Mass spectrometry analysis of etch products from CR-39 plastic irradiated by heavy ions

Science.gov (United States)

Kodaira, S.; Nanjo, D.; Kawashima, H.; Yasuda, N.; Konishi, T.; Kurano, M.; Kitamura, H.; Uchihori, Y.; Naka, S.; Ota, S.; Ideguchi, Y.; Hasebe, N.; Mori, Y.; Yamauchi, T.

2012-09-01

As a feasibility study, gas chromatography-mass spectrometry (GC-MS) and matrix-assisted laser desorption ionization-mass spectrometry (MALDI-MS) have been applied to analyze etch products of CR-39 plastic (one of the most frequently used solid states nuclear track detector) for the understanding of track formation and etching mechanisms by heavy ion irradiation. The etch products of irradiated CR-39 dissolved in sodium hydroxide solution (NaOH) contain radiation-induced fragments. For the GC-MS analysis, we found peaks of diethylene glycol (DEG) and a small but a definitive peak of ethylene glycol (EG) in the etch products from CR-39 irradiated by 60 MeV N ion beams. The etch products of unirradiated CR-39 showed a clear peak of DEG, but no other significant peaks were found. DEG is known to be released from the CR-39 molecule as a fragment by alkaline hydrolysis reaction of the polymer. We postulate that EG was formed as a result of the breaking of the ether bond (C-O-C) of the DEG part of the CR-39 polymer by the irradiation. The mass distribution of polyallylalcohol was obtained from the etch products from irradiated and unirradiated CR-39 samples by MALDI-MS analysis. Polyallylalcohol, with the repeating mass interval of m/z = 58 Da (dalton) between m/z = 800 and 3500, was expected to be produced from CR-39 by alkaline hydrolysis. We used IAA as a matrix to assist the ionization of organic analyte in MALDI-MS analysis and found that peaks from IAA covered mass spectrum in the lower m/z region making difficult to identify CR-39 fragment peaks which were also be seen in the same region. The mass spectrometry analysis using GC-MS and MALDI-MS will be powerful tools to investigate the radiation-induced polymeric fragments and helping to understand the track formation mechanism in CR-39 by heavy ions.

Gamma irradiation effects on the thermal, optical and structural properties of Cr-39 nuclear track detector

International Nuclear Information System (INIS)

Nouh, S.A.; Said, A.F.; Atta, M.R.; EL-Mellegy, W.M.; EL-Meniawi, S.

2006-01-01

A study of the effect of gamma irradiation on the thermal, optical and structural properties of CR-39 diglycol carbonate solid state nuclear track detector (SSNTD) has been carried out. Samples from CR-39 polymer were irradiated with gamma doses at levels between 20 and 300 KGy. Non-isothermal studies were carried out using thermo-gravimetry (TG), differential thermo-gravimetry (DTG) and differential thermal analysis (DTA) to obtain the activation energy of decomposition and the transition temperatures for the non-irradiated and irradiated CR-39 samples. In addition, optical and structural property studies were performed on non-irradiated and irradiated CR-39 samples using refractive index and X-ray diffraction measurements. The variation of onset temperature of decomposition (To) thermal activation energy of decomposition (Ea) melting temperature (Tm) refractive index (n) and the mass fraction of the amorphous phase with the gamma dose were studied. It was found that many changes in the thermal, optical and structural properties of the CR-39 polymer could be produced by gamma irradiation via the degradation and cross linking mechanisms. Also, the gamma dose gave an advantage for increasing the correlation between the thermal stability of CR-39 polymer and the bond formation created by the ionizing effect of gamma radiation

Study of gamma irradiation effects on the etching and optical properties of CR-39 solid state nuclear track detector and its application to uranium assay in soil samples

International Nuclear Information System (INIS)

Amol Mhatre; Kalsi, P.C.

2011-01-01

The gamma irradiation effects in the dose range of 2.5-43.0 Mrad on the etching and optical characteristics of CR-39 solid state nuclear track detector (SSNTD) have been studied by using etching and UV-Visible spectroscopic techniques. From the measured bulk etch rates at different temperatures, the activation energies for bulk etching at different doses have also been determined. It is seen that the bulk etch rates increase and the activation energies for bulk etching decrease with the increase in gamma dose. The optical band gaps of the unirradiated and the gamma -irradiated detectors determined from the UV-Visible spectra were found to decrease with the increase in gamma dose. These results have been explained on the basis of scission of the detector due to gamma irradiation. The present studies can be used for the estimation of gamma dose in the range of 2.5-43.0 Mrad and can also be used for estimating track registration efficiency in the presence of gamma dose. The CR-39 detector has also been applied for the assay of uranium in some soil samples of Jammu city. (author)

A new method for studying the transport of radon and thoron in various building materials using CR-39 and LR-115 solid state nuclear track detectors

International Nuclear Information System (INIS)

Misdaq, M.A.; Ktata, A.; Bakhchi, A.

2000-01-01

Radon ( 222 Rn) and thoron ( 220 Rn) α-activities per unit volume were measured inside and outside different building materials by using two types of solid state nuclear track detectors (SSNTD) (CR-39 and LR-115 type II). In addition, the radon and thoron emanation coefficients of the studied materials were evaluated. Based on these data, the transport of radon and thoron across parallelepipedic blocks of the building materials could be investigated and radon and thoron global α-activities per unit volume outside different building material blocks were determined. Moreover, the diffusion length and the effective diffusion coefficient of radon in the building materials were evaluated and the total alpha activity due to radon in the atmospheres of different rooms consisting of different building materials was studied

Particularisation of Alpha Contamination using CR-39 Track Detectors

International Nuclear Information System (INIS)

Zakia, M.F.; El-Shaer, Y.H.

2008-01-01

Solid-state nuclear track detectors have found wide use in various domains of science and technology, e.g. in environmental experiments. The measurement of alpha activity on sources in an environment, such as air is not easy because of short penetration range of the alpha particles. Furthermore, the measurement of alpha activity by most gas ionization detectors suffers from the high background induced by the accompanying gamma radiation. Solid State Nuclear Track Detectors (SSNTDs) have been used successfully as detecting devices as passive system to detect the alpha contamination different surfaces. This work presents the response of CR-39 (for two types) to alpha particles from two sources, 238 Pu with energy 5 MeV and 241 Am with energy 5.4 MeV. The methods of etching and counting are investigated, along with the achievable linearity, efficiency and reproducibility. The sensitivity to low activity and energy resolution are studied

Characterization of saturation of CR-39 detector at high alpha-particle fluence

Directory of Open Access Journals (Sweden)

M. El Ghazaly

2018-04-01

Full Text Available The occurrence of saturation in the CR-39 detector reduces and limits its detection dynamic range; nevertheless, this range could be extended using spectroscopic techniques and by measuring the net bulk rate of the saturated CR-39 detector surface. CR-39 detectors were irradiated by 1.5 MeV high alpha-particle fluence varying from 0.06 × 108 to 7.36 × 108 alphas/cm2 from Am-241 source; thereafter, they were etched in a 6.25N NaOH solution at a temperature of 70°C for different durations. Net bulk etch rate measurement of the 1.5 MeV alpha-irradiated CR-39 detector surface revealed that rate increases with increasing etching time and reaches its maximum value at the end of the alpha-particle range. It is also correlated with the alpha-particle fluence. The measurements of UV–Visible (UV–Vis absorbance at 500 and 600 nm reveal that the absorbance is linearly correlated with the fluence of alpha particles at the etching times of 2 and 4 hour. For extended etching times of 6, 10, and 14.5 hour, the absorbance is saturated for fluence values of 4.05 × 108, 5.30 × 108, and 7.36 × 108 alphas/cm2. These new methods pave the way to extend the dynamic range of polymer-based solid state nuclear track detectors (SSNTDs in measurement of high fluence of heavy ions as well as in radiation dosimetry. Keywords: Alpha Particle, Bulk Etch Rate, CR-39 Detector, Saturated Regime, UV–Vis Spectroscopy

Coherent light scattering by nuclear etched tracks in the PADC (a form of CR-39)

Energy Technology Data Exchange (ETDEWEB)

Groetz, J.E.; Chambaudet, A. [Universite de Franche-Comte, Besancon (France). Lab. de Microanalyses Nucleaires; Lacourt, A. [Laboratoire d`Optique P.M. Duffieux, UMR 6603 CNRS, Universite de Franche-Comte, 16 route de Gray, 25030 Besancon Cedex (France)

1998-08-01

A new kind of measurement has been proposed to improve the reading of the solid state nuclear track detector CR-39. This method is based on coherent light scattering (He-Ne laser) by etched proton tracks, and is complementary to observation under an optical microscope and reading by optical density of the CR-39. The irradiated and chemically etched CR-39 sample is illuminated by a laser beam under a normal incidence angle. The light intensity diffracted by the tracks beyond the sample - defined with the bi-directional transmissive distribution functions - is measured with a photodiode. Thus, the bi-directional transmissive distribution functions depend on the characteristics of the irradiation, namely the track density, track sizes and orientations. We have performed a track light diffraction model calculation through the use of the Fraunhofer diffraction, Babinet`s principle and the spatial coherence and incoherence. We compared calculations and experimental results for the different shapes of tracks: conical, oblique and spherical-shaped. (orig.) 14 refs.

Coherent light scattering by nuclear etched tracks in the PADC (a form of CR-39)

International Nuclear Information System (INIS)

Groetz, J.E.; Chambaudet, A.

1998-01-01

A new kind of measurement has been proposed to improve the reading of the solid state nuclear track detector CR-39. This method is based on coherent light scattering (He-Ne laser) by etched proton tracks, and is complementary to observation under an optical microscope and reading by optical density of the CR-39. The irradiated and chemically etched CR-39 sample is illuminated by a laser beam under a normal incidence angle. The light intensity diffracted by the tracks beyond the sample - defined with the bi-directional transmissive distribution functions - is measured with a photodiode. Thus, the bi-directional transmissive distribution functions depend on the characteristics of the irradiation, namely the track density, track sizes and orientations. We have performed a track light diffraction model calculation through the use of the Fraunhofer diffraction, Babinet's principle and the spatial coherence and incoherence. We compared calculations and experimental results for the different shapes of tracks: conical, oblique and spherical-shaped. (orig.)

Studies of biocompatibility of chemically etched CR-39 SSNTDs in view of their applications in alpha-particle radiobiological experiments

International Nuclear Information System (INIS)

Li, W.Y.; Chan, K.F.; Tse, A.K.W.; Fong, W.F.; Yu, K.N.

2006-01-01

Alpha-particle radiobiological experiments involve irradiating cells with alpha particles and require thin biocompatible materials which can record alpha-particle traversals as substrates for cell cultures. The biocompatibilities of chemically etched CR-39 solid-state nuclear track detectors (SSNTDs) using aqueous NaOH or NaOH/ehtanol are studied through the abundance and morphology of the cultured HeLa cells. The wetting properties of these etched CR-39 SSNTDs are also studied. The moderately hydrophobic CR-39 SSNTDs as well as the hydrophobic NaOH/ethanol-etched CR-39 SSNTDs are more biocompatible than the hydrophilic aqueous-NaOH-etched SSNTDs. Too small water contact angles, too large surface energy (γ s ) or the polar component γ s p do not favor the cell culture. On the other hand, the dispersive component γ s d of the surface energy and the ratio γ s p /γ s d do not seem to significantly affect the biocompatibility

Proton Radiography with CR-39 by Using the Protons from High Power Femto-second Laser System

International Nuclear Information System (INIS)

Choi, Chang Il; Lee, Dong Hoon; Kang, Byoung Hwi; Kim, Yong Kyun; Choi, Il Woo; Ko, Do Kyeong; Lee, Jong Min

2008-01-01

Proton radiography techniques are useful to obtain a high quality image of a thin object, because protons travel straight in matter. Generation of the high energy proton using conventional accelerator costs high and requires large accelerating facility. But proton radiography using high power femto-second(10-15 second) laser has been interested, because it can generate high energy protons at lower price than the conventional accelerator like a cyclotron. For this study, we used the CR-39 SSNTD (Solid State Nuclear Track Detector) as the proton radiography screen. Commonly, CR-39 is used to detect the tracks of energetic charged particles. Incident energetic charged particles left latent tracks in the CR-39, in the form of broken molecular chains and free radicals. These latent tracks show high chemical reactivity. After chemical etching with the caustic alkali solution such as NaOH or KOH, tracks are appeared to forms of hole. If protons with various energies enter the two targets with another thickness, number of protons passed through the target per unit area is different each other. Using this feature of protons, we can a proton radiographic image with CR-39. We studied proton radiography with CR-39 by using energetic protons from high power femto-second laser and evaluated potentiality of femto-second laser as new energetic proton generator for radiography

Development of optical monitor of alpha radiations based on CR-39.

Science.gov (United States)

Joshirao, Pranav M; Shin, Jae Won; Vyas, Chirag K; Kulkarni, Atul D; Kim, Hojoong; Kim, Taesung; Hong, Seung-Woo; Manchanda, Vijay K

2013-11-01

Fukushima accident has highlighted the need to intensify efforts to develop sensitive detectors to monitor the release of alpha emitting radionuclides in the environment caused by the meltdown of the discharged spent fuel. Conventionally, proportional counting, scintillation counting and alpha spectrometry are employed to assay the alpha emitting radionuclides but these techniques are difficult to be configured for online operations. Solid State Nuclear Track Detectors (SSNTDs) offer an alternative off line sensitive technique to measure alpha emitters as well as fissile radionuclides at ultra-trace level in the environment. Recently, our group has reported the first ever attempt to use reflectance based fiber optic sensor (FOS) to quantify the alpha radiations emitted from (232)Th. In the present work, an effort has been made to develop an online FOS to monitor alpha radiations emitted from (241)Am source employing CR-39 as detector. Here, we report the optical response of CR-39 (on exposure to alpha radiations) employing techniques such as Atomic Force Microscopy (AFM) and Reflectance Spectroscopy. In the present work GEANT4 simulation of transport of alpha particles in the detector has also been carried out. Simulation includes validation test wherein the projected ranges of alpha particles in the air, polystyrene and CR-39 were calculated and were found to agree with the literature values. An attempt has been further made to compute the fluence as a function of the incidence angle and incidence energy of alphas. There was an excellent correlation in experimentally observed track density with the simulated fluence. The present work offers a novel approach to design an online CR-39 based fiber optic sensor (CRFOS) to measure the release of nanogram quantity of (241)Am in the environment. © 2013 Elsevier Ltd. All rights reserved.

Estimation of track registration efficiency in solution medium and study of gamma irradiation effects on the bulk-etch rate and the activation energy for bulk etching of CR-39 (DOP) Solid State Nuclear Track Detector

International Nuclear Information System (INIS)

Kalsi, P.C.

2010-01-01

The fission track registration efficiency of diethylene glycol bis allyl carbonate (dioctyl phthalate doped) (CR-39 (DOP)) solid state nuclear track detector (SSNTD) in solution medium (K wet ) has been experimentally determined and is found to be (9.7 ± 0.5).10 -4 cm. This is in good agreement with the values of other SSNTDs. The gamma irradiation effects in the dose range of 50.0-220.0 kGy on the bulk etch rate, V b and the activation energy for bulk etching, E of this solid state nuclear track detector (SSNTD) have also been studied. It is observed that the bulk etch rates increase and the activation energies for bulk etching decrease with the increase in gamma dose. These results have been explained on the basis of scission of the detector due to gamma irradiation

Response of CR-39 SSNTD to high energy neutrons using zirconium convertors - a Monte Carlo and experimental study

International Nuclear Information System (INIS)

Pal, Rupali; Sapra, B.K.; Bakshi, A.K.; Datta, D.; Biju, K.; Suryanarayana, S.V.; Nayak, B.K.

2016-01-01

Neutron dosimetry in ion accelerators is a challenging field as the neutron spectrum varies from thermal, to fast and high-energy neutrons usually extending beyond 20 MeV. Solid-state Nuclear Track Detectors (SSNTDs) have been increasingly used in numerous fields related to nuclear physics. Extensive work has also been carried out on determining the response characteristics of such detectors as nuclear spectrometers. In nuclear reaction studies, identification of reaction products according to their type and energy is frequently required. For normally incident particles, energy-dispersive track-diameter methods have become useful scientific tools using CR-39 SSNTD. CR-39 along with 1 mm polyethylene convertor can cover a neutron energy range from 100 keV to 10 MeV. The neutron interacts with the hydrogen in CR-39 producing recoil protons from elastic collisions. This detectable neutron energy range can be increased by modification in the radiator/convertor used along with CR-39. CR39 detectors placed in conjunction with judiciously chosen thicknesses of a polyethylene radiator and a lead absorber (or degrader) are used to increase energy range upto 19 MeV. A portable neutron counter has been proposed for high-energy neutron measurement with 1 cm thick Zirconium (Zr) as the converter outside a spherical HDPE shell of 7 inch diameter. Zr metal has been found to show (n,2n) cross section for energies above 10 MeV starting from 0.01 barns for 8 MeV upto 1 barns for 22 MeV. Above these energies, the experimental data is scarce. In this paper, Zr was used in conjunction with CR-39 which showed an enhancement of track density on the CR-39. This paper demonstrates the enhancement of neutron response using Zr on CR-39 with both theoretical and experimental studies

gamma-induced modification on optical band gap of CR-39 SSNTD

International Nuclear Information System (INIS)

Zaki, M.F.

2010-01-01

effect of gamma irradiation on optical absorption of nuclear track detectors like CR-39 was studied at different absorbed doses using ultraviolet-visible (UV-VIS)spectroscopy. the existence of the peaks, their shifting and broadening as a result of gamma irradiation has been discussed. the width of the tail of localized states in the band gap (E u )was evaluated using the Urbach edge method. finally the indirect and direct band gap in pristine and gamma irradiated CR-39 have been determined. the values of indirect band gap have been found to be lower than the corresponding values of direct band gap. a decrease in the optical energy gap with increasing the gamma absorbed dose can be discussed on the basis of gamma-irradiation-induced defects in the CR-39. the correlation between optical band gap and the number of carbon atoms in a cluster with modified Tauc's equation has been discussed in case of CR-39.

LET calibration for CR-39 detectors in different oxygen environments

International Nuclear Information System (INIS)

Zhou, D.; Semones, E.; Weyland, M.; Benton, E.R.

2007-01-01

High LET (linear energy transfer) radiation is the main contributor to the radiation field in low Earth orbit (LEO) in terms of dose equivalent. CR-39 plastic nuclear track detectors (PNTDs) can measure the LET spectrum and charge spectrum for the complicated radiation field in space. Previous research indicated that the sensitivity of CR-39 is different for CR-39 PNTDs working in different oxygen environments. LET calibration for CR-39 detectors in different oxygen environments is needed. Almost all the previous LET calibration work was carried out for CR-39 detectors in good-oxygen condition, LET calibration work for CR-39 in poor-oxygen condition has not been conducted until our work. Systematic LET calibrations were carried out by JSC-SRAG (Space Radiation Analysis Group) for CR-39 detectors working in different oxygen environments and abundant results of LET calibrations were obtained. This paper introduces the method for CR-39 LET calibration, presents and discusses the calibration results and some applications

Investigations of CR39 dosimeters for neutron routine dosimetry

International Nuclear Information System (INIS)

Weinstein, M.; Abraham, A.; Tshuva, A.; German, U.

2004-01-01

CR-39 is a polymeric nuclear track detector which is widely used for neutron dosimetry. CR-39 detector development was conducted at a number of laboratories throughout the world(1,2) , and was accepted also for routine dosimetry. However, there are shortcomings which must be taken into consideration the lack of a dosimetry grade material which causes batch variations, significant angular dependence and a moderate sensitivity. CR-39 also under-responds for certain classes of neutron spectra (lower energy neutrons from reactors or high energy accelerator-produced neutrons).In order to introduce CR-39 as a routine dosimeter at NRCN, a series of checks were performed. The present work describes the results of some of our checks, to characterize the main properties of CR-39 dosimeters

Calibration of detectors type CR-39 for methodology implementation for Radon-222 determination in CRCN-NE, Brazil

International Nuclear Information System (INIS)

Silva, Karolayne E.M. da; Santos, Mariana L. de O.; Amaral, Déric S. do; Vilela, Eldice C.; França, Elvis J. de; Hazin, Clovis A.; Farias, Emerson E.G. de

2017-01-01

Radon-222 is a radioactive gas, a product of the decay of uranium-238, which emits alpha particles and represents more than 50% of the dose of natural radiation received by the population. Therefore, monitoring of this gas is essential. For indoor measurement, solid state detectors can be used, the most common of which is CR-39. For monitoring using CR-39, alpha particles, generated by radon-222 and the daughter radionuclides, strike the surface of the detector and generate traces. To relate the trace density per exposure area in environments with unknown activity concentration, it is necessary to determine the calibration factor. The objective of this study was to calibrate CR-39 type detectors for the implementation of the radon determination methodology in Centro Regional de Ciencias Nucleares do Nordeste - CRCN-NE of Brazilian Nuclear Energy Commission - CNEN. In order to determine the CR-39 calibration factor, 19 exposures of the detectors were performed in the CRCN-NE calibration chamber (RN1-CRCN) at an activity of 5.00 kBq m -3 , with the exposure time varying from 24 to 850 hours. For the detection of the detectors, sodium hydroxide was used in a thermostat bath at 90 ° C for 5 hours. The count of number of traits per unit of field was performed with the aid of optical microscopy with an increase of 100 times, being read 30 fields per dosimeters. As a result, the calibration factor was obtained, and the linear response of the trace density as a function of exposure was observed. The results allow the use of CR-39 in the determination of radon-222 by CRCN-NE

Solid-state diffusion bonding of high-Cr ODS ferritic steel

Energy Technology Data Exchange (ETDEWEB)

Noh, Sanghoon, E-mail: sh-noh@iae.kyoto-u.ac.jp [Institute of Advanced Energy, Kyoto University, Gokasho, Uji, Kyoto (Japan); Kasada, Ryuta; Kimura, Akihiko [Institute of Advanced Energy, Kyoto University, Gokasho, Uji, Kyoto (Japan)

2011-05-15

Research highlights: > Oxide dispersion strengthened ferritic steel joined by solid-state diffusion bonding. > Free of precipitates and micro-voids at the bonding interface was existed. > Joints had the same tensile properties with anisotropy of the base material. > USE of joints was fully reserved in L-R bonding orientation. > Cracks did not propagate on the bonding interface at the Charpy impact test. - Abstract: Solid-state diffusion bonding (SSDB) was employed to join high-Cr oxide dispersion strengthened (ODS) ferritic steel (Fe-15Cr-2W-0.2Ti-0.35Y{sub 2}O{sub 3}) blocks under uniaxial hydrostatic pressure using a high-vacuum hot press, and the microstructure and mechanical properties of the joints were investigated. High-Cr ODS ferritic steels were successfully diffusion bonded at 1200 deg. C for 1 h, without precipitates and microvoids at the bonding interface or degradation in the base materials. Transmission electron microscopic observation revealed that the nano-oxide particles near the bonding interface were uniformly distributed in the matrix and that the chemical composition across the bonding interface was virtually constant. At room temperature, the joint had nearly the same tensile properties and exhibited anisotropic behavior similar to that of the base material. The tensile strength of the joint region at elevated temperatures is nearly the same as that of the base material, with necking behavior at several micrometers from the bonding interface. The total elongation of the joint region decreased slightly at 700 {sup o}C, with an exfoliation fracture surface at the bonding interface. Although a small ductile-brittle transition temperature shift was observed in the joints, the upper shelf energy was fully reserved in the case of joints with L-R bonding orientation, for which cracks did not propagate on the bonding interface. Therefore, it is concluded that SSDB can be potentially employed as a joining method for high-Cr ODS ferritic steel owing to

Optimization of CR-39 for fast neutron dosimetry applications

International Nuclear Information System (INIS)

Vilela, E.; Fantuzzi, E.; Giacomelli, G.; Giorgini, M.; Morelli, B.; Patrizii, L.; Serra, P.; Togo, V.

1999-01-01

We present the results of an experimental work aimed at improving the performances of the CR-39[reg] (Registered Trademark of PPG Industries Inc.) nuclear track detector for neutron dosimetry applications. The work was done in collaboration with the Intercast Europe S.p.A., producer of CR-39 for commercial and scientific applications. We compare the CR-39 made with different additives concentrations and different polymerization processes. We evaluate the response of the CR-39 to fast neutrons from three sources: 241 Am-Be, 252 Cf and 238 Pu-Li. Particular attention was paid to background fluctuations that limit the lower detectable dose

Optimization of CR-39 for fast neutron dosimetry applications

CERN Document Server

Vilela, E; Giacomelli, G; Giorgini, M; Morelli, B; Patrizii, L; Serra, P; Togo, V

1999-01-01

We present the results of an experimental work aimed at improving the performances of the CR-39[reg] (Registered Trademark of PPG Industries Inc.) nuclear track detector for neutron dosimetry applications. The work was done in collaboration with the Intercast Europe S.p.A., producer of CR-39 for commercial and scientific applications. We compare the CR-39 made with different additives concentrations and different polymerization processes. We evaluate the response of the CR-39 to fast neutrons from three sources: sup 2 sup 4 sup 1 Am-Be, sup 2 sup 5 sup 2 Cf and sup 2 sup 3 sup 8 Pu-Li. Particular attention was paid to background fluctuations that limit the lower detectable dose.

Cr-39 fast neutron dosemeter based on A (n, α) converter

International Nuclear Information System (INIS)

Widayati, S.; Budiantari, T.

1998-01-01

The aim of this experiment is to obtained the response of Cr-39 as fast neutron dosemeter based on an (n, α) converter. Cr-39 was irradiated to AmBe fast neutron flux from 0.10 mSv to 2.5 mSv. Cr-39 processed by chemical etching with NaOH 20 % at temperature of 60 oC in six hours. The results of experiment showed that the response of Cr-39 based on an (n, α) converter is 6 times bigger than the response of Cr-39 without (n, α) converter. (author)

Measuring depths of sub-micron tracks in a CR-39 detector from replicas using Atomic Force Microscopy

International Nuclear Information System (INIS)

Yu, K.N.; Ng, F.M.F.; Nikezic, D.

2005-01-01

One of the challenging tasks in the application of solid-state nuclear track detectors (SSNTDs) is the measurement of the depth of the tracks, in particular, the shallow ones resulting from short etching periods. In the present work, a method is proposed to prepare replicas of tracks from α particles in the CR-39 SSNTDs and to measure their heights using atomic force microscopy (AFM). After irradiation, the detectors were etched in a 6.25N aqueous solution of NaOH maintained at 70 deg. C. The etched detectors were immersed into a beaker of the replicating fluid, which was placed in a water bath under ultrasonic vibration and maintained at room temperature to facilitate the filling of the etched tracks with the replicating fluid. As an example of application, these results have been used to derive a V function for the CR-39 detectors used in the present study (for the specified etching conditions)

The LLNL CR-39 personnel neutron dosimeter

International Nuclear Information System (INIS)

Hankins, D.E.; Homann, S.; Westermark, J.

1987-01-01

We developed a personnel neutron dosimetry system based on the electrochemical etching of CR-39 plastic at elevated temperatures. The doses obtained using this dosimeter system are more accurate than those obtained using other dosimetry systems, especially when varied neutron spectra are encountered. This CR-39 dosimetry system does not have the severe energy dependence that exists with albedo neutron dosimeters or the fading and reading problems encountered with NTA film. 3 refs., 4 figs

Empirical assessment of the detection efficiency of CR-39 at high proton fluence and a compact, proton detector for high-fluence applications

Energy Technology Data Exchange (ETDEWEB)

Rosenberg, M. J., E-mail: mrosenbe@mit.edu; Séguin, F. H.; Waugh, C. J.; Rinderknecht, H. G.; Orozco, D.; Frenje, J. A.; Johnson, M. Gatu; Sio, H.; Zylstra, A. B.; Sinenian, N.; Li, C. K.; Petrasso, R. D. [Plasma Science and Fusion Center, Massachusetts Institute of Technology, Cambridge, Massachusetts 02139 (United States); Glebov, V. Yu.; Stoeckl, C.; Hohenberger, M.; Sangster, T. C. [Laboratory for Laser Energetics, University of Rochester, Rochester, New York 14623 (United States); LePape, S.; Mackinnon, A. J.; Bionta, R. M.; Landen, O. L. [Lawrence Livermore National Laboratory, Livermore, California 94550 (United States); and others

2014-04-15

CR-39 solid-state nuclear track detectors are widely used in physics and in many inertial confinement fusion (ICF) experiments, and under ideal conditions these detectors have 100% detection efficiency for ∼0.5–8 MeV protons. When the fluence of incident particles becomes too high, overlap of particle tracks leads to under-counting at typical processing conditions (5 h etch in 6N NaOH at 80 °C). Short etch times required to avoid overlap can cause under-counting as well, as tracks are not fully developed. Experiments have determined the minimum etch times for 100% detection of 1.7–4.3-MeV protons and established that for 2.4-MeV protons, relevant for detection of DD protons, the maximum fluence that can be detected using normal processing techniques is ≲3 × 10{sup 6} cm{sup −2}. A CR-39-based proton detector has been developed to mitigate issues related to high particle fluences on ICF facilities. Using a pinhole and scattering foil several mm in front of the CR-39, proton fluences at the CR-39 are reduced by more than a factor of ∼50, increasing the operating yield upper limit by a comparable amount.

High energy charged particle registration in CR-39 polycarbonated detector

International Nuclear Information System (INIS)

Abdel-Wahab, M.S.; El Enany, N.; El Fiki, S.; Eissa, H.M.; El-Adl, E.H.; El-Feky, M.A.

1991-01-01

Track etch rate characteristics of CR-39 plastic detector exposed to 28 Si ions of 670 MeV energy have been investigated. Experimental results were obtained in terms of frequency distribution of the track diameter, track density and bulk etching rate. A dependence of the mean track diameter on energy was found. The application of the radiation effect of heavy ions on CR-39 in the field of radiation detection and dosimetry are discussed. Results indicated that it is possible to produce etchable tracks of 28 Si in this energy range in CR-39. We also report the etching characteristics of these tracks in the CR-39 detector. (orig.) [de

CR-39 track detector for multi-MeV ion spectroscopy.

Science.gov (United States)

Jeong, T W; Singh, P K; Scullion, C; Ahmed, H; Hadjisolomou, P; Jeon, C; Yun, H; Kakolee, K F; Borghesi, M; Ter-Avetisyan, S

2017-05-19

We present the characteristics of track formation on the front and rear surfaces of CR-39 produced by laser-driven protons and carbon ions. A methodological approach, based on bulk etch length, is proposed to uniquely characterize the particle tracks in CR-39, enabling comparative description of the track characteristics in different experiments. The response of CR-39 to ions is studied based on the energy dependent growth rate of the track diameter to understand the intrinsic particle stopping process within the material. A large non-uniformity in the track diameter is observed for CR-39 with thickness matching with the stopping range of particles. Simulation and experimental results show the imprint of longitudinal range straggling for energetic protons. Moreover, by exploiting the energy dependence of the track diameter, the energy resolution (δE/E) of CR-39 for few MeV protons and Carbon ion is found to be about 3%.

Imaging of fast-neutron sources using solid-state track-recorder pinhole radiography

International Nuclear Information System (INIS)

Ruddy, F.H.; Gold, R.; Roberts, J.H.; Kaiser, B.J.; Preston, C.C.

1983-08-01

Pinhole imaging methods are being developed and tested for potential future use in imaging the intense neutron source of the Fusion Materials Irradiation Test (FMIT) Facility. Previously reported, extensive calibration measurements of the proton, neutron, and alpha particle response characteristics of CR-39 polymer solid state track recorders (SSTRs) are being used to interpret the results of imaging experiments using both charged particle and neutron pinhole collimators. High resolution, neutron pinhole images of a 252 Cf source have been obtained in the form of neutron induced proton recoil tracks in CR-39 polymer SSTR. These imaging experiments are described as well as their potential future applications to FMIT

Fast neutron detection using solid state nuclear track detectors

International Nuclear Information System (INIS)

Vilela, E.C.

1990-01-01

CR-39 and Makrofol-E solid state nuclear track detectors were studied aiming their application to fast neutron detection. Optimum etching conditions of those two kinds of materials were determined the followings - the Makrofol-E detector is electrochemically etched in a PEW solution (15% KOH, 40% ethilic alcohol and 45% water) for 2 h., with an applied electric field strength of 30 kV/cm (r/m/s/) and frequency of 2 kHz, at room temperature; - the CR-39 detector is chemically pre-etched during 1 h in a 20% (w/v) NaOH solution at 70 sup(0)C, followed by 13 h electrochemical etch using the same solution at room temperature and an electric field strength of 30 kV/cm (r.m.s.) and frequency of 2 kHz.(E.G.)

Characterization of plastic nuclear track detectors on solid state, CR-39 and LR-115 and its possibilities application on thermal and fast neutron dosimetry

International Nuclear Information System (INIS)

Vallejo Delgado, L.R.

1989-01-01

This work is an study about the use feasibility of plastic nuclear track detectors, LR 115, II-B (of Eastmann Kodak Co) and CR-39 (of American Acrylics and Plastics), for thermal and fast neutron dosimetry, respectively. The LR-115 with converter (n, alpha) was exposed to thermal neutrons with energy of 0,046 e V, proceeding from nuclear reactor RECH-1 of Nuclear Energy Chilean Commission. The irradiated films were submited to a chemical etching with NaOH, plus a washing and brushing. The CR-39 with polyethylene irradiator, was exposed to fast neutrons proceeding of calibrated sources of Am-Se. The irradiated plates were submited to a chemical pre-etching with KOH and a electrochemical post-etching. (author)

A study on alpha particles range in Cr-39

International Nuclear Information System (INIS)

Ibrahim, Z.A.; Talaat, T.M.; Abdel-Aziz, Kh.M.A.; El-Asser, M.R.

2000-01-01

Cr-39 plastic nuclear track detector has been used in range determination of alpha particles. A set of experiments was carried out for studying alpha energy and track diameter relationships. This work was done under the optimum conditions of Cr-39 etching in 6.25 N NaOH at 70 degree C for various etching times. Determination of alpha range in Cr-39 recorders was studied at different energy values using the over etched track profile technique. Data are discussed within the framework of track formation theory in plastic foils, comparison between experimental and theoretical values of alpha range is included

Theoretical calculation on CR-39 response for radon measurements and optimum diffusion chambers dimensions

Energy Technology Data Exchange (ETDEWEB)

Askari, H.R.; Ghandi, Kh. [Department of Physics, Faculty of Science, Vali-e-Asr University, Rafsanjan 7713936417 (Iran, Islamic Republic of); Rahimi, M. [Department of Physics, Faculty of Science, Vali-e-Asr University, Rafsanjan 7713936417 (Iran, Islamic Republic of)], E-mail: rahimi_bam@yahoo.com; Negarestani, A. [International Center for Science and High Technology and Environmental Sciences, Kerman (Iran, Islamic Republic of)

2008-11-11

One method to measure radon gas concentration in the air with a long time of radiation is trace chemical etching technique. There is a direct proportion between the number of traces on solid-state nuclear track detectors (SSNTDs) and activity concentration of radon. In this paper, calibration constant for a cylindrical chamber with CR-39 detector has been measured analytically. Using this measurement, trace curves on the base of concentration for chambers with different heights and radii have been drawn. The results show that to measure radon gas concentration, the optimum chamber should have a height between 3.5 and 4 cm and a radius between 2.5 and 3.2 cm.

Theoretical calculation on CR-39 response for radon measurements and optimum diffusion chambers dimensions

International Nuclear Information System (INIS)

Askari, H.R.; Ghandi, Kh.; Rahimi, M.; Negarestani, A.

2008-01-01

One method to measure radon gas concentration in the air with a long time of radiation is trace chemical etching technique. There is a direct proportion between the number of traces on solid-state nuclear track detectors (SSNTDs) and activity concentration of radon. In this paper, calibration constant for a cylindrical chamber with CR-39 detector has been measured analytically. Using this measurement, trace curves on the base of concentration for chambers with different heights and radii have been drawn. The results show that to measure radon gas concentration, the optimum chamber should have a height between 3.5 and 4 cm and a radius between 2.5 and 3.2 cm.

A study of the molecular structure in CR-39

International Nuclear Information System (INIS)

Stejny, J.; Portwood, T.

1986-01-01

A technique is presented for examining the molecular structure of CR-39 by analysis of the etch products from hydrolysis of the polymer network. The CR-39 network consists of polyallyl chains jointed by diethyleneglycol dicarbonate links. The etching cuts the carbonate links and liberates the polyallyl chains which makes them amenable to common analytical methods. Gel Permeation Chromatography was used to characterize the chain lengths and their distribution. It was found that the average length is rather short and that it decreases with increasing concentration of the initiator. This technique has been also used to identify the radiation sensitive link in the CR-39 network. It was found that the length of polyallyl chain is not changed in 60 Co γ-irradiated plastic while the etch rate significantly increases. This shows that the polyallyl chains are relatively inert and not responsible for the radiation sensitivity of CR-39 and that it is the diethyleneglycol dicarbonate links which are damaged by radiation. (author)

The Effect of Radiator on CR-39 Registration of Fast Neutrons

International Nuclear Information System (INIS)

El-Badrya, B.A.; Hegazya, T.M.; Morsya, A.A.; Zaki, M.F.

2008-01-01

Three different configurations of a personal neutron dosimeter using CR-39 plastic detector were placed in Plastiplast pouch composed from inside to outside of Aluminum ( 27 Al, 40 Ξ m), polyethylene (PE, 20 Ξ m), Cellulose Nitrate (CN, 40 Ξ m). One dosimeter was composed of a CR-39 detector and a PE radiator (1 mm thick), another of two CR-39 detectors with one serving as radiator, and the other of CR-39 alone (without radiator). These dosimeters have been irradiated with fast neutrons of average energy 4.5 MeV with neutron fluence ranging from 5.5 x 10 6 to 0.5 x 10 8 cm - 2 emitted from 241 Am-Be neutron source. The polymeric materials have been chosen on the basis of their hydrogen contents, which are as followed: CR-39, 48%, Polyethylene, 66.7% and CN, 32% by atomic ratio to produce protons via (n, p) elastic scattering with hydrogen and increasing the detection efficiency of CR-39. After irradiation, the dose equivalent response of the detectors has been studied by using conventional etching for two periods, 6h and 8h for these configurations. The thicknesses and compositions of the radiators are chosen so as to suppress the CR-39 response below 4 MeV by preventing the recoils of hydrogen nuclei, out of the hydrogen-rich radiators (PE, CR-39), from reaching the post-etch surface of the detector. Track counting was performed using an automated system. It was found that the dosemeter responses were linear as a function of a neutron equivalent dose and that the CR-39 detector has the same response with radiator or without radiator and thus appears as a promising fast neutron dosimeter. The results are discussed and compared with the literature

Calibration of detectors type CR-39 for methodology implementation for Radon-222 determination in CRCN-NE, Brazil; Calibração de detectores do tipo CR-39 para implementação da metodologia de determinação de radônio-222 no CRCN-NE

Energy Technology Data Exchange (ETDEWEB)

Silva, Karolayne E.M. da; Santos, Mariana L. de O.; Amaral, Déric S. do; Vilela, Eldice C.; França, Elvis J. de; Hazin, Clovis A.; Farias, Emerson E.G. de, E-mail: keesthefany@gmail.com, E-mail: marianasantos_ufpe@hotmail.com, E-mail: dericsoares@gmail.com, E-mail: ecvilela@cnen.gov.br, E-mail: ejfrana@cnen.gov.br, E-mail: chazin@cnen.gov.br, E-mail: emersonemiliamo@yahoo.com.br [Centro Regional de Ciências Nucleares do Nordeste (CRCN-NE/CNEN-PE), Recife, PE (Brazil)

2017-07-01

Radon-222 is a radioactive gas, a product of the decay of uranium-238, which emits alpha particles and represents more than 50% of the dose of natural radiation received by the population. Therefore, monitoring of this gas is essential. For indoor measurement, solid state detectors can be used, the most common of which is CR-39. For monitoring using CR-39, alpha particles, generated by radon-222 and the daughter radionuclides, strike the surface of the detector and generate traces. To relate the trace density per exposure area in environments with unknown activity concentration, it is necessary to determine the calibration factor. The objective of this study was to calibrate CR-39 type detectors for the implementation of the radon determination methodology in Centro Regional de Ciencias Nucleares do Nordeste - CRCN-NE of Brazilian Nuclear Energy Commission - CNEN. In order to determine the CR-39 calibration factor, 19 exposures of the detectors were performed in the CRCN-NE calibration chamber (RN1-CRCN) at an activity of 5.00 kBq m{sup -3}, with the exposure time varying from 24 to 850 hours. For the detection of the detectors, sodium hydroxide was used in a thermostat bath at 90 ° C for 5 hours. The count of number of traits per unit of field was performed with the aid of optical microscopy with an increase of 100 times, being read 30 fields per dosimeters. As a result, the calibration factor was obtained, and the linear response of the trace density as a function of exposure was observed. The results allow the use of CR-39 in the determination of radon-222 by CRCN-NE.

Personnel neutron dosimetry using electrochemically etched CR-39 foils

International Nuclear Information System (INIS)

Hankins, D.E.; Homann, S.; Westermark, J.

1986-01-01

A personnel neutron dosimetry system has been developed based on the electrochemical etching of CR-39 plastic at elevated temperatures. The doses obtained using this dosimeter system are more accurate than those obtained using other dosimetry systems, especially when varied neutron spectra are encountered. This Cr-39 dosimetry system does not have the severe energy dependence that exists with albedo neutron dosimeters or the fading and reading problems encountered with NTA film. The dosimetry system employs an electrochemical etch procedure that be used to process large numbers of Cr-39 dosimeters. The etch procedure is suitable for operations where the number of personnel requires that many CR-39 dosimeters be processed. Experience shows that one full-time technician can etch and evaluate 2000 foils per month. The energy response to neutrons is fairly flat from about 80 keV to 3.5 MeV, but drops by about a factor of three in the 13 to 16 MeV range. The sensitivity of the dosimetry system is about 7 tracks/cm 2 /mrem, with a background equivalent to about 8 mrem for new CR-39 foils. The limit of sensitivity is approximately 10 mrem. The dosimeter has a significant variation in directional dependence, dropping to about 20% at 90 0 . This dosimeter has been used for personnel neutron dosimetry at the Lawrence Livermore National Laboratory for more tha 18 months. 6 refs., 23 figs., 2 tabs

A new method for determining the uranium and thorium distribution in volcanic rock samples using solid state nuclear track detectors

International Nuclear Information System (INIS)

Misdaq, M.A.; Bakhchi, A.; Ktata, A.; Koutit, A.; Lamine, J.; Ait nouh, F.; Oufni, L.

2000-01-01

A method based on using solid state nuclear track detectors (SSNTD) CR- 39 and LR-115 type II and calculating the probabilities for the alpha particles emitted by the uranium and thorium series to reach and be registered on these films was utilized for uranium and thorium contents determination in various geological samples. The distribution of uranium and thorium in different volcanic rocks has been investigated using the track fission method. In this work, the uranium and thorium contents have been determined in different volcanic rock samples by using CR-39 and LR-115 type II solid state nuclear track detectors (SSNTD). The mean critical angles of etching of the solid state nuclear track detectors utilized have been calculated. A petrographical study of the volcanic rock thin layers studied has been conducted. The uranium and thorium distribution inside different rock thin layers has been studied. The mechanism of inclusion of the uranium and thorium nuclei inside the volcanic rock samples studied has been investigated. (author)

Measurement of indoor radon concentration by CR-39 track detector

International Nuclear Information System (INIS)

Yamamoto, Masayoshi; Yoneda, Shigeru; Nakanishi, Takashi.

1990-01-01

A convenient and cheap method for measuring indoor radon ( 222 Rn) concentration with a CR-39 track detector is described. The detector consisted of two sheets of CR-39 enclosed separately in two plastic pots : one covered by a filter (cup method) and another no covering (bare method). The bare method was used here to supplement the cup method. To compare with the result of the CR-39 detector, alpha-ray spectrometry was carried out with a Si(Au) detector in a controlled radon exposure chamber. Indoor radon concentration measured in 133 houses in several districts of Ishikawa Prefecture have been found to range from 6 Bq/m 3 to as high as 113 Bq/m 3 with a median value of 24 Bq/m 3 . The problems to measure indoor radon concentration using the CR-39 detector are also discussed with emphasis on the position of setting the detector in the room and the possible thoron contribution to the detector. (author)

Calculating CR-39 Response to Radon in Water Using Monte Carlo Simulation

International Nuclear Information System (INIS)

Razaie Rayeni Nejad, M. R.

2012-01-01

CR-39 detectors are widely used for Radon and progeny measurement in the air. In this paper, using the Monte Carlo simulation, the possibility of using the CR-39 for direct measurement of Radon and progeny in water is investigated. Assuming the random position and angle of alpha particle emitted by Radon and progeny, alpha energy and angular spectrum that arrive at CR-39, the calibration factor, and the suitable depth of chemical etching of CR-39 in air and water was calculated. In this simulation, a range of data were obtained from SRIM2008 software. Calibration factor of CR-39 in water is calculated as 6.6 (kBq.d/m 3 )/(track/cm 2 ) that is corresponding with EPA standard level of Radon concentration in water (10-11 kBq/m 3 ). With replacing the skin instead of CR-39, the volume affected by Radon and progeny was determined to be 2.51 mm 3 for one m 2 of skin area. The annual dose conversion factor for Radon and progeny was calculated to be between 8.8-58.8 nSv/(Bq.h/m 3 ). Using the CR-39 for Radon measurement in water can be beneficial. The annual dose conversion factor for Radon and progeny was calculated to be between 8.8-58.8 nSv/ (Bq.h/m 3 ).

Gamma dosimetry with CR-39 etch track detector

International Nuclear Information System (INIS)

Matiullah; Dogar, A.H.; Ahmad, N.; Amin, M.; Kudo, Katsuhisa

1999-01-01

To preserve and improve the safety of food for commercial purposes, it is exposed to high gamma-ray doses. The gamma-ray doses used for this purpose range from 0.15 kGy to 50 kGy. At such high doses, the etching characteristics of CR-39 are severely affected. This property, therefore, can be used to develop a CR-39-based gamma dosimeter. In this context, systematic studies were carried out and the bulk etching rate was determined as a function of gamma-ray dose using different methods. (author)

Track sensitivity and the surface roughness measurements of CR-39 with atomic force microscope

CERN Document Server

Yasuda, N; Amemiya, K; Takahashi, H; Kyan, A; Ogura, K

1999-01-01

Atomic Force Microscope (AFM) has been applied to evaluate the surface roughness and the track sensitivity of CR-39 track detector. We experimentally confirmed the inverse correlation between the track sensitivity and the roughness of the detector surface after etching. The surface of CR-39 (CR-39 doped with antioxidant (HARZLAS (TD-1)) and copolymer of CR-39/NIPAAm (TNF-1)) with high sensitivity becomes rough by the etching, while the pure CR-39 (BARYOTRAK) with low sensitivity keeps its original surface clarity even for the long etching.

Alpha-particle radiobiological experiments using thin CR-39 detectors

International Nuclear Information System (INIS)

Chan, K. F.; Siu, S. Y. M.; McClella, K. E.; Tse, A. K. W.; Lau, B. M. F.; Nikezic, D.; Richardson, B. J.; Lam, P. K. S.; Fong, W. F.; Yu, K. N.

2006-01-01

The present paper studied the feasibility of applying comet assay to evaluate the DNA damage in individual HeLa cervix cancer cells after alpha-particle irradiation. We prepared thin CR-39 detectors (<20 μm) as cell-culture substrates, with UV irradiation to shorten the track formation time. After irradiation of the HeLa cells by alpha particles, the tracks on the underside of the CR-39 detector were developed by chemical etching in (while floating on) a 14 N KOH solution at 37 deg. C. Comet assay was then applied. Diffusion of DNA out of the cells could be generally observed from the images of stained DNA. The alpha-particle tracks corresponding to the comets developed on the underside of the CR-39 detectors could also be observed by just changing the focal plane of the confocal microscope. (authors)

Dose-equivalent response CR-39 track detector for personnel neutron dosimetry

International Nuclear Information System (INIS)

Oda, K.; Ito, M.; Yoneda, H.; Miyake, H.; Yamamoto, J.; Tsuruta, T.

1991-01-01

A dose-equivalent response detector based on CR-39 has been designed to be applied for personnel neutron dosimetry. The intrinsic detection efficiency of bare CR-39 was first evaluated from irradiation experiments with monoenergetic neutrons and theoretical calculations. In the second step, the radiator effect was investigated for the purpose of sensitization to fast neutrons. A two-layer radiator consisting of deuterized dotriacontane (C 32 D 66 ) and polyethylene (CH 2 ) was designed. Finally, we made the CR-39 detector sensitive to thermal neutrons by doping with orthocarbone (B 10 H 12 C 2 ), and also estimated the contribution of albedo neutrons. It was found that the new detector - boron-doped CR-39 with the two-layer radiator - would have a flat response with an error of about 70% in a wide energy region, ranging from thermal to 15 MeV. (orig.)

Calculation of thermal effects occurring during the manufacture of CR-39 sheets

Energy Technology Data Exchange (ETDEWEB)

Szilagyi, S.; Somogyi, G. (Magyar Tudomanyos Akademia, Debrecen. Atommag Kutato Intezete)

1984-01-01

To manufacture a good-quality, uniform CR-39 track detector, the polymerization rate should be chosen below a critical value to avoid the development of undesirable thermal gradients and internal temperature fluctuations in the sheet being cast. To improve curing cycles, especially for thick CR-39 sheets, a computer programme was developed by which we could study the trends of thermal effects under different casting conditions. Our calculations are based on the solution of the one dimensional heat transport equation, taking into account the relations proposed by Dial et al (1955) for describing the chemical kinetics of CR-39 polymerization. We have revised the empirical parameters available to such calculations. With new 'Dial constants' we have calculated the critical initial bath temperature (which results in thermal runaway at the central plane of the sheet being cast) as a function of the CR-39 thickness and IPP initiator concentration. Results are also presented for the temperature profile developing in the depth of cast CR-39 sheets.

Calculation of thermal effects occurring during the manufacture of CR-39 sheets

International Nuclear Information System (INIS)

Szilagyi, S.; Somogyi, G.

1984-01-01

To manufacture a good-quality, uniform CR-39 track detector, the polymerization rate should be chosen below a critical value to avoid the development of undesirable thermal gradients and internal temperature fluctuations in the sheet being cast. To improve curing cycles, especially for thick CR-39 sheets, a computer programme was developed by which we could study the trends of thermal effects under different casting conditions. Our calculations are based on the solution of the one dimensional heat transport equation, taking into account the relations proposed by Dial et al (1955) for describing the chemical kinetics of CR-39 polymerization. We have revised the empirical parameters available to such calculations. With new 'Dial constants' we have calculated the critical initial bath temperature (which results in thermal runaway at the central plane of the sheet being cast) as a function of the CR-39 thickness and IPP initiator concentration. Results are also presented for the temperature profile developing in the depth of cast CR-39 sheets. (author)

The response of CR-39 nuclear track detector to 1-9 MeV protons

International Nuclear Information System (INIS)

Sinenian, N.; Rosenberg, M. J.; Manuel, M.; McDuffee, S. C.; Casey, D. T.; Zylstra, A. B.; Rinderknecht, H. G.; Gatu Johnson, M.; Seguin, F. H.; Frenje, J. A.; Li, C. K.; Petrasso, R. D.

2011-01-01

The response of CR-39 nuclear track detector (TasTrak) to protons in the energy range of 0.92-9.28 MeV has been studied. Previous studies of the CR-39 response to protons have been extended by examining the piece-to-piece variability in addition to the effects of etch time and etchant temperature; it is shown that the shape of the CR-39 response curve to protons can vary from piece-to-piece. Effects due to the age of CR-39 have also been studied using 5.5 MeV alpha particles over a 5-year period. Track diameters were found to degrade with the age of the CR-39 itself rather than the age of the tracks, consistent with previous studies utilizing different CR-39 over shorter time periods.

Neutron detection using CR-39 and Atomic Force Microscopy (AFM)

International Nuclear Information System (INIS)

Vazquez L, C.; Fragoso, R.; Felix, R.; Golzarri, J.I.; Espinosa, G.; Castillo, F.

2007-01-01

AFM has been applied in many CR-39 track formation analyses. In this paper, the use of AFM in the neutron detection and analysis of the track formation is reported. The irradiation was made with an 1.5 GBq (0.5 Ci) 241 Am-Be neutron source, with and without a polyethylene radiator. The surface analysis was made to the CR-39 fresh material without irradiation, after the irradiation, and after a very short etching time. The results show important differences between the irradiation, with and without polyethylene radiator, and the latent tracks of the neutron in the CR-39 polycarbonate. The development of track formation after very short etching time and pits characterization were measured too using the AFM facilities. (Author)

Detection of light charged particles from plasma focus by CR-39

Energy Technology Data Exchange (ETDEWEB)

Antanasijevic, R.; Vukovic, J.; Popovic, S.; Popovic, M. (Belgrade Univ. (Yugoslavia). Inst. za Fiziku); Puric, J.; Cuk, M. (Faculty of Physical Science, Belgrade (Yugoslavia))

1991-01-01

An analysis of a deuteron (D{sup +}) beam, emitted from a plasma focus has been carried out, using a CR-39 plastic nuclear track detector. The CR-39 was pretreated using different processes to destroy the existing background before exposing it to the particles produced in the plasma focus. From measurements of the diameters of the tracks, the estimated energy of the D{sup +} ions is about 0.5 MeV. The total number of emitted D{sup +} ions was 10 particles/pulse. Some preliminary results on imaging etched CR-39 with an Atomic Force Microscope (NanoScope AFM) are also presented. (author).

Detection of light charged particles from plasma focus by CR-39

International Nuclear Information System (INIS)

Antanasijevic, R.; Vukovic, J.; Popovic, S.; Popovic, M.

1991-01-01

An analysis of a deuteron (D + ) beam, emitted from a plasma focus has been carried out, using a CR-39 plastic nuclear track detector. The CR-39 was pretreated using different processes to destroy the existing background before exposing it to the particles produced in the plasma focus. From measurements of the diameters of the tracks, the estimated energy of the D + ions is about 0.5 MeV. The total number of emitted D + ions was 10 particles/pulse. Some preliminary results on imaging etched CR-39 with an Atomic Force Microscope (NanoScope AFM) are also presented. (author)

Density of Ni-Cr Alloy in the Mushy State

Institute of Scientific and Technical Information of China (English)

无

2003-01-01

The density of Ni-Cr alloy in the mushy state has been measured using the modified sessile drop method. The density of Ni-Cr alloy in the mushy state was found to decrease with increasing temperature and Cr concentration in alloy.The molar volume of Ni-Cr alloy in the mushy state therefore increases with increasing the Cr concentration in alloy.The ratio of the difference of density divided by the temperature difference between liquidus and solidus temperatures decreases with increasing Cr concentration. The density of the alloy increased with the precipitation of a solid phase in alloy during the solidification process. The temperature dependence of the density of alloy in the mushy state was not linear but biquadratic.

Development of neutron dosimeter using CR-39 for measurement of ambient dose equivalent

International Nuclear Information System (INIS)

Maki, Daisuke; Shinozaki, Wakako; Ohguchi, Hiroyuki; Yamamoto, Takayoshi; Nakamura, Takayoshi

2010-01-01

A CR-39 has good advantages such as cumulative type dosimeter, small fading effect and gamma-ray insensitive. Therefore, we developed the wide energy-range environmental neutron dosimeter using eight CR-39s for area monitoring in this study. This dosimeter is made of octagonal columnar polyethylene block which height is 60 mm and bottom side is 25 mm. The dosimeter contains two types of CR-39s for fast neutron detection and slow neutron detection. Four CR-39s for fast neutron detection are used for detection of recoil protons produced by H (n, p) reactions. Four CR-39s for slow neutron detection are used with boron nitride converter to detect alpha-rays produced by 10 B (n, α) 7 Li reactions. Ambient dose equivalent is obtained by adding the number of etch-pits observed in four CR-39s for fast neutron detection to the number of etch-pits observed in four CR-39s for slow neutron detection with appropriate constants respectively. Dosimeters were irradiated with some energetic neutrons and evaluated results of ambient dose equivalent were compared with results from neutron transport calculations. Energy response of dosimeter shows good agreement with neutron fluence to ambient dose equivalent conversion coefficients. Directional dependence of dosimeter is at the same level as the rem-counter. (author)

Tetraethyl ammonium hydroxide (TEAH) as etchant of CR-39 for the determination of fluence of alpha particles

Energy Technology Data Exchange (ETDEWEB)

Joshirao, Pranav M.; Vyas, Chirag K.; Eappen, K.P. [Department of Energy Science, Sungkyunkwan University, Suwon 440746 (Korea, Republic of); Shin, Jae Won [Department of Physics, Sungkyunkwan University, Suwon 440746 (Korea, Republic of); Hong, Seung-Woo [Department of Energy Science, Sungkyunkwan University, Suwon 440746 (Korea, Republic of); Department of Physics, Sungkyunkwan University, Suwon 440746 (Korea, Republic of); Manchanda, Vijay K., E-mail: vkm49@skku.edu [Department of Energy Science, Sungkyunkwan University, Suwon 440746 (Korea, Republic of); School of Electronics and Electrical Engineering, Sungkyunkwan University, Suwon 440746 (Korea, Republic of)

2014-04-01

Highlights: • Etching time of CR-39 with TEAH–NaOH mixture (at 80 °C) is less than 20 min. • Etched products enhance etching rate. • V{sub B} and V{sub T} values increase exponentially with temperature. • Activation energy of bulk etching and track etching were determined as 0.87 ± 0.02 eV. - Abstract: Choice of chemical etchant and temperature are pivotal to the successful employment of organic/polymeric solid state nuclear track detectors for determining the fluence of charged particles like protons, alpha and other heavy ions. Poly(diethyleneglycol-bis-(allylcarbonate)) (CR-39) is one of the most sensitive detectors for monitoring the alpha particles but suffers from the drawback of long etching period. An attempt has been made in the present work to investigate a mixture, 20% (v/v) tetraethylammonium hydroxide (40%) – 80% NaOH (6 M) (TEAH–NaOH) at varying temperature as an alternate etchant. It was found that bulk/track etch rate increased and as a consequence etching time decreased significantly (about 10 times) when the mixture was used at 80 °C. Mechanistically, improved efficiency of TEAH–NaOH was attributed to its larger organophilicity and lower etching activation energy as compared to NaOH.

Design and development of wide energy neutron REM equivalent spectrometer-dosimeters based on polycarbonates and Cr-39

International Nuclear Information System (INIS)

Faermann, S.

1985-03-01

This work describes a system composed of a Rem response personnel neutron dosemeter, based on boron radiators and a polycarbonate track detector, for monitoring dose equivalents in the energy range 1 eV to 14 MeV, an electrochemical etching system for revealing damage sites in solid state track etch detectors, a reader for magnifying the etched pits and a microprocessor for evaluating the dose equivalents and their uncertainties. The performance and directional dependence of the dosemeter when exposed to monoenergetic and polyenergetic neutron fields in the epithermal and fast energy regions are discussed. Saturation effects in polycarbonate foils are presented and a comparison is made between the response of polycarbonate and CR-39 foils, used as passive detectors in the dosemeter. A new passive miniature fast neutron spectrometer-dosimeter is also described. The device is based on the detection of proton tracks by electrochemical etching of CR-39 foils covered with thin polyethylene layers of different thicknesses. By means of this device it is possible to assess the fast neutron energy spectrum in 10 energy intervals in the energy range 0.5-15 MeV. Dose equivalents can be determined in the dose equivalent range 20 mRem to 8 Rem, approximately (author)

Calibration factor determination for solid nuclear track detectors CR-39 type exposed to Rn-222

International Nuclear Information System (INIS)

Cazula, Camila Dias; Campos, Marcia Pires de; Mazzilli, Barbara Paci

2014-01-01

In the detection method with solid nuclear track detector, when a heavy particle rests on the detector surface, causes a breakdown in their molecular structure forming a trace. One of the typical applications of these detectors is the measurement of the concentration of Rn -222 in air, a noble radioactive gas, part of the U-238 series, emitting alpha particles and important in epidemiological studies to protect individuals from natural radiation. To determine the concentration of Rn -222 in the air in a room is necessary to know the density of lines (traces / cm 2 ) on the detector surface, the exposure time and the calibration factor. The determination of the calibration factor for CR-39 detectors was taken from the exposure of these to a known concentration of Rn-222. Therefore, the detectors were placed inside a cell of Lucas adapted and subsequently exposed to a concentration of Rn-222 15 kBq / m 3 , by means of the apparatus RN-150 Pylon Electronics Incorporation, which has a source of Ra-226 and releases known concentrations of Rn-222. Six calibration factor determinations were performed, the average value obtained was 0.0534 ±0.0021 (traces / cm 2 per Bq / m 3 day). The results are consistent with literature values for the same type of detector and showed good reproducibility

Simple preparation of thin CR-39 detectors for alpha-particle radiobiological experiments

International Nuclear Information System (INIS)

Chan, K.F.; Lau, B.M.F.; Nikezic, D.; Tse, A.K.W.; Fong, W.F.; Yu, K.N.

2007-01-01

Alpha-particle radiobiological experiments involve irradiating cells with alpha particles and require accurate positions where the alpha particles hit the cells. In the present work, we prepared thin CR-39 detectors from commercially available CR-39 SSNTDs with a thickness of 100 μm by etching them in 1 N NaOH/ethanol at 40 deg. C to below 20 μm. The desired final thickness was achieved within ∼8 h. Such etching conditions can provide relatively small roughness of the detector as revealed by atomic force microscope, and thus provide transparent detectors for radiobiological experiments. UV radiation was employed to shorten track formation time on these thin CR-39 detectors. After exposure to UV light (UVA + B radiation) for 2-3 h with doses from 259 to 389 W/cm 2 , 5 MeV alpha-particle tracks can be seen to develop on these CR-39 detectors clearly under the optical microscope within 2 h in 14 N KOH at 37 deg. C. As an example for practical use, custom-made petri dishes, with a hole drilled at the bottom and covered with a thin CR-39 detector, were used for culturing HeLa cells. The feasibility of using these thin CR-39 detectors is demonstrated by taking photographs of the cells and alpha-particle tracks together under the optical microscope, which can allow the hit positions on the cells by the alpha particles to be determined accurately

Polymerization, structure and track recording properties of CR-39 cured with UV photoinitiators

International Nuclear Information System (INIS)

Stejny, J.; Carrell, J.; Palmer, M.J.

2000-01-01

CR-39 monomer was cured isothermally at temperatures from 54.5 to 115 deg. C with UV sensitive photoinitiators to high conversions. The use of photoinitiators allowed the cure of CR-39 isothermally at high temperatures and eliminated the danger of thermal runaway present in the conventionally used thermal initiation with peroxides. It was found that the properties of the UV photoinitiated CR-39 were similar to the conventionally polymerized resin

Determination of detection efficiency for radon and radon daughters with CR 39 track detector - a Monte Carlo study

International Nuclear Information System (INIS)

Nikezic, D.

1994-01-01

The detection effciency, ρ, (or a calibration coefficient k) for radon measurements with a solid state nuclear track detector CR 39 was determined by many authors. There is a considerable discrepancy among reported values for ρ. This situation was a challenge to develop a software program to calculation ρ. This software is based on Bethe-Bloch's expression for the stopping power for heavy charged particles in a medium, as wll as on the Monte Carlo Method. Track parameters were calculated by using an iterative procedure as given in G. Somogyi et al., Nucl. Instr. and Meth. 109 (1973) 211. Results for an open detector and for the detector in a diffusion chamber were presented in this article. (orig.)

Studies on nitrogen mapping by various CR-39 track detectors

Energy Technology Data Exchange (ETDEWEB)

Somogyi, G.; Varga, Zs.; Hunyadi, I.; Freyer, K.; Treutler, H.Ch.

1986-01-01

The use of CR-39 track detectors for nitrogen distribution measurements via the /sup 14/N(n,p)/sup 14/C reaction is studied. The proton detection properties of different CR-39 products have been analyzed. The variation of background track density induced in the bulk of detectors is examined under different conditions of neutron irradiation. Analysis of our experimental data has led to the conclusion that the sources of proton background tracks are the fast neutron component of the neutron source, chlorine impurities in the detector and nitrogen diffused from the air into the upper layer of the detector. Efforts have been made to decrease the nitrogen content of diffusion origin by removing the upper detector layer and by outgassing the CR-39 sheet in vacuum before irradiation. Finally the ''signal/noise'' ratio for a steel specimen and the sensitivity of nitrogen determination are given.

The influence of chemical etching time on efficiency of radon detection using CR-39

Energy Technology Data Exchange (ETDEWEB)

Reway, Adriana P.; Kappke, Jaqueline; Narloch, Danielle C., E-mail: adrireway@hotmail.com, E-mail: jaquelinekappke@gmail.com, E-mail: daninarloch@hotmail.com [Universidade Tecnologica Federal do Parana (UTFPR), Curitiba, PR (Brazil). Departamento Academico de Fisica; Del Claro, Flavia; Paschuk, Sergei A., E-mail: flaviadelclaro@gmail.com, E-mail: spaschuk@gmail.com [Universidade Tecnologica Federal do Parana (UTFPR), Curitiba, PR (Brazil). Programa de Pos-Graduaca em Engenharia Eletrica e Informatica Industrial; Correa, Janine N., E-mail: janine_nicolosi@hotmail.com [Universidade Tecnologica Federal do Parana (UTFPR), Curitiba, PR (Brazil). Departamento Academico de Construcao Civil

2015-07-01

Natural radiation is the principal source of human exposure to ionizing radiation. Radon is noble radioactive gas that emanates from the soil and rocks entering the atmosphere of dwellings where it could be accumulated. The inhalation of {sup 222}Rn represents a significant health risk. Solid-State Nuclear Track Detectors (SSNTD) represents an efficient method for alpha particle detection and measurements of the activity concentration of {sup 222}Rn. The aim of present work was to study the etching time impact on CR-39 efficiency in radon activity measurements. The investigation was performed using 80 CR-39 detectors, which were exposed to a source of radon. After the exposition, alpha particle tracks development was achieved by chemical etching using 6.25M NaOH solution and ethanol (2%) at 70°C. Etching alpha particle tracks were identified and counted manually using the optical microscope with magnification of 100x and glass overlay mask. The etching time ranged from 7 to 14 hours. The results show that there is an increase in the number of visible tracks with increased etching time. The number of traces obtained for 7 hours and 8 hours of revelation was 1430 +/- 90 and 2090 +/- 160, respectively. However, for etching time of 13 and 14 hours was not observed statistical increase in the number of visible tracks. The number of tracks in this situation was 3630 +/- 180 and 3870 +/- 160 to 13 and 14 hours etching. Thus, for assumed etching parameters, the etching optimal time was observed 14 hours. (author)

The influence of chemical etching time on efficiency of radon detection using CR-39

International Nuclear Information System (INIS)

Reway, Adriana P.; Kappke, Jaqueline; Narloch, Danielle C.; Del Claro, Flavia; Paschuk, Sergei A.; Correa, Janine N.

2015-01-01

Natural radiation is the principal source of human exposure to ionizing radiation. Radon is noble radioactive gas that emanates from the soil and rocks entering the atmosphere of dwellings where it could be accumulated. The inhalation of 222 Rn represents a significant health risk. Solid-State Nuclear Track Detectors (SSNTD) represents an efficient method for alpha particle detection and measurements of the activity concentration of 222 Rn. The aim of present work was to study the etching time impact on CR-39 efficiency in radon activity measurements. The investigation was performed using 80 CR-39 detectors, which were exposed to a source of radon. After the exposition, alpha particle tracks development was achieved by chemical etching using 6.25M NaOH solution and ethanol (2%) at 70°C. Etching alpha particle tracks were identified and counted manually using the optical microscope with magnification of 100x and glass overlay mask. The etching time ranged from 7 to 14 hours. The results show that there is an increase in the number of visible tracks with increased etching time. The number of traces obtained for 7 hours and 8 hours of revelation was 1430 +/- 90 and 2090 +/- 160, respectively. However, for etching time of 13 and 14 hours was not observed statistical increase in the number of visible tracks. The number of tracks in this situation was 3630 +/- 180 and 3870 +/- 160 to 13 and 14 hours etching. Thus, for assumed etching parameters, the etching optimal time was observed 14 hours. (author)

Determination of boron in aqueous solutions by solid state nuclear track detectors technique, using a filtered neutron beam

International Nuclear Information System (INIS)

Moraes, M.A.P.V. de; Pugliesi, R.; Khouri, M.T.F.C.

1985-11-01

The solid state nuclear track detectors technique has been used for determination of boron in aqueous solutions, using a filtered neutron beam. The particles tracks from the 10 B(n,α)Li 7 reaction were registered in the CR-39 film, chemically etched in a (30%) KOH solution 70 0 C during 90 minutes. The obtained results showed the usefulness of this technique for boron determination in the ppm range. The inferior detectable limit was 9 ppm. The combined track registration efficiency factor K has been evaluated in the solutions, for the CR-39 detector and its values is K= (4,60 - + 0,06). 10 -4 cm. (Author) [pt

Alpha-particle response characteristics of CR-39

International Nuclear Information System (INIS)

Abou El-Khier, A.A.; Gaber, M.; El-Khatib, A.M.; Fawzy, M.A.

1987-01-01

The form of the response curve of the polycarbonate CR-39 for α-particles at relatively low energies has been established. The investigation included measurements of both bulk- and track-etch rates. The latter was measured as a function of α-particle energies. (author)

A CR-39 track dosemeter for routine individual neutron monitoring

International Nuclear Information System (INIS)

Luszik-Bhadra, M.; Alberts, W.G.; Dietz, E.; Guldbakke, S.; Matzke, M.; d'Errico, F.

1994-01-01

A personal neutron dosemeter for routine individual monitoring is proposed. It is based on a CR-39 track detector covered on three separate areas by converters with different boron contents and inserted into a commercial TLD albedo dosemeter capsule. The dose readings from three areas of the electrochemically etched CR-39 detector are combined to yield a dose equivalent response which is almost independent of the incident neutron energy in the range from thermal neutrons up to 20 MeV. In addition, the dose contributions of thermal, intermediate and fast neutrons can be determined separately. Unlike the TLD albedo dosemeter, which in general requires prior in-field calibration and whose use is then restricted to that field, this dosemeter can be used in neutron fields without any knowledge of the spectral distribution with the same calibration factor. The angular dependence of the dosemeter's response has been measured and compared with that of the directional dose equivalent H'(10). The lower limit of detection is 0.15 mSv. It is possible to obtain an independent, second dose reading from the same Cr-39 detector for neutron energies above 100 keV. The dosemeter has also been successfully tested for use in accident dosimetry applying chemical etching and an optical density reading of the CR-39 detector. (author)

Measurement of track opening contours of oblique incident 4He and 7Li-ions in CR-39: Relevance for calculation of track formation parameters

International Nuclear Information System (INIS)

Hermsdorf, D.; Reichelt, U.

2010-01-01

Solid State Nuclear Track Detectors (SSNTD) irradiated in realistic radiation fields exhibits after chemical etching very complex track images resulting from different species of particles and their energy spectra and randomly distributed angles of incidence or emission. Reading out such an etched detector surface with a light microscope, quite different track opening contours are observed. Beside the number of tracks, typically their major and minor axes are measured. In this work following problems arising from such experimental situations will be investigated: ·the measurement of track contour parameters for oblique incident 4 He and 7 Li-ions of different energies and angles in CR-39 detectors ·the theoretical description of the angular variation of both axes. ·the possibility to extract physical and spectroscopic information from major and minor track axes. This analysis is based on an intensive experimental program and the comprehensive study of theoretical models available for description of track revealing processes in CR-39.

Calculation of thermal effects occuring during the manufacture of CR-39 sheets

Energy Technology Data Exchange (ETDEWEB)

Szilagyi, S.; Somogyi, G.

1984-01-01

To manufacture a good-quality, uniform CR-39 track detector, the polymerization rate should be below a critical value to avoid the development of undesirable thermal gradients and internal temperature fluctuations in the sheet being cast. To improve curing cycles a computer program was developed to study the trends of thermal effects under different casting conditions. These calculations are based on the solution of the one-dimensional heat transport equation and take into account the relations proposed by Dial et. al. for describing the chemical kinetics of CR-39 polymerization. The authors have revised the empirical parameters available to such calculations. With new ''Dial constants'' they have calculated the critical initial bath temperature (which results in thermal runaway at the central plane of the sheet being cast) as a function of the CR-39 thickness and IPP initiator concentration. Results are also presented for the temperature profile in the depth of cast CR-39 sheets.

New approach of modeling charged particles track development in CR-39 detectors

International Nuclear Information System (INIS)

Azooz, A.A.; Hermsdorf, D.; Al-Jubbori, M.A.

2013-01-01

In this work, previous modeling of protons and alpha particles track length development in CR-39 solid state nuclear track detectors SSNTD is modified and further extended. The extension involved the accommodation of heavier ions into the model. These ions include deuteron, lithium, boron, carbon, nitrogen and oxygen ions. The new modeling does not contain any case sensitive free fitting parameters. Model calculation results are found to be in good agreement with both experimental data and SRIM software range energy dependence predictions. The access to a single unified and differentiable track length development equation results in the ability to obtain direct results for track etching rates. - Highlights: • New modeling of ions track length evolution measured by different authors. • Ions considered are p, d, α, Li, B, C, N, O. • Equations obtained to describe L(t) and etch rate for all ions at wide energy range. • Equations obtained do not involve any free fitting parameters. • Ions range values obtained compare well with results of SRIM software

Note: Fast neutron efficiency in CR-39 nuclear track detectors

Energy Technology Data Exchange (ETDEWEB)

Cavallaro, S. [Dipartimento di Fisica ed Astronomia,Università di Catania, Via S. Sofia 44, 95123 Catania, Italy and INFN-LNS, Via S. Sofia 42, 95123 Catania (Italy)

2015-03-15

CR-39 samples are commonly employed for fast neutron detection in fusion reactors and in inertial confinement fusion experiments. The literature reported efficiencies are strongly depending on experimental conditions and, in some cases, highly dispersed. The present note analyses the dependence of efficiency as a function of various parameters and experimental conditions in both the radiator-assisted and the stand-alone CR-39 configurations. Comparisons of literature experimental data with Monte Carlo calculations and optimized efficiency values are shown and discussed.

Cutting thin sheets of allyl diglycol carbonate (CR-39) with a CW CO2, laser

International Nuclear Information System (INIS)

Kukreja, L.M.; Bhawalkar, D.D.; Basu, C.; Goswami, J.N.

1984-01-01

Recent studies have shown that Allyl Diglycol Carbonate, commercially known as CR-39 (the most sensitive among etch track detectors) can detect relativistic oxygen and other heavier nuclei. We are using large sheets of special grade CR-39 (DOP) in our experiment in Space Shuttle-Spacelab-3. As CR-39 is a highly brittle substance, special care is required to cut CR-39 shetts, especially in case of large sheets and circular cuts. A study of cutting of CR-39 sheets using laser light is described in this paper. It has been found that this method is sufficiently fast to handle large number of sheets and also equally safe for big sheets. A maximum speed up to 200 cm/min with a 5 x 10 4 W/cm 2 laser is obtained during the present study. This study also shows that laser cutting does not affect the track properties of CR-39. (orig.)

Development of hybrid track detector using CR39 and photographic plate

International Nuclear Information System (INIS)

Kuge, Kenichi; Endo, Yusuke; Hayashi, Kentaro; Hasegawa, Akira; Kumagai, Hiroshi

2004-01-01

Hybrid track detector using CR39 and color photography was prepared by coating multi-layered color photographic emulsions on one side of CR39. Etch pits and color tracks were observed at the same time. Photographic plate with different sensitivity emulsions and couplers were exposed to light, α-, β- and γ-rays. We observed sensitivity difference to the radiation by color changes on one plate. (authors)

Proton an alpha detections by track recording technique in CR-39

International Nuclear Information System (INIS)

Oliveira, W.A. de; Franco, M.A.R.; Herdade, S.B.; Khouri, M.C.F.; Goncalez, O.L.

1986-07-01

The plastic CR-39 is utilized as proton track detector in the study of the reaction 27 A (e, p) and 59 Co (e, p), near threshold. Preliminary results are presented for the energy calibration (mean track diameter as a function of proton energy) of CR-39 with mono-energetic protons of a Van de Graaff accelerator, in the energy range 1-3 MeV. (author) [pt

Effect of radiation on the electrical properties of plastic detector CR-39

International Nuclear Information System (INIS)

Mahmoud, S.A.; Hamed, A.E.; Abou El-Kier, A.A.; Mousse, M.G.; Kassem, M.E.; El-Shafey, E.M.

1994-01-01

The effect of high alpha-particle fluence on plastic detector CR-39 was studied by measuring the electrical properties of the detector as a function of irradiation dose and frequency using an impedance meter in the frequency range 0.005-500 kHz. When the plastic detector CR-39 is exposed to high irradiation doses, it loses its advantage as a track detector, because of the overlapping of the tracks occurring in the detector at high irradiation fluence. Through the present measurements of dielectric permittivity and conductivity at different frequencies and temperatures, CR-39 could be used as a dosimeter for high irradiation doses

Effect of radiation on the electrical properties of plastic detector CR-39

Energy Technology Data Exchange (ETDEWEB)

Mahmoud, S.A.; Hamed, A.E.; Abou El-Kier, A.A.; Mousse, M.G.; Kassem, M.E.; El-Shafey, E.M. (Physics Department Faculty of Science, Alexandria University, Alexandria (Egypt))

1994-10-15

The effect of high alpha-particle fluence on plastic detector CR-39 was studied by measuring the electrical properties of the detector as a function of irradiation dose and frequency using an impedance meter in the frequency range 0.005-500 kHz. When the plastic detector CR-39 is exposed to high irradiation doses, it loses its advantage as a track detector, because of the overlapping of the tracks occurring in the detector at high irradiation fluence. Through the present measurements of dielectric permittivity and conductivity at different frequencies and temperatures, CR-39 could be used as a dosimeter for high irradiation doses.

Ablation and cone formation mechanism on CR-39 by ArF laser irradiation

Energy Technology Data Exchange (ETDEWEB)

Shakeri Jooybari, B., E-mail: baninshakery@gmail.com, E-mail: hafarideh@aut.ac.ir [Department of Energy Engineering and Physics, Amirkabir University of Technology, P.O. Box 15875-4413, Tehran, Islamic Republic of Iran (Iran, Islamic Republic of); Nuclear Science and Technology Research Institute NSRT, Tehran (Iran, Islamic Republic of); Afarideh, H., E-mail: baninshakery@gmail.com, E-mail: hafarideh@aut.ac.ir [Department of Energy Engineering and Physics, Amirkabir University of Technology, P.O. Box 15875-4413, Tehran, Islamic Republic of Iran (Iran, Islamic Republic of); Lamehi-Rachti, M. [Nuclear Science and Technology Research Institute NSRT, Tehran (Iran, Islamic Republic of); Ghergherehchi, M. [Department of Energy Engineering and Physics, Amirkabir University of Technology, P.O. Box 15875-4413, Tehran, Islamic Republic of Iran (Iran, Islamic Republic of); College of Information and Communication Engineering, Sungkyunkwan University, Suwon (Korea, Republic of)

2015-03-07

In this work, chemical properties, surface modification, and micro structures formation on ablated polyallyl di-glycol carbonate (CR-39) polymer by ArF laser irradiation (λ = 193 nm) at various fluences and pulse number were investigated. CR-39 samples have been irradiated with an ArF laser (193 nm) at a repetition rate of 1 Hz. Threshold fluence of ablation and effective absorption coefficient of CR-39 were determined. Conical microstructures (Taylor cone) formed on laser-ablated CR-39 exhibit: smooth, Taylor cone shape walls and sharp tips together with interference and well defined fringe-structure with a period of 230 nm, around cone base. Mechanism of cone formation and cone evolution of CR-39 ablated surface were investigated by change of fluences (at a given pulse number) and pulse number (at a given fluence). Cone height, cone base, and region of interface were increased in micrometer steps by increasing the total fluence. Depression on the base of the cone and the circular fringe were simulated. FTIR spectra were measured and energy dispersive x-ray analysis of irradiated and un-irradiated samples was performed.

Technical aspects in the obtention of tissue autoradiography using solid state nuclear track detectors

International Nuclear Information System (INIS)

Saint Martin, Gisela; Bernaola, Omar A.; Pozzi, Emiliano; Thorp, Silvia; Cabrini, Romulo L.; Tomasi, V.H.

2007-01-01

The autoradiography images produced in solid state nuclear track detectors by heavy ions originated in tissue provide relevant information about the spatial biodistribution of heavy particle emitters. Some preliminary aspects of the autoradiography technique are evaluated by two experiments which are in progress, using Lexan and CR 39 foils as solid state nuclear track detectors. In the first case, a tissue sample from rat kidney intoxicated with UO 2 (NO 3 ) 2 was embedded in paraffin and put in contact with a 1 mm thick CR 39 foil. After a two months exposure the foil was chemically developed resulting in scarce tracks. A satisfactory image cannot be obtained in these conditions. More prolonged exposure time is needed to obtain better images of such samples. The second experience consisted in the irradiation of fresh kidney tissue slices from healthy rats in contact with 250 μm thick Lexan foils, in a thermal neutrons flux. The irradiation was performed at the RA-3 facility of the Ezeiza Atomic Center (CAE). The contribution to image produced by tracks of particles due to reactions between neutrons and tissue elements (i.e. 14 N) was evaluated. The etching conditions should be modified in order to desensitize the detector material. (author) [es

LET spectrum measurements in Cr-39 PNTD with AFM

Energy Technology Data Exchange (ETDEWEB)

Johnson, Carl Edward [Los Alamos National Laboratory; De Witt, Joel M [OSU, PHYSICS; Benton, Eric R [OSU, PHYSICS; Yasuda, Nakahiro [NIRS, HIMAC; Benton, Eugene V [UNIV OF SAN FRANCISCO

2010-01-01

Energetic protons, neutrons, and heavy ions undergoing collisions with target nuclei of varying Z can produce residual heavy recoil fragments via intra-nuclear cascade/evaporation reactions. The particles produced in these non-elastic collisions generally have such extremely short range ({approx}< 10 {mu}m) that they cannot be directly observed by conventional detection methods including CR-39 plastic nuclear track detector (PNTD) that has been chemically etched for analysis by standard visible light microscopy. However, high-LET recoil fragments having range on the order of several cell diameters can be produced in tissue during radiotherapy using proton and carbon beams. We have developed a method to analyze short-range, high-LET tracks in CR-39 plastic nuclear track detector (PNTD) using short duration chemical etching ({approx}< 1 {mu}m) followed by automated atomic force microscope (AFM) scanning. The post-scan data processing used in this work was based on semi-automated matrix analysis opposed to traditional grey-scale image analysis. This method takes advantage of the 3-D data obtained via AFM to achieve robust discrimination of nuclear tracks from other features. Through automation of AFM scanning, sufficient AFM scan frames were obtained to attain an LET spectrum spanning the LET range from 200-1500 keV/{mu}m. In addition to our experiments, simulations were carried out with the Monte Carlo transport code, FLUKA. To demonstrate this method, CR-39 PNTD was exposed to the proton therapy beam at Loma Linda University Medical Center (LLUMC) at 60 and 230 MeV. Additionally, detectors were exposed to I GeV protons at the NASA Space Radiation Laboratory (NSRL) at Brookhaven National Laboratory (BNL). For these exposures CR-39 PNTD, Al and Cu target foils were used between detector layers.

LET spectrum measurements in Cr-39 PNTD with AFM

International Nuclear Information System (INIS)

Johnson, Carl Edward; DeWitt, Joel M.; Benton, Eric R.; Yasuda, Nakahiro; Benton, Eugene V.

2010-01-01

Energetic protons, neutrons, and heavy ions undergoing collisions with target nuclei of varying Z can produce residual heavy recoil fragments via intra-nuclear cascade/evaporation reactions. The particles produced in these non-elastic collisions generally have such extremely short range (∼< 10 μm) that they cannot be directly observed by conventional detection methods including CR-39 plastic nuclear track detector (PNTD) that has been chemically etched for analysis by standard visible light microscopy. However, high-LET recoil fragments having range on the order of several cell diameters can be produced in tissue during radiotherapy using proton and carbon beams. We have developed a method to analyze short-range, high-LET tracks in CR-39 plastic nuclear track detector (PNTD) using short duration chemical etching (∼< 1 μm) followed by automated atomic force microscope (AFM) scanning. The post-scan data processing used in this work was based on semi-automated matrix analysis opposed to traditional grey-scale image analysis. This method takes advantage of the 3-D data obtained via AFM to achieve robust discrimination of nuclear tracks from other features. Through automation of AFM scanning, sufficient AFM scan frames were obtained to attain an LET spectrum spanning the LET range from 200-1500 keV/μm. In addition to our experiments, simulations were carried out with the Monte Carlo transport code, FLUKA. To demonstrate this method, CR-39 PNTD was exposed to the proton therapy beam at Loma Linda University Medical Center (LLUMC) at 60 and 230 MeV. Additionally, detectors were exposed to I GeV protons at the NASA Space Radiation Laboratory (NSRL) at Brookhaven National Laboratory (BNL). For these exposures CR-39 PNTD, Al and Cu target foils were used between detector layers.

Effect of Gamma Rays on Fast Neutron Registration in CR-39

CERN Document Server

Kobzev, A P; El-Halem, A A; Abdul-Ghaphar, U S; Salama, T A

2002-01-01

A set of CR-39 plastic detectors with front PE radiator was exposed to Am-Be neutron source, which has an emission rate of 0.86\\cdot 10^{7} sec^{-1}, and the neutron dose equivalent rate 1 m apart from the source is equal to 11 mrem/hr. Another set of samples was irradiated by a neutron dose of 4 rem, then exposed to different gamma-ray doses using ^{60}Co source. It was found that the track density grows with the increase of neutron dose and etching time. It was also found that the bulk etching rate V_{B}, the track diameter and the sensitivity of the CR-39 plastic detector with respect to the neutron irradiation increased with increasing gamma-ray dose in the range 1?10 Mrad. These results show that CR-39 can be considered as a promising fast neutron dosimeter and gamma-ray dosimeter.

Sensitivity determination of CR-39 from Normal and inclined incidence

International Nuclear Information System (INIS)

Abou, A.A.; El-Kheir, A.A.; Daas, A.F.; Awwad, Z.; Reda, A.M.

2000-01-01

An experimental study have been carried out on alpha- particle track opening (Major and minor axes) using alpha-particles of different energies incident with different angels in addition to the normal incidence. The sensitivity of CR-39 in present work is determined for each of normal and inclined incidence. The results indicated a difference in the sensitivity according to angle of incidence. The variation of alpha- particle tracks (major and minor axes) are calculated and compared with our measured values. Also, it is found that the sensitivity of CR-39 detector is change due to the storage time at room temperature

Study of projectile fragmentation in the reaction (158 A GeV) Pb + Pb using CR-39

CERN Document Server

Qureshi, I E; Javed, M T; Manzoor, S; Sher, G; Aleem, F; Khan, H A

2005-01-01

The fragmentation of Pb ions at 158 A GeV energy produced in the interaction with Pb target has been studied using a CR-39 track detector. A stack comprising of 64 detectors was prepared such that a target of 1 cm thickness was sandwiched between the sheets of CR-39. The purpose of this exposure geometry was to calibrate CR-39 with respect to relativistic heavy ions as well as to study the fragmentation of Pb ions at 158 A GeV energy. The exposure was carried out at the SPS beam facility of CERN at normal incidence with a fluence of . Two detectors from the exposed stack have been selected for this study: one before and the other after the target material. After etching, the detectors were scanned using an optical microscope and the etched track lengths and the diameters of the track openings were measured manually. Considering that the lengths of tracks provide the best charge resolution for Z>65, we have measured track lengths for a sufficiently large number of fragments to identify individual charge states...

Microstructure, ferromagnetic and photoluminescence properties of ITO and Cr doped ITO nanoparticles using solid state reaction

Science.gov (United States)

Babu, S. Harinath; Kaleemulla, S.; Rao, N. Madhusudhana; Rao, G. Venugopal; Krishnamoorthi, C.

2016-11-01

Indium-tin-oxide (ITO) (In0.95Sn0.05)2O3 and Cr doped indium-tin-oxide (In0.90Sn0.05Cr0.05)2O3 nanoparticles were prepared using simple low cost solid state reaction method and characterized by different techniques to study their structural, optical and magnetic properties. Microstructures, surface morphology, crystallite size of the nanoparticles were studied using X-ray diffractometer (XRD), field emission scanning electron microscope (FE-SEM). From these methods it was found that the particles were about 45 nm. Chemical composition and valence states of the nanoparticles were studied using energy dispersive analysis of X-rays (EDAX) and X-ray photoelectron spectroscopy (XPS). From these techniques it was observed that the elements of indium, tin, chromium and oxygen were present in the system in appropriate ratios and they were in +3, +4, +3 and -2 oxidation states. Raman studies confirmed that the nanoparticle were free from unintentional impurities. Two broad emission peaks were observed at 330 nm and 460 nm when excited wavelength of 300 nm. Magnetic studies were carried out at 300 K and 100 K using vibrating sample magnetometer (VSM) and found that the ITO nanoparticles were ferromagnetic at 100 K and 300 K. Where-as the room temperature ferromagnetism completely disappeared in Cr doped ITO nanoparticles at 100 K and 300 K.

Calibration of CR-39 for radon-related parameters using sealed cup technique

International Nuclear Information System (INIS)

Abo-Elmagd, M.; Daif, M. M.

2010-01-01

Effective radium content, mass and areal radon exhalation rates of soil and rock samples are important radon-related parameters and can be used as a better indicator of radon risk. A sealed cup fitted to a CR-39 detector and to the sample under measurement is an advantageous passive device for the measurement of these parameters. The main factors affecting the results are the detector calibration factor and the sample weight. The results of an active technique (Lucas cell) and the CR-39 detector have been found to be correlated resulting in a reliable detector calibration factor. The result illustrates the dependence of the CR-39 calibration factor with the sample weight which is difficult to use in practice, because each sample weight has its own calibration factor of CR-39. It is reported to demonstrate the advantage of a back diffusion correction. After correcting the results for back diffusion effects, one obtains an approximately constant calibration factor for the sample volumes up to one-third the total sealed cup volume. For this condition the calibration factor is equal to 0.237 track cm -2 per Bq m -3 d with about 1% uncertainty. (authors)

Range energy for heavy ions in CR-39

International Nuclear Information System (INIS)

Gil, L.R.; Marques, A.

1987-01-01

Range-energy relations in CR-39, for ions from He to Ar, are obtained after their effective nuclear charge. Comparison with earlier calculations and numerical results in the energy range 0,1 to 200 Mev/ Nucleon are also given. (M.W.O.)

CR-39 nuclear track detector used for neutron dosimetry: system calibration

International Nuclear Information System (INIS)

Saint Martin, G.; Lopez, F.; Bernaola, Omar A.

2009-01-01

Stacks composed by 1 mm thickness CR-39 foils and polyethylene and PVC films were evaluated to be used as neutron dosemeters. Irradiations were made with a calibrated 241 Am-Be source in a dose range from 0 to 3.1 mSv and the etching conditions were optimized. The measurements of number of tracks per surface unit in the CR-39 detectors showed a good linear behaviour as a function of the dose. The minimum detectable dose equivalent (MDDE) was calculated. (author)

Measurement of fast neutron spectrum using CR-39 detectors and a new image analysis program (autoTRAKn)

International Nuclear Information System (INIS)

Paul, Sabyasachi; Tripathy, S.P.; Sahoo, G.S.; Bandyopadhyay, T.; Sarkar, P.K.

2013-01-01

An attempt is made to estimate the neutron spectrum using the CR-39 (Solid state nuclear track) detector and a new image analyzing program. For this purpose the earlier developed program (autoTRAK) is modified by introducing the required features such as angular correction for the recoil particles, fluence-to-dose conversion coefficient, detection sensitivity of CR-39 detectors, etc. to make it applicable for neutron spectrometry and dosimetry. This upgraded program (autoTRAK n ) is tested with a mono-energetic source (D–T) and two other standard neutron sources, viz. 241 Am–Be and 252 Cf. The program is validated by reproducing these standard spectra, and comparing with the spectra reported by other investigators using different measuring techniques. The ratios of dose equivalent (H ⁎ (10)) to fluence (Φ) are also estimated from the spectra and are compared with the reference values for these neutron sources. An additional feature of this program is explored for counting high density overlapping tracks more precisely and effectively compared to other commonly used image analyzing softwares. This method is found to be simple and promising, which can always be used as a supplementary measuring technique. The details of the modified program, reproduction and comparison of the neutron spectra, reproducibility of the methodology and example of overlapping track counting are presented and discussed. -- Highlights: •A novel image analysis technique (autoTRAK n ) is developed to evaluate CR-39 detectors used for neutron spectrometry and dosimetry. •The methodology is tested to reproduce three standard neutron spectra, (a) D–T, (b) 241 Am–Be, and (c) 252 Cf. •A good matching is observed between dosimetric values obtained by the program and the available reference values. •The program autoTRAK n is also observed to be efficient to distinguish high density overlapping tracks without any segregation procedure. •The methodology seems to be simple, which

Calibration of CR-39 plastic detectors in various modes and radon measurement in the north-western region of Bangladesh

International Nuclear Information System (INIS)

Islam, G.S.; Islam, M.A.; Haque, A.K.F.

1998-04-01

Solid State track detectors have been extensively used for the measurement of time integrated radon levels in dwellings under different conditions. The CR-39 plastic detectors were calibrated for bare as well as cup with membrane mode, along with a mono dispersal aerosol 0.2μm in size in an exposure chamber, to find the relationship between track densities and the radon concentration as well as potential alpha energy concentration (WL) of radon. Measurement of the indoor radon and radon daughter concentrations were performed in houses in the north-western region of Bangladesh. In total 163 detectors were placed for measurement of indoor radon activities and 230 detectors for measurement of radon daughter concentrations. To study the underground radon activity, 114 CR-39 detectors in cylinders were used. The indoor radon activity in Naogaon was, in general, found to be higher than that in Rajshahi. The working levels in the mud-built houses were greater than that in brick-built houses. The underground radon activity of Naogaon was found to be 6 times higher than that of Rajshahi. No direct correlation was observed between the underground and indoor radon activity. The average values of radon activity and the working level for the north-western zone of Bangladesh are found to be 91 Bq. m -3 and 16 mWL respectively. (author)

Microstructure, ferromagnetic and photoluminescence properties of ITO and Cr doped ITO nanoparticles using solid state reaction

Energy Technology Data Exchange (ETDEWEB)

Babu, S. Harinath [Thin Films Laboratory, Centre for Crystal Growth, VIT University, Vellore-632014, Tamilnadu, India. (India); Kaleemulla, S., E-mail: skaleemulla@gmail.com [Thin Films Laboratory, Centre for Crystal Growth, VIT University, Vellore-632014, Tamilnadu, India. (India); Rao, N. Madhusudhana [Thin Films Laboratory, Centre for Crystal Growth, VIT University, Vellore-632014, Tamilnadu, India. (India); Rao, G. Venugopal [Materials Physics Division, Indira Gandhi Centre for Atomic Research, Kalpakkam-603102, Tamilnadu (India); Krishnamoorthi, C. [Thin Films Laboratory, Centre for Crystal Growth, VIT University, Vellore-632014, Tamilnadu, India. (India)

2016-11-01

Indium-tin-oxide (ITO) (In{sub 0.95}Sn{sub 0.05}){sub 2}O{sub 3} and Cr doped indium-tin-oxide (In{sub 0.90}Sn{sub 0.05}Cr{sub 0.05}){sub 2}O{sub 3} nanoparticles were prepared using simple low cost solid state reaction method and characterized by different techniques to study their structural, optical and magnetic properties. Microstructures, surface morphology, crystallite size of the nanoparticles were studied using X-ray diffractometer (XRD), field emission scanning electron microscope (FE-SEM). From these methods it was found that the particles were about 45 nm. Chemical composition and valence states of the nanoparticles were studied using energy dispersive analysis of X-rays (EDAX) and X-ray photoelectron spectroscopy (XPS). From these techniques it was observed that the elements of indium, tin, chromium and oxygen were present in the system in appropriate ratios and they were in +3, +4, +3 and −2 oxidation states. Raman studies confirmed that the nanoparticle were free from unintentional impurities. Two broad emission peaks were observed at 330 nm and 460 nm when excited wavelength of 300 nm. Magnetic studies were carried out at 300 K and 100 K using vibrating sample magnetometer (VSM) and found that the ITO nanoparticles were ferromagnetic at 100 K and 300 K. Where-as the room temperature ferromagnetism completely disappeared in Cr doped ITO nanoparticles at 100 K and 300 K.

Effects of additives and impurities on the properties of CR-39 neutron dosimeters

International Nuclear Information System (INIS)

Tarle, G.

1982-01-01

Several problems have plagued users of commercial CR-39 for neutron dosimetry work. Large variations in sensitivity have been observed in samples received from different manufacturers, from different batches from the same manufacturer and even within a given sheet. The latter variations have taken several forms. Clear etching regions of lower sensitivity near the gasket and sometimes extending well away from the gasket in drip-like patterns have been observed. Large demarcated patches of differing sensitivity and sensitivity variations with depth have been found in many commercial samples of CR-39. In addition, we have observed a general roughening of the post-etch surface and a patchiness of bulk etching associated with contact patterns of adjacent sheets, which have been stored for extended (greater than or equal to 6 mos) periods of time. All of these problems combine to make commercially available CR-39 unreliable as a neutron dosimeter. In an attempt to identify and correct the causes of these problems, a systematic study of the effects of additives, impurities and manufacturing conditions on the uniformity of CR-39 track detectors has been undertaken, and is reported in this paper

Use of CR-39 foils for personnel neutron dosimetry: improved electrochemical etching chambers and procedures

International Nuclear Information System (INIS)

Hankins, D.E.; Homann, S.G.; Westermark, J.

1986-01-01

The electrochemical etching procedures for the new dosimetry system that uses foils of CR-39 plastic has been improved. During 1985, the etching chambers were modified to correct several problems and the changes to the etching procedures were studied, which gave a more uniform track density and size. The currently recommended etch parameters are given. A new generation of CR-39 material from the manufacturer proved to have a considerably lower background track density and a higher sensitivity; the new foils are also more uniform in thickness, which eliminates the need to numerically compensate for thickness variations. The energy dependence of the CR-39 using monoenergetic neutrons from accelerators at Battelle Northwest Laboratories and at Los Alamos National Laboratory was determined. Some variation was found in the energy dependence, but it is believed this was caused by changes in the etching procedures and by uncertainties in the fluences of the neutrons from the accelerators. A means by which the counting of CR-39 tracks may be automated is suggested; this would be very useful in adapting the CR-39 dosimetry system to large-scale use

Fast neutron dosimetry using CR-39 track detectors with polyethylene as radiator

International Nuclear Information System (INIS)

Castillo, F.; Espinosa, G.; Golzarri, J.I.; Osorio, D.; Rangel, J.; Reyes, P.G.; Herrera, J.J.E.

2013-01-01

The chemical etching parameters (etching time, temperature, normality of etchant, etc.) for the use of CR-39 (allyl diglycol carbonate – Lantrack ® ) as a fast neutron dosimeter have been optimized. The CR-39 chips, placed under a 1.5 mm polyethylene radiator, were exposed for calibration to an 241 Am-Be source at different time intervals for a given neutron fluence. After several chemical etching processes of the detectors with different conditions, the optimum characteristics for the chemical etching were found at 6N KOH solution, 60 ± 1 °C, for 12 h. An accurate relationship between the dose and fluence calculations was obtained as a function of the track density. - Highlights: ► Optimum etching time for fast neutron irradiated CR-39 track detectors is found. ► Relationship between dose and fluence obtained as a function of the track density. ► Results are consistent with those reported elsewhere, and extend the dose range

The Use Of Optical Properties Of Cr-39 In Alpha Particle Equivalent Dose Measurements

International Nuclear Information System (INIS)

Shnishin, K.A.

2007-01-01

In this work, optical properties of alpha irradiated Cr-39 were measured as a function of optical photon wavelength from 200-1100 nm. Optical energy gap and optical absorption at finite wavelength was also calculated and correlated to alpha fluence and dose equivalent. Alpha doses were calculated from the corresponding irradiation fluence and specific energy loss using TRIM computer program. It was found that, the optical absorption of unattached Cr-39 was varied with alpha fluence and corresponding equivalent doses. Also the optical energy gab was varied with fluence and dose equivalent of alpha particles. This work introduces a reasonably simple method for the Rn dose equivalent calculation by Cr-39 track

Chromium 51 em K2CrO4: reactions of dopant atoms in solid state

International Nuclear Information System (INIS)

Valim, J.B.; Nascimento, R.L.G. do; Collins, C.H.; Collins, K.E.

1986-01-01

The study of the chemistry of 'dopant' 51 Cr(III) atoms in crystalline Cr(VI) compounds began as a sub-field of Hot Atom Chemistry. We shall review the attempts to use 'dopant' chromium-51 atoms as surrogate chromium recoil atoms with the special property of having a low-energy, recoil-dam-age-free history. These dopant atoms have shown behaviors very similar to those of high energy recoil 51 Gr atoms, thus offering little hope of learning about special damage site structures and reactions by behavioral differences. Recent work has shown that at least some of the 'dopant' 51 Cr(III) is present as a second, non-chromate solid phase in 'doped crystal' experiments. Monodisperse 51 Cr(OH) 3 particles mixed with pure K 2 CrO 4 are very reactive. (Author) [pt

Track etch parameters and annealing kinetics assessment of protons of low energy in CR-39 detector

International Nuclear Information System (INIS)

Jain, R.K.; Kumar, Ashok; Singh, B.K.

2012-01-01

Highlights: ► We calibrate CR-39 detector with very low energy protons. ► We establish linear relationship between track diameter and time/energy up to 200 keV. ► We determine activation energy of annealing using different models. ► We justify concept of single annealing activation energy in CR-39. - Abstract: In this paper threshold of the registration sensitivity of very low energy proton in CR-39 is investigated. Irradiation of CR-39 (poly-allyl-diglycol carbonate) was carried out with very low energy mono energetic protons of 20–60 keV from a mini proton accelerator. Nearly 10 4 /cm 2 fluence of protons was used. The variation of track diameter with etching time as well as proton energy response curve was carefully calibrated. The bulk and track etch rates were measured by using proton track diameters. Bulk etch rate was also measured by the thickness of removed surface layer. The thermal annealing of proton track at temperatures ranging from 100 to 200 °C in CR-39 was studied by several models. Activation energy of annealed CR-39 detectors was calculated by slope of track etch rate and temperature plot. The data of proton tracks of 200, 250 and 300 keV from 400 kV Van-de-Graaff accelerator was also used and compared with the track diameters of different energies of proton.

Impact of x-ray dose on the response of CR-39 to 1-5.5 MeV alphas

International Nuclear Information System (INIS)

Rojas-Herrera, J.; Rinderknecht, H. G.; Zylstra, A. B.; Gatu Johnson, M.; Orozco, D.; Rosenberg, M. J.; Sio, H.; Seguin, F. H.; Frenje, J. A.; Li, C. K.; Petrasso, R. D.

2015-01-01

The CR-39 nuclear track detector is used in many nuclear diagnostics fielded at inertial confinement fusion (ICF) facilities. Large x-ray uences generated by ICF experiments may impact the CR-39 response to incident charged particles. To determine the impact of x-ray exposure on the CR-39 response to alpha particles, a thick-target bremsstrahlung x-ray generator was used to expose CR-39 to various doses of 8 keV Cu-K α and K β x-rays. The CR-39 detectors were then exposed to 1-5.5 MeV alphas from an Am-241 source. The regions of the CR-39 exposed to x-rays showed a smaller track diameter than those not exposed to x-rays: for example, a dose of 3.0 ± 0.1 Gy causes a decrease of (19 ± 2)% in the track diameter of a 5.5 MeV alpha particle, while a dose of 60.0 ± 1.3 Gy results in a decrease of (45 ± 5)% in the track diameter. The reduced track diameters were found to be predominantly caused by a comparable reduction in the bulk etch rate of the CR-39 with x-ray dose. A residual effect depending on alpha particle energy is characterized using an empirical formula

Alpha particle track coloration in CR-39: Improved observability

CERN Document Server

Oezguemues, A

1999-01-01

A comparative study of the observability of alpha particle tracks in CR-39 was performed with an optical microscope before and after coloration. The implantation of ink helped in observing the damage zones. At first glance through the microscope, the coloration makes the tracks stand out right away. This coloration is helpful, from the start, in the morphological study of the tracks (size, area, orientation, shape, perimeter). This operation is advantageous in distinguishing the alpha particle tracks from stains or scratches. Thus, the routine counting of the tracks is more easily performed. Consequently, this procedure allowed us: to decrease significantly the standard deviation of the approximate total of the parameters given from the image analysis system (Olympus CUE2); to envision the possibility of reasonably decreasing the etching time in order to limit the loss of information caused by the destruction of the CR-39 during chemical etching and to use a weaker enlarging lens in order to cover a larger fi...

Etching characteristics of nuclear tracks in CR-39 plastics

International Nuclear Information System (INIS)

Tsuruta, Takao; Isobe, Ginko.

1984-01-01

In using CR-39 plastics for individual neutron dosimeters, changes of etching efficiency cause significant error in dose estimation. Etching efficiency is subject to a number of parameters. In this study the influences of the parameters were examined by measuring the diameters of etch-pits formed by alpha-particles and enlarged by aqueous solutions of 25-35% KOH at 55-65 0 C for 4 hr. It has been observed that diameter changes at the rate of 8.3%/ 0 C in temperature, 8.2%/wt% in concentration and -0.60%/day in time after preparation of etchant. The diameter is unaffected by the supplying of up to 280ml/l, of distilled water for evaporation of etchant or by increase up to 5g/l of CR-39 dissolved in etchant. The magnitude of possible error has been estimated by parameter as well as in general, so as to obtain suggestions for improving etching treatment. (author)

Neutron dosimeter utilizing CR-39

International Nuclear Information System (INIS)

Souza, H.V.C. de.

1991-05-01

A personnel neutron dosimeter has been developed with discretization in a wide range of energies of real interest, utilizing the CR-39 polymer, to detect recoil protons in the fast range, and alpha particles in the thermal and epithermal ranges, with possibility to be disposed in the IRD/CNEN's conventional film badge suport. They are presented, abstractly, the difficulties and importance of the neutron dosimetry, beyond the general objectives that motivated this work execution. The details of the materials utilized in the dosimeter confection, and the experimental methodology employed to obtain the performance curves are presented. The results about linearity response of the dosimeter with respect to equivalent dose, in a wide range of doses, and about the verified angular dependence are analysed. (author)

The possibility of using plastic detectors CR-39 as UV dosimeters

International Nuclear Information System (INIS)

Shweikani, R.; Raja, G.; Sawaf, A.A.

2004-01-01

The effects of solar ultraviolet (SUV) and ultraviolet type A (UVA) produced by a solar UV simulator on CR-39 detectors were studied. This was done using three techniques: 1 - Alpha tracks diameters and tracks densities, 2 - UV-Vis spectrometry and 3 - FTIR spectrometry. The detectors were divided into two groups, the first was exposed to UV and then to alpha particles, the second group was exposed to alpha particles first and then to UV. The results showed that the effect of UVA on CR-39 was not clear using the three techniques. While, the effect of SUV was clear when using UV-Vis and FTIR spectrometric, and not clear when using track parameters. (author)

The possibility of using plastic detectors CR-39 as UV dosimeters

International Nuclear Information System (INIS)

Shweikani, R.; Raja, G.; Sawaf, A.A.

2002-01-01

The effects of solar ultraviolet (SUV) and ultraviolet type A (UVA) produced by a solar UV simulator on CR-39 detectors were studied. This was done using three techniques: 1 - Alpha tracks diameters and tracks densities, 2 - UV-Vis spectrometry and 3 - FTIR spectrometry. The detectors were divided into two groups, the first was exposed to UV and then to alpha particles, the second group was exposed to alpha particles first and then to UV. The results showed that the effect of UVA on CR-39 was not clear using the three techniques. While, the effect of SUV was clear when using UV-Vis and FTIR spectrometric, and not clear when using track parameters

On registration properties of Intercast Company CR-39

International Nuclear Information System (INIS)

Golovchenko, A.N.

1991-01-01

The CR-39 response function has been determined by using the accelerated particles of intermediate ( 2 H, 4 He, 12 C, 16 O, 20 Ne and 40 Ar) and relativistic ( 19 F) energies. The irradiated detectors were etched in 6N NaOH kept at 70 deg C. The response function is determined in a wide range of the ionization change. 10 refs.; 1 fig.; 2 tabs

Beam profile measurement with CR-39 track detector for low-energy ions

CERN Document Server

Sato, F; Tanaka, T; Iida, T; Yamauchi, T; Oda, K

1999-01-01

A CR-39 track detector was successfully used to measure the outline of thin low-energy ion beams. After the etching, the surface of the detector was examined with an observation system composed of a Normarski microscope, a CCD camera and a digital image processing computer. Beam images obtained with the system were in good agreement on the outline of the beam formed with a beam aperture. Also, the resolving power in the beam outline measurement was roughly explained from the consideration of the ion range and the etch-pit growth in the chemical etching for the CR-39 detector.

Alkaline erosion of CR 39 polymer surfaces

International Nuclear Information System (INIS)

Faiman, Laurence

2009-01-01

We have investigated the mechanism of erosion of CR 39 polymer in alkaline environments. We observed the kinetics of absorption of water and methanol into both unirradiated and γ-irradiated samples. We use a capillary model to interpret our results. We etched our samples in both KOH solutions, and KOH solutions doped with methanol. Etch rate was desensitizing to γ-irradiation when KOH concentration approached saturation, but KOH solutions doped with methanol were not desensitizing, unlike with nuclear tracks. We account for this difference

CR-39 (PADC) Reflection and Transmission of Light in the Ultraviolet-Near-Infrared (UV-NIR) Range.

Science.gov (United States)

Traynor, Nathan B J; McLauchlin, Christopher; Dodge, Kenneth; McGarrah, James E; Padalino, Stephen J; McCluskey, Michelle; Sangster, T C; McLean, James G

2018-04-01

The spectral reflection (specular and diffuse) and transmission of Columbia Resin 39 (CR-39) were measured for incoherent light with wavelengths in the range of 200-2500 nm. These results will be of use for the optical characterization of CR-39, as well as in investigations of the chemical modifications of the polymer caused by ultraviolet (UV) exposure. A Varian Cary 5000 was used to perform spectroscopy on several different thicknesses of CR-39. With proper analysis for the interdependence of reflectance and transmittance, results are consistent across all samples. The reflectivity from each CR-39-air boundary reveals an increase in the index of refraction in the near-UV. Absorption observations are consistent with the Beer-Lambert law. Strong absorption of UV light of wavelength shorter than 350 nm suggests an optical band gap of 3.5 eV, although the standard analysis is not conclusive. Absorption features observed in the near infrared are assigned to molecular vibrations, including some that are new to the literature.

Auto-counting of high density overlapping tracks and neutron spectrum measurement using CR-39 detectors and in-house image analysis program

International Nuclear Information System (INIS)

Paul, Sabyasachi; Tripathy, S.P.; Sahoo, G.S.; Joshi, D.S.; Bandyopadhyay, T.

2014-01-01

An effort is made in this work to overcome the difficulty of counting highly dense and overlapping tracks in solid polymeric track detectors (SPTD) such as CR-39. A program is developed to automatically count the track density which is found to be faster and more precise compared to other commonly used image analysing software. The results obtained by the present methodology are compared with those obtained using other software. (author)

Personnel neutron dosimetry applications of track-size distributions on electrochemically etched CR-39 foils

International Nuclear Information System (INIS)

Hankins, D.E.; Homann, S.G.; Westermark, J.

1988-01-01

The track-size distribution on electrochemically etched CR-39 foils can be used to obtain some limited information on the incident neutron spectra. Track-size distributions on CR-39 foils can also be used to determine if the tracks were caused by neutrons or if they are merely background tracks (which have a significantly different track-size distribution). Identifying and discarding the high-background foils reduces the number of foils that must be etched. This also lowers the detection limit of the dosimetry system. We have developed an image analyzer program that can more efficiently determine the track density and track-size distribution, as well as read the laser-cut identification numbers on each foil. This new image analyzer makes the routine application of track-size distributions on CR-39 foils feasible. 2 refs., 3 figs

Response of CR-39 based personnel neutron dosemeter in terms of directional dose equivalent, in free air and on phantom

International Nuclear Information System (INIS)

Pal, Rupali R.; Sathian, Deepa; Jayalakshmi, V.; Chougaonkar, M.P.

2011-01-01

CR-39 is the most sensitive of nuclear track detectors for protons and is recommended as an effective neutron dosimeter because of it's low threshold energy of 100 keV neutrons. The fraction of protons that gives detectable tracks in CR-39 depends on the energy of the proton angle of incidence and etching conditions. As a consequence the registration efficiency of neutrons in the CR-39 plastics used for neutron personnel monitoring is strongly influenced by the direction of radiation incidence. This paper presents the relative response of CR-39 at varying neutron incident angles, for 241 Am-Be neutron source spectra in free air and on ISO phantom, in terms of operational quantities. It is observed that the angular dependence of CR-39 for irradiations in air and on phantom is essentially the same indicating that the phantom does not affect the directional response of CR-39. (author)

An energy and direction independent fast neutron dosemeter based on electrochemically etched CR-39 nuclear track detectors

International Nuclear Information System (INIS)

James, K.; Matiullah; Durrani, S.A.

1987-01-01

A computer-based model is presented, which simulates the dose equivalent response of electrochemically etched CR-39 to fast neutrons of various energies and angles of incidence. Most previous calculations of the response of CR-39 have neglected the production of recoiling oxygen and carbon nuclei as well as α particles in the CR-39. We calculate that these 'heavy recoils' and α particles are the major source of electrochemically etchable tracks in bare CR-39 at neutron energies above approx. 2 MeV under typical etching conditions. Our calculations have been extended to predict the response of CR-39 used in conjunction with various combinations of polymeric front radiators and we have determined the radiator stack configuration with produces the most energy independent response. Again, the heavy recoils and α particles cannot be neglected and, for energies above approx. 2 MeV, these produce typically about 20% of the total response of our optimum stack. This type of fast neutron dosemeter is, however, strongly direction dependent. We have integrated the response over all appropriate angles to predict the dose equivalent response for two representative neutron fields, and we suggest a method for minimising the angular dependence. (author)

Characteristics of latent damage trails due to high energy 208Pb and 238U ions in CR-39 and muscovite mica

International Nuclear Information System (INIS)

Chohan, A.S.; Akhtar, S.M.

1988-01-01

Experiments have been performed to study the characteristics of latent damage trails produced by (a) 17.14 MeV/nucleon- 208 Pb ions in mica and CR-39 track detectors and (b) 13.7 MeV/nucleon- 238 U in CR-39 track detectors. The parameters studied include (a) V t , average etching velocity along the track, (b) thermal stability of the latent damage trails, (c) the total etchable ranges, and (d) V g the general etching velocity of CR-39 track detectors previously annealed at different temperatures. It has been observed that the latent damage trails in CR-39 are greatly affected at temperatures around 200 0 C in CR-39 track detectors. The general etching velocity of a CR-39 detector has been found to increase with increasing annealing temperatures. (author)

Impact of x-ray dose on the response of CR-39 to 1–5.5 MeV alphas

Energy Technology Data Exchange (ETDEWEB)

Rojas-Herrera, J., E-mail: jimmy06@mit.edu; Rinderknecht, H. G.; Zylstra, A. B.; Gatu Johnson, M.; Orozco, D.; Rosenberg, M. J.; Sio, H.; Seguin, F. H.; Frenje, J. A.; Li, C. K.; Petrasso, R. D. [Plasma Science and Fusion Center, Massachusetts Institute of Technology, Cambridge, Massachusetts 02139 (United States)

2015-03-15

The CR-39 nuclear track detector is used in many nuclear diagnostics fielded at inertial confinement fusion (ICF) facilities. Large x-ray fluences generated by ICF experiments may impact the CR-39 response to incident charged particles. To determine the impact of x-ray exposure on the CR-39 response to alpha particles, a thick-target bremsstrahlung x-ray generator was used to expose CR-39 to various doses of 8 keV Cu-K{sub α} and K{sub β} x-rays. The CR-39 detectors were then exposed to 1–5.5 MeV alphas from an Am-241 source. The regions of the CR-39 exposed to x-rays showed a smaller track diameter than those not exposed to x-rays: for example, a dose of 3.0 ± 0.1 Gy causes a decrease of (19 ± 2)% in the track diameter of a 5.5 MeV alpha particle, while a dose of 60.0 ± 1.3 Gy results in a decrease of (45 ± 5)% in the track diameter. The reduced track diameters were found to be predominantly caused by a comparable reduction in the bulk etch rate of the CR-39 with x-ray dose. A residual effect depending on alpha particle energy is characterized using an empirical formula.

Advances in the development of Cr-39 based neutron dosimeters

International Nuclear Information System (INIS)

Hadlock, D.E.; Parkhurst, M.A.

1987-12-01

A combination thermoluminescent dosimeter (TLD) and track etch dosimeter (TED), which can be used for detecting neutrons over a wide energy range, has been developed through recent research in passive neutron dosimetery. This dosimeter uses Li-600 TLDs to detect thermal and low energy neutrons reflected from the body, and the TED polymer of CR-39, to detect fast neutrons from proton recoil interactions with the polyethylene radiator or with CR-39 itself. Some form of the combination dosimeter is currently in use at several US Department of Energy (DOE) facilities, and its use is expected to expand over the next year to include all DOE facilities where significant neutron exposures may occur. The extensive research conducted on the TED component over the past six years has continually focused on material improvements, reduction in processing time and dosimeter handling, and ease of sample readout with the goal of automating the process as much as possible. 1 fig

Efficient alpha particle detection by CR-39 applying 50 Hz-HV electrochemical etching method

International Nuclear Information System (INIS)

Sohrabi, M.; Soltani, Z.

2016-01-01

Alpha particles can be detected by CR-39 by applying either chemical etching (CE), electrochemical etching (ECE), or combined pre-etching and ECE usually through a multi-step HF-HV ECE process at temperatures much higher than room temperature. By applying pre-etching, characteristics responses of fast-neutron-induced recoil tracks in CR-39 by HF-HV ECE versus KOH normality (N) have shown two high-sensitivity peaks around 5–6 and 15–16 N and a large-diameter peak with a minimum sensitivity around 10–11 N at 25°C. On the other hand, 50 Hz-HV ECE method recently advanced in our laboratory detects alpha particles with high efficiency and broad registration energy range with small ECE tracks in polycarbonate (PC) detectors. By taking advantage of the CR-39 sensitivity to alpha particles, efficacy of 50 Hz-HV ECE method and CR-39 exotic responses under different KOH normalities, detection characteristics of 0.8 MeV alpha particle tracks were studied in 500 μm CR-39 for different fluences, ECE duration and KOH normality. Alpha registration efficiency increased as ECE duration increased to 90 ± 2% after 6–8 h beyond which plateaus are reached. Alpha track density versus fluence is linear up to 10 6  tracks cm −2 . The efficiency and mean track diameter versus alpha fluence up to 10 6  alphas cm −2 decrease as the fluence increases. Background track density and minimum detection limit are linear functions of ECE duration and increase as normality increases. The CR-39 processed for the first time in this study by 50 Hz-HV ECE method proved to provide a simple, efficient and practical alpha detection method at room temperature. - Highlights: • Alpha particles of 0.8 MeV were detected in CR-39 by 50 Hz-HV ECE method. • Efficiency/track diameter was studied vs fluence and time for 3 KOH normality. • Background track density and minimum detection limit vs duration were studied. • A new simple, efficient and low-cost alpha detection method

Observation of anomalons in CR-39 track detectors

International Nuclear Information System (INIS)

Tincknell, M.L.; Price, P.B.

1984-01-01

The authors have observed fragments of 1.85 GeV/nucleon 40 Ar in CR-39 etched track detector and they find anomalously short mean free paths (mfp's) of secondary nuclei with 11 less than or equal to Z less than or equal to 17 in the first 2 cm after their production, at approx.3 standard deviations. This confirms previous reports of this anomalon effect in nuclear emulsion in a new detector with dissimilar potential systematic errors

Synthesis of S/Cr doped mesoporous TiO2 with high-active visible light degradation property via solid state reaction route

International Nuclear Information System (INIS)

Liu Shaoyou; Tang Qunli; Feng Qingge

2011-01-01

S/Cr doped mesoporous TiO 2 (S-TiO 2 , Cr-TiO 2 , S-Cr-TiO 2 ) were successfully synthesized via a simple, effective and environmental benign solid state reaction route. The low angle XRD patterns demonstrated that the resulting samples possess mesostructures. The further characterizations via N 2 adsorption-desorption and XPS showed that the typical S/Cr co-doped mesoporous TiO 2 (S-Cr-TiO 2 (5S-5Cr)) possesses mesopore with the high specific surface area of 118.4 m 2 /g and narrow pore size distribution, and both S and Cr have been incorporated into the lattice of TiO 2 with the amounts of 4.16% sulfur and 7.88% chromium, respectively. And Raman spectroscopy shows that the surface of S-Cr-TiO 2 (5S-5Cr) material possesses stretching vibrational peaks at ∼709, ∼793 cm -1 are assignable to the Ti-O-Cr, O-Cr (Ti)-OH bonds, respectively. Interestingly, the UV-vis displayed that the absorption regions of S/Cr doped mesoporous TiO 2 cover the visible light region. As for the series of S-Cr-TiO 2 samples, the absorption region even extends to near infrared region with strong adsorption. Moreover, compared with the pure titanium dioxide (P25-TiO 2 ), the photodegradation properties of bromocresol green (BCG) on the S/Cr doped mesoporous TiO 2 showed excellent photocatalytic properties under visible light irradiation. Within 50 min visible light irradiation, 82.6% of the initial BCG was degraded for the S-Cr-TiO 2 (6S-4Cr) photocatalyst.

Fast Neutron Dosimetry Using CR-39 Nuclear Track Detector

International Nuclear Information System (INIS)

ZAKI, M.; ABDEL-NABY, A.; MORSY, A.

2010-01-01

Measurement of the neutron dose in and around the neutron sources is important for the purpose of personnel and environmental neutron dosimetry. In the present study, a method for the measurement of neutron dose using the UV-Vis spectra of CR-39 plastic track detector was investigated. A set of CR-39 plastic detectors was exposed to 252 Cf neutron source, which had the yield of 0.68x10 8 /s, and neutron dose equivalent rate 1m apart from the source is equal to 3.8 mrem/h. The samples were etched for 10 h in 6.25 N NaOH at 70 o C. The absorbance of the etched samples was measured using UV-visible spectrophotometer as a function of neutron dose. It was observed that there was a linear relationship between the optical absorption of these detectors and neutron dose. This means that the exposure dose of neutron can be determined by knowing the optical absorption of the sample. These results were compared with previous study. It was found that there was a matching and good agreement with their investigations.

Operational trials of single- and multi-element CR-39 dosemeters for the DIDO and PLUTO reactors at the Harwell Laboratory

International Nuclear Information System (INIS)

Gallacher, G.G.; Perks, C.A.

1993-01-01

Single- and multi-element CR-39 dosemeters, developed at the Harwell Laboratory, and a commercially available multi-element CR-39 dosemeter (obtained from Track Analysis Systems Ltd), were evaluated for their potential as neutron dosemeters for personnel working at Harwell Laboratory's research reactors. Owing to the angular dependence of the CR-39 (processed using electrochemical etching), the single-element dosemeter was found to be impractical. Consequently, a multi-element dosemeter was developed, which consisted of a cube of side 36 mm with CR-39 elements (also processed using electrochemical etching) attached to each of the sides. Although this dosemeter was technically suitable for this type of dosimetry, it was considered to be unacceptably bulky in personnel trials. The commercially available CR-39 dosemeter tested was much smaller (the CR-39 was only chemically etched) and this was considered to be acceptable as a personnel dosemeter. In addition, trials with personnel working at active handling glove boxes indicated that single-element dosemeters might be adequate, but further work would be needed to verify this. (author)

Bulk etching characteristics of CR-39 track detectors in hydroxide solutions

International Nuclear Information System (INIS)

Fonseca, E.S. da; Knoefel, T.M.J.; Tavares, O.A.P.

1983-01-01

A systematic study of the bulk etch rate of CR-39 track detectors in KOH and NaOH aqueous solutions is presented. A number of unirradiated and non-thermally treated CR-39 samples were chemically attacked in KOH and NaOH solutions of concentration and temperature in the range 2-10 N and 50-90 0 C, respectively. From measurements of the thickness of layers removed as a function of the etching time, the bulk etch rate υ β and the induction time T ο for surface removal were obtained for each etching condition. For both NaOH and KOH solution the activation energy of the process was derived as E = 0.76 ± 0.05 eV. It was observed that the induction time decreases both with increasing normality and temperature of the solution. (author) [pt

Diallyl phthalate (DAP) solid state nuclear track detector

CERN Document Server

Koguchi, Y; Ashida, T; Tsuruta, T

2003-01-01

Diallyl phthalate (DAP) solid state nuclear track detector is suitable for detecting heavy ions such as fission fragments, because it is insensitive to right ions such as alpha particles and protons. Detection efficiency of fission tracks is about 100%, which is unaffected under conditions below 240degC lasting for 1h or below 1 MGy of gamma-ray irradiation. Optimum etching condition for the DAP detector for detection of fission fragments is 2-4 h using 30% KOH aqueous solution at 90degC or 8-15 min using PEW-65 solution at 60degC. DAP detector is useful in detecting induced fission tracks for dating of geology or measuring intense heavy ions induced by ultra laser plasma. The fabrication of copolymers of DAP and CR-39 makes it possible to control the discrimination level for detection threshold of heavy ions. (author)

Extended solid solubility of a Co–Cr system by mechanical alloying

International Nuclear Information System (INIS)

Betancourt-Cantera, J.A.; Sánchez-De Jesús, F.; Torres-Villaseñor, G.; Bolarín-Miró, A.M.; Cortés-Escobedo, C.A.

2012-01-01

Highlights: ► Solubility of the Co–Cr system is modified by means of Mechanical Alloying (MA). ► MA induces the formation of new solid solutions of Co–Cr system in non-equilibrium. ► MA promote the formation of metastable Co–Cr phases with greater solubility. - Abstract: Mechanical alloying, MA, has been successfully used to extend the limits of solid solubility in many commercially important metallic systems. The aim of this work is to demonstrate that MA modifies the solid solubility of the Co–Cr system. Co and Cr elemental powders were used as precursors and mixed in an adequate weight ratio to obtain Co 100−x Cr x (0 ≤ x ≤ 100, Δx = 10) to study the effect of mechanical processing in the solubility of the Co–Cr system. Processing was carried out at room temperature in a shaker mixer mill using vials and balls of hardened steel as milling media with a ball:powder weight ratio of 10:1. Crystalline structure characterization of the milled powders was conducted using X-ray diffraction, and phase transformations as a function of composition were analyzed. Thermal analysis confirmed structural changes occurred in the mechanically alloyed powders. The evolution of the phase transformations with composition is reported for each composition. The results showed that after high energy ball milling for 7 h, the solid solubility between Co and Cr could be evidently extended, despite the low solid solubility at the equilibrium conditions of this system. Additionally, the micrographs of the milled powders showed that increasing composition of chromium changes the shape and size of the particles while simultaneously reducing their agglomeration; this effect is possibly attributed to the brittleness of elemental chrome.

Extended solid solubility of a Co-Cr system by mechanical alloying

Energy Technology Data Exchange (ETDEWEB)

Betancourt-Cantera, J.A. [Area Academica de Ciencias de la Tierra y Materiales, UAEH Carr. Pachuca-Tulancingo Km. 4.5, Pachuca, Hidalgo 42184 (Mexico); Sanchez-De Jesus, F., E-mail: fsanchez@uaeh.edu.mx [Area Academica de Ciencias de la Tierra y Materiales, UAEH Carr. Pachuca-Tulancingo Km. 4.5, Pachuca, Hidalgo 42184 (Mexico); Torres-Villasenor, G. [Instituto de Investigaciones en Materiales-UNAM, Apdo. Postal 70-360, 04510 Mexico, DF (Mexico); Bolarin-Miro, A.M. [Area Academica de Ciencias de la Tierra y Materiales, UAEH Carr. Pachuca-Tulancingo Km. 4.5, Pachuca, Hidalgo 42184 (Mexico); Cortes-Escobedo, C.A. [Centro de Investigacion e Innovacion Tecnologica del IPN Cda. CECATI S/N, Col. Sta. Catarina, Azcapotzalco, 02250 Mexico, DF (Mexico)

2012-07-15

Highlights: Black-Right-Pointing-Pointer Solubility of the Co-Cr system is modified by means of Mechanical Alloying (MA). Black-Right-Pointing-Pointer MA induces the formation of new solid solutions of Co-Cr system in non-equilibrium. Black-Right-Pointing-Pointer MA promote the formation of metastable Co-Cr phases with greater solubility. - Abstract: Mechanical alloying, MA, has been successfully used to extend the limits of solid solubility in many commercially important metallic systems. The aim of this work is to demonstrate that MA modifies the solid solubility of the Co-Cr system. Co and Cr elemental powders were used as precursors and mixed in an adequate weight ratio to obtain Co{sub 100-x}Cr{sub x} (0 {<=} x {<=} 100, {Delta}x = 10) to study the effect of mechanical processing in the solubility of the Co-Cr system. Processing was carried out at room temperature in a shaker mixer mill using vials and balls of hardened steel as milling media with a ball:powder weight ratio of 10:1. Crystalline structure characterization of the milled powders was conducted using X-ray diffraction, and phase transformations as a function of composition were analyzed. Thermal analysis confirmed structural changes occurred in the mechanically alloyed powders. The evolution of the phase transformations with composition is reported for each composition. The results showed that after high energy ball milling for 7 h, the solid solubility between Co and Cr could be evidently extended, despite the low solid solubility at the equilibrium conditions of this system. Additionally, the micrographs of the milled powders showed that increasing composition of chromium changes the shape and size of the particles while simultaneously reducing their agglomeration; this effect is possibly attributed to the brittleness of elemental chrome.

Personal Dosemeter of Thermal Neutron Using A Cr-39 Detector with Filter Natural LiF

International Nuclear Information System (INIS)

Sofyan, Hasnel; Thamrin, M.Thoyib

1996-01-01

The research of personal dosemeter for thermal neutron using Cr-39 detector with different thicknesses of natural LiF filter was carried out. The irradiation of Cr-39 detector with neutron source from reactor research TRIGA mark II of Rikkyo University Tokyo, Japan. Nuclear track was counted by automatic method with ASPECT ver.4.22 Series A4T124 software and manual method for correction. The result of research, the maximum of nuclear tracks was obtained at 8 mm of LiF filter was 10 mm with 11,630x10E-5 track/neutron for air radiation. And on phantom radiation, the thickness of filter was 10 mm with 11,630x10E-5 track/neutron. Its values were 3.6 and 7.5 bigger than the response of Cr-39 non filter in air and on phantom radiation, respectively

CR-39 and Lexan calibrated as low-LET radiation dosimeter, for three Mexican irradiation facilities

International Nuclear Information System (INIS)

Tavera, L.; Balcazar, M.; Matamoros, H.; Carrasco, H.

2005-01-01

An experimental calibration of two common nuclear track detectors, CR-39 and Lexan, for gamma and electrons radiation, was performed using various irradiation facilities. The dose response was obtained as a function of two parameters, the bulk etch rate and the UV absorbance for a wide dose range from 10 to 1000 kGy. The bulk etch rate sensitivity, for gamma and electrons, in CR-39 detector is higher than for Lexan detector. Lexan has a well-defined UV absorbance spectrum, but presents saturation for doses higher than 500 kGy, the same saturation characteristic is observed for the corresponding bulk etch rate response. For electron and gamma radiation, CR-39 shows a good response for doses from 10 kGy up to 1000 kGy, where data fit well an exponential curve for electrons and a lineal curve for gamma radiation

Preliminary results of fission induced by (1068 MeV) pi in Cu, Sn, Au and Bi using CR-39 detectors

CERN Document Server

Khan, H A; Shahzad, M I; Manzoor, S; Farooq, M A; Sher, G; Khan, E U; Peterson, R J

1999-01-01

Fission probabilities in pion induced reactions exhibit characteristic variations with respect to pion energies and target fissility values. At incident energies well above the pion-nucleon resonances, the statistical model seems to give good description of the observed data. We have used negative pions of energy 1068 MeV, in order to study fission induced in four target materials with fissility values [(Z-1)2/A] ranging from 12 to 32. All targets were arranged in a single stack in such a way that each target coated on a CR-39 detector was sandwiched by another uncoated CR-39 detector plate. The stack was irradiated at the AGS of Brookhaven National Laboratory (USA). This set-up ensures solid angle coverage of almost 4 pi degrees, so that for each fission event one of the fission fragments is expected to be trapped by the forward detector and one by the detector covering backward hemisphere. The effect of pion momentum transfer to the struck nucleus was observed in the form of asymmetry between events counted...

Characterization of a alpha particle detector CR-39 exposed to a source of radium

International Nuclear Information System (INIS)

Maino, Leandro Marcondes

2009-01-01

In this project, the main goal is the characterization of a alpha particle detector CR-39 exposed to a source of radio. Three detectors were exposed to a source of radium and then chemically treated for different periods. This way, we could analyze these samples and collect the information needed to verify that at least one of the chemical attack, there has been a separation of the energies alpha particles incident with distinct peaks, thus characterizing the CR-39 as alpha spectrometer in the range 2.5 to 6.3 MeV . (author)

Impact of x-ray dose on track formation and data analysis for CR-39-based proton diagnostics

Energy Technology Data Exchange (ETDEWEB)

Rinderknecht, H. G., E-mail: rinderknecht1@llnl.gov; Rojas-Herrera, J.; Zylstra, A. B.; Frenje, J. A.; Gatu Johnson, M.; Sio, H.; Sinenian, N.; Rosenberg, M. J.; Li, C. K.; Séguin, F. H.; Petrasso, R. D. [Massachusetts Institute of Technology, Cambridge, Massachusetts 02139 (United States); Filkins, T.; Steidle, Jessica A.; Traynor, N.; Freeman, C. [State University of New York at Geneseo, Geneseo, New York 14454 (United States); Steidle, Jeffrey A. [Rochester Institute of Technology, Rochester, New York 14623 (United States)

2015-12-15

The nuclear track detector CR-39 is used extensively for charged particle diagnosis, in particular proton spectroscopy, at inertial confinement fusion facilities. These detectors can absorb x-ray doses from the experiments in the order of 1–100 Gy, the effects of which are not accounted for in the previous detector calibrations. X-ray dose absorbed in the CR-39 has previously been shown to affect the track size of alpha particles in the detector, primarily due to a measured reduction in the material bulk etch rate [Rojas-Herrera et al., Rev. Sci. Instrum. 86, 033501 (2015)]. Similar to the previous findings for alpha particles, protons with energies in the range 0.5–9.1 MeV are shown to produce tracks that are systematically smaller as a function of the absorbed x-ray dose in the CR-39. The reduction of track size due to x-ray dose is found to diminish with time between exposure and etching if the CR-39 is stored at ambient temperature, and complete recovery is observed after two weeks. The impact of this effect on the analysis of data from existing CR-39-based proton diagnostics on OMEGA and the National Ignition Facility is evaluated and best practices are proposed for cases in which the effect of x rays is significant.

Impact of x-ray dose on track formation and data analysis for CR-39-based proton diagnostics

International Nuclear Information System (INIS)

Rinderknecht, H. G.; Rojas-Herrera, J.; Zylstra, A. B.; Frenje, J. A.; Gatu Johnson, M.; Sio, H.; Sinenian, N.; Rosenberg, M. J.; Li, C. K.; Séguin, F. H.; Petrasso, R. D.; Filkins, T.; Steidle, Jessica A.; Traynor, N.; Freeman, C.; Steidle, Jeffrey A.

2015-01-01

The nuclear track detector CR-39 is used extensively for charged particle diagnosis, in particular proton spectroscopy, at inertial confinement fusion facilities. These detectors can absorb x-ray doses from the experiments in the order of 1–100 Gy, the effects of which are not accounted for in the previous detector calibrations. X-ray dose absorbed in the CR-39 has previously been shown to affect the track size of alpha particles in the detector, primarily due to a measured reduction in the material bulk etch rate [Rojas-Herrera et al., Rev. Sci. Instrum. 86, 033501 (2015)]. Similar to the previous findings for alpha particles, protons with energies in the range 0.5–9.1 MeV are shown to produce tracks that are systematically smaller as a function of the absorbed x-ray dose in the CR-39. The reduction of track size due to x-ray dose is found to diminish with time between exposure and etching if the CR-39 is stored at ambient temperature, and complete recovery is observed after two weeks. The impact of this effect on the analysis of data from existing CR-39-based proton diagnostics on OMEGA and the National Ignition Facility is evaluated and best practices are proposed for cases in which the effect of x rays is significant

Suitability of CR-39 dosimeters for personal dosimetry around CANDU reactors

International Nuclear Information System (INIS)

Cross, W.G.

1992-08-01

The capabilities and limitations of CR-39 damage track detectors have been evaluated for their use as personal neutron dosimeters around CANDU reactors. Since the energy response is a critical characteristic, the neutron energy spectra expected within CANDU containments were studied. In the boiler rooms, around the moderator cooling systems, and in most of the fueling machine vaults, the spectra vary considerably, but the majority of the dose is expected to be delivered by neutrons above 80 keV, the approximate threshold for electrochemically-etched CR-39 detectors. In the Pickering A fueling machine vault, and in areas in other stations to which neutrons from reactors have been multiply scattered, lower energy neutrons may be important. In nearly all areas where people work, it appears that working times will be limited by gamma rays rather than by neutrons. The characteristics of other neutron dosimeters - bubble and superheated drop detectors, albedo detectors, and Si real-time detectors - were also reviewed. For workers who typically receive neutron doses that are small compared with regulatory limits, CR-39 is the most suitable available dosimeter for demonstrating compliance. All single dosimeters have poor angular response over the range 0 to 180 degrees because of the shielding of the body. Albedo and Si detectors have particularly poor energy responses over the energy range of importance. Bubble and superheated drop detectors have the advantages of immediate readout and high sensitivity, but the disadvantages of inability to integrate doses over a long period, temperature dependence, very limited range and higher cost. (Author) (110 refs., 45 figs.)

Exposure of CR39 Stacks to Oxygen and Sulphur Beams at the CERN-SPS

CERN Multimedia

2002-01-01

We plan to expose 8 stacks of CR39 sheets to oxygen and sulphur ions of 60 and 200~GeV at the CERN-SPS.\\\\ \\\\ The main purpose of the exposures is the calibration of the CR39 sheets used for a large area experimental search for magnetic monopoles at the Gran Sasso Laboratory (experiment MACRO). \\\\ \\\\ The stacks have 20~layers of CR39, each layer 13~cm~x~7~cm and 1.4~mm thick. A copper absorber is located after the first 6 layers. \\\\ \\\\ We require exposures of about 2000 tracks per cm$^2$ over the entire area of the stack with a uniform illumination. The standard beam used for the emulsion experiments is normally adequate for this purpose.\\\\ \\\\ We have performed one exposure to sulphur ions. The etched tracks have been measured automatically with the Elbeck image analyser system. We measured the incoming sulphur ions as well as the nuclear fragments produced in the copper absorber. Clean separation among the peaks due to the various fragments is obtained (there is no indication of nuclei with fractional electri...

The effect of solarradiation and UV photons on the CR-39 nuclear track detector

International Nuclear Information System (INIS)

Saad, A.F.

2003-01-01

The effects induced in the CR-39 polymer detector by total solar radiation (TSR) and UV photons were investigated. Thr exposure of detector samples to solar photons was carried out according to certain conditions. The TSR exposure period started in the middle of july and lasted unitel 12 th of september. 2000: the hottest months in zagazig, egypt. Another set of detector samples was exposed to UV photons from a UV lamp for different intervals. After UV exposure, these detectors were analysed with an FT-IR sepectrometer of jasco type 5300 in transmission mode. The FT-IR spectra does not show any considerable modifications due to UV irradiation in that detector. The effects of UV light were compared with those of solar radiation containing ultraviolet photons , on the registration properties of this polymer detector. Preliminaryresults revealed a proportionate increase in bluk etch rate of CR-39 detector with the increase of exposure time to the solar radiation. The results indicated that the CR-39 polymer detector can be used as a solar radiation dosimeter

Wide-range neutron dose determination with CR-39

International Nuclear Information System (INIS)

Arneja, A.R.; Waker, A.J.

1995-01-01

Optical density measurements of CR-30 irradiated with 252 Cf neutrons and chemically etched with 6.5 N KOH solution have been used to determine neutron absorbed doses between 0.1 and 10 Gy. Optimum etching conditions will depend upon the absorbed dose. Since it is not always possible to know the range of absorbed dose on a CR-39 dosemeter collected from personnel and area monitor stations in a criticality accident situation, a three-step two-hour chemical etch at 60 o C has been found to be appropriate. If after a total of six hours of chemical etching the optical density is found to be below 0.04 for 500 nm light (transmission > 90%) then further treatment in the form of electrochemical etching can be carried out to determine the lower absorbed dose. In this manner, absorbed doses below 0.1 Gy can be determined by counting tracks over a unit area. (author)

Characteristics of neutron-irradiated CR-39 foils treated by sequential chemical and electrochemical etching

International Nuclear Information System (INIS)

Somogyi, G.; Dajko, G.; Turek, K.; Spurny, F.

1982-01-01

The density of background spots revealed by chemical (CE) and electrochemical (ECE) etching and by their sequential application (CE + ECE) has been measured in several sorts of CR-39 material. The trends in the variation of sensitivity to Am-Be neutrons have been determined in CR-39 sheets covered by thick proton-radiator, when changing the field strength, frequency, etchant concentration, pre-etch duration and the fluence of neutrons. The results are analyzed in order to find out an optimum set of experimental parameters which may be proposed to attain high registration sensitivity to neutrons. (author)

Synthesis and structural stability of Cr-doped Li2MnSiO4/C cathode materials by solid-state method

Science.gov (United States)

Cheng, Hong-Mei; Zhao, Shi-Xi; Wu, Xia; Zhao, Jian-Wei; Wei, Lei; Nan, Ce-Wen

2018-03-01

The crystal structure of the Li2MnSiO4 cathode material would collapse during the charge and discharge process because of that the Mn-O coordination polyhedron changed from [MnO4] into [MnO6] in the process of Mn+2 to Mn+4, but the Cr element could remain [CrO4] crystal ligand from Cr+2 to Cr+4, so Cr element substitution was used to improve the structural stability of the Li2MnSiO4 cathode material. In this work, Li2Mn1-xCrxSiO4/C nanocomposites were synthesized by solid-state method. XRD, SEM and TEM observations show that the as-prepared Li2Mn1-xCrxSiO4/C materials presents an orthorhombic crystal structure (S.G. Pmn21), the particle size of Li2Mn1-xCrxSiO4/C powder ranges from 50 to 100 nm. The XRD and XPS results indicate that Cr+2 is successfully doped into Li2MnSiO4 lattice and has well compatibility with Li2MnSiO4. The electrochemical results display that Li2Mn92.5%Cr7.5%SiO4/C exhibits significantly enhanced cycle stability and discharge capability. The initial discharge capacity of the Li2Mn92.5%Cr7.5%SiO4/C sample is 255 mAh g-1, and the discharge capacity was still about 60 mAh g-1 after 50 cycles. Furthermore, the XRD patterns, TEM images and Raman analysis reveal that the Cr doping enhances the structural stability of Li2Mn1-xCrxSiO4/C and improves the electrochemical activity of the cathode. Thus, the Li2Mn92.5%Cr7.5%SiO4/C have shown potential applications for lithium ion batteries.

High resolution alpha-autoradiography for measurement of 10B distribution in subcellular scale using CR-39 and AFM

International Nuclear Information System (INIS)

Amemiya, K.; Takahashi, H.; Yasuda, N.

2000-01-01

In order to measure 10 B distribution in tumor tissues for BNCT at subcellular scale, we have developed a new method for high resolution alpha-autoradiography using contact X-ray microscopy technique with CR-39 plastic track detectors. Sliced sections of boron-injected brain tumors in rats were mounted on CR-39 and irradiated with thermal neutrons at KUR. Then the samples were exposed to soft X-rays from a laser plasma source. After etching the CR-39 in NaOH solution for a short time (1-5 min.), transmission X-ray image of tumor cells appeared as relief on CR-39 surface, and could be observed with the atomic force microscopy (AFM). Very small etch pits of about 100 nm in diameter corresponding to particle tracks from 10 B(n, α) 7 Li reactions were also observed in the image simultaneously. This method provides an accurate distribution of 10 B inside the cell. (author)

Potential of solid state fermentation for production of ergot alkaloids

OpenAIRE

Trejo Hernandez, M.R.; Raimbault, Maurice; Roussos, Sevastianos; Lonsane, B.K.

1992-01-01

Production of total ergot alkaloids by #Claviceps fusiformis$ in solid state fermentation was 3.9 times higher compared to that in submerged fermentation. Production was equal in the case of #Claviceps purpurea$ but the spectra of alkaloids were advantageous with the use of solid state fermentation. The data establish potential of solid state fermentation which was not explored earlier for production of ergot alkaloids. (Résumé d'auteur)

CR-39 α track detector and its application in observing of the hot particles in environment

International Nuclear Information System (INIS)

Zou Benchuan

1992-01-01

CR-39 α track detector is a new α remitting radionuclides plastic detector. It is audio-visual, convenient and economic in the detection of α particle track and the distribution of α emitting radionuclides in environmental samples. CR-39 α track detector is used to observe the hot particles in rock and the hot particles coming from the liquid effluents discharged by spent fuel reprocessing plant in UK in marine environment and got good results

Relation between the size of fog droplets and their contact angles with CR39 surfaces

International Nuclear Information System (INIS)

Grosu, G; Andrzejewski, L; Veilleux, G; Ross, G G

2004-01-01

The formation of fog on CR39 surfaces has been studied. Water droplets form fog coalesce with time, especially during the first 20 s at the beginning of the formation of fog. Consequently, their mean diameter increases. Formation of fog being related to the wettability of the surfaces, the latter has been increased by the implantation of Ar ions into CR39 surfaces under an oxygen partial pressure. A very wetting CR39 surface with advancing (ACA) and receding (RCA) contact angles below 5 deg. has been obtained with an implantation dose of 1.28x10 17 Ar + cm -2 . In this condition, no formation of fog was observed. Characterization using x-ray photoelectron spectroscopy has shown that the molecular structure of CR39 is strongly modified by Ar + implantation, which would be responsible for the increase in wettability. Unfortunately, both ACA and RCA increase with time, which is called ageing, and the formation of fog is again observed. The diameter and concentration of water droplets forming fog have been plotted against the contact angle. These plots show that no formation of fog occurs for ACA 15 He + cm -2 and an energy of 2 keV, sufficient to push the ions deeper than the Ar depth profile, delays the ageing effect in such a way that ACA ≅ 40 deg. is reached after ∼2000 h and no formation of fog is observed during these first ∼2000 h

Angular and dose dependence of CR-39 neutron response for shape-selected tracks

CERN Document Server

Tam, N C; Lakosi, L

1999-01-01

A shape selection method corresponding to an energy discrimination was used to eliminate unwanted events disturbing evaluation of CR-39 detectors in detecting tracks induced by particles both of perpendicular and oblique incidence. The angular dependence of the response was examined, detecting fast neutrons from sup 2 sup 5 sup 2 Cf with shape selection technique at various angles and distances. Also, the CR-39 track detectors with the sup 2 sup 5 sup 2 Cf source were exposed to high gamma-intensity of a sup 6 sup 0 Co irradiation facility in the range 0.1 to 4.5 kGy, similar to the exposures inside spent fuel assemblies. Using the two functions the lower limit of burnup could be determined by the method.

Solid-State Electrochromic Device Consisting of Amorphous WO3 and Various Thin Oxide Layers

Science.gov (United States)

Shizukuishi, Makoto; Shimizu, Isamu; Inoue, Eiichi

1980-11-01

A mixed oxide containing Cr2O3 was introduced into an amorphous WO3 solid-state electrochromic device (ECD) in order to improve its colour memory effect. The electrochromic characteristics were greatly affected by the chemical constituents of a dielectric layer on the a-WO3 layer. Particularly, long memory effect and low power dissipation were attained in a solid-state ECD consisting of a-WO3 and Cr2O3\\cdotV2O5(50 wt.%). Some electrochromic characteristics of the a-WO3/Cr2O3\\cdotV2O5 ECD and the role of V2O5 were investigated.

Solid-state e.m.f. and calorimetric measurements on Cs2Cr2O7(I)

International Nuclear Information System (INIS)

Venugopal, V.; Iyer, V.S.; Agarwal, R.; Roy, K.N.; Prasad, R.; Sood, D.D.

1987-01-01

The standard molar Gibbs free energy of formation of Cs 2 Cr 2 O 7 (1) has been determined in the temperature range 797 to 874 K, using a solid-oxide-electrolyte galvanic cell. The melting and transition temperatures, molar enthalpies of fusion and of transition of the same caesium compound were determined in the temperature range 662 to 826 K, using a high temperature Calvet microcalorimeter. Results on the standard molar enthalpy of formation of Cs 2 Cr 2 O 7 at 298.15 K are in good agreement with those reported by other workers. (U.K.)

Energy-dependent etching-related impacts on CR-39 alpha detection efficiency for the Rn-222 and Rn-220 decay chains

Science.gov (United States)

Tan, Y.; Yuan, H.; Kearfott, K. J.

2018-04-01

CR-39 detectors are widely used to measure environmental levels of Rn-222, Rn-220 and their progeny. Prior research reported the CR-39 detection efficiency for alpha particles from Rn-222, Rn-220 and their progeny under a variety of etching conditions. This paper provides an explanation for interesting observations included in that work, namely that the critical incidence angle decreases with the increasing particle energy and the detection efficiency for 8.78 MeV alpha particles is zero. This paper explains these phenomena from a consideration of the interaction of alpha particles with the CR-39 detectors and the physics of etching dynamics. The proposed theory provides a rationale for an approach to optimizing the etching conditions of CR-39 detector for measuring Rn-222, Rn-220 and their progenies.

Effect of certain production parameters and post-production treatments on the etching characteristics of CR-39 sheets

Energy Technology Data Exchange (ETDEWEB)

Somogyi, G.; Toth-Szilagyi, M.; Hunyadi, I.; Hafez, A.-F.

1986-01-01

There is a permanent need in producing track recording detectors of well defined behaviour from CR-39 monomer. Therefore, more studies on the role of production parameters determining the stability of main etching characteristics (bulk etch rate, Vsub(B);etch rate ratio, Vsub(T)/Vsub(B);opaqueness after longer etching periods) are highly required. In our studies we have examined different commercial CR-39 sheets (Homalite, Pershore, MA-ND) to compare their registration sensitivity to selected alpha and proton energies. In addition, we have investigated the main etching parameters of CR-39 sheets manufactured under different casting conditions varying the concentration of initiator and certain additives. Finally, the effect of some post-production treatments, annealing and storage in vacuum, on the Vsub(B) and Vsub(T)/Vsub(B) values is studied.

Neutron measurement in 12,13C+ 27Al system using CR-39 detectors and neutron rem meter

International Nuclear Information System (INIS)

Sahoo, G.S.; Tripathy, S.P.; Shanbhag, A.A.; Sunil, C.; Joshi, D.S.; Sarkar, P.K.

2011-01-01

In this work, neutron measurements carried out for the interaction of 60 and 67.5 MeV 12 C, 57.3 and 65 MeV 13 C ions with thick aluminium target by using CR-39 detectors and neutron rem meter is reported. Both the detector systems were irradiated at different angles viz. 0 deg, 30 deg, 60 deg, 90 deg with respect to the beam direction. The normalized track density measurements (tracks/cm 2 /projectile at 1m) in CR-39 detectors were correlated with the normalized dose equivalent values (μSv/projectile at 1m) obtained using the neutron rem meter. The track density was found to be more in case of 13 C than 12 C. However in all the cases, the track density per incident projectile was found to decrease as the angle with respect to beam direction increases, indicating non-isotropic nature of neutron emission. The ratio between measured dose equivalent in rem meter to the measured track densities in CR-39 detectors was found to be 2.8±0.2, which remains constant irrespective of the change in angle from beam direction as well as neutron spectrum, indicating a flat dose response of CR-39 detectors. (author)

Study of the weekly irrigation cycle of a cultivated field in a semi-arid area (Marrakech region, Morocco) by using CR-39 and LR-115 II track detectors and radon as a natural tracer

International Nuclear Information System (INIS)

Misdaq, M.A.; Essaouif, Z.

2007-01-01

Uranium ( 238 U) and thorium ( 232 Th) concentrations were measured in the soil of a cultivated field situated in a semi-arid area (Marrakech, Morocco) by using CR-39 and LR-115 type II solid state nuclear track detectors (SSNTDs). The same track detectors were used for measuring alpha- and beta-activities due to radon and thoron gases emanating from the soil of the studied irrigated agricultural field. The influence of the humidity (soil water content), soil depth and climate conditions on the weekly irrigation cycle of the studied cultivated field was investigated by exploiting radon measurements

Alpha particle radiography and the track plastic detector CR-39

International Nuclear Information System (INIS)

Souza, Bismarck Amilar de.

1991-05-01

This work develops the radiographic technique using charged particle beams. This technique complements the X-ray conventional radiography, and presents some advantages in certain cases. The material used as nuclear plastic detector was CR-39, manufactured by Pershre Mould. England, of 250 and 1000 μm nominal thicknesses. The irradiations were made with 7 MeV/Nucleon alpha particles beams, accelerated in the CV-28 Cyclotron of Instituto de Engenharia Nuclear/CNEN - Rio de Janeiro. The etch conditions used were a Na OH 6,25 N solution at 70 0 C, varying the etch time, so that the best etch time was found to be six hours. The calibration curve is presented, which permits images interpretation, showed in terms of light transmittance (obtained using a micro densitometer), and in terms of energy losses suffered by alpha particles in several aluminum degradating thicknesses. This curve was checked by the use of other degradating materials: Mylar, Makrofol, and CR-39 itself. The influence of alpha particle beam FWHM widening on images quality, when it crosses several degradating materials, is also presented. Radiographs of some specimen are presented, including some images obtained varying some irradiation and etch parameters. (author). 62 refs., 22 figs., 19 tabs

Proton radiographic characteristics of thin CR-39 detector

International Nuclear Information System (INIS)

Waheed, A.; Manzoor, S.; Khan, H.A.; Urlep, I.; Ilic, R.

1991-01-01

Two parameters, track registration sensitivity and densitometric response, were measured in radiography with a low energy (∼4.5 MeV) proton beam and a stack of thin (100μm) CR-39 detector foils. The optimum image quality was obtained at a layer removal thickness of about 1 μm. The image obtained under these conditions is characterized by a high track registration sensitivity (∼60%), high image contrast (the maximum value of the net optical density is ∼0.7) and high spatial resolution (∼1 μm). The application of the technique in biomedicine is illustrated by proton radiographs of botanical samples. (author)

Effect of d electrons on defect properties in equiatomic NiCoCr and NiCoFeCr concentrated solid solution alloys

Science.gov (United States)

Zhao, Shijun; Egami, Takeshi; Stocks, G. Malcolm; Zhang, Yanwen

2018-01-01

The role of d electrons in determining distributions of formation and migration energies for point defects in equiatomic NiCoCr and NiCoFeCr concentrated solid solution alloys (CSAs) are studied regarding electron density deformation flexibility based on first-principles calculations. The disordered state is taken into account by constructing special quasirandom structures. The migration barriers are determined by directly optimizing the saddle point. It is found that the formation energies of interstitials in CSAs are lower than those in pure Ni, whereas the formation energies of vacancies are higher. In both NiCoCr and NiCoFeCr, Co-related dumbbell interstitials exhibit lower formation energies. Notably, the distributions of migration energies for Cr interstitials and vacancies exhibit a remarkable overlap region. A detailed analysis of electronic properties reveals that the electronic charge deformation flexibility regarding eg to t2g transition has a dominant effect on defect energetics for different elements in CSAs. Thus the electron deformation ability is suggested as a key factor in understanding the peculiar defect behavior in CSAs.

Range to cone length relations for light ions in CR-39

International Nuclear Information System (INIS)

Gil, L.R.; Marques, A.

1988-01-01

Curves ''range x cone lenght'' and ''diameter x cone lenght'' are calculated for tracks left by low energy light ions in CR-39. The calculations cover ions from helium to iron and are performed for 6.25 N NaOH at 70 0 C and a standard etching time but can be easily extended to other etching conditions. (author) [pt

A quick method for maintaining the molarity of NaOH solution during continuous etching of CR-39

International Nuclear Information System (INIS)

Khan, E.U.; Husaini, S.N.; Malik, F.; Sajid, M.; Karim, S.; Qureshi, I.E.

2002-01-01

A series of experiments have been performed to investigate the physio-chemical changes that occurred in the 6 M NaOH solution after etching CR-39 (Pershore and Homalite) detectors, each for 3, 6, 9, 12 and 15 h. Various physical parameters like concentration, electrical conductivity (EC) and density of the solutions have been measured after each etching interval. Results have been discussed in the light of stoichiometrical equation for the interaction of CR-39 with NaOH. It is found that the concentration, EC and the density of the solution, in which CR-39 has been etched, increase linearly with respect to the etching time. The inter-relationship of EC-concentration and density-concentration suggest that the concentration of the etchant can be maintained at certain desired value by adjusting the corresponding value of EC or density, measured through non-destructive and quick methods

Testing Novel CR-39 Detector Deployment System For Identification of Subsurface Fractures, Soda Springs, ID

Energy Technology Data Exchange (ETDEWEB)

McLing, Travis [Idaho National Lab. (INL), Idaho Falls, ID (United States); Carpenter, Michael [Idaho National Lab. (INL), Idaho Falls, ID (United States); Brandon, William [Idaho National Lab. (INL), Idaho Falls, ID (United States); Zavala, Bernie [Idaho National Lab. (INL), Idaho Falls, ID (United States)

2015-06-01

The Environmental Protection Agency (EPA) has teamed with Battelle Energy Alliance, LLC (BEA) at Idaho National Laboratory (INL) to facilitate further testing of geologic-fracture-identification methodology at a field site near the Monsanto Superfund Site located in Soda Springs, Idaho. INL has the necessary testing and technological expertise to perform this work. Battelle Memorial Institute (BMI) has engaged INL to perform this work through a Work for Others (WFO) Agreement. This study continues a multi-year collaborative effort between INL and EPA to test the efficacy of using field deployed Cr-39 radon in soil portals. This research enables identification of active fractures capable of transporting contaminants at sites where fractures are suspected pathways into the subsurface. Current state of the art methods for mapping fracture networks are exceedingly expensive and notoriously inaccurate. The proposed WFO will evaluate the applicability of using cheap, readily available, passive radon detectors to identify conductive geologic structures (i.e. fractures, and fracture networks) in the subsurface that control the transport of contaminants at fracture-dominated sites. The proposed WFO utilizes proven off-the-shelf technology in the form of CR-39 radon detectors, which have been widely deployed to detect radon levels in homes and businesses. In an existing collaborative EPA/INL study outside of this workscope,. CR-39 detectors are being utilized to determine the location of active transport fractures in a fractured granitic upland adjacent to a landfill site at the Fort Devens, MA that EPA-designated as National Priorities List (NPL) site. The innovative concept of using an easily deployed port that allows the CR-39 to measure the Rn-222 in the soil or alluvium above the fractured rock, while restricting atmospheric Rn-222 and soil sourced Ra from contaminating the detector is unique to INL and EPA approach previously developed. By deploying a series of these

Studying the response of CR-39 to radon in non-polar liquids above water by Monte Carlo simulation and measurement

International Nuclear Information System (INIS)

Rezaie, Mohammad Reza; Sohrabi, Mehdi; Negarestani, Ali

2013-01-01

The application of CR-39 has been extensive for measurement of radon and progeny in air of dwellings, but limited as regards to measurements of radon in water. In this paper, a new method is introduced for efficient measurement of radon in water by registering alpha particle tracks in a CR-39 detector placed in a non-polar medium such as cyclohexane, hexane and olive oil when each mixed with water, then separated and fixed above water, as a two-phase media. The method introduced here is however different from the widely used liquid - liquid extraction technique by liquid scintillation spectrometry since it is a passive detection method (CR-39) in a non-polar liquid with enhanced absorption of radon in the liquid, it has a capability for long sample counting to decrease the minimum detection limit (MDL), it does not require sophisticated low light counting systems, and it has the potential for simultaneous measurements of large number of samples for large-scale applications. It also has a low cost and is readily available. A new Monte Carlo calculation of energy-distance travelled by alphas from radon and progeny in a medium was also investigated. The sensitivity of CR-39 detector to radon and progeny in water was determined under two conditions; in a single-phase and two-phase media. In a single-phase medium, CR-39 is directly placed either in air, water, cyclohexane, hexane or olive oil. When CR-39 is placed directly in water, its sensitivity is (2.4 ± 0.1) × 10 −4 (track/cm 2 )/(Bq.d/m 3 ). In the two-phase media, CR-39 is placed either in cyclohexane, hexane or olive oil when each is fixed above water. The sensitivities in the two-phase media are significantly enhanced and are respectively (1.98 ± 0.10) × 10 −2 , (2.8 ± 0.15) × 10 −2 and (2.86 ± 0.15) × 10 −2 (track/cm 2 )/(Bq.d/m 3 ). The sensitivies are about 76, 82 and 110 times more than that of when CR-39 is directly placed in water. The new method is a novel alternative for radon

Solid-liquid phase equilibria of Fe-Cr-Al alloys and spinels

Science.gov (United States)

McMurray, J. W.; Hu, R.; Ushakov, S. V.; Shin, D.; Pint, B. A.; Terrani, K. A.; Navrotsky, A.

2017-08-01

Ferritic FeCrAl alloys are candidate accident tolerant cladding materials. There is a paucity of data concerning the melting behavior for FeCrAl and its oxides. Analysis tools have therefore had to utilize assumptions for simulations using FeCrAl cladding. The focus of this study is to examine in some detail the solid-liquid phase equilibria of FeCrAl alloys and spinels with the aim of improving the accuracy of severe accident scenario computational studies.

Changes in CR-39 proton sensitivity due to prolonged exposure to high vacuums relevant to the National Ignition Facility and OMEGA.

Science.gov (United States)

Manuel, M J-E; Rosenberg, M J; Sinenian, N; Rinderknecht, H; Zylstra, A B; Séguin, F H; Frenje, J; Li, C K; Petrasso, R D

2011-09-01

When used at facilities like OMEGA and the NIF, CR-39 is exposed to high vacuum environments before and after irradiation by charged particles and neutrons. Using an electrostatic linear accelerator at MIT, studies have been conducted to investigate the effects of high vacuum exposure on the sensitivity of CR-39 to fusion protons in the ~1-9 MeV energy range. High vacuum conditions, of order 10(-5) Torr, experienced by CR-39 samples at these facilities were emulated. It is shown that vacuum exposure times longer than ~16 h before proton irradiation result in a decrease in proton sensitivity, whereas no effect was observed for up to 67 h of vacuum exposure after proton irradiation. CR-39 sensitivity curves are presented for samples with prolonged exposure to high vacuum before and after proton irradiation. © 2011 American Institute of Physics

Electrochemical development of particle tracks in CR-39 polymer dosimeter

International Nuclear Information System (INIS)

Hadlock, D.E.; Parkhurst, M.A.; Yang, C.S.; Groeger, J.; Johnson, J.R.; Huang, S.J.

1985-09-01

Electrochemical etching of CR-39 polymeric track etch neutron detectors results in proton-recoil tracks can be distinguished from background tracks much better than tracks developed solely by chemical etching. A newly designed and constructed electrochemical etching apparatus allows large numbers of dosimeters to be processed simultaneously with consistent results. Many processing systems have been developed for chemical and electrochemical etching of the track etch dosimeters. Three systems specifically show great promise and are being studied extensively

Characterization of CR 39 nuclear track detector for use as a radon/thoron dosemeter

International Nuclear Information System (INIS)

Kandaiya, S.

1988-02-01

For the estimation of radon, thoron and their short-lived daughter products in air radon diffusion chambers with passive α-track etch detectors have been used. The report describes the properties of CR 39 track etch detectors in particular with respect to the spectrometric detection of α-particles in the energy range up to 8.77 MeV using chemical and a combination of chemical-electrochemical etching technique. In order to optimize the etching conditions for an α-energy discrimination in the energy range up to 8.77 MeV, the ECE track size diameter and the track density have been investigated as a function of the chemical pre-etching time using three electrical field strengths. In a mixed α-spectrum the contributions of various α-particles with energies between 4.6 to 8.77 MeV have been determined experimentally in CR 39 and compared with the spectral measurement using a surface barrier detector and the same irradiation geometry. Beside CR 39 detectors etched chemically and electrochemically, in addition surface barrier detectors and a Monte Carlo calculation have been used to evaluate the α-energy spectrum for thoron and its daughter products emitted by α-decays in the air volume and the plate-out of daughters at the inner surface on the diffusion chamber. (orig./HP) [de

A fast neutron spectrometer based on an electrochemically etched CR-39 detector with degrader and front radiator

International Nuclear Information System (INIS)

Matiullah; Durrani, S.A.

1987-01-01

In addition to having promising applications for the development of a fast-neutron dosemeter, electrochemically etched (ECE) CR-39 detectors also offer the possibility of energy-selective fast-neutron detection. This property stems basically from the fact that, to produce 'sparkable' trails in the polymeric detector subjected to ECE, the charged particle resulting from a neutron interaction must fall within a definite 'energy window'. The lower and upper limits of proton energies that can yield ECE spots in CR-39 have been experimentally determined to be ∼ 50 keV and ∼ 2.2 MeV under our processing conditions. To accomplish our objective, we have developed a technique based on ECE spot-density measurements in CR-39 detectors placed in conjuction with judiciously chosen thicknesses of a polyethylene radiator and a lead degrader. The optimum thicknesses of the radiator and the degrader, for a given neutron energy, are determined by computer calculations. (author)

Solid-state reactions during mechanical alloying of ternary Fe-Al-X (X=Ni, Mn, Cu, Ti, Cr, B, Si) systems: A review

Science.gov (United States)

Hadef, Fatma

2016-12-01

The last decade has witnessed an intensive research in the field of nanocrystalline materials due to their enhanced properties. A lot of processing techniques were developed in order to synthesis these novel materials, among them mechanical alloying or high-energy ball milling. In fact, mechanical alloying is one of the most common operations in the processing of solids. It can be used to quickly and easily synthesize a variety of technologically useful materials which are very difficult to manufacture by other techniques. One advantage of MA over many other techniques is that is a solid state technique and consequently problems associated with melting and solidification are bypassed. Special attention is being paid to the synthesis of alloys through reactions mainly occurring in solid state in many metallic ternary Fe-Al-X systems, in order to improve mainly Fe-Al structural and mechanical properties. The results show that nanocrystallization is the common result occurring in all systems during MA process. The aim of this work is to illustrate the uniqueness of MA process to induce phase transformation in metallic Fe-Al-X (X=Ni, Mn, Cu, Ti, Cr, B, Si) systems.

Modifications in the optical and thermal properties of a CR-39 polymeric detector induced by high doses of γ-radiation

Science.gov (United States)

Saad, A. F.; Ibraheim, Mona H.; Nwara, Aya M.; Kandil, S. A.

2018-04-01

Effects of γ-radiation on the optical and thermal properties of a poly allyl diglycol carbonate (PADC), a form of CR-39, polymer have been investigated. CR-39 detectors were exposed to γ-rays at very high doses ranging from 5.0 × 105 to 3.0 × 106 Gy. The induced changes were analyzed using ultraviolet-visible spectroscopy (UV-VIS) in absorbance mode, and thermogravimetric analysis (TGA). The UV-visible spectra of the virgin and γ-irradiated CR-39 polymer detectors displayed a significant decreasing trend in their optical energy band gaps for indirect transitions, whereas for the direct ones showed a little change. This drop in the energy band gap with increasing dose is discussed on the basis of the gamma irradiation induced modifications in the CR-39 polymeric detector. The TGA thermograms show that the weight loss rate increased with increase in dose, which may be due to the disordered system via scission followed by crosslinking in the irradiated polymer detector. The TGA thermograms also indicated that the CR-39 detector decomposed in three/four stages for the virgin and irradiated samples. The activation energy for thermal decomposition was determined using a type of Arrhenius equation based on the TGA experimental results. These experimental results so obtained can be well used in radiation dosimetry.

Response of CR-39 Detector Against Fast Neutron Using D-Polyethylene and H-Polyethylene Radiator

International Nuclear Information System (INIS)

Sofyan, Hasnel

1996-01-01

The research on the response of detector CR-39 by using D-Polyethylene and H-Polyethylene radiator has been carried out. The optimum number of nuclear tracks was found with the use of 30 % NaOH at 80 + 0,5oC for 80 minutes of etching time. The comparison of CR-39 detector response caused by D-Polyethylene radiator against H-Polyethylene radiator of irradiation in air, were found to be 1.18 and 0.84 for 241Am-Be neutron source and neutron source from reactor respectively. For phantom irradiation, the results were found to be 1.75 for 241Am-Be neutron source, and 0.77 for neutron source from reactor

An automatic analyzer of solid state nuclear track detectors using an optic RAM as image sensor

International Nuclear Information System (INIS)

Staderini, E.M.; Castellano, A.

1986-01-01

An optic RAM is a conventional digital random access read/write dynamic memory device featuring a quartz windowed package and memory cells regularly ordered on the chip. Such a device is used as an image sensor because each cell retains data stored in it for a time depending on the intensity of the light incident on the cell itself. The authors have developed a system which uses an optic RAM to acquire and digitize images from electrochemically etched CR39 solid state nuclear track detectors (SSNTD) in the track count rate up to 5000 cm -2 . On the digital image so obtained, a microprocessor, with appropriate software, performs image analysis, filtering, tracks counting and evaluation. (orig.)

Response of CR39 detector to 5 A GeV Si14+ ions and measurement of total charge changing cross-section

International Nuclear Information System (INIS)

Gupta, Renu; Kumar, Ashavani

2013-01-01

In the present work, response of CR39 track etch detector was obtained by cone-height measurement technique. CR39 track etch detector was used to identify the incident charged particles and their fragments by the measurements of cone-height of tracks using an optical microscope DM6000 M and automated image analyzer system installed with Leica QWin Plus software. The CR39 detector was calibrated and the response points were fitted with a linear relation and all the points are within the limits of the experimental errors. The charge resolution of the detector was calculated to be 0.2e. The response function is obtained and fitted with a linear relation which is good throughout Z/β=6.1–14.1. The experimental value of the total charge changing cross-section of 5 A GeV Si 14+ ion beam in polyethylene and CR39 combined target is σ tot =(734±128) mb. The total charge changing cross-section is compared with the experimental results of others based on cone base-area measurement technique and also fitted by the Bradt–Peters geometrical cross-section. - Highlights: • Charge resolution of 0.2e was obtained by cone-height measurement. • Consistency in manual measurements of cone-heights is presented. • Response of CR39 detector was obtained and fitted with first degree polynomial. • Total charge changing cross-section of 5 A GeV Si 14+ ions in CH 2 and CR39 as a combined target was calculated

Development of hybrid track detector using CR39 and photographic plate

International Nuclear Information System (INIS)

Kuge, K.; Endo, Y.; Hayashi, K.; Iwakiri, S.; Hasegawa, A.; Yasuda, N.; Kumagai, H.

2005-01-01

To improve the hybrid track detector using both CR39 and silver halide photography the gold deposition development technique was applied to this. Nuclear tracks composed of gold clusters were obtained. This method has several advantages; 1. no filament formation, 2. easy control of the cluster size owing to the independence of the size of silver halide grain, 3. easy treatment of the waste solution of developer. (author)

Contribution to the study of radio toxicity of aromatic and medicinal plants using solid state nuclear track detectors

International Nuclear Information System (INIS)

Mortassim, A.; Misdaq, M.A.; Naaman, A

2009-01-01

The concentrations of uranium (238 U), thorium (232 Th), radon (222 Rn) and thoron (220 Rn) were measured in twenty aromatic and medicinal plants in f ind a new method based on using solid state nuclear track detectors type Cr-39 and Rs-115. He emerges from this study that the verbena and salvia have higher levels of uranium (radon) higher than that of other plants while the leaves of olive and saturja have concentrations of thorium (thoron) higher than other plants therefore radio toxicity of these plants is higher than that of others and may pose a radiological hazard if the masses are incorporated by consumers high. [fr

Measurement of indoor radon levels in Erbil capital by using solid state nuclear track detectors

International Nuclear Information System (INIS)

Mansour, H.H.; Khdar, S. per; Abdulla, H.Y.; Muhamad, N.Q.; Othman, M.M.; Qader, S.

2005-01-01

Radon alpha activity concentration has been measured in 28 homes in the Erbil Capital-Iraqi Kurdistan region during the autumn season by using time-integrated passive radon dosimeters containing CR-39 solid state nuclear track detectors 'SSNTDs'. The radon activity concentrations in these homes range from (10.33-90.34) Bqm -3 with an average of 44+/-23Bqm -3 . The average absorption effective dose equivalent for a person living in homes for which the investigation were done was found to be 1.3+/-0.65mSvy -1 , obtained by using an equilibrium factor of 0.5 and an occupancy factor of 0.8. The average lung cancer cases per year per 10 6 person was found to be 23+/-12

Measurements of radon in dwellings with CR-39 track detectors

DEFF Research Database (Denmark)

Majborn, Benny

1986-01-01

A passive integrating dosemeter has been designed for measuring natural radiation in dwellings. The dosemeter contains one or two CR-39 track detectors to measure radon and three thermoluminescence dosemeters to measure external radiation. The dosemeter was investigated in a pilot study in 1983....../84, and it is now used in a nationwide survey of natural radiation in Danish dwellings. The characteristics of the dosemeter with respect to radon measurements are presented, and the radon monitoring results obtained in the pilot study are summarized...

Formation of solid solutions of gallium in Fe–Cr and Fe–Co alloys: Mössbauer studies and first-principles calculations

Energy Technology Data Exchange (ETDEWEB)

Serikov, V.V. [Institute of Metal Physics UB RAS, S. Kovalevskaya str. 18, 620990 Ekaterinburg (Russian Federation); Kleinerman, N.M., E-mail: kleinerman@imp.uran.ru [Institute of Metal Physics UB RAS, S. Kovalevskaya str. 18, 620990 Ekaterinburg (Russian Federation); Vershinin, A.V.; Mushnikov, N.V.; Protasov, A.V.; Stashkova, L.A. [Institute of Metal Physics UB RAS, S. Kovalevskaya str. 18, 620990 Ekaterinburg (Russian Federation); Gorbatov, O.I. [Institute of Metal Physics UB RAS, S. Kovalevskaya str. 18, 620990 Ekaterinburg (Russian Federation); Department of Materials Science and Engineering, KTH Royal Institute of Technology, SE - 100 44 Stockholm (Sweden); Ruban, A.V. [Department of Materials Science and Engineering, KTH Royal Institute of Technology, SE - 100 44 Stockholm (Sweden); Gornostyrev, Yu.N. [Institute of Metal Physics UB RAS, S. Kovalevskaya str. 18, 620990 Ekaterinburg (Russian Federation)

2014-11-25

Highlights: • Structure features of the formation of quasibinary solid solutions Fe–Co–Ga and Fe–Cr–Ga are found. • The first-principles calculation of mixing and solubility energies for Ga in an Fe–X alloy are given. • Ga handicaps the processes of phase separation in the Fe–Cr system and ordering in the Fe–Co system. • Preference of Ga entering in the neighborhood of a second element can help study multielement alloys. - Abstract: Investigation of Ga influence on the structure of Fe–Cr and Fe–Co alloys was performed with the use of Mössbauer spectroscopy and X-ray diffraction methods. The experimental results are compared with results of first-principles calculations of the mixing and solubility energies for Ga in an Fe–X (X = Co, Cr) alloy both in ferromagnetic and paramagnetic states. It is shown that Ga mainly goes into the solid solutions of the base alloys. In the alloys of the Fe–Cr system, doping with Ga handicaps the decomposition of solid solutions, observed in the binary alloys, and increases its stability. In the alloys with Co, Ga also favors the uniformity of solid solutions. The results of the first-principles calculations testify in favor of a preferable dissolution of Ga in the FeCo regions of a multicomponent structure rather than FeCr regions, both types of regions being in the ferromagnetic state at the temperature of annealing. The analysis of Mössbauer experiments gives some grounds to conclude that if, owing to liquation, clusterization, or initial stages of phase separation, there exist regions enriched in iron, some amount of Ga atoms prefer to enter the nearest surroundings of iron atoms, thus forming binary Fe–Ga regions (or phases)

Effect of oxygen pressure on sensitivity of CR-39 used for astronauts radiation dosimetry

International Nuclear Information System (INIS)

Murai, T.; Yabe, S.; Nagamatsu, A.; Tawara, H.; Kumagai, H.; Miyazawa, Y.; Kitajo, K.; Kodaira, S.; Yasuda, N.

2006-01-01

The personal radiation dosimeters for astronauts are exposed to low-pressure oxygen gas (0.29 atmospheres) during extra-vehicle activities. CR-39 plastic track detectors are one of the typical passive dosimeters for space radiation monitoring. We investigated change in track formation sensitivity of the antioxidant-doped CR-39 plastic with which oxygen gas comes in contact at different pressures up to 2 atmospheres for 1h to 10 days. The oxygen effect on sensitivity was measured for the C, Si and Fe ions (10-200 keV/μm) from the HIMAC heavy ion accelerator. The sensitivity is obviously sensitive to oxygen pressure at heavy-ion exposures, but not sensitive to the experience of oxygen atmosphere before and after the ion exposures. The maximum sensitivity is obtained at 0.29 atmospheres. The present experimental data suggested that the effect depends on LET of incident particles. (author)

Solid state lasers II; Proceedings of the Meeting, Los Angeles, CA, Jan. 24, 25, 1991

International Nuclear Information System (INIS)

Dube, G.

1991-01-01

Topics presented include an upgrade of the LLNL Nova laser for inertial confinement fusion, the design and energy characteristics of a multisegment glass-disk amplifier, a wavemeter for tuning solid state lasers, and the fabrication of laser materials by laser-heated pedestal growth. Also presented are the suppression of relaxation oscillations in flash-pumped 2-micron lasers, diode pumping of tunable Cr-doped lasers, 2D periodic structures in a solid state laser resonator, and single-frequency solid state lasers and amplifiers

Vacuum treatment of CR-39 for the reduction of background in neutron induced autoradiography of boron

International Nuclear Information System (INIS)

Freyer, K.; Treutler, H.C.; Dietze, K.; Hunyadi, I.; Csige, I.; Somogyi, G.

1991-01-01

The influence of etching time and vacuum processing before, during, and after neutron irradiation on the ''signal/noise'' ratio of the neutron induced autoradiography of boron using CR-39 track detectors has been investigated. The neutron irradiation was carried out in a vacuum chamber using the Cf-252 neutron source of the Central Institute of Isotope and Radiation Research at Leipzig. Hungarian-made CR-39 type track detectors, MA-ND/p and MA-ND/α, produced in different years, are compared. After a few hours of 2 kPa (about 10 -2 Torr) vacuum treatment, the ''signal/noise'' ratio for boron determination is improved remarkably in most cases of the detector and etching-time combinations used. (author)

Environmental dosimetry of radon-222 and daughters: measurement of absolute calibration factors of CR-39 considering the plate-out effects and environmental factors; Dosimetria ambiental de Rn-222 e filhos: medida da eficiencia absoluta do CR-39 levando-se em conta os efeitos do plate-out e fatores ambientais

Energy Technology Data Exchange (ETDEWEB)

Paulo, S.R. de

1991-08-01

The subject of this work concerns with the measurement of absolute calibration factors for the use of CR-39 as an absolute detector in indoor and daughters monitoring. Up to now the usefulness of calibration factors was restricted to environmental conditions equal (or very close) to those worthing during their determinations. This fact is consequence of the difficulties related to the understanding of the plate-out properties of radon daughters activity in the air. The plate-out effects on radon daughters monitoring performed by SSNTDs are studied. Our experimental results are in agreement with those of other authors about the great sensitivity of CR-39 to the plate-out effects, fact that recommended its use in this work. Being succeeded in the employment of CR-39 as an alpha-spectrometer we concluded that some important information (like the radon daughters deposition rates on the walls of an environment) can be achieved. The knowledge about the behavior of plate-out made possible the determination of the ranges in zenithal angle and energy where CR-39 can detect alpha-particles with efficiency of 100%, at our conditions of track observation. In this way, we obtained calibration factors for CR-39 that are weakly dependent on environmental conditions. We think that these results can contribute to the improvement of RD (Radiation Detector) detection techniques. (author). 159 refs, 106 figs, 05 tabs.

Solid-state reactions during mechanical alloying of ternary Fe–Al–X (X=Ni, Mn, Cu, Ti, Cr, B, Si) systems: A review

Energy Technology Data Exchange (ETDEWEB)

Hadef, Fatma, E-mail: hadef77@yahoo.fr [Laboratoire de Recherche sur la Physico-Chimie des Surfaces et Interfaces, LRPCSI, Université 20 Août 1955, BP 26, Route d’El-Haddaiek, Skikda 21000 (Algeria); Département de Physique, Faculté des Sciences, Université 20 Août 1955, BP 26, Route d’El-Haddaiek, Skikda 21000 (Algeria)

2016-12-01

The last decade has witnessed an intensive research in the field of nanocrystalline materials due to their enhanced properties. A lot of processing techniques were developed in order to synthesis these novel materials, among them mechanical alloying or high-energy ball milling. In fact, mechanical alloying is one of the most common operations in the processing of solids. It can be used to quickly and easily synthesize a variety of technologically useful materials which are very difficult to manufacture by other techniques. One advantage of MA over many other techniques is that is a solid state technique and consequently problems associated with melting and solidification are bypassed. Special attention is being paid to the synthesis of alloys through reactions mainly occurring in solid state in many metallic ternary Fe–Al–X systems, in order to improve mainly Fe–Al structural and mechanical properties. The results show that nanocrystallization is the common result occurring in all systems during MA process. The aim of this work is to illustrate the uniqueness of MA process to induce phase transformation in metallic Fe–Al–X (X=Ni, Mn, Cu, Ti, Cr, B, Si) systems. - Highlights: • A review of state of the art on binary Fe–Al alloys was presented. • Structural and microstructural properties of MA ternary Fe–Al–X alloys were summerized. • MA process is a powerful tool for producing metallic alloys at the nanometer scale.

Review of the state of the art in personnel neutron monitoring with solid state detectors

International Nuclear Information System (INIS)

Griffith, R.V.

1987-01-01

Albedo systems are the mainstay at many facilities and continue to be refined. Advanced electrochemical etching techniques for CR-39 now yield a dose equivalent response that is nearly constant from 0.1 to 4.0 MeV. Recent studies include use of converters to enhance CR-39 response at both low and high energies. Methods have been suggested for use of CR-39, either alone or in conjunction with albedo and other detectors to provide spectral information as a step to more accurate dosimetry. Limitations in the use of CR-39 primarily center on the lack of consistent, high-quality, dosimetry-grade material, significant angular dependence, and poor dose equivalent response at both low and high energies. Work continues on silicon diodes, with some new designs. The most attractive new dosimetry technique is the bubble-damage or superheated drop detector. Metal-on-silicon (MOS) microelectronics present exciting possibilities for the future. 25 refs., 6 figs

Study on structural and optical properties of α-(AlxCr1-x)2O3 (0 ≤ x ≤ 1) solid solutions

Science.gov (United States)

Jangir, Ravindra; Kumar, Dharmendra; Srihari, Velaga; Ganguli, Tapas

2018-04-01

We report on structural and optical properties for ternary α-(AlxCr1-x)2O3 (0 ≤ x ≤ 1) solid solutions synthesized by using solid sate reaction method. Single R-3c phase was obtained for the Aluminum composition of 0 ≤ x ≤ 1. Due to difference in the ionic radia of Al3+ and Cr3+, in plane lattice parameter showed deviation from the vegard's law. Optical absorption spectra for the solid solutions showed a blue shift of ˜ 0.5 eV in the optical gap. It has also been observed that Cr 3d level shifted towards the O 2p level in the valance band which indicates the enhancement of hybridization in the d and p levels, which is related to the delocalization of hole states, responsible for p-type conduction in wide band gap semiconductors. The results suggests that ternary α-(AlxCr1-x)2O3 (0 ≤ x ≤ 1) can be useful in the field of UV transparent electronics and UV photodetectors.

Vacuum treatment of CR-39 for the reduction of background in neutron induced autoradiography of boron

Energy Technology Data Exchange (ETDEWEB)

Freyer, K.; Treutler, H.C.; Dietze, K. (Central Inst. of Isotope and Radiation Research, Leipzig (Germany, F.R.)); Hunyadi, I.; Csige, I.; Somogyi, G. (Magyar Tudomanyos Akademia, Debrecen (Hungary). Atommag Kutato Intezete)

1991-01-01

The influence of etching time and vacuum processing before, during, and after neutron irradiation on the ''signal/noise'' ratio of the neutron induced autoradiography of boron using CR-39 track detectors has been investigated. The neutron irradiation was carried out in a vacuum chamber using the Cf-252 neutron source of the Central Institute of Isotope and Radiation Research at Leipzig. Hungarian-made CR-39 type track detectors, MA-ND/p and MA-ND/{alpha}, produced in different years, are compared. After a few hours of 2 kPa (about 10{sup -2} Torr) vacuum treatment, the ''signal/noise'' ratio for boron determination is improved remarkably in most cases of the detector and etching-time combinations used. (author).

Influence of tracks densities in solid state nuclear track detectors

International Nuclear Information System (INIS)

Guedes O, S.; Hadler N.; Lunes, P.; Saenz T, C.

1996-01-01

When Solid State Nuclear Track Detectors (SSNTD) is employed to measure nuclear tracks produced mainly by fission fragments and alpha particles, it is considered that the tracks observation work is performed under an efficiency, ε 0 , which is independent of the track density (number of tracks/area unit). There are not published results or experimental data supporting such an assumption. In this work the dependence of ε 0 with track density is studied basing on experimental data. To perform this, pieces of CR-39 cut from a sole 'mother sheet' were coupled to thin uranium films for different exposition times and the resulting ratios between track density and exposition time were compared. Our results indicate that ε 0 is constant for track densities between 10 3 and 10 5 cm -2 . At our etching conditions track overlapping makes impossible the counting for densities around 1.7 x 10 5 cm -2 . For track densities less than 10 3 cm -2 , ε 0 , was not observed to be constant. (authors). 4 refs., 2 figs

Status of development in the field of Cr-39 track detectors

International Nuclear Information System (INIS)

Somogyi, G.

1982-01-01

The present situation concerning the manufacture and etching characteristics of the CR-39 nuclear track detector is surveyed. Especial attention is paid to the trends in research and to the outstanding questions related to the subject. The requirements and procedures in connection with the manufacture of high-quality, thick and thin detector foils are discussed. The main bulk and track etching characteristics are presented, involving the effects of various environmental parameters as well. A statistical account of the typical directions in application is given. (author)

The effect of ArF laser irradiation (193 nm) on the photodegradation and etching properties of alpha-irradiated CR-39 detectors

Energy Technology Data Exchange (ETDEWEB)

Shakeri Jooybari, B. [Department of Energy Engineering and Physics, Amirkabir University of Technology, P.O. Box 15875-4413, Tehran, Islamic Republic of Iran (Iran, Islamic Republic of); Nuclear Science and Technology Research Institute (NSRT), Tehran, Islamic Republic of Iran (Iran, Islamic Republic of); Ghergherehchi, M. [College of Information and Technology/ school of Electronic and Electrical Engineering, Sungkyunkwan University, Suwon (Korea, Republic of); Afarideh, H., E-mail: hafarideh@aut.ac.ir [Department of Energy Engineering and Physics, Amirkabir University of Technology, P.O. Box 15875-4413, Tehran, Islamic Republic of Iran (Iran, Islamic Republic of); Lamehi-Rachti, M. [Nuclear Science and Technology Research Institute (NSRT), Tehran, Islamic Republic of Iran (Iran, Islamic Republic of)

2015-01-01

The effects of ArF laser irradiation (λ=193nm) at various fluences (energy dose or energy density) on the etching properties of pre-exposed (laser + alpha) CR-39 detectors were studied. First, UV–Vis and Fourier transform infrared (FTIR) spectra were acquired for non-laser-irradiated and laser-irradiated samples to detect the influence of the ArF laser on the chemical modification of the CR-39. Changes observed in the spectra indicated that the predominant process that occurred upon ArF laser irradiation was a bond-scission process. Thereafter, the mean track and bulk etching parameters were experimentally measured in ArF-laser-irradiated CR-39 detectors exposed to an alpha source ({sup 241}Am, E = 5.49 MeV). Inhomogeneous regions in the laser-irradiated side of the CR-39 demonstrated a variable etching rate on only the front side of the CR-39 detector. New equations are also presented for the average bulk etching rate for these inhomogeneous regions (front side). The mean bulk and track etching rates and the mean track dimensions increased in a fluence range of 0–37.03 mJ/cm{sup 2} because of photodegradation and the scission of chemical bonds, which are the predominant processes in this range. When the fluence was increased from 37.03 to 123.45 mJ/cm{sup 2}, the bulk and track etching rates and the track dimensions slowly decreased because of the formation of cross-linked structures on the CR-39 surface. The behavior of the bulk and track etching rates and the track dimensions appears to be proportional to the dose absorbed on the detector surface. It was observed that as the etching time was increased, the bulk and track etching rates and the track dimensions of the laser-irradiated samples decreased because of the shallow penetration depth of the 193 nm laser and the reduction in the oxygen penetration depth.

Applications of solid-state nuclear track detectors (SSNTDs) for fast ion and fusion reaction product measurements in TEXTOR experiments

Energy Technology Data Exchange (ETDEWEB)

Szydlowski, A.; Malinowski, K.; Malinowska, A. [Association EURTOM-IPPLM Warsaw, The Andrzej Soltan Institute for Nuclear Studies, 05-400 Otwock-Swierk (Poland); Wassenhove, G. Van [EURATOM-Belgium State Association, LPP, ERM/KMS, Trilateral Euregio Cluster, B-1000 Brussels (Belgium); Schweer, B. [Association EURATOM-FZJ, Institutte of Plasma Physicx, Juelich (Germany)

2011-07-01

Full text of publication follows: The paper reports on measurements of fusion reaction protons which were performed on TEXTOR facility in January 2009. The basic experimental scheme was similar to that applied in the previous measurements [1, 2]. The main experimental tool equipment was a small ion pinhole camera which was equipped with a PM-355 detector sample and was attached to a water cooled manipulator. The camera was placed below the plasma ring in the direction of ion drifts, at a distance of 4.4 cm from LCFS. However, in the described experiment it was aligned at an angle to the mayor TEXTOR radius (contrary to previous experiments), so that the input pinhole was oriented first at {gamma} = 45 degrees (shots 108799 - 108818) and then {gamma} = 600 (shots 108832 - 108847). The discharges were executed with one neutral beam of the total power 0.6 - 1.0 MW. In the first series (Nos 108799 - 108818) the plasma was additionally heated by ICRH of frequency 38 MHz. The irradiated detector samples were subjected to the same interrupted etching procedure as the samples used in the CR-39/PM-355 detector calibration measurements [1, 2]. After that, track density distributions and track diameter histograms were measured under an optical microscope. By the use of the calibration curves, it was possible to distinguish craters produced by protons from other craters and to convert the obtained histograms into proton energy spectra. The craters induced by lower energy ions appeared to be concentrated in narrower areas, whereas higher energy ions were registered in a more diffused detector fields. The paper shows again that the CR-39/PM-355 detector is an useful diagnostic tool for tokamak experiments, for measurement of charged ions. References: [1] A. Szydlowski, A. Malinowska, M. Jaskola, A. Korman, M.J. Sadowski, G. Van Wassenhove, B. Schweer and the TEXTOR team, A. Galkowski, 'Application of Solid State Nuclear Track Detectors in TEXTOR Experiment for Measurements

Assessment of radiation shielding materials for protection of space crews using CR-39 plastic nuclear track detector

International Nuclear Information System (INIS)

DeWitt, J.M.; Benton, E.R.; Uchihori, Y.; Yasuda, N.; Benton, E.V.; Frank, A.L.

2009-01-01

A significant obstacle to long duration human space exploration such as the establishment of a permanent base on the surface of the Moon or a human mission to Mars is the risk posed by prolonged exposure to space radiation. In order to keep mission costs at acceptable levels while simultaneously minimizing the risk from radiation to space crew health and safety, a judicious use of optimized shielding materials will be required. We have undertaken a comprehensive study using CR-39 plastic nuclear track detector (PNTD) to characterize the radiation shielding properties of a range of materials-both common baseline materials such as Al and polyethylene, and novel multifunctional materials such as carbon composites-at heavy ion accelerators. The study consists of analyzing CR-39 PNTD exposed in front of and behind shielding targets of varying composition and at a number of depths (target thicknesses) relevant to the development and testing of materials for space radiation shielding. Most targets consist of 10 cm x 10 cm slabs of solid materials ranging in thickness from 1 to >30 g/cm 2 . Exposures have been made to beams of C, O, Ne, Si, Ar, and Fe at energies ranging from 290 MeV/amu to 1 GeV/amu at the National Institute of Radiological Sciences HIMAC and the NASA Space Radiation Laboratory (NSRL) at Brookhaven National Laboratory. Analysis of the exposed detectors yields LET spectrum, dose, and dose equivalent as functions of target depth and composition, and incident heavy ion charge, energy, and fluence. Efforts are currently underway to properly weigh and combine these results into a single quantitative estimate of a material's ability to shield space crews from the interplanetary galactic cosmic ray flux.

Determination of exhalation rate of radon from walls and indoor radon by CR-39 detectors

International Nuclear Information System (INIS)

Vasidov, A.; Tillaev, T.S.

2007-01-01

Full text: The knowledge of true value exhalation rate of radon gas from building materials represents scientific and practical interest in environmental radiation protection. This point of view in the paper exhalation rate of radon gas from building materials and a surface of walls with different constructions were determined by detectors CR-39. The values of the exhalation rate of radon per unit area of the granite, concrete, fired and unfired bricks, sand, cement, alabaster varied 0.091 - 0.1 Bq·m -2 ·h -1 . The surface of walls of dwellings constructed from different building materials the exhalation rate of radon are within in limits of 0.083-1.12 Bq·m -2 ·h -1 . Were measurements with CR-39 detectors a level of radon within 50-520 Bq/m 3 in air of rooms constructed of the different building materials

Pershore made CR-39(DOP) as a 1.015 GeV/n 197Au-ion detector

International Nuclear Information System (INIS)

Bhattacharyya, D.P.; Chakrabarty, S.; Rakshit, R.; Basu, B.; Pal, P.; Biswas, S.

1993-01-01

Pershore made CR-39(DOP) stack was exposed at a zenith angle of 30deg by 197 Au-ions of energy 1.015 GeV/n using LBL BEVALAC beam. The top of the irradiated plate of the stack has been etched in 6.25N NaOH solution at 70degC for one hour. About 1202 cone lengths were optically measured. The estimated etch rate ratio of the incident 197 Au projectile beam in CR-39 has been found to be 27±2. The result has been compared with earlier observation. The charge resolution of the detector has been estimated from the average of double cone lengths and has been found to have a value of (0.58±0.03)e for 197 Au-ions. (orig.)

Environmental dosimetry of radon-222 and daughters: measurement of absolute calibration factors of CR-39 considering the plate-out effects and environmental factors

International Nuclear Information System (INIS)

Paulo, S.R. de.

1991-08-01

The subject of this work concerns with the measurement of absolute calibration factors for the use of CR-39 as an absolute detector in indoor and daughters monitoring. Up to now the usefulness of calibration factors was restricted to environmental conditions equal (or very close) to those worthing during their determinations. This fact is consequence of the difficulties related to the understanding of the plate-out properties of radon daughters activity in the air. The plate-out effects on radon daughters monitoring performed by SSNTDs are studied. Our experimental results are in agreement with those of other authors about the great sensitivity of CR-39 to the plate-out effects, fact that recommended its use in this work. Being succeeded in the employment of CR-39 as an alpha-spectrometer we concluded that some important information (like the radon daughters deposition rates on the walls of an environment) can be achieved. The knowledge about the behavior of plate-out made possible the determination of the ranges in zenithal angle and energy where CR-39 can detect alpha-particles with efficiency of 100%, at our conditions of track observation. In this way, we obtained calibration factors for CR-39 that are weakly dependent on environmental conditions. We think that these results can contribute to the improvement of RD (Radiation Detector) detection techniques. (author). 159 refs, 106 figs, 05 tabs

A parameterization of nuclear track profiles in CR-39 detector

Science.gov (United States)

Azooz, A. A.; Al-Nia'emi, S. H.; Al-Jubbori, M. A.

2012-11-01

In this work, the empirical parameterization describing the alpha particles’ track depth in CR-39 detectors is extended to describe longitudinal track profiles against etching time for protons and alpha particles. MATLAB based software is developed for this purpose. The software calculates and plots the depth, diameter, range, residual range, saturation time, and etch rate versus etching time. The software predictions are compared with other experimental data and with results of calculations using the original software, TRACK_TEST, developed for alpha track calculations. The software related to this work is freely downloadable and performs calculations for protons in addition to alpha particles. Program summary Program title: CR39 Catalog identifier: AENA_v1_0 Program summary URL:http://cpc.cs.qub.ac.uk/summaries/AENA_v1_0.html Program obtainable from: CPC Program Library, Queen’s University, Belfast, N. Ireland Licensing provisions: Copyright (c) 2011, Aasim Azooz Redistribution and use in source and binary forms, with or without modification, are permitted provided that the following conditions are met • Redistributions of source code must retain the above copyright, this list of conditions and the following disclaimer. • Redistributions in binary form must reproduce the above copyright notice, this list of conditions and the following disclaimer in the documentation and/or other materials provided with the distribution This software is provided by the copyright holders and contributors “as is” and any express or implied warranties, including, but not limited to, the implied warranties of merchantability and fitness for a particular purpose are disclaimed. In no event shall the copyright owner or contributors be liable for any direct, indirect, incidental, special, exemplary, or consequential damages (including, but not limited to, procurement of substitute goods or services; loss of use, data, or profits; or business interruption) however caused and

Effect of argon ion implantation on the electrical and dielectric properties of CR-39

International Nuclear Information System (INIS)

Chawla, Mahak; Shekhawat, Nidhi; Goyal, Meetika; Gupta, Divya; Sharma, Annu; Aggarwal, Sanjeev

2016-01-01

The objective of the present work is to study the effect of 130 keV Ar"+ ions on the electrical and dielectric properties of CR-39 samples at various doses 5×10"1"4, 1×10"1"5 and 1×10"1"6 Ar"+ cm"−"2. Current-Voltage (I-V characteristics) measurements have been used to study the electrical properties of virgin and Ar"+ implanted CR-39 specimens. The current has been found to be increased with increasing voltage as well as with increasing ion dose. The dielectric spectroscopy of these specimens has been done in the frequency range of 100 kHz-100 MHz. The dielectric constant has been found to be decreasing whereas dielectric loss factor increases with increasing ion fluence. These kind of behavior observed in the implanted specimens indicate towards the formation of carbonaceous clusters due to the cross linking, chemical bond cleavage, formation of free radicals. The changes observed in the dielectric behavior have been further correlated with the structural changes observed through I-V characteristics.

Long-term measurements of equilibrium factor with electrochemically etched CR-39 SSNTD

International Nuclear Information System (INIS)

Ng, F.M.F.; Nikezic, D.; Yu, K.N.

2007-01-01

Recently, our group proposed a method (proxy equilibrium factor method) using a bare LR 115 detector for long-term monitoring of the equilibrium factor. Due to the presence of an upper alpha-particle energy threshold for track formation in the LR 115 detector, the partial sensitivities to 222 Rn, 218 Po and 214 Po were the same, which made possible measurements of a proxy equilibrium factor F p that was well correlated with the equilibrium factor. In the present work, the method is extended to CR-39 detectors which have better-controlled etching properties but do not have an upper energy threshold. An exposed bare CR-39 detector is first pre-etched in 6.25 N NaOH solution at 70 o C for 6 h, and then etched electrochemically in a 6.25 N NaOH solution with ac voltage of 400 V (peak to peak) and 5 kHz applied across the detectors for 1 h at room temperature. Under these conditions, for tracks corresponding to incident angles larger than or equal to 50 deg., the treeing efficiency is 0% and 100% for incident energies smaller than and larger than 4 MeV, respectively. A simple method is then proposed to obtain the total number of tracks formed below the upper energy threshold of 4 MeV, from which the proxy equilibrium factor method can apply

Calibrations of CR39 and Makrofol nuclear track detectors and search for exotic particles

CERN Document Server

Ambrosio, M; Auriemma, G; Bakari, D; Baldini, A; Barbarino, G C; Barish, B C; Battistoni, G; Becherini, Y; Bellotti, R; Bemporad, C; Bernardini, P; Bilokon, H; Bloise, C; Bower, C; Brigida, M; Bussino, S; Cafagna, F; Calicchio, M; Campana, D; Carboni, M; Caruso, R; Cecchini, S; Cei, F; Chiarella, V; Chiarusi, T; Choudhary, B C; Coutu, S; Cozzi, M; De Cataldo, G; De Marzo, C; De Mitri, I; De Vincenzi, M; Dekhissi, H; Derkaoui, J; Di Credico, A; Erriquez, O; Favuzzi, C; Forti, C; Fusco, P; Giacomelli, G; Giannini, G; Giglietto, N; Giorgini, M; Grassi, M; Grillo, A; Guarino, F; Gustavino, C; Habig, A; Hanson, K; Heinz, R; Iarocci, E; Katsavounidis, E; Katsavounidis, I; Kearns, E; Kim, H; Kumar, A; Kyriazopoulou, S; Lamanna, E; Lane, C; Levin, D S; Lipari, P; Longley, N P; Longo, M J; Loparco, F; Maaroufi, F; Mancarella, G; Mandrioli, G; Manzoor, S; Margiotta, A; Marini, A; Martello, D; Marzari-Chiesa, A; Matteuzzi, D; Mazziotta, M N; Michael, D G; Monacelli, P; Montaruli, T; Monteno, M; Mufson, S; Musser, J; Nicolò, D; Nolty, R; Orth, C; Osteria, G; Palamara, O; Patera, V; Patrizii, L; Pazzi, R; Peck, C W; Perrone, L; Petrera, S; Pistilli, P; Popa, V; Rainó, A; Reynoldson, J; Ronga, F; Rrhioua, A; Satriano, C; Scapparone, E; Scholberg, K; Sciubba, A; Serra, P; Sioli, M; Sirri, G; Sitta, M; Spinelli, P; Spinetti, M; Spurio, M; Steinberg, R; Stone, J L; Sulak, L R; Surdo, A; Tarle, G; Togo, V; Vakili, M; Walter, C W; Webb, R; 10.1016/S0920-5632(03)02249-7

2003-01-01

We present the final results of the search for exotic massive particles in the cosmic radiation performed with the MACRO underground experiment. Magnetic monopoles and nuclearites flux upper limits obtained with the CR39 nuclear track subdetector, the scintillation and streamer tube subdetectors are given. Searches at high altitude with the SLIM experiment are in progress.

Ventilation rate in equilibrium factor measurements with solid state nuclear track detectors (SSNTD)

International Nuclear Information System (INIS)

Gil, L.R.; Leitao, R.M.S.; Marques, A.; Rivera, A.

1994-08-01

Ventilation rate values are calculated from track density measurements in solid state nuclear track detectors (SSNTD), both when ventilation is the main cause of radioactive disequilibrium in radon progeny and when it shares importance with other agents. The method consists in exposing a SSNTD of high intrinsic efficiency (CR-39) in filtered and unfiltered conditions and, in addition, covered with a thin Aluminium foil, to stop alpha particles from 218 Po and 222 Rn. No calibrations are required but, when necessary, independent measurements of the loss rates of radioactivity to aerosol and to walls have to perform. Ventilation rates depend upon geometry detection efficiencies for alpha particles, here obtained by Monte Carlo simulation, taking into account the space distribution of emission positions. This may lead to sizeable corrections in ventilation and equilibrium factor values. Since geometric detection efficiencies depend upon alpha-particle ranges in air, the influences of barometric variables are also discussed. (author). 7 refs

The use of CH3OH additive to NaOH for etching alpha particle tracks in a CR-39 plastic nuclear track detector

International Nuclear Information System (INIS)

Ashry, A.H.; Abdalla, A.M.; Rammah, Y.S.; Eisa, M.; Ashraf, O.

2014-01-01

Fast detection of alpha particles in CR-39 detectors was investigated using a new chemical etchant. 252 Cf and 241 Am sources were used for irradiating samples of CR-39 SSNTDs with fission fragments and alpha particles in air at normal temperature and pressure. A series of experimental chemical etching are carried out using new etching solution (8 ml of 10N NaOH+1 ml CH 3 OH) at 60 °C to detect alpha particle in short time in CR-39 detectors. Suitable analyzing software has been used to analyze experimental data. From fission and alpha track diameters, the value of bulk etching rate is equal to 2.73 μm/h. Both the sensitivity and etching efficiency were found to vary with the amount of methanol in the etching solution. Pure NaOH was used as a control to compare with the result from etching in NaOH with different concentrations of CH 3 OH. The etching efficiency is determined and compared with conventional aqueous solution of 6.25N NaOH at 70 °C for etching time equals 5 h. In this study, the obtained etching efficiency shows a considerable agreement with the previous work. - Highlights: • The value of bulk etching rate is equal to 2.73 μm/h. • Fast detection of alpha particles in CR-39 detectors. • Samples of CR-39 have been irradiated with fission fragments. • Etching efficiency was determined

Solid state physics

CERN Document Server

Burns, Gerald

2013-01-01

Solid State Physics, International Edition covers the fundamentals and the advanced concepts of solid state physics. The book is comprised of 18 chapters that tackle a specific aspect of solid state physics. Chapters 1 to 3 discuss the symmetry aspects of crystalline solids, while Chapter 4 covers the application of X-rays in solid state science. Chapter 5 deals with the anisotropic character of crystals. Chapters 6 to 8 talk about the five common types of bonding in solids, while Chapters 9 and 10 cover the free electron theory and band theory. Chapters 11 and 12 discuss the effects of moveme

Effects of high neutron doses and duration of the chemical etching on the optical properties of CR-39

International Nuclear Information System (INIS)

Sahoo, G.S.; Tripathy, S.P.; Paul, S.; Sharma, S.C.; Joshi, D.S.; Gupta, A.K.; Bandyopadhyay, T.

2015-01-01

Effects of the duration of chemical etching on the transmittance, absorbance and optical band gap width of the CR-39 (Polyallyl diglycol carbonate) detectors irradiated to high neutron doses (12.7, 22.1, 36.0 and 43.5 Sv) were studied. The neutrons were produced by bombardment of a thick Be target with 12 MeV protons of different fluences. The unirradiated and neutron-irradiated CR-39 detectors were subjected to a stepwise chemical etching at 1 h intervals. After each step, the transmission spectra of the detectors were recorded in the range from 200 to 900 nm, and the absorbances and optical band gap widths were determined. The effect of the etching on the light transmittance of unirradiated detectors was insignificant, whereas it was very significant in the case of the irradiated detectors. The dependence of the optical absorbance on the neutron dose is linear at short etching periods, but exponential at longer ones. The optical band gap narrows with increasing etching time. It is more significant for the irradiated dosimeters than for the unirradiated ones. The rate of the narrowing of the optical band gap with increasing neutron dose increases with increasing duration of the etching. - Highlights: • The variation of optical properties of CR-39 at very high neutron dose is analyzed. Etching process is found to play a crucial role for change in optical properties of neutron-irradiated CR-39. • The optical absorbance varies linearly at lower dose, at very high dose absorbance saturation occurs. The dose at which saturation absorbance is observed shifts towards lower neutron dose with increase in etching time. • The rate of decrease in optical band gap with respect to neutron dose is found to be more at higher etching durations

Structural analysis and magnetic properties of solid solutions of Co–Cr system obtained by mechanical alloying

International Nuclear Information System (INIS)

Betancourt-Cantera, J.A.; Sánchez-De Jesús, F.; Bolarín-Miró, A.M.; Betancourt, I.; Torres-Villaseñor, G.

2014-01-01

In this paper, a systematic study on the structural and magnetic properties of Co 100−x Cr x alloys (0 1−x Cr x (0 2 /kg) for the Co 90 Cr 10 , which decreases with the increasing of the Cr content up to x=80, as a consequence of the dilution effect of the magnetic moment which is caused by the Cr content and by the competition between ferromagnetic and antiferromagnetic exchange interactions. The coercivity increases up to 34 kA/m (435 Oe) for Co 40 Cr 60 . For Cr rich compositions, it is observed an important decrease reaching 21 kA/m (272 Oe) for Co 10 Cr 90, it is related to the grain size and the structural change. Besides, the magnetic anisotropy constant was determined for each composition. Magnetic thermogravimetric analysis allowed to obtain Curie temperatures corresponding to the formation of hcp-Co(Cr) and fcc-Co(Cr) solid solutions. - Highlights: • Mechanical alloying (MA) induces the formation of solid solutions of Co–Cr system in non-equilibrium. • We report the crystal structure and the magnetic behavior of Co–Cr alloys produced by MA. • MA improves the magnetic properties of Co–Cr system

Thermal degradation of CR-39 polymer in an inert atmosphere

International Nuclear Information System (INIS)

Kalsi, P.C.; Pandey, A.K.; Iyer, R.H.; Singh Mudher, K.D.

1995-01-01

The thermal degradation of CR-39 (allyl diglycol carbonate), a polymer widely used in nuclear science and technology, in an inert atmosphere has been studied using thermogravimetric analysis (TGA) and differential thermal analysis (DTA) techniques. The results are compared with the thermal degradation data of the polymer in an air atmosphere. The present studies showed that the thermal degradation of the polymer proceeds in two steps in an argon atmosphere as compared to three steps in air atmosphere. The mass losses in air are higher than that in argon due to the oxidative decomposition of the residue. The kinetics of the different stages of degradation were also evaluated from the TG curves. (author). 7 refs., 1 tab

The development of an automatic scanning method for CR-39 neutron dosimeter

International Nuclear Information System (INIS)

Tawara, Hiroko; Miyajima, Mitsuhiro; Sasaki, Shin-ichi; Hozumi, Ken-ichi

1989-01-01

A method of measuring low level neutron dose has been developed with CR-39 track detectors using an automatic scanning system. It is composed of the optical microscope with a video camera, an image processor and a personal computer. The focus point of the microscope and the X-Y stage are controlled from the computer. The minimum detectable neutron dose is estimated at 4.6 mrem in the uniform field of neutron with equivalent energy spectrum to Am-Be source from the results of automatic measurements. (author)

Alpha activity of 190 Pt isotope measured with CR-39 track detector

International Nuclear Information System (INIS)

Tavares, O.A.P.; Terranova, M.L.

1996-11-01

A new method to measure alpha activity of long-lived radioisotopes is reported. The method consists basically in using CR-39 track detectors in close contact with thick samples of the radioelement to be investigated. Accordingly, a long-term exposure experiment has been performed using metallic sheets of natural platinum to measure alpha activity of platinum 190 isotope. The half-life of platinum 190 has been obtained in good agreement with two recent theoretical half-life predictions. (author). 21 refs., 3 figs., 2 tabs

Alpha-particle dosimetry using solid state nuclear track detectors. Application to 222Rn and its daughters

International Nuclear Information System (INIS)

Barillon, R.; Chambaudet, A.

2000-01-01

A methodology for the determination of the detection efficiency of a solid state nuclear track detector for radon and its short-lived daughters was presented. First, particular attention is paid to the α-particles having energies and angles of incidence that lead to observable tracks after an adapted chemical etching. The results are then incorporated in a mathematical model to determine the theoretical radon detection efficiency of a polymeric detector placed in a cylindrical cell. When applied to LR115 and CR39 detectors, the model reveals the influence of the position of the radon daughters inside the cell. Radon daughters tend to link up with natural atmospheric aerosols and then settle on the cell's inside wall. This model allows to determine, among other things, the cell size for which the detector response is independent of the fraction daughters plated out. (author)

Structural analysis and magnetic properties of solid solutions of Co–Cr system obtained by mechanical alloying

Energy Technology Data Exchange (ETDEWEB)

Betancourt-Cantera, J.A. [Área Académica de Ciencias de la Tierra y Materiales, UAEH Carr., Pachuca-Tulancingo Km. 4.5, Pachuca, Hidalgo 42184 (Mexico); Sánchez-De Jesús, F., E-mail: fsanchez@uaeh.edu.mx [Área Académica de Ciencias de la Tierra y Materiales, UAEH Carr., Pachuca-Tulancingo Km. 4.5, Pachuca, Hidalgo 42184 (Mexico); Bolarín-Miró, A.M. [Área Académica de Ciencias de la Tierra y Materiales, UAEH Carr., Pachuca-Tulancingo Km. 4.5, Pachuca, Hidalgo 42184 (Mexico); Betancourt, I.; Torres-Villaseñor, G. [Departamento de Materiales Metálicos y Cerámicos, Instituto de Investigaciones en Materiales, Universidad Nacional Autónoma de México, México D.F. 04510 (Mexico)

2014-03-15

In this paper, a systematic study on the structural and magnetic properties of Co{sub 100−x}Cr{sub x} alloys (0Cr elemental powders were used as precursors, and mixed in an adequate weight ratio to obtain Co{sub 1−x}Cr{sub x} (0solid solutions based on Co-hcp, Co-fcc and Cr-bcc structures were obtained. The saturation polarization indicated a maximum value of 1.17 T (144 Am{sup 2}/kg) for the Co{sub 90}Cr{sub 10}, which decreases with the increasing of the Cr content up to x=80, as a consequence of the dilution effect of the magnetic moment which is caused by the Cr content and by the competition between ferromagnetic and antiferromagnetic exchange interactions. The coercivity increases up to 34 kA/m (435 Oe) for Co{sub 40}Cr{sub 60}. For Cr rich compositions, it is observed an important decrease reaching 21 kA/m (272 Oe) for Co{sub 10}Cr{sub 90,} it is related to the grain size and the structural change. Besides, the magnetic anisotropy constant was determined for each composition. Magnetic thermogravimetric analysis allowed to obtain Curie temperatures corresponding to the formation of hcp-Co(Cr) and fcc-Co(Cr) solid solutions. - Highlights: • Mechanical alloying (MA) induces the formation of solid solutions of Co–Cr system in non-equilibrium. • We report the crystal structure and the magnetic behavior of Co–Cr alloys produced by MA. • MA improves the magnetic properties of Co–Cr system.

High-spin states in the A=39 mirror nuclei 39Ca and 39K

International Nuclear Information System (INIS)

Andersson, T.; Rudolph, D.; Fahlander, C.; Eberth, J.; Thomas, H.G.; Haslip, D.; Svensson, C.E.; Waddington, J.C.; LaFosse, D.R.; Sarantites, D.G.; Weintraub, W.; Wilson, J.N.; Brown, B.A.

1999-01-01

High-spin states of the mass A=39 mirror pair 39 K and 39 Ca were investigated via the fusion-evaporation reaction 28 Si+ 16 O at 125 MeV beam energy. The gammasphere array in conjunction with the 4π charged-particle detector array microball and neutron detectors was used to detect γ rays in coincidence with evaporated light particles. The results of the first high-spin study of the T z =-1/2 nucleus 39 Ca are discussed in terms of mirror symmetry and compared to spherical shell-model calculations in the 1d 3/2 -1f 7/2 configuration space. (orig.)

Solid-state, flat-panel, digital radiography detectors and their physical imaging characteristics

Energy Technology Data Exchange (ETDEWEB)

Cowen, A.R. [LXi Research, Academic Unit of Medical Physics, University of Leeds, West Yorkshire (United Kingdom)], E-mail: a.r.cowen@leeds.ac.uk; Kengyelics, S.M.; Davies, A.G. [LXi Research, Academic Unit of Medical Physics, University of Leeds, West Yorkshire (United Kingdom)

2008-05-15

Solid-state, digital radiography (DR) detectors, designed specifically for standard projection radiography, emerged just before the turn of the millennium. This new generation of digital image detector comprises a thin layer of x-ray absorptive material combined with an electronic active matrix array fabricated in a thin film of hydrogenated amorphous silicon (a-Si:H). DR detectors can offer both efficient (low-dose) x-ray image acquisition plus on-line readout of the latent image as electronic data. To date, solid-state, flat-panel, DR detectors have come in two principal designs, the indirect-conversion (x-ray scintillator-based) and the direct-conversion (x-ray photoconductor-based) types. This review describes the underlying principles and enabling technologies exploited by these designs of detector, and evaluates their physical imaging characteristics, comparing performance both against each other and computed radiography (CR). In standard projection radiography indirect conversion DR detectors currently offer superior physical image quality and dose efficiency compared with direct conversion DR and modern point-scan CR. These conclusions have been confirmed in the findings of clinical evaluations of DR detectors. Future trends in solid-state DR detector technologies are also briefly considered. Salient innovations include WiFi-enabled, portable DR detectors, improvements in x-ray absorber layers and developments in alternative electronic media to a-Si:H.

Contribution to the study of radio toxicity of aromatic and medicinal plants using solid state nuclear track detectors; Contribution a l etude de la radio toxicite des plantes aromatiques et medicinales au moyen des detecteurs solides de traces nucleaires

Energy Technology Data Exchange (ETDEWEB)

Mortassim, A; Misdaq, M A; Naaman, A

2009-07-01

The concentrations of uranium (238 U), thorium (232 Th), radon (222 Rn) and thoron (220 Rn) were measured in twenty aromatic and medicinal plants in {sup f}ind a new method based on using solid state nuclear track detectors type Cr-39 and Rs-115. He emerges from this study that the verbena and salvia have higher levels of uranium (radon) higher than that of other plants while the leaves of olive and saturja have concentrations of thorium (thoron) higher than other plants therefore radio toxicity of these plants is higher than that of others and may pose a radiological hazard if the masses are incorporated by consumers high. [French] Les concentrations en uranium (238U), thorium (232Th), radon (222Rn), et thoron (220Rn) ont ete mesurees dans vingt plantes aromatiques et medicinales en utilsant une nouvelle methode basee sur l utilisation des detecteurs solides de traces nucleaires de types CR-39 et LR-115. Il en sort de cette etude que la verveine et la salvia presentent des teneurs en uranium (radon) superieurs a celle des autres plantes alors que les feuilles d olivier et la saturja presentent des concentrations en thorium (thoron) plus elevee que celles des autres plantes par consequent la radio toxicite de ces plantes est superieure a celles des autres et peuvent presenter un risque radiologique si les masses incorporees par les consommateurs sont elevees.

Regular self-microstructuring on CR39 using high UV laser dose

International Nuclear Information System (INIS)

Parvin, P.; Refahizadeh, M.; Mortazavi, S.Z.; Silakhori, K.; Mahdiloo, A.; Aghaii, P.

2014-01-01

The UV laser induced replicas in the form of self-lining microstructures are created by high dose (with high fluence) ArF laser irradiation on CR39. Microstructures as the self-induced contours, in the form of concentric circles, appear when the laser fluence is well above the ablation threshold. It leads to the regular periodic parallel lines, i.e. circles with large radii having spatial separation 100–200 nm and line width 300–600 nm, where the number of shots increases to achieve higher UV doses. The surface wettability is also investigated after laser texturing to exhibit that a notable hydrophilicity takes place at high doses.

Sensitivity of chemically and electrochemically etched CR 39 polymers to the neutrons of AmBe source

International Nuclear Information System (INIS)

Turek, K.; Spurny, F.; Dajko, G.; Somogyi, G.

1981-01-01

Seven samples of polymers by different manufacturers were used in a study of the sensitivity of CR 39 polymers to Am-Be neutrons. In the polymer, proton tracks for a relatively broad energy range can also be recorded. The following characteristics were studied: the sample background for different etching methods, the dependence of sensitivity on the etched thickness and on neutron fluence, the effect of type and thickness of external proton emitters, and the effect of the choice of electric parameters on the resulting sensitivity in electrochemical etching. Good results were obtained when chemical and electrochemical etching was used in combination. It was found that with electrochemical etching, sensitivity decreases for neutron fluence exceeding 10 8 cm -2 . The sensitivity of the studied CR 39 polymer samples only little differed. When the most sensitive polymer was used, the minimum dose equivalent in the human body for Am-Be neutrons which could be determined using combination etching was 0.4 mSv (ie., 40 mrems). (B.S.)

Cr(VI) generation during sample preparation of solid samples – A ...

African Journals Online (AJOL)

Cr(VI) generation during sample preparation of solid samples – A chromite ore case study. R.I Glastonbury, W van der Merwe, J.P Beukes, P.G van Zyl, G Lachmann, C.J.H Steenkamp, N.F Dawson, M.H Stewart ...

A novel method to recover DD fusion proton CR-39 data corrupted by fast ablator ions at OMEGA and the National Ignition Facility

Energy Technology Data Exchange (ETDEWEB)

Sutcliffe, G. D., E-mail: gdsut@mit.edu; Milanese, L. M.; Orozco, D.; Lahmann, B.; Gatu Johnson, M.; Séguin, F. H.; Sio, H.; Frenje, J. A.; Li, C. K.; Petrasso, R. D. [Plasma Science and Fusion Center, Massachusetts Institute of Technology, Cambridge, Massachusetts 02139 (United States); Park, H.-S.; Rygg, J. R.; Casey, D. T.; Bionta, R.; Turnbull, D. P.; Huntington, C. M.; Ross, J. S. [Lawrence Livermore National Laboratory, Livermore, California 94550 (United States); Zylstra, A. B. [Los Alamos National Laboratory, Los Alamos, New Mexico 87545 (United States); Rosenberg, M. J.; Glebov, V. Yu. [Laboratory for Laser Energetics, Rochester, New York 14623 (United States)

2016-11-15

CR-39 detectors are used routinely in inertial confinement fusion (ICF) experiments as a part of nuclear diagnostics. CR-39 is filtered to stop fast ablator ions which have been accelerated from an ICF implosion due to electric fields caused by laser-plasma interactions. In some experiments, the filtering is insufficient to block these ions and the fusion-product signal tracks are lost in the large background of accelerated ion tracks. A technique for recovering signal in these scenarios has been developed, tested, and implemented successfully. The technique involves removing material from the surface of the CR-39 to a depth beyond the endpoint of the ablator ion tracks. The technique preserves signal magnitude (yield) as well as structure in radiograph images. The technique is effective when signal particle range is at least 10 μm deeper than the necessary bulk material removal.

A novel method to recover DD fusion proton CR-39 data corrupted by fast ablator ions at OMEGA and the National Ignition Facility

International Nuclear Information System (INIS)

Sutcliffe, G. D.; Milanese, L. M.; Orozco, D.; Lahmann, B.; Gatu Johnson, M.; Séguin, F. H.; Sio, H.; Frenje, J. A.; Li, C. K.; Petrasso, R. D.; Park, H.-S.; Rygg, J. R.; Casey, D. T.; Bionta, R.; Turnbull, D. P.; Huntington, C. M.; Ross, J. S.; Zylstra, A. B.; Rosenberg, M. J.; Glebov, V. Yu.

2016-01-01

CR-39 detectors are used routinely in inertial confinement fusion (ICF) experiments as a part of nuclear diagnostics. CR-39 is filtered to stop fast ablator ions which have been accelerated from an ICF implosion due to electric fields caused by laser-plasma interactions. In some experiments, the filtering is insufficient to block these ions and the fusion-product signal tracks are lost in the large background of accelerated ion tracks. A technique for recovering signal in these scenarios has been developed, tested, and implemented successfully. The technique involves removing material from the surface of the CR-39 to a depth beyond the endpoint of the ablator ion tracks. The technique preserves signal magnitude (yield) as well as structure in radiograph images. The technique is effective when signal particle range is at least 10 μm deeper than the necessary bulk material removal.

A novel method to recover DD fusion proton CR-39 data corrupted by fast ablator ions at OMEGA and the National Ignition Facility

Energy Technology Data Exchange (ETDEWEB)

Sutcliffe, G. D. [Plasma Science and Fusion Center, Massachusetts Institute of Technology, Cambridge, Massachusetts 02139, USA; Milanese, L. M. [Plasma Science and Fusion Center, Massachusetts Institute of Technology, Cambridge, Massachusetts 02139, USA; Orozco, D. [Plasma Science and Fusion Center, Massachusetts Institute of Technology, Cambridge, Massachusetts 02139, USA; Lahmann, B. [Plasma Science and Fusion Center, Massachusetts Institute of Technology, Cambridge, Massachusetts 02139, USA; Gatu Johnson, M. [Plasma Science and Fusion Center, Massachusetts Institute of Technology, Cambridge, Massachusetts 02139, USA; Séguin, F. H. [Plasma Science and Fusion Center, Massachusetts Institute of Technology, Cambridge, Massachusetts 02139, USA; Sio, H. [Plasma Science and Fusion Center, Massachusetts Institute of Technology, Cambridge, Massachusetts 02139, USA; Frenje, J. A. [Plasma Science and Fusion Center, Massachusetts Institute of Technology, Cambridge, Massachusetts 02139, USA; Li, C. K. [Plasma Science and Fusion Center, Massachusetts Institute of Technology, Cambridge, Massachusetts 02139, USA; Petrasso, R. D. [Plasma Science and Fusion Center, Massachusetts Institute of Technology, Cambridge, Massachusetts 02139, USA; Park, H. -S. [Lawrence Livermore National Laboratory, Livermore, California 94550, USA; Rygg, J. R. [Lawrence Livermore National Laboratory, Livermore, California 94550, USA; Casey, D. T. [Lawrence Livermore National Laboratory, Livermore, California 94550, USA; Bionta, R. [Lawrence Livermore National Laboratory, Livermore, California 94550, USA; Turnbull, D. P. [Lawrence Livermore National Laboratory, Livermore, California 94550, USA; Huntington, C. M. [Lawrence Livermore National Laboratory, Livermore, California 94550, USA; Ross, J. S. [Lawrence Livermore National Laboratory, Livermore, California 94550, USA; Zylstra, A. B. [Los Alamos National Laboratory, Los Alamos, New Mexico 87545, USA; Rosenberg, M. J. [Laboratory for Laser Energetics, Rochester, New York 14623, USA; Glebov, V. Yu. [Laboratory for Laser Energetics, Rochester, New York 14623, USA

2016-08-05

CR-39 detectors are used routinely in inertial confinement fusion (ICF) experiments as a part of nuclear diagnostics. CR-39 is filtered to stop fast ablator ions which have been accelerated from an ICF implosion due to electric fields caused by laser-plasma interactions. In some experiments, the filtering is insufficient to block these ions and the fusion-product signal tracks are lost in the large background of accelerated ion tracks. A technique for recovering signal in these scenarios has been developed, tested, and implemented successfully. The technique involves removing material from the surface of the CR-39 to a depth beyond the endpoint of the ablator ion tracks. The technique preserves signal magnitude (yield) as well as structure in radiograph images. The technique is effective when signal particle range is at least 10 μm deeper than the necessary bulk material removal.

Alpha-particle autoradiography in CR-39: a technique for quantitative assessment of alpha-emitters in biological tissue

International Nuclear Information System (INIS)

Fews, A.P.; Henshaw, D.L.

1983-01-01

The techniques for α-particle autoradiography based on the plastic nuclear track detector CR-39, previously reported, have been developed considerably. The techniques are applied to α-autoradiography of human lung tissue in particular but are applicable to any biological tissue. The most important developments are: (i) Improvements in the manufacture and pre-etching of the plastic. (ii) High resolution α-particle spectroscopy in CR-39 plastic based on the analysis of the structure of the etched track. (iii) Calculation of the effective thickness of tissue sampled by the plastic. (iv) A deconvolution analysis which takes the distributions of track length and dip angle in the plastic and determines the α-particle range spectrum and distribution of tissue activity with height above the plastic surface. (v) The analysis of radon diffusion in tissue to determine the mean radon diffusion distance in tissue and plastic. (author)

Bulk and surface properties of liquid Al-Cr and Cr-Ni alloys

International Nuclear Information System (INIS)

Novakovic, R

2011-01-01

The energetics of mixing and structural arrangement in liquid Al-Cr and Cr-Ni alloys has been analysed through the study of surface properties (surface tension and surface segregation), dynamic properties (chemical diffusion) and microscopic functions (concentration fluctuations in the long-wavelength limit and chemical short-range order parameter) in the framework of statistical mechanical theory in conjunction with quasi-lattice theory. The Al-Cr phase diagram exhibits the existence of different intermetallic compounds in the solid state, while that of Cr-Ni is a simple eutectic-type phase diagram at high temperatures and includes the low-temperature peritectoid reaction in the range near a CrNi 2 composition. Accordingly, the mixing behaviour in Al-Cr and Cr-Ni alloy melts was studied using the complex formation model in the weak interaction approximation and by postulating Al 8 Cr 5 and CrNi 2 chemical complexes, respectively, as energetically favoured.

Bulk and surface properties of liquid Al-Cr and Cr-Ni alloys.

Science.gov (United States)

Novakovic, R

2011-06-15

The energetics of mixing and structural arrangement in liquid Al-Cr and Cr-Ni alloys has been analysed through the study of surface properties (surface tension and surface segregation), dynamic properties (chemical diffusion) and microscopic functions (concentration fluctuations in the long-wavelength limit and chemical short-range order parameter) in the framework of statistical mechanical theory in conjunction with quasi-lattice theory. The Al-Cr phase diagram exhibits the existence of different intermetallic compounds in the solid state, while that of Cr-Ni is a simple eutectic-type phase diagram at high temperatures and includes the low-temperature peritectoid reaction in the range near a CrNi(2) composition. Accordingly, the mixing behaviour in Al-Cr and Cr-Ni alloy melts was studied using the complex formation model in the weak interaction approximation and by postulating Al(8)Cr(5) and CrNi(2) chemical complexes, respectively, as energetically favoured.

STUDYING THE STRUCTURAL, OPTICAL, CHEMICAL AND ELECTROCHEMICAL ETCHING CHANGES OF CR-39 FOR DOSEMETRIC APPLICATIONS.

Science.gov (United States)

Zaki, M F; Elshaer, Y H; Taha, Doaa H

2017-12-01

The present work shows the induced modification of the structural, optical, chemical etching and electrochemical etching parameters of CR-39 irradiated with alpha-particles. CR-39 polymer track detectors were irradiated with different fluences (1.62 × 106, 2.72 × 106, 3.82 × 106 and 5.21 × 106 particles/cm2) of alpha-particles using 241Am source. The structural and optical properties were measured by FT-IR spectroscopy, X-ray diffraction and UV/Vis spectroscopy, respectively. The FT-IR spectra reveal that no major changes in the typical functional groups of irradiated polymer detectors. The X-ray diffraction patterns show that a broad band in the region of 12° 27°, which refers to the presence of the combination of amorphous and crystalline phases. UV/Vis responses of irradiated polymer track detectors exhibit a single absorption band in the range of 254-352 nm that is correlated to the occurrence of electronic transition. Also, the changes in the chemical and electrochemical parameters due to alpha-irradiation are examined and thoroughly discussed. © The Author 2017. Published by Oxford University Press. All rights reserved. For Permissions, please email: journals.permissions@oup.com.

Solid State Division

International Nuclear Information System (INIS)

Green, P.H.; Watson, D.M.

1989-08-01

This report contains brief discussions on work done in the Solid State Division of Oak Ridge National Laboratory. The topics covered are: Theoretical Solid State Physics; Neutron scattering; Physical properties of materials; The synthesis and characterization of materials; Ion beam and laser processing; and Structure of solids and surfaces

Sulfur solubility of liquid and solid Fe-Cr alloys. A thermodynamic analysis

Energy Technology Data Exchange (ETDEWEB)

Waldner, Peter [Leoben Univ. (Austria). Dept. of General, Analytical and Physical Chemistry

2015-04-15

Gibbs energy modeling for sulfur solving liquid and solid iron-chromium phases with body- and face-centered cubic structure has been carried out using a substitutional approach. Experimental data available from the literature on sulfur potentials in the temperature range 1 525 to 1 755 C for the liquid metallic phase and 1 000 to 1 300 C for the solid alloys have been taken into consideration. Recent thermodynamic evaluations of the Fe-S and Cr-S binary subsystems served as basis for the presented work. The obtained models allow a satisfactory reproduction of the majority of the sulfur potential data as well as the prediction of an isothermal partial section at 1 300 C. Consistent embedding of the optimized Gibbs energies within a recent thermodynamic modeling of the complete Cr-Fe-S system is achieved.

Study of the pore-opening process of latent tracks of light low-energetic ions in CR-39 by means of electrolytic etching

International Nuclear Information System (INIS)

Oganesyan, V.R.

2005-01-01

In this thesis the irradiation of 10-μm thick CR-39 foils with 5.5-7 MeV protons and of 22-400 μm thick CR-39 foils with 4.85-28 MeV α-particles with subsequent determination of the etching velocities is described. By means of scanning electron microscopy (SEM) the pore shape after irradiation was determined. From the analysis of the track profiles by means of SEM the track-nucleus diameter for 28 MeV α particles was determined to 1.4 nm. (HSI)

Solid state welding processes for an oxide dispersion strengthened nickel-chromium-aluminum alloy

Science.gov (United States)

Moore, T. J.

1975-01-01

Solid-state welding processes were evaluated for joining TD-NiCrAl (Ni-16Cr-4Al-2ThO2) alloy sheet. Both hot-press and resistance spot welding techniques were successfully applied in terms of achieving grain growth across the bond line. Less success was achieved with a resistance seam welding process. In stress-rupture shear and tensile shear tests of lap joints at 1100 C, most failures occurred in the parent material, which indicates that the weld quality was good and that the welds were not a plane of weakness. The overall weld quality was not as good as previously attained with TD-NiCr, probably because the presence of alumina at the faying surfaces and the developmental TD-NiCrAl sheet, which was not of the quality of the TD-NiCr sheet in terms of surface flatness and dimensional control.

Solid State Division

Energy Technology Data Exchange (ETDEWEB)

Green, P.H.; Watson, D.M. (eds.)

1989-08-01

This report contains brief discussions on work done in the Solid State Division of Oak Ridge National Laboratory. The topics covered are: Theoretical Solid State Physics; Neutron scattering; Physical properties of materials; The synthesis and characterization of materials; Ion beam and laser processing; and Structure of solids and surfaces. (LSP)

Charge resolution of a Hungarian brand CR-39(MA-ND) detector exposed to a 84Kr beam of energy 0.45A GeV

International Nuclear Information System (INIS)

Bhattacharyya, D.P.; Basu, B.; Pal, P.; Mukherjee, S.C.; Ganguly, A.K.; Hunyady, I.

1990-01-01

The Hungarian brand CR-39(MA-ND) plastic has been irradiated with a 84 Kr ion beam of energy 0.45A GeV and etched for four different etching times, viz. 4, 6, 8 and 12 h. The estimated charge resolution of a CR-39(MA-ND) detector for registering the nuclei 32 ≤ Z ≤ 36 was found to be 0.18e which is close to our previous observation of the response with a CR-39(DOP) Pershore made plate exposed to a 1.88A GeV 56 Fe beam at the Lawrence Berkeley Laboratory's Bevalac. It was found that the estimated etch rate ratio V T /V G is independent of etching time. The cone length and minor axis of the etch pits has been found to increase with etching time. (orig.)

Microstructure, state of internal stress and corrosion resistance of the short-time laser heat-treated nitrogen high-alloyed tool steel X30CrMoN151; Mikrostruktur, Eigenspannungszustand und Korrosionsbestaendigkeit des kurzzeitlaserwaermebehandelten hochstickstofflegierten Werkzeugstahls X30CrMoN151

Energy Technology Data Exchange (ETDEWEB)

Bohne, C. (ed.)

2000-07-01

This study compares the crystalline structure, state of internal stress and chemical properties of the high-alloyed nitrogen tool steel X30CrMoN15 1 and conventional cold work steel X39CrMo17 1. Transformation points A{sub c}1b and A{sub c}1e were calculated from residual austenite analysis and the c{sub m}/a{sub m} martensite ratios for various heating rates. This was used to generate a TTA (time-temperature-austenitisation) graph for X30CrMoN15 1 for the first time. Transmission electron microscopy and small-angle neutron scattering show that precipitates in nitrogen high-alloyed steel X30CrMoN15 1 can be eliminated completely by short-time laser heat treatment. The corrosion tests show that in contrast to X39CrMo17 1 X30CrMoN15 1 reacts more sensitively to parameter changes during short-time heat treatment in oxidising acid at pH 5-6. [German] Im Rahmen der Arbeit werden die Gefuegeausbildung, Eigenspannungen und chemische Eigenschaften des hochstickstofflegierten Werkzeugstahls X30CrMoN15 1 und des konventionellen Kaltarbeitsstahls X39CrMo17 1 verglichen. Aus den Restaustenitanalysen und den c{sub m}/a{sub m}-Verhaeltnissen des Martensits konnten die Umwandlungspunkte A{sub c1b} und A{sub c1e} fuer verschiedene Aufheizraten bestimmt und daraus ein bisher nicht bekanntes ZTA-Schaubild fuer den X30CrMoN15 1 erstellt werden. Transmissionselektronenmikroskopie und Neutronenkleinwinkelstreuung zeigen, dass sich die Ausscheidungen im hochstickstofflegierten Stahl X30CrMoN14 1 durch die Kurzzeitlaserwaermebehandlung vollstaendig aufloesen koennen. Die Korrosionsversuche zeigen, dass im Gegensatz zum X39CrMo17 1 der X30CrMoN15 1 in oxidierender Saeure bei pH 5-6 empfindlicher auf Parameteraenderungen bei der Kurzzeitwaermebehandlung reagiert. (orig.)

A solid-state hybrid density functional theory study of Prussian blue analogues and related chlorides at pressure

Energy Technology Data Exchange (ETDEWEB)

Middlemiss, Derek S; Lawton, Lorreta M; Wilson, Chick C [Department of Chemistry and WestCHEM Research School, University Avenue, University of Glasgow, Glasgow G12 8QQ (United Kingdom)], E-mail: c.c.wilson@chem.gla.ac.uk

2008-08-20

The variations with pressure in the structural, electronic and magnetic properties of a series of Prussian blue analogues (PBAs) K{sup I}M{sup II}[Cr{sup III}(CN){sub 6}] (M = V{sup II}, Mn{sup II} and Ni{sup II}) and associated isomorphous chlorides K{sup I}M{sup II}Cr{sup III}Cl{sub 6} are investigated within a series of solid-state hybrid density functional calculations. The sensitivity of the computed properties to the choice of Hamiltonian is tested by application of functionals containing 35%, 65% and 100% admixtures of Fock exchange. Magnetic coupling constants (J) are obtained at a range of cell volumes (V), with fits of the Bloch relationship (J {proportional_to} V{sup -{epsilon}}, {epsilon} typically 3-4) yielding exponents {epsilon} in the ranges 5.16-6.34, 8.48-12.07 and 4.00-4.51 for the antiferromagnetic (AF) V{sup II}Cr{sup III}-, ferrimagnetic (FI) Mn{sup II}Cr{sup III}- and ferromagnetic (FO) Ni{sup II}Cr{sup III} PBAs, respectively; and 3.33-4.99, 1.86-3.09 and 1.65-3.28 for the AF V{sup II}Cr{sup III}-, FO Mn{sup II}Cr{sup III}- and FO Ni{sup II}Cr{sup III} chlorides, respectively. The Mn{sup II}Cr{sup III} PBA range encloses the high values {epsilon}{approx}9-10 obtained in a recent joint experimental and theoretical study, and it is suggested that this strong magnetostructural effect arises due to the presence of competing AF and FO interactions in this material. Estimates of the spin ordering temperatures derived from the combination of the 35%-functional couplings with a mean field approach are in good agreement with experiment in the V{sup II}Cr{sup III} and Ni{sup II}Cr{sup III} PBAs, but are too low in the Mn{sup II}Cr{sup III} system. The variations with pressure in the structural parameters, charges and spin moments are also detailed, the PBA and chloride energy-volume data yielding bulk moduli in the ranges 39-53 and 36-50 GPa, respectively. Finally, the energies governing CN{sup -} ligand isomerization are estimated and successfully

Issues concerning the determination of solubility products of sparingly soluble crystalline solids. Solubility of HfO2(cr)

International Nuclear Information System (INIS)

Rai, Dhanpat; Kitamura, Akira; Rosso, Kevin M.; Sasaki, Takayuki; Kobayashi, Taishi

2016-01-01

Solubility studies were conducted with HfO 2 (cr) solid as a function HCl and ionic strength ranging from 2.0 to 0.004 mol kg -1 . These studies involved (1) using two different amounts of the solid phase, (2) acid washing the bulk solid phase, (3) preheating the solid phase to 1400 C, and (4) heating amorphous HfO 2 (am) suspensions to 90 C to ascertain whether the HfO 2 (am) converts to HfO 2 (cr) and to determine the solubility from the oversaturation direction. Based on the results of these treatments it is concluded that the HfO 2 (cr) contains a small fraction of less crystalline, but not amorphous, material [HfO 2 (lcr)] and this, rather than the HfO 2 (cr), is the solubility-controlling phase in the range of experimental variables investigated in this study. The solubility data are interpreted using both the Pitzer and SIT models and they provide log 10 K 0 values of -(59.75±0.35) and -(59.48±0.41), respectively, for the solubility product of HfO 2 (lcr)[HfO 2 (lcr) + 2H 2 O ↔ Hf 4+ + 4OH - ]. The log 10 of the solubility product of HfO 2 (cr) is estimated to be < -63. The observation of a small fraction of less crystalline higher solubility material is consistent with the general picture that mineral surfaces are often structurally and/or compositionally imperfect leading to a higher solubility than the bulk crystalline solid. This study stresses the urgent need, during interpretation of solubility data, of taking precautions to make certain that the observed solubility behavior for sparingly-soluble solids is assigned to the proper solid phase.

Application of combined TLD and CR-39 PNTD method for measurement of total dose and dose equivalent on ISS

International Nuclear Information System (INIS)

Benton, E.R.; Deme, S.; Apathy, I.

2006-01-01

To date, no single passive detector has been found that measures dose equivalent from ionizing radiation exposure in low-Earth orbit. We have developed the I.S.S. Passive Dosimetry System (P.D.S.), utilizing a combination of TLD in the form of the self-contained Pille TLD system and stacks of CR-39 plastic nuclear track detector (P.N.T.D.) oriented in three mutually orthogonal directions, to measure total dose and dose equivalent aboard the International Space Station (I.S.S.). The Pille TLD system, consisting on an on board reader and a large number of Ca 2 SO 4 :Dy TLD cells, is used to measure absorbed dose. The Pille TLD cells are read out and annealed by the I.S.S. crew on orbit, such that dose information for any time period or condition, e.g. for E.V.A. or following a solar particle event, is immediately available. Near-tissue equivalent CR-39 P.N.T.D. provides Let spectrum, dose, and dose equivalent from charged particles of LET ∞ H 2 O ≥ 10 keV/μm, including the secondaries produced in interactions with high-energy neutrons. Dose information from CR-39 P.N.T.D. is used to correct the absorbed dose component ≥ 10 keV/μm measured in TLD to obtain total dose. Dose equivalent from CR-39 P.N.T.D. is combined with the dose component <10 keV/μm measured in TLD to obtain total dose equivalent. Dose rates ranging from 165 to 250 μGy/day and dose equivalent rates ranging from 340 to 450 μSv/day were measured aboard I.S.S. during the Expedition 2 mission in 2001. Results from the P.D.S. are consistent with those from other passive detectors tested as part of the ground-based I.C.C.H.I.B.A.N. intercomparison of space radiation dosimeters. (authors)

Theoretical solid state physics

CERN Document Server

Haug, Albert

2013-01-01

Theoretical Solid State Physics, Volume 1 focuses on the study of solid state physics. The volume first takes a look at the basic concepts and structures of solid state physics, including potential energies of solids, concept and classification of solids, and crystal structure. The book then explains single-electron approximation wherein the methods for calculating energy bands; electron in the field of crystal atoms; laws of motion of the electrons in solids; and electron statistics are discussed. The text describes general forms of solutions and relationships, including collective electron i

L-shell photoabsorption spectroscopy for solid metals: Ti, V, Cr, Fe, Ni, Cu

International Nuclear Information System (INIS)

Del Grande, N.K.

1989-01-01

Synchrotron radiation measurements of near-threshold and broad-range (400--1500 eV) absolute photoabsorption cross sections were made for five transition metals with ±10% overall uncertainties. Fine structure details of 2p-3d autoionizing resonances are shown with better than 1.0 eV resolution for solid metals: Ti, V, Cr, Fe, Ni, and Cu. Fine structure similar to what we measured can be produced using a multi-configuration Dirac Fock (MCDF) model if a statistical distribution is assumed for the initial atomic states. Calculations were performed in intermediate coupling with configuration interactions by Mau H. Chen. The results are compared with other experimental work and theoretical methodologies. 18 refs., 7 figs

Solid-state ring laser gyroscope

Science.gov (United States)

Schwartz, S.

The ring laser gyroscope is a rotation sensor used in most kinds of inertial navigation units. It usually consists in a ring cavity filled with a mixture of helium and neon, together with high-voltage pumping electrodes. The use of a gaseous gain medium, while resulting naturally in a stable bidirectional regime enabling rotation sensing, is however the main industrially limiting factor for the ring laser gyroscopes in terms of cost, reliability and lifetime. We study in this book the possibility of substituting for the gaseous gain medium a solid-state medium (diode-pumped Nd-YAG). For this, a theoretical and experimental overview of the lasing regimes of the solid-state ring laser is reported. We show that the bidirectional emission can be obtained thanks to a feedback loop acting on the states of polarization and inducing differential losses proportional to the difference of intensity between the counterpropagating modes. This leads to the achievement of a solid-state ring laser gyroscope, whose frequency response is modified by mode coupling effects. Several configurations, either mechanically or optically based, are then successively studied, with a view to improving the quality of this frequency response. In particular, vibration of the gain crystal along the longitudinal axis appears to be a very promising technique for reaching high inertial performances with a solid-state ring laser gyroscope. Gyrolaser à état solide. Le gyrolaser est un capteur de rotation utilisé dans la plupart des centrales de navigation inertielle. Dans sa forme usuelle, il est constitué d'une cavité laser en anneau remplie d'un mélange d'hélium et de néon pompé par des électrodes à haute tension. L'utilisation d'un milieu amplificateur gazeux, si elle permet de garantir naturellement le fonctionnement bidirectionnel stable nécessaire à la mesure des rotations, constitue en revanche la principale limitation industrielle des gyrolasers actuels en termes de coût, fiabilit

Fast neutron spectrometry based on proton detection in CR-39 detector

Energy Technology Data Exchange (ETDEWEB)

Dajko, G.; Somogyi, G.

1986-01-01

The authors have developed a home-made proton-sensitive CR-39 track detector called MA-ND/p. Using this and the n-p scattering process the performance of a fast neutron spectrometer has been studied by applying two different methods. These are based on track density determinations by using varying radiator thicknesses at constant etching time and by using varying etching times at fixed radiator thickness, respectively. For both methods studied a computer programme is made to calculate the theoretically expected neutron sensitivity as a function of neutron energy. For both methods the neutron sensitivities, expressed in terms of observable etched proton tracks per neutron, are determined experimentally for 3.3 and 14.7 MeV neutron energies. The theoretical and experimental data obtained are compared.

Fast neutron spectrometry based on proton detection in CR-39 detector

International Nuclear Information System (INIS)

Dajko, G.; Somogyi, G.

1986-01-01

The authors have developed a home-made proton-sensitive CR-39 track detector called MA-ND/p. Using this and the n-p scattering process the performance of a fast neutron spectrometer has been studied by applying two different methods. These are based on track density determinations by using varying radiator thicknesses at constant etching time and by using varying etching times at fixed radiator thickness, respectively. For both methods studied a computer programme is made to calculate the theoretically expected neutron sensitivity as a function of neutron energy. For both methods the neutron sensitivities, expressed in terms of observable etched proton tracks per neutron, are determined experimentally for 3.3 and 14.7 MeV neutron energies. The theoretical and experimental data obtained are compared. (author)

Use of Image Pro Plus for counting of {alpha} particles tracks in CR-39; Uso do Image Pro Plus para contagem de tracos de particulas {alpha} em CR-39

Energy Technology Data Exchange (ETDEWEB)

Miranda, Marcia Valeria F.E. Sa [Coordenacao dos Programas de Pos-Graduacao de Engenharia (COPPE/UFRJ), Rio de Janeiro, RJ (Brazil). Programa de Engenharia Nuclear; Centro Regional de Ciencias Nucleares (CRCN-NE/CNEN-PE), Recife, PE (Brazil); Crispim, Verginia Reis [Coordenacao dos Programas de Pos-Graduacao de Engenharia (COPPE/UFRJ), Rio de Janeiro, RJ (Brazil). Programa de Engenharia Nuclear; Gomes, Rogerio dos S.; Gomes, Joana D' Arc R. Lopes, E-mail: mvaleria@cnen.gov.b, E-mail: verginia@con.ufrj.b, E-mail: rogeriog@cnen.gov.b, E-mail: jlopes@cnen.gov.b [Comissao Nacional de Energia Nuclear (CNEN), Rio de Janeiro, RJ (Brazil)

2011-10-26

This paper measured the radon radiations present in NORM samples, through the diffusion chambers which contained a nuclear track detector (CR-39). For automatic counting of those tracks the computer program Image Pro plus was used. This paper reports the application of Image Pro plus for counting the nuclear tracks, coming from the radon radiation present in NORM samples. As the radiation rate of {sup 222}Rn if proportional to the number of these tracks, the methodology allowed to compare the levels of contamination of the analysed samples. Also, tables and graphics are presented with counting results referring to the stage of validation of Image Pro plus

Optical, structural, and chemical properties of CR-39 implanted with 5.2 MeV doubly charged carbon ions

Science.gov (United States)

Ali, Dilawar; Butt, M. Z.; Ishtiaq, Mohsin; Waqas Khaliq, M.; Bashir, Farooq

2016-11-01

Poly-allyl-diglycol-carbonate (CR-39) specimens were irradiated with 5.2 MeV doubly charged carbon ions using Pelletron accelerator. Ion dose was varied from 5 × 1013 to 5 × 1015 ions cm-2. Optical, structural, and chemical properties were investigated by UV-vis spectroscopy, x-ray diffractometer, and FTIR/Raman spectroscopy, respectively. It was found that optical absorption increases with increasing ion dose. Absorption edge shifts from UV region to visible region. The measured opacity values of pristine and ion implanted CR-39 range from 0.0519 to 4.7959 mm-1 following an exponential growth (9141%) with the increase in ion dose. The values of direct and indirect band gap energy decrease exponentially with an increase in ion dose by 59% and 71%, respectively. However, average refractive index in the visible region increases from 1.443 to 2.864 with an increase in ion dose, by 98%. A linear relation between band gap energy and crystallite size was observed. Both the number of carbon atoms in conjugation length and the number of carbon atoms per cluster increase linearly with the increase in ion dose. FTIR spectra showed that on C+2 ions irradiation, the intensity of all bands decreases gradually without appearance of any new band, indicating degradation of polymer after irradiation. Raman spectra revealed that the density of -CH2- group decreases on C+2 ions irradiation. However, the structure of CR-39 is completely destroyed on irradiation with ion dose 1 × 1015 and 5 × 1015 ions cm-2.

Solid state radiation dosimetry

International Nuclear Information System (INIS)

Moran, P.R.

1976-01-01

Important recent developments provide accurate, sensitive, and reliable radiation measurements by using solid state radiation dosimetry methods. A review of the basic phenomena, devices, practical limitations, and categories of solid state methods is presented. The primary focus is upon the general physics underlying radiation measurements with solid state devices

Luminescence and the solid state

CERN Document Server

Ropp, Richard C

2013-01-01

Since the discovery of the transistor in 1948, the study of the solid state has been burgeoning. Recently, cold fusion and the ceramic superconductor have given cause for excitement. There are two approaches possible to this area of science, namely, that of solid state physics and solid state chemistry, although both overlap extensively. The former is more concerned with electronic states in solids (including electromagnetics) whereas the latter is more concerned with interactions of atoms in solids. The area of solid state physics is well documented, however, there are very few texts which de

Solid state video cameras

CERN Document Server

Cristol, Y

2013-01-01

Solid State Video Cameras reviews the state of the art in the field of solid-state television cameras as compiled from patent literature. Organized into 10 chapters, the book begins with the basic array types of solid-state imagers and appropriate read-out circuits and methods. Documents relating to improvement of picture quality, such as spurious signal suppression, uniformity correction, or resolution enhancement, are also cited. The last part considerssolid-state color cameras.

Issues concerning the determination of solubility products of sparingly soluble crystalline solids. Solubility of HfO{sub 2}(cr)

Energy Technology Data Exchange (ETDEWEB)

Rai, Dhanpat [Rai Enviro-Chem, LLC, Yachats, OR (United States); Kitamura, Akira [Japan Atomic Energy Agency, Ibaraki (Japan); Rosso, Kevin M. [Pacific Northwest National Laboratory, Richland, WA (United States); Sasaki, Takayuki; Kobayashi, Taishi [Kyoto Univ. (Japan)

2016-11-01

Solubility studies were conducted with HfO{sub 2}(cr) solid as a function HCl and ionic strength ranging from 2.0 to 0.004 mol kg{sup -1}. These studies involved (1) using two different amounts of the solid phase, (2) acid washing the bulk solid phase, (3) preheating the solid phase to 1400 C, and (4) heating amorphous HfO{sub 2}(am) suspensions to 90 C to ascertain whether the HfO{sub 2}(am) converts to HfO{sub 2}(cr) and to determine the solubility from the oversaturation direction. Based on the results of these treatments it is concluded that the HfO{sub 2}(cr) contains a small fraction of less crystalline, but not amorphous, material [HfO{sub 2}(lcr)] and this, rather than the HfO{sub 2}(cr), is the solubility-controlling phase in the range of experimental variables investigated in this study. The solubility data are interpreted using both the Pitzer and SIT models and they provide log{sub 10} K{sup 0} values of -(59.75±0.35) and -(59.48±0.41), respectively, for the solubility product of HfO{sub 2}(lcr)[HfO{sub 2}(lcr) + 2H{sub 2}O ↔ Hf{sup 4+} + 4OH{sup -}]. The log{sub 10} of the solubility product of HfO{sub 2}(cr) is estimated to be < -63. The observation of a small fraction of less crystalline higher solubility material is consistent with the general picture that mineral surfaces are often structurally and/or compositionally imperfect leading to a higher solubility than the bulk crystalline solid. This study stresses the urgent need, during interpretation of solubility data, of taking precautions to make certain that the observed solubility behavior for sparingly-soluble solids is assigned to the proper solid phase.

Measurement of D-3He proton yield with CR-39 as a diagnostic for inertial confinement fusion experiments. Final report, 7 January 1983-30 September 1984

International Nuclear Information System (INIS)

Blue, T.E.; Wehring, B.W.

1985-04-01

The first phase of our research project has as its main goal the development of an image analysis system for Solid State Nuclear Track Detectors (SSNTD) readout. Section I, of this report is an introduction to SSNTDs and image analysis systems for automatic track counting. The development of the image analysis system is described in Section II. The development of our foil holder system is described in Section III. The performance of an image analysis system can only be judged with respect to a particular type of image which is to be analyzed. In order to insure the workability of our image analysis system in analyzing CR-39 SSNTDs, we have made an effort to improve our etching system and our etch procedure. The development of our etching system and our etch procedure is outlined in Section IV. Also included in Section IV are images of protons and alpha particle tracks for our etch procedure. The performance of our image analysis system is reported in Section V for the proton and alpha particle tracks which are reported in Section IV. Also, the performance of the image analysis system is reported for some test images

A study of CR-39 track response to charged particles from NOVA implosions

International Nuclear Information System (INIS)

Phillips, T.W.; Cable, M.D.; Hicks, D.G.; Li, C.K.; Petrasso, R.D.; Seguin, F.H.

1996-01-01

We have exposed CR-39 track recording material to a number of NOVA implosions. Radiation from the implosion passed through an array of ranging filters, which aided identification of the incident particles and their energies. The etching procedure was calibrated by including a piece of track exposed to DD protons from a small accelerator. For the same shots, we quantitatively compare the DD neutron yield with the DD proton yield determined from the track. In DT implosions, tracks produced by neutron interactions prevent observation of charged-particle tracks that are produced by the processes of knock-on, secondary or tertiary fusion

Study of the influence of the soil and plant natures and pollution on the radon and thoron alpha activities inside various herbal infusions by using solid state nuclear track detectors

International Nuclear Information System (INIS)

Misdaq, M.A.; Ait nouh, F.; Bourzik, W.; Lamine, J.

2000-01-01

Different medicinal plant, spinach and cereal samples have been analysed by using neutron activation analysis and radiochemical separation. The solid state nuclear track detectors technique was utilized for uranium and thorium contents determination as well as for alpha, beta, and gamma dose rates evaluation in various geological and ceramic samples. In this study, uranium and thorium contents have been determined in different plant samples, soils in which they have been grown and in herbal infusions made by boiling the studied plants in potable water by using CR-39 and LR-115 solid state nuclear track detectors. Radon and thoron alpha activities per unit volume inside the plants, soils and herbal infusions studied have been evaluated. The radon transfers between soils and plants as well as between plants and herbal infusions have been investigated. The influence of pollution due to different material dusts on radon and thoron alpha activities inside the plants and their corresponding infusions has been studied. (author)

Autoradiographic measurement of low concentrations of alpha-active nuclides using CR-39 track detectors

International Nuclear Information System (INIS)

Freyer, K.; Dietze, K.; Weisse, S.; Kummer, G.

1991-01-01

An autoradiographic method for the determination of alpha emission rates from plastic packaging materials for VLSI silicon memory devices based on long-time exposure of the samples on CR-39 detectors has been tested. The lower limit of detection will be strongly influenced by the background of the detector material and amounts at times to 0.002 alpha particles cm -2 h -1 after 200 days exposure. A mathematical method for the interpretation of very low track densities is discussed. The first results of its application are presented. (author)

Search for α + core states in even-even Cr isotopes

Energy Technology Data Exchange (ETDEWEB)

Souza, M.A. [Universidade de Sao Paulo, Instituto de Fisica, Sao Paulo, SP (Brazil); Instituto Federal de Educacao, Ciencia e Tecnologia de Sao Paulo, Departamento de Mecanica, Sao Paulo, SP (Brazil); Miyake, H. [Universidade de Sao Paulo, Instituto de Fisica, Sao Paulo, SP (Brazil)

2017-07-15

The α + core structure is investigated in even-even Cr isotopes from the viewpoint of the local potential model. The comparison of Q{sub α}/A values for even-even Cr isotopes and even-even A = 46, 54, 56, 58 isobars indicates that {sup 46}Cr and {sup 54}Cr are the most favorable even-even Cr isotopes for the α + core configuration. The ground state bands of the two Cr isotopes are calculated through a local α + core potential containing a nuclear term with (1 + Gaussian) x (W.S. + W.S.{sup 3}) shape. The calculated spectra give a very good description of most experimental {sup 46}Cr and {sup 54}Cr levels, including the 0{sup +} bandheads. The reduced α-widths, rms intercluster separations and B(E2) transition rates are determined for the ground state bands. The calculations reproduce the order of magnitude of the available experimental B(E2) values without using effective charges, indicate that the low-spin members of the ground state bands present a stronger α-cluster character, and point out that the {sup 46}Cr ground state band has a significant degree of α-clustering in comparison with {sup 44}Ti. The volume integral per nucleon pair and rms radius obtained for the α + {sup 50}Ti potential are consistent with those reported previously in the analysis of α elastic scattering on {sup 50}Ti. (orig.)

Response of LR-115 type II and CR-39 plastic track detectors to Am-Be and 14.1-MeV neutrons

International Nuclear Information System (INIS)

Bradley, D.A.; Chong, C.S.; Saat, Ahmat; Sidik, A.G.; Ghose, A.M.

1987-01-01

The fast-neutron response of the plastic LR-115 type II and CR-39 track detectors have been compared, using a 14.1-MeV neutron generator and a radionuclide Am-Be neutron source (effective primary neutron energy 4.5-MeV). The distribution of track diameters for a range of etching times has been evaluated, taking into account track registration efficiency and the relevant fast neutron scattering cross-sections. The efficiency of etched-track formation in LR-115 type II due to neutron irradiation is approximately double that in CR-39. The 14.1-MeV neutrons also tend to produce tracks in both materials with somewhat greater efficiency than do the lower energy neutrons from the radionuclide source, for a given etching time. (author)

Magnetic solid-phase extraction combined with graphite furnace atomic absorption spectrometry for speciation of Cr(III) and Cr(VI) in environmental waters.

Science.gov (United States)

Jiang, Hong-mei; Yang, Ting; Wang, Yan-hong; Lian, Hong-zhen; Hu, Xin

2013-11-15

A new approach of magnetic solid phase extraction (MSPE) coupled with graphite furnace atomic absorption spectrometry (GFAAS) has been developed for the speciation of Cr(III) and Cr(VI) using zincon-immobilized silica-coated magnetic Fe3O4 nanoparticles (Zincon-Si-MNPs) as the MSPE absorbent. Cr(III) was quantitatively reserved on the absorbent at pH 9.1 while total Cr was reserved at pH 6.5. The absorbed Cr species were eluted by using 2 mol/L HCl and detected by GFAAS. The concentration of Cr(VI) could be calculated by subtracting Cr(III) from total Cr. All the parameters affecting the separation and extraction efficiency of Cr species such as pH, extraction time, concentration and volume of eluent, sample volume and influence of co-existing ions were systematically examined and the optimized conditions were established accordingly. The detection limit (LOD) of the method was 0.016 and 0.011 ng mL(-1) for Cr(III) and Cr(VI), respectively, with the enrichment factor of 100 and 150. The precisions of this method (Relative standard deviation, RSD, n=7) for Cr(III) and Cr(VI) at 0.1 ng mL(-1) were 6.0% and 6.2%, respectively. In order to validate the proposed method, a certified reference material of environmental water was analyzed, and the result of Cr speciation was in good agreement with the certified value. This MSPE-GFAAS method has been successfully applied for the speciation of Cr(III) and Cr(VI) in lake and tap waters with the recoveries of 88-109% for the spiked samples. Moreover, the MSPE separation mechanism of Cr(III) and Cr(VI) based on their adsorption-desorption on Zincon-Si-MNPs has been explained through various spectroscopic characterization. © 2013 Elsevier B.V. All rights reserved.

Solid state nuclear track detectors in the measurement of alpha to fission branching ratios of heavy actinides

International Nuclear Information System (INIS)

Pandey, A.K.; Sharma, R.C.; Padalkar, S.K.; Kalsi, P.C.; Iyer, R.H.

1992-01-01

A sequential etching procedure for revelation of alpha and fission tracks in CR-39 was developed and optimized. Using this technique alpha and fission tracks can be differentiated unambiguously because of significant differences in their sizes and etching times. This registration and revelation procedure for alpha and fission tracks may be used for the studies of half lives, alpha to fission branching ratios and identification of radionuclides based on their decay schemes. It has the added advantage that both alpha decay and fission events can be studied using one detector and hence uncertainties related to efficiency, registration geometry, registration times, amount of radionuclides etc can be eliminated or minimized. The effects of neutron, gamma and alpha radiations on the alpha and fission fragment tracks registration and revelation properties of CR-39 detectors [CR-39, CR-39 (DOP)] were also studied. The IR spectra were also studied to find out the nature of chemical changes produced by these radiations on CR-39. (author). 32 refs., 7 figs., 4 tabs

Measurement of concentrations of radon and its daughters in indoor atmosphere using CR-39 nuclear track detector

International Nuclear Information System (INIS)

Farid, S.M.

1993-01-01

This paper presents the results of the measurements of indoor 222 Rn and daughter levels in houses of different types located in different parts of Bangladesh. The passive time-integrated method of using a solid state nuclear track detector (CR-39) was employed for measuring both the 222 Rn gas concentration as well as the potential alpha energy exposure (PAEE) level from the short lived daughters of 222 Rn. The 222 Rn concentration from cup exposure and the PAEE from the bare exposure were obtained directly from the track density using calibration curves. A total of 275 exposures were made in the bare mode in 15 locations and 71 exposures in the cup mode in 6 locations. The geometric mean PAEE level obtained is 9.5 mWL with a geometric standard deviation of 1.9. The corresponding value for 222 Rn concentration are 61.3 Bq.M -3 and 2.4. The total data was collected over a period of one and a half year. The monthly variation of the geometric mean of PAEE is also shown. The annual effective dose equivalent has been estimated for each location by using the conversion factor of 9 mWv per WLM as obtained from ICRP-50. The average PAEE level obtained from the total data is below the intervention level as suggested by US EPA. However, the individual averages for each location show that in 8 out of 15 locations intervention may be considered and in others not intervention is called for. The 222 Rn concentrations at the seven locations are equal or less than the equilibrium equivalent 222 Rn concentration value as suggested by EPA. Attempts have also been made to see the variation in the PAEE levels according to different type of construction material used for the houses. (Author)

Thermodynamic modeling of La2O3-SrO-Mn2O3-Cr2O3 for solid oxide fuel cell applications

DEFF Research Database (Denmark)

Povoden-Karadeniz, E.; Chen, Ming; Ivas, Toni

2012-01-01

The thermodynamic La–Sr–Mn–Cr–O oxide database is obtained as an extension of thermodynamic descriptions of oxide subsystems using the calculation of phase diagrams approach. Concepts of the thermodynamic modeling of solid oxide phases are discussed. Gibbs energy functions of SrCrO4, Sr2.67Cr2O8......, Sr2CrO4, and SrCr2O4 are presented, and thermodynamic model parameters of La–Sr–Mn–Chromite perovskite are given. Experimental solid solubilities and nonstoichiometries in La1xSrxCrO3d and LaMn1xCrxO3d are reproduced by the model. The presented oxide database can be used for applied computational...... thermodynamics of traditional lanthanum manganite cathode with Cr-impurities. It represents the fundament for extensions to higher orders, aiming on thermodynamic calculations in noble symmetric solid oxide fuel cells...

Solid-state laser engineering

CERN Document Server

Koechner, Walter

1999-01-01

Solid-State Laser Engineering, written from an industrial perspective, discusses in detail the characteristics, design, construction, and performance of solid-state lasers. Emphasis is placed on engineering and practical considerations; phenomenological aspects using models are preferred to abstract mathematical derivations. This new edition has extensively been updated to account for recent developments in the areas of diode-laser pumping, laser materials, and nonlinear crystals. Walter Koechner received a doctorate in Electrical Engineering from the University of Technology in Vienna, Austria, in 1965. He has published numerous papers in the fields of solid-state physics, optics, and lasers. Dr. Koechner is founder and president of Fibertek, Inc., a research firm specializing in the design, development, and production of advanced solid-state lasers, optical radars, and remote-sensing systems.

The influence of the soil and plant natures and pollution on the radon and thoron alpha-activities inside various herbal infusions by using solid state nuclear track detectors

International Nuclear Information System (INIS)

Misdaq, M.A.; Nouh, F.A.; Bourzik, W.

2001-01-01

Uranium and thorium contents were determined in samples of various plants in the soils in which the plants were grown, and in herbal infusions made by boiling the plants in potable water, using CR-39 and LR-115 solid state nuclear track detectors. In addition, radon and thoron alpha-activities per unit volume inside the plants, soils and herbal infusions were measured. These measurements were completed by an investigation of the radon transfer between soils and plants and that between plants and herbal infusions, and also by the investigation of the influence of pollution due to different material dusts on the radon and thoron alpha activities inside the plants and their infusions. (author)

Cr 3d surface and bulk states in Sn1-xCrxTe/Cr crystals

International Nuclear Information System (INIS)

Guziewicz, E.; Szamota-Sadowska, K.; Kowalski, B.J.; Grodzicka, E.; Story, T.; Orlowski, B.A.; Johnson, R.L.

1997-01-01

We report a new approach to investigate metal-semiconductor interface formation. Photoemission spectroscopy was applied in order to investigate the clean surface of a Sn 0.97 Cr 0.03 Te crystal and to observe its changes under sequential deposition of small amounts of Cr atoms. In order to analyse the Cr 3d contribution to the valence band, the Fano-type resonance tuned to the Cr 3p-3d transmission was used. The experiment was designed to follow the Sn 0.97 Cr 0.03 Te/Cr interface formation process. At the clean Sn 0.97 Cr 0.03 Te surface, the Cr 3d states contribution to the valence band was found to be positioned 0.8 eV below Fermi level. After the Cr deposition processes the contribution shifted to a higher binding energy and another contribution 5.8 eV below the Fermi level also observed. (author)

Ratio dependence of the visible light photocatalytic efficiency for Zn{sub 2}Ti{sub 0.9}Cr{sub y}Fe{sub [0.1-y]}O{sub 4}: Cr/Fe (0.02 < y < 0.08) photocatalyst synthesized by using a solid state reaction method

Energy Technology Data Exchange (ETDEWEB)

Borse, P. H. [International Advanced Research Center for Powder Metallurgy and New Materials, Hyderabad (India); Cho, C. R. [Pusan National University, Miryang (Korea, Republic of); Lim, K. T. [Pukyong National University, Busan (Korea, Republic of); Lee, Y. J.; Bae, J. S.; Jeong, E. D.; Kim, H. G. [Korea Basic Science Institute, Busan (Korea, Republic of)

2011-07-15

We synthesized four different photocatalyst systems of Zn{sub 2}TiO{sub 4}, Zn{sub 2}Ti{sub 1-x}Fe{sub x}O{sub 4}, Zn{sub 2}Ti{sub 1-x}Cr{sub x}O{sub 4} (0 {<=} x < 0.8) and Zn{sub 2}Ti{sub 0.9}Cr{sub y}Fe{sub [0.1]-y}O{sub 4} (0.02 < y < 0.08) by using a solid state reaction method. For the first time, the UV-active photocatalyst Zn{sub 2}TiO{sub 4} was converted to a visible light active material by controlled doping/co-doping with Cr and Fe metal-ions at Ti substitutional sites, and investigated the structural, optical and photocatalytic water decomposition properties of that materials. The co-doping induces strong absorption bands (at {lambda} {approx} 480 nm and {lambda} {approx} 620 nm) within the Zn{sub 2}TiO{sub 4} band gap. The optimum system of Zn{sub 2}Ti{sub 0.9}Cr{sub 0.05}Fe{sub 0.05}O{sub 4} yielded maximum H{sub 2} generation. In contrast to the visible light inactivity of Fe- and Cr-doped Zn{sub 2}TiO{sub 4}, the H{sub 2} production from co-doped samples under visible light irradiation increased till the optimum 'y' value. Consequently, here exists an optimal co-dopant concentration for efficient photocatalytic hydrogen production under visible light ({lambda} {>=} 420 nm).

KAJIAN ADSORPSI ION LOGAM Cr(VI OLEH ADSORBEN KOMBINASI ARANG AKTIF SEKAM PADI DAN ZEOLIT MENGGUNAKAN METODE SOLID-PHASE SPECTROPHOTOMETRY (SPS

Directory of Open Access Journals (Sweden)

Sulistyo Saputro

2016-10-01

  This study aims to study the use of activated rice husk charcoal and zeolite as combination adsorbents to adsorb Cr(VI metal ions; the effect of the combination adsorbents of activated rice husk charcoal and zeolite’s compositions to adsorb Cr(VI metal ions; and the sensitivity of solid-phase spectrophotometry (SPS as a method to determine the reduced levels of Cr(VI metal ions in the level of 15μ"> g/L. The activated rice husk charcoal used were obtained through the activation process by soaking in a solution of ZnCl2 10% while the zeolite with a solution of H2SO4 10%. The contacting process of the adsorbents with Cr(VI metal ions was done by varying the compositions of the activated rice husk charcoal and zeolite adsorbent, 1:1, 1:2, 1:3, and 2:1. The data analysis of the Cr(VI level used solid-phase spectrophotometry (SPS method. Characterization of activated rice husk charcoal and zeolite used FTIR. The results showed that: (1 a combination of activated rice husk charcoal and zeolite can be used as adsorbent to adsorb Cr(VI metal ions with the adsorption capacity was 0,28 15μ"> g/g; (2 the optimum composition of adsorbents was 1:2 with the percentage of absorption was 40,99%; (3 solid-phase spectrophotometry (SPS is a sensitive method to determine the reduced levels of Cr(VI in the level of 15μ"> g/L with the limit of detection (LOD was 0,021 15μ"> g/L.   Keywords: adsorption, Cr(VI,  activated  rice husk charcoal,  zeolite, solid-phase spectrophotometry

Solid State Ionic Materials - Proceedings of the 4th Asian Conference on Solid State Ionics

Science.gov (United States)

Chowdari, B. V. R.; Yahaya, M.; Talib, I. A.; Salleh, M. M.

1994-07-01

The Table of Contents for the full book PDF is as follows: * Preface * I. INVITED PAPERS * Diffusion of Cations and Anions in Solid Electrolytes * Silver Ion Conductors in the Crystalline State * NMR Studies of Superionic Conductors * Hall Effect and Thermoelectric Power in High Tc Hg-Ba-Ca-Cu-O Ceramics * Solid Electrolyte Materials Prepared by Sol-Gel Chemistry * Preparation of Proton-Conducting Gel Films and their Application to Electrochromic Devices * Thin Film Fuel Cells * Zirconia based Solid Oxide Ion Conductors in Solid Oxide Fuel Cells * The Influence of Anion Substitution on Some Phosphate-based Ion Conducting Glasses * Lithium Intercalation in Carbon Electrodes and its Relevance in Rocking Chair Batteries * Chemical Sensors using Proton Conducting Ceramics * NMR/NQR Studies of Y-Ba-Cu-O Superconductors * Silver Molybdate Glasses and Battery Systems * New Highly Conducting Polymer Ionics and their Application in Electrochemical Devices * Study of Li Electrokinetics on Oligomeric Electrolytes using Microelectrodes * Calculation of Conductivity for Mixed-Phase Electrolytes PEO-MX-Immiscible Additive by Means of Effective Medium Theory * II. CONTRIBUTED PAPERS * Phase Relationship and Electrical Conductivity of Sr-V-O System with Vanadium Suboxide * Amorphous Li+ Ionic Conductors in Li2SO4-Li2O-P2O5 System * Fast Ion Transport in KCl-Al2O3 Composites * The Effect of the Second Phase Precipitation on the Ionic Conductivity of Zr0.85Mg0.15O1.85 * Conductivity Measurements and Phase Relationships in CaCl2-CaHCl Solid Electrolyte * Relationships Between Crystal Structure and Sodium Ion Conductivity in Na7Fe4(AsO4)6 and Na3Al2(AsO4)3 * Electrical Conductivity and Solubility Limit of Ti4+ Ion in Na1+x TiyZr2-ySixP3-xO12 System * Study on Sodium Fast Ion Conductors of Na1+3xAlxTi2-xSi2xP3-2xO12 System * Influences of Zirconia on the Properties of β''-Alumina Ceramics * Decay of Luminescence from Cr3+ Ions in β-Alumina * Lithium Ion Conductivity in the Li4XO4-Li2

Understanding solid state physics

CERN Document Server

Holgate, Sharon Ann

2009-01-01

Where Sharon Ann Holgate has succeeded in this book is in packing it with examples of the application of solid state physics to technology. … All the basic elements of solid state physics are covered … . The range of materials is good, including as it does polymers and glasses as well as crystalline solids. In general, the style makes for easy reading. … Overall this book succeeds in showing the relevance of solid state physics to the modern world … .-Contemporary Physics, Vol. 52, No. 2, 2011I was indeed amused and inspired by the wonderful images throughout the book, carefully selected by th

A study of CR-39 plastic charged-particle detector replacement by consumer imaging sensors

Energy Technology Data Exchange (ETDEWEB)

Plaud-Ramos, K. O.; Freeman, M. S.; Wei, W.; Guardincerri, E.; Bacon, J. D.; Cowan, J.; Durham, J. M.; Huang, D.; Gao, J.; Hoffbauer, M. A.; Morley, D. J.; Morris, C. L.; Poulson, D. C.; Wang, Zhehui, E-mail: zwang@lanl.gov [Los Alamos National Laboratory, Los Alamos, New Mexico 87545 (United States)

2016-11-15

Consumer imaging sensors (CIS) are examined for real-time charged-particle detection and CR-39 plastic detector replacement. Removing cover glass from CIS is hard if not impossible, in particular for the latest inexpensive webcam models. We show that $10-class CIS are sensitive to MeV and higher energy protons and α-particles by using a {sup 90}Sr β-source with its cover glass in place. Indirect, real-time, high-resolution detection is also feasible when combining CIS with a ZnS:Ag phosphor screen and optics. Noise reduction in CIS is nevertheless important for the indirect approach.

Solid-state laser engineering

CERN Document Server

Koechner, Walter

1996-01-01

Solid-State Laser Engineering, written from an industrial perspective, discusses in detail the characteristics, design, construction, and performance of solid-state lasers. Emphasis is placed on engineering and practical considerations; phenomenological aspects using models are preferred to abstract mathematical derivations. This new edition has extensively been updated to account for recent developments in the areas of diode-laser pumping, mode locking, ultrashort-pulse generation etc. Walter Koechner received a doctorate in Electrical Engineering from the University of Technology in Vienna, Austria, in 1965. He has published numerous papers in the fields of solid-state physics, optics, and lasers. Dr. Koechner is founder and president of Fibertek, Inc., a research firm specializing in the design, development, and production of advanced solid-state lasers, optical radars, and remote-sensing systems.

Registration properties of different types of CR-39 in vacuum conditions of irradiation

International Nuclear Information System (INIS)

Golovchenko, A.N.; Tret'yakova, S.P.

1991-01-01

Sensitivity change has been studied of different types of CR-39 detectors (Pershore, Tastrak, Intercast, Ma-ND/α) in dependence on holding time of detector in vacuum chamber at the residual pressure P ≅ 2x10 -2 and ≅ 5x10 -3 Pa before their irradiation with alpha particles from thin 238 Pu source and accelerated charged ions with atomic number Z=2-10 and energy of 9.1 MeV/nucleon. Polymer of Intercast Company turned out to be the most stable one to vacuum effect, and detector does not change the sensitivity up to response function REL 200 ≅ 1 MeVxcm 2 xmg -1 in the mentioned experiment conditions. 7 refs.; 3 figs

Solid state chemistry an introduction

CERN Document Server

Smart, Lesley E

2012-01-01

""Smart and Moore are engaging writers, providing clear explanations for concepts in solid-state chemistry from the atomic/molecular perspective. The fourth edition is a welcome addition to my bookshelves. … What I like most about Solid State Chemistry is that it gives simple clear descriptions for a large number of interesting materials and correspondingly clear explanations of their applications. Solid State Chemistry could be used for a solid state textbook at the third or fourth year undergraduate level, especially for chemistry programs. It is also a useful resource for beginning graduate

Measurement of the variable track-etch rate of hydrogen, carbon and oxygen Ions in CR-39

International Nuclear Information System (INIS)

Lengar, I.; Skvarc, J.; Ilic, R.

2003-01-01

The ratio of the track-etch rate to the bulk-etch rate for hydrogen, carbon and oxygen ions was studied for the CR-39 detector with addition of dioctylphthalate. The response was reconstructed from etch-pit growth curves obtained by the multi-step etching technique. A theoretical analysis of the correctness of the method due to the 'missing track segment' is assessed and utilisation of the results obtained for the calibration of fast neutron dosimetry is discussed. (author)

Synthesis of (Cr,V){sub 2}(C,N) solid solution powders by thermal processing precursors

Energy Technology Data Exchange (ETDEWEB)

Liu, Anrui [School of Materials Science & Engineering, Sichuan University, Chengdu, 610065 (China); Liu, Ying [School of Materials Science & Engineering, Sichuan University, Chengdu, 610065 (China); Key Laboratory of Advanced Special Material & Technology, Ministry of Education, Chengdu, 610065 (China); Ma, Shiqing; Qiu, Yuchong; Rong, Pengcheng; Ye, Jinwen [School of Materials Science & Engineering, Sichuan University, Chengdu, 610065 (China)

2017-06-01

The single-phase (Cr,V){sub 2}(C,N) solid solution powders were fabricated via carbothermal reduction-nitridation (CRN) processing technique. The effects of heat treatment temperature, nitrogen pressure and carbon proportion were experimentally studied in detail by X-ray Diffraction (XRD), Scanning Electron Microscope (SEM), Transmission Electron Microscope (TEM) and thermal analysis. The chemical transformations of vanadium and chromium compounds were as follows: precursors → V{sub 2}O{sub 3}, Cr{sub 2}O{sub 3} → Cr{sub 3}C{sub 2}, Cr{sub 2}O{sub 3}, (Cr,V){sub 2}(C,N) → (Cr,V){sub 2}(C,N). When the heat-treated temperature was below 1200 °C, chromium oxides didn’t completely react. However, higher temperature ∼1300 °C could not only lead to the segregation of some nitrides and carbon black, but also to the occurrence of fiber-bridged particles. The system nitrogen pressure over 0.03 MPa would cause a subtle transformation of (Cr,V){sub 2}(C,N) to VCrN{sub 2}. When the carbon proportion was below 15 wt%, the oxides could not be completely reduced, while when the carbon proportion was above 15.5 wt%, some undesired carbides, like Cr{sub 23}C{sub 6} and Cr{sub 3}C{sub 2}, would form. Ultimately, the homogeneously distributed pure-phase (Cr,V){sub 2}(C,N) spherical particles with the average size of ∼1.5 μm were obtained at the optimal conditions of the treatment of precursors at 1200 °C for 1 h with the nitrogen pressure of 0.03 MPa and carbon content of 15.5 wt%. The chemical composition of the solid solution with the optimal process could be drawn as (Cr{sub 0.85}V{sub 0.15}){sub 2}(C{sub 0.57}N{sub 0.43}). Thermal processing precursors method shows the advantages of lower synthesis temperature, shorter period and finer particles when comparing with the conventional preparations. - Highlights: • Single phase of (Cr,V){sub 2}(C,N) powders were synthesized for the first time. • Precursors were used to prepared the powders by carbothermal

The solid state maser

CERN Document Server

Orton, J W; Walling, J C; Ter Haar, D

1970-01-01

The Solid State Maser presents readings related to solid state maser amplifier from the first tentative theoretical proposals that appeared in the early 1950s to the successful realization of practical devices and their application to satellite communications and radio astronomy almost exactly 10 years later. The book discusses a historical account of the early developments (including that of the ammonia maser) of solid state maser; the properties of paramagnetic ions in crystals; the development of practical low noise amplifiers; and the characteristics of maser devices designed for communica

A performance test of a new high-surface-quality and high-sensitivity CR-39 plastic nuclear track detector – TechnoTrak

Energy Technology Data Exchange (ETDEWEB)

Kodaira, S., E-mail: kodaira.satoshi@qst.go.jp [Radiation Measurement Research Team, National Institute of Radiological Sciences, National Institutes for Quantum and Radiological Science and Technology, Chiba (Japan); Morishige, K. [Research Institute for Science and Engineering, Waseda University, Tokyo (Japan); Kawashima, H.; Kitamura, H.; Kurano, M. [Radiation Measurement Research Team, National Institute of Radiological Sciences, National Institutes for Quantum and Radiological Science and Technology, Chiba (Japan); Hasebe, N. [Research Institute for Science and Engineering, Waseda University, Tokyo (Japan); Koguchi, Y.; Shinozaki, W. [Oarai Research Center, Chiyoda Technol Corporation, Ibaraki (Japan); Ogura, K. [College of Industrial Technology, Nihon University, Chiba (Japan)

2016-09-15

We have studied the performance of a newly-commercialized CR-39 plastic nuclear track detector (PNTD), “TechnoTrak”, in energetic heavy ion measurements. The advantages of TechnoTrak are derived from its use of a purified CR-39 monomer to improve surface quality combined with an antioxidant to improve sensitivity to low-linear-energy-transfer (LET) particles. We irradiated these detectors with various heavy ions (from protons to krypton) with various energies (30–500 MeV/u) at the heavy ion accelerator facilities in the National Institute of Radiological Sciences (NIRS). The surface roughness after chemical etching was improved to be 59% of that of the conventional high-sensitivity CR-39 detector (HARZLAS/TD-1). The detectable dynamic range of LET was found to be 3.5–600 keV/μm. The LET and charge resolutions for three ions tested ranged from 5.1% to 1.5% and 0.14 to 0.22 c.u. (charge unit), respectively, in the LET range of 17–230 keV/μm, which represents an improvement over conventional products (HARZLAS/TD-1 and BARYOTRAK). A correction factor for the angular dependence was determined for correcting the LET spectrum in an isotropic radiation field. We have demonstrated the potential of TechnoTrak, with its two key features of high surface quality and high sensitivity to low-LET particles, to improve automatic analysis protocols in radiation dosimetry and various other radiological applications.

Etching characteristics of a CR-39 track detector at room temperature in different etching solutions

International Nuclear Information System (INIS)

Dajko, G.

1991-01-01

Investigations were carried out to discover how the etching characteristics of CR-39 detectors change with varying conditions of the etching process. Measurements were made at room temperature in pure NaOH and KOH solutions; in different alcoholic KOH solutions (PEW solution, i.e. potassium hydroxide, ethyl alcohol, water); and in NaOH and KOH solutions containing different additives. The bulk etching rate of the detector (V B ) and the V (= V T /V B ) function, i.e. track to bulk etch rates ratio, for 6.1 MeV α-particles, were measured systematically. (author)

Solid state chemistry and its applications

CERN Document Server

West, Anthony R

2013-01-01

Solid State Chemistry and its Applications, 2nd Edition: Student Edition is an extensive update and sequel to the bestselling textbook Basic Solid State Chemistry, the classic text for undergraduate teaching in solid state chemistry worldwide. Solid state chemistry lies at the heart of many significant scientific advances from recent decades, including the discovery of high-temperature superconductors, new forms of carbon and countless other developments in the synthesis, characterisation and applications of inorganic materials. Looking forward, solid state chemistry will be crucial for the

Experimental and Monte Carlo simulation studies of open cylindrical radon monitoring device using CR-39 detector

Energy Technology Data Exchange (ETDEWEB)

Rehman, Fazal-ur- E-mail: fazalr@kfupm.edu.sa; Jamil, K.; Zakaullah, M.; Abu-Jarad, F.; Mujahid, S.A

2003-07-01

There are several methods of measuring radon concentrations but nuclear track detector cylindrical dosimeters are widely employed. In this investigation, the consequence of effective volumes of the dosimeters on the registration of alpha tracks in a CR-39 detector was studied. In a series of experiments an optimum radius for a CR-39-based open cylindrical radon dosimeter was found to be about 3 cm. Monte Carlo simulation techniques hav been employed to verify the experimental results. In this context, a computer code Monte Carlo simulation dosimetry (MOCSID) was developed. Monte Carlo simulation experiments gave the optimum radius of the dosimeters as 3.0 cm. The experimental results are in good agreement with those obtained by Monte Carlo design calculations. In addition to this, plate-out effects of radon progeny were also studied. It was observed that the contribution of radon progeny ({sup 218}Po and {sup 214}Po) plated-out on the wall of the dosimeters increases with an increase of dosimeter radii and then decrease to 0 at a radius of about 3 cm if a point detector has been installed at the center of the dosimeter base. In the code MOCSID different types of random number generators were employed. The results of this research are very useful for designing an optimum size of radon dosimeters.

Experimental and Monte Carlo simulation studies of open cylindrical radon monitoring device using CR-39 detector

International Nuclear Information System (INIS)

Rehman, Fazal-ur-; Jamil, K.; Zakaullah, M.; Abu-Jarad, F.; Mujahid, S.A.

2003-01-01

There are several methods of measuring radon concentrations but nuclear track detector cylindrical dosimeters are widely employed. In this investigation, the consequence of effective volumes of the dosimeters on the registration of alpha tracks in a CR-39 detector was studied. In a series of experiments an optimum radius for a CR-39-based open cylindrical radon dosimeter was found to be about 3 cm. Monte Carlo simulation techniques hav been employed to verify the experimental results. In this context, a computer code Monte Carlo simulation dosimetry (MOCSID) was developed. Monte Carlo simulation experiments gave the optimum radius of the dosimeters as 3.0 cm. The experimental results are in good agreement with those obtained by Monte Carlo design calculations. In addition to this, plate-out effects of radon progeny were also studied. It was observed that the contribution of radon progeny ( 218 Po and 214 Po) plated-out on the wall of the dosimeters increases with an increase of dosimeter radii and then decrease to 0 at a radius of about 3 cm if a point detector has been installed at the center of the dosimeter base. In the code MOCSID different types of random number generators were employed. The results of this research are very useful for designing an optimum size of radon dosimeters

Efficiency and threshold pump intensity of CW solar-pumped solid-state lasers

Science.gov (United States)

Hwang, In H.; Lee, Ja H.

1991-01-01

The authors consider the relation between the threshold pumping intensity, the material properties, the resonator parameters, and the ultimate slope efficiencies of various solid-state laser materials for solar pumping. They clarify the relation between the threshold pump intensity and the material parameters and the relation between the ultimate slope efficiency and the laser resonator parameters such that a design criterion for the solar-pumped solid-state laser can be established. Among the laser materials evaluated, alexandrite has the highest slope efficiency of about 12.6 percent; however, it does not seem to be practical for a solar-pumped laser application because of its high threshold pump intensity. Cr:Nd:GSGG is the most promising for solar-pumped lasing. Its threshold pump intensity is about 100 air-mass-zero (AM0) solar constants and its slope efficiency is about 12 percent when thermal deformation is completely prevented.

Crystallochemical features of solid solutions based on Ga/sub 2/3/Cr/sub 2/S/sub 4/

Energy Technology Data Exchange (ETDEWEB)

Titov, V.V.; Kesler, Ya.A.; Gordeev, I.V.; Stupnikov, V.A.

1988-04-01

Ga/sub 2/3/Cr/sub 2/S/sub 4/ shows a rare type of phase transition where increases in temperature and pressure produce the disordered modification. A source of disordering can be isomorphous substitution in the tetrahedral sublattice. The authors therefore made and examined solid solutions of Ga/sub (2/3-2x/3)/M/sub x/(Cr/sub 2/)S/sub 4/ type, where M = Fe, Co, Ni, Cu. Specimens containing Fe and show a quasi-continuous solid-solution series, where the Fe system obeys Vegard's rule. Specimens containing nickel show a narrow ordering range. The most interesting results have been obtained for specimens containing copper. Cu/sub x/Ga/sub 2/3(1-x)/Cr/sub 2/S/sub 4/ specimens show a transition from a structure ordered on the tetrahedral positions, symmetry F/anti/43m, to the normal-spinel structure, Fd3m.

Use of Image Pro Plus for counting of α particles tracks in CR-39

International Nuclear Information System (INIS)

Miranda, Marcia Valeria F.E. Sa; Crispim, Verginia Reis

2011-01-01

This paper measured the radon radiations present in NORM samples, through the diffusion chambers which contained a nuclear track detector (CR-39). For automatic counting of those tracks the computer program Image Pro plus was used. This paper reports the application of Image Pro plus for counting the nuclear tracks, coming from the radon radiation present in NORM samples. As the radiation rate of 222 Rn if proportional to the number of these tracks, the methodology allowed to compare the levels of contamination of the analysed samples. Also, tables and graphics are presented with counting results referring to the stage of validation of Image Pro plus

Cr{sub 2}O{sub 5} as new cathode for rechargeable sodium ion batteries

Energy Technology Data Exchange (ETDEWEB)

Feng, Xu-Yong; Chien, Po-Hsiu; Rose, Alyssa M.; Zheng, Jin [Department of Chemistry and Biochemistry, Florida State University, Tallahassee, FL 32306 (United States); Hung, Ivan; Gan, Zhehong [Centre of Interdisciplinary Magnetic Resonance, National High Magnetic Field Laboratory, 1800 East Paul Dirac Drive, Tallahassee, FL 32310 (United States); Hu, Yan-Yan, E-mail: hu@chem.fsu.edu [Department of Chemistry and Biochemistry, Florida State University, Tallahassee, FL 32306 (United States); Centre of Interdisciplinary Magnetic Resonance, National High Magnetic Field Laboratory, 1800 East Paul Dirac Drive, Tallahassee, FL 32310 (United States)

2016-10-15

Chromium oxide, Cr{sub 2}O{sub 5}, was synthesized by pyrolyzing CrO{sub 3} at 350 °C and employed as a new cathode in rechargeable sodium ion batteries. Cr{sub 2}O{sub 5}/Na rechargeable batteries delivered high specific capacities up to 310 mAh/g at a current density of C/16 (or 20 mA/g). High-resolution solid-state {sup 23}Na NMR both qualitatively and quantitatively revealed the reversible intercalation of Na ions into the bulk electrode and participation of Na ions in the formation of the solid-electrolyte interphase largely at low potentials. Amorphization of the electrode structure occurred during the first discharge revealed by both NMR and X-ray diffraction data. CrO{sub 3}-catalyzed electrolyte degradation and loss in electronic conductivity led to gradual capacity fading. The specific capacity stabilized at >120 mAh/g after 50 charge-discharge cycles. Further improvement in electrochemical performance is possible via electrode surface modification, polymer binder incorporation, or designs of new morphologies. - Graphical abstract: Electrochemical profile of a Cr{sub 2}O{sub 5}/Na battery cell and high-resolution solid-state {sup 23}Na MAS NMR spectrum of a Cr{sub 2}O{sub 5} electrode discharged to 2 V. - Highlights: • Cr{sub 2}O{sub 5} was synthesized and used as a new cathode in rechargeable Na ion batteries. • A high capacity of 310 mAh/g and an energy density of 564 Wh/kg were achieved. • High-resolution solid-state {sup 23}Na NMR was employed to follow the reaction mechanisms.

Practical consequences for the use of a personal dosimeter for fast neutrons based on CR39 exposed up to one year

International Nuclear Information System (INIS)

Boschung, Markus; Fiechtner, Annette; Mayer, Sabine; Wernli, Christian

2008-01-01

Full text: At the Paul Scherrer Institut a personal neutron dosimetry system based on chemically etched CR-39 detectors and automatic track counting is in routine use since 1998. In its original design, the dosimeter is sensitive to thermal neutrons and to neutrons in the energy range from 200 keV up to several MeV. The standard exposition period is 3 months. Recently, a novel concept for individual monitoring was implemented at CERN. In this concept, each worker who possibly enters a radiation zone is equipped with a combined dosimeter for the measurement of personal photon and neutron doses. The dosimeter for photon dose measurement has an instant readout capability and dose measurements are done monthly. The dosimeter for neutron measurement is based on CR-39 detectors and is sensitive to fast neutrons only. The CR-39 detector is only evaluated and a neutron dose determined if the monthly personal photon dose exceeds 2 mSv or if the exposition period of the neutron dosimeter exceeds one year. This novel regime of use of the neutron dosimeter has had some important consequences for its practical implementation. A priori, the wearing period of a neutron dosimeter is not known and can range from 1 month up to 12 or even more months. A good knowledge of the long-term behaviour and characteristics of the detector material is needed. But also organisational and administrative issues have to be considered. The paper will outline the adopted procedure covering not only technical but also organisational aspects. The long-term behaviour of background track density and response to 241 Am-Be over one year are described as well as calibrations performed with 241 Am-Be and 252 Cf sources and in the High-Energy Reference Field Facility at CERN (CERF). The concept of individual monitoring at CERN could be transferred to other locations with high energy accelerators such as PSI and DESY. The experience gained with the neutron dosimeter based on CR-39 since introduction of the

Einstein and solid-state physics

International Nuclear Information System (INIS)

Aut, I.

1982-01-01

A connection between the development of solid-state physics and the works and activity of Albert Einstein is traced. A tremendous Einstein contribution to solid state physics is marked. A strict establishment of particle-wave dualism; a conclusion about the applicability of the Plank radiation law not only to black body radiation; finding out particles indistinguishability - all three discoveries have a principle significance for solid state physics too

Preliminary results of NAPL contamination in a disused industry in the city of Sao Paulo, Brazil, by radon evaluation with CR-39 detectors

International Nuclear Information System (INIS)

Mateus, Crislene; Pecequilo, Brigitte Roxana Soreanu

2015-01-01

Contaminated sites by NAPL (Non-Aqueous Phase-Liquids) may lead to safety risks to human health and to ecosystems, restrictions to urban development and decrease of real estate value. This work used the radon gas as an indicator for the analysis of subsurface soil gas, once this noble gas presents good solubility in a wide range of NAPL, being partially retained in the NAPL contamination. Therefore, a decrease of the activity of radon in the contaminated soil gas can be expected, due to the high capacity of partitioning of radon in NAPL, which allows that the NAPL retain part of the radon previously available in the soil pores. The survey was carried out at a disused industry, contaminated by low volatile NAPL, located at east of Sao Paulo city, in March/2015. Radon was evaluated by passive detection methodology with CR-39 solid state nuclear track detectors (SSNTD). Radon concentrations for the eight monitoring stations at non-contaminated locations in March/2015 varied from 16.4 ± 1.2 kBq.m -3 to 55 ± 4 kBq.m -3 . For the two monitoring stations assumed as contaminated locations in March/2015, radon concentrations were 1.17 ± 0.08 kBq.m -3 and 4.2 ± 0.3 kBq.m -3 , diminished in a range from 92% to 98% when compared with the results for the non-contaminated areas. (author)

Preliminary results of NAPL contamination in a disused industry in the city of Sao Paulo, Brazil, by radon evaluation with CR-39 detectors

Energy Technology Data Exchange (ETDEWEB)

Mateus, Crislene; Pecequilo, Brigitte Roxana Soreanu, E-mail: crislene@ipen.br, E-mail: brigitte@ipen.br [Instituto de Pesquisas Energeticas e Nucleares (IPEN/CNEN-SP), Sao Paulo, SP (Brazil)

2015-07-01

Contaminated sites by NAPL (Non-Aqueous Phase-Liquids) may lead to safety risks to human health and to ecosystems, restrictions to urban development and decrease of real estate value. This work used the radon gas as an indicator for the analysis of subsurface soil gas, once this noble gas presents good solubility in a wide range of NAPL, being partially retained in the NAPL contamination. Therefore, a decrease of the activity of radon in the contaminated soil gas can be expected, due to the high capacity of partitioning of radon in NAPL, which allows that the NAPL retain part of the radon previously available in the soil pores. The survey was carried out at a disused industry, contaminated by low volatile NAPL, located at east of Sao Paulo city, in March/2015. Radon was evaluated by passive detection methodology with CR-39 solid state nuclear track detectors (SSNTD). Radon concentrations for the eight monitoring stations at non-contaminated locations in March/2015 varied from 16.4 ± 1.2 kBq.m{sup -3} to 55 ± 4 kBq.m{sup -3}. For the two monitoring stations assumed as contaminated locations in March/2015, radon concentrations were 1.17 ± 0.08 kBq.m{sup -3} and 4.2 ± 0.3 kBq.m{sup -3}, diminished in a range from 92% to 98% when compared with the results for the non-contaminated areas. (author)

Solid-state circuits

CERN Document Server

Pridham, G J

2013-01-01

Solid-State Circuits provides an introduction to the theory and practice underlying solid-state circuits, laying particular emphasis on field effect transistors and integrated circuits. Topics range from construction and characteristics of semiconductor devices to rectification and power supplies, low-frequency amplifiers, sine- and square-wave oscillators, and high-frequency effects and circuits. Black-box equivalent circuits of bipolar transistors, physical equivalent circuits of bipolar transistors, and equivalent circuits of field effect transistors are also covered. This volume is divided

Change in the sensitivity of CR-39 for alpha-tracks after the storage at different temperatures

International Nuclear Information System (INIS)

Enomoto, Hiroko; Ishigure, Nobuhito

2000-01-01

The effect of storage on track registration property of CR-39 has been investigated. Pieces of CR-39 plate were irradiated with normally incident α-particles and fission fragments using a 252 Cf source prior and posterior to the storage of them in air for one year at different temperatures of -80degC, -23degC, 4degC, 23degC and 35degC. Periodical etching was performed for the pieces stored at different temperatures using the solution of NaOH with 7 mol+l -1 at 70degC for 4 hours. Bulk etch rate (V b ) was obtained from the etch pit diameter (D f ) of fission tracks using the equation: V b =D f /(2t), where t is etching time (h). The sensitivity for α-tracks (S) was obtained from the ratio of the etch pit diameters between α-tracks (D a ) and fission-tracks using the equation: S={1+(D a /D f ) 2 }/{1-(D a /D f ) 2 }-1. The present results show that both the bulk etch rate and α-track sensitivity are not constant, which tend to decrease with storage times and storage temperatures. At -80degC, -23degC and 4degC the change in the sensitivity was negligible. On the other hand, the storage at 23degC for 1 year decreased the sensitivity down to 74%. The most significant effect was observed on the α-track sensitivity at 35degC, which was reduced to 80% for one month, 61% for three months, 42% for six months and 32% for one year. By the comparison of experiments between fading and ageing it is shown that such storage effect is attributed not to fading of latent tracks but mainly to some changes in the detector itself. When CR-39 is used of radon monitoring or neutron monitoring, the following points should be paid attention to: (1) the detector should be stored in a refrigerator before exposure and until etching after the exposure, (2) the change in the sensitivity between the time of calibration and the time of use should be evaluated and the counting efficiency at the measurement should be corrected and (3) for comparison or for interpretation of experimental results

CR-39 track detector calibration for H, He, and C ions from 0.1-0.5 MeV up to 5 MeV for laser-induced nuclear fusion product identification.

Science.gov (United States)

Baccou, C; Yahia, V; Depierreux, S; Neuville, C; Goyon, C; Consoli, F; De Angelis, R; Ducret, J E; Boutoux, G; Rafelski, J; Labaune, C

2015-08-01

Laser-accelerated ion beams can be used in many applications and, especially, to initiate nuclear reactions out of thermal equilibrium. We have experimentally studied aneutronic fusion reactions induced by protons accelerated by the Target Normal Sheath Acceleration mechanism, colliding with a boron target. Such experiments require a rigorous method to identify the reaction products (alpha particles) collected in detectors among a few other ion species such as protons or carbon ions, for example. CR-39 track detectors are widely used because they are mostly sensitive to ions and their efficiency is near 100%. We present a complete calibration of CR-39 track detector for protons, alpha particles, and carbon ions. We give measurements of their track diameters for energy ranging from hundreds of keV to a few MeV and for etching times between 1 and 8 h. We used these results to identify alpha particles in our experiments on proton-boron fusion reactions initiated by laser-accelerated protons. We show that their number clearly increases when the boron fuel is preformed in a plasma state.

New materials for solid state electrochemistry

International Nuclear Information System (INIS)

Ferloni, P.; Consiglio Nazionale delle Ricerche, Pavia; Magistris, A.; Consiglio Nazionale delle Ricerche, Pavia

1994-01-01

Solid state electrochemistry is an interdisciplinary area, undergoing nowadays a fast development. It is related on the one hand to chemistry, and on the other hand to crystallography, solid state physics and materials science. In this paper structural and electrical properties of some families of new materials interesting for solid state electrochemistry are reviewed. Attention is focused essentially on ceramic and crystalline materials, glasses and polymers, displaying high ionic conductivity and potentially suitable for various applications in solid state electrochemical devices. (orig.)

Theoretical solid state physics

International Nuclear Information System (INIS)

Anon.

1977-01-01

Research activities at ORNL in theoretical solid state physics are described. Topics covered include: surface studies; particle-solid interactions; electronic and magnetic properties; and lattice dynamics

Solid-State Physics Introduction to the Theory

CERN Document Server

Patterson, James

2010-01-01

Learning Solid State Physics involves a certain degree of maturity, since it involves tying together diverse concepts from many areas of physics. The objective is to understand, in a basic way, how solid materials behave. To do this one needs both a good physical and mathematical background. One definition of Solid State Physics is it is the study of the physical (e.g. the electrical, dielectric, magnetic, elastic, and thermal) properties of solids in terms of basic physical laws. In one sense, Solid State Physics is more like chemistry than some other branches of physics because it focuses on common properties of large classes of materials. It is typical that Solid State Physics emphasizes how physics properties link to electronic structure. We have retained the term Solid Modern solid state physics came of age in the late thirties and forties and is now is part of condensed matter physics which includes liquids, soft materials, and non-crystalline solids. This solid state/condensed matter physics book begin...

Neutron powder diffraction investigation of magnetic structure and spin reorientation transition of HoFe{sub 1-x}Cr{sub x}O{sub 3} solid solutions

Energy Technology Data Exchange (ETDEWEB)

Liu, Xinzhi [Department of Nuclear Physics, China Institute of Atomic Energy, Beijing 102413 (China); Hao, Lijie, E-mail: haolijie@ciae.ac.cn [Department of Nuclear Physics, China Institute of Atomic Energy, Beijing 102413 (China); Liu, Yuntao; Ma, Xiaobai; Meng, Siqin; Li, Yuqing; Gao, Jianbo; Guo, Hao; Han, Wenze; Sun, Kai; Wu, Meimei [Department of Nuclear Physics, China Institute of Atomic Energy, Beijing 102413 (China); Chen, Xiping; Xie, Lei [Institute of Nuclear Physics and Chemistry, CAEP, Mianyang 621900 (China); Klose, Frank [Australian Nuclear Science and Technology Organization, Lucas Heights, New South Wales 2234 (Australia); Department of Physics and Materials Science, The City University of Hong Kong, Hong Kong (China); Chen, Dongfeng, E-mail: dongfeng@ciae.ac.cn [Department of Nuclear Physics, China Institute of Atomic Energy, Beijing 102413 (China)

2016-11-01

Orthoferrite solid solution HoFe{sub 1−x}Cr{sub x}O{sub 3} (x=0, 0.2,…,1.0) was synthesized via solid state reaction methods. The crystal structure, magnetism and spin reorientation properties of this system were investigated by X-ray diffraction, neutron powder diffraction and magnetic measurements. For compositions of x≤0.6, the system exhibits similar magnetic properties to HoFeO{sub 3}. With increasing Cr-doping, the system adopts a Γ{sub 4}(G{sub x}A{sub y}F{sub z}) magnetic configuration with a decreased Neel temperature from 640 K to 360 K. A Γ{sub 42} spin reorientation of Fe(Cr){sup 3+} was also observed in this system with an increase in transition temperature from 56 K to about 200 K due to competition between the Fe(Cr)–Fe(Cr) and Ho–Fe(Cr) interactions. For the x≥0.8, the system behaves more like HoCrO{sub 3} which adopts a Γ{sub 2}(F{sub x}C{sub y}G{sub z}) configuration with no spin reorientation below the Neel temperature T{sub N}. Throughout the whole substitution range, we found that the saturated moment of Fe(Cr) was less than the ideal value for a free ion, which implies the existence of spin fluctuation in this system. A systematic magnetic structure variation with Cr-substitution is revealed by Rietveld refinement. A phase diagram combining the results of the magnetic measurements and neutron powder diffraction results was obtained. - Highlights: • With Cr-substitution in the HoFe{sub 1−x}Cr{sub x}O{sub 3} system, A Γ{sub 42} spin reorientation of Fe(Cr){sup 3+} was observed with an increase in transition temperature from 56 K to about 200 K for x=0−0.6. • The saturated moment of Fe(Cr) position was found to be systematically less than the ideal value of free ion, and thus implies the presence of spin quantum fluctuation. • A composition–temperature phase diagram throughout x=0–1 for HoFe{sub 1−x}Cr{sub x}O{sub 3} system was established.

Evidence of formation of trans-Fe nuclei in Fe+Al interactions at 1.88 GeV using Cr-39 (DOP) detector

International Nuclear Information System (INIS)

Ganguly, A.K.; Chaudhuri, Biva

1991-01-01

A wedge-shaped aluminium target was irradiated with 1.88 A GeV Fe beam to study various features of Fe+Al nucleus-nucleus interaction and their dependence on target thickness. The detector employed was a stack of CR-39 (DOP) and Lexan plastic nuclear track detectors which have a characteristically high charge resolution property. To distinguish the actual events from background and buildup a selection criteria for easy and unambiguous rejection of unwanted interfering events the stack of detectors was placed at an angle of 60deg with respect to the beam. After irradiation the CR-39 (DOP) detectors were etched and the elliptic etch-pit diameters were scanned. The diameter distribution of the elliptic etch-pits exhibits the existence of trans Fe nuclei. The production of trans Fe fraction is seen to increase with the thickness of the aluminium target. The possible causes of this increase are being investigated. (author). 12 refs., 4 figs

Quantum Computing in Solid State Systems

CERN Document Server

Ruggiero, B; Granata, C

2006-01-01

The aim of Quantum Computation in Solid State Systems is to report on recent theoretical and experimental results on the macroscopic quantum coherence of mesoscopic systems, as well as on solid state realization of qubits and quantum gates. Particular attention has been given to coherence effects in Josephson devices. Other solid state systems, including quantum dots, optical, ion, and spin devices which exhibit macroscopic quantum coherence are also discussed. Quantum Computation in Solid State Systems discusses experimental implementation of quantum computing and information processing devices, and in particular observations of quantum behavior in several solid state systems. On the theoretical side, the complementary expertise of the contributors provides models of the various structures in connection with the problem of minimizing decoherence.

Solid state theory

CERN Document Server

Harrison, Walter A

2011-01-01

""A well-written text . . . should find a wide readership, especially among graduate students."" - Dr. J. I. Pankove, RCA.The field of solid state theory, including crystallography, semi-conductor physics, and various applications in chemistry and electrical engineering, is highly relevant to many areas of modern science and industry. Professor Harrison's well-known text offers an excellent one-year graduate course in this active and important area of research. While presenting a broad overview of the fundamental concepts and methods of solid state physics, including the basic quantum theory o

Solid-State Nanopore

Directory of Open Access Journals (Sweden)

Zhishan Yuan

2018-02-01

Full Text Available Abstract Solid-state nanopore has captured the attention of many researchers due to its characteristic of nanoscale. Now, different fabrication methods have been reported, which can be summarized into two broad categories: “top-down” etching technology and “bottom-up” shrinkage technology. Ion track etching method, mask etching method chemical solution etching method, and high-energy particle etching and shrinkage method are exhibited in this report. Besides, we also discussed applications of solid-state nanopore fabrication technology in DNA sequencing, protein detection, and energy conversion.

Activation energy of etching for CR-39 as a function of linear energy transfer of the incident particles

CERN Document Server

Awad, E M

1999-01-01

In this work, we have studied the effect of the radiation damage caused by the incident particles on the activation energy of etching for CR-39 samples. The damage produced by the incident particle is expressed in terms of the linear energy transfer (LET). CR-39 samples from American Acrylic were irradiated to three different LET particles. These are N (LET sub 2 sub 0 sub 0 = 20 KeV/mu m) as a light particle, Fe (LET sub 2 sub 0 sub 0 = 110 KeV/mu m) as a medium particle and fission fragments (ff) from a sup 2 sup 5 sup 2 Cf source as heavy particles. In general the bulk etch rate was calculated using the weight difference method and the track etch rate was determined using the track geometry at various temperatures (50-90 deg. C) and concentrations (4-9 N) of the NaOH etchant. The average activation energy E sub b related to the bulk etch rate v sub b was calculated from 1n v sub b vs. 1/T. The average activation energy E sub t related to the track etch rate v sub t was estimated from 1n v sub t vs. 1/T. It...

Triton, deuteron and proton responses of the CR-39 track detector

Energy Technology Data Exchange (ETDEWEB)

Yamauchi, Tomoya; Matsumoto, Hiroyoshi; Oda, Keiji [Kobe Univ. of Mercantile Marine (Japan)

1996-07-01

In the present study, we assessed the response of the CR-39 detector to proton, deuteron and triton from their etch-pit growth curves obtained by multi-step etching technique and the difference among their track registration properties was discussed. In order to avoid incorrect evaluation due to the missing track effect, particle irradiation was performed at various incident energies. The response function, S(R), etch rate ratio, S, as a function of the residual range, R, was experimentally evaluated for all hydrogen isotopes by this method. In the next, we obtained another form of response functions of S(E), S({beta}) and S(LET{sub 200}), which were presented as functions of the particle energy, E, the particle velocity, {beta}(=v/c), and the linear energy transfer in the case where the cut-off energy is 200 eV, LET{sub 200}, respectively. These information will be useful also in understanding the fundamentals of the latent track formation mechanism in the plastic track detectors. (J.P.N.)

Interaction of 84 MeV/u 12C with 208Pb target investigated with CR-39 plastic track detector

International Nuclear Information System (INIS)

Grabez, B.

1984-01-01

The interaction of the 84 MeV/u 12 C ions with 208 Pb target was investigated using CR-39 plastic track detector. The first part of the work was dedicated to the examination of the methodology of the recently presented CR-39 detector and its calibration. Measurements have been done on tracks of various ions in the broad atomic number region from Z = 2 to Z = 92. The possibility of the identification of low energy fragments produced in nuclear interactions by measurements on the finished tracks was studied. Our results show that very good charge resolution can be achieved through determination of the mean etch rate ratio and the range of low energy ions. In the second part of the work it was shown that the main reaction channels in the interaction of 84 MeV/u C with Pb target are spallation, fission and fragmentation. The contribution of the multifragmentation is less than 1% of the total reaction cross section. From our results follows that the most probable reaction channels after collision with small impact parameter are fragmentation and deep spallation. The spallation and fission come after more peripheral collisions. (orig./HSI)

Measurement of concentrations of radon and its daughters in indoor atmosphere using CR-39 nuclear track detector

International Nuclear Information System (INIS)

Khan, A.J.; Sharma, K.C.; Varshney, A.K.; Prasad, Rajendra; Tyagi, R.K.

1988-01-01

The concentrations of radon and its daughters in rooms having different environmental conditions are measured using CR-39 nuclear track detector. It has been found that the radon concentration inside the rooms depends on ventilation, sub-soil emanation and the housed materials. The use of internal wall coverings such as plaster, distemper and white washing may reduce the radon emanation inside the rooms. The use of paints on walls is the best for reducing the radon concentration inside the rooms. (author). 11 refs

Solid State Physics Introduction to the Theory

CERN Document Server

Patterson, James D

2007-01-01

Learning Solid State Physics involves a certain degree of maturity, since it involves tying together diverse concepts from many areas of physics. The objective is to understand, in a basic way, how solid materials behave. To do this one needs both a good physical and mathematical background. One definition of Solid State Physics is it is the study of the physical (e.g. the electrical, dielectric, magnetic, elastic, and thermal) properties of solids in terms of basic physical laws. In one sense, Solid State Physics is more like chemistry than some other branches of physics because it focuses on common properties of large classes of materials. It is typical that Solid State Physics emphasizes how physics properties link to electronic structure. We have retained the term Solid State Physics, even though Condensed Matter Physics is more commonly used. Condensed Matter Physics includes liquids and non-crystalline solids such as glass, which we shall not discuss in detail. Modern Solid State Physics came of age in ...

Hydrogen storage in TiCr1.2(FeV)x BCC solid solutions

International Nuclear Information System (INIS)

Santos, Sydney F.; Huot, Jacques

2009-01-01

The Ti-V-based BCC solid solutions have been considered attractive candidates for hydrogen storage due to their relatively large hydrogen absorbing capacities near room temperature. In spite of this, improvements of some issues should be achieved to allow the technological applications of these alloys. Higher reversible hydrogen storage capacity, decreasing the hysteresis of PCI curves, and decrease in the cost of the raw materials are needed. In the case of vanadium-rich BCC solid solutions, which usually have large hydrogen storage capacities, the search for raw materials with lower cost is mandatory since pure vanadium is quite expensive. Recently, the substitutions of vanadium in these alloys have been tried and some interesting results were achieved by replacing vanadium by commercial ferrovanadium (FeV) alloy. In the present work, this approach was also adopted and TiCr 1.2 (FeV) x alloy series was investigated. The XRD patterns showed the co-existence of a BCC solid solution and a C14 Laves phase in these alloys. SEM analysis showed the alloys consisted of dendritic microstructure and C14 colonies. The amount of C14 phase increases when the amount of (FeV) decreases in these alloys. Concerning the hydrogen storage, the best results were obtained for the TiCr 1.2 (FeV) 0.4 alloy, which achieved 2.79 mass% of hydrogen storage capacity and 1.36 mass% of reversible hydrogen storage capacity

Synthesis of surface Cr (VI)-imprinted magnetic nanoparticles for selective dispersive solid-phase extraction and determination of Cr (VI) in water samples.

Science.gov (United States)

Qi, Xue; Gao, Shuang; Ding, Guosheng; Tang, An-Na

2017-01-01

A facile, rapid and selective magnetic dispersed solid-phase extraction (dSPE) method for the extraction and enrichment of Cr (VI) prior to flame atomic absorption spectrometry (AAS) was introduced. For highly selective and efficient extraction, magnetic Cr (VI)-imprinted nanoparticles (Fe 3 O 4 @ Cr (VI) IIPs) were prepared by hyphenating surface ion-imprinted with sol-gel techniques. In the preparation process, chromate (Cr(VI)) was used as the template ion; vinylimidazole and 3-aminopropyltriethoxysilane were selected as organic functional monomer and co-monomer respectively. Another reagent, methacryloxypropyltrimethoxysilane was adopted as coupling agent to form the stable covalent bonding between organic and inorganic phases. The effects of various parameters on the extraction efficiency, such as pH of sample solution, the amount of adsorbent, extraction time, the type and concentration of eluent were systematically investigated. Furthermore, the thermodynamic and kinetic properties of the adsorption process were studied to explore the internal adsorption mechanism. Under optimized conditions, the preconcentration factor, limit of detection and linear range of the established dSPE-AAS method for Cr (VI) were found to be 98, 0.29μgL -1 and 4-140μgL -1 , respectively. The developed method was also successfully applied to the analysis of Cr (VI) in different water samples with satisfactory results, proving its reliability and feasibility in real sample analysis. Copyright © 2016 Elsevier B.V. All rights reserved.

Solid-state devices and applications

CERN Document Server

Lewis, Rhys

1971-01-01

Solid-State Devices and Applications is an introduction to the solid-state theory and its devices and applications. The book also presents a summary of all major solid-state devices available, their theory, manufacture, and main applications. The text is divided into three sections. The first part deals with the semiconductor theory and discusses the fundamentals of semiconductors; the kinds of diodes and techniques in their manufacture; the types and modes of operation of bipolar transistors; and the basic principles of unipolar transistors and their difference with bipolar transistors. The s

A novel solid phase extraction procedure on Amberlite XAD-1180 for speciation of Cr(III), Cr(VI) and total chromium in environmental and pharmaceutical samples

International Nuclear Information System (INIS)

Narin, Ibrahim; Kars, Ayse; Soylak, Mustafa

2008-01-01

Due to the toxicity of chromium, species depend on their chemical properties and bioavailabilities, speciation of chromium is very important in environmental samples. A speciation procedure for chromium(III), chromium(VI) and total chromium in environmental samples is presented in this work, prior to flame atomic absorption spectrometric determination of chromium. The procedure is based on the adsorption of Cr(III)-diphenylcarbazone complex on Amberlite XAD-1180 resin. After oxidation of Cr(III), the developed solid phase extraction system was applied to determinate the total chromium. Cr(III) was calculated as the difference between the total Cr content and the Cr(VI) content. The analytical conditions for the quantitative recoveries of Cr(VI) on Amberlite XAD-1180 resin were investigated. The effects of some alkaline, earth alkaline, metal ions and also some anions were also examined. Preconcentration factor was found to be 75. The detection limits (LOD) based on three times sigma of the blank (N: 21) for Cr(VI) and total chromium were 7.7 and 8.6 μg/L, respectively. Satisfactory results for the analysis of total chromium in the stream sediment (GBW7310) certified reference material for the validation of the presented method was obtained. The procedure was applied to food, water and pharmaceutical samples successfully

Solid-state polymeric dye lasers

CERN Document Server

Singh, S; Sridhar, G; Muthuswamy, V; Raja, K

2003-01-01

This paper presents a review of the organic solid-state polymer materials, which have become established as a new laser media. The photostability of these materials is discussed. Different types of solid-state lasers built around these materials are also reviewed.

The effect of gas double-dynamic on mass distribution in solid-state fermentation.

Science.gov (United States)

Chen, Hong-Zhang; Zhao, Zhi-Min; Li, Hong-Qiang

2014-05-10

The mass distribution regularity in substrate of solid-state fermentation (SSF) has rarely been reported due to the heterogeneity of solid medium and the lack of suitable instrument and method, which limited the comprehensive analysis and enhancement of the SSF performance. In this work, the distributions of water, biomass, and fermentation product in different medium depths of SSF were determined using near-infrared spectroscopy (NIRS) and the developed models. Based on the mass distribution regularity, the effects of gas double-dynamic on heat transfer, microbial growth and metabolism, and product distribution gradient were systematically investigated. Results indicated that the maximum temperature of substrate and the maximum carbon dioxide evolution rate (CER) were 39.5°C and 2.48mg/(hg) under static aeration solid-state fermentation (SASSF) and 33.9°C and 5.38mg/(hg) under gas double-dynamic solid-state fermentation (GDSSF), respectively, with the environmental temperature for fermentation of 30±1°C. The fermentation production (cellulase activity) ratios of the upper, middle, and lower levels were 1:0.90:0.78 at seventh day under SASSF and 1:0.95:0.89 at fifth day under GDSSF. Therefore, combined with NIRS analysis, gas double-dynamic could effectively strengthen the solid-state fermentation performance due to the enhancement of heat transfer, the stimulation of microbial metabolism and the increase of the homogeneity of fermentation products. Copyright © 2014 Elsevier Inc. All rights reserved.

Nuclear tracks in CR-39 produced by carbon, oxygen, aluminium and titanium ions.

Science.gov (United States)

Rickards, J; Romo, V; Golzarri, J I; Espinosa, G

2002-01-01

This work describes the response of CR-39 (allyl diglycol polycarbonate) to different ions (C, O, Al and Ti) produced by the Instituto de Fisica 3 MV 9SDH-2 Pelletron accelerator and backscattered from a thin Au film on a C support. The ion energies were chosen in series such that the ranges of the different ions in the detector were 2, 3, 4, 5, 6, 7 and 8 microm respectively for each series. Once exposed, the detectors were etched with a solution of 6.25 M KOH at 60 degrees C, and the reading was carried out using a digital image analysis system. An analysis of the measured track diameters of all the types of ions indicates that, for a given range, track kinetics are independent of type of ion, energy and stopping power.

Organic solid-state lasers

CERN Document Server

Forget, Sébastien

2013-01-01

Organic lasers are broadly tunable coherent sources, potentially compact, convenient and manufactured at low-costs. Appeared in the mid 60’s as solid-state alternatives for liquid dye lasers, they recently gained a new dimension after the demonstration of organic semiconductor lasers in the 90's. More recently, new perspectives appeared at the nanoscale, with organic polariton and surface plasmon lasers. After a brief reminder to laser physics, a first chapter exposes what makes organic solid-state organic lasers specific. The laser architectures used in organic lasers are then reviewed, with a state-of-the-art review of the performances of devices with regard to output power, threshold, lifetime, beam quality etc. A survey of the recent trends in the field is given, highlighting the latest developments with a special focus on the challenges remaining for achieving direct electrical pumping of organic semiconductor lasers. A last chapter covers the applications of organic solid-state lasers.

Study of α-energy discrimination in CR-39 track etch detectors for use as a radon/thoron dosemeter

International Nuclear Information System (INIS)

Kandaiya, S.; Al-Najjar, S.A.R.; Piesch, E.

1988-01-01

The properties of CR 39 nuclear track detectors were evaluated for their α-energy discrimination up to 8.77 MeV using a combination of chemical-electrochemical track revealing techniques. Using three field strengths, α-energy discrimination by ECE track diameter and track density as a function of chemical pre-etching time were studied. α-energy spectra using different irradiation geometries were then evaluated using the optimum conditions and then compared with those obtained form other techniques. (author)

Magnetism on quasi-1-D lattices in novel non-centrosymmetric Ba{sub 3}CrVS{sub 4}O{sub 3} and in centrosymmetric La{sub 3}TMWS{sub 3}O{sub 6} (TM = Cr, Fe, Co)

Energy Technology Data Exchange (ETDEWEB)

Kim, Jinkwang; Lai, Kwing To; Valldor, Martin, E-mail: martin.valldor@cpfs.mpg.de

2017-08-01

Highlights: • Quasi 1-D chains of magnetic ions exist in Ba{sub 3}CrVS{sub 4}O{sub 3} and La{sub 3}TMWS{sub 3}O{sub 6} (TM = Cr, Fe, Co). • The magnetism of non-centrosymmetric Ba{sub 3}CrVS{sub 4}O{sub 3} is different from centrosymmetric La{sub 3}CrWS{sub 3}O{sub 6}. • Several intrinsic magnetic anomalies are observed without long-ranged spin orderings. - Abstract: La{sub 3}TMWS{sub 3}O{sub 6} (TM = Fe, Co) and novel Ba{sub 3}CrVS{sub 4}O{sub 3} can be obtained as pure polycrystalline samples by mineralizer aided solid-state reactions and a solid-state reaction with further purification by water, respectively. In contrast, La{sub 3}CrWS{sub 3}O{sub 6} needs a standard solid-state reaction to form but the final product contains observable impurities. All four compounds contain similar quasi-1-D magnetic lattices although La-based ones are centrosymmetric (P6{sub 3}/m) and the Ba-containing one is polar and non-centrosymmetric (P6{sub 3}). Strong antiferromagnetic couplings are observed along the magnetic chains in the Fe and Cr containing compounds. As a result, short-range magnetic order is suggested at low temperatures for the Fe-chain, which can be related to magneto-electric couplings. The Co{sup 3+}-homologue shows typical diamagnetic behavior, as supported by its insulating nature, which is due to a low-spin state. The polar Cr{sup 3+}-compound exhibits very different magnetic behavior compared to its corresponding non-polar relative. This proves a strong influence on the physical properties from the crystallographic symmetry.

Solid-State NMR Study of New Copolymers as Solid Polymer Electrolytes

Directory of Open Access Journals (Sweden)

Jean-Christophe Daigle

2018-01-01

Full Text Available We report the analysis of comb-like polymers by solid-state NMR. The polymers were previously evaluated as solid-polymer-electrolytes (SPE for lithium-polymer-metal batteries that have suitable ionic conductivity at 60 °C. We propose to develop a correlation between 13C solid-state NMR measurements and phase segregation. 13C solid-state NMR is a perfect tool for differentiating polymer phases with fast or slow motions. 7Li was used to monitor the motion of lithium ions in the polymer, and activation energies were calculated.

Solid Lithium Ion Conductors (SLIC) for Lithium Solid State Batteries

Data.gov (United States)

National Aeronautics and Space Administration — To identify the most lithium-ion conducting solid electrolytes for lithium solid state batteries from the emerging types of solid electrolytes, based on a...

Monolithic All-Phosphate Solid-State Lithium-Ion Battery with Improved Interfacial Compatibility.

Science.gov (United States)

Yu, Shicheng; Mertens, Andreas; Tempel, Hermann; Schierholz, Roland; Kungl, Hans; Eichel, Rüdiger-A

2018-06-22

High interfacial resistance between solid electrolyte and electrode of ceramic all-solid-state batteries is a major reason for the reduced performance of these batteries. A solid-state battery using a monolithic all-phosphate concept based on screen printed thick LiTi 2 (PO 4 ) 3 anode and Li 3 V 2 (PO 4 ) 3 cathode composite layers on a densely sintered Li 1.3 Al 0.3 Ti 1.7 (PO 4 ) 3 solid electrolyte has been realized with competitive cycling performance. The choice of materials was primarily based on the (electro-)chemical and mechanical matching of the components instead of solely focusing on high-performance of individual components. Thus, the battery utilized a phosphate backbone in combination with tailored morphology of the electrode materials to ensure good interfacial matching for a durable mechanical stability. Moreover, the operating voltage range of the active materials matches with the intrinsic electrochemical window of the electrolyte which resulted in high electrochemical stability. A highly competitive discharge capacity of 63.5 mAh g -1 at 0.39 C after 500 cycles, corresponding to 84% of the initial discharge capacity, was achieved. The analysis of interfacial charge transfer kinetics confirmed the structural and electrical properties of the electrodes and their interfaces with the electrolyte, as evidenced by the excellent cycling performance of the all-phosphate solid-state battery. These interfaces have been studied via impedance analysis with subsequent distribution of relaxation times analysis. Moreover, the prepared solid-state battery could be processed and operated in air atmosphere owing to the low oxygen sensitivity of the phosphate materials. The analysis of electrolyte/electrode interfaces after cycling demonstrates that the interfaces remained stable during cycling.

The etching property of the surface of CR-39 and the track core radius of fission fragment

CERN Document Server

Mineyama, D; Yamauchi, T; Oda, K; El-Rahman, A

2002-01-01

The etch pits of fission fragments in CR-39 detector have been observed carefully using an atomic force microscope (AFM) after extremely short chemical etching in stirred 6N KOH solution kept at 70degC. It was found that there existed a thin layer where the bulk etch rate is relativity from large the etch-pit growth curve for the etching duration between 10 and 1800 seconds. The track core radius of fission fragment was evaluated to be about 6 nm from the extrapolation of the growth curve in a thinner region. (author)

Monitoring tetracycline through a solid-state nanopore sensor

Science.gov (United States)

Zhang, Yuechuan; Chen, Yanling; Fu, Yongqi; Ying, Cuifeng; Feng, Yanxiao; Huang, Qimeng; Wang, Chao; Pei, De-Sheng; Wang, Deqiang

2016-06-01

Antibiotics as emerging environmental contaminants, are widely used in both human and veterinary medicines. A solid-state nanopore sensing method is reported in this article to detect Tetracycline, which is based on Tet-off and Tet-on systems. rtTA (reverse tetracycline-controlled trans-activator) and TRE (Tetracycline Responsive Element) could bind each other under the action of Tetracycline to form one complex. When the complex passes through nanopores with 8 ~ 9 nanometers in diameter, we could detect the concentrations of Tet from 2 ng/mL to 2000 ng/mL. According to the Logistic model, we could define three growth zones of Tetracycline for rtTA and TRE. The slow growth zone is 0-39.5 ng/mL. The rapid growth zone is 39.5-529.7 ng/mL. The saturated zone is > 529.7 ng/mL. Compared to the previous methods, the nanopore sensor could detect and quantify these different kinds of molecule at the single-molecule level.

Solid state magnetism

CERN Document Server

Crangle, John

1991-01-01

Solid state magnetism is important and attempts to understand magnetic properties have led to an increasingly deep insight into the fundamental make up of solids. Both experimental and theoretical research into magnetism continue to be very active, yet there is still much ground to cover before there can be a full understanding. There is a strong interplay between the developments of materials science and of magnetism. Hundreds of new materials have been dis­ covered, often with previously unobserved and puzzling magnetic prop­ erties. A large and growing technology exists that is based on the magnetic properties of materials. Very many devices used in everyday life involve magnetism and new applications are being invented all the time. Under­ standing the fundamental background to the applications is vital to using and developing them. The aim of this book is to provide a simple, up-to-date introduction to the study of solid state magnetism, both intrinsic and technical. It is designed to meet the needs a...

Thermodynamic behavior of very stable binary compounds with a wide homogeneity range: Their influence in the liquid phase in ternary and higher component systems in the solid state

International Nuclear Information System (INIS)

Hoch, M.

1988-01-01

The Hoch-Arpshofen model is combined with the Schottky-Wagner disorder model to describe first binary liquid systems, where a very stable solid protrudes into the liquid. We analyze the systems K-I 2 , Cs-I 2 , U-UO 3 , Ag-S and Al-Sb. The system Al-Sb can be described as Al-Sb and as Al-AlSb-Sb. Then we examine the Al-Co, Al-Ni, and Al-Fe systems to describe the stable compounds CoAl, NiAl, and FeAl, which all have a wide homogeneity range in the solid state. Here the Schottky-Wagner model is sufficient. Finally we describe a model which treats the influence of these stable binary compounds in ternary and larger systems such as Al-Cr-Ni and Al-Cr-Fe, again in the solid state. (orig./IHOE) [de

Performance Improvement of V-Fe-Cr-Ti Solid State Hydrogen Storage Materials in Impure Hydrogen Gas.

Science.gov (United States)

Ulmer, Ulrich; Oertel, Daria; Diemant, Thomas; Bonatto Minella, Christian; Bergfeldt, Thomas; Dittmeyer, Roland; Behm, R Jürgen; Fichtner, Maximilian

2018-01-17

Two approaches of engineering surface structures of V-Ti-based solid solution hydrogen storage alloys are presented, which enable improved tolerance toward gaseous oxygen (O 2 ) impurities in hydrogen (H 2 ) gas. Surface modification is achieved through engineering lanthanum (La)- or nickel (Ni)-rich surface layers with enhanced cyclic stability in an H 2 /O 2 mixture. The formation of a Ni-rich surface layer does not improve the cycling stability in H 2 /O 2 mixtures. Mischmetal (Mm, a mixture of La and Ce) agglomerates are observed within the bulk and surface of the alloy when small amounts of this material are added during arc melting synthesis. These agglomerates provide hydrogen-transparent diffusion pathways into the bulk of the V-Ti-Cr-Fe hydrogen storage alloy when the remaining oxidized surface is already nontransparent for hydrogen. Thus, the cycling stability of the alloy is improved in an O 2 -containing hydrogen environment as compared to the same alloy without addition of Mm. The obtained surface-engineered storage material still absorbs hydrogen after 20 cycles in a hydrogen-oxygen mixture, while the original material is already deactivated after 4 cycles.

39 CFR 221.1 - The United States Postal Service.

Science.gov (United States)

2010-07-01

... 39 Postal Service 1 2010-07-01 2010-07-01 false The United States Postal Service. 221.1 Section 221.1 Postal Service UNITED STATES POSTAL SERVICE ORGANIZATION AND ADMINISTRATION GENERAL ORGANIZATION § 221.1 The United States Postal Service. The United States Postal Service was established as an...

α-cluster states in {sup 46,54}Cr from double-folding potentials

Energy Technology Data Exchange (ETDEWEB)

Mohr, Peter [Diakonie-Klinikum, Schwaebisch Hall (Germany); Institute for Nuclear Research (Atomki), Debrecen (Hungary)

2017-10-15

α-cluster states in {sup 46}Cr and {sup 54}Cr are investigated in the double-folding model. This study complements a recent similar work by Souza and Miyake, Eur. Phys. J. A 53, 146 (2017), which was based on a specially shaped potential. Excitation energies, reduced widths, intercluster separations, and intra-band transition strengths are calculated and compared to experimental values for the ground state bands in {sup 46}Cr and {sup 54}Cr. The α-cluster potential is also applied to elastic scattering at low and intermediate energies. Here, as a byproduct, a larger radial extent of the neutron density in {sup 50}Ti is found. (orig.)

High-powered, solid-state rf systems

International Nuclear Information System (INIS)

Reid, D.W.

1987-01-01

Over the past two years, the requirement to supply megawatts of rf power for space-based applications at uhf and L-band frequencies has caused dramatic increases in silicon solid-state power capabilities in the frequency range from 10 to 3000 MHz. Radar and communications requirements have caused similar increases in gallium arsenide solid-state power capabilities in the frequency ranges from 3000 to 10,000 MHz. This paper reviews the present state of the art for solid-state rf amplifiers for frequencies from 10 to 10,000 MHz. Information regarding power levels, size, weight, and cost will be given. Technical specifications regarding phase and amplitude stability, efficiency, and system architecture will be discussed. Solid-stage rf amplifier susceptibility to radiation damage will also be examined

Solid-state lithium battery

Science.gov (United States)

Ihlefeld, Jon; Clem, Paul G; Edney, Cynthia; Ingersoll, David; Nagasubramanian, Ganesan; Fenton, Kyle Ross

2014-11-04

The present invention is directed to a higher power, thin film lithium-ion electrolyte on a metallic substrate, enabling mass-produced solid-state lithium batteries. High-temperature thermodynamic equilibrium processing enables co-firing of oxides and base metals, providing a means to integrate the crystalline, lithium-stable, fast lithium-ion conductor lanthanum lithium tantalate (La.sub.1/3-xLi.sub.3xTaO.sub.3) directly with a thin metal foil current collector appropriate for a lithium-free solid-state battery.

Interaction mean free path measurements for relativistic heavy ion fragments using CR39 plastic track detectors

International Nuclear Information System (INIS)

Drechsel, H.; Brechtmann, C.; Dreute, J.; Sonntag, S.; Trakowski, W.; Beer, J.; Heinrich, W.

1984-01-01

This paper describes an experiment measuring the interaction mean free paths for charge changing nuclear collisions of relativistic heavy ion fragments. We use a stack of CR39 plastic nuclear track detectors that was irradiated with 1.8 GeV/nucleon 40 Ar ions at the Berkeley Bevalac. About 1.5 x 10 7 etch cones were measured in this experiment using an automatic measuring system. By tracing the etch cones over successive plastic foils the particle trajectories in the stack were reconstructed. For 14185 trajectories with 6444 nuclear collisions of fragments with charge 9-15 the interaction mean free path in the plastic was determined. (orig.)

Radon measurements in the interior of the great pyramid

Energy Technology Data Exchange (ETDEWEB)

Kenawy, M A; Morsy, A A [Ain Shams Univ., Cairo (Egypt). College for Girls

1991-01-01

Radon concentration measurements were made in the interior of the great pyramid of ''Cheops'' at Giza. Measurements were carried out using CR-39 as a solid state nuclear track detector. The CR-39 sheets were placed inside the Queen's and King's chambers and along the ascending corridor leading to them. An evaluation of the radon concentration is presented and discussed. (author).

Radon measurements in the interior of the great pyramid

International Nuclear Information System (INIS)

Kenawy, M.A.; Morsy, A.A.

1991-01-01

Radon concentration measurements were made in the interior of the great pyramid of ''Cheops'' at Giza. Measurements were carried out using CR-39 as a solid state nuclear track detector. The CR-39 sheets were placed inside the Queen's and King's chambers and along the ascending corridor leading to them. An evaluation of the radon concentration is presented and discussed. (author)

Fluidized Bed Reactor as Solid State Fermenter

Directory of Open Access Journals (Sweden)

Krishnaiah, K.

2005-01-01

Full Text Available Various reactors such as tray, packed bed, rotating drum can be used for solid-state fermentation. In this paper the possibility of fluidized bed reactor as solid-state fermenter is considered. The design parameters, which affect the performances are identified and discussed. This information, in general can be used in the design and the development of an efficient fluidized bed solid-state fermenter. However, the objective here is to develop fluidized bed solid-state fermenter for palm kernel cake conversion into enriched animal and poultry feed.

Cr(VI) and Cr(III) removal from aqueous solution by raw and modified lignocellulosic materials: a review.

Science.gov (United States)

Miretzky, P; Cirelli, A Fernandez

2010-08-15

In aqueous systems, chromium usually exists in both trivalent and hexavalent oxidation states, being Cr(VI) of particular importance and concern due to its great toxicity. Industrial sources of Cr(VI) are leather tanning, mining of chrome ore, production of steel and alloys, etc. The most common conventional method for Cr(VI) removal is reduction to Cr(III) at pH 2.0 and precipitation of Cr (OH)(3) with lime at pH 9-10. The disadvantage of precipitation is the disposal of the solid waste. Adsorption of Cr by different low cost materials seems to be a suitable choice for wastewater treatment. Many by-products of agriculture have proved to be suitable low cost adsorbents for Cr(VI) and Cr(III) removal from water. Lignocellulosic residues, which include both wood residues and agricultural residues, have adsorption capacity comparable to other natural sorbents, but they have the advantage of very low or no cost, great availability and simple operational process. This study is a review of the recent literature on the use of natural and modified lignocellulosic residues for Cr adsorption. The Cr maximum adsorption capacity and the adsorption mechanism under different experimental conditions are reported when possibly. Copyright 2010 Elsevier B.V. All rights reserved.

Solid state physics for metallurgists

CERN Document Server

Weiss, Richard J

2013-01-01

Metal Physics and Physical Metallurgy, Volume 6: Solid State Physics for Metallurgists provides an introduction to the basic understanding of the properties that make materials useful to mankind. This book discusses the electronic structure of matter, which is the domain of solid state physics.Organized into 12 chapters, this volume begins with an overview of the electronic structure of free atoms and the electronic structure of solids. This text then examines the basis of the Bloch theorem, which is the exact periodicity of the potential. Other chapters consider the fundamental assumption in

Solid-State Powered X-band Accelerator

Energy Technology Data Exchange (ETDEWEB)

Othman, Mohamed A.K. [SLAC National Accelerator Lab., Menlo Park, CA (United States); Nann, Emilio A. [SLAC National Accelerator Lab., Menlo Park, CA (United States); Dolgashev, Valery A. [SLAC National Accelerator Lab., Menlo Park, CA (United States); Tantawi, Sami [SLAC National Accelerator Lab., Menlo Park, CA (United States); Neilson, Jeff [SLAC National Accelerator Lab., Menlo Park, CA (United States)

2017-03-06

In this report we disseminate the hot test results of an X-band 100-W solid state amplifier chain for linear accelerator (linac) applications. Solid state power amplifiers have become increasingly attractive solutions for achieving high power in radar and maritime applications. Here the performance of solid state amplifiers when driving an RF cavity is investigated. Commercially available, matched and fully-packaged GaN on SiC HEMTs are utilized, comprising a wideband driver stage and two power stages. The amplifier chain has a high poweradded- efficiency and is able to supply up to ~1.2 MV/m field gradient at 9.2 GHz in a simple test cavity, with a peak power exceeding 100 W. These findings set forth the enabling technology for solid-state powered linacs.

Calibration of thermal neutron detection compound BN-1 and CR-39 in the exposure room of Triga Reactor in Ljubljana

International Nuclear Information System (INIS)

Kristof, E.; Ilic, R.; Skvarc, J.; Dijanosic, R.

1994-01-01

Description of determination of thermal neutron fluences in the range from 1.E+02 to 1.E+12 cm -2 for calibration of the neutron sensitive compound consisting of the neutron converter BN-1 and charged particle detector CR-39 is given. The method employs two proportional BF3 detectors supplemented by a Ge(Li) gamma spectometer utilizing gold foils. The results of the measurements are also presented. (author)

Background tracks in CR-39 SSNTD sheets: their control and prediction through an interplay of etching parameters

International Nuclear Information System (INIS)

Bhagwat, A.M.; Naik, G.R.; Thampan, S.; Rudran, K.; Joshi, V.B.; Iyer, M.R.

1992-01-01

High sensitivity of CR-39 film in turn leads to higher and variable background track-densities. A two-step etching process, each consisting of CE and ECE, is therefore suggested which permits not only partial freezing of the background but also allows to know its level. The procedure identifies bad pieces with scratches and determines the minimum detection limit (MDL) of each film individually. Activities as low as 0.2 mBq (∼ 5 x 10 -15 curies) can thus be measured with low background films for exposure periods of 7-10 days (exposure is carried out after first processing). (author)

Alkaline hydrothermal stabilization of Cr(VI) in soil using glass and aluminum from recycled municipal solid wastes.

Science.gov (United States)

Gattullo, Concetta Eliana; D'Alessandro, Caterina; Allegretta, Ignazio; Porfido, Carlo; Spagnuolo, Matteo; Terzano, Roberto

2018-02-15

Hexavalent chromium was stabilized in soil by using a mixture of glass and aluminum recovered from municipal solid wastes under alkaline hydrothermal conditions. Cr(VI) concentration was reduced by 94-98% already after 7days of treatment. After the same period, more than 90% of total Cr was stabilized in highly recalcitrant and scarcely mobile chemical forms, with 50% in the residual fraction (when the samples were treated at 1/10w/w mixture/soil ratio). Longer treatments increased Cr stabilization. X-ray microanalyses revealed that Cr was stabilized in geopolymeric structures within large aluminosilicate mineral aggregates (containing both amorphous and crystalline phases). 3D microstructural analyses showed a limited compaction of the soil with still a 20% internal porosity in the neoformed aggregates. Increased pH and salinity after the treatment can be restored by simple soil amendments and washing. Copyright © 2017. Published by Elsevier B.V.

The Tribological Performance of CrMoN/MoS2 Solid Lubrication Coating on a Piston Ring

Directory of Open Access Journals (Sweden)

Yuelan Di

2017-05-01

Full Text Available In order to improve the tribological properties of an engine piston ring and enhance its service life, magnetron sputtering technology and low temperature ion sulphurizing treatment technology were used to prepare CrMoN/MoS2 solid lubricant coating on the surface of an engine piston ring. The morphologies and compositions of the surface and cross-section of the sulfuration layer were analyzed by field emission scanning electron microscopy (FESEM, and wear property under high load, high speed and high temperature conditions were tested by a SRV®4 friction and wear testing machine. The results show that the CrMoN/MoS2 composite coatings appear as a dense grain structure, and the coating is an ideal solid lubrication layer that possesses an excellent high temperature wear resistance, reducing the engine operating temperature abrasion effectively and prolonging the service life of the engine.

Experimental and theoretical investigation of Cr_1-xSc_xN solid solutions for thermoelectrics

DEFF Research Database (Denmark)

Kerdsongpanya, Sit; Sun, Bo; Eriksson, Fredrik

2016-01-01

The ScN- and CrN-based transition-metal nitrides have recently emerged as a novel and unexpected class of materials for thermoelectrics. These materials constitute well-defined model systems for investigating mixing thermodynamics, phase stability, and band structure aiming for property tailoring......-factor improvement by Sc3d orbital delocalization on Cr3d electrons giving decreasing electrical resistivity, while localized Cr3d orbitals with a large DOS slope may yield an improved Seebeck coefficient. Sc-rich solid solutions show a large improvement in power factor compared to pure ScN, and all films have power...

Interaction of low-intensity nuclear radiation dose with the human blood: Using the new technique of CR-39NTDs for an in vitro study

International Nuclear Information System (INIS)

Ismail, Asaad H.; Jaafar, Mohamad S.

2011-01-01

Complete blood counts were analyzed for 30 samples of human blood with radiation dose rate ranging between 10 and 41 μSv/h using a Radium-226 source with different time of exposure. A new technique involving a nuclear track detector type CR-39(CR-39 NTDs) was used to estimate the alpha particle density incident on the blood samples. The results show that the ranges of alpha particle in blood samples and on the surface of CR-39NTDs vary exponentially with energy of alpha particles. This depends on the restricted energy loss and target density. Changes in the blood components due to irradiation occurred for different durations of irradiation, and the duration of irradiation that influenced the blood samples in this study was 6 min. The change in red blood cell (RBC) was negligible, so it is less affected than other blood components. In addition, most changes in the blood contents began at a low radiation dose (10.38-13.41 μSv/h). For the doses 13.41-21.77 μSv/h, platelet (PLT) counts increased rapidly and adversely with the RBC and white blood cell (WBC) due to chromosomal aberration. Besides, rapid PLT count reduction rapidly at high dose (42.1 μSv h) causes thrombocytopenia; in contrast, WBC increased, which is an indication of cancer caused due to increase in alpha particle dose. Generally, our results are in agreement with the essentials of blood content and the principles of biological radiation interaction.

Usage of an interactive image analysis system for studying various parameters of etched tracks in CR-39 and Makrofol E

International Nuclear Information System (INIS)

Abu-Jarad, F.; Islam, M.A.; Que, A.

1991-01-01

An Automated Interactive Built Analysis System (IBAS) is being used to analyze the alpha and fission fragment tracks in CR-39 and Makrofol E detectors. It primarily consists of a control computer (IBAS1) and an image processor (IBAS2). The system is used for counting the nuclear tracks, measuring their areas, diameters, statistics and displaying the frequency distribution of their sizes. All information can be printed out or stored on floppy disks. (author)

CR-39 nuclear track detector application for the diagnostics of low energy high power ion beams

Energy Technology Data Exchange (ETDEWEB)

Opekounov, M S; Pechenkin, S A; Remnev, G E [Nuclear Physics Institute, Tomsk (Russian Federation); Ivonin, I V [Siberian Physical-Technical Institute, Tomsk (Russian Federation)

1997-12-31

The results of investigation of the spectral composition of ion beams generated by the magneto-insulated ion diode of the MUK-M and TEMP accelerators. The energy and mass characteristics of the accelerated ion beam were determined by a Thomson spectrometer with a CR-39 plate detector (MOM - Atomki Nuclear Track Detector, Type MA-ND/p). The accelerated ion energy was from 40 to 240 keV. The ion current density range was from 1 to 10 A/cm{sup 2}. The mass composition contained hydrogen, nitrogen, carbon and aluminum ions. The individual track analysis showed the track form, depth and diameter in dependence on the ion mass and energy. (author). 2 figs., 5 refs.

Solid-state lighting-a benevolent technology

International Nuclear Information System (INIS)

Schubert, E Fred; Kim, Jong Kyu; Luo Hong; Xi, J-Q

2006-01-01

Solid-state light sources are in the process of profoundly changing the way humans generate light for general lighting applications. Solid-state light sources possess two highly desirable features, which set them apart from most other light sources: (i) they have the potential to create light with essentially unit power efficiency and (ii) the properties of light, such as spectral composition and temporal modulation, can be controlled to a degree that is not possible with conventional light sources such as incandescent and fluorescent lamps. The implications are enormous and, as a consequence, many positive developments are to be expected including a reduction in global energy consumption, reduction of global-warming-gas and pollutant emissions and a multitude of new functionalities benefiting numerous applications. This review will assess the impact of solid-state lighting technology on energy consumption, the environment and on emerging application fields that make use of the controllability afforded by solid-state sources. The review will also discuss technical areas that fuel continued progress in solid-state lighting. Specifically, we will review the use of novel phosphor distributions in white light-emitting diodes (LEDs) and show the strong influence of phosphor distribution on efficiency. We will also review the use of reflectors in LEDs with emphasis on 'perfect' reflectors, i.e. reflectors with highly reflective omni-directional characteristics. Finally, we will discuss a new class of thin-film materials with an unprecedented low refractive index. Such low-n materials may strongly contribute to the continuous progress in solid-state lighting

Non-monotonic compositional dependence of isothermal bulk modulus of the (Mg1–xMnxCr2O4 spinel solid solutions, and its origin and implication

Directory of Open Access Journals (Sweden)

Xi Liu

2016-12-01

Full Text Available The compressibility of the spinel solid solutions, (Mg1−xMnxCr2O4 with x = 0.00 (0, 0.20 (0, 0.44 (2, 0.61 (2, 0.77 (2 and 1.00 (0, has been investigated by using a diamond-anvil cell coupled with synchrotron X-ray radiation up to ∼10 GPa (ambient T. The second-order Birch–Murnaghan equation of state was used to fit the PV data, yielding the following values for the isothermal bulk moduli (KT, 198.2 (36, 187.8 (87, 176.1 (32, 168.7 (52, 192.9 (61 and 199.2 (61 GPa, for the spinel solid solutions with x = 0.00 (0, 0.20 (0, 0.44 (2, 0.61 (2, 0.77 (2 and 1.00 (0, respectively (KT′ fixed as 4. The KT value of the MgCr2O4 spinel is in good agreement with existing experimental determinations and theoretical calculations. The correlation between the KT and x is not monotonic, with the KT values similar at both ends of the binary MgCr2O4MnCr2O4, but decreasing towards the middle. This non-monotonic correlation can be described by two equations, KT = −49.2 (11x + 198.0 (4 (x ≤ ∼0.6 and KT = 92 (41x + 115 (30 (x ≥ ∼0.6, and can be explained by the evolution of the average bond lengths of the tetrahedra and octahedra of the spinel solid solutions. Additionally, the relationship between the thermal expansion coefficient and composition is correspondingly reinterpreted, the continuous deformation of the oxygen array is demonstrated, and the evolution of the component polyhedra is discussed for this series of spinel solid solutions. Our results suggest that the correlation between the KT and composition of a solid solution series may be complicated, and great care should be paid while estimating the KT of some intermediate compositions from the KT of the end-members.

Two dimensional solid state NMR

International Nuclear Information System (INIS)

Kentgens, A.P.M.

1987-01-01

This thesis illustrates, by discussing some existing and newly developed 2D solid state experiments, that two-dimensional NMR of solids is a useful and important extension of NMR techniques. Chapter 1 gives an overview of spin interactions and averaging techniques important in solid state NMR. As 2D NMR is already an established technique in solutions, only the basics of two dimensional NMR are presented in chapter 2, with an emphasis on the aspects important for solid spectra. The following chapters discuss the theoretical background and applications of specific 2D solid state experiments. An application of 2D-J resolved NMR, analogous to J-resolved spectroscopy in solutions, to natural rubber is given in chapter 3. In chapter 4 the anisotropic chemical shift is mapped out against the heteronuclear dipolar interaction to obtain information about the orientation of the shielding tensor in poly-(oxymethylene). Chapter 5 concentrates on the study of super-slow molecular motions in polymers using a variant of the 2D exchange experiment developed by us. Finally chapter 6 discusses a new experiment, 2D nutation NMR, which makes it possible to study the quadrupole interaction of half-integer spins. 230 refs.; 48 figs.; 8 tabs

Fragmentation cross section measurements of iron projectiles using CR-39 plastic nuclear track detectors

CERN Document Server

Flesch, F; Huentrup, G; Roecher, H; Streibel, T; Winkel, E; Heinrich, W

1999-01-01

For long term space missions in which larger radiation doses are accumulated it is necessary to improve the precision of models predicting the space radiation environment. Different models are available to determine the flux of cosmic ray heavy ions behind shielding material. The accuracy of these predictions depends on the knowledge of the fragmentation cross sections, especially at energies of several hundred MeV/nucleon, where the particle flux is at a maximum and especially for those particles with high LET, i.e. iron nuclei. We have measured fragmentation cross sections of sup 5 sup 6 Fe projectiles at beam energies of 700 and 1700 A MeV using experimental set-ups with plastic nuclear track detectors. In this paper we describe the experimental technique to study the fragmentation reactions of sup 5 sup 6 Fe projectiles using CR-39 plastic nuclear track detectors. Results for different targets are presented.

Change of Cr-39(DOP) track detector response as a result of space exposure

International Nuclear Information System (INIS)

Yadav, J.S.; Singh, R.K.

1990-01-01

The response functions for CR-39(DOP) plastic track detectors are calculated, using the simplex method for nonlinear least squares fit, from experimental data obtained from accelerator beams as well as space exposure. The average detector sensitivity is reduced by over 30% in the case of space exposure. The average charge shift for the oxygen group is one charge unit, and it increases with particle charge. The effect decreases with restricted energy loss, which is contrary to that observed in the registration temperature effect. We have discussed various environmental parameters which may produce the observed effect. The registration temperature effect may account for the observed effect (within the errors) for the worst case (temperature) analysis. However, a more reasonable estimate suggests that both the registration temperature as well as pressure during exposure contribute to the observed effect. To discriminate between the separate contributions, further experimental data is needed. (author)

Mass defect of 37Cl(t, p)39Cl: Coulomb displacement energy of the T=5/2, Jsup(π)=3+/2 states in 39Cl-39Ar

International Nuclear Information System (INIS)

Antony, M.S.; Britz, J.; Bueb, J.B.; Pape, A.

1984-01-01

From the Q-value (5701.9+-2.5)keV of the reaction 37 Cl(t, p) 39 Cl, the ground-state mass defect of 39 Cl is found to be (-29802.8+-2.5)keV, an improvement upon the existing value of (-29803+-18)keV. The Coulomb displacement energy of the mirror nuclei 39 Cl- 39 Ar for T=5/2, Jsup(π)=3 + /2 is found to be (6422.1+-10.6)keV. The r 0 parameter of the charge radius is approximately 1.32 fm for A=39

Entrepreneurial actions in public management: analysis of the Programme “Crédito Solidário” (PCS in a southern town of Minas Gerais State [doi: 10.21529/RECADM.2016005

Directory of Open Access Journals (Sweden)

Camila Assis Silva

2017-01-01

Full Text Available One of the current trends in the Campo de Públicas is the inclusion of entrepreneurship subject in the discussion on the public policy formulation and implementation. This kind of thinking came from the understanding that with the globalization process it was necessary for the public sector to adapt to changes through a more flexible management that could respond to society’s demands. This research aims to analyze, from the beneficiaries’s point of view of the Programme “Programa Crédito Solidário” (PCS in a town in the southern of Minas Gerais State, in levels of economic, social and political emancipation of those who benefit from this public policy. It becomes clear how this type of action represents a process of implementation and formulation of public projects in a paradoxical condition, because at the same time it promotes new alternatives for the development of small business from the Economia Solidária (Solidarity Economy, it alters to be rather weak in a context of economical, social and political emancipation of beneficiaries.   Keywords Public entrepreneurship; Solidarity economy; Emancipation.

Macroscopic modelling of solid-state fermentation

NARCIS (Netherlands)

Hoogschagen, M.J.

2007-01-01

Solid-state fermentation is different from the more well known process of liquid fermentation because no free flowing water is present. The technique is primarily used in Asia. Well-known products are the foods tempe, soy sauce and saké. In industrial solid-state fermentation, the substrate usually

Alpha particle spectroscopy for CR-39 detector utilizing matrix of energy equations

Energy Technology Data Exchange (ETDEWEB)

Awad, E.M. [Department of General Sciences, Yanbu Industrial College, PO Box 30436, Madinat Yanbu Al-Sinaiya (Saudi Arabia); Physics Department, Faculty of Science, Menofia University, Shebin El-Koom (Egypt)], E-mail: ayawad@yahoo.com; Soliman, A.A. [Department of Mathematics, Faculty of Education (AL-Arish), Suez Canal University, AL-Arish 45111 (Egypt); Department of Mathematics, Teacher' s College (Bisha), King Khalid University, Bisha, PO Box 551 (Saudi Arabia)], E-mail: asoliman_99@yahoo.com; Rammah, Y.S. [Physics Department, Faculty of Science, Menofia University, Shebin El-Koom (Egypt)

2007-10-01

A method for determining alpha-particle energy using CR-39 detector by utilizing matrix of energy equation was described. The matrix was composed from two axes; the track minor axis (m) and diameter of etched out track end (d) axis of some selected elliptical tracks. The energy E in (m,d) coordinate was approximated by matrix of energy equations given by: E{sub k}={sigma}{sub i,j=0}{sup 2}a{sub ij}d{sub k}{sup i}m{sub k}{sup j}, which was identified using two different approaches. First, i and j were treated as power exponents for d and m. The adjusting parameters values a{sub ij} were obtained and the energy of a given track was deduced directly from it. Second, i and j were treated as indices of some chosen tracks that were fitted to obtain iso-energy curves that were superimposed on m-d scatter plot as calibration curves. The energy between any two successive iso-energy curves in this case was assumed varied linearly with d for a given m. The energy matrix in both cases was solved numerically. Results of the two approaches were compared.

Application of CR-39 microfilm for rapid discrimination between alpha-particle sources

Energy Technology Data Exchange (ETDEWEB)

Dwaikat, Nidal; Al-karmi, Anan M. [Dept. of Physics, King Fahd University of Petroleum and Minerals, Dhahran (Saudi Arabia)

2017-06-15

This work presents a new technique for discriminating between alpha particles of different energy levels. In a first study, two groups of alpha particles emitted from radium-226 and americium-241 sources were successfully separated using a CR-39 microfilm of appropriate thickness. This thickness was adjusted by chemical etching before and after irradiation so that lower-energy particles were stopped within the detector, while higher-energy particles were revealed on the back side of the detector. The number of tracks on the front side of the microfilm represented all alpha particles incident on that side from the two sources. However, the number of tracks on the back side of the microfilm represented only the long-range alpha particles of higher energy that arrived at that side. Therefore, by subtracting the number of tracks on the back side from the number of tracks on the front side, one could easily determine the number of tracks for the short-range alpha particles of lower energy that remained embedded in the microfilm. Discrimination of the two energy levels is thus achieved in a simple, fast, and reliable process.

Atomistic simulation of the influence of Cr on the mobility of the edge dislocation in Fe(Cr) alloys

International Nuclear Information System (INIS)

Hafez Haghighat, S.M.; Terentyev, D.; Schaeublin, R.

2011-01-01

In this work Fe-Cr compounds, as model alloys for the ferritic base steels that are considered as main candidates for the structural materials of the future fusion reactors, are studied using molecular dynamics simulations. The Cr or so-called α' precipitates, which are obstacles to dislocations, affect mechanical properties, leading to hardening and loss of ductility. The flow stress to move an edge dislocation in a Cr solid solution in pure Fe is studied as a function of Cr content. The strength of a nanometric Cr precipitate as obstacle to an edge dislocation in pure Fe is investigated as a function of its Cr content. Results show that with increasing Cr content the precipitate obstacle strength increases, with a strong sensitivity to the local atomic order. Temperature induces a monotonic decrease of the flow stress of the Cr solid solution and of the Cr precipitate obstacle strength.

Identification of charged particles by etching the solid state nuclear track detectors in successive intervals

International Nuclear Information System (INIS)

Randhawa, G.S.; Virk, H.S.

1997-01-01

The suitability of the method of charged particle identification by etching the samples in successive intervals developed by Grabez et al. has been checked in CR-39 exposed to heavy ions 238 U, 208 Pb, 197 Au and 132 Xe in the interval 11.0 to 17.0 MeV/u. A similar study has been made on soda glass detectors irradiated by 238 U, 132 Xe, 56 Fe and 48 Ti ions having energy 4.0 to 6.0 MeV/u. It is concluded that this method of particle identification can be used successfully in CR-39 and soda glass detectors. (author)

Preparation of La{sub 0.75}Sr{sub 0.25}Cr{sub 0.5}Mn{sub 0.5}O{sub 3-{delta}} fine powders by carbonate coprecipitation for solid oxide fuel cells

Energy Technology Data Exchange (ETDEWEB)

Ha, Sang Bu; Cho, Pyeong-Seok; Cho, Yoon Ho; Lee, Dokyol; Lee, Jong-Heun [Department of Materials Science and Engineering, Korea University, Anam-dong, Sungbuk-ku, Seoul 136-713 (Korea)

2010-01-01

A range of La{sub 0.75}Sr{sub 0.25}Cr{sub 0.5}Mn{sub 0.5}O{sub 3-{delta}} (LSCM) powders is prepared by the carbonate coprecipitation method for use as anodes in solid oxide fuel cells. The supersaturation ratio (R = [(NH{sub 4}){sub 2}CO{sub 3}]/([La{sup 3+}] + [Sr{sup 2+}] + [Cr{sup 3+}] + [Mn{sup 2+}])) during the coprecipitation determines the relative compositions of La, Sr, Cr, and Mn. The composition of the precursor approaches the stoichiometric one at the supersaturation range of 4 {<=} R {<=} 12.5, whereas Sr and Mn components are deficient at R < 4 and excessive at R = 25. The fine and phase-pure LSCM powders are prepared by heat treatment at very low temperature (1000 C) at R = 7.5 and 12.5. By contrast, the solid-state reaction requires a higher heat-treatment temperature (1400 C). The catalytic activity of the LSCM electrodes is enhanced by using carbonate-derived powders to manipulate the electrode microstructures. (author)

Heavy metals pollution at municipal solid waste dumpsites in Kano and Kaduna states in Nigeria

Directory of Open Access Journals (Sweden)

W.U. Anake

2009-08-01

Full Text Available Soil samples collected from two major dumpsites each in Kano and Kaduna states were investigated for heavy metals pollution. Each of the dumpsite was divided into north, south, east and west. Four soil samples were collected at a depth of 0-15 cm from each part and pooled to form a composite sample. Soil samples from reserve areas within the same geographical locations as the dumpsites were collected as control. Acid-extractable cadmium (Cd, chromium (Cr, nickel (Ni and lead (Pb were determined using 2 M nitric acid solution and atomic absorption spectroscopy. The ranges of Cd, Cr, Ni and Pb levels for all the dumpsites were 0.30−49.8, 5.76−139, 0.39−19.1 and 42.6−9662 mg/kg, respectively. Kano dumpsite 2 was found to pollute most with Cd, Cr and Pb in 50-100 % soil samples collected having concentrations higher than the threshold limits set by regulatory body. Paper and food scraps showed higher percentages in both Kano and Kaduna dumpsites. The soil was high is sand for all the dumpsites implying high leaching potentials of the heavy metals pollutants.

Dose-rate effects on the bulk etch-rate of CR-39 track detector exposed to low-LET radiations

CERN Document Server

Yamauchi, T; Oda, K; Ikeda, T; Honda, Y; Tagawa, S

1999-01-01

The effect of gamma-rays and pulsed electrons has been investigated on the bulk etch rate of CR-39 detector at doses up to 100 kGy under various dose-rate between 0.0044 and 35.0 Gy/s. The bulk etch rate increased exponentially with the dose at every examined dose-rates. It was reveled to be strongly depend on the dose-rate: the bulk etch rate was decreased with increasing dose-rate at the same total dose. A primitive model was proposed to explain the dose-rate effect in which oxygen dissolved was assumed to dominate the damage formation process.

Thermodynamic properties of the solid solutions CuCr/sub 2/S/sub 4/ in Cu/sub 1///sub 2/M/sub 1///sub 2/Cr/sub 2/S/sub 4/ (M=Ga, In)

Energy Technology Data Exchange (ETDEWEB)

Titov, V.V.; Gordeev, I.V.; Kesler, Y.A.; Shchelkotunov, V.A.; Tret' yakov, Y.D.

1985-09-01

Using an adiabatic calorimeter and a quartz dilatometer, the temperature dependences of the heat capacity for the solid solutions CuCr/sub 2/S/sub 4/ in Cu/sub 1///sub 2/M/sub 1///sub 2/Cr/sub 2/S/sub 4/ (M - Ga, In) were determined, the different components of the heat capacity were evaluated, and the thermodynamic parameters of the magnetic transformation were calculated.

Solid State Photovoltaic Research Branch

Energy Technology Data Exchange (ETDEWEB)

1990-09-01

This report summarizes the progress of the Solid State Photovoltaic Research Branch of the Solar Energy Research Institute (SERI) from October 1, 1988, through September 30,l 1989. Six technical sections of the report cover these main areas of SERIs in-house research: Semiconductor Crystal Growth, Amorphous Silicon Research, Polycrystalline Thin Films, III-V High-Efficiency Photovoltaic Cells, Solid-State Theory, and Laser Raman and Luminescence Spectroscopy. Sections have been indexed separately for inclusion on the data base.

Energy spectrum of iron nuclei measured inside the MIR space craft using CR-39 track detectors

International Nuclear Information System (INIS)

Guenther, W.; Leugner, D.; Becker, E.; Flesch, F.; Heinrich, W.; Huentrup, G.; Reitz, G.; Roecher, H.; Streibel, T.

1999-01-01

We have exposed stacks of CR-39 plastic nuclear track detectors inside the MIR space craft during the EUROMIR95 space mission for almost 6 months. Over this long period a large number of tracks of high LET events was accumulated in the detector foils. The etching and measuring conditions for this experiment were optimized to detect tracks of stopping iron nuclei. We found 185 stopping iron nuclei inside the stack and identified their trajectories through the material of the experiment. Based on the energy-range relation the energy at the surface of the stack was determined. These particles allow the determination of the low energy part of the spectrum of iron nuclei behind shielding material inside the MIR station

Track Detection Technique Using CR-39 for Determining Depleted Uranium in Biological Specimens

International Nuclear Information System (INIS)

Murbat, S.M.

2013-01-01

Track detecting technique using CR-39 track detector has been implemented for determining depleted uranium concentration in biological specimens (tissues, bones, and blood) of patients infected with cancer diseases. Results were compared with specimens of patients infected with conventional diseases (noncancerous). Specimens were collected from middle and south of Iraq have been contaminated with depleted uranium in the Gulf war in 1991. Results show that this technique is efficient for determining depleted uranium concentration in biological specimens. It was found that all studies samples determine for patients infected with cancer diseases contain a high concentration of depleted uranium (more than the international standard) comparing with noncancerous diseases. Moreover, it was found that persons infected with Leukemia show more sensitive to uranium concentrations to induce the diseases (66-202 ppb), while (116- 1910 ppb) concentrations were needed for inducing cancer diseases in organs and tissues. Result confirmed the correlation between cancerous diseases and the munitions made of depleted uranium used in the Gulf war in 1991 leads to contaminate the Iraqi environment and causes a high risk against people in Iraq.

Measurement of target fragments produced by 160 MeV proton beam in aluminum and polyethylene with CR-39 plastic nuclear track detectors

Czech Academy of Sciences Publication Activity Database

Ambrožová, Iva; Yasuda, N.; Kodaira, S.; Sihver, L.

2014-01-01

Roč. 64, MAY (2014), s. 29-34 ISSN 1350-4487 R&D Projects: GA AV ČR KJB100480901; GA AV ČR IAA100480902; GA MŠk LG14004 Institutional support: RVO:61389005 Keywords : target fragments * high-energy protons * Aluminium * Polyethylene * plastic nuclear track detectors * CR-39 Subject RIV: BG - Nuclear, Atomic and Molecular Physics, Colliders Impact factor: 1.213, year: 2014

Análises Quase-experimentais Sobre o Impacto das Cooperativas de Crédito Rural Solidário no PIB Municipal da Agropecuária

Directory of Open Access Journals (Sweden)

Amanda Massaneira de Souza Schuntzemberger

2015-09-01

Full Text Available Resumo: No meio rural brasileiro, muitos municípios ainda não possuem agências bancárias, e as cooperativas de crédito surgem como instituições alternativas no fornecimento de crédito, distinguindo-se dos bancos por sua importância para o desenvolvimento local. Este artigo busca medir o impacto da implantação de cooperativas de crédito rural solidário nos municípios brasileiros sobre o PIB per capita da agropecuária (valor adicionado, usando dois métodos quase-experimentais para dar robustez às conclusões sobre o impacto. Verifica-se uma relação causal positiva pelo método de Diferenças-em-Diferenças com pareamento por escore de propensão, indicando um impacto médio da presença de cooperativas de crédito rural solidário sobre o PIB per capita da agropecuária em 2010 de R$ 987,66, significativo a 5%. Coeficientes positivos para a variável de tratamento também foram verificados nas regressões por MQO ponderadas pelos escores de propensão, sendo o PIB per capita da agropecuária cerca de 20% maior para os municípios que constituíram cooperativas de crédito rural solidário entre 2008 e 2009. Esses resultados evidenciam a importância de criar cooperativas de crédito rural solidário para as áreas rurais dos municípios brasileiros, principalmente naqueles que ainda não possuem, uma vez que o papel dessas cooperativas vem sendo desempenhado de forma a contribuir para o crescimento local.

Solid-state NMR basic principles and practice

CERN Document Server

Apperley, David C; Hodgkinson, Paul

2014-01-01

Nuclear Magnetic Resonance (NMR) has proved to be a uniquely powerful and versatile tool for analyzing and characterizing chemicals and materials of all kinds. This book focuses on the latest developments and applications for "solid-state" NMR, which has found new uses from archaeology to crystallography to biomaterials and pharmaceutical science research. The book will provide materials engineers, analytical chemists, and physicists, in and out of lab, a survey of the techniques and the essential tools of solid-state NMR, together with a practical guide on applications. In this concise introduction to the growing field of solid-state nuclear magnetic resonance spectroscopy The reader will find: * Basic NMR concepts for solids, including guidance on the spin-1/2 nuclei concept * Coverage of the quantum mechanics aspects of solid state NMR and an introduction to the concept of quadrupolar nuclei * An understanding relaxation, exchange and quantitation in NMR * An analysis and interpretation of NMR data, with e...

Photoemission from solids: the transition from solid-state to atomic physics

International Nuclear Information System (INIS)

Shirley, D.A.

1980-08-01

As the photon energy is increased, photoemission from solids undergoes a slow transition from solid-state to atomic behavior. However, throughout the energy range hν = 10 to 1000 eV or higher both types of phenomena are present. Thus angle-resolved photoemission can only be understood quantitatively if each experimenter recognizes the presence of band-structure, photoelectron diffraction, and photoelectron asymmetry effects. The quest for this understanding will build some interesting bridges between solid-state and atomic physics and should also yield important new insights about the phenomena associated with photoemission

Lithium-ion transport in inorganic solid state electrolyte

International Nuclear Information System (INIS)

Gao Jian; Li Hong; Zhao Yu-Sheng; Shi Si-Qi

2016-01-01

An overview of ion transport in lithium-ion inorganic solid state electrolytes is presented, aimed at exploring and designing better electrolyte materials. Ionic conductivity is one of the most important indices of the performance of inorganic solid state electrolytes. The general definition of solid state electrolytes is presented in terms of their role in a working cell (to convey ions while isolate electrons), and the history of solid electrolyte development is briefly summarized. Ways of using the available theoretical models and experimental methods to characterize lithium-ion transport in solid state electrolytes are systematically introduced. Then the various factors that affect ionic conductivity are itemized, including mainly structural disorder, composite materials and interface effects between a solid electrolyte and an electrode. Finally, strategies for future material systems, for synthesis and characterization methods, and for theory and calculation are proposed, aiming to help accelerate the design and development of new solid electrolytes. (topical review)

Advances in Solid State Physics

CERN Document Server

Haug, Rolf

2008-01-01

The present volume 47 of the Advances in Solid State Physics contains the written version of a large number of the invited talks of the 2007 Spring Meeting of the Arbeitskreis Festkörperphysik which was held in Regensburg, Germany, from March 26 to 30, 2007 in conjunction with the 71st Annual Meeting of the Deutsche Physikalische Gesellschaft.It gives an overview of the present status of solid state physics where low-dimensional systems such as quantum dots and quantum wires are dominating. The importance of magnetic materials is reflected by the large number of contributions in the part dealing with ferromagnetic films and particles. One of the most exciting achievements of the last couple of years is the successful application of electrical contacts to and the investigation of single layers of graphene. This exciting physics is covered in Part IV of this book. Terahertz physics is another rapidly moving field which is presented here by five contributions. Achievements in solid state physics are only rarely...

Atomic layer deposition of lithium phosphates as solid-state electrolytes for all-solid-state microbatteries

International Nuclear Information System (INIS)

Wang, Biqiong; Liu, Jian; Sun, Qian; Li, Ruying; Sun, Xueliang; Sham, Tsun-Kong

2014-01-01

Atomic layer deposition (ALD) has been shown as a powerful technique to build three-dimensional (3D) all-solid-state microbattery, because of its unique advantages in fabricating uniform and pinhole-free thin films in 3D structures. The development of solid-state electrolyte by ALD is a crucial step to achieve the fabrication of 3D all-solid-state microbattery by ALD. In this work, lithium phosphate solid-state electrolytes were grown by ALD at four different temperatures (250, 275, 300, and 325 °C) using two precursors (lithium tert-butoxide and trimethylphosphate). A linear dependence of film thickness on ALD cycle number was observed and uniform growth was achieved at all four temperatures. The growth rate was 0.57, 0.66, 0.69, and 0.72 Å/cycle at deposition temperatures of 250, 275, 300, and 325 °C, respectively. Furthermore, x-ray photoelectron spectroscopy confirmed the compositions and chemical structures of lithium phosphates deposited by ALD. Moreover, the lithium phosphate thin films deposited at 300 °C presented the highest ionic conductivity of 1.73 × 10 −8 S cm −1 at 323 K with ∼0.51 eV activation energy based on the electrochemical impedance spectroscopy. The ionic conductivity was calculated to be 3.3 × 10 −8 S cm −1 at 26 °C (299 K). (paper)

Solid-state membrane module

Science.gov (United States)

Gordon, John Howard [Salt Lake City, UT; Taylor, Dale M [Murray, UT

2011-06-07

Solid-state membrane modules comprising at least one membrane unit, where the membrane unit has a dense mixed conducting oxide layer, and at least one conduit or manifold wherein the conduit or manifold comprises a dense layer and at least one of a porous layer and a slotted layer contiguous with the dense layer. The solid-state membrane modules may be used to carry out a variety of processes including the separating of any ionizable component from a feedstream wherein such ionizable component is capable of being transported through a dense mixed conducting oxide layer of the membrane units making up the membrane modules. For ease of construction, the membrane units may be planar.

Determination Of Uranium Concentration In Teeth Female Samples Using Fission Tracks In CR-39 From Different Countries

International Nuclear Information System (INIS)

Hummadi, S.S

2010-01-01

The present study was under taken to measure the uranium concentration in female teeth samples collected from different nationalities.The determination of uranium concentration in these samples has been done by using CR-39 track detector.The nuclear reaction is used as a source of nuclear fission fragments is (n, f) obtained by the bombardment of U-235 with thermal neutrons with flux (5*10 3 n/cm 2 .s) was used from (Am-Be) neutron source.The obtained results show the concentration is ranging from (0.58±0.7ppm) in Oman and Uae to (0.35±0.03ppm)in Iraqi for male, the uranium concentration was the highest in Oman and Uae for female

Oriented solid-state NMR spectrosocpy

DEFF Research Database (Denmark)

Bertelsen, Kresten

This thesis is concerned with driving forward oriented solid-state NMR spectroscopy as a viable technique for studying peptides in membrane bilayers. I will show that structural heterogeneity is an intrinsic part of the peptide/lipid system and that NMR can be used to characterize static...... and dynamic structural features of the peptides and its local surroundings. In fact one need to take into account the dynamical features of the system in order to correctly predict the structure from oriented solid-state NMR spectra.      ...

Solid State Lighting Reliability Components to Systems

CERN Document Server

Fan, XJ

2013-01-01

Solid State Lighting Reliability: Components to Systems begins with an explanation of the major benefits of solid state lighting (SSL) when compared to conventional lighting systems including but not limited to long useful lifetimes of 50,000 (or more) hours and high efficacy. When designing effective devices that take advantage of SSL capabilities the reliability of internal components (optics, drive electronics, controls, thermal design) take on critical importance. As such a detailed discussion of reliability from performance at the device level to sub components is included as well as the integrated systems of SSL modules, lamps and luminaires including various failure modes, reliability testing and reliability performance. This book also: Covers the essential reliability theories and practices for current and future development of Solid State Lighting components and systems Provides a systematic overview for not only the state-of-the-art, but also future roadmap and perspectives of Solid State Lighting r...

Solid state multinuclear NMR. A versatile tool for studying the reactivity of solid systems

Energy Technology Data Exchange (ETDEWEB)

MacKenzie, Kenneth J.D. [MacDiarmid Institute for Advanced Materials and Nanotechnology, Victoria University of Wellington, P.O. Box 600, Wellington (New Zealand)

2004-08-31

Traditionally, X-ray powder diffraction has been a favoured method for studying chemical reactions in the solid state, but the increasing importance of energy-efficient synthesis methods for solids (e.g. sol-gel synthesis, mechanochemical synthesis) has led to the need for an analytical method not dependent on long-range structural periodicity. Multinuclear solid state nuclear magnetic resonance (NMR) represents a technique which is equally applicable to amorphous or crystalline solids, and is now used in increasing numbers of solid state studies.This paper briefly outlines the principles and practical details of this powerful technique and gives examples of its use in solid-state chemistry, particularly in very recent studies of mechanochemical synthesis of advanced sialon ceramics. The temperature at which these technically important silicon aluminium oxynitride compounds are formed can be significantly lowered by high-energy grinding of their components to produce X-ray amorphous precursors. Solid-state NMR has been used to provide detailed information which could not have been obtained by any other means about the chemical environment of the Si and Al atoms in these amorphous precursors, and the various atomic movements undergone as they crystallise to the final product.

Utilization of modified corn silk as a biosorbent for solid-phase extraction of Cr(III) and chromium speciation.

Science.gov (United States)

Yu, Hongmei; Pang, Jing; Wu, Mei; Wu, Qiaoli; Huo, Cuixiu

2014-01-01

The ues of corn silk modified with diluted nitric acid (HNO3-MCS) as a novel biosorbent has been established for solid-phase extraction of Cr(III) and chromium speciation in water samples. The functional groups of the HNO3-MCS surface are favorable for the adsorption of Cr(III). Effective extraction conditions were optimized in both batch and column methods. At pH 3.0 - 6.0, a discrimination of Cr(III) and Cr(VI) is achieved on the HNO3-MCS surface. Cr(III) ions are retained onto the HNO3-MCS surface, however, the adsorption of Cr(VI) is negligible under the same conditions. The adsorption isotherm of HNO3-MCS for Cr(III) has been demonstrated in accordance with a linear form of the Langmuir equation, and the maximum adsorption capacity is 35.21 mg g(-1). The well fitted linear regression of the pseudo-second order model showed the indication of a chemisorption mechanism for the entire concentration range. Thermodynamic studies have shown that the adsorption process is spontaneous and endothermic. The adsorbed Cr(III) was quantitatively eluted by a nitric acid solution with detection by flame atomic absorption spectrometry (FAAS). With a sample volume of 30 mL, a detection limit (3σ) of 0.85 μg L(-1) and a precision of 2.0% RSD at the 40 μg L(-1) level were achieved. The concentration of Cr(III) could be accurately quantified within a linear range of 3 - 200 μg L(-1). After Cr(VI) has been reduced to Cr(III) with hydroxylamine hydrochloride, the total amount of chromium was obtained, and the content of Cr(VI) was given by subtraction. The procedure was validated by analyzing chromium in a certified reference material (GBW (E) 080039). It was also successfully applied for the speciation of chromium in wastewater samples.

The charge transfer induced by Cr doping in MgB2

International Nuclear Information System (INIS)

Zhang Huarong; Zhao Jiyin; Shi Lei

2005-01-01

Mg 1-x Cr x B 2 polycrystal bulk samples with 0 x 5% have been synthesized by a solid-state reaction and studied by X-ray diffraction, SEM and Raman spectrum. It is found that the c-axis of the lattice decreases as the Cr content increases, while the a-axis remains unchanged. Moreover, crystal grain size increases apparently with Cr doping concentration increase. The normal-state resistivity increases and the superconducting transition temperature (T c ) decreases from 38.2 K (x = 0) to 35.1 K (x 0.03) with the increase of Cr content. It is suggested that the charge transfer between the Mg-layer and the B-layer causes the decrease of the charge carrier concentration and induces the changes of T c and normal-state resistivity. On the other hand, by the Raman scattering study, it is found that the linewidth of Raman spectrum increases with the increase of Cr content, which is resulted by the competition between the electron-phonon interaction and substitution-induced disorder. The Raman peak has no evident shift due to the countervailing between the effects of the electron-phonon coupling and the grain size

Solid state ionics: a Japan perspective

Science.gov (United States)

Yamamoto, Osamu

2017-12-01

The 70-year history of scientific endeavor of solid state ionics research in Japan is reviewed to show the contribution of Japanese scientists to the basic science of solid state ionics and its applications. The term 'solid state ionics' was defined by Takehiko Takahashi of Nagoya University, Japan: it refers to ions in solids, especially solids that exhibit high ionic conductivity at a fairly low temperature below their melting points. During the last few decades of exploration, many ion conducting solids have been discovered in Japan such as the copper-ion conductor Rb4Cu16I7Cl13, proton conductor SrCe1-xYxO3, oxide-ion conductor La0.9Sr0.9Ga0.9Mg0.1O3, and lithium-ion conductor Li10GeP2S12. Rb4Cu16I7Cl13 has a conductivity of 0.33 S cm-1 at 25 °C, which is the highest of all room temperature ion conductive solid electrolytes reported to date, and Li10GeP2S12 has a conductivity of 0.012 S cm-1 at 25 °C, which is the highest among lithium-ion conductors reported to date. Research on high-temperature proton conducting ceramics began in Japan. The history, the discovery of novel ionic conductors and the story behind them are summarized along with basic science and technology.

Introduction to solid state electronics

CERN Document Server

Wang, FFY

1989-01-01

This textbook is specifically tailored for undergraduate engineering courses offered in the junior year, providing a thorough understanding of solid state electronics without relying on the prerequisites of quantum mechanics. In contrast to most solid state electronics texts currently available, with their generalized treatments of the same topics, this is the first text to focus exclusively and in meaningful detail on introductory material. The original text has already been in use for 10 years. In this new edition, additional problems have been added at the end of most chapters. These proble

Solid state physics an introduction

CERN Document Server

Hofmann, Philip

2015-01-01

A must-have textbook for any undergraduate studying solid state physics. This successful brief course in solid state physics is now in its second edition. The clear and concise introduction not only describes all the basic phenomena and concepts, but also such advanced issues as magnetism and superconductivity. Each section starts with a gentle introduction, covering basic principles, progressing to a more advanced level in order to present a comprehensive overview of the subject. The book is providing qualitative discussions that help undergraduates understand concepts even if they can?t foll

Ultrasonic methods in solid state physics

CERN Document Server

Truell, John; Elbaum, Charles

1969-01-01

Ultrasonic Methods in Solid State Physics is devoted to studies of energy loss and velocity of ultrasonic waves which have a bearing on present-day problems in solid-state physics. The discussion is particularly concerned with the type of investigation that can be carried out in the megacycle range of frequencies from a few megacycles to kilomegacycles; it deals almost entirely with short-duration pulse methods rather than with standing-wave methods. The book opens with a chapter on a classical treatment of wave propagation in solids. This is followed by separate chapters on methods and techni

The former tests realized to a personal neutron dosemeter based on solid nuclear tracks detector

International Nuclear Information System (INIS)

Camacho, M.E.; Tavera, L.; Balcazar, M.

1997-01-01

Due to the increase in the use of neutron radiation a personal neutron dosemeter based on solid nuclear tracks detector (DSTN) was designed and constructed. The personal dosemeter design consists of three arrangements. The first one consists of a plastic nuclear tracks detector (LR115 or CR39) in contact with a LiF pellet. The second one is the same that above but it placed among two cadmium pellets and, the third one is formed by the alone detector without converter neither neutron absorber. The three arrangements are placed inside a plastic porta detector hermetically closed to avoid the bottom produced by environmental radon whichever both detectors (LR115 and CR39) are sensitive. In this work the former tests realized to that dosemeter are presented. (Author)

Crystal structure, Raman scattering and magnetic properties of CuCr2-xZrxSe4 and CuCr2-xSnxSe4 selenospinels

Science.gov (United States)

Pinto, C.; Galdámez, A.; Barahona, P.; Moris, S.; Peña, O.

2018-06-01

Selenospinels, CuCr2-xMxSe4 (M = Zr and Sn), were synthesized via conventional solid-state reactions. The crystal structure of CuCr1.5Sn0.5Se4, CuCr1.7Sn0.3Se4, CuCr1.5Zr0.5Se4, and CuCr1.8Zr0.2Se4 were determined using single-crystal X-ray diffraction. All the phases crystallized in a cubic spinel-type structure. The chemical compositions of the single-crystals were examined using energy-dispersive X-ray analysis (EDS). Powder X-ray diffraction patterns of CuCr1.3Sn0.7Se4 and CuCr1.7Sn0.3Se4 were consistent with phases belonging to the Fd 3 bar m Space group. An analysis of the vibrational properties on the single-crystals was performed using Raman scattering measurements. The magnetic properties showed a spin glass behavior with increasing Sn content and ferromagnetic order for CuCr1.7Sn0.3Se4.

Evolution of etched nuclear track profiles of alpha particles in CR-39 by atomic force microscopy

International Nuclear Information System (INIS)

Félix-Bautista, R.; Hernández-Hernández, C.; Zendejas-Leal, B.E.; Fragoso, R.; Golzarri, J.I.; Vázquez-López, C.; Espinosa, G.

2013-01-01

A series of atomic force microscopy (AFM) images of etched nuclear tracks has been obtained and used to calculate the nuclear track registration sensitivity parameter V(x) = Vt(x)/Vb. Due to the AFM limitations the samples were irradiated normally to the surface, and with energies attenuated in order to include the Bragg peak region in the AFM piezo-scanner z movement range. The simulation of the track profile evolution was then obtained. The different stages of etched nuclear track profiles were rendered. - Highlights: ► Using AFM we reach that Bragg peak region of etched tracks in CR-39. ► The etched track sensitivity V was calculated by data obtained by AFM. ► The evolucion of etched nuclear tracks was simulated by data achieved by AFM

The reactivity of Fe(II) associated with goethite formed during short redox cycles toward Cr(VI) reduction under oxic conditions

Energy Technology Data Exchange (ETDEWEB)

Tomaszewski, Elizabeth J.; Lee, Seungyeol; Rudolph, Jared; Xu, Huifang; Ginder-Vogel, Matthew (UW)

2017-08-01

Chromium (Cr) is a toxic metal that causes a myriad of health problems and enters the environment as a result of anthropogenic activities and/or natural processes. The toxicity and solubility of chromium is linked to its oxidation state; Cr(III) is poorly soluble and relatively nontoxic, while Cr(VI) is soluble and a known carcinogen. Solid Fe(II) in iron-bearing minerals, such as pyrite, magnetite, and green rusts, reduce the oxidation state of chromium, reducing its toxicity and mobility. However, these minerals are not the only potential sources of solid-associated Fe(II) available for Cr(VI) reduction. For example, ferric (Fe(III)) (hydr)oxides, such as goethite or hematite, can have Fe(II) in the solid without phase transformation; however, the reactivity of Fe(II) within Fe(III) (hydr)oxides with contaminants, has not been previously investigated. Here, we cyclically react goethite with dissolved Fe(II) followed by dissolved O2, leading to the formation of reactive Fe(II) associated with goethite. In separate reactors, the reactivity of this Fe(II) is probed under oxic conditions, by exposure to chromate (CrO42 -) after either one, two, three or four redox cycles. Cr is not present during redox cycling; rather, it is introduced to a subset of the solid after each oxidation half-cycle. Analysis of X-ray absorption near edge structure (XANES) spectra reveals that the extent of Cr(VI) reduction to Cr(III) depends not only on solid Fe(II) content but also surface area and mean size of ordered crystalline domains, determined by BET surface area analysis and X-ray diffraction (XRD), respectively. Shell-by-shell fitting of the extended X-ray absorption fine structure (EXAFS) spectra demonstrates chromium forms both single and double corner sharing complexes on the surface of goethite, in addition to sorbed Cr(III) species. Finally, transmission electron microscope (TEM) imaging and X-ray energy-dispersive spectroscopy (EDS) illustrate that Cr preferentially

X-ray study of rapidly cooled ribbons of Al-Cr-Zr and Al-Ni-Y-Cr-Zr alloys

International Nuclear Information System (INIS)

Betsofen, S.Ya.; Osintsev, O.E.; Lutsenko, A.N.; Konkevich, V.Yu.

2002-01-01

One investigated into phase composition, lattice spacing and structure of rapidly cooled 25-200 μm gauge strips made of Al-4,1Cr-3,2Zr and Al-1,5Cr-1,5Zr-4Ni-3Y alloys, wt. %, produced by melt spinning to a water-cooled copper disk. In Al-4,1Cr-3,2Zr alloy one detected intermetallic phases: Al 3 Zr and two Al 86 Cr 14 composition icosahedral phases apart from aluminium solid solution with 4.040-4.043 A lattice spacing. In Al-1,5Cr-1,5Zr-4Ni-3Y alloy one identified two Al 86 Cr 14 icosahedral phases and two AlNiY and Al 3 Y yttrium-containing ones, lattice spacing of aluminium solid solution was equal to 4.052-4.053 A [ru

Phase stability and elastic properties of Cr-V alloys

Science.gov (United States)

Gao, M. C.; Suzuki, Y.; Schweiger, H.; Doǧan, Ö. N.; Hawk, J.; Widom, M.

2013-02-01

V is the only element in the periodic table that forms a complete solid solution with Cr and thus is particularly important in alloying strategy to ductilize Cr. This study combines first-principles density functional theory calculations and experiments to investigate the phase stability and elastic properties of Cr-V binary alloys. The cluster expansion study reveals the formation of various ordered compounds at low temperatures that were not previously known. These compounds become unstable due to the configurational entropy of bcc solid solution as the temperature is increased. The elastic constants of ordered and disordered compounds are calculated at both T = 0 K and finite temperatures. The overall trends in elastic properties are in agreement with measurements using the resonant ultrasound spectroscopy method. The calculations predict that addition of V to Cr decreases both the bulk modulus and the shear modulus, and enhances the Poisson’s ratio, in agreement with experiments. Decrease in the bulk modulus is correlated to decrease in the valence electron density and increase in the lattice constant. An enhanced Poisson’s ratio for bcc Cr-V alloys (compared to pure Cr) is associated with an increased density of states at the Fermi level. Furthermore, the difference charge density in the bonding region in the (110) slip plane is highest for pure Cr and decreases gradually as V is added. The present calculation also predicts a negative Cauchy pressure for pure Cr, and it becomes positive upon alloying with V. The intrinsic ductilizing effect from V may contribute, at least partially, to the experimentally observed ductilizing phenomenon in the literature.

Silicon solid state devices and radiation detection

CERN Document Server

Leroy, Claude

2012-01-01

This book addresses the fundamental principles of interaction between radiation and matter, the principles of working and the operation of particle detectors based on silicon solid state devices. It covers a broad scope with respect to the fields of application of radiation detectors based on silicon solid state devices from low to high energy physics experiments including in outer space and in the medical environment. This book covers stateof- the-art detection techniques in the use of radiation detectors based on silicon solid state devices and their readout electronics, including the latest developments on pixelated silicon radiation detector and their application.

Determination of uranium and thorium contents inside different materials using track detectors and mean critical angles

CERN Document Server

Misdaq, M A; Ktata, A; Merzouki, A; Youbi, N

1999-01-01

The critical angles of the CR-39 (theta sub c) and LR-115 type II (theta sub c ') solid state nuclear track detectors (SSNTD) for detecting alpha-particles emitted by the uranium and thorium series have been evaluated by calculating the corresponding ranges of the emitted alpha-particles in different material samples and in the SSNTD studied. The influence of the emitted alpha-particles initial and residual energies on the critical angles of the SSNTD studied has been investigated. The uranium and thorium contents of different geological samples have been evaluated by exploiting data obtained for the critical angles of the CR-39 and LR-115 type II solid state nuclear track detectors and measuring the corresponding densities of tracks.

Protein enrichment, cellulase production and in vitro digestion improvement of pangolagrass with solid state fermentation.

Science.gov (United States)

Hu, Chan-Chin; Liu, Li-Yun; Yang, Shang-Shyng

2012-02-01

Pangolagrass, Digitaria decumbens Stent, is a major grass for cow feeding, and may be a good substrate for protein enrichment. To improve the quality of pangolagrass for animal feeding, cellulolytic microbes were isolated from various sources and cultivated with solid state fermentation to enhance the protein content, cellulase production and in vitro digestion. The microbes, culture conditions and culture media were studied. Cellulolytic microbes were isolated from pangolagrass and its extracts, and composts. Pangolagrass supplemented with nitrogen and minerals was used to cultivate the cellulolytic microbes with solid state fermentation. The optimal conditions for protein enrichment and cellulase activity were pangolagrass substrate at initial moisture 65-70%, initial pH 6.0-8.0, supplementation with 2.5% (NH(4))(2)SO(4), 2.5% KH(2)PO(4) and K(2)HPO(4) mixture (2:1, w/w) and 0.3% MgSO(4).7H(2)O and cultivated at 30(o)C for 6 days. The protein content of fermented pangolagrass increased from 5.97-6.28% to 7.09-16.96% and the in vitro digestion improved from 4.11-4.38% to 6.08-19.89% with the inoculation of cellulolytic microbes by solid state fermentation. Each 1 g of dried substrate yielded Avicelase 0.93-3.76 U, carboxymethylcellulase 1.39-4.98 U and β-glucosidase 1.20-6.01 U. The isolate Myceliophthora lutea CL3 was the strain found to be the best at improving the quality of pangolagrass for animal feeding with solid state fermentation. Solid state fermentation of pangolagrass inoculated with appropriate microbes is a feasible process to enrich protein content, increase in vitro digestibility and improve the quality for animal feeding. Copyright © 2011. Published by Elsevier B.V.

Solid state laser technology - A NASA perspective

Science.gov (United States)

Allario, F.

1985-01-01

NASA's program for developing solid-state laser technology and applying it to the Space Shuttle and Space Platform is discussed. Solid-state lasers are required to fulfill the Earth Observation System's requirements. The role of the Office of Aeronautics and Space Technology in developing a NASA tunable solid-state laser program is described. The major goals of the program involve developing a solid-state pump laser in the green, using AlGaAs array technology, pumping a Nd:YAG/SLAB crystal or glass, and fabricating a lidar system, with either a CO2 laser at 10.6 microns or a Nd:YAG laser at 1.06 microns, to measure tropospheric winds to an accuracy of + or - 1 m/s and a vertical resolution of 1 km. The procedures to be followed in order to visualize this technology plan include: (1) material development and characterization, (2) laser development, and (3) implementation of the lasers.

A comparison of the neutron response of CR-39 made by different manufacturers

International Nuclear Information System (INIS)

Ipe, N.E.; Liu, J.C.; Buddemeier, B.R.; Miles, C.J.; Yoder, R.C.

1991-09-01

CR-39 was obtained from American Acrylics and Plastics, Inc. (A.A), N. E. Technology, Ltd. (N.E), and Tech/Ops Landauer, Inc. (LT). The dosemeters were exposed to radioisotopic neutron sources at SLAC, and moderated 252 Cf at ORNL. The A.A. and N.E. dosemeters were electrochemically etched (pre-etch in 6.5 N KOH at 60 degrees C for 1 hour and 45 minutes, a 5 hour etch at 3000 V and 60 Hz, a 23 minute blow-up step at 2 kHz and a post-etch for 15 minutes). Track densities were determined with the Homann Track Size Image Analyzer. The LT dosemeters were chemically etched in 5.5 N NaOH at 70 degrees C for 15.5 hours. Some A.A., N.E., and LT dosemeters were etched in 6.25 N NaOH at 70 degrees C for 6 hours. A pre-etch step in 60% methanol and 40% NaOH at 70 degrees C for 1 hour was added for some N.E. dosemeters. The results of these studies are reported in this paper. 3 refs., 2 figs., 2 tabs

Solid state track detectors

International Nuclear Information System (INIS)

Reuther, H.

1976-11-01

This paper gives a survey of the present state of the development and the application of solid state track detectors. The fundamentals of the physical and chemical processes of the track formation and development are explained, the different detector materials and their registration characteristics are mentioned, the possibilities of the experimental practice and the most variable applications are discussed. (author)

Study of nuclear tracks on different polycarbonate foils and their feasibility for use in personnel monitoring

International Nuclear Information System (INIS)

Jayalakshmi, V.; Rohatgi, Rupali; Sathian, Deepa; Marathe, P.K.; Nair, Sarala; Chourasiya, G.; Kannan, S.

2009-01-01

CR-39 (PDAC) a solid state nuclear track detector, is used as a routine personnel monitor. 1800 workers are being monitored quarterly for fast neutron using CR-39 foils. These foils procured from Pershore Mouldings, UK are very expensive and indigenous development will make the foils cost effective. The aim of this paper is to find a suitable alternative to the imported CR-39 foils for use in personnel monitoring. The foils from three different manufacturers have been compared with CR-39 foils from Pershore Moulding, UK, presently in use. Out of the three, only sample no 1 is promising. It has a background and sensitivity comparable with CR-39 presently used. The sample 2 is CR-39 being developed in India, has a relatively high background and poor sensitivity. Efforts are being made to improve the quality of this sample. The sample 3 was a poly carbonate from local manufacturer which produced very few tracks and the standard deviation of track counts was very large and hence not useful for personnel monitoring. (author)

Monolithic solid-state lasers for spaceflight

Science.gov (United States)

Krainak, Michael A.; Yu, Anthony W.; Stephen, Mark A.; Merritt, Scott; Glebov, Leonid; Glebova, Larissa; Ryasnyanskiy, Aleksandr; Smirnov, Vadim; Mu, Xiaodong; Meissner, Stephanie; Meissner, Helmuth

2015-02-01

A new solution for building high power, solid state lasers for space flight is to fabricate the whole laser resonator in a single (monolithic) structure or alternatively to build a contiguous diffusion bonded or welded structure. Monolithic lasers provide numerous advantages for space flight solid-state lasers by minimizing misalignment concerns. The closed cavity is immune to contamination. The number of components is minimized thus increasing reliability. Bragg mirrors serve as the high reflector and output coupler thus minimizing optical coatings and coating damage. The Bragg mirrors also provide spectral and spatial mode selection for high fidelity. The monolithic structure allows short cavities resulting in short pulses. Passive saturable absorber Q-switches provide a soft aperture for spatial mode filtering and improved pointing stability. We will review our recent commercial and in-house developments toward fully monolithic solid-state lasers.

Chromium sorption and Cr(VI) reduction to Cr(III) by grape stalks and yohimbe bark.

Science.gov (United States)

Fiol, Núria; Escudero, Carlos; Villaescusa, Isabel

2008-07-01

In this work, two low cost sorbents, grape stalks and yohimbe bark wastes were used to remove Cr(VI) and Cr(III) from aqueous solutions. Batch experiments were designed to obtain Cr(VI) and Cr(III) sorption data. The mechanism of Cr(III) and Cr(VI) removal and Cr(VI) reduction to Cr(III) by the two vegetable wastes, has been investigated. Fourier transform infrared rays (FTIR) and X-ray photoelectron spectroscopy (XPS) analysis on solid phase were performed to determine the main functional groups that might be involved in metal uptake and to confirm the presence of Cr(III) on the sorbent, respectively. Results put into evidence that both sorbents are able to reduce Cr(VI) to its trivalent form.

Phase transformations in a Cu−Cr alloy induced by high pressure torsion

International Nuclear Information System (INIS)

Korneva, Anna; Straumal, Boris; Kilmametov, Askar; Chulist, Robert; Straumal, Piotr; Zięba, Paweł

2016-01-01

Phase transformations induced by high pressure torsion (HPT) at room temperature in two samples of the Cu-0.86 at.% Cr alloy, pre-annealed at 550 °C and 1000 °C, were studied in order to obtain two different initial states for the HPT procedure. Observation of microstructure of the samples before HPT revealed that the sample annealed at 550 °C contained two types of Cr precipitates in the Cu matrix: large particles (size about 500 nm) and small ones (size about 70 nm). The sample annealed at 1000 °C showed only a little fraction of Cr precipitates (size about 2 μm). The subsequent HPT process resulted in the partial dissolution of Cr precipitates in the first sample and dissolution of Cr precipitates with simultaneous decomposition of the supersaturated solid solution in another. However, the resulting microstructure of the samples after HPT was very similar from the standpoint of grain size, phase composition, texture analysis and hardness measurements. - Highlights: • Cu−Cr alloy with two different initial states was deformed by HPT. • Phase transformations in the deformed materials were studied. • SEM, TEM and X-ray diffraction techniques were used for microstructure analysis. • HPT leads to formation the same microstructure independent of the initial state.

Optimization of microwave-induced chemical etching for rapid development of neutron-induced recoil tracks in CR-39 detectors

International Nuclear Information System (INIS)

Sahoo, G.S.; Tripathy, S.P.; Bandyopadhyay, T.

2014-01-01

A systematic investigation is carried out to optimize the recently established microwave-induced chemical etching (MICE) parameters for rapid development of neutron-induced recoil tracks in CR-39 detectors. Several combinations of all available microwave powers with different etching durations were analysed to determine the most suitable etching condition. The etching duration was found to reduce with increasing microwave power and the tracks were observed at about 18, 15, 12, and 6 min for 300, 450, 600 and 900 W of microwave powers respectively compared to a few hours in chemical etching (CE) method. However, for complete development of tracks the etching duration of 30, 40, 50 and 60 min were found to be suitable for the microwave powers of 900, 600, 450 and 300 W, respectively. Temperature profiles of the etchant for all the available microwave powers at different etching durations were generated to regulate the etching process in a controlled manner. The bulk etch rates at different microwave powers were determined by 2 methods, viz., gravimetric and removed thickness methods. A logarithmic expression was used to fit the variation of bulk etch rate with microwave power. Neutron detection efficiencies were obtained for all the cases and the results on track parameters obtained with MICE technique were compared with those obtained from another detector processed with chemical etching. - Highlights: • Microwave-induced chemical etching method is optimized for rapid development of recoil tracks due to neutrons in CR-39 detector. • Several combinations of microwave powers and etching durations are investigated to standardize the suitable etching condition. • Bulk-etch rates are determined for all microwave powers by two different methods, viz. gravimetric and removed thickness method. • The method is found to be simple, effective and much faster compared to conventional chemical etching

Solid state physics

CERN Document Server

Grosso, Giuseppe

2013-01-01

Solid State Physics is a textbook for students of physics, material science, chemistry, and engineering. It is the state-of-the-art presentation of the theoretical foundations and application of the quantum structure of matter and materials. This second edition provides timely coverage of the most important scientific breakthroughs of the last decade (especially in low-dimensional systems and quantum transport). It helps build readers' understanding of the newest advances in condensed matter physics with rigorous yet clear mathematics. Examples are an integral part of the text, carefully de

Studies of isothermal annealing of fission fragment and alpha particle tracks in Cr-39 polymer detectors

International Nuclear Information System (INIS)

Zaky, M.F.; Youssef, A.A.

2002-01-01

Two groups of CR-39 detectors samples are exposed to two types of charged particle radiation. The first group are severe damaged with fission fragment tracks from 2 52C f source. The second accepted alpha particles resulting from the interaction of highly energetic 1 9F -ions and a copper disk with thickness 1 cm, which are of less damage tracks than fission fragments. , The isothermal annealing of tracks in the temperature range from 175 to 300 degree C in step 25 degree C for annealing time of 10,15,20,25 and 30 minutes has been investigated. The changes introduced in the track density and track diameter for two types of irradiation in the detector have been observed and compared between them. The results indicate that the track density and the size of the tracks are considerably changed due to annealing

Synthesis, macroscopic and local probe characterization of AgCrO$_2$ and CdCr$_2$S$_4$

CERN Document Server

Oliveira, Gonçalo; Araujo, J P

The search of new materials with new and/or enhanced physical properties has, nowadays, a strict relation with the evolution of technology. The hunt for systems exhibiting simultaneous (anti)ferroelectric and (anti)ferromagnetic orders has re-started in the last years, and remains as one of the hot topics for Physic, Chemistry and Materials Science scientific communities. This is triggered by the possibility to apply these materials into, ${e.g.}$, new multiferroic memories that could be written electrically and read magnetically (or vice-versa). This thesis presents an experimental study on two of these so-called multiferroic materials, the AgCrO$_2$ delafossite and CdCr$_2$S$_4$ spinel type compounds. Different methods have been tested for the synthesis of delafossite silver chromium oxide AgCrO$_2$ namely, solid state reaction (ssr) and sol-gel combustion. The processes were optimized regarding complexing/combusting agents, temperature and duration of the heat treatments, as well as the processing atmosphe...

SOLID-STATE STORAGE DEVICE FLASH TRANSLATION LAYER

DEFF Research Database (Denmark)

2017-01-01

Embodiments of the present invention include a method for storing a data page d on a solid-state storage device, wherein the solid-state storage device is configured to maintain a mapping table in a Log-Structure Merge (LSM) tree having a C0 component which is a random access memory (RAM) device...

Evaluation of radon concentration in dwellings and well water of Parana State-Brazil

International Nuclear Information System (INIS)

Correa, Janine Nicolosi

2011-01-01

Considering the growing interest of International Agencies and national Governmental organs in studies and measurements of radon activity in air, soil gas and ground water (mainly from artesian wells) as well as scarceness of such measurements at Brazilian territory, present studies were initiated by the Laboratory of Applied Nuclear Physics of Federal University of Technology - Parana (UTFPR) in collaboration with the Institute of Radiation Protection and Dosimetry (IRD) and the Center of Nuclear Technology Development (CDTN) of Brazilian Commission on Nuclear Energy (CNEN). This Collaboration started in 2003. Radon monitoring program is based mainly on use of Solid State Nuclear Track Detectors for radon activity measurements in air. Continuous electronic radon detectors are used for radon measurements in soil gas and water. Current work presents the results of indoor 222 Rn activity of dwellings and working places of Curitiba-PR and radon concentration in ground water samples from artesian wells from aquifers of the same area. The indoor measurements of radon activity were performed using Solid State Nuclear Track Detectors CR-39. After the exposition, CR-39 detectors were submitted to chemical development which permitted to make alpha particle tracks counting. The results of calibration of CR-39 together with efficiency of used exhalation chambers as well as alpha particle tracks chemical development procedure were performed in cooperation with CDTN and collaboration with the National Institute of Radiological Sciences (NIRS). The major part of indoor 222 Rn concentration in residences was found below 100 Bq/m3. In the case of working places, all measurements present 222 Rn concentration bellow 100 Bq/m3. The studies of radon activity in water were performed using the samples of water from artesian wells submitted to recursive measurements by instant radon detector AlphaGUARD PQ2000 PRO during few weeks with intervals of about 4 days between each measurement

optimisation of solid optimisation of solid state fermentation

African Journals Online (AJOL)

eobe

from banana peels via solid state fermentation using Aspergillus niger. ermentation ... [7,8], apple pomace [9], banana peels [4], date palm. [10], carob ... powder, jams, juice, bar, biscuits, wine etc results in ... Yeast extract was taken as nitrogen.

Studies on neutron detection with solid state nuclear track detectors

International Nuclear Information System (INIS)

Khouri, M.C.; Vilela, E.C.; Andrade, C. de.

1993-03-01

The detection of thermal and fast neutrons was studied. For thermal neutrons, alpha sensitive plastic was used in order to register the products of nuclear reactions taking place in boron and /or lithium converters. Fast neutrons produce recoil tracks within the detector. In the present case, CR-39 and Makrofol E were used. Chemical and electrochemical etching processes were used for thermal and fast neutron detectors, respectively. (F.E.). 6 refs, 4 figs, 6 tabs

Solid state electrolytes for all-solid-state 3D lithium-ion batteries

NARCIS (Netherlands)

Kokal, I.

2012-01-01

The focus of this Ph.D. thesis is to understand the lithium ion motion and to enhance the Li-ionic conductivities in commonly known solid state lithium ion conductors by changing the structural properties and preparation methods. In addition, the feasibility for practical utilization of several

Synthesis and characterization of Ge–Cr-based intermetallic compounds: GeCr3, GeCCr3, and GeNCr3

International Nuclear Information System (INIS)

Lin, S.; Tong, P.; Wang, B.S.; Huang, Y.N.; Song, W.H.; Sun, Y.P.

2014-01-01

Highlights: • Polycrystalline samples of GeCr 3 , GeCCr 3 , and GeNCr 3 are synthesized by using solid state reaction method. • A good quality of our samples is verified by the Rietveld refinement and electrical transport measurement. • We present a comprehensive understanding of physical properties of GeCr 3 , GeCCr 3 , and GeNCr 3 . -- Abstract: We report the synthesis of GeCr 3 , GeCCr 3 , and GeNCr 3 polycrystalline compounds, and present a systematic study of this series by the measurements of X-ray diffraction (XRD), magnetism, electrical/thermal transport, specific heat, and Hall coefficient. Good quality of our samples is verified by quite small value of residual resistivity and considerably large residual resistivity ratio. Based on the Rietveld refinement of XRD data, the crystallographic parameters are obtained, and, correspondingly, the sketches of crystal structure are plotted for all the samples. The ground states of GeCr 3 , GeCCr 3 , and GeNCr 3 are paramagnetic/antiferromagnetic metal, and even a Fermi-liquid behavior is observed in electrical transport at low temperatures. Furthermore, the analysis of the thermal conductivity data suggests the electron thermal conductivity plays a major role in total thermal conductivity for GeCr 3 at low temperatures, while the phonon thermal conductivity is dominant for GeCCr 3 and GeNCr 3 at high temperatures. The negative value of Seebeck coefficient and Hall coefficient indicate that the charge carriers are electron-type for GeCr 3 , GeCCr 3 , and GeNCr 3

A method for in situ absolute DD yield calibration of neutron time-of-flight detectors on OMEGA using CR-39-based proton detectors

Energy Technology Data Exchange (ETDEWEB)

Waugh, C. J., E-mail: cjwaugh@mit.edu; Zylstra, A. B.; Frenje, J. A.; Séguin, F. H.; Petrasso, R. D. [Plasma Science and Fusion Center, MIT, Cambridge, Massachusetts 02139 (United States); Rosenberg, M. J.; Glebov, V. Yu.; Sangster, T. C.; Stoeckl, C. [Laboratory for Laser Energetics, Rochester, New York 14623 (United States)

2015-05-15

Neutron time of flight (nTOF) detectors are used routinely to measure the absolute DD neutron yield at OMEGA. To check the DD yield calibration of these detectors, originally calibrated using indium activation systems, which in turn were cross-calibrated to NOVA nTOF detectors in the early 1990s, a direct in situ calibration method using CR-39 range filter proton detectors has been successfully developed. By measuring DD neutron and proton yields from a series of exploding pusher implosions at OMEGA, a yield calibration coefficient of 1.09 ± 0.02 (relative to the previous coefficient) was determined for the 3m nTOF detector. In addition, comparison of these and other shots indicates that significant reduction in charged particle flux anisotropies is achieved when bang time occurs significantly (on the order of 500 ps) after the trailing edge of the laser pulse. This is an important observation as the main source of the yield calibration error is due to particle anisotropies caused by field effects. The results indicate that the CR-39-nTOF in situ calibration method can serve as a valuable technique for calibrating and reducing the uncertainty in the DD absolute yield calibration of nTOF detector systems on OMEGA, the National Ignition Facility, and laser megajoule.

A method for in situ absolute DD yield calibration of neutron time-of-flight detectors on OMEGA using CR-39-based proton detectors.

Science.gov (United States)

Waugh, C J; Rosenberg, M J; Zylstra, A B; Frenje, J A; Séguin, F H; Petrasso, R D; Glebov, V Yu; Sangster, T C; Stoeckl, C

2015-05-01

Neutron time of flight (nTOF) detectors are used routinely to measure the absolute DD neutron yield at OMEGA. To check the DD yield calibration of these detectors, originally calibrated using indium activation systems, which in turn were cross-calibrated to NOVA nTOF detectors in the early 1990s, a direct in situ calibration method using CR-39 range filter proton detectors has been successfully developed. By measuring DD neutron and proton yields from a series of exploding pusher implosions at OMEGA, a yield calibration coefficient of 1.09 ± 0.02 (relative to the previous coefficient) was determined for the 3m nTOF detector. In addition, comparison of these and other shots indicates that significant reduction in charged particle flux anisotropies is achieved when bang time occurs significantly (on the order of 500 ps) after the trailing edge of the laser pulse. This is an important observation as the main source of the yield calibration error is due to particle anisotropies caused by field effects. The results indicate that the CR-39-nTOF in situ calibration method can serve as a valuable technique for calibrating and reducing the uncertainty in the DD absolute yield calibration of nTOF detector systems on OMEGA, the National Ignition Facility, and laser megajoule.

A method for in situ absolute DD yield calibration of neutron time-of-flight detectors on OMEGA using CR-39-based proton detectors

International Nuclear Information System (INIS)

Waugh, C. J.; Zylstra, A. B.; Frenje, J. A.; Séguin, F. H.; Petrasso, R. D.; Rosenberg, M. J.; Glebov, V. Yu.; Sangster, T. C.; Stoeckl, C.

2015-01-01

Neutron time of flight (nTOF) detectors are used routinely to measure the absolute DD neutron yield at OMEGA. To check the DD yield calibration of these detectors, originally calibrated using indium activation systems, which in turn were cross-calibrated to NOVA nTOF detectors in the early 1990s, a direct in situ calibration method using CR-39 range filter proton detectors has been successfully developed. By measuring DD neutron and proton yields from a series of exploding pusher implosions at OMEGA, a yield calibration coefficient of 1.09 ± 0.02 (relative to the previous coefficient) was determined for the 3m nTOF detector. In addition, comparison of these and other shots indicates that significant reduction in charged particle flux anisotropies is achieved when bang time occurs significantly (on the order of 500 ps) after the trailing edge of the laser pulse. This is an important observation as the main source of the yield calibration error is due to particle anisotropies caused by field effects. The results indicate that the CR-39-nTOF in situ calibration method can serve as a valuable technique for calibrating and reducing the uncertainty in the DD absolute yield calibration of nTOF detector systems on OMEGA, the National Ignition Facility, and laser megajoule

Track detection on the cells exposed to high Linear Energy Transfer heavy-ions by Cr-39 plastic and terminal deoxynucleotidyl transferase(Td T)

International Nuclear Information System (INIS)

Mehnati, P.; Keshtkar, A.; Mesbahi, A.; Sasaki, H.

2006-01-01

The fatal effect of ionizing radiation on cells depends on Linear Energy Transfer level. The distribution of ionizing radiation is sparse and homogeneous for low Linear Energy Transfer radiations such as X or y, but it is dense and concentrated for high Linear Energy Transfer radiation such as heavy-ions radiation. Materials and Methods: Chinese hamster ovary cells (CHO-K1) were exposed to 4 Gy Fe-ion 2000 keV/μm. The Cr-39 is a special and sensitive plastic used to verify exact position of heavy-ions traversal. Terminal deoxynucleotidyl transferase is an enzyme labeled with [3 H ] d ATP for detection of cellular DNA damage by autoradiography assay. Results: The track of heavy ions traversals presented by pit size was almost similar for all different doses of radiation. No pits to show the track of traversal were found in 20% of the cell nuclei of the irradiation. Apparently these fractions of cells wave not hit by heavy ions. Conclusion: This study indicated the possible usefulness of both the Cr-39 plastics and DNA labeling with Terminal deoxynucleotidyl transferase method for evaluating the biological effect of heavy-ions in comparison with low Linear Energy Transfer ionizing radiation

Polarized photon scattering of 52Cr: Determining the parity of dipole states

Science.gov (United States)

Krishichayan, Fnu; Bhike, M.; Tornow, W.

2014-03-01

Observation of dipole states in nuclei are important because they provide information on various collective and single-particle nuclear excitation modes, e.g., pygmy dipole resonance (PDR) and spin-flip M1 resonance. The PDR has been extensively studied in the higher and medium mass region, whereas not much information is available around the low mass (A ~ 50) region where, apparently,the PDR starts to form. The present photoresponse of 52Cr has been investigated to test the evolution of the PDR in a nucleus with a small number of excess neutrons as well as to look for spin-flip M1 resonance excitation mode. Spin-1 states in 52Cr between 5.0 to 9.5 MeV excitation energy were excited by exploiting fully polarized photons using the (γ ,γ') nuclear resonance fluorescence technique, a completely model-independent electromagnetic method. The de-excitation γ-rays were detected using a HPGe array. The experiment was carried out using the HIGS facility at TUNL. Results of unambiguous parity determinations of dipole states in 52Cr will be presented.

Analysis of precipitation in a Cu-Cr-Zr alloy

Institute of Scientific and Technical Information of China (English)

Zhao Mei; Lin Guobiao; Wang Zidong; Zhang Maokui

2008-01-01

Precipites in Cu-0.42%Cr-0.21%Zr alloy were analyzed by using scanning electron microscope (SEM), energy dispersive X-ray spectroscopy (EDXS) and transmission electron microscope (TEM). After the solid solution was performed at 980℃ for 2 h, water-quenched and aged at 450℃ for 20 h, the precipite had a bimodal distribution of precipitate size. The coarse precipitates are pure Cr and Cu5Zr, the dispersed fine precipitate is CrCu2(Zr, Mg) and pure Cr ranging from 1 to 50 nm. The coarse phases formed during solidification and were left undissolved during solid solution. The fine precipitates are the hardening precipitates that form due to decomposition of the supersaturated solid solution during aging.

Passivation-free solid state battery

Science.gov (United States)

Abraham, Kuzhikalail M.; Peramunage, Dharmasena

1998-01-01

This invention pertains to passivation-free solid-state rechargeable batteries composed of Li.sub.4 Ti.sub.5 O.sub.12 anode, a solid polymer electrolyte and a high voltage cathode. The solid polymer electrolyte comprises a polymer host, such as polyacrylonitrile, poly(vinyl chloride), poly(vinyl sulfone), and poly(vinylidene fluoride), plasticized by a solution of a Li salt in an organic solvent. The high voltage cathode includes LiMn.sub.2 O.sub.4, LiCoO.sub.2, LiNiO.sub.2 and LiV.sub.2 O.sub.5 and their derivatives.

The Oxford solid state basics

CERN Document Server

Simon, Steven H

2013-01-01

The study of solids is one of the richest, most exciting, and most successful branches of physics. While the subject of solid state physics is often viewed as dry and tedious this new book presents the topic instead as an exciting exposition of fundamental principles and great intellectual breakthroughs. Beginning with a discussion of how the study of heat capacity of solids ushered in the quantum revolution, the author presents the key ideas of the field while emphasizing the deepunderlying concepts. The book begins with a discussion of the Einstein/Debye model of specific heat, and the Drude

Unusual inhomogeneous microstructures in charge glass state of PbCrO3

Science.gov (United States)

Kurushima, Kosuke; Tsukasaki, Hirofumi; Ogata, Takahiro; Sakai, Yuki; Azuma, Masaki; Ishii, Yui; Mori, Shigeo

2018-05-01

We investigated the microstructures and local structures of perovskite PbCrO3, which shows a metal-to-insulator transition and a 9.8% volume collapse, by electron diffraction, high-resolution transmission electron microscopy (TEM), and high-angle annular dark-field scanning transmission electron microscopy (HAADF-STEM). It is revealed that the charge glass state is characterized by the unique coexistence of the crystalline state with a cubic symmetry on average and the noncrystalline state. HAADF-STEM observation at atomic resolution revealed that Pb ions were displaced from the ideal A site position of the cubic perovskite structure, which gives rise to characteristic diffuse scatterings around the fundamental Bragg reflections. These structural inhomogeneities are crucial to the understanding of the unique physical properties in the charge glass state of PbCrO3.

Chromium Oxidation State in Planetary Basalts: Oxygen Fugacity Indicator and Critical Variable for Cr-Spinel Stability

Science.gov (United States)

Bell, A. S.; Burger, P. V.; Le, Loan; Papike, J. J.; Jone, J.; Shearer, C. K.

2014-01-01

Cr is a ubiquitous and relatively abundant minor element in basaltic, planetary magmas. At the reduced oxidation states (Cr is present in melts as both divalent and trivalent forms. The ratio of trivalent to divalent Cr present in the melt has many consequences for the stability and Cr concentration of magmatic phases such as spinel, clinopyroxene, and olivine. However, understanding the Cr valence in quenched melts has historically been plagued with analytical issues, and only recently has reliable methodology for quantifying Cr valence in quenched melts been developed. Despite this substantial difficulty, the pioneering works of Hanson and Jones and Berry and O'Neill provided important insights into the oxidation state of Cr in in silicate melts. Here we present a series of 1-bar gas mixing experiments performed with a Fe-rich basaltic melt in which have determined the Cr redox ratio of the melt at over a range of fO2 values by measuring this quantity in olivine with X-ray Absorption Near Edge Spectroscopy (XANES). The measured Cr redox ratio of the olivine phenocrysts can be readily converted to the ratio present in the conjugate melt via the ratio of crystal-liquid partition coefficients for Cr3+ and Cr2+. We have applied these results to modeling Cr spinel stability and Cr redox ratios in a primitive, iron-rich martian basalt.