based model of cell motility and proliferation. We show that, depending on the way in which domain growth is implemented, different steady-state densities are predicted for an agent population. Furthermore, we demonstrate that the way in which domain growth is implemented can result in the evolution of the agent density depending on the size of the domain. Continuum approximations that ignore spatial correlations cannot capture these behaviors, while those that account for spatial correlations do. These results will be of interest to researchers in developmental biology, as they suggest that the nature of domain growth can determine the characteristics of cell populations.

  14. Grain Growth Behavior, Tensile Impact Ductility, and Weldability of Cerium-Doped Iridium Alloys

    Energy Technology Data Exchange (ETDEWEB)

    McKamey, C.G.

    2002-05-28

    An iridium alloy doped with small amounts of cerium and thorium is being developed as a potential replacement for the iridium-based DOP-26 alloy (doped with thorium only) that is currently used by the National Aeronautics and Space Administration (NASA) for cladding and post-impact containment of the radioactive fuel in radioisotope thermoelectric generator (RTG) heat sources which provide electric power for interplanetary spacecraft. This report summarizes results of studies conducted to date under the Iridium Alloy Characterization and Development subtask of the Radioisotope Power System Materials Production and Technology Program to characterize the properties of the iridium-based alloy (designated as DOP-40) containing both cerium and thorium. Included within this report are data on grain growth of sheet material in vacuum and low-pressure oxygen environments, grain growth in vacuum of the clad vent set cup material, weldability, and the effect of grain size and test temperature on tensile properties. Where applicable, data for the DOP-26 alloy are included for comparison. Both grain size and grain-boundary cohesion affect the ductility of iridium alloys. In this study it was found that cerium and thorium, when added together, refine grain size more effectively than when thorium is added by itself (especially at high temperatures). In addition, the effect of cerium additions on grain-boundary cohesion is similar to that of thorium. Mechanical testing at both low ({approx} 10{sup -3}s{sup -1}) and high ({approx} 10{sup -3}s{sup -1}) strain rates showed that the Ce/Th-doped alloys have tensile ductilities that are as good or better than the DOP-26 alloy. The general conclusion from these studies is that cerium can be used to replace some of the radioactive thorium currently used in DOP-26 while maintaining or improving its metallurgical properties. The current DOP-26 alloy meets all requirements for cladding the radioactive fuel in the RTG heat source, but the

  15. Lithium Behavior during Growth of Metasedimentary Garnets from the Cignana UHP Locality, Italy

    Science.gov (United States)

    Bebout, G. E.; Tsujimori, T.; Ota, T.; Shimaki, Y.; Kunihiro, T.; Carlson, W. D.; Nakamura, E.

    2014-12-01

    We investigated major and trace element concentrations and δ7Li in garnets in Lago di Cignana metasedimentary rocks (peak conditions ~550˚C, 2.5-3.0 GPa), following the EPMA-SIMS approach of Tsujimori et al. (2014; IMA conference abstract). Previous work on the devolatilization history of these rocks (Bebout et al., 2013; Cook-Kollars et al., 2014; both in Chemical Geology) provides a petrologic and geochemical context for this study. Lithium is of interest as a tracer of fluid-rock interactions and because of its potential to isotopically fractionate during diffusional processes. All garnets are almandine-rich with strongly decreasing MnO and increasing MgO toward rims. HREEs, Y, and Li also show strong zoning, with elevated concentrations in cores (15-50 ppm Li) and marked high-concentration anomalies (up to 117 ppm Li, 5500 ppm Y), with little or no major element shift, as growth annuli at which some garnets have elevated δ7Li. In all garnets, rutile inclusions appear abruptly at annuli and outward toward rims, accompanied by inclusions of a Ca- and LREE-rich phase and decreased Nb concentrations in garnet. These relationships appear to reflect prograde garnet-forming reaction(s) that in part involved titanite breakdown to stabilize rutile, which resulted in delivery of more abundant Y and HREEs at surfaces of growing garnets to produce growth annuli. The co-enrichment of Li and Y+REEs is attributed to their mutual incorporation via a charge-coupled substitution (Carlson et al., 2014; American Mineralogist); thus the increased Li uptake is a passive consequence of the elevated concentrations of Y+REEs. Distributions of δ7Li are complex, with most garnets showing only subtle core-to-rim variation other than at Y+REE annuli. At annuli, some garnets display elevated δ7Li (by up to 8‰), while others in the same rock do not. Small-scale fluctuations in δ7Li may correlate with abrupt shifts in major and trace element concentrations, suggesting that changes in

  16. Behavior and role of superficial oxygen in Cu for the growth of large single-crystalline graphene

    Science.gov (United States)

    Ding, Dong; Solís-Fernández, Pablo; Yunus, Rozan Mohamad; Hibino, Hiroki; Ago, Hiroki

    2017-06-01

    Decreasing the nucleation density of graphene grown on copper (Cu) foil by chemical vapor deposition (CVD) is essential for the synthesis of large-area single-crystalline graphene. Here, the behavior of the copper oxide layer and its impact on the graphene growth have been investigated. We found that a small amount of oxygen dissolves into the Cu when the oxide layer decomposes during the heating up in a non-reducing Ar environment. The remaining oxygen in the Cu foil can play an important role in decreasing the graphene nucleation density. The dissolved oxygen can withstand at high temperatures even in reducing H2 environments without completely losing its effectiveness for maintaining a low graphene nucleation density. However, heating up in a H2 environment significantly reduces the copper oxide layer during the very first moments of the process at low temperatures, preventing the oxygen to dissolve into the Cu and significantly increasing the nucleation density. These findings will help to improve the graphene growth on Cu catalyst by increasing the grain size while decreasing the grain density.

  17. In situ TEM observation of growth behavior of Kr bubbles in zirconium alloy during post-implantation annealing

    Energy Technology Data Exchange (ETDEWEB)

    Ran, Guang, E-mail: gran@xmu.edu.cn [School of Energy Research, Xiamen University, Xiamen City, Fujian Province 361005 (China); Department of Nuclear Engineering and Radiological Sciences, University of Michigan, Ann Arbor 48109 (United States); Xu, Jiangkun; Shen, Qiang; Zhang, Jian; Li, Ning [School of Energy Research, Xiamen University, Xiamen City, Fujian Province 361005 (China); Wang, Lumin, E-mail: lmwang@umich.edu [School of Energy Research, Xiamen University, Xiamen City, Fujian Province 361005 (China); Department of Nuclear Engineering and Radiological Sciences, University of Michigan, Ann Arbor 48109 (United States); Department of Materials Science and Engineering, University of Michigan, Ann Arbor 48109 (United States)

    2013-07-15

    The growth behavior of the Kr bubbles in Kr{sup +} irradiated Zr–1.1Nb–1.51Fe–0.26Cu–0.72Ni alloy was studied by in situ transmission electron microscopy. Results show that the distributions of Kr bubbles are not uniform in the zirconium alloy matrix after annealing at 700 K, 875 K, 1025 K, 1125 K and 1225 K, respectively. The Kr bubbles started to grow slowly when the sample was annealed at a temperature below 1025 K. The average sizes of the gas bubbles were observed to grow only about 0.4 nm in diameter at 700 K for 170 min and 0.9 nm at 875 K for 240 min, respectively. However, gas bubbles grew very quickly at 1225 K. The largest size of the gas bubbles is over 200 nm after 180 min annealing. The relationship between the bubble size and the annealing time was obtained at the designed annealing temperature. An empirical formula for calculating the bubble size was suggested by fitting equations derived from the experiment data. Finally, the growth mechanism of the bubbles in the zirconium alloy was discussed.

  18. Influence of the volume-contact area ratio on the growth behavior of the Cu-Sn intermetallic phase

    Science.gov (United States)

    Giddaluri, Venkatakamakshi Supraja

    Solder Joints play a very important role in electronic packaging industry by serving as mechanical support and provides integrity to the device. The increasing demand for high performance, environmental and economic feasibility and miniaturization led to the development of high density interconnects. With the reduction in the size/standoff height of the solder reliability issues in the surface mount assemblies and packaging structures under various rigorous environments are becoming significant. One of the most important impact factors that affect the solder joint reliability is the growth rate IMC formed between the solder and substrate with reduction in joint size. IMC formation is required to ensure good bonding and connectivity of the device in packaging. However excess IMC growth rate is detrimental to the device from mechanical aspects due to its brittle nature. Thus there is a need to study effect the IMC growth rate behavior with the solder joint size/standoff height. In this present study, two solder joints of different standoff heights and same composition (pure Sn solder) are used subjected to reflow process at 270°C for 1--7 min to study solid liquid interfacial reaction on joint size and the same experiment is repeated with SAC alloy of composition (96.5% Sn, 3.0% Ag, 0.5% Cu) to investigate the effect of joint size and initial copper concentration on IMC growth rate. The IMC thickness of the Sn 15microm solder joint at 1 min and 7 min is found to be 1.52microm and 2.86microm respectively while that of Sn 150microm solder joint is 1.31microm and 3.16 microm. The thickness is high in low standoff height sample at the early stage of reaction with decrease in IMC growth rate as the time of reflow increases. In case of 25microm SAC alloy solder joint the IMC thickness from 1 and 7 min is found to be 2.1microm and 3.5microm while that of 250microm SAC alloy solder joint its 1.43microm and3.235microm. Similar trend is observed but the IMC thickness is more

  19. Stick-slip behavior identified in helium cluster growth in the subsurface of tungsten: effects of cluster depth

    Science.gov (United States)

    Wang, Jinlong; Niu, Liang-Liang; Shu, Xiaolin; Zhang, Ying

    2015-10-01

    We have performed a molecular dynamics study on the growth of helium (He) clusters in the subsurface of tungsten (W) (1 0 0) at 300 K, focusing on the role of cluster depth. Irregular ‘stick-slip’ behavior exhibited during the evolution of the He cluster growth is identified, which is due to the combined effects of the continuous cluster growth and the loop punching induced pressure relief. We demonstrate that the He cluster grows via trap-mutation and loop punching mechanisms. Initially, the self-interstitial atom SIA clusters are almost always attached to the He cluster; while they are instantly emitted to the surface once a critical cluster pressure is reached. The repetition of this process results in the He cluster approaching the surface via a ‘stop-and-go’ manner and the formation of surface adatom islands (surface roughening), ultimately leading to cluster bursting and He escape. We reveal that, for the Nth loop punching event, the critical size of the He cluster to trigger loop punching and the size of the emitted SIA clusters are correspondingly increased with the increasing initial cluster depth. We tentatively attribute the observed depth effects to the lower formation energies of Frenkel pairs and the greatly reduced barriers for loop punching in the stress field of the W subsurface. In addition, some intriguing features emerge, such as the morphological transformation of the He cluster from ‘platelet-like’ to spherical, to ellipsoidal with a ‘bullet-like’ tip, and finally to a ‘bottle-like’ shape after cluster rupture.

  20. Effect of TMBi supply on low-temperature MOVPE growth behavior of GaN

    Energy Technology Data Exchange (ETDEWEB)

    Saidi, C.; Chaaben, N.; Laifi, J.; Sekrafi, T. [Unité de Recherche sur les Hétéro-Epitaxies et Applications, Faculté des Sciences de Monastir, Avenue de l’Environnement, 5019 Monastir (Tunisia); Tottereau, O. [Centre de Recherche sur l’Hétéro-Epitaxie et Ses Applications, Centre National de la Recherche Scientifique, CRHEA-CNRS, Rue Bernard Grégory, F-06560 Valbonne, Sophia Antipolis (France); Bchetnia, A.; El Jani, B. [Unité de Recherche sur les Hétéro-Epitaxies et Applications, Faculté des Sciences de Monastir, Avenue de l’Environnement, 5019 Monastir (Tunisia)

    2015-03-15

    Highlights: • We examined the Bi doping effect on GaN layers properties, grown by LT-MOVPE. • No obvious dependence of growth rate with TMBi flow rate. • TMBi flow rate addition resulted in a reduction of reflectivity oscillation mean value. • We note the appearance of islands and columns containing Bi on layers surface. • While there is a decrease in surface roughness suggesting Bi surfactant effect. - Abstract: Undoped GaN and diluted GaNBi alloys were grown on (0 0 0 1) sapphire substrate by metal–organic vapor phase epitaxy (MOVPE) at 480 °C. By using in-situ laser reflectometry, it is found that the increase of TMBi flow rate leads to a reduction of the average value of reflectivity oscillations. Scanning electron microscopy (SEM) images gave a clear observation of the TMBi increasing amount effect on the surface morphology. The appearance of different structure (islands and columns) on GaN surface could be responsible to the reduction of the reflectivity oscillations average value. The energy dispersive X-ray (EDX) analysis showed that the observed structures were only composed of Bi compared to the flat GaN surface. Moreover, the surface morphology between islands and columns is improved when we increase the TMBi flow rate. This improvement is consistent with the decrease of root mean square (RMS) roughness, as measured by atomic force microscopy (AFM)

  1. Acoustic emission studies for characterization of fatigue crack growth behavior in HSLA steel

    Science.gov (United States)

    Kumar, Jalaj; Ahmad, S.; Mukhopadhyay, C. K.; Jayakumar, T.; Kumar, Vikas

    2016-01-01

    High strength low alloy (HSLA) steels are a group of low carbon steels and used in oil and gas pipelines, automotive components, offshore structures and shipbuilding. Fatigue crack growth (FCG) characteristics of a HSLA steel have been studied at two different stress ratios (R = 0.3 and 0.5). Acoustic emission (AE) signals generated during the FCG tests have been used to understand the FCG processes. The AE signals were captured by mounting two piezoelectric sensors on compact tension specimens in liner location configuration. The AE generated in stage II of the linear Paris region of FCG has been attributed to the presence of two sub-stages with two different slopes. The AE generated at higher values of stress intensity factor is found to be useful to identify the transition from stage II to stage III of the FCG. AE location analysis has provided support for increased damage at the crack tip for higher stress ratio. The peak stress intensity (Kmax) values at the crack tip have shown good correlation with the transitions from stage IIa to stage IIb and stage II to stage III of the FCG for the two stress ratios.

  2. Microstructure vs. Near-threshold Fatigue Crack Growth Behavior of an Heat-treated Ductile Iron

    Directory of Open Access Journals (Sweden)

    Radomila KONEČNÁ

    2012-03-01

    Full Text Available Perferritic isothermal ductile iron (IDI® is an intermediate grade between the low-strength grades of austempered ductile iron (ADI and pearlitic ductile iron (DI recently developed by Zanardi Fonderie Italy. IDI is produced by heat-treating an unalloyed nodular cast iron. The specific matrix microstructure is called “Perferritic” and consists predominantly of ferrite and pearlite. Compared to the pearlitic grades of nodular ductile iron, IDI combines similar strength with higher toughness as a result of the isothermal heat treatment. In this contribution the fatigue crack growth resistance and Kath of IDI are investigated and correlated to mechanical properties and microstructural features. The threshold Ka was determined using the load shedding technique as per ASTM Standard E-647 using CT specimens extracted from a cast block. Tensile specimens were extracted from the broken CT halves and used to determine the static mechanical properties. A metallographic investigation was carried out to correlate structural features and mechanical properties.DOI: http://dx.doi.org/10.5755/j01.ms.18.1.1336

  3. Behavior of vascular endothelial growth factor and erythropoietin throughout the menstrual cycle in healthy women.

    Science.gov (United States)

    Caccamo, Chiara; Nostro, Lorena; Giorgianni, Giovanna; Mondello, Stefania; Crascì, Eleonora; Frisina, Nicola; Buemi, Michele

    2007-11-01

    To evaluate any correlations between erythropoietin (EPO) and vascular endothelial growth factor (VEGF) levels in the serum and the menstrual fluid of healthy women during the different phases of the menstrual cycle. Blood samples from 25 healthy female volunteers were obtained for serum VEGF and EPO detection on the 1st, 7th, 14th, 21st and 25th days of the menstrual cycle. Menstrual fluid samples for VEGF and EPO detection were obtained on the 1st and 4th days of menstruation. Circulating VEGF levels were found to increase in a stage-dependent cyclic manner. The mean VEGF concentration in menstrual blood on the 1st day of the cycle was significantly higher than the mean plasma value and was reduced to a significant extent on the 4th day of the cycle. We found no significant changes in serum EPO levels. Mean EPO concentration detected in menstrual blood was comparable to those in serum blood either on the 1st or 4th day of the menstrual cycle. During menstruation, a local production of VEGF occurs independent of systemic production, thus sustaining angiogenic activity in autonomous, independent ways. Our findings demonstrate the presence of an "open compartment" that reflects the systemic pattern of EPO at the uterine level that allows us to speculate on different effects beyond the angiogenic action of EPO.

  4. Intraguild predation by shore crabs affects mortality, behavior, growth, and densities of California horn snails

    Science.gov (United States)

    Lorda, J.; Hechinger, R.F.; Cooper, S. D.; Kuris, A. M.; Lafferty, Kevin D.

    2016-01-01

    The California horn snail, Cerithideopsis californica, and the shore crabs, Pachygrapsus crassipesand Hemigrapsus oregonensis, compete for epibenthic microalgae, but the crabs also eat snails. Such intraguild predation is common in nature, despite models predicting instability. Using a series of manipulations and field surveys, we examined intraguild predation from several angles, including the effects of stage-dependent predation along with direct consumptive and nonconsumptive predator effects on intraguild prey. In the laboratory, we found that crabs fed on macroalgae, snail eggs, and snails, and the size of consumed snails increased with predator crab size. In field experiments, snails grew less in the presence of crabs partially because snails behaved differently and were buried in the sediment (nonconsumptive effects). Consistent with these results, crab and snail abundances were negatively correlated in three field surveys conducted at three different spatial scales in estuaries of California, Baja California, and Baja California Sur: (1) among 61 sites spanning multiple habitat types in three estuaries, (2) among the habitats of 13 estuaries, and (3) among 34 tidal creek sites in one estuary. These results indicate that shore crabs are intraguild predators on California horn snails that affect snail populations via predation and by influencing snail behavior and performance.

  5. Mechanical properties and crack growth behavior of polycrystalline copper using molecular dynamics simulation

    Science.gov (United States)

    Qiu, Ren-Zheng; Li, Chi-Chen; Fang, Te-Hua

    2017-08-01

    This study investigated the mechanical properties and crack propagation behavior of polycrystalline copper using a molecular dynamics simulation. The effects of temperature, grain size, and crack length were evaluated in terms of atomic trajectories, slip vectors, common neighbor analysis, the material’s stress-strain diagram and Young’s modulus. The simulation results show that the grain boundary of the material is more easily damaged at high temperatures and that grain boundaries will combine at the crack tip. From the stress-strain diagram, it was observed that the maximum stress increased as the temperature decreased. In contrast, the maximum stress was reduced by increasing the temperature. With regard to the effect of the grain size, when the grain size was too small, the structure of the sample deformed due to the effect of atomic interactions, which caused the grain boundary structure to be disordered in general. However, when the grain size was larger, dislocations appeared and began to move from the tip of the crack, which led to a new dislocation phenomenon. With regards to the effect of the crack length, the tip of the crack did not affect the sample’s material when the crack length was less than 5 nm. However, when the crack length was above 7.5 nm, the grain boundary was damaged, and twinning structures and dislocations appeared on both sides of the crack tip. This is because the tip of the crack was blunt at first before sharpening due to the dislocation effect.

  6. Crack growth behavior under creep-fatigue conditions using compact and double edge notch tension-compression specimens

    Science.gov (United States)

    Narasimha Chary, Santosh Balaji

    inspection of fatigue surfaces, it has been found that that better alignment control procedures are needed to ensure symmetric crack fronts for the DEN(T-C) specimen. Creep-fatigue crack growth tests were conducted on 9Cr-1Mo (P91) steels at 625°C with various hold times. These tests were conducted using C(T) specimens under constant load amplitude conditions (tension-tension) and DEN(T-C) specimens under displacement like conditions (tension-compression). Crack growth data generated under creep-fatigue conditions using standard C(T) specimens correlated well with crack growth data generated using DEN(T-C) specimens. The crack growth rates per cycle increased significantly with increase in hold time when crack growth data were plotted with the cyclic stress intensity parameter, Delta-K. A transient behavior in the initial portion of da/dN versus Delta-K plots were observed for the hold time tests, as reported previously by several other researchers. It is shown for the C(T) specimens that the creep-fatigue interactions during crack growth for various hold times are represented better by the (Ct)avg parameter implying that the P91 steel behaves in a creep-ductile manner. Significant differences (factors of 2 to 5) were observed between the calculated values of (Ct)avg and those based on measured values of force-line deflection. It is also shown that there is a high risk of obtaining invalid data in longer hold time tests under force-control conditions. The usefulness of DEN(T-C) specimens for crack growth studies under displacement controlled conditions to combat ratcheting problems in tests conducted under load conditions is established. The tests conditions for the round-robin program on creep-fatigue crack growth testing in support of ASTM E-2760 are finalized. Further developments needed in creep-fatigue crack growth testing are also presented.

  7. Growth and seasonal behavior of Anguilla anguilla in the River Minho tidal freshwater wetlands

    Directory of Open Access Journals (Sweden)

    Helena Correia

    2015-11-01

    Full Text Available The River Minho estuary, located on the northwest coast of the Iberian Peninsula, is a mesotidal estuary, partially mixed that during the period of high floods it tends to evolve towards a salt wedge estuary. The influence of spring tides extends approximately 40 km upstream and the tidal freshwater wetlands (TFWs are located in the upper 30 km. The Minho estuary is part of a Natura 2000 site, which includes the entire international section of the river being considered a very important river concerning migratory fish species. In the River Minho TFWs several fish species have ecological and economic value (Salmo trutta, Alosa fallax, Platichthys flesus, Anguilla anguilla, Salmo salar, Alosa alosa and Petromyzon marinus. European eel, A. anguilla, is in Appendix II of CITES list, that includes species not necessarily threatened with extinction, but in which trade must be controlled in order to avoid utilization incompatible with their survival. Between January 2007 and December 2014, in a selected semi-enclosed area of TFW and using 5 fyke-nets, were captured 1303 eels. All eels were measured and weighted, ocular index was determined and also marked with pit-tags and released in the same area. During these 8 years of work, around 15% of the total captured eels were recaptured once, less than 3% were recapture twice, less than 1% three times and 3 eels were recaptured 4 times. Eels marked in 2009 are until now the ones that were recaptured more times. Biological data as eel growth, seaward migration state, seasonal differences of by-catch will be crossed with abiotic data namely river flow, precipitation and water temperature.

  8. Vascular endothelial growth factor behavior in different stages of tooth germ development.

    Science.gov (United States)

    Mastrangelo, Filiberto; Sberna, Maria T; Vinci, Raffaele; Iaderosa, Giovanni; Tettamanti, Lucia; Cantatore, Giuseppe; Tagliabue, Angelo; Gherlone, Enrico F

    2016-08-01

    Scientific studies show a possible influence of intercellular and intracellular proteins (VEGF) on the development of physiological and pathological tissue. VEGF, a key regulator of angiogenesis, it would seem essential to take action during the embryonic development of the dental germ. The purpose of the study is to investigate the importance of the enzymatic activity of VEGF through protein quantification at different stages of tooth germ development. The quantification of VEGF protein was performed by 3 different laboratory tests: Western-blot analysis, semi-quantitative reverse transcriptase-polymerase chain reaction analysis (RT-PCR) and finally immunohistochemical analysis. Cell cultures of tooth tissue examined are: endothelial cells, stellate reticulum cells, odontoblasts and ameoblast. The VEGF peptide seems to induce an intense cell proliferation, not concomitant with differentiation towards the endothelial line. The expression of VEGF in the inner enamel epithelium (ameloblasts) would seem to depend on the stage of differentiation, leading us to deduce that VEGF and its respective receptor are expressed in dental germ and that induce alterations not only on the vascularization, but also on the inner epithelium activation and then on dental enamel development, respectively on cap and bell stages of embryogenesis. In our survey, the positive expression of VEGF in all the samples examined, might suggest a fundamental role of angiogenic gene proteins during all stages of embryonic tooth development. It is also characteristic the behavior of stellate reticulum cells, with a significant reduction in VEGF action between early and late stage, which could suggest a possible role of stellate reticulum cells, which would be able to promote and maintain an adequate energy supply to the tissues during early and late stages of differentiation and proliferation.

  9. Nondestructive inspection of corrosion and delamination at the concrete-steel reinforcement interface

    Science.gov (United States)

    Miller, Tri Huu

    The proposed study explores the feasibility of detecting and quantifying corrosion and delamination (physical separation) at the interface between reinforcing steel bars and concrete using ultrasonic guided waves. The problem of corrosion of the reinforcing steel in structures has increased significantly in recent years. The emergence of this type of concrete deterioration, which was first observed in marine structures and chemical manufacturing plants, coincided with the increased applications of deicing salts (sodium and calcium chlorides) to roads and bridges during winter months in those states where ice and snow are of major concern. Concrete is strengthened by the inclusion of the reinforcement steel such as deformed or corrugated steel bars. Bonding between the two materials plays a vital role in maximizing performance capacity of the structural members. Durability of the structure is of concern when it is exposed to aggressive environments. Corrosion of reinforcing steel has led to premature deterioration of many concrete members before their design life is attained. It is therefore, important to be able to detect and measure the level of corrosion in reinforcing steel or delamination at the interface. The development and implementation of damage detection strategies, and the continuous health assessment of concrete structures then become a matter of utmost importance. The ultimate goal of this research is to develop a nondestructive testing technique to quantify the amount of corrosion in the reinforcing steel. The guided mechanical wave approach has been explored towards the development of such methodology. The use of an embedded ultrasonic network for monitoring corrosion in real structures is feasible due to its simplicity. The ultrasonic waves, specifically cylindrical guided waves can p ropagate a long distance along the reinforcing steel bars and are found to be sensitive to the interface conditions between steel bars and concrete. Ultrasonic

  10. A combined experimental and theoretical approach to establish the relationship between shear force and clay platelet delamination in melt-processed polypropylene nanocomposites

    CSIR Research Space (South Africa)

    Bandyopadhyay, J

    2014-04-01

    Full Text Available In this article, a combined experimental and theoretical approach has been proposed to establish a relationship between the required shear force and the degree of delamination of clay tactoids during the melt-processing of polymer nanocomposites...

  11. Edge Delamination and Residual Properties of Drilled Carbon Fiber Composites with and without Short-Aramid-Fiber Interleaf

    Science.gov (United States)

    Sun, Zhi; Hu, Xiaozhi; Shi, Shanshan; Guo, Xu; Zhang, Yupeng; Chen, Haoran

    2016-10-01

    Edge delamination is frequently observed in carbon fiber reinforced plastic (CFRP) laminates after machining, due to the low fracture toughness of the resin interfaces between carbon fiber plies. In this study, the effects of incorporating tough aramid fibers into the brittle CFRP system are quantified by measuring the residual properties of bolted CFRP. By adding short-aramid-fiber interleaves in CFRP laminates, the residual tensile strength have been substantially increased by 14 % for twill-weave laminates and 45 % for unidirectional laminates respectively. Moreover, tensile failure was observed as the major mode of toughened laminates, in contrast to shear failure of plain laminates. The qualitative FEM results agreed well with the experimental results that edge delamination would cause relatively higher shear stress and therefore alter the failure mode from tensile failure to shear failure.

  12. Application of layered finite elements in the numerical analysis of laminated composite and sandwich structures with delaminations

    Directory of Open Access Journals (Sweden)

    Vuksanović Đorđe

    2015-01-01

    Full Text Available Laminar composites are modern engineering materials widely used in the mechanical and civil engineering. In the paper, some recent advances in a numerical analysis of laminated composite and sandwich plates and shells of different shapes, with existing zones of partial delamination, are presented. The layered finite elements, based on the extended version of the Generalized Laminated Plate Theory of Reddy, are applied for the numerical solution of several structural problems. After the verification of the proposed model for intact structures using the existing data from the literature, the effects of the size and the position of embedded delamination zones on the structural response of laminated structures are investigated numerically by means of a variety of numerical applications.

  13. Synthesis of Diamond Film on Molybdenum Substrate Surface by Combustion Flame Considering the Delamination of the Interface

    Science.gov (United States)

    Takahashi, Mamoru; Ito, Shunichi; Kamiya, Osamu; Ohyoshi, Tadashi

    Diamond films were synthesized on a Mo substrate using combustion flame. During cooling process, the most diamond films delaminated from the Mo substrate because of their thermal expansion mismatch. To prevent the delamination, a three-step synthesis method was proposed. The first step was synthesis of the Mo2C and the diamond phases on the Mo substrate, and the second and the third steps were synthesis of the diamond phase. The interfacial stress between the film and substrate was calculated by a finite element method. According to the results, the stress in the film made by the method was smaller than that by an one-step synthesis method. The three-step method is useful for synthesizing the diamond film.

  14. Quantitative 3D X-ray imaging of densification, delamination and fracture in a micro-composite under compression

    DEFF Research Database (Denmark)

    Bø Fløystad, Jostein; Skjønsfjell, Eirik Torbjørn Bakken; Guizar-Sicairos, Manuel

    2015-01-01

    Phase-contrast three-dimensional tomograms showing in unprecedented detail the mechanical response of a micro-composite subjected to a mechanical compression test are reported. The X-ray ptychography images reveal the deformation and fracture processes of a 10 μm diameter composite, consisting......-dimensional tomograms reveal with unprecedented detail the mechanical response, including delamination, densification and fracture, of a polymer-core/silver-shell micro-composite subjected in situ to a mechanical compression test....

  15. Influence of sugar beet pulp on feeding behavior, growth performance, carcass quality and gut health of fattening pigs

    Directory of Open Access Journals (Sweden)

    Laitat, M.

    2015-01-01

    Full Text Available Description of the subject. Dietary fiber is largely used in pig production but some contradictions appear in the literature regarding the effects on performance and health. Objectives. This paper aims to contribute to the clarification of the effects of a diet rich in sugar beet pulp on animal behavior, growth performance, carcass quality and gut health of fattening pigs. Method. Two successive batches of 24 fattening pigs were each divided into two groups fed ad libitum either a standard diet based on cereals (STD, 19% NSP [non-starch-polysaccharides] or a fibrous diet based on 23% sugar beet pulp (HFD, 31% NSP. Results. Pigs activity rate and feeder occupancy duration were increased by 57% and 165% for group fed HFD, respectively (P < 0.05. The fecal bacteria counts showed increases with HFD for Lactobacillus (10.21 vs 9.84 log10 of cfu·g-1 of feces dry matter, P < 0.05 and Bifidobacterium (9.49 vs 8.88, P < 0.01 but decreases for Enterobacteriaceae (4.85 vs 5.97, P < 0.001. Reductions of the average daily gain (788 vs 876 g per day, P < 0.001 and the dressing percentage (75.7 vs 78.9%, P < 0.001 were observed with HFD. Gastric lesion score was decreased with HFD (0.82 vs 1.55, P < 0.05. For pigs fed HFD, the proportion of surface area occupied by goblet cells was increased in the jejunum (10.06 vs 7.99%, P < 0.01 and the number of CD3 lymphocytes was increased in the colon (1.24 vs 0.90·mm-², P < 0.05. Conclusions. HFD contributes to strengthen the gut health of fattening pigs, but it impairs growth performance and carcass traits.

  16. Sex-related effects of an immune challenge on growth and begging behavior of barn swallow nestlings.

    Science.gov (United States)

    Romano, Andrea; Rubolini, Diego; Caprioli, Manuela; Boncoraglio, Giuseppe; Ambrosini, Roberto; Saino, Nicola

    2011-01-01

    Parent-offspring conflicts lead the offspring to evolve reliable signals of individual quality, including parasite burden, which may allow parents to adaptively modulate investment in the progeny. Sex-related variation in offspring reproductive value, however, may entail differential investment in sons and daughters. Here, we experimentally manipulated offspring condition in the barn swallow (Hirundo rustica) by subjecting nestlings to an immune challenge (injection with bacterial lipopolysaccharide, LPS) that simulates a bacterial infection, and assessed the effects on growth, feather quality, expression of morphological (gape coloration) and behavioral (posture) begging displays involved in parent-offspring communication, as well as on food allocation by parents. Compared to sham-injected controls, LPS-treated chicks suffered a depression of body mass and a reduction of palate color saturation. In addition, LPS treatment resulted in lower feather quality, with an increase in the occurrence of fault bars on wing feathers. The color of beak flanges, feather growth and the intensity of postural begging were affected by LPS treatment only in females, suggesting that chicks of either sex are differently susceptible to the immune challenge. However, irrespective of the effects of LPS, parents equally allocated food among control and challenged offspring both under normal food provisioning and after a short period of food deprivation of the chicks. These results indicate that bacterial infection and the associated immune response entail different costs to offspring of either sex, but a decrease in nestling conditions does not affect parental care allocation, possibly because the barn swallow adopts a brood-survival strategy. Finally, we showed that physiological stress induced by pathogens impairs plumage quality, a previously neglected major negative impact of bacterial infection which could severely affect fitness, particularly among long-distance migratory birds.

  17. The effect of the weak androgen oxandrolone on psychological and behavioral characteristics in growth hormone-treated girls with Turner syndrome.

    NARCIS (Netherlands)

    Menke, L.A.; Sas, T.C.J.; Visser, M. de; Kreukels, B.P.; Stijnen, T.; Zandwijken, G.R.; Muinck Keizer-Schrama, S.M.P.F. de; Otten, B.J.; Wit, J.M.; Cohen-Kettenis, P.T.

    2010-01-01

    The weak androgen oxandrolone (Ox) increases height gain in growth-hormone (GH) treated girls with Turner syndrome (TS), but may also give rise to virilizing side effects. To assess the effect of Ox, at a conventional and low dosage, on behavior, aggression, romantic and sexual interest, mood, and g

  18. The Role of Peer Contacts in the Relationship between Parental Knowledge and Adolescents' Externalizing Behaviors: A Latent Growth Curve Modeling Approach

    Science.gov (United States)

    Reitz, Ellen; Prinzie, Peter; Dekovic, Maja; Buist, Kirsten L.

    2007-01-01

    The purpose of the present study was to examine the direct and indirect effects (through peer contacts) of parental knowledge on adolescents' delinquent and aggressive problem behavior, using latent growth curve modeling. A sample of 457 13- to 14-year old adolescents at first measurement wave (M = 13.27; SD = 0.45 years) filled out questionnaires…

  19. Role of organoclay in controlling the morphology and crystal-growth behavior of biodegradable polymer-blend thin films studied using atomic force microscopy

    CSIR Research Space (South Africa)

    Malwela, T

    2014-09-01

    Full Text Available clays, their organic modifications and their initial d(sub001)-spacing on the morphology and crystal growth behavior of the PLA/PBSA blend were studied. An atomic force microscopy equipped with a hot-stage scanner was used to examine the crystalline...

  20. Application of Electric Capacity Measurements to Detecting Delamination in Blades of Helicopter’s Lifting and Auxiliary Rotors

    Directory of Open Access Journals (Sweden)

    Gębura Andrzej

    2017-06-01

    Full Text Available This paper represents a series of the authors’ publications concerning effects of atmospheric conditions on aircraft [5-6, 11]. Hazards connected with separation ( delamination of heating elements from blade’s spar , namely: increased susceptibility to ice formation as a result of change in aerodynamic profile, decreased deicing effectiveness, shortened life of heating elements , weakened strength of blade’s structure, are described. In order to monitor the above mentioned delamination process during its early phase, these authors proposed to measure systematically electric capacity between the heating element and blade’s spar by means of a technical method. The electric capacity measurements performed by these authors on blades both in laboratory and service conditions demonstrated their practical usefulness for assessing delamination extent as well as for identifying areas where heating element separation from spar occurred. The method in question is simple , cheap , fast and non-interferring (non-destructive as well as it does not require dismounting the blades off the helicopter. As proved in practice , it is especially useful in sea-rescue or military operational conditions. Special attention was paid to application of the method to composite blades where coming-off the heating element tape causes local overheating the blade structure , that impairs flexibility of composite’s layers and may lead even to local cracks which may trigger helicopter crash. These authors desire to apply the method as a standard unit of on-board diagnostic system in the future.